MO-7402_36069_CA_CAPR_20221229

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

December 30, 2022

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Corrective Action Performance Report
September-November 2022
Handy Stop #7
1500 Rock Barn Road
Conover, Catawba County
North Carolina
Facility ID Number: 0-00-0000031674
Incident Number: 36069
GRI Project Number: 3067

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc. Ms. Gail Williams; Shell Brothers Distributors, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Corrective Action Performance Report
September – November 2022
Handy Stop #7
1500 Rock Barn Road
Conover, Catawba County
North Carolina
Facility ID Number: 0-00-0000031674
Incident Number: 36069
GRI Project Number: 3067

Prepared for:

Shell Brothers Distributors, Inc.
Ms. Gail Shell Williams
1-C Fountain Manor Drive
Greensboro, North Carolina 27405

December 29, 2022

Joanna Alley, P.E.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
i
EXECUTIVE SUMMARY
Handy Stop #7 is located at 1500 Rock Barn Road in Conover, Catawba County, North Carolina. The site is
currently owned and operated by C.C Royal Enterprises, LLC as a petroleum retail facility and convenience
store. According to the North Carolina Registered Tank database, three 10,000-gallon gasoline USTs, one
5,200-gallon diesel UST and one 5,200-gallon kerosene UST are in use at the site. According to historical
information from the previous consultants, a release was discovered in March 2006 during a Phase II ESA.
The site and surrounding area are primarily commercial and residential. According to the 2013 update to
the receptor survey, a total of fourteen water supply wells were identified within 1,500 feet of the subject
site. There are five non-potable water supply wells located within 1,000 feet of the site. Please note that
on July 22, 2021, the property of water supply well WSW-3 was connected to municipal water. Public
water is available to the site and surrounding properties within 1,500 feet of the site.

In accordance with the 2009 CAP and 2016 system redesign, an AS and SVE system was installed at the
site and activated on February 20, 2018. The system installation included the installation and connection
of a total of five AS wells and six SVE wells throughout the contaminant plume. No projected milestones
were established in the CAP.

O&M site visits were conducted on October 13 and October 24, 2022. Please note that the remediation
system was off upon arrival during the November 14, 2022 sampling event and was unable to be restarted.
Hour meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum
readings were collected during each site visit. Additionally, SVE effluent air samples were collected during
both October 2022 site visits and submitted for laboratory analysis.

On November 14, 2022, ten monitoring wells, two observation wells and three telescoping wells were
gauged, purged, and/or sampled. Please note that OW-1 had a limited volume and could not be sampled.
A car was parked over DW-2, so a ground water sample was not collected. No free product was observed
in any of the wells. The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene,
TAA, TAME, TBA, isopropylbenzene, IPE, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1R, MW-3, MW-4, DW-1,
DW-3, and OW-2 exceeded the MACs. All contaminant concentrations were below the GCLs.

The concentrations reported from the May 2017 sampling event were used as a baseline for contaminant
mass calculations. Based on the May 2017 sampling event, the contaminant plume was divided into four
areas based on the proximity to impacted monitoring wells to determine the baseline contaminant mass
at the site. Calculations based on the November 14, 2022 ground water sampling event indicate that the
contaminant mass has decreased by 76.1%, 65.9%, 87.7% and 96.7% in Areas 1 through 4, respectively,
when compared to the baseline sampling event. The contaminant concentrations in Areas 1 through Area
4 have generally decreased over time; however, Area 2 has intermittently contained free product. The
overall contaminant mass at the site has decreased by approximately 73.6% from the May 2017 sampling
event to the November 2022 sampling event.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
ii
Based on this information, the risk classification for the site should remain intermediate risk. GRI
recommends that a feasibility study should be conducted to address the contamination in telescoping
well DW-2. GRI is gathering information about potential injection technologies to address the
contamination in DW-2; however, some of the options are still in the process of getting approved as an
approved innovative technology. Semi-annual ground water monitoring should continue for telescoping
well DW-2 and observation well OW-2; annual ground water monitoring should be conducted on wells
MW-1R, MW-3, MW-4, OW-1, OW-2, and DW-1 through DW-3 to monitor for potential rebound of
contaminant concentrations. Based on the November 2022 sampling event, contaminant concentrations
in all shallow monitoring wells were below GCLs; therefore, the remediation system should remain off for
the first quarter of 2023. The next semi-annual ground water sampling event is scheduled tentatively for
May 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
iii
SITE INFORMATION
1. Site Identification
 Handy Stop #7 (Facility ID 0-00-0000031674)
 Incident Number 36069 – Intermediate Risk (I210A)
 Location of Source Area: 1500 Rock Barn Road
Conover, NC 28314
Catawba County
35.7222431°N, 81.1843913°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Royal Enterprises, Inc.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
704-633-2434

UST/AST Operator
Royal Enterprises, Inc.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
704-633-2434

Property Owner
C.C. Royal Enterprises, LLC.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
Phone No. Unknown

Property Occupant
C.C. Royal Enterprises, LLC.
322 East Fisher Street, Suite 101
Salisbury, NC 28144-5059
[e-mail]
Phone No. Unknown

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered on March 14, 2006
 An unknown amount of product was released from the leaking UST System
 Three 10,000-gallon gasoline, one 5,200-gallon diesel and one 5,200-gallon kerosene USTs and
associated pumps and product piping are active at the site

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
3.0 FREE PRODUCT REMOVAL ........................................................................................................5
4.0 REMEDIATION SYSTEM ............................................................................................................5
5.0 AIR SAMPLING.........................................................................................................................5
6.0 SOIL AND GROUND WATER REMEDIATION ...............................................................................6
7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................8
8.0 CONCLUSIONS .........................................................................................................................8
9.0 LIMITATIONS ...........................................................................................................................9
10.0 STATEMENTS AND CERTIFICATION ...........................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Remediation Well Location Map
Figure 7: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Summary of Remediation System O&M Visits
Table 8: Summary of Air Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Reports
Appendix F: O&M Field Data Sheets
Appendix G: Overall Remediation Costs
Appendix H: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of ongoing O&M and ground water sampling activities conducted between
September and November 2022 at the Handy Stop #7 site, located at 1500 Rock Barn Road in Conover,
Catawba County, North Carolina (Figure 1). These activities were conducted in accordance with GRI
Proposal No. 22-639, which was submitted to the NCDEQ on September 27, 2022, and was approved as
Task Authorization No. 36069-60 on September 30, 2022. State correspondence is included as Appendix
A.

The site is currently owned and operated by C.C. Royal, Enterprises, LLC as a petroleum retail facility and
convenience store. According to historical information from the previous consultants, a release was
discovered in March 2006 during a Phase II ESA. Currently, three 10,000-gallon gasoline, one 5,200-gallon
diesel and one 5,200-gallon kerosene USTs are active at the site. UST owner/operator information and
UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown
below:

The site and surrounding area consist of primarily commercial and residential properties. A copy of the
Land Use table is included as Appendix B. The site contains three buildings (the store, car wash and
remediation system building) and is primarily capped with concrete and asphalt. The overall topography
at the site is relatively flat with a fairly steep elevation drop to the northeast and east of the site. Ten
Type II monitoring wells (MW-1 through MW-10), three Type III monitoring wells (DW-1 through DW-3),
two observation wells (OW-1 and OW-2), five air sparging wells (AS-1 through AS-5) and six vapor
extraction wells (SVE-1 through SVE-6) were installed at the site during previous ground water assessment
activities. Monitoring wells (MW-1R and MW-2) are 4” recovery wells. Monitoring well MW-3’s well pad
and well casing were previously damaged at grade level and were repaired during the February 2019 site
visit. During repair of the well, the well casing was shortened and the top-of-casing elevation needs to be

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
2
re-measured. A Site Map showing the locations of the monitoring wells and the structures on-site has
been included as Figure 2.

An update to the receptor survey was conducted in January 2013. A total of fourteen water supply wells
were identified within 1,500 feet of the subject site. There are five non-potable water supply wells located
within 1,000 feet of the site. Please note that on July 22, 2021, the property containing WSW-3 was
connected to municipal water; therefore, WSW-3 is no longer potable. Public water is available to the
site and surrounding properties within 1,500 feet of the site. No surface water bodies were identified
within a 500-foot radius of the site with the closest surface water body being an unnamed tributary of
Mull Creek, located approximately 800 feet southeast of the site. Receptor information is provided in
Table 3. Adjacent property owner information is presented in Table 4. A Site Vicinity Map showing the
adjacent properties and a Zoning Map showing the zoning information are included as Figures 3A and 3B,
respectively.

Please note that the historical information contained in this report was obtained under the supervision of
the previous consultants. Although GRI cannot verify the accuracy of the information obtained by
previous consultants, for the purpose of this report it is assumed to be correct and any inferences or
interpretations made by GRI based on data that may be incorrect are not the responsibility of GRI. Please
refer to earlier submittals for additional information regarding previous assessment activities.

Two AST incidents (Incident Nos. 91567 and 95863) have been reported on the highway adjacent to the
site. Copies of the NCDEQ Incident Reports are included as Appendix C. A map showing the locations of
additional incidents in the vicinity of the site is shown below:

36069
95863
91567
8396
14413 14351

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
3

In accordance with the 2009 CAP and 2016 system redesign, SVE and AS systems were installed at the site
and activated on February 20, 2018. The system installation included the installation and connection of a
total of five AS wells and six SVE wells throughout the contaminant plume. Due to the presence of free
product in OW-2 during previous ground water sampling activities in August 2018, air flow was shut off to
AS-4. Because free product has not been detected in OW-2 since January 2020, air flow to AS-4 was re-
established on May 19, 2021. The remediation system was shut down and winterized during the January
2022 site visit. To date, six MMPE events have been conducted at the site. A total of approximately
18,052.30 gallons of contaminated ground water and free product have been removed from the site.
Please note that no projected milestones were established in the CAP.

Based on this information, the site risk classification should remain intermediate.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
from previous consultants is included as Appendix D.

On November 14, 2022, ten Type II monitoring wells (MW-1R and MW-2 through MW-10), two
observation wells (OW-1 and OW-2), and three telescoping wells (DW-1 through DW-3) were gauged,
purged, and/or sampled in accordance with the NCDEQ guidelines. No free product was observed in any
of the wells. OW-1 did not produce sufficient volume of ground water for a sample to be collected, and a
car was parked over DW-2, so a ground water sample was not collected. Please note that attempts to
locate the owner of the car were unsuccessful. Depths to ground water in the Type II monitoring wells
ranged from 31.72 feet to 49.87 feet below TOC. Ground water elevations in the Type II monitoring wells
ranged from 51.87 feet to 68.76 feet based on an assumed elevation of 100.00 feet assigned to MW-5.
Ground water flow converged towards a hydraulic low located at the front of the store, with a horizontal
gradient of approximately 0.20 feet per foot. The vertical gradient between paired wells DW-2 and MW-
3 could not be calculated because the top-of-casing elevation for MW-3 needs to be re-measured. Well
construction and gauging information is presented in Table 5. A Water Table Surface Map based on the
Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is
shown below:
Well ID
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
MW-1R 30 - 45 45 101.58 36.08 --- 65.50
MW-2 30 - 45 45 NM 32.73 --- NM
MW-3 30 - 45 45 NM 44.25 --- NM
MW-4 30 - 45 45 101.72 35.06 --- 66.66
MW-5 30 - 50 50 100.00 31.72 --- 68.28
MW-6 30 - 50 50 100.96 32.20 --- 68.76
MW-7 30 - 50 50 101.45 49.43 --- 52.02
MW-8 30 - 50 50 101.74 49.87 --- 51.87
MW-9 35 - 50 50 98.62 36.46 --- 62.16

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
4
Well ID
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
MW-10 35 - 50 50 98.82 35.36 --- 63.46
DW-1 60 - 65 65 NM 37.73 --- NM
DW-2 85 - 90 90 100.06 37.84 --- 62.22
DW-3 115-120 120 NM 40.23 --- NM
OW-1 35 - 50 50 NM 36.80 --- NM
OW-2 35 - 50 50 NM 45.45 --- NM

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene,
TAA, TAME, TBA, isopropylbenzene, IPE, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1R, MW-3, MW-4, DW-1,
DW-3, and OW-2 exceeded the MACs. All contaminant concentrations were below the GCLs; however,
DW-2 historically contains contamination above the GCLs. A summary of the analytical results for ground
water samples collected on November 14, 2022 is presented in Table 6. A Ground Water Quality Map
based on the November 2022 data is included as Figure 5. A complete report of laboratory analyses of
the ground water samples collected from the monitoring wells during the November 2022 sampling event
has been included as Appendix E. A summary of the current ground water analytical data is shown below:
Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
Date
Collected
(mm/dd/yy)
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1R 11/14/22 16.4 177 19.1 308 677 15.2
MW-2 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-3 11/14/22 <0.180 14.8 41.0 288 19.3 28.9
MW-4 11/14/22 0.312 J <0.220 <0.170 0.728 4.05 <0.470
MW-5 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-6 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-7 11/14/22 <0.180 0.335 J <0.170 <0.210 2.07 <0.470
MW-8 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-9 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-10 11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
DW-1 11/14/22 0.260 J 0.474 J <0.170 0.464 J 217 <0.470
DW-2 11/14/22 NS NS NS NS NS NS
DW-3 11/14/22 350 1.21 0.861 127 144 5.02
OW-1 11/14/22 NS NS NS NS NS NS
OW-2 11/14/22 3,210 24,600 2,270 15,800 1,100 1,480

The site is in the Piedmont Physiographic Province of North Carolina. The soils in the area are the result
of in-place weathering of the underlying bedrock, except along stream valleys where the soils are
comprised of alluvial materials and their weathered products. The water table has a seasonal high depth
to water of approximately 27 to 30 feet BGS.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
5
3.0 FREE PRODUCT REMOVAL
Free product was historically present in monitoring wells MW-1R, MW-3 and OW-2. To date, six MMPE
events have been conducted at the site. A total of approximately 18,052.30 gallons of contaminated
ground water and free product have been removed from the site. No free product has been identified
since the January 2020 sampling event.
4.0 REMEDIATION SYSTEM
In accordance with the 2009 CAP and 2016 system redesign, a SVE and AS system was installed at the site
and activated on February 20, 2018. The system installation included the installation and connection of a
total of five AS wells and six SVE wells throughout the contaminant plume. A map showing the locations
of the remediation wells is included as Figure 6.

O&M site visits were conducted on October 13 and October 24, 2022. Please note that the remediation
system was off upon arrival during the November 14, 2022 sampling event and was unable to be restarted.
Hour meter, system vacuum, pressure, air flow, temperature, AS well pressure, and SVE well vacuum
readings were collected during both site visits. Additionally, SVE effluent air samples were collected
during both site visits and submitted for laboratory analysis of BTEX by EPA Method TO-3.

The SVE system operated for a total of 267 hours and the system vacuum ranged from 1.7 to 2.5 inches
of Hg during the current quarter of O&M (September through November 2022). The AS system operated
for a total of 267 hours during the reporting period with system pressures ranging from 1.7 to 2.4 PSI.
Please refer to the individual O&M data sheets for additional system measurements. System flows were
adjusted as needed. General condition of the system was also noted. Work conducted during the site
visits along with hour meter readings is summarized in Table 7. O&M field data sheets are included as
Appendix F.
5.0 AIR SAMPLING
Air samples were collected from the exhaust of the SVE system on October 13 and October 24, 2022. A
summary of the analytical results for air samples collected during the current quarter of system operation
is presented in Table 8. Complete reports of laboratory analyses are included as Appendix E. A summary
of air sampling results during the current quarter is shown below:
Sample Date Benzene Toluene Ethylbenzene Xylenes MTBE Total
BTEX TPH
10/13/2022 <0.010 0.46 <0.10 <0.30 <0.15 0.46 16.5
10/24/2022 <0.010 0.48 <0.10 <0.30 <0.15 0.48 15.2

Overall, remediation and monitoring activities from CAP implementation through the current quarter
have cost $341,437.22. A breakdown of the costs is included as Appendix G and summarized below:
225
(Claim has
not been
submitted)
4.031 Cost for Sampling Wells $1,452.00
$11,238.59
4.090 Cost for Analytical $1,892.00
4.091 Sample Shipping $40.00
6.106 Corrective Action Performance Report $2,250.00
7.201 Cost for Scheduled Maintenance $1,302.00

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
6
7.260 Cost for Remediation Operating Expenses $2,502.59
12.050 Consultant Mobilization $1,500.00
12.055 Temporary Impact Increase $300.00
Total Cost Since System Installation $341,437.22
6.0 SOIL AND GROUND WATER REMEDIATION
The May 2017 ground water sampling event was used as the baseline event per the direction of the
NCDEQ. Based on the May 2017 Benzene Isoconcentration Map, the contaminant plume was broadly
divided into four areas (Areas 1 through 4). A map showing the estimated contaminant mass areas has
been included as Figure 7.

Available historical data for the site was reviewed in order to develop a strategy for measuring
remediation progress against an established baseline for the contaminant plume. To calculate
contaminant mass present at the site, the following three avenues of contaminant migration/source were
evaluated as well as the data required for each source. The calculations were revised to estimate the
influence of fluctuations in ground water elevation.

1. Contamination present in ground water: The May 2017 ground water sampling data and total
BTEX, MTBE, and naphthalene constituents were used to determine the baseline contaminant
mass in each area. Area #1 had approximately 3.57 grams of contaminant mass; Area #2 had
approximately 36,954.63 grams of contaminant mass; Area #3 had approximately 13,116.70
grams of contaminant mass and Area #4 had approximately 4,315.92 grams of contaminant mass,
respectively.

Calculations based on the November 14, 2022 ground water sampling event indicate that the
contaminant mass has decreased by 76.1%, 65.9%, 87.7% and 96.7% in Areas 1 through 4,
respectively, when compared to the baseline sampling event. The contaminant concentrations in
Areas 1 through Area 4 have generally decreased over time; however, Area 2 has intermittently
contained free product. The overall contaminant mass at the site has decreased by approximately
73.6% from the May 2017 sampling event to the November 2022 sampling event. Contaminant
mass calculations are included as Appendix H. A chart depicting the overall trend in contaminant
mass and the changes in average water column depth over time is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
7

2. Contamination due to leaching effect from unsaturated soils: Soil quality data from the former
source areas as well as from the vicinity of the above referenced source area monitoring wells is
not available. Therefore, it is not possible at this point to factor in the effect of this potential on-
going source of ground water contamination. However, since the water table surface is much
shallower than during the baseline event, it is likely that contaminant leaching from previously
unsaturated soils is contributing to increases in contaminant mass. If soil sampling is deemed
necessary for the calculation of any secondary source inputs, they will be proposed at a later date.
3. Contamination input due to the presence of free product: Free product was observed in
observation well OW-2 during the August 2018, October 2018, January 2019, April 2019, July
2019, and January 2020 ground water sampling events and prior to the September 2019 MMPE
event and the site has had a history of free product in the past. Free product was also observed
in MW-3 during the February 2019 ground water sampling event. If free product is observed at
the site in future sampling events, free product removal should be continued in order to reduce
the effects of free product acting as a secondary source of ground water contamination.

Monitoring Plan:
Based on the Intermediate site risk ranking, the following monitoring plan is recommended:
 Collect a ground water sample from telescoping well DW-2 and observation well OW-2 on a semi-
annual basis since the contamination concentrations in DW-2 remain above the GCLs and the
contaminant concentrations in OW-2 fluctuate above and below the GCLs.
 Include a comprehensive ground water sampling event that includes wells MW-1R, MW-3, MW-
0.00
5.00
10.00
15.00
20.00
25.00
-
10,000
20,000
30,000
40,000
50,000
60,000
70,000
80,000
90,000
Water Column Height (ft.)Total Contaminant Mass (grams)Total Contaminant Mass vs Time
Handy Stop #7
Total Contaminant Mass
(grams)
Average Water Column Height (ft)

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
8
4, OW-1, OW-2 and DW-1 through DW-3 on an annual basis to monitor for rebound and
downgradient migration.
 Conduct soil sampling on an as-needed basis.

Performance Monitoring:
 The remediation system appears to have been effective at reducing ground water contaminant
concentration in the targeted wells; however, the system was not designed to address the deeper
contamination found in telescoping well DW-2. Additional remediation is necessary to address
the remaining contamination in DW-2. Please note that milestones were not established in the
CAP
 The remediation system should remain off for the first quarter of 2023.
7.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.
8.0 CONCLUSIONS
 O&M site visits were conducted on October 13 and October 24, 2022. Please note that the
remediation system was off upon arrival during the November 14, 2022 sampling event and was
unable to be restarted. Hour meter, system vacuum, pressure, air flow, temperature, AS well
pressure, and SVE well vacuum readings were collected during each site visit. Additionally, SVE
effluent air samples were collected during both October 2022 site visits and submitted for
laboratory analysis.
 On November 14, 2022, ten monitoring wells, two observation wells and three telescoping wells
were gauged, purged, and/or sampled. Please note that OW-1 had a limited volume and could
not be sampled. A car was parked over DW-2, so a ground water sample was not collected. No
free product was observed in any of the wells. Ground water flow converged towards a hydraulic
low located at the front of the store, with a horizontal gradient of approximately 0.20 feet per
foot. The vertical gradient between paired wells DW-2 and MW-3 could not be calculated because
the top-of-casing elevation for MW-3 needs to be re-measured.
 The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, TAA, TAME,
TBA, isopropylbenzene, IPE, n-propylbenzene, styrene, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene reported in the ground water samples collected from MW-1R, MW-3, MW-4,
DW-1, DW-3, and OW-2 exceeded the MACs. All contaminant concentrations were below the
GCLs.
 Calculations based on the November 14, 2022 ground water sampling event indicate that the
contaminant mass has decreased by 76.1%, 65.9%, 87.7% and 96.7% in Areas 1 through 4,
respectively, when compared to the baseline sampling event. The contaminant concentrations in
Areas 1 through Area 4 have generally decreased over time; however, Area 2 has intermittently
contained free product. The overall contaminant mass at the site has decreased by approximately
73.6% from the May 2017 sampling event to the November 2022 sampling event.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Corrective Action Performance Report
Prepared on: December 29, 2022 Handy Stop #7
Project Manager: Joanna Alley, P.E. GRI Project No. 3067
9
 Based on the results of the November 2022 ground water sampling event, GRI recommends that
the risk ranking of the site should remain Intermediate. GCL exceedances remain in telescoping
well DW-2; however, the remediation system was not designed to address deep contamination.
GRI is gathering information about potential injection technologies to address the contamination
in DW-2; however, some of the options are still in the process of getting approved as an approved
innovative technology. Semi-annual ground water monitoring should continue for telescoping
well DW-2 and observation well OW-2; while annual ground water monitoring should be
conducted on wells MW-1, MW-3, MW-4, MW-8 through MW-10, OW-1, and DW-1 through DW-
3 to monitor for potential contaminant rebound. Based on the November 2022 sampling event,
contaminant concentrations in all shallow monitoring wells were below GCLs; therefore, the
remediation system should remain off for the first quarter of 2023. The next semi-annual ground
water sampling event is scheduled tentatively for May 2023.
9.0 LIMITATIONS
This report has been prepared for the exclusive use of Shell Brothers Distributors, Inc. for specific
application to the referenced site in Catawba County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by the NCDEQ and with resources adequate only
for that scope of work. Our findings have been developed in accordance with generally accepted
standards of environmental practices in the State of North Carolina, available information, and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
10.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A

FIGURES
Copyright (C) 2009 MyTopo, 2006-2018 TomTom
081.2000000° W
081.2000000° W
081.1833333° W
081.1833333° W
081.1666666° W
081.1666666° W35.7535.7535.7333333° N35.7333333° N35.7166666° N35.7166666° N35.7000000° N35.7000000° NSCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 7.50° W
MN
Figure 1
Site Location Map
Handy Stop #7
1500 Rock Barn Road, Conover, Catawba County, NC
Incident No. 36069
GRI Project No. 3067
Date: 08/15/18
Scale: 1 inch = 2,000 ft.Copyright (C) 2009 MyTopo
Location: 035.7222431° N 081.1843913° W
Site Location
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J"J
"J "J
"J
SITE
E I 40 W I 40ROCK BARN RD NEE I 4 0 O N
W I 40 ON
BANNER RD NE
L AP RD N E
B
R
A
D
L
E
Y D
R
E I 40 OFF W I 40 OFF JOHN DANI
EL DR NEUnknown Tribu tary
Unknown TributaryUnknown TributaryUnknown Tributary
Unknown Tr
i
but
ar
yWSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-19
WSW-18WSW-17
WSW-16 WSW-15
WSW-12
WSW-11
WSW-10
375210364087
375213133824
375209152625
375213042584
375213240895
375209253926
375213139813
375213037912
375213243117
375209159389
375213048172
375209251067
3
7
5
2
1
3
0
4
5
0
6
2
375213147933 375209253474375209251253375213148271375209254897
FIGURE 3A: SITE VICINITY MAPHANDY STOP #71500 ROCK BARN ROADCONOVER, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 36069GRI NO. 3067
PREPARED BYGEOLOGICAL RESOURCES, INC.MAY 9, 20181,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
Streams
Street Centerlines
Parcels
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J"J
"J "J
"J
SITE
E I 40 W I 40ROCK BARN RD NEE I 4 0 O N
W I 40 ON
BANNER RD NE
L AP RD N E
B
R
A
D
L
E
Y D
R
E I 40 OFF W I 40 OFF JOHN DANI
EL DR NEUnknown Tribu tary
Unknown TributaryUnknown TributaryUnknown Tributary
Unknown Tr
i
but
ar
yWSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-19
WSW-18WSW-17
WSW-16 WSW-15
WSW-12
WSW-11
WSW-10
FIGURE 3B: ZONING MAPHANDY STOP #71500 ROCK BARN ROADCONOVER, CATAWBA COUNTYNORTH CAROLINAINCIDENT NO. 36069GRI NO. 3067
PREPARED BYGEOLOGICAL RESOURCES, INC.DECEMBER 14, 20211,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
³
0 300150Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
Street Centerlines
Streams
ZONING O-I
ZONING - M-1
ZONING - R-20
ZONING - B-4
ZONING - B-2
Parcels

TABLES
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
0-031674
Name of Owner or Operator Dates of Ownership / Operation
Royal Enterprises Inc. 10/01/2006-Present
Address Telephone Number
322 E. Fisher Street Suite 101, Salisbury, NC 28144-5059 704-633-2434
1024 Browning Road, Greensboro, NC 27410 336-339-1394
0-031674
Name of Owner or Operator Dates of Ownership / Operation
Shell Brothers, Inc. 02/19/1990 - 10/01/2006
Address Telephone Number
Page 1 of 1
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
2 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
3 Gasoline Gasoline 10,000 02/19/90 Steel 8' X 26.6' Fiberglass Current Yes
4 Diesel Diesel 5,200 02/19/90 Steel 8' X 13.4' Fiberglass Current No
5 Kerosene Kerosene 5,200 02/19/90 Steel 8' X 13.4' Fiberglass Current No
Construction
Details Tank Dimensions
Description
of
Associated
Product Piping
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 01/13/2020 Facility ID # : 0-031674
UST ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Tank Date
Installed
Page 1 of 1
Facility ID # : 0-031674
Well ID.Previous
Well ID.Parcel ID No.Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Municipal
Water
Connected?
Well
Depth
(ft. BGS)
Type of
Well
(Drilled/
Bored)
Well
Casing
Depth
(ft. BGS)
Well
Screen
Interval
(x to y ft.
BGS)
Distance from
source area of
release
(ft.)
Comments
WSW-3 WSW-7 375209251067 GATEWAY 4 PROPERTIES, LLC 785 HIGHWAY 70 SE, SUITE 100
HICKORY, NC 28602
1506 ROCK BARN RD NE
CONOVER, NC 28613 Irrigational Yes Unknown Unknown Unknown Unknown ~520' NE
Interviewed
resident
WSW-4 WSW-8 375209251253 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
1508 ROCK BARN RD NE
CONOVER, NC 28613
Not In Use/No
pump Yes Unknown Unknown Unknown Unknown ~560' NE
Owner
Confirmed
WSW-5 WSW-9 375209253474 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
1510/1512 ROCK BARN RD NE
CONOVER, NC 28613
Non-
Potable/garage
use only
Yes Unknown Unknown Unknown Unknown ~735' NE
No water meter
found
WSW-6 WSW-11 375209254897 EDWARD ELLIOTT 3525 ROCK BARN RD NE
CONOVER, NC 28613
3525 ROCK BARN RD NE
CONOVER, NC 28613 Not in Use Yes Unknown Unknown Unknown Unknown ~1,186' NE
WSW-7 WSW-10 375209253926 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
3557 ROCK BARN RD NE
CONOVER, NC 28613
Not In Use/No
Pump Yes Unknown Unknown Unknown Unknown ~1,107' NE
WSW-8 WSW-6 375209159389 JERRY WAYNE ISENHOUR 1399 BRANDYWINE
HICKORY, NC 28602-8269
1505 ROCK BARN RD NE
CONOVER, 28613 Irrigational Yes Unknown Unknown Unknown Unknown ~675' NE
Owner
Confirmed
WSW-9 WSW-12 375210364087 HUNSUCKER FARMS LLC 3223 JOHN DANIEL DRIVE
CONOVER, NC 28613
3223 JOHN DANIEL DRIVE
CONOVER, NC 28613 Yes No Unknown Unknown Unknown Unknown ~1,279' E
WSW-10 WSW-4 375209152625 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
2061 BRADLEY DRIVE
CONOVER, 28613 Potable Unknown Unknown Unknown Unknown Unknown ~1,115' NW
WSW-12 WSW-3 375209152625 WILLIAM MACKIE HUNSUCKER 840 HAMILTON STREET
NEWTON, NC 28658
1503 ROCK BARN RD NE
CONOVER, 28613
Not In Use/No
Power to well Yes Unknown Unknown Unknown Unknown ~581' NW
WSW-15 WSW-15 375213037912
ALTON EUGENE & CHARLSE D.
ROBERTS
1340 ROCK BARN RD NE
CONOVER, 28613
1346 ROCK BARN RD NE
CONOVER, 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,500' SW
Left a well use
survey at
residence,
survey not
returned.
WSW-16 WSW-17 375213045062 MICHAEL DEAN ROBERTS
1344 ROCK BARN RD NE
CONOVER, 28613
1344 ROCK BARN RD NE
CONOVER, 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,234' SW Residence
vacant
WSW-17 WSW-16 375213048172 MARY SHOOK ROBERTS HEIRS
2729 SIDES DRIVE
CONNELLYS SPRINGS, NC 28612
1346 ROCK BARN RD NE
CONOVER, 28613 Unknown Unknown Unknown Unknown Unknown Unknown ~1,320' SW
Left a well use
survey at
residence,
survey not
returned.
WSW-18 WSW-13 375213133824 OLD DOMINION FREIGHT LINE, INC 500 OLD DOMINION WAY
THOMASVILLE, NC 27360
102 BANNER ROAD NE
CONOVER, NC 28613
Non-
Potable/Washing
trucks
Yes Unknown Unknown Unknown Unknown ~1,121' SW
WSW-19 WSW-18 375213139813 CHARLES DEAN ROBERTS, LFI
114 BANNER ROAD NE
CONOVER, NC 28613
114 BANNER ROAD NE
CONOVER, NC 28613 Potable No Unknown Unknown Unknown Unknown ~1,253' S Interviewed
resident
Notes:
• Water supply wells are keyed to Figure 3.
• Ft. BGS : Feet below ground surface
• Receptor survey last updated January 2013.
Date: 12/12/2022
TABLE 3
WATER SUPPLY WELL INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Page 1 of 1
DATE: 12/12/2022 Facility ID #: 0-031674
Parcel ID Address Owner Name Owner Address
375213147933
(site)
1500 Rock Barn Road NE
Conover, NC C.C. Royal Properties, LLC 322 E Fisher Street, Suite 101
Salisbury, NC 28144
375209152625 1503 Rock Barn Road NE
Conover, NC Hunsucker Farms, LLC 3223 John Daniel Drive NE
Conover, NC 28613
375209159389 1505 Rock Barn Road NE
Conover, NC Jerry Wayne Isenhour 1399 Brandywine
Hickory, NC 28602
375213240895 1504 Rock Barn Road NE
Conover, NC Estes Express Lines 3901 W Broad Street
Richmond, VA 23230
Note:
• Properties are keyed to Figure 3A.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Page 1 of 1
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
08/23/06 39.85 --- --- 61.73
12/05/07 43.87 43.84 0.03 57.73
10/20/08 43.69 43.66 0.03 57.91
11/24/08 44.15 44.14 0.01 57.44
12/12/08 44.25 --- --- 57.33
08/04/09 40.81 --- --- 60.77
09/06/11 40.89 --- --- 60.69
05/20/13 39.24 --- --- 62.34
02/28/14 36.92 --- --- 62.34
04/08/14 38.13 --- --- 63.45 Pre AS Test
06/16/14 36.71 --- --- 64.87
08/11/14 37.82 37.81 0.01 63.77 Pre-MMPE
08/15/14 42.98 --- --- 58.60 Post-MMPE
09/02/14 38.21 --- --- 63.37
01/19/15 39.21 --- --- 62.37 Pre-MMPE
01/23/15 44.05 --- --- 57.53 Post-MMPE
01/30/15 39.38 --- --- 62.20
04/15/15 39.56 --- --- 62.02
06/15/15 38.96 --- --- 62.62 Pre-MMPE
06/19/15 43.03 --- --- 58.55 Post-MMPE
07/28/15 30.98 --- --- 70.60
04/06/16 36.82 --- --- 64.76
07/11/16 37.41 --- --- 64.17 Pre-MMPE
07/15/16 39.35 --- --- 62.23 Post-MMPE
08/09/16 37.61 --- --- 63.97
05/02/17 40.72 --- --- 60.86
04/19/18 38.38 --- --- 63.20
08/13/18 36.93 --- --- 64.65
10/15/18 36.23 --- --- 65.35
01/22/19 32.60 --- --- 68.98
04/08/19 31.72 --- --- 69.86
07/29/19 31.72 --- --- 69.86
10/08/19 34.25 --- --- 67.33
01/02/20 34.21 --- --- 67.37
10/13/20 29.55 --- --- 72.03
04/08/21 28.78 --- --- 72.80
10/20/21 34.18 --- --- 67.40
04/05/22 36.81 --- 0.00 64.77
11/14/22 36.08 --- --- 65.50
08/23/06 39.56 --- --- NM
12/05/07 DRY DRY DRY NM
10/20/08 DRY DRY DRY NM
11/24/08 DRY DRY DRY NM
12/12/08 38.57 --- --- NM
08/04/09 37.18 --- --- NM
09/06/11 36.75 --- --- NM
05/20/13 36.52 --- --- NM
08/11/14 35.46 --- --- NM Pre-MMPE
08/15/14 35.41 --- --- NM Post-MMPE
09/02/14 35.56 --- --- NM
07/28/15 35.79 --- --- NM
04/06/16 33.99 --- --- NM
05/02/17 36.26 --- --- NM
04/19/18 35.36 --- --- NM
08/13/18 34.20 --- --- NM
10/15/18 NM --- --- NM Blocked By Car
01/22/19 29.42 --- --- NM
04/08/19 29.31 --- --- NM
07/29/19 30.25 --- --- NM
10/08/19 33.84 --- --- NM
01/02/20 31.48 --- --- NM
04/14/20 29.50 --- --- NM
10/13/20 27.00 --- --- NM
04/08/21 27.29 --- --- NM
04/05/22 33.93 --- 0.00 NM
11/14/22 32.73 --- --- NM
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
MW-1R 08/10/06 4 30 30-45 45 101.58
MW-2 08/10/06 4 30 30-45 45 NM
Page 1 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
08/23/06 39.49 --- --- 62.51
12/05/07 42.93 --- --- 59.07
10/20/08 43.82 --- --- 58.18
11/24/08 43.99 --- --- 58.01
12/12/08 44.09 --- --- 57.91
08/04/09 41.01 --- --- 60.99
09/06/11 40.45 --- --- 61.55
05/20/13 39.55 --- --- 62.45
06/16/14 36.74 --- --- 65.26
07/28/15 NM NM NM NM
04/06/16 NM NM NM NM
02/28/19 NM NM 0.25 NM
Bailer
Confirmed***03/11/19 33.30 33.27 0.03 NM Pre-MMPE
03/15/19 41.01 --- --- NM Post-MMPE
04/08/19 32.80 NM NM NM F.P. After Bailing
07/29/19 33.37 --- --- NM
09/09/19 33.26 --- --- NM Pre-MMPE
09/13/19 33.43 --- --- NM Post-MMPE
10/08/19 34.08 --- --- NM
01/02/20 34.85 --- --- NM
10/13/20 30.43 --- --- NM
04/08/21 28.94 --- --- NM
10/20/21 37.13 --- --- NM Sheen
04/05/22 36.35 --- 0.00 NM
11/14/22 44.25 --- --- NM
08/23/06 38.87 --- --- 62.85
12/05/07 42.18 --- --- 59.54
10/20/08 43.33 --- --- 58.39
11/24/08 43.50 --- --- 58.22
12/12/08 43.66 --- --- 58.06
08/04/09 40.65 --- --- 61.07
09/06/11 39.88 --- --- 61.84
05/20/13 39.19 --- --- 62.53
07/28/15 38.96 --- --- 62.76
04/06/16 37.04 --- --- 64.68
08/09/16 37.32 --- --- 64.40
05/02/17 40.33 --- --- 61.39
04/19/18 38.81 --- --- 62.91
08/13/18 37.36 --- --- 64.36
10/15/18 37.06 --- --- 64.66
01/22/19 35.28 --- --- 66.44
04/08/19 33.43 --- --- 68.29
07/29/19 32.71 --- --- 69.01
10/08/19 34.08 --- --- 67.64
01/02/20 35.07 --- --- 66.65
10/13/20 31.29 --- --- 70.43
04/08/21 29.97 --- --- 71.75
10/20/21 33.90 --- --- 67.82
04/05/22 36.53 --- 0.00 65.19
11/14/22 35.06 --- --- 66.66
12/05/07 37.60 --- --- 62.40
10/20/08 35.35 --- --- 64.65
11/24/08 37.91 --- --- 62.09
12/12/08 37.05 --- --- 62.95
08/04/09 35.45 --- --- 64.55
09/06/11 36.44 --- --- 63.56
05/20/13 33.53 --- --- 66.47
07/28/15 36.19 --- --- 63.81
04/06/16 33.33 --- --- 66.67
05/02/17 35.72 --- --- 64.28
04/19/18 34.31 --- --- 65.69
08/13/18 32.08 --- --- 67.92
10/15/18 31.71 --- --- 68.29
01/22/19 29.56 --- --- 70.44
04/08/19 28.53 --- --- 71.47
07/29/19 28.83 --- --- 71.17
10/08/19 31.82 --- --- 68.18
01/02/20 29.80 --- --- 70.20
10/13/20 26.45 --- --- 73.55
04/08/21 25.67 --- --- 74.33
04/05/22 31.68 --- 0.00 68.32
11/14/22 31.72 --- --- 68.28
Well Casing
Blocked
102.00
MW-3 08/10/06
MW-4 08/10/06
MW-5 12/03/07
2 30 30-45 45
NM
2 30 30-45 45 101.72
2 30 30-50 50 100.00
Page 2 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
12/05/07 43.11 --- --- 57.85
10/20/08 41.06 --- --- 59.90
11/24/08 42.28 --- --- 58.68
12/12/08 42.52 --- --- 58.44
08/04/09 37.72 --- --- 63.24
09/06/11 39.42 --- --- 61.54
05/20/13 34.99 --- --- 65.97
07/28/15 37.89 --- --- 63.07
04/06/16 33.56 --- --- 67.40
05/02/17 37.69 --- --- 63.27
04/19/18 35.38 --- --- 65.58
08/13/18 33.71 --- --- 67.25
10/15/18 NM --- --- NM Blocked by Car
01/22/19 29.01 --- --- 71.95
04/08/19 29.05 --- --- 71.91
07/29/19 30.04 --- --- 70.92
10/08/19 33.77 --- --- 67.19
01/02/20 30.91 --- --- 70.05
10/13/20 28.72 --- --- 72.24
04/08/21 26.93 --- --- 74.03
04/05/22 33.12 --- 0.00 67.84
11/14/22 32.20 --- --- 68.76
12/05/07 41.73 --- --- 59.72
10/20/08 42.83 --- --- 58.62
11/24/08 42.88 --- --- 58.57
12/12/08 43.08 --- --- 58.37
08/04/09 39.86 --- --- 61.59
09/06/11 39.23 --- --- 62.22
05/20/13 38.51 --- --- 62.94
07/28/15 38.17 --- --- 63.28
04/06/16 36.03 --- --- 65.42
05/02/17 49.06 --- --- 52.39
04/19/18 37.89 --- --- 63.56
08/13/18 36.39 --- --- 65.06
10/15/18 49.42 --- --- 52.03
01/22/19 48.99 --- --- 52.46
04/08/19 32.26 --- --- 69.19
07/29/19 31.79 --- --- 69.66
10/08/19 49.53 --- --- 51.92
01/02/20 34.39 --- --- 67.06
10/13/20 30.32 --- --- 71.13
04/08/21 29.05 --- --- 72.40
04/05/22 35.79 --- 0.00 65.66
11/14/22 49.43 --- --- 52.02
2 30 30-50 50 101.45
MW-6 12/03/07
MW-7 12/03/07
2 30 30-50 50 100.96
Page 3 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
12/05/07 44.17 --- --- 57.57
10/20/08 44.51 --- --- 57.23
11/24/08 44.88 --- --- 56.86
12/12/08 45.03 --- --- 56.71
08/04/09 41.35 --- --- 60.39
09/06/11 41.50 --- --- 60.24
05/20/13 39.75 --- --- 61.99
02/28/14 49.65 --- --- 52.09
04/08/14 38.31 --- --- 63.43 Pre AS Test
08/11/14 38.39 --- --- 63.35 Pre-MMPE
08/15/14 38.95 --- --- 62.79 Post-MMPE
09/02/14 38.78 --- --- 62.96
01/19/15 39.88 --- --- 61.86 Pre-MMPE
01/23/15 40.38 --- --- 61.36 Post-MMPE
01/30/15 39.98 --- --- 61.76
04/15/15 39.36 --- --- 62.38
06/15/15 39.49 --- --- 62.25 Pre-MMPE
06/19/15 40.16 --- --- 61.58 Post-MMPE
07/28/15 40.49 --- --- 61.25
04/06/16 37.19 --- --- 64.55
07/11/16 37.98 --- --- 63.76 Pre-MMPE
07/15/16 38.35 --- --- 63.39 Post-MMPE
08/09/16 38.19 --- --- 63.55
05/02/17 41.35 --- --- 60.39
04/19/18 39.49 --- --- 62.25
08/13/18 37.40 --- --- 64.34
10/15/18 36.90 --- --- 64.84
01/22/19 33.63 --- --- 68.11
03/11/19 32.47 --- --- 69.27 Pre-MMPE
03/15/19 32.61 --- --- 69.13 Post-MMPE
04/08/19 32.32 --- --- 69.42
07/29/19 32.68 --- --- 69.06
09/09/19 34.17 --- --- 67.57 Pre-MMPE
09/13/19 34.59 --- --- 67.15 Post-MMPE
10/08/19 49.52 --- --- 52.22
01/02/20 35.40 --- --- 66.34
10/13/20 30.66 --- --- 71.08
04/08/21 29.64 --- --- 72.10
10/20/21 49.70 --- --- 52.04
04/05/22 37.63 --- 0.00 64.11
11/14/22 49.87 --- --- 51.87
01/16/13 42.61 --- --- 56.01
05/20/13 38.64 --- --- 59.98
07/28/15 40.23 --- --- 58.39
04/06/16 36.30 --- --- 62.32
05/02/17 41.02 --- --- 57.60
04/19/18 38.56 --- --- 60.06
08/13/18 37.44 --- --- 61.18
10/15/18 36.84 --- --- 61.78
01/22/19 32.91 --- --- 65.71
04/08/19 31.68 --- --- 66.94
07/29/19 32.81 --- --- 65.81
10/08/19 35.65 --- --- 62.97
01/02/20 35.58 --- --- 63.04
10/13/20 30.76 --- --- 67.86
04/08/21 29.40 --- --- 69.22
10/20/21 36.32 --- --- 62.30
04/05/22 37.49 --- 0.00 61.13
11/14/22 36.46 --- --- 62.16
01/16/13 41.00 --- --- 57.82
05/20/13 38.02 --- --- 60.80
07/28/15 38.90 --- --- 59.92
04/06/16 35.71 --- --- 63.11
05/02/17 39.81 --- --- 59.01
04/19/18 37.68 --- --- 61.14
08/13/18 36.45 --- --- 62.37
10/15/18 36.11 --- --- 62.71
01/22/19 32.94 --- --- 65.88
04/08/19 31.66 --- --- 67.16
07/29/19 32.09 --- --- 66.73
10/08/19 34.44 --- --- 64.38
01/02/20 34.72 --- --- 64.10
10/13/20 30.34 --- --- 68.48
04/08/21 29.20 --- --- 69.62
10/20/21 34.58 --- --- 64.24
04/05/22 36.06 --- 0.00 62.76
11/14/22 35.36 --- --- 63.46
MW-8 12/03/07 2 30 30-50 50 101.74
MW-9 01/02/13
MW-10 01/02/13
2 35 35-50 50 98.62
2 35 35-50 50 98.82
Page 4 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
11/24/08 45.16 --- --- NM
12/12/08 46.09 --- --- NM
08/04/09 41.81 --- --- NM
09/06/11 41.95 --- --- NM
05/20/13 40.33 --- --- NM
07/28/15 40.91 --- --- NM
04/06/16 38.09 --- --- NM
08/09/16 38.81 --- --- NM
05/02/17 41.76 --- --- NM
04/19/18 39.88 --- --- NM
08/13/18 38.54 --- --- NM
10/15/18 37.91 --- --- NM
01/22/19 35.08 --- --- NM
04/08/19 33.75 --- --- NM
07/29/19 33.83 --- --- NM
10/08/19 38.18 --- --- NM
01/02/20 36.21 --- --- NM
10/13/20 DRY --- --- NM
04/08/21 30.30 --- --- NM
10/20/21 63.03 --- --- NM Limited Volume
04/05/22 37.97 --- 0.00 NM
11/14/22 37.73 --- --- NM
01/16/13 43.28 --- --- 56.78
02/11/13 42.48 --- --- 57.58
05/20/13 40.78 --- --- 59.28
07/28/15 41.66 --- --- 58.40
04/06/16 38.64 --- --- 61.42
08/09/16 39.57 --- --- 60.49
05/02/17 42.31 --- --- 57.75
04/19/18 40.76 --- --- 59.30
08/13/18 39.26 --- --- 60.80
10/15/18 38.55 --- --- 61.51
01/22/19 35.77 --- --- 64.29
03/11/19 34.65 --- --- 65.41 Pre-MMPE
03/15/19 41.03 --- --- 59.03 Post-MMPE
04/08/19 34.47 --- --- 65.59
07/29/19 34.70 --- --- 65.36
09/09/19 36.04 --- --- 64.02 Pre-MMPE
09/13/19 39.01 --- --- 61.05 Post-MMPE
10/08/19 36.20 --- --- 63.86
01/02/20 36.87 --- --- 63.19
10/13/20 34.00 --- --- 66.06
04/08/21 31.75 --- --- 68.31
10/20/21 36.82 --- --- 63.24
04/05/22 38.51 --- 0.00 61.55
11/14/22 37.84 --- --- 62.22
03/26/13 NM NM NM NM
05/20/13 24.31 --- --- NM
07/28/15 43.76 --- --- NM
04/06/16 40.35 --- --- NM
05/02/17 44.73 --- --- NM
04/19/18 41.92 --- --- NM
08/13/18 41.36 --- --- NM
10/15/18 40.43 --- --- NM
01/22/19 37.56 --- --- NM
03/11/19 36.37 --- --- NM Pre-MMPE
03/15/19 36.68 --- --- NM Post-MMPE
04/08/19 36.47 --- --- NM
07/29/19 37.25 --- --- NM
09/09/19 33.73 --- --- NM Pre-MMPE
09/13/19 39.07 --- --- NM Post-MMPE
10/08/19 39.86 --- --- NM
01/02/20 39.18 --- --- NM
10/13/20 35.15 --- --- NM
04/08/21 34.02 --- --- NM
10/20/21 44.35 --- --- NM
04/05/22 40.61 --- 0.00 NM
11/14/22 40.23 --- --- NM
2 115 115-120 120 NM
DW-2 01/03/13
DW-3 03/26/13
DW-1 11/24/08 2 60 60-65 65 NM
2 85 85-90 90 100.06
Page 5 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
02/28/14 37.89 --- --- NM
04/08/14 38.70 --- --- NM
06/16/14 37.38 --- --- NM
08/11/14 38.52 --- --- NM Pre-MMPE
08/15/14 39.60 --- --- NM Post-MMPE
09/02/14 38.91 --- --- NM
01/19/15 39.99 --- --- NM Pre-MMPE
01/23/15 40.91 --- --- NM Post-MMPE
01/30/15 40.13 --- --- NM
04/15/15 39.74 --- --- NM
06/15/15 39.68 --- --- NM Pre-MMPE
06/19/15 40.91 --- --- NM Post-MMPE
07/28/15 40.64 --- --- NM
04/06/16 37.38 --- --- NM
07/11/16 38.17 --- --- NM Pre-MMPE
07/15/16 38.93 --- --- NM Post-MMPE
08/09/16 38.34 --- --- NM
05/02/17 41.46 --- --- NM
04/19/18 39.53 --- --- NM
08/13/18 37.86 --- --- NM
10/15/18 37.26 --- --- NM
01/22/19 34.10 --- --- NM
03/11/19 32.85 --- --- NM Pre-MMPE
03/15/19 33.08 --- --- NM Post-MMPE
04/08/19 34.55 --- --- NM
07/29/19 32.91 --- --- NM
09/09/19 34.46 --- --- NM Pre-MMPE
09/13/19 39.04 --- --- NM Post-MMPE
10/08/19 35.44 --- --- NM
01/02/20 35.53 --- --- NM
10/13/20 35.53 --- --- NM
04/08/21 30.12 --- --- NM
10/20/21 35.61 --- --- NM Mud
04/05/22 37.16 --- 0.00 NM
11/14/22 36.80 --- --- NM
02/28/14 38.38 --- --- NM
04/08/14 NM Observed ~3 NM
Equipment
Malfunction, bailer
confirmed
06/16/14 39.30 36.27 3.03 NM
08/11/14 40.27 37.40 2.87 NM Pre-MMPE
08/15/14 43.96 --- --- NM Post-MMPE
09/02/14 39.21 38.16 1.05 NM
01/19/15 40.82 39.01 1.81 NM Pre-MMPE
01/23/15 45.91 --- --- NM Post-MMPE
01/30/15 39.52 --- --- NM
04/15/15 39.14 --- --- NM
06/15/15 39.17 39.11 0.06 NM Pre-MMPE
06/19/15 47.32 --- --- NM Post-MMPE
07/28/15 40.13 --- --- NM
04/06/16 37.84 ₳ ₳ NM Bailer Confirmed
07/11/16 37.28 --- --- NM Pre-MMPE
07/15/16 41.75 --- --- NM Post-MMPE
08/09/16 37.88 37.77 0.11 NM
05/02/17 40.91 --- --- NM
04/19/18 39.04 --- --- NM
08/13/18 38.35 37.19 1.16 NM Bailer Confirmed
10/15/18 37.54 36.72 0.82 NM Bailer Confirmed
01/22/19 33.71 33.41 0.30 NM Bailer Confirmed
03/11/19 32.56 32.53 0.03 NM Pre-MMPE
03/15/19 42.08 --- --- NM Post-MMPE
04/08/19 31.63 31.60 0.03 NM
07/29/19 32.34 32.23 0.11 NM
09/09/19 33.85 33.62 0.23 NM Pre-MMPE
09/13/19 40.03 --- --- NM Post-MMPE
10/08/19 34.81 --- --- NM
01/02/20 34.73 34.72 0.01 NM Bailer Confirmed
04/14/20 31.90 --- --- NM
10/13/20 32.05 --- --- NM
04/08/21 29.02 --- --- NM
10/20/21 34.81 --- --- NM
04/05/22 37.02 --- 0.00 NM
11/14/22 45.45 --- --- NM
OW-2 02/24/14
2 35 35-50OW-1 02/24/14 50 NM
2 35 35-50 50 NM
Page 6 of 7
Well ID
Date
Installed
(mm/dd/ yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Inner
Diameter
(in.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Depth to
Product
(ft)
Free Product
Thickness**
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Facility ID # : 0-031674Date: 12/12/22
02/28/14 37.44 --- --- NM
04/08/14 37.06 --- --- NM Pre AS Test
08/11/14 38.25 --- --- NM Pre-MMPE
08/15/14 39.56 --- --- NM Post-MMPE
09/02/14 38.84 --- --- NM
01/19/15 39.62 --- --- NM Pre-MMPE
01/23/15 40.93 --- --- NM Post-MMPE
01/30/15 40.09 --- --- NM
04/15/15 39.52 --- --- NM
06/15/15 39.45 --- --- NM Pre-MMPE
06/19/15 41.45 --- --- NM Post-MMPE
07/28/15 40.46 --- --- NM
04/06/16 37.21 --- --- NM
07/11/16 37.82 --- --- NM Pre-MMPE
07/15/16 39.20 --- --- NM Post-MMPE
08/09/16 38.11 --- --- NM
05/02/17 41.55 --- --- NM
AS-2 03/21/17 05/02/17 2 50 50-55 55 NM 41.63 --- --- NM
AS-3 03/21/17 05/02/17 2 50 50-55 55 NM 40.67 --- --- NM
AS-4 03/21/17 05/02/17 2 50 50-55 55 NM 40.82 --- --- NM
AS-5 03/22/17 05/02/17 2 50 50-55 55 NM 41.19 --- --- NM
Notes:
• * : Reference point for elevation measurements.
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• *** : Well pad was repaired, casing was cut and well was unblocked on February 28, 2019.
• ft BGS : feet below ground surface.
• N/A: Not available.
• NM: Not measured.
• Well construction information (where available) is reproduced from the previous consultants reports and available field notes.
• ₳: No interface probe, bailer checked - 9.73" product w/ scale
NM5550-5550202/24/14AS-1
Page 7 of 7
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NE
09/06/11 8,660 36,200 2,790 16,310 905 918 NR NR NR NR NR 801 171 J 2,290 568 258 <5.0 61,900 31,950 <95 19,160
05/20/13 9,620 38,100 3,590 21,700 889 1,490 NR NR NR NR NR 946 302 3,900 932 602 NR 28,400 13,500 <980 16,870
07/29/15 2,880 16,500 2,010 13,600 619 1,420 NR NR NR NR NR 450 200 2,530 613 NR NR NR NR NR NR
04/06/16 1,260 10,300 1,360 10,900 335 1,210 NR NR NR NR NR 271 114 2,470 759 NR NR NR NR NR NR
08/09/16 2,350 14,100 2,140 16,300 538 1,530 NR NR NR NR NR 350 208 3,050 690 NR NR NR NR NR NR
05/03/17 1,380 12,800 1,700 13,200 330 1,060 NR NR NR NR NR 272 217 2,820 747 NR NR NR NR NR NR
04/19/18 1,740 14,600 1,360 14,000 255 992 NR NR NR NR NR 256 119 2,230 606 NR NR NR NR NR NR
08/13/18 1,420 11,200 1,090 11,500 448 1,150 NR NR NR NR NR 281 108 J 2,260 646 NR NR NR NR NR NR
10/15/18 1,510 13,000 1,460 12,200 553 1,500 NR NR NR NR NR 249 162 2,800 688 NR NR NR NR NR NR
01/22/19 742 11,700 1,440 12,500 748 904 NR NR NR NR NR 196 128 2,440 570 NR NR NR NR NR NR
04/08/19 332 10,900 1,660 14,300 259 667 NR NR NR NR NR 52 122 J 2,410 579 NR NR NR NR NR NR
07/29/19 655 15,600 1,920 13,100 403 720 NR NR NR NR NR 92.7 J 126 J 2,060 534 NR NR NR NR NR NR
10/08/19 1,050 17,600 2,250 13,500 352 1,080 NR NR NR NR NR 97.7 J 163 J 2,450 621 NR NR NR NR NR NR
01/02/20 154 3,740 430 5,990 96.7 381 <200 30.1 J NR * NR 17.9 J 33.0 J 1,390 391 NR NR NR NR NR NR
10/13/20 193 2,390 254 5,260 168 469 318 J 29.8 J NR * NR 60.3 34.8 1,640 346 NR NR NR NR NR NR
04/08/21 58.4 610 55.9 2,390 365 50.7 881 53.8 <2.5 * <2.5 97.3 9.3 J 975 242 NR NR NR NR NR NR
10/20/21 16.1 100 11.7 90.5 286 3.1 J 1,430 35.3 <1.3 <20 <1.3 52.0 2.1 J 15.4 50.4 NR NR NR NR NR NR
04/05/22 128 1,930 176 2,190 682 107 555 52.3 <6.3 <100 <6.3 153 9.7 J 390 127 NR NR NR NR NR NR
11/14/22 16.4 177 19.1 308 677 15.2 387 J 67.1 <0.160 287 <0.190 99.7 1.08 34.5 19.7 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 <0.54 6.8 <35 <130 222 165
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.68 NR <35 <132 <97 <185
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.16 J NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 0.17 J 0.96 0.15 J 0.74 J <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 NS NS NS NS NS NS NR NR NR NR NR NS NS NS NS NS NS NS NS NS NS
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
GCL (mg/l)
MW-1R
MW-2 2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)Page 1 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)09/06/11 713 3,520 2,200 11,770 19,400 761 NR NR NR NR NR 3,110 274 2,530 679 199 <5.0 22,500 25,820 <100 18,610
05/20/13 303 3,670 2,580 14,800 12,100 1,170 NR NR NR NR NR 1,820 394 3,360 856 NA NR <35 3,937.5 <980 4,184
07/29/15 NS NS NS NS NS NS NR NR NR NR NR NS NS NS NS NS NS NS NS NS NS
04/06/16 NS NS NS NS NS NS NR NR NR NR NR NS NS NS NS NS NS NS NS NS NS
03/11/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/29/19 697 10,200 1,880 12,500 912 889 NR NR NR NR NR 213 567 5,900 1,620 NR NR NR NR NR NR
10/08/19 504 5,950 2,180 13,400 614 804 NR NR NR NR NR 148 373 4,080 1,060 NR NR NR NR NR NR
01/02/20 373 7,870 2,460 16,100 629 1,110 511 J 118 J NR *NR 144 815 7,060 2,070 NR NR NR NR NR NR
10/13/20 17.0 524 49.3 2,610 326 207 472 48.6 NR * NR 66.9 67.5 2,400 1,120 NR NR NR NR NR NR
04/08/21 <1.3 1.5 J <1.3 20.3 308 18.1 191 47.2 <1.3 * <1.3 54.9 3.6 J 209 167 NR NR NR NR NR NR
10/20/21 < 0.63 6.2 2.7 46.1 141 8.8 182 13.1 <0.63 <10 <0.63 27.8 2.5 63.0 46.4 NR NR NR NR NR NR
04/05/22 <0.63 23.2 29.7 296 214 30.7 63.5 21.7 <0.63 <10 <0.63 62.4 4.3 152 69.9 NR NR NR NR NR NR
11/14/22 <0.180 14.8 41.0 288 19.3 28.9 <1.90 <0.280 <0.160 18.8 <0.190 5.26 19.8 215 77.2 NR NR NR NR NR NR
09/06/11 12.6 12.8 0.85 13.7 7.8 <0.10 NR NR NR NR NR 1.2 <0.11 0.33 J 1.5 <0.56 9.9 861 47.5 J <100 92.2 J
05/20/13 77.9 28.3 4.0 101 4.5 0.56 NR NR NR NR NR 4 0.20 J 3.8 9.1 <0.66 NR 595 <131 <96 959.6
07/29/15 92.3 5.9 4.7 95.6 5.8 <0.24 NR NR NR NR NR 12 <0.31 5.3 13.8 NR NR NR NR NR NR
04/06/16 72.5 1.4 3.1 25.8 5.3 0.30 J NR NR NR NR NR 13.3 0.14 J 4.9 14.9 NR NR NR NR NR NR
08/09/16 46.2 2.5 2.2 18.8 6.3 0.62 NR NR NR NR NR 15.1 <0.13 3 10.2 NR NR NR NR NR NR
05/03/17 30.5 0.55 1.1 7.4 5.6 0.24 J NR NR NR NR NR 12.4 <0.13 1.6 6.4 NR NR NR NR NR NR
04/19/18 0.16 J 0.89 <0.13 0.64 J <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 11.8 0.25 J 0.32 J 1.8 5.4 0.15 J NR NR NR NR NR 12.9 <0.13 0.24 J 2.9 NR NR NR NR NR NR
10/15/18 13.9 0.29 J 0.30 J 2.5 5.4 0.19 J NR NR NR NR NR 12.3 <0.13 0.33 J 1.5 NR NR NR NR NR NR
01/22/19 22.6 0.92 0.38 J 12.3 4.7 0.17 J NR NR NR NR NR 12.6 <0.22 1 1.7 NR NR NR NR NR NR
04/08/19 41.2 1.6 0.68 7.1 4.4 <0.13 NR NR NR NR NR 11.4 <0.13 0.44 J 1.7 NR NR NR NR NR NR
07/29/19 1.5 0.46 J <0.13 3.9 4.4 0.15 J NR NR NR NR NR 11.1 <0.13 0.14 J 0.54 NR NR NR NR NR NR
10/08/19 5.1 0.36 J <0.13 2.5 5.1 0.17 J NR NR NR NR NR 12.7 <0.13 <0.13 0.34 J NR NR NR NR NR NR
01/02/20 0.42 J <0.13 <0.13 1.6 4.4 0.19 J 1,530 0.29 J NR * NR 8.8 <0.13 <0.13 0.37 J NR NR NR NR NR NR
10/13/20 0.75 0.50 <0.13 2.0 3.6 <0.13 985 0.26 J NR * NR 9.1 <0.13 <0.13 0.35 J NR NR NR NR NR NR
04/08/21 0.23 J 0.17 J <0.13 1.5 3.0 <0.13 702 <0.20 <0.13 * <0.13 7.4 <0.13 <0.13 0.44 J NR NR NR NR NR NR
10/20/21 0.84 0.23 J <0.13 2.2 5.7 0.53 2,890 E 0.59 J <0.13 361 <0.13 12.5 <0.13 0.40 J 0.97 NR NR NR NR NR NR
04/05/22 0.32 J 0.23 J <0.13 0.44 J 4.9 0.22 J 1,660 0.39 J <0.13 223 <0.13 12.1 <0.13 0.21 J 2.3 NR NR NR NR NR NR
11/14/22 0.312 J <0.220 <0.170 0.728 4.05 <0.470 859 J 0.397 J <0.160 400 J <0.190 10.4 <0.190 0.517 1.01 NR NR NR NR NR NR
MW-3
MW-4
Page 2 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 <0.57 <5.0 <35 <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.66 NR <35 102 J <96 1,010
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 <0.55 7.7 <35 <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.66 NR <35 <132 <97 562
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 0.34 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 NS NS NS NS NS NS NR NR NR NR NR NS NS NS NS NS NS NS NS NS NS
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 0.30 J <0.13 0.38 J <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
MW-5
MW-6
Page 3 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)09/06/11 <0.13 <0.13 <0.15 <0.30 20.7 <0.10 NR NR NR NR NR 76.0 <0.11 <0.10 <0.10 <0.54 <5.0 83.0 J <135 <100 <135
05/20/13 <0.10 <0.10 <0.10 <0.22 29.0 <0.15 NR NR NR NR NR 39.3 <0.10 <0.10 <0.10 <0.66 NR <35 <131 <96 179 J
07/29/15 <0.17 <0.17 <0.15 <0.43 17.1 <0.12 NR NR NR NR NR 20.3 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 16.1 <0.13 NR NR NR NR NR 10.4 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 11.6 <0.13 NR NR NR NR NR 13.5 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 14.3 <0.13 NR NR NR NR NR 14.7 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 12.3 <0.13 NR NR NR NR NR 2.1 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 11.3 <0.13 NR NR NR NR NR 0.48 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 2.5 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 11.6 <0.13 NR NR NR NR NR 1.1 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 10.1 <0.13 NR NR NR NR NR 0.26 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 8.7 <0.13 NR NR NR NR NR 0.44 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 5.9 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 4.9 <0.13 <2.0 <0.20 NR * NR 0.14 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 2.9 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 4.2 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 0.63 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 0.335 J <0.170 <0.210 2.07 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
09/06/11 144 588 184 739 1.6 J 16.0 NR NR NR NR NR <1.1 55.0 243 68.2 16.3 <5.0 4,480 3,978 <95 9,888
05/20/13 156 2,280 759 4,600 <0.10 301 NR NR NR NR NR 0.77 130 894 193 48.3 NR 2,490 1,430 <110 5,299
07/29/15 152 662 162 741 <1.6 39.2 NR NR NR NR NR <1.6 49.3 238 52.5 NR NR NR NR NR NR
04/06/16 137 1,180 468 2,750 <1.3 246 NR NR NR NR NR <1.3 108 838 127 NR NR NR NR NR NR
08/09/16 8.1 26.0 7.2 29.9 <0.13 1.6 NR NR NR NR NR <0.13 2.5 9.0 1.5 NR NR NR NR NR NR
05/03/17 182 499 130 477 <1.3 28.4 NR NR NR NR NR <1.3 47.3 139 33.8 NR NR NR NR NR NR
04/19/18 206 531 164 604 <1.3 13.8 NR NR NR NR NR <1.3 51.5 162 42.7 NR NR NR NR NR NR
08/13/18 122 301 98.6 365 <1.3 25.4 NR NR NR NR NR <1.3 37.5 114 33.0 NR NR NR NR NR NR
10/15/18 167 363 92.6 224 <1.3 6.6 NR NR NR NR NR <1.3 38.4 63.1 25.2 NR NR NR NR NR NR
01/22/19 147 522 232 1,120 <0.68 82.5 NR NR NR NR NR <0.73 61.7 349 58.5 NR NR NR NR NR NR
04/08/19 128 416 180 802 <1.3 56.0 NR NR NR NR NR <1.3 50.8 251 39.5 NR NR NR NR NR NR
07/29/19 8.4 11.5 4.7 12.1 <0.13 1.1 NR NR NR NR NR <0.13 2.0 2.6 2.3 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 0.13 J 0.16 J <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 2.1 J <0.20 <0.13 2.1 J <0.13 0.15 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.34 J <0.13 0.59 J <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 0.26 J <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 0.561 <0.190 <0.190 0.371 J NR NR NR NR NR NR
MW-8
MW-7
Page 4 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)01/16/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.67 7.6 <35 <131 <96 <131
05/20/13 1.4 0.11 J 0.11 J 1.4 J 0.46 J 0.27 J NR NR NR NR NR 0.38 J <0.10 0.17 J <0.10 <0.66 NR <35 <131 <96 228
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 0.16 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.31 J <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
01/16/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.67 <5.0 <35 <133 <98 <133
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.66 NR <35 <131 <96 166 J
07/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/03/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 0.25 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 0.18 J <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 0.35 J <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <2.0 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <0.160 <1.60 <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
MW-9
MW-10
Page 5 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)09/06/11 467 4.5 J 43.7 525 708 79.2 NR NR NR NR NR 487 13.3 56.5 23.0 15.0 <5.0 2,280 1,614 <110 1,219
05/20/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.66 NR <35 <131 <96 156 J
07/29/15 3,220 166 603 3,600 759 460 NR NR NR NR NR 612 84.3 707 120 NR NR NR NR NR NR
04/06/16 167 8.8 13.9 79.0 45.9 13.9 NR NR NR NR NR 32.7 1.5 J 12.6 1.3 J NR NR NR NR NR NR
08/09/16 3,420 37.6 J 533 2,450 826 276 NR NR NR NR NR 641 48.3 J 418 52.8 NR NR NR NR NR NR
05/03/17 3,370 40.3 J 464 2,460 800 240 NR NR NR NR NR 652 42.7 J 449 60.8 NR NR NR NR NR NR
04/19/18 0.40 J <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 1,850 8.7 J 193 227 321 57.1 NR NR NR NR NR 240 17.2 J 78.6 18.3 J NR NR NR NR NR NR
01/22/19 1,320 9.8 J 167 457 402 98.5 NR NR NR NR NR 330 16.3 149 11.8 NR NR NR NR NR NR
04/08/19 408 5.2 66.9 195 113 44.5 NR NR NR NR NR 86.3 8.6 72.4 6.8 NR NR NR NR NR NR
07/29/19 3,190 51.4 314 1,140 679 111 NR NR NR NR NR 503 21.9 J 200 21.2 J NR NR NR NR NR NR
10/09/19 4,080 107 611 2,150 789 223 NR NR NR NR NR 632 36.3 J 361 41.5 J NR NR NR NR NR NR
01/02/20 4,250 122 643 2,820 924 233 5,190 178 NR *NR 710 42.3 J 446 42.7 J NR NR NR NR NR NR
04/08/21 7.6 0.49 J 0.72 2.7 220 0.23 J 67.1 31.3 <0.13 * <0.13 80.6 <0.13 2.4 1.0 NR NR NR NR NR NR
10/20/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/05/22 1.3 4.3 0.46 J 2.2 8.6 0.18 J <2.0 0.50 J <0.13 <2.0 <0.13 4.9 <0.13 0.19 J <0.13 NR NR NR NR NR NR
11/14/22 0.260 J 0.474 J <0.170 0.464 J 217 <0.470 <1.90 13.5 <0.160 22.5 <0.190 82.7 <0.190 <0.190 <0.180 NR NR NR NR NR NR
01/16/13 5,310 14,800 1,350 7,070 2,010 350 NR NR NR NR NR 882 100 J 777 133 J 52.9 <5.0 43,300 4,110 <96 3,976
02/12/13 5,960 15,700 1,600 8,610 2,230 466 NR NR NR NR NR 921 136 1,210 218 NR NR NR NR NR NR
05/20/13 11,000 29,900 2,620 13,500 3,590 556 NR NR NR NR NR 1,820 219 1,610 378 130 NR 16,000 J 2,420 <190 433
07/29/15 11,800 28,900 2,520 12,900 7,970 705 NR NR NR NR NR 2,570 198 J 1,570 343 J NR NR NR NR NR NR
04/06/16 14,300 34,100 3,010 15,700 11,000 816 NR NR NR NR NR 3,380 241 J 2,020 468 NR NR NR NR NR NR
08/09/16 14,300 33,900 3,060 13,800 13,100 884 NR NR NR NR NR 4,160 228 2,130 453 NR NR NR NR NR NR
05/03/17 12,500 31,800 2,390 14,000 10,200 837 NR NR NR NR NR 3,090 166 J 1,650 384 NR NR NR NR NR NR
04/19/18 13,800 33,600 3,260 17,600 11,700 599 NR NR NR NR NR 3,080 236 2,200 535 NR NR NR NR NR NR
08/13/18 16,300 38,400 2,770 15,100 15,800 779 NR NR NR NR NR 4,250 189 J 1,830 475 J NR NR NR NR NR NR
10/15/18 17,400 44,100 2,970 15,800 15,500 583 NR NR NR NR NR 3,850 186 J 1,670 412 J NR NR NR NR NR NR
01/22/19 18,500 42,400 3,210 18,600 22,800 801 NR NR NR NR NR 6,480 212 J 2,220 489 NR NR NR NR NR NR
03/11/19 18,200 41,600 3,060 15,600 19,400 694 NR NR NR NR NR 5,400 NR NR NR NR NR NR NR NR NR
04/08/19 14,300 36,600 2,380 11,900 16,600 353 J NR NR NR NR NR 3,930 132 J 947 277 J NR NR NR NR NR NR
07/29/19 16,900 43,400 2,600 12,500 18,800 325 J NR NR NR NR NR 4,490 140 J 1,060 318 J NR NR NR NR NR NR
10/09/19 17,300 41,300 2,900 13,700 19,700 568 NR NR NR NR NR 4,900 155 J 1,300 362 J NR NR NR NR NR NR
01/02/20 17,600 43,500 3,000 15,900 22,700 541 44,500 1,150 NR *NR 5,390 163 J 1,320 381 J NR NR NR NR NR NR
10/13/20 18,400 47,300 2,850 16,200 26,000 626 37,100 1,430 NR *NR 5,940 193 J 1,660 491 J NR NR NR NR NR NR
04/08/21 12,500 29,200 1,940 10,900 15,600 476 J 29,500 895 J <130 *<130 3,950 <130 1,260 328 J NR NR NR NR NR NR
10/20/21 14,700 30,900 2,080 11,500 22,500 481 J 53,300 1,250 <130 <2,000 <130 5,220 162 J 1,300 342 J NR NR NR NR NR NR
04/05/22 9,670 19,200 1,750 9,780 13,800 496 15,900 871 <63 <1,000 <63 3,680 287 1,170 1,160 NR NR NR NR NR NR
11/14/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
DW-2
DW-1
Page 6 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)03/26/13 0.83 <0.10 <0.10 0.83 J 0.17 J 0.26 J NR NR NR NR NR <0.10 <0.10 0.26 J <0.10 <0.69 NR 265 <134 <99 <185
05/20/13 0.66 <0.10 <0.10 0.49 J 0.13 J 0.16 J NR NR NR NR NR <0.10 <0.10 <0.10 <0.10 <0.66 NR 213 <131 <96 220
07/28/15 4.4 <0.17 0.18 J 4.7 2.1 0.36 J NR NR NR NR NR 1.0 <0.16 0.76 <0.14 NR NR NR NR NR NR
04/06/16 10.8 6.2 1.0 18.7 7.7 4.5 NR NR NR NR NR 3.4 0.25 J 5.2 0.57 NR NR NR NR NR NR
05/03/17 26.3 0.35 J 0.32 J 27.5 17.1 0.91 NR NR NR NR NR 7.5 0.21 J 3.7 0.22 J NR NR NR NR NR NR
04/19/18 40.7 16.4 2.1 53.1 28.3 1.6 NR NR NR NR NR 14.4 J 0.43 J 8.4 0.69 NR NR NR NR NR NR
08/13/18 42.6 0.67 0.75 45.6 28.7 1.4 NR NR NR NR NR 11.4 0.46 J 7.8 0.48 J NR NR NR NR NR NR
10/15/18 46.5 0.41 J 0.80 51.3 30.3 1.4 NR NR NR NR NR 12.5 0.45 J 7.4 0.43 J NR NR NR NR NR NR
01/22/19 50.2 0.37 J 0.51 58.5 29.5 1.2 NR NR NR NR NR 14.7 0.42 J 9.5 0.41 J NR NR NR NR NR NR
04/08/19 43.7 0.24 J 0.49 J 50.5 24.2 1.0 NR NR NR NR NR 10.9 0.36 J 6.6 0.33 J NR NR NR NR NR NR
07/29/19 43.5 0.25 J 0.38 J 44.5 19.9 0.92 NR NR NR NR NR 9.9 0.31 J 5.0 0.20 J NR NR NR NR NR NR
10/09/19 44.5 0.19 J 0.30 J 33.2 16.4 1.1 NR NR NR NR NR 9.4 0.29 J 4.8 <0.13 NR NR NR NR NR NR
01/02/20 31.7 0.52 0.16 J 25.3 17.0 1.0 113 0.66 J NR * NR 8.9 0.21 J 3.7 0.20 J NR NR NR NR NR NR
10/13/20 43.7 <0.13 0.28 J 17.8 25.3 1.1 146 1.1 NR * NR 12.7 0.28 J 4.2 0.18 J NR NR NR NR NR NR
04/08/21 58.8 3.9 1.5 24.4 26.6 1.5 192 1.1 J <0.25 * <0.25 14.3 0.62 J 6.3 0.32 J NR NR NR NR NR NR
10/20/21 120 4.2 1.1 J 45.8 50.9 1.6 J 388 2.3 J <0.63 <10 <0.63 27.0 1.1 J 12.9 1.0 J NR NR NR NR NR NR
04/05/22 212 2.1 J 1.1 J 86.3 90.1 3.4 573 4.3 J <0.63 <10 <0.63 45.6 1.4 J 31.0 4.0 NR NR NR NR NR NR
11/14/22 350 1.21 0.861 127 144 5.02 549 J 6.92 J <0.160 77.6 <0.190 62.0 2.89 47.5 5.35 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR * NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/15/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 * <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/19 NS NS NS NS NS NS NS NS NR NS NR NS NS NS NS NS NS NS NS NS NS
01/02/20 NS NS NS NS NS NS NS NS NR NS NR NS NS NS NS NS NS NS NS NS NS
01/15/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 4.9 *0.43 J <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR
04/06/16 NS NS NS NS NS NS NS NS NR NS NR NS NS NS NS NS NS NS NS NS NS
DW-3
WSW-6
WSW-3
WSW-5
WSW-4
Page 7 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR
04/06/16 NS NS NS NS NS NS NS NS NR NS NR NS NS NS NS NS NS NS NS NS NS
09/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 NR NR NR NR NR <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
01/02/20 0.14 J <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 NR *NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/28/15 7,090 24,700 2,830 16,200 436 1,390 NR NR NR NR NR 740 262 2,700 652 NR NR NR NR NR NR
04/06/16 6,390 24,600 2,710 19,300 256 1,170 NR NR NR NR NR 563 236 J 3,040 735 NR NR NR NR NR NR
08/09/16 7,740 25,900 3,080 16,000 453 1,220 NR NR NR NR NR 978 288 2,760 664 NR NR NR NR NR NR
05/03/17 7,060 21,800 2,610 18,100 486 913 NR NR NR NR NR 973 232 2,820 688 NR NR NR NR NR NR
04/19/18 6,400 22,500 2,700 15,100 583 750 NR NR NR NR NR 731 248 2,600 659 NR NR NR NR NR NR
08/13/18 5,410 25,600 3,020 19,300 231 J 875 NR NR NR NR NR 510 284 J 2,930 814 NR NR NR NR NR NR
10/15/18 4,570 24,800 2,710 18,100 184 J 913 NR NR NR NR NR 362 214 J 2,680 650 NR NR NR NR NR NR
01/22/19 1,970 16,300 2,280 16,900 33.6 J 1,040 NR NR NR NR NR 121 180 2,860 685 NR NR NR NR NR NR
04/08/19 1,610 20,400 2,800 20,700 <63 776 NR NR NR NR NR <63 205 J 2,890 757 NR NR NR NR NR NR
07/29/19 3,040 24,600 3,220 18,900 110 J 761 NR NR NR NR NR 204 J 238 J 2,720 685 NR NR NR NR NR NR
10/08/19 3,120 22,800 3,240 17,600 227 J 859 NR NR NR NR NR 287 224 J 2,480 619 NR NR NR NR NR NR
01/02/20 2,340 23,300 3,330 23,400 153 J 862 1,030 J <100 NR * NR 153 J 266 3,080 796 NR NR NR NR NR NR
10/13/20 1,130 3,800 315 2,140 306 221 3,860 54.5 J NR * NR 269 23.1 J 366 76.7 NR NR NR NR NR NR
04/08/21 416 1,820 203 1,510 124 342 1,090 23.8 J <6.3 * <6.3 123 13.3 J 255 50.0 NR NR NR NR NR NR
10/20/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/05/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/14/22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/28/15 10,800 32,600 2,690 14,100 12,100 682 NR NR NR NR NR 3,360 266 J 2,180 558 NR NR NR NR NR NR
04/06/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/09/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/03/17 12,100 38,500 3,570 21,200 9,720 1,300 NR NR NR NR NR 3,230 370 3,520 845 NR NR NR NR NR NR
04/19/18 12,100 43,400 4,900 28,200 11,800 1,590 NR NR NR NR NR 2,920 656 5,490 1,480 NR NR NR NR NR NR
08/13/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/15/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/22/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/11/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/29/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/08/19 7,380 40,000 4,060 21,400 5,110 1,020 NR NR NR NR NR 1,710 282 J 2,810 731 NR NR NR NR NR NR
01/02/20 FP FP FP FP FP FP FP FP NR FP NR FP FP FP FP FP FP FP FP FP FP
10/13/20 6,520 44,500 4,140 24,700 2,460 1,520 9,780 J 533 J NR *NR 1,430 352 J 3,530 883 NR NR NR NR NR NR
04/08/21 4,090 27,200 2,800 21,300 3,610 1,740 8,540 J 519 J <130 *<130 1,370 384 J 4,610 1,200 NR NR NR NR NR NR
10/20/21 722 6,220 1,180 9,310 1,490 1,390 228 J <31 <31 1,250 <31 334 271 3410 809 NR NR NR NR NR NR
04/05/22 6,930 30,300 2,490 19,300 1,030 1,860 <2,000 269 J <130 <2,000 <130 684 224 J 3,540 961 NR NR NR NR NR NR
11/14/22 3,210 24,600 2,270 15,800 1,100 1,480 <190 213 J <16.0 <160 <19.0 358 212 3,110 758 NR NR NR NR NR NR
OW-2
OW-1
WSW-7
WSW-8
Page 8 of 9
Facility ID #: 0-031674
EPA
Method
625
EPA
6010C/
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 0.6 10 0.4 70 70 400 400 30 15 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 NE 10,000 400 70,000 26,100 28,500 24,100 12,000 15,000 NE NE NE NEGCL (mg/l)2-MethylnaphthaleneDi-isopropyl etherAnalytical Method →
Date: 12/12/22
1,2,4-TrimethylbenzeneMAC (mg/l)NaphthaleneTolueneMethyl-tert-butyl ether(MTBE)Total Xylenesn-PropylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
MADEP Methods EPH and VPH
C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsLead1,3,5-TrimethylbenzeneEthylbenzeneBenzeneContaminant of Concern →
EPA 6200B Plus 5 Oxygenates and Ethanol or 601/602 tert-Amyl alcohol(TAA)tert-Amyl methyl ether (TAME)DibromochloromethaneBromodichloromethanetert-Butyl Alcohol(TBA)07/28/15 2,640 15,200 1,410 6,830 <82 416 NR NR NR NR NR <80 122 J 1,080 299 NR NR NR NR NR NR
04/06/16 3,580 27,500 2,660 14,500 <63 795 NR NR NR NR NR 67.7 J 191 J 1,800 423 NR NR NR NR NR NR
08/09/16 3,510 19,700 2,080 11,000 37.9 J 541 NR NR NR NR NR 94.0 J 192 1,800 430 NR NR NR NR NR NR
05/03/17 2,870 17,500 1,740 9,170 38.1 J 560 NR NR NR NR NR 104 186 1,660 435 NR NR NR NR NR NR
AS-2 05/03/17 7,390 22,100 2,390 14,800 1,560 706 NR NR NR NR NR 810 172 2,020 475 NR NR NR NR NR NR
AS-3 05/03/17 1,930 21,500 3,340 21,000 20,800 1,020 NR NR NR NR NR 3,230 322 3,180 750 NR NR NR NR NR NR
AS-4 05/03/17 2,410 7,980 1,370 6,770 130 266 NR NR NR NR NR 209 256 1,770 505 NR NR NR NR NR NR
AS-5 05/03/17 36.7 185 220 2,470 <3.1 334 NR NR NR NR NR <3.1 91.5 1,650 140 NR NR NR NR NR NR
07/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 NR NR NR NR NR <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR
04/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/09/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/19/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
08/13/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/15/18 <0.13 0.13 J <0.13 0.49 J <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 0.14 J <0.13 NR NR NR NR NR NR
01/22/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 NR NR NR NR NR <0.073 <0.22 <0.15 <0.16 NR NR NR NR NR NR
04/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/29/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/08/19 NS NS NS NS NS NS NS NS NR NS NR NS NS NS NS NS NS NS NS NS NS
01/02/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/14/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
07/23/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/13/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/08/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
10/20/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
04/05/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 NR <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/14/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.160 NR <0.190 <0.500 <0.190 <0.190 <0.180 NR NR NR NR NR NR
Notes:
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum allowable concentrations, specified in T15A NCAC 2L.0202.
• For other compounds reported that did not exceed the MACs, refer to the laboratory reports.
• Concentrations in bold exceeded MACs; concentrations in bold and italics exceeded the GCLs.
• GCL: Gross contamination level.
• Other contaminant concentrations that exceeded the MACs are as follows: 05/20/13 - isopropylbenzene, styrene and/or tetrachloroethylene in MW-1R, MW-3, MW-8 and MW-10; 07/29/15 - isopropylbenzene, methylene chloride, styrene
and/or tetrachloroethylene in MW-1R, MW-9 and OW-1; 04/06/16 - isopropylbenzene, styrene, tetrachloroethylene, dibromochloromethane and/or 1,1,2,2-tetrachloroethane in MW-1R, MW-8, MW-9, OW-1, DW-2,WSW-4 and WSW-5;
08/09/16 - isopropylbenzene, methylene chloride and/or styrene in MW-1R, AS-1 and OW-1; 05/03/17 - PCE, isopropylbenzene, styrene and/or hexachlorobutadiene in MW-1R, AS-3 and/or OW-2; 04/19/18 - PCE, isopropylbenzene, styrene
and/or n-butylbenzene in MW-1R and/or OW-2; 08/13/18 - PCE in MW-9; 10/15/18 - methylene chloride and/or PCE in MW-8, MW-9, DW-1, DW-2 and/or OW-1; 01/22/19 - methylene chloride in MW-1R, DW-1, DW-2 and OW-1, styrene in
OW-1; 07/29/19 - o-chlorotoluene, isopropylbenzene and/or methylene chloride in MW-3, DW-1 and/or OW-1; 10/08/19 - isopropylbenzene in (MW-3); bromodichloromethane, dibromochloromethane and methyl chloride in WSW-3;
01/02/20 - n-buytlbenzene, isopropylbenzene and p-isopropyltoluene in MW-3; tert-butyl alcohol in MW-4; 10/13/20 - methylene chloride and styrene in OW-2.
• FP: Free Product.
• NS: Not Sampled.
• NR: Not Requested.
• *: For laboratory results from prior events, please refer to previous laboratory reports.
TRIP BLANK
• Results reported in µg/l.
AS-1
Page 9 of 9
Facility ID # : 0-031674
Date Travel Site
Purpose of
Maintenance Visit
(Scheduled or
Unscheduled)
O&M
(hrs.)
Hour Meter
Reading
Upon
Arrival
Hour Meter
Reading
Upon
Departure
10/13/2022 09:45-10:30
13:15-16:00 10:30-13:15 Scheduled 2.75
AS: 23,096
SVE: 32,586
AS: 23,098
SVE: 32,588
10/24/2022 10:15-12:15
14:30-17:15 12:15-14:30 Scheduled 2.25
AS: 23,361
SVE: 32,851
AS: 23,363
SVE: 32,853
5.00
Note:
TABLE 7
SUMMARY OF REMEDIATION SYSTEM O&M VISITS
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 12/12/22
Description of Maintance Activities
AS: 267 SVE: 267
• Operation and Maintenance (hrs.) includes only time spent onsite.
Restarted system, collected system readings, checked oil
levels, and collected air sample
Restarted system, collected system readings, checked oil
levels, and collected air sample
Total (hrs) Total Operational Hours
Page 1 of 1
0-031674
Benzene Toluene Ethylbenzene Xylenes MTBE Total BTEX TPH
02/20/2018 3.7 16.6 3.3 11.3 5.2 34.9 867
03/26/2018 5.0 46.3 5.8 25.6 0.74 82.70 486
04/19/2018 3.5 43.2 5.9 27.3 0.47 J 79.90 454
05/29/2018 <0.10 <0.10 <0.10 <0.30 <0.15 <0.60 <2.4
06/25/2018 1.6 21.0 3.4 16.4 0.40 J 42.4 251
08/13/2018 2.3 25.7 4.7 25.0 1.20 57.70 366
08/23/2018 2.2 23.1 4.3 22.2 NR 51.80 NR
09/19/2018 2.2 22.5 4.1 22.0 NR 50.80 NR
10/29/2018+1.8 25.1 5.0 26.2 0.56 58.10 316
11/20/2018 1.4 27.2 5.7 31.0 0.34 65.30 357
12/03/2018 1.2 21.0 4.2 22.7 <0.15 49.10 283
01/22/2019 0.6 16.5 3.6 20.2 <0.15 40.88 259
02/28/2019 0.51 15.6 3.5 19.2 <0.15 38.81 246
03/11/2019 0.52 15.9 3.4 18.9 <0.15 38.72 230
04/08/2019 0.60 17.5 3.8 21.7 <0.15 43.60 267
05/20/2019 0.61 14.8 3.2 18.3 <0.15 36.91 212
06/10/2019 0.66 13.2 2.9 16.9 NR 33.66 NR
07/29/2019 0.34 10.0 2.5 15.0 <0.15 27.84 188
08/13/2019 0.50 8.3 1.7 8.6 <0.0087 19.10 116
09/09/2019 <0.10 12.6 2.2 14.0 <0.15 28.80 204
10/08/2019 <0.10 11.9 2.2 14.6 <0.15 28.70 192
12/11/2019 <0.10 9.2 1.6 11.1 NR 21.90 NR
01/02/2020 <0.10 11.0 2.4 15.5 <0.15 28.90 206
03/03/2020 <0.50 7.5 2.8 15.3 <0.50 25.60 156
04/14/2020 2.0 13.2 3.1 17.0 <0.50 35.30 252
05/19/2020 <0.10 3.8 1.5 7.5 <0.15 12.80 103
07/23/2020 <0.10 1.8 1.4 9.4 <0.15 12.60 120
08/18/2020 <0.10 1.5 1.4 9.6 <0.15 12.50 98.1
09/17/2020 <0.10 1.2 1.1 7.7 <0.15 10.00 82.1
10/13/2020 <0.10 1.8 1.1 7.6 <0.15 10.50 112
12/02/2020 <0.10 1.7 0.90 6.5 <0.15 9.10 101
12/16/2020 <0.10 1.7 0.85 6.0 <0.15 8.55 74.0
01/15/2021 <0.10 1.7 0.87 6.5 <0.15 9.07 82.1
02/11/2021 <0.10 1.5 0.78 5.9 <0.15 8.18 67.0
03/04/2021 <0.10 1.3 0.74 5.7 <0.15 7.74 70.2
04/08/2021 <0.10 1.1 0.60 4.3 <0.15 6.00 57.3
08/23/2021 <0.10 1.3 0.65 4.4 <0.15 6.35 70.4
09/07/2021 <0.10 1.5 0.69 4.5 <0.15 6.69 68.0
10/20/2021 <0.10 2.4 0.86 5.8 <0.15 9.06 80.4
11/04/2021 <0.10 2.2 0.74 4.9 <0.15 7.84 66.0
12/16/2021 <0.10 <0.10 <0.10 <0.30 <0.15 <0.75 <2.4
06/21/2022 <0.010 0.20 0.053 0.67 <0.0087 0.92 33.1
08/25/2022 <0.010 0.26 0.067 0.72 <0.0087 1.05 11.1
10/13/2022 <0.010 0.46 <0.10 <0.30 <0.15 0.46 16.5
10/24/2022 <0.010 0.48 <0.10 <0.30 <0.15 0.48 15.2
Notes:
• Results reported in ppmv (parts per million volume).
• *Air samples collected from the exhaust of the vacuum blower may be named differently in the lab report.
• <: Less than the method detection limit specified in the laboratory report.
• +Air sample was collected on 11/20/18 and date was mislabeled on chain-of-custody.
• NR: Not Reported.
Well No.Sample Date
(mm/dd/yy)
EPA METHOD TO-3
SVE AIR
EXHAUST*
TABLE 8
SUMMARY OF AIR ANALYTICAL RESULTS
HANDY STOP #7 (INCIDENT NO. 36069)
Date: 12/12/22 Facility ID #:
Parge 1 of 1

APPENDICES

APPENDIX A
State Correspondence

October 6, 2022 Shell Brothers Distributing, Inc.
451 Eugene Street, Apt 2T Greensboro, North Carolina 27401 Attention: Gail Williams
Re: Acknowledgement of Receipt/ Corrective Action Performance Report Handy Stop #7 1500 Rock Barn Road, Conover Catawba County Incident Number: 36069 Risk Classification: High Dear Ms. Williams: On September 30, 2022, the Underground Storage Tank Section of the Division of Waste Management, Mooresville Regional Office, received the Corrective Action Performance Report for the above-referenced site. The reports have been reviewed and will remain in the UST Section’s files. The next groundwater sampling event should be scheduled for November 2022. The Corrective Action Performance Report must be received by this office no later than December 31, 2022. If you have any questions, please contact me at the address or telephone number listed below. Sincerely,
Brad C. Newton, P.G. Hydrogeologist Mooresville Regional Office
UST Section, Division of Waste Management, NCDENR cc: Joanna Alley – Geological Resources, Inc. (via e-mail)
Catawba County Health Department
Site Name City / County /Catawba Incident #36069
Resp Pty Name / Contact Incident Mgr Region MORRP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #59
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:60 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I210A RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 15 /wells y $110.00 y $1,650.00 $1,650.00 /
4.090 #240 15 /samples y $94.00 y $1,410.00 $1,410.00 /
4.090 #272 1 /sample y $66.00 y $66.00 $66.00 /
4.090 #880 3 /samples y $151.00 y $453.00 $453.00 /
4.091 3 /shipments y $60.00 y $180.00 $180.00 /
6.090 1 /report y $1,125.00 n $1,125.00 $0.00 /
6.106 1 /report y $1,125.00 y $1,125.00 $1,125.00 /
7.201 15 /hours y $93.00 y $1,395.00 $1,395.00 /
7.250 1 /system y $2,000.00 y $2,000.00 $2,000.00 /
7.260 1 /system y $3,300.00 y $3,300.00 $3,300.00 /
12.050 3 /trips y $250.00 y $750.00 $750.00 /
12.055 3 /trips y $50.00 y $150.00 $150.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$13,604.00 $12,479.00 TOTAL:
Total Standard Costs (Not Third Party)$13,604.00 $12,479.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty CostsProcess Tracking (Date)
TA Submittal:9/27/22 by:(PM)(Reserved for RO)
RO Review:9/27/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 9/30/2022
CO Review:9/30/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/costnegotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RPis not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
Conover
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010 (Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Handy Stop 7
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA requestdesignated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12months ofthe completion date of the FIRST completed task to remain within the Statute ofLimitations.All ePATAs submitted withina claim areclosed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimedamount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
bcn
HB
(Initials)
JRA
Proposed
Units / Type
(Consultant)
Brad Newton
YES22-639 Sep - Nov 2022
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
[e-mail]
Shell Brothers Gail Williams
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
Task 6.090 not eligible for reimbursement for sites with mechanical remedial systems in operation
10/13/22

APPENDIX B
Land Use Information
Date: 12/12/22 Facility ID # : 0-031674
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a O-I Office-Institutional n/a n/a
n/a M-1 General Manufacturing n/a n/a
n/a R-20 Residential Genera n/a n/a
n/a B-4 General Business n/a n/a
n/a B-2 Highway Business n/a n/a
Note:
• Properties are keyed to Figure 3A.
APPENDIX B
LAND USE INFORMATION
HANDY STOP #7 (INCIDENT NO. 36069)
Page 1 of 1

APPENDIX C
Incident Reports
NCDEQ Incident Report
RP/Company SHELL BROTHERS DISTRIBUTING
RPAddress 241 1ST AVE DR SE
RPCity TAYLORSVILLE
Contact GAIL SHELL WILLIAMS
RPState NC
TELEPHONE [phone]
IncidentNumber 36069 USTNum MO-7402
IncidentName HANDY STOP NO. 7
FacilID 00-0-0000031674
Address 1500 ROCK BARN ROAD
CityTown CONOVER State NC
ZipCode
DateOccurred 3 /14/2006
DateReported 4 /25/2006
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr BCNLongitude-81.184286 Latitude 35.722272
County CATAW
SCH 7/21/2006 7/28/2006 10/26/2006
LSA2 11/16/2006 11/29/2006 11/30/2006
CSAM 7/25/2008 8/7/2008 8/7/2008
FPRI 11/19/2008 12/11/2008 12/11/2008
CAP 9/29/2009 10/15/2009 10/15/2009
Thursday, May 5, 2022 Page 1 of 4
RMR 11/3/2011 11/22/2011 11/22/2011
FPRS 3/4/2015 4/1/2015 4/1/2015
MRP 8/31/2015 9/29/2015 9/29/2015
MRP 5/27/2016 6/1/2016 6/1/2016
MRP 8/31/2016 9/12/2016 9/12/2016
RMR 7/5/2018 7/19/2018 7/19/2018
INCORRECT. UNABLE TO CORRECT DATABASE.
RMR 8/20/2018 9/5/2018 9/5/2018
RMR 10/26/2018 11/1/2018 11/1/2018
gw monitioring report approved. Capr forwarded to scott ryals.
RMR 12/31/2018 1/17/2019 1/17/2019
CAPR 3/27/2019 4/2/2019 4/2/2019
this report should not be approved per SCR it was not PE stamped. RUST
will not allow deletion of approval date.
Thursday, May 5, 2022 Page 2 of 4
RMR 3/27/2019 4/2/2019 4/2/2019
MRP 9/3/2019 9/11/2019 9/11/2019
RMR 12/9/2019 12/17/2019 12/17/2019
MRP 3/2/2020 3/13/2020 3/16/2020
LET 5/5/2020 5/18/2020 5/18/2020
CAPR 5/27/2020 6/1/2020 6/1/2020
approved by scott ryals, stf branch
LET 8/17/2020 8/31/2020 8/31/2020
CAPR 9/11/2020 9/24/2020 9/24/2020
CAPR 12/3/2020 12/10/2020 12/10/2020
MRP 12/3/2020 12/29/2020 12/29/2020
Thursday, May 5, 2022 Page 3 of 4
LET 1/27/2021 2/10/2021 2/10/2021
CAPR 2/18/2021 3/3/2021 3/3/2021
FPRS 2/18/2021 3/3/2021 3/3/2021
CAPR 5/25/2021 6/7/2021 6/7/2021
MRP 5/25/2021 6/7/2021 6/7/2021
LET 8/11/2021 8/12/2021 8/12/2021
CAPR 8/27/2021 9/10/2021 9/10/2021
MRP 12/17/2021 1/4/2021 1/4/2021
CAPR 12/17/2021 1/4/2021 1/4/2021
CAPR 2/21/2022 2/28/2022 2/28/2022
Thursday, May 5, 2022 Page 4 of 4
NCDEQ Incident Information
RP/Company NLS CARRIER CORP Contact
RPAddress 109 WHITE OAK LANE, SUITE 7
RPCity OLD BRIDGE
RPZipCode 08857-
RPState NJ
TELEPHONE [phone]
IncidentNumber 91567
IncidentName NLS CARRIERS DIESEL SPILL
Address I-40 EAST, EXIT 133
CityTown CONOVER State NC
County CATAWZipCode
Lattitude 35.721066 Longitude -81.185174
COMMENT
DateOccurred 1 /27/2020
DateReported 1 /28/2020
CloseOut
FacilID USTNum MO-88772
Mgr BCN
Conf Risk
Site Priority
Tuesday, December 14, 2021 Page 1 of 1
NCDEQ Incident Information
RP/Company STEVENS TRANSPORT Contact
RPAddress 9757 MILITARY PARKWAY
RPCity DALLAS
RPZipCode 75227-
RPState TX
TELEPHONE
IncidentNumber 95863
IncidentName STEVENS TRANSPORT DIESEL SPILL
Address ROCK BARN ROAD & I-40
CityTown CONOVER State
County CATAWZipCode
Lattitude 35.721767 Longitude -81.185766
COMMENT
NFA required at this site, but NFA letter not issued as the RP information was not submitted.
DateOccurred 8 /25/2020
DateReported 9 /25/2020
CloseOut
FacilID USTNum MO-88804
Mgr BCN
Conf Risk
Site Priority
Tuesday, December 14, 2021 Page 1 of 1

APPENDIX D
Historical Soil Quality Information

APPENDIX E
Laboratory Analytical Reports
10/18/22
Technical Report for
GRI (Geological Resources Inc.)
Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
36069/3067
SGS Job Number: FA99703
Sampling Date: 10/13/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: Corey Buchanan
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 10/18/22
e-Hardcopy 2.0
Automated Report
13
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 13
FA99703
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA99703-1: AIR ...........................................................................................................6
Section 4: Misc. Forms ............................................................................................................7
4.1: Chain of Custody ...........................................................................................................8
Section 5: GC Volatiles - QC Data Summaries .....................................................................10
5.1: Method Blank Summary ................................................................................................11
5.2: Blank Spike Summary ...................................................................................................12
5.3: Duplicate Summary .......................................................................................................13 123452 of 13
FA99703
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA99703
Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Project No: 36069/3067
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA99703-1 10/13/22 13:15 JB 10/14/22 AIR Air AIR
3 of 13
FA997031
Summary of Hits Page 1 of 1
Job Number:FA99703
Account:GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Collected:10/13/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA99703-1 AIR
Toluene 0.46 J 0.50 0.10 ppmv EPA TO-3
TPH as Equiv Pentane 16.5 5.0 2.4 ppmv EPA TO-3
Toluene 1.7 J 1.9 0.38 mg/m3 EPA TO-3
TPH as Equiv Pentane 48.6 15 7.1 mg/m3 EPA TO-3
4 of 13
FA997032
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 13
FA997033
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:AIR
Lab Sample ID:FA99703-1 Date Sampled:10/13/22
Matrix:AIR - Air Date Received:10/14/22
Method:EPA TO-3 Percent Solids:n/a
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 HH064161.D 1 10/14/22 12:57 TD n/a n/a GHH3934
Run #2
Initial Volume
Run #1 0.50 ml
Run #2
Purgeable Aromatics
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
71-43-2 78.11 Benzene ND 0.50 0.10 ppmv ND 1.6 0.32 mg/m3
108-88-3 92.14 Toluene 0.46 0.50 0.10 ppmv J 1.7 1.9 0.38 mg/m3
100-41-4 106.2 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 0.43 mg/m3
1330-20-7 106.2 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 1.3 mg/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3
72 TPH as Equiv Pentane 16.5 5.0 2.4 ppmv 48.6 15 7.1 mg/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 120%54-142%
460-00-4 4-Bromofluorobenzene 110%54-142%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 13
FA9970333.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
7 of 13
FA997034
FA99703: Chain of Custody
Page 1 of 2
8 of 13
FA9970344.1
Job Number:FA99703 Client:GEOLOGICAL RESOURCES INC
Date / Time Received:10/14/2022 9:30:00 AM Delivery Method:FX
Project:HANDY STOP #7
Airbill #'s:100963798905
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
N/A
N/A
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:Therm CF:# of Coolers:N/A
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:ZANEB Date:Date:10/14/2022 9:30:00 A
FA99703: Chain of Custody
Page 2 of 2
9 of 13
FA9970344.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
10 of 13
FA997035
Method Blank Summary Page 1 of 1
Job Number:FA99703
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH3934-MB HH064156.D 1 10/14/22 TD n/a n/a GHH3934
The QC reported here applies to the following samples:Method: EPA TO-3
FA99703-1
CAS No.Compound Result RL MDL Units Q Result RL Units
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 mg/m3
71-43-2 Benzene ND 0.50 0.10 ppmv ND 1.6 mg/m3
108-88-3 Toluene ND 0.50 0.10 ppmv ND 1.9 mg/m3
100-41-4 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 mg/m3
1330-20-7 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 mg/m3
TPH as Equiv Pentane ND 5.0 2.4 ppmv ND 15 mg/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 127%54-142%
460-00-4 4-Bromofluorobenzene 122%54-142%
11 of 13
FA9970355.1.1
Blank Spike Summary Page 1 of 1
Job Number:FA99703
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH3934-BS HH064155.D 1 10/14/22 TD n/a n/a GHH3934
The QC reported here applies to the following samples:Method: EPA TO-3
FA99703-1
Spike BSP BSP
CAS No.Compound ppmv ppmv %Limits
1634-04-4 Methyl Tert Butyl Ether 10 8.5 85 60-111
71-43-2 Benzene 10 9.4 94 64-111
108-88-3 Toluene 10 10.1 101 60-112
100-41-4 Ethylbenzene 10 10.8 108 59-112
1330-20-7 Xylenes (total)30 32.9 110 58-110
TPH as Equiv Pentane 135 143 106 66-116
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 126%54-142%
460-00-4 4-Bromofluorobenzene 125%54-142%
* = Outside of Control Limits.
12 of 13
FA9970355.2.1
Duplicate Summary Page 1 of 1
Job Number:FA99703
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA99683-3DUP HH064160.D 1 10/14/22 TD n/a n/a GHH3934
FA99683-3 HH064159.D 1 10/14/22 TD n/a n/a GHH3934
The QC reported here applies to the following samples:Method: EPA TO-3
FA99703-1
FA99683-3 DUP
CAS No.Compound ppmv Q ppmv Q RPD Limits
1634-04-4 Methyl Tert Butyl Ether 0.50 U ND nc 10
71-43-2 Benzene 0.50 U ND nc 11
108-88-3 Toluene 0.50 U ND nc 14
100-41-4 Ethylbenzene 0.50 U ND nc 13
1330-20-7 Xylenes (total)1.5 U ND nc 15
TPH as Equiv Pentane 5.0 U ND nc 28
CAS No.Surrogate Recoveries DUP FA99683-3 Limits
460-00-4 4-Bromofluorobenzene 118%119%54-142%
460-00-4 4-Bromofluorobenzene 112%114%54-142%
* = Outside of Control Limits.
13 of 13
FA9970355.3.1
11/01/22
Technical Report for
GRI (Geological Resources Inc.)
Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
36069/3067
SGS Job Number: FC2
Sampling Date: 10/24/22
Report to:
[e-mail]
[e-mail]
ATTN: Distribution6
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 11/01/22
e-Hardcopy 2.0
Automated Report
13
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 13
FC2
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FC2-1: AIR ...................................................................................................................6
Section 4: Misc. Forms ............................................................................................................7
4.1: Chain of Custody ...........................................................................................................8
Section 5: GC Volatiles - QC Data Summaries .....................................................................10
5.1: Method Blank Summary ................................................................................................11
5.2: Blank Spike Summary ...................................................................................................12
5.3: Duplicate Summary .......................................................................................................13 123452 of 13
FC2
SGS LabLink@13:34 01-Nov-2022
Sample Summary
GRI (Geological Resources Inc.)
Job No:FC2
Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Project No: 36069/3067
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC2-1 10/24/22 14:30 JB 10/25/22 AIR Air AIR
3 of 13
FC21
Summary of Hits Page 1 of 1
Job Number:FC2
Account:GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Collected:10/24/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC2-1 AIR
Toluene 0.48 J 0.50 0.10 ppmv EPA TO-3
TPH as Equiv Pentane 15.2 5.0 2.4 ppmv EPA TO-3
Toluene 1.8 J 1.9 0.38 mg/m3 EPA TO-3
TPH as Equiv Pentane 44.8 15 7.1 mg/m3 EPA TO-3
4 of 13
FC22
SGS LabLink@13:34 01-Nov-2022
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 13
FC23
SGS LabLink@13:34 01-Nov-2022
Report of Analysis Page 1 of 1
Client Sample ID:AIR
Lab Sample ID:FC2-1 Date Sampled:10/24/22
Matrix:AIR - Air Date Received:10/25/22
Method:EPA TO-3 Percent Solids:n/a
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 HH064182.D 1 10/25/22 15:38 JR n/a n/a GHH3936
Run #2
Initial Volume
Run #1 0.50 ml
Run #2
Purgeable Aromatics
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
71-43-2 78.11 Benzene ND 0.50 0.10 ppmv ND 1.6 0.32 mg/m3
108-88-3 92.14 Toluene 0.48 0.50 0.10 ppmv J 1.8 1.9 0.38 mg/m3
100-41-4 106.2 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 0.43 mg/m3
1330-20-7 106.2 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 1.3 mg/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 0.54 mg/m3
72 TPH as Equiv Pentane 15.2 5.0 2.4 ppmv 44.8 15 7.1 mg/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 114%54-142%
460-00-4 4-Bromofluorobenzene 107%54-142%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 13
FC233.1
SGS LabLink@13:34 01-Nov-2022
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
7 of 13
FC24
FC2: Chain of Custody
Page 1 of 2
8 of 13
FC244.1
Job Number:FC2 Client:GRI
Date / Time Received:10/25/2022 9:00:00 AM Delivery Method:FEDEX
Project:HANDY STOP #7
Airbill #'s:1009 6379 9588
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
N/A
N/A
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:Therm CF:# of Coolers:N/A
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SAMUELM Date:Date:10/25/2022 9:00:00 A
FC2: Chain of Custody
Page 2 of 2
9 of 13
FC244.1
SGS LabLink@13:34 01-Nov-2022
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
10 of 13
FC25
Method Blank Summary Page 1 of 1
Job Number:FC2
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH3936-MB HH064180.D 1 10/25/22 JR n/a n/a GHH3936
The QC reported here applies to the following samples:Method: EPA TO-3
FC2-1
CAS No.Compound Result RL MDL Units Q Result RL Units
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.15 ppmv ND 1.8 mg/m3
71-43-2 Benzene ND 0.50 0.10 ppmv ND 1.6 mg/m3
108-88-3 Toluene ND 0.50 0.10 ppmv ND 1.9 mg/m3
100-41-4 Ethylbenzene ND 0.50 0.10 ppmv ND 2.2 mg/m3
1330-20-7 Xylenes (total)ND 1.5 0.30 ppmv ND 6.5 mg/m3
TPH as Equiv Pentane ND 5.0 2.4 ppmv ND 15 mg/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 120%54-142%
460-00-4 4-Bromofluorobenzene 111%54-142%
11 of 13
FC255.1.1
Blank Spike Summary Page 1 of 1
Job Number:FC2
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GHH3936-BS HH064179.D 1 10/25/22 JR n/a n/a GHH3936
The QC reported here applies to the following samples:Method: EPA TO-3
FC2-1
Spike BSP BSP
CAS No.Compound ppmv ppmv %Limits
1634-04-4 Methyl Tert Butyl Ether 10 8.2 82 60-111
71-43-2 Benzene 10 8.8 88 64-111
108-88-3 Toluene 10 9.4 94 60-112
100-41-4 Ethylbenzene 10 9.9 99 59-112
1330-20-7 Xylenes (total)30 29.9 100 58-110
TPH as Equiv Pentane 135 134 99 66-116
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 115%54-142%
460-00-4 4-Bromofluorobenzene 115%54-142%
* = Outside of Control Limits.
12 of 13
FC255.2.1
Duplicate Summary Page 1 of 1
Job Number:FC2
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handy Stop 7; 1500 Rock Barn Rd, Conover, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2-1DUP HH064181.D 1 10/25/22 JR n/a n/a GHH3936
FC2-1 HH064182.D 1 10/25/22 JR n/a n/a GHH3936
The QC reported here applies to the following samples:Method: EPA TO-3
FC2-1
FC2-1 DUP
CAS No.Compound ppmv Q ppmv Q RPD Limits
1634-04-4 Methyl Tert Butyl Ether ND ND nc 10
71-43-2 Benzene ND ND nc 11
108-88-3 Toluene 0.48 J 0.48 J 0 14
100-41-4 Ethylbenzene ND ND nc 13
1330-20-7 Xylenes (total)ND ND nc 15
TPH as Equiv Pentane 15.2 14.2 7 28
CAS No.Surrogate Recoveries DUP FC2-1 Limits
460-00-4 4-Bromofluorobenzene 118%114%54-142%
460-00-4 4-Bromofluorobenzene 110%107%54-142%
* = Outside of Control Limits.
13 of 13
FC255.3.1

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/23/2022
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 22-320-0043 Client Project Description: Handy Stop #7
GRI #3067
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/16/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 87
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-320-0043
Page 2 of 87
Report Number:
Sample Summary Table
Client Project Description:
22-320-0043
Handy Stop #7
GRI #3067
Lab No Client Sample ID Matrix Date Collected Date Received
11/14/2022 12:53Aqueous 93367 MW-1R 11/16/2022 15:45
11/14/2022 11:09Aqueous 93368 MW-2 11/16/2022 15:45
11/14/2022 12:15Aqueous 93369 MW-3 11/16/2022 15:45
11/14/2022 12:30Aqueous 93370 MW-4 11/16/2022 15:45
11/14/2022 11:20Aqueous 93371 MW-5 11/16/2022 15:45
11/14/2022 10:56Aqueous 93372 MW-6 11/16/2022 15:45
11/14/2022 10:38Aqueous 93373 MW-7 11/16/2022 15:45
11/14/2022 13:07Aqueous 93374 MW-8 11/16/2022 15:45
11/14/2022 10:30Aqueous 93375 MW-9 11/16/2022 15:45
11/14/2022 10:42Aqueous 93376 MW-10 11/16/2022 15:45
11/14/2022 13:50Aqueous 93377 DW-1 11/16/2022 15:45
11/14/2022 13:31Aqueous 93378 DW-3 11/16/2022 15:45
11/14/2022 12:43Aqueous 93379 OW-2 11/16/2022 15:45
11/14/2022 08:30Aqueous 93380 Trip Blanks 11/16/2022 15:45
Page 3 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-320-0043
Report Limit
Project:Handy Stop #7
V 93367MW-1R
14.2 11/19/2022 21:066200BAcetoneµg/L 1.80
16.4 11/19/2022 21:066200BBenzeneµg/L 0.180
99.7 11/19/2022 21:066200BDi-Isopropyl Ether (DIPE)µg/L 0.500
19.1 11/19/2022 21:066200BEthylbenzeneµg/L 0.170
10.2 11/19/2022 21:066200B2-Hexanone µg/L 0.380
0.643 11/19/2022 21:066200BIsopropylbenzeneµg/L 0.180
6.33 11/19/2022 21:066200BMethyl Ethyl Ketone (MEK)µg/L 0.710
677 11/21/2022 23:216200BMethyl tert-butyl ether (MTBE)µg/L 14.0
15.2 11/19/2022 21:066200BNaphthaleneµg/L 0.470
1.08 11/19/2022 21:066200Bn-Propylbenzene µg/L 0.190
287 11/21/2022 23:216200Btert-Butyl Alcohol (TBA)µg/L 160
J38711/21/2022 23:216200Btert-Amyl Alcohol (TAA)µg/L 190
67.1 11/19/2022 21:066200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
177 11/21/2022 23:216200BTolueneµg/L 22.0
34.5 11/19/2022 21:066200B1,2,4-Trimethylbenzene µg/L 0.190
19.7 11/19/2022 21:066200B1,3,5-Trimethylbenzene µg/L 0.180
185 11/21/2022 23:216200Bo-Xylene µg/L 21.0
123 11/19/2022 21:066200Bm,p-Xylene µg/L 0.420
308 11/19/2022 21:066200BXylene (Total)µg/L 0.420
V 93369MW-3
18.8 11/19/2022 22:006200BAcetoneµg/L 1.80
5.26 11/19/2022 22:006200BDi-Isopropyl Ether (DIPE)µg/L 0.500
41.0 11/19/2022 22:006200BEthylbenzeneµg/L 0.170
15.8 11/19/2022 22:006200BIsopropylbenzeneµg/L 0.180
19.3 11/19/2022 22:006200BMethyl tert-butyl ether (MTBE)µg/L 0.140
28.9 11/19/2022 22:006200BNaphthaleneµg/L 0.470
19.8 11/19/2022 22:006200Bn-Propylbenzene µg/L 0.190
18.8 11/19/2022 22:006200Btert-Butyl Alcohol (TBA)µg/L 1.60
14.8 11/19/2022 22:006200BTolueneµg/L 0.220
215 11/21/2022 17:576200B1,2,4-Trimethylbenzene µg/L 1.90
77.2 11/19/2022 22:006200B1,3,5-Trimethylbenzene µg/L 0.180
95.1 11/19/2022 22:006200Bo-Xylene µg/L 0.210
193 11/19/2022 22:006200Bm,p-Xylene µg/L 0.420
288 11/19/2022 22:006200BXylene (Total)µg/L 0.210
V 93370MW-4
J0.312 11/19/2022 22:276200BBenzeneµg/L 0.180
Page 4 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-320-0043
Report Limit
Project:Handy Stop #7
V 93370MW-4
10.4 11/19/2022 22:276200BDi-Isopropyl Ether (DIPE)µg/L 0.500
4.05 11/19/2022 22:276200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J40011/21/2022 22:276200Btert-Butyl Alcohol (TBA)µg/L 160
J85911/21/2022 22:276200Btert-Amyl Alcohol (TAA)µg/L 190
J0.397 11/19/2022 22:276200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
0.517 11/19/2022 22:276200B1,2,4-Trimethylbenzene µg/L 0.190
1.01 11/19/2022 22:276200B1,3,5-Trimethylbenzene µg/L 0.180
0.728 11/19/2022 22:276200Bo-Xylene µg/L 0.210
0.728 11/19/2022 22:276200BXylene (Total)µg/L 0.210
V 93373MW-7
2.07 11/19/2022 23:496200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J0.335 11/19/2022 23:496200BTolueneµg/L 0.220
V 93374MW-8
0.561 11/20/2022 00:166200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.371 11/20/2022 00:166200B1,3,5-Trimethylbenzene µg/L 0.180
V 93377DW-1
J0.260 11/20/2022 01:376200BBenzeneµg/L 0.180
82.7 11/20/2022 01:376200BDi-Isopropyl Ether (DIPE)µg/L 0.500
217 11/21/2022 18:246200BMethyl tert-butyl ether (MTBE)µg/L 1.40
22.5 11/20/2022 01:376200Btert-Butyl Alcohol (TBA)µg/L 1.60
13.5 11/20/2022 01:376200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
J0.474 11/20/2022 01:376200BTolueneµg/L 0.220
J0.464 11/20/2022 01:376200Bm,p-Xylene µg/L 0.420
J0.464 11/20/2022 01:376200BXylene (Total)µg/L 0.210
V 93378DW-3
350 11/21/2022 22:546200BBenzeneµg/L 18.0
2.94 11/20/2022 02:046200Bn-Butylbenzene µg/L 0.180
0.831 11/20/2022 02:046200Bsec-Butyl benzene µg/L 0.200
2.32 11/20/2022 02:046200BChloroformµg/L 0.220
62.0 11/20/2022 02:046200BDi-Isopropyl Ether (DIPE)µg/L 0.500
0.861 11/20/2022 02:046200BEthylbenzeneµg/L 0.170
9.96 11/20/2022 02:046200BIsopropylbenzeneµg/L 0.180
144 11/21/2022 22:546200BMethyl tert-butyl ether (MTBE)µg/L 14.0
5.02 11/20/2022 02:046200BNaphthaleneµg/L 0.470
Page 5 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-320-0043
Report Limit
Project:Handy Stop #7
V 93378DW-3
2.89 11/20/2022 02:046200Bn-Propylbenzene µg/L 0.190
77.6 11/20/2022 02:046200Btert-Butyl Alcohol (TBA)µg/L 1.60
J54911/21/2022 22:546200Btert-Amyl Alcohol (TAA)µg/L 190
J6.92 11/20/2022 02:046200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
1.21 11/20/2022 02:046200BTolueneµg/L 0.220
47.5 11/20/2022 02:046200B1,2,4-Trimethylbenzene µg/L 0.190
5.35 11/20/2022 02:046200B1,3,5-Trimethylbenzene µg/L 0.180
25.6 11/20/2022 02:046200Bo-Xylene µg/L 0.210
101 11/20/2022 02:046200Bm,p-Xylene µg/L 0.420
127 11/20/2022 02:046200BXylene (Total)µg/L 0.210
V 93379OW-2
1100 11/20/2022 02:596200BAcetoneµg/L 180
3210 11/20/2022 02:596200BBenzeneµg/L 18.0
358 11/20/2022 02:596200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2270 11/20/2022 02:596200BEthylbenzeneµg/L 17.0
73.7 11/20/2022 02:596200BIsopropylbenzeneµg/L 18.0
520 11/20/2022 02:596200BMethyl Ethyl Ketone (MEK)µg/L 71.0
1100 11/20/2022 02:596200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1480 11/20/2022 02:596200BNaphthaleneµg/L 47.0
212 11/20/2022 02:596200Bn-Propylbenzene µg/L 19.0
154 11/20/2022 02:596200BStyreneµg/L 22.0
J21311/20/2022 02:596200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
24600 11/22/2022 01:106200BTolueneµg/L 220
3110 11/20/2022 02:596200B1,2,4-Trimethylbenzene µg/L 19.0
758 11/20/2022 02:596200B1,3,5-Trimethylbenzene µg/L 18.0
5390 11/20/2022 02:596200Bo-Xylene µg/L 21.0
10400 11/20/2022 02:596200Bm,p-Xylene µg/L 42.0
15800 11/20/2022 02:596200BXylene (Total)µg/L 21.0
Page 6 of 87

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Handy Stop #7 Lab Report Number: 22-320-0043
Date: 11/23/2022
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Vinyl acetate QC Batch No: V26806/V26696
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.

Page 7 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-1R
93367 Matrix:
11/14/2022 12:53
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 21:06 6200BENM
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/21/22 23:21100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-1R
93367 Matrix:
11/14/2022 12:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
14.2 µg/L 1.80 10.0Acetone 1 11/19/22 21:06 V26697ENM
16.4 µg/L 0.180 0.500Benzene 1 11/19/22 21:06 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 21:06 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 21:06 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 21:06 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 21:06 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 21:06 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 21:06 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 21:06 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 21:06 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 21:06 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 21:06 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 21:06 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 21:06 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 21:06 V26697ENM
99.7 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 21:06 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 21:06 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 21:06 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-1R
93367 Matrix:
11/14/2022 12:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 21:06 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 21:06 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 21:06 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 21:06 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 21:06 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 21:06 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 21:06 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 21:06 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 21:06 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 21:06 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 21:06 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 21:06 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 21:06 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 21:06 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 21:06 V26697ENM
19.1 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 21:06 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 21:06 V26697ENM
10.2 µg/L 0.380 1.002-Hexanone 1 11/19/22 21:06 V26697ENM
0.643 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 21:06 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 21:06 V26697ENM
6.33 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 21:06 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-1R
93367 Matrix:
11/14/2022 12:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
677 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 11/21/22 23:21 V26806MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 21:06 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 21:06 V26697ENM
15.2 µg/L 0.470 1.00Naphthalene 1 11/19/22 21:06 V26697ENM
1.08 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 21:06 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 21:06 V26697ENM
287 µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/21/22 23:21 V26806MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 21:06 V26697ENM
387 J
µg/L 190 1000
tert-Amyl Alcohol (TAA)100 11/21/22 23:21 V26806MSA
67.1 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 21:06 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 21:06 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 21:06 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 21:06 V26697ENM
177 µg/L 22.0 50.0Toluene 100 11/21/22 23:21 V26806MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 21:06 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 21:06 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 21:06 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 21:06 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 21:06 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 21:06 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 21:06 V26697ENM
34.5 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 21:06 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-1R
93367 Matrix:
11/14/2022 12:53
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
19.7 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 21:06 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 21:06 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 21:06 V26697ENM
185 µg/L 21.0 50.0o-Xylene 100 11/21/22 23:21 V26806MSA
123 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 21:06 V26697ENM
308 µg/L 0.420 1.00Xylene (Total)1 11/19/22 21:06 V26806
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.0 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/19/22 21:061 ENM V26697
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%11/21/22 23:21100 MSA V26806
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/21/22 23:21100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-2
93368 Matrix:
11/14/2022 11:09
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 21:33 6200BENM
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: Toluene-d8 98.8 Limits: 70-130%11/19/22 21:331 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-2
93368 Matrix:
11/14/2022 11:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 21:33 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 21:33 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 21:33 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 21:33 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 21:33 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 21:33 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 21:33 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 21:33 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 21:33 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 21:33 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 21:33 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 21:33 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 21:33 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-2
93368 Matrix:
11/14/2022 11:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 21:33 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 21:33 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 21:33 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 21:33 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 21:33 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 21:33 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 21:33 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 21:33 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 21:33 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 21:33 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 21:33 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 21:33 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 21:33 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 21:33 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 21:33 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 21:33 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 21:33 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-2
93368 Matrix:
11/14/2022 11:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 21:33 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 21:33 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 21:33 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 21:33 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 21:33 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/19/22 21:33 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 21:33 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/19/22 21:33 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 21:33 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 21:33 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 21:33 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 21:33 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/19/22 21:33 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 21:33 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 21:33 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 21:33 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 21:33 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 21:33 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 21:33 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 21:33 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-2
93368 Matrix:
11/14/2022 11:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 21:33 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 21:33 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 21:33 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/19/22 21:33 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 21:33 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/19/22 21:33 V26697
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%11/19/22 21:331 ENM V26697
Surrogate: Toluene-d8 98.8 Limits: 70-130%11/19/22 21:331 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-3
93369 Matrix:
11/14/2022 12:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 22:00 6200BENM
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 17:5710 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-3
93369 Matrix:
11/14/2022 12:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
18.8 µg/L 1.80 10.0Acetone 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 22:00 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 22:00 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 22:00 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 22:00 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 22:00 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 22:00 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 22:00 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 22:00 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 22:00 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 22:00 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 22:00 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 22:00 V26697ENM
5.26 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 22:00 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 22:00 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 22:00 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-3
93369 Matrix:
11/14/2022 12:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 22:00 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 22:00 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 22:00 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 22:00 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 22:00 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 22:00 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 22:00 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 22:00 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 22:00 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 22:00 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 22:00 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 22:00 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 22:00 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 22:00 V26697ENM
41.0 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 22:00 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 22:00 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 22:00 V26697ENM
15.8 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 22:00 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 22:00 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 22:00 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-3
93369 Matrix:
11/14/2022 12:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
19.3 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 22:00 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 22:00 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 22:00 V26697ENM
28.9 µg/L 0.470 1.00Naphthalene 1 11/19/22 22:00 V26697ENM
19.8 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 22:00 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 22:00 V26697ENM
18.8 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/19/22 22:00 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 22:00 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/19/22 22:00 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 22:00 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 22:00 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 22:00 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 22:00 V26697ENM
14.8 µg/L 0.220 0.500Toluene 1 11/19/22 22:00 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 22:00 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 22:00 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 22:00 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 22:00 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 22:00 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 22:00 V26697ENM
215 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 11/21/22 17:57 V26806MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-3
93369 Matrix:
11/14/2022 12:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
77.2 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 22:00 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 22:00 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 22:00 V26697ENM
95.1 µg/L 0.210 0.500o-Xylene 1 11/19/22 22:00 V26697ENM
193 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 22:00 V26697ENM
288 µg/L 0.210 0.500Xylene (Total)1 11/19/22 22:00 V26697
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/19/22 22:001 ENM V26697
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%11/21/22 17:5710 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 17:5710 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-4
93370 Matrix:
11/14/2022 12:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 22:27 6200BENM
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 99.4 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-4
93370 Matrix:
11/14/2022 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 22:27 V26697ENM
0.312 J µg/L 0.180 0.500Benzene 1 11/19/22 22:27 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 22:27 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 22:27 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 22:27 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 22:27 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 22:27 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 22:27 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 22:27 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 22:27 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 22:27 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 22:27 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 22:27 V26697ENM
10.4 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 22:27 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 22:27 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 22:27 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-4
93370 Matrix:
11/14/2022 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 22:27 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 22:27 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 22:27 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 22:27 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 22:27 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 22:27 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 22:27 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 22:27 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 22:27 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 22:27 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 22:27 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 22:27 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 22:27 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 22:27 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 22:27 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 22:27 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 22:27 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 22:27 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 22:27 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-4
93370 Matrix:
11/14/2022 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
4.05 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 22:27 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 22:27 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 22:27 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 22:27 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 22:27 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 22:27 V26697ENM
400 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/21/22 22:27 V26806MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 22:27 V26697ENM
859 J
µg/L 190 1000
tert-Amyl Alcohol (TAA)100 11/21/22 22:27 V26806MSA
0.397 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 22:27 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 22:27 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 22:27 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 22:27 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/19/22 22:27 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 22:27 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 22:27 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 22:27 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 22:27 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 22:27 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 22:27 V26697ENM
0.517 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 22:27 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-4
93370 Matrix:
11/14/2022 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
1.01 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 22:27 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 22:27 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 22:27 V26697ENM
0.728 µg/L 0.210 0.500o-Xylene 1 11/19/22 22:27 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 22:27 V26697ENM
0.728 µg/L 0.210 0.500Xylene (Total)1 11/19/22 22:27 V26697
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/19/22 22:271 ENM V26697
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: Dibromofluoromethane 96.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 99.4 Limits: 70-130%11/21/22 22:27100 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 22:27100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-5
93371 Matrix:
11/14/2022 11:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 22:55 6200BENM
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: Dibromofluoromethane 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.2 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-5
93371 Matrix:
11/14/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 22:55 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 22:55 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 22:55 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 22:55 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 22:55 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 22:55 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 22:55 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 22:55 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 22:55 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 22:55 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 22:55 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 22:55 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 22:55 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-5
93371 Matrix:
11/14/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 22:55 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 22:55 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 22:55 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 22:55 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 22:55 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 22:55 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 22:55 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 22:55 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 22:55 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 22:55 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 22:55 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 22:55 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 22:55 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 22:55 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 22:55 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 22:55 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 22:55 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-5
93371 Matrix:
11/14/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 22:55 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 22:55 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 22:55 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 22:55 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 22:55 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/19/22 22:55 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 22:55 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/19/22 22:55 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 22:55 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 22:55 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 22:55 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 22:55 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/19/22 22:55 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 22:55 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 22:55 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 22:55 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 22:55 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 22:55 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 22:55 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 22:55 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-5
93371 Matrix:
11/14/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 22:55 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 22:55 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 22:55 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/19/22 22:55 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 22:55 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/19/22 22:55 V26697
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: Dibromofluoromethane 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 96.2 Limits: 70-130%11/19/22 22:551 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/19/22 22:551 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-6
93372 Matrix:
11/14/2022 10:56
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 23:22 6200BENM
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: Dibromofluoromethane 104 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/19/22 23:221 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-6
93372 Matrix:
11/14/2022 10:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 23:22 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 23:22 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 23:22 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 23:22 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 23:22 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 23:22 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 23:22 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 23:22 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 23:22 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 23:22 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 23:22 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 23:22 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 23:22 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-6
93372 Matrix:
11/14/2022 10:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 23:22 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 23:22 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 23:22 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 23:22 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 23:22 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 23:22 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 23:22 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 23:22 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 23:22 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 23:22 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 23:22 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 23:22 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 23:22 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 23:22 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 23:22 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 23:22 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 23:22 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-6
93372 Matrix:
11/14/2022 10:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 23:22 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 23:22 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 23:22 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 23:22 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 23:22 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/19/22 23:22 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 23:22 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/19/22 23:22 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 23:22 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 23:22 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 23:22 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 23:22 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/19/22 23:22 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 23:22 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 23:22 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 23:22 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 23:22 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 23:22 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 23:22 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 23:22 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-6
93372 Matrix:
11/14/2022 10:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 23:22 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 23:22 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 23:22 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/19/22 23:22 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 23:22 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/19/22 23:22 V26697
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: Dibromofluoromethane 104 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.0 Limits: 70-130%11/19/22 23:221 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/19/22 23:221 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-7
93373 Matrix:
11/14/2022 10:38
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/19/22 23:49 6200BENM
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-7
93373 Matrix:
11/14/2022 10:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 23:49 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 23:49 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 23:49 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 23:49 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 23:49 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 23:49 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 23:49 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 23:49 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 23:49 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 23:49 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 23:49 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 23:49 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 23:49 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-7
93373 Matrix:
11/14/2022 10:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 23:49 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 23:49 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 23:49 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 23:49 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 23:49 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 23:49 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 23:49 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 23:49 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 23:49 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 23:49 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 23:49 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 23:49 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 23:49 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 23:49 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 23:49 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 23:49 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 23:49 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-7
93373 Matrix:
11/14/2022 10:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
2.07 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 23:49 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 23:49 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 23:49 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 23:49 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 23:49 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/19/22 23:49 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/19/22 23:49 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/19/22 23:49 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/19/22 23:49 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 23:49 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 23:49 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/19/22 23:49 V26697ENM
0.335 J µg/L 0.220 0.500Toluene 1 11/19/22 23:49 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 23:49 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/19/22 23:49 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 23:49 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 23:49 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/19/22 23:49 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 23:49 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 23:49 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-7
93373 Matrix:
11/14/2022 10:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 23:49 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 23:49 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 23:49 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/19/22 23:49 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 23:49 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/19/22 23:49 V26697
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/19/22 23:491 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-8
93374 Matrix:
11/14/2022 13:07
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/20/22 00:16 6200BENM
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/20/22 00:161 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-8
93374 Matrix:
11/14/2022 13:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/20/22 00:16 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/20/22 00:16 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/20/22 00:16 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/20/22 00:16 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/20/22 00:16 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/20/22 00:16 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/20/22 00:16 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/20/22 00:16 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/20/22 00:16 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/20/22 00:16 V26697ENM
0.561 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/20/22 00:16 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/20/22 00:16 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/20/22 00:16 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-8
93374 Matrix:
11/14/2022 13:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/20/22 00:16 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/20/22 00:16 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/20/22 00:16 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/20/22 00:16 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/20/22 00:16 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/20/22 00:16 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/20/22 00:16 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/20/22 00:16 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/20/22 00:16 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/20/22 00:16 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/20/22 00:16 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/20/22 00:16 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/20/22 00:16 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/20/22 00:16 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/20/22 00:16 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/20/22 00:16 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/20/22 00:16 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-8
93374 Matrix:
11/14/2022 13:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/20/22 00:16 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/20/22 00:16 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/20/22 00:16 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/20/22 00:16 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/20/22 00:16 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/20/22 00:16 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/20/22 00:16 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/20/22 00:16 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/20/22 00:16 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/20/22 00:16 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/20/22 00:16 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/20/22 00:16 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/20/22 00:16 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/20/22 00:16 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/20/22 00:16 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/20/22 00:16 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/20/22 00:16 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/20/22 00:16 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/20/22 00:16 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/20/22 00:16 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-8
93374 Matrix:
11/14/2022 13:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
0.371 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/20/22 00:16 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/20/22 00:16 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/20/22 00:16 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/20/22 00:16 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/20/22 00:16 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/20/22 00:16 V26697
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 70-130%11/20/22 00:161 ENM V26697
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/20/22 00:161 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-9
93375 Matrix:
11/14/2022 10:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/20/22 00:43 6200BENM
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: Dibromofluoromethane 101 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: Toluene-d8 99.6 Limits: 70-130%11/20/22 00:431 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-9
93375 Matrix:
11/14/2022 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/20/22 00:43 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/20/22 00:43 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/20/22 00:43 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/20/22 00:43 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/20/22 00:43 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/20/22 00:43 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/20/22 00:43 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/20/22 00:43 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/20/22 00:43 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/20/22 00:43 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/20/22 00:43 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/20/22 00:43 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/20/22 00:43 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-9
93375 Matrix:
11/14/2022 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/20/22 00:43 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/20/22 00:43 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/20/22 00:43 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/20/22 00:43 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/20/22 00:43 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/20/22 00:43 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/20/22 00:43 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/20/22 00:43 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/20/22 00:43 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/20/22 00:43 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/20/22 00:43 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/20/22 00:43 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/20/22 00:43 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/20/22 00:43 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/20/22 00:43 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/20/22 00:43 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/20/22 00:43 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-9
93375 Matrix:
11/14/2022 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/20/22 00:43 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/20/22 00:43 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/20/22 00:43 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/20/22 00:43 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/20/22 00:43 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/20/22 00:43 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/20/22 00:43 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/20/22 00:43 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/20/22 00:43 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/20/22 00:43 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/20/22 00:43 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/20/22 00:43 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/20/22 00:43 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/20/22 00:43 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/20/22 00:43 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/20/22 00:43 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/20/22 00:43 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/20/22 00:43 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/20/22 00:43 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/20/22 00:43 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-9
93375 Matrix:
11/14/2022 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/20/22 00:43 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/20/22 00:43 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/20/22 00:43 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/20/22 00:43 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/20/22 00:43 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/20/22 00:43 V26697
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: Dibromofluoromethane 101 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%11/20/22 00:431 ENM V26697
Surrogate: Toluene-d8 99.6 Limits: 70-130%11/20/22 00:431 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-10
93376 Matrix:
11/14/2022 10:42
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/20/22 01:10 6200BENM
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: Dibromofluoromethane 101 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/20/22 01:101 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-10
93376 Matrix:
11/14/2022 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/20/22 01:10 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/20/22 01:10 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/20/22 01:10 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/20/22 01:10 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/20/22 01:10 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/20/22 01:10 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/20/22 01:10 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/20/22 01:10 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/20/22 01:10 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/20/22 01:10 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/20/22 01:10 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/20/22 01:10 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/20/22 01:10 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-10
93376 Matrix:
11/14/2022 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/20/22 01:10 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/20/22 01:10 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/20/22 01:10 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/20/22 01:10 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/20/22 01:10 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/20/22 01:10 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/20/22 01:10 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/20/22 01:10 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/20/22 01:10 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/20/22 01:10 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/20/22 01:10 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/20/22 01:10 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/20/22 01:10 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/20/22 01:10 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/20/22 01:10 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/20/22 01:10 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/20/22 01:10 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-10
93376 Matrix:
11/14/2022 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/20/22 01:10 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/20/22 01:10 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/20/22 01:10 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/20/22 01:10 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/20/22 01:10 V26697ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/20/22 01:10 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/20/22 01:10 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/20/22 01:10 V26697ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/20/22 01:10 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/20/22 01:10 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/20/22 01:10 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/20/22 01:10 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/20/22 01:10 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/20/22 01:10 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/20/22 01:10 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/20/22 01:10 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/20/22 01:10 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/20/22 01:10 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/20/22 01:10 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/20/22 01:10 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:MW-10
93376 Matrix:
11/14/2022 10:42
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/20/22 01:10 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/20/22 01:10 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/20/22 01:10 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/20/22 01:10 V26697ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/20/22 01:10 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/20/22 01:10 V26697
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: Dibromofluoromethane 101 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%11/20/22 01:101 ENM V26697
Surrogate: Toluene-d8 100 Limits: 70-130%11/20/22 01:101 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-1
93377 Matrix:
11/14/2022 13:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/20/22 01:37 6200BENM
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 18:2410 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-1
93377 Matrix:
11/14/2022 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/20/22 01:37 V26697ENM
0.260 J µg/L 0.180 0.500Benzene 1 11/20/22 01:37 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/20/22 01:37 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/20/22 01:37 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/20/22 01:37 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/20/22 01:37 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/20/22 01:37 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/20/22 01:37 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/20/22 01:37 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/20/22 01:37 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/20/22 01:37 V26697ENM
82.7 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/20/22 01:37 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/20/22 01:37 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/20/22 01:37 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-1
93377 Matrix:
11/14/2022 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/20/22 01:37 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/20/22 01:37 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/20/22 01:37 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/20/22 01:37 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/20/22 01:37 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/20/22 01:37 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/20/22 01:37 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/20/22 01:37 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/20/22 01:37 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/20/22 01:37 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/20/22 01:37 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/20/22 01:37 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/20/22 01:37 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/20/22 01:37 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/20/22 01:37 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/20/22 01:37 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/20/22 01:37 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-1
93377 Matrix:
11/14/2022 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
217 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 11/21/22 18:24 V26806MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/20/22 01:37 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/20/22 01:37 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/20/22 01:37 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/20/22 01:37 V26697ENM
22.5 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/20/22 01:37 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/20/22 01:37 V26697ENM
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 11/20/22 01:37 V26697ENM
13.5 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/20/22 01:37 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/20/22 01:37 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/20/22 01:37 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/20/22 01:37 V26697ENM
0.474 J µg/L 0.220 0.500Toluene 1 11/20/22 01:37 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/20/22 01:37 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/20/22 01:37 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/20/22 01:37 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/20/22 01:37 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/20/22 01:37 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/20/22 01:37 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/20/22 01:37 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-1
93377 Matrix:
11/14/2022 13:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/20/22 01:37 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/20/22 01:37 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/20/22 01:37 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/20/22 01:37 V26697ENM
0.464 J µg/L 0.420 1.00m,p-Xylene 1 11/20/22 01:37 V26697ENM
0.464 J µg/L 0.210 0.500Xylene (Total)1 11/20/22 01:37 V26697
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/20/22 01:371 ENM V26697
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.2 Limits: 70-130%11/21/22 18:2410 MSA V26806
Surrogate: Toluene-d8 99.0 Limits: 70-130%11/21/22 18:2410 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-3
93378 Matrix:
11/14/2022 13:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 11/20/22 02:04 6200BENM
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: Toluene-d8 98.8 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/21/22 22:54100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-3
93378 Matrix:
11/14/2022 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/20/22 02:04 V26697ENM
350 µg/L 18.0 50.0Benzene 100 11/21/22 22:54 V26806MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/20/22 02:04 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/20/22 02:04 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/20/22 02:04 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/20/22 02:04 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/20/22 02:04 V26697ENM
2.94 µg/L 0.180 0.500n-Butylbenzene 1 11/20/22 02:04 V26697ENM
0.831 µg/L 0.200 0.500
sec-Butyl benzene 1 11/20/22 02:04 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/20/22 02:04 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/20/22 02:04 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/20/22 02:04 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/20/22 02:04 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/20/22 02:04 V26697ENM
2.32 µg/L 0.220 0.500Chloroform 1 11/20/22 02:04 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/20/22 02:04 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/20/22 02:04 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/20/22 02:04 V26697ENM
62.0 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/20/22 02:04 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/20/22 02:04 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/20/22 02:04 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/20/22 02:04 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-3
93378 Matrix:
11/14/2022 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/20/22 02:04 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/20/22 02:04 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/20/22 02:04 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/20/22 02:04 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/20/22 02:04 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/20/22 02:04 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/20/22 02:04 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/20/22 02:04 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/20/22 02:04 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/20/22 02:04 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/20/22 02:04 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/20/22 02:04 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/20/22 02:04 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/20/22 02:04 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/20/22 02:04 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/20/22 02:04 V26697ENM
0.861 µg/L 0.170 0.500Ethylbenzene 1 11/20/22 02:04 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/20/22 02:04 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/20/22 02:04 V26697ENM
9.96 µg/L 0.180 0.500Isopropylbenzene 1 11/20/22 02:04 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/20/22 02:04 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/20/22 02:04 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-3
93378 Matrix:
11/14/2022 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
144 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 11/21/22 22:54 V26806MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/20/22 02:04 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/20/22 02:04 V26697ENM
5.02 µg/L 0.470 1.00Naphthalene 1 11/20/22 02:04 V26697ENM
2.89 µg/L 0.190 0.500n-Propylbenzene 1 11/20/22 02:04 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/20/22 02:04 V26697ENM
77.6 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 11/20/22 02:04 V26697ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 11/20/22 02:04 V26697ENM
549 J
µg/L 190 1000
tert-Amyl Alcohol (TAA)100 11/21/22 22:54 V26806MSA
6.92 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 11/20/22 02:04 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/20/22 02:04 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/20/22 02:04 V26697ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/20/22 02:04 V26697ENM
1.21 µg/L 0.220 0.500Toluene 1 11/20/22 02:04 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/20/22 02:04 V26697ENM
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 11/20/22 02:04 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/20/22 02:04 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/20/22 02:04 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/20/22 02:04 V26697ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 11/20/22 02:04 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/20/22 02:04 V26697ENM
47.5 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/20/22 02:04 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:DW-3
93378 Matrix:
11/14/2022 13:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
5.35 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/20/22 02:04 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/20/22 02:04 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/20/22 02:04 V26697ENM
25.6 µg/L 0.210 0.500o-Xylene 1 11/20/22 02:04 V26697ENM
101 µg/L 0.420 1.00m,p-Xylene 1 11/20/22 02:04 V26697ENM
127 µg/L 0.210 0.500Xylene (Total)1 11/20/22 02:04 V26697
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: Toluene-d8 98.8 Limits: 70-130%11/20/22 02:041 ENM V26697
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/21/22 22:54100 MSA V26806
Surrogate: Toluene-d8 99.4 Limits: 70-130%11/21/22 22:54100 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:OW-2
93379 Matrix:
11/14/2022 12:43
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 11/20/22 02:59 6200BENM
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/22/22 01:101000 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:OW-2
93379 Matrix:
11/14/2022 12:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
1100 µg/L 180 1000Acetone 100 11/20/22 02:59 V26697ENM
3210 µg/L 18.0 50.0Benzene 100 11/20/22 02:59 V26697ENM
<21.0 µg/L 21.0 50.0Bromobenzene 100 11/20/22 02:59 V26697ENM
<42.0 µg/L 42.0 100Bromochloromethane 100 11/20/22 02:59 V26697ENM
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 11/20/22 02:59 V26697ENM
<150 µg/L 150 500Bromoform 100 11/20/22 02:59 V26697ENM
<28.0 µg/L 28.0 100Bromomethane 100 11/20/22 02:59 V26697ENM
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.0
sec-Butyl benzene 100 11/20/22 02:59 V26697ENM
<92.0 µg/L 92.0 200tert-Butyl benzene 100 11/20/22 02:59 V26697ENM
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 11/20/22 02:59 V26697ENM
<19.0 µg/L 19.0 50.0Chlorobenzene 100 11/20/22 02:59 V26697ENM
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 11/20/22 02:59 V26697ENM
<43.0 µg/L 43.0 100Chloroethane 100 11/20/22 02:59 V26697ENM
<22.0 µg/L 22.0 50.0Chloroform 100 11/20/22 02:59 V26697ENM
<22.0 µg/L 22.0 50.0
Chloromethane 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 11/20/22 02:59 V26697ENM
358 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 11/20/22 02:59 V26697ENM
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 11/20/22 02:59 V26697ENM
<23.0 µg/L 23.0 50.0Dibromomethane 100 11/20/22 02:59 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:OW-2
93379 Matrix:
11/14/2022 12:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 11/20/22 02:59 V26697ENM
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 11/20/22 02:59 V26697ENM
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 11/20/22 02:59 V26697ENM
<120 µg/L 120 500Dichlorodifluoromethane 100 11/20/22 02:59 V26697ENM
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 11/20/22 02:59 V26697ENM
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 11/20/22 02:59 V26697ENM
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 11/20/22 02:59 V26697ENM
<18.0 µg/L 18.0 50.0
trans-1,2-Dichloroethene 100 11/20/22 02:59 V26697ENM
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 11/20/22 02:59 V26697ENM
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 11/20/22 02:59 V26697ENM
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 11/20/22 02:59 V26697ENM
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 11/20/22 02:59 V26697ENM
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 11/20/22 02:59 V26697ENM
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 11/20/22 02:59 V26697ENM
<4200 µg/L 4200 20000
Ethanol 100 11/20/22 02:59 V26697ENM
2270 µg/L 17.0 50.0Ethylbenzene 100 11/20/22 02:59 V26697ENM
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 11/20/22 02:59 V26697ENM
<38.0 µg/L 38.0 1002-Hexanone 100 11/20/22 02:59 V26697ENM
73.7 µg/L 18.0 50.0Isopropylbenzene 100 11/20/22 02:59 V26697ENM
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 11/20/22 02:59 V26697ENM
520 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 11/20/22 02:59 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:OW-2
93379 Matrix:
11/14/2022 12:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
1100 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 11/20/22 02:59 V26697ENM
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 11/20/22 02:59 V26697ENM
<33.0 µg/L 33.0 200Methylene Chloride 100 11/20/22 02:59 V26697ENM
1480 µg/L 47.0 100Naphthalene 100 11/20/22 02:59 V26697ENM
212 µg/L 19.0 50.0n-Propylbenzene 100 11/20/22 02:59 V26697ENM
154 µg/L 22.0 50.0Styrene 100 11/20/22 02:59 V26697ENM
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/20/22 02:59 V26697ENM
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 11/20/22 02:59 V26697ENM
<190 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 11/20/22 02:59 V26697ENM
213 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 11/20/22 02:59 V26697ENM
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 11/20/22 02:59 V26697ENM
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 11/20/22 02:59 V26697ENM
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 11/20/22 02:59 V26697ENM
24600 µg/L 220 500Toluene 1000 11/22/22 01:10 V26806MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 11/20/22 02:59 V26697ENM
<31.0 µg/L 31.0 50.0
1,2,4-Trichlorobenzene 100 11/20/22 02:59 V26697ENM
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 11/20/22 02:59 V26697ENM
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 11/20/22 02:59 V26697ENM
<18.0 µg/L 18.0 50.0Trichloroethene 100 11/20/22 02:59 V26697ENM
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 11/20/22 02:59 V26697ENM
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 11/20/22 02:59 V26697ENM
3110 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 11/20/22 02:59 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:OW-2
93379 Matrix:
11/14/2022 12:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00 V26804 11/21/22 09:00
758 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 11/20/22 02:59 V26697ENM
<100 µg/L 100 500Vinyl Acetate 100 11/20/22 02:59 V26697ENM
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 11/20/22 02:59 V26697ENM
5390 µg/L 21.0 50.0o-Xylene 100 11/20/22 02:59 V26697ENM
10400 µg/L 42.0 100m,p-Xylene 100 11/20/22 02:59 V26697ENM
15800 µg/L 21.0 50.0Xylene (Total)100 11/20/22 02:59 V26697
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/20/22 02:59100 ENM V26697
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: 1,2-Dichloroethane - d4 97.6 Limits: 70-130%11/22/22 01:101000 MSA V26806
Surrogate: Toluene-d8 98.4 Limits: 70-130%11/22/22 01:101000 MSA V26806
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:Trip Blanks
93380 Matrix:
11/14/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500Benzene 1 11/19/22 19:18 V26697ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/19/22 19:18 V26697ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/19/22 19:18 V26697ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/19/22 19:18 V26697ENM
<1.50 µg/L 1.50 5.00Bromoform 1 11/19/22 19:18 V26697ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 11/19/22 19:18 V26697ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/19/22 19:18 V26697ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 11/19/22 19:18 V26697ENM
<0.220 µg/L 0.220 0.500Chloroform 1 11/19/22 19:18 V26697ENM
<0.220 µg/L 0.220 0.500
Chloromethane 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/19/22 19:18 V26697ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/19/22 19:18 V26697ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/19/22 19:18 V26697ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/19/22 19:18 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:Trip Blanks
93380 Matrix:
11/14/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/19/22 19:18 V26697ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/19/22 19:18 V26697ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 11/19/22 19:18 V26697ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/19/22 19:18 V26697ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/19/22 19:18 V26697ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/19/22 19:18 V26697ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/19/22 19:18 V26697ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/19/22 19:18 V26697ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/19/22 19:18 V26697ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/19/22 19:18 V26697ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/19/22 19:18 V26697ENM
<42.0 µg/L 42.0 200
Ethanol 1 11/19/22 19:18 V26697ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/19/22 19:18 V26697ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/19/22 19:18 V26697ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/19/22 19:18 V26697ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/19/22 19:18 V26697ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/19/22 19:18 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:Trip Blanks
93380 Matrix:
11/14/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/19/22 19:18 V26697ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/19/22 19:18 V26697ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/19/22 19:18 V26697ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/19/22 19:18 V26697ENM
<0.220 µg/L 0.220 0.500Styrene 1 11/19/22 19:18 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/19/22 19:18 V26697ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/19/22 19:18 V26697ENM
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 11/19/22 19:18 V26697ENM
<0.220 µg/L 0.220 0.500Toluene 1 11/19/22 19:18 V26697ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/19/22 19:18 V26697ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 11/19/22 19:18 V26697ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/19/22 19:18 V26697ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 11/19/22 19:18 V26697ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/19/22 19:18 V26697ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/19/22 19:18 V26697ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/19/22 19:18 V26697ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/19/22 19:18 V26697ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 11/19/22 19:18 V26697ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 11/19/22 19:18 V26697ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-320-0043
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3067 Received : 11/16/2022
Handy Stop #7
Report Date : 11/23/2022
Sample ID :
Lab No :
Sampled:Trip Blanks
93380 Matrix:
11/14/2022 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V26696 11/19/22 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/19/22 19:18 V26697ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/19/22 19:18 V26697
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%11/19/22 19:181 ENM V26697
Surrogate: Dibromofluoromethane 103 Limits: 70-130%11/19/22 19:181 ENM V26697
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 70-130%11/19/22 19:181 ENM V26697
Surrogate: Toluene-d8 98.8 Limits: 70-130%11/19/22 19:181 ENM V26697
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
Associated Lab Samples: 93367, 93368, 93369, 93370, 93371, 93372, 93373, 93374, 93375, 93376, 93377, 93378, 93379, 93380
LRB-V26696 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/19/22 17:5610.01.80<1.80µg/LAcetone
11/19/22 17:560.5000.180<0.180µg/LBenzene
11/19/22 17:560.5000.210<0.210µg/LBromobenzene
11/19/22 17:561.000.420<0.420µg/LBromochloromethane
11/19/22 17:560.5000.160<0.160µg/LBromodichloromethane
11/19/22 17:565.001.50<1.50µg/LBromoform
11/19/22 17:561.000.280<0.280µg/LBromomethane
11/19/22 17:560.5000.180<0.180µg/Ln-Butylbenzene
11/19/22 17:560.5000.200<0.200µg/Lsec-Butyl benzene
11/19/22 17:562.000.920<0.920µg/Ltert-Butyl benzene
11/19/22 17:560.5000.180<0.180µg/LCarbon Tetrachloride
11/19/22 17:560.5000.190<0.190µg/LChlorobenzene
11/19/22 17:560.5000.190<0.190µg/LChlorodibromomethane
11/19/22 17:561.000.430<0.430µg/LChloroethane
11/19/22 17:560.5000.220<0.220µg/LChloroform
11/19/22 17:560.5000.220<0.220µg/LChloromethane
11/19/22 17:560.5000.200<0.200µg/L2-Chlorotoluene
11/19/22 17:560.5000.200<0.200µg/L4-Chlorotoluene
11/19/22 17:560.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
11/19/22 17:562.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
11/19/22 17:560.5000.200<0.200µg/L1,2-Dibromoethane
11/19/22 17:560.5000.230<0.230µg/LDibromomethane
11/19/22 17:560.5000.220<0.220µg/L1,2-Dichlorobenzene
11/19/22 17:560.5000.190<0.190µg/L1,3-Dichlorobenzene
11/19/22 17:560.5000.210<0.210µg/L1,4-Dichlorobenzene
11/19/22 17:565.001.20<1.20µg/LDichlorodifluoromethane
11/19/22 17:560.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 8Date:11/23/2022 05:59 PM
Page 77 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
Associated Lab Samples: 93367, 93368, 93369, 93370, 93371, 93372, 93373, 93374, 93375, 93376, 93377, 93378, 93379, 93380
LRB-V26696 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/19/22 17:560.5000.150<0.150µg/L1,2-Dichloroethane
11/19/22 17:560.5000.150<0.150µg/L1,1-Dichloroethene
11/19/22 17:560.5000.200<0.200µg/Lcis-1,2-Dichloroethene
11/19/22 17:560.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
11/19/22 17:560.5000.190<0.190µg/L1,2-Dichloropropane
11/19/22 17:560.5000.130<0.130µg/L1,3-Dichloropropane
11/19/22 17:562.000.210<0.210µg/L2,2-Dichloropropane
11/19/22 17:560.5000.200<0.200µg/L1,1-Dichloropropene
11/19/22 17:560.5000.210<0.210µg/Lcis-1,3-Dichloropropene
11/19/22 17:560.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
11/19/22 17:5620042.0<42.0µg/LEthanol
11/19/22 17:560.5000.170<0.170µg/LEthylbenzene
11/19/22 17:563.000.350<0.350µg/LHexachlorobutadiene
11/19/22 17:561.000.380<0.380µg/L2-Hexanone
11/19/22 17:560.5000.180<0.180µg/LIsopropylbenzene
11/19/22 17:560.5000.089<0.089µg/L4-Isopropyl toluene
11/19/22 17:565.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
11/19/22 17:561.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/19/22 17:561.000.078<0.078µg/L4-Methyl-2-Pentanone
11/19/22 17:562.000.330<0.330µg/LMethylene Chloride
11/19/22 17:561.000.470<0.470µg/LNaphthalene
11/19/22 17:560.5000.190<0.190µg/Ln-Propylbenzene
11/19/22 17:560.5000.220<0.220µg/LStyrene
11/19/22 17:5610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
11/19/22 17:5610.00.350<0.350µg/Ltert-Butyl formate (TBF)
11/19/22 17:5610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
11/19/22 17:5610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 8Date:11/23/2022 05:59 PM
Page 78 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
Associated Lab Samples: 93367, 93368, 93369, 93370, 93371, 93372, 93373, 93374, 93375, 93376, 93377, 93378, 93379, 93380
LRB-V26696 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/19/22 17:560.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
11/19/22 17:560.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
11/19/22 17:560.5000.220<0.220µg/LTetrachloroethene
11/19/22 17:560.5000.220<0.220µg/LToluene
11/19/22 17:560.5000.380<0.380µg/L1,2,3-Trichlorobenzene
11/19/22 17:560.5000.310<0.310µg/L1,2,4-Trichlorobenzene
11/19/22 17:560.5000.160<0.160µg/L1,1,1-Trichloroethane
11/19/22 17:560.5000.096<0.096µg/L1,1,2-Trichloroethane
11/19/22 17:560.5000.180<0.180µg/LTrichloroethene
11/19/22 17:560.5000.180<0.180µg/LTrichlorofluoromethane
11/19/22 17:560.5000.270<0.270µg/L1,2,3-Trichloropropane
11/19/22 17:560.5000.190<0.190µg/L1,2,4-Trimethylbenzene
11/19/22 17:560.5000.180<0.180µg/L1,3,5-Trimethylbenzene
11/19/22 17:565.001.00<1.00µg/LVinyl Acetate
11/19/22 17:560.5000.170<0.170µg/LVinyl Chloride
11/19/22 17:560.5000.210<0.210µg/Lo-Xylene
11/19/22 17:561.000.420<0.420µg/Lm,p-Xylene
11/19/22 17:5610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
11/19/22 17:564-Bromofluorobenzene (S)99.0 70-130
11/19/22 17:56Dibromofluoromethane (S)104 70-130
11/19/22 17:561,2-Dichloroethane - d4 (S)98.8 70-130
11/19/22 17:56Toluene-d8 (S)99.2 70-130
Page 3 of 8Date:11/23/2022 05:59 PM
Page 79 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
LCS-V26696 LCSD-V26696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.3 88.288.535.440.0µg/LAcetone 40-160 0.2 20.0
20.0 10098.519.720.0µg/LBenzene 70-130 1.5 20.0
19.8 99.098.519.720.0µg/LBromobenzene 70-130 0.5 20.0
21.2 10610721.420.0µg/LBromochloromethane 70-130 0.9 20.0
20.6 10310721.320.0µg/LBromodichloromethane 70-130 3.3 20.0
21.9 11010821.520.0µg/LBromoform 70-130 1.8 20.0
21.0 10511422.820.0µg/LBromomethane 60-140 8.2 20.0
19.5 97.597.019.420.0µg/Ln-Butylbenzene 70-130 0.5 20.0
19.7 98.596.019.220.0µg/Lsec-Butyl benzene 70-130 2.5 20.0
19.8 99.096.019.220.0µg/Ltert-Butyl benzene 70-130 3.0 20.0
24.5 12311923.720.0µg/LCarbon Tetrachloride 70-130 3.3 20.0
20.4 10210120.220.0µg/LChlorobenzene 70-130 0.9 20.0
19.6 98.099.519.920.0µg/LChlorodibromomethane 70-130 1.5 20.0
21.4 10710420.720.0µg/LChloroethane 60-140 3.3 20.0
20.9 10510821.520.0µg/LChloroform 70-130 2.8 20.0
19.0 95.094.018.820.0µg/LChloromethane 60-140 1.0 20.0
19.7 98.598.519.720.0µg/L2-Chlorotoluene 70-130 0.0 20.0
19.4 97.095.519.120.0µg/L4-Chlorotoluene 70-130 1.5 20.0
19.5 97.599.019.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.5 20.0
21.9 11012825.520.0µg/L1,2-Dibromo-3-Chloropropane 70-130 15.1 20.0
21.1 10610420.820.0µg/L1,2-Dibromoethane 70-130 1.4 20.0
20.9 10510821.520.0µg/LDibromomethane 70-130 2.8 20.0
20.2 10110120.220.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0
21.1 10610320.520.0µg/L1,3-Dichlorobenzene 70-130 2.8 20.0
19.7 98.510120.120.0µg/L1,4-Dichlorobenzene 70-130 2.0 20.0
21.5 10810520.920.0µg/LDichlorodifluoromethane 60-140 2.8 20.0
Page 4 of 8Date:11/23/2022 05:59 PM
Page 80 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
LCS-V26696 LCSD-V26696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510120.120.0µg/L1,1-Dichloroethane 70-130 1.0 20.0
21.2 10610621.220.0µg/L1,2-Dichloroethane 70-130 0.0 20.0
19.2 96.096.019.220.0µg/L1,1-Dichloroethene 70-130 0.0 20.0
19.5 97.597.519.520.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
19.4 97.097.519.520.0µg/Ltrans-1,2-Dichloroethene 70-130 0.5 20.0
20.4 10210420.820.0µg/L1,2-Dichloropropane 70-130 1.9 20.0
20.6 10310320.520.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
20.7 10410320.520.0µg/L2,2-Dichloropropane 70-130 0.9 20.0
21.9 11011022.020.0µg/L1,1-Dichloropropene 70-130 0.4 20.0
20.5 10310521.020.0µg/Lcis-1,3-Dichloropropene 70-130 2.4 20.0
20.8 10410721.420.0µg/Ltrans-1,3-Dichloropropene 70-130 2.8 20.0
607 121103517500µg/LEthanol 60-140 16.0 20.0
19.7 98.597.019.420.0µg/LEthylbenzene 70-130 1.5 20.0
21.2 10698.019.620.0µg/LHexachlorobutadiene 70-130 7.8 20.0
19.4 97.095.519.120.0µg/L2-Hexanone 60-140 1.5 20.0
20.0 10097.519.520.0µg/LIsopropylbenzene 70-130 2.5 20.0
20.2 10198.519.720.0µg/L4-Isopropyl toluene 70-130 2.5 20.0
25.8 12911122.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 15.4 20.0
20.7 10410320.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.4 20.0
18.5 92.595.519.120.0µg/L4-Methyl-2-Pentanone 60-140 3.1 20.0
18.6 93.093.518.720.0µg/LMethylene Chloride 70-130 0.5 20.0
18.5 92.590.018.020.0µg/LNaphthalene 70-130 2.7 20.0
19.6 98.095.019.020.0µg/Ln-Propylbenzene 70-130 3.1 20.0
19.7 98.510120.120.0µg/LStyrene 70-130 2.0 20.0
47.6 11912349.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.5 20.0
42.6 10711044.040.0µg/Ltert-Butyl formate (TBF)40-140 3.2 20.0
Page 5 of 8Date:11/23/2022 05:59 PM
Page 81 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26696
LCS-V26696 LCSD-V26696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.5 11887.517.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 29.2*20.0
42.2 10610742.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.6 20.0
21.5 10810821.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.0 20.0
22.0 11011322.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.2 20.0
20.7 10410621.120.0µg/LTetrachloroethene 70-130 1.9 20.0
19.8 99.010120.120.0µg/LToluene 70-130 1.5 20.0
22.3 11297.519.520.0µg/L1,2,3-Trichlorobenzene 70-130 13.3 20.0
21.6 10896.019.220.0µg/L1,2,4-Trichlorobenzene 70-130 11.7 20.0
23.0 11511222.420.0µg/L1,1,1-Trichloroethane 70-130 2.6 20.0
22.3 11211322.520.0µg/L1,1,2-Trichloroethane 70-130 0.8 20.0
21.6 10810621.220.0µg/LTrichloroethene 70-130 1.8 20.0
21.4 10710621.220.0µg/LTrichlorofluoromethane 60-140 0.9 20.0
24.3 12212124.120.0µg/L1,2,3-Trichloropropane 70-130 0.8 20.0
19.0 95.094.518.920.0µg/L1,2,4-Trimethylbenzene 70-130 0.5 20.0
19.2 96.095.019.020.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0
24.5 12312525.020.0µg/LVinyl Acetate 60-140 2.0 20.0
20.1 10110320.620.0µg/LVinyl Chloride 60-140 2.4 20.0
19.1 95.594.018.820.0µg/Lo-Xylene 70-130 1.5 20.0
40.4 10110240.740.0µg/Lm,p-Xylene 70-130 0.7 20.0
20.6 10311723.420.0µg/L3,3-Dimethyl-1-butanol 70-130 12.7 20.0
10198.84-Bromofluorobenzene (S)70-130
114114Dibromofluoromethane (S)70-130
97.298.41,2-Dichloroethane - d4 (S)70-130
98.299.6Toluene-d8 (S)70-130
Page 6 of 8* QC Fail Date:11/23/2022 05:59 PM
Page 82 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26806QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26804
Associated Lab Samples: 93367, 93369, 93370, 93377, 93378, 93379
LRB-V26804 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/21/22 16:080.5000.180<0.180µg/LBenzene
11/21/22 16:081.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/21/22 16:0810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
11/21/22 16:0810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
11/21/22 16:080.5000.220<0.220µg/LToluene
11/21/22 16:080.5000.190<0.190µg/L1,2,4-Trimethylbenzene
11/21/22 16:080.5000.210<0.210µg/Lo-Xylene
11/21/22 16:084-Bromofluorobenzene (S)96.8 70-130
11/21/22 16:08Dibromofluoromethane (S)95.8 70-130
11/21/22 16:081,2-Dichloroethane - d4 (S)97.6 70-130
11/21/22 16:08Toluene-d8 (S)98.4 70-130
LCS-V26804 LCSD-V26804Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.5 10310320.620.0µg/LBenzene 70-130 0.4 20.0
21.2 10610621.220.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
49.3 12310541.840.0µg/Ltert-Butyl Alcohol (TBA)40-140 16.4 20.0
24.6 12313827.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 11.1 20.0
21.0 10510420.820.0µg/LToluene 70-130 0.9 20.0
19.5 97.510120.220.0µg/L1,2,4-Trimethylbenzene 70-130 3.5 20.0
19.9 99.510020.020.0µg/Lo-Xylene 70-130 0.5 20.0
96.099.44-Bromofluorobenzene (S)70-130
108103Dibromofluoromethane (S)70-130
98.497.21,2-Dichloroethane - d4 (S)70-130
Page 7 of 8Date:11/23/2022 05:59 PM
Page 83 of 87
Quality Control Data
22-320-0043Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Stop #7
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V26806QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V26804
LCS-V26804 LCSD-V26804Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
99.4100Toluene-d8 (S)70-130
Page 8 of 8Date:11/23/2022 05:59 PM
Page 84 of 87
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-320-0043
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/16/2022 18:05:51
Special precautions or instructions included?
Comments:
Page 85 of 87
Page 86 of 87
Page 87 of 87

APPENDIX F
O&M Field Data Sheets

APPENDIX G
Overall Remediation Costs
Date: 12/13/22 Facility ID #: 0-031674
Claim Number Task Code Task Code Description Cost Claim Amount
3.101 Supervision of Field Work $3,800.00
3.113 Installation of 2-inch Well $11,000.00
3.114 Installation of 4-inch Well $9,600.00
3.398 Cost for Drill Rig Mobization $250.00
7.040 Cost for SVE System $41,586.11
7.060 Cost for Air Sparge System $41,586.10
7.081 Remediation System Installation Inspection $5,208.00
7.100 Cost for Installation of Remediation System $68,819.15
7.201 Cost for Scheduled Maintenance $930.00
7.260 Cost for Remediation Operating Expenses $450.00
8.055 Injection Notice of Intent $300.00
12.030 Overnight Lodging $1,224.56
12.050 Consultant Travel $1,540.00
4.031 Cost for Sampling Well $2,330.00
4.090 Cost for Analytical $2,650.00
4.091 Sampling Shipping $160.00
6.091 Monitoring Report (Subs)$1,250.00
6.105 Corrective Action Performance Report $1,000.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $3,568.41
7.250 Cost for Remediation Supplies and Equipment $291.80
7.260 Cost for Remediation Operating Expenses $3,476.00
12.050 Consultant Mobilization $2,420.00
4.031 Cost for Sampling Wells $940.00
4.090 Cost for Analytical $1,170.00
4.091 Sampling Shipping $180.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $720.75
7.260 Cost for Remediation Operating Expenses $2,213.05
12.050 Consultant Mobilization $880.00
4.031 Cost for Sampling Wells $1,150.00
4.090 Cost for Analytical $1,294.00
4.091 Sampling Shipping $140.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $678.90
7.250 Cost for Remediation Supplies and Equipment $839.68
7.260 Cost for Remediation Operating Expenses $2,600.89
9.020 Cost for Disposal of Free Product and Ground Water $784.00
12.050 Consultant Mobilization $660.00
213 $17,646.67
APPENDIX G
OVERALL REMEDIATION COSTS (TO DATE)
HANDY STOP #7 (INCIDENT NO. 36069)
212 $186,293.92
214 $16,651.27
Page 1 of 4
Date: 12/13/22 Facility ID #: 0-031674
Claim Number Task Code Task Code Description Cost Claim Amount
APPENDIX G
OVERALL REMEDIATION COSTS (TO DATE)
HANDY STOP #7 (INCIDENT NO. 36069)
4.031 Cost for Sampling Wells $1,440.00
4.041 Cost for Sampling Water Supply Wells $90.00
4.090 Cost for Analytical $1,455.00
4.091 Sampling Shipping $100.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $1,395.00
7.250 Cost for Remediation Supplies and Equipment $0.00
7.260 Cost for Remediation Operating Expenses $2,532.83
7.420 MMPE $7,267.90
12.050 Consultant Mobilization $880.00
2.087 Cost for Free Product Check $50.00
4.031 Cost for Sampling Wells $1,180.00
4.041 Cost for Sampling Water Supply Wells $90.00
4.090 Cost for Analytical $1,480.00
4.091 Sampling Shipping $140.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $837.00
7.250 Cost for Remediation Supplies and Equipment $304.19
7.260 Cost for Remediation Operating Expenses $2,041.12
12.050 Consultant Mobilization $660.00
4.031 Cost for Sampling Wells $1,260.00
4.041 Cost for Sampling Water Supply Wells $45.00
4.090 Cost for Analytical $1,418.00
4.091 Sampling Shipping $140.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $1,890.69
7.250 Cost for Remediation Supplies and Equipment $15.42
7.260 Cost for Remediation Operating Expenses $2,537.53
7.420 MMPE $7,273.50
12.050 Consultant Mobilization $880.00
4.031 Cost for Sampling Wells $1,230.00
4.041 Cost for Sampling Water Supply Wells $90.00
4.090 Cost for Analytical $1,754.00
4.091 Sampling Shipping $100.00
6.091 Monitoring Report (Subs)$625.00
6.106 Corrective Action Performance Report $500.00
7.201 Cost for Scheduled Maintenance $767.25
7.250 Cost for Remediation Supplies and Equipment $2,219.68
7.260 Cost for Remediation Operating Expenses $1,627.52
12.050 Consultant Mobilization $440.00
$16,345.63
218 $9,353.45
217
215 $16,157.83
216 $7,907.31
Page 2 of 4
Date: 12/13/22 Facility ID #: 0-031674
Claim Number Task Code Task Code Description Cost Claim Amount
APPENDIX G
OVERALL REMEDIATION COSTS (TO DATE)
HANDY STOP #7 (INCIDENT NO. 36069)
4.041 Cost for Sampling Water Supply Wells $150.00
4.090 Cost for Analytical $522.00
4.091 Sampling Shipping $80.00
6.106 Corrective Action Performance Report $500.00
6.190 Letter Report $300.00
7.201 Cost for Scheduled Maintenance $534.75
7.260 Cost for Remediation Operating Expenses $2,848.76
12.050 Consultant Mobilization $440.00
4.041 Cost for Sampling Water Supply Wells $150.00
4.090 Cost for Analytical $1,966.00
4.091 Sampling Shipping $160.00
6.091 Monitoring Report (Subs)$900.00
6.106 Corrective Action Performance Report $1,000.00
7.201 Cost for Scheduled Maintenance $1,092.75
7.250 Cost for Remediation Supplies and Equipment $8.04
7.260 Cost for Remediation Operating Expenses $2,464.39
9.020 Cost for Disposal of Free Product and Ground Water $0.00
12.050 Consultant Mobilization $750.00
4.041 Water Supply Well Sampling $150.00
4.090 Cost for Analytical $612.00
4.091 Sample Shipping $120.00
6.106 Corrective Action Performance Report $1,000.00
6.190 Letter Report $500.00
7.201 Cost for Scheduled Maintenance $821.19
7.250 Cost for Remediation Supplies and Equipment $954.69
7.260 Cost for Remediation Operating Expenses $2,837.72
9.020 Cost for Disposal of Free Product and Ground Water $0.00
12.050 Consultant Mobilization $750.00
4.031 Cost for Sampling Wells $1,650.00
4.041 Water Supply Well Sampling $150.00
4.090 Cost for Analytical $2,410.00
4.091 Sample Shipping $320.00
6.091 Ground Water Monitoring Report $900.00
6.106 Corrective Action Performance Report $2,000.00
6.190 Letter Report $500.00
7.201 Cost for Scheduled Maintenance $1,495.44
7.260 Cost for Remediation Operating Expenses $5,352.96
9.020 Cost for Disposal of Free Product and Ground Water $746.50
11.020 Agreement to Connect Users to Municipal Water $300.00
11.050 Cost for Water Connections $1,300.00
11.060 Municipal Water Fees $700.00
12.050 Consultant Mobilization $1,750.00
220 $8,491.18
221 $7,745.60
222 $19,574.90
219 $5,375.51
Page 3 of 4
Date: 12/13/22 Facility ID #: 0-031674
Claim Number Task Code Task Code Description Cost Claim Amount
APPENDIX G
OVERALL REMEDIATION COSTS (TO DATE)
HANDY STOP #7 (INCIDENT NO. 36069)
4.031 Cost for Sampling Wells $1,010.00
4.090 Cost for Analytical $1,564.00
4.091 Sample Shipping $260.00
6.091 Ground Water Monitoring Report $900.00
6.106 Corrective Action Performance Report $2,000.00
7.201 Cost for Scheduled Maintenance $1,348.50
7.260 Cost for Remediation Operating Expenses $5,118.86
12.050 Consultant Mobilization $1,500.00
4.031 Cost for Sampling Wells $1,550.00
4.090 Cost for Analytical $1,294.00
4.091 Sample Shipping $60.00
6.090 Ground Water Monitoring Report $1,800.00
12.050 Consultant Mobilization $250.00
4.031 Cost for Sampling Wells $1,452.00
4.090 Cost for Analytical $1,892.00
4.091 Sample Shipping $40.00
6.106 Corrective Action Performance Report $2,250.00
7.201 Cost for Scheduled Maintenance $1,302.00
7.260 Cost for Remediation Operating Expenses $2,502.59
12.050 Consultant Mobilization $1,500.00
12.055 Temporary Impact Increase $300.00
$341,437.22Total Cost Since System Installation
223 $13,701.36
224 $4,954.00
$11,238.59
225
(Claim has not
been
submitted)
Page 4 of 4

APPENDIX H
Contaminant Mass Calculations
Area ID Well IDs Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
05/03/17 30.50 0.55 1.10 7.40 5.60 0.24 45.39 40.33 4.67 3.57 --- ---
04/19/18 0.16 0.89 0.00 0.64 0.00 0.00 1.69 38.81 6.19 0.18 95.1% 95.1%
08/13/18 11.80 0.25 0.32 1.80 5.40 0.15 19.72 37.36 7.64 2.54 -1340.2%28.9%
10/15/18 13.90 0.29 0.30 2.50 5.40 0.19 22.58 37.06 7.94 3.02 -19.0%15.4%
01/22/19 22.60 0.92 0.38 12.30 4.70 0.17 41.07 35.28 9.72 6.73 -122.7%-88.3%
04/08/19 41.20 1.60 0.68 7.10 4.40 0.00 54.98 33.43 11.57 10.72 -59.3%-200.1%
07/29/19 1.50 0.46 0.00 3.90 4.40 0.15 10.41 32.71 12.29 2.16 79.9%39.6%
10/08/19 5.10 0.36 0.00 2.50 5.10 0.17 13.23 34.08 10.92 2.43 -12.9%31.8%
01/02/20 0.42 0.00 0.00 1.60 4.40 0.19 6.61 35.07 9.93 1.11 54.6%69.0%
10/13/20 0.75 0.50 0.00 2.00 3.60 0.00 6.85 31.29 13.71 1.58 -43.1%55.7%
04/08/21 0.23 0.17 0.00 1.50 3.00 0.00 4.90 29.97 15.03 1.24 21.6%65.3%
10/20/21 0.84 0.23 0.00 2.20 5.70 0.53 9.50 33.90 11.10 1.78 -43.2%50.3%
04/05/22 0.32 0.23 0.00 0.44 4.9 0.22 6.11 36.53 8.47 0.87 50.9%75.6%
11/14/22 0.31 0.00 0.00 0.728 4.05 0.00 5.09 35.06 9.94 0.85 2.3%76.1%
05/03/17 12100.00 38500.00 3570.00 21200.00 9720.00 1300.00 86390.00 40.91 11.59 36954.63 --- ---
04/19/18 12100.00 43400.00 4900.00 28200.00 11800.00 1590.00 101990.00 39.04 13.46 50666.92 -37.1% -37.1%
08/13/18 FP FP FP FP FP FP FP FP NA FP --- ---
10/15/18 FP FP FP FP FP FP FP FP NA FP --- ---
01/22/19 FP FP FP FP FP FP FP FP NA FP --- ---
04/08/19 FP FP FP FP FP FP FP FP NA FP --- ---
07/29/19 FP FP FP FP FP FP FP FP NA FP --- ---
10/08/19 7380.00 40000.00 4060.00 21400.00 5110.00 1020.00 78970.00 34.81 17.69 51559.88 -1.8% -39.5%
01/02/20 FP FP FP FP FP FP FP FP NA FP --- ---
10/13/20 6520.00 44500.00 4140.00 24700.00 2460.00 1520.00 83840.00 32.05 20.45 63280.00 -22.7% -71.2%
04/08/21 4090.00 27200.00 2800.00 21300.00 3610.00 1740.00 60740.00 29.02 23.48 52637.44 16.8%-42.4%
10/20/21 722.00 6220.00 1180.00 9310.00 1490.00 1390.00 20312.00 34.81 17.69 13261.80 74.8% 64.1%
04/05/22 6,930 30,300 2,490 19,300 1,030 1,860 61910.00 37.02 15.48 35371.51 -166.7%4.3%
11/14/22 3,210 24,600 2,270 15,800 1,100 1,480 48460.00 45.45 7.05 12609.40 64.4%65.9%
APPENDIX H
CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
MW-4Area 1
Area 2 OW-2
Page 1 of 4
Area ID Well IDs Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX H
CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
05/03/17 7060.00 21800.00 2610.00 18100.00 486.00 913.00 50969.00 41.46 11.04 13116.70 ------
04/19/18 6400.00 22500.00 2700.00 15100.00 583.00 750.00 48033.00 39.53 12.97 14522.09 -10.7% -10.7%
08/13/18 5410.00 25600.00 3020.00 19300.00 231.00 875.00 54436.00 38.35 14.15 17955.28 -23.6% -36.9%
10/15/18 4570.00 24800.00 2710.00 18100.00 184.00 913.00 51277.00 37.26 15.24 18216.17 -1.5%-38.9%
01/22/19 1970.00 16300.00 2280.00 16900.00 33.60 1040.00 38523.60 34.10 18.40 16523.20 9.3%-26.0%
04/08/19 1610.00 20400.00 2800.00 20700.00 0.00 776.00 46286.00 34.55 17.95 19367.06 -17.2%-47.7%
07/29/19 3040.00 24600.00 3220.00 18900.00 110.00 761.00 50631.00 32.91 19.59 23120.67 -19.4%-76.3%
10/08/19 3120.00 22800.00 3240.00 17600.00 227.00 859.00 47846.00 35.44 17.06 19027.17 17.7%-45.1%
01/02/20 2340.00 23300.00 3330.00 23400.00 153.00 862.00 53385.00 35.53 16.97 21117.89 -11.0%-61.0%
10/13/20 1130.00 3800.00 315.00 2140.00 306.00 221.00 7912.00 35.53 16.97 3129.81 85.2%76.1%
04/08/21 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 30.12 22.38 2303.25 26.4%82.4%
10/20/21 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 35.61 16.89 1738.24 24.5%86.7%
04/05/22 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 37.16 15.34 1578.72 9.2%88.0%
11/14/22 416.00 1820.00 203.00 1510.00 124.00 342.00 4415.00 36.80 15.70 1615.77 -2.3%87.7%
MW-1R 1380.00 12800.00 1700.00 13200.00 330.00 1060.00 30470.00 40.72
MW-8 182.00 499.00 130.00 477.00 0.00 28.40 1316.40 41.35
Avg.781.00 6649.50 915.00 6838.50 165.00 544.20 15893.20 41.04
MW-1R 1740.00 14600.00 1360.00 14000.00 255.00 992.00 32947.00 38.38
MW-8 206.00 531.00 164.00 604.00 0.00 13.80 1518.80 39.49
Avg.973.00 7565.50 762.00 7302.00 127.50 502.90 17232.90 38.94
MW-1R 1420.00 11200.00 1090.00 11500.00 448.00 1150.00 26808.00 36.93
MW-8 122.00 301.00 98.60 365.00 0.00 25.40 912.00 37.40
Avg.771.00 5750.50 594.30 5932.50 224.00 587.70 13860.00 37.17
MW-1R 1510.00 13000.00 1460.00 12200.00 553.00 1500.00 30223.00 36.23
MW-8 167.00 363.00 92.60 224.00 0.00 6.60 853.20 36.90
Avg.838.50 6681.50 776.30 6212.00 276.50 753.30 15538.10 36.57
MW-1R 742.00 11700.00 1440.00 12500.00 748.00 904.00 28034.00 32.60
MW-8 147.00 522.00 232.00 1120.00 0.00 82.50 2103.50 33.63
Avg.444.50 6111.00 836.00 6810.00 374.00 493.25 15068.75 33.12
MW-1R 332.00 10900.00 1660.00 14300.00 259.00 667.00 28118.00 31.72
MW-8 128.00 416.00 180.00 802.00 0.00 56.00 1582.00 32.32
Avg.230.00 5658.00 920.00 7551.00 129.50 361.50 14850.00 32.02
MW-1R 655.00 15600.00 1920.00 13100.00 403.00 720.00 32398.00 31.72
MW-8 8.40 11.50 4.70 12.10 0.00 1.10 37.80 32.68
Avg.331.70 7805.75 962.35 6556.05 201.50 360.55 16217.90 32.20
--- ---
5575.98 -29.2% -29.2%
10.97
13.0704/19/18
05/03/17 4315.92
Area 4 10/15/18
04/08/19
-37.6%
07/29/19 7952.68 -8.2% -84.3%
8.7%-18.0%
7047.71 -18.7% -63.3%
5939.61
08/13/18
01/22/19
-4.3%
-16.6%
18.89
7348.1119.98
19.80
5092.1914.84
15.44
-70.3%
OW-1Area 3
Page 2 of 4
Area ID Well IDs Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX H
CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
MW-1R 1050.00 17600.00 2250.00 13500.00 352.00 1080.00 35832.00 34.25
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 49.52
Avg.525.00 8800.00 1125.00 6750.00 176.00 540.00 17916.00 41.89
MW-1R 154.00 3740.00 430.00 5990.00 96.70 381.00 10791.70 34.21
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 35.40
Avg.77.00 1870.00 215.00 2995.00 48.35 190.50 5395.85 34.81
MW-1R 38.50 935.00 107.50 1497.50 24.18 95.25 2697.93 29.55
MW-8 57.75 1402.50 161.25 2246.25 36.26 142.88 4046.89 30.66
Avg.48.13 1168.75 134.38 1871.88 30.22 119.06 3372.41 30.11
MW-1R 58.40 610.00 55.90 2390.00 365.00 50.70 3530.00 28.78
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 29.64
Avg.29.20 305.00 27.95 1195.00 182.50 25.35 1765.00 29.21
MW-1R 16.10 100.00 11.70 90.50 286.00 3.10 507.40 34.18
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 49.70
Avg.8.05 50.00 5.85 45.25 143.00 1.55 253.70 41.94
MW-1R 128 1,930 176 2,190 682 107 5213.00 36.81
MW-8 0.00 0.34 0.00 0.59 0.00 0.00 0.93 37.63
Avg.64.00 965.17 88.00 1095.30 341.00 53.50 2606.97 37.22
MW-1R 16.4 177 19.1 308 677 15.2 1212.70 36.08
MW-8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 49.87
Avg.8.20 88.50 9.55 154.00 338.50 7.60 606.35 42.98
Date Average Water
Column Height (ft)
05/03/17 9.57
04/19/18 11.42
08/13/18 12.21
10/15/18 12.87
01/22/19 15.67
04/08/19 16.50
07/29/19 17.23
10/08/19 13.95
01/02/20 14.70
10/13/20 18.26
04/08/21 20.92
10/20/21 13.94
04/05/22 13.52
11/14/22 10.43
37,905 -151.6%30.3%
-25.5%9.0%
22.79 996.19 45.5% 76.9%
-37.8%
75,078
--- ---
-30.1% -30.1%
77.9%
81,742
-4.2%
14.78 954.25
0.8%-36.5%
73,717
55,938
-4.0%4488.08 43.6%10/08/19 10.12
04/05/22 -1409.7%
10/13/20
01/02/20
21.90 1828.68
04/08/21
98.5%93.7%63.2110.06
48.8% 46.8%2297.82
20.4% 57.6%
17.20
18.0%-2.8%
68,240
74,977
8.2%-38.0%
0.1%
-35.5%
-1.5%
-4.2% -42.3%
74,826
74,245
77,393
-37.6%
-5.6% -50.3%
85.8% 96.9%
Area 4
(cont.)
14,362 62.1%73.6%
11/14/22 9.03 135.53
15,065 73.1% 72.3%
10/20/21
Total Contaminant Mass
(grams)Percent Reduction Compared to
Previous Event
Percent Reduction To Date
54,391
70,765
Page 3 of 4
Area ID Well IDs Area
(ft²)
Average Well
Depth
(ft)
Average
Depth to
Water
(ft)
Water Column
Height
(ft)
Volume
(ft³)Volume (L) Effective Porosity
Effective
Volume (L)
1 MW-4 2,975 45.0 38.44 6.56 19,529 553,010 110,602
2 AS-2
OW-2 6,517 52.5 38.48 14.02 91,345 2,586,604 517,321
3 AS-3
OW-1 4,116 52.5 37.89 14.61 60,139 1,702,937 340,587
4
MW-1R
MW-8
AS-1
AS-4
AS-5
4,373 52.0 38.97 13.03 56,974 1,613,316 322,663
Area Date Well
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Xylenes
(µg/L)
MTBE
(µg/L)
Naphthalene
(µg/L)
Total
(µg/L)
DTW
(ft)
Average Water
Column Height
(ft)
Total Average
Mass (g)Percent Red. To Date Red.
APPENDIX H
CONTAMINANT MASS CALCULATIONS
HANDY STOP #7 (INCIDENT NO. 36069)
0.20
Baseline Event
Note:
• In areas containing free product, the last known contaminant mass without free product is used to calculate the total contaminant mass calculations.
• The air sparging wells have not been included in the total contaminant mass calculations due to the inability to sample the air sparging wells during future ground water sampling events.
• The telescoping wells have not been included in the total contaminant mass calculations due to the inability to calucate a volume.
• The percentage reduction for areas containing free product cannot be caluclated.
Page 4 of 4