MO-5392_18748_M_RP_20170303

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
February 28, 2017

Mr. Brad Newton
NCDEQ-DWM-UST Section
Mooresville Regional Office
610 East Center Avenue
Mooresville, NC 28115

Re: Water Supply Well Sampling Results
Gate #402
2520 Bessemer City Road
Bessemer City, Gaston County, NC
Ground Water Incident Number: 18748
GRI Project Number: 2451

Dear Mr. Newton:

Please find enclosed the referenced analytical results for three water supply wells sampled on February 20, 2017.
This sampling event was conducted per Task Authorization #18748-56 dated February 16, 2017, for the above
mentioned site. Geological Resources, Inc. sampled WSW-4 at 1053 Dallas-Bessemer City Highway, Bessemer
City, NC and WSW-9 at 523 Oates Road, Gastonia, NC. Water supply well WSW-10 at 101 Fraley Road, Gastonia,
NC was out of service. There was no electrical power on at the site and the residential structure there did not appear
to be inhabited. With the exception of the sample collected from WSW-4, all of the samples collected have
analytical results below the 2L Standard. The concentration of 1,2-Dichloroethane detected in the sample collected
from WSW-4 exceeded the 2L Standard.

If you have any questions, please contact me at [phone].

Sincerely,
Geological Resources, Inc.

W. Scott Ball
Sr. Project Manager

enclosures
cc: Ms. Marlene Talley, Gate Petroleum Company
Mr. Ken Czoer, Applied Science and Engineering
file
02/27/17
Technical Report for
GRI (Geological Resources Inc.)
Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
18748/2451
SGS Accutest Job Number: FA41430
Sampling Date: 02/20/17
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: Michael Senglaub
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 02/27/17
e-Hardcopy 2.0
Automated Report
20
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
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FA41430
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA41430-1: WSW-4 .....................................................................................................6
3.2: FA41430-2: WSW-9 .....................................................................................................8
Section 4: Misc. Forms ............................................................................................................10
4.1: Chain of Custody ...........................................................................................................11
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................14
5.1: Method Blank Summary ................................................................................................15
5.2: Blank Spike Summary ...................................................................................................17
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................19 123452 of 20
FA41430
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA41430
Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Project No: 18748/2451
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA41430-1 02/20/17 08:15 WB 02/21/17 AQ Water WSW-4
FA41430-2 02/20/17 08:39 WB 02/21/17 AQ Water WSW-9
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FA414301
Summary of Hits Page 1 of 1
Job Number:FA41430
Account:GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Collected:02/20/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA41430-1 WSW-4
Chloroform 0.20 J 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 0.52 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.24 J 0.50 0.13 ug/l SM 6200B
FA41430-2 WSW-9
Chloroform 0.41 J 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.27 J 0.50 0.13 ug/l SM 6200B
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FA414302
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
5 of 20
FA414303
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA41430-1 Date Sampled:02/20/17
Matrix:AQ - Water Date Received:02/21/17
Method:SM 6200B Percent Solids:n/a
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E051173.D 1 02/21/17 TD n/a n/a VE1700
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.20 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.52 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4143033.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA41430-1 Date Sampled:02/20/17
Matrix:AQ - Water Date Received:02/21/17
Method:SM 6200B Percent Solids:n/a
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.24 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4143033.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:WSW-9
Lab Sample ID:FA41430-2 Date Sampled:02/20/17
Matrix:AQ - Water Date Received:02/21/17
Method:SM 6200B Percent Solids:n/a
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E051174.D 1 02/21/17 TD n/a n/a VE1700
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 0.41 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4143033.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:WSW-9
Lab Sample ID:FA41430-2 Date Sampled:02/20/17
Matrix:AQ - Water Date Received:02/21/17
Method:SM 6200B Percent Solids:n/a
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.27 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4143033.2
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
10 of 20
FA414304
FA41430: Chain of Custody
Page 1 of 3
11 of 20
FA4143044.1
FA41430: Chain of Custody
Page 2 of 3
12 of 20
FA4143044.1
FA41430: Chain of Custody
Page 3 of 3
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FA4143044.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
14 of 20
FA414305
Method Blank Summary Page 1 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1700-MB E051163.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
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FA4143055.1.1
Method Blank Summary Page 2 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1700-MB E051163.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
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FA4143055.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1700-BS E051162.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.4 104 70-130
108-86-1 Bromobenzene 10 9.8 98 70-130
74-97-5 Bromochloromethane 10 9.2 92 70-130
75-27-4 Bromodichloromethane 10 9.3 93 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 9.3 93 70-130
98-06-6 tert-Butylbenzene 10 9.1 91 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 9.7 97 60-140
67-66-3 Chloroform 10 9.8 98 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.0 90 70-130
124-48-1 Dibromochloromethane 10 9.4 94 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.5 85 70-130
106-93-4 1,2-Dibromoethane 10 9.2 92 70-130
75-71-8 Dichlorodifluoromethane 10 10.2 102 60-140
95-50-1 1,2-Dichlorobenzene 10 9.2 92 70-130
541-73-1 1,3-Dichlorobenzene 10 9.4 94 70-130
106-46-7 1,4-Dichlorobenzene 10 9.1 91 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 10.2 102 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10 100 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.2 92 70-130
142-28-9 1,3-Dichloropropane 10 8.5 85 70-130
594-20-7 2,2-Dichloropropane 10 11.3 113 70-130
563-58-6 1,1-Dichloropropene 10 9.8 98 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.3 93 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
108-20-3 Di-Isopropyl Ether 10 9.5 95 70-130
100-41-4 Ethylbenzene 10 10.5 105 70-130
87-68-3 Hexachlorobutadiene 10 9.7 97 70-130
98-82-8 Isopropylbenzene 10 9.5 95 70-130
* = Outside of Control Limits.
17 of 20
FA4143055.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1700-BS E051162.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl Bromide 10 10.1 101 60-140
74-87-3 Methyl Chloride 10 10.7 107 60-140
74-95-3 Methylene Bromide 10 9.2 92 70-130
75-09-2 Methylene Chloride 10 9.1 91 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 70-130
91-20-3 Naphthalene 10 10.8 108 70-130
103-65-1 n-Propylbenzene 10 9.2 92 70-130
100-42-5 Styrene 10 9.7 97 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10 100 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.6 86 70-130
127-18-4 Tetrachloroethylene 10 9.8 98 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 9.1 91 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 11.7 117 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.8 98 70-130
75-01-4 Vinyl Chloride 10 10.3 103 60-140
m,p-Xylene 20 20.7 104 70-130
95-47-6 o-Xylene 10 9.2 92 70-130
1330-20-7 Xylene (total)30 29.9 100 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
18 of 20
FA4143055.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA41430-1MS E051178.D 1 02/21/17 TD n/a n/a VE1700
FA41430-1MSD E051179.D 1 02/21/17 TD n/a n/a VE1700
FA41430-1 E051173.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
FA41430-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.8 108 10 9.8 98 10 70-130/20
108-86-1 Bromobenzene ND 10 10.2 102 10 9.0 90 13 70-130/20
74-97-5 Bromochloromethane ND 10 9.4 94 10 8.8 88 7 70-130/20
75-27-4 Bromodichloromethane ND 10 9.0 90 10 7.8 78 14 70-130/20
75-25-2 Bromoform ND 10 7.5 75 10 6.3 63*17 70-130/20
104-51-8 n-Butylbenzene ND 10 10.3 103 10 9.0 90 13 70-130/20
135-98-8 sec-Butylbenzene ND 10 9.6 96 10 8.5 85 12 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.4 94 10 8.3 83 12 70-130/20
56-23-5 Carbon Tetrachloride ND 10 9.6 96 10 8.2 82 16 70-130/20
108-90-7 Chlorobenzene ND 10 9.4 94 10 8.5 85 10 70-130/20
75-00-3 Chloroethane ND 10 8.2 82 10 6.8 68 19 60-140/20
67-66-3 Chloroform 0.20 J 10 9.6 94 10 8.9 87 8 70-130/20
95-49-8 o-Chlorotoluene ND 10 10 100 10 8.8 88 13 70-130/20
106-43-4 p-Chlorotoluene ND 10 9.2 92 10 8.1 81 13 70-130/20
124-48-1 Dibromochloromethane ND 10 8.5 85 10 7.0 70 19 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.4 84 10 7.6 76 10 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.7 97 10 8.9 89 9 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.1 81 10 7.2 72 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 9.4 94 10 8.5 85 10 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 9.6 96 10 8.5 85 12 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.2 92 10 8.0 80 14 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.9 99 10 9.2 92 7 70-130/20
107-06-2 1,2-Dichloroethane 0.52 10 10 95 10 9.3 88 7 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.2 102 10 9.2 92 10 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.8 98 10 9.1 91 7 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10 100 10 9.0 90 11 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.5 95 10 8.7 87 9 70-130/20
142-28-9 1,3-Dichloropropane ND 10 8.9 89 10 8.2 82 8 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.7 107 10 9.4 94 13 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.6 96 10 8.7 87 10 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.5 85 10 7.4 74 14 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 8.9 89 10 7.7 77 14 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 9.5 95 10 8.8 88 8 70-130/20
100-41-4 Ethylbenzene ND 10 10.5 105 10 9.6 96 9 70-130/20
87-68-3 Hexachlorobutadiene ND 10 9.6 96 10 8.5 85 12 70-130/20
98-82-8 Isopropylbenzene ND 10 9.4 94 10 8.4 84 11 70-130/20
* = Outside of Control Limits.
19 of 20
FA4143055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA41430
Account:GRINCC GRI (Geological Resources Inc.)
Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA41430-1MS E051178.D 1 02/21/17 TD n/a n/a VE1700
FA41430-1MSD E051179.D 1 02/21/17 TD n/a n/a VE1700
FA41430-1 E051173.D 1 02/21/17 TD n/a n/a VE1700
The QC reported here applies to the following samples:Method: SM 6200B
FA41430-1, FA41430-2
FA41430-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.5 105 10 9.2 92 13 70-130/20
74-83-9 Methyl Bromide ND 10 7.0 70 10 5.5 55*24*60-140/20
74-87-3 Methyl Chloride ND 10 8.3 83 10 7.6 76 9 60-140/20
74-95-3 Methylene Bromide ND 10 9.5 95 10 8.8 88 8 70-130/20
75-09-2 Methylene Chloride ND 10 8.8 88 10 8.2 82 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 9.8 98 10 9.0 90 9 70-130/20
91-20-3 Naphthalene ND 10 10.9 109 10 10.2 102 7 70-130/20
103-65-1 n-Propylbenzene ND 10 9.5 95 10 8.2 82 15 70-130/20
100-42-5 Styrene ND 10 9.7 97 10 8.6 86 12 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.9 99 10 8.8 88 12 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.0 90 10 8.2 82 9 70-130/20
127-18-4 Tetrachloroethylene 0.24 J 10 10.3 101 10 9.0 88 13 70-130/20
108-88-3 Toluene ND 10 10.2 102 10 9.3 93 9 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.8 98 10 9.3 93 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10 100 10 9.1 91 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.3 93 10 8.3 83 11 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.2 92 10 8.7 87 6 70-130/20
79-01-6 Trichloroethylene ND 10 9.9 99 10 8.9 89 11 70-130/20
75-69-4 Trichlorofluoromethane ND 10 8.9 89 10 7.9 79 12 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 9.4 94 10 8.3 83 12 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.2 102 10 8.9 89 14 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.9 99 10 8.8 88 12 70-130/20
75-01-4 Vinyl Chloride ND 10 8.4 84 10 7.5 75 11 60-140/20
m,p-Xylene ND 20 21.0 105 20 18.6 93 12 70-130/20
95-47-6 o-Xylene ND 10 9.2 92 10 8.3 83 10 70-130/20
1330-20-7 Xylene (total)ND 30 30.2 101 30 26.9 90 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA41430-1 Limits
1868-53-7 Dibromofluoromethane 101%100%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%100%103%70-130%
2037-26-5 Toluene-D8 98%98%101%70-130%
460-00-4 4-Bromofluorobenzene 102%99%103%70-130%
* = Outside of Control Limits.
20 of 20
FA4143055.3.1