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Home My WebLink AboutMO-28025_47306_CA_UST‐61_20200715 UST-61 24-Hour Release and UST Leak Reporting Form. For Releases in NC This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or suspected release (DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________ Reported by (circle one): Phone, Fax or Report Region _______ Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______ Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________ Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________ Reg/Non-regulated? _____________ INCIDENT DESCRIPTION Incident Name: Address: County: City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS  Topographic map  GIS Address matching  Other  Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release Code) (Check one)  Release Detection Equipment or Methods  During UST Closure/Removal  Property Transfer  Visual/Odor  Water in Tank  Water Supply Well Contamination  Groundwater Contamination  Surface Water Contamination  Other (specify) _______________ SOURCE OF CONTAMINATION Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)  Tank  Piping  Dispenser  Submersible Turbine Pump  Delivery Problem  Spill Bucket  Other  Unknown Definitions presented on reverse  Spill  Overfill  Corrosion  Physical/Mechanical Damage  Install Problem  Other  Unknown Definitions presented on reverse  Petroleum  Non-Petroleum  Both Location (Check one)  Facility  Residence  Other  Gasoline/ Diesel/ Kerosene  Heating Oil  Other Petroleum Products  Metals  Other Inorganics  Other Organics  Diesel/Veg. Oil Blend  Vegetable Oil 100%  E10 – E20  E21 – E84  E85 – E99  Ethanol 100%  E01 – E09 Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 Y YY N COMM Proposed New Pineville Town Hall and Library 505-511 Main Street Mecklenburg Pineville 28134 35.086632 -80.893153 UNKOWN 7/10/20 Due Diligence of the site revealed a former UST site located on the property. The Little General Store with address of 105 Yandle Street. According to database records, the store operated 1-14,000-gallon, 1-6,000-gallon and 1-1,000-gallon USTs. The USTs operated from 1973 to 1991 when records indicate they were removed. No facilty ID could be located. Geotechnical Investigation identfied petro odors. A Phase II ESA consisting of 12 soil samples and 6 groundwater samples was conducted (attached). Groundwater and soil exceedances of NC 2L and MSCC soil-to water were identified. Property is vacant and unused IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________ Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map Person Reporting Incident Company Telephone Number Title Address Date UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined NA - Former Little General Store Little General Store Town of Pineville 200 Dover Street Pineville NC 28134 Patrick Lowery, Snr Env Mngr SUMMIT ELT for Town of Pineville 7/15/20 803-230-5087 3575 Centre Cir Drive, Ft Mill, SC 29715 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 9571.40692463Area of feature in internal units squared: 356.311310411Length of feature in internal units: 758Sites designated as superfund cleanup sites: 491412.9375Y-value coordinate in feet: 1435661.125X-value coordinate in feet: 356.31130981Total perimeter in coverage units: 9571.40625Total area in coverage units: 35 5 7.983647 80 53 11.508125Lat/Long: 046 148 540Superfund ID: FederalSite Type: HSDS: 1720 ft. 1/4-1/2 ESE , NC Region N/A HSDS NC HSDSCENTRAL TRANSPORT COMPANY S102442859 RemovedTank Status: 2Tank Id: UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 4000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: RemovedTank Status: 1Tank Id: -80.89318Longitude: 35.08701Latitude: MecklenburgFIPS County Desc: LANCASTER, SC 29720-1317Contact City/State/Zip: Not reportedContact Address2: PO BOX 1317 /120 S MAIN STContact Address1: SHAUN-SEJ CORP DBA CHEM OILContact: 00-0-0000017182Facility Id: PINEVILLE, NC 28134City,State,Zip: 105 YANDLE ST & HWY 51Address: LITTLE GENERALName: UST: 118 ft. 0.022 mi. Relative: Higher Actual: 575 ft. < 1/8 PINEVILLE, NC 28134 SE 105 YANDLE ST & HWY 51 N/A 1 NC USTLITTLE GENERAL U001197105 TC6029023.2s Page 8 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 6000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: RemovedTank Status: 3Tank Id: UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: LITTLE GENERAL (Continued)U001197105 05/15/2006Cleanup: 05/15/2006Date Occur: 05/18/2006Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 36087Incident Number: MO-7430UST Number: Not reportedFacility ID: PINEVILLE, NC 28134City,State,Zip: 106 CRANFORD DRIVEAddress: CLAYTON PROPERTYName: LUST: 396 ft. Site 1 of 2 in cluster A 0.075 mi. Relative: Higher Actual: 573 ft. < 1/8 NC IMDPINEVILLE, NC 28134 NE NC LUST TRUST106 CRANFORD DRIVE N/A A2 NC LUSTCLAYTON PROPERTY S107998527 TC6029023.2s Page 9 Source:USGS Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 1 1 inch = 2000 feet Site Location Plan New Town Hall & Library505-511 Main Street Pineville, NC Town of Pineville N Subject Property Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 2As Shown Sampling Location Plan New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 SS-1 KEY Soil Boring Temporary Monitoring Well TMW-2SS-2 TMW-3 SS-3 TMW-4SS-4 TMW-5 SS-5 TMW-6 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 3As Shown Soil Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N SS-1 KEY MSCC Soil to Water Exceedances SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 4As Shown Groundwater Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 KEY B-BENZENE E-ETHYLBENZENE T-TOLUENE X-XYLENES N-NAPHTHALENE Resutls in ug/L TMW-2 TMW-3 TMW-4 TMW-5 TMW-6 Groundwater Flow Direction B-130 T-220 E-3000X-4200N-760 B-300T-1100E-5600X-13300N-1400 B-NDT-64E-2600 X-5700 N-900 B-ND T-ND E-12X-19.7N-8 B-NDT-NDE-6.7X-12.5N-5.1 DRY SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMMIT-companies.com Phone: (704) 504-1717 Fax: (704) 504-1125 July 10, 2020 Mr. Chip Hill Town of Pineville 200 Dover Street Pineville, NC 28134 Subject: Limited Phase II Environmental Site Assessment New Pineville Town Hall & Library 505-511 Main Street Pineville, Mecklenburg County, North Carolina SUMMIT Project No. 7563.E0001 Dear Mr. Hill: SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. (SUMMIT) is pleased to submit the following report of our Limited Phase II ESA in connection with Recognized Environmental Conditions (RECs) identified in an April 2020 Phase I ESA completed others. The subject property is an approximately 2-acre portion of Mecklenburg County Parcel 22105115, situated in the south of the intersection of Jack Hughes Lane and Main Street in Pineville, North Carolina. This report includes a description of the methodology of our investigation and a summary of our findings and conclusions. If you have any questions regarding our assessment of the subject property or our conclusions, please do not hesitate to call us at (704) 504-1717. Sincerely, SUMMIT Patrick W. Lowery, LG Michael D. Zavislak, NRCC-EAC, CIH, PE Senior Environmental Manager Environmental Department Manager NC LG No: 2421 SUMMIT NC Engineering Firm License No. C-2530 LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT PINEVILLE NEW TOWN HALL AND LIBRARY PINEVILLE MECKLENBURG COUNTY NORTH CAROLINA SUMMIT PROJECT NO. 7563.E0001 Prepared For: Town of Pineville 200 Dover Street Pineville, NC 28134 Prepared By: SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 704-504-1717 July 10, 2020 Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc i TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY ............................................................................................................................................ 1 2.0 INTRODUCTION....................................................................................................................................................... 3 2.1 PURPOSE ............................................................................................................................................................ 3 2.2 SITE DESCRIPTION .............................................................................................................................................. 3 2.3 ASSESSMENT HISTORY ....................................................................................................................................... 3 2.4 WORK PLAN OBJECTIVES ................................................................................................................................... 4 3.0 PROPERTY SETTING................................................................................................................................................. 5 3.1 TOPOGRAPHIC SETTING .................................................................................................................................... 5 3.2 GEOLOGIC SETTING ........................................................................................................................................... 5 3.3 HYDROLOGIC SETTING ....................................................................................................................................... 6 4.0 SUMMARY OF PHASE II ACTIVITIES ........................................................................................................................ 7 4.1 UTILITY LOCATE .................................................................................................................................................. 7 4.2 DRILLING ACTIVITES AND METHODS ................................................................................................................. 7 4.3 SAMPLING .......................................................................................................................................................... 8 4.4 GROUNDWATER MEASURMENTS ...................................................................................................................... 9 4.5 PACKING AND SHIPMENT ................................................................................................................................ 10 4.6 SAMPLING POINT ABANDONMENT ................................................................................................................ 10 5.0 SUMMARY OF LABORATORY ANALYSIS ................................................................................................................ 11 6.0 DATA QUALITY ....................................................................................................................................................... 13 6.1.1. SENSITIVITY ............................................................................................................................................ 13 6.1.2. LABORATORY DATA EVALUATION ........................................................................................................... 13 7.0 FINDINGS & CONCLUSIONS .................................................................................................................................. 14 8.0 RECOMMENDATIONS ........................................................................................................................................... 16 9.0 QUALIFICATION OF REPORT.................................................................................................................................. 17 10.0 ADDITIONAL SERVICES .......................................................................................................................................... 18 11.0 REFERENCES .......................................................................................................................................................... 19 APPENDICES Appendix I: ANALYTICAL SUMMARY Appendix II: FIGURES Appendix III: ANALYTICAL RESULTS Appendix IV: BORING LOGS Appendix V: WELL RECORDS/PERMITS Appendix VI: UST-61 24-HR RELEASE NOTIFICATION Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 1 1.0 EXECUTIVE SUMMARY SUMMIT was retained to complete due diligence services of the New Pineville Town Hall and Library property, in Pineville, North Carolina. A Phase I ESA completed by others, identified the historical usage of the subject property to include the Little General Store, a gasoline service station. The environmental database listing indicated that the Little General Store at 105 Yancey Street operated 14,000-gallon, 6,000-gallon and 1,000-gallon USTs which were reportedly installed in 1973 and removed from service in 1991. Additionally, a geotechnical investigation conducted by others reported petroleum odors in borings completed as part of that investigation. A Limited Phase II ESA was recommended in order to assess the potential environmental concerns. In summary, twelve (12) soil samples and six (6) groundwater samples were collected during this assessment. This sampling scope of services was completed to determine if former historical use of the subject site as Little General Store, a gasoline service station that previously operated three (3) Underground Storage Tanks (USTs), has impacted the subject site. The soil borings and temporary monitoring wells were advanced by hollow stem auger drill and split-spoon sampler. All collected soil samples were submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via EPA Method 8260, Semi-Volatile Organic Compounds (SVOCs) via EPA Method 8270, Volatile Petroleum Hydrocarbons (VPH) by MADEP and Extractable Petroleum Hydrocarbons (EPH) by MADEP. All collected groundwater samples were submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via Method 6200, Semi-Volatile Organic Compounds (SVOCs) via Method 625, VPH/EPH via MADEP, 1,2-DBE via Method 504.1 and Lead via Method 6010. All soil samples collected, reported detections of VOC and SVOC petroleum related compounds. Benzene was detected in sample SS-5 at concentrations exceeding NC MSCCs Soil-to-Water standard. Additionally, VPH C9-C10 Aromatics was reported above MSCCs Soil-to-Water in SS-5 and SS-7. No other soil exceedances were reported. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 2 All five (5) collected groundwater samples reported Naphthalene at concentrations exceeding the NC Groundwater Standards (NC 2L). In addition to Naphthalene, multiple VOCs, SVOCs, VPH and EPH constituents were reported at concentrations exceeding the established NC Groundwater Standards. TMW-2, TMW-4, and TMW-5 document the highest concentrations of petroleum compounds in the groundwater. Groundwater results were additionally compared to the NC Non-Residential Vapor Intrusion Groundwater Screening Levels (Feb. 2018). Benzene was reported at concentrations of 300 ug/L and 130 ug/L in TMW-4 and TMW-5 respectively, exceeding the VI GWS of 69 ug/L. Additionally, Ethylbenzene, Naphthalene, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, and Xylenes (total) exceeded the established VI GWS in TMW-2, TMW-4 and TMW-5. Based on the results of this assessment, SUMMIT concludes the Little General Store (former UST site) has impacted the environmental quality of the subject property. Based on a comparison to the NC Vapor Intrusion Groundwater Screening Levels for Non-Residential, SUMMIT further concludes that a Vapor Intrusion condition exists at the subject property. Based on the results of this Limited Phase II ESA, SUMMIT recommends the Town of Pineville submit a UST-61 24-Hour Release Notification to the North Carolina Department of Environmental Quality, Mooresville Office. A copy of the completed form is included in Appendix VI for review. SUMMIT can submit the completed form on your behalf if requested. Additionally, based on the groundwater concentrations present at the subject property, a Vapor Intrusion condition exists. If future development of the site is anticipated, SUMMIT recommends the use of vapor mitigation measures. Consultation with an Environmental Attorney may be beneficial, in order to properly navigate the regulatory requirements related to the identified impacts at the subject property. removal. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 3 2.0 INTRODUCTION 2.1 PURPOSE SUMMIT was retained by the Town of Pineville to perform a Limited Phase II ESA of the New Pineville Town Hall and Library property located in Pineville, Mecklenburg County, North Carolina (2-acre portion of Mecklenburg County Parcel ID: 22105115). The Limited Phase II ESA was requested in order to assess environmental concerns identified during a Phase I ESA investigation, performed by others. This report presents the results of our Limited Phase II ESA of New Pineville Town Hall and Library property. 2.2 SITE DESCRIPTION The approximate 2-acre subject property is comprised of a portion of Tax Parcel No. 22105115 and is located south of the intersection of Main Street and Jack Hughes Lane in Pineville, Mecklenburg County, North Carolina. The subject property is currently vacant and undeveloped. The property has listed street address 505, 507 and 511 Main Street. According to the Mecklenburg County POLARIS GIS website, the owner of the subject tax parcel is listed as Town of Pineville, PO Box 249, Pineville, NC 28134. Refer to the Site Location Map shown in Figure 1 of Appendix II for the location of the subject property. 2.3 ASSESSMENT HISTORY A Phase I ESA was completed by ESP Associates, Inc, dated April 21, 2020. The Phase I ESA identified the follow Recognized Environmental Conditions (RECs): • The Little General store, reportedly located at 105 Yandle Street and HWY 51 in Pineville, North Carolina, and associated underground storage tanks (USTs) is believed to have been located on the northeastern corner of the subject property. The Little General store UTS were reportedly installed in 1973 and removed from ground in 1991. The store was demolished in 2010-2011. Geotechnical borings completed for due diligence reported petroleum odors from 8.5-10 feet below ground surface (ft bgs) Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 4 depth intervals in multiple borings. Field screening of collected soils confirmed the presence of Volatile Organic Compounds (VOCs). The Phase I ESA reported the historical use as a REC. The Phase I ESA reported the potential petroleum impacts as a Vapor Intrusion (VI) concern. No other site specific or surrounding area assessment history is known at the time of this report. 2.4 WORK PLAN OBJECTIVES SUMMIT proposed to perform a Limited Phase II ESA according to our understanding of the most likely potential for impact, in general accordance with ASTM E1903, and in accordance with the USEPA Field Branches Quality System and Technical Procedures Manual. The proposed scope of services included the collection of twelve (12) soil samples and the installation and sampling of six (6) temporary monitoring wells (TMW) in order to assess the groundwater quality at the subject site. The proposed sampling locations were placed in accessible locations and in areas that represented the highest potential for on-site impacts. All samples collected were scheduled to be relinquished to a NC certified laboratory for analysis. All collected soil samples will be submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via EPA Method 8260, Semi-Volatile Organic Compounds (SVOCs) via EPA Method 8270, Volatile Petroleum Hydrocarbons (VPH) by MADEP and Extractable Petroleum Hydrocarbons (EPH) by MADEP. All collected groundwater samples will be submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via Method 6200, Semi-Volatile Organic Compounds (SVOCs) via Method 625, VPH/EPH via MADEP, 1,2-DBE via Method 504.1 and Lead via Method 6010. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 5 3.0 PROPERTY SETTING 3.1 TOPOGRAPHIC SETTING The United States Geological Survey (USGS) “Fort Mill” 7.5 minute topographic quadrangle map was reviewed. According to the contour lines on the topographic map, the elevation of the subject site ranges from approximately 550 feet to approximately 545 feet above Mean Sea Level (MSL). The contour lines indicate the general direction of downward slope is to the west towards unnamed tributaries of Sugar Creek that flows south. Refer to Figure 1 in Appendix II of this report. 3.2 GEOLOGIC SETTING The property is located in Mecklenburg County, North Carolina, which is located in the south- central Piedmont Physiographic Province. The Piedmont Province generally consists of well- rounded hills and ridges which are dissected by a well-developed system of draws and streams. The Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed directly from molten material) which were initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks deposited in the Piedmont Province during the Precambrian era were the host from the metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods of igneous emplacement, with at least episodes of regional metamorphism resulting in the majority of the rock types seen today. The topography and relief of the Piedmont Province has developed from differential weathering of the igneous and metamorphic rock. Ridges and hills have been developed on the more easily weathered and erodible rock. Because of the continued chemical and physical weathering, the rocks in the Piedmont Province are now generally covered with a mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness and are referred to as residuum or residual soils. The residuum is typically finer grained and has higher clay content near the surface Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 6 because of the advanced weathering. Similarly, the soils typically become coarser grained with increasing depth because of decreased weathering. As the weathering decreases, the residual soils generally retain the overall appearance, texture, gradation and foliations of the parent rock. 3.3 HYDROLOGIC SETTING Based on a review of the United States Geological Survey (USGS) “Fort Mill” quadrangle topographic map, inferred groundwater flow direction based on topography appears to be to the west towards Sugar Creek. Refer to Figure 1 in Appendix II for a topographic map for the subject property. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 7 4.0 SUMMARY OF PHASE II ACTIVITIES 4.1 UTILITY LOCATE Prior to conducting the field services, SUMMIT, marked the boring locations at the subject property and contacted North Carolina 811 to locate underground utilities. In addition to the 811 Utility Locate, SUMMIT contracted with a third-party specialty contractor to scan the boring locations at property for the presence of underground utilities and anomalies at each boring location. As a result of the Utility Locate services, several boring locations were relocated from locations that were proposed prior to the start of the project. Actual boring and sampling location can be viewed on Figure 2 in Appendix II of this report. 4.2 DRILLING ACTIVITES AND METHODS On June 8, 2020, SUMMIT personnel conducted the field activities scope of the Limited Phase II ESA. The twelve (12) soil borings were completed at the locations shown on Figure 2, in Appendix II. Soil borings were completed utilizing a hollow stem auger drill rig and decontaminated stainless- steel split-spoon sampler. At each location, a boring was mechanically advanced and continuous split-spoon samples were collected to a depth of 10 feet below ground surface (bgs). The collected soils were logged by a Field Geologist and field screened for the presence of Volatile Organic Compounds (VOCs) utilizing a calibrated Photo-Ionizing Detection (PID) supplied by Enviro- Equipment of Charlotte, NC. The soil interval displaying the highest PID reading was collected for analysis. If the field screening was inconclusive, the 9-10’ bgs interval was selected for analysis. Each boring generally encountered six (6) inches of surface material and subgrade followed by tan/brown/white fine to medium grained sandy silts to termination depths. Boring Logs can be viewed in Appendix IV of this report. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 8 At six (6) select locations, the soil boring was advanced to 13’ bgs for the installation of a 2-inch temporary monitoring well (TMW). TMW locations are shown on Figure 2, in Appendix II of this report. The TMWs consisted of 2-inch schedule 40 PVC riser and 5 ft of 0.010-inch slotted PVC well screen, installed to intersect the water table. The resulting borehole anulus was filled with Type 3 filter sand to approximately 2 ft above the top of the well screen followed by a hydrated bentonite seal extending to the ground surface. TMW Well Logs can be viewed in Appendix IV of this report. Upon completion of the drilling activities at each location, the drilling equipment was decontaminated by the well driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse (sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was performed prior to starting drilling activities, and upon the completion of drilling activities at each boring/well location. 4.3 SAMPLING Soil samples were collected from each boring following the completion of field screening. Based on field screening results, the following sample intervals were selected from each boring. ID PID Reading Sample Interval ID PID Reading Sample Interval SB-1 0.0 9-10’ bgs SB-7 343.0 9-10’ bgs SB-2 126.8 9-10’ bgs SB-8 85.0 3-4’ bgs SB-3 0.0 9-10’ bgs SB-9 8.9 3-4’ bgs SB-4 555.0 9-10’ bgs SB-10 5.5 3-4’ bgs SB-5 342.0 9-10’ bgs SB-11 151.0 9-10’ bgs SB-6 0.0 9-10’ bgs SB-12 115.0 9-10’ bgs Prior to groundwater sample collection, the monitoring well was gauged and developed by the removed a minimum of 3 well volumes of groundwater from each well. Following well development, the TMW was sampled via the low-flow method using a variable speed peristaltic pump and new dedicated tubing. If drawdown could not be controlled during low-flow sampling Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 9 (i.e. the well runs dry), the sample was be collected following static recharge of the monitoring well. The groundwater sample were collected in the laboratory provided vials and containers. A copy of the analysis and chains of custody are included in Appendix III of this report. Groundwater was not encountered in TMW-3 and was considered dry. Groundwater was encountered in all other completed TMWs. TMW-2 was considered a low-yield and was sampled following static recharge following pumping dry 4.4 GROUNDWATER MEASURMENTS Following temporary well installation, each well was gauged for the presence of groundwater. TMW-3 was considered dry following installation. TMW-2 contained approximately 6 ft of groundwater following installation. TMW-1, TMW-2, TMW-4, TMW-5 and TMW-6 were directly following installation and following a 30-minute equilibrium time. During installation, the Field Geologist indicated that the water table is encountered between 12 and 13 feet bgs. Water table elevations were observed to rise following equilibrium time, indicating a semi-confided groundwater table condition. The following Depth to Water readings were recorded prior to sampling: Well ID DTW @ Install DTW @ Sampling TMW-1 12.3’ 10.1’ TMW-2 DRY 12.7’ TMW-3 DRY DRY’ TMW-4 11.3’ 8.7’ TMW-5 10.9’ 9.0’ TMW-6 10.5’ 8.65’ Depth to Water (DTW) is recorded as feet below the ground surface (bgs). Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 10 4.5 PACKING AND SHIPMENT Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly fastened, and the jars encapsulated in shock-resistant plastic bags. The samples and ice were double-bagged in large plastic bags, tied off with rubber bands, and packed into a cooler. The samples were delivered to Pace Analytical, in West Columbia, SC. The vials and jars used for the collection of the samples at this site were prepared by Pace, and were pre-labeled and contained analyte-appropriate preservatives. A listing of the preservatives in the sample containers utilized for the collection of the samples at this site are cataloged in the Chain-Of-Custody record, attached in Appendix III of this report. The secured samples were relinquished to laboratory on June 9, 2020 for laboratory analysis. 4.6 SAMPLING POINT ABANDONMENT All boreholes and temporary wells were abandoned the same day by the certified well drillers. A copy of the NC GW-30 Abandonment Record is included in Appendix V of this report. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 11 5.0 SUMMARY OF LABORATORY ANALYSIS All samples were relinquished to Pace Analytical on June 9, 2020 for the prescribe analysis. Summary Tables in Appendix I of this report summarizes all detections. The analytical detections are summarized below: Soil Soil sample results were compared to the North Carolina Maximum Soil Contaminant Concentration Levels (MSCCs) for Commercial/Industrial Use and the MSCC for Soil-to-Water. • Benzene was detected at 0.012 mg/kg, above the Soil-to-Water MSCC concentration of .0056 mg/kg in sample SS-5 from SB-5 at 9-10’ bgs. • VPH constituent C9-C10 Aromatics was reported above the Soil-to-Water MSCCs in samples SS-5 (SB-5 @ 9-10’ bgs) and SS-7 (SB-7 @ 9-10’ bgs) of 31 mg/kg. The samples were reported at 35 mg/kg and 59 mg/kg respectively. • Petroleum compounds were identified in all soil samples submitted at concentrations below established MSCCs. No other soil exceedances were reported. Groundwater Groundwater sample results were compared to the North Carolina Groundwater Standards (NC 2L), Gross Contamination Levels (GCLs) and the February 2018 North Carolina Non-Residential Vapor Intrusion Ground Water Screening Levels. • TMW-1 Naphthalene and 1-Methylnaphthalene were reported at 8.3 ug/L and 2.7 ug/L respectively, exceeding the established NC Groundwater Standards of 6 ug/L and 1 ug/L. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 12 • TMW-2 Ethylbenzene, Isopropylbenzene, Naphthalene, n-propylbenzene, 1,3,5- Trimethylbenzene, 1,2,4-Trimethylbenzene, Xylenes (total), 1-Methylnaphthalene, 2- Methylnaphthalene, EPH and VPH were reported at concentrations that exceeded its respective NC Groundwater Standard. Furthermore, Ethylbenzene, Naphthalene, 1,3,5- Trimethylbenzene, 1,2,4-Trimethylbenzene, and Xylenes (total) concentrations exceed the respective NC Non-Residential VI Groundwater Screening Level. • TMW-4 Benzene, Ethylbenzene, Isopropylbenzene, Naphthalene, n-propylbenzene, Toluene, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, Xylenes (total), 1- Methylnaphthalene, 2-Methylnaphthalene, 1,2-Dibromethane (EDB), EPH and VPH were reported at concentrations that exceeded its respective NC Groundwater Standard. Furthermore, Benzene, Ethylbenzene, Naphthalene, 1,3,5-Trimethylbenzene, 1,2,4- Trimethylbenzene, and Xylenes (total) concentrations exceed the respective NC Non- Residential VI Groundwater Screening Level. • TMW-5 Benzene, n-butylbenzene, Ethylbenzene, Isopropylbenzene, Methylene Chloride, Naphthalene, n-propylbenzene, Toluene, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, Xylenes (total), 1-Methylnaphthalene, 2-Methylnaphthalene, EPH and VPH were reported at concentrations that exceeded its respective NC Groundwater Standard. Furthermore, Benzene, Ethylbenzene, Naphthalene, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, and Xylenes (total) concentrations exceed the respective NC Non-Residential VI Groundwater Screening Level. • TMW-6 Naphthalene and 1-Methylnaphthalene were reported at 5.1 ug/L and 2.3 ug/L respectively, exceeding the established NC Groundwater Standards of 6 ug/L and 1 ug/L. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 13 6.0 DATA QUALITY 6.1.1. SENSITIVITY Laboratory RDLs and method detection limits (MDLs) were sufficient to report concentrations below regulatory standards for the majority of analytes. 6.1.2. LABORATORY DATA EVALUATION The laboratory completed validation and verification of laboratory processes and data, and delivered a laboratory report to SUMMIT. The laboratory report and the QC information provide documentation of compliance with the industry standards. In reviewing the laboratory results, several analytes are reported as detections with “J” data qualifiers, indicating the reported value is an estimate reported within the 95% confidence interval. These compounds were detected above the MDL, but below the RDL. The MDL is the lowest concentration at which an analyte can be detected in a sample by the particular laboratory method used. “Detected” indicates that the analyte can be distinguished from the blank with reasonable certainty. The RDL (also called practical quantitation limit, or PQL) is approximately five times the MDL or the lower calibration standard, whichever is higher. Results above the report limit can be distinguished from the blank and fall within applicable standard curves. For the purposes of this assessment, all “J” qualified data are considered acceptable for making site management decisions. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 14 7.0 FINDINGS & CONCLUSIONS In summary, twelve (12) soil samples and six (6) groundwater samples were collected during this assessment. This sampling scope of services was completed to determine if former historical use of the subject site as Little General Store, a gasoline service station that previously operated three (3) Underground Storage Tanks (USTs). The soil borings and temporary monitoring wells were advanced by hollow stem auger drill and split-spoon sampler. All collected soil samples will be submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via EPA Method 8260, Semi-Volatile Organic Compounds (SVOCs) via EPA Method 8270, Volatile Petroleum Hydrocarbons (VPH) by MADEP and Extractable Petroleum Hydrocarbons (EPH) by MADEP. All collected groundwater samples will be submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via Method 6200, Semi-Volatile Organic Compounds (SVOCs) via Method 625, VPH/EPH via MADEP, 1,2-DBE via Method 504.1 and Lead via Method 6010. All soil samples collected reported detections of VOC and SVOC petroleum related compounds. Benzene was detected in sample SS-5 at concentrations exceeding NC MSCCs Soil-to-Water standard. Additionally, VPH C9-C10 Aromatics was reported above MSCCs Soil-to-Water in SS-5 and SS-7. No other soil exceedances were reported. All five (5) collected groundwater samples reported Naphthalene at concentrations exceeding the NC Groundwater Standards (NC 2L). In addition to Naphthalene, multiple VOCs, SVOCs, VPH and EPH constituents were reported at concentrations exceeding the established NC Groundwater Standards. TMW-2, TMW-4, and TMW-5 document the highest concentrations of petroleum compounds in the groundwater. Groundwater results were additionally compared to the NC Non-Residential Vapor Intrusion Groundwater Screening Levels (Feb. 2018). Benzene was reported at concentrations of 300 ug/L and 130 ug/L in TMW-4 and TMW-5 respectively, exceeding the VI GWS of 69 ug/L. Additionally, Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 15 Ethylbenzene, Naphthalene, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, and Xylenes (total) exceeded the established VI GWS in TMW-2, TMW-4 and TMW-5. Based on the results of this assessment, SUMMIT concludes the Little General Store (former UST site) has impacted the environmental quality of the subject property. Based on a comparison to the NC Vapor Intrusion Groundwater Screening Levels for Non-Residential, SUMMIT further concludes that a Vapor Intrusion condition exists at the subject property. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 16 8.0 RECOMMENDATIONS Based on the results of this Limited Phase II ESA, SUMMIT recommends the Town of Pineville submit a UST-61 24-Hour Release Notification to the North Carolina Department of Environmental Quality, Mooresville Office. A copy of the completed form is included in Appendix VI for review. SUMMIT can submit the completed form on your behalf if requested. Additionally, based on the groundwater concentrations present at the subject property, a Vapor Intrusion condition exists. If future development of the site is anticipated, SUMMIT recommends the use of vapor mitigation measures. Consultation with an Environmental Attorney may be beneficial, in order to properly navigate the regulatory requirements related to the identified impacts at the subject property. removal. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 17 9.0 QUALIFICATION OF REPORT The Limited Phase II ESA was performed in general accordance with ASTM E1903, and in accordance with the US EAP Quality System and Technical Procedures for LSASD Field Branches. The findings detailed in this report are specific to the conditions in the immediate vicinity of the sample locations for this particular project. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 18 10.0 ADDITIONAL SERVICES This report does not include any environmental assessment of surface water, the determination of wetlands, the determination of noise impact, the assessment of air quality, the identification of cultural resources, or the identification of endangered species. These services are beyond the scope of services of this limited sampling and analysis. No additional services were provided. Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc 19 11.0 REFERENCES United States Geological Survey (USGS) 7.5 minute Topographic Map of the Fort Mill topographic Quadrangle, Delorme 2002. United States Department of Agriculture (USDA) Soil Conservation Service, Web Soil Survey http://websoilsurvey.sc.egov.usda.gov/App/WebSoilSurvey.aspx Mecklenburg County Polaris GIS – http://polaris3g.mecklenburgcountync.gov/ EPA National Primary Drinking Water Regulations - http://water.epa.gov/drink/contaminants/index.cfm 15A NCAC 2L Standards – http://portal.ncdenr.org/web/wq/ps/csu/gwstandards EPA Regional Screening Levels – http://www.epa.gov/region9/superfund/prg/ North Carolina Maximum Soil Contaminant Concentrations – https://deq.nc.gov/document/msccs-041612 North Carolina Vapor Intrusion Guidance - https://deq.nc.gov/about/divisions/waste-management/waste-management-permit- guidance/dwm-vapor-intrusion-guidance Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\7563.E0001 - New Pineville Town Hall & Library - Phase II ESA.doc APPENDIX I ANALYTICAL SUMMARY Page 1 of 3 CAS VOC Analyte Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL 67-64-1 Acetone 3.60E+05 2.40E+01 ND 0.02 0.022 0.02 0.012 J 0.02 0.012 J 0.02 0.029 0.02 ND 0.02 71-43-2 Benzene 1.64E+02 5.60E-03 ND 0.005 ND 0.005 ND 0.005 ND 0.005 0.012 0.005 ND 0.005 78-93-3 2-Butanone (MEK)2.45E+05 1.60E+01 ND 0.02 0.004 J 0.02 ND 0.02 ND 0.02 0.007 J 0.02 ND 0.02 75-15-0 Carbon disulfide 4.09E+04 4.30E+00 ND 0.005 0.004 J 0.005 ND 0.005 ND 0.005 0.002 J 0.005 ND 0.005 100-41-4 Ethylbenzene 4.00E+04 4.90E+00 ND 0.005 0.077 0.005 ND 0.005 0.008 0.005 1.1 0.36 ND 0.005 98-82-8 Isopropylbenzene 4.09E+04 1.70E+00 ND 0.005 0.026 0.005 ND 0.005 0.002 J 0.005 0.17 0.005 ND 0.005 108-87-2 Methylcyclohexane NA NA ND 0.005 0.11 0.005 ND 0.005 0.006 0.005 0.2 0.005 ND 0.005 108-88-3 Toluene 3.20E+04 4.30E+00 ND 0.005 ND 0.005 ND 0.005 ND 0.005 0.025 0.005 ND 0.005 1330-20-7 Xylenes (total)8.18E+04 4.60E+00 ND 0.01 0.12 0.01 ND 0.01 0.026 0.01 2.2 0.7 ND 0.01 CAS SVOC Analyte Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL 83-32-9 Acenaphthene 2.40E+04 8.20E+00 ND 0.002 ND 0.002 ND 0.003 ND 0.002 0.002 J 0.003 ND 0.003 208-96-8 Acenaphthylene 1.23E+04 1.10E+01 ND 0.002 ND 0.002 ND 0.003 ND 0.002 ND 0.003 ND 0.003 120-12-7 Anthracene 1.22E+05 9.40E+02 ND 0.002 0.002 J 0.002 ND 0.003 0.002 J 0.002 0.002 J 0.003 ND 0.003 100-52-7 Benzaldehyde NA NA ND 0.014 ND 0.014 ND 0.016 ND 0.014 ND 0.015 ND 0.016 56-55-3 Benzo(a)anthracene 8.00E+00 3.50E-01 ND 0.002 ND 0.002 0.005 0.003 ND 0.002 ND 0.003 ND 0.003 50-32-8 Benzo(a)pyrene 7.80E-01 9.60E-02 ND 0.002 ND 0.002 0.006 0.003 ND 0.002 ND 0.003 ND 0.003 205-99-2 Benzo(b)fluoranthene 8.00E+00 1.20E+00 ND 0.002 ND 0.002 0.009 0.003 ND 0.002 ND 0.003 ND 0.003 191-24-2 Benzo(g,h,i)perylene 1.23E+04 6.40E+03 ND 0.002 ND 0.002 0.005 0.003 ND 0.002 ND 0.003 ND 0.003 207-08-9 Benzo(k)fluoranthene 7.80E+01 1.20E+01 ND 0.002 ND 0.002 0.003 J 0.003 ND 0.002 ND 0.003 ND 0.003 92-52-4 1,1'-Biphenyl NA NA ND 0.014 ND 0.014 ND 0.016 ND 0.014 0.006 J 0.015 ND 0.016 218-01-9 Chrysene 7.80E+02 3.90E+01 ND 0.002 ND 0.002 0.006 0.003 ND 0.002 ND 0.003 ND 0.003 84-74-2 Di-n-butyl phthalate NA NA 0.006 J 0.014 0.006 J 0.014 ND 0.016 ND 0.014 ND 0.015 ND 0.016 206-44-0 Fluoranthene 1.64E+04 2.90E+02 ND 0.002 ND 0.002 0.008 0.003 ND 0.002 0.001 J 0.003 0.001 J 0.003 86-73-7 Fluorene 1.64E+04 4.70E+01 ND 0.002 0.001 J 0.002 ND 0.003 0.002 J 0.002 0.003 0.003 ND 0.003 193-39-5 Indeno(1,2,3-c,d)pyrene 8.00E+00 3.40E+00 ND 0.002 ND 0.002 0.003 0.003 ND 0.002 ND 0.003 ND 0.003 91-57-6 2-Methylnaphthalene 1.64E+03 3.60E+00 ND 0.002 0.023 0.002 0.002 J 0.003 0.037 0.002 0.35 0.003 0.003 0.003 91-20-3 Naphthalene 8.18E+03 3.60E+00 ND 0.002 0.006 0.002 0.002 J 0.003 0.004 0.002 0.15 0.003 0.002 J 0.003 85-01-8 Phenanthrene 1.23E+04 5.60E+01 ND 0.002 0.004 0.002 0.003 J 0.003 0.004 0.002 0.006 0.003 ND 0.003 129-00-0 Pyrene 1.23E+04 2.70E+02 ND 0.002 0.002 J 0.002 0.008 0.003 0.002 J 0.002 0.002 J 0.003 0.002 J 0.003 CAS MA VPH Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL SESI-0029 C5 - C8 Aliphatics 2.45E+04 6.80E+01 ND 4.4 9.2 4.1 ND 5 ND 4.5 24 5.5 ND 4.4 SESI-0030 C9 - C12 Aliphatics 4.00E+04 5.40E+02 ND 4.4 5 4.1 ND 5 2.3 J 4.5 35 5.5 ND 4.4 SESI-0031 C9 - C10 Aromatics 1.23E+04 3.10E+01 ND 1.5 5.9 1.4 ND 1.7 1.7 1.5 35 1.8 ND 1.5 ND = Not detected at or above MDL J = Estimated Concentration (=<RL>MDL) BOLD = Concentration Above Reference Values NT = Not Tested MDL = Method Detection Limit MSCCs = Maximum Soil Contaminant Concentration Levels 9-10'9-10'9-10' 0.0 126.8 9-10'10-11' 0.0 555.0 342.0 Table 1: Soil Sample Detection Summary Table DEQ Reference Values Sample ID Sample Date Sample Depth ('bgs) Field Screening Result (ppm) SS-1 SS-2 6/8/2020 6/8/2020 SS-5SS-3 SS-4 6/8/2020 All Values in mg/kg 6/8/2020 6/8/2020 SS-6 6/8/2020 9-10' 0.0 New Pineville Townhall Library Pineville, NC July 8, 2020 SUMMIT Project No: 7563.E001 Page 2 of 3 CAS VOC Analyte Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL 67-64-1 Acetone 3.60E+05 2.40E+01 0.016 J 0.022 ND 0.02 ND 0.02 ND 0.028 ND 0.016 0.017 J 0.025 71-43-2 Benzene 1.64E+02 5.60E-03 0.0054 J 0.005 ND 0.005 ND 0.005 ND 0.007 ND 0.004 ND 0.006 78-93-3 2-Butanone (MEK)2.45E+05 1.60E+01 ND 0.02 ND 0.02 ND 0.02 ND 0.028 ND 0.016 ND 0.025 75-15-0 Carbon disulfide 4.09E+04 4.30E+00 ND 0.005 ND 0.005 ND 0.005 ND 0.007 ND 0.004 0.044 J 0.006 100-41-4 Ethylbenzene 4.00E+04 4.90E+00 0.49 0.32 0.24 E 0.005 ND 0.005 0.005 J 0.007 0.014 0.004 2.1 0.29 98-82-8 Isopropylbenzene 4.09E+04 1.70E+00 0.35 E 0.005 0.048 0.005 ND 0.005 ND 0.007 0.003 J 0.004 0.18 0.006 108-87-2 Methylcyclohexane NA NA 0.24 E 0.005 0.055 0.005 ND 0.005 ND 0.007 ND 0.004 0.15 0.006 108-88-3 Toluene 3.20E+04 4.30E+00 0.056 0.005 0.007 0.005 ND 0.005 ND 0.007 ND 0.004 ND 0.006 1330-20-7 Xylenes (total)8.18E+04 4.60E+00 1.6 0.64 0.7 0.61 ND 0.01 0.029 0.014 0.069 0.008 2.2 0.59 CAS SVOC Analyte Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL 83-32-9 Acenaphthene 2.40E+04 8.20E+00 ND 0.033 0.006 0.003 ND 0.003 ND 0.016 ND 0.003 ND 0.003 208-96-8 Acenaphthylene 1.23E+04 1.10E+01 ND 0.033 ND 0.003 0.002 J 0.003 ND 0.016 ND 0.003 ND 0.003 120-12-7 Anthracene 1.22E+05 9.40E+02 ND 0.033 0.006 0.003 0.003 0.003 ND 0.016 0.001 J 0.003 0.004 0.003 100-52-7 Benzaldehyde NA NA ND 0.16 ND 0.016 0.012 J 0.017 ND 0.079 ND 0.014 ND 0.015 56-55-3 Benzo(a)anthracene 8.00E+00 3.50E-01 0.04 0.033 0.003 0.003 0.012 0.003 0.02 0.016 ND 0.003 ND 0.003 50-32-8 Benzo(a)pyrene 7.80E-01 9.60E-02 0.034 0.033 ND 0.003 0.013 0.003 0.018 0.016 ND 0.003 ND 0.003 205-99-2 Benzo(b)fluoranthene 8.00E+00 1.20E+00 0.056 0.033 ND 0.003 0.02 0.003 0.027 0.016 ND 0.003 ND 0.003 191-24-2 Benzo(g,h,i)perylene 1.23E+04 6.40E+03 0.021 J 0.033 ND 0.003 0.006 0.003 0.008 J 0.016 ND 0.003 ND 0.003 207-08-9 Benzo(k)fluoranthene 7.80E+01 1.20E+01 ND 0.033 ND 0.003 0.006 0.003 0.009 J 0.016 ND 0.003 ND 0.003 92-52-4 1,1'-Biphenyl NA NA ND 0.16 0.024 0.016 ND 0.017 ND 0.079 ND 0.014 ND 0.015 218-01-9 Chrysene 7.80E+02 3.90E+01 0.035 0.033 0.001 J 0.003 0.013 0.003 0.015 J 0.016 ND 0.003 ND 0.003 132-64-9 Dibenzofuran 1.64E+03 4.70E+00 ND 0.016 ND 0.016 0.01 J 0.017 ND 0.079 ND 0.014 ND 0.015 84-74-2 Di-n-butyl phthalate NA NA ND 0.16 0.007 J 0.016 0.009 J 0.017 0.032 J 0.079 0.007 J 0.014 ND 0.015 206-44-0 Fluoranthene 1.64E+04 2.90E+02 0.054 0.033 0.003 0.003 0.016 0.003 0.019 0.016 ND 0.003 0.001 J 0.003 86-73-7 Fluorene 1.64E+04 4.70E+01 ND 0.033 0.01 0.003 ND 0.003 ND 0.016 ND 0.003 0.003 0.003 193-39-5 Indeno(1,2,3-c,d)pyrene 8.00E+00 3.40E+00 0.018 0.033 ND 0.003 0.004 0.003 0.008 J 0.016 ND 0.003 ND 0.003 91-57-6 2-Methylnaphthalene 1.64E+03 3.60E+00 0.68 0.033 1.4 0.003 0.049 0.003 0.032 0.016 0.058 0.003 0.037 0.003 91-20-3 Naphthalene 8.18E+03 3.60E+00 0.68 0.033 1 0.003 0.042 0.003 0.026 0.016 0.037 0.003 0.039 0.003 85-01-8 Phenanthrene 1.23E+04 5.60E+01 0.064 0.033 0.014 0.003 0.026 0.003 0.013 J 0.016 0.001 J 0.003 0.007 0.003 129-00-0 Pyrene 1.23E+04 2.70E+02 0.05 0.033 0.006 0.003 0.017 0.003 0.021 0.016 0.002 J 0.003 0.004 0.003 CAS MA VPH Commercial MSCC Soil-to-Water MSCC Result RL Result RL Result RL Result RL Result RL Result RL SESI-0029 C5 - C8 Aliphatics 2.45E+04 6.80E+01 20 5 5.7 4.7 ND 5.2 ND 5.1 ND 4.3 9.7 4 SESI-0030 C9 - C12 Aliphatics 4.00E+04 5.40E+02 50 5 6.6 4.7 1.9 J 5.2 ND 5.1 ND 4.3 27 4 SESI-0031 C9 - C10 Aromatics 1.23E+04 3.10E+01 59 1.7 8.2 1.6 1.7 1.7 0.83 J 1.7 1 J 1.4 25 1.3 ND = Not detected at or above MDL J = Estimated Concentration (=<RL>MDL) BOLD = Concentration Above Reference Values NT = Not Tested MDL = Method Detection Limit MSCCs = Maximum Soil Contaminant Concentration Levels SS-11SS-7 SS-8 SS-9 SS-10 DEQ Reference Values 151.0 All Values in mg/kg 3-4'9-10'9-10' 6/8/2020 6/8/2020 6/8/20206/8/2020 6/8/2020 9-10'3-4'3-4' SS-12 115.0 Table 1: Soil Sample Detection Summary Table (continued) Sample ID Sample Date Sample Depth ('bgs) Field Screening Result (ppm)343.0 85.0 8.9 5.5 6/8/2020 New Pineville Townhall Library Pineville, NC July 8, 2020 SUMMIT Project No: 7563.E001 Page 3 of 3 CAS VOC Analyte NC 2L GWQS GCL Non-Res Vapor GWSL Result RL Result RL Result RL Result RL Result RL Result RL 67-64-1 Acetone 6.00E+03 6.00E+06 1.90E+07 23 10 ND 200 NT ND 500 ND 200 5.7 J 10 71-43-2 Benzene 1.00E+00 5.00E+03 6.90E+01 ND 0.5 ND 10 NT 300 25 130 10 ND 0.5 78-93-3 2-Butanone (MEK)4.00E+03 4.00E+06 1.90E+06 4.5 J 10 ND J 200 NT ND 500 ND 200 ND 10 104-51-8 n-Butylbenzene 7.00E+01 6.90E+03 NE 1.5 0.5 ND 10 NT ND 25 130 10 4 0.5 135-98-8 sec-Butylbenzene 7.00E+01 8.50E+03 NE 0.79 0.5 31 10 NT 27 25 37 10 0.84 0.5 74-87-3 Chloromethane 3.00E+00 3.00E+03 2.20E+02 0.47 J 0.5 ND 10 NT ND 25 ND 10 ND 0.5 108-20-3 Diisopropyl ether (IPE)7.00E+01 7.00E+04 5.90E+03 ND 0.5 ND 10 NT ND 25 11 10 17 0.5 100-41-4 Ethylbenzene 6.00E+02 8.45E+04 1.50E+02 12 0.5 2600 10 NT 5600 25 3000 10 6.7 0.5 98-82-8 Isopropylbenzene 7.00E+01 2.50E+04 7.50E+02 1.6 0.5 130 10 NT 190 25 150 10 1.2 0.5 99-87-6 p-Isopropyltoluene 2.50E+01 1.17E+04 NE 0.46 J 0.5 18 10 NT ND 25 21 10 0.53 0.5 1634-04-4 Methyl tertiary butyl ether (MTBE)2.00E+01 2.00E+04 2.00E+04 ND 0.5 ND 10 NT ND 25 ND 10 3.2 0.5 75-09-2 Methylene chloride 5.00E+00 5.00E+03 4.00E+03 ND 0.5 ND 10 NT ND 25 8 J 10 ND 0.5 91-20-3 Naphthalene 6.00E+00 6.00E+03 1.50E+02 8.3 0.5 900 10 NT 1400 25 760 10 5.1 0.5 103-65-1 n-Propylbenzene 7.00E+01 3.00E+04 2.00E+03 5.4 0.5 420 10 NT 570 25 510 10 4.8 0.5 108-88-3 Toluene 6.00E+02 2.60E+05 1.60E+04 ND 0.5 64 10 NT 1100 25 220 10 ND 0.5 108-67-8 1,3,5-Trimethylbenzene 4.00E+02 2.85E+04 1.50E+02 9.9 0.5 770 10 NT 1000 25 580 10 6.5 0.5 95-63-6 1,2,4-Trimethylbenzene 4.00E+02 2.50E+04 2.10E+02 36 0.5 3000 10 NT 4300 25 1700 10 22 0.5 179601-23-1 m+p-Xylenes NA NA 13 0.5 3000 10 NT 6000 25 1700 10 6.1 0.5 95-47-6 o-Xylenes NA NA 6.7 0.5 2700 10 NT 7300 25 2500 10 6.4 0.5 1330-20-7 Xylenes (total)5.00E+02 8.55E+04 3.20E+02 19.7 0.5 5700 10 NT 13300 25 4200 10 12.5 0.5 CAS SVOC Analyte NC 2L GWQS GCL GCL Result RL Result RL Result RL Result RL Result RL Result RL 84-66-2 Diethylphthalate 6.00E+03 NA NE 8.9 B 3.2 ND 16 NT ND 16 ND 16 17 B 3.2 131-11-3 Dimethyl phthalate NA NA NE 1.6 J 3.2 ND 16 NT ND 16 ND 16 2.2 J 3.2 105-67-9 2,4-Dimethylphenol 1.00E+02 1.00E+05 NE 3 BJ 3.2 97 16 NT 40 16 61 16 24 B 3.2 84-74-2 Di-n-butyl phthalate NA NA NE ND 3.2 0.006 J 16 NT ND 16 ND 16 ND 3.2 90-12-0 1-Methylnaphthalene 1.00E+00 1.00E+03 NE 2.7 J 3.2 97 16 NT 140 16 120 16 2.3 J 3.2 91-57-6 2-Methylnaphthalene 3.00E+01 1.25E+04 NE 4.6 3.2 170 16 NT 260 16 210 16 4.2 3.2 108-5-2 Phenol 3.00E+01 3.00E+04 NE ND 3.2 ND 16 NT ND 16 9.9 J 16 2.3 J 3.2 CAS EDB NC 2L GWQS GCL GCL Result RL Result RL Result RL Result RL Result RL Result RL 106-93-4 1,2-Dibromoethane 2.00E-02 5.00E+01 7.70E+00 ND 0.0097 ND 0.0097 NT 0.013 0.0096 ND 0.0097 ND 0.0099 CAS MA EPH NC 2L GWQS GCL GCL Result RL Result RL Result RL Result RL Result RL Result RL C11 - C22 Aromatics 2.00E+02 NE NE ND 100 1500 100 NT 1700 100 1200 100 120 100 C9 - C18 Aliphatics 7.00E+02 NE NE ND 100 130 100 NT ND 100 110 100 ND 100 CAS MA VPH NC 2L GWQS GCL GCL Result RL Result RL Result RL Result RL Result RL Result RL SESI-0029 C5 - C8 Aliphatics 4.00E+02 NE NE ND 75 1600 J 3800 NT 3300 7500 4400 3800 22 J 75 SESI-0030 C9 - C12 Aliphatics 7.00E+02 NE NE 140 75 16000 3800 NT 25000 J 7500 12000 3800 91 75 SESI-0031 C9 - C10 Aromatics 2.00E+02 NE NE 190 25 10000 1300 NT 18000 2500 8200 1300 160 25 CAS Metals NC 2L GWQS GCL GCL Result RL Result RL Result RL Result RL Result RL Result RL 7439-92-1 Lead 1.50E+01 1.50E+04 NA 1.4E-05 0.00001 6.8E-06 J 0.00001 NT 1.4E-05 1.4E-05 1.3E-05 0.00001 1.3E-05 0.00001 ND = Not detected at or above MDL J = Estimated Concentration (=<RL>MDL) BOLD = Concentration Above Reference Values NT = Not Tested MDL = Method Detection Limit NC 2L = NC Groundwater Standards NE = Not Established GCL = NC Gross Contamination Levels GWSL = February 2018 Non-Residential Vapor Intrusion Groundwater Screening Levels Table 2: Soil Sample Detection Summary Table Sample ID TMW-1 TMW-2 TMW-3 TMW-4 TMW-5 TMW-6 Sample Date 6/8/2020 6/8/2020 6/8/2020 6/8/2020 6/8/2020 6/8/2020 13'13' Depth to Water ('bgs)10.1'12.7'DRY 8.7'9.0'8.65' Temp Well Depth ('bgs)13'13'13'13' All Values in ug/L DEQ Reference Values New Pineville Townhall Library Pineville, NC July 8, 2020 SUMMIT Project No: 7563.E001 Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Appendix II.rtf APPENDIX II FIGURES Source:USGS Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 1 1 inch = 2000 feet Site Location Plan New Town Hall & Library505-511 Main Street Pineville, NC Town of Pineville N Subject Property Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 2As Shown Sampling Location Plan New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 SS-1 KEY Soil Boring Temporary Monitoring Well TMW-2SS-2 TMW-3 SS-3 TMW-4SS-4 TMW-5 SS-5 TMW-6 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 3As Shown Soil Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N SS-1 KEY MSCC Soil to Water Exceedances SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 4As Shown Groundwater Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 KEY B-BENZENE E-ETHYLBENZENE T-TOLUENE X-XYLENES N-NAPHTHALENE Resutls in ug/L TMW-2 TMW-3 TMW-4 TMW-5 TMW-6 Groundwater Flow Direction B-130 T-220 E-3000X-4200N-760 B-300T-1100E-5600X-13300N-1400 B-NDT-64E-2600 X-5700 N-900 B-ND T-ND E-12X-19.7N-8 B-NDT-NDE-6.7X-12.5N-5.1 DRY Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Appendix III - Lab Results.rtf APPENDIX III ANALYTICAL RESULTS The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC. Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Report of Analysis SUMMIT Engineering,Laboratory &Testing,P.C. 3575 Centre Circle Fort Mill,SC 28715 Attention:Patrick Lowery Project Name:Pineville Town Hall Project Number:7563.E0001 Lot Number:VF09036 Date Completed:06/25/2020 Project Manager:Lucas Odom 06/26/2020 12:02 PM Approved and released by: Project Manager:Kelly M.Nance Page 1 of 170 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com Case Narrative SUMMIT Engineering,Laboratory &Testing,P.C. Lot Number:VF09036 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved NELAC standards,the Pace Analytical Services,LLC ("Pace")Quality Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Pace policies.Any exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or discussed below. Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Volatiles Sample -012 had methylcyclohexane and isopropylbenzene recovered above the instrument's calibration range.The sample was re-analyzed high level but the results were ND.The samples have been flagged with a "E"qualifier. Sample -012 had ethylbenzene recovered above the instrument's calibration range.The sample was re- analyzed high level but the results were ND.The samples have been flagged with a "E"qualifier. Semivolatiles The method blank associated with batch 56546 had diethyl phthalate and di-n-butyl phthalate detected at a concentration that was above ½the LOQ.All samples associated with this method blank have detections for these compounds at least ten times greater than the detection in the blank or the detection was below the LOQ.The samples have been flagged with a “B”qualifier. The method blank associated with batch 56992 had di-n-butyl phthalate detected at a concentration that was above ½the LOQ.All samples associated with this method blank have detections for this compounds below the LOQ.The samples have been flagged with a “B”qualifier. The laboratory control sample (LCS)associated with batch 57409 had butyl benzyl phthalate recovered above the acceptance limits.This could potentially result in a high bias on analytical results.There were no detections for this compound in the samples associated with this batch;therefore,data quality is not impacted. The matrix spike/matrix spike duplicate (MS/MSD)associated with sample -007 had 2-methylphenol recovered outside of the acceptance limits.The LCS was recovered within the required acceptance limits; therefore,this likely demonstrates a matrix effect. MADEPH EPH The laboratory control sample (LCS)associated with batch 56889 had C9-C18 Aliphatics recovered below the acceptance limits.Additionally,the RPD exceeded the acceptance limit.This could potentially Page 2 of 170 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com result in a low bias on analytical results.There was insufficient sample volume remaining for re- extraction/re-analysis;results for this compound in the samples associated with this batch should be considered estimated. The RPD for C11-C22 Aromatics exceeded the acceptance limit in batch 56890;however,all other criteria for this compound in the LCS/LCSD were within acceptance limits.The associated sample results were reported and no corrective action was required. Page 3 of 170 PACE ANALYTICAL SERVICES, LLC Sample Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: VF09036 Sample Number Sample ID Matrix Date Sampled Date Received 001 06/08/2020 1240TMW-1 Aqueous 06/09/2020 002 06/08/2020 1130TMW-2 Aqueous 06/09/2020 003 06/08/2020 1400TMW-4 Aqueous 06/09/2020 004 06/08/2020 1430TMW-5 Aqueous 06/09/2020 005 06/08/2020 1545TMW-6 Aqueous 06/09/2020 006 06/08/2020 1115SS-1 Solid 06/09/2020 007 06/08/2020 0940SS-2 Solid 06/09/2020 008 06/08/2020 1150SS-3 Solid 06/09/2020 009 06/08/2020 1320SS-4 Solid 06/09/2020 010 06/08/2020 1345SS-5 Solid 06/09/2020 011 06/08/2020 1415SS-6 Solid 06/09/2020 012 06/08/2020 1450SS-7 Solid 06/09/2020 013 06/08/2020 1500SS-8 Solid 06/09/2020 014 06/08/2020 1515SS-9 Solid 06/09/2020 015 06/08/2020 1520SS-10 Solid 06/09/2020 016 06/08/2020 1530SS-11 Solid 06/09/2020 017 06/08/2020 1540SS-12 Solid 06/09/2020 (17 samples) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 4 of 170 PACE ANALYTICAL SERVICES, LLC Detection Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 TMW-1 Aqueous Acetone SM 6200B-23 ug/L 11 001 TMW-1 Aqueous 2-Butanone (MEK)SM 6200B-4.5 J ug/L 11 001 TMW-1 Aqueous n-Butylbenzene SM 6200B-1.5 ug/L 11 001 TMW-1 Aqueous sec-Butylbenzene SM 6200B-0.79 ug/L 11 001 TMW-1 Aqueous Chloromethane (Methyl SM 6200B-0.47 J ug/L 11 001 TMW-1 Aqueous Ethylbenzene SM 6200B-12 ug/L 11 001 TMW-1 Aqueous Isopropylbenzene SM 6200B-1.6 ug/L 12 001 TMW-1 Aqueous p-Isopropyltoluene (p-SM 6200B-0.46 J ug/L 12 001 TMW-1 Aqueous Naphthalene SM 6200B-8.0 ug/L 12 001 TMW-1 Aqueous n-Propylbenzene SM 6200B-5.4 ug/L 12 001 TMW-1 Aqueous 1,3,5-Trimethylbenzene SM 6200B-9.9 ug/L 12 001 TMW-1 Aqueous 1,2,4-Trimethylbenzene SM 6200B-36 ug/L 12 001 TMW-1 Aqueous m+p - Xylenes SM 6200B-13 ug/L 12 001 TMW-1 Aqueous o - Xylenes SM 6200B-6.7 ug/L 12 001 TMW-1 Aqueous Diethylphthalate 625.1 8.9 B ug/L 13 001 TMW-1 Aqueous Dimethyl phthalate 625.1 1.6 J ug/L 13 001 TMW-1 Aqueous Di-n-butyl phthalate 625.1 3.0 BJ ug/L 13 001 TMW-1 Aqueous 1-Methylnaphthalene 625.1 2.7 J ug/L 13 001 TMW-1 Aqueous 2-Methylnaphthalene 625.1 4.6 ug/L 13 001 TMW-1 Aqueous Naphthalene 625.1 8.3 ug/L 14 001 TMW-1 Aqueous C9 - C12 Aliphatics MADEP-VPH-140 ug/L 15 001 TMW-1 Aqueous C9 - C10 Aromatics MADEP-VPH-190 ug/L 15 001 TMW-1 Aqueous Lead 6010D 0.014 mg/L 16 002 TMW-2 Aqueous sec-Butylbenzene SM 6200B-31 ug/L 17 002 TMW-2 Aqueous Ethylbenzene SM 6200B-2600 ug/L 17 002 TMW-2 Aqueous Isopropylbenzene SM 6200B-130 ug/L 18 002 TMW-2 Aqueous p-Isopropyltoluene (p-SM 6200B-18 ug/L 18 002 TMW-2 Aqueous Naphthalene SM 6200B-900 ug/L 18 002 TMW-2 Aqueous n-Propylbenzene SM 6200B-420 ug/L 18 002 TMW-2 Aqueous Toluene SM 6200B-64 ug/L 18 002 TMW-2 Aqueous 1,3,5-Trimethylbenzene SM 6200B-770 ug/L 18 002 TMW-2 Aqueous 1,2,4-Trimethylbenzene SM 6200B-3000 ug/L 18 002 TMW-2 Aqueous m+p - Xylenes SM 6200B-2700 ug/L 18 002 TMW-2 Aqueous o - Xylenes SM 6200B-1700 ug/L 18 002 TMW-2 Aqueous 2,4-Dimethylphenol 625.1 97 ug/L 19 002 TMW-2 Aqueous 1-Methylnaphthalene 625.1 97 ug/L 19 002 TMW-2 Aqueous 2-Methylnaphthalene 625.1 170 ug/L 19 002 TMW-2 Aqueous Naphthalene 625.1 410 ug/L 20 002 TMW-2 Aqueous C11 - C22 Aromatics MADEP-EPH-1500 ug/L 20 002 TMW-2 Aqueous C9 - C18 Aliphatics MADEP-EPH-130 ug/L 21 002 TMW-2 Aqueous C5 - C8 Aliphatics MADEP-VPH-1600 J ug/L 21 002 TMW-2 Aqueous C9 - C12 Aliphatics MADEP-VPH-16000 ug/L 21 002 TMW-2 Aqueous C9 - C10 Aromatics MADEP-VPH-10000 ug/L 21 002 TMW-2 Aqueous Lead 6010D 0.0068 J mg/L 22 003 TMW-4 Aqueous Benzene SM 6200B-300 ug/L 23 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 5 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 003 TMW-4 Aqueous sec-Butylbenzene SM 6200B-27 ug/L 23 003 TMW-4 Aqueous Ethylbenzene SM 6200B-5600 ug/L 23 003 TMW-4 Aqueous Isopropylbenzene SM 6200B-190 ug/L 24 003 TMW-4 Aqueous Naphthalene SM 6200B-1400 ug/L 24 003 TMW-4 Aqueous n-Propylbenzene SM 6200B-570 ug/L 24 003 TMW-4 Aqueous Toluene SM 6200B-1100 ug/L 24 003 TMW-4 Aqueous 1,3,5-Trimethylbenzene SM 6200B-1000 ug/L 24 003 TMW-4 Aqueous 1,2,4-Trimethylbenzene SM 6200B-4300 ug/L 24 003 TMW-4 Aqueous m+p - Xylenes SM 6200B-6000 ug/L 24 003 TMW-4 Aqueous o - Xylenes SM 6200B-7300 ug/L 24 003 TMW-4 Aqueous 2,4-Dimethylphenol 625.1 40 ug/L 25 003 TMW-4 Aqueous 1-Methylnaphthalene 625.1 140 ug/L 25 003 TMW-4 Aqueous 2-Methylnaphthalene 625.1 260 ug/L 26 003 TMW-4 Aqueous Naphthalene 625.1 800 ug/L 26 003 TMW-4 Aqueous 1,2-Dibromoethane (EDB)504.1 0.013 ug/L 26 003 TMW-4 Aqueous C11 - C22 Aromatics MADEP-EPH-1700 ug/L 27 003 TMW-4 Aqueous C5 - C8 Aliphatics MADEP-VPH-3300 J ug/L 27 003 TMW-4 Aqueous C9 - C12 Aliphatics MADEP-VPH-25000 ug/L 27 003 TMW-4 Aqueous C9 - C10 Aromatics MADEP-VPH-18000 ug/L 27 003 TMW-4 Aqueous Lead 6010D 0.014 mg/L 28 004 TMW-5 Aqueous Benzene SM 6200B-130 ug/L 29 004 TMW-5 Aqueous n-Butylbenzene SM 6200B-130 ug/L 29 004 TMW-5 Aqueous sec-Butylbenzene SM 6200B-37 ug/L 29 004 TMW-5 Aqueous Diisopropyl ether (IPE)SM 6200B-11 ug/L 29 004 TMW-5 Aqueous Ethylbenzene SM 6200B-3000 ug/L 29 004 TMW-5 Aqueous Isopropylbenzene SM 6200B-150 ug/L 30 004 TMW-5 Aqueous p-Isopropyltoluene (p-SM 6200B-21 ug/L 30 004 TMW-5 Aqueous Methylene chloride SM 6200B-8.0 J ug/L 30 004 TMW-5 Aqueous Naphthalene SM 6200B-760 ug/L 30 004 TMW-5 Aqueous n-Propylbenzene SM 6200B-510 ug/L 30 004 TMW-5 Aqueous Toluene SM 6200B-220 ug/L 30 004 TMW-5 Aqueous 1,3,5-Trimethylbenzene SM 6200B-580 ug/L 30 004 TMW-5 Aqueous 1,2,4-Trimethylbenzene SM 6200B-1700 ug/L 30 004 TMW-5 Aqueous m+p - Xylenes SM 6200B-1700 ug/L 30 004 TMW-5 Aqueous o - Xylenes SM 6200B-2500 ug/L 30 004 TMW-5 Aqueous 2,4-Dimethylphenol 625.1 61 ug/L 31 004 TMW-5 Aqueous 1-Methylnaphthalene 625.1 120 ug/L 31 004 TMW-5 Aqueous 2-Methylnaphthalene 625.1 210 ug/L 31 004 TMW-5 Aqueous Naphthalene 625.1 420 ug/L 32 004 TMW-5 Aqueous Phenol 625.1 9.9 J ug/L 32 004 TMW-5 Aqueous C11 - C22 Aromatics MADEP-EPH-1200 ug/L 32 004 TMW-5 Aqueous C9 - C18 Aliphatics MADEP-EPH-110 ug/L 33 004 TMW-5 Aqueous C5 - C8 Aliphatics MADEP-VPH-4400 ug/L 33 004 TMW-5 Aqueous C9 - C12 Aliphatics MADEP-VPH-12000 ug/L 33 004 TMW-5 Aqueous C9 - C10 Aromatics MADEP-VPH-8200 ug/L 33 004 TMW-5 Aqueous Lead 6010D 0.013 mg/L 34 005 TMW-6 Aqueous Acetone SM 6200B-5.7 J ug/L 35 005 TMW-6 Aqueous n-Butylbenzene SM 6200B-4.0 ug/L 35 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 6 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 005 TMW-6 Aqueous sec-Butylbenzene SM 6200B-0.84 ug/L 35 005 TMW-6 Aqueous Diisopropyl ether (IPE)SM 6200B-17 ug/L 35 005 TMW-6 Aqueous Ethylbenzene SM 6200B-6.7 ug/L 35 005 TMW-6 Aqueous Isopropylbenzene SM 6200B-1.2 ug/L 36 005 TMW-6 Aqueous p-Isopropyltoluene (p-SM 6200B-0.53 ug/L 36 005 TMW-6 Aqueous Methyl tertiary butyl ether SM 6200B-3.2 ug/L 36 005 TMW-6 Aqueous Naphthalene SM 6200B-5.1 ug/L 36 005 TMW-6 Aqueous n-Propylbenzene SM 6200B-4.8 ug/L 36 005 TMW-6 Aqueous 1,3,5-Trimethylbenzene SM 6200B-6.5 ug/L 36 005 TMW-6 Aqueous 1,2,4-Trimethylbenzene SM 6200B-22 ug/L 36 005 TMW-6 Aqueous m+p - Xylenes SM 6200B-6.1 ug/L 36 005 TMW-6 Aqueous o - Xylenes SM 6200B-6.4 ug/L 36 005 TMW-6 Aqueous Diethylphthalate 625.1 17 B ug/L 37 005 TMW-6 Aqueous Dimethyl phthalate 625.1 2.2 J ug/L 37 005 TMW-6 Aqueous Di-n-butyl phthalate 625.1 24 B ug/L 37 005 TMW-6 Aqueous 1-Methylnaphthalene 625.1 2.3 J ug/L 37 005 TMW-6 Aqueous 2-Methylnaphthalene 625.1 4.2 ug/L 37 005 TMW-6 Aqueous Naphthalene 625.1 5.4 ug/L 38 005 TMW-6 Aqueous Phenol 625.1 2.3 J ug/L 38 005 TMW-6 Aqueous C11 - C22 Aromatics MADEP-EPH-120 ug/L 38 005 TMW-6 Aqueous C5 - C8 Aliphatics MADEP-VPH-22 J ug/L 39 005 TMW-6 Aqueous C9 - C12 Aliphatics MADEP-VPH-91 ug/L 39 005 TMW-6 Aqueous C9 - C10 Aromatics MADEP-VPH-160 ug/L 39 005 TMW-6 Aqueous Lead 6010D 0.013 mg/L 40 006 SS-1 Solid Di-n-butyl phthalate 8270E 6.5 BJ ug/kg 43 007 SS-2 Solid Acetone 8260D 22 ug/kg 46 007 SS-2 Solid 2-Butanone (MEK)8260D 4.6 J ug/kg 46 007 SS-2 Solid Carbon disulfide 8260D 4.3 J ug/kg 46 007 SS-2 Solid Ethylbenzene 8260D 77 ug/kg 46 007 SS-2 Solid Isopropylbenzene 8260D 26 ug/kg 46 007 SS-2 Solid Methylcyclohexane 8260D 110 ug/kg 46 007 SS-2 Solid Xylenes (total)8260D 120 ug/kg 47 007 SS-2 Solid Anthracene 8270E 2.4 J ug/kg 47 007 SS-2 Solid Di-n-butyl phthalate 8270E 6.4 BJ ug/kg 48 007 SS-2 Solid Fluorene 8270E 1.5 J ug/kg 48 007 SS-2 Solid 2-Methylnaphthalene 8270E 23 ug/kg 48 007 SS-2 Solid Naphthalene 8270E 6.8 ug/kg 48 007 SS-2 Solid Phenanthrene 8270E 4.8 ug/kg 49 007 SS-2 Solid Pyrene 8270E 2.5 J ug/kg 49 007 SS-2 Solid C5 - C8 Aliphatics MADEP-VPH-9.2 mg/kg 50 007 SS-2 Solid C9 - C12 Aliphatics MADEP-VPH-5.0 mg/kg 50 007 SS-2 Solid C9 - C10 Aromatics MADEP-VPH-5.9 mg/kg 50 008 SS-3 Solid Acetone 8260D 12 J ug/kg 51 008 SS-3 Solid Benzo(a)anthracene 8270E 5.7 ug/kg 52 008 SS-3 Solid Benzo(a)pyrene 8270E 6.2 ug/kg 52 008 SS-3 Solid Benzo(b)fluoranthene 8270E 9.3 ug/kg 52 008 SS-3 Solid Benzo(g,h,i)perylene 8270E 5.0 ug/kg 52 008 SS-3 Solid Benzo(k)fluoranthene 8270E 3.2 J ug/kg 52 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 7 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 008 SS-3 Solid Chrysene 8270E 6.6 ug/kg 53 008 SS-3 Solid Fluoranthene 8270E 8.0 ug/kg 53 008 SS-3 Solid Indeno(1,2,3-c,d)pyrene 8270E 3.9 ug/kg 53 008 SS-3 Solid 2-Methylnaphthalene 8270E 2.6 J ug/kg 53 008 SS-3 Solid Naphthalene 8270E 2.4 J ug/kg 53 008 SS-3 Solid Phenanthrene 8270E 3.3 J ug/kg 54 008 SS-3 Solid Pyrene 8270E 8.0 ug/kg 54 009 SS-4 Solid Acetone 8260D 12 J ug/kg 56 009 SS-4 Solid Ethylbenzene 8260D 8.3 ug/kg 56 009 SS-4 Solid Isopropylbenzene 8260D 2.2 J ug/kg 56 009 SS-4 Solid Methylcyclohexane 8260D 6.1 ug/kg 56 009 SS-4 Solid Xylenes (total)8260D 26 ug/kg 57 009 SS-4 Solid Anthracene 8270E 2.4 J ug/kg 57 009 SS-4 Solid Fluorene 8270E 2.0 J ug/kg 58 009 SS-4 Solid 2-Methylnaphthalene 8270E 37 ug/kg 58 009 SS-4 Solid Naphthalene 8270E 4.8 ug/kg 58 009 SS-4 Solid Phenanthrene 8270E 4.7 ug/kg 59 009 SS-4 Solid Pyrene 8270E 2.3 J ug/kg 59 009 SS-4 Solid C9 - C12 Aliphatics MADEP-VPH-2.3 J mg/kg 60 009 SS-4 Solid C9 - C10 Aromatics MADEP-VPH-1.7 mg/kg 60 010 SS-5 Solid Acetone 8260D 29 ug/kg 61 010 SS-5 Solid Benzene 8260D 12 ug/kg 61 010 SS-5 Solid 2-Butanone (MEK)8260D 7.7 J ug/kg 61 010 SS-5 Solid Carbon disulfide 8260D 2.5 J ug/kg 61 010 SS-5 Solid Ethylbenzene 8260D 1100 ug/kg 61 010 SS-5 Solid Isopropylbenzene 8260D 170 ug/kg 61 010 SS-5 Solid Methylcyclohexane 8260D 200 ug/kg 61 010 SS-5 Solid Toluene 8260D 25 ug/kg 62 010 SS-5 Solid Xylenes (total)8260D 2200 ug/kg 62 010 SS-5 Solid Acenaphthene 8270E 2.1 J ug/kg 62 010 SS-5 Solid Anthracene 8270E 2.6 J ug/kg 62 010 SS-5 Solid 1,1'-Biphenyl 8270E 6.4 J ug/kg 62 010 SS-5 Solid Fluoranthene 8270E 1.6 J ug/kg 63 010 SS-5 Solid Fluorene 8270E 3.8 ug/kg 63 010 SS-5 Solid 2-Methylnaphthalene 8270E 350 ug/kg 63 010 SS-5 Solid Naphthalene 8270E 150 ug/kg 63 010 SS-5 Solid Phenanthrene 8270E 6.4 ug/kg 64 010 SS-5 Solid Pyrene 8270E 2.6 J ug/kg 64 010 SS-5 Solid C5 - C8 Aliphatics MADEP-VPH-24 mg/kg 65 010 SS-5 Solid C9 - C12 Aliphatics MADEP-VPH-35 mg/kg 65 010 SS-5 Solid C9 - C10 Aromatics MADEP-VPH-35 mg/kg 65 011 SS-6 Solid Fluoranthene 8270E 1.9 J ug/kg 68 011 SS-6 Solid 2-Methylnaphthalene 8270E 3.6 ug/kg 68 011 SS-6 Solid Naphthalene 8270E 2.0 J ug/kg 68 011 SS-6 Solid Pyrene 8270E 2.6 J ug/kg 69 012 SS-7 Solid Acetone 8260D 16 J ug/kg 71 012 SS-7 Solid Benzene 8260D 5.4 J ug/kg 71 012 SS-7 Solid Ethylbenzene 8260D 490 ug/kg 71 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 8 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 012 SS-7 Solid Isopropylbenzene 8260D 350 E ug/kg 71 012 SS-7 Solid Methylcyclohexane 8260D 240 E ug/kg 71 012 SS-7 Solid Toluene 8260D 56 ug/kg 72 012 SS-7 Solid Xylenes (total)8260D 1600 ug/kg 72 012 SS-7 Solid Benzo(a)anthracene 8270E 40 ug/kg 72 012 SS-7 Solid Benzo(a)pyrene 8270E 34 ug/kg 72 012 SS-7 Solid Benzo(b)fluoranthene 8270E 56 ug/kg 72 012 SS-7 Solid Benzo(g,h,i)perylene 8270E 21 J ug/kg 72 012 SS-7 Solid Chrysene 8270E 35 ug/kg 73 012 SS-7 Solid Fluoranthene 8270E 54 ug/kg 73 012 SS-7 Solid Indeno(1,2,3-c,d)pyrene 8270E 18 J ug/kg 73 012 SS-7 Solid 2-Methylnaphthalene 8270E 680 ug/kg 73 012 SS-7 Solid Naphthalene 8270E 660 ug/kg 73 012 SS-7 Solid Phenanthrene 8270E 64 ug/kg 74 012 SS-7 Solid Pyrene 8270E 50 ug/kg 74 012 SS-7 Solid C5 - C8 Aliphatics MADEP-VPH-20 mg/kg 75 012 SS-7 Solid C9 - C12 Aliphatics MADEP-VPH-50 mg/kg 75 012 SS-7 Solid C9 - C10 Aromatics MADEP-VPH-59 mg/kg 75 013 SS-8 Solid Ethylbenzene 8260D 240 E ug/kg 76 013 SS-8 Solid Isopropylbenzene 8260D 48 ug/kg 76 013 SS-8 Solid Methylcyclohexane 8260D 55 ug/kg 76 013 SS-8 Solid Toluene 8260D 7.4 ug/kg 77 013 SS-8 Solid Xylenes (total)8260D 700 ug/kg 77 013 SS-8 Solid Acenaphthene 8270E 6.0 ug/kg 77 013 SS-8 Solid Anthracene 8270E 6.9 ug/kg 77 013 SS-8 Solid Benzo(a)anthracene 8270E 3.4 ug/kg 77 013 SS-8 Solid 1,1'-Biphenyl 8270E 24 ug/kg 77 013 SS-8 Solid Chrysene 8270E 1.8 J ug/kg 78 013 SS-8 Solid Di-n-butyl phthalate 8270E 7.3 J ug/kg 78 013 SS-8 Solid Fluoranthene 8270E 3.6 ug/kg 78 013 SS-8 Solid Fluorene 8270E 10 ug/kg 78 013 SS-8 Solid 2-Methylnaphthalene 8270E 1400 ug/kg 78 013 SS-8 Solid Naphthalene 8270E 1000 ug/kg 78 013 SS-8 Solid Phenanthrene 8270E 14 ug/kg 79 013 SS-8 Solid Pyrene 8270E 6.2 ug/kg 79 013 SS-8 Solid C5 - C8 Aliphatics MADEP-VPH-5.7 mg/kg 80 013 SS-8 Solid C9 - C12 Aliphatics MADEP-VPH-6.6 mg/kg 80 013 SS-8 Solid C9 - C10 Aromatics MADEP-VPH-8.2 mg/kg 80 014 SS-9 Solid Acenaphthylene 8270E 2.0 J ug/kg 82 014 SS-9 Solid Anthracene 8270E 3.7 ug/kg 82 014 SS-9 Solid Benzaldehyde 8270E 12 J ug/kg 82 014 SS-9 Solid Benzo(a)anthracene 8270E 12 ug/kg 82 014 SS-9 Solid Benzo(a)pyrene 8270E 13 ug/kg 82 014 SS-9 Solid Benzo(b)fluoranthene 8270E 20 ug/kg 82 014 SS-9 Solid Benzo(g,h,i)perylene 8270E 6.0 ug/kg 82 014 SS-9 Solid Benzo(k)fluoranthene 8270E 6.8 ug/kg 82 014 SS-9 Solid Chrysene 8270E 13 ug/kg 83 014 SS-9 Solid Dibenzofuran 8270E 10 J ug/kg 83 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 9 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 014 SS-9 Solid Di-n-butyl phthalate 8270E 9.6 J ug/kg 83 014 SS-9 Solid Fluoranthene 8270E 16 ug/kg 83 014 SS-9 Solid Indeno(1,2,3-c,d)pyrene 8270E 4.5 ug/kg 83 014 SS-9 Solid 2-Methylnaphthalene 8270E 49 ug/kg 83 014 SS-9 Solid Naphthalene 8270E 42 ug/kg 83 014 SS-9 Solid Phenanthrene 8270E 26 ug/kg 84 014 SS-9 Solid Pyrene 8270E 17 ug/kg 84 014 SS-9 Solid C9 - C12 Aliphatics MADEP-VPH-1.9 J mg/kg 85 014 SS-9 Solid C9 - C10 Aromatics MADEP-VPH-1.7 mg/kg 85 015 SS-10 Solid Ethylbenzene 8260D 5.7 J ug/kg 86 015 SS-10 Solid Xylenes (total)8260D 29 ug/kg 87 015 SS-10 Solid Benzo(a)anthracene 8270E 20 ug/kg 87 015 SS-10 Solid Benzo(a)pyrene 8270E 18 ug/kg 87 015 SS-10 Solid Benzo(b)fluoranthene 8270E 27 ug/kg 87 015 SS-10 Solid Benzo(g,h,i)perylene 8270E 8.4 J ug/kg 87 015 SS-10 Solid Benzo(k)fluoranthene 8270E 9.0 J ug/kg 87 015 SS-10 Solid Chrysene 8270E 15 J ug/kg 88 015 SS-10 Solid Di-n-butyl phthalate 8270E 32 J ug/kg 88 015 SS-10 Solid Fluoranthene 8270E 19 ug/kg 88 015 SS-10 Solid Indeno(1,2,3-c,d)pyrene 8270E 8.1 J ug/kg 88 015 SS-10 Solid 2-Methylnaphthalene 8270E 32 ug/kg 88 015 SS-10 Solid Naphthalene 8270E 26 ug/kg 88 015 SS-10 Solid Phenanthrene 8270E 13 J ug/kg 89 015 SS-10 Solid Pyrene 8270E 21 ug/kg 89 015 SS-10 Solid C9 - C10 Aromatics MADEP-VPH-0.83 J mg/kg 90 016 SS-11 Solid Ethylbenzene 8260D 14 ug/kg 91 016 SS-11 Solid Isopropylbenzene 8260D 3.6 J ug/kg 91 016 SS-11 Solid Xylenes (total)8260D 69 ug/kg 92 016 SS-11 Solid Anthracene 8270E 1.5 J ug/kg 92 016 SS-11 Solid Di-n-butyl phthalate 8270E 7.0 J ug/kg 93 016 SS-11 Solid 2-Methylnaphthalene 8270E 58 ug/kg 93 016 SS-11 Solid Naphthalene 8270E 37 ug/kg 93 016 SS-11 Solid Phenanthrene 8270E 1.9 J ug/kg 94 016 SS-11 Solid Pyrene 8270E 2.0 J ug/kg 94 016 SS-11 Solid C9 - C10 Aromatics MADEP-VPH-1.0 J mg/kg 95 017 SS-12 Solid Acetone 8260D 17 J ug/kg 96 017 SS-12 Solid Carbon disulfide 8260D 4.4 J ug/kg 96 017 SS-12 Solid Ethylbenzene 8260D 2100 ug/kg 96 017 SS-12 Solid Isopropylbenzene 8260D 180 ug/kg 96 017 SS-12 Solid Methylcyclohexane 8260D 150 ug/kg 96 017 SS-12 Solid Xylenes (total)8260D 2200 ug/kg 97 017 SS-12 Solid Anthracene 8270E 4.6 ug/kg 97 017 SS-12 Solid Fluoranthene 8270E 1.9 J ug/kg 98 017 SS-12 Solid Fluorene 8270E 3.5 ug/kg 98 017 SS-12 Solid 2-Methylnaphthalene 8270E 37 ug/kg 98 017 SS-12 Solid Naphthalene 8270E 39 ug/kg 98 017 SS-12 Solid Phenanthrene 8270E 7.3 ug/kg 99 017 SS-12 Solid Pyrene 8270E 4.3 ug/kg 99 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 10 of 170 Detection Summary (Continued) Lot Number: VF09036 Sample Sample ID Matrix Parameter Method Result Q Units Page 017 SS-12 Solid C5 - C8 Aliphatics MADEP-VPH-9.7 mg/kg 100 017 SS-12 Solid C9 - C12 Aliphatics MADEP-VPH-27 mg/kg 100 017 SS-12 Solid C9 - C10 Aromatics MADEP-VPH-25 mg/kg 100 (288 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 11 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 6200B-SM 6200B-2011 1 06/16/2020 1036 TML 57073 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 SM 6200B-2011 23 2ug/L4.010 Benzene 71-43-2 SM 6200B-2011 ND 2ug/L0.400.50 Bromobenzene 108-86-1 SM 6200B-2011 ND 2ug/L0.400.50 Bromochloromethane 74-97-5 SM 6200B-2011 ND 2ug/L0.400.50 Bromodichloromethane 75-27-4 SM 6200B-2011 ND 2ug/L0.400.50 Bromoform 75-25-2 SM 6200B-2011 ND 2ug/L0.400.50 Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 2ug/L0.400.50 2-Butanone (MEK)78-93-3 SM 6200B-2011 4.5 J 2ug/L2.010 n-Butylbenzene 104-51-8 SM 6200B-2011 1.5 2ug/L0.400.50 sec-Butylbenzene 135-98-8 SM 6200B-2011 0.79 2ug/L0.400.50 tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 2ug/L0.400.50 Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 2ug/L0.400.50 Chlorobenzene 108-90-7 SM 6200B-2011 ND 2ug/L0.400.50 Chloroethane 75-00-3 SM 6200B-2011 ND 2ug/L0.400.50 Chloroform 67-66-3 SM 6200B-2011 ND 2ug/L0.400.50 Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 0.47 J 2ug/L0.400.50 2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 2ug/L0.400.50 4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 2ug/L0.400.50 Dibromochloromethane 124-48-1 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 2ug/L0.400.50 Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 2ug/L0.400.50 1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 2ug/L0.400.50 1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 2ug/L0.400.50 Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 2ug/L0.400.50 cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 2ug/L0.400.50 trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 2ug/L0.400.50 1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 2ug/L0.400.50 2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 2ug/L0.400.50 cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 2ug/L0.400.50 trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 2ug/L0.400.50 Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 ND 2ug/L0.400.50 Ethylbenzene 100-41-4 SM 6200B-2011 12 2ug/L0.400.50 Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 2ug/L0.400.50 2-Hexanone 591-78-6 SM 6200B-2011 ND 2ug/L2.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 12 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 6200B-SM 6200B-2011 1 06/16/2020 1036 TML 57073 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 1.6 2ug/L0.400.50 p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 0.46 J 2ug/L0.400.50 Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 ND 2ug/L0.400.50 4-Methyl-2-pentanone 108-10-1 SM 6200B-2011 ND 2ug/L2.010 Methylene chloride 75-09-2 SM 6200B-2011 ND 2ug/L0.400.50 Naphthalene 91-20-3 SM 6200B-2011 8.0 2ug/L0.400.50 n-Propylbenzene 103-65-1 SM 6200B-2011 5.4 2ug/L0.400.50 Styrene 100-42-5 SM 6200B-2011 ND 2ug/L0.400.50 1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 2ug/L0.400.50 Tetrachloroethene 127-18-4 SM 6200B-2011 ND 2ug/L0.400.50 Toluene 108-88-3 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 2ug/L0.400.50 1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 2ug/L0.400.50 1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 2ug/L0.400.50 1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 2ug/L0.400.50 Trichloroethene 79-01-6 SM 6200B-2011 ND 2ug/L0.400.50 Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 2ug/L0.400.50 1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 2ug/L0.400.50 1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 9.9 2ug/L0.400.50 1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 36 2ug/L0.400.50 Vinyl chloride 75-01-4 SM 6200B-2011 ND 2ug/L0.400.50 m+p - Xylenes 179601-23-1 SM 6200B-2011 13 2ug/L0.400.50 o - Xylenes 95-47-6 SM 6200B-2011 6.7 2ug/L0.400.50 AcceptanceRun 2 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 101 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2039 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 625.1 ND 1ug/L1.63.2 Acenaphthylene 208-96-8 625.1 ND 1ug/L1.63.2 Anthracene 120-12-7 625.1 ND 1ug/L1.63.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 13 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2039 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L1.63.2 Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L1.63.2 Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L1.63.2 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L1.63.2 Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L1.63.2 Benzyl alcohol 100-51-6 625.1 ND 1ug/L4.06.4 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L1.63.2 Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L1.63.2 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L1.63.2 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L1.63.2 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L1.63.2 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L1.63.2 2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L1.63.2 2-Chlorophenol 95-57-8 625.1 ND 1ug/L1.63.2 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L1.63.2 Chrysene 218-01-9 625.1 ND 1ug/L1.63.2 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L1.63.2 Dibenzofuran 132-64-9 625.1 ND 1ug/L2.03.2 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L1.616 2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L1.63.2 Diethylphthalate 84-66-2 625.1 8.9 B 1ug/L1.63.2 Dimethyl phthalate 131-11-3 625.1 1.6 J 1ug/L1.63.2 2,4-Dimethylphenol 105-67-9 625.1 ND 1ug/L1.63.2 Di-n-butyl phthalate 84-74-2 625.1 3.0 BJ 1ug/L1.63.2 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L1.616 2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L1.616 Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L1.63.2 1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L1.63.2 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 1ug/L8.016 Fluoranthene 206-44-0 625.1 ND 1ug/L1.63.2 Fluorene 86-73-7 625.1 ND 1ug/L1.63.2 Hexachlorobenzene 118-74-1 625.1 ND 1ug/L1.63.2 Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L1.63.2 Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L8.016 Hexachloroethane 67-72-1 625.1 ND 1ug/L1.63.2 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L1.63.2 Isophorone 78-59-1 625.1 ND 1ug/L1.63.2 1-Methylnaphthalene 90-12-0 625.1 2.7 J 1ug/L0.803.2 2-Methylnaphthalene 91-57-6 625.1 4.6 1ug/L0.803.2 2-Methylphenol 95-48-7 625.1 ND 1ug/L1.33.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 14 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2039 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 3+4-Methylphenol 106-44-5 625.1 ND 1ug/L3.03.2 Naphthalene 91-20-3 625.1 8.3 1ug/L1.63.2 Nitrobenzene 98-95-3 625.1 ND 1ug/L1.63.2 2-Nitrophenol 88-75-5 625.1 ND 1ug/L1.66.4 4-Nitrophenol 100-02-7 625.1 ND 1ug/L8.016 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L1.63.2 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L1.63.2 Pentachlorophenol 87-86-5 625.1 ND 1ug/L8.016 Phenanthrene 85-01-8 625.1 ND 1ug/L1.63.2 Phenol 108-95-2 625.1 ND 1ug/L1.63.2 Pyrene 129-00-0 625.1 ND 1ug/L1.63.2 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L1.63.2 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L1.63.2 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 98 37-129 2-Fluorophenol 52 24-127 Nitrobenzene-d5 95 38-127 Phenol-d5 82 28-128 Terphenyl-d14 121 10-148 2,4,6-Tribromophenol 100 41-144 EDB & DBCP by Microextraction Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 504.1 504.1 1 06/11/2020 1418 JJG 06/11/2020 0930 56595 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,2-Dibromoethane (EDB)106-93-4 504.1 ND 1ug/L0.00390.0097 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,1,1,2-Tetrachloroethane 86 57-137 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0541 JJG 06/14/2020 1533 56890 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1ug/L100100 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 15 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl (aromatic)77 40-140 2-Fluorobiphenyl (fractionation 1)107 40-140 2-Bromonaphthalene (fractionation 2)111 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0012 JJG 06/14/2020 1535 56889 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1ug/L100100 C19 - C36 Aliphatics MADEP-EPH-04 ND 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)45 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/11/2020 2344 STM 56710 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1ug/L1575 C9 - C12 Aliphatics MADEP-VPH-18-140 1ug/L1575 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)110 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/11/2020 2344 STM 56711 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-190 1ug/L5.025 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)112 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 16 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-1 VF09036-001 06/08/2020 1240 06/09/2020 Aqueous ICP-AES Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010D 1 06/17/2020 0343 KSH2 06/13/2020 1626 56859 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Lead 7439-92-1 6010D 0.014 1mg/L0.00470.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 17 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 20 06/11/2020 1347 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 SM 6200B-2011 ND 1ug/L80200 Benzene 71-43-2 SM 6200B-2011 ND 1ug/L8.010 Bromobenzene 108-86-1 SM 6200B-2011 ND 1ug/L8.010 Bromochloromethane 74-97-5 SM 6200B-2011 ND 1ug/L8.010 Bromodichloromethane 75-27-4 SM 6200B-2011 ND 1ug/L8.010 Bromoform 75-25-2 SM 6200B-2011 ND 1ug/L8.010 Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 1ug/L8.010 2-Butanone (MEK)78-93-3 SM 6200B-2011 ND 1ug/L40200 n-Butylbenzene 104-51-8 SM 6200B-2011 ND 1ug/L8.010 sec-Butylbenzene 135-98-8 SM 6200B-2011 31 1ug/L8.010 tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 1ug/L8.010 Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 1ug/L8.010 Chlorobenzene 108-90-7 SM 6200B-2011 ND 1ug/L8.010 Chloroethane 75-00-3 SM 6200B-2011 ND 1ug/L8.010 Chloroform 67-66-3 SM 6200B-2011 ND 1ug/L8.010 Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 ND 1ug/L8.010 2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 1ug/L8.010 4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 1ug/L8.010 Dibromochloromethane 124-48-1 SM 6200B-2011 ND 1ug/L8.010 1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 1ug/L8.010 Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 1ug/L8.010 1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 1ug/L8.010 1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 1ug/L8.010 Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 1ug/L8.010 cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 1ug/L8.010 trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 1ug/L8.010 1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 1ug/L8.010 2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 1ug/L8.010 cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 1ug/L8.010 trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 1ug/L8.010 Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 ND 1ug/L8.010 Ethylbenzene 100-41-4 SM 6200B-2011 2600 1ug/L8.010 Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 1ug/L8.010 2-Hexanone 591-78-6 SM 6200B-2011 ND 1ug/L40200 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 18 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 20 06/11/2020 1347 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 130 1ug/L8.010 p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 18 1ug/L8.010 Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 ND 1ug/L8.010 4-Methyl-2-pentanone 108-10-1 SM 6200B-2011 ND 1ug/L40200 Methylene chloride 75-09-2 SM 6200B-2011 ND 1ug/L8.010 Naphthalene 91-20-3 SM 6200B-2011 900 1ug/L8.010 n-Propylbenzene 103-65-1 SM 6200B-2011 420 1ug/L8.010 Styrene 100-42-5 SM 6200B-2011 ND 1ug/L8.010 1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 1ug/L8.010 1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 1ug/L8.010 Tetrachloroethene 127-18-4 SM 6200B-2011 ND 1ug/L8.010 Toluene 108-88-3 SM 6200B-2011 64 1ug/L8.010 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 1ug/L8.010 1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 1ug/L8.010 1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 1ug/L8.010 1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 1ug/L8.010 1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 1ug/L8.010 Trichloroethene 79-01-6 SM 6200B-2011 ND 1ug/L8.010 Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 1ug/L8.010 1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 1ug/L8.010 1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 770 1ug/L8.010 1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 3000 1ug/L8.010 Vinyl chloride 75-01-4 SM 6200B-2011 ND 1ug/L8.010 m+p - Xylenes 179601-23-1 SM 6200B-2011 2700 1ug/L8.010 o - Xylenes 95-47-6 SM 6200B-2011 1700 1ug/L8.010 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 101 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 103 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2103 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 625.1 ND 1ug/L8.016 Acenaphthylene 208-96-8 625.1 ND 1ug/L8.016 Anthracene 120-12-7 625.1 ND 1ug/L8.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 19 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2103 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L8.016 Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L8.016 Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L8.016 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L8.016 Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L8.016 Benzyl alcohol 100-51-6 625.1 ND 1ug/L2032 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L8.016 Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L8.016 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L8.016 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L8.016 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L8.016 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L8.016 2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L8.016 2-Chlorophenol 95-57-8 625.1 ND 1ug/L8.016 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L8.016 Chrysene 218-01-9 625.1 ND 1ug/L8.016 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L8.016 Dibenzofuran 132-64-9 625.1 ND 1ug/L1016 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L8.080 2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L8.016 Diethylphthalate 84-66-2 625.1 ND 1ug/L8.016 Dimethyl phthalate 131-11-3 625.1 ND 1ug/L8.016 2,4-Dimethylphenol 105-67-9 625.1 97 1ug/L8.016 Di-n-butyl phthalate 84-74-2 625.1 ND 1ug/L8.116 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L8.080 2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L8.080 Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L8.016 1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L8.016 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 1ug/L4080 Fluoranthene 206-44-0 625.1 ND 1ug/L8.016 Fluorene 86-73-7 625.1 ND 1ug/L8.016 Hexachlorobenzene 118-74-1 625.1 ND 1ug/L8.016 Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L8.016 Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L4080 Hexachloroethane 67-72-1 625.1 ND 1ug/L8.016 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L8.016 Isophorone 78-59-1 625.1 ND 1ug/L8.016 1-Methylnaphthalene 90-12-0 625.1 97 1ug/L4.016 2-Methylnaphthalene 91-57-6 625.1 170 1ug/L4.016 2-Methylphenol 95-48-7 625.1 ND 1ug/L6.716 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 20 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2103 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 3+4-Methylphenol 106-44-5 625.1 ND 1ug/L1516 Naphthalene 91-20-3 625.1 410 1ug/L8.016 Nitrobenzene 98-95-3 625.1 ND 1ug/L8.016 2-Nitrophenol 88-75-5 625.1 ND 1ug/L8.032 4-Nitrophenol 100-02-7 625.1 ND 1ug/L4080 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L8.016 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L8.016 Pentachlorophenol 87-86-5 625.1 ND 1ug/L4080 Phenanthrene 85-01-8 625.1 ND 1ug/L8.016 Phenol 108-95-2 625.1 ND 1ug/L8.016 Pyrene 129-00-0 625.1 ND 1ug/L8.016 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L8.016 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L8.016 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 92 37-129 2-Fluorophenol 62 24-127 Nitrobenzene-d5 100 38-127 Phenol-d5 92 28-128 Terphenyl-d14 110 10-148 2,4,6-Tribromophenol 79 41-144 EDB & DBCP by Microextraction Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 504.1 504.1 1 06/11/2020 1443 JJG 06/11/2020 0930 56595 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,2-Dibromoethane (EDB)106-93-4 504.1 ND 1ug/L0.00390.0097 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,1,1,2-Tetrachloroethane 85 57-137 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0610 JJG 06/14/2020 1533 56890 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 1500 1ug/L100100 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 21 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl (aromatic)69 40-140 2-Fluorobiphenyl (fractionation 1)107 40-140 2-Bromonaphthalene (fractionation 2)102 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0042 JJG 06/14/2020 1535 56889 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 130 1ug/L100100 C19 - C36 Aliphatics MADEP-EPH-04 ND 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)45 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 50 06/12/2020 0013 STM 56710 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-1600 J 1ug/L7503800 C9 - C12 Aliphatics MADEP-VPH-18-16000 1ug/L7503800 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)109 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 50 06/12/2020 0013 STM 56711 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-10000 1ug/L2501300 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)106 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 22 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-2 VF09036-002 06/08/2020 1130 06/09/2020 Aqueous ICP-AES Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010D 1 06/17/2020 0348 KSH2 06/13/2020 1626 56859 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Lead 7439-92-1 6010D 0.0068 J 1mg/L0.00470.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 23 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 50 06/11/2020 1545 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 SM 6200B-2011 ND 1ug/L200500 Benzene 71-43-2 SM 6200B-2011 300 1ug/L2025 Bromobenzene 108-86-1 SM 6200B-2011 ND 1ug/L2025 Bromochloromethane 74-97-5 SM 6200B-2011 ND 1ug/L2025 Bromodichloromethane 75-27-4 SM 6200B-2011 ND 1ug/L2025 Bromoform 75-25-2 SM 6200B-2011 ND 1ug/L2025 Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 1ug/L2025 2-Butanone (MEK)78-93-3 SM 6200B-2011 ND 1ug/L100500 n-Butylbenzene 104-51-8 SM 6200B-2011 ND 1ug/L2025 sec-Butylbenzene 135-98-8 SM 6200B-2011 27 1ug/L2025 tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 1ug/L2025 Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 1ug/L2025 Chlorobenzene 108-90-7 SM 6200B-2011 ND 1ug/L2025 Chloroethane 75-00-3 SM 6200B-2011 ND 1ug/L2025 Chloroform 67-66-3 SM 6200B-2011 ND 1ug/L2025 Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 ND 1ug/L2025 2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 1ug/L2025 4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 1ug/L2025 Dibromochloromethane 124-48-1 SM 6200B-2011 ND 1ug/L2025 1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 1ug/L2025 Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 1ug/L2025 1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 1ug/L2025 1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 1ug/L2025 1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 1ug/L2025 Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 1ug/L2025 1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 1ug/L2025 1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 1ug/L2025 1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 1ug/L2025 cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 1ug/L2025 trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 1ug/L2025 1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 1ug/L2025 1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 1ug/L2025 2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 1ug/L2025 1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 1ug/L2025 cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 1ug/L2025 trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 1ug/L2025 Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 ND 1ug/L2025 Ethylbenzene 100-41-4 SM 6200B-2011 5600 1ug/L2025 Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 1ug/L2025 2-Hexanone 591-78-6 SM 6200B-2011 ND 1ug/L100500 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 24 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 50 06/11/2020 1545 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 190 1ug/L2025 p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 ND 1ug/L2025 Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 ND 1ug/L2025 4-Methyl-2-pentanone 108-10-1 SM 6200B-2011 ND 1ug/L100500 Methylene chloride 75-09-2 SM 6200B-2011 ND 1ug/L2025 Naphthalene 91-20-3 SM 6200B-2011 1400 1ug/L2025 n-Propylbenzene 103-65-1 SM 6200B-2011 570 1ug/L2025 Styrene 100-42-5 SM 6200B-2011 ND 1ug/L2025 1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 1ug/L2025 1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 1ug/L2025 Tetrachloroethene 127-18-4 SM 6200B-2011 ND 1ug/L2025 Toluene 108-88-3 SM 6200B-2011 1100 1ug/L2025 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 1ug/L2025 1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 1ug/L2025 1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 1ug/L2025 1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 1ug/L2025 1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 1ug/L2025 Trichloroethene 79-01-6 SM 6200B-2011 ND 1ug/L2025 Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 1ug/L2025 1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 1ug/L2025 1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 1000 1ug/L2025 1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 4300 1ug/L2025 Vinyl chloride 75-01-4 SM 6200B-2011 ND 1ug/L2025 m+p - Xylenes 179601-23-1 SM 6200B-2011 6000 1ug/L2025 o - Xylenes 95-47-6 SM 6200B-2011 7300 1ug/L2025 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 94 70-130 Bromofluorobenzene 95 70-130 Toluene-d8 94 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2128 JCG 06/10/2020 1759 56546 2 625.1 625.1 20 06/17/2020 1847 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 625.1 ND 1ug/L8.016 Acenaphthylene 208-96-8 625.1 ND 1ug/L8.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 25 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2128 JCG 06/10/2020 1759 56546 2 625.1 625.1 20 06/17/2020 1847 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Anthracene 120-12-7 625.1 ND 1ug/L8.016 Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L8.016 Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L8.016 Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L8.016 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L8.016 Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L8.016 Benzyl alcohol 100-51-6 625.1 ND 1ug/L2032 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L8.016 Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L8.016 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L8.016 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L8.016 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L8.016 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L8.016 2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L8.016 2-Chlorophenol 95-57-8 625.1 ND 1ug/L8.016 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L8.016 Chrysene 218-01-9 625.1 ND 1ug/L8.016 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L8.016 Dibenzofuran 132-64-9 625.1 ND 1ug/L1016 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L8.080 2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L8.016 Diethylphthalate 84-66-2 625.1 ND 1ug/L8.016 Dimethyl phthalate 131-11-3 625.1 ND 1ug/L8.016 2,4-Dimethylphenol 105-67-9 625.1 40 1ug/L8.016 Di-n-butyl phthalate 84-74-2 625.1 ND 1ug/L8.116 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L8.080 2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L8.080 Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L8.016 1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L8.016 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 1ug/L4080 Fluoranthene 206-44-0 625.1 ND 1ug/L8.016 Fluorene 86-73-7 625.1 ND 1ug/L8.016 Hexachlorobenzene 118-74-1 625.1 ND 1ug/L8.016 Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L8.016 Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L4080 Hexachloroethane 67-72-1 625.1 ND 1ug/L8.016 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L8.016 Isophorone 78-59-1 625.1 ND 1ug/L8.016 1-Methylnaphthalene 90-12-0 625.1 140 1ug/L4.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 26 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2128 JCG 06/10/2020 1759 56546 2 625.1 625.1 20 06/17/2020 1847 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 2-Methylnaphthalene 91-57-6 625.1 260 1ug/L4.016 2-Methylphenol 95-48-7 625.1 ND 1ug/L6.716 3+4-Methylphenol 106-44-5 625.1 ND 1ug/L1516 Naphthalene 91-20-3 625.1 800 2ug/L1632 Nitrobenzene 98-95-3 625.1 ND 1ug/L8.016 2-Nitrophenol 88-75-5 625.1 ND 1ug/L8.032 4-Nitrophenol 100-02-7 625.1 ND 1ug/L4080 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L8.016 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L8.016 Pentachlorophenol 87-86-5 625.1 ND 1ug/L4080 Phenanthrene 85-01-8 625.1 ND 1ug/L8.016 Phenol 108-95-2 625.1 ND 1ug/L8.016 Pyrene 129-00-0 625.1 ND 1ug/L8.016 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L8.016 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L8.016 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ 2-Fluorobiphenyl 92 37-129 81 37-129 2-Fluorophenol 70 24-127 50 24-127 Nitrobenzene-d5 99 38-127 82 38-127 Phenol-d5 85 28-128 78 28-128 Terphenyl-d14 111 10-148 88 10-148 2,4,6-Tribromophenol 80 41-144 67 41-144 EDB & DBCP by Microextraction Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 504.1 504.1 1 06/11/2020 1455 JJG 06/11/2020 0930 56595 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,2-Dibromoethane (EDB)106-93-4 504.1 0.013 1ug/L0.00390.0096 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,1,1,2-Tetrachloroethane 109 57-137 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 27 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0640 JJG 06/14/2020 1533 56890 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 1700 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl (aromatic)80 40-140 2-Fluorobiphenyl (fractionation 1)99 40-140 2-Bromonaphthalene (fractionation 2)92 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0112 JJG 06/14/2020 1535 56889 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1ug/L100100 C19 - C36 Aliphatics MADEP-EPH-04 ND 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)43 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 100 06/12/2020 0041 STM 56710 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-3300 J 1ug/L15007500 C9 - C12 Aliphatics MADEP-VPH-18-25000 1ug/L15007500 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)96 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 100 06/12/2020 0041 STM 56711 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-18000 1ug/L5002500 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 28 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-4 VF09036-003 06/08/2020 1400 06/09/2020 Aqueous AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)96 70-130 ICP-AES Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010D 1 06/17/2020 0405 KSH2 06/13/2020 1626 56859 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Lead 7439-92-1 6010D 0.014 1mg/L0.00470.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 29 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 20 06/11/2020 1411 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 SM 6200B-2011 ND 1ug/L80200 Benzene 71-43-2 SM 6200B-2011 130 1ug/L8.010 Bromobenzene 108-86-1 SM 6200B-2011 ND 1ug/L8.010 Bromochloromethane 74-97-5 SM 6200B-2011 ND 1ug/L8.010 Bromodichloromethane 75-27-4 SM 6200B-2011 ND 1ug/L8.010 Bromoform 75-25-2 SM 6200B-2011 ND 1ug/L8.010 Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 1ug/L8.010 2-Butanone (MEK)78-93-3 SM 6200B-2011 ND 1ug/L40200 n-Butylbenzene 104-51-8 SM 6200B-2011 130 1ug/L8.010 sec-Butylbenzene 135-98-8 SM 6200B-2011 37 1ug/L8.010 tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 1ug/L8.010 Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 1ug/L8.010 Chlorobenzene 108-90-7 SM 6200B-2011 ND 1ug/L8.010 Chloroethane 75-00-3 SM 6200B-2011 ND 1ug/L8.010 Chloroform 67-66-3 SM 6200B-2011 ND 1ug/L8.010 Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 ND 1ug/L8.010 2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 1ug/L8.010 4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 1ug/L8.010 Dibromochloromethane 124-48-1 SM 6200B-2011 ND 1ug/L8.010 1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 1ug/L8.010 Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 1ug/L8.010 1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 1ug/L8.010 1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 1ug/L8.010 Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 1ug/L8.010 cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 1ug/L8.010 trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 1ug/L8.010 1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 1ug/L8.010 1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 1ug/L8.010 2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 1ug/L8.010 1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 1ug/L8.010 cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 1ug/L8.010 trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 1ug/L8.010 Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 11 1ug/L8.010 Ethylbenzene 100-41-4 SM 6200B-2011 3000 1ug/L8.010 Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 1ug/L8.010 2-Hexanone 591-78-6 SM 6200B-2011 ND 1ug/L40200 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 30 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 6200B-SM 6200B-2011 20 06/11/2020 1411 TML 56611 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 150 1ug/L8.010 p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 21 1ug/L8.010 Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 ND 1ug/L8.010 4-Methyl-2-pentanone 108-10-1 SM 6200B-2011 ND 1ug/L40200 Methylene chloride 75-09-2 SM 6200B-2011 8.0 J 1ug/L8.010 Naphthalene 91-20-3 SM 6200B-2011 760 1ug/L8.010 n-Propylbenzene 103-65-1 SM 6200B-2011 510 1ug/L8.010 Styrene 100-42-5 SM 6200B-2011 ND 1ug/L8.010 1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 1ug/L8.010 1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 1ug/L8.010 Tetrachloroethene 127-18-4 SM 6200B-2011 ND 1ug/L8.010 Toluene 108-88-3 SM 6200B-2011 220 1ug/L8.010 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 1ug/L8.010 1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 1ug/L8.010 1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 1ug/L8.010 1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 1ug/L8.010 1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 1ug/L8.010 Trichloroethene 79-01-6 SM 6200B-2011 ND 1ug/L8.010 Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 1ug/L8.010 1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 1ug/L8.010 1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 580 1ug/L8.010 1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 1700 1ug/L8.010 Vinyl chloride 75-01-4 SM 6200B-2011 ND 1ug/L8.010 m+p - Xylenes 179601-23-1 SM 6200B-2011 1700 1ug/L8.010 o - Xylenes 95-47-6 SM 6200B-2011 2500 1ug/L8.010 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 103 70-130 Bromofluorobenzene 105 70-130 Toluene-d8 105 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2152 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 625.1 ND 1ug/L8.016 Acenaphthylene 208-96-8 625.1 ND 1ug/L8.016 Anthracene 120-12-7 625.1 ND 1ug/L8.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 31 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2152 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L8.016 Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L8.016 Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L8.016 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L8.016 Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L8.016 Benzyl alcohol 100-51-6 625.1 ND 1ug/L2032 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L8.016 Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L8.016 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L8.016 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L8.016 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L8.016 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L8.016 2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L8.016 2-Chlorophenol 95-57-8 625.1 ND 1ug/L8.016 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L8.016 Chrysene 218-01-9 625.1 ND 1ug/L8.016 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L8.016 Dibenzofuran 132-64-9 625.1 ND 1ug/L1016 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L8.080 2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L8.016 Diethylphthalate 84-66-2 625.1 ND 1ug/L8.016 Dimethyl phthalate 131-11-3 625.1 ND 1ug/L8.016 2,4-Dimethylphenol 105-67-9 625.1 61 1ug/L8.016 Di-n-butyl phthalate 84-74-2 625.1 ND 1ug/L8.116 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L8.080 2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L8.080 Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L8.016 1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L8.016 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 1ug/L4080 Fluoranthene 206-44-0 625.1 ND 1ug/L8.016 Fluorene 86-73-7 625.1 ND 1ug/L8.016 Hexachlorobenzene 118-74-1 625.1 ND 1ug/L8.016 Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L8.016 Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L4080 Hexachloroethane 67-72-1 625.1 ND 1ug/L8.016 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L8.016 Isophorone 78-59-1 625.1 ND 1ug/L8.016 1-Methylnaphthalene 90-12-0 625.1 120 1ug/L4.016 2-Methylnaphthalene 91-57-6 625.1 210 1ug/L4.016 2-Methylphenol 95-48-7 625.1 ND 1ug/L6.716 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 32 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 06/16/2020 2152 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 3+4-Methylphenol 106-44-5 625.1 ND 1ug/L1516 Naphthalene 91-20-3 625.1 420 1ug/L8.016 Nitrobenzene 98-95-3 625.1 ND 1ug/L8.016 2-Nitrophenol 88-75-5 625.1 ND 1ug/L8.032 4-Nitrophenol 100-02-7 625.1 ND 1ug/L4080 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L8.016 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L8.016 Pentachlorophenol 87-86-5 625.1 ND 1ug/L4080 Phenanthrene 85-01-8 625.1 ND 1ug/L8.016 Phenol 108-95-2 625.1 9.9 J 1ug/L8.016 Pyrene 129-00-0 625.1 ND 1ug/L8.016 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L8.016 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L8.016 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 97 37-129 2-Fluorophenol 58 24-127 Nitrobenzene-d5 95 38-127 Phenol-d5 92 28-128 Terphenyl-d14 110 10-148 2,4,6-Tribromophenol 79 41-144 EDB & DBCP by Microextraction Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 504.1 504.1 1 06/11/2020 1507 JJG 06/11/2020 0930 56595 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,2-Dibromoethane (EDB)106-93-4 504.1 ND 1ug/L0.00390.0097 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,1,1,2-Tetrachloroethane 120 57-137 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0710 JJG 06/14/2020 1533 56890 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 1200 1ug/L100100 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 33 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl (aromatic)77 40-140 2-Fluorobiphenyl (fractionation 1)106 40-140 2-Bromonaphthalene (fractionation 2)106 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0142 JJG 06/14/2020 1535 56889 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 110 1ug/L100100 C19 - C36 Aliphatics MADEP-EPH-04 ND 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)48 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 50 06/12/2020 0110 STM 56710 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-4400 1ug/L7503800 C9 - C12 Aliphatics MADEP-VPH-18-12000 1ug/L7503800 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)96 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 50 06/12/2020 0110 STM 56711 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-8200 1ug/L2501300 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)93 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 34 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-5 VF09036-004 06/08/2020 1430 06/09/2020 Aqueous ICP-AES Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010D 1 06/17/2020 0410 KSH2 06/13/2020 1626 56859 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Lead 7439-92-1 6010D 0.013 1mg/L0.00470.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 35 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 6200B-SM 6200B-2011 1 06/16/2020 1100 TML 57073 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 SM 6200B-2011 5.7 J 2ug/L4.010 Benzene 71-43-2 SM 6200B-2011 ND 2ug/L0.400.50 Bromobenzene 108-86-1 SM 6200B-2011 ND 2ug/L0.400.50 Bromochloromethane 74-97-5 SM 6200B-2011 ND 2ug/L0.400.50 Bromodichloromethane 75-27-4 SM 6200B-2011 ND 2ug/L0.400.50 Bromoform 75-25-2 SM 6200B-2011 ND 2ug/L0.400.50 Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 2ug/L0.400.50 2-Butanone (MEK)78-93-3 SM 6200B-2011 ND 2ug/L2.010 n-Butylbenzene 104-51-8 SM 6200B-2011 4.0 2ug/L0.400.50 sec-Butylbenzene 135-98-8 SM 6200B-2011 0.84 2ug/L0.400.50 tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 2ug/L0.400.50 Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 2ug/L0.400.50 Chlorobenzene 108-90-7 SM 6200B-2011 ND 2ug/L0.400.50 Chloroethane 75-00-3 SM 6200B-2011 ND 2ug/L0.400.50 Chloroform 67-66-3 SM 6200B-2011 ND 2ug/L0.400.50 Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 ND 2ug/L0.400.50 2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 2ug/L0.400.50 4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 2ug/L0.400.50 Dibromochloromethane 124-48-1 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 2ug/L0.400.50 Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 2ug/L0.400.50 1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 2ug/L0.400.50 1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 2ug/L0.400.50 Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 2ug/L0.400.50 cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 2ug/L0.400.50 trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 2ug/L0.400.50 1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 2ug/L0.400.50 1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 2ug/L0.400.50 2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 2ug/L0.400.50 1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 2ug/L0.400.50 cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 2ug/L0.400.50 trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 2ug/L0.400.50 Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 17 2ug/L0.400.50 Ethylbenzene 100-41-4 SM 6200B-2011 6.7 2ug/L0.400.50 Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 2ug/L0.400.50 2-Hexanone 591-78-6 SM 6200B-2011 ND 2ug/L2.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 36 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 6200B-SM 6200B-2011 1 06/16/2020 1100 TML 57073 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 1.2 2ug/L0.400.50 p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 0.53 2ug/L0.400.50 Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 3.2 2ug/L0.400.50 4-Methyl-2-pentanone 108-10-1 SM 6200B-2011 ND 2ug/L2.010 Methylene chloride 75-09-2 SM 6200B-2011 ND 2ug/L0.400.50 Naphthalene 91-20-3 SM 6200B-2011 5.1 2ug/L0.400.50 n-Propylbenzene 103-65-1 SM 6200B-2011 4.8 2ug/L0.400.50 Styrene 100-42-5 SM 6200B-2011 ND 2ug/L0.400.50 1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 2ug/L0.400.50 Tetrachloroethene 127-18-4 SM 6200B-2011 ND 2ug/L0.400.50 Toluene 108-88-3 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 2ug/L0.400.50 1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 2ug/L0.400.50 1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 2ug/L0.400.50 1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 2ug/L0.400.50 1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 2ug/L0.400.50 Trichloroethene 79-01-6 SM 6200B-2011 ND 2ug/L0.400.50 Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 2ug/L0.400.50 1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 2ug/L0.400.50 1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 6.5 2ug/L0.400.50 1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 22 2ug/L0.400.50 Vinyl chloride 75-01-4 SM 6200B-2011 ND 2ug/L0.400.50 m+p - Xylenes 179601-23-1 SM 6200B-2011 6.1 2ug/L0.400.50 o - Xylenes 95-47-6 SM 6200B-2011 6.4 2ug/L0.400.50 AcceptanceRun 2 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 99 70-130 Bromofluorobenzene 98 70-130 Toluene-d8 99 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2217 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 625.1 ND 1ug/L1.63.2 Acenaphthylene 208-96-8 625.1 ND 1ug/L1.63.2 Anthracene 120-12-7 625.1 ND 1ug/L1.63.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 37 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2217 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L1.63.2 Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L1.63.2 Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L1.63.2 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L1.63.2 Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L1.63.2 Benzyl alcohol 100-51-6 625.1 ND 1ug/L4.06.4 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L1.63.2 Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L1.63.2 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L1.63.2 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L1.63.2 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L1.63.2 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L1.63.2 2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L1.63.2 2-Chlorophenol 95-57-8 625.1 ND 1ug/L1.63.2 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L1.63.2 Chrysene 218-01-9 625.1 ND 1ug/L1.63.2 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L1.63.2 Dibenzofuran 132-64-9 625.1 ND 1ug/L2.03.2 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L1.616 2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L1.63.2 Diethylphthalate 84-66-2 625.1 17 B 1ug/L1.63.2 Dimethyl phthalate 131-11-3 625.1 2.2 J 1ug/L1.63.2 2,4-Dimethylphenol 105-67-9 625.1 ND 1ug/L1.63.2 Di-n-butyl phthalate 84-74-2 625.1 24 B 1ug/L1.63.2 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L1.616 2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L1.616 Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L1.63.2 1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L1.63.2 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 1ug/L8.016 Fluoranthene 206-44-0 625.1 ND 1ug/L1.63.2 Fluorene 86-73-7 625.1 ND 1ug/L1.63.2 Hexachlorobenzene 118-74-1 625.1 ND 1ug/L1.63.2 Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L1.63.2 Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L8.016 Hexachloroethane 67-72-1 625.1 ND 1ug/L1.63.2 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L1.63.2 Isophorone 78-59-1 625.1 ND 1ug/L1.63.2 1-Methylnaphthalene 90-12-0 625.1 2.3 J 1ug/L0.803.2 2-Methylnaphthalene 91-57-6 625.1 4.2 1ug/L0.803.2 2-Methylphenol 95-48-7 625.1 ND 1ug/L1.33.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 38 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 06/16/2020 2217 JCG 06/10/2020 1759 56546 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 3+4-Methylphenol 106-44-5 625.1 ND 1ug/L3.03.2 Naphthalene 91-20-3 625.1 5.4 1ug/L1.63.2 Nitrobenzene 98-95-3 625.1 ND 1ug/L1.63.2 2-Nitrophenol 88-75-5 625.1 ND 1ug/L1.66.4 4-Nitrophenol 100-02-7 625.1 ND 1ug/L8.016 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L1.63.2 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L1.63.2 Pentachlorophenol 87-86-5 625.1 ND 1ug/L8.016 Phenanthrene 85-01-8 625.1 ND 1ug/L1.63.2 Phenol 108-95-2 625.1 2.3 J 1ug/L1.63.2 Pyrene 129-00-0 625.1 ND 1ug/L1.63.2 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L1.63.2 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L1.63.2 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 94 37-129 2-Fluorophenol 50 24-127 Nitrobenzene-d5 91 38-127 Phenol-d5 79 28-128 Terphenyl-d14 104 10-148 2,4,6-Tribromophenol 88 41-144 EDB & DBCP by Microextraction Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 504.1 504.1 1 06/11/2020 1520 JJG 06/11/2020 0930 56595 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,2-Dibromoethane (EDB)106-93-4 504.1 ND 1ug/L0.00390.0099 AcceptanceRun 1 Surrogate Q % Recovery Limits 1,1,1,2-Tetrachloroethane 78 57-137 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0740 JJG 06/14/2020 1533 56890 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 120 1ug/L100100 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 39 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl (aromatic)87 40-140 2-Fluorobiphenyl (fractionation 1)99 40-140 2-Bromonaphthalene (fractionation 2)135 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/24/2020 0212 JJG 06/14/2020 1535 56889 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1ug/L100100 C19 - C36 Aliphatics MADEP-EPH-04 ND 1ug/L100100 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)43 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/12/2020 0139 STM 56710 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-22 J 1ug/L1575 C9 - C12 Aliphatics MADEP-VPH-18-91 1ug/L1575 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)100 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/12/2020 0139 STM 56711 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-160 1ug/L5.025 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)98 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 40 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. TMW-6 VF09036-005 06/08/2020 1545 06/09/2020 Aqueous ICP-AES Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3005A 6010D 1 06/17/2020 0416 KSH2 06/13/2020 1626 56859 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Lead 7439-92-1 6010D 0.013 1mg/L0.00470.010 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 41 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-1 VF09036-006 06/08/2020 1115 06/09/2020 Solid % Solids:89.4 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1127 JM1 56477 5.49 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg8.120 Benzene 71-43-2 8260D ND 1ug/kg2.05.1 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.05.1 Bromoform 75-25-2 8260D ND 1ug/kg2.05.1 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.15.1 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.120 Carbon disulfide 75-15-0 8260D ND 1ug/kg2.05.1 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.05.1 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.05.1 Chloroethane 75-00-3 8260D ND 1ug/kg2.05.1 Chloroform 67-66-3 8260D ND 1ug/kg2.05.1 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.15.1 Cyclohexane 110-82-7 8260D ND 1ug/kg2.05.1 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.05.1 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.05.1 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.05.1 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.05.1 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.05.1 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.05.1 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.15.1 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.05.1 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.05.1 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.05.1 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.05.1 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.05.1 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.05.1 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.05.1 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.05.1 Ethylbenzene 100-41-4 8260D ND 1ug/kg2.05.1 2-Hexanone 591-78-6 8260D ND 1ug/kg4.110 Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.05.1 Methyl acetate 79-20-9 8260D ND 1ug/kg2.05.1 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.05.1 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.110 Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.05.1 Methylene chloride 75-09-2 8260D ND 1ug/kg2.05.1 Styrene 100-42-5 8260D ND 1ug/kg2.05.1 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.05.1 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.05.1 Toluene 108-88-3 8260D ND 1ug/kg2.05.1 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 42 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-1 VF09036-006 06/08/2020 1115 06/09/2020 Solid % Solids:89.4 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1127 JM1 56477 5.49 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.05.1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.05.1 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.05.1 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.05.1 Trichloroethene 79-01-6 8260D ND 1ug/kg2.05.1 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.05.1 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.15.1 Xylenes (total)1330-20-7 8260D ND 1ug/kg4.110 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 99 47-138 1,2-Dichloroethane-d4 89 53-142 Toluene-d8 94 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1634 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.902.9 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.02.9 Acetophenone 98-86-2 8270E ND 1ug/kg5.414 Anthracene 120-12-7 8270E ND 1ug/kg0.562.9 Atrazine 1912-24-9 8270E ND 1ug/kg5.414 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.414 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.642.9 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.722.9 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.542.9 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.712.9 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.522.9 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.414 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.414 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.414 Caprolactam 105-60-2 8270E ND 1ug/kg5.414 Carbazole 86-74-8 8270E ND 1ug/kg5.414 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.414 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.414 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.414 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.414 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 43 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-1 VF09036-006 06/08/2020 1115 06/09/2020 Solid % Solids:89.4 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1634 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.414 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.414 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.414 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.414 Chrysene 218-01-9 8270E ND 1ug/kg0.492.9 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.562.9 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.414 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.414 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.414 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.414 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.114 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.414 Di-n-butyl phthalate 84-74-2 8270E 6.5 BJ 1ug/kg5.414 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2773 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2773 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1129 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1129 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.414 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2773 Fluoranthene 206-44-0 8270E ND 1ug/kg0.462.9 Fluorene 86-73-7 8270E ND 1ug/kg0.622.9 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.414 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.414 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2773 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.414 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.12.9 Isophorone 78-59-1 8270E ND 1ug/kg5.414 2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1.12.9 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.414 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1129 Naphthalene 91-20-3 8270E ND 1ug/kg1.12.9 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1129 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1129 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1129 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.414 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1129 4-Nitrophenol 100-02-7 8270E ND 1ug/kg2773 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.414 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.414 Pentachlorophenol 87-86-5 8270E ND 1ug/kg2773 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 44 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-1 VF09036-006 06/08/2020 1115 06/09/2020 Solid % Solids:89.4 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1634 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E ND 1ug/kg0.782.9 Phenol 108-95-2 8270E ND 1ug/kg5.414 Pyrene 129-00-0 8270E ND 1ug/kg0.542.9 Pyridine 110-86-1 8270E ND 1ug/kg5.414 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.414 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.414 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 80 33-102 2-Fluorophenol 83 35-115 Nitrobenzene-d5 76 22-109 Phenol-d5 94 33-122 Terphenyl-d14 96 41-120 2,4,6-Tribromophenol 80 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0000 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1111 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)84 40-140 2-Fluorobiphenyl (fractionation 1)87 40-140 o - Terphenyl (aromatic)74 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1534 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)66 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 45 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-1 VF09036-006 06/08/2020 1115 06/09/2020 Solid % Solids:89.4 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1150 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg0.884.4 C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg0.884.4 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)97 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1150 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-ND 1mg/kg0.591.5 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 46 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-2 VF09036-007 06/08/2020 0940 06/09/2020 Solid % Solids:92.4 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1222 JM1 56477 5.25 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 22 1ug/kg8.221 Benzene 71-43-2 8260D ND 1ug/kg2.15.2 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.15.2 Bromoform 75-25-2 8260D ND 1ug/kg2.15.2 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.15.2 2-Butanone (MEK)78-93-3 8260D 4.6 J 1ug/kg4.121 Carbon disulfide 75-15-0 8260D 4.3 J 1ug/kg2.15.2 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.15.2 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.15.2 Chloroethane 75-00-3 8260D ND 1ug/kg2.15.2 Chloroform 67-66-3 8260D ND 1ug/kg2.15.2 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.15.2 Cyclohexane 110-82-7 8260D ND 1ug/kg2.15.2 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.15.2 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.15.2 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.15.2 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.15.2 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.15.2 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.15.2 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.15.2 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.15.2 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.15.2 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.15.2 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.15.2 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.15.2 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.15.2 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.15.2 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.15.2 Ethylbenzene 100-41-4 8260D 77 1ug/kg2.15.2 2-Hexanone 591-78-6 8260D ND 1ug/kg4.110 Isopropylbenzene 98-82-8 8260D 26 1ug/kg2.15.2 Methyl acetate 79-20-9 8260D ND 1ug/kg2.15.2 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.15.2 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.110 Methylcyclohexane 108-87-2 8260D 110 1ug/kg2.15.2 Methylene chloride 75-09-2 8260D ND 1ug/kg2.15.2 Styrene 100-42-5 8260D ND 1ug/kg2.15.2 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.15.2 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.15.2 Toluene 108-88-3 8260D ND 1ug/kg2.15.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 47 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-2 VF09036-007 06/08/2020 0940 06/09/2020 Solid % Solids:92.4 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1222 JM1 56477 5.25 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.15.2 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.15.2 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.15.2 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.15.2 Trichloroethene 79-01-6 8260D ND 1ug/kg2.15.2 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.15.2 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.15.2 Xylenes (total)1330-20-7 8260D 120 1ug/kg4.110 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 97 47-138 1,2-Dichloroethane-d4 86 53-142 Toluene-d8 106 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1836 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.872.8 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.02.8 Acetophenone 98-86-2 8270E ND 1ug/kg5.314 Anthracene 120-12-7 8270E 2.4 J 1ug/kg0.542.8 Atrazine 1912-24-9 8270E ND 1ug/kg5.314 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.314 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.622.8 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.702.8 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.532.8 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.692.8 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.512.8 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.314 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.314 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.314 Caprolactam 105-60-2 8270E ND 1ug/kg5.314 Carbazole 86-74-8 8270E ND 1ug/kg5.314 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.314 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.314 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.314 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.314 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 48 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-2 VF09036-007 06/08/2020 0940 06/09/2020 Solid % Solids:92.4 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1836 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.314 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.314 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.314 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.314 Chrysene 218-01-9 8270E ND 1ug/kg0.472.8 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.542.8 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.314 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.314 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.314 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.314 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg7.814 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.314 Di-n-butyl phthalate 84-74-2 8270E 6.4 BJ 1ug/kg5.314 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2671 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2671 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1128 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1128 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.314 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2671 Fluoranthene 206-44-0 8270E ND 1ug/kg0.442.8 Fluorene 86-73-7 8270E 1.5 J 1ug/kg0.602.8 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.314 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.314 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2671 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.314 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.12.8 Isophorone 78-59-1 8270E ND 1ug/kg5.314 2-Methylnaphthalene 91-57-6 8270E 23 1ug/kg1.02.8 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.314 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1128 Naphthalene 91-20-3 8270E 6.8 1ug/kg1.02.8 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1128 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1128 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1128 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.314 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1128 4-Nitrophenol 100-02-7 8270E ND 1ug/kg2671 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.314 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.314 Pentachlorophenol 87-86-5 8270E ND 1ug/kg2671 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 49 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-2 VF09036-007 06/08/2020 0940 06/09/2020 Solid % Solids:92.4 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1836 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 4.8 1ug/kg0.762.8 Phenol 108-95-2 8270E ND 1ug/kg5.314 Pyrene 129-00-0 8270E 2.5 J 1ug/kg0.532.8 Pyridine 110-86-1 8270E ND 1ug/kg5.314 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.314 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.314 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 81 33-102 2-Fluorophenol 87 35-115 Nitrobenzene-d5 78 22-109 Phenol-d5 94 33-122 Terphenyl-d14 100 41-120 2,4,6-Tribromophenol 86 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0030 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)80 40-140 2-Fluorobiphenyl (fractionation 1)83 40-140 o - Terphenyl (aromatic)73 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1604 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)72 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 50 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-2 VF09036-007 06/08/2020 0940 06/09/2020 Solid % Solids:92.4 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1219 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-9.2 1mg/kg0.814.1 C9 - C12 Aliphatics MADEP-VPH-18-5.0 1mg/kg0.814.1 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)93 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1219 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-5.9 1mg/kg0.541.4 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 51 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-3 VF09036-008 06/08/2020 1150 06/09/2020 Solid % Solids:78.1 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1245 JM1 56477 6.66 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 12 J 1ug/kg7.719 Benzene 71-43-2 8260D ND 1ug/kg1.94.8 Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.94.8 Bromoform 75-25-2 8260D ND 1ug/kg1.94.8 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.94.8 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.819 Carbon disulfide 75-15-0 8260D ND 1ug/kg1.94.8 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.94.8 Chlorobenzene 108-90-7 8260D ND 1ug/kg1.94.8 Chloroethane 75-00-3 8260D ND 1ug/kg1.94.8 Chloroform 67-66-3 8260D ND 1ug/kg1.94.8 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.94.8 Cyclohexane 110-82-7 8260D ND 1ug/kg1.94.8 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.94.8 Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.94.8 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.94.8 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.94.8 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.94.8 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.94.8 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.94.8 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.94.8 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.94.8 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.94.8 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.94.8 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.94.8 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.94.8 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.94.8 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.94.8 Ethylbenzene 100-41-4 8260D ND 1ug/kg1.94.8 2-Hexanone 591-78-6 8260D ND 1ug/kg3.89.6 Isopropylbenzene 98-82-8 8260D ND 1ug/kg1.94.8 Methyl acetate 79-20-9 8260D ND 1ug/kg1.94.8 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.94.8 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.89.6 Methylcyclohexane 108-87-2 8260D ND 1ug/kg1.94.8 Methylene chloride 75-09-2 8260D ND 1ug/kg1.94.8 Styrene 100-42-5 8260D ND 1ug/kg1.94.8 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.94.8 Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.94.8 Toluene 108-88-3 8260D ND 1ug/kg1.94.8 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 52 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-3 VF09036-008 06/08/2020 1150 06/09/2020 Solid % Solids:78.1 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1245 JM1 56477 6.66 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.94.8 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.94.8 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.94.8 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.94.8 Trichloroethene 79-01-6 8260D ND 1ug/kg1.94.8 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.94.8 Vinyl chloride 75-01-4 8260D ND 1ug/kg2.94.8 Xylenes (total)1330-20-7 8260D ND 1ug/kg3.89.6 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 96 47-138 1,2-Dichloroethane-d4 83 53-142 Toluene-d8 99 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1950 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg1.03.4 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.23.4 Acetophenone 98-86-2 8270E ND 1ug/kg6.216 Anthracene 120-12-7 8270E ND 1ug/kg0.643.4 Atrazine 1912-24-9 8270E ND 1ug/kg6.216 Benzaldehyde 100-52-7 8270E ND 1ug/kg6.216 Benzo(a)anthracene 56-55-3 8270E 5.7 1ug/kg0.743.4 Benzo(a)pyrene 50-32-8 8270E 6.2 1ug/kg0.823.4 Benzo(b)fluoranthene 205-99-2 8270E 9.3 1ug/kg0.623.4 Benzo(g,h,i)perylene 191-24-2 8270E 5.0 1ug/kg0.813.4 Benzo(k)fluoranthene 207-08-9 8270E 3.2 J 1ug/kg0.603.4 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg6.216 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg6.216 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg6.216 Caprolactam 105-60-2 8270E ND 1ug/kg6.216 Carbazole 86-74-8 8270E ND 1ug/kg6.216 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg6.216 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg6.216 4-Chloroaniline 106-47-8 8270E ND 1ug/kg6.216 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg6.216 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 53 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-3 VF09036-008 06/08/2020 1150 06/09/2020 Solid % Solids:78.1 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1950 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg6.216 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg6.216 2-Chlorophenol 95-57-8 8270E ND 1ug/kg6.216 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg6.216 Chrysene 218-01-9 8270E 6.6 1ug/kg0.563.4 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.643.4 Dibenzofuran 132-64-9 8270E ND 1ug/kg6.216 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg6.216 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg6.216 Diethylphthalate 84-66-2 8270E ND 1ug/kg6.216 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg9.216 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg6.216 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg6.216 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg3184 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg3184 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1234 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1234 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg6.216 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg3184 Fluoranthene 206-44-0 8270E 8.0 1ug/kg0.523.4 Fluorene 86-73-7 8270E ND 1ug/kg0.713.4 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg6.216 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg6.216 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg3184 Hexachloroethane 67-72-1 8270E ND 1ug/kg6.216 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 3.9 1ug/kg1.23.4 Isophorone 78-59-1 8270E ND 1ug/kg6.216 2-Methylnaphthalene 91-57-6 8270E 2.6 J 1ug/kg1.23.4 2-Methylphenol 95-48-7 8270E ND 1ug/kg6.216 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1234 Naphthalene 91-20-3 8270E 2.4 J 1ug/kg1.23.4 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1234 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1234 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1234 Nitrobenzene 98-95-3 8270E ND 1ug/kg6.216 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1234 4-Nitrophenol 100-02-7 8270E ND 1ug/kg3184 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg6.216 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg6.216 Pentachlorophenol 87-86-5 8270E ND 1ug/kg3184 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 54 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-3 VF09036-008 06/08/2020 1150 06/09/2020 Solid % Solids:78.1 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1950 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 3.3 J 1ug/kg0.903.4 Phenol 108-95-2 8270E ND 1ug/kg6.216 Pyrene 129-00-0 8270E 8.0 1ug/kg0.623.4 Pyridine 110-86-1 8270E ND 1ug/kg6.216 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg6.216 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg6.216 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 80 33-102 2-Fluorophenol 80 35-115 Nitrobenzene-d5 75 22-109 Phenol-d5 97 33-122 Terphenyl-d14 101 41-120 2,4,6-Tribromophenol 78 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0100 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)82 40-140 2-Fluorobiphenyl (fractionation 1)86 40-140 o - Terphenyl (aromatic)71 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1634 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)68 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 55 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-3 VF09036-008 06/08/2020 1150 06/09/2020 Solid % Solids:78.1 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1247 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.0 C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)107 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1247 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-ND 1mg/kg0.671.7 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)108 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 56 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-4 VF09036-009 06/08/2020 1320 06/09/2020 Solid % Solids:94.3 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1307 JM1 56477 5.72 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 12 J 1ug/kg7.419 Benzene 71-43-2 8260D ND 1ug/kg1.94.6 Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.94.6 Bromoform 75-25-2 8260D ND 1ug/kg1.94.6 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.84.6 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.719 Carbon disulfide 75-15-0 8260D ND 1ug/kg1.94.6 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.94.6 Chlorobenzene 108-90-7 8260D ND 1ug/kg1.94.6 Chloroethane 75-00-3 8260D ND 1ug/kg1.94.6 Chloroform 67-66-3 8260D ND 1ug/kg1.94.6 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.84.6 Cyclohexane 110-82-7 8260D ND 1ug/kg1.94.6 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.94.6 Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.94.6 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.94.6 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.94.6 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.94.6 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.94.6 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.84.6 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.94.6 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.94.6 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.94.6 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.94.6 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.94.6 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.94.6 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.94.6 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.94.6 Ethylbenzene 100-41-4 8260D 8.3 1ug/kg1.94.6 2-Hexanone 591-78-6 8260D ND 1ug/kg3.79.3 Isopropylbenzene 98-82-8 8260D 2.2 J 1ug/kg1.94.6 Methyl acetate 79-20-9 8260D ND 1ug/kg1.94.6 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.94.6 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.79.3 Methylcyclohexane 108-87-2 8260D 6.1 1ug/kg1.94.6 Methylene chloride 75-09-2 8260D ND 1ug/kg1.94.6 Styrene 100-42-5 8260D ND 1ug/kg1.94.6 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.94.6 Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.94.6 Toluene 108-88-3 8260D ND 1ug/kg1.94.6 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 57 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-4 VF09036-009 06/08/2020 1320 06/09/2020 Solid % Solids:94.3 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1307 JM1 56477 5.72 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.94.6 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.94.6 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.94.6 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.94.6 Trichloroethene 79-01-6 8260D ND 1ug/kg1.94.6 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.94.6 Vinyl chloride 75-01-4 8260D ND 1ug/kg2.84.6 Xylenes (total)1330-20-7 8260D 26 1ug/kg3.79.3 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 97 47-138 1,2-Dichloroethane-d4 87 53-142 Toluene-d8 95 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1659 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.872.8 Acenaphthylene 208-96-8 8270E ND 1ug/kg0.992.8 Acetophenone 98-86-2 8270E ND 1ug/kg5.214 Anthracene 120-12-7 8270E 2.4 J 1ug/kg0.532.8 Atrazine 1912-24-9 8270E ND 1ug/kg5.214 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.214 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.622.8 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.692.8 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.522.8 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.682.8 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.502.8 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.214 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.214 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.214 Caprolactam 105-60-2 8270E ND 1ug/kg5.214 Carbazole 86-74-8 8270E ND 1ug/kg5.214 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.214 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.214 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.214 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.214 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 58 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-4 VF09036-009 06/08/2020 1320 06/09/2020 Solid % Solids:94.3 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1659 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.214 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.214 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.214 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.214 Chrysene 218-01-9 8270E ND 1ug/kg0.472.8 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.532.8 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.214 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.214 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.214 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.214 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg7.714 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.214 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg5.214 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2670 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2670 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1028 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1028 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.214 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2670 Fluoranthene 206-44-0 8270E ND 1ug/kg0.442.8 Fluorene 86-73-7 8270E 2.0 J 1ug/kg0.602.8 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.214 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.214 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2670 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.214 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.02.8 Isophorone 78-59-1 8270E ND 1ug/kg5.214 2-Methylnaphthalene 91-57-6 8270E 37 1ug/kg1.02.8 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.214 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1028 Naphthalene 91-20-3 8270E 4.8 1ug/kg1.02.8 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1028 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1028 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1028 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.214 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1028 4-Nitrophenol 100-02-7 8270E ND 1ug/kg2670 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.214 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.214 Pentachlorophenol 87-86-5 8270E ND 1ug/kg2670 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 59 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-4 VF09036-009 06/08/2020 1320 06/09/2020 Solid % Solids:94.3 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1659 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 4.7 1ug/kg0.752.8 Phenol 108-95-2 8270E ND 1ug/kg5.214 Pyrene 129-00-0 8270E 2.3 J 1ug/kg0.522.8 Pyridine 110-86-1 8270E ND 1ug/kg5.214 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.214 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.214 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 76 33-102 2-Fluorophenol 77 35-115 Nitrobenzene-d5 70 22-109 Phenol-d5 87 33-122 Terphenyl-d14 98 41-120 2,4,6-Tribromophenol 82 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0130 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)80 40-140 2-Fluorobiphenyl (fractionation 1)83 40-140 o - Terphenyl (aromatic)71 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1704 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)69 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 60 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-4 VF09036-009 06/08/2020 1320 06/09/2020 Solid % Solids:94.3 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1316 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg0.894.5 C9 - C12 Aliphatics MADEP-VPH-18-2.3 J 1mg/kg0.894.5 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)112 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1316 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-1.7 1mg/kg0.591.5 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)114 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 61 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-5 VF09036-010 06/08/2020 1345 06/09/2020 Solid % Solids:81.7 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1546 JM1 56477 5.85 2 5035 High 8260D 1 06/11/2020 1556 JM1 56630 5.11 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 29 1ug/kg8.421 Benzene 71-43-2 8260D 12 1ug/kg2.15.2 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.15.2 Bromoform 75-25-2 8260D ND 1ug/kg2.15.2 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.15.2 2-Butanone (MEK)78-93-3 8260D 7.7 J 1ug/kg4.221 Carbon disulfide 75-15-0 8260D 2.5 J 1ug/kg2.15.2 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.15.2 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.15.2 Chloroethane 75-00-3 8260D ND 1ug/kg2.15.2 Chloroform 67-66-3 8260D ND 1ug/kg2.15.2 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.15.2 Cyclohexane 110-82-7 8260D ND 1ug/kg2.15.2 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.15.2 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.15.2 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.15.2 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.15.2 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.15.2 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.15.2 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.15.2 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.15.2 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.15.2 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.15.2 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.15.2 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.15.2 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.15.2 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.15.2 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.15.2 Ethylbenzene 100-41-4 8260D 1100 2ug/kg140360 2-Hexanone 591-78-6 8260D ND 1ug/kg4.210 Isopropylbenzene 98-82-8 8260D 170 1ug/kg2.15.2 Methyl acetate 79-20-9 8260D ND 1ug/kg2.15.2 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.15.2 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.210 Methylcyclohexane 108-87-2 8260D 200 1ug/kg2.15.2 Methylene chloride 75-09-2 8260D ND 1ug/kg2.15.2 Styrene 100-42-5 8260D ND 1ug/kg2.15.2 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.15.2 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.15.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 62 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-5 VF09036-010 06/08/2020 1345 06/09/2020 Solid % Solids:81.7 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1546 JM1 56477 5.85 2 5035 High 8260D 1 06/11/2020 1556 JM1 56630 5.11 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Toluene 108-88-3 8260D 25 1ug/kg2.15.2 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.15.2 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.15.2 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.15.2 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.15.2 Trichloroethene 79-01-6 8260D ND 1ug/kg2.15.2 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.15.2 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.15.2 Xylenes (total)1330-20-7 8260D 2200 2ug/kg280710 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ Bromofluorobenzene 96 47-138 99 47-138 1,2-Dichloroethane-d4 83 53-142 90 53-142 Toluene-d8 112 68-124 97 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1723 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E 2.1 J 1ug/kg0.983.2 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.13.2 Acetophenone 98-86-2 8270E ND 1ug/kg5.915 Anthracene 120-12-7 8270E 2.6 J 1ug/kg0.603.2 Atrazine 1912-24-9 8270E ND 1ug/kg5.915 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.915 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.703.2 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.783.2 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.593.2 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.773.2 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.573.2 1,1'-Biphenyl 92-52-4 8270E 6.4 J 1ug/kg5.915 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.915 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.915 Caprolactam 105-60-2 8270E ND 1ug/kg5.915 Carbazole 86-74-8 8270E ND 1ug/kg5.915 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.915 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.915 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 63 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-5 VF09036-010 06/08/2020 1345 06/09/2020 Solid % Solids:81.7 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1723 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.915 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.915 bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.915 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.915 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.915 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.915 Chrysene 218-01-9 8270E ND 1ug/kg0.533.2 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.603.2 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.915 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.915 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.915 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.915 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.815 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.915 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg5.915 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg3079 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg3079 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1232 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1232 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.915 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg3079 Fluoranthene 206-44-0 8270E 1.6 J 1ug/kg0.503.2 Fluorene 86-73-7 8270E 3.8 1ug/kg0.683.2 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.915 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.915 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg3079 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.915 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.23.2 Isophorone 78-59-1 8270E ND 1ug/kg5.915 2-Methylnaphthalene 91-57-6 8270E 350 1ug/kg1.23.2 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.915 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1232 Naphthalene 91-20-3 8270E 150 1ug/kg1.13.2 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1232 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1232 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1232 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.915 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1232 4-Nitrophenol 100-02-7 8270E ND 1ug/kg3079 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.915 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 64 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-5 VF09036-010 06/08/2020 1345 06/09/2020 Solid % Solids:81.7 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1723 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.915 Pentachlorophenol 87-86-5 8270E ND 1ug/kg3079 Phenanthrene 85-01-8 8270E 6.4 1ug/kg0.853.2 Phenol 108-95-2 8270E ND 1ug/kg5.915 Pyrene 129-00-0 8270E 2.6 J 1ug/kg0.593.2 Pyridine 110-86-1 8270E ND 1ug/kg5.915 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.915 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.915 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 72 33-102 2-Fluorophenol 81 35-115 Nitrobenzene-d5 71 22-109 Phenol-d5 90 33-122 Terphenyl-d14 103 41-120 2,4,6-Tribromophenol 87 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0159 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)83 40-140 2-Fluorobiphenyl (fractionation 1)86 40-140 o - Terphenyl (aromatic)76 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1733 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 65 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-5 VF09036-010 06/08/2020 1345 06/09/2020 Solid % Solids:81.7 06/09/2020 2356 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)67 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1539 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-24 1mg/kg1.15.5 C9 - C12 Aliphatics MADEP-VPH-18-35 1mg/kg1.15.5 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)103 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1539 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-35 1mg/kg0.731.8 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 66 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-6 VF09036-011 06/08/2020 1415 06/09/2020 Solid % Solids:82.0 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1523 JM1 56477 6.35 2 5035 8260D 1 06/12/2020 1526 JM1 56756 5.60 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg7.719 Benzene 71-43-2 8260D ND 1ug/kg1.94.8 Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.94.8 Bromoform 75-25-2 8260D ND 1ug/kg1.94.8 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.94.8 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.819 Carbon disulfide 75-15-0 8260D ND 1ug/kg1.94.8 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.94.8 Chlorobenzene 108-90-7 8260D ND 1ug/kg1.94.8 Chloroethane 75-00-3 8260D ND 1ug/kg1.94.8 Chloroform 67-66-3 8260D ND 1ug/kg1.94.8 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.94.8 Cyclohexane 110-82-7 8260D ND 1ug/kg1.94.8 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.94.8 Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.94.8 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.94.8 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.94.8 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.94.8 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.94.8 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.94.8 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.94.8 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.94.8 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.94.8 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.94.8 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.94.8 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.94.8 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.94.8 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.94.8 Ethylbenzene 100-41-4 8260D ND 2ug/kg2.25.4 2-Hexanone 591-78-6 8260D ND 1ug/kg3.89.6 Isopropylbenzene 98-82-8 8260D ND 1ug/kg1.94.8 Methyl acetate 79-20-9 8260D ND 1ug/kg1.94.8 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.94.8 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.89.6 Methylcyclohexane 108-87-2 8260D ND 1ug/kg1.94.8 Methylene chloride 75-09-2 8260D ND 1ug/kg1.94.8 Styrene 100-42-5 8260D ND 1ug/kg1.94.8 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.94.8 Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.94.8 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 67 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-6 VF09036-011 06/08/2020 1415 06/09/2020 Solid % Solids:82.0 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1523 JM1 56477 6.35 2 5035 8260D 1 06/12/2020 1526 JM1 56756 5.60 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Toluene 108-88-3 8260D ND 1ug/kg1.94.8 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.94.8 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.94.8 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.94.8 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.94.8 Trichloroethene 79-01-6 8260D ND 1ug/kg1.94.8 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.94.8 Vinyl chloride 75-01-4 8260D ND 1ug/kg2.94.8 Xylenes (total)1330-20-7 8260D ND 2ug/kg4.411 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ Bromofluorobenzene 99 47-138 101 47-138 1,2-Dichloroethane-d4 84 53-142 85 53-142 Toluene-d8 96 68-124 96 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1748 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.993.2 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.13.2 Acetophenone 98-86-2 8270E ND 1ug/kg6.016 Anthracene 120-12-7 8270E ND 1ug/kg0.613.2 Atrazine 1912-24-9 8270E ND 1ug/kg6.016 Benzaldehyde 100-52-7 8270E ND 1ug/kg6.016 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.713.2 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.793.2 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.603.2 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.783.2 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.573.2 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg6.016 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg6.016 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg6.016 Caprolactam 105-60-2 8270E ND 1ug/kg6.016 Carbazole 86-74-8 8270E ND 1ug/kg6.016 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg6.016 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg6.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 68 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-6 VF09036-011 06/08/2020 1415 06/09/2020 Solid % Solids:82.0 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1748 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Chloroaniline 106-47-8 8270E ND 1ug/kg6.016 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg6.016 bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg6.016 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg6.016 2-Chlorophenol 95-57-8 8270E ND 1ug/kg6.016 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg6.016 Chrysene 218-01-9 8270E ND 1ug/kg0.543.2 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.613.2 Dibenzofuran 132-64-9 8270E ND 1ug/kg6.016 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg6.016 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg6.016 Diethylphthalate 84-66-2 8270E ND 1ug/kg6.016 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.816 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg6.016 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg6.016 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg3080 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg3080 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1232 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1232 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg6.016 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg3080 Fluoranthene 206-44-0 8270E 1.9 J 1ug/kg0.503.2 Fluorene 86-73-7 8270E ND 1ug/kg0.683.2 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg6.016 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg6.016 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg3080 Hexachloroethane 67-72-1 8270E ND 1ug/kg6.016 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.23.2 Isophorone 78-59-1 8270E ND 1ug/kg6.016 2-Methylnaphthalene 91-57-6 8270E 3.6 1ug/kg1.23.2 2-Methylphenol 95-48-7 8270E ND 1ug/kg6.016 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1232 Naphthalene 91-20-3 8270E 2.0 J 1ug/kg1.23.2 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1232 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1232 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1232 Nitrobenzene 98-95-3 8270E ND 1ug/kg6.016 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1232 4-Nitrophenol 100-02-7 8270E ND 1ug/kg3080 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg6.016 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 69 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-6 VF09036-011 06/08/2020 1415 06/09/2020 Solid % Solids:82.0 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/16/2020 1748 SCD 06/15/2020 2347 56992 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg6.016 Pentachlorophenol 87-86-5 8270E ND 1ug/kg3080 Phenanthrene 85-01-8 8270E ND 1ug/kg0.863.2 Phenol 108-95-2 8270E ND 1ug/kg6.016 Pyrene 129-00-0 8270E 2.6 J 1ug/kg0.603.2 Pyridine 110-86-1 8270E ND 1ug/kg6.016 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg6.016 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg6.016 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 75 33-102 2-Fluorophenol 84 35-115 Nitrobenzene-d5 73 22-109 Phenol-d5 95 33-122 Terphenyl-d14 98 41-120 2,4,6-Tribromophenol 81 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0229 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)82 40-140 2-Fluorobiphenyl (fractionation 1)85 40-140 o - Terphenyl (aromatic)73 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1803 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 70 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-6 VF09036-011 06/08/2020 1415 06/09/2020 Solid % Solids:82.0 06/09/2020 2356 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)71 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1345 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg0.884.4 C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg0.884.4 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)106 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1345 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-ND 1mg/kg0.591.5 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 71 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-7 VF09036-012 06/08/2020 1450 06/09/2020 Solid % Solids:80.1 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1609 JM1 56477 5.59 2 5035 High 8260D 1 06/11/2020 1619 JM1 56630 6.03 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 16 J 1ug/kg8.922 Benzene 71-43-2 8260D 5.4 J 1ug/kg2.25.6 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.25.6 Bromoform 75-25-2 8260D ND 1ug/kg2.25.6 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.35.6 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.522 Carbon disulfide 75-15-0 8260D ND 1ug/kg2.25.6 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.25.6 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.25.6 Chloroethane 75-00-3 8260D ND 1ug/kg2.25.6 Chloroform 67-66-3 8260D ND 1ug/kg2.25.6 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.35.6 Cyclohexane 110-82-7 8260D ND 1ug/kg2.25.6 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.25.6 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.25.6 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.25.6 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.25.6 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.25.6 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.25.6 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.35.6 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.25.6 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.25.6 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.25.6 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.25.6 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.25.6 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.25.6 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.25.6 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.25.6 Ethylbenzene 100-41-4 8260D 490 2ug/kg130320 2-Hexanone 591-78-6 8260D ND 1ug/kg4.511 Isopropylbenzene 98-82-8 8260D 350 E 1ug/kg2.25.6 Methyl acetate 79-20-9 8260D ND 1ug/kg2.25.6 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.25.6 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.511 Methylcyclohexane 108-87-2 8260D 240 E 1ug/kg2.25.6 Methylene chloride 75-09-2 8260D ND 1ug/kg2.25.6 Styrene 100-42-5 8260D ND 1ug/kg2.25.6 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.25.6 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.25.6 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 72 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-7 VF09036-012 06/08/2020 1450 06/09/2020 Solid % Solids:80.1 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1609 JM1 56477 5.59 2 5035 High 8260D 1 06/11/2020 1619 JM1 56630 6.03 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Toluene 108-88-3 8260D 56 1ug/kg2.25.6 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.25.6 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.25.6 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.25.6 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.25.6 Trichloroethene 79-01-6 8260D ND 1ug/kg2.25.6 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.25.6 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.35.6 Xylenes (total)1330-20-7 8260D 1600 2ug/kg260640 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ Bromofluorobenzene 93 47-138 116 47-138 1,2-Dichloroethane-d4 82 53-142 103 53-142 Toluene-d8 115 68-124 112 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 10 06/19/2020 1422 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg1033 Acenaphthylene 208-96-8 8270E ND 1ug/kg1233 Acetophenone 98-86-2 8270E ND 1ug/kg62160 Anthracene 120-12-7 8270E ND 1ug/kg6.333 Atrazine 1912-24-9 8270E ND 1ug/kg62160 Benzaldehyde 100-52-7 8270E ND 1ug/kg62160 Benzo(a)anthracene 56-55-3 8270E 40 1ug/kg7.333 Benzo(a)pyrene 50-32-8 8270E 34 1ug/kg8.133 Benzo(b)fluoranthene 205-99-2 8270E 56 1ug/kg6.233 Benzo(g,h,i)perylene 191-24-2 8270E 21 J 1ug/kg8.033 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg5.933 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg62160 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg62160 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg62160 Caprolactam 105-60-2 8270E ND 1ug/kg62160 Carbazole 86-74-8 8270E ND 1ug/kg62160 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg62160 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg62160 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 73 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-7 VF09036-012 06/08/2020 1450 06/09/2020 Solid % Solids:80.1 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 10 06/19/2020 1422 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Chloroaniline 106-47-8 8270E ND 1ug/kg62160 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg62160 bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg62160 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg62160 2-Chlorophenol 95-57-8 8270E ND 1ug/kg62160 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg62160 Chrysene 218-01-9 8270E 35 1ug/kg5.533 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg6.333 Dibenzofuran 132-64-9 8270E ND 1ug/kg62160 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg62160 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg62160 Diethylphthalate 84-66-2 8270E ND 1ug/kg62160 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg91160 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg62160 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg62160 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg310830 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg310830 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg120330 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg120330 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg62160 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg310830 Fluoranthene 206-44-0 8270E 54 1ug/kg5.233 Fluorene 86-73-7 8270E ND 1ug/kg7.033 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg62160 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg62160 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg310830 Hexachloroethane 67-72-1 8270E ND 1ug/kg62160 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 18 J 1ug/kg1233 Isophorone 78-59-1 8270E ND 1ug/kg62160 2-Methylnaphthalene 91-57-6 8270E 680 1ug/kg1233 2-Methylphenol 95-48-7 8270E ND 1ug/kg62160 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg120330 Naphthalene 91-20-3 8270E 660 1ug/kg1233 2-Nitroaniline 88-74-4 8270E ND 1ug/kg120330 3-Nitroaniline 99-09-2 8270E ND 1ug/kg120330 4-Nitroaniline 100-01-6 8270E ND 1ug/kg120330 Nitrobenzene 98-95-3 8270E ND 1ug/kg62160 2-Nitrophenol 88-75-5 8270E ND 1ug/kg120330 4-Nitrophenol 100-02-7 8270E ND 1ug/kg310830 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg62160 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 74 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-7 VF09036-012 06/08/2020 1450 06/09/2020 Solid % Solids:80.1 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 10 06/19/2020 1422 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg62160 Pentachlorophenol 87-86-5 8270E ND 1ug/kg310830 Phenanthrene 85-01-8 8270E 64 1ug/kg8.933 Phenol 108-95-2 8270E ND 1ug/kg62160 Pyrene 129-00-0 8270E 50 1ug/kg6.233 Pyridine 110-86-1 8270E ND 1ug/kg62160 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg62160 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg62160 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 101 33-102 2-Fluorophenol 90 35-115 Nitrobenzene-d5 96 22-109 Phenol-d5 95 33-122 Terphenyl-d14 101 41-120 2,4,6-Tribromophenol 83 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0259 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)85 40-140 2-Fluorobiphenyl (fractionation 1)88 40-140 o - Terphenyl (aromatic)76 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1833 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 75 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-7 VF09036-012 06/08/2020 1450 06/09/2020 Solid % Solids:80.1 06/09/2020 2356 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)67 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1607 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-20 1mg/kg1.05.0 C9 - C12 Aliphatics MADEP-VPH-18-50 1mg/kg1.05.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)128 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1607 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-59 1mg/kg0.671.7 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)129 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 76 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-8 VF09036-013 06/08/2020 1500 06/09/2020 Solid % Solids:80.3 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1330 JM1 56477 6.61 2 5035 High 8260D 1 06/11/2020 1641 JM1 56630 6.35 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg7.519 Benzene 71-43-2 8260D ND 1ug/kg1.94.7 Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.94.7 Bromoform 75-25-2 8260D ND 1ug/kg1.94.7 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.84.7 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.819 Carbon disulfide 75-15-0 8260D ND 1ug/kg1.94.7 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.94.7 Chlorobenzene 108-90-7 8260D ND 1ug/kg1.94.7 Chloroethane 75-00-3 8260D ND 1ug/kg1.94.7 Chloroform 67-66-3 8260D ND 1ug/kg1.94.7 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.84.7 Cyclohexane 110-82-7 8260D ND 1ug/kg1.94.7 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.94.7 Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.94.7 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.94.7 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.94.7 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.94.7 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.94.7 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.84.7 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.94.7 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.94.7 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.94.7 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.94.7 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.94.7 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.94.7 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.94.7 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.94.7 Ethylbenzene 100-41-4 8260D 240 E 1ug/kg1.94.7 2-Hexanone 591-78-6 8260D ND 1ug/kg3.89.4 Isopropylbenzene 98-82-8 8260D 48 1ug/kg1.94.7 Methyl acetate 79-20-9 8260D ND 1ug/kg1.94.7 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.94.7 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.89.4 Methylcyclohexane 108-87-2 8260D 55 1ug/kg1.94.7 Methylene chloride 75-09-2 8260D ND 1ug/kg1.94.7 Styrene 100-42-5 8260D ND 1ug/kg1.94.7 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.94.7 Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.94.7 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 77 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-8 VF09036-013 06/08/2020 1500 06/09/2020 Solid % Solids:80.3 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1330 JM1 56477 6.61 2 5035 High 8260D 1 06/11/2020 1641 JM1 56630 6.35 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Toluene 108-88-3 8260D 7.4 1ug/kg1.94.7 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.94.7 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.94.7 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.94.7 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.94.7 Trichloroethene 79-01-6 8260D ND 1ug/kg1.94.7 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.94.7 Vinyl chloride 75-01-4 8260D ND 1ug/kg2.84.7 Xylenes (total)1330-20-7 8260D 700 2ug/kg250610 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ Bromofluorobenzene 85 47-138 114 47-138 1,2-Dichloroethane-d4 87 53-142 106 53-142 Toluene-d8 107 68-124 111 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1447 SCD 06/18/2020 1801 57409 2 3546 8270E 5 06/19/2020 1650 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E 6.0 1ug/kg1.03.3 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.23.3 Acetophenone 98-86-2 8270E ND 1ug/kg6.216 Anthracene 120-12-7 8270E 6.9 1ug/kg0.633.3 Atrazine 1912-24-9 8270E ND 1ug/kg6.216 Benzaldehyde 100-52-7 8270E ND 1ug/kg6.216 Benzo(a)anthracene 56-55-3 8270E 3.4 1ug/kg0.733.3 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.823.3 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.623.3 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.803.3 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.593.3 1,1'-Biphenyl 92-52-4 8270E 24 1ug/kg6.216 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg6.216 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg6.216 Caprolactam 105-60-2 8270E ND 1ug/kg6.216 Carbazole 86-74-8 8270E ND 1ug/kg6.216 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg6.216 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 78 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-8 VF09036-013 06/08/2020 1500 06/09/2020 Solid % Solids:80.3 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1447 SCD 06/18/2020 1801 57409 2 3546 8270E 5 06/19/2020 1650 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg6.216 4-Chloroaniline 106-47-8 8270E ND 1ug/kg6.216 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg6.216 bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg6.216 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg6.216 2-Chlorophenol 95-57-8 8270E ND 1ug/kg6.216 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg6.216 Chrysene 218-01-9 8270E 1.8 J 1ug/kg0.563.3 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.633.3 Dibenzofuran 132-64-9 8270E ND 1ug/kg6.216 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg6.216 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg6.216 Diethylphthalate 84-66-2 8270E ND 1ug/kg6.216 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg9.216 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg6.216 Di-n-butyl phthalate 84-74-2 8270E 7.3 J 1ug/kg6.216 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg3183 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg3183 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1233 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1233 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg6.216 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg3183 Fluoranthene 206-44-0 8270E 3.6 1ug/kg0.523.3 Fluorene 86-73-7 8270E 10 1ug/kg0.713.3 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg6.216 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg6.216 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg3183 Hexachloroethane 67-72-1 8270E ND 1ug/kg6.216 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.23.3 Isophorone 78-59-1 8270E ND 1ug/kg6.216 2-Methylnaphthalene 91-57-6 8270E 1400 2ug/kg6.117 2-Methylphenol 95-48-7 8270E ND 1ug/kg6.216 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1233 Naphthalene 91-20-3 8270E 1000 2ug/kg6.017 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1233 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1233 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1233 Nitrobenzene 98-95-3 8270E ND 1ug/kg6.216 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1233 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 79 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-8 VF09036-013 06/08/2020 1500 06/09/2020 Solid % Solids:80.3 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1447 SCD 06/18/2020 1801 57409 2 3546 8270E 5 06/19/2020 1650 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Nitrophenol 100-02-7 8270E ND 1ug/kg3183 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg6.216 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg6.216 Pentachlorophenol 87-86-5 8270E ND 1ug/kg3183 Phenanthrene 85-01-8 8270E 14 1ug/kg0.893.3 Phenol 108-95-2 8270E ND 1ug/kg6.216 Pyrene 129-00-0 8270E 6.2 1ug/kg0.623.3 Pyridine 110-86-1 8270E ND 1ug/kg6.216 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg6.216 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg6.216 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ 2-Fluorobiphenyl 83 33-102 84 33-102 2-Fluorophenol 71 35-115 84 35-115 Nitrobenzene-d5 76 22-109 66 22-109 Phenol-d5 75 33-122 94 33-122 Terphenyl-d14 91 41-120 92 41-120 2,4,6-Tribromophenol 90 30-117 68 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0329 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)86 40-140 2-Fluorobiphenyl (fractionation 1)88 40-140 o - Terphenyl (aromatic)80 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1903 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 80 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-8 VF09036-013 06/08/2020 1500 06/09/2020 Solid % Solids:80.3 06/09/2020 2356 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1903 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)75 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1636 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-5.7 1mg/kg0.944.7 C9 - C12 Aliphatics MADEP-VPH-18-6.6 1mg/kg0.944.7 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)104 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1636 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-8.2 1mg/kg0.631.6 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 81 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-9 VF09036-014 06/08/2020 1515 06/09/2020 Solid % Solids:77.6 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1353 JM1 56477 5.93 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg8.722 Benzene 71-43-2 8260D ND 1ug/kg2.25.4 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.25.4 Bromoform 75-25-2 8260D ND 1ug/kg2.25.4 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.35.4 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.322 Carbon disulfide 75-15-0 8260D ND 1ug/kg2.25.4 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.25.4 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.25.4 Chloroethane 75-00-3 8260D ND 1ug/kg2.25.4 Chloroform 67-66-3 8260D ND 1ug/kg2.25.4 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.35.4 Cyclohexane 110-82-7 8260D ND 1ug/kg2.25.4 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.25.4 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.25.4 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.25.4 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.25.4 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.25.4 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.25.4 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.35.4 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.25.4 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.25.4 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.25.4 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.25.4 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.25.4 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.25.4 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.25.4 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.25.4 Ethylbenzene 100-41-4 8260D ND 1ug/kg2.25.4 2-Hexanone 591-78-6 8260D ND 1ug/kg4.311 Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.25.4 Methyl acetate 79-20-9 8260D ND 1ug/kg2.25.4 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.25.4 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.311 Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.25.4 Methylene chloride 75-09-2 8260D ND 1ug/kg2.25.4 Styrene 100-42-5 8260D ND 1ug/kg2.25.4 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.25.4 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.25.4 Toluene 108-88-3 8260D ND 1ug/kg2.25.4 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 82 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-9 VF09036-014 06/08/2020 1515 06/09/2020 Solid % Solids:77.6 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1353 JM1 56477 5.93 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.25.4 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.25.4 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.25.4 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.25.4 Trichloroethene 79-01-6 8260D ND 1ug/kg2.25.4 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.25.4 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.35.4 Xylenes (total)1330-20-7 8260D ND 1ug/kg4.311 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 92 47-138 1,2-Dichloroethane-d4 85 53-142 Toluene-d8 103 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1511 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg1.13.5 Acenaphthylene 208-96-8 8270E 2.0 J 1ug/kg1.23.5 Acetophenone 98-86-2 8270E ND 1ug/kg6.417 Anthracene 120-12-7 8270E 3.7 1ug/kg0.663.5 Atrazine 1912-24-9 8270E ND 1ug/kg6.417 Benzaldehyde 100-52-7 8270E 12 J 1ug/kg6.417 Benzo(a)anthracene 56-55-3 8270E 12 1ug/kg0.763.5 Benzo(a)pyrene 50-32-8 8270E 13 1ug/kg0.853.5 Benzo(b)fluoranthene 205-99-2 8270E 20 1ug/kg0.643.5 Benzo(g,h,i)perylene 191-24-2 8270E 6.0 1ug/kg0.843.5 Benzo(k)fluoranthene 207-08-9 8270E 6.8 1ug/kg0.623.5 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg6.417 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg6.417 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg6.417 Caprolactam 105-60-2 8270E ND 1ug/kg6.417 Carbazole 86-74-8 8270E ND 1ug/kg6.417 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg6.417 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg6.417 4-Chloroaniline 106-47-8 8270E ND 1ug/kg6.417 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg6.417 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 83 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-9 VF09036-014 06/08/2020 1515 06/09/2020 Solid % Solids:77.6 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1511 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg6.417 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg6.417 2-Chlorophenol 95-57-8 8270E ND 1ug/kg6.417 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg6.417 Chrysene 218-01-9 8270E 13 1ug/kg0.583.5 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.663.5 Dibenzofuran 132-64-9 8270E 10 J 1ug/kg6.417 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg6.417 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg6.417 Diethylphthalate 84-66-2 8270E ND 1ug/kg6.417 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg9.517 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg6.417 Di-n-butyl phthalate 84-74-2 8270E 9.6 J 1ug/kg6.417 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg3286 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg3286 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1335 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1335 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg6.417 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg3286 Fluoranthene 206-44-0 8270E 16 1ug/kg0.543.5 Fluorene 86-73-7 8270E ND 1ug/kg0.733.5 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg6.417 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg6.417 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg3286 Hexachloroethane 67-72-1 8270E ND 1ug/kg6.417 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 4.5 1ug/kg1.33.5 Isophorone 78-59-1 8270E ND 1ug/kg6.417 2-Methylnaphthalene 91-57-6 8270E 49 1ug/kg1.33.5 2-Methylphenol 95-48-7 8270E ND 1ug/kg6.417 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1335 Naphthalene 91-20-3 8270E 42 1ug/kg1.23.5 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1335 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1335 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1335 Nitrobenzene 98-95-3 8270E ND 1ug/kg6.417 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1335 4-Nitrophenol 100-02-7 8270E ND 1ug/kg3286 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg6.417 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg6.417 Pentachlorophenol 87-86-5 8270E ND 1ug/kg3286 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 84 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-9 VF09036-014 06/08/2020 1515 06/09/2020 Solid % Solids:77.6 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1511 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 26 1ug/kg0.933.5 Phenol 108-95-2 8270E ND 1ug/kg6.417 Pyrene 129-00-0 8270E 17 1ug/kg0.643.5 Pyridine 110-86-1 8270E ND 1ug/kg6.417 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg6.417 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg6.417 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 84 33-102 2-Fluorophenol 94 35-115 Nitrobenzene-d5 80 22-109 Phenol-d5 100 33-122 Terphenyl-d14 86 41-120 2,4,6-Tribromophenol 88 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0359 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)84 40-140 2-Fluorobiphenyl (fractionation 1)85 40-140 o - Terphenyl (aromatic)72 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 1933 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1212 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)70 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 85 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-9 VF09036-014 06/08/2020 1515 06/09/2020 Solid % Solids:77.6 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1413 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.2 C9 - C12 Aliphatics MADEP-VPH-18-1.9 J 1mg/kg1.05.2 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)124 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1413 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-1.7 1mg/kg0.691.7 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)121 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 86 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-10 VF09036-015 06/08/2020 1520 06/09/2020 Solid % Solids:81.5 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1415 JM1 56477 4.32 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg1128 Benzene 71-43-2 8260D ND 1ug/kg2.87.1 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.87.1 Bromoform 75-25-2 8260D ND 1ug/kg2.87.1 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg4.37.1 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg5.728 Carbon disulfide 75-15-0 8260D ND 1ug/kg2.87.1 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.87.1 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.87.1 Chloroethane 75-00-3 8260D ND 1ug/kg2.87.1 Chloroform 67-66-3 8260D ND 1ug/kg2.87.1 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg4.37.1 Cyclohexane 110-82-7 8260D ND 1ug/kg2.87.1 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.87.1 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.87.1 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.87.1 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.87.1 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.87.1 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.87.1 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg4.37.1 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.87.1 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.87.1 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.87.1 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.87.1 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.87.1 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.87.1 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.87.1 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.87.1 Ethylbenzene 100-41-4 8260D 5.7 J 1ug/kg2.87.1 2-Hexanone 591-78-6 8260D ND 1ug/kg5.714 Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.87.1 Methyl acetate 79-20-9 8260D ND 1ug/kg2.87.1 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.87.1 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg5.714 Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.87.1 Methylene chloride 75-09-2 8260D ND 1ug/kg2.87.1 Styrene 100-42-5 8260D ND 1ug/kg2.87.1 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.87.1 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.87.1 Toluene 108-88-3 8260D ND 1ug/kg2.87.1 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 87 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-10 VF09036-015 06/08/2020 1520 06/09/2020 Solid % Solids:81.5 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1415 JM1 56477 4.32 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.87.1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.87.1 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.87.1 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.87.1 Trichloroethene 79-01-6 8260D ND 1ug/kg2.87.1 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.87.1 Vinyl chloride 75-01-4 8260D ND 1ug/kg4.37.1 Xylenes (total)1330-20-7 8260D 29 1ug/kg5.714 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 94 47-138 1,2-Dichloroethane-d4 89 53-142 Toluene-d8 97 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 5 06/19/2020 1536 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg5.016 Acenaphthylene 208-96-8 8270E ND 1ug/kg5.716 Acetophenone 98-86-2 8270E ND 1ug/kg3079 Anthracene 120-12-7 8270E ND 1ug/kg3.116 Atrazine 1912-24-9 8270E ND 1ug/kg3079 Benzaldehyde 100-52-7 8270E ND 1ug/kg3079 Benzo(a)anthracene 56-55-3 8270E 20 1ug/kg3.616 Benzo(a)pyrene 50-32-8 8270E 18 1ug/kg4.016 Benzo(b)fluoranthene 205-99-2 8270E 27 1ug/kg3.016 Benzo(g,h,i)perylene 191-24-2 8270E 8.4 J 1ug/kg3.916 Benzo(k)fluoranthene 207-08-9 8270E 9.0 J 1ug/kg2.916 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg3079 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg3079 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg3079 Caprolactam 105-60-2 8270E ND 1ug/kg3079 Carbazole 86-74-8 8270E ND 1ug/kg3079 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg3079 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg3079 4-Chloroaniline 106-47-8 8270E ND 1ug/kg3079 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg3079 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 88 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-10 VF09036-015 06/08/2020 1520 06/09/2020 Solid % Solids:81.5 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 5 06/19/2020 1536 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg3079 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg3079 2-Chlorophenol 95-57-8 8270E ND 1ug/kg3079 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg3079 Chrysene 218-01-9 8270E 15 J 1ug/kg2.716 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg3.116 Dibenzofuran 132-64-9 8270E ND 1ug/kg3079 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg3079 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg3079 Diethylphthalate 84-66-2 8270E ND 1ug/kg3079 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg4579 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg3079 Di-n-butyl phthalate 84-74-2 8270E 32 J 1ug/kg3079 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg150410 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg150410 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg61160 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg61160 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg3079 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg150410 Fluoranthene 206-44-0 8270E 19 1ug/kg2.516 Fluorene 86-73-7 8270E ND 1ug/kg3.416 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg3079 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg3079 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg150410 Hexachloroethane 67-72-1 8270E ND 1ug/kg3079 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 8.1 J 1ug/kg6.116 Isophorone 78-59-1 8270E ND 1ug/kg3079 2-Methylnaphthalene 91-57-6 8270E 32 1ug/kg6.016 2-Methylphenol 95-48-7 8270E ND 1ug/kg3079 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg61160 Naphthalene 91-20-3 8270E 26 1ug/kg5.916 2-Nitroaniline 88-74-4 8270E ND 1ug/kg61160 3-Nitroaniline 99-09-2 8270E ND 1ug/kg61160 4-Nitroaniline 100-01-6 8270E ND 1ug/kg61160 Nitrobenzene 98-95-3 8270E ND 1ug/kg3079 2-Nitrophenol 88-75-5 8270E ND 1ug/kg61160 4-Nitrophenol 100-02-7 8270E ND 1ug/kg150410 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg3079 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg3079 Pentachlorophenol 87-86-5 8270E ND 1ug/kg150410 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 89 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-10 VF09036-015 06/08/2020 1520 06/09/2020 Solid % Solids:81.5 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 5 06/19/2020 1536 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 13 J 1ug/kg4.416 Phenol 108-95-2 8270E ND 1ug/kg3079 Pyrene 129-00-0 8270E 21 1ug/kg3.016 Pyridine 110-86-1 8270E ND 1ug/kg3079 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg3079 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg3079 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 88 33-102 2-Fluorophenol 83 35-115 Nitrobenzene-d5 63 22-109 Phenol-d5 96 33-122 Terphenyl-d14 96 41-120 2,4,6-Tribromophenol 76 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0428 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1111 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)85 40-140 2-Fluorobiphenyl (fractionation 1)87 40-140 o - Terphenyl (aromatic)59 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 2002 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)58 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 90 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-10 VF09036-015 06/08/2020 1520 06/09/2020 Solid % Solids:81.5 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1442 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.1 C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg1.05.1 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)105 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1442 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-0.83 J 1mg/kg0.681.7 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)100 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 91 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-11 VF09036-016 06/08/2020 1530 06/09/2020 Solid % Solids:90.5 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1438 JM1 56477 6.74 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D ND 1ug/kg6.616 Benzene 71-43-2 8260D ND 1ug/kg1.64.1 Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.64.1 Bromoform 75-25-2 8260D ND 1ug/kg1.64.1 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.54.1 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.316 Carbon disulfide 75-15-0 8260D ND 1ug/kg1.64.1 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.64.1 Chlorobenzene 108-90-7 8260D ND 1ug/kg1.64.1 Chloroethane 75-00-3 8260D ND 1ug/kg1.64.1 Chloroform 67-66-3 8260D ND 1ug/kg1.64.1 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.54.1 Cyclohexane 110-82-7 8260D ND 1ug/kg1.64.1 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.64.1 Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.64.1 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.64.1 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.64.1 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.64.1 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.64.1 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.54.1 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.64.1 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.64.1 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.64.1 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.64.1 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.64.1 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.64.1 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.64.1 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.64.1 Ethylbenzene 100-41-4 8260D 14 1ug/kg1.64.1 2-Hexanone 591-78-6 8260D ND 1ug/kg3.38.2 Isopropylbenzene 98-82-8 8260D 3.6 J 1ug/kg1.64.1 Methyl acetate 79-20-9 8260D ND 1ug/kg1.64.1 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.64.1 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.38.2 Methylcyclohexane 108-87-2 8260D ND 1ug/kg1.64.1 Methylene chloride 75-09-2 8260D ND 1ug/kg1.64.1 Styrene 100-42-5 8260D ND 1ug/kg1.64.1 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.64.1 Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.64.1 Toluene 108-88-3 8260D ND 1ug/kg1.64.1 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 92 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-11 VF09036-016 06/08/2020 1530 06/09/2020 Solid % Solids:90.5 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1438 JM1 56477 6.74 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.64.1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.64.1 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.64.1 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.64.1 Trichloroethene 79-01-6 8260D ND 1ug/kg1.64.1 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.64.1 Vinyl chloride 75-01-4 8260D ND 1ug/kg2.54.1 Xylenes (total)1330-20-7 8260D 69 1ug/kg3.38.2 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 98 47-138 1,2-Dichloroethane-d4 85 53-142 Toluene-d8 97 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1601 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.902.9 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.02.9 Acetophenone 98-86-2 8270E ND 1ug/kg5.414 Anthracene 120-12-7 8270E 1.5 J 1ug/kg0.552.9 Atrazine 1912-24-9 8270E ND 1ug/kg5.414 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.414 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.642.9 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.722.9 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.542.9 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.702.9 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.522.9 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.414 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.414 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.414 Caprolactam 105-60-2 8270E ND 1ug/kg5.414 Carbazole 86-74-8 8270E ND 1ug/kg5.414 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.414 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.414 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.414 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.414 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 93 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-11 VF09036-016 06/08/2020 1530 06/09/2020 Solid % Solids:90.5 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1601 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.414 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.414 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.414 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.414 Chrysene 218-01-9 8270E ND 1ug/kg0.492.9 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.552.9 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.414 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.414 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.414 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.414 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.014 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.414 Di-n-butyl phthalate 84-74-2 8270E 7.0 J 1ug/kg5.414 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2773 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2773 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1129 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1129 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.414 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2773 Fluoranthene 206-44-0 8270E ND 1ug/kg0.462.9 Fluorene 86-73-7 8270E ND 1ug/kg0.622.9 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.414 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.414 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2773 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.414 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.12.9 Isophorone 78-59-1 8270E ND 1ug/kg5.414 2-Methylnaphthalene 91-57-6 8270E 58 1ug/kg1.12.9 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.414 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1129 Naphthalene 91-20-3 8270E 37 1ug/kg1.12.9 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1129 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1129 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1129 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.414 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1129 4-Nitrophenol 100-02-7 8270E ND 1ug/kg2773 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.414 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.414 Pentachlorophenol 87-86-5 8270E ND 1ug/kg2773 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 94 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-11 VF09036-016 06/08/2020 1530 06/09/2020 Solid % Solids:90.5 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1601 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Phenanthrene 85-01-8 8270E 1.9 J 1ug/kg0.782.9 Phenol 108-95-2 8270E ND 1ug/kg5.414 Pyrene 129-00-0 8270E 2.0 J 1ug/kg0.542.9 Pyridine 110-86-1 8270E ND 1ug/kg5.414 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.414 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.414 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 85 33-102 2-Fluorophenol 89 35-115 Nitrobenzene-d5 79 22-109 Phenol-d5 109 33-122 Terphenyl-d14 101 41-120 2,4,6-Tribromophenol 73 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0458 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)88 40-140 2-Fluorobiphenyl (fractionation 1)90 40-140 o - Terphenyl (aromatic)79 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 2032 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1010 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)74 40-140 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 95 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-11 VF09036-016 06/08/2020 1530 06/09/2020 Solid % Solids:90.5 06/09/2020 2356 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1510 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg0.874.3 C9 - C12 Aliphatics MADEP-VPH-18-ND 1mg/kg0.874.3 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)96 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1510 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-1.0 J 1mg/kg0.581.4 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)92 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 96 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-12 VF09036-017 06/08/2020 1540 06/09/2020 Solid % Solids:87.2 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1501 JM1 56477 4.64 2 5035 High 8260D 1 06/11/2020 1704 JM1 56630 5.57 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260D 17 J 1ug/kg9.925 Benzene 71-43-2 8260D ND 1ug/kg2.56.2 Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.56.2 Bromoform 75-25-2 8260D ND 1ug/kg2.56.2 Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.76.2 2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.925 Carbon disulfide 75-15-0 8260D 4.4 J 1ug/kg2.56.2 Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.56.2 Chlorobenzene 108-90-7 8260D ND 1ug/kg2.56.2 Chloroethane 75-00-3 8260D ND 1ug/kg2.56.2 Chloroform 67-66-3 8260D ND 1ug/kg2.56.2 Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.76.2 Cyclohexane 110-82-7 8260D ND 1ug/kg2.56.2 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.56.2 Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.56.2 1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.56.2 1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.56.2 1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.56.2 1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.56.2 Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.76.2 1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.56.2 1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.56.2 1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.56.2 cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.56.2 trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.56.2 1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.56.2 cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.56.2 trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.56.2 Ethylbenzene 100-41-4 8260D 2100 2ug/kg120290 2-Hexanone 591-78-6 8260D ND 1ug/kg4.912 Isopropylbenzene 98-82-8 8260D 180 1ug/kg2.56.2 Methyl acetate 79-20-9 8260D ND 1ug/kg2.56.2 Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.56.2 4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.912 Methylcyclohexane 108-87-2 8260D 150 1ug/kg2.56.2 Methylene chloride 75-09-2 8260D ND 1ug/kg2.56.2 Styrene 100-42-5 8260D ND 1ug/kg2.56.2 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.56.2 Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.56.2 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 97 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-12 VF09036-017 06/08/2020 1540 06/09/2020 Solid % Solids:87.2 06/09/2020 2356 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 06/10/2020 1501 JM1 56477 4.64 2 5035 High 8260D 1 06/11/2020 1704 JM1 56630 5.57 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Toluene 108-88-3 8260D ND 1ug/kg2.56.2 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.56.2 1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.56.2 1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.56.2 1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.56.2 Trichloroethene 79-01-6 8260D ND 1ug/kg2.56.2 Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.56.2 Vinyl chloride 75-01-4 8260D ND 1ug/kg3.76.2 Xylenes (total)1330-20-7 8260D 2200 2ug/kg240590 AcceptanceAcceptanceRun 2Run 1 Surrogate Q % Recovery Limits % Recovery LimitsQ Bromofluorobenzene 94 47-138 104 47-138 1,2-Dichloroethane-d4 85 53-142 95 53-142 Toluene-d8 106 68-124 101 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1625 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270E ND 1ug/kg0.953.1 Acenaphthylene 208-96-8 8270E ND 1ug/kg1.13.1 Acetophenone 98-86-2 8270E ND 1ug/kg5.715 Anthracene 120-12-7 8270E 4.6 1ug/kg0.583.1 Atrazine 1912-24-9 8270E ND 1ug/kg5.715 Benzaldehyde 100-52-7 8270E ND 1ug/kg5.715 Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.673.1 Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.753.1 Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.573.1 Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.743.1 Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.553.1 1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.715 4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.715 Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.715 Caprolactam 105-60-2 8270E ND 1ug/kg5.715 Carbazole 86-74-8 8270E ND 1ug/kg5.715 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.715 4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.715 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 98 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-12 VF09036-017 06/08/2020 1540 06/09/2020 Solid % Solids:87.2 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1625 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL 4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.715 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.715 bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.715 2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.715 2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.715 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.715 Chrysene 218-01-9 8270E ND 1ug/kg0.513.1 Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.583.1 Dibenzofuran 132-64-9 8270E ND 1ug/kg5.715 3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.715 2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.715 Diethylphthalate 84-66-2 8270E ND 1ug/kg5.715 Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.415 2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.715 Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg5.715 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2876 2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2876 2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1131 2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1131 Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.715 bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2876 Fluoranthene 206-44-0 8270E 1.9 J 1ug/kg0.483.1 Fluorene 86-73-7 8270E 3.5 1ug/kg0.653.1 Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.715 Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.715 Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2876 Hexachloroethane 67-72-1 8270E ND 1ug/kg5.715 Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.13.1 Isophorone 78-59-1 8270E ND 1ug/kg5.715 2-Methylnaphthalene 91-57-6 8270E 37 1ug/kg1.13.1 2-Methylphenol 95-48-7 8270E ND 1ug/kg5.715 3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1131 Naphthalene 91-20-3 8270E 39 1ug/kg1.13.1 2-Nitroaniline 88-74-4 8270E ND 1ug/kg1131 3-Nitroaniline 99-09-2 8270E ND 1ug/kg1131 4-Nitroaniline 100-01-6 8270E ND 1ug/kg1131 Nitrobenzene 98-95-3 8270E ND 1ug/kg5.715 2-Nitrophenol 88-75-5 8270E ND 1ug/kg1131 4-Nitrophenol 100-02-7 8270E ND 1ug/kg2876 N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.715 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 99 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-12 VF09036-017 06/08/2020 1540 06/09/2020 Solid % Solids:87.2 06/09/2020 2356 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270E 1 06/19/2020 1625 SCD 06/18/2020 1801 57409 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.715 Pentachlorophenol 87-86-5 8270E ND 1ug/kg2876 Phenanthrene 85-01-8 8270E 7.3 1ug/kg0.823.1 Phenol 108-95-2 8270E ND 1ug/kg5.715 Pyrene 129-00-0 8270E 4.3 1ug/kg0.573.1 Pyridine 110-86-1 8270E ND 1ug/kg5.715 2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.715 2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.715 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 78 33-102 2-Fluorophenol 88 35-115 Nitrobenzene-d5 80 22-109 Phenol-d5 95 33-122 Terphenyl-d14 95 41-120 2,4,6-Tribromophenol 86 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/17/2020 0528 JJG 06/15/2020 0921 56906 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg1111 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2)84 40-140 2-Fluorobiphenyl (fractionation 1)86 40-140 o - Terphenyl (aromatic)75 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH-MADEP-EPH-04 1 06/16/2020 2102 JJG 06/15/2020 0921 56905 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 C19 - C36 Aliphatics MADEP-EPH-04 ND 1mg/kg1111 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 100 of 170 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SUMMIT Engineering, Laboratory & Testing, P.C. SS-12 VF09036-017 06/08/2020 1540 06/09/2020 Solid % Solids:87.2 06/09/2020 2356 AcceptanceRun 1 Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic)72 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1704 JM1 57092 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C5 - C8 Aliphatics MADEP-VPH-18-9.7 1mg/kg0.794.0 C9 - C12 Aliphatics MADEP-VPH-18-27 1mg/kg0.794.0 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID)93 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 06/16/2020 1704 JM1 57090 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL C9 - C10 Aromatics MADEP-VPH-18-25 1mg/kg0.531.3 AcceptanceRun 1 Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID)109 70-130 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 101 of 170 QC Summary 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 102 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56477-001 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Acetone ND 06/10/2020 0909208.0 ug/kg1 Benzene ND 06/10/2020 09095.0 2.0 ug/kg1 Bromodichloromethane ND 06/10/2020 09095.0 2.0 ug/kg1 Bromoform ND 06/10/2020 09095.0 2.0 ug/kg1 Bromomethane (Methyl bromide)ND 06/10/2020 09095.0 3.0 ug/kg1 2-Butanone (MEK)ND 06/10/2020 0909204.0 ug/kg1 Carbon disulfide ND 06/10/2020 09095.0 2.0 ug/kg1 Carbon tetrachloride ND 06/10/2020 09095.0 2.0 ug/kg1 Chlorobenzene ND 06/10/2020 09095.0 2.0 ug/kg1 Chloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 Chloroform ND 06/10/2020 09095.0 2.0 ug/kg1 Chloromethane (Methyl chloride)ND 06/10/2020 09095.0 3.0 ug/kg1 Cyclohexane ND 06/10/2020 09095.0 2.0 ug/kg1 1,2-Dibromo-3-chloropropane (DBCP)ND 06/10/2020 09095.0 2.0 ug/kg1 Dibromochloromethane ND 06/10/2020 09095.0 2.0 ug/kg1 1,2-Dibromoethane (EDB)ND 06/10/2020 09095.0 2.0 ug/kg1 1,2-Dichlorobenzene ND 06/10/2020 09095.0 2.0 ug/kg1 1,3-Dichlorobenzene ND 06/10/2020 09095.0 2.0 ug/kg1 1,4-Dichlorobenzene ND 06/10/2020 09095.0 2.0 ug/kg1 Dichlorodifluoromethane ND 06/10/2020 09095.0 3.0 ug/kg1 1,1-Dichloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 1,2-Dichloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 1,1-Dichloroethene ND 06/10/2020 09095.0 2.0 ug/kg1 cis-1,2-Dichloroethene ND 06/10/2020 09095.0 2.0 ug/kg1 trans-1,2-Dichloroethene ND 06/10/2020 09095.0 2.0 ug/kg1 1,2-Dichloropropane ND 06/10/2020 09095.0 2.0 ug/kg1 cis-1,3-Dichloropropene ND 06/10/2020 09095.0 2.0 ug/kg1 trans-1,3-Dichloropropene ND 06/10/2020 09095.0 2.0 ug/kg1 Ethylbenzene ND 06/10/2020 09095.0 2.0 ug/kg1 2-Hexanone ND 06/10/2020 0909104.0 ug/kg1 Isopropylbenzene ND 06/10/2020 09095.0 2.0 ug/kg1 Methyl acetate ND 06/10/2020 09095.0 2.0 ug/kg1 Methyl tertiary butyl ether (MTBE)ND 06/10/2020 09095.0 2.0 ug/kg1 4-Methyl-2-pentanone ND 06/10/2020 0909104.0 ug/kg1 Methylcyclohexane ND 06/10/2020 09095.0 2.0 ug/kg1 Methylene chloride ND 06/10/2020 09095.0 2.0 ug/kg1 Styrene ND 06/10/2020 09095.0 2.0 ug/kg1 1,1,2,2-Tetrachloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 Tetrachloroethene ND 06/10/2020 09095.0 2.0 ug/kg1 Toluene ND 06/10/2020 09095.0 2.0 ug/kg1 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 06/10/2020 09095.0 2.0 ug/kg1 1,2,4-Trichlorobenzene ND 06/10/2020 09095.0 2.0 ug/kg1 1,1,1-Trichloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 1,1,2-Trichloroethane ND 06/10/2020 09095.0 2.0 ug/kg1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 103 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56477-001 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Trichloroethene ND 06/10/2020 09095.0 2.0 ug/kg1 Trichlorofluoromethane ND 06/10/2020 09095.0 2.0 ug/kg1 Vinyl chloride ND 06/10/2020 09095.0 3.0 ug/kg1 Xylenes (total)ND 06/10/2020 0909104.0 ug/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 101 47-138 1,2-Dichloroethane-d4 87 53-142 Toluene-d8 95 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 104 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56477-002 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Acetone 100 06/10/2020 082310510060-1401 Benzene 48 06/10/2020 0823975070-1301 Bromodichloromethane 49 06/10/2020 0823975070-1301 Bromoform 47 06/10/2020 0823955070-1301 Bromomethane (Methyl bromide)46 06/10/2020 0823925070-1301 2-Butanone (MEK)100 06/10/2020 082310210060-1401 Carbon disulfide 46 06/10/2020 0823935070-1301 Carbon tetrachloride 46 06/10/2020 0823935070-1301 Chlorobenzene 49 06/10/2020 0823975070-1301 Chloroethane 46 06/10/2020 0823925070-1301 Chloroform 45 06/10/2020 0823895070-1301 Chloromethane (Methyl chloride)44 06/10/2020 0823875060-1401 Cyclohexane 41 06/10/2020 0823815070-1301 1,2-Dibromo-3-chloropropane (DBCP)44 06/10/2020 0823875070-1301 Dibromochloromethane 48 06/10/2020 0823965070-1301 1,2-Dibromoethane (EDB)48 06/10/2020 0823965070-1301 1,2-Dichlorobenzene 50 06/10/2020 0823995070-1301 1,3-Dichlorobenzene 50 06/10/2020 0823995070-1301 1,4-Dichlorobenzene 50 06/10/2020 0823995070-1301 Dichlorodifluoromethane 45 06/10/2020 0823905060-1401 1,1-Dichloroethane 45 06/10/2020 0823895070-1301 1,2-Dichloroethane 47 06/10/2020 0823945070-1301 1,1-Dichloroethene 46 06/10/2020 0823935070-1301 cis-1,2-Dichloroethene 45 06/10/2020 0823915070-1301 trans-1,2-Dichloroethene 47 06/10/2020 0823935070-1301 1,2-Dichloropropane 47 06/10/2020 0823945070-1301 cis-1,3-Dichloropropene 49 06/10/2020 0823985070-1301 trans-1,3-Dichloropropene 48 06/10/2020 0823955070-1301 Ethylbenzene 50 06/10/2020 0823995070-1301 2-Hexanone 100 06/10/2020 082310310070-1301 Isopropylbenzene 50 06/10/2020 08231015070-1301 Methyl acetate 40 06/10/2020 0823815070-1301 Methyl tertiary butyl ether (MTBE)44 06/10/2020 0823895070-1301 4-Methyl-2-pentanone 89 06/10/2020 08238910070-1301 Methylcyclohexane 48 06/10/2020 0823955070-1301 Methylene chloride 43 06/10/2020 0823855070-1301 Styrene 49 06/10/2020 0823995070-1301 1,1,2,2-Tetrachloroethane 46 06/10/2020 0823935070-1301 Tetrachloroethene 51 06/10/2020 08231025070-1301 Toluene 49 06/10/2020 0823985070-1301 1,1,2-Trichloro-1,2,2-Trifluoroethane 43 06/10/2020 0823865070-1301 1,2,4-Trichlorobenzene 51 06/10/2020 08231025070-1301 1,1,1-Trichloroethane 46 06/10/2020 0823925070-1301 1,1,2-Trichloroethane 47 06/10/2020 0823955070-1301 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 105 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56477-002 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Trichloroethene 50 06/10/2020 08231015070-1301 Trichlorofluoromethane 45 06/10/2020 0823895070-1301 Vinyl chloride 46 06/10/2020 0823925070-1301 Xylenes (total)99 06/10/2020 08239910070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 99 47-138 1,2-Dichloroethane-d4 95 53-142 Toluene-d8 97 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 106 of 170 Volatile Organic Compounds by GC/MS - MS Batch:Prep Method: Sample ID:VF09036-006MS 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Acetone 110 06/10/2020 163111410070-130ND1 Benzene 46 06/10/2020 1631915070-130ND1 Bromodichloromethane 45 06/10/2020 1631905070-130ND1 Bromoform 46 06/10/2020 1631925070-130ND1 Bromomethane (Methyl bromide)41 06/10/2020 1631815070-130ND1 2-Butanone (MEK)110 06/10/2020 163110710070-130ND1 Carbon disulfide 45 06/10/2020 1631895070-130ND1 Carbon tetrachloride 45 06/10/2020 1631895070-130ND1 Chlorobenzene 46 06/10/2020 1631925070-130ND1 Chloroethane 42 06/10/2020 1631835070-130ND1 Chloroform 43 06/10/2020 1631845070-130ND1 Chloromethane (Methyl chloride)39 06/10/2020 1631785060-140ND1 Cyclohexane 46 06/10/2020 1631905070-130ND1 1,2-Dibromo-3-chloropropane (DBCP)44 06/10/2020 1631885070-130ND1 Dibromochloromethane 47 06/10/2020 1631935070-130ND1 1,2-Dibromoethane (EDB)46 06/10/2020 1631925070-130ND1 1,2-Dichlorobenzene 47 06/10/2020 1631935070-130ND1 1,3-Dichlorobenzene 48 06/10/2020 1631945070-130ND1 1,4-Dichlorobenzene 48 06/10/2020 1631945070-130ND1 Dichlorodifluoromethane 48 06/10/2020 1631955060-140ND1 1,1-Dichloroethane 42 06/10/2020 1631835070-130ND1 1,2-Dichloroethane 44 06/10/2020 1631885070-130ND1 1,1-Dichloroethene 46 06/10/2020 1631915070-130ND1 cis-1,2-Dichloroethene 44 06/10/2020 1631875070-130ND1 trans-1,2-Dichloroethene 44 06/10/2020 1631875070-130ND1 1,2-Dichloropropane 45 06/10/2020 1631895070-130ND1 cis-1,3-Dichloropropene 47 06/10/2020 1631935070-130ND1 trans-1,3-Dichloropropene 46 06/10/2020 1631925070-130ND1 Ethylbenzene 47 06/10/2020 1631945070-130ND1 2-Hexanone 110 06/10/2020 163111210070-130ND1 Isopropylbenzene 49 06/10/2020 1631965070-130ND1 Methyl acetate 49 06/10/2020 1631975070-130ND1 Methyl tertiary butyl ether (MTBE)44 06/10/2020 1631865070-130ND1 4-Methyl-2-pentanone 92 06/10/2020 16319110070-130ND1 Methylcyclohexane 55 06/10/2020 16311105070-130ND1 Methylene chloride 41 06/10/2020 1631815070-130ND1 Styrene 48 06/10/2020 1631945070-130ND1 1,1,2,2-Tetrachloroethane 46 06/10/2020 1631905070-130ND1 Tetrachloroethene 50 06/10/2020 1631995070-130ND1 Toluene 47 06/10/2020 1631935070-130ND1 1,1,2-Trichloro-1,2,2-Trifluoroethane 50 06/10/2020 1631995070-130ND1 1,2,4-Trichlorobenzene 47 06/10/2020 1631935070-130ND1 1,1,1-Trichloroethane 43 06/10/2020 1631865070-130ND1 1,1,2-Trichloroethane 47 06/10/2020 1631925070-130ND1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 107 of 170 Volatile Organic Compounds by GC/MS - MS Batch:Prep Method: Sample ID:VF09036-006MS 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Trichloroethene 48 06/10/2020 1631955070-130ND1 Trichlorofluoromethane 47 06/10/2020 1631935070-130ND1 Vinyl chloride 42 06/10/2020 1631845070-130ND1 Xylenes (total)96 06/10/2020 16319510070-130ND1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 93 47-138 1,2-Dichloroethane-d4 88 53-142 Toluene-d8 89 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 108 of 170 Volatile Organic Compounds by GC/MS - Duplicate Batch:Prep Method: Sample ID:VF09036-008DU 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q Analysis Date% RPD % RPD Limit Sample Amount Dil(ug/kg)(ug/kg) Acetone ND 06/10/2020 16540.00 20121 Benzene ND 06/10/2020 16540.00 20ND1 Bromodichloromethane ND 06/10/2020 16540.00 20ND1 Bromoform ND 06/10/2020 16540.00 20ND1 Bromomethane (Methyl bromide)ND 06/10/2020 16540.00 20ND1 2-Butanone (MEK)ND 06/10/2020 16540.00 20ND1 Carbon disulfide ND 06/10/2020 16540.00 20ND1 Carbon tetrachloride ND 06/10/2020 16540.00 20ND1 Chlorobenzene ND 06/10/2020 16540.00 20ND1 Chloroethane ND 06/10/2020 16540.00 20ND1 Chloroform ND 06/10/2020 16540.00 20ND1 Chloromethane (Methyl chloride)ND 06/10/2020 16540.00 20ND1 Cyclohexane ND 06/10/2020 16540.00 20ND1 1,2-Dibromo-3-chloropropane (DBCP)ND 06/10/2020 16540.00 20ND1 Dibromochloromethane ND 06/10/2020 16540.00 20ND1 1,2-Dibromoethane (EDB)ND 06/10/2020 16540.00 20ND1 1,2-Dichlorobenzene ND 06/10/2020 16540.00 20ND1 1,3-Dichlorobenzene ND 06/10/2020 16540.00 20ND1 1,4-Dichlorobenzene ND 06/10/2020 16540.00 20ND1 Dichlorodifluoromethane ND 06/10/2020 16540.00 20ND1 1,1-Dichloroethane ND 06/10/2020 16540.00 20ND1 1,2-Dichloroethane ND 06/10/2020 16540.00 20ND1 1,1-Dichloroethene ND 06/10/2020 16540.00 20ND1 cis-1,2-Dichloroethene ND 06/10/2020 16540.00 20ND1 trans-1,2-Dichloroethene ND 06/10/2020 16540.00 20ND1 1,2-Dichloropropane ND 06/10/2020 16540.00 20ND1 cis-1,3-Dichloropropene ND 06/10/2020 16540.00 20ND1 trans-1,3-Dichloropropene ND 06/10/2020 16540.00 20ND1 Ethylbenzene ND 06/10/2020 16540.00 20ND1 2-Hexanone ND 06/10/2020 16540.00 20ND1 Isopropylbenzene ND 06/10/2020 16540.00 20ND1 Methyl acetate ND 06/10/2020 16540.00 20ND1 Methyl tertiary butyl ether (MTBE)ND 06/10/2020 16540.00 20ND1 4-Methyl-2-pentanone ND 06/10/2020 16540.00 20ND1 Methylcyclohexane ND 06/10/2020 16540.00 20ND1 Methylene chloride ND 06/10/2020 16540.00 20ND1 Styrene ND 06/10/2020 16540.00 20ND1 1,1,2,2-Tetrachloroethane ND 06/10/2020 16540.00 20ND1 Tetrachloroethene ND 06/10/2020 16540.00 20ND1 Toluene ND 06/10/2020 16540.00 20ND1 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 06/10/2020 16540.00 20ND1 1,2,4-Trichlorobenzene ND 06/10/2020 16540.00 20ND1 1,1,1-Trichloroethane ND 06/10/2020 16540.00 20ND1 1,1,2-Trichloroethane ND 06/10/2020 16540.00 20ND1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 109 of 170 Volatile Organic Compounds by GC/MS - Duplicate Batch:Prep Method: Sample ID:VF09036-008DU 56477 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q Analysis Date% RPD % RPD Limit Sample Amount Dil(ug/kg)(ug/kg) Trichloroethene ND 06/10/2020 16540.00 20ND1 Trichlorofluoromethane ND 06/10/2020 16540.00 20ND1 Vinyl chloride ND 06/10/2020 16540.00 20ND1 Xylenes (total)ND 06/10/2020 16540.00 20ND1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 95 47-138 1,2-Dichloroethane-d4 84 53-142 Toluene-d8 101 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 110 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56611-001 56611 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Acetone ND 06/11/2020 0912104.0 ug/L1 Benzene ND 06/11/2020 09120.50 0.40 ug/L1 Bromobenzene ND 06/11/2020 09120.50 0.40 ug/L1 Bromochloromethane ND 06/11/2020 09120.50 0.40 ug/L1 Bromodichloromethane ND 06/11/2020 09120.50 0.40 ug/L1 Bromoform ND 06/11/2020 09120.50 0.40 ug/L1 Bromomethane (Methyl bromide)ND 06/11/2020 09120.50 0.40 ug/L1 2-Butanone (MEK)ND 06/11/2020 0912102.0 ug/L1 n-Butylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 sec-Butylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 tert-Butylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 Carbon tetrachloride ND 06/11/2020 09120.50 0.40 ug/L1 Chlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 Chloroethane ND 06/11/2020 09120.50 0.40 ug/L1 Chloroform ND 06/11/2020 09120.50 0.40 ug/L1 Chloromethane (Methyl chloride)ND 06/11/2020 09120.50 0.40 ug/L1 2-Chlorotoluene ND 06/11/2020 09120.50 0.40 ug/L1 4-Chlorotoluene ND 06/11/2020 09120.50 0.40 ug/L1 Dibromochloromethane ND 06/11/2020 09120.50 0.40 ug/L1 1,2-Dibromoethane (EDB)ND 06/11/2020 09120.50 0.40 ug/L1 Dibromomethane (Methylene bromide)ND 06/11/2020 09120.50 0.40 ug/L1 1,2-Dichlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 1,3-Dichlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 1,4-Dichlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 Dichlorodifluoromethane ND 06/11/2020 09120.50 0.40 ug/L1 1,1-Dichloroethane ND 06/11/2020 09120.50 0.40 ug/L1 1,2-Dichloroethane ND 06/11/2020 09120.50 0.40 ug/L1 1,1-Dichloroethene ND 06/11/2020 09120.50 0.40 ug/L1 cis-1,2-Dichloroethene ND 06/11/2020 09120.50 0.40 ug/L1 trans-1,2-Dichloroethene ND 06/11/2020 09120.50 0.40 ug/L1 1,2-Dichloropropane ND 06/11/2020 09120.50 0.40 ug/L1 1,3-Dichloropropane ND 06/11/2020 09120.50 0.40 ug/L1 2,2-Dichloropropane ND 06/11/2020 09120.50 0.40 ug/L1 1,1-Dichloropropene ND 06/11/2020 09120.50 0.40 ug/L1 cis-1,3-Dichloropropene ND 06/11/2020 09120.50 0.40 ug/L1 trans-1,3-Dichloropropene ND 06/11/2020 09120.50 0.40 ug/L1 Diisopropyl ether (IPE)ND 06/11/2020 09120.50 0.40 ug/L1 Ethylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 Hexachlorobutadiene ND 06/11/2020 09120.50 0.40 ug/L1 2-Hexanone ND 06/11/2020 0912102.0 ug/L1 Isopropylbenzene (Cumene)ND 06/11/2020 09120.50 0.40 ug/L1 p-Isopropyltoluene (p-Cymene)ND 06/11/2020 09120.50 0.40 ug/L1 Methyl tertiary butyl ether (MTBE)ND 06/11/2020 09120.50 0.40 ug/L1 4-Methyl-2-pentanone ND 06/11/2020 0912102.0 ug/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 111 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56611-001 56611 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Methylene chloride ND 06/11/2020 09120.50 0.40 ug/L1 Naphthalene ND 06/11/2020 09120.50 0.40 ug/L1 n-Propylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 Styrene ND 06/11/2020 09120.50 0.40 ug/L1 1,1,1,2-Tetrachloroethane ND 06/11/2020 09120.50 0.40 ug/L1 1,1,2,2-Tetrachloroethane ND 06/11/2020 09120.50 0.40 ug/L1 Tetrachloroethene ND 06/11/2020 09120.50 0.40 ug/L1 Toluene ND 06/11/2020 09120.50 0.40 ug/L1 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 06/11/2020 09120.50 0.40 ug/L1 1,2,3-Trichlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 1,2,4-Trichlorobenzene ND 06/11/2020 09120.50 0.40 ug/L1 1,1,1-Trichloroethane ND 06/11/2020 09120.50 0.40 ug/L1 1,1,2-Trichloroethane ND 06/11/2020 09120.50 0.40 ug/L1 Trichloroethene ND 06/11/2020 09120.50 0.40 ug/L1 Trichlorofluoromethane ND 06/11/2020 09120.50 0.40 ug/L1 1,2,3-Trichloropropane ND 06/11/2020 09120.50 0.40 ug/L1 1,3,5-Trimethylbenzene (Mesitylene)ND 06/11/2020 09120.50 0.40 ug/L1 1,2,4-Trimethylbenzene ND 06/11/2020 09120.50 0.40 ug/L1 Vinyl chloride ND 06/11/2020 09120.50 0.40 ug/L1 m+p - Xylenes ND 06/11/2020 09120.50 0.40 ug/L1 o - Xylenes ND 06/11/2020 09120.50 0.40 ug/L1 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 100 70-130 Bromofluorobenzene 102 70-130 Toluene-d8 103 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 112 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56611-002 56611 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Acetone 83 06/11/2020 08118310060-1401 Benzene 49 06/11/2020 0811975070-1301 Bromobenzene 49 06/11/2020 0811985070-1301 Bromochloromethane 47 06/11/2020 0811955070-1301 Bromodichloromethane 49 06/11/2020 0811985070-1301 Bromoform 50 06/11/2020 08111005070-1301 Bromomethane (Methyl bromide)44 06/11/2020 0811885060-1401 2-Butanone (MEK)100 06/11/2020 081110010060-1401 n-Butylbenzene 55 06/11/2020 08111105070-1301 sec-Butylbenzene 51 06/11/2020 08111025070-1301 tert-Butylbenzene 50 06/11/2020 08111005070-1301 Carbon tetrachloride 48 06/11/2020 0811975070-1301 Chlorobenzene 48 06/11/2020 0811975070-1301 Chloroethane 48 06/11/2020 0811955042-1631 Chloroform 46 06/11/2020 0811935070-1301 Chloromethane (Methyl chloride)50 06/11/2020 08111005020-1581 2-Chlorotoluene 49 06/11/2020 0811975070-1301 4-Chlorotoluene 52 06/11/2020 08111045070-1301 Dibromochloromethane 51 06/11/2020 08111025070-1301 1,2-Dibromoethane (EDB)49 06/11/2020 0811995070-1301 Dibromomethane (Methylene bromide)48 06/11/2020 0811965070-1301 1,2-Dichlorobenzene 48 06/11/2020 0811975070-1301 1,3-Dichlorobenzene 50 06/11/2020 08111005070-1301 1,4-Dichlorobenzene 49 06/11/2020 0811985070-1301 Dichlorodifluoromethane 58 06/11/2020 08111175060-1401 1,1-Dichloroethane 49 06/11/2020 0811975070-1301 1,2-Dichloroethane 47 06/11/2020 0811945070-1301 1,1-Dichloroethene 49 06/11/2020 0811985070-1301 cis-1,2-Dichloroethene 48 06/11/2020 0811975070-1301 trans-1,2-Dichloroethene 49 06/11/2020 0811985070-1301 1,2-Dichloropropane 49 06/11/2020 0811975070-1301 1,3-Dichloropropane 49 06/11/2020 0811975070-1301 2,2-Dichloropropane 49 06/11/2020 0811985070-1301 1,1-Dichloropropene 49 06/11/2020 0811985070-1301 cis-1,3-Dichloropropene 53 06/11/2020 08111065070-1301 trans-1,3-Dichloropropene 53 06/11/2020 08111065070-1301 Diisopropyl ether (IPE)51 06/11/2020 08111015070-1301 Ethylbenzene 51 06/11/2020 08111025070-1301 Hexachlorobutadiene 50 06/11/2020 08111015070-1301 2-Hexanone 110 06/11/2020 081110910060-1401 Isopropylbenzene (Cumene)52 06/11/2020 08111045070-1301 p-Isopropyltoluene (p-Cymene)53 06/11/2020 08111055070-1301 Methyl tertiary butyl ether (MTBE)47 06/11/2020 0811945070-1301 4-Methyl-2-pentanone 110 06/11/2020 081110810070-1301 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 113 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56611-002 56611 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Methylene chloride 47 06/11/2020 0811935070-1301 Naphthalene 47 06/11/2020 0811945050-1401 n-Propylbenzene 53 06/11/2020 08111065070-1301 Styrene 54 06/11/2020 08111085070-1301 1,1,1,2-Tetrachloroethane 50 06/11/2020 0811995070-1301 1,1,2,2-Tetrachloroethane 47 06/11/2020 0811955070-1301 Tetrachloroethene 49 06/11/2020 0811985070-1301 Toluene 49 06/11/2020 0811995070-1301 1,1,2-Trichloro-1,2,2-Trifluoroethane 50 06/11/2020 08111005070-1301 1,2,3-Trichlorobenzene 56 06/11/2020 08111115070-1301 1,2,4-Trichlorobenzene 55 06/11/2020 08111115070-1301 1,1,1-Trichloroethane 49 06/11/2020 0811985070-1301 1,1,2-Trichloroethane 48 06/11/2020 0811965070-1301 Trichloroethene 48 06/11/2020 0811965070-1301 Trichlorofluoromethane 50 06/11/2020 0811995060-1401 1,2,3-Trichloropropane 46 06/11/2020 0811935070-1301 1,3,5-Trimethylbenzene (Mesitylene)51 06/11/2020 08111025070-1301 1,2,4-Trimethylbenzene 51 06/11/2020 08111025070-1301 Vinyl chloride 50 06/11/2020 08111005060-1401 m+p - Xylenes 51 06/11/2020 08111035070-1301 o - Xylenes 51 06/11/2020 08111025070-1301 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 90 70-130 Bromofluorobenzene 95 70-130 Toluene-d8 94 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 114 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56630-001 56630 5035 High Analytical Method:8260D Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Ethylbenzene ND 06/11/2020 1158250100ug/kg1 Xylenes (total)ND 06/11/2020 1158500200ug/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 96 47-138 1,2-Dichloroethane-d4 84 53-142 Toluene-d8 95 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 115 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56630-002 56630 5035 High Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Ethylbenzene 3000 06/11/2020 1135121250070-1301 Xylenes (total)6000 06/11/2020 1135120500070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 111 47-138 1,2-Dichloroethane-d4 96 53-142 Toluene-d8 109 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 116 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ56756-001 56756 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Ethylbenzene ND 06/12/2020 09205.0 2.0 ug/kg1 Xylenes (total)ND 06/12/2020 0920104.0 ug/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 103 47-138 1,2-Dichloroethane-d4 84 53-142 Toluene-d8 97 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 117 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ56756-002 56756 5035 Analytical Method:8260D Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Ethylbenzene 48 06/12/2020 0834965070-1301 Xylenes (total)97 06/12/2020 08349710070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 98 47-138 1,2-Dichloroethane-d4 88 53-142 Toluene-d8 92 68-124 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 118 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ57073-001 57073 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Acetone ND 06/16/2020 0938104.0 ug/L1 Benzene ND 06/16/2020 09380.50 0.40 ug/L1 Bromobenzene ND 06/16/2020 09380.50 0.40 ug/L1 Bromochloromethane ND 06/16/2020 09380.50 0.40 ug/L1 Bromodichloromethane ND 06/16/2020 09380.50 0.40 ug/L1 Bromoform ND 06/16/2020 09380.50 0.40 ug/L1 Bromomethane (Methyl bromide)ND 06/16/2020 09380.50 0.40 ug/L1 2-Butanone (MEK)ND 06/16/2020 0938102.0 ug/L1 n-Butylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 sec-Butylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 tert-Butylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 Carbon tetrachloride ND 06/16/2020 09380.50 0.40 ug/L1 Chlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 Chloroethane ND 06/16/2020 09380.50 0.40 ug/L1 Chloroform ND 06/16/2020 09380.50 0.40 ug/L1 Chloromethane (Methyl chloride)ND 06/16/2020 09380.50 0.40 ug/L1 2-Chlorotoluene ND 06/16/2020 09380.50 0.40 ug/L1 4-Chlorotoluene ND 06/16/2020 09380.50 0.40 ug/L1 Dibromochloromethane ND 06/16/2020 09380.50 0.40 ug/L1 1,2-Dibromoethane (EDB)ND 06/16/2020 09380.50 0.40 ug/L1 Dibromomethane (Methylene bromide)ND 06/16/2020 09380.50 0.40 ug/L1 1,2-Dichlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 1,3-Dichlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 1,4-Dichlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 Dichlorodifluoromethane ND 06/16/2020 09380.50 0.40 ug/L1 1,1-Dichloroethane ND 06/16/2020 09380.50 0.40 ug/L1 1,2-Dichloroethane ND 06/16/2020 09380.50 0.40 ug/L1 1,1-Dichloroethene ND 06/16/2020 09380.50 0.40 ug/L1 cis-1,2-Dichloroethene ND 06/16/2020 09380.50 0.40 ug/L1 trans-1,2-Dichloroethene ND 06/16/2020 09380.50 0.40 ug/L1 1,2-Dichloropropane ND 06/16/2020 09380.50 0.40 ug/L1 1,3-Dichloropropane ND 06/16/2020 09380.50 0.40 ug/L1 2,2-Dichloropropane ND 06/16/2020 09380.50 0.40 ug/L1 1,1-Dichloropropene ND 06/16/2020 09380.50 0.40 ug/L1 cis-1,3-Dichloropropene ND 06/16/2020 09380.50 0.40 ug/L1 trans-1,3-Dichloropropene ND 06/16/2020 09380.50 0.40 ug/L1 Diisopropyl ether (IPE)ND 06/16/2020 09380.50 0.40 ug/L1 Ethylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 Hexachlorobutadiene ND 06/16/2020 09380.50 0.40 ug/L1 2-Hexanone ND 06/16/2020 0938102.0 ug/L1 Isopropylbenzene (Cumene)ND 06/16/2020 09380.50 0.40 ug/L1 p-Isopropyltoluene (p-Cymene)ND 06/16/2020 09380.50 0.40 ug/L1 Methyl tertiary butyl ether (MTBE)ND 06/16/2020 09380.50 0.40 ug/L1 4-Methyl-2-pentanone ND 06/16/2020 0938102.0 ug/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 119 of 170 Volatile Organic Compounds by GC/MS - MB Batch:Prep Method: Sample ID:VQ57073-001 57073 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Methylene chloride ND 06/16/2020 09380.50 0.40 ug/L1 Naphthalene ND 06/16/2020 09380.50 0.40 ug/L1 n-Propylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 Styrene ND 06/16/2020 09380.50 0.40 ug/L1 1,1,1,2-Tetrachloroethane ND 06/16/2020 09380.50 0.40 ug/L1 1,1,2,2-Tetrachloroethane ND 06/16/2020 09380.50 0.40 ug/L1 Tetrachloroethene ND 06/16/2020 09380.50 0.40 ug/L1 Toluene ND 06/16/2020 09380.50 0.40 ug/L1 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 06/16/2020 09380.50 0.40 ug/L1 1,2,3-Trichlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 1,2,4-Trichlorobenzene ND 06/16/2020 09380.50 0.40 ug/L1 1,1,1-Trichloroethane ND 06/16/2020 09380.50 0.40 ug/L1 1,1,2-Trichloroethane ND 06/16/2020 09380.50 0.40 ug/L1 Trichloroethene ND 06/16/2020 09380.50 0.40 ug/L1 Trichlorofluoromethane ND 06/16/2020 09380.50 0.40 ug/L1 1,2,3-Trichloropropane ND 06/16/2020 09380.50 0.40 ug/L1 1,3,5-Trimethylbenzene (Mesitylene)ND 06/16/2020 09380.50 0.40 ug/L1 1,2,4-Trimethylbenzene ND 06/16/2020 09380.50 0.40 ug/L1 Vinyl chloride ND 06/16/2020 09380.50 0.40 ug/L1 m+p - Xylenes ND 06/16/2020 09380.50 0.40 ug/L1 o - Xylenes ND 06/16/2020 09380.50 0.40 ug/L1 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 104 70-130 Bromofluorobenzene 98 70-130 Toluene-d8 103 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 120 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ57073-002 57073 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Acetone 76 06/16/2020 08257610060-1401 Benzene 48 06/16/2020 0825975070-1301 Bromobenzene 46 06/16/2020 0825925070-1301 Bromochloromethane 47 06/16/2020 0825945070-1301 Bromodichloromethane 48 06/16/2020 0825965070-1301 Bromoform 47 06/16/2020 0825935070-1301 Bromomethane (Methyl bromide)50 06/16/2020 0825995060-1401 2-Butanone (MEK)95 06/16/2020 08259510060-1401 n-Butylbenzene 52 06/16/2020 08251055070-1301 sec-Butylbenzene 48 06/16/2020 0825965070-1301 tert-Butylbenzene 47 06/16/2020 0825935070-1301 Carbon tetrachloride 48 06/16/2020 0825975070-1301 Chlorobenzene 47 06/16/2020 0825945070-1301 Chloroethane 54 06/16/2020 08251075042-1631 Chloroform 47 06/16/2020 0825945070-1301 Chloromethane (Methyl chloride)54 06/16/2020 08251085020-1581 2-Chlorotoluene 46 06/16/2020 0825915070-1301 4-Chlorotoluene 49 06/16/2020 0825995070-1301 Dibromochloromethane 49 06/16/2020 0825985070-1301 1,2-Dibromoethane (EDB)49 06/16/2020 0825985070-1301 Dibromomethane (Methylene bromide)48 06/16/2020 0825965070-1301 1,2-Dichlorobenzene 46 06/16/2020 0825925070-1301 1,3-Dichlorobenzene 48 06/16/2020 0825955070-1301 1,4-Dichlorobenzene 46 06/16/2020 0825935070-1301 Dichlorodifluoromethane 59 06/16/2020 08251185060-1401 1,1-Dichloroethane 49 06/16/2020 0825975070-1301 1,2-Dichloroethane 47 06/16/2020 0825955070-1301 1,1-Dichloroethene 50 06/16/2020 08251005070-1301 cis-1,2-Dichloroethene 48 06/16/2020 0825965070-1301 trans-1,2-Dichloroethene 49 06/16/2020 0825985070-1301 1,2-Dichloropropane 48 06/16/2020 0825955070-1301 1,3-Dichloropropane 48 06/16/2020 0825965070-1301 2,2-Dichloropropane 51 06/16/2020 08251025070-1301 1,1-Dichloropropene 48 06/16/2020 0825965070-1301 cis-1,3-Dichloropropene 51 06/16/2020 08251025070-1301 trans-1,3-Dichloropropene 51 06/16/2020 08251025070-1301 Diisopropyl ether (IPE)50 06/16/2020 08251005070-1301 Ethylbenzene 50 06/16/2020 08251005070-1301 Hexachlorobutadiene 48 06/16/2020 0825955070-1301 2-Hexanone 110 06/16/2020 082510510060-1401 Isopropylbenzene (Cumene)51 06/16/2020 08251015070-1301 p-Isopropyltoluene (p-Cymene)50 06/16/2020 08251005070-1301 Methyl tertiary butyl ether (MTBE)47 06/16/2020 0825945070-1301 4-Methyl-2-pentanone 110 06/16/2020 082510710070-1301 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 121 of 170 Volatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Sample ID:VQ57073-002 57073 SM 6200B-2011 Analytical Method:SM 6200B-2011 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Methylene chloride 50 06/16/2020 0825995070-1301 Naphthalene 43 06/16/2020 0825865050-1401 n-Propylbenzene 50 06/16/2020 08251005070-1301 Styrene 53 06/16/2020 08251065070-1301 1,1,1,2-Tetrachloroethane 49 06/16/2020 0825975070-1301 1,1,2,2-Tetrachloroethane 45 06/16/2020 0825905070-1301 Tetrachloroethene 48 06/16/2020 0825955070-1301 Toluene 49 06/16/2020 0825975070-1301 1,1,2-Trichloro-1,2,2-Trifluoroethane 51 06/16/2020 08251035070-1301 1,2,3-Trichlorobenzene 51 06/16/2020 08251035070-1301 1,2,4-Trichlorobenzene 50 06/16/2020 0825995070-1301 1,1,1-Trichloroethane 49 06/16/2020 0825975070-1301 1,1,2-Trichloroethane 47 06/16/2020 0825945070-1301 Trichloroethene 47 06/16/2020 0825945070-1301 Trichlorofluoromethane 55 06/16/2020 08251115060-1401 1,2,3-Trichloropropane 44 06/16/2020 0825885070-1301 1,3,5-Trimethylbenzene (Mesitylene)48 06/16/2020 0825965070-1301 1,2,4-Trimethylbenzene 48 06/16/2020 0825975070-1301 Vinyl chloride 55 06/16/2020 08251105060-1401 m+p - Xylenes 50 06/16/2020 08251005070-1301 o - Xylenes 50 06/16/2020 0825995070-1301 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 93 70-130 Bromofluorobenzene 97 70-130 Toluene-d8 96 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 122 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ56546-001 56546 625.1 06/10/2020 1759Analytical Method:625.1 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Acenaphthene ND 06/16/2020 11151.6 0.80 ug/L1 Acenaphthylene ND 06/16/2020 11151.6 0.80 ug/L1 Anthracene ND 06/16/2020 11151.6 0.80 ug/L1 Benzo(a)anthracene ND 06/16/2020 11151.6 0.80 ug/L1 Benzo(a)pyrene ND 06/16/2020 11151.6 0.80 ug/L1 Benzo(b)fluoranthene ND 06/16/2020 11151.6 0.80 ug/L1 Benzo(g,h,i)perylene ND 06/16/2020 11151.6 0.80 ug/L1 Benzo(k)fluoranthene ND 06/16/2020 11151.6 0.80 ug/L1 Benzyl alcohol ND 06/16/2020 11153.2 2.0 ug/L1 4-Bromophenyl phenyl ether ND 06/16/2020 11151.6 0.80 ug/L1 Butyl benzyl phthalate ND 06/16/2020 11151.6 0.80 ug/L1 bis (2-Chloro-1-methylethyl) ether ND 06/16/2020 11151.6 0.80 ug/L1 4-Chloro-3-methyl phenol ND 06/16/2020 11151.6 0.80 ug/L1 bis(2-Chloroethoxy)methane ND 06/16/2020 11151.6 0.80 ug/L1 bis(2-Chloroethyl)ether ND 06/16/2020 11151.6 0.80 ug/L1 2-Chloronaphthalene ND 06/16/2020 11151.6 0.80 ug/L1 2-Chlorophenol ND 06/16/2020 11151.6 0.80 ug/L1 4-Chlorophenyl phenyl ether ND 06/16/2020 11151.6 0.80 ug/L1 Chrysene ND 06/16/2020 11151.6 0.80 ug/L1 Dibenzo(a,h)anthracene ND 06/16/2020 11151.6 0.80 ug/L1 Dibenzofuran ND 06/16/2020 11151.6 1.0 ug/L1 3,3'-Dichlorobenzidine ND 06/16/2020 11158.0 0.80 ug/L1 2,4-Dichlorophenol ND 06/16/2020 11151.6 0.80 ug/L1 Diethylphthalate 0.84 06/16/2020 1115J1.6 0.80 ug/L1 Dimethyl phthalate ND 06/16/2020 11151.6 0.80 ug/L1 2,4-Dimethylphenol ND 06/16/2020 11151.6 0.80 ug/L1 Di-n-butyl phthalate 1.7 06/16/2020 11151.6 0.81 ug/L1 4,6-Dinitro-2-methylphenol ND 06/16/2020 11158.0 0.80 ug/L1 2,4-Dinitrophenol ND 06/16/2020 11158.0 0.80 ug/L1 Di-n-octylphthalate ND 06/16/2020 11151.6 0.80 ug/L1 1,2-Diphenylhydrazine(as azobenzene)ND 06/16/2020 11151.6 0.80 ug/L1 bis(2-Ethylhexyl)phthalate ND 06/16/2020 11158.0 4.0 ug/L1 Fluoranthene ND 06/16/2020 11151.6 0.80 ug/L1 Fluorene ND 06/16/2020 11151.6 0.80 ug/L1 Hexachlorobenzene ND 06/16/2020 11151.6 0.80 ug/L1 Hexachlorobutadiene ND 06/16/2020 11151.6 0.80 ug/L1 Hexachlorocyclopentadiene ND 06/16/2020 11158.0 4.0 ug/L1 Hexachloroethane ND 06/16/2020 11151.6 0.80 ug/L1 Indeno(1,2,3-c,d)pyrene ND 06/16/2020 11151.6 0.80 ug/L1 Isophorone ND 06/16/2020 11151.6 0.80 ug/L1 1-Methylnaphthalene ND 06/16/2020 11151.6 0.40 ug/L1 2-Methylnaphthalene ND 06/16/2020 11151.6 0.40 ug/L1 2-Methylphenol ND 06/16/2020 11151.6 0.67 ug/L1 3+4-Methylphenol ND 06/16/2020 11151.6 1.5 ug/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 123 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ56546-001 56546 625.1 06/10/2020 1759Analytical Method:625.1 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Naphthalene ND 06/16/2020 11151.6 0.80 ug/L1 Nitrobenzene ND 06/16/2020 11151.6 0.80 ug/L1 2-Nitrophenol ND 06/16/2020 11153.2 0.80 ug/L1 4-Nitrophenol ND 06/16/2020 11158.0 4.0 ug/L1 N-Nitrosodi-n-propylamine ND 06/16/2020 11151.6 0.80 ug/L1 N-Nitrosodiphenylamine (Diphenylamine)ND 06/16/2020 11151.6 0.80 ug/L1 Pentachlorophenol ND 06/16/2020 11158.0 4.0 ug/L1 Phenanthrene ND 06/16/2020 11151.6 0.80 ug/L1 Phenol ND 06/16/2020 11151.6 0.80 ug/L1 Pyrene ND 06/16/2020 11151.6 0.80 ug/L1 1,2,4-Trichlorobenzene ND 06/16/2020 11151.6 0.80 ug/L1 2,4,6-Trichlorophenol ND 06/16/2020 11151.6 0.80 ug/L1 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 92 37-129 2-Fluorophenol 48 24-127 Nitrobenzene-d5 85 38-127 Phenol-d5 68 28-128 Terphenyl-d14 117 10-148 2,4,6-Tribromophenol 93 41-144 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 124 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56546-002 56546 625.1 06/10/2020 1759Analytical Method:625.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Acenaphthene 19 06/16/2020 1140942047-1451 Acenaphthylene 20 06/16/2020 1140982033-1451 Anthracene 20 06/16/2020 11401012027-1331 Benzo(a)anthracene 22 06/16/2020 11401102033-1431 Benzo(a)pyrene 20 06/16/2020 1140992017-1631 Benzo(b)fluoranthene 22 06/16/2020 11401112024-1591 Benzo(g,h,i)perylene 24 06/16/2020 1140119201-2191 Benzo(k)fluoranthene 22 06/16/2020 11401082011-1621 Benzyl alcohol 16 06/16/2020 1140792030-1301 4-Bromophenyl phenyl ether 19 06/16/2020 1140962053-1271 Butyl benzyl phthalate 26 06/16/2020 1140130201-1521 bis (2-Chloro-1-methylethyl) ether 23 06/16/2020 11401142036-1661 4-Chloro-3-methyl phenol 19 06/16/2020 1140952022-1471 bis(2-Chloroethoxy)methane 19 06/16/2020 1140942033-1841 bis(2-Chloroethyl)ether 21 06/16/2020 11401072012-1581 2-Chloronaphthalene 19 06/16/2020 1140932060-1201 2-Chlorophenol 18 06/16/2020 1140892023-1341 4-Chlorophenyl phenyl ether 19 06/16/2020 1140952025-1581 Chrysene 22 06/16/2020 11401122017-1681 Dibenzo(a,h)anthracene 24 06/16/2020 1140118201-2271 Dibenzofuran 19 06/16/2020 1140952048-1181 3,3'-Dichlorobenzidine 4.2 06/16/2020 114021201-2621 2,4-Dichlorophenol 17 06/16/2020 1140852039-1351 Diethylphthalate 22 06/16/2020 1140108201-1201 Dimethyl phthalate 21 06/16/2020 1140104201-1201 2,4-Dimethylphenol 20 06/16/2020 11401012032-1201 Di-n-butyl phthalate 23 06/16/2020 1140115201-1201 4,6-Dinitro-2-methylphenol 18 06/16/2020 114091201-1811 2,4-Dinitrophenol 29 06/16/2020 114073401-1911 Di-n-octylphthalate 22 06/16/2020 1140109204-1461 1,2-Diphenylhydrazine(as azobenzene)18 06/16/2020 114092201-1501 bis(2-Ethylhexyl)phthalate 26 06/16/2020 1140131208-1581 Fluoranthene 20 06/16/2020 11401002026-1371 Fluorene 19 06/16/2020 1140972059-1211 Hexachlorobenzene 19 06/16/2020 114096201-1521 Hexachlorobutadiene 15 06/16/2020 1140752024-1201 Hexachlorocyclopentadiene 45 06/16/2020 1140451001-1501 Hexachloroethane 16 06/16/2020 1140802040-1201 Indeno(1,2,3-c,d)pyrene 22 06/16/2020 1140112201-1711 Isophorone 20 06/16/2020 11401012021-1961 1-Methylnaphthalene 18 06/16/2020 1140892042-1261 2-Methylnaphthalene 18 06/16/2020 1140892040-1321 2-Methylphenol 19 06/16/2020 1140952030-1301 3+4-Methylphenol 21 06/16/2020 11401072030-1301 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 125 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56546-002 56546 625.1 06/10/2020 1759Analytical Method:625.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) Naphthalene 18 06/16/2020 1140892021-1331 Nitrobenzene 20 06/16/2020 11401002035-1801 2-Nitrophenol 19 06/16/2020 1140932029-1821 4-Nitrophenol 39 06/16/2020 114097401-1321 N-Nitrosodi-n-propylamine 24 06/16/2020 1140121201-2301 N-Nitrosodiphenylamine (Diphenylamine)9.6 06/16/2020 114048201-1501 Pentachlorophenol 33 06/16/2020 1140834014-1761 Phenanthrene 20 06/16/2020 1140992054-1201 Phenol 17 06/16/2020 114083205-1201 Pyrene 23 06/16/2020 11401162052-1201 1,2,4-Trichlorobenzene 16 06/16/2020 1140802044-1421 2,4,6-Trichlorophenol 18 06/16/2020 1140922037-1441 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 94 37-129 2-Fluorophenol 47 24-127 Nitrobenzene-d5 86 38-127 Phenol-d5 84 28-128 Terphenyl-d14 113 10-148 2,4,6-Tribromophenol 100 41-144 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 126 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ56992-001 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Acenaphthene ND 06/16/2020 10262.7 0.83 ug/kg1 Acenaphthylene ND 06/16/2020 10262.7 0.95 ug/kg1 Acetophenone ND 06/16/2020 1026135.0 ug/kg1 Anthracene ND 06/16/2020 10262.7 0.51 ug/kg1 Atrazine ND 06/16/2020 1026135.0 ug/kg1 Benzaldehyde ND 06/16/2020 1026135.0 ug/kg1 Benzo(a)anthracene ND 06/16/2020 10262.7 0.59 ug/kg1 Benzo(a)pyrene ND 06/16/2020 10262.7 0.66 ug/kg1 Benzo(b)fluoranthene ND 06/16/2020 10262.7 0.50 ug/kg1 Benzo(g,h,i)perylene ND 06/16/2020 10262.7 0.65 ug/kg1 Benzo(k)fluoranthene ND 06/16/2020 10262.7 0.48 ug/kg1 1,1'-Biphenyl ND 06/16/2020 1026135.0 ug/kg1 4-Bromophenyl phenyl ether ND 06/16/2020 1026135.0 ug/kg1 Butyl benzyl phthalate ND 06/16/2020 1026135.0 ug/kg1 Caprolactam ND 06/16/2020 1026135.0 ug/kg1 Carbazole ND 06/16/2020 1026135.0 ug/kg1 bis (2-Chloro-1-methylethyl) ether ND 06/16/2020 1026135.0 ug/kg1 4-Chloro-3-methyl phenol ND 06/16/2020 1026135.0 ug/kg1 4-Chloroaniline ND 06/16/2020 1026135.0 ug/kg1 bis(2-Chloroethoxy)methane ND 06/16/2020 1026135.0 ug/kg1 bis(2-Chloroethyl)ether ND 06/16/2020 1026135.0 ug/kg1 2-Chloronaphthalene ND 06/16/2020 1026135.0 ug/kg1 2-Chlorophenol ND 06/16/2020 1026135.0 ug/kg1 4-Chlorophenyl phenyl ether ND 06/16/2020 1026135.0 ug/kg1 Chrysene ND 06/16/2020 10262.7 0.45 ug/kg1 Dibenzo(a,h)anthracene ND 06/16/2020 10262.7 0.51 ug/kg1 Dibenzofuran ND 06/16/2020 1026135.0 ug/kg1 3,3'-Dichlorobenzidine ND 06/16/2020 1026135.0 ug/kg1 2,4-Dichlorophenol ND 06/16/2020 1026135.0 ug/kg1 Diethylphthalate ND 06/16/2020 1026135.0 ug/kg1 Dimethyl phthalate ND 06/16/2020 1026137.4 ug/kg1 2,4-Dimethylphenol ND 06/16/2020 1026135.0 ug/kg1 Di-n-butyl phthalate 7.9 06/16/2020 1026J135.0 ug/kg1 4,6-Dinitro-2-methylphenol ND 06/16/2020 10266725ug/kg1 2,4-Dinitrophenol ND 06/16/2020 10266725ug/kg1 2,4-Dinitrotoluene ND 06/16/2020 10262710ug/kg1 2,6-Dinitrotoluene ND 06/16/2020 10262710ug/kg1 Di-n-octylphthalate ND 06/16/2020 1026135.0 ug/kg1 bis(2-Ethylhexyl)phthalate ND 06/16/2020 10266725ug/kg1 Fluoranthene ND 06/16/2020 10262.7 0.42 ug/kg1 Fluorene ND 06/16/2020 10262.7 0.57 ug/kg1 Hexachlorobenzene ND 06/16/2020 1026135.0 ug/kg1 Hexachlorobutadiene ND 06/16/2020 1026135.0 ug/kg1 Hexachlorocyclopentadiene ND 06/16/2020 10266725ug/kg1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 127 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ56992-001 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Hexachloroethane ND 06/16/2020 1026135.0 ug/kg1 Indeno(1,2,3-c,d)pyrene ND 06/16/2020 10262.7 1.0 ug/kg1 Isophorone ND 06/16/2020 1026135.0 ug/kg1 2-Methylnaphthalene ND 06/16/2020 10262.7 0.99 ug/kg1 2-Methylphenol ND 06/16/2020 1026135.0 ug/kg1 3+4-Methylphenol ND 06/16/2020 10262710ug/kg1 Naphthalene ND 06/16/2020 10262.7 0.97 ug/kg1 2-Nitroaniline ND 06/16/2020 10262710ug/kg1 3-Nitroaniline ND 06/16/2020 10262710ug/kg1 4-Nitroaniline ND 06/16/2020 10262710ug/kg1 Nitrobenzene ND 06/16/2020 1026135.0 ug/kg1 2-Nitrophenol ND 06/16/2020 10262710ug/kg1 4-Nitrophenol ND 06/16/2020 10266725ug/kg1 N-Nitrosodi-n-propylamine ND 06/16/2020 1026135.0 ug/kg1 N-Nitrosodiphenylamine (Diphenylamine)ND 06/16/2020 1026135.0 ug/kg1 Pentachlorophenol ND 06/16/2020 10266725ug/kg1 Phenanthrene ND 06/16/2020 10262.7 0.72 ug/kg1 Phenol ND 06/16/2020 1026135.0 ug/kg1 Pyrene ND 06/16/2020 10262.7 0.50 ug/kg1 Pyridine ND 06/16/2020 1026135.0 ug/kg1 2,4,5-Trichlorophenol ND 06/16/2020 1026135.0 ug/kg1 2,4,6-Trichlorophenol ND 06/16/2020 1026135.0 ug/kg1 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 69 33-102 2-Fluorophenol 88 35-115 Nitrobenzene-d5 77 22-109 Phenol-d5 101 33-122 Terphenyl-d14 88 41-120 2,4,6-Tribromophenol 93 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 128 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56992-002 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Acenaphthene 100 06/16/2020 10517713012-1111 Acenaphthylene 110 06/16/2020 10518313044-1221 Acetophenone 110 06/16/2020 10518013048-1111 Anthracene 110 06/16/2020 10518513016-1221 Atrazine 110 06/16/2020 10518513048-1161 Benzaldehyde 48 06/16/2020 10513613010-1101 Benzo(a)anthracene 130 06/16/2020 10519413040-1211 Benzo(a)pyrene 120 06/16/2020 10519113036-1141 Benzo(b)fluoranthene 120 06/16/2020 10519113038-1231 Benzo(g,h,i)perylene 130 06/16/2020 10519913043-1201 Benzo(k)fluoranthene 120 06/16/2020 10518713040-1261 1,1'-Biphenyl 100 06/16/2020 10517913049-1101 4-Bromophenyl phenyl ether 100 06/16/2020 10517713046-1181 Butyl benzyl phthalate 140 06/16/2020 105110813046-1281 Caprolactam 140 06/16/2020 105110713043-1211 Carbazole 120 06/16/2020 10519313047-1281 bis (2-Chloro-1-methylethyl) ether 110 06/16/2020 10518213031-1021 4-Chloro-3-methyl phenol 120 06/16/2020 10519013049-1181 4-Chloroaniline 63 06/16/2020 10514713017-1061 bis(2-Chloroethoxy)methane 110 06/16/2020 10518513039-1081 bis(2-Chloroethyl)ether 110 06/16/2020 10518413032-1051 2-Chloronaphthalene 100 06/16/2020 10517813031-1271 2-Chlorophenol 120 06/16/2020 10518813037-1061 4-Chlorophenyl phenyl ether 100 06/16/2020 10517713047-1161 Chrysene 120 06/16/2020 10519213041-1241 Dibenzo(a,h)anthracene 130 06/16/2020 10519513038-1251 Dibenzofuran 110 06/16/2020 10517913045-1121 3,3'-Dichlorobenzidine 110 06/16/2020 10518113010-1191 2,4-Dichlorophenol 110 06/16/2020 10518513041-1131 Diethylphthalate 120 06/16/2020 10518813049-1231 Dimethyl phthalate 120 06/16/2020 10518713048-1201 2,4-Dimethylphenol 140 06/16/2020 105110413033-1231 Di-n-butyl phthalate 130 06/16/2020 10519913051-1291 4,6-Dinitro-2-methylphenol 110 06/16/2020 10518113040-1301 2,4-Dinitrophenol 190 06/16/2020 10517227032-1151 2,4-Dinitrotoluene 120 06/16/2020 10519013048-1241 2,6-Dinitrotoluene 120 06/16/2020 10518713047-1251 Di-n-octylphthalate 120 06/16/2020 10518813049-1421 bis(2-Ethylhexyl)phthalate 130 06/16/2020 105110013045-1281 Fluoranthene 110 06/16/2020 10518413026-1331 Fluorene 110 06/16/2020 10517913019-1081 Hexachlorobenzene 100 06/16/2020 10517613044-1221 Hexachlorobutadiene 90 06/16/2020 10516713033-1031 Hexachlorocyclopentadiene 420 06/16/2020 10516467018-1211 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 129 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56992-002 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Hexachloroethane 89 06/16/2020 10516713030-961 Indeno(1,2,3-c,d)pyrene 130 06/16/2020 10519513042-1231 Isophorone 120 06/16/2020 10519013041-1131 2-Methylnaphthalene 110 06/16/2020 10517913010-1071 2-Methylphenol 110 06/16/2020 10518613032-1071 3+4-Methylphenol 120 06/16/2020 10519213039-1081 Naphthalene 110 06/16/2020 10518113010-1121 2-Nitroaniline 130 06/16/2020 10519513045-1231 3-Nitroaniline 93 06/16/2020 10517013024-1271 4-Nitroaniline 130 06/16/2020 10519513048-1271 Nitrobenzene 100 06/16/2020 10517813033-1141 2-Nitrophenol 110 06/16/2020 10518413035-1081 4-Nitrophenol 220 06/16/2020 10518127018-1541 N-Nitrosodi-n-propylamine 120 06/16/2020 10518913032-1151 N-Nitrosodiphenylamine (Diphenylamine)120 06/16/2020 10518913053-1501 Pentachlorophenol 200 06/16/2020 10517427027-1381 Phenanthrene 110 06/16/2020 10518113016-1231 Phenol 120 06/16/2020 10519213036-1081 Pyrene 130 06/16/2020 10519713034-1211 Pyridine 110 06/16/2020 10517913030-1301 2,4,5-Trichlorophenol 110 06/16/2020 10518613046-1221 2,4,6-Trichlorophenol 110 06/16/2020 10518113038-1151 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 69 33-102 2-Fluorophenol 84 35-115 Nitrobenzene-d5 77 22-109 Phenol-d5 95 33-122 Terphenyl-d14 88 41-120 2,4,6-Tribromophenol 83 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 130 of 170 Semivolatile Organic Compounds by GC/MS - MS Batch:Prep Method: Prep Date: Sample ID:VF09036-007MS 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Acenaphthene 100 06/16/2020 19017114012-111ND1 Acenaphthylene 110 06/16/2020 19017714044-122ND1 Acetophenone 100 06/16/2020 19017314030-130ND1 Anthracene 110 06/16/2020 19017914016-1222.4 1 Atrazine 110 06/16/2020 19017914030-130ND1 Benzaldehyde 61 06/16/2020 19014314010-110ND1 Benzo(a)anthracene 130 06/16/2020 19018814040-121ND1 Benzo(a)pyrene 130 06/16/2020 19018814036-114ND1 Benzo(b)fluoranthene 120 06/16/2020 19018514038-123ND1 Benzo(g,h,i)perylene 120 06/16/2020 19018714043-120ND1 Benzo(k)fluoranthene 120 06/16/2020 19018614040-126ND1 1,1'-Biphenyl 110 06/16/2020 19017414030-130ND1 4-Bromophenyl phenyl ether 100 06/16/2020 19017114030-130ND1 Butyl benzyl phthalate 170 06/16/2020 190111914030-130ND1 Caprolactam 130 06/16/2020 19019514030-130ND1 Carbazole 120 06/16/2020 19018414030-130ND1 bis (2-Chloro-1-methylethyl) ether 110 06/16/2020 19017714030-130ND1 4-Chloro-3-methyl phenol 120 06/16/2020 19018214030-130ND1 4-Chloroaniline 75 06/16/2020 19015314017-106ND1 bis(2-Chloroethoxy)methane 110 06/16/2020 19017814030-130ND1 bis(2-Chloroethyl)ether 110 06/16/2020 19017714030-130ND1 2-Chloronaphthalene 100 06/16/2020 19017214030-130ND1 2-Chlorophenol 110 06/16/2020 19017814030-130ND1 4-Chlorophenyl phenyl ether 100 06/16/2020 19017214030-130ND1 Chrysene 120 06/16/2020 19018614041-124ND1 Dibenzo(a,h)anthracene 120 06/16/2020 19018814038-125ND1 Dibenzofuran 100 06/16/2020 19017414030-130ND1 3,3'-Dichlorobenzidine 100 06/16/2020 19017214010-119ND1 2,4-Dichlorophenol 110 06/16/2020 19017714030-130ND1 Diethylphthalate 120 06/16/2020 19018414030-130ND1 Dimethyl phthalate 110 06/16/2020 19018114030-130ND1 2,4-Dimethylphenol 140 06/16/2020 19019614030-130ND1 Di-n-butyl phthalate 130 06/16/2020 19018914030-1306.4 1 4,6-Dinitro-2-methylphenol 86 06/16/2020 19016014030-130ND1 2,4-Dinitrophenol 130 06/16/2020 19014628030-130ND1 2,4-Dinitrotoluene 120 06/16/2020 19018514030-130ND1 2,6-Dinitrotoluene 110 06/16/2020 19018014030-130ND1 Di-n-octylphthalate 130 06/16/2020 19018914030-130ND1 bis(2-Ethylhexyl)phthalate 140 06/16/2020 19019814030-130ND1 Fluoranthene 110 06/16/2020 19017714026-133ND1 Fluorene 110 06/16/2020 19017314019-1081.5 1 Hexachlorobenzene 100 06/16/2020 19017114030-130ND1 Hexachlorobutadiene 90 06/16/2020 19016314030-130ND1 Hexachlorocyclopentadiene 350 06/16/2020 19014971030-130ND1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 131 of 170 Semivolatile Organic Compounds by GC/MS - MS Batch:Prep Method: Prep Date: Sample ID:VF09036-007MS 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Hexachloroethane 100 06/16/2020 19017114030-130ND1 Indeno(1,2,3-c,d)pyrene 130 06/16/2020 19018914042-123ND1 Isophorone 120 06/16/2020 19018214030-130ND1 2-Methylnaphthalene 120 06/16/2020 19017114010-107231 2-Methylphenol 190 06/16/2020 1901N13214030-130ND1 3+4-Methylphenol 130 06/16/2020 19019014030-130ND1 Naphthalene 110 06/16/2020 19017314010-1126.8 1 2-Nitroaniline 140 06/16/2020 19019614030-130ND1 3-Nitroaniline 80 06/16/2020 19015614030-130ND1 4-Nitroaniline 110 06/16/2020 19018114030-130ND1 Nitrobenzene 100 06/16/2020 19017314030-130ND1 2-Nitrophenol 110 06/16/2020 19017714030-130ND1 4-Nitrophenol 220 06/16/2020 19017728030-130ND1 N-Nitrosodi-n-propylamine 120 06/16/2020 19018214030-130ND1 N-Nitrosodiphenylamine (Diphenylamine)120 06/16/2020 19018814030-130ND1 Pentachlorophenol 180 06/16/2020 19016328030-130ND1 Phenanthrene 110 06/16/2020 19017414016-1234.8 1 Phenol 120 06/16/2020 19018214030-130ND1 Pyrene 130 06/16/2020 19018814034-1212.5 1 Pyridine 110 06/16/2020 19017714030-130ND1 2,4,5-Trichlorophenol 110 06/16/2020 19017914030-130ND1 2,4,6-Trichlorophenol 100 06/16/2020 19017314030-130ND1 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 68 33-102 2-Fluorophenol 73 35-115 Nitrobenzene-d5 68 22-109 Phenol-d5 82 33-122 Terphenyl-d14 84 41-120 2,4,6-Tribromophenol 75 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 132 of 170 Semivolatile Organic Compounds by GC/MS - MSD Batch:Prep Method: Prep Date: Sample ID:VF09036-007MD 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Acenaphthene 110 06/16/2020 19257414012-1114.6 30ND1 Acenaphthylene 110 06/16/2020 19257914044-1222.6 30ND1 Acetophenone 110 06/16/2020 19257414030-1301.7 40ND1 Anthracene 120 06/16/2020 19257914016-1220.79 302.4 1 Atrazine 120 06/16/2020 19258214030-1304.9 40ND1 Benzaldehyde 62 06/16/2020 19254314010-1101.7 40ND1 Benzo(a)anthracene 130 06/16/2020 19258814040-1210.12 30ND1 Benzo(a)pyrene 120 06/16/2020 19258514036-1143.0 30ND1 Benzo(b)fluoranthene 120 06/16/2020 19258214038-1232.9 30ND1 Benzo(g,h,i)perylene 120 06/16/2020 19258414043-1203.6 30ND1 Benzo(k)fluoranthene 120 06/16/2020 19258114040-1265.2 30ND1 1,1'-Biphenyl 110 06/16/2020 19257514030-1302.2 40ND1 4-Bromophenyl phenyl ether 100 06/16/2020 19257214030-1301.8 40ND1 Butyl benzyl phthalate 170 06/16/2020 192511714030-1300.47 40ND1 Caprolactam 140 06/16/2020 19259514030-1301.2 40ND1 Carbazole 120 06/16/2020 19258514030-1301.4 40ND1 bis (2-Chloro-1-methylethyl) ether 110 06/16/2020 19257514030-1301.8 40ND1 4-Chloro-3-methyl phenol 120 06/16/2020 19258314030-1301.5 40ND1 4-Chloroaniline 83 06/16/2020 19255814017-1069.9 40ND1 bis(2-Chloroethoxy)methane 110 06/16/2020 19257914030-1303.1 40ND1 bis(2-Chloroethyl)ether 110 06/16/2020 19257514030-1302.1 40ND1 2-Chloronaphthalene 110 06/16/2020 19257414030-1304.0 40ND1 2-Chlorophenol 110 06/16/2020 19257714030-1300.85 40ND1 4-Chlorophenyl phenyl ether 100 06/16/2020 19257214030-1301.5 40ND1 Chrysene 120 06/16/2020 19258514041-1240.23 30ND1 Dibenzo(a,h)anthracene 120 06/16/2020 19258314038-1255.1 30ND1 Dibenzofuran 110 06/16/2020 19257514030-1302.5 40ND1 3,3'-Dichlorobenzidine 110 06/16/2020 19257414010-1193.3 40ND1 2,4-Dichlorophenol 110 06/16/2020 19257714030-1301.4 40ND1 Diethylphthalate 120 06/16/2020 19258414030-1301.1 40ND1 Dimethyl phthalate 120 06/16/2020 19258214030-1302.4 40ND1 2,4-Dimethylphenol 140 06/16/2020 19259814030-1302.5 40ND1 Di-n-butyl phthalate 130 06/16/2020 19258814030-1300.40 406.4 1 4,6-Dinitro-2-methylphenol 90 06/16/2020 19256314030-1304.7 40ND1 2,4-Dinitrophenol 140 06/16/2020 19254929030-1306.0 40ND1 2,4-Dinitrotoluene 120 06/16/2020 19258614030-1302.5 40ND1 2,6-Dinitrotoluene 120 06/16/2020 19258314030-1304.2 40ND1 Di-n-octylphthalate 120 06/16/2020 19258314030-1305.9 40ND1 bis(2-Ethylhexyl)phthalate 140 06/16/2020 19259614030-1301.1 40ND1 Fluoranthene 110 06/16/2020 19257614026-1330.58 30ND1 Fluorene 110 06/16/2020 19257514019-1083.0 301.5 1 Hexachlorobenzene 100 06/16/2020 19257214030-1301.5 40ND1 Hexachlorobutadiene 94 06/16/2020 19256514030-1303.8 40ND1 Hexachlorocyclopentadiene 350 06/16/2020 19254971030-1300.68 40ND1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 133 of 170 Semivolatile Organic Compounds by GC/MS - MSD Batch:Prep Method: Prep Date: Sample ID:VF09036-007MD 56992 3546 06/15/2020 2347Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD Limit Sample Amount Dil(ug/kg)(ug/kg)(ug/kg) Hexachloroethane 110 06/16/2020 19257414030-1305.2 40ND1 Indeno(1,2,3-c,d)pyrene 120 06/16/2020 19258414042-1234.6 30ND1 Isophorone 120 06/16/2020 19258314030-1302.2 40ND1 2-Methylnaphthalene 140 06/16/2020 19257914010-1079.6 30231 2-Methylphenol 190 06/16/2020 192513014030-1301.4 40ND1 3+4-Methylphenol 130 06/16/2020 19259014030-1300.12 40ND1 Naphthalene 120 06/16/2020 19257714010-1124.7 306.8 1 2-Nitroaniline 140 06/16/2020 192510014030-1304.3 40ND1 3-Nitroaniline 92 06/16/2020 19256414030-13015 40ND1 4-Nitroaniline 120 06/16/2020 19258714030-1307.9 40ND1 Nitrobenzene 110 06/16/2020 19257414030-1302.4 40ND1 2-Nitrophenol 110 06/16/2020 19258014030-1304.0 40ND1 4-Nitrophenol 220 06/16/2020 19257829030-1302.1 40ND1 N-Nitrosodi-n-propylamine 120 06/16/2020 19258214030-1300.0059 40ND1 N-Nitrosodiphenylamine (Diphenylamine)130 06/16/2020 19258814030-1301.6 40ND1 Pentachlorophenol 180 06/16/2020 19256229030-1300.23 40ND1 Phenanthrene 110 06/16/2020 19257514016-1232.2 304.8 1 Phenol 120 06/16/2020 19258114030-1300.52 40ND1 Pyrene 130 06/16/2020 19258814034-1211.5 302.5 1 Pyridine 110 06/16/2020 19257714030-1300.62 40ND1 2,4,5-Trichlorophenol 120 06/16/2020 19258214030-1304.5 40ND1 2,4,6-Trichlorophenol 110 06/16/2020 19257514030-1302.9 40ND1 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 72 33-102 2-Fluorophenol 74 35-115 Nitrobenzene-d5 73 22-109 Phenol-d5 84 33-122 Terphenyl-d14 88 41-120 2,4,6-Tribromophenol 77 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 134 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ57409-001 57409 3546 06/18/2020 1801Analytical Method:8270E Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Acenaphthene ND 06/19/2020 10402.7 0.83 ug/kg1 Acenaphthylene ND 06/19/2020 10402.7 0.95 ug/kg1 Acetophenone ND 06/19/2020 1040135.0 ug/kg1 Anthracene ND 06/19/2020 10402.7 0.51 ug/kg1 Atrazine ND 06/19/2020 1040135.0 ug/kg1 Benzaldehyde ND 06/19/2020 1040135.0 ug/kg1 Benzo(a)anthracene ND 06/19/2020 10402.7 0.59 ug/kg1 Benzo(a)pyrene ND 06/19/2020 10402.7 0.66 ug/kg1 Benzo(b)fluoranthene ND 06/19/2020 10402.7 0.50 ug/kg1 Benzo(g,h,i)perylene ND 06/19/2020 10402.7 0.65 ug/kg1 Benzo(k)fluoranthene ND 06/19/2020 10402.7 0.48 ug/kg1 1,1'-Biphenyl ND 06/19/2020 1040135.0 ug/kg1 4-Bromophenyl phenyl ether ND 06/19/2020 1040135.0 ug/kg1 Butyl benzyl phthalate ND 06/19/2020 1040135.0 ug/kg1 Caprolactam ND 06/19/2020 1040135.0 ug/kg1 Carbazole ND 06/19/2020 1040135.0 ug/kg1 bis (2-Chloro-1-methylethyl) ether ND 06/19/2020 1040135.0 ug/kg1 4-Chloro-3-methyl phenol ND 06/19/2020 1040135.0 ug/kg1 4-Chloroaniline ND 06/19/2020 1040135.0 ug/kg1 bis(2-Chloroethoxy)methane ND 06/19/2020 1040135.0 ug/kg1 bis(2-Chloroethyl)ether ND 06/19/2020 1040135.0 ug/kg1 2-Chloronaphthalene ND 06/19/2020 1040135.0 ug/kg1 2-Chlorophenol ND 06/19/2020 1040135.0 ug/kg1 4-Chlorophenyl phenyl ether ND 06/19/2020 1040135.0 ug/kg1 Chrysene ND 06/19/2020 10402.7 0.45 ug/kg1 Dibenzo(a,h)anthracene ND 06/19/2020 10402.7 0.51 ug/kg1 Dibenzofuran ND 06/19/2020 1040135.0 ug/kg1 3,3'-Dichlorobenzidine ND 06/19/2020 1040135.0 ug/kg1 2,4-Dichlorophenol ND 06/19/2020 1040135.0 ug/kg1 Diethylphthalate ND 06/19/2020 1040135.0 ug/kg1 Dimethyl phthalate ND 06/19/2020 1040137.4 ug/kg1 2,4-Dimethylphenol ND 06/19/2020 1040135.0 ug/kg1 Di-n-butyl phthalate ND 06/19/2020 1040135.0 ug/kg1 4,6-Dinitro-2-methylphenol ND 06/19/2020 10406725ug/kg1 2,4-Dinitrophenol ND 06/19/2020 10406725ug/kg1 2,4-Dinitrotoluene ND 06/19/2020 10402710ug/kg1 2,6-Dinitrotoluene ND 06/19/2020 10402710ug/kg1 Di-n-octylphthalate ND 06/19/2020 1040135.0 ug/kg1 bis(2-Ethylhexyl)phthalate ND 06/19/2020 10406725ug/kg1 Fluoranthene ND 06/19/2020 10402.7 0.42 ug/kg1 Fluorene ND 06/19/2020 10402.7 0.57 ug/kg1 Hexachlorobenzene ND 06/19/2020 1040135.0 ug/kg1 Hexachlorobutadiene ND 06/19/2020 1040135.0 ug/kg1 Hexachlorocyclopentadiene ND 06/19/2020 10406725ug/kg1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 135 of 170 Semivolatile Organic Compounds by GC/MS - MB Batch:Prep Method: Prep Date: Sample ID:VQ57409-001 57409 3546 06/18/2020 1801Analytical Method:8270E Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil Hexachloroethane ND 06/19/2020 1040135.0 ug/kg1 Indeno(1,2,3-c,d)pyrene ND 06/19/2020 10402.7 1.0 ug/kg1 Isophorone ND 06/19/2020 1040135.0 ug/kg1 2-Methylnaphthalene ND 06/19/2020 10402.7 0.99 ug/kg1 2-Methylphenol ND 06/19/2020 1040135.0 ug/kg1 3+4-Methylphenol ND 06/19/2020 10402710ug/kg1 Naphthalene ND 06/19/2020 10402.7 0.97 ug/kg1 2-Nitroaniline ND 06/19/2020 10402710ug/kg1 3-Nitroaniline ND 06/19/2020 10402710ug/kg1 4-Nitroaniline ND 06/19/2020 10402710ug/kg1 Nitrobenzene ND 06/19/2020 1040135.0 ug/kg1 2-Nitrophenol ND 06/19/2020 10402710ug/kg1 4-Nitrophenol ND 06/19/2020 10406725ug/kg1 N-Nitrosodi-n-propylamine ND 06/19/2020 1040135.0 ug/kg1 N-Nitrosodiphenylamine (Diphenylamine)ND 06/19/2020 1040135.0 ug/kg1 Pentachlorophenol ND 06/19/2020 10406725ug/kg1 Phenanthrene ND 06/19/2020 10402.7 0.72 ug/kg1 Phenol ND 06/19/2020 1040135.0 ug/kg1 Pyrene ND 06/19/2020 10402.7 0.50 ug/kg1 Pyridine ND 06/19/2020 1040135.0 ug/kg1 2,4,5-Trichlorophenol ND 06/19/2020 1040135.0 ug/kg1 2,4,6-Trichlorophenol ND 06/19/2020 1040135.0 ug/kg1 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 77 33-102 2-Fluorophenol 89 35-115 Nitrobenzene-d5 76 22-109 Phenol-d5 101 33-122 Terphenyl-d14 103 41-120 2,4,6-Tribromophenol 81 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 136 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ57409-002 57409 3546 06/18/2020 1801Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Acenaphthene 110 06/19/2020 11048513012-1111 Acenaphthylene 120 06/19/2020 11049013044-1221 Acetophenone 110 06/19/2020 11047913048-1111 Anthracene 130 06/19/2020 11049413016-1221 Atrazine 130 06/19/2020 11049813048-1161 Benzaldehyde 56 06/19/2020 11044213010-1101 Benzo(a)anthracene 140 06/19/2020 110410413040-1211 Benzo(a)pyrene 140 06/19/2020 110410513036-1141 Benzo(b)fluoranthene 140 06/19/2020 110410313038-1231 Benzo(g,h,i)perylene 150 06/19/2020 110411213043-1201 Benzo(k)fluoranthene 140 06/19/2020 110410213040-1261 1,1'-Biphenyl 110 06/19/2020 11048513049-1101 4-Bromophenyl phenyl ether 120 06/19/2020 11048713046-1181 Butyl benzyl phthalate 170 06/19/2020 1104N13113046-1281 Caprolactam 150 06/19/2020 110411013043-1211 Carbazole 140 06/19/2020 110410313047-1281 bis (2-Chloro-1-methylethyl) ether 120 06/19/2020 11049313031-1021 4-Chloro-3-methyl phenol 120 06/19/2020 11049113049-1181 4-Chloroaniline 110 06/19/2020 11048213017-1061 bis(2-Chloroethoxy)methane 110 06/19/2020 11048213039-1081 bis(2-Chloroethyl)ether 120 06/19/2020 11049013032-1051 2-Chloronaphthalene 110 06/19/2020 11048513031-1271 2-Chlorophenol 120 06/19/2020 11048813037-1061 4-Chlorophenyl phenyl ether 120 06/19/2020 11048713047-1161 Chrysene 140 06/19/2020 110410413041-1241 Dibenzo(a,h)anthracene 140 06/19/2020 110410613038-1251 Dibenzofuran 120 06/19/2020 11048913045-1121 3,3'-Dichlorobenzidine 120 06/19/2020 11049213010-1191 2,4-Dichlorophenol 110 06/19/2020 11048513041-1131 Diethylphthalate 130 06/19/2020 11049713049-1231 Dimethyl phthalate 130 06/19/2020 11049613048-1201 2,4-Dimethylphenol 140 06/19/2020 110410613033-1231 Di-n-butyl phthalate 150 06/19/2020 110410913051-1291 4,6-Dinitro-2-methylphenol 110 06/19/2020 11048513040-1301 2,4-Dinitrophenol 180 06/19/2020 11046727032-1151 2,4-Dinitrotoluene 140 06/19/2020 110410213048-1241 2,6-Dinitrotoluene 130 06/19/2020 11049713047-1251 Di-n-octylphthalate 140 06/19/2020 110410513049-1421 bis(2-Ethylhexyl)phthalate 150 06/19/2020 110411213045-1281 Fluoranthene 120 06/19/2020 11049213026-1331 Fluorene 120 06/19/2020 11048913019-1081 Hexachlorobenzene 110 06/19/2020 11048213044-1221 Hexachlorobutadiene 100 06/19/2020 11047513033-1031 Hexachlorocyclopentadiene 470 06/19/2020 11047167018-1211 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 137 of 170 Semivolatile Organic Compounds by GC/MS - LCS Batch:Prep Method: Prep Date: Sample ID:VQ57409-002 57409 3546 06/18/2020 1801Analytical Method:8270E Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/kg)(ug/kg) Hexachloroethane 99 06/19/2020 11047413030-961 Indeno(1,2,3-c,d)pyrene 140 06/19/2020 110410713042-1231 Isophorone 120 06/19/2020 11049113041-1131 2-Methylnaphthalene 110 06/19/2020 11048113010-1071 2-Methylphenol 120 06/19/2020 11049213032-1071 3+4-Methylphenol 140 06/19/2020 110410513039-1081 Naphthalene 110 06/19/2020 11048213010-1121 2-Nitroaniline 140 06/19/2020 110410413045-1231 3-Nitroaniline 110 06/19/2020 11048613024-1271 4-Nitroaniline 140 06/19/2020 110410813048-1271 Nitrobenzene 110 06/19/2020 11048013033-1141 2-Nitrophenol 110 06/19/2020 11048513035-1081 4-Nitrophenol 250 06/19/2020 11049227018-1541 N-Nitrosodi-n-propylamine 130 06/19/2020 11049513032-1151 N-Nitrosodiphenylamine (Diphenylamine)130 06/19/2020 11049913053-1501 Pentachlorophenol 190 06/19/2020 11047027027-1381 Phenanthrene 120 06/19/2020 11048913016-1231 Phenol 120 06/19/2020 11049213036-1081 Pyrene 150 06/19/2020 110411513034-1211 Pyridine 140 06/19/2020 110410713030-1301 2,4,5-Trichlorophenol 130 06/19/2020 11049813046-1221 2,4,6-Trichlorophenol 110 06/19/2020 11048613038-1151 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 66 33-102 2-Fluorophenol 72 35-115 Nitrobenzene-d5 69 22-109 Phenol-d5 82 33-122 Terphenyl-d14 107 41-120 2,4,6-Tribromophenol 85 30-117 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 138 of 170 EDB & DBCP by Microextraction - MB Batch:Prep Method: Prep Date: Sample ID:VQ56595-001 56595 504.1 06/11/2020 0930Analytical Method:504.1 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil 1,2-Dibromoethane (EDB)ND 06/11/2020 11390.010 0.0040 ug/L1 Surrogate Q % Rec Acceptance Limit 1,1,1,2-Tetrachloroethane 84 57-137 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 139 of 170 EDB & DBCP by Microextraction - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56595-002 56595 504.1 06/11/2020 0930Analytical Method:504.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) 1,2-Dibromoethane (EDB)0.23 06/11/2020 1151920.25 70-1301 Surrogate Q % Rec Acceptance Limit 1,1,1,2-Tetrachloroethane 84 57-137 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 140 of 170 MADEP EPH (aliphatics) - MB Batch:Prep Method: Prep Date: Sample ID:VQ56889-001 56889 MADEP-EPH-04 06/14/2020 1535Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil C9 - C18 Aliphatics ND 06/23/2020 2242100100ug/L1 C19 - C36 Aliphatics ND 06/23/2020 2242100100ug/L1 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)69 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 141 of 170 MADEP EPH (aliphatics) - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56889-002 56889 MADEP-EPH-04 06/14/2020 1535Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) C9 - C18 Aliphatics 120 06/23/2020 2312N3930040-1401 C19 - C36 Aliphatics 320 06/23/2020 23127940040-1401 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)62 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 142 of 170 MADEP EPH (aliphatics) - LCSD Batch:Prep Method: Prep Date: Sample ID:VQ56889-003 56889 MADEP-EPH-04 06/14/2020 1535Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) C9 - C18 Aliphatics 88 06/23/2020 2342N,+29300 40-14028 251 C19 - C36 Aliphatics 250 06/23/2020 23426240040-14024 251 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)59 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 143 of 170 MADEP EPH (aromatics) - MB Batch:Prep Method: Prep Date: Sample ID:VQ56890-001 56890 MADEP-EPH-04 06/14/2020 1533Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil C11 - C22 Aromatics ND 06/24/2020 0411100100ug/L1 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic)80 40-140 2-Fluorobiphenyl (fractionation 1)92 40-140 2-Bromonaphthalene (fractionation 2)87 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 144 of 170 MADEP EPH (aromatics) - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56890-002 56890 MADEP-EPH-04 06/14/2020 1533Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) C11 - C22 Aromatics 490 06/24/2020 04415785040-1401 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic)85 40-140 2-Fluorobiphenyl (fractionation 1)97 40-140 2-Bromonaphthalene (fractionation 2)95 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 145 of 170 MADEP EPH (aromatics) - LCSD Batch:Prep Method: Prep Date: Sample ID:VQ56890-003 56890 MADEP-EPH-04 06/14/2020 1533Analytical Method:MADEP-EPH-04 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) C11 - C22 Aromatics 350 06/24/2020 0511+41850 40-14033 251 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic)66 40-140 2-Fluorobiphenyl (fractionation 1)92 40-140 2-Bromonaphthalene (fractionation 2)89 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 146 of 170 MA EPH (aliphatics) - MB Batch:Prep Method: Prep Date: Sample ID:VQ56905-001 56905 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil C9 - C18 Aliphatics ND 06/16/2020 14051010mg/kg1 C19 - C36 Aliphatics ND 06/16/2020 14051010mg/kg1 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)75 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 147 of 170 MA EPH (aliphatics) - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56905-002 56905 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(mg/kg)(mg/kg) C9 - C18 Aliphatics 19 06/16/2020 1434623040-1401 C19 - C36 Aliphatics 33 06/16/2020 1434824040-1401 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)73 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 148 of 170 MA EPH (aliphatics) - LCSD Batch:Prep Method: Prep Date: Sample ID:VQ56905-003 56905 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(mg/kg)(mg/kg) C9 - C18 Aliphatics 19 06/16/2020 1504643040-1402.0 251 C19 - C36 Aliphatics 32 06/16/2020 1504814040-1401.7 251 Surrogate Q % Rec Acceptance Limit 1-Chloro-octadecane (aliphatic)76 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 149 of 170 MA EPH (aromatics) - MB Batch:Prep Method: Prep Date: Sample ID:VQ56906-001 56906 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil C11 - C22 Aromatics ND 06/16/2020 22311010mg/kg1 Surrogate Q % Rec Acceptance Limit 2-Bromonaphthalene (fractionation 2)84 40-140 2-Fluorobiphenyl (fractionation 1)87 40-140 o - Terphenyl (aromatic)77 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 150 of 170 MA EPH (aromatics) - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56906-002 56906 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(mg/kg)(mg/kg) C11 - C22 Aromatics 67 06/16/2020 2301788540-1401 Surrogate Q % Rec Acceptance Limit 2-Bromonaphthalene (fractionation 2)92 40-140 2-Fluorobiphenyl (fractionation 1)92 40-140 o - Terphenyl (aromatic)81 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 151 of 170 MA EPH (aromatics) - LCSD Batch:Prep Method: Prep Date: Sample ID:VQ56906-003 56906 MADEP-EPH-04 06/15/2020 0921Analytical Method:MADEP-EPH-04 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(mg/kg)(mg/kg) C11 - C22 Aromatics 62 06/16/2020 2331738540-1407.8 251 Surrogate Q % Rec Acceptance Limit 2-Bromonaphthalene (fractionation 2)90 40-140 2-Fluorobiphenyl (fractionation 1)91 40-140 o - Terphenyl (aromatic)77 40-140 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 152 of 170 MADEP VPH (aliphatics) - MB Batch:Prep Method: Sample ID:VQ56710-001 56710 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil C5 - C8 Aliphatics ND 06/11/2020 22227515ug/L1 C9 - C12 Aliphatics ND 06/11/2020 22227515ug/L1 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)93 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 153 of 170 MADEP VPH (aliphatics) - LCS Batch:Prep Method: Sample ID:VQ56710-002 56710 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) C5 - C8 Aliphatics 150 06/11/2020 19459915070-1301 C9 - C12 Aliphatics 160 06/11/2020 19459318070-1301 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)95 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 154 of 170 MADEP VPH (aliphatics) - LCSD Batch:Prep Method: Sample ID:VQ56710-003 56710 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) C5 - C8 Aliphatics 160 06/11/2020 201310315070-1304.6 251 C9 - C12 Aliphatics 170 06/11/2020 20139918070-1305.4 251 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)100 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 155 of 170 MADEP VPH (aromatics) - MB Batch:Prep Method: Sample ID:VQ56711-001 56711 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil C9 - C10 Aromatics ND 06/11/2020 2222255.0 ug/L1 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)93 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 156 of 170 MADEP VPH (aromatics) - LCS Batch:Prep Method: Sample ID:VQ56711-002 56711 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(ug/L)(ug/L) C9 - C10 Aromatics 24 06/11/2020 1945982570-1301 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)96 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 157 of 170 MADEP VPH (aromatics) - LCSD Batch:Prep Method: Sample ID:VQ56711-003 56711 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(ug/L)(ug/L) C9 - C10 Aromatics 25 06/11/2020 20131022570-1304.0 251 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)98 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 158 of 170 MADEP VPH (aromatics) - MB Batch:Prep Method: Sample ID:VQ57090-001 57090 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil C9 - C10 Aromatics ND 06/16/2020 10591.3 0.50 mg/kg1 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)100 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 159 of 170 MADEP VPH (aromatics) - LCS Batch:Prep Method: Sample ID:VQ57090-002 57090 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(mg/kg)(mg/kg) C9 - C10 Aromatics 1.3 06/16/2020 10011041.3 70-1301 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)108 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 160 of 170 MADEP VPH (aromatics) - LCSD Batch:Prep Method: Sample ID:VQ57090-003 57090 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(mg/kg)(mg/kg) C9 - C10 Aromatics 1.3 06/16/2020 10301041.3 70-1300.00 251 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (PID)108 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 161 of 170 MADEP VPH (aliphatics) - MB Batch:Prep Method: Sample ID:VQ57092-001 57092 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil C5 - C8 Aliphatics ND 06/16/2020 10593.8 0.75 mg/kg1 C9 - C12 Aliphatics ND 06/16/2020 10593.8 0.75 mg/kg1 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)98 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 162 of 170 MADEP VPH (aliphatics) - LCS Batch:Prep Method: Sample ID:VQ57092-002 57092 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(mg/kg)(mg/kg) C5 - C8 Aliphatics 7.5 06/16/2020 10011007.5 70-1301 C9 - C12 Aliphatics 9.0 06/16/2020 10011038.8 70-1301 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)101 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 163 of 170 MADEP VPH (aliphatics) - LCSD Batch:Prep Method: Sample ID:VQ57092-003 57092 VPH Analytical Method:MADEP-VPH-18-2.1 Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD % Rec Limit % RPD LimitDil(mg/kg)(mg/kg) C5 - C8 Aliphatics 7.8 06/16/2020 10301047.5 70-1304.6 251 C9 - C12 Aliphatics 9.2 06/16/2020 10301058.8 70-1302.2 251 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID)99 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 164 of 170 ICP-AES Metals - MB Batch:Prep Method: Prep Date: Sample ID:VQ56859-001 56859 3005A 06/13/2020 1626Analytical Method:6010D Matrix:Aqueous Parameter Result Q LOQ DL Units Analysis DateDil Lead ND 06/17/2020 03320.010 0.0047 mg/L1 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 165 of 170 ICP-AES Metals - LCS Batch:Prep Method: Prep Date: Sample ID:VQ56859-002 56859 3005A 06/13/2020 1626Analytical Method:6010D Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date % Rec LimitDil(mg/L)(mg/L) Lead 0.41 06/17/2020 03381030.40 80-1201 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40% + = RPD is out of criteria_DL = Detection Limit LOD = Limit of Detection 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 166 of 170 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 167 of 170 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 168 of 170 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 169 of 170 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 170 of 170 Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Appendix IIV Boring Logs.rtf APPENDIX IV BORING LOGS Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring TMW-1 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME55x Groundwater Level and Date Measured 10.1 Borehole Backfill Logged By CE Drill Bit Size/Type 6.25 Drilling Contractor SUMMIT Sampling Method(s)Split Spoon Location Checked By PWL Total Depth of Borehole 13 Approximate Surface Elevation 0 Hammer Data Material TypeSM-ML SM-ML SM-ML REMARKS AND OTHER TESTS Soil Sample 9-10'Graphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTION Brown-Orange Sandy SILT Tan Sandy SILT Tan Fine Grained Sandy SILT Bottom of BoringDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)0 -5 -10 -15 -20 -25 -30 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring TMW-2 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME55x Groundwater Level and Date Measured 12.7 Borehole Backfill Logged By CE Drill Bit Size/Type 6.25 Drilling Contractor SUMMIT Sampling Method(s)Split Spoon Location Checked By PWL Total Depth of Borehole 13 Approximate Surface Elevation 0 Hammer Data Material TypeSM-ML SM-ML SM-ML REMARKS AND OTHER TESTS Soil SampleGraphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTION Brown-Orange Sandy SILT Tan Sandy SILT Tan Fine Grained Sandy SILT Bottom of BoringDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)0 -5 -10 -15 -20 -25 -30 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring TMW-4 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME55x Groundwater Level and Date Measured 8.7 Borehole Backfill Logged By CE Drill Bit Size/Type 6.25 Drilling Contractor SUMMIT Sampling Method(s)Split Spoon Location Checked By PWL Total Depth of Borehole 13 Approximate Surface Elevation 0 Hammer Data Material TypeSM-ML SM-ML SM-ML REMARKS AND OTHER TESTS Soil Sample 11'Graphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTION Brown-Orange Sandy SILT Tan Sandy SILT Tan Fine Grained Sandy SILT Bottom of BoringDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)0 -5 -10 -15 -20 -25 -30 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring TMW-5 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME55x Groundwater Level and Date Measured 9 Borehole Backfill Logged By CE Drill Bit Size/Type 6.25 Drilling Contractor SUMMIT Sampling Method(s)Split Spoon Location Checked By PWL Total Depth of Borehole 13 Approximate Surface Elevation 0 Hammer Data Material TypeSM-ML SM-ML SM-ML REMARKS AND OTHER TESTS Soil Sample 11'Graphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTION Brown-Orange Sandy SILT Tan Sandy SILT Tan Fine Grained Sandy SILT Bottom of BoringDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)0 -5 -10 -15 -20 -25 -30 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring TMW-6 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME55x Groundwater Level and Date Measured 8.65 Borehole Backfill Logged By CE Drill Bit Size/Type 6.25 Drilling Contractor SUMMIT Sampling Method(s)Split Spoon Location Checked By PWL Total Depth of Borehole 13 Approximate Surface Elevation 0 Hammer Data Material TypeSM-ML SM-ML SM-ML REMARKS AND OTHER TESTS Soil Sample 11'Graphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTION Brown-Orange Sandy SILT Tan Sandy SILT Tan Fine Grained Sandy SILT Bottom of BoringDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)0 -5 -10 -15 -20 -25 -30 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Key to Log of Boring Material TypeREMARKS AND OTHER TESTSGraphic LogWell LogWater Content, %Dry Unit Weight, pcfMATERIAL DESCRIPTIONDepth (feet)Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)1 2 3 4 5 6 7 8 9 10 11 12 COLUMN DESCRIPTIONS 1 Elevation (feet): Elevation (MSL, feet). 2 Depth (feet): Depth in feet below the ground surface. 3 Sample Type: Type of soil sample collected at the depth interval shown. 4 Sample Number: Sample identification number. 5 Sampling Resistance, blows/ft: Number of blows to advance driven sampler one foot (or distance shown) beyond seating interval using the hammer identified on the boring log. 6 Material Type: Type of material encountered. 7 Graphic Log: Graphic depiction of the subsurface material encountered. 8 MATERIAL DESCRIPTION: Description of material encountered. May include consistency, moisture, color, and other descriptive text. 9 Water Content, %: Water content of the soil sample, expressed as percentage of dry weight of sample. 10 Dry Unit Weight, pcf: Dry weight per unit volume of soil sample measured in laboratory, in pounds per cubic foot. 11 Well Log: Graphical representation of well installed upon completion of drilling and sampling. 12 REMARKS AND OTHER TESTS: Comments and observations regarding drilling or sampling made by driller or field personnel. FIELD AND LABORATORY TEST ABBREVIATIONS CHEM: Chemical tests to assess corrosivity COMP: Compaction test CONS: One-dimensional consolidation test LL: Liquid Limit, percent PI: Plasticity Index, percent SA: Sieve analysis (percent passing No. 200 Sieve) UC: Unconfined compressive strength test, Qu, in ksf WA: Wash sieve (percent passing No. 200 Sieve) MATERIAL GRAPHIC SYMBOLS Bentonite chips Clayey SAND (SC) Silty SAND to Sandy SILT (SM-ML) TYPICAL SAMPLER GRAPHIC SYMBOLS Auger sampler Bulk Sample 3-inch-OD California w/ brass rings CME Sampler Grab Sample 2.5-inch-OD Modified California w/ brass liners Pitcher Sample 2-inch-OD unlined split spoon (SPT) Shelby Tube (Thin-walled, fixed head) OTHER GRAPHIC SYMBOLS Water level (at time of drilling, ATD) Water level (after waiting) Minor change in material properties within a stratum Inferred/gradational contact between strata ?Queried contact between strata GENERAL NOTES 1: Soil classifications are based on the Unified Soil Classification System. Descriptions and stratum lines are interpretive, and actual lithologic changes may be gradual. Field descriptions may have been modified to reflect results of lab tests. 2: Descriptions on these logs apply only at the specific boring locations and at the time the borings were advanced. They are not warranted to be representative of subsurface conditions at other locations or times.C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Well Logs.bg4[(master well 2 lab).tpl]Figure B-1 Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-7 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 9'- 343 PIDGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-8 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 3'- 85 PIDGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-9 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 3'- 8.9 PIDGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-10 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 3'- 5.5 PID - odorsGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-11 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 9'- 151 PIDGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Log of Boring SS-12 Date(s) Drilled 6/8/20 Drilling Method HSA Drill Rig Type CME Groundwater Level and Date Measured Borehole Backfill Cuttings Logged By MD Drill Bit Size/Type 6.5 Drilling Contractor Sampling Method(s)Split Spoon Location Checked By PL Total Depth of Borehole 10 Approximate Surface Elevation Hammer Data Material TypeSM-SC SM-SC REMARKS AND OTHER TESTS Sample Collected 9'- 115 PIDGraphic LogMATERIAL DESCRIPTION Tan-Brown Sandy Silt Tan-White Fine Grained Sandy Silt - DRYDepth (feet)0 5 10 15 20 25 30 Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Sheet 1 of 1 Project:New Pineville Townhall & Library Project Location:Pineville, NC Project Number:7563.E0001 Key to Log of Boring Material TypeREMARKS AND OTHER TESTSGraphic LogMATERIAL DESCRIPTIONDepth (feet)Sample NumberSample TypeSampling Resistance, blows/ftElevation (feet)1 2 3 4 5 6 7 8 9 COLUMN DESCRIPTIONS 1 Elevation (feet): Elevation (MSL, feet). 2 Depth (feet): Depth in feet below the ground surface. 3 Sample Type: Type of soil sample collected at the depth interval shown. 4 Sample Number: Sample identification number. 5 Sampling Resistance, blows/ft: Number of blows to advance driven sampler one foot (or distance shown) beyond seating interval using the hammer identified on the boring log. 6 Material Type: Type of material encountered. 7 Graphic Log: Graphic depiction of the subsurface material encountered. 8 MATERIAL DESCRIPTION: Description of material encountered. May include consistency, moisture, color, and other descriptive text. 9 REMARKS AND OTHER TESTS: Comments and observations regarding drilling or sampling made by driller or field personnel. FIELD AND LABORATORY TEST ABBREVIATIONS CHEM: Chemical tests to assess corrosivity COMP: Compaction test CONS: One-dimensional consolidation test LL: Liquid Limit, percent PI: Plasticity Index, percent SA: Sieve analysis (percent passing No. 200 Sieve) UC: Unconfined compressive strength test, Qu, in ksf WA: Wash sieve (percent passing No. 200 Sieve) MATERIAL GRAPHIC SYMBOLS Silty to Clayey SAND (SM-SC) TYPICAL SAMPLER GRAPHIC SYMBOLS Auger sampler Bulk Sample 3-inch-OD California w/ brass rings CME Sampler Grab Sample 2.5-inch-OD Modified California w/ brass liners Pitcher Sample 2-inch-OD unlined split spoon (SPT) Shelby Tube (Thin-walled, fixed head) OTHER GRAPHIC SYMBOLS Water level (at time of drilling, ATD) Water level (after waiting) Minor change in material properties within a stratum Inferred/gradational contact between strata ?Queried contact between strata GENERAL NOTES 1: Soil classifications are based on the Unified Soil Classification System. Descriptions and stratum lines are interpretive, and actual lithologic changes may be gradual. Field descriptions may have been modified to reflect results of lab tests. 2: Descriptions on these logs apply only at the specific boring locations and at the time the borings were advanced. They are not warranted to be representative of subsurface conditions at other locations or times.C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Soil Borings Only.bg4[(master 0 lab).tpl]Figure B-1 Sheet 1 of 1 Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Appendix V Well Permits.rtf APPENDIX V WELL RECORDS/PERMITS SIP Form – revised 2/15/11 Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202 Phone: (704) 336-5103 Fax: (704) 336-6894 http://groundwater.charmeck.org Permit Issuance Date: _______________ Permit Number: ____________________ SUBSURFACE INVESTIGATION PERMIT I. Well Owner Information Name: ___________________________________ Attn: _____________________________________ Phone #: _____________________ Address 1: ________________________________ Address 2: ________________________________ City: __________________________ State: _______ Zip: _____________ II. Agent Information (if applicable) Name: ___________________________________ Attn: _____________________________________ Phone #: _____________________ Address 1: ________________________________ Address 2: ________________________________ City: __________________________ State: _______ Zip: _____________ III. Site Information Site Name; ________________________________ Parcel ID Number: _____________________ Address: ________________________________ City: __________________________ State: _______ Zip: _____________ General Conditions of This Permit: • This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance. • This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation and made available to a Department representative upon request. • A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit. • All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations. • All temporary wells, including those installed using Direct Push Technology, must be abandoned to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations. • Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the analytical results are received. Agent 6/5/2020 70002752 Town of Pineville Chip Hill 7046513339 200 Dover St. Pineville NC 28134 Summit ELT Patrick Lowery 8032305087 101 Rice Bent Way Unit 9 none Columbia SC 29882 New Pineville Town Hall and Library 22105115 NC WELL ABANDONMENT RECORD Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1.Well Contractor Information: Well Contractor Name (or well owner personally abandoning well on his/her property) NC Well Contractor Certification Number Company Name 2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known 3.Well use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply)□Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer □Geothermal (Heating/Cooling Return) □Other (explain under 7g) 4. Date well(s) abandoned: 5a. Well location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction record(s) if available. For multiple injection or non-water supply wells ONLY with the same construction/abandonment, you can submit one form. 6a. Well ID#: 6b. Total well depth: (ft.) 6c. Borehole diameter: (in.) 6d. Water level below ground surface: (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) 6g. Screen length (if known): (ft.) WELL ABANDONMENT DETAILS 7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of wells abandoned: 7b. Approximate volume of water remaining in well(s): (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): □Neat Cement Grout □Bentonite Chips or Pellets □Sand Cement Grout □Dry Clay □Concrete Grout □Drill Cuttings □Specialty Grout □Gravel □Bentonite Slurry □Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 7g. Provide a brief description of the abandonment procedure: 8.Certification: Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9.Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Injection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. For Internal Use ONLY: Roy Charles Killian 4169-B 6 2 SUMMIT ELT, PC 70002752 500 lb 6/8/20 remove well casing, pump bentonite slurry from base to surface with trailer mount grout pump Town of Pineville 505-511 Main Street, Pineville, NC 7/10/2020 Mecklenburg 22105115 TMW-1,2,3,4,5 &6 13 6.25 8 8 5 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-1 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 10.1 6.25 auger 12 13 sandy silt 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt Print Form 7/10/2020 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-2 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 12.7 6.25 auger 12 13 sandy silt 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt Print Form 7/10/2020 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-3 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 DRY 6.25 auger DRY WELLL 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt DRY WELL Print Form 7/10/2020 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-4 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 8.7 6.25 auger 12 13 sandy silt 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt Print Form 7/10/2020 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-5 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 9.0 6.25 auger 12 13 sandy silt 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt Print Form 7/10/2020 WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only: Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016 1. Well Contractor Information: Well Contractor Name NC Well Contractor Certification Number Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation Non-Water Supply Well: □Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks) 4. Date Well(s) Completed: Well ID# 5a. Well Location: Facility/Owner Name Facility ID# (if applicable) Physical Address, City, and Zip County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W 6. Is(are) the well(s): □Permanent or □Temporary 7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells drilled: 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount: 14. WATER ZONES FROM TO DESCRIPTION ft. ft. ft. ft. 15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING (geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL ft. ft. in. ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT ft. ft. ft. ft. ft. ft. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD ft. ft. ft. ft. 20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS 22. Certification: Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Injection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Roy Charles Killian 4169--B SUMMIT ELT, PC 70002752 6/8/20 TMW-6 Town of Pineville 505-511 Main Street, Pineville, NC Mecklenburg 22105115 13 8.65 6.25 auger 12 13 sandy silt 13 8 2 13 6 #3 filter sand gravity 0 13 Brown/tan/white fine grain sandy silt Print Form 7/10/2020 Limited Phase II ESA – New Pineville Town Hall and Library SUMMIT Project No. 7563.E0001 Pineville, North Carolina July 10, 2020 C:\plowery\Documents\2-Projects\7563.E0001 New Pineville Town Hall & Library\Appendix VI UST61.rtf APPENDIX VI UST-61 24-HR RELEASE NOTIFICATION UST-61 24-Hour Release and UST Leak Reporting Form. For Releases in NC This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or suspected release (DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________ Reported by (circle one): Phone, Fax or Report Region _______ Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______ Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________ Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________ Reg/Non-regulated? _____________ INCIDENT DESCRIPTION Incident Name: Address: County: City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS  Topographic map  GIS Address matching  Other  Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release Code) (Check one)  Release Detection Equipment or Methods  During UST Closure/Removal  Property Transfer  Visual/Odor  Water in Tank  Water Supply Well Contamination  Groundwater Contamination  Surface Water Contamination  Other (specify) _______________ SOURCE OF CONTAMINATION Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)  Tank  Piping  Dispenser  Submersible Turbine Pump  Delivery Problem  Spill Bucket  Other  Unknown Definitions presented on reverse  Spill  Overfill  Corrosion  Physical/Mechanical Damage  Install Problem  Other  Unknown Definitions presented on reverse  Petroleum  Non-Petroleum  Both Location (Check one)  Facility  Residence  Other  Gasoline/ Diesel/ Kerosene  Heating Oil  Other Petroleum Products  Metals  Other Inorganics  Other Organics  Diesel/Veg. Oil Blend  Vegetable Oil 100%  E10 – E20  E21 – E84  E85 – E99  Ethanol 100%  E01 – E09 Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 Y YY N COMM Proposed New Pineville Town Hall and Library 505-511 Main Street Mecklenburg Pineville 28134 35.086632 -80.893153 UNKOWN 7/10/20 Due Diligence of the site revealed a former UST site located on the property. The Little General Store with address of 105 Yandle Street. According to database records, the store operated 1-14,000-gallon, 1-6,000-gallon and 1-1,000-gallon USTs. The USTs operated from 1973 to 1991 when records indicate they were removed. No facilty ID could be located. Geotechnical Investigation identfied petro odors. A Phase II ESA consisting of 12 soil samples and 6 groundwater samples was conducted (attached). Groundwater and soil exceedances of NC 2L and MSCC soil-to water were identified. Property is vacant and unused IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________ Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map Person Reporting Incident Company Telephone Number Title Address Date UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined NA - Former Little General Store Little General Store Town of Pineville 200 Dover Street Pineville NC 28134 Patrick Lowery, Snr Env Mngr SUMMIT ELT for Town of Pineville 7/15/20 803-230-5087 3575 Centre Cir Drive, Ft Mill, SC 29715 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 9571.40692463Area of feature in internal units squared: 356.311310411Length of feature in internal units: 758Sites designated as superfund cleanup sites: 491412.9375Y-value coordinate in feet: 1435661.125X-value coordinate in feet: 356.31130981Total perimeter in coverage units: 9571.40625Total area in coverage units: 35 5 7.983647 80 53 11.508125Lat/Long: 046 148 540Superfund ID: FederalSite Type: HSDS: 1720 ft. 1/4-1/2 ESE , NC Region N/A HSDS NC HSDSCENTRAL TRANSPORT COMPANY S102442859 RemovedTank Status: 2Tank Id: UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 4000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: RemovedTank Status: 1Tank Id: -80.89318Longitude: 35.08701Latitude: MecklenburgFIPS County Desc: LANCASTER, SC 29720-1317Contact City/State/Zip: Not reportedContact Address2: PO BOX 1317 /120 S MAIN STContact Address1: SHAUN-SEJ CORP DBA CHEM OILContact: 00-0-0000017182Facility Id: PINEVILLE, NC 28134City,State,Zip: 105 YANDLE ST & HWY 51Address: LITTLE GENERALName: UST: 118 ft. 0.022 mi. Relative: Higher Actual: 575 ft. < 1/8 PINEVILLE, NC 28134 SE 105 YANDLE ST & HWY 51 N/A 1 NC USTLITTLE GENERAL U001197105 TC6029023.2s Page 8 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 6000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: RemovedTank Status: 3Tank Id: UnknownDecode for PSYS_KEY: Single Wall SteelDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: Gasoline, Gas MixProduct Name: 01/31/1991Perm Close Date: 04/21/1973Installed Date: LITTLE GENERAL (Continued)U001197105 05/15/2006Cleanup: 05/15/2006Date Occur: 05/18/2006Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 36087Incident Number: MO-7430UST Number: Not reportedFacility ID: PINEVILLE, NC 28134City,State,Zip: 106 CRANFORD DRIVEAddress: CLAYTON PROPERTYName: LUST: 396 ft. Site 1 of 2 in cluster A 0.075 mi. Relative: Higher Actual: 573 ft. < 1/8 NC IMDPINEVILLE, NC 28134 NE NC LUST TRUST106 CRANFORD DRIVE N/A A2 NC LUSTCLAYTON PROPERTY S107998527 TC6029023.2s Page 9 Source:USGS Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 1 1 inch = 2000 feet Site Location Plan New Town Hall & Library505-511 Main Street Pineville, NC Town of Pineville N Subject Property Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 2As Shown Sampling Location Plan New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 SS-1 KEY Soil Boring Temporary Monitoring Well TMW-2SS-2 TMW-3 SS-3 TMW-4SS-4 TMW-5 SS-5 TMW-6 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 3As Shown Soil Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N SS-1 KEY MSCC Soil to Water Exceedances SS-2 SS-3 SS-4 SS-5 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11 SS-12 Source: Drawn by SUMMIT Prepared By\Date:PL/07/20Checked By\Date:MZ/07/20 Scale Figure 4As Shown Groundwater Concentration Map New Town Hall & Library Town of Pineville 505-511 Main StreetPineville, NC N TMW-1 KEY B-BENZENE E-ETHYLBENZENE T-TOLUENE X-XYLENES N-NAPHTHALENE Resutls in ug/L TMW-2 TMW-3 TMW-4 TMW-5 TMW-6 Groundwater Flow Direction B-130 T-220 E-3000X-4200N-760 B-300T-1100E-5600X-13300N-1400 B-NDT-64E-2600 X-5700 N-900 B-ND T-ND E-12X-19.7N-8 B-NDT-NDE-6.7X-12.5N-5.1 DRY