Loading...
HomeMy WebLinkAboutFA-7962_42202_CA_MRP_20210114_SW6993January 14, 2021 Ms. Sarah Brown North Carolina Department of Environmental Quality Division of Waste Management – UST Section 225 Green Street, Suite 714 Fayetteville, North Carolina 28301-5095 Subject:GROUNDWATER MONITORING REPORT SPEEDWAY 6993 670 NORTH REILLY ROAD FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA DWM INCIDENT NO: 30467 FACILITY ID NO.: 00-0-0015515 MID-ATLANTIC JOB NO. R3243.02 Dear Ms. Brown: Speedway LLC is pleased to present this report of environmental services for the Speedway 6993 facility located at 670 North Reilly Road, Fayetteville, North Carolina. The attached report documents the recent Groundwater Monitoring activities. If you have any questions or need additional information, please feel free to contact me at (919) 516-8069 or Troy Holzschuh with Mid-Atlantic Associates, Inc. at (980) 585-1271. Sincerely, SPEEDWAY LLC Charles A. Chiara Environmental Representative Located at: 670 North Reilly Road Fayetteville,Cumberland County,North Carolina Prepared for (Users): Speedway, LLC 500 Speedway Drive Enon,Ohio 45323 (919) 516-8069 Report Date: January 14, 2021 MAA Project: R3243.02 Groundwater Monitoring Report Speedway 6993 Facility ID#:00-0-0015515 670 North Reilly Road Fayetteville,North Carolina Incident No.:42202 Prepared By: Mid-Atlantic Associates Inc. 409 Rogers View Court, Raleigh,North Carolina 27610 (919) 250-9918 GROUNDWATER MONITORING REPORT A. SITE INFORMATION 1. Site Identification Date of Report: January 14, 2021 Facility ID:00-0-0015515 UST Incident No. (if known):42202 Site Risk:Intermediate Site Rank:I-115-D Land Use Classification:Unassigned Site Name:Speedway 6993 Site Location:670 North Reilly Road,Fayetteville,North Carolina Nearest City/Town:Fayetteville County:Cumberland Latitude:35.099832 N Longitude:-78.010845 W Description of Geographical Data Point: Site Property Location Method:Google Earth 2. Information about Contacts Associated with the Leaking UST System UST Owner:Speedway LLC Address:500 Speedway Drive, Enon, Ohio 45323 Phone:(919) 516-8069 UST Operator:Same as UST Owner Address:Phone: Property Owner:Same as UST Owner Address:Phone: Property Occupant:Same as UST Owner Address:Phone: Consultant/Contractor:Mid-Atlantic Associates, Inc. Address:409 Rogers View Ct., Raleigh, NC 27610 Phone:(919) 250-9918 3. Release Information Date Discovered:March 1, 2019 Estimated Quantity of Release:unknown Cause of Release:Unknown Source of Release (Piping/UST):diesel dispenser Sizes and contents of UST system(s) from which release occurred:Two 10,000-gallon gasoline USTs containing gasoline, one 10,000-gallon UST containing diesel fuel, and one 6,000-gallon UST containing kerosene Criteria Used to Classify Risk:dissolved phase concentrations above GCLs Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 1 I,Raymond S. Marchant, III, PG ,a Professional Engineer/Licensed Geologist (circle one) for Mid-Atlantic Associates, Inc.(firm or company of employment), do certify that the information contained in this report is correct and accurate to the best of my knowledge. (Please affix seal and signature) Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 2 TABLE OF CONTENTS List of Acronyms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1.0 BACKGROUND INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 2.0 SITE HISTORY AND SOURCE CHARACTERIZATION . . . . . . . . . . . . . . . . . . . . 3 2.1 UST Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2.2 UST System Owner/Operator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2.3 Information on Source of Release . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2.4 Regional Geology and Hydrogeology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2.5 Site Geology and Hydrogeology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3.0 POTENTIAL RECEPTORS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 4.0 FIELD ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 4.1 Liquid Level Measurements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 4.2 Monitoring Well Sample Collection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 5.0 DISCUSSION OF SAMPLING RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 5.1 Summary of Analytical Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 5.2 Description of Current Plume Size and Location . . . . . . . . . . . . . . . . . . . . . 5 5.3 Additional Monitoring Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 6.0 FUTURE SITE REMEDIATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 7.0 SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS . . . . . . . . . . . . . . . . 7 8.0 STATEMENTS AND CERTIFICATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 DRAWINGS Drawing 1.1 -Topographic Site Map Drawing 1.2 - Site and Monitoring Well Location Map Drawing 5.1 - Benzene Isoconcentration Map TABLES Table 4.1 - Monitoring Well Construction Data Table 4.2 - Summary of Historical Liquid Level Measurements Table 5.1 - Summary of Historical Groundwater Quality Data for Selected Compounds APPENDICES Appendix A Selected Historical Site Information Appendix B Mid-Atlantic Field Procedures Appendix C Laboratory Analytical Reports and Chain-of-Custody Records for Groundwater Samples i LIST OF ACRONYMS 2012 Guidelines Underground Storage Tank Section Guidelines for Assessment and Corrective Action For UST Releases, DENR, Division of Waste Management UST Section, July 15, 2008 Version, Change 2, Effective October 1, 2012 AFVR Aggressive Fluid-Vapor Recovery AS Air Sparge AST Aboveground Storage Tank BQL Below (Laboratory Practical) Quantitation Limit BLS Below Land Surface BTEX Benzene, Toluene, Ethylbenzene, Xylenes CAP Corrective Action Plan cm Centimeter COC Constituents of Concern CSA Comprehensive Site Assessment DIPE Diisopropyl Ether (also IPE: Isopropyl Ether) DNAPL Dense Non-Aqueous Phase Liquids DO Dissolved Oxygen DPE Dual-Phase Extraction DPT Direct Push Technology DRO Diesel Range Organics DSCA North Carolina Dry-Cleaning Solvent Act DTW Depth to Water DWM Division of Waste Management DWQ Division of Water Quality EDB Ethylene di-bromide EPA Environmental Protection Agency EPH Extractable Petroleum Hydrocarbons FID Flame Ionization Detector FT Feet GCL Gross Contamination Level GIS Geographic Information System GPM Gallons Per Minute GPS Global Positioning System GRO Gasoline Range Organics ID Identification IDW Investigation Derived Waste IGQS Interim Groundwater Quality Standards LSA Limited Site Assessment LUST Leaking Underground Storage Tank m Meter MADEP Massachusetts Department of Environmental Protection Mid-Atlantic Mid-Atlantic Associates, Inc. MDL Method Detection Limit mg/Kg Milligrams per Kilogram mg/L Milligrams per Liter MMP Minimum Management Practices MMPE Mobile Multi-Phase Extraction MNA Monitored Natural Attenuation MSCC Maximum Soil Contaminant Concentration MSL Mean Sea Level MTBE Methyl tertiary butyl ether g/Kg Micrograms per Kilogram g/L Micrograms per Liter NA Not Analyzed N/A Not Applicable NC North Carolina NCAC North Carolina Administrative Code NCDEQ North Carolina Department of Environmental Quality NCDOT North Carolina Department of Transportation NCGQS North Carolina Groundwater Quality Standards NCSWQS North Carolina Surface Water Quality Standards ND Not Detected NM Not Measured NORR Notice of Regulatory Requirements NOV Notice of Violation NS Not Sampled ORP Oxidation-Reduction Potential OVA Organic Vapor Analyzer PA Prioritization Assessment PAA Prioritization Assessment Agreement PAH Polynuclear Aromatic Hydrocarbons Pb Lead PCBs Polychlorinated Biphenyls PCE Perchloroethylene (also tetrachloroethene) PPB Parts Per Billion PPM Parts Per Million PID Photo Ionization Detector POTW Publicly Owned Treatment Works PQL Practical Quantitation Limit PRF Prioritization Ranking Form PVC Polyvinyl chloride RBCA Risk-Based Corrective Action RCRA Resource Conservation and Recovery Act ROI Radius of Influence s Seconds SAR Soil Assessment Report SOW Scope of Work STG Soil-to-Groundwater SVE Soil Vapor Extraction SVOC Semi-Volatile Organic Compound TDHF Toxicologically Defined Hydrocarbon Fractions TCLP Toxicity Characteristic Leaching Procedure TIC Tentatively Identified Compound TOC Top of Casing TPH Total Petroleum Hydrocarbons US United States USCS Unified Soil Classification System USGS United States Geological Survey UST Underground Storage Tank UT Unnamed Tributary VOC Volatile Organic Compounds VPH Volatile Petroleum Hydrocarbons yr Year 1.0 BACKGROUND INFORMATION The site is the Speedway 6993 located at 670 North Reilly Road, Fayetteville, Cumberland County,North Carolina (Drawings 1.1 & 1.2). The site is a closed petroleum retail facility and convenience store and contained four underground storage tanks (USTs) total: three 10,000-gallon capacity USTs (regular gasoline, premium gasoline, and diesel fuel) and one 6,000-gallon capacity UST (kerosene). The three 10,000-gallon capacity USTs were located to the north of the building and dispensers, and the one 6,000-gallon capacity UST was located to the east.The site topographic location is shown on Drawing 1.1, and the site drawing with the approximate locations of the USTs is presented as Drawing 1.2. UST closure activities were performed in February 2019. During the tank closure, petroleum impact was identified in the overburden of the three 10,000-gallon tanks. The impacted material was segregated and disposed of offsite at an approved facility. On February 28, 2019, diesel fuel contamination was encountered in the vicinity of the diesel dispenser during the UST closure activities. Initial soil sampling confirmed the release and initial abatement measure were taken. Approximately one ton of impacted soil was excavated and disposed of at the A&D Environmental (A&D) facility in High Point, North Carolina. The extent of the excavation was limited due to the structural concerns of undermining the canopy. Drawing 1.2 shows the location of the former UST basins, product lines, diesel dispenser (source area), and monitoring wells. A 24-Hour Release and UST Leak Reporting Form was submitted to the North Carolina Department of Environmental Quality (NCDEQ) by Mid-Atlantic on March 1, 2019. A UST Closure and Initial Abatement Action Report was submitted on June 3, 2019. The NCDEQ issued a Notice of Regulatory Requirements on June 24, 2019 requiring the completion of a Limited Site Assessment (LSA). Based on the results of the LSA, NCDEQ classified the site as intermediate risk with a Risk, Ranking, and Abatement score of I 115 D and additional groundwater monitoring was requested. A comprehensive groundwater monitoring sampling event was conducted in August 2020 and the report was submitted to the NCDEQ by Mid-Atlantic on September 25, 2020. The NCDEQ issued the acknowledgement of report receipt on On October 23, 2020 requiring an additional groundwater sampling event and the submittal of a Groundwater Monitoring Report to the Fayetteville division by January 22, 2021. This report documents the results of this sampling. The opinions included herein are based on our experience and the information obtained during the study. This report is based on limited observations made on the dates noted using the procedures described herein. If additional information becomes available, we request the opportunity to review the information, reassess the potential environmental concerns and modify our conclusions and recommendations, if appropriate. Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 2 2.0 SITE HISTORY AND SOURCE CHARACTERIZATION 2.1 UST Information According to the UST Section’s Registration database, the site’s Facility I.D. number is 00-0-0015515. The following table summarizes the UST System information. SmartTable UST ID Number Previous Contents Capacity (Gallons) Tank Dimensions Construction Details Date Installed Status of UST Release Associated with System 1 Gasoline 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 No 2 Gasoline 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 No 3 Diesel 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 Yes 4 Kerosene 6,000 Approximately 8’ x 16’ Single-walled steel 1979 Removed 2/27/19 No 2.2 UST System Owner/Operator The UST system is owned and operated by Speedway LLC. 2.3 Information on Source of Release On February 28, 2019, diesel fuel contamination was encountered in the vicinity of the diesel dispenser during the UST closure activities. Initial soil sampling confirmed the release and initial abatement measures were taken. Approximately one ton of impacted soil was excavated and disposed of at the A&D Environmental (A&D) facility in High Point, North Carolina. 2.4 Regional Geology and Hydrogeology According to the map titled Geology of North Carolina (1985), prepared by the North Carolina Geological Survey Section of the NCDEQ, the subject site is located in the Middendorf Formation (Geologic Unit: Km). The site appears to be located in an area of “sand, sandstone, and mudstone, gray to pale gray with an orange cast, mottled; clay balls and iron-cemented concretions common, beds laterally discontinuous, cross bedding common”. Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 3 The subject site is located in the Coastal Plain physiographic region. In the coastal plain, an aquifer is typically composed of one to several layers of eastward thickening, permeable sands or limestone split by discontinuous, clay-rich materials. Confining units, consisting of clay-rich sediments, exist above and below an aquifer. These confining units are more continuous clay layers and separate the aquifer. The surficial or unconfined aquifer overlies all the confined aquifers in the coastal plain. 2.5 Site Geology and Hydrogeology Selected historical site assessment data is provided in Appendix A. GENERAL GEOLOGIC PROFILE Depth (FT BLS)GEOLOGIC DESCRIPTION 0 - 30 feet (approx.)Natural deposits primarily consist of sands and sandy clayey silts with varying thicknesses. 30 - 40 feet Clays and clayey silty sand. Bedrock not encountered to a depth of 40 feet. HYDROGEOLOGICAL PARAMETERS - PHASE II LIMITED SITE ASSESSMENT REPORT, APRIL 17, 2020 UNLESS OTHERWISE NOTED PARAMETER RESULT Average Depth to Shallow Groundwater, February 2020 25.42 feet Maximum Observed Seasonal Fluctuation in Depth to Groundwater (February to August 2020) Approximately 3.02 feet Groundwater Flow Direction Not calculated - see text for explanation Hydraulic Gradient (Horizontal)Not calculated - see text for explanation Hydraulic Conductivity (measured by rising head testing) Data not available - aquifer testing not performed to date Groundwater Flow Velocity1 Data not available - aquifer testing not performed to date 3.0 POTENTIAL RECEPTORS Receptor information for the site was previously documented in Mid-Atlantic’s Phase II Limited Site Assessment Report dated April 17, 2020. A receptor survey update was not conducted during this monitoring event. Please refer to previous reports for detailed receptor information. As indicated, the site is currently classified as “intermediate” risk due to the exceedance of GCLs for benzene in MW-1. According to the USGS topographic quadrangle map of Cliffdale, North Carolina (Drawing 1.1), the nearest surface water body is Persimmon Creek, located approximately 2,770 feet to the northeast of the source area of the release. Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 4 4.0 FIELD ACTIVITIES On November 18, 2020 Mid-Atlantic personnel mobilized to the site to conduct groundwater sampling, which included liquid level measurements. 4.1 Liquid Level Measurements Mid-Atlantic personnel collected depth to free product and/or depth to groundwater measurements from site monitoring wells on November 18, 2020. Monitoring well construction details are provided in Table 4.1. Liquid level measurements, along with historical measurements, are summarized in Table 4.2 As indicated, MW-1, MW-2, MW-3R and MW-4R did not exhibit free product.Liquid level measurements were collected using the procedures described in Appendix B. 4.2 Monitoring Well Sample Collection Mid-Atlantic personnel collected groundwater samples from monitoring well MW-1 on November 18, 2020. Groundwater samples were collected using the procedures described in Appendix B. Samples were shipped to Pace Analytical Services (Pace) in Mt. Juliet, Tennessee and analyzed by the methods shown on the chain-of-custody record provided in Appendix C. 5.0 DISCUSSION OF SAMPLING RESULTS 5.1 Summary of Analytical Results Laboratory analytical reports and chain-of-custody records for groundwater samples collected in November 2020 are provided in Appendix C, with the results of selected target compounds summarized in Table 5.1. As summarized, the groundwater samples collected from well MW-1 exhibited several contaminant concentrations above the NCGQS. However, only benzene in MW-1 exhibited a concentration greater than the GCL. 5.2 Description of Current Plume Size and Location Free Product On November 18, 2020, Mid-Atlantic measured the depth to water in the monitoring wells using an electronic water level indicator. No evidence of free product was observed in the monitoring wells. Groundwater Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 5 An isoconcentration map for benzene for the November 18, 2020 groundwater sampling event is provided as Drawing 5.1. The contaminant plume appears to be migrating towards the south/southwest. 5.3 Additional Monitoring Information •Proximity of Plume to Nearest Receptor Based on the results of the LSA receptor survey, three water supply wells were observed within 1,500 feet of the release area during the area reconnaissance. Mid-Atlantic spoke with the owner of Pro Carwash & Detail located at 648 N. Reilly Road regarding their onsite water supply well. He said that the well is used for irrigation only and is not used for drinking water. Mid-Atlantic used GIS software to measure the distance from the diesel dispenser to the water supply well and determined that the well is located 264 feet from the source area of the release. The Property is connected to city water. Mid-Atlantic spoke with Mr. Heavner, the property owner of the two water supply wells located at 735 N Reilly Road, and he indicated that the wells are not currently in use and have been out of service for a long time. Both Properties are connected to city water. According to the Fayetteville Public Works Commission (PWC) Water Resources Engineering Department municipal-supply system is available to all the properties within the 1,500-foot radius search area of the search area of the release. The nearest surface water body is Persimmon Creek, located approximately 2,770 feet to the northeast of the source area of the release. •Groundwater Flow Direction Based on the available data, it is not possible to accurately determine horizontal groundwater flow direction at the site. Based on general observation of water levels in the on-site wells, however, it appears that groundwater may flow towards the south. Wells MW-1 and MW-2 were set to depths of 22 feet BLS, while MW-3R and MW-4R were set to 40 feet BLS. Wells MW-3 and MW-4 were initially set to 22 feet BLS, but did not produce any water. Therefore, the depth to water near wells MW-1 and MW-2 is significantly shallower than the depth to water in wells MW-3R and MW-4R. Mid-Atlantic suspects that MW-1 and MW-2 may be set in a perched aquifer and/or are hydraulically separated from a deeper, surficial aquifer in which MW-3R and MW-4R were constructed. Vertical groundwater flow direction beneath the site has not been determined, since a deeper, Type III well has not been constructed to date. Bedrock was not encountered at the site when drilling to 40 feet, and mostly sandy material was encountered. Based on the soil types encountered, it does not appear that a confining layer was encountered. Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 6 6.0 FUTURE SITE REMEDIATION Dissolved phase concentrations of the target compound benzene have slightly decreased in the sample collected from monitoring well MW-1. MW-1 returned results for benzene above the GCL;however, no free product was found. Mid-Atlantic recommends continued groundwater monitoring events to monitor plume movement and to evaluate whether an active remedial approach may be necessary. The next sampling event should take place in the first half of 2021. 7.0 SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS Based on the results of the November 2020 assessment activities, Mid-Atlantic concludes the following: •Free product was not detected in site monitoring wells; •A groundwater sample collected from well MW-1 exhibited several contaminant concentrations above the NCGQS. However, only benzene was detected at a concentration greater than the GCL; •Groundwater flow direction could not be accurately determined based on the degree of variance in the depth to water between wells MW-1 and MW-2, and wells MW-3R and MW-4R. Mid-Atlantic suspects that MW-1 and MW-2 were installed within a perched aquifer and/or are hydraulically separated from a deeper, surficial aquifer in which MW-3R and MW-4R were constructed. Based on the results, Mid-Atlantic recommends the following: •Continued periodic sampling (at least semi-annual) of the monitoring wells to evaluate contaminant plume movement; and, •Submittal of this report to the NCDEQ for their review and comment. 8.0 STATEMENTS AND CERTIFICATION The following statements must be included at the closing of the document text, and must display the seal and signature of the certifying P.E. or L.G. in addition to the name and certification number of the company or corporation [See 15A NCAC 2L .0103(e).] NO.DESCRIPTION YES NO 1 Enter the date the monitoring report was due.January 22, 2021.Will this report be submitted after the established due date? 2 Was any required information from the above template missing from this report? Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 7 NO.DESCRIPTION YES NO If the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. Pertinent information regarding site groundwater conditions is provided throughout the report and selected historical assessment information is provided in Appendix A. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) N/A - the VE system has been shut down and the remedial approach is being re-evaluated If the answer to question #3 is “NO”, skip to the certification under #8 below. If the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline proposed remedies. (This should be described in more detail in the report text above.) Natural attenuation is not currently part of the remedial strategy at this site, although it may be in the future. Remedial efforts to date have focused on removing free product from the water table 4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation?  5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source?  If the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions recommended to further assess or clean up this known or suspected source. Estimated mass calculations indicate fluctuations in volume of free product in the subsurface over time. Ethanol and oxygenates analysis of the free product was performed in December 2018 and the sample did not contain these compounds (were not indicative of a new/ongoing release). Therefore, fluctuations in volume may be related to natural fluctuation of the water table, resulting in fluctuating free product thicknesses. These data are best evaluated as trends over time. Free product thicknesses have remained relatively steady overall since the beginning of 2019. 6 Certification: I,Raymond S. Marchant, III, PG, a Licensed Geologist for Mid-Atlantic Associates, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. Mid-Atlantic Associates, Inc.is licensed to practice geology/engineering in North Carolina. The certification numbers of the company or corporation are C-186 & F-0967. Groundwater Monitoring Report Speedway 6993 Fayetteville, North Carolina January 14, 2021 Page 8 DRAWINGS DRAWN BY: DATE: ENG. CHECK: JOB NO:DRAFTCHECK: GIS NO: SITELOCATION ´ 1:12,000SCALE: Hope Mills Fort Bragg Fayetteville §¨¦I95 §¨¦U1 §¨¦U13 F §¨¦S24 §¨¦U401 B§¨¦U401HOKE CUMBERLAND HARNETT MOORE ROBESON LEE BLADEN 0 1,000 2,000500Feet REFERENCES:1. USGS TOPOGRAPHIC QUADRANGLES: CLIFDALE, NC; FAYETTEVILLE, NC - 20162. PROPERTY BOUNDARY FROM CUMBERLAND COUNTY GIS AREA SHOWN WITHINNORTH CAROLINA TOPOGRAPHIC SITE MAP SPEEDWAY #6993670 N. REILLY ROAD FAYETTEVILLE, NORTH CAROLINA APPROVAL: September 2020 000R3243.01 05G-R3243.00-01DWG NO: 1.1 @A @A !?!? @A @A UST-1 UST-2UST-3 UST-4 MW-4 MW-3 MW-2 MW-1 MW-4R MW-3RN REILLY RDFILLYAW RD ´ DRAWN BY: DRAFT CHECK BY: ENGINEER CHECK BY: APPROVED BY: SITE AND MONITORING WELL LOCATION MAPSPEEDWAY #6993670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES DATE: SEPTEMBER 2020 JOB NO.: 000R3243.01B GIS NO.: 5G-000R3243.01B-1.3 DRAWING NO.: 1.2 0 20 40 60 8010Feet Legend MONITORING WELL !?Abandoned @A Active PRODUCT LINE EXCAVATION TRENCH (Approximate) FORMER UST LOCATION (Approximate) UST EXCAVATION EXTENT (Approximate) SITE BOUNDARY STREETS TLH RSM @A @A !?!? @A @A 1.0 5,000 NOTES:(8,020) = BENZENE CONCENTRATION AT LOCATION (ug/L)(ND) = NOT DETECTED AT OR ABOVE LABORATORY METHOD DETECTION LIMIT(NS) = NOT SAMPLEDNC GROUNDWATER QUALITY STANDARD (NCGQS) FOR BENZENE = 1.0 ug/LGROSS CONTAMINATION LEVEL (GCL) FOR BENZENE = 5,000 ug/LSAMPLE COLLECTED ON NOVEMBER 18, 2020.MW-3R PREVIOUSLY HAD A CONCENTRATION OF 15.2 ug/L FOR BENZENE DURING THE AUGUST 2020 SAMPLING EVENT. MW-4(NS)MW-3(NS) MW-2(NS) MW-4R(NS) MW-1(8,020) MW-3R(NS) ´ DRAWN BY: DRAFT CHECK BY: ENGINEER CHECK BY: APPROVED BY: ESTIMATED ISOCONCENTRATION MAP - BENZENE IN SHALLOW GROUNDWATERSPEEDWAY #6993670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES DATE: DECEMBER 2020 JOB NO.: 000R3243.02 GIS NO.: 5G-000R3243.02-5.1 DRAWING NO.: 5.1 0 20 40 60 8010Feet Legend MONITORING WELL !?Abandoned @A Active ESTIMATED BENZNE ISOCONCENTRATION LINE SITE BOUNDARY STREETS TLH RSM TABLES MW-1 2 7/10/2019 21.5 6.5-21.5 MW-2 2 12/11/2019 22.0 7.0-22.0 MW-3**2 12/11/2019 22.0 7.0-22.0 MW-3R 2 2/11/2020 40.0 20.0-40.0 MW-4**2 12/11/2019 22.0 7.0-22.0 MW-4R 2 2/11/2020 40.0 20.0-40.0 NOTE: BLS = Below Land Surface ** = Monitoring Well Abandononed on 2/12/2020 MID-ATLANTIC JOB NO. 000R3243.02 TABLE 4.1 MONITORING WELL CONSTRUCTION DATA SPEEDWAY #6993 670 NORTH REILLY ROAD FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA WELL I.D. WELL DIAMETER (INCHES) INSTALLATION DATE TOTAL WELL DEPTH (FEET) SCREENED INTERVAL (FEET BLS) WELL NUMBER DATE ELEVATION (ft)DTP (ft), BLS APPARENT FP THICKNESS DTW (ft), BLS CORRECTED DTW (ft) STATIC WATER LEVEL ELEVATION (ft) MW-1 MW-1 7/11/2019 100.11 ----15.30 --84.81 MW-1 12/11/2019 100.11 ----17.09 --83.02 MW-1 12/12/2019 100.11 ----17.13 --82.98 MW-1 12/20/2020 100.11 ----17.05 --83.06 MW-1 2/11/2020 100.11 ----16.32 --83.79 MW-1 2/12/2020 100.11 ----16.32 --83.79 MW-1 8/5/2020 100.11 ----15.69 --84.42 MW-1 11/18/2020 100.11 ----16.45 --83.66 MW-2 MW-2 12/12/2020 99.49 ----Dry ---- MW-2 12/20/2020 99.49 ----13.21 --86.28 MW-2 2/11/2020 99.49 --12.45 --87.04 MW-2 2/12/2020 99.49 ----12.45 --87.04 MW-2 8/5/2020 99.49 ----12.09 --87.40 MW-2 11/18/2020 99.49 ----13.50 --85.99 MW-3 MW-3 12/12/2019 100.50 ----Dry ---- MW-3 12/20/2020 100.50 ----Dry ---- MW-3 2/11/2020 100.50 ----Dry ---- MW-3 MW-3R MW-3R 2/12/2020 100.50 ----36.88 --63.62 MW-3R 8/5/2020 100.50 ----33.96 --66.54 MW-3R 11/18/2020 100.50 ----34.60 --65.90 MW-4 MW-4 12/12/2019 99.58 ----Dry ---- MW-4 12/20/2020 99.58 ----Dry ---- MW-4 12/11/2020 99.58 ----Dry ---- MW-4 MW-4R MW-4R 2/12/2020 99.58 ----36.03 --63.55 MW-4R 8/5/2020 99.58 ----33.01 --66.57 MW-4R 11/18/2020 99.58 ----33.59 --65.99 Notes: DTP - Depth to Product (in feet) FP - Free Product ft - feet DTW - Depth to Water (in feet) NM - Not Measured Well installed 12/11/2019 Well installed 12/11/2019 Well installed 12/11/2019 TABLE 4.2 SUMMARY OF HISTORICAL LIQUID LEVEL MEASUREMENTS SPEEDWAY #6993 670 NORTH REILLY ROAD FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA MID-ATLANTIC JOB NO. 000R3243.02 Well installed 7/10/2019 BLS - Below Land Surface Well abandoned 2/12/2020 Well abandoned 2/12/2020 Well installed 2/11/2020 Well installed 2/11/2020 1 70 600 20 6 600 500 0.05 0.05 NE 6 200 400 700 10,000 200 5,000 70,000 84,500 20,000 6,000 260,000 85,500 4.7 0.75 NE 6,000 410 NE NE NE NE Naphthalene MW-1 7/11/2019 2,650 ND 2,690 ND 798 14,200 14,100 ND ND ND 206 ND 38,200 31,830 ND 15,020 MW-1 12/20/2019 7,770 ND 3,240 ND 899 26,900 15,310 ND ND 0.387J 594 ND 77,300 50,065 43.5J 7,234 MW-1 2/12/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-1 8/5/2020 8,390 ND 4,140 ND 674 33,800 22,050 ND ND ND 529 0.188 63,900 31,291 59.9 9,620 MW-1 11/18/2020 8,020 ND 3,360 ND 749 J 30,800 17,470 ND ND ND 611 0.120 J 55,600 27,751 ND 1,160 MW-2 12/20/2019 ND ND ND ND ND ND ND ND ND 0.403J ND ND ND 55.5J ND 53.0J MW-2 2/12/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-2 8/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND 41.2 34.2 ND MW-2 11/18/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-3 12/20/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-3 2/12/2020 MW-3R 2/12/2020 0.807 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-3R 8/5/2020 15.2 ND 0.777 0.523 1.21 0.754 28.384 0.199 0.13 0.453 0.739 ND 80.3 52.4 33.6 43.5 MW-3R 11/18/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-4 12/20/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-4 2/12/2020 MW-4R 2/12/2020 ND ND ND ND ND ND ND ND ND 0.523J ND 0.444J ND ND ND ND MW-4R 8/5/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND 58.7 40 ND MW-4R 11/18/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NOTES: All values reported in ug/L (micrograms per liter)NCGQS = North Carolina Groundwater Quality Standard J = Estimated value, detected value is below the instrument calibration limits GCL = Gross Contamination Level NR = Not Reported BOLD values equal or exceed NCGQS ND = Not detected at or above the laboratory's quantitation limit NS - Not Sampled P = RPD between the primary and confirmatory analysis exceeded 40%DIPE = Di-Isopropyl Ether NE = Not established Di-isopropyl ether Ethylbezene MTBE VOLATILE ORGANIC COMPOUNDS - SM 602 SEMI VOLATILE ORGANIC COMPOUNDS - SM 625 Naphthalene PhenathreneToluene MADEP VPH & EPH C19-C36 ALIPHATICS Well abandoned C5-C8 ALIPHATICS C9-C18 ALIPHATICS C9-C22 AROMATICS Well abandoned Total Xylenes Benzo (a) anthracene Benzo (b) fluoranthene Di-n-butly phthalate NCGQS GCL Benzene WELL NUMBER SAMPLE DATE MID-ATLANTIC JOB NO. 000R3243.02 TABLE 5.1 SUMMARY OF HISTORICAL GROUNDWATER QUALITY DATA FOR SELECTED COMPOUNDS SPEEDWAY 6993 670 NORTH REILLY ROAD FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA Page 1 of 1 APPENDIX A SELECTED HISTORICAL SITE INFORMATION &( &( &( ^_FORT B R A G G WSW-2 WSW-3 WSW-1 FILLYAW RD DANDRIDGE DR N REILLY RD DECATUR DR GODFREY DR BE D F O R D R D ENFIELD DR TELFAIR DR ROUNDTREE DR WAKEFIELD DR CHANNING DR LEMONT DR KISCO DR NC HWY 295 N AVALON D R NC HWY 295 S CROWN AVE SMITHFIELD ST GARFIELD DR SQUIRE LN SEATON PL BASHLO T P L R U T O N C T FAIRVALE DR QUIMBY CT ASHWOOD CIR AP P L E W O O D L N BLACK DR STANDISH CT D E C A T U R P L ´ DRAWN BY: DRAFT CHECK BY: ENGINEER CHECK BY: APPROVED BY: RECEPTOR SURVEY MAP SPEEDWAY #6993670 N. REILLY ROAD FAYETTEVILLE, NORTH CAROLINA REFERENCE: CUMBERLAND COUNTY GIS. MID-ATLANTIC FIELD NOTES DATE: APRIL 2020 JOB NO.: 000R3243.0A GIS NO.: 5G-R3243.0A-5.1 DRAWING NO.: 5.1 Legend ^_DIESEL DISPENSER SITE BOUNDARY 500' BUFFER 1,000' BUFFER 1,500' BUFFER BUILDING FOOTPRINT &(WATER SUPPLY WELL COMMERCIAL RESIDENTIAL STREETS @A @A !?!? @A @A 1.0 5,000 NOTES:(7,770) = BENZENE CONCENTRATION AT LOCATION (ug/L)(ND) = NOT DETECTED AT OR ABOVE LABORATORY METHOD DETECTION LIMIT(NS) = NOT SAMPLED - WELL DRYNC GROUNDWATER QUALITY STANDARD (NCGQS) FOR BENZENE = 1.0 ug/LGROSS CONTAMINATION LEVEL (GCL) FOR BENZENE = 5,000 ug/LMW-1 AND MW-2 SAMPLED 12/20/2019; MW-3R AND MW-4R SAMPLED 2/12/2020 MW-4 (NS) MW-3(NS) MW-2 (ND) MW-4R(ND) MW-1(7,770) MW-3R(0.807)N REILLY RDFILLYAW RD ´ DRAWN BY: DRAFT CHECK BY: ENGINEER CHECK BY: APPROVED BY: ESTIMATED ISOCONCENTRATION MAP - BENZENE IN SHALLOW GROUNDWATERSPEEDWAY #6993 670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES DATE: APRIL 2020 JOB NO.: 000R3243.0C GIS NO.: 5G-000R3243.0C-6.1 DRAWING NO.: 6.1 0 20 40 60 8010Feet Legend MONITORING WELL !?Abandoned @A Active ESTIMATED BENZNE ISOCONCENTRATION LINE SITE BOUNDARY STREETS WELL NO.OWNER NAME AND ADDRESSUSER NAME & ADDRESSUSES OF WELLWELL DEPTHWELL CASING DEPTHWELL SCREEN INTERVALDISTANCE & DIRECTION FROM SOURCE AREA1WAINGOLD, RITA205 SE SERVICE RD 237SOUTHERN PINES, NC 28387PRO Car Wash & Detail 648 N. Reilly RoadIrrigation Unknown Unknown Unknown 264 feet S-SE2Not currently in useUnknown Unknown Unknown 766 feet N-NW3Not currently in useUnknown Unknown Unknown 764 feet NWTABLE 5.1WATER-SUPPLY WELL INVENTORY RESULTSSPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC PROJECT NO.: 000R3243.0CHeavner's Acres 703 N. Reilly RoadHEAVNER, CECIL B;CHARLES, O HEAVNER HEIRS JRPO BOX 1266SMITHFIELD, NC 27577 Limited Site Assessment Risk Classification and Land Use Form Part I – Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non-drinking purposes? YES/NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? YES/NO 3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release? YES/NO 4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there is no other source of water supply other than the groundwater)? YES/NO 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? YES/NO If yes, describe. ________________________________________________________________ ________________________________________________________________ ________________________________________________________________ __________________________________________ 6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the environment? YES/NO If yes, describe. ________________________________________________________________ ________________________________________________________________ ____________________________ Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release? YES/NO If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YES/NO 8. Is the source area of the release located within a approved or planned wellhead protection area as defined in 42 USC 300h-7(e)? YES/NO If yes, describe. ________________________________________________________________ ________________________________________________________________ ____________________________ 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of North Carolina” published by the Department in 1985? YES/NO ________ See text Section 5.5. ______________________________________ ________________________________________________________________ ________________________________________________________________ If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water? YES/NO If YES, describe. __________________________________________________ ________________________________________________________________ ________________________________________________________________ 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (See Table 2.) established by the Department? YES/NO Part II - Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? YES/NO Describe. ______________________________________________________________ ______________________________________________________________ ____________________________ 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? YES/NO Describe. ______________________________________________________________ ______________________________________________________________ __________________________ 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YES/NO Describe. The property contains an inactive/closed retail petroleum station.____________ ________________________________________________________________ 4. Do children visit the property? YES/NO Explain. ________________________________________________________________ ________________________________________________________________ ____________________________ Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? YES/NO Explain. ____________________________ 5. Do pavement, buildings, or other structures cap the contaminated soil? YES/NO Describe. _____Pavement___________________________________________________ ________________________________________________________________ ____________________________________ If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? ________________________________________________________________ ________________________________________________________________ ________________________________________________________________ 6. What is the zoning status of the property? ______________________________ ____Limited Commercial (LC)________________________________________ ________________________________________________________________ 7. Is the use of the property likely to change in the next 20 years? YES/NO Explain. __No known redevelopment plans. Property is inactive and will likely be redeveloped at some point in time. ________________________________________________________________ Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source area of the release): 1. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? __170 feet_______________ ________________________________________________ 2. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? ___1,500 feet south (Village Baptist Church)________________________________________________________ 3. What is the zoning status of properties in the surrounding area? _____________ ___Limited Commercial (LC), Single Family Residential (SF10)______________ ________________________________________________________________ ________________________________________________________________ 4. Briefly characterize the use and activities of the land in the surrounding area. __Commercial (north, southeast, southwest), residential (northeast, east, west) ________________________________________________________________ ________________________________________________________________ APPENDIX B MID-ATLANTIC FIELD PROCEDURES Groundwater Sampling Procedures I. Sample Collection A. Monitoring Wells Prior to sample collection, each well is purged of three to five standing well volumes or to dryness to remove stagnant water from the well and well bore in an effort to collect samples that are representative of the water quality in the formation surrounding each well. Purging is performed either with a new, polyethylene bailer dedicated to each well, or with a decontaminated pump. Samples are retrieved from the monitoring well using the dedicated bailer. New nylon string is used on each dedicated bailer, and new nitrile sampling gloves are donned prior to purging and sampling of each well. B. Geoprobe “Screen Point Sampler” The screen point sampler is a “grab” sampling device that is driven into the saturated zone and a surrounding metal sheath is retracted, exposing a screen. Groundwater entering the screen is then drawn to land surface through disposable tubing that is placed through the hollow push rods. The sample is collected from the tubing into the appropriate sampling glassware. C. Water-Supply Wells Water samples are typically collected from the available spigot that is nearest to the well. The water is allowed to run at a high flow from the spigot for approximately 10 to 15 minutes to allow the water in the delivery lines to be purged. The sample flow is then reduced and the samples are collected directly into pre-labeled containers as described below. New nitrile sampling gloves are donned prior to sampling of each well. D. Treatment System Influent/Effluent Samples are typically collected from the influent or effluent of pump-and-treat groundwater remediation systems using designated sampling ports in the influent and effluent water transport lines. The water is typically allowed to run for several seconds to clear potential debris in the sampling port. The sample is then collected directly into sampling containers as described below. New nitrile sampling gloves are donned prior to sample collection. II. Preparation for Laboratory Analysis Groundwater samples are decanted directly into laboratory-prepared, pre-labeled, sampling containers, packed in ice, and shipped to a certified laboratory under chain-of-custody control. Laboratory analyses performed on the samples are specified on the chain-of-custody. APPENDIX C LABORATORY ANALYTICAL REPORTS AND CHAIN- OF-CUSTODY RECORDS FOR GROUNDWATER SAMPLES ANALYTICAL REPORT December 01, 2020 Mid-Atlantic - Speedway NC Sample Delivery Group:L1287678 Samples Received:11/19/2020 Project Number:R1039.02(A) Description:Speedway 6993 Site:6993 Report To:Mr. Troy Holzschuh 409 Rogers View Court Raleigh, NC 27610 Entire Report Reviewed By: December 01, 2020 [Preliminary Report] T. Alan Harvill Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 1 of 22 December 02, 2020 T. Alan Harvill Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 1 of 22 ONE LAB. NATIONWIDE.TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 TRIP BLANK L1287678-01 5 MW-01 L1287678-02 6 Qc: Quality Control Summary 8 Volatile Petroleum Hydrocarbons by Method MADEPV 8 Volatile Organic Compounds (GC/MS) by Method 602MS 9 TPH by Method MADEPE 12 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 13 Gl: Glossary of Terms 17 Al: Accreditations & Locations 18 Sc: Sample Chain of Custody 19 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 2 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 2 of 22 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time TRIP BLANK L1287678-01 GW Gary A Fisher 11/18/20 00:00 11/19/20 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 602MS WG1583242 1 11/27/20 23:37 11/27/20 23:37 JHH Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 602MS WG1584227 1 11/30/20 14:47 11/30/20 14:47 JHH Mt. Juliet, TN Collected by Collected date/time Received date/time MW-01 L1287678-02 GW Gary A Fisher 11/18/20 08:15 11/19/20 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Petroleum Hydrocarbons by Method MADEPV WG1580669 25 11/23/20 12:30 11/23/20 12:30 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 602MS WG1584410 200 12/01/20 01:55 12/01/20 01:55 ACG Mt. Juliet, TN TPH by Method MADEPE WG1579739 1 11/20/20 06:46 11/24/20 05:17 DMG Mt. Juliet, TN TPH by Method MADEPE WG1579739 1 11/20/20 06:46 11/24/20 06:23 DMG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1581306 1 11/24/20 11:09 11/25/20 01:58 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1581306 5 11/24/20 11:09 11/26/20 21:13 SHG Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 3 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 3 of 22 ONE LAB. NATIONWIDE.CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] T. Alan Harvill Project Manager Sample Delivery Group (SDG) Narrative Analyzed from headspace vial. Lab Sample ID Project Sample ID Method L1287678-01 TRIP BLANK 602MS 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 4 of 22 T. Alan Harvill Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 4 of 22 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L1287678 TRIP BLANK Collected date/time: 11/18/20 00:00 Volatile Organic Compounds (GC/MS) by Method 602MS Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Benzene U 0.0941 1.00 1 11/27/2020 23:37 WG1583242 Di-isopropyl ether U 0.105 1.00 1 11/27/2020 23:37 WG1583242 Ethylbenzene U 0.137 1.00 1 11/27/2020 23:37 WG1583242 Methyl tert-butyl ether U 0.101 1.00 1 11/27/2020 23:37 WG1583242 Naphthalene U 1.00 5.00 1 11/30/2020 14:47 WG1584227 Toluene U 0.278 1.00 1 11/27/2020 23:37 WG1583242 m&p-Xylenes U 0.430 2.00 1 11/27/2020 23:37 WG1583242 o-Xylene U 0.174 1.00 1 11/27/2020 23:37 WG1583242 (S) Toluene-d8 97.8 80.0-120 11/27/2020 23:37 WG1583242 (S) Toluene-d8 107 80.0-120 11/30/2020 14:47 WG1584227 (S) 4-Bromofluorobenzene 101 77.0-126 11/27/2020 23:37 WG1583242 (S) 4-Bromofluorobenzene 92.4 77.0-126 11/30/2020 14:47 WG1584227 (S) 1,2-Dichloroethane-d4 96.7 70.0-130 11/27/2020 23:37 WG1583242 (S) 1,2-Dichloroethane-d4 101 70.0-130 11/30/2020 14:47 WG1584227 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 5 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 5 of 22 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L1287678 MW-01 Collected date/time: 11/18/20 08:15 Volatile Petroleum Hydrocarbons by Method MADEPV Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Unadjusted C5-C8 Aliphatics 55600 833 2500 25 11/23/2020 12:30 WG1580669 Unadjusted C9-C12 Aliphatics 26900 833 2500 25 11/23/2020 12:30 WG1580669 Unadjusted C9-C10 Aromatics 6770 833 2500 25 11/23/2020 12:30 WG1580669 Total VPH 89300 833 2500 25 11/23/2020 12:30 WG1580669 (S) 2,5-Dibromotoluene(FID)83.3 70.0-130 11/23/2020 12:30 WG1580669 (S) 2,5-Dibromotoluene(PID)83.2 70.0-130 11/23/2020 12:30 WG1580669 Volatile Organic Compounds (GC/MS) by Method 602MS Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Benzene 8020 18.8 200 200 12/01/2020 01:55 WG1584410 Di-isopropyl ether U 21.0 200 200 12/01/2020 01:55 WG1584410 Ethylbenzene 3360 27.4 200 200 12/01/2020 01:55 WG1584410 Methyl tert-butyl ether U 20.2 200 200 12/01/2020 01:55 WG1584410 Naphthalene 749 J 200 1000 200 12/01/2020 01:55 WG1584410 Toluene 30800 55.6 200 200 12/01/2020 01:55 WG1584410 m&p-Xylenes 11600 86.0 400 200 12/01/2020 01:55 WG1584410 o-Xylene 5870 34.8 200 200 12/01/2020 01:55 WG1584410 (S) Toluene-d8 101 80.0-120 12/01/2020 01:55 WG1584410 (S) 4-Bromofluorobenzene 93.4 77.0-126 12/01/2020 01:55 WG1584410 (S) 1,2-Dichloroethane-d4 99.5 70.0-130 12/01/2020 01:55 WG1584410 Sample Narrative: L1287678-02 WG1584410: Target compounds too high to run at a lower dilution. TPH by Method MADEPE Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Unadjusted C9-C18 Aliphatics 851 33.3 100 1 11/24/2020 05:17 WG1579739 Unadjusted C19-C36 Aliphatics U 33.3 100 1 11/24/2020 05:17 WG1579739 Unadjusted C11-C22 Aromatics 1160 33.3 100 1 11/24/2020 06:23 WG1579739 Unadjusted Total Petroleum Hydrocarbons 2010 33.3 100 1 11/24/2020 06:23 WG1579739 (S) o-Terphenyl 65.0 40.0-140 11/24/2020 06:23 WG1579739 (S) 1-Chloro-octadecane 48.3 40.0-140 11/24/2020 05:17 WG1579739 (S) 2-Fluorobiphenyl 86.3 40.0-140 11/24/2020 06:23 WG1579739 (S) 2-Bromonaphthalene 77.9 40.0-140 11/24/2020 06:23 WG1579739 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,2,4-Trichlorobenzene U 0.0698 10.0 1 11/25/2020 01:58 WG1581306 1,2-Dichlorobenzene U 0.0713 10.0 1 11/25/2020 01:58 WG1581306 1,3-Dichlorobenzene U 0.132 10.0 1 11/25/2020 01:58 WG1581306 1,4-Dichlorobenzene U 0.0942 10.0 1 11/25/2020 01:58 WG1581306 2,4-Dinitrotoluene U 0.0983 10.0 1 11/25/2020 01:58 WG1581306 2,6-Dinitrotoluene U 0.250 10.0 1 11/25/2020 01:58 WG1581306 2-Chloronaphthalene U 0.0648 1.00 1 11/25/2020 01:58 WG1581306 3,3-Dichlorobenzidine U 0.212 10.0 1 11/25/2020 01:58 WG1581306 4-Bromophenyl-phenylether U 0.0877 10.0 1 11/25/2020 01:58 WG1581306 4-Chlorophenyl-phenylether U 0.0926 10.0 1 11/25/2020 01:58 WG1581306 Acenaphthene 0.235 J 0.0886 1.00 1 11/25/2020 01:58 WG1581306 Acenaphthylene U 0.0921 1.00 1 11/25/2020 01:58 WG1581306 Anthracene U 0.0804 1.00 1 11/25/2020 01:58 WG1581306 Benzidine U 3.74 10.0 1 11/25/2020 01:58 WG1581306 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 6 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 6 of 22 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L1287678 MW-01 Collected date/time: 11/18/20 08:15 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Benzo(a)anthracene U 0.199 1.00 1 11/25/2020 01:58 WG1581306 Benzo(a)pyrene U 0.0381 1.00 1 11/25/2020 01:58 WG1581306 Benzo(b)fluoranthene U 0.130 1.00 1 11/25/2020 01:58 WG1581306 Benzo(g,h,i)perylene U 0.121 1.00 1 11/25/2020 01:58 WG1581306 Benzo(k)fluoranthene U 0.120 1.00 1 11/25/2020 01:58 WG1581306 Bis(2-chlorethoxy)methane U 0.116 10.0 1 11/25/2020 01:58 WG1581306 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 11/25/2020 01:58 WG1581306 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 11/25/2020 01:58 WG1581306 Benzylbutyl phthalate U 0.765 3.00 1 11/25/2020 01:58 WG1581306 Chrysene U 0.130 1.00 1 11/25/2020 01:58 WG1581306 Di-n-butyl phthalate U 0.453 3.00 1 11/25/2020 01:58 WG1581306 Di-n-octyl phthalate U 0.932 3.00 1 11/25/2020 01:58 WG1581306 Dibenz(a,h)anthracene U 0.0644 1.00 1 11/25/2020 01:58 WG1581306 Diethyl phthalate U 0.287 3.00 1 11/25/2020 01:58 WG1581306 Dimethyl phthalate U 0.260 3.00 1 11/25/2020 01:58 WG1581306 Fluoranthene U 0.102 1.00 1 11/25/2020 01:58 WG1581306 Fluorene 0.236 J 0.0844 1.00 1 11/25/2020 01:58 WG1581306 Hexachlorobenzene U 0.0755 1.00 1 11/25/2020 01:58 WG1581306 Hexachloro-1,3-butadiene U 0.0968 10.0 1 11/25/2020 01:58 WG1581306 Hexachlorocyclopentadiene U 0.0598 10.0 1 11/25/2020 01:58 WG1581306 Hexachloroethane U 0.127 10.0 1 11/25/2020 01:58 WG1581306 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 11/25/2020 01:58 WG1581306 Isophorone U 0.143 10.0 1 11/25/2020 01:58 WG1581306 n-Nitrosodi-n-propylamine U 0.261 10.0 1 11/25/2020 01:58 WG1581306 n-Nitrosodimethylamine U 0.998 10.0 1 11/25/2020 01:58 WG1581306 n-Nitrosodiphenylamine U 2.37 10.0 1 11/25/2020 01:58 WG1581306 Naphthalene 611 0.795 5.00 5 11/26/2020 21:13 WG1581306 Nitrobenzene U 0.297 10.0 1 11/25/2020 01:58 WG1581306 Phenanthrene 0.120 J 0.112 1.00 1 11/25/2020 01:58 WG1581306 Pyrene U 0.107 1.00 1 11/25/2020 01:58 WG1581306 (S) Nitrobenzene-d5 76.5 15.0-314 11/25/2020 01:58 WG1581306 (S) Nitrobenzene-d5 58.7 15.0-314 11/26/2020 21:13 WG1581306 (S) 2-Fluorobiphenyl 60.3 22.0-127 11/25/2020 01:58 WG1581306 (S) 2-Fluorobiphenyl 69.6 22.0-127 11/26/2020 21:13 WG1581306 (S) p-Terphenyl-d14 69.9 29.0-141 11/25/2020 01:58 WG1581306 (S) p-Terphenyl-d14 81.3 29.0-141 11/26/2020 21:13 WG1581306 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 7 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 7 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1580669 Volatile Petroleum Hydrocarbons by Method MADEPV L1287678-02 Method Blank (MB) (MB) R3597484-3 11/23/20 01:15 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Unadjusted C5-C8 Aliphatics U 33.3 100 Unadjusted C9-C12 Aliphatics U 33.3 100 Unadjusted C9-C10 Aromatics U 33.3 100 Total VPH U 33.3 100 (S) 2,5-Dibromotoluene(FID)82.1 70.0-130 (S) 2,5-Dibromotoluene(PID)81.8 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3597484-1 11/22/20 21:36 • (LCSD) R3597484-2 11/22/20 22:47 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Unadjusted C5-C8 Aliphatics 1200 1050 1170 87.5 97.5 70.0-130 10.8 25 Unadjusted C9-C12 Aliphatics 1400 1400 1330 100 95.0 70.0-130 5.13 25 Unadjusted C9-C10 Aromatics 200 200 195 100 97.5 70.0-130 2.53 25 Total VPH 2800 2650 2700 94.6 96.4 70.0-130 1.87 25 (S) 2,5-Dibromotoluene(FID) 86.5 86.0 70.0-130 (S) 2,5-Dibromotoluene(PID) 88.5 88.5 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 8 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 8 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1583242 Volatile Organic Compounds (GC/MS) by Method 602MS L1287678-01 Method Blank (MB) (MB) R3598497-3 11/27/20 22:25 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Benzene U 0.0941 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 Methyl tert-butyl ether U 0.101 1.00 Toluene U 0.278 1.00 o-Xylene U 0.174 1.00 m&p-Xylene U 0.430 2.00 (S) Toluene-d8 97.2 80.0-120 (S) 4-Bromofluorobenzene 101 77.0-126 (S) 1,2-Dichloroethane-d4 98.4 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3598497-1 11/27/20 20:21 • (LCSD) R3598497-2 11/27/20 20:42 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Benzene 5.00 5.36 5.25 107 105 70.0-123 2.07 20 Di-isopropyl ether 5.00 3.37 3.34 67.4 66.8 58.0-138 0.894 20 Ethylbenzene 5.00 4.55 4.53 91.0 90.6 79.0-123 0.441 20 Methyl tert-butyl ether 5.00 5.16 5.24 103 105 68.0-125 1.54 20 Toluene 5.00 4.58 4.54 91.6 90.8 79.0-120 0.877 20 o-Xylene 5.00 4.46 4.35 89.2 87.0 80.0-122 2.50 20 m&p-Xylene 10.0 9.03 8.97 90.3 89.7 80.0-122 0.667 20 (S) Toluene-d8 95.4 95.3 80.0-120 (S) 4-Bromofluorobenzene 102 101 77.0-126 (S) 1,2-Dichloroethane-d4 96.9 99.5 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 9 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 9 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1584227 Volatile Organic Compounds (GC/MS) by Method 602MS L1287678-01 Method Blank (MB) (MB) R3598677-3 11/30/20 12:41 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Naphthalene U 1.00 5.00 (S) Toluene-d8 103 80.0-120 (S) 4-Bromofluorobenzene 89.1 77.0-126 (S) 1,2-Dichloroethane-d4 99.7 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3598677-1 11/30/20 11:19 • (LCSD) R3598677-2 11/30/20 11:39 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Naphthalene 5.00 3.88 4.02 77.6 80.4 54.0-135 3.54 20 (S) Toluene-d8 105 105 80.0-120 (S) 4-Bromofluorobenzene 92.5 94.7 77.0-126 (S) 1,2-Dichloroethane-d4 95.2 102 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 10 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 10 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1584410 Volatile Organic Compounds (GC/MS) by Method 602MS L1287678-02 Method Blank (MB) (MB) R3598982-3 12/01/20 01:34 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Benzene U 0.0941 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 Toluene U 0.278 1.00 o-Xylene U 0.174 1.00 m&p-Xylenes U 0.430 2.00 (S) Toluene-d8 105 80.0-120 (S) 4-Bromofluorobenzene 92.4 77.0-126 (S) 1,2-Dichloroethane-d4 102 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3598982-1 12/01/20 00:33 • (LCSD) R3598982-2 12/01/20 00:54 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Benzene 5.00 5.03 4.94 101 98.8 70.0-123 1.81 20 Di-isopropyl ether 5.00 3.62 3.72 72.4 74.4 58.0-138 2.72 20 Ethylbenzene 5.00 4.94 5.14 98.8 103 79.0-123 3.97 20 Methyl tert-butyl ether 5.00 4.82 5.19 96.4 104 68.0-125 7.39 20 Naphthalene 5.00 3.99 4.37 79.8 87.4 54.0-135 9.09 20 Toluene 5.00 5.26 5.40 105 108 79.0-120 2.63 20 o-Xylene 5.00 4.78 4.79 95.6 95.8 80.0-122 0.209 20 m&p-Xylenes 10.0 9.85 10.0 98.5 100 80.0-122 1.51 20 (S) Toluene-d8 103 103 80.0-120 (S) 4-Bromofluorobenzene 91.6 89.1 77.0-126 (S) 1,2-Dichloroethane-d4 101 97.4 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 11 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 11 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1579739 TPH by Method MADEPE L1287678-02 Method Blank (MB) (MB) R3596725-1 11/24/20 00:53 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Unadjusted C9-C18 Aliphatics U 33.3 100 Unadjusted C19-C36 Aliphatics U 33.3 100 (S) 1-Chloro-octadecane 79.1 40.0-140 Method Blank (MB) (MB) R3596725-4 11/24/20 01:59 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Unadjusted C11-C22 Aromatics U 33.3 100 (S) o-Terphenyl 78.3 40.0-140 (S) 2-Fluorobiphenyl 83.1 40.0-140 (S) 2-Bromonaphthalene 79.1 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3596725-2 11/24/20 01:15 • (LCSD) R3596725-3 11/24/20 01:37 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Unadjusted C9-C18 Aliphatics 600 317 314 52.8 52.3 40.0-140 0.951 25 Unadjusted C19-C36 Aliphatics 800 494 481 61.7 60.1 40.0-140 2.67 25 (S) 1-Chloro-octadecane 71.1 70.7 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3596725-5 11/24/20 02:21 • (LCSD) R3596725-6 11/24/20 02:43 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Unadjusted C11-C22 Aromatics 1700 1430 1130 84.1 66.5 40.0-140 23.4 25 (S) o-Terphenyl 85.4 66.4 40.0-140 (S) 2-Fluorobiphenyl 93.0 73.0 40.0-140 (S) 2-Bromonaphthalene 83.3 67.8 40.0-140 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 12 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 12 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1581306 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1287678-02 Method Blank (MB) (MB) R3597387-2 11/24/20 22:54 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acenaphthene U 0.0886 1.00 Acenaphthylene U 0.0921 1.00 Anthracene U 0.0804 1.00 Benzidine U 3.74 10.0 Benzo(a)anthracene U 0.199 1.00 Benzo(b)fluoranthene U 0.130 1.00 Benzo(k)fluoranthene U 0.120 1.00 Benzo(g,h,i)perylene U 0.121 1.00 Benzo(a)pyrene U 0.0381 1.00 Bis(2-chlorethoxy)methane U 0.116 10.0 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 4-Bromophenyl-phenylether U 0.0877 10.0 2-Chloronaphthalene U 0.0648 1.00 4-Chlorophenyl-phenylether U 0.0926 10.0 Chrysene U 0.130 1.00 Dibenz(a,h)anthracene U 0.0644 1.00 1,2-Dichlorobenzene U 0.0713 10.0 1,3-Dichlorobenzene U 0.132 10.0 1,4-Dichlorobenzene U 0.0942 10.0 3,3-Dichlorobenzidine U 0.212 10.0 2,4-Dinitrotoluene U 0.0983 10.0 2,6-Dinitrotoluene U 0.250 10.0 Fluoranthene U 0.102 1.00 Fluorene U 0.0844 1.00 Hexachlorobenzene U 0.0755 1.00 Hexachloro-1,3-butadiene U 0.0968 10.0 Hexachlorocyclopentadiene U 0.0598 10.0 Hexachloroethane U 0.127 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.143 10.0 Naphthalene U 0.159 1.00 Nitrobenzene U 0.297 10.0 n-Nitrosodimethylamine U 0.998 10.0 n-Nitrosodiphenylamine U 2.37 10.0 n-Nitrosodi-n-propylamine U 0.261 10.0 Phenanthrene U 0.112 1.00 Benzylbutyl phthalate U 0.765 3.00 Bis(2-ethylhexyl)phthalate U 0.895 3.00 Di-n-butyl phthalate U 0.453 3.00 Diethyl phthalate U 0.287 3.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 13 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 13 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1581306 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1287678-02 Method Blank (MB) (MB) R3597387-2 11/24/20 22:54 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Dimethyl phthalate U 0.260 3.00 Di-n-octyl phthalate U 0.932 3.00 Pyrene U 0.107 1.00 1,2,4-Trichlorobenzene U 0.0698 10.0 (S) Nitrobenzene-d5 59.4 15.0-314 (S) 2-Fluorobiphenyl 67.6 22.0-127 (S) p-Terphenyl-d14 71.4 29.0-141 Laboratory Control Sample (LCS) (LCS) R3597387-1 11/24/20 22:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acenaphthene 50.0 29.6 59.2 47.0-145 Acenaphthylene 50.0 30.8 61.6 33.0-145 Anthracene 50.0 33.2 66.4 27.0-133 Benzidine 100 25.2 25.2 1.00-120 Benzo(a)anthracene 50.0 35.9 71.8 33.0-143 Benzo(b)fluoranthene 50.0 34.9 69.8 24.0-159 Benzo(k)fluoranthene 50.0 36.8 73.6 11.0-162 Benzo(g,h,i)perylene 50.0 33.8 67.6 1.00-219 Benzo(a)pyrene 50.0 36.4 72.8 17.0-163 Bis(2-chlorethoxy)methane 50.0 29.5 59.0 1.00-219 2,2-Oxybis(1-Chloropropane)50.0 33.1 66.2 36.0-166 4-Bromophenyl-phenylether 50.0 33.9 67.8 53.0-127 2-Chloronaphthalene 50.0 30.0 60.0 60.0-120 4-Chlorophenyl-phenylether 50.0 31.7 63.4 25.0-158 Chrysene 50.0 34.6 69.2 17.0-168 Dibenz(a,h)anthracene 50.0 33.5 67.0 1.00-227 1,2-Dichlorobenzene 50.0 31.7 63.4 27.0-120 1,3-Dichlorobenzene 50.0 30.7 61.4 26.0-120 1,4-Dichlorobenzene 50.0 29.9 59.8 26.0-120 3,3-Dichlorobenzidine 100 67.0 67.0 1.00-262 2,4-Dinitrotoluene 50.0 32.4 64.8 39.0-139 2,6-Dinitrotoluene 50.0 33.0 66.0 50.0-158 Fluoranthene 50.0 35.1 70.2 26.0-137 Fluorene 50.0 31.2 62.4 59.0-121 Hexachlorobenzene 50.0 35.9 71.8 1.00-152 Hexachloro-1,3-butadiene 50.0 27.7 55.4 24.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 14 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 14 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1581306 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1287678-02 Laboratory Control Sample (LCS) (LCS) R3597387-1 11/24/20 22:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Hexachlorocyclopentadiene 50.0 15.5 31.0 10.0-120 Hexachloroethane 50.0 29.6 59.2 40.0-120 Indeno(1,2,3-cd)pyrene 50.0 32.6 65.2 1.00-171 Isophorone 50.0 30.3 60.6 21.0-196 Naphthalene 50.0 26.6 53.2 21.0-133 Nitrobenzene 50.0 26.0 52.0 35.0-180 n-Nitrosodimethylamine 50.0 21.0 42.0 10.0-120 n-Nitrosodiphenylamine 50.0 31.7 63.4 44.0-120 n-Nitrosodi-n-propylamine 50.0 38.3 76.6 1.00-230 Phenanthrene 50.0 35.0 70.0 54.0-120 Benzylbutyl phthalate 50.0 37.2 74.4 1.00-152 Bis(2-ethylhexyl)phthalate 50.0 36.9 73.8 8.00-158 Di-n-butyl phthalate 50.0 36.0 72.0 1.00-120 Diethyl phthalate 50.0 34.3 68.6 1.00-120 Dimethyl phthalate 50.0 33.5 67.0 1.00-120 Di-n-octyl phthalate 50.0 32.8 65.6 4.00-146 Pyrene 50.0 36.8 73.6 52.0-120 1,2,4-Trichlorobenzene 50.0 27.2 54.4 44.0-142 (S) Nitrobenzene-d5 53.7 15.0-314 (S) 2-Fluorobiphenyl 63.5 22.0-127 (S) p-Terphenyl-d14 65.8 29.0-141 L1287927-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1287927-08 11/24/20 23:36 • (MS) R3597387-3 11/24/20 23:57 • (MSD) R3597387-4 11/25/20 00:18 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Acenaphthene 50.0 U 31.7 31.4 63.4 62.8 1 47.0-145 0.951 48 Acenaphthylene 50.0 U 33.1 32.8 66.2 65.6 1 33.0-145 0.910 74 Anthracene 50.0 U 36.1 35.8 72.2 71.6 1 27.0-133 0.834 66 Benzidine 100 U 24.3 16.0 24.3 16.0 1 1.00-120 J3 41.2 40 Benzo(a)anthracene 50.0 U 36.4 36.5 72.8 73.0 1 33.0-143 0.274 53 Benzo(b)fluoranthene 50.0 U 34.6 34.9 69.2 69.8 1 24.0-159 0.863 71 Benzo(k)fluoranthene 50.0 U 37.2 36.0 74.4 72.0 1 11.0-162 3.28 63 Benzo(g,h,i)perylene 50.0 U 36.0 35.8 72.0 71.6 1 1.00-219 0.557 97 Benzo(a)pyrene 50.0 U 37.4 36.7 74.8 73.4 1 17.0-163 1.89 72 Bis(2-chlorethoxy)methane 50.0 U 32.7 32.6 65.4 65.2 1 33.0-184 0.306 54 2,2-Oxybis(1-Chloropropane)50.0 U 35.6 32.9 71.2 65.8 1 36.0-166 7.88 76 4-Bromophenyl-phenylether 50.0 U 35.9 34.6 71.8 69.2 1 53.0-127 3.69 43 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 15 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 15 of 22 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1581306 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1287678-02 L1287927-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1287927-08 11/24/20 23:36 • (MS) R3597387-3 11/24/20 23:57 • (MSD) R3597387-4 11/25/20 00:18 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% 2-Chloronaphthalene 50.0 U 33.2 32.1 66.4 64.2 1 60.0-120 3.37 24 4-Chlorophenyl-phenylether 50.0 U 34.4 33.3 68.8 66.6 1 25.0-158 3.25 61 Chrysene 50.0 U 34.9 34.7 69.8 69.4 1 17.0-168 0.575 87 Dibenz(a,h)anthracene 50.0 U 37.1 36.3 74.2 72.6 1 1.00-227 2.18 126 1,2-Dichlorobenzene 50.0 U 33.4 31.7 66.8 63.4 1 14.0-125 5.22 24 1,3-Dichlorobenzene 50.0 U 32.9 30.6 65.8 61.2 1 12.0-123 7.24 22 1,4-Dichlorobenzene 50.0 U 32.7 30.7 65.4 61.4 1 12.0-125 6.31 23 3,3-Dichlorobenzidine 100 U 74.7 74.2 74.7 74.2 1 1.00-262 0.672 108 2,4-Dinitrotoluene 50.0 U 34.5 35.3 69.0 70.6 1 39.0-139 2.29 42 2,6-Dinitrotoluene 50.0 U 35.1 35.2 70.2 70.4 1 50.0-158 0.284 48 Fluoranthene 50.0 U 35.6 34.5 71.2 69.0 1 26.0-137 3.14 66 Fluorene 50.0 U 33.9 33.7 67.8 67.4 1 59.0-121 0.592 38 Hexachlorobenzene 50.0 U 36.4 35.3 72.8 70.6 1 1.00-152 3.07 55 Hexachloro-1,3-butadiene 50.0 U 29.2 28.2 58.4 56.4 1 24.0-120 3.48 62 Hexachlorocyclopentadiene 50.0 U 22.2 21.4 44.4 42.8 1 10.0-146 3.67 34 Hexachloroethane 50.0 U 33.3 31.1 66.6 62.2 1 40.0-120 6.83 52 Indeno(1,2,3-cd)pyrene 50.0 U 35.8 34.5 71.6 69.0 1 1.00-171 3.70 99 Isophorone 50.0 U 31.5 31.9 63.0 63.8 1 21.0-196 1.26 93 Naphthalene 50.0 0.190 29.3 28.1 58.2 55.8 1 21.0-133 4.18 65 Nitrobenzene 50.0 U 30.6 29.8 61.2 59.6 1 35.0-180 2.65 62 n-Nitrosodimethylamine 50.0 U 20.5 20.0 41.0 40.0 1 10.0-120 2.47 40 n-Nitrosodiphenylamine 50.0 U 36.4 33.7 72.8 67.4 1 16.0-160 7.70 28 n-Nitrosodi-n-propylamine 50.0 U 38.6 37.8 77.2 75.6 1 1.00-230 2.09 87 Phenanthrene 50.0 U 35.9 34.5 71.8 69.0 1 54.0-120 3.98 39 Benzylbutyl phthalate 50.0 U 35.9 35.9 71.8 71.8 1 1.00-152 0.000 60 Bis(2-ethylhexyl)phthalate 50.0 U 34.8 35.3 69.6 70.6 1 8.00-158 1.43 82 Di-n-butyl phthalate 50.0 U 35.7 34.7 71.4 69.4 1 1.00-120 2.84 47 Diethyl phthalate 50.0 0.375 36.0 36.4 71.3 72.1 1 1.00-120 1.10 100 Dimethyl phthalate 50.0 U 36.0 35.4 72.0 70.8 1 1.00-120 1.68 183 Di-n-octyl phthalate 50.0 U 32.5 32.8 65.0 65.6 1 4.00-146 0.919 69 Pyrene 50.0 U 35.5 36.5 71.0 73.0 1 52.0-120 2.78 49 1,2,4-Trichlorobenzene 50.0 U 29.5 28.3 59.0 56.6 1 44.0-142 4.15 50 (S) Nitrobenzene-d5 62.4 59.4 15.0-314 (S) 2-Fluorobiphenyl 68.7 69.4 22.0-127 (S) p-Terphenyl-d14 67.2 68.1 29.0-141 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 16 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 16 of 22 ONE LAB. NATIONWIDE.GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. RDL Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 17 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 17 of 22 ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. State Accreditations Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹n/a Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶90010 South Carolina 84004 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana ¹LA180010 Texas T104704245-18-15 Maine TN0002 Texas ⁵LAB0152 Maryland 324 Utah TN00003 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA Third Party Federal Accreditations A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/01/20 18:14 18 of 22 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Mid-Atlantic - Speedway NC R1039.02(A)L1287678 12/02/20 08:13 18 of 22 Page 1 of 1 TURN AROUND TIME STANDARD Chain-of-Custody-Record Speedway Project Information Speedway Store #: C210006993 Facility ID 0000015515 Address:670 N Reilly Rd City:Fayetteville State:NC Phone #:Fax #: Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY** AFE #:190112 Work Order #:1103701744 COC ID # 00054238 Lab Information Lab:Pace Analytical Services (TN) Consultant:Mid-Atlantic Associates, Inc. - Charlotte, NC Project Mgr: Troy Holzschuh Address:1125 E Moorehead Street Charlotte, NC 28204-2849 Phone #:Fax #: Sampler:Gary Fisher Shipped:FedExp Tracking #:received Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks MW-01 11/18/2020 08:15am W 10 40 ML AMBER VOA HCL VPH MADEP VPH VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602 100 ML AMBER GLASS NONE SVOCs/BNA/TICS 625 1LG HCL EPH MADEP EPH TRIP BLANK 11/18/2020 12:00am W 1 VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602 Relinquished by:Date Time Received by:Date Time Relinquished by:Date Time Received by laboratory:Date Time Special Reporting Requirements:Lab Notes:Temp Speedway LLC.1/1 https://www.speedway-ids.com Chain of Custody Analysis to be Performed Chain-of-Custody-Record COC ID # 54238 Printed: 01/16/2021 Analysis Name: BTEX/MTBE/IPE/Naph ( Water ) Analysis Description / Method:EPA Modified 602 / 602 Container Type / Preservative:VOA - 40 MILL / HCL Analytes: Benzene ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Methyl tert butyl ether ug/L, Naphthalene ug/L, Toluene ug/L, m,p-Xylene ug/L, o-Xylene ug/L Analysis Name: EPH ( Water ) Analysis Description / Method:Extractable Petroleum Hydrocarbons / MADEP EPH Container Type / Preservative:1LG / HCL Analytes: C11-C22 Aromatics ug/L, C19-C36 Aliphatics ug/L, C9-C18 Aliphatics ug/L, Extractable Petroleum Hydrocarbons ug/L Analysis Name: SVOCs/BNA/TICS ( Water ) Analysis Description / Method:Water / 625 Container Type / Preservative:100 ML AMBER GLASS / NONE Analytes: 1,2,4-Trichlorobenzene ug/L, 1,2-Dichlorobenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,4-Dichlorobenzene ug/L, 2,2'-oxybis(1-Chloropropane) ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L, 3,3'-Dichlorobenzidine ug/L, 4-Bromophenyl phenyl ether ug/L, 4-Chlorophenyl phenyl ether ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzidine ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene ug/L, Benzo(b)fluoranthene ug/L, Benzo(g,h,I)perylene ug/L, Benzo(k)fluoranthene ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl phthalate ug/L, Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenz(a,h)anthracene ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L, Hexachlorobenzene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Hexchloro-1,3-butadiene ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodimethylamine ug/L, N-Nitrosodiphenylamine ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Phenanthrene ug/L, Pyrene ug/L Analysis Name: VPH ( Water ) Analysis Description / Method:Volatile Petroleum Hydrocarbons / MADEP VPH Speedway LLC.1/2 https://www.speedway-ids.com Chain of Custody Analysis to be Performed Chain-of-Custody-Record COC ID # 54238 Printed: 01/16/2021 Container Type / Preservative:40 ML AMBER VOA / HCL Analytes: C5-C8 Aliphatics ug/L, C9-C10 Aromatics ug/L, C9-C12 Aliphatics ug/L, Total Volatile Hydrocarbons ug/L Speedway LLC.2/2 https://www.speedway-ids.com