FA-29644_48868_CA_CLO_20230118

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone]
Eastcoastenv.com

January 18, 2023

Liz Price
Hydrogeologist / Wilmington Regional Office
Division of Waste Management, UST Section
North Carolina Department of Environmental Quality

Re: Underground Storage Tank Closure Report Prepared for
Commercial Underground Storage Tanks Closed at:
Stewart’s Tire & Auto, Inc.
2615 Murchison Road
Fayetteville, Cumberland County, NC

Dear Ms. Price,

This correspondence is to present one copy of ECE’s Underground Storage Tank Closure Report prepared
for the above referenced project site.

We appreciate the opportunity to be of service in the completion of this project. Should you have any
questions, comments, or require additional information, please feel free to contact me at your earliest
opportunity.

Cordially,
East Coast Environmental, P.A.

Thomas Will
President
East Coast Environmental, PA

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone]
Eastcoastenv.com

UNDERGROUND STORAGE TANK CLOSURE REPORT
PREPARED FOR UNDERGROUND STORAGE TANK SYSTEMS
REMOVED FROM:

STEWART’S TIRE AND AUTO, INC.
2615 MURCHISON ROAD
FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA
FACILITY ID # 00-00025012

January 17, 2022

Current Property Owner:
Mr. James Stewart
2615 Murchison Road
Fayetteville, NC 28301
[phone]

Consultant:
East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, North Carolina 27603
[phone]

UST Size and Contents: (3) 4,000-gallon gasoline, (1) 3,000-gallon Diesel UST systems
Latitude: N 35.09053 Longitude: W -78.91044

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
2
TABLE OF CONTENTS

A SITE IDENTIFICATION AND CONTACT INFORMATION .................................................................................................. 3
B SITE HISTORY AND CHARACTERIZATION .......................................................................................................................... 4
B.1 UST OWNER AND OPERATOR INFORMATION .................................................................................................................................. 4
B.2 UST INFORMATION ......................................................................................................................................................................... 4
B.3 NON-UST INFORMATION ................................................................................................................................................................ 4
B.4 HISTORICAL RELEASE DESCRIPTION ............................................................................................................................................... 4
B.5 SITE CHARACTERISTICS .................................................................................................................................................................. 5
C UST CLOSURE ............................................................................................................................................................................... 6
C.1 PREPARATIONS FOR UST CLOSURE ................................................................................................................................................ 6
C.2 UST RESIDUALS ............................................................................................................................................................................. 6
C.3 CLOSURE PROCEDURES .................................................................................................................................................................. 6
C.4 FIELD SCREENING PROCEDURES AND OBSERVATIONS .................................................................................................................... 7
C.5 SOIL SAMPLING .............................................................................................................................................................................. 7
C.6 GROUNDWATER SAMPLING ............................................................................................................................................................ 7
C.7 QUALITY CONTROL MEASURES ...................................................................................................................................................... 7
C.8 GROUNDWATER SAMPLING ............................................................................................................................................................ 8
D CONCLUSIONS .............................................................................................................................................................................. 8
E LIMITATIONS ................................................................................................................................................................................ 9

Appendix I Figures

Figure 1 Topographic Site Location Map
Figure 2 Site Map with UST System Locations
Figure 3 Site Map with UST System Closure Soil Sample Locations

Appendix II Tables

Table 1 UST Owner and Operator Information
Table 2 Analytical Data – Soil

Appendix III UST-3 (Notice of Intent)
UST-2A (Site Investigation Report)
UST Disposal Certificate
City of Fayetteville Fire Marshall Permit Fee Receipt

Appendix IV

Laboratory Report

ENCO Laboratories

NC-DEQ Approval to Abandon UST in Place
Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
3

Underground Storage Tank Closure Report

A SITE IDENTIFICATION AND CONTACT INFORMATION

A.1 Site Identification
Date of Report: January 17, 2023
Facility I.D.: 00-000025012
Site Name: Stewart’s Tire & Auto, Inc.
Site Address: 2615 Murchison Road
Nearest City/Town: Fayetteville County: Cumberland
Latitude: N 35.09053 Longitude: W -78.91044

A.2 Contact Information

UST Owner/Operator: Stewart’s Tire & Auto, Inc.
Address: 2615 Murchison Road, Fayetteville, NC 28301 Phone: [phone]

Property Owner: James Stewart
Address: 420 Lakeside Lane, Sanford, NC 27332 Phone: [phone]

Property Occupants: Stewart’s Tire & Auto, Inc.
Address: 2615 Murchison Road, Fayetteville, NC 28301 Phone: [phone]

Consultant/Contractor: East Coast Environmental, P.A.
Address: 3815 Junction Blvd., Raleigh, NC 27603 Phone: [phone]

Analytical Laboratory: Environmental Conservation Laboratories
Address: 102-A Woodwinds Industrial Court, Cary, NC 27511 Phone: [phone]

I, Thomas R. Will a Licensed Geologist for East Coast Environmental, P.A. do certify that the information contained in this
report is correct and accurate to the best of my knowledge.
East Coast Environmental, P.A. is licensed to practice geology in North Carolina. The certification number for East Coast Environmental, P.A. is C-
136

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
4

B SITE HISTORY AND CHARACTERIZATION

B.1 UST Owner and Operator Information

General information regarding Underground Storage Tank (UST) history and ownership is displayed in Table 1
in Appendix II.

B.2 UST Information

The subject USTs were constructed of single walled steel that later were lined with fiberglass and are registered
with the North Carolina Department of Environmental Quality (NC-DEQ) UST Section. The NC-DEQ UST
database reports that the diesel UST was installed during May 1982 while the three 4,000-gallon gasoline USTs
were added during May 1984. Product piping associated with the UST systems was single walled steel. See
Appendix I, Figure 2 for Site map indicating former UST system locations. Three of the four USTs were closed
by removal while the fourth UST (T-8 in Figure 2) had to be closed in-place by filling with concrete because it
was located too close to the Stewarts Tire Store, Inc. building to safely remove without undermining the building
foundation. Associated product lines were partially removed as well as part of the closure activities. There are
no longer any operational petroleum UST systems located on the Site.

General information for the USTs removed from the Stewart’s Tire & Auto, Inc. (hereinafter referred to as the
“Site”) is based on historical information obtained from the NC-DEQ Registered UST Database, observation
made while the UST systems were being removed and from Site representatives. This information is displayed
in Table 1 in Appendix II.

B.3 Non-UST Information

There were no petroleum Aboveground Storage Tanks (ASTs) noted on the Site during the UST removal
activities.

B.4 Historical Release Description

The Site once contained a 2,000-gallon kerosene UST system which released kerosene under the associated
product dispenser at some time in the past. The kerosene UST system was removed along with 7.5-tons of
petroleum contaminated soil during February 2006. See Figure 2 for former kerosene UST system location. The
NC-DEQ assigned the release incident number 29284. Finally, incident 29824 was closed out by the NC-DEQ
through issuance of a letter of no further action dated December 6, 2006.

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
5
B.5 Site Characteristics

The Site is currently occupied by the Stewart’s Tire & Auto, Inc. (Figures 1 and 2). The immediately surrounding
properties are currently being used primarily for commercial and residential purposes. The Site reportedly did
contain four petroleum UST systems prior to the ones that are the subject of this closure report but no new UST
systems are planned for installation on the Site. The NC-DEQ database reports that the subject UST systems
were installed during 1982 and 1984 and there is no record of a previous petroleum release incident associated
with the subject USTs. See Table I for historical summary of all known USTs.

The Site has an approximate elevation of 190-feet above mean sea level (MSL) and the Site and surrounding area
is gently flat with a very mild slope to the west. Locally, groundwater is expected to flow to the west as well. No
subsurface utilities were observed in the excavation while removing the UST systems.

The Geologic Map of North Carolina1 locates the Site as being underlain by the Middendorf Formation of the
Coastal Plain Physiographic Province. Further, the Geologic Map describes the Middendorf Formation as “Sand,
sandstone and mudstone gray to pale gray with an orange cast, mottled; clay balls and iron cemented concretions
common, beds laterally discontinuous, cross bedding common”.

Observations made by ECE during removal of the USTs revealed that this location is underlain by yellow-orange
mottled clayey silt to approximately twelve feet below land surface. Neither groundwater nor rock was observed
at the bottom of the excavation.

The Site and all surrounding properties utilize potable water supplied by the City of Fayetteville as their water
supply. No water supply wells were noted to be located within a 1,000-foot radius of the former UST area.

1 Reference Geologic Map of North Carolina, Department of Natural Resources and Community Development, Division of Land Resources, 1985
edition.
Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
6
C UST CLOSURE

C.1 Preparations for UST Closure

A UST-3 (Notice of Intent) form was prepared and submitted to the NC-DEQ Fayetteville Regional Office and
NC-DEQ Central Office before removal of the subject UST systems. The City of Fayetteville Fire Marshal’s
Office was also contacted in order to obtain a permit for the removal of the USTs. See Appendix III for UST-3,
UST-2a and City of Fayetteville Fire Marshal UST removal permit fee receipt.

C.2 UST Residuals

None of the three 4,000-gallon gasoline USTs contained residual liquids. The 3,000-gallon diesel fuel UST
contained approximately six inches of water that was removed and disposed of by Creekside Land Development
prior to beginning closure activities.

C.3 Closure Procedures

The UST closure activities were performed by Creekside Land Development during December 14-16, 2022
utilizing an excavator. The subject tanks were noted to be single walled steel which had been upgraded at some
time in the past with the installation of internal fiberglass coatings. The associated product lines were constructed
of single walled galvanized steel. See Figure 2 for former UST system locations.

The excavation made to remove the tanks measured as much as 40-feet in length by 22-feet in width and was up
to 12-feet in depth. Observations made by ECE during removal of the USTs revealed that this location is underlain
by yellow-orange mottled clayey silt. Neither groundwater nor rock was observed at the bottom of the excavation.
Finally, no obvious signs of a petroleum release to the soils under and around the tanks was noted during the UST
closure excavation.

As sated previously, three of the four USTs were closed by removal while the fourth UST (T-8 in Figure 2) had
to be closed in-place by filling with concrete because it was located too close to the Stewarts Tire Store building
to safely remove without undermining the building foundation. Associated product lines were partially removed
as well as part of the closure activities. There are no longer any operational petroleum UST systems located on
the Site.

A UST-3 was submitted to the NC-DEQ Central Office and NC-DEQ Fayetteville Regional Office prior to
beginning UST closure activities. A UST-2a (Site Investigation Report) has also been submitted to the NC-DEQ
Central Office and NC-DEQ Wilmington Regional Office and included as part of this UST Closure Report. See
Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
7
Appendix III for a copy of the UST-3 and UST-2a forms. A UST disposal certificate is also included in
Appendix III.

C.4 Field Screening Procedures and Observations

Field screening of soils consisted of their visual and olfactory profiling after the UST systems were removed from
the ground. No petroleum odors or staining were noted in the soils under and surrounding the any of the USTs
after their removal. Further, no petroleum odors or staining were noted in soil samples collected from under the
former product dispenser locations or from under the product lines collected as part of the UST closure activities.

C.5 Soil Sampling

At the conclusion of UST removal activities, ECE collected a series of eleven excavation bottom samples from
the bottom limits of the UST excavations utilizing a hand auger as shown in Figure 2. Nine additional soil
samples were also collected from under the product lines and dispensers for completion of the UST closure
activities also utilizing a hand auger. See Figure 3 in Appendix I for soil closure sample locations.

Soil samples collected for closure of the UST systems were submitted to ENCO Laboratories of Cary, NC for
analysis by EPA method 8015 for Gasoline Range Organics (GRO) and Diesel Range Organics (DRO). Closure
samples were collected in order to comply with the North Carolina Department of Environmental Quality (NC-
DEQ) “Guidelines for Site Checks, Tank Closure and Initial Response and Abatement for UST Releases March
1, 2007 Version, Change 11 2021” Hereinafter referred to as “The Guidelines”.

The results for the soil closure samples collected from under the diesel and gasoline USTs and associated product
lines were all below the action levels of 50-mg/kg and 100-mg/kg for GRO and DRO.

C.6 Groundwater Sampling

No groundwater was encountered while completing the UST excavation therefore no groundwater samples were
collected for completion of these UST closure activities.

C.7 Quality Control Measures

The soil samples collected for laboratory analysis were handled only with clean nitrile gloves and placed in the
appropriate laboratory supplied bottles for transportation on ice to ENCO Laboratories or Cary, NC for testing by
EPA Method 8015 for GRO and DRO.
Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
8

Specific information related to the samples collected, including date and time of collection, is found on the Chain
of Custody forms at the back of the laboratory analytical report in Appendix IV.

All nitrile gloves used by ECE personnel during petroleum contaminated soil removal activities were properly
discarded, along with any other potentially contaminated articles, immediately after their use.

ECE followed standard EPA and NC-DEQ protocols and guidelines for collecting soil samples. It is ECE's belief
that the laboratory analytical results provided in this report should not have been adversely affected by our
sampling, handling and shipment procedures.

Summary of Soil Analytical Results

Analytical results for all soil samples collected for completion of these UST closure activities showed either
GRO or DRO at concentrations in excess of their action levels of 50 mg/kg and 100-mg/kg, respectively as set
forth in the Guidelines. The sample locations for these soil samples can be found in Figure 3. A summary of
the analytical data can be found in Table 2 located in Appendix II.

C.8 Groundwater Sampling

No groundwater samples were collected as part of these closure activities as no groundwater was observed
entering the excavation.

D CONCLUSIONS

ECE has reviewed the information obtained after the removal of three gasoline and one diesel fuel UST systems
from the subject locations. Based on ECE's Site observations and the laboratory results for twenty-two soil
samples collected for completion of the UST closure activities, it can be concluded that no release of either
gasoline or diesel fuel was noted or detected during these closure activities at concentrations in excess of their
action levels as set forth in the Guidelines.

A copy of this Underground Storage Tank Closure Report should be forwarded to the NC-DEQ Wilmington
Regional Office to the attention of Liz Price for review.

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
9

E LIMITATIONS

This report has been prepared for the exclusive use of Stewarts Tire and Auto, Inc, their successors, assigns or
designees. This study was conducted in accordance with generally accepted environmental practices. No other
warranty, expressed or implied, is made. ECE's conclusions and recommendations are based on information
supplied by others, together with ECE's own site observations. Although ECE cannot be responsible for the
accuracy of data supplied by others, ECE has no reason to suspect that any of the information is inaccurate. The
observations described herein are based upon conditions readily visible at the site at the time of ECE's visit, in
addition to information provided by the Client.

ECE, by virtue of providing the services indicated in this report, does not assume responsibility for the person(s)
in charge of the site, nor is ECE responsible for reporting to any local, state or federal public agencies any
conditions at the Site that may present a potential danger to public health, safety or the environment. It is the
responsibility of the owner to notify the appropriate local, state or federal public agencies as required by law, or
otherwise to disclose, in a timely manner, any information that may be necessary to prevent any danger to public
health, safety or the environment.

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
10

Appendix I

Figures

East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 1
Site Location Map

Stewart's Tire & Auto
2615 Murchison Road
Fayetteville, Cumberland County, NC
Scale:Prep. By:Rev. By:Date:
NTS TRW TRW 12/10/2022
N
Site Location
Source: USGS Fayetteville NC Quandrangle 2022
East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 2
Site Map With Former UST
System Locations
Stewart's Tire & Auto
2615 Murchison Road
Fayetteville, Cumberland County, NC
Scale:Prep. By:Rev. By:Date:
1” = 20'TRW TRW 1/6/2023
N
T-
6
(
D
i
e
s
el)T-7 (G asolin e)Pelt D riveMu
r
c
hi
s
o
n
Roa
d
T-5 (G asoline) 2,000 gallon Kerosene UST
System (Removed 2/2006)
NC-DEQ Incident # 29284
Gasoline
Product
Dispensers
UST System Excavation and Removal will be Completed Using a Doosan Model 255 Excavator T-8 (G asoline)Product Line
Diesel Product
Dispenser
East Coast
Environmental, P.A.
3815 Junction Boulevard
Raleigh, North Carolina 27603
[phone]
Figure 3
Site Map UST System and
Excavation Locations
Stewart's Tire & Auto
2615 Murchison Road
Fayetteville,Cumberland County, NC
Scale:Prep. By:Rev. By:Date:
1” = 10'TRW TRW 12/21/2022
N
T
-
6 (Die
s
el)T-5 (G asoline)T-1 S-1 T-7 (G asoline) T-8 (G asoline)
Estimated Extent of UST ExcavationT-3 S-3
T-1 S-2
T-2 S-1
P-1
T-2 S-3
P-2
T-3 S-2
T-3 S-1
T-4 S-1
T-4 S-2
T-2 S-2
T-4 S-3
L-1
- Indicates Closure Soil Sample Location
L-3
L-4
P-1
L-2
P-3
P-4
Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
11

Appendix II

Tables

Table 1
Site History – UST Owner and Operator Information
Stewart’s Tire & Auto
2615 Murchison Road Fayetteville, NC

Facility ID Number

Name of Registered Owner /Operator Dates of Ownership
(mm/dd/yy to mm/dd/yy)

0-000025012
Stewart’s Tire & Auto
2615 Murchison Road
Henderson, North Carolina 27536
[phone]

12/1993 – 4/2022
Name of Property Owner

Dates of Operation
(mm/dd/yy to mm/dd/yy)

12/1993 – 4/2022
Street Address
2615 Murchison Road
City State Zip Telephone Number
Fayetteville NC 28301 [phone]

Table 1 (continued)
Stewart’s Tire & Auto
2615 Murchison Road Fayetteville, NC
UST
ID #
Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Descriptions
of Associated
Piping
Date Tank
Installed
Status of
UST
Was release
associated
with UST
T-1 Gasoline Gasoline 1,000

Single Walled
Steel
Unknown Unknown 11/1973 Removed
12//1986
Unknown
T-2 Heating
Oil
Heating Oil 280 Single Walled
Steel
Unknown Unknown 11/1967 Removed Unknown
T-3

Heating
Oil
Heating Oil 550 Single Walled
Steel
Unknown Unknown 11/1967 Removed Unknown
T-4 Kerosene Kerosene 2,000 Single Walled
Steel
5’ x 12’ Unknown 11/1984 Removed
1/25/2006
Yes
*T-5 Gasoline Gasoline 4,000

Single Walled
Fiberglass
Coated Steel
5’ x 24’ Single Walled
Steel
5/1982 Removed
12/15/22
No
*T-6 Diesel Diesel 3,000 Single Walled
Fiberglass
Coated Steel
5’ x 18’ Single Walled
Steel
5/1982 Removed
12/15/22
No
*T-7

Gasoline Gasoline 4,000

Single Walled
Fiberglass
Coated Steel
5’ x 24’ Single Walled
Steel
5/1984 Removed
12/15/22
No
*T-8 Gasoline Gasoline 4,000

Single Walled
Fiberglass
Coated Steel

5’ x 24’
Single Walled
Steel
5/1984 Closed in
Placed
12/16/22
No

* USTs 5, 6, 7, 8 are the subject of this UST Closure Report

Table 1 (continued)
Previous Site Petroleum Release(s)
Stewart’s Tire & Auto
2615 Murchison Road Fayetteville, NC
Incident
Number
Material
Released
Date of
Release Description of Release
29284 Kerosene 2/2006 The Site once contained a 2,000-gallon kerosene UST system which released kerosene under the
associated product dispenser at some time in the past. The kerosene UST system was removed along
with 7.5-tons of petroleum contaminated soil were removed during February 2006. The NC-DEQ
assigned the incident number 29284. Finally, incident 29824 was closed out by the NC-DEQ through
issuance of a letter of no further action dated December 6, 2006.

Table 2
Summary of Analytical Data – Soil
EPA Method 8015 (GRO/DRO)
Stewart’s Tire & Auto
2615 Murchison Road Fayetteville, NC
Analytical Method >

EPA 8015 w/5030 EPA 8015 w/3550
Sample
ID
Contaminant of Concern > Low Boiling Point TPH (GRO) High Boiling Point TPH (DRO) Date Collected
(m/dd/yy)
Sample
Depth (ft)
T-1 S-1 (Diesel UST #6) 12/13/2022 11’ 12 11
T-1 S-2 (Diesel UST #6) 12/13/2022 11’ 10 ND
P-1 (Diesel Pump) 12/13/2022 3’ ND ND
T-2 S-1 (Gas UST #5) 12/14/2022 11’ ND ND
T-2 S-2 (Gas UST #5) 12/14/2022 11’ ND NT
T-2 S-3 (Gas UST #5) 12/14/2022 11’ ND NT
T-3 S-1 (Gas UST #7) 12/14/2022 11’ ND NT
T-3 S-2 (Gas UST #7) 12/14/2022 11’ ND NT
T-4 S-1 (Gas UST #8) 12/14/2022 11’ ND NT
T-4 S-2 (Gas UST #8) 12/14/2022 11’ ND NT
T-4 S-3 (Gas UST #8) 12/14/2022 11’ ND NT
P-2 (Gas Pump) 12/14/2022 3’ ND NT
P-3 (Gas Pump) 12/14/2022 3’ ND NT
P-4 (Gas Pump) 12/14/2022 3’ ND NT
P-5 (Gas Pump) 12/14/2022 3’ ND NT
Stockpile 12/14/2022 - ND 17
T-3 S-3 (Gas UST#7) 12/14/2022 11’ ND NT
L-1 (Gas Line) 12/16/2022 3’ 8.7 NT
L-2 (Gas Line) 12/16/2022 3’ ND NT
L-3 (Gas Line) 12/16/2022 3’ ND NT
L-4 (Gas Line) 12/16/2022 3’ ND NT
NC-DEQ Action Level 50 100

Results are in mg/kg
ND - Not Detected
NT – Not Tested

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
12

Appendix III

UST-3 (Notice of Intent)

UST-2A (Site Investigation Report)

UST Disposal Certificate

City of Fayetteville Fire Marshall Permit Fee
Receipt

NC-DEQ Approval to Complete In-Place UST
Closure

1/4/23, 3:08 PM Shopping Cart
https://fayetteville.idtplans.com/secure/orders/cart/?step=invoice&orderid=108687&history=now&printable=yes 1/1
Order Grand Total
$500.00

Plan Review Fees
Project review
no.
Description Fee Qty Total
2615 Murchison Road
UST Removal
2 105.7.8 Flammable and Combustible Liquids:
Install and remove AST/UST
$500.00 1 $500.00
Sub-Total:$500.00
Please remit payment to:
433 Hay Street
Fayetteville, NC 28301
Checks should be made out to:
"City of Fayetteville" and include the project number
and what payment is for.
RECEIPT
Bill To
Company East Coast Environmental
Contact Tom Will
Address 3815 Junction Boulevard
Raleigh, NC 27603
Phone [phone]
Email [e-mail]
Order Details
Order ID 108687
Project No.907997
Reference No.002822
Paid On 12/7/22 11:49 AM
Paid By Visa **** **** **** 5623
Transaction ID 017094

Approval for In-Place Closure of an Underground Storage Tank

Date: December 21, 2022

Subject:
Site Name (if any): Stewarts Tire & Auto
Address (Street, City, Zip Code): 2615 Murchison Road, Fayetteville 28301

Facility Number (if applicable): 00‐0‐0000025012

I, Liz Price, approved an in-place closure of the tank identified as Tank “M” on the attached site diagram,
located at the subject site. The last known contents of Tank “M” was Gasoline

(Signature)
Hydrogeologist
(Position)
Wilmington Regional Office
UST Section, Division of Waste Management, NCDEQ

Underground Storage Tank Closure Report
Stewart’s Tire & Auto, Inc. 2615 Murchison Road, Fayetteville Cumberland County, North Carolina

East Coast Environmental, P.A.
3815 Junction Blvd.
Raleigh, N.C. 27603
13

Appendix IV

Laboratory Reports

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:[TOC_1]ENCO Laboratories, Inc.[TOC]
ENCO Workorder(s): CF14992
Raleigh, NC 27603
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Stewarts
Attn: Tom Will
East Coast Environmental (EA030)
3815 Junction Blvd.
Bill Scott
Project Manager
Friday, January 6, 2023
RE: Laboratory Results for
Dear Tom Will,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, December 15, 2022.
Enclosure(s)
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 1 of 11Page 1 of 12
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SAMPLE SUMMARY/LABORATORY CHRONICLE [TOC_1]Sample Chronical[TOC]
T-1 S-1 CF14992-01 Sampled:12/13/22 13:50 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/27/22 12/16/22 04:56 12/16/22 10:24EPA 5035
T-1 S-2 CF14992-02 Sampled:12/13/22 13:55 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/27/22 12/16/22 04:56 12/16/22 10:59EPA 5035
P-1 CF14992-03 Sampled:12/13/22 15:00 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/27/22 12/16/22 04:56 12/16/22 11:45EPA 5035
T-2 S-1 CF14992-04 Sampled:12/14/22 10:05 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 12:20EPA 5035
T-2 S-2 CF14992-05 Sampled:12/14/22 10:07 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 13:02EPA 5035
T-2 S-3 CF14992-06 Sampled:12/14/22 10:10 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 13:37EPA 5035
T-3 S-1 CF14992-07 Sampled:12/14/22 14:10 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 14:11EPA 5035
T-3 S-2 CF14992-08 Sampled:12/14/22 14:15 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 14:45EPA 5035
T-4 S-1 CF14992-09 Sampled:12/14/22 16:20 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 15:54EPA 5035
T-4 S-2 CF14992-10 Sampled:12/14/22 16:25 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 16:28EPA 5035
T-4 S-3 CF14992-11 Sampled:12/14/22 16:30 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 17:02EPA 5035
P-2 CF14992-12 Sampled:12/14/22 11:20 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 17:36EPA 5035
P-3 CF14992-13 Sampled:12/14/22 11:30 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 18:11EPA 5035
P-4 CF14992-14 Sampled:12/14/22 11:40 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 18:45EPA 5035
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 2 of 11Page 2 of 12
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SAMPLE SUMMARY/LABORATORY CHRONICLE
P-5 CF14992-15 Sampled:12/14/22 11:50 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 19:19EPA 5035
Stockpile CF14992-16 Sampled:12/14/22 11:30 Received:12/15/22 07:42Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/16/22 04:56 12/16/22 19:53EPA 5035
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 3 of 11Page 3 of 12
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SAMPLE DETECTION SUMMARY [TOC_1]Detection Summary[TOC]
Lab ID:Client ID:T-1 S-1 CF14992-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
12 7.2 mg/kg dry EPA 8015C GRO (C6-C10)2.6
Lab ID:Client ID:T-1 S-2 CF14992-02
Analyte MethodUnitsPQLResultsFlag NotesMDL
10 5.6 mg/kg dry EPA 8015C GRO (C6-C10)2.0
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 4 of 11Page 4 of 12
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ANALYTICAL RESULTS
[TOC_1]Analytical Results[TOC]
T-1 S-1Description:Lab Sample ID:CF14992-01 12/15/22 07:42Received:
CF14992Work Order:12/13/22 13:50Sampled:SoilMatrix:
76.40% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-1 S-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 10:24GRO (C6-C10)^2.6 OWS2L160017.212 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168108 %OWSEPA 8015C 12/16/22 10:242L160011312.2 1
T-1 S-2Description:Lab Sample ID:CF14992-02 12/15/22 07:42Received:
CF14992Work Order:12/13/22 13:55Sampled:SoilMatrix:
86.00% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-1 S-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 10:59GRO (C6-C10)^2.0 OWS2L160015.610 0.88
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168120 %OWSEPA 8015C 12/16/22 10:592L160011210.2 0.88
P-1Description:Lab Sample ID:CF14992-03 12/15/22 07:42Received:
CF14992Work Order:12/13/22 15:00Sampled:SoilMatrix:
69.30% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]P-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 11:45GRO (C6-C10)^2.5 OWS2L160017.0ND 0.882
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168121 %OWSEPA 8015C 12/16/22 11:452L160011512.7 0.882
T-2 S-1Description:Lab Sample ID:CF14992-04 12/15/22 07:42Received:
CF14992Work Order:12/14/22 10:05Sampled:SoilMatrix:
81.00% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-2 S-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 12:20GRO (C6-C10)^2.2 OWS2L160016.1ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168115 %OWSEPA 8015C 12/16/22 12:202L160011311.1 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 5 of 11Page 5 of 12
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ANALYTICAL RESULTS
T-2 S-2Description:Lab Sample ID:CF14992-05 12/15/22 07:42Received:
CF14992Work Order:12/14/22 10:07Sampled:SoilMatrix:
84.30% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-2 S-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 13:02GRO (C6-C10)^2.1 OWS2L160015.8ND 0.882
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168117 %OWSEPA 8015C 12/16/22 13:022L160011210.5 0.882
T-2 S-3Description:Lab Sample ID:CF14992-06 12/15/22 07:42Received:
CF14992Work Order:12/14/22 10:10Sampled:SoilMatrix:
79.50% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-2 S-3[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 13:37GRO (C6-C10)^2.3 OWS2L160016.2ND 0.896
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168120 %OWSEPA 8015C 12/16/22 13:372L160011411.3 0.896
T-3 S-1Description:Lab Sample ID:CF14992-07 12/15/22 07:42Received:
CF14992Work Order:12/14/22 14:10Sampled:SoilMatrix:
77.10% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-3 S-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 14:11GRO (C6-C10)^2.1 OWS2L160015.6ND 0.791
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168118 %OWSEPA 8015C 12/16/22 14:112L160011210.3 0.791
T-3 S-2Description:Lab Sample ID:CF14992-08 12/15/22 07:42Received:
CF14992Work Order:12/14/22 14:15Sampled:SoilMatrix:
77.60% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-3 S-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 14:45GRO (C6-C10)^2.1 OWS2L160015.8ND 0.814
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168109 %OWSEPA 8015C 12/16/22 14:452L160011110.5 0.814
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 6 of 11Page 6 of 12
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ANALYTICAL RESULTS
T-4 S-1Description:Lab Sample ID:CF14992-09 12/15/22 07:42Received:
CF14992Work Order:12/14/22 16:20Sampled:SoilMatrix:
76.90% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-4 S-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 15:54GRO (C6-C10)^2.6 OWS2L160017.2ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168110 %OWSEPA 8015C 12/16/22 15:542L160011312.0 1
T-4 S-2Description:Lab Sample ID:CF14992-10 12/15/22 07:42Received:
CF14992Work Order:12/14/22 16:25Sampled:SoilMatrix:
84.70% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-4 S-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 16:28GRO (C6-C10)^1.8 OWS2L160015.0ND 0.768
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168108 %OWSEPA 8015C 12/16/22 16:282L160019.8 9.07 0.768
T-4 S-3Description:Lab Sample ID:CF14992-11 12/15/22 07:42Received:
CF14992Work Order:12/14/22 16:30Sampled:SoilMatrix:
75.50% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-4 S-3[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 17:02GRO (C6-C10)^2.4 OWS2L160016.6ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168115 %OWSEPA 8015C 12/16/22 17:022L160011412.0 1
P-2Description:Lab Sample ID:CF14992-12 12/15/22 07:42Received:
CF14992Work Order:12/14/22 11:20Sampled:SoilMatrix:
86.50% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]P-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 17:36GRO (C6-C10)^1.7 OWS2L160014.6ND 0.729
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168104 %OWSEPA 8015C 12/16/22 17:362L160018.8 8.43 0.729
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 7 of 11Page 7 of 12
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ANALYTICAL RESULTS
P-3Description:Lab Sample ID:CF14992-13 12/15/22 07:42Received:
CF14992Work Order:12/14/22 11:30Sampled:SoilMatrix:
81.80% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]P-3[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 18:11GRO (C6-C10)^2.1 OWS2L160015.9ND 0.873
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168113 %OWSEPA 8015C 12/16/22 18:112L160011210.7 0.873
P-4Description:Lab Sample ID:CF14992-14 12/15/22 07:42Received:
CF14992Work Order:12/14/22 11:40Sampled:SoilMatrix:
85.70% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]P-4[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 18:45GRO (C6-C10)^1.6 OWS2L160014.4ND 0.691
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168103 %OWSEPA 8015C 12/16/22 18:452L160018.3 8.06 0.691
P-5Description:Lab Sample ID:CF14992-15 12/15/22 07:42Received:
CF14992Work Order:12/14/22 11:50Sampled:SoilMatrix:
85.70% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]P-5[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 19:19GRO (C6-C10)^1.7 OWS2L160014.6ND 0.723
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168108 %OWSEPA 8015C 12/16/22 19:192L160019.1 8.43 0.723
StockpileDescription:Lab Sample ID:CF14992-16 12/15/22 07:42Received:
CF14992Work Order:12/14/22 11:30Sampled:SoilMatrix:
17.00% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]Stockpile[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/16/22 19:53GRO (C6-C10)^10 OWS2L1600129ND 0.887
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168109 %OWSEPA 8015C 12/16/22 19:532L160015752.1 0.887
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 8 of 11Page 8 of 12
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QUALITY CONTROL DATA [TOC_1]QC Data[TOC]
Gasoline Range Organics by GC - Quality Control
Batch 2L16001 - EPA 5035
Prepared: 12/16/2022 04:56 Analyzed: 12/16/2022 07:16Blank (2L16001-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.52.0 U GRO (C6-C10)
mg/kg wet 9.69 59-1682,5-Dibromotoluene 11111
Prepared: 12/16/2022 04:56 Analyzed: 12/16/2022 06:35LCS (2L16001-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 47.7 51-12011454 GRO (C6-C10)
mg/kg wet 9.54 59-1682,5-Dibromotoluene 10810
Prepared: 12/16/2022 04:56 Analyzed: 12/16/2022 07:50Matrix Spike (2L16001-MS1)
Source: CF18832-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 49.1 45-1621212.0 U59 GRO (C6-C10)
mg/kg wet 9.82 59-1682,5-Dibromotoluene 11711
Prepared: 12/16/2022 04:56 Analyzed: 12/16/2022 08:24Matrix Spike Dup (2L16001-MSD1)
Source: CF18832-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 48.7 2445-162117 42.0 U57 GRO (C6-C10)
mg/kg wet 9.75 59-1682,5-Dibromotoluene 11311
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 9 of 11Page 9 of 12
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FLAGS/NOTES AND DEFINITIONS [TOC_1]Flags/Notes[TOC]
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.PQL
Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.[CALC]
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 10 of 11Page 10 of 12
Page 11 of 12
Page 12 of 12
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:[TOC_1]ENCO Laboratories, Inc.[TOC]
ENCO Workorder(s): CF19176
Raleigh, NC 27603
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Stewarts
Attn: Tom Will
East Coast Environmental (EA030)
3815 Junction Blvd.
Bill Scott
Project Manager
Friday, January 6, 2023
RE: Laboratory Results for
Dear Tom Will,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Saturday, December 17, 2022.
Enclosure(s)
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 1 of 8Page 1 of 8
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SAMPLE SUMMARY/LABORATORY CHRONICLE [TOC_1]Sample Chronical[TOC]
T-3 S-3 CF19176-01 Sampled:12/14/22 14:25 Received:12/17/22 08:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/28/22 12/20/22 05:49 12/20/22 10:51EPA 5035
L-1 CF19176-02 Sampled:12/16/22 13:30 Received:12/17/22 08:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/30/22 12/20/22 05:49 12/20/22 11:25EPA 5035
L-2 CF19176-03 Sampled:12/16/22 13:40 Received:12/17/22 08:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/30/22 12/20/22 05:49 12/20/22 11:59EPA 5035
L-3 CF19176-04 Sampled:12/16/22 13:50 Received:12/17/22 08:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/30/22 12/20/22 05:49 12/20/22 12:33EPA 5035
L-4 CF19176-05 Sampled:12/16/22 14:00 Received:12/17/22 08:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 8015C 12/30/22 12/20/22 05:49 12/20/22 13:08EPA 5035
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 2 of 8Page 2 of 8
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SAMPLE DETECTION SUMMARY [TOC_1]Detection Summary[TOC]
Lab ID:Client ID:L-1 CF19176-02
Analyte MethodUnitsPQLResultsFlag NotesMDL
8.7 5.6 mg/kg dry EPA 8015C GRO (C6-C10)2.0
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 3 of 8Page 3 of 8
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ANALYTICAL RESULTS
[TOC_1]Analytical Results[TOC]
T-3 S-3Description:Lab Sample ID:CF19176-01 12/17/22 08:55Received:
CF19176Work Order:12/14/22 14:25Sampled:SoilMatrix:
85.00% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]T-3 S-3[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/20/22 10:51GRO (C6-C10)^2.4 OWS2L200026.5ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168100 %OWSEPA 8015C 12/20/22 10:512L200021110.9 1
L-1Description:Lab Sample ID:CF19176-02 12/17/22 08:55Received:
CF19176Work Order:12/16/22 13:30Sampled:SoilMatrix:
79.70% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]L-1[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/20/22 11:25GRO (C6-C10)^2.0 OWS2L200025.68.7 0.81
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168107 %OWSEPA 8015C 12/20/22 11:252L200021110.2 0.81
L-2Description:Lab Sample ID:CF19176-03 12/17/22 08:55Received:
CF19176Work Order:12/16/22 13:40Sampled:SoilMatrix:
83.40% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]L-2[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/20/22 11:59GRO (C6-C10)^2.0 OWS2L200025.6ND 0.847
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168104 %OWSEPA 8015C 12/20/22 11:592L200021110.2 0.847
L-3Description:Lab Sample ID:CF19176-04 12/17/22 08:55Received:
CF19176Work Order:12/16/22 13:50Sampled:SoilMatrix:
84.20% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]L-3[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/20/22 12:33GRO (C6-C10)^2.0 OWS2L200025.6ND 0.861
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168108 %OWSEPA 8015C 12/20/22 12:332L200021110.2 0.861
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 4 of 8Page 4 of 8
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ANALYTICAL RESULTS
L-4Description:Lab Sample ID:CF19176-05 12/17/22 08:55Received:
CF19176Work Order:12/16/22 14:00Sampled:SoilMatrix:
83.60% Solids:Thomas WillSampled By:Project:Stewarts
[TOC_2]L-4[TOC]
Gasoline Range Organics by GC
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/kg dry EPA 8015C 12/20/22 13:08GRO (C6-C10)^2.0 OWS2L200025.4ND 0.818
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2,5-Dibromotoluene 59-168104 %OWSEPA 8015C 12/20/22 13:082L20002109.79 0.818
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 5 of 8Page 5 of 8
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QUALITY CONTROL DATA [TOC_1]QC Data[TOC]
Gasoline Range Organics by GC - Quality Control
Batch 2L20002 - EPA 5035
Prepared: 12/20/2022 05:49 Analyzed: 12/20/2022 08:00Blank (2L20002-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.52.0 U GRO (C6-C10)
mg/kg wet 9.54 59-1682,5-Dibromotoluene 10710
Prepared: 12/20/2022 05:49 Analyzed: 12/20/2022 07:14LCS (2L20002-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 48.4 51-12011154 GRO (C6-C10)
mg/kg wet 9.69 59-1682,5-Dibromotoluene 10410
Prepared: 12/20/2022 05:49 Analyzed: 12/20/2022 08:34Matrix Spike (2L20002-MS1)
Source: CF18832-08
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 49.1 45-1621182.0 U58 GRO (C6-C10)
mg/kg wet 9.82 59-1682,5-Dibromotoluene 11812
Prepared: 12/20/2022 05:49 Analyzed: 12/20/2022 09:08Matrix Spike Dup (2L20002-MSD1)
Source: CF18832-08
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/kg wet5.5 48.8 2445-162121 22.0 U59 GRO (C6-C10)
mg/kg wet 9.77 59-1682,5-Dibromotoluene 12212
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 6 of 8Page 6 of 8
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FLAGS/NOTES AND DEFINITIONS [TOC_1]Flags/Notes[TOC]
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.PQL
Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.[CALC]
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 7 of 8Page 7 of 8
Page 8 of 8
ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bill Scott
Environmental Conservation Laboratories
102 Woodwinds Industrial Ct, Suite A
Cary, North Carolina 27511
Generated 1/4/2023 9:51:17 AM
JOB DESCRIPTION
CF14992
JOB NUMBER
680-227941-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
1/4/2023 9:51:17 AM
Authorized for release by
Naomi Flanagan, Project Manager
[e-mail]
Designee for
Sheila Hoffman, Project Manager II
[e-mail]@et.eurofinsus.com
[phone]
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Method Summary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Method Method Description LaboratoryProtocol
SW8468015DDiesel Range Organics (DRO) (GC)EET SAV
EPAMoisturePercent Moisture EET SAV
SW8463546Microwave Extraction EET SAV
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Sample Summary
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Lab Sample ID Client Sample ID Matrix Collected Received
680-227941-1 T-1 S-1 Solid 12/14/22 13:50 12/16/22 06:00
680-227941-2 T-1 S-2 Solid 12/14/22 13:55 12/16/22 06:00
680-227941-3 P-1 Solid 12/14/22 15:00 12/16/22 06:00
680-227941-4 T-2 S-1 Solid 12/14/22 10:05 12/16/22 06:00
680-227941-5 T-2 S-2 Solid 12/14/22 10:07 12/16/22 06:00
680-227941-6 T-2 S-3 Solid 12/14/22 10:10 12/16/22 06:00
680-227941-7 T-3 S-1 Solid 12/14/22 14:10 12/16/22 06:00
680-227941-8 T-3 S-2 Solid 12/14/22 14:15 12/16/22 06:00
680-227941-9 T-4 S-1 Solid 12/14/22 16:20 12/16/22 06:00
680-227941-10 T-4 S-2 Solid 12/14/22 16:25 12/16/22 06:00
680-227941-11 T-4 S-3 Solid 12/14/22 16:30 12/16/22 06:00
680-227941-12 P-2 Solid 12/14/22 11:20 12/16/22 06:00
680-227941-13 P-3 Solid 12/14/22 11:30 12/16/22 06:00
680-227941-14 P-4 Solid 12/14/22 11:40 12/16/22 06:00
680-227941-15 P-5 Solid 12/14/22 11:50 12/16/22 06:00
680-227941-16 Stockpile Solid 12/14/22 11:30 12/16/22 06:00
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Definitions/Glossary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Qualifiers
GC Semi VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Case Narrative
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Job ID: 680-227941-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-227941-1
Receipt
The samples were received on 12/16/2022 6:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.3°C
Diesel Range Organics
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Detection Summary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Client Sample ID: T-1 S-1 Lab Sample ID: 680-227941-1
☼Diesel Range Organics [C10-C28]
RL
10 mg/Kg3.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1118015D
Client Sample ID: T-1 S-2 Lab Sample ID: 680-227941-2
No Detections.
Client Sample ID: P-1 Lab Sample ID: 680-227941-3
No Detections.
Client Sample ID: T-2 S-1 Lab Sample ID: 680-227941-4
No Detections.
Client Sample ID: T-2 S-2 Lab Sample ID: 680-227941-5
No Detections.
Client Sample ID: T-2 S-3 Lab Sample ID: 680-227941-6
No Detections.
Client Sample ID: T-3 S-1 Lab Sample ID: 680-227941-7
No Detections.
Client Sample ID: T-3 S-2 Lab Sample ID: 680-227941-8
No Detections.
Client Sample ID: T-4 S-1 Lab Sample ID: 680-227941-9
No Detections.
Client Sample ID: T-4 S-2 Lab Sample ID: 680-227941-10
No Detections.
Client Sample ID: T-4 S-3 Lab Sample ID: 680-227941-11
No Detections.
Client Sample ID: P-2 Lab Sample ID: 680-227941-12
No Detections.
Client Sample ID: P-3 Lab Sample ID: 680-227941-13
No Detections.
Client Sample ID: P-4 Lab Sample ID: 680-227941-14
No Detections.
Client Sample ID: P-5 Lab Sample ID: 680-227941-15
No Detections.
Client Sample ID: Stockpile Lab Sample ID: 680-227941-16
Diesel Range Organics [C10-C28]
RL
7.9 mg/Kg2.6
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1F2178015D
Eurofins Savannah
This Detection Summary does not include radiochemical test results.
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-1Client Sample ID: T-1 S-1
Matrix: SolidDate Collected: 12/14/22 13:50
Percent Solids: 76.4Date Received: 12/16/22 06:00
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL
11 10 3.3 mg/Kg ☼12/19/22 18:15 12/20/22 16:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 69 15-139 12/19/22 18:15 12/20/22 16:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL
76.4 0.01 0.01 %12/28/22 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-2Client Sample ID: T-1 S-2
Matrix: SolidDate Collected: 12/14/22 13:55
Percent Solids: 86.0Date Received: 12/16/22 06:00
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL
<2.9 9.1 2.9 mg/Kg ☼12/19/22 18:15 12/20/22 16:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 59 15-139 12/19/22 18:15 12/20/22 16:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL
86.0 0.01 0.01 %12/28/22 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-3Client Sample ID: P-1
Matrix: SolidDate Collected: 12/14/22 15:00
Percent Solids: 69.3Date Received: 12/16/22 06:00
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL
<3.7 11 3.7 mg/Kg ☼12/19/22 18:15 12/20/22 16:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 46 15-139 12/19/22 18:15 12/20/22 16:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL
69.3 0.01 0.01 %12/28/22 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-4Client Sample ID: T-2 S-1
Matrix: SolidDate Collected: 12/14/22 10:05
Percent Solids: 81.0Date Received: 12/16/22 06:00
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL
<3.2 9.8 3.2 mg/Kg ☼12/19/22 18:15 12/20/22 16:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 61 15-139 12/19/22 18:15 12/20/22 16:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL
81.0 0.01 0.01 %12/28/22 13:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-5Client Sample ID: T-2 S-2
Matrix: SolidDate Collected: 12/14/22 10:07
Date Received: 12/16/22 06:00
General Chemistry
RL
84.3 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-6Client Sample ID: T-2 S-3
Matrix: SolidDate Collected: 12/14/22 10:10
Date Received: 12/16/22 06:00
General Chemistry
RL
79.5 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-7Client Sample ID: T-3 S-1
Matrix: SolidDate Collected: 12/14/22 14:10
Date Received: 12/16/22 06:00
General Chemistry
RL
77.1 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-8Client Sample ID: T-3 S-2
Matrix: SolidDate Collected: 12/14/22 14:15
Date Received: 12/16/22 06:00
General Chemistry
RL
77.6 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-9Client Sample ID: T-4 S-1
Matrix: SolidDate Collected: 12/14/22 16:20
Date Received: 12/16/22 06:00
General Chemistry
RL
76.9 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-10Client Sample ID: T-4 S-2
Matrix: SolidDate Collected: 12/14/22 16:25
Date Received: 12/16/22 06:00
General Chemistry
RL
84.7 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-11Client Sample ID: T-4 S-3
Matrix: SolidDate Collected: 12/14/22 16:30
Date Received: 12/16/22 06:00
General Chemistry
RL
75.5 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-12Client Sample ID: P-2
Matrix: SolidDate Collected: 12/14/22 11:20
Date Received: 12/16/22 06:00
General Chemistry
RL
86.5 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-13Client Sample ID: P-3
Matrix: SolidDate Collected: 12/14/22 11:30
Date Received: 12/16/22 06:00
General Chemistry
RL
81.8 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-14Client Sample ID: P-4
Matrix: SolidDate Collected: 12/14/22 11:40
Date Received: 12/16/22 06:00
General Chemistry
RL
85.7 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-15Client Sample ID: P-5
Matrix: SolidDate Collected: 12/14/22 11:50
Date Received: 12/16/22 06:00
General Chemistry
RL
85.7 0.01 0.01 %01/03/23 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Solids (EPA Moisture)
Eurofins Savannah
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Client Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Lab Sample ID: 680-227941-16Client Sample ID: Stockpile
Matrix: SolidDate Collected: 12/14/22 11:30
Date Received: 12/16/22 06:00
Method: SW846 8015D - Diesel Range Organics (DRO) (GC)
RL
17 F2 7.9 2.6 mg/Kg 12/28/22 15:50 12/30/22 03:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Diesel Range Organics [C10-C28]
o-Terphenyl 65 15-139 12/28/22 15:50 12/30/22 03:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Savannah
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QC Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Method: 8015D - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 680-755960/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756114 Prep Batch: 755960
RL
Diesel Range Organics [C10-C28]<2.6 7.9 2.6 mg/Kg 12/19/22 18:15 12/20/22 15:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 66 15-139 12/20/22 15:07 1
MB MB
Surrogate
12/19/22 18:15
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-755960/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 756114 Prep Batch: 755960
Diesel Range Organics
[C10-C28]
32.9 28.1 mg/Kg 86 26-133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 680-757101/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 757323 Prep Batch: 757101
RL
Diesel Range Organics [C10-C28]<2.6 7.9 2.6 mg/Kg 12/28/22 15:50 12/30/22 02:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 86 15-139 12/30/22 02:47 1
MB MB
Surrogate
12/28/22 15:50
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-757101/14-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 757323 Prep Batch: 757101
Diesel Range Organics
[C10-C28]
32.4 27.3 mg/Kg 84 26-133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: StockpileLab Sample ID: 680-227941-16 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 757323 Prep Batch: 757101
Diesel Range Organics
[C10-C28]
17 F2 33.2 34.6 mg/Kg 54 26-133
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
o-Terphenyl 15 -139
Surrogate
93
MS MS
Qualifier Limits%Recovery
Eurofins Savannah
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QC Sample Results
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Method: 8015D - Diesel Range Organics (DRO) (GC) (Continued)
Client Sample ID: StockpileLab Sample ID: 680-227941-16 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 757323 Prep Batch: 757101
Diesel Range Organics
[C10-C28]
17 F2 32.7 58.3 F2 mg/Kg 127 26-133 51 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
o-Terphenyl 15 -139
Surrogate
96
MSD MSD
Qualifier Limits%Recovery
Eurofins Savannah
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QC Association Summary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
GC Semi VOA
Prep Batch: 755960
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227941-1 T-1 S-1 Total/NA
Solid 3546680-227941-2 T-1 S-2 Total/NA
Solid 3546680-227941-3 P-1 Total/NA
Solid 3546680-227941-4 T-2 S-1 Total/NA
Solid 3546MB 680-755960/7-A Method Blank Total/NA
Solid 3546LCS 680-755960/8-A Lab Control Sample Total/NA
Analysis Batch: 756114
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015D 755960680-227941-1 T-1 S-1 Total/NA
Solid 8015D 755960680-227941-2 T-1 S-2 Total/NA
Solid 8015D 755960680-227941-3 P-1 Total/NA
Solid 8015D 755960680-227941-4 T-2 S-1 Total/NA
Solid 8015D 755960MB 680-755960/7-A Method Blank Total/NA
Solid 8015D 755960LCS 680-755960/8-A Lab Control Sample Total/NA
Prep Batch: 757101
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546680-227941-16 Stockpile Total/NA
Solid 3546MB 680-757101/13-A Method Blank Total/NA
Solid 3546LCS 680-757101/14-A Lab Control Sample Total/NA
Solid 3546680-227941-16 MS Stockpile Total/NA
Solid 3546680-227941-16 MSD Stockpile Total/NA
Analysis Batch: 757323
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015D 757101680-227941-16 Stockpile Total/NA
Solid 8015D 757101MB 680-757101/13-A Method Blank Total/NA
Solid 8015D 757101LCS 680-757101/14-A Lab Control Sample Total/NA
Solid 8015D 757101680-227941-16 MS Stockpile Total/NA
Solid 8015D 757101680-227941-16 MSD Stockpile Total/NA
General Chemistry
Analysis Batch: 757069
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-227941-1 T-1 S-1 Total/NA
Solid Moisture680-227941-2 T-1 S-2 Total/NA
Solid Moisture680-227941-3 P-1 Total/NA
Solid Moisture680-227941-4 T-2 S-1 Total/NA
Analysis Batch: 757609
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-227941-5 T-2 S-2 Total/NA
Solid Moisture680-227941-6 T-2 S-3 Total/NA
Solid Moisture680-227941-7 T-3 S-1 Total/NA
Solid Moisture680-227941-8 T-3 S-2 Total/NA
Solid Moisture680-227941-9 T-4 S-1 Total/NA
Solid Moisture680-227941-10 T-4 S-2 Total/NA
Solid Moisture680-227941-11 T-4 S-3 Total/NA
Solid Moisture680-227941-12 P-2 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
General Chemistry (Continued)
Analysis Batch: 757609 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-227941-13 P-3 Total/NA
Solid Moisture680-227941-14 P-4 Total/NA
Solid Moisture680-227941-15 P-5 Total/NA
Eurofins Savannah
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Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Client Sample ID: T-1 S-1 Lab Sample ID: 680-227941-1
Matrix: SolidDate Collected: 12/14/22 13:50
Date Received: 12/16/22 06:00
Analysis Moisture KF12/28/22 13:211 EET SAV757069
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-1 S-1 Lab Sample ID: 680-227941-1
Matrix: SolidDate Collected: 12/14/22 13:50
Percent Solids: 76.4Date Received: 12/16/22 06:00
Prep 3546 MEW12/19/22 18:15 EET SAV755960
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.84 g 1 mL
Analysis 8015D 1 756114 12/20/22 16:09 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: T-1 S-2 Lab Sample ID: 680-227941-2
Matrix: SolidDate Collected: 12/14/22 13:55
Date Received: 12/16/22 06:00
Analysis Moisture KF12/28/22 13:211 EET SAV757069
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-1 S-2 Lab Sample ID: 680-227941-2
Matrix: SolidDate Collected: 12/14/22 13:55
Percent Solids: 86.0Date Received: 12/16/22 06:00
Prep 3546 MEW12/19/22 18:15 EET SAV755960
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.80 g 1 mL
Analysis 8015D 1 756114 12/20/22 16:24 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: P-1 Lab Sample ID: 680-227941-3
Matrix: SolidDate Collected: 12/14/22 15:00
Date Received: 12/16/22 06:00
Analysis Moisture KF12/28/22 13:211 EET SAV757069
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-1 Lab Sample ID: 680-227941-3
Matrix: SolidDate Collected: 12/14/22 15:00
Percent Solids: 69.3Date Received: 12/16/22 06:00
Prep 3546 MEW12/19/22 18:15 EET SAV755960
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.30 g 1 mL
Analysis 8015D 1 756114 12/20/22 16:39 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Client Sample ID: T-2 S-1 Lab Sample ID: 680-227941-4
Matrix: SolidDate Collected: 12/14/22 10:05
Date Received: 12/16/22 06:00
Analysis Moisture KF12/28/22 13:211 EET SAV757069
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-2 S-1 Lab Sample ID: 680-227941-4
Matrix: SolidDate Collected: 12/14/22 10:05
Percent Solids: 81.0Date Received: 12/16/22 06:00
Prep 3546 MEW12/19/22 18:15 EET SAV755960
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.28 g 1 mL
Analysis 8015D 1 756114 12/20/22 16:54 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Client Sample ID: T-2 S-2 Lab Sample ID: 680-227941-5
Matrix: SolidDate Collected: 12/14/22 10:07
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-2 S-3 Lab Sample ID: 680-227941-6
Matrix: SolidDate Collected: 12/14/22 10:10
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-3 S-1 Lab Sample ID: 680-227941-7
Matrix: SolidDate Collected: 12/14/22 14:10
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-3 S-2 Lab Sample ID: 680-227941-8
Matrix: SolidDate Collected: 12/14/22 14:15
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Client Sample ID: T-4 S-1 Lab Sample ID: 680-227941-9
Matrix: SolidDate Collected: 12/14/22 16:20
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-4 S-2 Lab Sample ID: 680-227941-10
Matrix: SolidDate Collected: 12/14/22 16:25
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: T-4 S-3 Lab Sample ID: 680-227941-11
Matrix: SolidDate Collected: 12/14/22 16:30
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-2 Lab Sample ID: 680-227941-12
Matrix: SolidDate Collected: 12/14/22 11:20
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-3 Lab Sample ID: 680-227941-13
Matrix: SolidDate Collected: 12/14/22 11:30
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: P-4 Lab Sample ID: 680-227941-14
Matrix: SolidDate Collected: 12/14/22 11:40
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Client Sample ID: P-5 Lab Sample ID: 680-227941-15
Matrix: SolidDate Collected: 12/14/22 11:50
Date Received: 12/16/22 06:00
Analysis Moisture WRB01/03/23 08:451 EET SAV757609
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: Stockpile Lab Sample ID: 680-227941-16
Matrix: SolidDate Collected: 12/14/22 11:30
Date Received: 12/16/22 06:00
Prep 3546 MEW12/28/22 15:50 EET SAV757101
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.42 g 1 mL
Analysis 8015D 1 757323 12/30/22 03:17 JCK EET SAVTotal/NA 1 mL 1 mL
CSGAB1Instrument ID:
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Environmental Conservation Laboratories Job Number: 680-227941-1
Login Number: 227941
Question Answer Comment
Creator: Johnson, Corey M
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-23
Eurofins Savannah
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Definitions/Glossary
Job ID: 680-227941-1Client: Environmental Conservation Laboratories
Project/Site: CF14992
Qualifiers
GC Semi VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-227941-1
Project/Site: CF14992
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-23
Eurofins Savannah
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