MO-8808_40318_CA_CAPR_20220105

CORRECTIVE ACTION
PERFORMANCE REPORT

TERRELL BAIT SHOP
7970 NC HIGHWAY 150
TERRELL, CATAWBA COUNTY, NORTH CAROLINA
FACILITY ID #00-0-00000218

Prepared For:
United Oil of the Carolinas
Post Office Box 68
Gastonia, North Carolina 28053

BLE Project Number J22-17256-03

January 5, 2023

January 5, 2023

Mr. Lewis Efird
United Oil of the Carolinas
Post Office Box 68
Gastonia, North Carolina 28053

Subject: Corrective Action Performance Report
Terrell Bait Shop, Incident 40318
7970 NC Highway 150
Terrell, Catawba County, North Carolina 28682
Facility ID #00-0-00000218
BLE Project No. J22-17256-03

Dear Mr. Efird:

Bunnell-Lammons Engineering, Inc. (BLE) has completed a Corrective Action Performance Report
(CAPR) in association with the former Terrell Bait Shop facility in Terrell, North Carolina (herein referred
to as “Site”). The purpose of the CAPR is to document the effectiveness of the soil and groundwater
remediation system in operation at the Site.

The CAPR was prepared in general accordance with the North Carolina Department of Environmental
Quality (NCDEQ) NCDEQ Underground Storage Tank (UST) Section Corrective Action Guidelines dated
January 19, 2021, and BLE Proposal No. P22-1724 dated October 12, 2022.

BLE appreciates the opportunity to assist United Oil of the Carolinas with this project. If you have any
questions regarding this report, please feel free to contact David R. Loftis at 828-277-0100.

Sincerely,

BUNNELL-LAMMONS ENGINEERING, INC.

Harold Cameron David R. Loftis, P.E.
Junior Environmental Scientist Senior Engineer
Licensed, North Carolina No. 028345

Corrective Action Performance Report January 5, 2023
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-01

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TABLE OF CONTENTS

1.0 INTRODUCTION.......................................................................................................................... 1
1.1 Site Identification ............................................................................................................................. 1
1.2 Information about Contacts Associated with the Leaking UST System .......................................... 1
1.3 Information about Release ............................................................................................................... 1
2.0 EXECUTIVE SUMMARY ........................................................................................................... 2
3.0 SITE HISTORY AND CHARACTERISTICS ............................................................................ 3
3.1 Property Information ........................................................................................................................ 3
3.2 Site History ...................................................................................................................................... 3
3.3 UST Information .............................................................................................................................. 3
3.4 Non-UST Information ...................................................................................................................... 3
3.5 Release Description ......................................................................................................................... 3
3.6 Site Characteristics........................................................................................................................... 3
3.7 Geology/Hydrogeology.................................................................................................................... 4
4.0 REMEDIATION SYSTEM OPERATION ................................................................................. 5
4.1 Equipment Operation Data .............................................................................................................. 5
4.2 Mass Removal by Soil Vapor Extraction ......................................................................................... 5
5.0 CONCLUSIONS ............................................................................................................................ 7

Appendices

Appendix A Supplementary Groundwater Report
Appendix B Figures
Appendix C Tables
Appendix D Laboratory Analytical Report

Corrective Action Performance Report January 5, 2023
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-01

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2.0 EXECUTIVE SUMMARY
The CAPR should be reviewed in conjunction with the Monitoring Report prepared by Mr. Richard Kelly,
P.G. with Southeastern Geological Services and dated November 14, 2022 – included in Appendix A

The Site is located at the intersection of Sherrills Ford Road at NC Highway 150 in Terrell, Catawba
County, North Carolina and was formerly operated as a retail fueling station from 1978 until May 2014. In
2014, soil and groundwater petroleum impacts were discovered as a result of releases from a 3,000-gallon
diesel UST, 4,000-gallon gasoline UST, and a 12,000-gallon gasoline UST. The release led to significant
groundwater impacts north of the Site with free product thicknesses ranging from 3.98 feet to 4.89 feet.

An air sparge (AS) and soil vapor extraction system (SVE) utilizing three AS wells and two SVE wells is
currently being employed to remove free product and reduce the dissolved petroleum concentrations to
below Gross Contamination Levels (GCLs). The remediation system was activated on February 7, 2018
and deactivated, according to Mr. Kelly, sometime around August 2019. The system was reactivated on
March 11, 2022. The CAPR documents the operation and performance of the remediation system from
June 2, 2022 to December 28, 2022. The SVE system operated approximately 89% of the available run
time while the AS system operated only 84% of the available run time. The reduced run time associated
with the AS was associated with power loss issues and adjustments with the compressor that are needed to
allow the air compressor to restart once the power loss scenario has been corrected. Other issues included
the SVE run time timer within the PLC system being inconsistent and inaccurate after September 30, 2022.
Horner, the manufacturer of the PLC system, has been contacted and the timer problem is being
troubleshooted.

During the groundwater sampling event summarized in the Monitoring Report, groundwater samples were
collected and analyzed from 16 monitoring wells. Free product was not detected in the Site’s monitoring
wells and has not been detected since December 2018. Only two Gross Contamination Level (GCL)
violations were identified during the current sampling event, naphthalene and 1,2,4-trimethylbenzene
concentrations in monitoring well MW-16.

During the operational period discussed as part of this CAPR (June 2, 2022 to December 28, 2022),
approximately 1,358 pounds of petroleum hydrocarbons (11.7 pounds as benzene) were removed from the
soil and groundwater via the SVE system. A review of the benzene mass in groundwater data indicates that
approximately 7 pounds of benzene have been removed from just groundwater between June 2022 to
December 2022.

A review of the historical groundwater data indicates that the groundwater remediation system is effectively
reducing the groundwater petroleum impacts. BLE recommends that the operation of the remediation
system be continued.

Corrective Action Performance Report January 5, 2023
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-01

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3.0 SITE HISTORY AND CHARACTERISTICS
3.1 Property Information

The Site is located at the intersection of Sherrills Ford Road at NC Highway 150 in Terrell, Catawba
County, North Carolina. The location of the Site is noted on Figures 1 and 2, in Appendix B. Figure 3,
Appendix B depicts the approximate location of the former UST system and the monitoring and
remediation wells.

The Site is a 0.28-acre parcel that is part of a 36-acre tract owned by Mr. Charles Connor.

3.2 Site History

A retail fueling station formerly operated on the subject property from 1978 until May 2014, when the UST
system components were permanently removed. A release of petroleum products leading to soil and
groundwater impacts was documented from the UST system.

3.3 UST Information

UST I.D.
Number Product Capacity
(gallons) Date Installed Date
Closed
Associated with
Suspected
Release?
1 Gasoline 4,000 8/18/78 5/7/14 No
2 Diesel 3,000 8/18/78 5/7/14 Yes
3 Gasoline 4,000 8/18/78 5/7/14 Yes
4 Gasoline 12,000 10/31/98 5/7/14 Yes

No USTs are currently located on the Site.

3.4 Non-UST Information

No above-ground storage tanks (ASTs) are located or were located at the Site.

3.5 Release Description

As noted in Section 3.2, a release was documented from a former UST system in May 2014. Petroleum-
impacted soil was documented in association with two (2) gasoline USTs (4,000 gallons and 12,000 gallons)
and one (1) 3,000-gallon diesel UST.

3.6 Site Characteristics

• Land Use of the Site: The Site is currently vacant and does not have a usage. The convenience
store structure has been demolished and only the soil and groundwater remediation system resides
on-Site.

• Land Use of Surrounding Area: The surrounding area is a mix of light commercial and residential.

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• Topography: The surface topography generally slopes to the northeast.

• Vegetation/Surface Cover: The Site’s surface includes concrete and asphalt pavement west and
south of the former convenience store structure and grass/weeds north and east of the former
convenience store structure.

• Surface Water: No surface water features were identified within 1,000 feet of the release area.

• Wells: There are six active water supply wells within 1,000 feet of the release area.

• Buildings: No buildings are currently on-Site.

• Depth to Nature of Bedrock: A soil boring has been completed to 70 feet below grade (BG) and
bedrock was not encountered.

3.7 Geology/Hydrogeology

The Site is divided between the Charlotte Belts and Kings Mountain with the upper three to seven feet of
silty clay overburden before transitioning to saprolite. Bedrock has not been encountered at the Site, but
according, to Mr. Richard Kelly, Geologist with Southern Geological Services, in the March 28, 2019
Corrective Action Performance Report (CAPR), the depth to bedrock is likely around 75 to 80 feet BG.
Mr. Kelly further noted in the CAPR that the depth to bedrock at the Terrell Shell incident, located south
of NC Highway 150, was around 85 feet BG.

The Site slopes to the northeast toward Beaverdam Creek; however, no surface water bodies are present
within 1,000 feet of the release area. The depth to groundwater at the site is approximately 40 feet BG and
is documented to generally flow to the north.

The Site is generally surrounded by properties utilized for light commercial and residential purposes.
Specifically, the adjacent property to the south-southeast is operated as a United States Postal Service office
and Terrell Camping Center, a recreational vehicles dealership.

Based on a 2018 updated receptor survey performed by Southern Geological Services, there are six active
water supply wells within 1,000 feet of the release area. Five of the active water supply well wells are
located upgradient of the Site and the remaining well is located downgradient of the Site and approximately
950 feet from the release area.

Corrective Action Performance Report January 5, 2023
Terrell Bait Shop, Terrell, Catawba County, North Carolina BLE Project No. J22-17256-01

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4.0 REMEDIATION SYSTEM OPERATION
The petroleum-impacted soil and groundwater are currently being remediated using AS and SVE. The
remediation system is comprised of three AS wells that receive compressed air from a 3 horsepower (HP)
air compressor and two SVE wells that supply influent air to a Roots-style blower driven by a 5 HP motor.
The remediation system primarily focuses on reduction in contaminant concentrations in the vicinity of
monitoring wells MW-2, MW-10 and MW-16, as this area has historically exhibited the greatest degree of
petroleum impacts. On January 3, 2018, and prior to beginning remedial actions, the free product thickness
in MW-2, MW-10, and MW-16 measured 3.98 feet, 4.89 feet, and 4.85 feet, respectively.

4.1 Equipment Operation Data

Table 1, Appendix C summarizes the operational data collected during March to a portion of December
2022. During the period, the SVE and AS systems operated 89% and 84% operated consistently with
generally no down time except when electrical repairs were being made.

4.2 Mass Removal by Soil Vapor Extraction

On July 14, 2022 and October 18, 2022, samples was collected from the emission stream from the soil
vapor extraction system and analyzed for benzene, ethylbenzene, toluene, total xylenes, methyl tert-butyl
ether (MTBE), and total petroleum hydrocarbons (TPH) by Method 18. The results of the emission
sampling is summarized in Table 1 and the laboratory report is included in Appendix D.

Using the emission sampling data, BLE estimated the total mass of BTEX (172 pounds), MTBE (0.19
pounds), and TPH (1,358 pounds) removed by the system during the operational period herein. The results
are summarized in Table 2.

4.3 Total Gallons of Water Treated

The remediation system treats an unspecified volume of petroleum-impacted groundwater within the
unconfined aquifer using AS and SVE techniques. The benzene isoconcentration data generated by
Southeastern Geological Services from December 2021 and November 2022 was utilized to estimate the
reduction in benzene from the Site’s groundwater. The analysis is summarized in Table 3, Appendix C
and indicates that the benzene mass was reduced by approximately 11.7 pounds from June 2022 to
November 2022.

The change in benzene mass was estimated using the following method and assumptions:

• The surface area between the isoconcentration contour lines prepared by Southeastern Geologic
were estimated by GIS Methods.
• The surface area for each isoconcentration interval was multiplied by the estimated depth of
contamination (assumed to be 25 feet). Assuming an estimated porosity of 0.30, the total volume
of groundwater between each isoconcentration line is calculated.
• The average compound concentration within an isoconcentration interval is calculated. For
example, if the isoconcentration interval is between the 1 microgram per liter (g/L)
isoconcentration line and the 5,000 g/L isoconcentration line the average compound concentration
for the isoconcentration interval would be 2,500 g/L.

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• The average compound concentration within an interval is multiplied by the total volume of
groundwater within the same interval, resulting in the contaminant mass within the isoconcentration
interval.
• The contamination masses within each isoconcentration interval are added together to obtain the
total contaminant mass in the unconfined aquifer.
• For this report, the total benzene mass based on the laboratory analytical results from the current
sampling event was compared to the total benzene mass based on the laboratory analytical results
from the prior sampling event to determine the change in total benzene mass.

Corrective Action Performance Report January 5, 2023
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5.0 CONCLUSIONS
The AS and SVE system was reactivated on March 11, 2022, after being deactivated around August 2019.
From June 2, 2022 to December 28, 2022, the SVE and AS systems operated approximately 89% and 84%,
respectively, of the available run time.

The emissions data from the SVE system indicated that approximately 1,358 pounds of petroleum
hydrocarbons (11.7 pounds as benzene) was removed from the soil and groundwater via the SVE system
from June 2022 to December 2022. A review of the benzene mass in groundwater data indicates that
approximately 7 pounds of benzene has been removed from groundwater from June 2022 to November
2022.

The most recent groundwater sampling event did not identify free product in the Site’s monitoring wells
and only one well, MW-16, exhibited a GCL exceedance. A review of the historical groundwater data
indicates that the groundwater remediation system is effectively reducing the groundwater petroleum
impacts. BLE recommends that the operation of the remediation system be continued.

Appendix A

Supplementary
Groundwater
Report

MW-7: BTEX/MTBE non detect,
MW-8: BTEX/MTBE non detect,
MW-9: BTEX/MTBE non detect,
MW-10: benzene and xylenes > standard, < GCL,
MW-11: BTEX/MTBE non-detect,
MW-12: benzene > standard, < GCL,
MW-16: BTEX > standard, < GCL (MTBE high report limit), and
MWs 3-4-5-15, VMW-1, and VMW-2: non-detect.
A comparison with the last sampling event follows.
MW-1: benzene decrease to < standard,
MW-2: BTEX/MTBE large decrease, ethylbenzene to < STD and benzene to < GCL,
MW-6: BTEX/MTBE increase from apparent anomalous non-detect, remains historically low,
MW-7: BTEX/MTBE remain non-detect,
MW-8: BTEX/MTBE remain non-detect,
MW-9: BTEX/MTBE remain non-detect,
MW-10: mixed increase and decrease, remain historically low,
MW-11: BTEX/MTBE remain non-detect,
MW-12: BTEX/MTBE extremely large decrease – second in a row,
MW-16: mixed results, benzene historically low – xylenes high, and
MWs 3-4-5-15, VMW-1, and VMW-2: remain non-detect.
1.3 Sampling Protocol
The monitor wells were sampled with new, disposable bailers after purging three well casing
volumes. The samples were placed in laboratory provided vials, fixed with a chain of custody,
and placed on ice for immediate delivery to PACE Analytical.
B. FREE PRODUCT
Free product was initially present in MWs 2, 10, and 16. The product has been removed, none
has been present since December 2018.
C. SOIL REMEDIATION – not applicable
D. GROUNDWATER REMEDIATION
The AS/SVE system was activated on March 11, 2022. It is maintained by Bunnell Lammons
Engineering (BLE). Mr. David Loftis of BLE prepared the Corrective Action Performance
Report for this period
E. CONCUSIONS
All contaminants decreased in MW-1 and are < standard. MW-1 is outside of the main plume
and is at the limits of the AS/SVE system. The main plume remains a narrow, shallow band that
follows the MWs 2-10-16-12 line. Overall, contaminants were reduced along this line, with the
highest contaminate levels in MW-16. MW-6 is just outside the upgradient end of the line.
Contaminant levels increased in MW-6 but are well below historical levels – this narrows the
plume.
The following show an overall positive trend: (1) consistent low contaminant levels in MW-1
after initial high levels, (2) free product has been eliminated, (3) sharp contaminant decreases in
MWs 10, 12, and 16, (4) steady decrease in contaminant levels to non detect in MW-7, a step out
well to the north-northwest, (5) decrease in contaminant levels in MW-6, thus narrowing the
plume, and (6) migration has not reached MW-5.
F. FIGURES
USGS Topographic Map
Site Map
Groundwater Flow Map
Benzene Iso-Concentration Map
Toluene Iso-Concentration Map
Ethylbenzene Iso-Concentration Map
Xylenes Iso-Concentration Map
MTBE Iso-Concentration Map
G. TABLES
Table B-4 Summary of Groundwater Sampling Results
Table 1 Historical Groundwater Sampling
Table B-7 Well Construction Information
H. APPENDICES
Contaminant Level Graphs: MWs 1, 2,6, 7, 10, 12, and 16 / linear & logarithmic scales
Laboratory Analysis/Chain of Custody
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B` 6200B 6200B 6200B 6200B 6200B 6200B 504.1
Contaminant of Concern/ Field
MeasurementBenzeneTolueneEthylbenzeneXylenesMTBEIPENaphthalene1,2DCEEDBEDBWell or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-1 11-14-22 MW-1 Monitor <1 2 <1 281 9 <1 33 <1 <1
MW-2 “ MW-2 “57 672 240 1798 73 99 546 <5 <5
MW-6 “ MW-6 “127 254 31 252 123 126 85 <1 <1
MW-7 “ MW-7 “ <1 1 <1 <2 <1 <1 <2 <1 <1
MW-8 “ MW-8 “ <1 <1 <1 <2 <1 <1 <2 <1 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)1 600 600 500 20 70 6 0.4 0.02 0.02
GCL (ug/l)5000 260000 84500 85500 20000 70000 6000 400 50 50
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
NOT SAMPLED: MWs 13-14
NON-DETECT (since original): MWs 3-4-5-15, VMW-1 & VMW-2
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B 6200B` 6200B` 6200B 6200B 6200B 6200B
Contaminant of Concern/ Field Measurementn-ButlybenzeneSec-ButylbenzeneTert-ButylbenzeneIsopropylbenzenen-PropylbenzeneStyrene1,2,4Trimethylbenzene1,3,5TrimethylbenzeneTCEWell or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-1 12-7-21 MW-1 Monitor <1 <1 <1 2 2 <1 200 61 <1
MW-2 “ MW-2 “ <5 <5 <5 17 70 <5 958 215 <5
MW-6 “ MW-6 “ <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-7 “ MW-7 <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-8 MW-8 <1 <1 <1 <1 <1 <1 <1 <1 <1
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)70 70 70 70 70 70 400 400 15
GCL (ug/l)6900 8500 15000 25000 30000 70000 28500 25000 15000
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B` 6200B 6200B 6200B 6200B 6200B 6200B 504.1
Contaminant of Concern/ Field
MeasurementBenzeneTolueneEthylbenzeneXylenesMTBEIPENaphthalene1,2DCEEDBEDBWell or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-9 12-7-21 MW-9 Monitor <1 <1 <1 <2 <1 <1 <2 <1 <1
MW-10 “ MW-10 “27 599 364 2177 <5 <5 658 <5 <5
MW-11 “ MW-11 “ <1 1 <1 <2 <1 <1 <2 <1 <1
MW-12 “ MW-12 “4 9 <1 8 14 12 7 <1 <1
MW-16 “ MW-16 “1210 16200 7320 43200 <500 <500 15200 <500 <500
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)1 600 600 500 20 70 6 0.4 0.02 0.02
GCL (ug/l)5000 260000 84500 85500 20000 70000 6000 400 50 50
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination level Rounded to Whole Numbers
NOT SAMPLED: MWs 13-14
NON-DETECT (since original): MWs 3-4-5-15, VMW-1 & VMW-2
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 12-27-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Analytical Method (e.g., VOC by SM6000B) or
Field Measurement (FM)6200B 6200B 6200B 6200B` 6200B` 6200B 6200B 6200B 6200B
Contaminant of Concern/ Field Measurementn-ButlybenzeneSec-ButylbenzeneTert-ButylbenzeneIsopropylbenzenen-PropylbenzeneStyrene1,2,4Trimethylbenzene1,3,5TrimethylbenzeneTCEWell or
SW ID
Date
Collected
Sample
ID
Incident
Phase
MW-9 12-7-21 MW-9 Monitor <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-10 “ MW-10 “ <5 <5 <5 55 248 <5 1780 503 <5
MW-11 “ MW-11 “ <1 <1 <1 <1 <1 <1 <1 <1 <1
MW-12 “ MW-12 <1 <1 <1 <1 <1 <1 3 <1 <1
MW-16 MW-16 2350 <500 <500 892 <500 <500 30100 7790 <500
Minimum Reporting Limit (ug/l)
2L Standard (ug/l)70 70 70 70 70 70 400 400 15
GCL (ug/l)6900 8500 15000 25000 30000 70000 28500 25000 15000
NC 2B Standard or EPA National Criteria
(ug/l)
Results must be reported in ug/l ug/l =micrograms per liter GCL = gross contamination
TABLE 1: HISTORICAL GROUNDWATER SAMPLING
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-1 10/16/2014 2820 21900 2830 15100 1230
10/17/2017 1120 8460 868 5520 387
5/31/2018 124 147 196 889 244
12/10/2018 7 10 1 133 112
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 9 90 29 193 23
6/16/2020 <1 10 11 406 21
12/21/2020 <3 31 34 837 60
7/4/2021 1 5 <1 445 45
12/7/2021 8 9 5 28 2
6/3/2022 1 23 63 1269 42
11/14/2022 <1 2 <1 281 9
MW-2 10/16/2014 FP
10/17/2017 FP
5/31/2018 FP
12/10/2018 no product
6/12/2019 no product
12/16/2019 10800 23500 2430 12850 1080
6/16/2020 8930 27400 3240 19020 762
12/21/2020 5780 18900 1630 9090 376
7/4/2021 7010 21700 2200 11080 98
12/7/2021 3370 12100 1420 8160 <62
6/3/2022 16500 15800 1670 9960 291
11/14/2022 57 672 240 1798 73
MW-3 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-4 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-5 10/16/2014 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-6 4/9/2015 236 376 35 160 839
10/17/2017 4560 9420 363 4000 877
5/31/2018 6710 12500 753 4570 1290
12/10/2018 1770 1910 166 1093 831
6/12/2019 1600 2990 322 1661 683
12/16/2019 3660 6000 503 2670 761
6/16/2020 1500 4670 581 2750 298
12/21/2020 1620 5060 601 2780 246
7/4/2021 4070 14700 1530 8600 602
12/7/2021 1830 9360 1080 6400 359
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 127 254 31 252 123
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-7 4/9/2017 18 18 <1 <2 256
10/17/2017 86 104 12 57 173
5/31/2018 <2 517 56 172 227
12/10/2018 206 558 44 230 158
6/12/2019 275 342 32 173 336
12/16/2019 <1 <1 <1 <2 15
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-8 4/9/2017 <1 <1 <1 <2 87
10/17/2017 <1 <1 <1 <2 24
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-9 7/30/2015 2 10 4 11 <1
10/17/2017 <1 <1 <1 <2 60
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-10 7/30/2017 14200 43400 5700 30360 590
10/17/2017 FP
5/31/2018 FP
12/10/2018 FP
6/12/2019 no product
12/16/2019 15600 49600 4150 19280 464
6/16/2020 10500 73900 19900 108100 743
12/21/2020 5490 23100 3240 17580 435
7/4/2021 8180 31000 4460 25110 203
12/7/2021 13800 78100 22300 138700 <1000
6/3/2022 233 983 145 1115 73
11/14/2022 27 599 364 2177 <5
MW-11 7/30/2017 <1 1 <1 <2 143
10/17/2017 35 30 <1 3 <1
5/31/2018 1 2 <1 <2 <1
12/10/2018 23 8 <1 2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-12 7/30/2017 118 258 24 92 8
10/17/2017 10600 27000 1720 9710 235
5/31/2018 2740 6310 253 2360 435
12/10/2018 964 3260 134 1656 245
6/12/2019 3280 9690 522 3890 264
12/16/2019 5800 24900 1800 12230 400
6/16/2020 5680 18500 1400 8120 412
12/21/2020 5090 18800 1420 7970 419
7/4/2021 6900 29100 2290 12520 422
12/7/2021 9090 32500 2410 13530 507
6/3/2022 2450 6380 415 3150 248
11/14/2022 4 9 <1 8 14
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
MW-13 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 discontinue sampling
MW-14 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 discontinue sampling
MW-15 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
MW-16 10/26/2017 FP
10/17/2017 FP
5/31/2018 FP
12/10/2018 FP
6/12/2019 no product
12/16/2019 9530 29600 3410 17610 308
6/16/2020 7940 28300 2820 14350 <125
12/21/2020 8780 25800 1720 8920 <100
7/4/2021 12800 37600 3300 16730 103
12/7/2021 15900 64800 9460 53500 <500
6/3/2022 3350 19100 2570 14750 165
11/14/2022 1210 16200 7320 43200 <500
Benzene Toluene Ethtlb.Xylenes MTBE
Standard 1 600 600 500 20
GCL 5000 260000 84500 85500 20000
VMW-1 10/26/2015 <1 <1 <1 <2 <1
10/17/2017 <1 <1 <1 <2 <1
5/31/2018 <1 <1 <1 <2 <1
12/10/2018 <1 <1 <1 <2 <1
6/12/2019 <1 <1 <1 <2 <1
12/16/2019 <1 <1 <1 <2 <1
6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
VMW-2 6/16/2020 <1 <1 <1 <2 <1
12/21/2020 <1 <1 <1 <2 <1
7/4/2021 <1 <1 <1 <2 <1
12/7/2021 <1 <1 <1 <2 <1
6/3/2022 <1 <1 <1 <2 <1
11/14/2022 <1 <1 <1 <2 <1
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 12-10-18 Incident Number and Name: Terrell Bait Shop Facility ID#:
Well
ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS)
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Free
Product
Thickness
**(ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
1 10-14-14 11-14-22 2 34 34-39 39 100.97 37.46 0 63.51 35.589343
80.977701
2 10-14-14 “ 2 34 34-39 39 100.50 37.42 0 63.08 35.589422
80.977766
3 10-18-14 “ 2 34 34-39 39 100.00 37.52 0 62.48 35.589486
80.977894
4 10-27-14 “ 2 34 34-39 39 98.31 35.40 0 62.91 35.589525
80.977496
5 10-27-14 “ 2 33 33-38 38 95.61 33.94 0 61.67 35.589692
80.777452
6 4-5-15 “ 2 34 34-39 39 99.19 36.30 0 62.89 35.589490
80.977791
7 4-5-15 “ 2 34 34-39 39 98.84 36.13 0 62.71 35.589557
80.977819
8 4-6-15 “ 2 34 34-39 39 98.29 35.91 0 62.38 35.589598
80.977821
9 7-29-15 “ 2 34 34-39 39 99.04 36.57 0 62.47 35.589551
80.977856
10 7-15-15 “ 2 34 34-39 39 98.89 35.89 0 63.00 35.589502
80.977659
11 7-29-15 “ 2 34 34-39 39 98.28 36.05 0 62.23 35.589594
80.977753
12 7-15-15 “ 2 34 34-39 39 98.04 35.63 0 62.41 35.589569
80.977621
Ft BGS = feet below ground surface
* Reference Point for Elevation MeasurementsMW-3 , Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
***The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 12-10-18 Incident Number and Name: Terrell Bait Shop Facility ID#: 021875
Well ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS)
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Free
Product
Thickness
**(ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
MW-13 10-24-15 6-3-22 2 34 68-70 49 98.78 36.66 0 62.12 35.589343
80.977702
MW-14 10-24-15 “ 2 34 34-49 49 98.11 36.39 0 61.72 35.589250
80.977579
W-15 10-25-15 “ 2 32 32-47 47 96.30 34.84 0 61.46 30.589344
80.977339
MW-16 10-25-15 “ 2 34 34-49 49 98.60 35.82 0 62.78 35.589557
80.977584
VMW-1 4-25-15 “ 2 68 68-70 70 100.93 35.89343
80.977702
VMW-2 6-14-20 2 75 73-75 75 35.589422
80.977766
TS-8 2 35.589250
80.977579
TS-11 35.589344
80.977339
Ft BGS = feet below ground surface
* Reference Point for Elevation MeasurementsMW-3 , Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
***The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
0
5000
10000
15000
20000
25000
MW-1
B T E X MTBE
1
10
100
1000
10000
100000
MW-1
B T E X MTBE
0
5000
10000
15000
20000
25000
30000
MW-2
B T E X MTBE
1
10
100
1000
10000
100000
MW-2
B T E X MTBE
0
2000
4000
6000
8000
10000
12000
14000
16000
MW-6
B T E X MTBE
1
10
100
1000
10000
100000
MW-6
B T E X MTBE
0
100
200
300
400
500
600
MW-7
B T E X MTBE
1
10
100
1000
MW-7
B T E X MTBE
0
20000
40000
60000
80000
100000
120000
140000
160000
MW-10
B T E X MTBE
1
10
100
1000
10000
100000
1000000
MW-10
B T E X MTBE
0
20
40
60
80
100
120
140
160
MW-11
B T E X MTBE
1
10
100
1000
MW-11
B T E X MTBE
0
5000
10000
15000
20000
25000
30000
35000
MW-12
B T E X MTBE
1
10
100
1000
10000
100000
MW-12
B T E X MTBE
0
10000
20000
30000
40000
50000
60000
70000
MW-16
B T E X MTBE
1
10
100
1000
10000
100000
MW-16
B T E X MTBE
#=CL#
November 26, 2022
LIMS USE: FR - RICHARD KELLY
LIMS OBJECT ID: 92636499
92636499
Project:
Pace Project No.:
RE:
Mr. Richard Kelly
SE Geologic
301 Windsor Dr.
Shelby, NC 28150
TERRELL BAIT SHOP
Dear Mr. Kelly:
Enclosed are the analytical results for sample(s) received by the laboratory on November 14, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 56
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 56
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92636499001 MW 1 SM 6200B 63 PASI-CSAS
92636499002 MW 2 SM 6200B 63 PASI-CSAS
92636499003 MW 3 SM 6200B 63 PASI-CSAS
92636499004 MW 4 SM 6200B 63 PASI-CSAS
92636499005 MW 5 SM 6200B 63 PASI-CSAS
92636499006 MW 6 SM 6200B 63 PASI-CSAS
92636499007 MW 7 SM 6200B 63 PASI-CSAS
92636499008 MW 8 SM 6200B 63 PASI-CSAS
92636499009 MW 9 SM 6200B 63 PASI-CSAS
92636499010 MW 10 SM 6200B 63 PASI-CSAS
92636499011 MW 11 SM 6200B 63 PASI-CSAS
92636499012 MW 12 SM 6200B 63 PASI-CSAS
92636499013 MW 15 SM 6200B 63 PASI-CSAS
92636499014 MW 16 SM 6200B 63 PASI-CSAS
92636499015 VMW 1 SM 6200B 63 PASI-CSAS
92636499016 VMW 2 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 1 Lab ID:92636499001 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/21/22 16:30 71-43-21.0 2
Bromobenzene ND ug/L 11/21/22 16:30 108-86-11.0 2
Bromochloromethane ND ug/L 11/21/22 16:30 74-97-51.0 2
Bromodichloromethane ND ug/L 11/21/22 16:30 75-27-41.0 2
Bromoform ND ug/L 11/21/22 16:30 75-25-21.0 2
Bromomethane ND ug/L 11/21/22 16:30 74-83-910.0 2
n-Butylbenzene ND ug/L 11/21/22 16:30 104-51-81.0 2
sec-Butylbenzene ND ug/L 11/21/22 16:30 135-98-81.0 2
tert-Butylbenzene ND ug/L 11/21/22 16:30 98-06-61.0 2
Carbon tetrachloride ND ug/L 11/21/22 16:30 56-23-51.0 2
Chlorobenzene ND ug/L 11/21/22 16:30 108-90-71.0 2
Chloroethane ND ug/L 11/21/22 16:30 75-00-32.0 2
Chloroform 3.5 ug/L 11/21/22 16:30 67-66-31.0 2
Chloromethane ND ug/L 11/21/22 16:30 74-87-32.0 2
2-Chlorotoluene ND ug/L 11/21/22 16:30 95-49-81.0 2
4-Chlorotoluene ND ug/L 11/21/22 16:30 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 11/21/22 16:30 96-12-82.0 2
Dibromochloromethane ND ug/L 11/21/22 16:30 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 11/21/22 16:30 106-93-41.0 2
Dibromomethane ND ug/L 11/21/22 16:30 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 11/21/22 16:30 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 11/21/22 16:30 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 11/21/22 16:30 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 11/21/22 16:30 75-71-81.0 2
1,1-Dichloroethane ND ug/L 11/21/22 16:30 75-34-31.0 2
1,2-Dichloroethane ND ug/L 11/21/22 16:30 107-06-21.0 2
1,1-Dichloroethene ND ug/L 11/21/22 16:30 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 11/21/22 16:30 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 11/21/22 16:30 156-60-51.0 2
1,2-Dichloropropane ND ug/L 11/21/22 16:30 78-87-51.0 2
1,3-Dichloropropane ND ug/L 11/21/22 16:30 142-28-91.0 2
2,2-Dichloropropane ND ug/L 11/21/22 16:30 594-20-71.0 2
1,1-Dichloropropene ND ug/L 11/21/22 16:30 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 11/21/22 16:30 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 11/21/22 16:30 10061-02-61.0 2
Diisopropyl ether ND ug/L 11/21/22 16:30 108-20-31.0 2
Ethylbenzene ND ug/L 11/21/22 16:30 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 11/21/22 16:30 87-68-34.0 2
Isopropylbenzene (Cumene)2.2 ug/L 11/21/22 16:30 98-82-81.0 2
Methylene Chloride ND ug/L 11/21/22 16:30 75-09-24.0 2
Methyl-tert-butyl ether 8.5 ug/L 11/21/22 16:30 1634-04-41.0 2
Naphthalene 32.6 ug/L 11/21/22 16:30 91-20-34.0 2
n-Propylbenzene 2.2 ug/L 11/21/22 16:30 103-65-11.0 2
Styrene ND ug/L 11/21/22 16:30 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 11/21/22 16:30 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 11/21/22 16:30 79-34-51.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 1 Lab ID:92636499001 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/21/22 16:30 127-18-41.0 2
Toluene 2.0 ug/L 11/21/22 16:30 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 11/21/22 16:30 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 11/21/22 16:30 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 11/21/22 16:30 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 11/21/22 16:30 79-00-51.0 2
Trichloroethene ND ug/L 11/21/22 16:30 79-01-61.0 2
Trichlorofluoromethane ND ug/L 11/21/22 16:30 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 11/21/22 16:30 96-18-41.0 2
1,2,4-Trimethylbenzene 200 ug/L 11/21/22 16:30 95-63-61.0 2
1,3,5-Trimethylbenzene 60.8 ug/L 11/21/22 16:30 108-67-81.0 2
Vinyl chloride ND ug/L 11/21/22 16:30 75-01-42.0 2
m&p-Xylene 182 ug/L 11/21/22 16:30 179601-23-12.0 2
o-Xylene 63.4 ug/L 11/21/22 16:30 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)85 %11/21/22 16:30 17060-07-070-130 2
4-Bromofluorobenzene (S)98 %11/21/22 16:30 460-00-470-130 2
Toluene-d8 (S)103 %11/21/22 16:30 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 2 Lab ID:92636499002 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 57.1 ug/L 11/21/22 17:24 71-43-25.0 10
Bromobenzene ND ug/L 11/21/22 17:24 108-86-15.0 10
Bromochloromethane ND ug/L 11/21/22 17:24 74-97-55.0 10
Bromodichloromethane ND ug/L 11/21/22 17:24 75-27-45.0 10
Bromoform ND ug/L 11/21/22 17:24 75-25-25.0 10
Bromomethane ND ug/L 11/21/22 17:24 74-83-950.0 10
n-Butylbenzene ND ug/L 11/21/22 17:24 104-51-85.0 10
sec-Butylbenzene ND ug/L 11/21/22 17:24 135-98-85.0 10
tert-Butylbenzene ND ug/L 11/21/22 17:24 98-06-65.0 10
Carbon tetrachloride ND ug/L 11/21/22 17:24 56-23-55.0 10
Chlorobenzene ND ug/L 11/21/22 17:24 108-90-75.0 10
Chloroethane ND ug/L 11/21/22 17:24 75-00-310.0 10
Chloroform ND ug/L 11/21/22 17:24 67-66-35.0 10
Chloromethane ND ug/L 11/21/22 17:24 74-87-310.0 10
2-Chlorotoluene ND ug/L 11/21/22 17:24 95-49-85.0 10
4-Chlorotoluene ND ug/L 11/21/22 17:24 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 11/21/22 17:24 96-12-810.0 10
Dibromochloromethane ND ug/L 11/21/22 17:24 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 11/21/22 17:24 106-93-45.0 10
Dibromomethane ND ug/L 11/21/22 17:24 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 11/21/22 17:24 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 11/21/22 17:24 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 11/21/22 17:24 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 11/21/22 17:24 75-71-85.0 10
1,1-Dichloroethane ND ug/L 11/21/22 17:24 75-34-35.0 10
1,2-Dichloroethane ND ug/L 11/21/22 17:24 107-06-25.0 10
1,1-Dichloroethene ND ug/L 11/21/22 17:24 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 11/21/22 17:24 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 11/21/22 17:24 156-60-55.0 10
1,2-Dichloropropane ND ug/L 11/21/22 17:24 78-87-55.0 10
1,3-Dichloropropane ND ug/L 11/21/22 17:24 142-28-95.0 10
2,2-Dichloropropane ND ug/L 11/21/22 17:24 594-20-75.0 10
1,1-Dichloropropene ND ug/L 11/21/22 17:24 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 11/21/22 17:24 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 11/21/22 17:24 10061-02-65.0 10
Diisopropyl ether 98.7 ug/L 11/21/22 17:24 108-20-35.0 10
Ethylbenzene 240 ug/L 11/21/22 17:24 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 11/21/22 17:24 87-68-320.0 10
Isopropylbenzene (Cumene)17.4 ug/L 11/21/22 17:24 98-82-85.0 10
Methylene Chloride ND ug/L 11/21/22 17:24 75-09-220.0 10
Methyl-tert-butyl ether 73.4 ug/L 11/21/22 17:24 1634-04-45.0 10
Naphthalene 546 ug/L 11/21/22 17:24 91-20-320.0 10
n-Propylbenzene 70.4 ug/L 11/21/22 17:24 103-65-15.0 10
Styrene ND ug/L 11/21/22 17:24 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 11/21/22 17:24 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 11/21/22 17:24 79-34-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 2 Lab ID:92636499002 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/21/22 17:24 127-18-45.0 10
Toluene 672 ug/L 11/21/22 17:24 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 11/21/22 17:24 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 11/21/22 17:24 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 11/21/22 17:24 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 11/21/22 17:24 79-00-55.0 10
Trichloroethene ND ug/L 11/21/22 17:24 79-01-65.0 10
Trichlorofluoromethane ND ug/L 11/21/22 17:24 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 11/21/22 17:24 96-18-45.0 10
1,2,4-Trimethylbenzene 958 ug/L 11/21/22 17:24 95-63-65.0 10
1,3,5-Trimethylbenzene 215 ug/L 11/21/22 17:24 108-67-85.0 10
Vinyl chloride ND ug/L 11/21/22 17:24 75-01-410.0 10
m&p-Xylene 1100 ug/L 11/21/22 17:24 179601-23-110.0 10
o-Xylene 698 ug/L 11/21/22 17:24 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)86 %11/21/22 17:24 17060-07-070-130 10
4-Bromofluorobenzene (S)99 %11/21/22 17:24 460-00-470-130 10
Toluene-d8 (S)99 %11/21/22 17:24 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 3 Lab ID:92636499003 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 02:51 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 02:51 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 02:51 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 02:51 75-27-40.50 1
Bromoform ND ug/L 11/19/22 02:51 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 02:51 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 02:51 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 02:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 02:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 02:51 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 02:51 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 02:51 75-00-31.0 1
Chloroform ND ug/L 11/19/22 02:51 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 02:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 02:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 02:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 02:51 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 02:51 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 02:51 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 02:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 02:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 02:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 02:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 02:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 02:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 02:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 02:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 02:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 02:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 02:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 02:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 02:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 02:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 02:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 02:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 02:51 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 02:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 02:51 87-68-3 M12.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 02:51 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 02:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 02:51 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 02:51 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 02:51 103-65-10.50 1
Styrene ND ug/L 11/19/22 02:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 02:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 02:51 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 3 Lab ID:92636499003 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 02:51 127-18-40.50 1
Toluene ND ug/L 11/19/22 02:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 02:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 02:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 02:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 02:51 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 02:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 02:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 02:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 02:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 02:51 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 02:51 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 02:51 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 02:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/19/22 02:51 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %11/19/22 02:51 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 02:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 4 Lab ID:92636499004 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 03:09 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 03:09 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 03:09 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 03:09 75-27-40.50 1
Bromoform ND ug/L 11/19/22 03:09 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 03:09 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 03:09 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 03:09 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 03:09 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 03:09 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 03:09 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 03:09 75-00-31.0 1
Chloroform ND ug/L 11/19/22 03:09 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 03:09 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 03:09 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 03:09 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 03:09 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 03:09 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 03:09 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 03:09 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 03:09 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 03:09 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 03:09 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 03:09 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 03:09 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 03:09 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 03:09 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 03:09 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 03:09 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 03:09 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 03:09 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 03:09 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 03:09 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 03:09 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 03:09 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 03:09 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 03:09 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 03:09 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 03:09 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 03:09 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 03:09 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 03:09 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 03:09 103-65-10.50 1
Styrene ND ug/L 11/19/22 03:09 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 03:09 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 03:09 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 4 Lab ID:92636499004 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 03:09 127-18-40.50 1
Toluene ND ug/L 11/19/22 03:09 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 03:09 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 03:09 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 03:09 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 03:09 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 03:09 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 03:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 03:09 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 03:09 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 03:09 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 03:09 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 03:09 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 03:09 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/19/22 03:09 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %11/19/22 03:09 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 03:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 5 Lab ID:92636499005 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 03:27 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 03:27 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 03:27 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 03:27 75-27-40.50 1
Bromoform ND ug/L 11/19/22 03:27 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 03:27 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 03:27 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 03:27 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 03:27 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 03:27 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 03:27 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 03:27 75-00-31.0 1
Chloroform ND ug/L 11/19/22 03:27 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 03:27 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 03:27 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 03:27 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 03:27 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 03:27 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 03:27 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 03:27 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 03:27 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 03:27 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 03:27 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 03:27 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 03:27 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 03:27 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 03:27 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 03:27 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 03:27 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 03:27 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 03:27 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 03:27 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 03:27 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 03:27 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 03:27 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 03:27 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 03:27 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 03:27 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 03:27 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 03:27 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 03:27 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 03:27 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 03:27 103-65-10.50 1
Styrene ND ug/L 11/19/22 03:27 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 03:27 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 03:27 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 5 Lab ID:92636499005 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 03:27 127-18-40.50 1
Toluene ND ug/L 11/19/22 03:27 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 03:27 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 03:27 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 03:27 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 03:27 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 03:27 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 03:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 03:27 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 03:27 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 03:27 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 03:27 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 03:27 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 03:27 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/19/22 03:27 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %11/19/22 03:27 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 03:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 6 Lab ID:92636499006 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 127 ug/L 11/21/22 15:18 71-43-21.2 2.5
Bromobenzene ND ug/L 11/21/22 15:18 108-86-11.2 2.5
Bromochloromethane ND ug/L 11/21/22 15:18 74-97-51.2 2.5
Bromodichloromethane ND ug/L 11/21/22 15:18 75-27-41.2 2.5
Bromoform ND ug/L 11/21/22 15:18 75-25-21.2 2.5
Bromomethane ND ug/L 11/21/22 15:18 74-83-912.5 2.5
n-Butylbenzene ND ug/L 11/21/22 15:18 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 11/21/22 15:18 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 11/21/22 15:18 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 11/21/22 15:18 56-23-51.2 2.5
Chlorobenzene ND ug/L 11/21/22 15:18 108-90-71.2 2.5
Chloroethane ND ug/L 11/21/22 15:18 75-00-32.5 2.5
Chloroform ND ug/L 11/21/22 15:18 67-66-31.2 2.5
Chloromethane ND ug/L 11/21/22 15:18 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 11/21/22 15:18 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 11/21/22 15:18 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 11/21/22 15:18 96-12-82.5 2.5
Dibromochloromethane ND ug/L 11/21/22 15:18 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 11/21/22 15:18 106-93-41.2 2.5
Dibromomethane ND ug/L 11/21/22 15:18 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 11/21/22 15:18 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 11/21/22 15:18 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 11/21/22 15:18 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 11/21/22 15:18 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 11/21/22 15:18 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 11/21/22 15:18 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 11/21/22 15:18 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 11/21/22 15:18 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 11/21/22 15:18 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 11/21/22 15:18 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 11/21/22 15:18 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 11/21/22 15:18 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 11/21/22 15:18 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 11/21/22 15:18 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 11/21/22 15:18 10061-02-61.2 2.5
Diisopropyl ether 126 ug/L 11/21/22 15:18 108-20-31.2 2.5
Ethylbenzene 31.2 ug/L 11/21/22 15:18 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 11/21/22 15:18 87-68-35.0 2.5
Isopropylbenzene (Cumene)1.6 ug/L 11/21/22 15:18 98-82-81.2 2.5
Methylene Chloride ND ug/L 11/21/22 15:18 75-09-25.0 2.5
Methyl-tert-butyl ether 123 ug/L 11/21/22 15:18 1634-04-41.2 2.5
Naphthalene 85.3 ug/L 11/21/22 15:18 91-20-35.0 2.5
n-Propylbenzene 4.5 ug/L 11/21/22 15:18 103-65-11.2 2.5
Styrene ND ug/L 11/21/22 15:18 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 11/21/22 15:18 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 11/21/22 15:18 79-34-51.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 6 Lab ID:92636499006 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/21/22 15:18 127-18-41.2 2.5
Toluene 254 ug/L 11/21/22 15:18 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 11/21/22 15:18 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 11/21/22 15:18 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 11/21/22 15:18 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 11/21/22 15:18 79-00-51.2 2.5
Trichloroethene ND ug/L 11/21/22 15:18 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 11/21/22 15:18 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 11/21/22 15:18 96-18-41.2 2.5
1,2,4-Trimethylbenzene 62.3 ug/L 11/21/22 15:18 95-63-61.2 2.5
1,3,5-Trimethylbenzene 14.7 ug/L 11/21/22 15:18 108-67-81.2 2.5
Vinyl chloride ND ug/L 11/21/22 15:18 75-01-42.5 2.5
m&p-Xylene 139 ug/L 11/21/22 15:18 179601-23-12.5 2.5
o-Xylene 113 ug/L 11/21/22 15:18 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/21/22 15:18 17060-07-070-130 2.5
4-Bromofluorobenzene (S)99 %11/21/22 15:18 460-00-470-130 2.5
Toluene-d8 (S)90 %11/21/22 15:18 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 7 Lab ID:92636499007 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/21/22 14:42 71-43-20.50 1
Bromobenzene ND ug/L 11/21/22 14:42 108-86-10.50 1
Bromochloromethane ND ug/L 11/21/22 14:42 74-97-50.50 1
Bromodichloromethane ND ug/L 11/21/22 14:42 75-27-40.50 1
Bromoform ND ug/L 11/21/22 14:42 75-25-20.50 1
Bromomethane ND ug/L 11/21/22 14:42 74-83-95.0 1
n-Butylbenzene ND ug/L 11/21/22 14:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/21/22 14:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/21/22 14:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/21/22 14:42 56-23-50.50 1
Chlorobenzene ND ug/L 11/21/22 14:42 108-90-70.50 1
Chloroethane ND ug/L 11/21/22 14:42 75-00-31.0 1
Chloroform ND ug/L 11/21/22 14:42 67-66-30.50 1
Chloromethane ND ug/L 11/21/22 14:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/21/22 14:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/21/22 14:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/21/22 14:42 96-12-81.0 1
Dibromochloromethane ND ug/L 11/21/22 14:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/21/22 14:42 106-93-40.50 1
Dibromomethane ND ug/L 11/21/22 14:42 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/21/22 14:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/21/22 14:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/21/22 14:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/21/22 14:42 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/21/22 14:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/21/22 14:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/21/22 14:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/21/22 14:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/21/22 14:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/21/22 14:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/21/22 14:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/21/22 14:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/21/22 14:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/21/22 14:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/21/22 14:42 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/21/22 14:42 108-20-30.50 1
Ethylbenzene ND ug/L 11/21/22 14:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/21/22 14:42 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/21/22 14:42 98-82-80.50 1
Methylene Chloride ND ug/L 11/21/22 14:42 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/21/22 14:42 1634-04-40.50 1
Naphthalene ND ug/L 11/21/22 14:42 91-20-32.0 1
n-Propylbenzene ND ug/L 11/21/22 14:42 103-65-10.50 1
Styrene ND ug/L 11/21/22 14:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/21/22 14:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/21/22 14:42 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 7 Lab ID:92636499007 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/21/22 14:42 127-18-40.50 1
Toluene ND ug/L 11/21/22 14:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/21/22 14:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/21/22 14:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/21/22 14:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/21/22 14:42 79-00-50.50 1
Trichloroethene ND ug/L 11/21/22 14:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/21/22 14:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/21/22 14:42 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/21/22 14:42 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/21/22 14:42 108-67-80.50 1
Vinyl chloride ND ug/L 11/21/22 14:42 75-01-41.0 1
m&p-Xylene ND ug/L 11/21/22 14:42 179601-23-11.0 1
o-Xylene ND ug/L 11/21/22 14:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/21/22 14:42 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/21/22 14:42 460-00-470-130 1
Toluene-d8 (S)101 %11/21/22 14:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 8 Lab ID:92636499008 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 04:21 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 04:21 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 04:21 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 04:21 75-27-40.50 1
Bromoform ND ug/L 11/19/22 04:21 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 04:21 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 04:21 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 04:21 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 04:21 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 04:21 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 04:21 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 04:21 75-00-31.0 1
Chloroform ND ug/L 11/19/22 04:21 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 04:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 04:21 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 04:21 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 04:21 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 04:21 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 04:21 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 04:21 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 04:21 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 04:21 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 04:21 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 04:21 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 04:21 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 04:21 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 04:21 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 04:21 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 04:21 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 04:21 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 04:21 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 04:21 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 04:21 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 04:21 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 04:21 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 04:21 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 04:21 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 04:21 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 04:21 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 04:21 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 04:21 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 04:21 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 04:21 103-65-10.50 1
Styrene ND ug/L 11/19/22 04:21 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 04:21 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 04:21 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 8 Lab ID:92636499008 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 04:21 127-18-40.50 1
Toluene ND ug/L 11/19/22 04:21 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 04:21 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 04:21 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 04:21 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 04:21 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 04:21 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 04:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 04:21 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 04:21 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 04:21 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 04:21 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 04:21 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 04:21 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/19/22 04:21 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/19/22 04:21 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 04:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 9 Lab ID:92636499009 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 04:39 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 04:39 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 04:39 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 04:39 75-27-40.50 1
Bromoform ND ug/L 11/19/22 04:39 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 04:39 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 04:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 04:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 04:39 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 04:39 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 04:39 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 04:39 75-00-31.0 1
Chloroform ND ug/L 11/19/22 04:39 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 04:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 04:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 04:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 04:39 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 04:39 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 04:39 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 04:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 04:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 04:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 04:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 04:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 04:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 04:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 04:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 04:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 04:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 04:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 04:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 04:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 04:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 04:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 04:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 04:39 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 04:39 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 04:39 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 04:39 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 04:39 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 04:39 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 04:39 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 04:39 103-65-10.50 1
Styrene ND ug/L 11/19/22 04:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 04:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 04:39 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 9 Lab ID:92636499009 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 04:39 127-18-40.50 1
Toluene ND ug/L 11/19/22 04:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 04:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 04:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 04:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 04:39 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 04:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 04:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 04:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 04:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 04:39 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 04:39 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 04:39 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 04:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/19/22 04:39 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/19/22 04:39 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 04:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 10 Lab ID:92636499010 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 27.3 ug/L 11/19/22 07:03 71-43-25.0 10
Bromobenzene ND ug/L 11/19/22 07:03 108-86-15.0 10
Bromochloromethane ND ug/L 11/19/22 07:03 74-97-55.0 10
Bromodichloromethane ND ug/L 11/19/22 07:03 75-27-45.0 10
Bromoform ND ug/L 11/19/22 07:03 75-25-25.0 10
Bromomethane ND ug/L 11/19/22 07:03 74-83-950.0 10
n-Butylbenzene ND ug/L 11/19/22 07:03 104-51-85.0 10
sec-Butylbenzene ND ug/L 11/19/22 07:03 135-98-85.0 10
tert-Butylbenzene ND ug/L 11/19/22 07:03 98-06-65.0 10
Carbon tetrachloride ND ug/L 11/19/22 07:03 56-23-55.0 10
Chlorobenzene ND ug/L 11/19/22 07:03 108-90-75.0 10
Chloroethane ND ug/L 11/19/22 07:03 75-00-310.0 10
Chloroform ND ug/L 11/19/22 07:03 67-66-35.0 10
Chloromethane ND ug/L 11/19/22 07:03 74-87-310.0 10
2-Chlorotoluene ND ug/L 11/19/22 07:03 95-49-85.0 10
4-Chlorotoluene ND ug/L 11/19/22 07:03 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 07:03 96-12-810.0 10
Dibromochloromethane ND ug/L 11/19/22 07:03 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 07:03 106-93-45.0 10
Dibromomethane ND ug/L 11/19/22 07:03 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 11/19/22 07:03 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 11/19/22 07:03 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 11/19/22 07:03 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 11/19/22 07:03 75-71-85.0 10
1,1-Dichloroethane ND ug/L 11/19/22 07:03 75-34-35.0 10
1,2-Dichloroethane ND ug/L 11/19/22 07:03 107-06-25.0 10
1,1-Dichloroethene ND ug/L 11/19/22 07:03 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 11/19/22 07:03 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 11/19/22 07:03 156-60-55.0 10
1,2-Dichloropropane ND ug/L 11/19/22 07:03 78-87-55.0 10
1,3-Dichloropropane ND ug/L 11/19/22 07:03 142-28-95.0 10
2,2-Dichloropropane ND ug/L 11/19/22 07:03 594-20-75.0 10
1,1-Dichloropropene ND ug/L 11/19/22 07:03 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 11/19/22 07:03 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 11/19/22 07:03 10061-02-65.0 10
Diisopropyl ether ND ug/L 11/19/22 07:03 108-20-35.0 10
Ethylbenzene 364 ug/L 11/19/22 07:03 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 11/19/22 07:03 87-68-320.0 10
Isopropylbenzene (Cumene)55.1 ug/L 11/19/22 07:03 98-82-85.0 10
Methylene Chloride ND ug/L 11/19/22 07:03 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 11/19/22 07:03 1634-04-45.0 10
Naphthalene 658 ug/L 11/19/22 07:03 91-20-320.0 10
n-Propylbenzene 248 ug/L 11/19/22 07:03 103-65-15.0 10
Styrene ND ug/L 11/19/22 07:03 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 07:03 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 07:03 79-34-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 10 Lab ID:92636499010 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 07:03 127-18-45.0 10
Toluene 599 ug/L 11/19/22 07:03 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 11/19/22 07:03 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 11/19/22 07:03 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 11/19/22 07:03 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 11/19/22 07:03 79-00-55.0 10
Trichloroethene ND ug/L 11/19/22 07:03 79-01-65.0 10
Trichlorofluoromethane ND ug/L 11/19/22 07:03 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 11/19/22 07:03 96-18-45.0 10
1,2,4-Trimethylbenzene 1780 ug/L 11/19/22 07:03 95-63-65.0 10
1,3,5-Trimethylbenzene 503 ug/L 11/19/22 07:03 108-67-85.0 10
Vinyl chloride ND ug/L 11/19/22 07:03 75-01-410.0 10
m&p-Xylene 1490 ug/L 11/19/22 07:03 179601-23-110.0 10
o-Xylene 687 ug/L 11/19/22 07:03 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/19/22 07:03 17060-07-070-130 10
4-Bromofluorobenzene (S)99 %11/19/22 07:03 460-00-470-130 10
Toluene-d8 (S)102 %11/19/22 07:03 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 11 Lab ID:92636499011 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 04:57 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 04:57 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 04:57 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 04:57 75-27-40.50 1
Bromoform ND ug/L 11/19/22 04:57 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 04:57 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 04:57 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 04:57 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 04:57 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 04:57 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 04:57 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 04:57 75-00-31.0 1
Chloroform ND ug/L 11/19/22 04:57 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 04:57 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 04:57 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 04:57 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 04:57 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 04:57 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 04:57 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 04:57 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 04:57 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 04:57 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 04:57 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 04:57 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 04:57 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 04:57 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 04:57 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 04:57 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 04:57 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 04:57 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 04:57 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 04:57 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 04:57 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 04:57 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 04:57 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 04:57 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 04:57 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 04:57 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 04:57 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 04:57 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 04:57 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 04:57 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 04:57 103-65-10.50 1
Styrene ND ug/L 11/19/22 04:57 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 04:57 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 04:57 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 11 Lab ID:92636499011 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 04:57 127-18-40.50 1
Toluene ND ug/L 11/19/22 04:57 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 04:57 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 04:57 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 04:57 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 04:57 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 04:57 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 04:57 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 04:57 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 04:57 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 04:57 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 04:57 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 04:57 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 04:57 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/19/22 04:57 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %11/19/22 04:57 460-00-470-130 1
Toluene-d8 (S)104 %11/19/22 04:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 12 Lab ID:92636499012 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3.6 ug/L 11/21/22 15:00 71-43-21.0 2
Bromobenzene ND ug/L 11/21/22 15:00 108-86-11.0 2
Bromochloromethane ND ug/L 11/21/22 15:00 74-97-51.0 2
Bromodichloromethane ND ug/L 11/21/22 15:00 75-27-41.0 2
Bromoform ND ug/L 11/21/22 15:00 75-25-21.0 2
Bromomethane ND ug/L 11/21/22 15:00 74-83-910.0 2
n-Butylbenzene ND ug/L 11/21/22 15:00 104-51-81.0 2
sec-Butylbenzene ND ug/L 11/21/22 15:00 135-98-81.0 2
tert-Butylbenzene ND ug/L 11/21/22 15:00 98-06-61.0 2
Carbon tetrachloride ND ug/L 11/21/22 15:00 56-23-51.0 2
Chlorobenzene ND ug/L 11/21/22 15:00 108-90-71.0 2
Chloroethane ND ug/L 11/21/22 15:00 75-00-32.0 2
Chloroform ND ug/L 11/21/22 15:00 67-66-31.0 2
Chloromethane ND ug/L 11/21/22 15:00 74-87-32.0 2
2-Chlorotoluene ND ug/L 11/21/22 15:00 95-49-81.0 2
4-Chlorotoluene ND ug/L 11/21/22 15:00 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 11/21/22 15:00 96-12-82.0 2
Dibromochloromethane ND ug/L 11/21/22 15:00 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 11/21/22 15:00 106-93-41.0 2
Dibromomethane ND ug/L 11/21/22 15:00 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 11/21/22 15:00 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 11/21/22 15:00 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 11/21/22 15:00 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 11/21/22 15:00 75-71-81.0 2
1,1-Dichloroethane ND ug/L 11/21/22 15:00 75-34-31.0 2
1,2-Dichloroethane ND ug/L 11/21/22 15:00 107-06-21.0 2
1,1-Dichloroethene ND ug/L 11/21/22 15:00 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 11/21/22 15:00 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 11/21/22 15:00 156-60-51.0 2
1,2-Dichloropropane ND ug/L 11/21/22 15:00 78-87-51.0 2
1,3-Dichloropropane ND ug/L 11/21/22 15:00 142-28-91.0 2
2,2-Dichloropropane ND ug/L 11/21/22 15:00 594-20-71.0 2
1,1-Dichloropropene ND ug/L 11/21/22 15:00 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 11/21/22 15:00 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 11/21/22 15:00 10061-02-61.0 2
Diisopropyl ether 11.6 ug/L 11/21/22 15:00 108-20-31.0 2
Ethylbenzene ND ug/L 11/21/22 15:00 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 11/21/22 15:00 87-68-34.0 2
Isopropylbenzene (Cumene)ND ug/L 11/21/22 15:00 98-82-81.0 2
Methylene Chloride ND ug/L 11/21/22 15:00 75-09-24.0 2
Methyl-tert-butyl ether 13.8 ug/L 11/21/22 15:00 1634-04-41.0 2
Naphthalene 6.6 ug/L 11/21/22 15:00 91-20-34.0 2
n-Propylbenzene ND ug/L 11/21/22 15:00 103-65-11.0 2
Styrene ND ug/L 11/21/22 15:00 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 11/21/22 15:00 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 11/21/22 15:00 79-34-51.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 12 Lab ID:92636499012 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/21/22 15:00 127-18-41.0 2
Toluene 9.0 ug/L 11/21/22 15:00 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 11/21/22 15:00 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 11/21/22 15:00 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 11/21/22 15:00 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 11/21/22 15:00 79-00-51.0 2
Trichloroethene ND ug/L 11/21/22 15:00 79-01-61.0 2
Trichlorofluoromethane ND ug/L 11/21/22 15:00 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 11/21/22 15:00 96-18-41.0 2
1,2,4-Trimethylbenzene 2.7 ug/L 11/21/22 15:00 95-63-61.0 2
1,3,5-Trimethylbenzene ND ug/L 11/21/22 15:00 108-67-81.0 2
Vinyl chloride ND ug/L 11/21/22 15:00 75-01-42.0 2
m&p-Xylene 4.0 ug/L 11/21/22 15:00 179601-23-12.0 2
o-Xylene 4.4 ug/L 11/21/22 15:00 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)91 %11/21/22 15:00 17060-07-0 D370-130 2
4-Bromofluorobenzene (S)101 %11/21/22 15:00 460-00-470-130 2
Toluene-d8 (S)97 %11/21/22 15:00 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 15 Lab ID:92636499013 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 05:15 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 05:15 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 05:15 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 05:15 75-27-40.50 1
Bromoform ND ug/L 11/19/22 05:15 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 05:15 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 05:15 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 05:15 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 05:15 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 05:15 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 05:15 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 05:15 75-00-31.0 1
Chloroform ND ug/L 11/19/22 05:15 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 05:15 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 05:15 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 05:15 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 05:15 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 05:15 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 05:15 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 05:15 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 05:15 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 05:15 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 05:15 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 05:15 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 05:15 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 05:15 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 05:15 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 05:15 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 05:15 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 05:15 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 05:15 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 05:15 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 05:15 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 05:15 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 05:15 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 05:15 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 05:15 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 05:15 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 05:15 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 05:15 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 05:15 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 05:15 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 05:15 103-65-10.50 1
Styrene ND ug/L 11/19/22 05:15 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 05:15 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 05:15 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 15 Lab ID:92636499013 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 05:15 127-18-40.50 1
Toluene ND ug/L 11/19/22 05:15 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 05:15 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 05:15 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 05:15 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 05:15 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 05:15 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 05:15 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 05:15 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 05:15 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 05:15 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 05:15 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 05:15 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 05:15 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/19/22 05:15 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/19/22 05:15 460-00-470-130 1
Toluene-d8 (S)103 %11/19/22 05:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 16 Lab ID:92636499014 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1210 ug/L 11/22/22 20:12 71-43-25001000
Bromobenzene ND ug/L 11/22/22 20:12 108-86-15001000
Bromochloromethane ND ug/L 11/22/22 20:12 74-97-55001000
Bromodichloromethane ND ug/L 11/22/22 20:12 75-27-45001000
Bromoform ND ug/L 11/22/22 20:12 75-25-25001000
Bromomethane ND ug/L 11/22/22 20:12 74-83-950001000
n-Butylbenzene 2350 ug/L 11/22/22 20:12 104-51-85001000
sec-Butylbenzene ND ug/L 11/22/22 20:12 135-98-85001000
tert-Butylbenzene ND ug/L 11/22/22 20:12 98-06-65001000
Carbon tetrachloride ND ug/L 11/22/22 20:12 56-23-55001000
Chlorobenzene ND ug/L 11/22/22 20:12 108-90-75001000
Chloroethane ND ug/L 11/22/22 20:12 75-00-310001000
Chloroform ND ug/L 11/22/22 20:12 67-66-35001000
Chloromethane ND ug/L 11/22/22 20:12 74-87-310001000
2-Chlorotoluene ND ug/L 11/22/22 20:12 95-49-85001000
4-Chlorotoluene ND ug/L 11/22/22 20:12 106-43-45001000
1,2-Dibromo-3-chloropropane ND ug/L 11/22/22 20:12 96-12-810001000
Dibromochloromethane ND ug/L 11/22/22 20:12 124-48-15001000
1,2-Dibromoethane (EDB)ND ug/L 11/22/22 20:12 106-93-45001000
Dibromomethane ND ug/L 11/22/22 20:12 74-95-35001000
1,2-Dichlorobenzene ND ug/L 11/22/22 20:12 95-50-15001000
1,3-Dichlorobenzene ND ug/L 11/22/22 20:12 541-73-15001000
1,4-Dichlorobenzene ND ug/L 11/22/22 20:12 106-46-75001000
Dichlorodifluoromethane ND ug/L 11/22/22 20:12 75-71-85001000
1,1-Dichloroethane ND ug/L 11/22/22 20:12 75-34-35001000
1,2-Dichloroethane ND ug/L 11/22/22 20:12 107-06-25001000
1,1-Dichloroethene ND ug/L 11/22/22 20:12 75-35-45001000
cis-1,2-Dichloroethene ND ug/L 11/22/22 20:12 156-59-25001000
trans-1,2-Dichloroethene ND ug/L 11/22/22 20:12 156-60-55001000
1,2-Dichloropropane ND ug/L 11/22/22 20:12 78-87-55001000
1,3-Dichloropropane ND ug/L 11/22/22 20:12 142-28-95001000
2,2-Dichloropropane ND ug/L 11/22/22 20:12 594-20-75001000
1,1-Dichloropropene ND ug/L 11/22/22 20:12 563-58-65001000
cis-1,3-Dichloropropene ND ug/L 11/22/22 20:12 10061-01-55001000
trans-1,3-Dichloropropene ND ug/L 11/22/22 20:12 10061-02-65001000
Diisopropyl ether ND ug/L 11/22/22 20:12 108-20-35001000
Ethylbenzene 7320 ug/L 11/22/22 20:12 100-41-45001000
Hexachloro-1,3-butadiene ND ug/L 11/22/22 20:12 87-68-320001000
Isopropylbenzene (Cumene)892 ug/L 11/22/22 20:12 98-82-85001000
Methylene Chloride ND ug/L 11/22/22 20:12 75-09-220001000
Methyl-tert-butyl ether ND ug/L 11/22/22 20:12 1634-04-45001000
Naphthalene 15200 ug/L 11/22/22 20:12 91-20-320001000
n-Propylbenzene ND ug/L 11/22/22 20:12 103-65-15001000
Styrene ND ug/L 11/22/22 20:12 100-42-55001000
1,1,1,2-Tetrachloroethane ND ug/L 11/22/22 20:12 630-20-65001000
1,1,2,2-Tetrachloroethane ND ug/L 11/22/22 20:12 79-34-55001000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:MW 16 Lab ID:92636499014 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/22/22 20:12 127-18-45001000
Toluene 16200 ug/L 11/22/22 20:12 108-88-35001000
1,2,3-Trichlorobenzene ND ug/L 11/22/22 20:12 87-61-620001000
1,2,4-Trichlorobenzene ND ug/L 11/22/22 20:12 120-82-120001000
1,1,1-Trichloroethane ND ug/L 11/22/22 20:12 71-55-65001000
1,1,2-Trichloroethane ND ug/L 11/22/22 20:12 79-00-55001000
Trichloroethene ND ug/L 11/22/22 20:12 79-01-65001000
Trichlorofluoromethane ND ug/L 11/22/22 20:12 75-69-410001000
1,2,3-Trichloropropane ND ug/L 11/22/22 20:12 96-18-45001000
1,2,4-Trimethylbenzene 30100 ug/L 11/22/22 20:12 95-63-65001000
1,3,5-Trimethylbenzene 7790 ug/L 11/22/22 20:12 108-67-85001000
Vinyl chloride ND ug/L 11/22/22 20:12 75-01-410001000
m&p-Xylene 29400 ug/L 11/22/22 20:12 179601-23-110001000
o-Xylene 13800 ug/L 11/22/22 20:12 95-47-65001000
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/22/22 20:12 17060-07-070-130 1000
4-Bromofluorobenzene (S)102 %11/22/22 20:12 460-00-470-130 1000
Toluene-d8 (S)82 %11/22/22 20:12 2037-26-570-130 1000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:VMW 1 Lab ID:92636499015 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 05:33 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 05:33 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 05:33 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 05:33 75-27-40.50 1
Bromoform ND ug/L 11/19/22 05:33 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 05:33 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 05:33 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 05:33 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 05:33 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 05:33 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 05:33 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 05:33 75-00-31.0 1
Chloroform ND ug/L 11/19/22 05:33 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 05:33 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 05:33 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 05:33 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 05:33 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 05:33 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 05:33 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 05:33 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 05:33 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 05:33 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 05:33 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 05:33 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 05:33 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 05:33 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 05:33 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 05:33 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 05:33 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 05:33 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 05:33 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 05:33 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 05:33 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 05:33 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 05:33 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 05:33 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 05:33 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 05:33 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 05:33 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 05:33 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 05:33 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 05:33 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 05:33 103-65-10.50 1
Styrene ND ug/L 11/19/22 05:33 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 05:33 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 05:33 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:VMW 1 Lab ID:92636499015 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 05:33 127-18-40.50 1
Toluene ND ug/L 11/19/22 05:33 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 05:33 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 05:33 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 05:33 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 05:33 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 05:33 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 05:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 05:33 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 05:33 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 05:33 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 05:33 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 05:33 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 05:33 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/19/22 05:33 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %11/19/22 05:33 460-00-470-130 1
Toluene-d8 (S)102 %11/19/22 05:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:VMW 2 Lab ID:92636499016 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/19/22 05:51 71-43-20.50 1
Bromobenzene ND ug/L 11/19/22 05:51 108-86-10.50 1
Bromochloromethane ND ug/L 11/19/22 05:51 74-97-50.50 1
Bromodichloromethane ND ug/L 11/19/22 05:51 75-27-40.50 1
Bromoform ND ug/L 11/19/22 05:51 75-25-20.50 1
Bromomethane ND ug/L 11/19/22 05:51 74-83-95.0 1
n-Butylbenzene ND ug/L 11/19/22 05:51 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/19/22 05:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/19/22 05:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/19/22 05:51 56-23-50.50 1
Chlorobenzene ND ug/L 11/19/22 05:51 108-90-70.50 1
Chloroethane ND ug/L 11/19/22 05:51 75-00-31.0 1
Chloroform ND ug/L 11/19/22 05:51 67-66-30.50 1
Chloromethane ND ug/L 11/19/22 05:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/19/22 05:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/19/22 05:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/19/22 05:51 96-12-81.0 1
Dibromochloromethane ND ug/L 11/19/22 05:51 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/19/22 05:51 106-93-40.50 1
Dibromomethane ND ug/L 11/19/22 05:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/19/22 05:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/19/22 05:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/19/22 05:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/19/22 05:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/19/22 05:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/19/22 05:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/19/22 05:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/19/22 05:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/19/22 05:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/19/22 05:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/19/22 05:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/19/22 05:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/19/22 05:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/19/22 05:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/19/22 05:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/19/22 05:51 108-20-30.50 1
Ethylbenzene ND ug/L 11/19/22 05:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/19/22 05:51 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/19/22 05:51 98-82-80.50 1
Methylene Chloride ND ug/L 11/19/22 05:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/19/22 05:51 1634-04-40.50 1
Naphthalene ND ug/L 11/19/22 05:51 91-20-32.0 1
n-Propylbenzene ND ug/L 11/19/22 05:51 103-65-10.50 1
Styrene ND ug/L 11/19/22 05:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/19/22 05:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/19/22 05:51 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Sample:VMW 2 Lab ID:92636499016 Collected:11/14/22 14:25 Received:11/14/22 15:08 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/19/22 05:51 127-18-40.50 1
Toluene ND ug/L 11/19/22 05:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/19/22 05:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/19/22 05:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/19/22 05:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/19/22 05:51 79-00-50.50 1
Trichloroethene ND ug/L 11/19/22 05:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/19/22 05:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/19/22 05:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/19/22 05:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/19/22 05:51 108-67-80.50 1
Vinyl chloride ND ug/L 11/19/22 05:51 75-01-41.0 1
m&p-Xylene ND ug/L 11/19/22 05:51 179601-23-11.0 1
o-Xylene ND ug/L 11/19/22 05:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/19/22 05:51 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/19/22 05:51 460-00-470-130 1
Toluene-d8 (S)103 %11/19/22 05:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
738197
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92636499003, 92636499004, 92636499005, 92636499008, 92636499009, 92636499010, 92636499011,
92636499013, 92636499015, 92636499016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3841818
Associated Lab Samples:92636499003, 92636499004, 92636499005, 92636499008, 92636499009, 92636499010, 92636499011,
92636499013, 92636499015, 92636499016
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/19/22 02:33
1,1,1-Trichloroethane ug/L ND 0.50 11/19/22 02:33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/19/22 02:33
1,1,2-Trichloroethane ug/L ND 0.50 11/19/22 02:33
1,1-Dichloroethane ug/L ND 0.50 11/19/22 02:33
1,1-Dichloroethene ug/L ND 0.50 11/19/22 02:33
1,1-Dichloropropene ug/L ND 0.50 11/19/22 02:33
1,2,3-Trichlorobenzene ug/L ND 2.0 11/19/22 02:33
1,2,3-Trichloropropane ug/L ND 0.50 11/19/22 02:33
1,2,4-Trichlorobenzene ug/L ND 2.0 11/19/22 02:33
1,2,4-Trimethylbenzene ug/L ND 0.50 11/19/22 02:33
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/19/22 02:33
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/19/22 02:33
1,2-Dichlorobenzene ug/L ND 0.50 11/19/22 02:33
1,2-Dichloroethane ug/L ND 0.50 11/19/22 02:33
1,2-Dichloropropane ug/L ND 0.50 11/19/22 02:33
1,3,5-Trimethylbenzene ug/L ND 0.50 11/19/22 02:33
1,3-Dichlorobenzene ug/L ND 0.50 11/19/22 02:33
1,3-Dichloropropane ug/L ND 0.50 11/19/22 02:33
1,4-Dichlorobenzene ug/L ND 0.50 11/19/22 02:33
2,2-Dichloropropane ug/L ND 0.50 11/19/22 02:33
2-Chlorotoluene ug/L ND 0.50 11/19/22 02:33
4-Chlorotoluene ug/L ND 0.50 11/19/22 02:33
Benzene ug/L ND 0.50 11/19/22 02:33
Bromobenzene ug/L ND 0.50 11/19/22 02:33
Bromochloromethane ug/L ND 0.50 11/19/22 02:33
Bromodichloromethane ug/L ND 0.50 11/19/22 02:33
Bromoform ug/L ND 0.50 11/19/22 02:33
Bromomethane ug/L ND 5.0 11/19/22 02:33
Carbon tetrachloride ug/L ND 0.50 11/19/22 02:33
Chlorobenzene ug/L ND 0.50 11/19/22 02:33
Chloroethane ug/L ND 1.0 11/19/22 02:33
Chloroform ug/L ND 0.50 11/19/22 02:33
Chloromethane ug/L ND 1.0 11/19/22 02:33
cis-1,2-Dichloroethene ug/L ND 0.50 11/19/22 02:33
cis-1,3-Dichloropropene ug/L ND 0.50 11/19/22 02:33
Dibromochloromethane ug/L ND 0.50 11/19/22 02:33
Dibromomethane ug/L ND 0.50 11/19/22 02:33
Dichlorodifluoromethane ug/L ND 0.50 11/19/22 02:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3841818
Associated Lab Samples:92636499003, 92636499004, 92636499005, 92636499008, 92636499009, 92636499010, 92636499011,
92636499013, 92636499015, 92636499016
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 11/19/22 02:33
Ethylbenzene ug/L ND 0.50 11/19/22 02:33
Hexachloro-1,3-butadiene ug/L ND 2.0 11/19/22 02:33
Isopropylbenzene (Cumene)ug/L ND 0.50 11/19/22 02:33
m&p-Xylene ug/L ND 1.0 11/19/22 02:33
Methyl-tert-butyl ether ug/L ND 0.50 11/19/22 02:33
Methylene Chloride ug/L ND 2.0 11/19/22 02:33
n-Butylbenzene ug/L ND 0.50 11/19/22 02:33
n-Propylbenzene ug/L ND 0.50 11/19/22 02:33
Naphthalene ug/L ND 2.0 11/19/22 02:33
o-Xylene ug/L ND 0.50 11/19/22 02:33
sec-Butylbenzene ug/L ND 0.50 11/19/22 02:33
Styrene ug/L ND 0.50 11/19/22 02:33
tert-Butylbenzene ug/L ND 0.50 11/19/22 02:33
Tetrachloroethene ug/L ND 0.50 11/19/22 02:33
Toluene ug/L ND 0.50 11/19/22 02:33
trans-1,2-Dichloroethene ug/L ND 0.50 11/19/22 02:33
trans-1,3-Dichloropropene ug/L ND 0.50 11/19/22 02:33
Trichloroethene ug/L ND 0.50 11/19/22 02:33
Trichlorofluoromethane ug/L ND 1.0 11/19/22 02:33
Vinyl chloride ug/L ND 1.0 11/19/22 02:33
1,2-Dichloroethane-d4 (S)%101 70-130 11/19/22 02:33
4-Bromofluorobenzene (S)%101 70-130 11/19/22 02:33
Toluene-d8 (S)%106 70-130 11/19/22 02:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3841819LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 63.950 128 60-140
1,1,1-Trichloroethane ug/L 61.850 124 60-140
1,1,2,2-Tetrachloroethane ug/L 62.850 126 60-140
1,1,2-Trichloroethane ug/L 62.250 124 60-140
1,1-Dichloroethane ug/L 57.150 114 60-140
1,1-Dichloroethene ug/L 59.450 119 60-140
1,1-Dichloropropene ug/L 65.950 132 60-140
1,2,3-Trichlorobenzene ug/L 62.250 124 60-140
1,2,3-Trichloropropane ug/L 62.150 124 60-140
1,2,4-Trichlorobenzene ug/L 60.050 120 60-140
1,2,4-Trimethylbenzene ug/L 58.250 116 60-140
1,2-Dibromo-3-chloropropane ug/L 61.550 123 60-140
1,2-Dibromoethane (EDB)ug/L 63.950 128 60-140
1,2-Dichlorobenzene ug/L 60.250 120 60-140
1,2-Dichloroethane ug/L 59.750 119 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3841819LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 58.250 116 60-140
1,3,5-Trimethylbenzene ug/L 59.750 119 60-140
1,3-Dichlorobenzene ug/L 60.850 122 60-140
1,3-Dichloropropane ug/L 60.350 121 60-140
1,4-Dichlorobenzene ug/L 57.750 115 60-140
2,2-Dichloropropane ug/L 58.950 118 60-140
2-Chlorotoluene ug/L 56.450 113 60-140
4-Chlorotoluene ug/L 56.450 113 60-140
Benzene ug/L 55.450 111 60-140
Bromobenzene ug/L 60.350 121 60-140
Bromochloromethane ug/L 64.250 128 60-140
Bromodichloromethane ug/L 62.150 124 60-140
Bromoform ug/L 66.750 133 60-140
Bromomethane ug/L 54.550 109 60-140
Carbon tetrachloride ug/L 59.050 118 60-140
Chlorobenzene ug/L 60.250 120 60-140
Chloroethane ug/L 52.650 105 60-140
Chloroform ug/L 59.350 119 60-140
Chloromethane ug/L 65.750 131 60-140
cis-1,2-Dichloroethene ug/L 59.750 119 60-140
cis-1,3-Dichloropropene ug/L 61.850 124 60-140
Dibromochloromethane ug/L 64.250 128 60-140
Dibromomethane ug/L 62.850 126 60-140
Dichlorodifluoromethane ug/L 69.350 139 60-140
Diisopropyl ether ug/L 59.750 119 60-140
Ethylbenzene ug/L 58.350 117 60-140
Hexachloro-1,3-butadiene ug/L 56.750 113 60-140
Isopropylbenzene (Cumene)ug/L 57.550 115 60-140
m&p-Xylene ug/L 116100 116 60-140
Methyl-tert-butyl ether ug/L 62.950 126 60-140
Methylene Chloride ug/L 57.050 114 60-140
n-Butylbenzene ug/L 58.450 117 60-140
n-Propylbenzene ug/L 58.450 117 60-140
Naphthalene ug/L 64.950 130 60-140
o-Xylene ug/L 60.450 121 60-140
sec-Butylbenzene ug/L 56.650 113 60-140
Styrene ug/L 61.750 123 60-140
tert-Butylbenzene ug/L 49.850 100 60-140
Tetrachloroethene ug/L 59.750 119 60-140
Toluene ug/L 58.750 117 60-140
trans-1,2-Dichloroethene ug/L 59.350 119 60-140
trans-1,3-Dichloropropene ug/L 60.750 121 60-140
Trichloroethene ug/L 62.050 124 60-140
Trichlorofluoromethane ug/L 54.450 109 60-140
Vinyl chloride ug/L 67.650 135 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3841819LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3841820MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636499003
3841821
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 129 60-140132 220ND25.7 26.4
1,1,1-Trichloroethane ug/L 20 120 60-140122 220ND24.0 24.3
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140111 020ND22.2 22.2
1,1,2-Trichloroethane ug/L 20 115 60-140114 020ND23.0 22.9
1,1-Dichloroethane ug/L 20 101 60-140101 120ND20.1 20.3
1,1-Dichloroethene ug/L 20 116 60-140116 020ND23.2 23.1
1,1-Dichloropropene ug/L 20 110 60-140110 120ND22.1 21.9
1,2,3-Trichlorobenzene ug/L 20 132 60-140133 120ND26.4 26.6
1,2,3-Trichloropropane ug/L 20 115 60-140115 020ND23.1 23.0
1,2,4-Trichlorobenzene ug/L 20 134 60-140129 320ND26.7 25.8
1,2,4-Trimethylbenzene ug/L 20 130 60-140129 120ND26.0 25.7
1,2-Dibromo-3-chloropropane ug/L 20 130 60-140130 020ND26.0 25.9
1,2-Dibromoethane (EDB)ug/L 20 123 60-140127 320ND24.6 25.3
1,2-Dichlorobenzene ug/L 20 123 60-140125 120ND24.7 25.0
1,2-Dichloroethane ug/L 20 105 60-140105 020ND21.0 21.0
1,2-Dichloropropane ug/L 20 104 60-140103 020ND20.7 20.7
1,3,5-Trimethylbenzene ug/L 20 132 60-140129 220ND26.4 25.9
1,3-Dichlorobenzene ug/L 20 123 60-140122 120ND24.7 24.4
1,3-Dichloropropane ug/L 20 116 60-140118 220ND23.2 23.6
1,4-Dichlorobenzene ug/L 20 121 60-140120 120ND24.3 24.1
2,2-Dichloropropane ug/L 20 120 60-140118 220ND24.0 23.6
2-Chlorotoluene ug/L 20 123 60-140124 120ND24.5 24.8
4-Chlorotoluene ug/L 20 125 60-140127 220ND24.9 25.3
Benzene ug/L 20 107 60-140106 020ND21.4 21.3
Bromobenzene ug/L 20 124 60-140125 120ND24.8 25.0
Bromochloromethane ug/L 20 108 60-140109 120ND21.6 21.9
Bromodichloromethane ug/L 20 122 60-140117 420ND24.3 23.4
Bromoform ug/L 20 136 60-140132 320ND27.2 26.5
Bromomethane ug/L 20 118 60-140120 120ND23.6 23.9
Carbon tetrachloride ug/L 20 136 60-140135 120ND27.2 26.9
Chlorobenzene ug/L 20 118 60-140120 220ND23.6 24.0
Chloroethane ug/L 20 123 60-140125 220ND24.6 25.1
Chloroform ug/L 20 109 60-140108 120ND21.8 21.6
Chloromethane ug/L 20 102 60-140102 020ND20.4 20.3
cis-1,2-Dichloroethene ug/L 20 103 60-140103 120ND20.5 20.7
cis-1,3-Dichloropropene ug/L 20 116 60-140113 320ND23.2 22.5
Dibromochloromethane ug/L 20 127 60-140127 020ND25.4 25.4
Dibromomethane ug/L 20 114 60-140115 120ND22.8 23.0
Dichlorodifluoromethane ug/L 20 128 60-140130 120ND25.7 26.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3841820MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636499003
3841821
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diisopropyl ether ug/L 20 86 60-14087 120ND17.3 17.4
Ethylbenzene ug/L 20 123 60-140123 020ND24.5 24.6
Hexachloro-1,3-butadiene ug/L M12014460-140146 120ND28.8 29.1
Isopropylbenzene (Cumene)ug/L 20 128 60-140124 420ND25.7 24.8
m&p-Xylene ug/L 40 125 60-140127 240ND49.9 50.7
Methyl-tert-butyl ether ug/L 20 97 60-14096 120ND19.4 19.3
Methylene Chloride ug/L 20 86 60-14087 120ND17.3 17.5
n-Butylbenzene ug/L 20 137 60-140131 420ND27.4 26.3
n-Propylbenzene ug/L 20 127 60-140128 120ND25.4 25.7
Naphthalene ug/L 20 128 60-140127 020ND25.5 25.4
o-Xylene ug/L 20 119 60-140123 320ND23.8 24.6
sec-Butylbenzene ug/L 20 135 60-140133 120ND27.0 26.6
Styrene ug/L 20 124 60-140122 220ND24.8 24.4
tert-Butylbenzene ug/L 20 113 60-140113 020ND22.6 22.6
Tetrachloroethene ug/L 20 126 60-140126 020ND25.2 25.3
Toluene ug/L 20 106 60-140103 220ND21.2 20.7
trans-1,2-Dichloroethene ug/L 20 106 60-140108 120ND21.2 21.5
trans-1,3-Dichloropropene ug/L 20 120 60-140119 120ND24.0 23.8
Trichloroethene ug/L 20 123 60-140121 220ND24.6 24.2
Trichlorofluoromethane ug/L 20 133 60-140135 220ND26.5 27.1
Vinyl chloride ug/L 20 113 60-140112 120ND22.7 22.5
1,2-Dichloroethane-d4 (S)%102 70-130103
4-Bromofluorobenzene (S)%104 70-130104
Toluene-d8 (S)%95 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
738550
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92636499001, 92636499002, 92636499006, 92636499007, 92636499012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3843424
Associated Lab Samples:92636499001, 92636499002, 92636499006, 92636499007, 92636499012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/21/22 14:06
1,1,1-Trichloroethane ug/L ND 0.50 11/21/22 14:06
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/21/22 14:06
1,1,2-Trichloroethane ug/L ND 0.50 11/21/22 14:06
1,1-Dichloroethane ug/L ND 0.50 11/21/22 14:06
1,1-Dichloroethene ug/L ND 0.50 11/21/22 14:06
1,1-Dichloropropene ug/L ND 0.50 11/21/22 14:06
1,2,3-Trichlorobenzene ug/L ND 2.0 11/21/22 14:06
1,2,3-Trichloropropane ug/L ND 0.50 11/21/22 14:06
1,2,4-Trichlorobenzene ug/L ND 2.0 11/21/22 14:06
1,2,4-Trimethylbenzene ug/L ND 0.50 11/21/22 14:06
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/21/22 14:06
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/21/22 14:06
1,2-Dichlorobenzene ug/L ND 0.50 11/21/22 14:06
1,2-Dichloroethane ug/L ND 0.50 11/21/22 14:06
1,2-Dichloropropane ug/L ND 0.50 11/21/22 14:06
1,3,5-Trimethylbenzene ug/L ND 0.50 11/21/22 14:06
1,3-Dichlorobenzene ug/L ND 0.50 11/21/22 14:06
1,3-Dichloropropane ug/L ND 0.50 11/21/22 14:06
1,4-Dichlorobenzene ug/L ND 0.50 11/21/22 14:06
2,2-Dichloropropane ug/L ND 0.50 11/21/22 14:06
2-Chlorotoluene ug/L ND 0.50 11/21/22 14:06
4-Chlorotoluene ug/L ND 0.50 11/21/22 14:06
Benzene ug/L ND 0.50 11/21/22 14:06
Bromobenzene ug/L ND 0.50 11/21/22 14:06
Bromochloromethane ug/L ND 0.50 11/21/22 14:06
Bromodichloromethane ug/L ND 0.50 11/21/22 14:06
Bromoform ug/L ND 0.50 11/21/22 14:06
Bromomethane ug/L ND 5.0 11/21/22 14:06
Carbon tetrachloride ug/L ND 0.50 11/21/22 14:06
Chlorobenzene ug/L ND 0.50 11/21/22 14:06
Chloroethane ug/L ND 1.0 11/21/22 14:06
Chloroform ug/L ND 0.50 11/21/22 14:06
Chloromethane ug/L ND 1.0 11/21/22 14:06
cis-1,2-Dichloroethene ug/L ND 0.50 11/21/22 14:06
cis-1,3-Dichloropropene ug/L ND 0.50 11/21/22 14:06
Dibromochloromethane ug/L ND 0.50 11/21/22 14:06
Dibromomethane ug/L ND 0.50 11/21/22 14:06
Dichlorodifluoromethane ug/L ND 0.50 11/21/22 14:06
Diisopropyl ether ug/L ND 0.50 11/21/22 14:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3843424
Associated Lab Samples:92636499001, 92636499002, 92636499006, 92636499007, 92636499012
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 11/21/22 14:06
Hexachloro-1,3-butadiene ug/L ND 2.0 11/21/22 14:06
Isopropylbenzene (Cumene)ug/L ND 0.50 11/21/22 14:06
m&p-Xylene ug/L ND 1.0 11/21/22 14:06
Methyl-tert-butyl ether ug/L ND 0.50 11/21/22 14:06
Methylene Chloride ug/L ND 2.0 11/21/22 14:06
n-Butylbenzene ug/L ND 0.50 11/21/22 14:06
n-Propylbenzene ug/L ND 0.50 11/21/22 14:06
Naphthalene ug/L ND 2.0 11/21/22 14:06
o-Xylene ug/L ND 0.50 11/21/22 14:06
sec-Butylbenzene ug/L ND 0.50 11/21/22 14:06
Styrene ug/L ND 0.50 11/21/22 14:06
tert-Butylbenzene ug/L ND 0.50 11/21/22 14:06
Tetrachloroethene ug/L ND 0.50 11/21/22 14:06
Toluene ug/L ND 0.50 11/21/22 14:06
trans-1,2-Dichloroethene ug/L ND 0.50 11/21/22 14:06
trans-1,3-Dichloropropene ug/L ND 0.50 11/21/22 14:06
Trichloroethene ug/L ND 0.50 11/21/22 14:06
Trichlorofluoromethane ug/L ND 1.0 11/21/22 14:06
Vinyl chloride ug/L ND 1.0 11/21/22 14:06
1,2-Dichloroethane-d4 (S)%91 70-130 11/21/22 14:06
4-Bromofluorobenzene (S)%103 70-130 11/21/22 14:06
Toluene-d8 (S)%101 70-130 11/21/22 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3843425LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.350 121 60-140
1,1,1-Trichloroethane ug/L 52.250 104 60-140
1,1,2,2-Tetrachloroethane ug/L 48.250 96 60-140
1,1,2-Trichloroethane ug/L 49.850 100 60-140
1,1-Dichloroethane ug/L 40.950 82 60-140
1,1-Dichloroethene ug/L 46.450 93 60-140
1,1-Dichloropropene ug/L 44.750 89 60-140
1,2,3-Trichlorobenzene ug/L 57.350 115 60-140
1,2,3-Trichloropropane ug/L 50.850 102 60-140
1,2,4-Trichlorobenzene ug/L 58.050 116 60-140
1,2,4-Trimethylbenzene ug/L 55.550 111 60-140
1,2-Dibromo-3-chloropropane ug/L 60.050 120 60-140
1,2-Dibromoethane (EDB)ug/L 57.850 116 60-140
1,2-Dichlorobenzene ug/L 53.550 107 60-140
1,2-Dichloroethane ug/L 47.750 95 60-140
1,2-Dichloropropane ug/L 44.850 90 60-140
1,3,5-Trimethylbenzene ug/L 56.750 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3843425LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 53.250 106 60-140
1,3-Dichloropropane ug/L 53.550 107 60-140
1,4-Dichlorobenzene ug/L 51.950 104 60-140
2,2-Dichloropropane ug/L 52.550 105 60-140
2-Chlorotoluene ug/L 52.950 106 60-140
4-Chlorotoluene ug/L 52.950 106 60-140
Benzene ug/L 45.150 90 60-140
Bromobenzene ug/L 54.650 109 60-140
Bromochloromethane ug/L 45.650 91 60-140
Bromodichloromethane ug/L 54.050 108 60-140
Bromoform ug/L 62.150 124 60-140
Bromomethane ug/L 46.250 92 60-140
Carbon tetrachloride ug/L 59.350 119 60-140
Chlorobenzene ug/L 50.850 102 60-140
Chloroethane ug/L 50.350 101 60-140
Chloroform ug/L 45.350 91 60-140
Chloromethane ug/L 38.750 77 60-140
cis-1,2-Dichloroethene ug/L 42.950 86 60-140
cis-1,3-Dichloropropene ug/L 52.850 106 60-140
Dibromochloromethane ug/L 58.650 117 60-140
Dibromomethane ug/L 49.050 98 60-140
Dichlorodifluoromethane ug/L 50.750 101 60-140
Diisopropyl ether ug/L 40.050 80 60-140
Ethylbenzene ug/L 51.450 103 60-140
Hexachloro-1,3-butadiene ug/L 60.450 121 60-140
Isopropylbenzene (Cumene)ug/L 52.650 105 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 42.050 84 60-140
Methylene Chloride ug/L 36.750 73 60-140
n-Butylbenzene ug/L 56.850 114 60-140
n-Propylbenzene ug/L 53.050 106 60-140
Naphthalene ug/L 58.050 116 60-140
o-Xylene ug/L 51.750 103 60-140
sec-Butylbenzene ug/L 55.350 111 60-140
Styrene ug/L 52.950 106 60-140
tert-Butylbenzene ug/L 47.450 95 60-140
Tetrachloroethene ug/L 54.850 110 60-140
Toluene ug/L 42.850 86 60-140
trans-1,2-Dichloroethene ug/L 44.950 90 60-140
trans-1,3-Dichloropropene ug/L 55.350 111 60-140
Trichloroethene ug/L 52.650 105 60-140
Trichlorofluoromethane ug/L 54.650 109 60-140
Vinyl chloride ug/L 44.850 90 60-140
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3843426MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92637042002
3843427
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12013660-140146 720ND27.2 29.2
1,1,1-Trichloroethane ug/L 20 120 60-140133 1020ND24.1 26.7
1,1,2,2-Tetrachloroethane ug/L 20 125 60-140133 720ND24.9 26.6
1,1,2-Trichloroethane ug/L 20 125 60-140139 1020ND25.0 27.7
1,1-Dichloroethane ug/L 20 108 60-140116 720ND21.7 23.2
1,1-Dichloroethene ug/L 20 120 60-140129 720ND24.1 25.9
1,1-Dichloropropene ug/L 20 118 60-140127 720ND23.6 25.4
1,2,3-Trichlorobenzene ug/L M12015160-140159 520ND30.2 31.8
1,2,3-Trichloropropane ug/L 20 128 60-140136 620ND25.6 27.1
1,2,4-Trichlorobenzene ug/L M12015060-140158 620ND29.9 31.7
1,2,4-Trimethylbenzene ug/L M12014060-140148 620ND28.0 29.7
1,2-Dibromo-3-chloropropane ug/L M12014960-140151 220ND29.7 30.3
1,2-Dibromoethane (EDB)ug/L M12014160-140150 620ND28.2 30.1
1,2-Dichlorobenzene ug/L M12013560-140145 720ND27.0 29.0
1,2-Dichloroethane ug/L 20 104 60-140115 1020ND20.8 23.0
1,2-Dichloropropane ug/L 20 117 60-140128 920ND23.3 25.6
1,3,5-Trimethylbenzene ug/L M12014260-140151 620ND28.4 30.1
1,3-Dichlorobenzene ug/L 20 135 60-140140 420ND26.9 28.1
1,3-Dichloropropane ug/L 20 131 60-140139 620ND26.2 27.8
1,4-Dichlorobenzene ug/L 20 132 60-140139 520ND26.5 27.8
2,2-Dichloropropane ug/L 20 126 60-140135 720ND25.2 27.1
2-Chlorotoluene ug/L 20 131 60-140140 720ND26.1 28.0
4-Chlorotoluene ug/L M12013360-140142 620ND26.6 28.3
Benzene ug/L 20 116 60-140128 1020ND23.3 25.6
Bromobenzene ug/L 20 133 60-140139 520ND26.5 27.9
Bromochloromethane ug/L 20 118 60-140130 920ND23.7 26.0
Bromodichloromethane ug/L 20 124 60-140137 1020ND24.8 27.5
Bromoform ug/L M12014260-140148 420ND28.3 29.6
Bromomethane ug/L 20 127 60-140135 620ND25.3 26.9
Carbon tetrachloride ug/L M12013460-140145 820ND26.7 29.0
Chlorobenzene ug/L 20 128 60-140132 420ND25.5 26.5
Chloroethane ug/L 20 134 60-140140 420ND26.8 28.0
Chloroform ug/L 20 116 60-140124 720ND23.2 24.9
Chloromethane ug/L 20 109 60-140112 320ND21.7 22.3
cis-1,2-Dichloroethene ug/L 20 106 60-140115 820ND21.3 23.0
cis-1,3-Dichloropropene ug/L 20 124 60-140137 1020ND24.8 27.3
Dibromochloromethane ug/L M12013560-140142 520ND27.1 28.4
Dibromomethane ug/L 20 123 60-140135 920ND24.6 26.9
Dichlorodifluoromethane ug/L 20 124 60-140131 520ND24.9 26.2
Diisopropyl ether ug/L 20 89 60-14098 920ND17.8 19.6
Ethylbenzene ug/L 20 130 60-140135 420ND26.0 27.0
Hexachloro-1,3-butadiene ug/L M12016360-140178 920ND32.7 35.7
Isopropylbenzene (Cumene)ug/L 20 136 60-140139 220ND27.2 27.7
m&p-Xylene ug/L 40 132 60-140137 440ND52.7 55.0
Methyl-tert-butyl ether ug/L 20 104 60-140115 1020ND20.8 23.0
Methylene Chloride ug/L 20 84 60-14092 920ND16.8 18.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3843426MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92637042002
3843427
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12014960-140156 520ND29.8 31.2
n-Propylbenzene ug/L M12013660-140144 520ND27.3 28.8
Naphthalene ug/L M12014760-140151 320ND29.3 30.2
o-Xylene ug/L 20 129 60-140136 520ND25.8 27.3
sec-Butylbenzene ug/L M12015160-140157 420ND30.2 31.5
Styrene ug/L 20 130 60-140138 620ND26.1 27.6
tert-Butylbenzene ug/L 20 122 60-140127 420ND24.3 25.4
Tetrachloroethene ug/L 20 137 60-140140 220ND27.5 28.1
Toluene ug/L 20 110 60-140120 920ND21.9 23.9
trans-1,2-Dichloroethene ug/L 20 117 60-140124 620ND23.3 24.8
trans-1,3-Dichloropropene ug/L 20 124 60-140138 1020ND24.9 27.6
Trichloroethene ug/L M12012960-140143 1020ND25.8 28.6
Trichlorofluoromethane ug/L 20 128 60-140138 720ND25.7 27.5
Vinyl chloride ug/L 20 124 60-140127 220ND24.8 25.4
1,2-Dichloroethane-d4 (S)%95 70-13097
4-Bromofluorobenzene (S)%102 70-130100
Toluene-d8 (S)%94 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
738836
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92636499014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3845000
Associated Lab Samples:92636499014
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/22/22 12:42
1,1,1-Trichloroethane ug/L ND 0.50 11/22/22 12:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/22/22 12:42
1,1,2-Trichloroethane ug/L ND 0.50 11/22/22 12:42
1,1-Dichloroethane ug/L ND 0.50 11/22/22 12:42
1,1-Dichloroethene ug/L ND 0.50 11/22/22 12:42
1,1-Dichloropropene ug/L ND 0.50 11/22/22 12:42
1,2,3-Trichlorobenzene ug/L ND 2.0 11/22/22 12:42
1,2,3-Trichloropropane ug/L ND 0.50 11/22/22 12:42
1,2,4-Trichlorobenzene ug/L ND 2.0 11/22/22 12:42
1,2,4-Trimethylbenzene ug/L ND 0.50 11/22/22 12:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/22/22 12:42
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/22/22 12:42
1,2-Dichlorobenzene ug/L ND 0.50 11/22/22 12:42
1,2-Dichloroethane ug/L ND 0.50 11/22/22 12:42
1,2-Dichloropropane ug/L ND 0.50 11/22/22 12:42
1,3,5-Trimethylbenzene ug/L ND 0.50 11/22/22 12:42
1,3-Dichlorobenzene ug/L ND 0.50 11/22/22 12:42
1,3-Dichloropropane ug/L ND 0.50 11/22/22 12:42
1,4-Dichlorobenzene ug/L ND 0.50 11/22/22 12:42
2,2-Dichloropropane ug/L ND 0.50 11/22/22 12:42
2-Chlorotoluene ug/L ND 0.50 11/22/22 12:42
4-Chlorotoluene ug/L ND 0.50 11/22/22 12:42
Benzene ug/L ND 0.50 11/22/22 12:42
Bromobenzene ug/L ND 0.50 11/22/22 12:42
Bromochloromethane ug/L ND 0.50 11/22/22 12:42
Bromodichloromethane ug/L ND 0.50 11/22/22 12:42
Bromoform ug/L ND 0.50 11/22/22 12:42
Bromomethane ug/L ND 5.0 11/22/22 12:42
Carbon tetrachloride ug/L ND 0.50 11/22/22 12:42
Chlorobenzene ug/L ND 0.50 11/22/22 12:42
Chloroethane ug/L ND 1.0 11/22/22 12:42
Chloroform ug/L ND 0.50 11/22/22 12:42
Chloromethane ug/L ND 1.0 11/22/22 12:42
cis-1,2-Dichloroethene ug/L ND 0.50 11/22/22 12:42
cis-1,3-Dichloropropene ug/L ND 0.50 11/22/22 12:42
Dibromochloromethane ug/L ND 0.50 11/22/22 12:42
Dibromomethane ug/L ND 0.50 11/22/22 12:42
Dichlorodifluoromethane ug/L ND 0.50 11/22/22 12:42
Diisopropyl ether ug/L ND 0.50 11/22/22 12:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3845000
Associated Lab Samples:92636499014
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 11/22/22 12:42
Hexachloro-1,3-butadiene ug/L ND 2.0 11/22/22 12:42
Isopropylbenzene (Cumene)ug/L ND 0.50 11/22/22 12:42
m&p-Xylene ug/L ND 1.0 11/22/22 12:42
Methyl-tert-butyl ether ug/L ND 0.50 11/22/22 12:42
Methylene Chloride ug/L ND 2.0 11/22/22 12:42
n-Butylbenzene ug/L ND 0.50 11/22/22 12:42
n-Propylbenzene ug/L ND 0.50 11/22/22 12:42
Naphthalene ug/L ND 2.0 11/22/22 12:42
o-Xylene ug/L ND 0.50 11/22/22 12:42
sec-Butylbenzene ug/L ND 0.50 11/22/22 12:42
Styrene ug/L ND 0.50 11/22/22 12:42
tert-Butylbenzene ug/L ND 0.50 11/22/22 12:42
Tetrachloroethene ug/L ND 0.50 11/22/22 12:42
Toluene ug/L ND 0.50 11/22/22 12:42
trans-1,2-Dichloroethene ug/L ND 0.50 11/22/22 12:42
trans-1,3-Dichloropropene ug/L ND 0.50 11/22/22 12:42
Trichloroethene ug/L ND 0.50 11/22/22 12:42
Trichlorofluoromethane ug/L ND 1.0 11/22/22 12:42
Vinyl chloride ug/L ND 1.0 11/22/22 12:42
1,2-Dichloroethane-d4 (S)%100 70-130 11/22/22 12:42
4-Bromofluorobenzene (S)%103 70-130 11/22/22 12:42
Toluene-d8 (S)%103 70-130 11/22/22 12:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3845001LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.850 100 60-140
1,1,1-Trichloroethane ug/L 49.150 98 60-140
1,1,2,2-Tetrachloroethane ug/L 47.750 95 60-140
1,1,2-Trichloroethane ug/L 48.950 98 60-140
1,1-Dichloroethane ug/L 44.650 89 60-140
1,1-Dichloroethene ug/L 48.050 96 60-140
1,1-Dichloropropene ug/L 52.750 105 60-140
1,2,3-Trichlorobenzene ug/L 49.050 98 60-140
1,2,3-Trichloropropane ug/L 41.450 83 60-140
1,2,4-Trichlorobenzene ug/L 49.550 99 60-140
1,2,4-Trimethylbenzene ug/L 47.550 95 60-140
1,2-Dibromo-3-chloropropane ug/L 47.450 95 60-140
1,2-Dibromoethane (EDB)ug/L 49.050 98 60-140
1,2-Dichlorobenzene ug/L 49.350 99 60-140
1,2-Dichloroethane ug/L 44.750 89 60-140
1,2-Dichloropropane ug/L 45.650 91 60-140
1,3,5-Trimethylbenzene ug/L 49.850 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3845001LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 50.750 101 60-140
1,3-Dichloropropane ug/L 46.350 93 60-140
1,4-Dichlorobenzene ug/L 47.750 95 60-140
2,2-Dichloropropane ug/L 49.650 99 60-140
2-Chlorotoluene ug/L 44.650 89 60-140
4-Chlorotoluene ug/L 44.650 89 60-140
Benzene ug/L 46.650 93 60-140
Bromobenzene ug/L 48.950 98 60-140
Bromochloromethane ug/L 50.550 101 60-140
Bromodichloromethane ug/L 48.750 97 60-140
Bromoform ug/L 52.150 104 60-140
Bromomethane ug/L 47.250 94 60-140
Carbon tetrachloride ug/L 48.850 98 60-140
Chlorobenzene ug/L 48.050 96 60-140
Chloroethane ug/L 48.150 96 60-140
Chloroform ug/L 47.450 95 60-140
Chloromethane ug/L 52.550 105 60-140
cis-1,2-Dichloroethene ug/L 46.450 93 60-140
cis-1,3-Dichloropropene ug/L 49.450 99 60-140
Dibromochloromethane ug/L 49.150 98 60-140
Dibromomethane ug/L 49.850 100 60-140
Dichlorodifluoromethane ug/L 57.450 115 60-140
Diisopropyl ether ug/L 44.050 88 60-140
Ethylbenzene ug/L 46.850 94 60-140
Hexachloro-1,3-butadiene ug/L 51.150 102 60-140
Isopropylbenzene (Cumene)ug/L 46.650 93 60-140
m&p-Xylene ug/L 94.4100 94 60-140
Methyl-tert-butyl ether ug/L 47.150 94 60-140
Methylene Chloride ug/L 41.650 83 60-140
n-Butylbenzene ug/L 51.350 103 60-140
n-Propylbenzene ug/L 49.050 98 60-140
Naphthalene ug/L 48.950 98 60-140
o-Xylene ug/L 47.050 94 60-140
sec-Butylbenzene ug/L 48.850 98 60-140
Styrene ug/L 48.750 97 60-140
tert-Butylbenzene ug/L 48.950 98 60-140
Tetrachloroethene ug/L 49.250 98 60-140
Toluene ug/L 47.650 95 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 48.050 96 60-140
Trichloroethene ug/L 51.250 102 60-140
Trichlorofluoromethane ug/L 45.150 90 60-140
Vinyl chloride ug/L 54.550 109 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3845002MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636528006
3845003
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 111 60-140115 42500ND27702870
1,1,1-Trichloroethane ug/L 2500 124 60-140119 42500ND31102980
1,1,2,2-Tetrachloroethane ug/L 2500 109 60-140107 22500ND27202680
1,1,2-Trichloroethane ug/L 2500 115 60-140111 42500ND28902770
1,1-Dichloroethane ug/L 2500 114 60-140110 32500ND28402750
1,1-Dichloroethene ug/L 2500 124 60-140120 42500ND31002990
1,1-Dichloropropene ug/L 2500 132 60-140131 12500ND33103290
1,2,3-Trichlorobenzene ug/L 2500 108 60-14099 92500ND27102470
1,2,3-Trichloropropane ug/L 2500 95 60-14094 12500ND23702360
1,2,4-Trichlorobenzene ug/L 2500 110 60-140104 62500ND27502600
1,2,4-Trimethylbenzene ug/L M1250015860-140136 102500153054904940
1,2-Dibromo-3-chloropropane ug/L 2500 106 60-140103 32500ND26502580
1,2-Dibromoethane (EDB)ug/L 2500 112 60-140115 22500ND28002860
1,2-Dichlorobenzene ug/L 2500 109 60-140108 12500ND27202700
1,2-Dichloroethane ug/L 2500 111 60-140104 62500ND27702600
1,2-Dichloropropane ug/L 2500 113 60-140105 82500ND28302620
1,3,5-Trimethylbenzene ug/L M1250015760-140122 22250045543703510
1,3-Dichlorobenzene ug/L 2500 113 60-140107 52500ND28302680
1,3-Dichloropropane ug/L 2500 109 60-140106 32500ND27202640
1,4-Dichlorobenzene ug/L 2500 111 60-140107 32500ND27602670
2,2-Dichloropropane ug/L 2500 122 60-140114 72500ND30602840
2-Chlorotoluene ug/L M1,R1250014260-14087 482500ND35502180
4-Chlorotoluene ug/L M1,R1250014260-14087 482500ND35502180
Benzene ug/L 2500 114 60-140112 2250024530903040
Bromobenzene ug/L M1250014460-140107 302500ND36102680
Bromochloromethane ug/L 2500 120 60-140121 12500ND29903020
Bromodichloromethane ug/L 2500 123 60-140113 92500ND30702810
Bromoform ug/L 2500 113 60-140113 02500ND28202820
Bromomethane ug/L 2500 89 60-140106 172500ND22302650
Carbon tetrachloride ug/L 2500 132 60-140118 112500ND32902960
Chlorobenzene ug/L 2500 113 60-140109 42500ND28402740
Chloroethane ug/L M1250014360-140138 32500ND35703450
Chloroform ug/L 2500 117 60-140115 22500ND29402870
Chloromethane ug/L 2500 125 60-140124 12500ND31303090
cis-1,2-Dichloroethene ug/L 2500 116 60-140114 22500ND29102840
cis-1,3-Dichloropropene ug/L 2500 118 60-140112 62500ND29502790
Dibromochloromethane ug/L 2500 111 60-140110 12500ND27702760
Dibromomethane ug/L 2500 119 60-140109 92500ND29902720
Dichlorodifluoromethane ug/L 2500 139 60-140129 72500ND34603230
Diisopropyl ether ug/L 2500 100 60-140105 52500ND25002620
Ethylbenzene ug/L M1250011860-140166 192500280057606950
Hexachloro-1,3-butadiene ug/L 2500 122 60-140107 132500ND30502680
Isopropylbenzene (Cumene)ug/L 2500 114 60-140113 0250086.2 2920 2920
m&p-Xylene ug/L M1500011660-140205 25500098501570020100
Methyl-tert-butyl ether ug/L 2500 112 60-140111 02500ND27902780
Methylene Chloride ug/L 2500 98 60-14092 62500ND24502300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3845002MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636528006
3845003
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 2500 112 60-140111 12500ND28002760
n-Propylbenzene ug/L M1250014960-140114 25250019239203040
Naphthalene ug/L 2500 107 60-140112 4250056832303380
o-Xylene ug/L M1250011560-140211 2625005130800010400
sec-Butylbenzene ug/L 2500 124 60-140110 112500ND30902760
Styrene ug/L 2500 115 60-140114 1250064.4 2940 2920
tert-Butylbenzene ug/L 2500 128 60-14097 272500ND32002430
Tetrachloroethene ug/L 2500 116 60-140113 32500ND28902820
Toluene ug/L M1250013360-140316 262500121001540019900
trans-1,2-Dichloroethene ug/L 2500 121 60-140118 32500ND30302940
trans-1,3-Dichloropropene ug/L 2500 117 60-140108 82500ND29202700
Trichloroethene ug/L 2500 124 60-140116 72500ND30902900
Trichlorofluoromethane ug/L 2500 130 60-140126 32500ND32403160
Vinyl chloride ug/L 2500 138 60-140133 32500ND34403330
1,2-Dichloroethane-d4 (S)%99 70-130103
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%103 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 56
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 56
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92636499
TERRELL BAIT SHOP
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92636499001 738550MW 1 SM 6200B
92636499002 738550MW 2 SM 6200B
92636499003 738197MW 3 SM 6200B
92636499004 738197MW 4 SM 6200B
92636499005 738197MW 5 SM 6200B
92636499006 738550MW 6 SM 6200B
92636499007 738550MW 7 SM 6200B
92636499008 738197MW 8 SM 6200B
92636499009 738197MW 9 SM 6200B
92636499010 738197MW 10 SM 6200B
92636499011 738197MW 11 SM 6200B
92636499012 738550MW 12 SM 6200B
92636499013 738197MW 15 SM 6200B
92636499014 738836MW 16 SM 6200B
92636499015 738197VMW 1 SM 6200B
92636499016 738197VMW 2 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/26/2022 09:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 56
Page 53 of 56
Page 54 of 56
Page 55 of 56
Page 56 of 56

Appendix B

Figures

LEGEND
Site
1
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Figures.mxd plotted by kelsey.cahill 07-19-2022REFERENCE:ESRI WORLD STREET BASEMAP
SITE LOCATION MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
500 0 500 1,000250
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!
LEGEND
Site
2
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Figures.mxd plotted by kelsey.cahill 07-19-2022REFERENCE:NGMDB.USGS.GOV/TOPOVIEWLAKE NORMAN NORTH, NC QUADRANGLE - 2019
USGS TOPOGRAPHIC MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
500 0 500 1,000250
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!
@A
@A
@A
@A@A
@A@A@A@A@A @A
@A
@A
@A
@A @A@A@A@A@A@A@A@A@A@A@AAS-2
AS-1MW-3
TS-8
MW-1
MW-2
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9
SVE-2
SVE-1
DMW-1
MW-17
MW-16
MW-18
TS-11
MW-10
MW-11
MW-12
MW-13
MW-14
MW-15
LEGEND
@A Air Sparge Well
@A Groundwater Monitoring Well
@A Soil Vapor Extraction Well
Approximate Former UST LocationsSite
3
FIGUREDrawing Path: X:\GIS\Asheville Projects\Terrell Bait Shop\Aerial.mxd plotted by kelsey.cahill 07-19-2022REFERENCE:NCONEMAP.GOV - 2018 AERIAL PHOTOGRAPHNOTES:BUILDING IS NO LONGER PRESENT ON-SITE
SITE MAPTERRELL BAIT SHOP7970 NC 150, TERRELLCATAWBA COUNTY, NORTH CAROLINA
30 0 30 6015
APPROXIMATE SCALE IN FEET
DATE:
JOB NO:CHECKED:
DRAWN:
APPROVED:DRLKLC
DRL J22-17256-017-19-22
!

Appendix C

Tables
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
Manifold
Pressure
(psi)
Well Head
Pressure
(psi)
Flow
(SCFM)
3/11/2022 10834.16 Off NA 188.0 Off NA 50 33 4.0 49 41 5.0 42 32 4.0 System re-start
3/15/2022 10930.36 On 100%271.0 Off 86%47 33 5.0 40 -5.0 42 -5.0 Air compressor off due to high temperature because of low oil.
4/1/2022 11337.26 On 100%343.0 Off 18%---------Air compressor off due to high temperature because of low oil. Air
compressor was left off until problem can be diagnosed.
4/26/2022 11934.56 On 100%343.0 Off 0%50 39 7.0 50 34 7.0 50 32 7.0 Air sparge has been off since prior visit.
4/28/2022 11983.17 On 101%390.0 On 98%50 39 7.0 50 34 7.0 50 32 7.0 No oil in condenstate. Oil carry over potentially solved.
5/9/2022 12248.33 On 100%431.0 Off 16%52 40 5.0 52 42 5.0 53 36 4.0 Air compressor off due to high temperature because of low oil.
Appears to be a scavenging issue.
5/17/2022 12439.32 On 99%492.0 Off 32%48 -3.0 50 -3.0 50 -3.0 Air compressor off due to high temperature because of low oil.
5/24/2022 12607.39 On 100%529.0 Off 22%---------Air compressor off due to high temperature because of low oil. Took
oil sample.
6/2/2022 12823.24 On 100%530.0 Off 0%24 -6.0 52 -6.0 52 -6.0 Removed scavenge orifice and discovered that orfice is clogged.
Cleaned and air compressor is scavenging oil properly.
7/14/2022 13816.24 On 99%1,322.0 On 79%48 -7.0 52 -7.0 56 -7.0 Sparge Compressor was off on 7-12-22 due to "Power Lose" at 1276
hours.
7/28/2022 14150.54 On 99%1,657.0 On 100%48 -8.0 54 -7.0 56 -7.0 Air compressor condensate drain is working.
8/12/2022 14512.17 On 100%1,973.0 Off 88%51 34 6.0 54 35 5.0 56 34 5.5 Electrical service rack in dire need of repairs. Stressing underground
and above ground conduit.
8/26/2022 14848.32 On 100%2,309.0 On 100%48 34 7.5 52 35 7.0 54 34 7.0 Electrical service rack still in dire need of repairs. Unable to make a
setting change in controller for auto restart after power loss.
9/12/2022 15255.57 On 100%2,716.0 On 100%47 34 7.0 53 35 7.0 54 34 7.0 Electrical service rack still in dire need of repairs. SVE moisture
separator shows water slightly above low level float.
9/30/2022 "Recheck"On 15,688 100%3,071.0 Off 82%56 -6.0 56 -5.5 58 -5.5 Issue with hour reading, readings recorded at visit are less than
readings at last visit.
10/18/2022 14906.34 On 16,120 100%3,505.0 On 100%50 32 7.0 56 35 7.5 57 38 7.5 Air sample was collected. 1 Tedlar bag sample - (SVE-1 @ 1435) and
delivered to PACE.
10/26/2022 14468.23 Off 16,168 25%3,524.0 Off 10%53 33 7.0 56 32 6.0 56 24 7.0 Both SVE blower system offline and Air Sparge System offline due to
electrical repairs on 10/20. System restart.
11/17/2022 15019.19 Off 16,672 95%4,048.0 Off 99%56 -8.0 56 -8.0 63 -8.0 Power loss reported on 11/16. 524 hours runtime reported for AS.
SVE inline filter element needs replacing.
12/2/2022 15133.25 Off 16,786 32%4,235.0 Off 52%56 -5.0 57 -5.0 62 -5.0 Drain check valve for moisture separator tank stuck closed. Opened
check valve and tank was drained.
12/15/2022 15144.27 On 17,098 100%4,521.0 Off 92%60 -6.0 58 -6.0 64 -6.0 Condensate tank drain working. No water in moisture separator drum.
12/28/2022 14468.01 Off 17,312 69%4,735.0 Off 69%60 46 6.0 54 31 7.0 61 26 6.0 Still no water in moisture separator drum. Motor contractor tripped, air
sparge solenoid closedTotal52%65%
Notes:
psi = pounds per square inch
SCFM = standard cubic feet per minute
- = no data
* Adjusted runtime was prepared as a result of the PLC timer reporting incorrect values
Date
SVE %
Run Since
Previous
Visit
Air Sparge %
Run Since
Previous Visit
Sparge Well AS-1
SVE
On/Off
SVE Run
Time
(hours)
Adjusted
SVE
Timer
(hours)*
Sparge Well AS-2 Sparge Well AS-3Air
Compressor
Run Time
(hours)
Air Sparge
On/Off Comments
TABLE 1
System Operational Data
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01
1 of 1
STACK DATA
Sample ID Date
Collected
SVE Effluent 7/14/22 13,100 85,900 15,200 43,300 <288 1,440,000
SVE Effluent 10/18/22 8,850 78,700 15,500 62,500 <72.1 1,110,000
AVERAGE 10,975.0 82,300.0 15,350.0 52,900.0 180.1 1,275,000
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Temp Rel Humid Water Qstd
(in-Hg)(ft/min)(in)(°F)(°K)(%/100)Vapor (%)(DSCFM)
7/14/22 3.0 3,328 2 104.2 313 0.271 0.0126 67.1
10/18/22 3.0 3,564 2 162.0 345 0.394 0.0958 59.7
AVERAGE 63.4
MASS REMOVAL RATE AND TOTAL MASS REMOVED
Start Date 06/02/22 12,823 hours
End Date 12/28/22 17,312 hours
% Run 89%
Total Run Time (hrs)4,488
Analyte
BenzeneTolueneEthylbenzeneTotal XylenesMTBETPH-GROMass Removal Rate (kg/hr)1.18E-03 8.86E-03 1.65E-03 5.70E-03 1.94E-05 1.37E-01
Total Mass Removed (kg)5.30E+00 3.98E+01 7.42E+00 2.56E+01 8.70E-02 6.16E+02
Total Mass Removed (lbs)11.69 87.69 16.36 56.36 0.19 1,358.48
NOTES:
µg/m3 = Micrograms per cubic meter
Qstd = Flow at dry standard cubic feet per minute (DSCFM)
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)MTBETPH-GRODate
TABLE 2
Analytical Method
Contaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMass Removal Via Vapor
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01
EPA Method 18 Target Compounds
(mg/m3)
Date
1.0 - 5,000 5,000 - 10,000 10,000 1.0 - 5,000 5,000 - 10,000 10,000
3,774 2,013 1,121 94,350 50,325 28,025
1.0 - 5,000 5,000 - 10,000 10,000 1.0 - 10 10 - 100 100 - 1,000
4,154 356 342 103,850 8,900 8,550
1.0 - 1,000 1,000 1.0 - 1,000 1,000
2,587 240 64,675 6,000
Date Total Mass
(kg)
Total Mass
(lbs)
2,500 7,500 10,000
2.00 3.21 2.38
2,500 7,500 10,000
2.21 0.57 0.73
500 1,000
0.27 0.05
Notes:
* Saturated Thickness of Dissolved Benzene is assumed to be 25 feet
November 2022 0.33 0.72
Surface Area between Contours (ft2)Area (ft2) x Depth of Contamination* (ft) = Volume (ft3)
Between Contours
December 2021
June 2022
Volume (ft3) Between Contours x Average
Contamination Concentration (mg/L) x 30%
Porosity
November 2022
December 2021 7.59 16.73
June 2022 3.50 7.71
TABLE 3
Contaminant Mass Estimate as Benzene
7970 NC Highway 150
Terrell, Catawba County, North Carolina
BLE Project No. J22-17256-01

Appendix D

Laboratory Analytical Report

#=CL#
July 19, 2022
LIMS USE: FR - DAVID LOFTIS, PE
LIMS OBJECT ID: 92614894
92614894
Project:
Pace Project No.:
RE:
David R. Loftis, PE
Bunnell Lammons Engineering
130 Oval Road
Suite 200
Arden, NC 28704
Loftis
Dear David Loftis, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on July 14, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 8
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92614894
Loftis
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 8
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92614894
Loftis
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92614894001 SVE-1 Method 18 Air MeOH & EtOH 8 PANFKG
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 8
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92614894
Loftis
Sample:SVE-1 Lab ID:92614894001 Collected:07/14/22 13:30 Received:07/14/22 15:00 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 13100 ug/m3 07/16/22 22:35 71-43-207/16/22 22:35256400
Toluene 85900 ug/m3 07/16/22 22:35 108-88-307/16/22 22:35753400
Ethylbenzene 15200 ug/m3 07/16/22 22:35 100-41-407/16/22 22:35347400
m&p-Xylene 43300 ug/m3 07/16/22 22:35 179601-23-107/16/22 22:35694400
o-Xylene 19200 ug/m3 07/16/22 22:35 95-47-607/16/22 22:35347400
Methyl-tert-butyl ether ND ug/m3 07/16/22 22:35 1634-04-407/16/22 22:35288400
Gasoline Range Organics 1440000 ug/m3 07/16/22 22:35 8006-61-907/16/22 22:35330000400
Surrogates
1,4-Dichlorobenzene-d4 (IS)90.6 %07/16/22 22:35 3855-82-107/16/22 22:3560.0-140 400
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 8
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92614894
Loftis
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1896191
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92614894001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3815759-3
Associated Lab Samples:92614894001
Matrix:Air
Analyzed
Benzene ppbv ND 0.200 07/16/22 06:59
Toluene ppbv ND 0.500 07/16/22 06:59
Ethylbenzene ppbv ND 0.200 07/16/22 06:59
m&p-Xylene ppbv ND 0.400 07/16/22 06:59
o-Xylene ppbv ND 0.200 07/16/22 06:59
Methyl-tert-butyl ether ppbv ND 0.200 07/16/22 06:59
Gasoline Range Organics ppbv ND 200 07/16/22 06:59
1,4-Dichlorobenzene-d4 (IS)%85.4 60.0-140 07/16/22 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3815759-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3815759-2
Benzene ppbv 3.893.75 104 70.0-1301043.91 0.513 25
Toluene ppbv 3.983.75 106 70.0-1301063.99 0.251 25
Ethylbenzene ppbv 4.173.75 111 70.0-1301114.16 0.240 25
m&p-Xylene ppbv 8.347.50 111 70.0-1301118.34 0.00 25
o-Xylene ppbv 4.073.75 109 70.0-1301094.07 0.00 25
Methyl-tert-butyl ether ppbv 3.903.75 104 70.0-1301043.90 0.00 25
Gasoline Range Organics ppbv 213203 105 70.0-130104212 0.471 25
1,4-Dichlorobenzene-d4 (IS)%90.5 60.0-14090.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
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Huntersville, NC 28078
[phone]
Page 5 of 8
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92614894
Loftis
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 6 of 8
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92614894
Loftis
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92614894001 1896191 1896191SVE-1 M18-Mod Method 18 Air MeOH &EtOH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 8
Page 8 of 8
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92614894
Loftis
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1896191
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92614894001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3815759-3
Associated Lab Samples:92614894001
Matrix:Air
Analyzed
Benzene ppbv ND 0.200 07/16/22 06:59
Toluene ppbv ND 0.500 07/16/22 06:59
Ethylbenzene ppbv ND 0.200 07/16/22 06:59
m&p-Xylene ppbv ND 0.400 07/16/22 06:59
o-Xylene ppbv ND 0.200 07/16/22 06:59
Methyl-tert-butyl ether ppbv ND 0.200 07/16/22 06:59
Gasoline Range Organics ppbv ND 200 07/16/22 06:59
1,4-Dichlorobenzene-d4 (IS)%85.4 60.0-140 07/16/22 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3815759-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3815759-2
Benzene ppbv 3.893.75 104 70.0-1301043.91 0.513 25
Toluene ppbv 3.983.75 106 70.0-1301063.99 0.251 25
Ethylbenzene ppbv 4.173.75 111 70.0-1301114.16 0.240 25
m&p-Xylene ppbv 8.347.50 111 70.0-1301118.34 0.00 25
o-Xylene ppbv 4.073.75 109 70.0-1301094.07 0.00 25
Methyl-tert-butyl ether ppbv 3.903.75 104 70.0-1301043.90 0.00 25
Gasoline Range Organics ppbv 213203 105 70.0-130104212 0.471 25
1,4-Dichlorobenzene-d4 (IS)%90.5 60.0-14090.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 8
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92614894
Loftis
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 8
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92614894
Loftis
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92614894001 1896191 1896191SVE-1 M18-Mod Method 18 Air MeOH &EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2022 11:00 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 8
Page 8 of 8
#=CL#
October 24, 2022
LIMS USE: FR - DAVID LOFTIS, PE
LIMS OBJECT ID: 92631749
92631749
Project:
Pace Project No.:
RE:
David R. Loftis, PE
Bunnell Lammons Engineering
130 Oval Road
Suite 200
Arden, NC 28704
TERRELL BAIT SHOP 17526-01
Dear David Loftis, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on October 18, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 9
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 9
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92631749001 SVE-1 Method 18 Air MeOH & EtOH 8 PANDAH, SDS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 9
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Sample:SVE-1 Lab ID:92631749001 Collected:10/18/22 14:35 Received:10/18/22 16:11 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 8850 ug/m3 10/21/22 02:13 71-43-210/21/22 02:1363.9 100
Toluene 78700 ug/m3 10/21/22 11:45 108-88-310/21/22 11:4518801000
Ethylbenzene 15500 ug/m3 10/21/22 02:13 100-41-410/21/22 02:1386.7 100
m&p-Xylene 46000 ug/m3 10/21/22 02:13 179601-23-110/21/22 02:13173100
o-Xylene 19400 ug/m3 10/21/22 02:13 95-47-610/21/22 02:1386.7 100
Methyl-tert-butyl ether ND ug/m3 10/21/22 02:13 1634-04-410/21/22 02:1372.1 100
Gasoline Range Organics 1100000 ug/m3 10/21/22 02:13 8006-61-910/21/22 02:1382600100
Surrogates
1,4-Dichlorobenzene-d4 (IS)102 %10/21/22 02:13 3855-82-110/21/22 02:1360.0-140 100
1,4-Dichlorobenzene-d4 (IS)87.8 %10/21/22 11:45 3855-82-110/21/22 11:4560.0-140 1000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/24/2022 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 9
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1946145
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92631749001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3851036-3
Associated Lab Samples:92631749001
Matrix:Air
Analyzed
Benzene ug/m3 ND 0.639 10/20/22 10:44
Ethylbenzene ug/m3 ND 0.867 10/20/22 10:44
m&p-Xylene ug/m3 ND 1.73 10/20/22 10:44
o-Xylene ug/m3 ND 0.867 10/20/22 10:44
Methyl-tert-butyl ether ug/m3 ND 0.721 10/20/22 10:44
Gasoline Range Organics ug/m3 ND 826 10/20/22 10:44
1,4-Dichlorobenzene-d4 (IS)%96.7 60.0-140 10/20/22 10:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3851036-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3851036-2
Benzene ug/m3 12.712.0 106 70.0-13010612.6 0.755 25
Ethylbenzene ug/m3 17.616.3 108 70.0-13010617.3 1.99 25
m&p-Xylene ug/m3 33.532.5 103 70.0-13010433.8 0.773 25
o-Xylene ug/m3 17.016.3 105 70.0-13010617.2 0.760 25
Methyl-tert-butyl ether ug/m3 14.313.5 106 70.0-13010714.5 1.25 25
Gasoline Range Organics ug/m3 967839 115 70.0-130116975 0.851 25
1,4-Dichlorobenzene-d4 (IS)%99.8 60.0-140100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/24/2022 03:00 PM
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Huntersville, NC 28078
[phone]
Page 5 of 9
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1946727
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92631749001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3851578-3
Associated Lab Samples:92631749001
Matrix:Air
Analyzed
Toluene ug/m3 ND 1.88 10/21/22 10:20
1,4-Dichlorobenzene-d4 (IS)%88.5 60.0-140 10/21/22 10:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3851578-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3851578-2
Toluene ug/m3 16.614.1 118 70.0-13011816.6 0.00 25
1,4-Dichlorobenzene-d4 (IS)%93.0 60.0-14092.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/24/2022 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 9
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/24/2022 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 9
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92631749
TERRELL BAIT SHOP 17526-01
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92631749001 1946145 1946145SVE-1 M18-Mod Method 18 Air MeOH &EtOH
92631749001 1946727 1946727SVE-1 M18-Mod Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/24/2022 03:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 9
Page 9 of 9