FA-88354_90172_CA_MRP_20211222

December 22, 2021
Mr. Kenneth Currie Hydrogeologist UST Section, Division of Waste Management North Carolina Department of Environmental Quality Systel Building, Suite 714 225 Green Street Fayetteville, North Carolina 28301
Re: 2020 Annual Groundwater Monitoring and AFVR Report Colonial Pipeline Company – Selma Station Incident Number: 90172 Site Ranking: I120D
Dear Mr. Currie:
On behalf of Colonial Pipeline Company, Apex Companies, LLC has prepared the attached Annual Groundwater Monitoring and Aggressive Fluid and Vapor Recovery (AFVR) Report. This report presents the combined results of the April and October 2020 groundwater sampling events and the
March and December 2020 AFVR events performed at the Colonial Pipeline Selma Station (Incident Number 90172).
If you have any questions or concerns, please do not hesitate to contact the undersigned at [phone].
Sincerely, Apex Companies, LLC
Jamie Moran Tom Nauman, P.G. Assistant Project Manager Senior Scientist NC License No. 2405
Enclosure
cc: Maribeth Hughes, Colonial Pipeline Company Jeff Morrison, Colonial Pipeline Company
Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page i

TABLE OF CONTENTS
1.0 INTRODUCTION ........................................................................................................................................... 1 
1.1 Site Background ........................................................................................................................ 1 
2.0 FIELD ACTIVITIES ........................................................................................................................................ 2 
2.1 Groundwater Gauging and LNAPL Thickness Measurements ............................................... 2 
2.2 Groundwater Investigation Activities and Results ................................................................... 2 
2.3 Aggressive Fluid Vapor and LNAPL Recovery Activities and Results .................................... 3 
3.0 WASTE HANDLING ...................................................................................................................................... 5 
4.0 CONCLUSIONS AND RECOMMENDATIONS ........................................................................................... 5 

Tables
Table 1: Summary of Groundwater Elevation Data
Table 2a: Summary of Groundwater Analytical Results – VOCs
Table 2b: Summary of Groundwater Analytical Results – Hydrocarbon Fractions
Table 3a: AFVR Field Data Sheet – March 2020
Table 3b: AFVR Field Data Sheet – December 2020
Table 4a: Summary of AFVR Effluent Sample Analytical Results – March 2020
Table 4b: Summary of AFVR Effluent Sample Analytical Results – December 2020
Table 5a: Vapor Phase Mass Removal Calculations – March 2020
Table 5b: Vapor Phase Mass Removal Calculations – December 2020
Table 6: Proposed Groundwater Monitoring Plan Summary
Figures
Figure 1: Site Location Map
Figure 2: Site Plan
Figure 3: Groundwater Potentiometric Surface Map – Surficial Aquifer (October 2020)
Figure 4: Groundwater Analytical Results – Detected Analytes (May & October 2020)
Appendices
Appendix A: Groundwater Sampling Logs
Appendix B: Laboratory Analytical Reports
Appendix C: Tank Specific Conversion Table
Appendix D: Waste Manifests
Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page 1

1.0 INTRODUCTION
This annual monitoring report presents the results of the May and October 2020 semiannual
groundwater monitoring events, as well as results of the March and December 2020 aggressive fluid
vapor recovery (AFVR) events performed at the Colonial Pipeline Company (CPC) Selma Station
located at 2335 West Oak Street in Selma, North Carolina (the ‘site’). Apex Companies, LLC
(Apex) prepared this report on behalf of CPC for submittal to the North Carolina Department of
Environmental Quality (NCDEQ).

A Site Location Map is provided as Figure 1. The site consists of one aboveground storage tank for
the transfer of refined petroleum products, pipelines, a manifold yard, a control building, and
associated above- and below-ground piping, as shown on the Site Plan on Figure 2.
1.1 Site Background

On September 5, 2013 dead vegetation and an odor were reported at the Site. Emergency response
actions were initiated, which included shutting down all delivery/shipper lines running through the
affected area of the site and locking out all associated valves. During initial emergency response
activities between September 5-18, 2013, approximately 60 gallons of gasoline and approximately
1,600 tons of soil were removed from the suspected release area. CPC estimates that approximately
200 gallons of gasoline were released. The release was assigned Incident Number 90172 by the
NCDEQ.
No apparent leaks were observed in the underground delivery/shipper lines exposed during the initial
excavation activities; however, a corroded section of pipe was discovered in the excavated area.
Physical inspection of the corroded area revealed significant pitting and the pipe was subsequently
repaired. On September 10, 2013, the three delivery/shipper lines were pressure tested. One of the
lines maintained pressure for the duration of the test and was cleared to return to service but the
other two lines did not maintain pressure during the test. The pressure loss was attributed to leaking
valves. On September 11, 2013, an acoustic emission test was conducted on the two lines that did
not pass the pressure test. The test results did not indicate evidence of a leak in either line. The
area that exhibited the highest noise during the acoustic emission test was excavated but no
evidence of a leak was identified in that area.
Following the results of the acoustic emission testing, additional excavation activities conducted
between September 13-18, 2013 extended the excavation trench along the pipeline to a total length
of 210 feet. Between September 24-26, 2013, the impacted soil was transported to Soilworks, Inc., a
permitted soil disposal facility in Selma, North Carolina. Following completion of excavation
activities, the trench was backfilled with clean fill and the area was restored.
An Initial Assessment Report was submitted to NCDEQ on April 6, 2015, and a Comprehensive Site
Assessment (CSA) Report was submitted to NCDEQ on October 29, 2015. A CAP proposing AFVR
technology combined with MNA to address petroleum impacted soil and groundwater at the site was
submitted to NCDEQ on October 2, 2018 and was approved by the agency on November 5, 2018.
Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page 2

The site is currently classified as intermediate risk because several dissolved phase constituents of
concern (COCs), including benzene, ethylbenzene, naphthalene, toluene, and xylenes, exceed the
NCAC 2B Surface Water Standards (2B Standards) by a factor of ten in the shallow, unconfined
aquifer, and because an unlined retention pond is located on the adjacent property approximately
500 feet in the direction of groundwater flow from the source area. Mill Creek, the receiving surface
water for the retention pond, is located approximately 1,500 feet downgradient of the source area.
Mill Creek is classified by NCDEQ Division of Water Resources as a Water Supply Class IV surface
water body.
2.0 FIELD ACTIVITIES
The following sections provide a summary of the field methods used for the May and October 2020
semiannual groundwater monitoring events, as well as the AFVR events performed in March and
December 2020.
2.1 Groundwater Gauging and LNAPL Thickness Measurements

Prior to sampling, groundwater monitoring wells were gauged to measure the depth to groundwater
and for the presence of light non-aqueous phase liquid (LNAPL). Upon arriving at the site, wells
were opened and allowed to equilibrate. Wells were gauged and later sampled in accordance with
the United States Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support Division Field Branches Quality System and Technical Procedures. Depths to groundwater
and LNAPL were measured using an electronic oil/water interface probe, with a measurement
accuracy of 0.01 feet (ft.). The interface probe was thoroughly decontaminated before collecting
measurements at each subsequent monitoring well.

On May 27, 2020 and October 20, 2020, twelve monitoring wells (AP-1, AP-2, AP-2D, AP-3, AP-4,
AP-5, AP-6, AP-7, AP-8, AP-9, AP-10, and AP-11) were gauged. The location of each monitoring
well is shown on Figure 2.
2.2 Groundwater Investigation Activities and Results

Semiannual groundwater sampling was performed at the site on May 27, 2020 and October 20,
2020. During both 2020 sampling events, groundwater samples were collected from nine monitoring
wells (AP-1, AP-2, AP-3, AP-4, AP-5, AP-8, AP-9, AP-10, and AP-11).

At each monitoring well location, a baseline set of water quality parameters (temperature, pH,
specific conductivity, dissolved oxygen, and turbidity) were measured using a Hanna 9829 water
quality meter and a Hach 2100Q turbidimeter. A minimum of three well volumes were purged from
each well using a disposable bailer before sample collection. Groundwater sampling logs
documenting the groundwater purging and sampling are included as Appendix A.

After purging an adequate volume of water from each well, a sample was collected in laboratory
supplied bottle ware and placed on ice in a cooler. Samples were submitted for analysis of benzene,
toluene, ethylbenzene, xylenes (BTEX) and naphthalene by EPA Method 6200B. Groundwater
samples collected on October 20, 2020 were also submitted for laboratory analysis of volatile
Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page 3

petroleum hydrocarbons (VPH) in accordance with Massachusetts Department of Environmental
Protection (MADEP) Method. Samples were submitted under standard chain-of-custody procedures
to Shealy Environmental Services, Inc (Shealy), a North Carolina-certified laboratory.

Two quality assurance/quality control samples were collected and analyzed for BTEX and
naphthalene using EPA Method 6200B and VPH via MADEP Method. During the May 27, 2020 and
October 20, 2020 sampling events, DUP-1 was collected as a duplicate sample of AP-9 and AP-11,
respectively. One equipment blank (EB-1) was collected following the completion of sampling
activities during both sampling events by pouring de-ionized water over a decontaminated interface
probe.

Groundwater gauging results collected on May 27, 2020 and October 20, 2020 are summarized in
Table 1. LNAPL was not detected in either gauging event. Depth to water and top of well casing
elevations were used to determine groundwater potentiometric elevations relative to an on-site
benchmark referenced to mean sea level datum. For shallow wells that are screened across the
water table surface, the groundwater potentiometric surface is approximately equal to the water table
elevation.

Groundwater potentiometric surface maps for the surficial aquifer unit were developed for the site
based on the October 20, 2020 gauging data (Figure 3). The potentiometric surface map indicates
that groundwater flows in a multi-directional pattern primarily toward the south, southwest, and
southeast which is consistent with historical data.

Groundwater analytical results for volatile organic compounds and hydrocarbon fractions during the
May and October 2020 sampling events are summarized along with historical analytical results in
Table 2a and Table 2b, respectively. Laboratory analytical reports and chain-of-custody records are
provided in Appendix B.
2.3 Aggressive Fluid Vapor and LNAPL Recovery Activities and Results

Eight-hour AFVR events were conducted on March 5, 2020 and December 15, 2020. Prior to
initiating AFVR activities, monitoring wells AP-3, AP-4, AP-5, AP-8, and AP-11 were gauged using
an electronic oil/water interface probe capable of detecting depth to water (DTW) and LNAPL (if
present) to an accuracy of 0.01 feet.

A vacuum truck operated by Legacy Environmental Services, LLC (Legacy) was mobilized to the
site. The vacuum truck was attached to the extraction well (AP-11) using vacuum hoses and a
piping manifold system. A drop tube was inserted into the extraction well, approximately six inches
below the water table surface and an airtight seal was established on the top of the well. The drop
tube depth was adjusted periodically during the AFVR event.

During the AFVR events, peripheral responses to the vacuums and fluid drawdowns were
monitored at nearby wells not used for direct fluid extraction. Vacuum readings as well as DTW
measurements at the peripheral wells (AP-3, AP-4, AP-5, and AP-8) were recorded every half hour
for the first two hours and every hour thereafter.
Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page 4

During both the March and December AFVR events, one vacuum truck tank effluent air sample
(collected at sample location AP-11) was collected for analysis of volatile organic compounds by EPA
Method TO-15 approximately 15 minutes after initiating the AFVR event. A second air sample
(collected from sample location AP-11) was collected near the end of the 8-hour AFVR event. Air
samples were collected in individual six-liter Summa canisters and submitted under chain-of-custody
procedures to Pace Analytical Services, LLC, a North Carolina-certified laboratory.

The air emissions from the vacuum truck tank were also qualitatively tested for volatile organic
vapors using a photoionization detector (PID), and airflow rates were recorded using a digital
anemometer. Following completion of the AFVR pilot test, temporary equipment was removed from
the extraction well and peripheral observations wells and DTW measurements were collected from
the extraction well and peripheral wells. The volume of fluid recovered in the vacuum truck after
the 8-hour AFVR event was also measured and recorded. Field data is summarized in Table 3a
and 3b.

During the March 2020 and December 2020 AFVR events, approximately 860 and 653 gallons of
petroleum impacted water were recovered respectively. The total liquid removed was determined by
lowering a measuring stick inside the tank of the vacuum truck and recording the depth of liquid. A
tank specific calibration curve table was then used to convert the depth measurements to gallons. A
copy of the tank-specific conversion table is provided as Appendix C.

The air sample analytical data were evaluated to assess the vapor recovery rates during the AFVR
event and to calculate the total volume of vapor-phase petroleum hydrocarbons removed, expressed
in equivalent gallons of gasoline. Summaries of the March 2020 and December 2020 air sampling
results are provided in Table 4a and Table 4b, respectively, and laboratory reports are included as
Appendix B. Vapor mass removal calculations are provided in Table 5a and Table 5b for March
2020 and December 2020 events.

Approximately 0.73 pounds (0.117 gallons) of vapor-phase petroleum hydrocarbons (as gasoline)
were removed during the March 2020 AFVR event. Comparison of the March 2020 air samples
collected within the first 30 minutes and the within the last 30 minutes of the AFVR event indicated a
reduction in vapor-phase VOC recovery rates after eight hours of AFVR duration.

Approximately 6.44 pounds (1.03 gallons equivalent) of vapor-phase petroleum hydrocarbons (as
gasoline) were removed during the December 2020 AFVR event. Comparison of the December
2020 air samples collected within the first 30 minutes and the within the last 30 minutes of the AFVR
event indicated an increase in vapor-phase VOC recovery rates after eight hours of AFVR duration.
This is most likely the result of a change in sample location. The initial air sample was collected from
the vacuum blower. Due to equipment malfunction during the AFVR event, the final air sample
location was changed to the vacuum pump.

Colonial Pipeline Company – Selma Station December 22, 2021
2020 Annual Groundwater Monitoring and AFVR Report Page 5
3.0 WASTE HANDLING
Wastes generated during the AFVR tests were contained within the vacuum truck. Following the
completion of each AFVR pilot test the total liquid contained within the vacuum truck was measured.
LNAPL was not present. A tank specific conversion table was used to convert the depth of liquid in
the vacuum truck to gallons (Appendix C). Waste was transported by Legacy to the Legacy Facility at
3637 N. Graham Street, Charlotte, Mecklenburg County, North Carolina, a North Carolina-permitted
waste handling facility. The waste manifests are included in Appendix D.
4.0 CONCLUSIONS AND RECOMMENDATIONS
Apex conducted semi-annual groundwater monitoring in May and October of 2020, as well as AFVR
events performed in March and December 2020. Results of these activities indicate:
LNAPL was not detected in any wells during the reporting period. LNAPL has not been
detected in any wells for over 7 years.
Groundwater exceedances of NCAC 2L Standards in Benzene, Ethylbenzene, Naphthalene,
Toluene, and Xylenes (Total)
Approximately 860 gallons of petroleum impacted groundwater were recovered from
extraction well AP-11 during the March 2020 AFVR event.
Approximately 653 gallons of petroleum impacted groundwater were recovered from
extraction well AP-11 during the December 2020 AFVR event.
Approximately 0.73 pounds (0.117 gallons equivalent) of vapor-phase petroleum
hydrocarbons (as gasoline) were removed during the March 2020 AFVR event.
Approximately 6.44 pounds (1.03 gallons equivalent) of vapor-phase petroleum hydrocarbons
(as gasoline) were removed during the December 2020 AFVR event.
AP-11 will continue to be the primary extraction point; however, additional wells (i.e., AP-4) may be
added as extraction wells utilizing a manifold system so that a vacuum can be applied to multiple
extraction wells simultaneously. Semiannual groundwater monitoring events will be performed
approximately 30 days following each AFVR event. Semiannual groundwater monitoring events are
proposed for completion in April and October of each year, and a submittal of an annual groundwater
monitoring and AFVR report is proposed by December 31st of each year. A summary of the
proposed semiannual groundwater sampling program is provided as Table 6.

TABLES
Table 1
Summary of Groundwater Elevation Data
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
6/12/2014 --5.72 -- 150.96
12/10/2014 --5.76 -- 150.92
12/31/2014 --4.33 -- 152.35
8/27/2015 --7.48 -- 149.20
6/1/2016 --4.57 -- 152.11
2/13/2019 --3.24 -- 153.44
10/16/2019 --7.97 -- 148.71
5/27/2020 --3.70 -- 152.98
10/20/2020 --4.20 -- 152.48
6/12/2014 --5.61 -- 152.65
12/10/2014 --5.18 -- 153.08
12/31/2014 --3.96 -- 154.30
8/27/2015 --7.71 -- 150.55
6/1/2016 --4.37 -- 153.89
2/13/2019 --2.85 -- 155.41
10/16/2019 --5.98 -- 152.28
5/27/2020 --4.00 -- 154.26
10/20/2020 --3.88 -- 154.38
8/27/2015 --8.45 -- 149.76
6/1/2016 --4.74 -- 153.47
2/13/2019 --5.37 -- 152.84
10/16/2019 --6.19 -- 152.02
5/27/2020 --5.35 -- 152.86
10/20/2020 --4.89 -- 153.32
12/31/2014 --4.32 -- 153.36
8/27/2015 --7.78 -- 149.90
6/1/2016 --4.60 -- 153.08
2/13/2019 --2.75 -- 154.93
6/20/2019 --4.07 -- 153.61
10/16/2019 --6.60 -- 151.08
5/27/2020 --3.55 -- 154.13
10/20/2020 --4.11 -- 153.57
12/31/2014 --4.30 -- 153.56
8/27/2015 --7.81 -- 150.05
6/1/2016 --4.19 -- 153.67
2/13/2019 --2.63 -- 155.23
6/20/2019 --3.68 -- 154.18
10/16/2019 --NM -- NM
5/27/2020 --3.43 -- 154.43
10/20/2020 --3.80 -- 154.06
Corrected
Groundwater
Elevation
(ft. MSL)
Well No.
Top of Casing
Elevation
(ft. MSL)
Depth to
LNAPL
(ft. TOC)
Depth to
Groundwater
(ft. TOC)
LNAPL
Thickness
(ft.)
Date
AP-1 156.68
AP-2 158.26
158.21AP-2D
AP-3 157.68
AP-4 157.86
Page 1 of 3
Table 1
Summary of Groundwater Elevation Data
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Corrected
Groundwater
Elevation
(ft. MSL)
Well No.
Top of Casing
Elevation
(ft. MSL)
Depth to
LNAPL
(ft. TOC)
Depth to
Groundwater
(ft. TOC)
LNAPL
Thickness
(ft.)
Date
12/31/2014 --3.97 -- 154.59
8/27/2015 --7.85 -- 150.71
6/1/2016 --5.48 -- 153.08
2/13/2019 --3.57 -- 154.99
6/20/2019 --5.55 -- 153.01
10/16/2019 --6.36 -- 152.20
5/27/2020 --3.50 -- 155.06
10/20/2020 --4.87 -- 153.69
12/31/2014 --2.06 -- 156.84
8/27/2015 --5.60 -- 153.30
6/1/2016 --2.77 -- 156.13
2/13/2019 --3.13 -- 155.77
10/16/2019 --2.48 -- 156.42
5/27/2020 --1.99 -- 156.91
10/20/2020 --2.19 -- 156.71
8/27/2015 --8.88 -- 151.12
6/1/2016 --5.24 -- 154.76
2/13/2019 --4.22 -- 155.78
10/16/2019 --7.04 -- 152.96
5/27/2020 --5.02 -- 154.98
10/20/2020 --4.81 -- 155.19
8/27/2015 --8.55 -- 150.22
6/1/2016 --6.59 -- 152.18
2/13/2019 --4.13 -- 154.64
6/20/2019 --5.11 -- 153.66
10/16/2019 --6.00 -- 152.77
5/27/2020 --4.56 -- 154.21
10/20/2020 --4.20 -- 154.57
8/27/2015 --7.76 -- 149.13
6/1/2016 --4.76 -- 152.13
2/13/2019 --3.44 -- 153.45
10/16/2019 --NM -- NM
5/27/2020 --3.80 -- 153.09
10/20/2020 --4.22 -- 152.67
8/27/2015 --8.13 -- 150.02
6/1/2016 --4.92 -- 153.23
2/13/2019 --3.40 -- 154.75
10/16/2019 --6.60 -- 151.55
5/27/2020 --3.80 -- 154.35
10/20/2020 --4.39 -- 153.76
158.15AP-10
AP-5 158.56
AP-6 158.90
AP-7 160.00
AP-8 158.77
AP-9 156.89
Page 2 of 3
Table 1
Summary of Groundwater Elevation Data
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Corrected
Groundwater
Elevation
(ft. MSL)
Well No.
Top of Casing
Elevation
(ft. MSL)
Depth to
LNAPL
(ft. TOC)
Depth to
Groundwater
(ft. TOC)
LNAPL
Thickness
(ft.)
Date
6/1/2016 --5.07 -- 153.22
2/13/2019 --4.11 -- 154.18
6/20/2019 --4.40 -- 153.89
10/16/2019 --6.63 -- 151.66
5/27/2020 --4.44 -- 153.85
10/20/2020 --4.55 -- 153.74
MW-7* 161.72 6/11/2014 --9.77 -- 151.95
Notes:
ft. - Feet
MSL - Mean Sea Level
TOC - Top of Casing
-- - Not Detected
LNAPL - Light Non-aqueous Phase Liquid
*MW-7 is located on the adjacent Marathon property. Gauging data supplied by others.
AP-11 158.29
Page 3 of 3
Table 2a
Summary of Groundwater Analytical Results - VOCs
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Benzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloromethaneDiisopropyl EtherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone (MIBK)Methyl-tert-Butyl EtherNaphthalenen-PropylbenzeneStyreneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)Date
Collected
Depth to
Water
(DTW)µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
5,000 4,000,000 6,900 8,500 3,000 70,000 84,500 25,000 11,700 5,000 100,000 20,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
1.19 20,000*3.9*NE 2.6*20,000*68**250*320*20**2,800*19*12*80*NE 11 390*130*670*
1 4,000 70 70 3 NE 600 70 25 5 100 20 6 70 70 600 400 400 500
06/12/14 5.72 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.47 J ND ND ND
12/10/14 5.76 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
Duplicate (AP-1)12/10/14 AP-1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
08/27/15 7.48 ND NS ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND ND ND
02/13/19 3.24 290 NS NS NS NS NS 0.44 J NS NS NS NS NS 7.6 NS NS 1.2 NS NS 19
10/16/19 7.97 280 NS NS NS NS NS <1.2 NS NS NS NS NS 10 NS NS <1.2 NS NS 1.3J
05/27/20 3.70 <0.50 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
10/20/20 4.20 179 NS NS NS NS NS <2.0 NS NS NS NS NS 1.3 J NS NS 1.4 J NS NS <2.0
06/12/14 5.61 2,620 ND ND ND ND ND 297 11.3 J ND 40.2 J ND 7.9 J 48.6 J 27.8 ND 840 251 66.7 1,879
12/10/14 5.18 1,890 ND ND ND ND ND 278 ND ND ND ND 3.9 ND ND 1.1 464 199 68 1,590
08/27/15 7.71 1,200 NS ND ND ND ND 110 12 ND ND NS ND 29 18 ND 300 59 69 750
Duplicate (AP-2)08/27/15 7.71 1,300 NS ND ND ND ND 120 ND ND ND NS ND 37 20 J ND 320 67 71 750
06/01/16 4.37 1,700 NS 19 <10 <10 <10 480 25 12 <10 NS <10 79 70 <10 240 480 140 1,005
02/13/19 2.85 1,300 NS NS NS NS NS 490 NS NS NS NS NS 94 NS NS 760 NS NS 1,100
10/16/19 5.98 609 NS NS NS NS NS 242 NS NS NS NS NS 55.6 NS NS 92.3 NS NS 350
05/27/20 4.00 180 NS NS NS NS NS 130 NS NS NS NS NS 23 NS NS 43 NS NS 77
10/20/20 3.88 498 NS NS NS NS NS 220 NS NS NS NS NS 49.1 NS NS 159 NS NS 478
Gross Contamination Levels
NCAC 2B Standards (Class WS Waters)
AP-2
AP-1
Analytical Method Volatile Organic Compounds
Sample ID
Constituent of
Concern
NCAC 2L Standards
AP-1
AP-2
Page 1 of 5
Table 2a
Summary of Groundwater Analytical Results - VOCs
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Benzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloromethaneDiisopropyl EtherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone (MIBK)Methyl-tert-Butyl EtherNaphthalenen-PropylbenzeneStyreneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)Date
Collected
Depth to
Water
(DTW)µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
5,000 4,000,000 6,900 8,500 3,000 70,000 84,500 25,000 11,700 5,000 100,000 20,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
1.19 20,000*3.9*NE 2.6*20,000*68**250*320*20**2,800*19*12*80*NE 11 390*130*670*
1 4,000 70 70 3 NE 600 70 25 5 100 20 6 70 70 600 400 400 500
Gross Contamination Levels
NCAC 2B Standards (Class WS Waters)
Analytical Method Volatile Organic Compounds
Sample ID
Constituent of
Concern
NCAC 2L Standards
08/27/15 8.45 2.8 NS ND ND ND ND ND ND ND ND NS ND 0.42 J ND ND 0.73 ND ND 1.97
06/01/16 4.74 1.1 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0
02/13/19 5.37 1.0 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
AP-3 12/31/14 4.32 294 ND ND ND 2.8 0.24 J 19.9 ND ND ND 0.90 J ND 2.7 ND ND 43.1 ND ND 142
Duplicate (AP-3)12/31/14 4.32 288 ND ND ND 2.9 0.24 J 20.3 ND ND ND ND ND 3.1 ND ND 42.3 ND ND 143
08/27/15 7.78 840 NS ND ND ND ND 150 5.7 ND ND NS ND 22 16 ND 600 78 30 570
06/01/16 4.60 120 NS <0.50 <0.50 <0.50 <0.50 2.4 <0.50 <0.50 <0.50 NS <0.50 <0.50 0.17 J <0.50 1.2 0.69 0.32 J 35
02/13/19 2.75 5.5 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS 0.42 J
06/20/19 4.07 7.3 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS 0.77
10/16/19 6.60 6.2 NS NS NS NS NS 1.4 NS NS NS NS NS <2.0 NS NS 2.2 NS NS 5.6
05/27/20 3.55 4.0 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
10/20/20 4.11 2.2 NS NS NS NS NS <1.0 NS NS NS NS NS 2.0 NS NS <1.0 NS NS <1.0
12/31/14 4.30 947 ND ND ND 8.1 0.91 J 61.6 ND ND ND ND 0.79 J 22.3 ND ND 119 ND ND 417
08/27/15 7.81 750 NS ND ND ND ND 82 3.5 ND ND NS 1.0 J 15 7.6 ND 280 55 14 460
06/01/16 4.19 95 NS <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NS <0.50 <0.50 <0.50 <0.50 0.48 J <0.50 <0.50 <1.0
02/13/19 2.63 31 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS 0.49 J
06/20/19 3.68 160 NS NS NS NS NS 110 NS NS NS NS NS 20 NS NS 330 NS NS 670
10/16/19 NM 0.70 NS NS NS NS NS <0.50 NS NS NS NS NS <2.0 NS NS <0.50 NS NS <1.0
05/27/20 3.43 35 NS NS NS NS NS 0.77 NS NS NS NS NS <0.50 NS NS <0.50 NS NS 1.9
10/20/20 3.80 37.7 NS NS NS NS NS 6.0 NS NS NS NS NS 3.4 NS NS <1.0 NS NS 8.4
AP-2D
AP-4
AP-3
Page 2 of 5
Table 2a
Summary of Groundwater Analytical Results - VOCs
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Benzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloromethaneDiisopropyl EtherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone (MIBK)Methyl-tert-Butyl EtherNaphthalenen-PropylbenzeneStyreneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)Date
Collected
Depth to
Water
(DTW)µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
5,000 4,000,000 6,900 8,500 3,000 70,000 84,500 25,000 11,700 5,000 100,000 20,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
1.19 20,000*3.9*NE 2.6*20,000*68**250*320*20**2,800*19*12*80*NE 11 390*130*670*
1 4,000 70 70 3 NE 600 70 25 5 100 20 6 70 70 600 400 400 500
Gross Contamination Levels
NCAC 2B Standards (Class WS Waters)
Analytical Method Volatile Organic Compounds
Sample ID
Constituent of
Concern
NCAC 2L Standards
12/31/14 3.97 454 2.6 J ND ND 3.2 0.38 J 54.5 ND ND ND ND 0.56 J 10.8 ND 0.35 J 145 ND ND 292
08/27/15 7.85 970 NS ND ND ND ND 170 9.3 J ND ND NS ND 22 14 ND 360 76 19 590
06/01/16 5.48 550 NS <2.5 <2.5 <2.5 <2.5 110 3.7 <2.5 <2.5 NS <2.5 18 8.9 <2.5 80 70 15 430
DUP-1 (AP-5)06/01/16 5.48 580 NS <2.5 <2.5 <2.5 <2.5 120 4.1 <2.5 <2.5 NS <2.5 20 9.1 <2.5 100 73 16 460
02/13/19 3.57 82 NS NS NS NS NS 76 NS NS NS NS NS 12 NS NS 0.53 NS NS 210
06/20/19 4.79 79 NS NS NS NS NS 140 NS NS NS NS NS 35 NS NS 29 NS NS 470
10/16/19 6.36 92.6 NS NS NS NS NS 118 NS NS NS NS NS 29.2 NS NS 14.4 NS NS 456
05/27/20 3.50 42 NS NS NS NS NS 80 NS NS NS NS NS 17 NS NS 17 NS NS 280
10/20/20 4.87 41.5 NS NS NS NS NS 96.3 NS NS NS NS NS 26.4 NS NS 3.3 NS NS 269
12/31/14 2.06 0.83 J ND ND ND ND ND 0.38 J ND ND ND ND ND 0.59 J ND ND 0.53 J ND ND 2.29 J
08/27/15 8.64 ND NS ND ND ND ND ND ND ND ND NS ND 0.47 J ND ND ND ND ND ND
02/13/19 3.13 <0.50 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
08/27/15 8.88 310 NS ND ND ND ND 210 10 ND ND NS ND 38 29 ND 970 220 60 1,250
06/01/16 5.24 940 NS <25 <25 <25 <25 1,000 52 <25 <25 NS <25 160 160 <25 2,300 1,200 280 3,870
02/13/19 4.22 130 NS NS NS NS NS 670 NS NS NS NS NS 110 NS NS 52 NS NS 780
DUP-1 (AP-7)02/13/19 4.22 130 NS NS NS NS NS 670 NS NS NS NS NS 110 NS NS 59 NS NS 860
AP-5
AP-6
AP-7
AP-5
Page 3 of 5
Table 2a
Summary of Groundwater Analytical Results - VOCs
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Benzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloromethaneDiisopropyl EtherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone (MIBK)Methyl-tert-Butyl EtherNaphthalenen-PropylbenzeneStyreneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)Date
Collected
Depth to
Water
(DTW)µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
5,000 4,000,000 6,900 8,500 3,000 70,000 84,500 25,000 11,700 5,000 100,000 20,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
1.19 20,000*3.9*NE 2.6*20,000*68**250*320*20**2,800*19*12*80*NE 11 390*130*670*
1 4,000 70 70 3 NE 600 70 25 5 100 20 6 70 70 600 400 400 500
Gross Contamination Levels
NCAC 2B Standards (Class WS Waters)
Analytical Method Volatile Organic Compounds
Sample ID
Constituent of
Concern
NCAC 2L Standards
08/27/15 8.55 240 NS ND ND ND ND 63 3.9 ND ND NS ND 1.8 J 6.7 ND 35 39 16 330
06/01/16 6.59 2,500 NS <25 9.9 J <25 <25 1,800 71 <25 12 J NS <25 280 220 <25 6,800 1,600 410 8,400
02/13/19 4.13 710 NS NS NS NS NS 2,200 NS NS NS NS NS 420 NS NS 110 NS NS 6,500
06/20/19 5.11 520 NS NS NS NS NS 2,200 NS NS NS NS NS 500 NS NS 89 NS NS 6,000
10/16/19 6.00 311 NS NS NS NS NS 1,180 NS NS NS NS NS 355 NS NS 53.4 NS NS 2,500
05/27/20 4.56 200 NS NS NS NS NS 1,300 NS NS NS NS NS 290 NS NS <25 NS NS 2,000
10/20/20 4.20 130 NS NS NS NS NS 884 NS NS NS NS NS 355 NS NS <5.0 NS NS 963
08/27/15 7.76 ND NS ND ND ND ND ND ND ND ND NS ND ND ND ND 0.39 J ND ND ND
02/13/19 3.44 <0.50 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
10/16/19 Not sampled as well was submerged in water
05/27/20 3.80 <0.50 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
DUP-1 (AP-9)05/27/20 3.80 <0.50 NS NS NS NS NS <0.50 NS NS NS NS NS <0.50 NS NS <0.50 NS NS <0.50
AP-9 10/20/20 4.22 <1.0 NS NS NS NS NS <1.0 NS NS NS NS NS <1.0 NS NS <1.0 NS NS <1.0
08/27/15 8.13 ND NS ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND ND ND
02/13/19 3.40 910 NS NS NS NS NS 95 NS NS NS NS NS 12 NS NS 33 NS NS 120
10/16/19 6.60 870 NS NS NS NS NS 119 NS NS NS NS NS 19.8 NS NS 31.7 NS NS 151
05/27/20 3.80 1,200 NS NS NS NS NS 310 NS NS NS NS NS 44 NS NS 59 NS NS 330
10/20/20 4.39 1,100 NS NS NS NS NS 274 NS NS NS NS NS 43.6 NS NS 25.7 NS NS 213
AP-10
AP-9
AP-8
Page 4 of 5
Table 2a
Summary of Groundwater Analytical Results - VOCs
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Benzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneChloromethaneDiisopropyl EtherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone(MIBK)Methyl-tert-Butyl EtherNaphthalenen-PropylbenzeneStyreneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (Total)Date
Collected
Depth to
Water
(DTW)µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
5,000 4,000,000 6,900 8,500 3,000 70,000 84,500 25,000 11,700 5,000 100,000 20,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
1.19 20,000*3.9*NE 2.6*20,000*68**250*320*20**2,800*19*12*80*NE 11 390*130*670*
1 4,000 70 70 3 NE 600 70 25 5 100 20 6 70 70 600 400 400 500
Gross Contamination Levels
NCAC 2B Standards (Class WS Waters)
Analytical Method Volatile Organic Compounds
Sample ID
Constituent of
Concern
NCAC 2L Standards
06/01/16 5.07 7,500 NS <100 <100 <100 <100 2,700 90 J <100 <100 NS <100 450 250 <100 29,000 2,200 510 19,000
02/13/19 4.11 2,000 NS NS NS NS NS 2,900 NS NS NS NS NS 540 NS NS 15,000 NS NS 18,000
06/20/19 4.43 270 NS NS NS NS NS 660 NS NS NS NS NS 310 NS NS 200 NS NS 4,700
DUP 062019 (AP-11)06/20/19 4.43 240 NS NS NS NS NS 560 NS NS NS NS NS 290 NS NS 180 NS NS 4,000
10/16/19 6.63 168 NS NS NS NS NS 560 NS NS NS NS NS 212 NS NS 498 NS NS 2,750
05/27/20 4.44 77 NS NS NS NS NS 460 NS NS NS NS NS 170 NS NS 23 NS NS 1,700
10/20/20 4.55 62.5 NS NS NS NS NS 556 NS NS NS NS NS 250 NS NS 62.8 NS NS 713
DUP-1 (AP-11)10/20/20 4.55 50.6 NS NS NS NS NS 477 NS NS NS NS NS 234 NS NS 34.6 NS NS 552
AP-11
Notes:
µg/L - micrograms per liter
WS - Water Supply
NE - No standard established
VOC - Volatile Organic Compounds
J - Estimated concentration below laboratory reporting limit
ND - Analyte concentration is below laboratory practical quantitative limits
NS - Not Sampled
Bold values exceed the NCAC 2L Standard
Shaded values exceed the 2B Standard by a factor of 10.
Italicized values exceed Gross Contamination Levels
*NC Protective Value for Surface Waters - criteria may be based on limited toxicological information.
**EPA Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health.
AP-11
Page 5 of 5
Table 2b
Summary of Groundwater Analytical Results – Hydrocarbon Fractions
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
C5-C8
Aliphatics
C9-C12
Aliphatics
C9-C18
Aliphatics
C19-C36
Aliphatics
C9-C10
Aromatics
C11-C22
Aromatics
Date
Collected
Depth to Water (DTW)µg/L µg/L µg/L µg/L µg/L µg/L
125(S)*210(S)*
400 10,000
06/12/14 5.72 ND ND NS NS ND NS
12/10/14 5.76 ND ND NS NS ND NS
Duplicate (AP-1)12/10/14 5.76 ND ND NS NS ND NS
08/27/15 7.48 ND ND ND ND ND ND
02/13/19 3.24 510 <380 NS NS 41 J NS
10/16/19 7.97 1,190 <50 NS NS 61 NS
10/20/20 4.20 270 <100 NS NS 56.2 J NS
06/12/14 5.61 13,200 6,320 NS NS ND NS
12/10/14 5.18 4,860 2,900 NS NS ND NS
08/27/15 7.71 3,700 J 1,500 J ND ND 710 ND
DUP-1 (AP-2)08/27/15 7.71 5,200 1,500 J ND ND 710 ND
06/01/16 4.37 7,300 1,700 NS NS 1,400 NS
02/13/19 2.85 5,000 1,900 NS NS 960 NS
10/16/19 5.98 4,170 1,120 NS NS 742 NS
10/20/20 3.88 2,880 1,450 NS NS 639 NS
08/27/15 8.45 ND 11 J ND ND ND ND
06/01/16 4.74 <75 <75 NS NS <25 NS
02/13/19 5.37 <75 <75 NS NS <25 NS
AP-3 12/31/14 4.32 529 ND NS NS ND NS
Duplicate (AP-3)12/31/14 4.32 689 434 NS NS ND NS
08/27/15 7.78 3,900 1,000 J ND ND 280 ND
06/01/16 4.6 200 50 J NS NS <25 NS
02/13/19 2.75 <75 <75 NS NS <25 NS
06/20/19 4.07 <75 <75 NS NS <25 NS
10/16/19 6.60 <50 <50 NS NS <50 NS
10/20/20 4.11 <100 <100 NS NS 39.2 J NS
12/31/14 4.30 1,750 ND NS NS ND NS
08/27/15 7.81 2,300 J ND ND ND ND ND
06/01/16 4.19 83 <75 NS NS <25 NS
02/13/19 2.63 33 J <75 NS NS <25 NS
06/20/19 3.68 890 1,100 NS NS 340 NS
10/16/19 NM <50 <50 NS NS <50 NS
10/20/20 3.80 105 <100 NS NS 42.4 J NS
AP-1
AP-2
200
MADEP EPH/VPH
Sample ID
Constituent of
Concern
NCAC 2L Standards
830(S)*
Analytical Method
NCAC 2B Standards (Class WS Water)
700
180(S)*
AP-1
AP-2
AP-2D
AP-3
AP-4
Page 1 of 3
Table 2b
Summary of Groundwater Analytical Results – Hydrocarbon Fractions
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
C5-C8
Aliphatics
C9-C12
Aliphatics
C9-C18
Aliphatics
C19-C36
Aliphatics
C9-C10
Aromatics
C11-C22
Aromatics
Date
Collected
Depth to Water (DTW)µg/L µg/L µg/L µg/L µg/L µg/L
125(S)*210(S)*
400 10,000 200
MADEP EPH/VPH
Sample ID
Constituent of
Concern
NCAC 2L Standards
830(S)*
Analytical Method
NCAC 2B Standards (Class WS Water)
700
180(S)*
12/31/14 3.97 1,020 865 NS NS ND NS
08/27/15 7.85 3,000 J 1,200 J ND ND ND ND
06/01/16 5.48 1,200 540 NS NS 220 NS
DUP-1 (AP-5)06/01/16 5.48 1,100 510 NS NS 210 NS
02/13/19 3.57 500 360 NS NS 180 NS
06/20/19 4.79 550 740 NS NS 320 NS
10/16/19 6.36 1,050 1,320 NS NS 600 NS
10/20/20 4.87 305 502 NS NS 245 NS
12/31/14 2.06 ND ND NS NS ND NS
08/27/15 8.64 80 ND ND ND ND ND
02/13/19 3.13 <75 <75 NS NS <25 NS
08/27/15 8.88 2,200 1,500 ND ND 700 170
06/01/16 5.24 11,000 4,300 NS NS 2,700 NS
02/13/19 4.22 4,600 2,500 NS NS 2,500 NS
DUP-1 (AP-7)02/13/19 4.22 4,400 3,900 NS NS 2,600 NS
08/27/15 8.55 660 370 J ND ND 150 ND
06/01/16 6.59 18,000 9,400 NS NS 4,500 NS
02/13/19 4.13 5,900 12,000 NS NS 8,100 NS
06/20/19 5.11 4,300 11,000 NS NS 7,600 NS
10/16/19 6.00 4,120 7,170 NS NS 6,240 NS
10/20/20 4.20 2,790 8,250 NS NS 3,750 NS
08/27/15 7.76 ND ND ND ND ND ND
02/13/19 3.44 <75 <75 NS NS <25 NS
10/20/20 4.22 <100 55.9 J NS NS 33.4 J NS
08/27/15 8.13 ND ND ND ND ND 9,000
02/13/19 3.4 2,200 400 J NS NS 240 J NS
10/16/19 6.60 5,340 781 NS NS 465 NS
10/20/20 4.39 4,020 946 NS NS 474 NS
AP-5
AP-7
AP-9
AP-10
AP-8
AP-6
Page 2 of 3
Table 2b
Summary of Groundwater Analytical Results – Hydrocarbon Fractions
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
C5-C8
Aliphatics
C9-C12
Aliphatics
C9-C18
Aliphatics
C19-C36
Aliphatics
C9-C10
Aromatics
C11-C22
Aromatics
Date
Collected
Depth to Water (DTW)µg/L µg/L µg/L µg/L µg/L µg/L
125(S)*210(S)*
400 10,000 200
MADEP EPH/VPH
Sample ID
Constituent of
Concern
NCAC 2L Standards
830(S)*
Analytical Method
NCAC 2B Standards (Class WS Water)
700
180(S)*
06/01/16 5.07 47,000 19,000 NS NS 5,900 NS
02/13/19 4.11 25,000 23,000 NS NS 9,000 NS
06/20/19 4.43 1,600 8,700 NS NS 7,700 NS
DUP 062019 (AP-11)06/20/19 4.43 1,700 10,000 NS NS 5,600 NS
10/16/19 6.63 2,270 6,560 NS NS 7,470 NS
10/20/20 4.55 1,010 6,710 NS NS 3,450 NS
DUP-1 (AP-11)10/20/20 4.55 1,040 7,050 NS NS 3,550 NS
Notes:
µg/L - micrograms per liter
Only detected constituents are shown
VPH - Volatile Petroleum Hydrocarbons according to the Massachusetts Department of Environmental Protection (MADEP) Method
EPH - Extractable Petroleum Hydrocarbons according to the MADEP Method
WS - Water Supply
J - Estimated concentration below laboratory reporting limit
ND - Analyte concentration is below laboratory practical quantitative limits
NS - Not sampled
Bold values exceed the NCAC 2L Standard
Shaded values exceed the 2B Standard by a factor of 10.
*NC Protective Value for Surface Waters - criteria may be based on limited toxicological information.
S - Toxicity exceeds solubility, no visible sheen or free product in water
AP-11
Page 3 of 3
Table 3aAFVR Field Data Sheet- March 2020Colonial Pipeline CompanySelma StationSelma, NCStinger Depth(ft. BTOC)Vacuum at Well(in Hg)PID/FID atWell Head(ppm)AP-11 AP-11 AP-3 AP-4 AP-5 AP-8 AP-3 AP-4 AP-5 AP-8 AP-11 AP-113/5/20 7:50 AM5.0------3.052.812.844.383.45----525 / 81503/5/20 8:30 AM 5.0 23.0 21.0 0.00 -0.05 -0.44 -1.00 3.08 2.85 3.02 4.79 5.00 3348 179.2 34.14 68.35 -3/5/20 9:00 AM 5.5 23.0 21.0 0.00 -0.05 -0.28 -1.20 3.13 2.85 3.12 4.78 5.50 4024 192.5 25.14 51.30 -3/5/20 9:30 AM 6.0 23.5 21.0 0.00 0.00 0.00 -1.203.16 2.85 3.16 4.89 6.00 4129 199.2 24.99 50.19 -3/5/20 10:00 AM 6.5 23.5 21.0 0.00 0.00 -0.08 -0.40 3.21 2.89 3.23 5.10 6.50 4002 198.7 23.28 48.35 -3/5/20 11:00 AM 6.5 23.5 21.0 0.00 0.00 -0.04 -0.40 3.31 2.96 3.32 5.20 6.50 4120 >200 23.17 47.29 -3/5/20 12:00 PM 6.5 23.5 21.0 -0.09 0.00 -0.02 -0.20 3.33 3.01 3.38 5.28 6.50 4012 >200 22.22 45.50 -3/5/20 1:00 PM 7.0 24.0 22.0 -0.02 0.00 0.00 -0.20 3.39 3.06 3.42 5.34 7.00 4350 >200 18.37 38.05 -3/5/20 2:00 PM 7.0 24.0 22.0 0.00 0.00 0.00 -0.203.42 3.08 3.44 5.38 7.00 4388 >200 17.27 33.41 -3/5/20 3:00 PM 8.5 24.5 22.0 0.00 0.00 0.00 -0.303.46 3.12 3.46 5.42 8.50 4292 186.3 15.31 30.47 -3/5/20 4:00 PM 9.5 27.0 22.0 0.00 -0.02 0.00 -0.30 3.48 3.15 3.48 5.45 9.50 4361 197.6 14.82 29.93 1.7 / 4.23/5/20 4:20 PM-------3.503.193.504.905.61----107 / 849Average 6.6 24.0 21.4 0.0 0.0 -0.1 -0.5 3.3 3.0 3.3 5.1 6.4 4102.6 192.3 21.9 44.3 211.2 / 9003.2Notes:dash indicates that no reading was availableNM = Not MeasuredPID = Photo Ionization DetectorFID = Flame Ionization DetectorAFVR = Aggressive Fluid Vapor Recoveryin Hg = Inches MercuryLNAPL = Light Non‐Aqueous Phase LiquidFPM = Feet Per Minuteppm = parts per millionVAC  = Vacuum °F = degrees Fahrenheitft = feetDate/TimeVAC @ Truck (in Hg)Air Flow(at Blower - FPM)FID(at Blower - ppm)Depth to Water/LNAPL (TOC)PID(at Blower - ppm)Temp(at Blower - °F)Vacuum at Surrounding Wells(Inches of Water Column)1 of 1
Table 3bAFVR Field Data Sheet- December 2020Colonial Pipeline CompanySelma StationSelma, NCStinger Depth (ft. BTOC)Vacuum at Well (in Hg)PID/FID at Well Head (ppm)AP-11 AP-11 AP-3 AP-4 AP-5 AP-8 AP-3 AP-4 AP-5 AP-8 AP-11 AP-1112/15/20 7:40 AM-------3.303.493.363.743.72----0.01 / 0.1412/15/20 8:30 AM 5.0 14.0 18.0 0.00 0.10 0.11 0.24 3.22 3.56 3.41 4.16 - 3995 100.4 0.63 1.84 -12/15/20 9:00 AM5.015.018.00.000.030.061.003.343.573.434.43------12/15/20 9:30 AM 5.0 16.0 18.0 0.10 0.10 0.13 0.04 3.35 3.60 3.48 4.68 - 3799 161.1 0.59 2.29 -12/15/20 10:00 AM5.016.018.00.100.070.040.103.383.633.544.77------12/15/20 10:30 AM 5.0 16.0 18.0 0.00 0.10 0.03 0.03 3.41 3.66 3.58 4.85 - 4255 141.7 0.47 3.13 -12/15/20 11:30 AM 5.0 16.0 18.0 0.00 0.07 0.14 0.11 3.46 3.69 3.62 4.95 - 4087 148.5 0.42 3.28 -12/15/20 12:30 PM 5.0 16.0 18.0 0.10 0.09 0.02 0.12 3.49 3.69 3.66 5.00 - 3581 >200.0 0.51 2.61 -12/15/20 1:30 PM 5.0 20.0 20.0 0.10 0.07 0.06 0.71 3.51 3.70 3.65 5.03 - 731 53.5 NM NM -12/15/20 2:30 PM 5.0 20.0 20.0 0.10 0.08 0.17 0.60 3.53 3.75 3.69 5.11 - 576 78.1 NM NM -12/15/20 3:30 PM 5.0 20.0 20.0 0.00 0.05 0.00 1.00 3.56 3.77 3.66 5.00 - 310 58.7 NM NM -12/15/20 4:30 PM 5.0 18.0 20.0 0.10 0.10 0.00 0.95 3.58 3.80 3.70 5.12 - 481 57.1 NM NM -12/15/20 4:45 PM-------3.583.823.704.745.72----NMAverage 5.0 17.0 18.7 0.05 0.08 0.07 0.45 3.44 3.67 3.58 4.74 4.72 2423.89 99.89 0.52 2.63 0.01 / 0.14Notes:dash indicates that no reading was availableNM = Not MeasuredPID = Photo Ionization DetectorFID = Flame Ionization DetectorAFVR = Aggressive Fluid Vapor Recoveryin Hg = Inches MercuryLNAPL = Light Non‐Aqueous Phase LiquidFPM = Feet Per Minuteppm = parts per millionVAC  = Vacuum °F = degrees Fahrenheitft = feet13:30 ‐ A truck malfunction required a change from the blower exhaust to the pump exhaust. PID/FID battery died; could not charge it.14:45 ‐ Pump was shut off for 20 minutes until 15:05 to prevent overheating.Date/TimeVAC @ Truck (in Hg)Air Flow(at Blower - FPM)FID(at Blower - ppm)Depth to Water/LNAPL (TOC)PID(at Blower - ppm)Temp(at Blower - °F)Vacuum at Surrounding Wells (Inches of Water Column)1 of 1
Table 4a
Summary of AFVR Effluent Sample Analytical Results- March 2020
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Date
Collected
Time
Collected
AS-1 (Startup)3/5/2020 8:30 7.91 96.5 1.4 62.3 2.5 18.2 941 2,590 195 147 229 109 1,570 2,840 815 307 4,300 2,020 8,928
AS-2 (End)3/5/2020 15:40 9.93 135 1.02 115 2.35 7.73 538 1,950 104 353 141 158 972 2,700 751 368 2,460 1,250 5,355
Average Concentration 3/5/2020 ----116 --------740 ----------1,271 ------3,380 1,635 7,141
Notes:
All concentrations reported in micrograms per cubic meter (µg/m3)
VOCs = Volatile Organic Compounds
ID = Identification
J = Estimated concentration above the method detection limit and below the reporting limit
ND = Analyte not detected at or above reporting limit
AFVR = Aggressive Fluid Vapor Recovery
Total BTEX = the sum of bezene, toluene, ethanol, and xylenes detections
Samples were collected in Summa cannisters approximately 30 minutes after beginning AFVR event and 30 minutes prior to completion of AFVR event m&p-xylenesTO-15
2,2,4-TrimethylpentaneTotal BTEXNaphthaleneo-XyleneChloromethaneCyclohexaneDichlorodifluoromethaneEthanoln-Heptanen-HexaneIsopropylbenzene (Cumene)1,3,5-TrimethylbenzeneConstituent
Analytical Method
Sample ID
Toluene1,2,4-Trimethylbenzene4-EthyltolueneBenzeneEthylbenzeneAcetonePage 1 of 1
Table 4b
Summary of AFVR Effluent Sample Analytical Results- December 2020
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
DateCollected Time Collected
AFVR- START 12/15/2020 9:05 10.0 21.8 3.3 5.6 60.9 19.3 10.8 10.6 5 1.1 7.8 39 1.5 1.6 51.4 18.6 98.8 34.1 243
AFVR- END 12/15/2020 15:30 3,920 12,100 ND ND 28,400 19,000 2,640 3,960 3,750 ND ND 23,200 ND ND 67,500 22,300 83,200 42,900 181,620
Average Concentration 12/15/2020 --1,965 ------14,230 ------------11,619 --------41,649 21,467 90,931
Notes:
All concentrations reported in micrograms per cubic meter (µg/m3)
VOCs = Volatile Organic Compounds
ID = Identification
J = Estimated concentration above the method detection limit and below the reporting limit
ND = Analyte not detected at or above reporting limit
AFVR = Aggressive Fluid Vapor Recovery
Total BTEX = the sum of bezene, toluene, ethanol, and xylenes detections
Samples were collected in Summa cannisters approximately 30 minutes after beginning AFVR event and 30 minutes prior to completion of AFVR event
*It is believed that increases in BTEX concentrations observed in the AFVR- End sample were due to a change in sample location as a result of an equipment malfunction.
Analytical Method
Sample ID
m&p-xylenesTO-15
Total BTEXNaphthaleneo-Xylene2-PropanolTetrachloroetheneTrichloroetheneTrichlorofluoromethane1,3,5-Trimethylbenzene4-EthyltolueneBenzeneEthylbenzeneCyclohexaneToluene1,2,4-Trimethylbenzenen-Heptanen-HexaneConstituent
Dichlorodifluoromethanecis-1,2-DichloroethenePage 1 of 1
Table 5a
Vapor Phase Mass Removal Calculations- March 2020
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Site: Colonial Pipeline Selma Facility
Extraction Locations: AP-11
Extraction Date: March 5, 2020
Average Air Velocity (FPM) 4,103
Vapor stack diameter (inches) 6
Vapor stack diameter (feet) 0.50
Vapor stack crossectional surface area (ft2)0.196 stack 8" x 12" rectangular
Actual cubic feet per minute (ACFM) 805.52
Average Vapor Temperature (oF) [TActual]192.3 (measured at vacuum truck vapor stack)
Average Vapor Temperature (oR) [TActual]652.3 (oF +460)
Standard Temperature (oR) [TSTP]528 (68o F+460)
Average Pressure (in H2O) [PActual]407 (29.92 in Hg = 407 in H2O)*
Average Pressure (in H2O) [PSTP]407 (29.92 in Hg = 407 in H2O)
Standard Cubic Feet Per Minute (SCFM) 652.02 [ACFM(TSTP /T actual)(PActual/PSTP )]
*velocity pressure of vapor discharge when released into atmosphere (STP)
Average Benzene concentration (mg/m3)*0.1160 Average BTEX concentration (mg/m3)7.1410
Benzene concentration (lb/ft3)7.2E-09 Total BTEX concentration (lb/ft3)4.5E-07
Average percent benzene in gasoline (% mass) 1.8 Average percent BTEX in gasoline (% mass) 19
Average vapor flow rate (SCFM) 652.02 Average vapor flow rate (SCFM) 652.02
Hours of operation at extraction location 8.0 Hours of operation at extraction location 8.0
Days of operation at extraction location 0.3 Days of operation at extraction location 0.3
Benzene removal rate (pounds/day) 6.80E-03 BTEX removal rate (pounds/day) 4.19E-01
Total mass benzene removed (pounds) 2.27E-03 Total mass BTEX removed (pounds) 1.40E-01
Total mass gasoline removed (pounds) 1.26E-01 Total mass gasoline removed (pounds) 7.34E-01
Total volume gasoline removed (gallons) 2.01E-02 Total volume gasoline removed (gallons) 1.17E-01
Total volume gasoline removed (gallons/day) 6.03E-02 Total volume gasoline removed (gallons/day) 3.52E-01
Notes:
Calculations assume Benzene and Total BTEX /gasoline removal = Benzene and Total BTEX ratio in fuel
Average percent benzene in gasoline = 1.8% by weight (Risher-Roberts, 1998)
Average percent BTEX in gasoline = 19% by weight (Health et al, Journal of Soil Contamination, 1993)
ACFM = Actual Cubic Feet per Minute
SCFM = Standard Cubic Feet per Minute
mg/m3 = milligrams per cubix meter
lb/ft3 = pounds per cubic foot
ft2 = square feet
% = percent
H2O = Water
T = Temperature
oF = degress Fahrenheit
oR = degrees Rankine
P = Pressure
FPM = Feet Per Minute
BTEX = sum of benzene, toluene, ethanol, and xylenes detections
STP = Standard Temperature and Pressure
Conversion from ACFM to SCFM
Benzene as Gasoline Total BTEX as Gasoline
1 of 1
Table 5b
Vapor Phase Mass Removal Calculations- December 2020
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Site: Colonial Pipeline Selma Facility
Extraction Locations: AP-11
Extraction Date: December 15, 2020
Average Air Velocity (FPM) 2,424
Vapor stack diameter (inches) 6
Vapor stack diameter (feet) 0.50
Vapor stack crossectional surface area (ft2)0.196 stack 8" x 12" rectangular
Actual cubic feet per minute (ACFM) 475.89
Average Vapor Temperature (oF) [TActual]99.9 (measured at vacuum truck vapor stack)
Average Vapor Temperature (oR) [TActual]559.9 (oF +460)
Standard Temperature (oR) [TSTP]528 (68o F+460)
Average Pressure (in H2O) [PActual]407 (29.92 in Hg = 407 in H2O)*
Average Pressure (in H2O) [PSTP]407 (29.92 in Hg = 407 in H2O)
Standard Cubic Feet Per Minute (SCFM) 448.78 [ACFM(TSTP /T actual)(PActual/PSTP )]
*velocity pressure of vapor discharge when released into atmosphere (STP)
Average Benzene concentration (mg/m3)*1.9650 Average BTEX concentration (mg/m3)90.9310
Benzene concentration (lb/ft3)1.2E-07 Total BTEX concentration (lb/ft3)5.7E-06
Average percent benzene in gasoline (% mass) 1.8 Average percent BTEX in gasoline (% mass) 19
Average vapor flow rate (SCFM) 448.78 Average vapor flow rate (SCFM) 448.78
Hours of operation at extraction location 8.0 Hours of operation at extraction location 8.0
Days of operation at extraction location 0.3 Days of operation at extraction location 0.3
Benzene removal rate (pounds/day) 7.93E-02 BTEX removal rate (pounds/day) 3.67E+00
Total mass benzene removed (pounds) 2.64E-02 Total mass BTEX removed (pounds) 1.22E+00
Total mass gasoline removed (pounds) 1.47E+00 Total mass gasoline removed (pounds) 6.44E+00
Total volume gasoline removed (gallons) 2.34E-01 Total volume gasoline removed (gallons) 1.03E+00
Total volume gasoline removed (gallons/day) 7.03E-01 Total volume gasoline removed (gallons/day) 3.08E+00
Notes:
Calculations assume Benzene and Total BTEX /gasoline removal = Benzene and Total BTEX ratio in fuel
Average percent benzene in gasoline = 1.8% by weight (Risher-Roberts, 1998)
Average percent BTEX in gasoline = 19% by weight (Health et al, Journal of Soil Contamination, 1993)
STP = Standard Temperature and Pressure
ACFM = Actual Cubic Feet per Minute
SCFM = Standard Cubic Feet per Minute
mg/m3 = milligrams per cubix meter
lb/ft3 = pounds per cubic foot
ft2 = square feet
% = percent
H2O = Water
T = Temperature
oF = degress Fahrenheit
oR = degrees Rankine
P = Pressure
FPM = Feet Per Minute
BTEX = sum of benzene, toluene, ethanol, and xylenes detections
STP = Standard Temperature and Pressure
Conversion from ACFM to SCFM
Benzene as Gasoline Total BTEX as Gasoline
1 of 1
Table 6
Proposed Groundwater Monitoring Program
Colonial Pipeline Company
Selma Facility
Selma, North Carolina
Well ID April Groundwater Monitoring
Event
October Groundwater
Monitoring Event
AP-1 BTEX, Naphthalene BTEX, Naphthalene
AP-2 BTEX, Naphthalene BTEX, Naphthalene
AP-2D Gauge Only BTEX, Naphthalene
AP-3 BTEX, Naphthalene BTEX, Naphthalene
AP-4 BTEX, Naphthalene BTEX, Naphthalene
AP-5 BTEX, Naphthalene BTEX, Naphthalene
AP-6 Gauge Only BTEX, Naphthalene
AP-7 Gauge Only BTEX, Naphthalene
AP-8 BTEX, Naphthalene BTEX, Naphthalene
AP-9 BTEX, Naphthalene BTEX, Naphthalene
AP-10 BTEX, Naphthalene BTEX, Naphthalene
AP-11 BTEX, Naphthalene BTEX, Naphthalene
Notes:
BTEX - Benzene, Toluene, Ethylbenzene, and Total Xylenes
BTEX and Naphthalene analyzed by EPA Method 6200B
1 of 1

FIGURES
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed May, 2020.
CHECK BY: AS
DRAWN BY: CW
DATE: 9/23/2021
SCALE: AS SHOWN
CAD NO.: CPC21008
PRJ NO.: CPC21008
FIGURE
SITE LOCATION MAP
COLONIAL PIPELINE COMPANYSELMA STATION2335 WEST OAK STREETSELMA, NORTH CAROLINA
³
0 1,000 2,000
Feet
1
SITE LOCATION
!A
!A"Ò)
!A
!A
!A
!A
!A
!A
!A
!A!A!>!>!>!>MARATHONPETROLEUMCOMPANY, LLC
W.OAKSTACCESSRDSITE BOUNDARY
POND
TANK
SOILSTAGINGAREA
OFFICEBUILDING
BIT.
GRASS
EXCAVATION AREA(210' X 20' X 7')
MW-11
MW-7
MW-15
MW-16
AP-1
AP-2
AP-2D
AP-3
AP-4
AP-5
AP-6
AP-7
AP-8
AP-9
AP-10AP-11
CHECK BY: AS
DRAWN BY: CW
DATE: 9/23/2021
SCALE: AS SHOWN
CAD NO.: CPC21008
PRJ NO.: CPC21008
SITE PLAN
COLONIAL PIPELINE COMPANYSELMA STATION2335 WEST OAK STREETSELMA, NORTH CAROLINA
!A SHALLOW MONITORING WELL
"Ò)DEEP MONITORING WELL
!>OFF-SITE MONITORING WELL
APPROXIMATE SITE BOUNDARY ³0 50 10025
Feet
2
FIGURE
LEGEND

APPENDIX A
GROUNDWATER SAMPLING LOGS

APPENDIX B
LABORATORY ANALYTICAL REPORTS
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Apex Companies,LLC
10610 Metromont Parkway
Suite 206
Charlotte,NC 28269
Attention:Andrew Street
Project Name:CPC Selma
Project Number:CPC 20104 Task 1
Lot Number:VE28082
Date Completed:06/04/2020
06/04/2020 2:21 PM
Approved and released by:
Lab Director -Greenville:Lucas Odom
Page 1 of 27
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Apex Companies,LLC
Lot Number:VE28082
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Pace Analytical Services,LLC ("Pace")Quality Assurance
Management Plan (QAMP),standard operating procedures (SOPs),and Pace policies.Any exceptions to
the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 27
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Apex Companies, LLC
Lot Number: VE28082

Sample Number Sample ID Matrix Date Sampled Date Received
001 05/27/2020 1155AP-3 Aqueous 05/28/2020
002 05/27/2020 1235AP-9 Aqueous 05/28/2020
003 05/27/2020DUP-1 Aqueous 05/28/2020
004 05/27/2020 1315AP-4 Aqueous 05/28/2020
005 05/27/2020 1345AP-1 Aqueous 05/28/2020
006 05/27/2020EB-1 Aqueous 05/28/2020
007 05/27/2020Trip Blank Aqueous 05/28/2020
008 05/27/2020 1218AP-2 Aqueous 05/28/2020
009 05/27/2020 1248AP-5 Aqueous 05/28/2020
010 05/27/2020 1330AP-8 Aqueous 05/28/2020
011 05/27/2020 1148AP-10 Aqueous 05/28/2020
012 05/27/2020 1408AP-11 Aqueous 05/28/2020
(12 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 27
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Apex Companies, LLC
Lot Number: VE28082

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 AP-3 Aqueous Benzene SM 6200B-4.0 ug/L 5
004 AP-4 Aqueous Benzene SM 6200B-35 ug/L 8
004 AP-4 Aqueous Ethylbenzene SM 6200B-0.77 ug/L 8
004 AP-4 Aqueous Xylenes (total)SM 6200B-1.9 ug/L 8
008 AP-2 Aqueous Benzene SM 6200B-180 ug/L 12
008 AP-2 Aqueous Ethylbenzene SM 6200B-130 ug/L 12
008 AP-2 Aqueous Toluene SM 6200B-43 ug/L 12
008 AP-2 Aqueous Xylenes (total)SM 6200B-77 ug/L 12
009 AP-5 Aqueous Benzene SM 6200B-42 ug/L 13
009 AP-5 Aqueous Ethylbenzene SM 6200B-80 ug/L 13
009 AP-5 Aqueous Toluene SM 6200B-17 ug/L 13
009 AP-5 Aqueous Xylenes (total)SM 6200B-280 ug/L 13
010 AP-8 Aqueous Benzene SM 6200B-200 ug/L 14
010 AP-8 Aqueous Ethylbenzene SM 6200B-1300 ug/L 14
010 AP-8 Aqueous Xylenes (total)SM 6200B-2000 ug/L 14
011 AP-10 Aqueous Benzene SM 6200B-1200 ug/L 15
011 AP-10 Aqueous Ethylbenzene SM 6200B-310 ug/L 15
011 AP-10 Aqueous Naphthalene SM 6200B-44 ug/L 15
011 AP-10 Aqueous Toluene SM 6200B-59 ug/L 15
011 AP-10 Aqueous Xylenes (total)SM 6200B-330 ug/L 15
012 AP-11 Aqueous Benzene SM 6200B-77 ug/L 16
012 AP-11 Aqueous Ethylbenzene SM 6200B-460 ug/L 16
012 AP-11 Aqueous Naphthalene SM 6200B-170 ug/L 16
012 AP-11 Aqueous Toluene SM 6200B-23 ug/L 16
012 AP-11 Aqueous Xylenes (total)SM 6200B-1700 ug/L 16
(25 detections)
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-3
VE28082-001
05/27/2020 1155
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0019 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-4.0 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 73 70-130
Toluene-d8 90 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-9
VE28082-002
05/27/2020 1235
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0044 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 75 70-130
Toluene-d8 90 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
DUP-1
VE28082-003
05/27/2020
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0109 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 74 70-130
Toluene-d8 89 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-4
VE28082-004
05/27/2020 1315
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0134 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-35 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-0.77 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-1.9 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 109 70-130
1,2-Dichloroethane-d4 74 70-130
Toluene-d8 89 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-1
VE28082-005
05/27/2020 1345
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0158 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 73 70-130
Toluene-d8 89 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
EB-1
VE28082-006
05/27/2020
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0223 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 109 70-130
1,2-Dichloroethane-d4 72 70-130
Toluene-d8 89 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
Trip Blank
VE28082-007
05/27/2020
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 06/02/2020 0248 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 109 70-130
1,2-Dichloroethane-d4 72 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-2
VE28082-008
05/27/2020 1218
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 SM 6200B-SM 6200B-2011 1 06/03/2020 1011 TML 55771
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-180 2ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-130 2ug/L0.50
Toluene 108-88-3 SM 6200B-43 2ug/L0.50
Xylenes (total)1330-20-7 SM 6200B-77 2ug/L0.50
AcceptanceRun 2
Surrogate Q % Recovery Limits
Bromofluorobenzene 123 70-130
1,2-Dichloroethane-d4 80 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Page 12 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-5
VE28082-009
05/27/2020 1248
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 5 06/02/2020 0313 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-42 1ug/L2.5
Ethylbenzene 100-41-4 SM 6200B-80 1ug/L2.5
Toluene 108-88-3 SM 6200B-17 1ug/L2.5
Xylenes (total)1330-20-7 SM 6200B-280 1ug/L2.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 74 70-130
Toluene-d8 87 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-8
VE28082-010
05/27/2020 1330
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 06/02/2020 0453 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-200 1ug/L25
Ethylbenzene 100-41-4 SM 6200B-1300 1ug/L25
Toluene 108-88-3 SM 6200B-ND 1ug/L25
Xylenes (total)1330-20-7 SM 6200B-2000 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 111 70-130
1,2-Dichloroethane-d4 71 70-130
Toluene-d8 87 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Page 14 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-10
VE28082-011
05/27/2020 1148
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 20 06/02/2020 0428 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-1200 1ug/L10
Ethylbenzene 100-41-4 SM 6200B-310 1ug/L10
Naphthalene 91-20-3 SM 6200B-44 1ug/L10
Toluene 108-88-3 SM 6200B-59 1ug/L10
Xylenes (total)1330-20-7 SM 6200B-330 1ug/L10
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 73 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Page 15 of 27
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Apex Companies, LLC
AP-11
VE28082-012
05/27/2020 1408
05/28/2020
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 10 06/02/2020 0403 JTH 55602
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-77 1ug/L5.0
Ethylbenzene 100-41-4 SM 6200B-460 1ug/L5.0
Naphthalene 91-20-3 SM 6200B-170 1ug/L5.0
Toluene 108-88-3 SM 6200B-23 1ug/L5.0
Xylenes (total)1330-20-7 SM 6200B-1700 1ug/L5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 111 70-130
1,2-Dichloroethane-d4 73 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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QC Summary
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ55602-001
55602 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Benzene ND 06/01/2020 22070.50 ug/L1
Ethylbenzene ND 06/01/2020 22070.50 ug/L1
Naphthalene ND 06/01/2020 22070.50 ug/L1
Toluene ND 06/01/2020 22070.50 ug/L1
Xylenes (total)ND 06/01/2020 22070.50 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 76 70-130
Toluene-d8 90 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ55602-002
55602 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 47 06/01/2020 2101955070-1301
Ethylbenzene 48 06/01/2020 2101955070-1301
Naphthalene 45 06/01/2020 2101905050-1401
Toluene 47 06/01/2020 2101945070-1301
Xylenes (total)93 06/01/2020 21019310070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 88 70-130
1,2-Dichloroethane-d4 90 70-130
Toluene-d8 95 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 19 of 27
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:VE28082-009MS
55602 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 300 06/02/2020 051810225070-130425
Ethylbenzene 340 06/02/2020 051810225070-130805
Toluene 270 06/02/2020 051810125070-130175
Xylenes (total)770 06/02/2020 05189850070-1302805
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 101 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:VE28082-009MD
55602 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 300 06/02/2020 054310225070-1300.73 20425
Ethylbenzene 340 06/02/2020 054310325070-1300.21 20805
Toluene 270 06/02/2020 054310025070-1301.1 20175
Xylenes (total)770 06/02/2020 05439950070-1300.33 202805
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ55771-001
55771 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Benzene ND 06/03/2020 09170.50 ug/L1
Ethylbenzene ND 06/03/2020 09170.50 ug/L1
Toluene ND 06/03/2020 09170.50 ug/L1
Xylenes (total)ND 06/03/2020 09170.50 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 121 70-130
1,2-Dichloroethane-d4 77 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 22 of 27
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ55771-002
55771 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 47 06/03/2020 0827955070-1301
Ethylbenzene 48 06/03/2020 0827955070-1301
Toluene 48 06/03/2020 0827965070-1301
Xylenes (total)92 06/03/2020 08279210070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Chain of Custody
and
Miscellaneous Documents
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PACE ANALYTICAL SERVICES, LLC

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PACE ANALYTICAL SERVICES, LLC

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PACE ANALYTICAL SERVICES, LLC

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#=CL#
March 13, 2020
LIMS USE: FR - ANDREW STREET
LIMS OBJECT ID: 92468355
92468355
Project:
Pace Project No.:
RE:
Andrew Street
Apex Companies
10610 Metromont Parkway
Charlotte, NC 28269
CPC19006-001 CPC Selma/19006
Dear Andrew Street:
Enclosed are the analytical results for sample(s) received by the laboratory on March 06, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:John McGuire, Apex Companies, LLC
Carimar Tavera-Batista, Apex Companies - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 1 of 15
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Lab ID Sample ID Matrix Date Collected Date Received
92468355001 AS-1 (Startup)Air 03/05/20 08:30 03/06/20 09:10
92468355002 AS-2 (End)Air 03/05/20 15:40 03/06/20 09:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92468355001 AS-1 (Startup)TO-15 68 PANCAW
92468355002 AS-2 (End)TO-15 68 PANCAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Sample:AS-1 (Startup)Lab ID:92468355001 Collected:03/05/20 08:30 Received:03/06/20 09:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15 Preparation Method: TO-15VOA (MS) TO-15
Acetone 7.91 ug/m3 03/10/20 17:21 67-64-103/10/20 17:212.97 0.0569 1
Allyl chloride <0.626 ug/m3 03/10/20 17:21 107-05-103/10/20 17:210.626 0.0546 1
Benzene 96.5 ug/m3 03/10/20 17:21 71-43-203/10/20 17:210.639 0.0460 1
Benzyl chloride <1.04 ug/m3 03/10/20 17:21 100-44-703/10/20 17:211.04 0.0598 1
Bromodichloromethane <1.34 ug/m3 03/10/20 17:21 75-27-403/10/20 17:211.34 0.0436 1
Bromoform <6.21 ug/m3 03/10/20 17:21 75-25-203/10/20 17:216.21 0.0786 1
Bromomethane <0.776 ug/m3 03/10/20 17:21 74-83-903/10/20 17:210.776 0.0609 1
1,3-Butadiene <4.43 ug/m3 03/10/20 17:21 106-99-003/10/20 17:214.43 0.0563 1
Carbon disulfide <0.622 ug/m3 03/10/20 17:21 75-15-003/10/20 17:210.622 0.0544 1
Carbon tetrachloride <1.26 ug/m3 03/10/20 17:21 56-23-503/10/20 17:211.26 0.0585 1
Chlorobenzene <0.924 ug/m3 03/10/20 17:21 108-90-703/10/20 17:210.924 0.0601 1
Chloroethane <0.528 ug/m3 03/10/20 17:21 75-00-303/10/20 17:210.528 0.0489 1
Chloroform <0.973 ug/m3 03/10/20 17:21 67-66-303/10/20 17:210.973 0.0574 1
Chloromethane 1.35 ug/m3 03/10/20 17:21 74-87-303/10/20 17:210.413 0.0544 1
2-Chlorotoluene <1.03 ug/m3 03/10/20 17:21 95-49-803/10/20 17:211.03 0.0605 1
Cyclohexane 62.3 ug/m3 03/10/20 17:21 110-82-703/10/20 17:210.689 0.0534 1
Dibromochloromethane <1.70 ug/m3 03/10/20 17:21 124-48-103/10/20 17:211.70 0.0494 1
1,2-Dibromoethane (EDB)<1.54 ug/m3 03/10/20 17:21 106-93-403/10/20 17:211.54 0.0185 1
1,2-Dichlorobenzene <1.20 ug/m3 03/10/20 17:21 95-50-103/10/20 17:211.20 0.0603 1
1,3-Dichlorobenzene <1.20 ug/m3 03/10/20 17:21 541-73-103/10/20 17:211.20 0.0597 1
1,4-Dichlorobenzene <1.20 ug/m3 03/10/20 17:21 106-46-703/10/20 17:211.20 0.0557 1
1,2-Dichloroethane <0.810 ug/m3 03/10/20 17:21 107-06-203/10/20 17:210.810 0.0616 1
1,1-Dichloroethane <0.802 ug/m3 03/10/20 17:21 75-34-303/10/20 17:210.802 0.0514 1
1,1-Dichloroethene <0.793 ug/m3 03/10/20 17:21 75-35-403/10/20 17:210.793 0.0490 1
cis-1,2-Dichloroethene <0.793 ug/m3 03/10/20 17:21 156-59-203/10/20 17:210.793 0.0389 1
trans-1,2-Dichloroethene <0.793 ug/m3 03/10/20 17:21 156-60-503/10/20 17:210.793 0.0464 1
1,2-Dichloropropane <0.924 ug/m3 03/10/20 17:21 78-87-503/10/20 17:210.924 0.0599 1
cis-1,3-Dichloropropene <0.908 ug/m3 03/10/20 17:21 10061-01-503/10/20 17:210.908 0.0588 1
trans-1,3-Dichloropropene <0.908 ug/m3 03/10/20 17:21 10061-02-603/10/20 17:210.908 0.0435 1
1,4-Dioxane (p-Dioxane)<0.721 ug/m3 03/10/20 17:21 123-91-103/10/20 17:210.721 0.0554 1
Ethanol 18.2 ug/m3 03/10/20 17:21 64-17-503/10/20 17:211.19 0.0832 1
Ethylbenzene 941 ug/m3 03/11/20 16:07 100-41-403/11/20 16:0743.4 0.0506 50
4-Ethyltoluene 2590 ug/m3 03/11/20 16:07 622-96-803/11/20 16:0749.1 0.0666 50
Trichlorofluoromethane <1.12 ug/m3 03/10/20 17:21 75-69-403/10/20 17:211.12 0.0673 1
Dichlorodifluoromethane 2.50 ug/m3 03/10/20 17:21 75-71-803/10/20 17:210.989 0.0601 1
1,1,2-Trichlorotrifluoroethane <1.53 ug/m3 03/10/20 17:21 76-13-103/10/20 17:211.53 0.0687 1
Dichlorotetrafluoroethane <1.40 ug/m3 03/10/20 17:21 76-14-203/10/20 17:211.40 0.0458 1
n-Heptane 229 ug/m3 03/10/20 17:21 142-82-503/10/20 17:210.818 0.0626 1
Hexachloro-1,3-butadiene <6.73 ug/m3 03/10/20 17:21 87-68-303/10/20 17:216.73 0.0656 1
n-Hexane 109 ug/m3 03/10/20 17:21 110-54-303/10/20 17:210.705 0.0457 1
Isopropylbenzene (Cumene)195 ug/m3 03/10/20 17:21 98-82-803/10/20 17:210.983 0.0563 1
Methylene Chloride <0.694 ug/m3 03/10/20 17:21 75-09-203/10/20 17:210.694 0.0465 1
2-Hexanone <5.11 ug/m3 03/10/20 17:21 591-78-603/10/20 17:215.11 0.0682 1
2-Butanone (MEK)<3.69 ug/m3 03/10/20 17:21 78-93-303/10/20 17:213.69 0.0493 1
4-Methyl-2-pentanone (MIBK)<5.12 ug/m3 03/10/20 17:21 108-10-103/10/20 17:215.12 0.0650 1
Methyl methacrylate <0.819 ug/m3 03/10/20 17:21 80-62-603/10/20 17:210.819 0.0773 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
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Page 5 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Sample:AS-1 (Startup)Lab ID:92468355001 Collected:03/05/20 08:30 Received:03/06/20 09:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15 Preparation Method: TO-15VOA (MS) TO-15
Methyl-tert-butyl ether <0.721 ug/m3 03/10/20 17:21 1634-04-403/10/20 17:210.721 0.0505 1
Naphthalene 147 ug/m3 03/10/20 17:21 91-20-303/10/20 17:213.30 0.1540 1
2-Propanol <3.07 ug/m3 03/10/20 17:21 67-63-003/10/20 17:213.07 0.0882 1
Propylene <0.689 ug/m3 03/10/20 17:21 115-07-103/10/20 17:210.689 0.0932 1
Styrene <0.851 ug/m3 03/10/20 17:21 100-42-503/10/20 17:210.851 0.0465 1
1,1,2,2-Tetrachloroethane <1.37 ug/m3 03/10/20 17:21 79-34-503/10/20 17:211.37 0.0576 1
Tetrachloroethene <1.36 ug/m3 03/10/20 17:21 127-18-403/10/20 17:211.36 0.0497 1
Tetrahydrofuran <0.590 ug/m3 03/10/20 17:21 109-99-903/10/20 17:210.590 0.0508 1
Toluene 1570 ug/m3 03/11/20 16:07 108-88-303/11/20 16:0737.7 0.0499 50
1,2,4-Trichlorobenzene <4.66 ug/m3 03/10/20 17:21 120-82-103/10/20 17:214.66 0.1480 1
1,1,1-Trichloroethane <1.09 ug/m3 03/10/20 17:21 71-55-603/10/20 17:211.09 0.0665 1
1,1,2-Trichloroethane <1.09 ug/m3 03/10/20 17:21 79-00-503/10/20 17:211.09 0.0287 1
Trichloroethene <1.07 ug/m3 03/10/20 17:21 79-01-603/10/20 17:211.07 0.0545 1
1,2,4-Trimethylbenzene 2840 ug/m3 03/11/20 16:07 95-63-603/11/20 16:0749.1 0.0483 50
1,3,5-Trimethylbenzene 815 ug/m3 03/11/20 16:07 108-67-803/11/20 16:0749.1 0.0631 50
2,2,4-Trimethylpentane 307 ug/m3 03/10/20 17:21 540-84-103/10/20 17:210.934 0.0456 1
Vinyl chloride <0.511 ug/m3 03/10/20 17:21 75-01-403/10/20 17:210.511 0.0457 1
Vinyl bromide <0.875 ug/m3 03/10/20 17:21 593-60-203/10/20 17:210.875 0.0727 1
Vinyl acetate <0.704 ug/m3 03/10/20 17:21 108-05-403/10/20 17:210.704 0.0639 1
m&p-Xylene 4300 ug/m3 03/11/20 16:07 179601-23-103/11/20 16:0786.7 0.0946 50
o-Xylene 2020 ug/m3 03/11/20 16:07 95-47-603/11/20 16:0743.4 0.0633 50
Surrogates
1,4-Dichlorobenzene-d4 (IS)150 %03/10/20 17:21 3855-82-1 ST03/10/20 17:2160.0-140 1
1,4-Dichlorobenzene-d4 (IS)103 %03/11/20 16:07 3855-82-103/11/20 16:0760.0-140 50
Sample:AS-2 (End)Lab ID:92468355002 Collected:03/05/20 15:40 Received:03/06/20 09:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15 Preparation Method: TO-15VOA (MS) TO-15
Acetone 9.93 ug/m3 03/10/20 17:59 67-64-103/10/20 17:592.97 0.0569 1
Allyl chloride <0.626 ug/m3 03/10/20 17:59 107-05-103/10/20 17:590.626 0.0546 1
Benzene 135 ug/m3 03/10/20 17:59 71-43-203/10/20 17:590.639 0.0460 1
Benzyl chloride <1.04 ug/m3 03/10/20 17:59 100-44-703/10/20 17:591.04 0.0598 1
Bromodichloromethane <1.34 ug/m3 03/10/20 17:59 75-27-403/10/20 17:591.34 0.0436 1
Bromoform <6.21 ug/m3 03/10/20 17:59 75-25-203/10/20 17:596.21 0.0786 1
Bromomethane <0.776 ug/m3 03/10/20 17:59 74-83-903/10/20 17:590.776 0.0609 1
1,3-Butadiene <4.43 ug/m3 03/10/20 17:59 106-99-003/10/20 17:594.43 0.0563 1
Carbon disulfide <0.622 ug/m3 03/10/20 17:59 75-15-003/10/20 17:590.622 0.0544 1
Carbon tetrachloride <1.26 ug/m3 03/10/20 17:59 56-23-503/10/20 17:591.26 0.0585 1
Chlorobenzene <0.924 ug/m3 03/10/20 17:59 108-90-703/10/20 17:590.924 0.0601 1
Chloroethane <0.528 ug/m3 03/10/20 17:59 75-00-303/10/20 17:590.528 0.0489 1
Chloroform <0.973 ug/m3 03/10/20 17:59 67-66-303/10/20 17:590.973 0.0574 1
Chloromethane 1.02 ug/m3 03/10/20 17:59 74-87-303/10/20 17:590.413 0.0544 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
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Page 6 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Sample:AS-2 (End)Lab ID:92468355002 Collected:03/05/20 15:40 Received:03/06/20 09:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15 Preparation Method: TO-15VOA (MS) TO-15
2-Chlorotoluene <1.03 ug/m3 03/10/20 17:59 95-49-803/10/20 17:591.03 0.0605 1
Cyclohexane 115 ug/m3 03/10/20 17:59 110-82-703/10/20 17:590.689 0.0534 1
Dibromochloromethane <1.70 ug/m3 03/10/20 17:59 124-48-103/10/20 17:591.70 0.0494 1
1,2-Dibromoethane (EDB)<1.54 ug/m3 03/10/20 17:59 106-93-403/10/20 17:591.54 0.0185 1
1,2-Dichlorobenzene <1.20 ug/m3 03/10/20 17:59 95-50-103/10/20 17:591.20 0.0603 1
1,3-Dichlorobenzene <1.20 ug/m3 03/10/20 17:59 541-73-103/10/20 17:591.20 0.0597 1
1,4-Dichlorobenzene <1.20 ug/m3 03/10/20 17:59 106-46-703/10/20 17:591.20 0.0557 1
1,2-Dichloroethane <0.810 ug/m3 03/10/20 17:59 107-06-203/10/20 17:590.810 0.0616 1
1,1-Dichloroethane <0.802 ug/m3 03/10/20 17:59 75-34-303/10/20 17:590.802 0.0514 1
1,1-Dichloroethene <0.793 ug/m3 03/10/20 17:59 75-35-403/10/20 17:590.793 0.0490 1
cis-1,2-Dichloroethene <0.793 ug/m3 03/10/20 17:59 156-59-203/10/20 17:590.793 0.0389 1
trans-1,2-Dichloroethene <0.793 ug/m3 03/10/20 17:59 156-60-503/10/20 17:590.793 0.0464 1
1,2-Dichloropropane <0.924 ug/m3 03/10/20 17:59 78-87-503/10/20 17:590.924 0.0599 1
cis-1,3-Dichloropropene <0.908 ug/m3 03/10/20 17:59 10061-01-503/10/20 17:590.908 0.0588 1
trans-1,3-Dichloropropene <0.908 ug/m3 03/10/20 17:59 10061-02-603/10/20 17:590.908 0.0435 1
1,4-Dioxane (p-Dioxane)<0.721 ug/m3 03/10/20 17:59 123-91-103/10/20 17:590.721 0.0554 1
Ethanol 7.73 ug/m3 03/10/20 17:59 64-17-503/10/20 17:591.19 0.0832 1
Ethylbenzene 538 ug/m3 03/11/20 16:43 100-41-403/11/20 16:4343.4 0.0506 50
4-Ethyltoluene 1950 ug/m3 03/11/20 16:43 622-96-803/11/20 16:4349.1 0.0666 50
Trichlorofluoromethane <1.12 ug/m3 03/10/20 17:59 75-69-403/10/20 17:591.12 0.0673 1
Dichlorodifluoromethane 2.35 ug/m3 03/10/20 17:59 75-71-803/10/20 17:590.989 0.0601 1
1,1,2-Trichlorotrifluoroethane <1.53 ug/m3 03/10/20 17:59 76-13-103/10/20 17:591.53 0.0687 1
Dichlorotetrafluoroethane <1.40 ug/m3 03/10/20 17:59 76-14-203/10/20 17:591.40 0.0458 1
n-Heptane 141 ug/m3 03/10/20 17:59 142-82-503/10/20 17:590.818 0.0626 1
Hexachloro-1,3-butadiene <6.73 ug/m3 03/10/20 17:59 87-68-303/10/20 17:596.73 0.0656 1
n-Hexane 158 ug/m3 03/10/20 17:59 110-54-303/10/20 17:590.705 0.0457 1
Isopropylbenzene (Cumene)104 ug/m3 03/10/20 17:59 98-82-803/10/20 17:590.983 0.0563 1
Methylene Chloride <0.694 ug/m3 03/10/20 17:59 75-09-203/10/20 17:590.694 0.0465 1
2-Hexanone <5.11 ug/m3 03/10/20 17:59 591-78-603/10/20 17:595.11 0.0682 1
2-Butanone (MEK)<3.69 ug/m3 03/10/20 17:59 78-93-303/10/20 17:593.69 0.0493 1
4-Methyl-2-pentanone (MIBK)<5.12 ug/m3 03/10/20 17:59 108-10-103/10/20 17:595.12 0.0650 1
Methyl methacrylate <0.819 ug/m3 03/10/20 17:59 80-62-603/10/20 17:590.819 0.0773 1
Methyl-tert-butyl ether <0.721 ug/m3 03/10/20 17:59 1634-04-403/10/20 17:590.721 0.0505 1
Naphthalene 353 ug/m3 03/10/20 17:59 91-20-303/10/20 17:593.30 0.1540 1
2-Propanol <3.07 ug/m3 03/10/20 17:59 67-63-003/10/20 17:593.07 0.0882 1
Propylene <0.689 ug/m3 03/10/20 17:59 115-07-103/10/20 17:590.689 0.0932 1
Styrene <0.851 ug/m3 03/10/20 17:59 100-42-503/10/20 17:590.851 0.0465 1
1,1,2,2-Tetrachloroethane <1.37 ug/m3 03/10/20 17:59 79-34-503/10/20 17:591.37 0.0576 1
Tetrachloroethene <1.36 ug/m3 03/10/20 17:59 127-18-403/10/20 17:591.36 0.0497 1
Tetrahydrofuran <0.590 ug/m3 03/10/20 17:59 109-99-903/10/20 17:590.590 0.0508 1
Toluene 972 ug/m3 03/11/20 16:43 108-88-303/11/20 16:4337.7 0.0499 50
1,2,4-Trichlorobenzene <4.66 ug/m3 03/10/20 17:59 120-82-103/10/20 17:594.66 0.1480 1
1,1,1-Trichloroethane <1.09 ug/m3 03/10/20 17:59 71-55-603/10/20 17:591.09 0.0665 1
1,1,2-Trichloroethane <1.09 ug/m3 03/10/20 17:59 79-00-503/10/20 17:591.09 0.0287 1
Trichloroethene <1.07 ug/m3 03/10/20 17:59 79-01-603/10/20 17:591.07 0.0545 1
1,2,4-Trimethylbenzene 2700 ug/m3 03/11/20 16:43 95-63-603/11/20 16:4349.1 0.0483 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 15
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Sample:AS-2 (End)Lab ID:92468355002 Collected:03/05/20 15:40 Received:03/06/20 09:10 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15 Preparation Method: TO-15VOA (MS) TO-15
1,3,5-Trimethylbenzene 751 ug/m3 03/11/20 16:43 108-67-803/11/20 16:4349.1 0.0631 50
2,2,4-Trimethylpentane 368 ug/m3 03/10/20 17:59 540-84-103/10/20 17:590.934 0.0456 1
Vinyl chloride <0.511 ug/m3 03/10/20 17:59 75-01-403/10/20 17:590.511 0.0457 1
Vinyl bromide <0.875 ug/m3 03/10/20 17:59 593-60-203/10/20 17:590.875 0.0727 1
Vinyl acetate <0.704 ug/m3 03/10/20 17:59 108-05-403/10/20 17:590.704 0.0639 1
m&p-Xylene 2460 ug/m3 03/11/20 16:43 179601-23-103/11/20 16:4386.7 0.0946 50
o-Xylene 1250 ug/m3 03/11/20 16:43 95-47-603/11/20 16:4343.4 0.0633 50
Surrogates
1,4-Dichlorobenzene-d4 (IS)135 %03/10/20 17:59 3855-82-103/10/20 17:5960.0-140 1
1,4-Dichlorobenzene-d4 (IS)104 %03/11/20 16:43 3855-82-103/11/20 16:4360.0-140 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1441065
TO-15
TO-15
VOA (MS) TO-15
Associated Lab Samples:92468355001, 92468355002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507393-3
Associated Lab Samples:92468355001, 92468355002
Matrix:Air
AnalyzedMDL
Acetone ppbv <1.25 1.25 03/10/20 10:150.0569
Allyl chloride ppbv <0.200 0.200 03/10/20 10:150.0546
Benzene ppbv <0.200 0.200 03/10/20 10:150.0460
Benzyl chloride ppbv <0.200 0.200 03/10/20 10:150.0598
Bromodichloromethane ppbv <0.200 0.200 03/10/20 10:150.0436
Bromoform ppbv <0.600 0.600 03/10/20 10:150.0786
Bromomethane ppbv <0.200 0.200 03/10/20 10:150.0609
1,3-Butadiene ppbv <2.00 2.00 03/10/20 10:150.0563
Carbon disulfide ppbv <0.200 0.200 03/10/20 10:150.0544
Carbon tetrachloride ppbv <0.200 0.200 03/10/20 10:150.0585
Chlorobenzene ppbv <0.200 0.200 03/10/20 10:150.0601
Chloroethane ppbv <0.200 0.200 03/10/20 10:150.0489
Chloroform ppbv <0.200 0.200 03/10/20 10:150.0574
Chloromethane ppbv <0.200 0.200 03/10/20 10:150.0544
2-Chlorotoluene ppbv <0.200 0.200 03/10/20 10:150.0605
Cyclohexane ppbv <0.200 0.200 03/10/20 10:150.0534
Dibromochloromethane ppbv <0.200 0.200 03/10/20 10:150.0494
1,2-Dibromoethane (EDB)ppbv <0.200 0.200 03/10/20 10:150.0185
1,2-Dichlorobenzene ppbv <0.200 0.200 03/10/20 10:150.0603
1,3-Dichlorobenzene ppbv <0.200 0.200 03/10/20 10:150.0597
1,4-Dichlorobenzene ppbv <0.200 0.200 03/10/20 10:150.0557
1,2-Dichloroethane ppbv <0.200 0.200 03/10/20 10:150.0616
1,1-Dichloroethane ppbv <0.200 0.200 03/10/20 10:150.0514
1,1-Dichloroethene ppbv <0.200 0.200 03/10/20 10:150.0490
cis-1,2-Dichloroethene ppbv <0.200 0.200 03/10/20 10:150.0389
trans-1,2-Dichloroethene ppbv <0.200 0.200 03/10/20 10:150.0464
1,2-Dichloropropane ppbv <0.200 0.200 03/10/20 10:150.0599
cis-1,3-Dichloropropene ppbv <0.200 0.200 03/10/20 10:150.0588
trans-1,3-Dichloropropene ppbv <0.200 0.200 03/10/20 10:150.0435
1,4-Dioxane (p-Dioxane)ppbv <0.200 0.200 03/10/20 10:150.0554
Trichlorofluoromethane ppbv <0.200 0.200 03/10/20 10:150.0673
Dichlorodifluoromethane ppbv <0.200 0.200 03/10/20 10:150.0601
1,1,2-Trichlorotrifluoroethane ppbv <0.200 0.200 03/10/20 10:150.0687
Dichlorotetrafluoroethane ppbv <0.200 0.200 03/10/20 10:150.0458
n-Heptane ppbv <0.200 0.200 03/10/20 10:150.0626
Hexachloro-1,3-butadiene ppbv <0.630 0.630 03/10/20 10:150.0656
n-Hexane ppbv <0.200 0.200 03/10/20 10:150.0457
Isopropylbenzene (Cumene)ppbv <0.200 0.200 03/10/20 10:150.0563
Methylene Chloride ppbv <0.200 0.200 03/10/20 10:150.0465
2-Hexanone ppbv <1.25 1.25 03/10/20 10:150.0682
2-Butanone (MEK)ppbv <1.25 1.25 03/10/20 10:150.0493
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507393-3
Associated Lab Samples:92468355001, 92468355002
Matrix:Air
AnalyzedMDL
4-Methyl-2-pentanone (MIBK)ppbv <1.25 1.25 03/10/20 10:150.0650
Methyl methacrylate ppbv <0.200 0.200 03/10/20 10:150.0773
Methyl-tert-butyl ether ppbv <0.200 0.200 03/10/20 10:150.0505
Naphthalene ppbv <0.630 0.630 03/10/20 10:150.154
2-Propanol ppbv <1.25 1.25 03/10/20 10:150.0882
Propylene ppbv 0.269J 0.400 J03/10/20 10:150.0932
Styrene ppbv <0.200 0.200 03/10/20 10:150.0465
1,1,2,2-Tetrachloroethane ppbv <0.200 0.200 03/10/20 10:150.0576
Tetrachloroethene ppbv <0.200 0.200 03/10/20 10:150.0497
Tetrahydrofuran ppbv <0.200 0.200 03/10/20 10:150.0508
1,2,4-Trichlorobenzene ppbv <0.630 0.630 03/10/20 10:150.148
1,1,1-Trichloroethane ppbv <0.200 0.200 03/10/20 10:150.0665
1,1,2-Trichloroethane ppbv <0.200 0.200 03/10/20 10:150.0287
Trichloroethene ppbv <0.200 0.200 03/10/20 10:150.0545
2,2,4-Trimethylpentane ppbv <0.200 0.200 03/10/20 10:150.0456
Vinyl chloride ppbv <0.200 0.200 03/10/20 10:150.0457
Vinyl bromide ppbv <0.200 0.200 03/10/20 10:150.0727
Vinyl acetate ppbv <0.200 0.200 03/10/20 10:150.0639
Ethanol ppbv <0.630 0.630 03/10/20 10:150.0832
1,4-Dichlorobenzene-d4 (IS)%92.6 60.0-140 03/10/20 10:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507393-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3507393-2
Ethanol ppbv 3.223.75 85.9 55.0-14871.22.67 18.7 25
Propylene ppbv 3.583.75 95.5 64.0-14486.43.24 9.97 25
Dichlorodifluoromethane ppbv 4.083.75 109 64.0-1391033.88 5.03 25
Dichlorotetrafluoroethane ppbv 4.153.75 111 70.0-1301023.84 7.76 25
Chloromethane ppbv 3.973.75 106 70.0-1301033.88 2.29 25
Vinyl chloride ppbv 4.203.75 112 70.0-1301084.04 3.88 25
1,3-Butadiene ppbv 3.793.75 101 70.0-13093.93.52 7.39 25
Bromomethane ppbv 4.033.75 107 70.0-1301114.15 2.93 25
Chloroethane ppbv 4.253.75 113 70.0-13099.23.72 13.3 25
Trichlorofluoromethane ppbv 3.783.75 101 70.0-1301033.85 1.83 25
1,1,2-Trichlorotrifluoroethane ppbv 4.003.75 107 70.0-1301063.96 1.01 25
1,1-Dichloroethene ppbv 4.023.75 107 70.0-1301114.15 3.18 25
1,1-Dichloroethane ppbv 4.083.75 109 70.0-1301084.05 0.738 25
Acetone ppbv 3.903.75 104 70.0-1301063.99 2.28 25
2-Propanol ppbv 3.953.75 105 70.0-1391114.15 4.94 25
Carbon disulfide ppbv 4.183.75 111 70.0-1301094.07 2.67 25
Methylene Chloride ppbv 3.893.75 104 70.0-1301033.87 0.515 25
Methyl-tert-butyl ether ppbv 3.813.75 102 70.0-1301043.90 2.33 25
trans-1,2-Dichloroethene ppbv 4.123.75 110 70.0-1301104.12 0.00 25
n-Hexane ppbv 4.043.75 108 70.0-1301134.23 4.59 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/13/2020 02:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 15
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507393-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3507393-2
Vinyl acetate ppbv 4.033.75 107 70.0-1301144.26 5.55 25
2-Butanone (MEK)ppbv 4.333.75 115 70.0-1301144.28 1.16 25
cis-1,2-Dichloroethene ppbv 4.133.75 110 70.0-1301074.02 2.70 25
Chloroform ppbv 4.083.75 109 70.0-1301074.03 1.23 25
Cyclohexane ppbv 3.863.75 103 70.0-1301033.86 0.00 25
1,1,1-Trichloroethane ppbv 3.873.75 103 70.0-13099.53.73 3.68 25
Carbon tetrachloride ppbv 3.913.75 104 70.0-1301043.90 0.256 25
Benzene ppbv 4.133.75 110 70.0-1301033.87 6.50 25
1,2-Dichloroethane ppbv 3.763.75 100 70.0-1301033.87 2.88 25
n-Heptane ppbv 4.273.75 114 70.0-1301144.26 0.234 25
Trichloroethene ppbv 3.853.75 103 70.0-1301043.90 1.29 25
1,2-Dichloropropane ppbv 4.093.75 109 70.0-1301124.21 2.89 25
1,4-Dioxane (p-Dioxane)ppbv 3.723.75 99.2 70.0-1401053.92 5.24 25
Bromodichloromethane ppbv 3.913.75 104 70.0-1301023.84 1.81 25
cis-1,3-Dichloropropene ppbv 4.183.75 111 70.0-1301063.99 4.65 25
4-Methyl-2-pentanone (MIBK)ppbv 3.833.75 102 70.0-1391063.97 3.59 25
trans-1,3-Dichloropropene ppbv 3.933.75 105 70.0-1301084.05 3.01 25
1,1,2-Trichloroethane ppbv 3.893.75 104 70.0-1301033.88 0.257 25
Tetrachloroethene ppbv 3.803.75 101 70.0-1301013.79 0.264 25
2-Hexanone ppbv 3.993.75 106 70.0-1491134.23 5.84 25
Dibromochloromethane ppbv 3.933.75 105 70.0-1301043.89 1.02 25
1,2-Dibromoethane (EDB)ppbv 4.113.75 110 70.0-1301074.01 2.46 25
Chlorobenzene ppbv 3.873.75 103 70.0-1301023.84 0.778 25
Styrene ppbv 3.963.75 106 70.0-1301094.08 2.99 25
Bromoform ppbv 3.973.75 106 70.0-1301033.85 3.07 25
1,1,2,2-Tetrachloroethane ppbv 4.113.75 110 70.0-1301074.02 2.21 25
1,3-Dichlorobenzene ppbv 3.973.75 106 70.0-1301074.01 1.00 25
1,4-Dichlorobenzene ppbv 4.053.75 108 70.0-1301074.00 1.24 25
Benzyl chloride ppbv 4.183.75 111 70.0-1521084.05 3.16 25
1,2-Dichlorobenzene ppbv 4.093.75 109 70.0-1301063.97 2.98 25
1,2,4-Trichlorobenzene ppbv 4.173.75 111 70.0-1601074.03 3.41 25
Hexachloro-1,3-butadiene ppbv 3.683.75 98.1 70.0-15199.23.72 1.08 25
Naphthalene ppbv 4.033.75 107 70.0-1591063.96 1.75 25
Allyl chloride ppbv 4.343.75 116 70.0-1301084.06 6.67 25
2-Chlorotoluene ppbv 3.863.75 103 70.0-1301063.96 2.56 25
Methyl methacrylate ppbv 3.903.75 104 70.0-1301023.84 1.55 25
Tetrahydrofuran ppbv 4.123.75 110 70.0-1371084.06 1.47 25
2,2,4-Trimethylpentane ppbv 4.273.75 114 70.0-1301104.14 3.09 25
Vinyl bromide ppbv 4.083.75 109 70.0-1301043.90 4.51 25
Isopropylbenzene (Cumene)ppbv 4.063.75 108 70.0-1301104.14 1.95 25
1,4-Dichlorobenzene-d4 (IS)%101 60.0-140100
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1441937
TO-15
TO-15
VOA (MS) TO-15
Associated Lab Samples:92468355001, 92468355002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3507856-3
Associated Lab Samples:92468355001, 92468355002
Matrix:Air
AnalyzedMDL
Ethylbenzene ppbv <0.200 0.200 03/11/20 09:550.0506
4-Ethyltoluene ppbv <0.200 0.200 03/11/20 09:550.0666
Toluene ppbv <0.200 0.200 03/11/20 09:550.0499
1,2,4-Trimethylbenzene ppbv <0.200 0.200 03/11/20 09:550.0483
1,3,5-Trimethylbenzene ppbv <0.200 0.200 03/11/20 09:550.0631
m&p-Xylene ppbv <0.400 0.400 03/11/20 09:550.0946
o-Xylene ppbv <0.200 0.200 03/11/20 09:550.0633
1,4-Dichlorobenzene-d4 (IS)%99.7 60.0-140 03/11/20 09:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3507856-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3507856-2
Toluene ppbv 4.233.75 113 70.0-1301114.15 1.91 25
Ethylbenzene ppbv 4.293.75 114 70.0-1301154.33 0.928 25
m&p-Xylene ppbv 8.807.50 117 70.0-1301168.71 1.03 25
o-Xylene ppbv 4.493.75 120 70.0-1301204.49 0.00 25
4-Ethyltoluene ppbv 4.473.75 119 70.0-1301164.35 2.72 25
1,3,5-Trimethylbenzene ppbv 4.263.75 114 70.0-1301174.37 2.55 25
1,2,4-Trimethylbenzene ppbv 4.403.75 117 70.0-1301164.36 0.913 25
1,4-Dichlorobenzene-d4 (IS)%102 60.0-140103
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
SAMPLE QUALIFIERS
Sample: 92468355001
Volatile Organic Compounds (MS) by Method TO-15 - Surrogate failure due to matrix interference.[1]
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Surrogate recovery was above laboratory control limits. Results may be biased high.ST
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Page 13 of 15
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92468355
CPC19006-001 CPC Selma/19006
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92468355001 1441065 1441065AS-1 (Startup)TO-15 TO-15
92468355001 1441937 1441937AS-1 (Startup)TO-15 TO-15
92468355002 1441065 1441065AS-2 (End)TO-15 TO-15
92468355002 1441937 1441937AS-2 (End)TO-15 TO-15
REPORT OF LABORATORY ANALYSIS
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Page 14 of 15
Page 15 of 15
#=CL#
November 02, 2020
LIMS USE: FR - ANDREW STREET
LIMS OBJECT ID: 92501426
92501426
Project:
Pace Project No.:
RE:
Andrew Street
Apex Companies
5900-O Northwoods Business
Parkway
Charlotte, NC 28269
CPC SELMA/CPC 20104
Dear Andrew Street:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
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Georgia Certification: NELAP
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Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
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Massachusetts Certification #: M-TN003
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Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
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Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Lab ID Sample ID Matrix Date Collected Date Received
92501426001 AP-1 Water 10/20/20 10:30 10/21/20 08:15
92501426002 AP-2 Water 10/20/20 12:45 10/21/20 08:15
92501426003 AP-3 Water 10/20/20 13:50 10/21/20 08:15
92501426004 AP-4 Water 10/20/20 14:20 10/21/20 08:15
92501426005 AP-5 Water 10/20/20 13:20 10/21/20 08:15
92501426006 AP-8 Water 10/20/20 14:45 10/21/20 08:15
92501426007 AP-9 Water 10/20/20 11:35 10/21/20 08:15
92501426008 AP-10 Water 10/20/20 11:05 10/21/20 08:15
92501426009 AP-11 Water 10/20/20 15:45 10/21/20 08:15
92501426010 EQUIPMENT BLANK-1 Water 10/20/20 15:50 10/21/20 08:15
92501426011 DUP-1 Water 10/20/20 00:00 10/21/20 08:15
92501426012 TB-1 Water 10/20/20 00:00 10/21/20 08:15
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92501426001 AP-1 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426002 AP-2 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CSAS
92501426003 AP-3 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426004 AP-4 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426005 AP-5 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426006 AP-8 MADEP VPH 6 PANACG, ADM
EPA 8260D 8 PASI-CCL
92501426007 AP-9 MADEP VPH 6 PANACG, ADM
EPA 8260D 8 PASI-CCL
92501426008 AP-10 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426009 AP-11 MADEP VPH 6 PANACG, ADM
EPA 8260D 8 PASI-CCL
92501426010 EQUIPMENT BLANK-1 MADEP VPH 6 PANACG
EPA 8260D 8 PASI-CCL
92501426011 DUP-1 MADEP VPH 6 PANACG, ADM
EPA 8260D 8 PASI-CCL
92501426012 TB-1 EPA 8260D 8 PASI-CCL
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-1 Lab ID:92501426001 Collected:10/20/20 10:30 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)270 ug/L 10/29/20 22:0110/29/20 22:0110033.3 1
Aliphatic (C09-C12)<100 ug/L 10/29/20 22:0110/29/20 22:0110033.3 1
Aromatic (C09-C10),Unadjusted 56.2J ug/L 10/29/20 22:01 TPHC9C10A J10/29/20 22:0110033.3 1
Total VPH 326 ug/L 10/29/20 22:01 VPH10/29/20 22:0110033.3 1
Surrogates
2,5-Dibromotoluene (FID)89.9 %10/29/20 22:01 615-59-8FID10/29/20 22:0170.0-130 1
2,5-Dibromotoluene (PID)95.9 %10/29/20 22:01 615-59-8PID10/29/20 22:0170.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 179 ug/L 10/26/20 06:25 71-43-22.0 0.30 2
Ethylbenzene <2.0 ug/L 10/26/20 06:25 100-41-42.0 0.51 2
Naphthalene 1.3J ug/L 10/26/20 06:25 91-20-32.0 0.70 2
Toluene 1.4J ug/L 10/26/20 06:25 108-88-32.0 0.49 2
Xylene (Total)<2.0 ug/L 10/26/20 06:25 1330-20-72.0 1.3 2
Surrogates
4-Bromofluorobenzene (S)99 %10/26/20 06:25 460-00-470-130 2
1,2-Dichloroethane-d4 (S)100 %10/26/20 06:25 17060-07-070-130 2
Toluene-d8 (S)100 %10/26/20 06:25 2037-26-570-130 2
Sample:AP-2 Lab ID:92501426002 Collected:10/20/20 12:45 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)2880 ug/L 10/29/20 22:3410/29/20 22:3410033.3 1
Aliphatic (C09-C12)1450 ug/L 10/29/20 22:3410/29/20 22:3410033.3 1
Aromatic (C09-C10),Unadjusted 639 ug/L 10/29/20 22:34 TPHC9C10A10/29/20 22:3410033.3 1
Total VPH 4970 ug/L 10/29/20 22:34 VPH10/29/20 22:3410033.3 1
Surrogates
2,5-Dibromotoluene (FID)94.1 %10/29/20 22:34 615-59-8FID10/29/20 22:3470.0-130 1
2,5-Dibromotoluene (PID)100 %10/29/20 22:34 615-59-8PID10/29/20 22:3470.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 498 ug/L 10/22/20 14:06 71-43-25.0 0.75 5
Ethylbenzene 220 ug/L 10/22/20 14:06 100-41-45.0 1.3 5
Naphthalene 49.1 ug/L 10/22/20 14:06 91-20-35.0 1.8 5
Toluene 159 ug/L 10/22/20 14:06 108-88-35.0 1.2 5
Xylene (Total)478 ug/L 10/22/20 14:06 1330-20-75.0 3.2 5
Surrogates
4-Bromofluorobenzene (S)97 %10/22/20 14:06 460-00-470-130 5
1,2-Dichloroethane-d4 (S)104 %10/22/20 14:06 17060-07-070-130 5
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-2 Lab ID:92501426002 Collected:10/20/20 12:45 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Surrogates
Toluene-d8 (S)99 %10/22/20 14:06 2037-26-570-130 5
Sample:AP-3 Lab ID:92501426003 Collected:10/20/20 13:50 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)<100 ug/L 10/29/20 23:0710/29/20 23:0710033.3 1
Aliphatic (C09-C12)<100 ug/L 10/29/20 23:0710/29/20 23:0710033.3 1
Aromatic (C09-C10),Unadjusted 39.2J ug/L 10/29/20 23:07 TPHC9C10A J10/29/20 23:0710033.3 1
Total VPH 39.2J ug/L 10/29/20 23:07 VPH J10/29/20 23:0710033.3 1
Surrogates
2,5-Dibromotoluene (FID)89.9 %10/29/20 23:07 615-59-8FID10/29/20 23:0770.0-130 1
2,5-Dibromotoluene (PID)95.7 %10/29/20 23:07 615-59-8PID10/29/20 23:0770.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 2.2 ug/L 10/22/20 10:25 71-43-21.0 0.15 1
Ethylbenzene <1.0 ug/L 10/22/20 10:25 100-41-41.0 0.26 1
Naphthalene 2.0 ug/L 10/22/20 10:25 91-20-31.0 0.35 1
Toluene <1.0 ug/L 10/22/20 10:25 108-88-31.0 0.24 1
Xylene (Total)<1.0 ug/L 10/22/20 10:25 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)99 %10/22/20 10:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/22/20 10:25 17060-07-070-130 1
Toluene-d8 (S)100 %10/22/20 10:25 2037-26-570-130 1
Sample:AP-4 Lab ID:92501426004 Collected:10/20/20 14:20 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)105 ug/L 10/29/20 23:4110/29/20 23:4110033.3 1
Aliphatic (C09-C12)<100 ug/L 10/29/20 23:4110/29/20 23:4110033.3 1
Aromatic (C09-C10),Unadjusted 42.4J ug/L 10/29/20 23:41 TPHC9C10A J10/29/20 23:4110033.3 1
Total VPH 147 ug/L 10/29/20 23:41 VPH10/29/20 23:4110033.3 1
Surrogates
2,5-Dibromotoluene (FID)91.3 %10/29/20 23:41 615-59-8FID10/29/20 23:4170.0-130 1
2,5-Dibromotoluene (PID)97.0 %10/29/20 23:41 615-59-8PID10/29/20 23:4170.0-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-4 Lab ID:92501426004 Collected:10/20/20 14:20 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 37.7 ug/L 10/22/20 09:48 71-43-21.0 0.15 1
Ethylbenzene 6.0 ug/L 10/22/20 09:48 100-41-41.0 0.26 1
Naphthalene 3.4 ug/L 10/22/20 09:48 91-20-31.0 0.35 1
Toluene <1.0 ug/L 10/22/20 09:48 108-88-31.0 0.24 1
Xylene (Total)8.4 ug/L 10/22/20 09:48 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)100 %10/22/20 09:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/22/20 09:48 17060-07-070-130 1
Toluene-d8 (S)100 %10/22/20 09:48 2037-26-570-130 1
Sample:AP-5 Lab ID:92501426005 Collected:10/20/20 13:20 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)305 ug/L 10/30/20 00:1410/30/20 00:1410033.3 1
Aliphatic (C09-C12)502 ug/L 10/30/20 00:1410/30/20 00:1410033.3 1
Aromatic (C09-C10),Unadjusted 245 ug/L 10/30/20 00:14 TPHC9C10A10/30/20 00:1410033.3 1
Total VPH 1050 ug/L 10/30/20 00:14 VPH10/30/20 00:1410033.3 1
Surrogates
2,5-Dibromotoluene (FID)95.7 %10/30/20 00:14 615-59-8FID10/30/20 00:1470.0-130 1
2,5-Dibromotoluene (PID)103 %10/30/20 00:14 615-59-8PID10/30/20 00:1470.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 41.5 ug/L 10/22/20 10:07 71-43-21.0 0.15 1
Ethylbenzene 96.3 ug/L 10/22/20 10:07 100-41-41.0 0.26 1
Naphthalene 26.4 ug/L 10/22/20 10:07 91-20-31.0 0.35 1
Toluene 3.3 ug/L 10/22/20 10:07 108-88-31.0 0.24 1
Xylene (Total)269 ug/L 10/22/20 10:07 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)98 %10/22/20 10:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/22/20 10:07 17060-07-070-130 1
Toluene-d8 (S)99 %10/22/20 10:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-8 Lab ID:92501426006 Collected:10/20/20 14:45 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)2790 ug/L 10/30/20 00:4710/30/20 00:4710033.3 1
Aliphatic (C09-C12)8250 ug/L 10/30/20 00:4710/30/20 00:4710033.3 1
Aromatic (C09-C10),Unadjusted 3750 ug/L 10/30/20 13:09 TPHC9C10A10/30/20 13:095001675
Total VPH 11000 ug/L 10/30/20 00:47 VPH10/30/20 00:4710033.3 1
Surrogates
2,5-Dibromotoluene (FID)99.4 %10/30/20 00:47 615-59-8FID10/30/20 00:4770.0-130 1
2,5-Dibromotoluene (FID)89.3 %10/30/20 13:09 615-59-8FID10/30/20 13:0970.0-130 5
2,5-Dibromotoluene (PID)103 %10/30/20 00:47 615-59-8PID10/30/20 00:4770.0-130 1
2,5-Dibromotoluene (PID)95.5 %10/30/20 13:09 615-59-8PID10/30/20 13:0970.0-130 5
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 130 ug/L 10/26/20 07:38 71-43-25.0 0.75 5
Ethylbenzene 884 ug/L 10/26/20 07:38 100-41-45.0 1.3 5
Naphthalene 355 ug/L 10/26/20 07:38 91-20-35.0 1.8 5
Toluene <5.0 ug/L 10/26/20 07:38 108-88-35.0 1.2 5
Xylene (Total)963 ug/L 10/26/20 07:38 1330-20-75.0 3.2 5
Surrogates
4-Bromofluorobenzene (S)100 %10/26/20 07:38 460-00-470-130 5
1,2-Dichloroethane-d4 (S)100 %10/26/20 07:38 17060-07-070-130 5
Toluene-d8 (S)98 %10/26/20 07:38 2037-26-570-130 5
Sample:AP-9 Lab ID:92501426007 Collected:10/20/20 11:35 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)<100 ug/L 10/30/20 01:2010/30/20 01:2010033.3 1
Aliphatic (C09-C12)55.9J ug/L 10/30/20 01:20 J10/30/20 01:2010033.3 1
Aromatic (C09-C10),Unadjusted 33.4J ug/L 10/30/20 13:42 TPHC9C10A J10/30/20 13:4210033.3 1
Total VPH 55.9J ug/L 10/30/20 01:20 VPH J10/30/20 01:2010033.3 1
Surrogates
2,5-Dibromotoluene (FID)88.7 %10/30/20 01:20 615-59-8FID10/30/20 01:2070.0-130 1
2,5-Dibromotoluene (FID)90.2 %10/30/20 13:42 615-59-8FID10/30/20 13:4270.0-130 1
2,5-Dibromotoluene (PID)92.4 %10/30/20 01:20 615-59-8PID10/30/20 01:2070.0-130 1
2,5-Dibromotoluene (PID)97.5 %10/30/20 13:42 615-59-8PID10/30/20 13:4270.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene <1.0 ug/L 10/26/20 05:49 71-43-21.0 0.15 1
Ethylbenzene <1.0 ug/L 10/26/20 05:49 100-41-41.0 0.26 1
Naphthalene <1.0 ug/L 10/26/20 05:49 91-20-31.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-9 Lab ID:92501426007 Collected:10/20/20 11:35 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Toluene <1.0 ug/L 10/26/20 05:49 108-88-31.0 0.24 1
Xylene (Total)<1.0 ug/L 10/26/20 05:49 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)99 %10/26/20 05:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/26/20 05:49 17060-07-070-130 1
Toluene-d8 (S)98 %10/26/20 05:49 2037-26-570-130 1
Sample:AP-10 Lab ID:92501426008 Collected:10/20/20 11:05 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)4020 ug/L 10/30/20 01:5310/30/20 01:5310033.3 1
Aliphatic (C09-C12)946 ug/L 10/30/20 01:5310/30/20 01:5310033.3 1
Aromatic (C09-C10),Unadjusted 474 ug/L 10/30/20 01:53 TPHC9C10A10/30/20 01:5310033.3 1
Total VPH 5440 ug/L 10/30/20 01:53 VPH10/30/20 01:5310033.3 1
Surrogates
2,5-Dibromotoluene (FID)95.1 %10/30/20 01:53 615-59-8FID10/30/20 01:5370.0-130 1
2,5-Dibromotoluene (PID)101 %10/30/20 01:53 615-59-8PID10/30/20 01:5370.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 1100 ug/L 10/26/20 08:14 71-43-210.0 1.5 10
Ethylbenzene 274 ug/L 10/26/20 08:14 100-41-410.0 2.6 10
Naphthalene 43.6 ug/L 10/26/20 08:14 91-20-310.0 3.5 10
Toluene 25.7 ug/L 10/26/20 08:14 108-88-310.0 2.4 10
Xylene (Total)213 ug/L 10/26/20 08:14 1330-20-710.0 6.3 10
Surrogates
4-Bromofluorobenzene (S)99 %10/26/20 08:14 460-00-470-130 10
1,2-Dichloroethane-d4 (S)101 %10/26/20 08:14 17060-07-070-130 10
Toluene-d8 (S)99 %10/26/20 08:14 2037-26-570-130 10
Sample:AP-11 Lab ID:92501426009 Collected:10/20/20 15:45 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)1010 ug/L 10/30/20 02:2710/30/20 02:2710033.3 1
Aliphatic (C09-C12)6710 ug/L 10/30/20 02:2710/30/20 02:2710033.3 1
Aromatic (C09-C10),Unadjusted 3450 ug/L 10/30/20 14:15 TPHC9C10A10/30/20 14:155001675
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:AP-11 Lab ID:92501426009 Collected:10/20/20 15:45 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Total VPH 7720 ug/L 10/30/20 02:27 VPH10/30/20 02:2710033.3 1
Surrogates
2,5-Dibromotoluene (FID)95.4 %10/30/20 02:27 615-59-8FID10/30/20 02:2770.0-130 1
2,5-Dibromotoluene (FID)90.2 %10/30/20 14:15 615-59-8FID10/30/20 14:1570.0-130 5
2,5-Dibromotoluene (PID)97.4 %10/30/20 02:27 615-59-8PID10/30/20 02:2770.0-130 1
2,5-Dibromotoluene (PID)96.5 %10/30/20 14:15 615-59-8PID10/30/20 14:1570.0-130 5
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 62.5 ug/L 10/26/20 07:02 71-43-24.0 0.60 4
Ethylbenzene 556 ug/L 10/26/20 07:02 100-41-44.0 1.0 4
Naphthalene 250 ug/L 10/26/20 07:02 91-20-34.0 1.4 4
Toluene 62.8 ug/L 10/26/20 07:02 108-88-34.0 0.98 4
Xylene (Total)713 ug/L 10/26/20 07:02 1330-20-74.0 2.5 4
Surrogates
4-Bromofluorobenzene (S)98 %10/26/20 07:02 460-00-470-130 4
1,2-Dichloroethane-d4 (S)101 %10/26/20 07:02 17060-07-070-130 4
Toluene-d8 (S)98 %10/26/20 07:02 2037-26-570-130 4
Sample:EQUIPMENT BLANK-1 Lab ID:92501426010 Collected:10/20/20 15:50 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)<100 ug/L 10/29/20 19:4810/29/20 19:4810033.3 1
Aliphatic (C09-C12)<100 ug/L 10/29/20 19:4810/29/20 19:4810033.3 1
Aromatic (C09-C10),Unadjusted <100 ug/L 10/29/20 19:48 TPHC9C10A10/29/20 19:4810033.3 1
Total VPH <100 ug/L 10/29/20 19:48 VPH10/29/20 19:4810033.3 1
Surrogates
2,5-Dibromotoluene (FID)87.7 %10/29/20 19:48 615-59-8FID10/29/20 19:4870.0-130 1
2,5-Dibromotoluene (PID)92.9 %10/29/20 19:48 615-59-8PID10/29/20 19:4870.0-130 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene <1.0 ug/L 10/22/20 05:49 71-43-21.0 0.15 1
Ethylbenzene <1.0 ug/L 10/22/20 05:49 100-41-41.0 0.26 1
Naphthalene <1.0 ug/L 10/22/20 05:49 91-20-31.0 0.35 1
Toluene <1.0 ug/L 10/22/20 05:49 108-88-31.0 0.24 1
Xylene (Total)<1.0 ug/L 10/22/20 05:49 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)98 %10/22/20 05:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/22/20 05:49 17060-07-070-130 1
Toluene-d8 (S)100 %10/22/20 05:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Sample:DUP-1 Lab ID:92501426011 Collected:10/20/20 00:00 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)1040 ug/L 10/30/20 03:0010/30/20 03:0010033.3 1
Aliphatic (C09-C12)7050 ug/L 10/30/20 03:0010/30/20 03:0010033.3 1
Aromatic (C09-C10),Unadjusted 3550 ug/L 10/30/20 14:47 TPHC9C10A10/30/20 14:475001675
Total VPH 8090 ug/L 10/30/20 03:00 VPH10/30/20 03:0010033.3 1
Surrogates
2,5-Dibromotoluene (FID)101 %10/30/20 03:00 615-59-8FID10/30/20 03:0070.0-130 1
2,5-Dibromotoluene (FID)90.8 %10/30/20 14:47 615-59-8FID10/30/20 14:4770.0-130 5
2,5-Dibromotoluene (PID)103 %10/30/20 03:00 615-59-8PID10/30/20 03:0070.0-130 1
2,5-Dibromotoluene (PID)96.9 %10/30/20 14:47 615-59-8PID10/30/20 14:4770.0-130 5
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene 50.6 ug/L 10/26/20 07:20 71-43-25.0 0.75 5
Ethylbenzene 477 ug/L 10/26/20 07:20 100-41-45.0 1.3 5
Naphthalene 234 ug/L 10/26/20 07:20 91-20-35.0 1.8 5
Toluene 34.6 ug/L 10/26/20 07:20 108-88-35.0 1.2 5
Xylene (Total)552 ug/L 10/26/20 07:20 1330-20-75.0 3.2 5
Surrogates
4-Bromofluorobenzene (S)99 %10/26/20 07:20 460-00-470-130 5
1,2-Dichloroethane-d4 (S)99 %10/26/20 07:20 17060-07-070-130 5
Toluene-d8 (S)101 %10/26/20 07:20 2037-26-570-130 5
Sample:TB-1 Lab ID:92501426012 Collected:10/20/20 00:00 Received:10/21/20 08:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Benzene <1.0 ug/L 10/22/20 05:12 71-43-21.0 0.15 1
Ethylbenzene <1.0 ug/L 10/22/20 05:12 100-41-41.0 0.26 1
Naphthalene <1.0 ug/L 10/22/20 05:12 91-20-31.0 0.35 1
Toluene <1.0 ug/L 10/22/20 05:12 108-88-31.0 0.24 1
Xylene (Total)<1.0 ug/L 10/22/20 05:12 1330-20-71.0 0.63 1
Surrogates
4-Bromofluorobenzene (S)99 %10/22/20 05:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/22/20 05:12 17060-07-070-130 1
Toluene-d8 (S)101 %10/22/20 05:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1566913
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92501426001, 92501426002, 92501426003, 92501426004, 92501426005, 92501426006, 92501426007,
92501426008, 92501426009, 92501426010, 92501426011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3587451-3
Associated Lab Samples:92501426001, 92501426002, 92501426003, 92501426004, 92501426005, 92501426006, 92501426007,
92501426008, 92501426009, 92501426010, 92501426011
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L <100 100 10/29/20 14:5933.3
Aliphatic (C09-C12)ug/L <100 100 10/29/20 14:5933.3
Aromatic (C09-C10),Unadjusted ug/L <100 100 10/29/20 14:5933.3
Total VPH ug/L <100 100 10/29/20 14:5933.3
2,5-Dibromotoluene (FID)%83.1 70.0-130 10/29/20 14:59
2,5-Dibromotoluene (PID)%88.6 70.0-130 10/29/20 14:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3587451-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3587451-2
Aliphatic (C05-C08)ug/L 10401200 86.7 70.0-13088.31060 1.90 25
Aliphatic (C09-C12)ug/L 13801400 98.6 70.0-1301001400 1.44 25
Aromatic (C09-C10),Unadjusted ug/L 216200 108 70.0-130110220 1.83 25
Total VPH ug/L 26402800 94.3 70.0-13095.72680 1.50 25
2,5-Dibromotoluene (FID)%88.5 70.0-13090.1
2,5-Dibromotoluene (PID)%95.2 70.0-13096.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568294
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92501426006, 92501426007, 92501426009, 92501426011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3587687-3
Associated Lab Samples:92501426006, 92501426007, 92501426009, 92501426011
Matrix:Water
AnalyzedMDL
Aromatic (C09-C10),Unadjusted ug/L <100 100 10/30/20 11:1533.3
2,5-Dibromotoluene (FID)%86.5 70.0-130 10/30/20 11:15
2,5-Dibromotoluene (PID)%92.7 70.0-130 10/30/20 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3587687-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3587687-2
Aromatic (C09-C10),Unadjusted ug/L 206200 103 70.0-130103206 0.00 25
2,5-Dibromotoluene (FID)%87.9 70.0-13091.1
2,5-Dibromotoluene (PID)%97.6 70.0-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
574844
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92501426003, 92501426004, 92501426005, 92501426010, 92501426012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3043246
Associated Lab Samples:92501426003, 92501426004, 92501426005, 92501426010, 92501426012
Matrix:Water
AnalyzedMDL
Benzene ug/L <1.0 1.0 10/22/20 04:360.15
Ethylbenzene ug/L <1.0 1.0 10/22/20 04:360.26
Naphthalene ug/L <1.0 1.0 10/22/20 04:360.35
Toluene ug/L <1.0 1.0 10/22/20 04:360.24
Xylene (Total)ug/L <1.0 1.0 10/22/20 04:360.63
1,2-Dichloroethane-d4 (S)%96 70-130 10/22/20 04:36
4-Bromofluorobenzene (S)%100 70-130 10/22/20 04:36
Toluene-d8 (S)%102 70-130 10/22/20 04:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3043247LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/L 52.350 105 70-130
Ethylbenzene ug/L 52.150 104 70-130
Naphthalene ug/L 57.950 116 70-133
Toluene ug/L 52.450 105 70-130
Xylene (Total)ug/L 162150 108 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3043248MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501397003
3043249
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/L 20 105 67-150113 8 3020ND21.0 22.7
Ethylbenzene ug/L 20 104 68-143112 8 3020ND20.7 22.4
Naphthalene ug/L M120-421 57-150-414 7 302010622.0 23.5
Toluene ug/L 20 103 47-157111 8 3020ND20.6 22.2
Xylene (Total)ug/L 60 106 66-145114 7 3060ND63.7 68.7
1,2-Dichloroethane-d4 (S)%96 70-13095
4-Bromofluorobenzene (S)%99 70-13099
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
574852
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92501426002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3043261
Associated Lab Samples:92501426002
Matrix:Water
AnalyzedMDL
Benzene ug/L <1.0 1.0 10/22/20 12:560.15
Ethylbenzene ug/L <1.0 1.0 10/22/20 12:560.26
Naphthalene ug/L <1.0 1.0 10/22/20 12:560.35
Toluene ug/L <1.0 1.0 10/22/20 12:560.24
Xylene (Total)ug/L <1.0 1.0 10/22/20 12:560.63
1,2-Dichloroethane-d4 (S)%105 70-130 10/22/20 12:56
4-Bromofluorobenzene (S)%96 70-130 10/22/20 12:56
Toluene-d8 (S)%102 70-130 10/22/20 12:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3043262LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/L 52.350 105 70-130
Ethylbenzene ug/L 51.250 102 70-130
Naphthalene ug/L 51.550 103 70-133
Toluene ug/L 50.650 101 70-130
Xylene (Total)ug/L 155150 103 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3043263MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501426002
3043264
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/L 100 124 67-15078 8 30100498622576
Ethylbenzene ug/L 100 118 68-143100 5 30100220338320
Naphthalene ug/L 100 94 57-150101 4 3010049.1 143 150
Toluene ug/L 100 110 47-15793 7 30100159269252
Xylene (Total)ug/L 300 112 66-14596 6 30300478813766
1,2-Dichloroethane-d4 (S)%116 70-130103
4-Bromofluorobenzene (S)%100 70-13096
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
575501
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92501426001, 92501426006, 92501426007, 92501426008, 92501426009, 92501426011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3046744
Associated Lab Samples:92501426001, 92501426006, 92501426007, 92501426008, 92501426009, 92501426011
Matrix:Water
AnalyzedMDL
Benzene ug/L <1.0 1.0 10/26/20 03:060.15
Ethylbenzene ug/L <1.0 1.0 10/26/20 03:060.26
Naphthalene ug/L <1.0 1.0 10/26/20 03:060.35
Toluene ug/L <1.0 1.0 10/26/20 03:060.24
Xylene (Total)ug/L <1.0 1.0 10/26/20 03:060.63
1,2-Dichloroethane-d4 (S)%99 70-130 10/26/20 03:06
4-Bromofluorobenzene (S)%101 70-130 10/26/20 03:06
Toluene-d8 (S)%100 70-130 10/26/20 03:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3046745LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/L 49.650 99 70-130
Ethylbenzene ug/L 50.050 100 70-130
Naphthalene ug/L 53.450 107 70-133
Toluene ug/L 50.650 101 70-130
Xylene (Total)ug/L 157150 105 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3046746MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501584010
3046747
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/L 20 123 67-150115 7 30201.0 U 24.6 22.9
Ethylbenzene ug/L 20 122 68-143113 8 30201.0 U 24.4 22.6
Naphthalene ug/L 20 117 57-150111 5 30201.0 U 23.4 22.2
Toluene ug/L 20 120 47-157113 6 30201.0 U 24.0 22.6
Xylene (Total)ug/L 60 122 66-145113 8 30601.0 U 73.1 67.8
1,2-Dichloroethane-d4 (S)%96 70-13094
4-Bromofluorobenzene (S)%102 70-13099
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
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Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92501426
CPC SELMA/CPC 20104
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92501426001 1566913 1566913AP-1 MADEPV MADEP VPH
92501426002 1566913 1566913AP-2 MADEPV MADEP VPH
92501426003 1566913 1566913AP-3 MADEPV MADEP VPH
92501426004 1566913 1566913AP-4 MADEPV MADEP VPH
92501426005 1566913 1566913AP-5 MADEPV MADEP VPH
92501426006 1566913 1566913AP-8 MADEPV MADEP VPH
92501426006 1568294 1568294AP-8 MADEPV MADEP VPH
92501426007 1566913 1566913AP-9 MADEPV MADEP VPH
92501426007 1568294 1568294AP-9 MADEPV MADEP VPH
92501426008 1566913 1566913AP-10 MADEPV MADEP VPH
92501426009 1566913 1566913AP-11 MADEPV MADEP VPH
92501426009 1568294 1568294AP-11 MADEPV MADEP VPH
92501426010 1566913 1566913EQUIPMENT BLANK-1 MADEPV MADEP VPH
92501426011 1566913 1566913DUP-1 MADEPV MADEP VPH
92501426011 1568294 1568294DUP-1 MADEPV MADEP VPH
92501426001 575501AP-1 EPA 8260D
92501426002 574852AP-2 EPA 8260D
92501426003 574844AP-3 EPA 8260D
92501426004 574844AP-4 EPA 8260D
92501426005 574844AP-5 EPA 8260D
92501426006 575501AP-8 EPA 8260D
92501426007 575501AP-9 EPA 8260D
92501426008 575501AP-10 EPA 8260D
92501426009 575501AP-11 EPA 8260D
92501426010 574844EQUIPMENT BLANK-1 EPA 8260D
92501426011 575501DUP-1 EPA 8260D
92501426012 574844TB-1 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/02/2020 08:27 AM
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Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
December 31, 2020
LIMS USE: FR - ANDREW STREET
LIMS OBJECT ID: 92512081
92512081
Project:
Pace Project No.:
RE:
Andrew Street
Apex Companies
5900-O Northwoods Business
Parkway
Charlotte, NC 28269
CPC 20104
Dear Andrew Street:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92512081
CPC 20104
Pace Analytical Services - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A2LA Certification #: 2926.01*
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605*
Georgia Certification #: 959
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Massachusetts DWP Certification #: via MN 027-053-137
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Certifcation #: via MN 027-053-137
Minnesota Petrofund Certification #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563*
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
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Page 2 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92512081
CPC 20104
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92512081001 AFVR - START TO-15 58 PASI-MDR1
92512081002 AFVR - END TO-15 58 PASI-MDR1
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92512081
CPC 20104
Sample:AFVR - START Lab ID:92512081001 Collected:12/15/20 09:05 Received:12/16/20 09:08 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15
Pace Analytical Services - Minneapolis
TO15 MSV AIR
Acetone ND ug/m3 12/30/20 21:18 67-64-18.1 1.34
Benzene 10.0 ug/m3 12/30/20 21:18 71-43-20.44 1.34
Bromodichloromethane ND ug/m3 12/30/20 21:18 75-27-41.8 1.34
Bromoform ND ug/m3 12/30/20 21:18 75-25-27.0 1.34
Bromomethane ND ug/m3 12/30/20 21:18 74-83-91.1 1.34
1,3-Butadiene ND ug/m3 12/30/20 21:18 106-99-00.60 1.34
2-Butanone (MEK)ND ug/m3 12/30/20 21:18 78-93-34.0 1.34
Carbon disulfide ND ug/m3 12/30/20 21:18 75-15-00.85 1.34
Carbon tetrachloride ND ug/m3 12/30/20 21:18 56-23-51.7 1.34
Chlorobenzene ND ug/m3 12/30/20 21:18 108-90-71.3 1.34
Chloroethane ND ug/m3 12/30/20 21:18 75-00-30.72 1.34
Chloroform ND ug/m3 12/30/20 21:18 67-66-30.66 1.34
Chloromethane ND ug/m3 12/30/20 21:18 74-87-30.56 1.34
Cyclohexane 21.8 ug/m3 12/30/20 21:18 110-82-72.3 1.34
Dibromochloromethane ND ug/m3 12/30/20 21:18 124-48-12.3 1.34
1,2-Dibromoethane (EDB)ND ug/m3 12/30/20 21:18 106-93-41.0 1.34
1,2-Dichlorobenzene ND ug/m3 12/30/20 21:18 95-50-11.6 1.34
1,3-Dichlorobenzene ND ug/m3 12/30/20 21:18 541-73-11.6 1.34
1,4-Dichlorobenzene ND ug/m3 12/30/20 21:18 106-46-74.1 1.34
Dichlorodifluoromethane 3.3 ug/m3 12/30/20 21:18 75-71-81.4 1.34
1,1-Dichloroethane ND ug/m3 12/30/20 21:18 75-34-31.1 1.34
1,2-Dichloroethane ND ug/m3 12/30/20 21:18 107-06-21.1 1.34
1,1-Dichloroethene ND ug/m3 12/30/20 21:18 75-35-41.1 1.34
cis-1,2-Dichloroethene 5.6 ug/m3 12/30/20 21:18 156-59-21.1 1.34
trans-1,2-Dichloroethene ND ug/m3 12/30/20 21:18 156-60-51.1 1.34
1,2-Dichloropropane ND ug/m3 12/30/20 21:18 78-87-51.3 1.34
cis-1,3-Dichloropropene ND ug/m3 12/30/20 21:18 10061-01-51.2 1.34
trans-1,3-Dichloropropene ND ug/m3 12/30/20 21:18 10061-02-61.2 1.34
Dichlorotetrafluoroethane ND ug/m3 12/30/20 21:18 76-14-21.9 1.34
Ethyl acetate ND ug/m3 12/30/20 21:18 141-78-60.98 1.34
Ethylbenzene 60.9 ug/m3 12/30/20 21:18 100-41-41.2 1.34
4-Ethyltoluene 19.3 ug/m3 12/30/20 21:18 622-96-83.4 1.34
n-Heptane 10.8 ug/m3 12/30/20 21:18 142-82-51.1 1.34
Hexachloro-1,3-butadiene ND ug/m3 12/30/20 21:18 87-68-37.3 1.34
n-Hexane 10.6 ug/m3 12/30/20 21:18 110-54-30.96 1.34
2-Hexanone ND ug/m3 12/30/20 21:18 591-78-65.6 1.34
Methylene Chloride ND ug/m3 12/30/20 21:18 75-09-24.7 1.34
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/30/20 21:18 108-10-15.6 1.34
Methyl-tert-butyl ether ND ug/m3 12/30/20 21:18 1634-04-44.9 1.34
Naphthalene 4.7 ug/m3 12/30/20 21:18 91-20-33.6 1.34
Propylene 1.1 ug/m3 12/30/20 21:18 115-07-10.47 1.34
Styrene ND ug/m3 12/30/20 21:18 100-42-51.2 1.34
1,1,2,2-Tetrachloroethane ND ug/m3 12/30/20 21:18 79-34-50.94 1.34
Tetrachloroethene 7.8 ug/m3 12/30/20 21:18 127-18-40.92 1.34
Tetrahydrofuran ND ug/m3 12/30/20 21:18 109-99-90.80 1.34
Toluene 38.8 ug/m3 12/30/20 21:18 108-88-31.0 1.34
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92512081
CPC 20104
Sample:AFVR - START Lab ID:92512081001 Collected:12/15/20 09:05 Received:12/16/20 09:08 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15
Pace Analytical Services - Minneapolis
TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/30/20 21:18 120-82-110.1 1.34
1,1,1-Trichloroethane ND ug/m3 12/30/20 21:18 71-55-61.5 1.34
1,1,2-Trichloroethane ND ug/m3 12/30/20 21:18 79-00-50.74 1.34
Trichloroethene 1.5 ug/m3 12/30/20 21:18 79-01-60.73 1.34
Trichlorofluoromethane 1.6 ug/m3 12/30/20 21:18 75-69-41.5 1.34
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/30/20 21:18 76-13-12.1 1.34
1,2,4-Trimethylbenzene 51.4 ug/m3 12/30/20 21:18 95-63-61.3 1.34
1,3,5-Trimethylbenzene 18.6 ug/m3 12/30/20 21:18 108-67-81.3 1.34
Vinyl acetate ND ug/m3 12/30/20 21:18 108-05-40.96 1.34
Vinyl chloride ND ug/m3 12/30/20 21:18 75-01-40.35 1.34
m&p-Xylene 98.8 ug/m3 12/30/20 21:18 179601-23-12.4 1.34
o-Xylene 34.1 ug/m3 12/30/20 21:18 95-47-61.2 1.34
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92512081
CPC 20104
Sample:AFVR - END Lab ID:92512081002 Collected:12/15/20 15:30 Received:12/16/20 09:08 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15
Pace Analytical Services - Minneapolis
TO15 MSV AIR
Acetone ND ug/m3 12/31/20 00:22 67-64-177701286
Benzene 3920 ug/m3 12/31/20 00:22 71-43-24181286
Bromodichloromethane ND ug/m3 12/31/20 00:22 75-27-417501286
Bromoform ND ug/m3 12/31/20 00:22 75-25-267501286
Bromomethane ND ug/m3 12/31/20 00:22 74-83-910101286
1,3-Butadiene ND ug/m3 12/31/20 00:22 106-99-05791286
2-Butanone (MEK)ND ug/m3 12/31/20 00:22 78-93-338601286
Carbon disulfide ND ug/m3 12/31/20 00:22 75-15-08141286
Carbon tetrachloride ND ug/m3 12/31/20 00:22 56-23-516501286
Chlorobenzene ND ug/m3 12/31/20 00:22 108-90-712001286
Chloroethane ND ug/m3 12/31/20 00:22 75-00-36901286
Chloroform ND ug/m3 12/31/20 00:22 67-66-36381286
Chloromethane ND ug/m3 12/31/20 00:22 74-87-35401286
Cyclohexane 12100 ug/m3 12/31/20 00:22 110-82-722501286
Dibromochloromethane ND ug/m3 12/31/20 00:22 124-48-122301286
1,2-Dibromoethane (EDB)ND ug/m3 12/31/20 00:22 106-93-410001286
1,2-Dichlorobenzene ND ug/m3 12/31/20 00:22 95-50-115701286
1,3-Dichlorobenzene ND ug/m3 12/31/20 00:22 541-73-115701286
1,4-Dichlorobenzene ND ug/m3 12/31/20 00:22 106-46-739401286
Dichlorodifluoromethane ND ug/m3 12/31/20 00:22 75-71-813001286
1,1-Dichloroethane ND ug/m3 12/31/20 00:22 75-34-310601286
1,2-Dichloroethane ND ug/m3 12/31/20 00:22 107-06-210601286
1,1-Dichloroethene ND ug/m3 12/31/20 00:22 75-35-410401286
cis-1,2-Dichloroethene ND ug/m3 12/31/20 00:22 156-59-210401286
trans-1,2-Dichloroethene ND ug/m3 12/31/20 00:22 156-60-510401286
1,2-Dichloropropane ND ug/m3 12/31/20 00:22 78-87-512101286
cis-1,3-Dichloropropene ND ug/m3 12/31/20 00:22 10061-01-511901286
trans-1,3-Dichloropropene ND ug/m3 12/31/20 00:22 10061-02-611901286
Dichlorotetrafluoroethane ND ug/m3 12/31/20 00:22 76-14-218301286
Ethyl acetate ND ug/m3 12/31/20 00:22 141-78-69431286
Ethylbenzene 28400 ug/m3 12/31/20 00:22 100-41-411401286
4-Ethyltoluene 19000 ug/m3 12/31/20 00:22 622-96-832201286
n-Heptane 2640 ug/m3 12/31/20 00:22 142-82-510701286
Hexachloro-1,3-butadiene ND ug/m3 12/31/20 00:22 87-68-369701286
n-Hexane 3960 ug/m3 12/31/20 00:22 110-54-39211286
2-Hexanone ND ug/m3 12/31/20 00:22 591-78-653501286
Methylene Chloride ND ug/m3 12/31/20 00:22 75-09-245401286
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/31/20 00:22 108-10-153501286
Methyl-tert-butyl ether ND ug/m3 12/31/20 00:22 1634-04-447101286
Naphthalene 3750 ug/m3 12/31/20 00:22 91-20-334201286
Propylene ND ug/m3 12/31/20 00:22 115-07-14501286
Styrene ND ug/m3 12/31/20 00:22 100-42-511101286
1,1,2,2-Tetrachloroethane ND ug/m3 12/31/20 00:22 79-34-58981286
Tetrachloroethene ND ug/m3 12/31/20 00:22 127-18-48861286
Tetrahydrofuran ND ug/m3 12/31/20 00:22 109-99-97721286
Toluene 23200 ug/m3 12/31/20 00:22 108-88-39851286
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Page 6 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92512081
CPC 20104
Sample:AFVR - END Lab ID:92512081002 Collected:12/15/20 15:30 Received:12/16/20 09:08 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15
Pace Analytical Services - Minneapolis
TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/31/20 00:22 120-82-197001286
1,1,1-Trichloroethane ND ug/m3 12/31/20 00:22 71-55-614301286
1,1,2-Trichloroethane ND ug/m3 12/31/20 00:22 79-00-57141286
Trichloroethene ND ug/m3 12/31/20 00:22 79-01-67021286
Trichlorofluoromethane ND ug/m3 12/31/20 00:22 75-69-414701286
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/31/20 00:22 76-13-120101286
1,2,4-Trimethylbenzene 67500 ug/m3 12/31/20 00:22 95-63-612901286
1,3,5-Trimethylbenzene 22300 ug/m3 12/31/20 00:22 108-67-812901286
Vinyl acetate ND ug/m3 12/31/20 00:22 108-05-49211286
Vinyl chloride ND ug/m3 12/31/20 00:22 75-01-43341286
m&p-Xylene 83200 ug/m3 12/31/20 00:22 179601-23-122801286
o-Xylene 42900 ug/m3 12/31/20 00:22 95-47-611401286
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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[phone]
Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718310
TO-15
TO-15
TO15 MSV AIR Low Level
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92512081001, 92512081002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3832568
Associated Lab Samples:92512081001, 92512081002
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 12/30/20 08:44
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 12/30/20 08:44
1,1,2-Trichloroethane ug/m3 ND 0.56 12/30/20 08:44
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 12/30/20 08:44
1,1-Dichloroethane ug/m3 ND 0.82 12/30/20 08:44
1,1-Dichloroethene ug/m3 ND 0.81 12/30/20 08:44
1,2,4-Trichlorobenzene ug/m3 ND 7.5 12/30/20 08:44
1,2,4-Trimethylbenzene ug/m3 ND 1.0 12/30/20 08:44
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 12/30/20 08:44
1,2-Dichlorobenzene ug/m3 ND 1.2 12/30/20 08:44
1,2-Dichloroethane ug/m3 ND 0.82 MN12/30/20 08:44
1,2-Dichloropropane ug/m3 ND 0.94 12/30/20 08:44
1,3,5-Trimethylbenzene ug/m3 ND 1.0 12/30/20 08:44
1,3-Butadiene ug/m3 ND 0.45 12/30/20 08:44
1,3-Dichlorobenzene ug/m3 ND 1.2 12/30/20 08:44
1,4-Dichlorobenzene ug/m3 ND 3.1 12/30/20 08:44
2-Butanone (MEK)ug/m3 ND 3.0 12/30/20 08:44
2-Hexanone ug/m3 ND 4.2 12/30/20 08:44
4-Ethyltoluene ug/m3 ND 2.5 12/30/20 08:44
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 12/30/20 08:44
Acetone ug/m3 ND 6.0 12/30/20 08:44
Benzene ug/m3 ND 0.32 12/30/20 08:44
Bromodichloromethane ug/m3 ND 1.4 12/30/20 08:44
Bromoform ug/m3 ND 5.2 12/30/20 08:44
Bromomethane ug/m3 ND 0.79 12/30/20 08:44
Carbon disulfide ug/m3 ND 0.63 12/30/20 08:44
Carbon tetrachloride ug/m3 ND 1.3 12/30/20 08:44
Chlorobenzene ug/m3 ND 0.94 12/30/20 08:44
Chloroethane ug/m3 ND 0.54 12/30/20 08:44
Chloroform ug/m3 ND 0.50 12/30/20 08:44
Chloromethane ug/m3 ND 0.42 12/30/20 08:44
cis-1,2-Dichloroethene ug/m3 ND 0.81 12/30/20 08:44
cis-1,3-Dichloropropene ug/m3 ND 0.92 12/30/20 08:44
Cyclohexane ug/m3 ND 1.8 12/30/20 08:44
Dibromochloromethane ug/m3 ND 1.7 12/30/20 08:44
Dichlorodifluoromethane ug/m3 ND 1.0 12/30/20 08:44
Dichlorotetrafluoroethane ug/m3 ND 1.4 12/30/20 08:44
Ethyl acetate ug/m3 ND 0.73 12/30/20 08:44
Ethylbenzene ug/m3 ND 0.88 12/30/20 08:44
Hexachloro-1,3-butadiene ug/m3 ND 5.4 12/30/20 08:44
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Huntersville, NC 28078
[phone]
Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3832568
Associated Lab Samples:92512081001, 92512081002
Matrix:Air
Analyzed
m&p-Xylene ug/m3 ND 1.8 12/30/20 08:44
Methyl-tert-butyl ether ug/m3 ND 3.7 12/30/20 08:44
Methylene Chloride ug/m3 ND 3.5 12/30/20 08:44
n-Heptane ug/m3 ND 0.83 12/30/20 08:44
n-Hexane ug/m3 ND 0.72 12/30/20 08:44
Naphthalene ug/m3 ND 2.7 12/30/20 08:44
o-Xylene ug/m3 ND 0.88 12/30/20 08:44
Propylene ug/m3 ND 0.35 12/30/20 08:44
Styrene ug/m3 ND 0.87 12/30/20 08:44
Tetrachloroethene ug/m3 ND 0.69 12/30/20 08:44
Tetrahydrofuran ug/m3 ND 0.60 12/30/20 08:44
Toluene ug/m3 ND 0.77 12/30/20 08:44
trans-1,2-Dichloroethene ug/m3 ND 0.81 12/30/20 08:44
trans-1,3-Dichloropropene ug/m3 ND 0.92 12/30/20 08:44
Trichloroethene ug/m3 ND 0.55 12/30/20 08:44
Trichlorofluoromethane ug/m3 ND 1.1 12/30/20 08:44
Vinyl acetate ug/m3 ND 0.72 12/30/20 08:44
Vinyl chloride ug/m3 ND 0.26 12/30/20 08:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3832569LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 67.357 118 70-130
1,1,2,2-Tetrachloroethane ug/m3 94.3 CH71.9 131 70-132
1,1,2-Trichloroethane ug/m3 65.357.3 114 70-133
1,1,2-Trichlorotrifluoroethane ug/m3 84.480.3 105 70-130
1,1-Dichloroethane ug/m3 52.442.7 123 70-130
1,1-Dichloroethene ug/m3 42.341.4 102 69-137
1,2,4-Trichlorobenzene ug/m3 129156 83 70-130
1,2,4-Trimethylbenzene ug/m3 62.951.5 122 70-137
1,2-Dibromoethane (EDB)ug/m3 92.380.3 115 70-138
1,2-Dichlorobenzene ug/m3 76.863.1 122 70-136
1,2-Dichloroethane ug/m3 52.642.4 124 70-130
1,2-Dichloropropane ug/m3 57.848.6 119 70-132
1,3,5-Trimethylbenzene ug/m3 62.351.6 121 70-136
1,3-Butadiene ug/m3 25.823.3 111 67-139
1,3-Dichlorobenzene ug/m3 70.363.4 111 70-138
1,4-Dichlorobenzene ug/m3 66.563.4 105 70-145
2-Butanone (MEK)ug/m3 35.831.4 114 61-130
2-Hexanone ug/m3 53.842.8 126 70-138
4-Ethyltoluene ug/m3 65.352.4 125 70-142
4-Methyl-2-pentanone (MIBK)ug/m3 53.543.6 123 70-134
Acetone ug/m3 121126 96 59-137
Benzene ug/m3 39.533.5 118 70-133
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Huntersville, NC 28078
[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3832569LABORATORY CONTROL SAMPLE:
LCSSpike
Bromodichloromethane ug/m3 84.271.5 118 70-130
Bromoform ug/m3 120110 109 60-140
Bromomethane ug/m3 42.941.3 104 70-131
Carbon disulfide ug/m3 35.533.3 106 70-130
Carbon tetrachloride ug/m3 76.166.2 115 70-133
Chlorobenzene ug/m3 60.248.3 125 70-131
Chloroethane ug/m3 29.728.1 106 70-141
Chloroform ug/m3 64.251.1 126 70-130
Chloromethane ug/m3 23.121.9 105 64-137
cis-1,2-Dichloroethene ug/m3 49.341.6 118 70-132
cis-1,3-Dichloropropene ug/m3 57.447.7 120 70-138
Cyclohexane ug/m3 35.436.7 96 70-133
Dibromochloromethane ug/m3 11290.7 123 70-139
Dichlorodifluoromethane ug/m3 55.751.6 108 70-130
Dichlorotetrafluoroethane ug/m3 78.572.7 108 65-133
Ethyl acetate ug/m3 47.638.6 123 70-135
Ethylbenzene ug/m3 54.445.6 119 70-142
Hexachloro-1,3-butadiene ug/m3 106112 95 70-134
m&p-Xylene ug/m3 10991.2 120 70-141
Methyl-tert-butyl ether ug/m3 46.438.4 121 70-131
Methylene Chloride ug/m3 213182 117 69-130
n-Heptane ug/m3 43.043.6 98 70-130
n-Hexane ug/m3 34.637.6 92 70-131
Naphthalene ug/m3 45.657.7 79 63-130
o-Xylene ug/m3 55.545.5 122 70-135
Propylene ug/m3 18.418.2 101 63-139
Styrene ug/m3 58.6 CH44.9 130 70-143
Tetrachloroethene ug/m3 80.971 114 70-136
Tetrahydrofuran ug/m3 36.231.5 115 70-137
Toluene ug/m3 45.939.5 116 70-136
trans-1,2-Dichloroethene ug/m3 49.942.2 118 70-132
trans-1,3-Dichloropropene ug/m3 57.747.7 121 70-139
Trichloroethene ug/m3 63.556.3 113 70-132
Trichlorofluoromethane ug/m3 59.859.7 100 65-136
Vinyl acetate ug/m3 43.234.5 125 66-140
Vinyl chloride ug/m3 28.526.7 107 68-141
Parameter Units
Dup
Result QualifiersRPDResult
10542923001
3833815SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 ND<0.25
1,1,2,2-Tetrachloroethane ug/m3 ND<0.29
1,1,2-Trichloroethane ug/m3 ND<0.23
1,1,2-Trichlorotrifluoroethane ug/m3 ND<0.31
1,1-Dichloroethane ug/m3 ND<0.17
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Huntersville, NC 28078
[phone]
Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10542923001
3833815SAMPLE DUPLICATE:
1,1-Dichloroethene ug/m3 ND<0.17
1,2,4-Trichlorobenzene ug/m3 ND<5.2
1,2,4-Trimethylbenzene ug/m3 .5J0.41J
1,2-Dibromoethane (EDB)ug/m3 ND<0.31
1,2-Dichlorobenzene ug/m3 ND<0.97
1,2-Dichloroethane ug/m3 ND<0.18
1,2-Dichloropropane ug/m3 ND<0.24
1,3,5-Trimethylbenzene ug/m3 ND<0.27
1,3-Butadiene ug/m3 ND<0.15
1,3-Dichlorobenzene ug/m3 ND<1.1
1,4-Dichlorobenzene ug/m3 ND<1.3
2-Butanone (MEK)ug/m3 1.9J1.9J
2-Hexanone ug/m3 ND<1.1
4-Ethyltoluene ug/m3 ND<0.29
4-Methyl-2-pentanone (MIBK)ug/m3 ND<0.15
Acetone ug/m3 9.5 910.4
Benzene ug/m3 1.6 51.7
Bromodichloromethane ug/m3 ND<0.30
Bromoform ug/m3 ND<1.2
Bromomethane ug/m3 ND<0.24
Carbon disulfide ug/m3 ND<0.14
Carbon tetrachloride ug/m3 ND<0.29
Chlorobenzene ug/m3 ND<0.22
Chloroethane ug/m3 ND<0.18
Chloroform ug/m3 ND<0.20
Chloromethane ug/m3 ND<0.10
cis-1,2-Dichloroethene ug/m3 ND<0.19
cis-1,3-Dichloropropene ug/m3 ND<0.22
Cyclohexane ug/m3 .83J0.88J
Dibromochloromethane ug/m3 ND<0.44
Dichlorodifluoromethane ug/m3 3.1 63.2
Dichlorotetrafluoroethane ug/m3 ND<0.32
Ethyl acetate ug/m3 ND<0.16
Ethylbenzene ug/m3 .49J0.50J
Hexachloro-1,3-butadiene ug/m3 ND<2.6
m&p-Xylene ug/m3 1.8J1.9J
Methyl-tert-butyl ether ug/m3 ND<0.18
Methylene Chloride ug/m3 ND<1.6
n-Heptane ug/m3 ND1.1J
n-Hexane ug/m3 2.0 61.9
Naphthalene ug/m3 ND<2.5
o-Xylene ug/m3 .67J0.67J
Propylene ug/m3 ND<0.32
Styrene ug/m3 ND<0.36
Tetrachloroethene ug/m3 ND<0.34
Tetrahydrofuran ug/m3 ND<0.18
Toluene ug/m3 3.9 44.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Huntersville, NC 28078
[phone]
Page 11 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10542923001
3833815SAMPLE DUPLICATE:
trans-1,2-Dichloroethene ug/m3 ND<0.22
trans-1,3-Dichloropropene ug/m3 ND<0.89
Trichloroethene ug/m3 ND<0.28
Trichlorofluoromethane ug/m3 ND1.7
Vinyl acetate ug/m3 ND<0.15
Vinyl chloride ug/m3 ND<0.11
Parameter Units
Dup
Result QualifiersRPDResult
10543047001
3833816SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 .48JND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 2.5 22.5
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 .62JND
1,3-Butadiene ug/m3 ND25.7
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 27.6 127.9
2-Hexanone ug/m3 3.1JND
4-Ethyltoluene ug/m3 1.1JND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 82.9 385.3
Benzene ug/m3 5.5 05.5
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 3.0 13.0
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 NDND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 2.1JND
Dibromochloromethane ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Page 12 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92512081
CPC 20104
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10543047001
3833816SAMPLE DUPLICATE:
Dichlorodifluoromethane ug/m3 3.1 43.0
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 3.9 03.9
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 7.3 56.9
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 NDND
n-Heptane ug/m3 5.1 75.4
n-Hexane ug/m3 3.3 03.3
Naphthalene ug/m3 6.4 46.1
o-Xylene ug/m3 3.0 12.9
Propylene ug/m3 76.6 277.8
Styrene ug/m3 2.8 CH62.6
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 9.4 59.8
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.4JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
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Page 13 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92512081
CPC 20104
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92512081001
Analysis performed at 1800 Elm Street.[1]
Sample: 92512081002
Analysis performed at 1800 Elm Street.[1]
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
The reporting limit has been raised in accordance with Minnesota Statutes 4740.2100 Subpart 8. C, D. Reporting Limit
Evaluation Rule.MN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92512081
CPC 20104
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92512081001 718310AFVR - START TO-15
92512081002 718310AFVR - END TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2020 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 16
Page 16 of 16

APPENDIX C
TANK CONVERSION TABLE

APPENDIX D
WASTE MANIFEST