FA-7962_42202_CA_LSA_20200417_PhaseIILSA

An Equal Opportunity Employer

April 17, 2020
Ms. Sarah Brown North Carolina Department of Environmental Quality
Division of Waste Management – UST Section
225 Green Street, Suite 714 Fayetteville, North Carolina 28301-5095
Subject: PHASE II LIMITED SITE ASSESSMENT REPORT SPEEDWAY 6993 670 NORTH REILLY ROAD
FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA DWM INCIDENT NO.: 42202
FACILITY ID NO.: 00-0-0015515 MID-ATLANTIC JOB NO.: 000R3243.0C Dear Ms. Brown:
Speedway LLC is pleased to present this report of environmental services for the Speedway
6993 facility located at 670 North Reilly Road, Fayetteville, North Carolina. The attached report documents the recent Limited Site Assessment activities. If you have any questions or need additional information, please feel free to contact me at (919)
516-8069 or Trey Marchant with Mid-Atlantic Associates, Inc. at [phone].
Sincerely, SPEEDWAY LLC

Charles A. Chiara Environmental Representative

Speedway LLC Speedway Office P.O. Box 1500 Springfield, OH 45501 Telephone [phone]

PHASE II LIMITED SITE ASSESSMENT REPORT SPEEDWAY #6993
670 NORTH REILLY ROAD, FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA
INCIDENT NO.: 42202 FACILITY I.D. NO.: 0000015515
MID-ATLANTIC JOB NO. 000R3243.0E

Risk Classification: Unassigned
Land Use: Unassigned
Latitude: N 35.099832 Longitude: W 78.010845
Date Discovered: March 1, 2019
Estimated Quantity of Release: Unknown
Cause/Source of Release: Diesel Dispenser

Prepared For:

Mr. Charles Chiara
Environmental Representative
Speedway, LLC
500 Speedway Dr.
Enon, OH 45323

Prepared By:

Mid-Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610

April 17, 2020

PHASE II LIMITED SITE ASSESSMENT REPORT A. Site Information
1. Site Identification
 Date of Report: April 17, 2020
 Facility I.D.: 15515 UST Incident Number (if known): 42202
 Site Name: Speedway 6993
 Site Street Address: 670 N. Reilly Road
 City/Town: Fayetteville Zip Code: 28303 County: Cumberland County
 Description of Geographical Data Point (e.g. diesel fill port): Property Centerpoint
 Location method (GPS, topographical map, other): Google Earth
 Latitude (decimal degrees): N 35.099832 Longitude (decimal degrees): W 78.010845

2. Information about Contacts Associated with the Release (Addresses must include street, city, state, zip
code and mailing address, if different).
 UST Owner: Speedway, LLC
 Address: 500 Speedway Drive, Enon, OH 45323 Phone: [phone]

 UST Operator: Same as UST Owner
 Address: Phone:
 Property Owner: Same as UST Owner
 Address: Same as UST Owner Phone: Same
 Property Occupant: Same as UST Owner
 Address: Phone:
 Consultant/Contractor: Mid-Atlantic Associates, Inc.
 Address: 409 Rogers View Court, Raleigh, NC 27610 Phone: [phone]
 Analytical Laboratory: Pace National State Certification No. 402
 Address: 12065 Lebanon Road, Mt. Juliet, TN 37122 Phone: [phone]

3. Information about Release:
 Date Discovered: March 1, 2019
 Estimated Quantity of Release: Unknown
 Cause of Release: Unknown
 Source of Release (e.g. Dispenser/Piping/UST): Diesel Dispenser
 Sizes and Contents of UST(s) (or other containment from which the release occurred): Three
10,000-gallon USTs containing regular unleaded gasoline, premium unleaded gasoline, and diesel.
One 6,000-gallon UST containing kerosene

4. Certification (The title page must display the seal and signature of the certifying P.E. or L.G. and
the name and certification number of the company or corporation, if applicable [See 15A NCAC
2L.0103(e)].)

I, Raymond S. Marchant, III , a Professional Engineer/Licensed
Geologist (circle one) for Mid-Atlantic Associates, Inc. (firm or company of employment), do
certify that the information contained in this report is correct and accurate to the best of my knowledge.
(Please Affix Seal and Signature)

Mid-Atlantic Associates, Inc. (Name of Company or Corporation) is licensed to practice geology/engineering
(circle one or both) in North Carolina. The certification number of the company or corporation is C-186 and F-0967

PHASE II LIMITED SITE ASSESSMENT REPORT
SPEEDWAY 6993 670 NORTH REILLY ROAD,
FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA INCIDENT NO.: 42202
FACILITY I.D. NO.: 0000015515 MID-ATLANTIC JOB NO. 000R3243.0E
April 17, 2020
Prepared For: Prepared By:
Mr. Charles Chiara MID-ATLANTIC ASSOCIATES, INC. Environmental Representative Speedway, LLC 500 Speedway Dr. Enon, OH 45323 John L. Sherrill, P.G. Project Geologist
Raymond S. Marchant, III, P.G.
Principal Geologist

TABLE OF CONTENTS 1.0 GENERAL INFORMATION ....................................................................................... 1 1.1 Introduction .................................................................................................. 1
1.2 Laboratory ................................................................................................... 1 1.3 Drilling Contractor ........................................................................................ 1
2.0 SITE HISTORY.......................................................................................................... 2
2.1 UST Information .......................................................................................... 2 2.2 UST System Owners ................................................................................... 2
3.0 SITE GEOLOGY ....................................................................................................... 2

4.0 RISK CLASSIFICATION ........................................................................................... 2 5.0 RECEPTOR INFORMATION .................................................................................... 3 5.1 Water-Supply Wells ..................................................................................... 3
5.2 Public Water Supplies .................................................................................. 4 5.3 Surface Water .............................................................................................. 4
5.4 Wellhead Protection Areas .......................................................................... 4 5.5 Deep Aquifers in the Coastal Plain Physiographic Region ........................... 4
5.6 Subsurface Structures ................................................................................. 5 5.7 Land Use ..................................................................................................... 5
5.8 Property Owners and Occupants ................................................................. 5
6.0 SUMMARY OF FIELD ACTIVITIES .......................................................................... 5 6.1 Soil Boring and Monitoring Well Installation ................................................. 5
6.2 Soil Sample Collection ................................................................................. 6 6.3 Liquid Level Measurements ......................................................................... 6
6.4 Groundwater Sample Collection .................................................................. 6 7.0 LABORATORY ANALYTICAL RESULTS ................................................................ 6 8.0 SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS .................................... 7
DRAWINGS
Drawing 1.1 Topographic Site Map
Drawing 1.2 Site Map Drawing 1.3 Monitoring Well Location Map
Drawing 5.1 Receptor Survey Map Drawing 5.2 Adjacent Properties Map
Drawing 6.1 Estimated Isoconcentration Map – Benzene in Shallow Groundwater

TABLE OF CONTENTS (Continued)
TABLES
Table 5.1 Water-Supply Well Inventory Results
Table 6.1 Groundwater Elevation Data Table 7.1 Summary of Chemical Constituents Detected in Soil
Table 7.2 Summary of Chemical Constituents Detected in Groundwater
APPENDICES
Appendix A Limited Site Assessment Risk Classification and Land Use Form
Appendix B Adjacent Property Owner Data Appendix C Soil Boring Logs and Well Construction Records Appendix D Laboratory Analytical Reports and Chain-of-Custody Records
Appendix E Mid-Atlantic Field Procedures

1.0 GENERAL INFORMATION
1.1 Introduction
The site is the Speedway Store #6993 located at 670 N. Reilly Road, Fayetteville, Cumberland
County, North Carolina (Drawings 1.1 & 1.2). The site is a closed petroleum retail facility and convenience store and contained four underground storage tanks (USTs) total: three 10,000 gallon
capacity USTs (regular gasoline, premium gasoline, and diesel fuel) and one 6,000 gallon capacity UST (kerosene). The three 10,000 gallon capacity USTs were located to the north of the building
and dispensers, and the one 6,000 gallon capacity UST was located to the east. The site topographic location is shown on Drawing 1.1, and the site drawing with the approximate locations of the USTs is
presented as Drawing 1.2.
UST closure activities were performed in February 2019. During the tank closure, petroleum impact was identified in the overburden of the three 10,000 gallon tanks. The impacted material was segregated
and disposed of offsite at an approved facility. On February 28, 2019, diesel fuel contamination was encountered in the vicinity of the diesel dispenser during the UST closure activities. Initial soil sampling
confirmed the release and initial abatement measure were taken. Approximately one ton of impacted
soil was excavated and disposed of at the A&D Environmental (A&D) facility in High Point, North
Carolina. The extent of the excavation was limited due to the structural concerns of undermining the canopy. Drawing 1.3 shows the location of the former UST basins, product lines, diesel dispenser
(source area), and monitoring wells.
A 24-Hour Release and UST Leak Reporting Form was submitted to the North Carolina Department of
Environmental Quality (NCDEQ) by Mid-Atlantic on March 1, 2019. A UST Closure and Initial
Abatement Action Report was submitted on June 3, 2019. The NCDEQ issued a Notice of Regulatory Requirements on June 24, 2019 requiring the completion of a Limited Site Assessment (LSA).
The opinions included herein are based on our experience and the information obtained during the
study. This report is based on limited observations made on the dates noted using the procedures
described herein. If additional information becomes available, we request the opportunity to review the
information, reassess the potential environmental concerns and modify our conclusions and recommendations, if appropriate.
1.2 Laboratory
Pace Analytical
12065 Lebanon Road Mt. Juliet, Tennessee 37122 [phone]
N.C. Certification No. 375 Contact: Mr. Alan Harvill

1.3 Drilling Contractor Geologic Exploration, Inc. 176 Commerce Boulevard
Statesville, North Carolina 28625 [phone]
N.C. Drillers Registration No. A4252
Contact: Mr. Jason Mantak
Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 2
Fayetteville, North Carolina

2.0 SITE HISTORY
The following sections summarize the UST systems currently or previously located at the site along
with current and previous owners and operators of the UST system(s).
2.1 UST Information
The following table summarizes the UST information.
UST ID Number Previous Contents Capacity (Gallons) Tank Dimensions Construction Details Date Installed Status of UST
Release
Associated with
System
1 Gasoline 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 No
2 Gasoline 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 No
3 Diesel 10,000 Approximately 10’ x 17’ Single-walled steel 1979 Removed 2/27/19 Yes
4 Kerosene 6,000 Approximately 8’ x 16’ Single-walled steel 1979 Removed 2/27/19 No

2.2 UST System Owners
According to the Moore County, North Carolina GIS mapping service, the current property owner of the subject site is listed as WilcoHess, LLC. On October 1, 2014, Speedway, LLC purchased the site from
WilcoHess.
3.0 SITE GEOLOGY
According to the map titled Geology of North Carolina (1985), prepared by the North Carolina
Geological Survey Section of the NCDEQ, the subject site is located in the Middendorf Formation (Geologic Unit: Km). The site appears to be located in an area of “sand, sandstone, and mudstone,
gray to pale gray with an orange cast, mottled; clay balls and iron-cemented concretions common, beds laterally discontinuous, cross bedding common”.

4.0 RISK CLASSIFICATION
Three categories (high, intermediate and low) of risk posed by a discharge or release at a site have been established under 15A NCAC 2L .0406. Sites classified as high risk must be remediated to the
North Carolina Groundwater Quality Standards (NCGQS), or as closely thereto as economically and
Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 3
Fayetteville, North Carolina

technologically feasible. Sites classified as intermediate risk must be remediated to gross
contamination levels (GCLs). GCLs are defined as levels of groundwater contamination for any contaminant except ethylene dibromide, benzene, and aliphatic and aromatic carbon fraction classes
that exceed 50 percent of the solubility of the contaminant at 25 degrees Celsius or 1,000 times the groundwater quality standard or interim standard, whichever is lower. For ethylene dibromide and
benzene, GCLs are established at 1,000 times the federal drinking water standard set out in 40 CFR 141. Aliphatic and aromatic carbon fraction classes are excluded from GCLs. A low risk classification
means that no further assessment or corrective action of groundwater is required.
In order for the State to classify the level of risk to human health and the environment posed by a discharge or release at the site, Mid-Atlantic conducted a receptor survey of the surrounding areas
and completed a “Limited Site Assessment Risk Classification and Land Use Form” (Appendix A). Information was collected regarding groundwater/surface water/vapor impacts, land use and other
information outlined in 15A NCAC 2L .0406 and summarized in the following section of the report.

5.0 RECEPTOR INFORMATION
5.1 Water-Supply Wells
Mid-Atlantic personnel performed an area reconnaissance survey to determine the location of water-
supply wells within a 1,500-foot radius search area of the source area of the release (Drawing 5.1).
Water supply well survey letters were sent via U.S. Mail to all property owners within a 1000-foot radius
of the release area. The survey letters explained the purpose of the investigation and requested a return phone call to Mid-Atlantic in the event that a water-supply well (either in-use or not in-use) was located
on the property. Properties located within 500 feet of the source area of the release also received a “Water Supply Well Information Survey” form to be completed by the property owner and returned to
Mid-Atlantic. In addition, a visual survey was conducted to locate water meters and well houses, as well
as determining the land use in the immediate area of the release.
The water-supply wells identified within the 1,500 foot search radius from the source area of the release
are summarized as follows:
Within 250 feet: No water-supply wells identified
250 to 1,000 feet: One water-supply well identified, not used for drinking; two water-supply wells identified, reportedly not in use 1,000 to 1,500 feet: No water-supply wells identified
Three water-supply wells were observed within 1,500 feet of the release area during the area
reconnaissance. Mid-Atlantic spoke with the owner of Pro Carwash & Detail located at 648 N. Reilly
Road regarding the onsite water supply well. He said that the well is used for irrigation only and is not used for drinking water. Mid-Atlantic used GIS software to measure the distance from the diesel dispenser to the water supply well, and determined that the well is located 264 feet from the source
area. The property is connected to city water. Mid-Atlantic spoke with Mr. Heavner, the property owner of the two water supply wells located at 735 N Reilly Road, and he indicated that the wells are
not currently in use and have been out of service for a long time. Both properties are connected to
city water. Water supply well information is provided in Table 5.1.
Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 4
Fayetteville, North Carolina

It should be noted that Mid-Atlantic received four Water Supply Well Surveys returned by mail. In
each case, the property owners indicated that their water was supplied by the City of Fayetteville’s Public Water System.
5.2 Public Water Supplies
Mid-Atlantic telephoned the Fayetteville Public Works Commission (PWC) Water Resources
Engineering Department to verify that the municipal water-supply system is available to all the properties within the 1,500-foot radius search area of the source area of the release. Ms. Liz Vasser of
the PWC stated that the area surrounding the site is serviced by the municipal water-supply system.
5.3 Surface Water
According to the USGS topographic quadrangle map of Cliffdale, North Carolina (Drawing 1.1), the nearest surface water body is Persimmon Creek, located approximately 2,770 feet to the northeast of
the source area of the release.
5.4 Wellhead Protection Areas
According to NCDEQ’s web site (https://www.arcgis.com/home/webmap/viewer.html?webmap= 7492e0fe11874ccca699679d03bc0751) updated on October 27, 2016, the subject site is not located
within an approved wellhead protection area.

5.5 Deep Aquifers in the Coastal Plain Physiographic Region
According to the map titled Geology of North Carolina (1985), prepared by the North Carolina Geological Survey Section of the NCDEQ, the subject site is located in the Middendorf Formation
(Geologic Unit: Km) of the Coastal Plain physiographic region. The site appears to be located in an area
of “Sand, sandstone, and mudstone, gray to pale gray with an orange cast, mottled; clay balls and iron-
cemented concretions common, beds laterally discontinuous, cross-bedding common”. According to the USGS (U.S. Geological Survey Professional Paper 1404-I), this unit, which is composed mostly of sand,
is overlain by the Black Creek confining unit, which is composed mostly of clay. The confining unit in the Sand Hills area is reported to be approximately 10 feet thick, and may be cut by stream erosion so that
there is direct hydraulic connection to the Black Creek aquifer from the overlying units.
Based on the available data, it is not possible to demonstrate the lack of potential impact to a deeper aquifer. Vertical groundwater flow direction beneath the site has not been determined. Bedrock was not
encountered at the site when drilling to 40 feet, and mostly sandy material was encountered. Based on the soil types encountered, it does not appear that a confining layer was encountered. However, MW-1
and MW-2 were set to depths of 22 feet BLS, while MW-3R and MW-4R were set to 40 feet BLS. MW-3
and MW-4 were initially set to 22 feet BLS, but did not produce any water. Mid-Atlantic suspects that MW-1 and MW-2 may be set in a perched zone and/or hydraulically separated from the deeper surficial aquifer that MW-3R and MW-4R were set in. Although groundwater flow direction could not be
established, it does not appear that the contamination has migrated vertically into the deeper surficial aquifer at this time.

Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 5
Fayetteville, North Carolina

5.6 Subsurface Structures
During the reconnaissance survey, subsurface utilities were identified at the subject site and in the area surrounding the site. No basements were identified in the receptor survey.
5.7 Land Use
The site is a closed petroleum sales and convenience market and contains typical store facilities,
petroleum dispensers, and a car wash. Surrounding properties to the north, east, and south are predominantly commercial and retail enterprises with the western properties being predominantly
residential. A listing of adjacent property owners is provided in Appendix B, and these properties are shown on Drawing 5.2. The zoning of the properties in the area is a mixture of Residential, and
Commercial Districts.
5.8 Property Owners and Occupants
The property is owned by WilcoHess, LLC/Speedway, LLC, and the facility is closed with no current occupants.

6.0 SUMMARY OF FIELD ACTIVITIES

A total of six monitoring wells (MW-1 through MW-4, and MW-3R and MW-4R) were installed in the vicinity of the source area of the release in accordance with 15A NCAC 2C .0100. The wells were
placed in the vicinity of the diesel dispenser, south of the former tank basin, and south of the diesel dispenser. The locations of the wells are shown on Drawing 1.3.

6.1 Soil Boring and Monitoring Well Installation
The soil boring for MW-1 was advanced on July 10, 2019 by Geologic Exploration, Inc. (GEX) under
Mid-Atlantic’s supervision. The boring was placed in close proximity to the release and was initially advanced using direct push technology (DPT). The boring was then advanced to a total depth of 22 feet
below land surface (BLS) using 4 ¼ -inch outer diameter hollow stem augers driven by a GeoProbe
7822DT drill rig. Soil samples were collected using a macrocore sampler at five-foot intervals and visually classified to characterize soil types.
The soil borings for MW-2, MW-3, and MW-4 were advanced on December 11, 2019 by GEX under Mid-Atlantic’s supervision. The borings were advanced to a depth of 22 feet BLS using 4 ¼ -inch outer
diameter hollow stem augers. Soil samples were collected using a split-spoon at five-foot intervals and
visually classified to characterize soil times. Each well was constructed to a depth of 22 feet BLS. Even after subsequent mobilizations to the site to gauge the wells, MW-3 and MW-4 did not appear to produce water.
Due to the lack of water production, Mid-Atlantic and GEX returned to the site on February 11, 2020 to
install deeper wells. Both MW-3 and MW-4 were abandoned and MW-3R and MW-4R were drilled adjacent to the original locations. MW-4R was initially advanced using DPT and macrocore samplers to
identify a water-bearing zone within the boring to a depth of 40 feet BLS. The boring was then advanced using 4 ¼ - inch hollow stem augers to the total depth of 40 feet BLS. Once the groundwater bearing
Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 6
Fayetteville, North Carolina

zone was identified in MW-4R, MW-3R was advanced utilizing hollow stems augers to a total depth of
40 feet BLS.
Monitoring wells were finished with a flush-mounted manhole and locking cap. Upon completion of well construction activities, each monitoring well was developed using a new, dedicated, polyethylene bailer
to remove the fine particles from the filter pack and to improve the hydraulic connection between the well and the aquifer.
The well construction records, well abandonment records, and boring logs are provided in Appendix
C.
6.2 Soil Sample Collection
Soil samples were collected from soil boring MW-1 (during Phase I of the LSA) at 10 feet and 15 feet BLS for laboratory analysis using the methods described on the chain of custody provided in Appendix
D. Soil samples were collected using the procedures outlined in Appendix E. Soil samples were sent under chain-of-custody to Pace Analytical (Pace) in Mt. Juliet, Tennessee for analysis.
6.3 Liquid Level Measurements
On February 12, 2020, Mid-Atlantic measured the depth to water in the monitoring wells using an
electronic water level indicator. The depth-to-water in the monitoring wells is provided in Table 6.3. Free
product was not observed in the monitoring wells at this time. Groundwater flow direction could not be
determined based on the degree of variance between wells MW-1 and MW-2, and MW-3R and MW-4R. Mid-Atlantic suspects that MW-1 and MW-2 were installed within a perched aquifer separate from the
deeper wells MW-3R and MW-4R.
6.4 Groundwater Sample Collection

A groundwater sample was collected from monitoring well MW-1 on July 17, 2019 according to procedures outlined in Appendix E. Mid-Atlantic collected an additional sample from MW-1 and MW-2
on December 20, 2019. Groundwater samples collected from MW-3R and MW-4R were collected on February 12, 2020. The respective samples were sent under chain-of-custody to Pace for analysis
using the methods described on the chain of custody provided in Appendix D.
7.0 LABORATORY ANALYTICAL RESULTS
The laboratory analytical report and chain-of-custody record for the soil samples collected during the
July 2019 field activities are included in Appendix D and summarized in Table 7.1. As summarized,
the soil samples collected at both intervals in MW-1 exhibited several petroleum compounds at concentrations above the Soil-to-Water Maximum Soil Contaminant Concentrations (MSCCs).
The laboratory analytical reports and chain-of-custody records for the groundwater samples collected during the July 2019, December 2019, and February 2020 field activities are included in
Appendix D and summarized in Table 7.2. As summarized, the groundwater sample collected from monitoring well MW-1 exhibited several petroleum compounds at concentrations exceeding their
respective North Carolina Groundwater Quality Standards (NCGQS). Additionally, benzene exceeded its Gross Contaminant Level (GCL).
Phase I Limited Site Assessment Report April 17, 2020
Speedway 6993 Page 7
Fayetteville, North Carolina

8.0 SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS
The results of the LSA are summarized as follows:

• During the receptor survey, three water-supply wells were identified within 1,500 feet of the
source area of the release. All three water-supply wells were identified within 1,000 feet of the source area of the release and each property is connected to the municipal water supply
system. One of the wells is currently in use for irrigation purposes only; this well is located more than 250 feet from the source area of the release. The other two of these wells are not
in use (see Section 5.1). Surface water was not discovered within 500 feet of the source area of the release. No basements or subsurface structures were identified nearby;

• The site is located in the Coastal Plain physiographic province. Based on the available data, it
is not possible to demonstrate the lack of potential impact to a deeper aquifer at this time;
• Laboratory analysis of soil collected from boring MW-1 exhibited petroleum contaminant concentrations in excess of MSCCs; and

• The groundwater samples collected from monitoring well MW-1 exhibited several petroleum
compounds in excess of their respective NCGQS but below their respective GCLs. Benzene in MW-1 was detected at a concentration in excess of both the NCGQS and the GCL.
Based on the results of our assessment, Mid-Atlantic concludes the following:

• It appears the site should be classified as “intermediate” risk due to the exceedance of GCLs for
benzene in MW-1. It appears that the land use should be classified as “residential” due to the nearby residences. The DWM UST Section will assign risk and land use classifications.
Based on our conclusions, Mid-Atlantic recommends the following:

• Submittal of this report to the NCDEQ, DWM, Fayetteville Regional Office, UST Section for
review and assignment of risk and land use classifications.

DRAWINGS
DRAWN BY:
DATE:
ENG. CHECK:
JOB NO:DRAFTCHECK: GIS NO:
SITE
LOCATION
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1:12,000SCALE:
Hope Mills
Fort Bragg
Fayetteville
§¨¦I95
§¨¦U1
§¨¦U13 F
§¨¦S24
§¨¦U401 B§¨¦U401HOKE
CUMBERLAND
HARNETT
MOORE
ROBESON
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0 1,000 2,000500Feet
REFERENCES:
1. USGS TOPOGRAPHIC QUADRANGLES: CLIFDALE, NC; FAYETTEVILLE, NC - 20162. PROPERTY BOUNDARY FROM CUMBERLAND COUNTY GIS
AREA SHOWN WITHINNORTH CAROLINA
TOPOGRAPHIC SITE MAP SPEEDWAY #6993
670 N. REILLY ROAD FAYETTEVILLE, NORTH CAROLINA
APPROVAL:
APRIL 2019
000R3243.00
05G-R3248.00-01
DWG NO: 1.1
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UST-1
UST-2UST-3
UST-4
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APPROVED BY:
SITE MAPSPEEDWAY #6993
670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA
REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES
DATE: MARCH 2020
JOB NO.: 000R3243.0C
GIS NO.: 5G-000R3243.0C-1.2
DRAWING NO.: 1.2
0 30 60 90 12015Feet
Legend
^_SOURCE AREA
PRODUCT LINE EXCAVATION TRENCH (approximate)
FORMER UST LOCATION (Approximate)
UST EXCAVATION EXTENT (Approximate)
SITE BOUNDARY
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ENGINEER CHECK BY:
APPROVED BY:
MONITORING WELL LOCATION MAPSPEEDWAY #6993
670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA
REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES
DATE: MARCH 2020
JOB NO.: 000R3243.0C
GIS NO.: 5G-000R3243.0C-1.3
DRAWING NO.: 1.3
0 20 40 60 8010Feet
Legend
MONITORING WELL
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@A Active
PRODUCT LINE EXCAVATION TRENCH (Approximate)
FORMER UST LOCATION (Approximate)
UST EXCAVATION EXTENT (Approximate)
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ENGINEER CHECK BY:
APPROVED BY:
RECEPTOR SURVEY MAP
SPEEDWAY #6993670 N. REILLY ROAD
FAYETTEVILLE, NORTH CAROLINA
REFERENCE: CUMBERLAND COUNTY GIS. MID-ATLANTIC FIELD NOTES
DATE: APRIL 2020
JOB NO.: 000R3243.0A
GIS NO.: 5G-R3243.0A-5.1
DRAWING NO.: 5.1
Legend
^_DIESEL DISPENSER
SITE BOUNDARY
500' BUFFER
1,000' BUFFER
1,500' BUFFER
BUILDING FOOTPRINT
&(WATER SUPPLY WELL
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1
4
2
WSW-1 FILLYAW RD
KISCO DR N REILLY RD GARFIELD DR SMITHFIELD ST BLACK DR APPLEWOOD LN SEATON PL LANSING CT
´
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
ADJACENT PROPERTIES MAP
SPEEDWAY #6993670 N. REILLY ROAD
FAYETTEVILLE, NORTH CAROLINA
REFERENCE: CUMBERLAND COUNTY GIS. MID-ATLANTIC FIELD NOTES
DATE: APRIL 2020
JOB NO.: 000R3243.0A
GIS NO.: 5G-R3243.0C-5.2
DRAWING NO.: 5.2
Legend
SPEEDWAY 6993
^_DIESEL DISPENSER
ADJACENTPROPERTY ID (SEE APPENDIX B)
PROPERTY LINES
STREETS
500' BUFFER 200 0 200100 Feet
@A
@A
!?!?
@A
@A
1.0
5,000
NOTES:(7,770) = BENZENE CONCENTRATION AT LOCATION (ug/L)(ND) = NOT DETECTED AT OR ABOVE LABORATORY METHOD DETECTION LIMIT(NS) = NOT SAMPLED - WELL DRYNC GROUNDWATER QUALITY STANDARD (NCGQS) FOR BENZENE = 1.0 ug/LGROSS CONTAMINATION LEVEL (GCL) FOR BENZENE = 5,000 ug/LMW-1 AND MW-2 SAMPLED 12/20/2019; MW-3R AND MW-4R SAMPLED 2/12/2020
MW-4
(NS)
MW-3(NS)
MW-2
(ND)
MW-4R(ND)
MW-1(7,770)
MW-3R(0.807)N REILLY RDFILLYAW RD
´
DRAWN BY:
DRAFT CHECK BY:
ENGINEER CHECK BY:
APPROVED BY:
ESTIMATED ISOCONCENTRATION MAP -
BENZENE IN SHALLOW GROUNDWATERSPEEDWAY #6993
670 N. REILLY ROADFAYETTEVILLE, NORTH CAROLINA
REFERENCE: 2017 AERIAL PHOTOGRAPH FROM NC ONEMAP GEOSPATIAL APPLICATION. MID-ATLANTIC FIELD NOTES
DATE: APRIL 2020
JOB NO.: 000R3243.0C
GIS NO.: 5G-000R3243.0C-6.1
DRAWING NO.: 6.1
0 20 40 60 8010Feet
Legend
MONITORING WELL
!?Abandoned
@A Active
ESTIMATED BENZNE ISOCONCENTRATION LINE
SITE BOUNDARY
STREETS

TABLES
WELL NO.OWNER NAME AND ADDRESSUSER NAME & ADDRESSUSES OF WELLWELL DEPTHWELL CASING DEPTHWELL SCREEN INTERVALDISTANCE & DIRECTION FROM SOURCE AREA1WAINGOLD, RITA205 SE SERVICE RD 237SOUTHERN PINES, NC 28387PRO Car Wash & Detail 648 N. Reilly RoadIrrigation Unknown Unknown Unknown 246 feet S-SE2Not currently in useUnknown Unknown Unknown 766 feet N-NW3Not currently in useUnknown Unknown Unknown 764 feet NWTABLE 5.1WATER-SUPPLY WELL INVENTORY RESULTSSPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC PROJECT NO.: 000R3243.0CHeavner's Acres 703 N. Reilly RoadHEAVNER, CECIL B;CHARLES, O HEAVNER HEIRS JRPO BOX 1266SMITHFIELD, NC 27577
Well IDTotal Depth from TOC (feet)Screen Length (feet)Screened Interval (feet)TOC ElevationDepth to Water (Feet)Groundwater ElevationMW-121.5156.5'-21.5'100.1116.3283.79MW-222157.5'-22.5'99.4912.4587.04MW-322.5157.5'-22.5'100.50Dry--MW-3R402020'-40'100.5036.8863.62MW-422.5157.5'-22.5'99.58Dry--MW-4R402020'-40'99.5836.0363.55Notes:TOC = Top of CasingEach well was constructed using 2" schedule 40 PVC casing with 0.010" mechanically slotted screen.Water level measurements were taken on February 11 and 12, 2020.TABLE 6.1GROUNDWATER ELEVATION DATASPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC PROJECT NO.: 000R3243.0CElevations were surveyed by Mid-Atlantic personnel using a laser level and benchmark elevation of 100.00.
1,2,3-Trimethylbenzene2.51 2.37NLNLNL1,2,4-Trimethylbenzene8.82.898.578220,4401,3,5-Trimethylbenzene2.61 2.428.378220,4401,4-DichlorobenzeneND 0.008180.0991101,000Benzene0.01840.6560.005618164Ethylbenzene2.07 2.514.91,56040,000Isopropylbenzene0.381 0.2991.71,56440,880Naphthalene0.9381.350.163138,176Toluene0.928 4.434.31,20032,000Xylenes, total10.6 12.64.63,12981,760Acenaphthene0.0182 J 0.0239 J8.294024,000FluorantheneND 0.00589 J29062016,400Fluorene0.0182 J 0.0270 J4762016,400Napthalene2.89 J4.430.163138,176Phenanthrene0.0289 J 0.0367 J5646912,264C5-C8 Aliphatics491 J33.16893924,528C9-C18 Aliphatics384.16 1465401,50040,000C19-C36 AliphaticsND ND#31,000810,000C9-C22 Aromatics244.8 81.43146912,264J = Detected below the laboratory reporting limit, but above the method detection limitNL = No MSCC listed for analyteB = The same analyte is found in the associated blankND = Not detected at or above labaoratory method detection limitsmg/kg - Milligrams per KilogramMSCC - Maximum Soil Contaminant Concentration# = Health based level > 100%MADEP VPH & EPHTABLE 7.1SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN SOILSPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC JOB NO. R3243.0CVolatile Organic Compounds - SM8260Soil-to-Water MSCC Residential Soil MSCCIndustrial / Commercial Soil MSCCCHEMICAL CONSTITUENTMW-1 (15')7/10/19Semi Volatile Organic Compounds - SM8270CONCENTRATION (mg/kg)MW-1 (10') 7/10/19
MW-1MW-1MW-2MW-3RMW-4R7/17/201912/20/201912/20/20192/12/20202/12/2020Benzene2,6507,770ND0.807ND15,000Di-isopropyl etherNDNDNDNDND7070,000Ethylbenzene2,6903,240NDNDND60084,500MTBENDNDNDNDND2020,000Naphthalene798899NDNDND66,000Toluene14,20026,900NDNDND600260,000Xylenes, total14,10015,310NDNDND50085,500Benzo(a)anthraceneNDNDNDNDND0.054.7Benzo(b)fluoranthene NDNDNDNDND0.050.75Di-n-butyl phthalateND0.387 J0.403 JND0.523 JNLNLNaphthalene206594NDNDND66,000PenanthreneNDNDNDND0.444 J200410.00C5-C8 Aliphatics38,20077,300NDNDND400NEC9-C18 Aliphatics31,83050,06555.5 JNDND700NEC19-C36 AliphaticsND43.5 JNDNDND10,000NEC9-C22 Aromatics15,0207,23453.0 JNDND200NENotes: (µg/L) = Microgram per literJ = Detected above the Method Detection Limit but below the Reporting Limit; therefore, result is an estimated concentration B - The same analyte is found in the associated blankND = Not detected at or above laboratory method detection limitsNL = No NCGQS listed for analyteNS = No StandardCONCENTRATION (µg/L)NC Groundwater Quality StandardsCHEMICAL CONSTITUENTGross Contamination Levels for Groundwater Bold values denote that analyte was detected above its 2L North Carolina Groundwater Quality Standard MADEP VPH & EPHTABLE 7.2SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN GROUNDWATERSPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC JOB NO. R3243.0BSemi Volatile Organic Compounds - SM 625Volatile Organic Compounds - SM 602

APPENDIX A
LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE FORM
Limited Site Assessment Risk Classification and Land Use Form

Part I – Groundwater/Surface Water/Vapor Impacts

High Risk
1. Has the release contaminated any water supply well including any well used for
non-drinking purposes? YES/NO

2. Is a water supply well used for drinking water located within 1,000 feet of the
source area of the release? YES/NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars,
industrial cooling water, filling swimming pools) located within 250 feet of the
source area of the release? YES/NO

4. Does groundwater within 500 feet of the source area of the release have the
potential for future use (there is no other source of water supply other than the
groundwater)? YES/NO

5. Do vapors from the release pose a threat of explosion because of accumulation of
the vapors in a confined space or pose any other serious threat to public health,
public safety or the environment? YES/NO
If yes, describe.
________________________________________________________________
________________________________________________________________
________________________________________________________________
__________________________________________

6. Are there any other factors that would cause the release to pose an imminent
danger to public health, public safety, or the environment? YES/NO
If yes, describe.
________________________________________________________________
________________________________________________________________
____________________________

Intermediate Risk

7. Is a surface water body located within 500 feet of the source area of the release?
YES/NO

If YES, does the maximum groundwater contaminant concentration exceed the
surface water quality standards and criteria found in 15A NCAC 2B .0200 by a
factor of 10? YES/NO

8. Is the source area of the release located within a approved or planned wellhead
protection area as defined in 42 USC 300h-7(e)? YES/NO
If yes, describe.
________________________________________________________________
________________________________________________________________
____________________________

9. Is the release located in the Coastal Plain physiographic region as designated on
a map entitled “Geology of North Carolina” published by the Department in 1985?
YES/NO
________ See text Section 5.5. ______________________________________
________________________________________________________________
________________________________________________________________
If YES, is the source area of the release located in an area in which there is
recharge to an unconfined or semi-confined deeper aquifer that is being used or
may be used as a source of drinking water? YES/NO
If YES, describe. __________________________________________________
________________________________________________________________
________________________________________________________________

10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels (See Table 2.) established by the Department? YES/NO

Part II - Land Use

Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.

1. Does the property contain one or more primary or secondary residences
(permanent or temporary)? YES/NO
Describe.
______________________________________________________________
______________________________________________________________
____________________________

2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly?
YES/NO
Describe.
______________________________________________________________
______________________________________________________________
__________________________

3. Does the property contain a commercial (e.g., retail, warehouse, office/business
space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and
development, chemical/petroleum bulk storage, etc.) enterprise, an inactive
commercial or industrial enterprise, or is the land undeveloped? YES/NO
Describe.

The property contains an inactive/closed retail petroleum station.____________
________________________________________________________________

4. Do children visit the property? YES/NO
Explain.
________________________________________________________________
________________________________________________________________
____________________________

Is access to the property reliably restricted consistent with its use (e.g., by
fences, security personnel or both)? YES/NO
Explain.

____________________________
5. Do pavement, buildings, or other structures cap the contaminated soil? YES/NO
Describe.
_____Pavement___________________________________________________
________________________________________________________________
____________________________________

If yes, what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future?
________________________________________________________________
________________________________________________________________
________________________________________________________________

6. What is the zoning status of the property? ______________________________
____Limited Commercial (LC)________________________________________
________________________________________________________________

7. Is the use of the property likely to change in the next 20 years? YES/NO
Explain. __No known redevelopment plans. Property is inactive and will likely be
redeveloped at some point in time.
________________________________________________________________

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the
release (excludes property containing source area of the release):

1. What is the distance from the source area of the release to the nearest primary
or secondary residence (permanent or temporary)? __170 feet_______________
________________________________________________

2. What is the distance from the source area of the release to the nearest school,
daycare center, hospital, playground, park, recreation area, church, nursing
home or other place of public assembly? ___1,500 feet south (Village Baptist
Church)________________________________________________________

3. What is the zoning status of properties in the surrounding area? _____________
___Limited Commercial (LC), Single Family Residential (SF10)______________
________________________________________________________________
________________________________________________________________

4. Briefly characterize the use and activities of the land in the surrounding area.
__Commercial (north, southeast, southwest), residential (northeast, east, west)
________________________________________________________________
________________________________________________________________

APPENDIX B ADJACENT PROPERTY OWNER DATA
ADJACENT PROPERTY ID NO (SEE DRAWING 5.2)PARCEL IDENTIFICATION NO. (PIN)STREET ADDRESS PROPERTY OWNERPROPERTY OWNER ADDRESS19499618358000690 N Reilly Rd SCHULTZ, EDWARD M;HARVEY, G71 KILBRIDE DRPINEHURST, NC 283742 94997101480007209 Fillyaw RdMCDOUGALD, RONALD W;MCDOUGALD, IRENE D KIRK7209 FILLYAW RDFAYETTEVILLE, NC 2830339499618042000648 N Reilly RdWAINGOLD, RITA205 SE SERVICE RD 237SOUTHERN PINES, NC 2838749499605949000649 N Reilly RdHINDS, DAVID ANDREW;HINDS, CHONG I120 KIRKWOOD DRFAYETTEVILLE, NC 2830359499612511000735 N Reilly RdHEAVNER, CECIL B;CHARLES, O HEAVNER HEIRS JRPO BOX 1266SMITHFIELD, NC 27577APPENDIX BADJACENT PROPERTY OWNER DATASPEEDWAY 6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC PROJECT NO.: 000R3243.0CReference: Tax parcel owner and address information retrieved from digital files downloaded from the Cumberland County GIS public access web site. For updated information, users should verify property ownership. Mid-Atlantic does not provide a warranty that public records used by Cumberland County to create the digital database are accurate.

APPENDIX C SOIL BORING LOGS AND WELL CONSTRUCTION RECORDS
ft -bgsSampling
Interval,
Odors PID (ppm)FID (ppm)SOIL DESCRIPTION (color, texture, moisture, etc.)Construction Deatails
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
ft - indicates depth in feet ppm - indicates parts per million
ft BLS - indicates feet below land surface
Speedway 6993
Hollow Stem Auger, Direct
Push Technology
N/A
16.32
Geologic Exploration
1Page:
Total Boring Depth (ft):
Well Depth (ft):
6.5-21.5
1125 E. Morehead Street
Suite 104
Charlotte, NC 28204
Ph: [phone]
Sampling Method:
Subcontractor/Drillers:
MW-1LOG OF BORING:
2
Screen Depth (ft):
4
10
8
1 of
Gary Fischer
6ft-BLS22.0
21.5
24
20
22
12
14
18
16
26
28
30
28
30
26
20
18
22
24
10
12
14
16
8
Fayetteville, NC
Site Name:
Project Number:
Location:
Drilling/Boring Method:
2
4
Date Started:
6
Date Completed:Monitoring Equipment:
Driller :
7/10/2019
7/10/2019
000R3243.0B
Vince Federle
MAA Field Staff:N/A
DTW (ft):
Boring terminated at 22 feet.
Backfill material and stone, so samples collected.
Ligh bown silty fine sand
Light brown clayey fine sand
Light brown slightly silty clayey sand
Probe terminated at 19 feet, converted to hollow-stem auger with 4 1/4" inner diamater, 8"
outer diameter
Light brown and grey clayey fine silt
Light reddish orange and tan slightly clayey fine sand
Light brown and tan fine sandy clay
ft -bgsSampling
Interval, Odors
PID (ppm)FID (PPM)Construction Details
ft-bgs16 16
18 18
20 20
22 22
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
DTW - Depth to Water ft - indicates depth in feet ppm - indicates parts per million
ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
23
1125 E. Morehead Street, Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-2
Page: 1 of 1
Site Name: Speedway 6993 Drilling/Boring Method:
Hollow Stem Auger (8"
Outside Diameter)Total Boring Depth (ft):
7.5-22.5
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):22.5
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration, Inc.Screen Depth (ft):
Troy Holzschuh
Date Started:12/11/2019 Driller :Vince Federle DTW (ft):
Dry on 12-11-19 13.21
on 12-20-19 14.12 on
1-8-20
SOIL DESCRIPTION (color, texture, moisture, etc.)
2
Date Completed:12/11/2019 Monitoring Equipment:N/A MAA Field Staff:
2
4 4
6 6
8 8
10 10
12 12
14 14
Asphalt/Aggregate
Tan, Sand, Fine, Moist
Orange and Yellow, Marbled, Clayey Sand
Orange, Slightly Silty, Clayey Sand
Red and Yellow, Marbled, Sand, Medium Grain, Moist
Orange and Yellow and White, Marbled Sandy Clay
ft -bgsSampling
Interval, Odors
PID (ppm)FID (PPM)Construction Details
ft-bgs16 16
18 18
20 20
22 22
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
DTW - Depth to Water ft - indicates depth in feet ppm - indicates parts per million
ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
23
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-3
Page: 1 of 1
Site Name: Speedway 6993 Drilling/Boring Method:
Hollow Stem Auger (8"
Outside Diameter)Total Boring Depth (ft):
7.5-22.5
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):22.5
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration, Inc.Screen Depth (ft):
Troy Holzschuh
Date Started:12/11/2019 Driller :Vince Federle DTW (ft):Dry
Date Completed:12/11/2019 Monitoring Equipment:N/A MAA Field Staff:
SOIL DESCRIPTION (color, texture, moisture, etc.)
Asphalt/Aggregate
0.2 1.1
2 2
0.3 0.8
4 4
0.5 0.6
6 6
1.0 0.5
8 8
0.9 0.0
10 10
0.7 0.1
12 12
0.7
0.0
0.1
14 14
0.5 0.1
0.0 0.0
0.0 0.0
0.2
Tan, Sand, Fine, Moist
Orange, Sand, Fine, Moist
Orange, Clayey Sandy Silt, Moist
Orange, Sandy Clayey Silt, Moist
Red and Orange and White, Marbled Sandy Clay
ft -bgsSampling
Interval,
Odors PID (ppm)FID (ppm)SOIL DESCRIPTION (color, texture, moisture, etc.)Construction Deatails
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
ft - indicates depth in feet ppm - indicates parts per million
ft BLS - indicates feet below land surface
Asphalt/Aggregate
Brownish orange clayey sandy silt, moist
Reddish orange clayey silty sand, moist
6.7
9.6
25
21
29
32
28 28
30 30
Tannish orange fine sand, moist
24 24
26 26
20 20
22 22
16 16
18 18
10 10
12 12
14 14ft-BLS2 2
4 4
6 6
8 8
Date Completed:2/11/2020 Monitoring Equipment:TVA-1000 MAA Field Staff:John L. Sherrill, P.G.
Date Started:2/11/2020 Driller :Jeremy Ringler DTW (ft):36.88
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration Screen Depth (ft):20-40
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):40
Site Name: Speedway 6993 Drilling/Boring Method:Hollow Stem Auger Total Boring Depth (ft):40.0
1125 E. Morehead Street
Suite 104
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-3R
Page:1 of 2
ft -bgsSampling
Interval,
Odors PID (ppm)FID (ppm)SOIL DESCRIPTION (color, texture, moisture, etc.)Construction Deatails
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
ft - indicates depth in feet ppm - indicates parts per million
ft BLS - indicates feet below land surface
60
Reddish orange clayey silty sand, moist
Boring Terminated at 40'
52 52
54 54
56 56
58 58
60
44 44
46 46
48 48
50 50
36
38 38
40 40
42 42ft-BLS41
32 32
34 34
16
36
Date Completed:2/11/2020 Monitoring Equipment:TVA-1000 MAA Field Staff:John L. Sherrill, P.G.
Date Started:2/11/2020 Driller :Jeremy Ringler DTW (ft):36.88
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration Screen Depth (ft):20-40
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):40
Site Name: Speedway 6993 Drilling/Boring Method:Hollow Stem Auger Total Boring Depth (ft):40.0
1125 E. Morehead Street
Suite 104
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-3R
Page:2 of 2
ft -bgsSampling
Interval, Odors
PID (ppm)FID (PPM)Construction Details
ft-bgs16 16
18 18
20 20
22 22
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
DTW - Depth to Water ft - indicates depth in feet ppm - indicates parts per million
ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
23
1125 E. Morehead Street, Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-4
Page: 1 of 1
Site Name: Speedway 6993 Drilling/Boring Method:
Hollow Stem Auger (8"
Outside Diameter)Total Boring Depth (ft):
7.5-22.5
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):22.5
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration, Inc.Screen Depth (ft):
Troy Holzschuh
Date Started:12/11/2019 Driller :Vince Federle DTW (ft):
Dry on 12-11-19 Dry
on 12-20-19 22.24 on
11-8-20
Date Completed:12/11/2019 Monitoring Equipment:N/A MAA Field Staff:
SOIL DESCRIPTION (color, texture, moisture, etc.)
Asphalt/Aggregate
0.2 1.6 Tan, Sand, Fine, Moist
2 2
0.0 0.0
Orange, Sand, Fine, Moist4 4
0.0 0.1
6 6
0.0 0.5
Orange, Clayey Sandy Silt, Moist8 8
0.0 0.6
10 10
0.0 0.1
Orange, Sandy Clayey Silt, Moist
12 12
0.0 0.5
14 14
0.3 0.2
0.1 0.1
Red and Orange and White, Marbled Sandy Clay0.6 0.5
0.1 0.6
ft -bgsSampling
Interval,
Odors PID (ppm)FID (ppm)SOIL DESCRIPTION (color, texture, moisture, etc.)Construction Deatails
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
ft - indicates depth in feet ppm - indicates parts per million
ft BLS - indicates feet below land surface
N/A
N/A
2.90
Orange fine sandy clayey silt, moist
Red, orange, and white mottled silty clay, moist
Orange medium fine sand, moist
N/A
N/A
N/A
N/A
N/A
N/A 3.10
2.85
2.95
N/A
N/A
N/A
N/A
N/A
N/A
N/A 2.95
2.91
7.20
2.70
3.80
2.50
30
Orange clayey sandy silt, moist
1.75
2.15
3.55
22 22
24 24
26 26
28 28
30
14 14
16 16
18 18
20 20
6
8 8
10 10
12 12ft-BLSAsphalt/Aggregate
Tannish orange fine sand, moist
2 2
4 4
6
Date Completed:2/11/2020 Monitoring Equipment:TVA-1000 MAA Field Staff:John L. Sherrill, P.G.
Date Started:2/11/2020 Driller :Jeremy Ringler DTW (ft):36.03
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration Screen Depth (ft):20-40
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):40
Site Name: Speedway 6993 Drilling/Boring Method:Hollow Stem Auger Total Boring Depth (ft):40.0
1125 E. Morehead Street
Suite 104
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-4R
Page:1 of 2
ft -bgsSampling
Interval,
Odors PID (ppm)FID (ppm)SOIL DESCRIPTION (color, texture, moisture, etc.)Construction Deatails
COMMENTS:in - indicates inches N/A - indicates not applicable to this boring
ft - indicates depth in feet ppm - indicates parts per million
ft BLS - indicates feet below land surface
Red, grey, orange mottled silty clay, moist
Thin medium sand seam, moist
Red fine sand into red, grey, and tan mottled silty clay, moist to slightly wet
54 54
56 56
58 58
60 60
46 46
48 48
50 50
52 52
38 38
40 40Boring Terminated at 40'
42 42
44 44ft-BLS4.5
32 32
34 34
8.7
36 36
Date Completed:2/11/2020 Monitoring Equipment:TVA-1000 MAA Field Staff:John L. Sherrill, P.G.
Date Started:2/11/2020 Driller :Jeremy Ringler DTW (ft):36.03
Location: Fayetteville, NC Subcontractor/Drillers: Geologic Exploration Screen Depth (ft):20-40
Project Number:000R3243.0B Sampling Method:N/A Well Depth (ft):40
Site Name: Speedway 6993 Drilling/Boring Method:Hollow Stem Auger Total Boring Depth (ft):40.0
1125 E. Morehead Street
Suite 104
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: MW-4R
Page:2 of 2
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WELL ABANDONMENT RECORD
This form can be used for single or multiple wells
Form GW-30 North Carolina Department of Environment and Natural Resources – Division of Water Quality Revised March 2013
1. Well Contractor Information:

Well Contractor Name (or well owner personally abandoning well on his/her property)

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply
wells ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)

WELL ABANDONMENT DETAILS

7a. Number of wells being abandoned:
For multiple injection or non-water supply wells ONLY with the same
construction/abandonment, you can submit one form.

7b. Approximate volume of water remaining in well(s): (gal.)

FOR WATER SUPPLY WELLS ONLY:

7c. Type of disinfectant used:

7d. Amount of disinfectant used:

7e. Sealing materials used (check all that apply):
Neat Cement Grout Bentonite Chips or Pellets
Sand Cement Grout Dry Clay
Concrete Grout Drill Cuttings
Specialty Grout Gravel
Bentonite Slurry Other (explain under 7g)

7f. For each material selected above, provide amount of materials used:

7g. Provide a brief description of the abandonment procedure:

8. Certification:

Signature of Certified Well Contractor or Well Owner Date

By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.

9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:

Division of Water Quality, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617

10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:

Division of Water Quality, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636

10c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well abandonment to the county health department of the county
where abandoned.
For Internal Use ONLY:
JEREMY RINGLER
A - 4422
GEOLOGIC EXPLORATION, INC

02/11/20
SPEEDWAY - 6993
670 NORTH REILLY ROAD FAYETTEVILLE 28303
CUMBERLAND
35° 05' 59.39" 79° 00' 39.04"
MW-3
22.5
2.0

1

3.75 GALLONS
WELL ABANDONED VIA TREMIE PIPE WITH
PORTLAND BENTONITE SLURRY

02/28/20
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WELL ABANDONMENT RECORD
This form can be used for single or multiple wells
Form GW-30 North Carolina Department of Environment and Natural Resources – Division of Water Quality Revised March 2013
1. Well Contractor Information:

Well Contractor Name (or well owner personally abandoning well on his/her property)

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply
wells ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)

WELL ABANDONMENT DETAILS

7a. Number of wells being abandoned:
For multiple injection or non-water supply wells ONLY with the same
construction/abandonment, you can submit one form.

7b. Approximate volume of water remaining in well(s): (gal.)

FOR WATER SUPPLY WELLS ONLY:

7c. Type of disinfectant used:

7d. Amount of disinfectant used:

7e. Sealing materials used (check all that apply):
Neat Cement Grout Bentonite Chips or Pellets
Sand Cement Grout Dry Clay
Concrete Grout Drill Cuttings
Specialty Grout Gravel
Bentonite Slurry Other (explain under 7g)

7f. For each material selected above, provide amount of materials used:

7g. Provide a brief description of the abandonment procedure:

8. Certification:

Signature of Certified Well Contractor or Well Owner Date

By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.

9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:

Division of Water Quality, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617

10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:

Division of Water Quality, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636

10c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well abandonment to the county health department of the county
where abandoned.
For Internal Use ONLY:
JEREMY RINGLER
A - 4422
GEOLOGIC EXPLORATION, INC

02/11/20
SPEEDWAY - 6993
670 NORTH REILLY ROAD FAYETTEVILLE 28303
CUMBERLAND
35° 05' 59.39" 79° 00' 39.04"
MW-4
22.5
2.0

1

3.75 GALLONS
WELL ABANDONED VIA TREMIE PIPE WITH
PORTLAND BENTONITE SLURRY

02/28/20
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APPENDIX D
LABORATORY ANALYTICAL REPORTS AND CHAIN-OF-CUSTODY RECORDS
ANALYTICAL REPORT
July 25, 2019
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1118060
Samples Received:07/12/2019
Project Number:R3243.0A
Description:Speedway 6993
Site:6993
Report To:Mr. Patrick Kelly
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
July 25, 2019
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 1 of 45
July 30, 2019
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 1 of 45
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 (10') L1118060-01 5
MW-1 (15') L1118060-02 8
MW-01 L1118060-03 12
Qc: Quality Control Summary 14
Total Solids by Method 2540 G-2011 14
Volatile Petroleum Hydrocarbons by Method MADEPV 15
Volatile Organic Compounds (GC/MS) by Method 602MS 17
Volatile Organic Compounds (GC/MS) by Method 8260D 18
TPH by Method MADEPE 25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 28
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 31
Gl: Glossary of Terms 36
Al: Accreditations & Locations 38
Sc: Sample Chain of Custody 39
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 2 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 2 of 45
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 (10') L1118060-01 Solid Gary A. Fischer 07/10/19 15:15 07/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1313450 1 07/18/19 14:43 07/18/19 14:53 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1313524 100 07/19/19 03:07 07/19/19 03:07 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1313610 8 07/10/19 15:15 07/18/19 16:59 ACG Mt. Juliet, TN
TPH by Method MADEPE WG1312529 3 07/16/19 13:55 07/17/19 14:59 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1312529 3 07/16/19 13:55 07/17/19 16:05 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1313771 1 07/18/19 16:50 07/19/19 03:37 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1313771 5 07/18/19 16:50 07/19/19 10:45 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 (15') L1118060-02 Solid Gary A. Fischer 07/10/19 15:25 07/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1313450 1 07/18/19 14:43 07/18/19 14:53 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1313524 50 07/19/19 02:35 07/19/19 02:35 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1313610 1 07/10/19 15:25 07/18/19 15:04 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1314146 20 07/10/19 15:25 07/19/19 13:19 JAH Mt. Juliet, TN
TPH by Method MADEPE WG1312529 3 07/16/19 13:55 07/17/19 15:21 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1312529 3 07/16/19 13:55 07/17/19 15:43 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1313771 1 07/18/19 16:50 07/19/19 04:35 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1313771 5 07/18/19 16:50 07/19/19 11:05 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-01 L1118060-03 GW Gary A. Fischer 07/11/19 07:25 07/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1313062 200 07/17/19 21:57 07/17/19 21:57 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1313111 100 07/18/19 11:03 07/18/19 11:03 DWR Mt. Juliet, TN
TPH by Method MADEPE WG1311838 1.04 07/15/19 12:07 07/16/19 14:19 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1311838 1.04 07/15/19 12:07 07/16/19 14:41 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1311664 1 07/18/19 14:35 07/19/19 01:44 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 4 of 45
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1118060
MW-1 (10')
Collected date/time: 07/10/19 15:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.0 1 07/18/2019 14:53 WG1313450
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 491 J6 4.01 12.1 100 07/19/2019 03:07 WG1313524
Unadjusted C9-C12 Aliphatics 376 J6 4.01 12.1 100 07/19/2019 03:07 WG1313524
Unadjusted C9-C10 Aromatics 233 V 4.01 12.1 100 07/19/2019 03:07 WG1313524
Total VPH 1100 J6 4.01 12.1 100 07/19/2019 03:07 WG1313524
(S) 2,5-Dibromotoluene(FID) 106 70.0-130 07/19/2019 03:07 WG1313524
(S) 2,5-Dibromotoluene(PID) 91.0 70.0-130 07/19/2019 03:07 WG1313524
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.00482 0.0241 8 07/18/2019 16:59 WG1313610
1,1,1-Trichloroethane U 0.00265 0.0241 8 07/18/2019 16:59 WG1313610
1,1,2,2-Tetrachloroethane U 0.00376 0.0241 8 07/18/2019 16:59 WG1313610
1,1,2-Trichloroethane U 0.00851 0.0241 8 07/18/2019 16:59 WG1313610
1,1,2-Trichlorotrifluoroethane U J0 0.00651 0.0241 8 07/18/2019 16:59 WG1313610
1,1-Dichloroethane U 0.00555 0.0241 8 07/18/2019 16:59 WG1313610
1,1-Dichloroethene U 0.00482 0.0241 8 07/18/2019 16:59 WG1313610
1,1-Dichloropropene U 0.00675 0.0241 8 07/18/2019 16:59 WG1313610
1,2,3-Trichlorobenzene U 0.00603 0.0241 8 07/18/2019 16:59 WG1313610
1,2,3-Trichloropropane U 0.0492 0.121 8 07/18/2019 16:59 WG1313610
1,2,3-Trimethylbenzene 2.51 0.0111 0.0482 8 07/18/2019 16:59 WG1313610
1,2,4-Trichlorobenzene U 0.0465 0.121 8 07/18/2019 16:59 WG1313610
1,2,4-Trimethylbenzene 8.80 0.0112 0.0482 8 07/18/2019 16:59 WG1313610
1,2-Dibromo-3-Chloropropane U 0.0492 0.241 8 07/18/2019 16:59 WG1313610
1,2-Dibromoethane U 0.00506 0.0241 8 07/18/2019 16:59 WG1313610
1,2-Dichlorobenzene U 0.0140 0.0482 8 07/18/2019 16:59 WG1313610
1,2-Dichloroethane U 0.00458 0.0241 8 07/18/2019 16:59 WG1313610
1,2-Dichloropropane U 0.0123 0.0482 8 07/18/2019 16:59 WG1313610
1,3,5-Trimethylbenzene 2.61 0.0104 0.0482 8 07/18/2019 16:59 WG1313610
1,3-Dichlorobenzene U 0.0164 0.0482 8 07/18/2019 16:59 WG1313610
1,3-Dichloropropane U 0.0169 0.0482 8 07/18/2019 16:59 WG1313610
1,4-Dichlorobenzene U 0.0190 0.0482 8 07/18/2019 16:59 WG1313610
2,2-Dichloropropane U 0.00764 0.0241 8 07/18/2019 16:59 WG1313610
2-Butanone (MEK)U 0.121 0.241 8 07/18/2019 16:59 WG1313610
2-Chlorotoluene U 0.00887 0.0241 8 07/18/2019 16:59 WG1313610
4-Chlorotoluene U 0.0109 0.0482 8 07/18/2019 16:59 WG1313610
4-Methyl-2-pentanone (MIBK) U 0.0964 0.241 8 07/18/2019 16:59 WG1313610
Acetone U 0.133 0.241 8 07/18/2019 16:59 WG1313610
Acrylonitrile U 0.0183 0.121 8 07/18/2019 16:59 WG1313610
Benzene 0.0184 0.00386 0.00964 8 07/18/2019 16:59 WG1313610
Bromobenzene U 0.0101 0.121 8 07/18/2019 16:59 WG1313610
Bromodichloromethane U 0.00759 0.0241 8 07/18/2019 16:59 WG1313610
Bromoform U 0.0576 0.241 8 07/18/2019 16:59 WG1313610
Bromomethane U 0.0357 0.121 8 07/18/2019 16:59 WG1313610
Carbon tetrachloride U 0.0104 0.0482 8 07/18/2019 16:59 WG1313610
Chlorobenzene U 0.00552 0.0241 8 07/18/2019 16:59 WG1313610
Chlorodibromomethane U 0.00434 0.0241 8 07/18/2019 16:59 WG1313610
Chloroethane U J0 0.0104 0.0482 8 07/18/2019 16:59 WG1313610
Chloroform U 0.00400 0.0241 8 07/18/2019 16:59 WG1313610
Chloromethane U 0.0134 0.121 8 07/18/2019 16:59 WG1313610
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1118060
MW-1 (10')
Collected date/time: 07/10/19 15:15
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Dibromomethane U 0.00964 0.0482 8 07/18/2019 16:59 WG1313610
Dichlorodifluoromethane U 0.00788 0.0241 8 07/18/2019 16:59 WG1313610
Di-isopropyl ether U 0.00338 0.00964 8 07/18/2019 16:59 WG1313610
Ethylbenzene 2.07 0.00511 0.0241 8 07/18/2019 16:59 WG1313610
Hexachloro-1,3-butadiene U 0.123 0.241 8 07/18/2019 16:59 WG1313610
Isopropylbenzene 0.381 0.00832 0.0241 8 07/18/2019 16:59 WG1313610
Methyl tert-butyl ether U 0.00284 0.00964 8 07/18/2019 16:59 WG1313610
Methylene Chloride U 0.0640 0.241 8 07/18/2019 16:59 WG1313610
Naphthalene 0.938 0.0301 0.121 8 07/18/2019 16:59 WG1313610
Styrene U 0.0263 0.121 8 07/18/2019 16:59 WG1313610
Tetrachloroethene U 0.00675 0.0241 8 07/18/2019 16:59 WG1313610
Toluene 0.926 0.0121 0.0482 8 07/18/2019 16:59 WG1313610
Trichloroethene U 0.00386 0.00964 8 07/18/2019 16:59 WG1313610
Trichlorofluoromethane U 0.00482 0.0241 8 07/18/2019 16:59 WG1313610
Vinyl chloride U 0.00658 0.0241 8 07/18/2019 16:59 WG1313610
Xylenes, Total 10.6 0.0460 0.0627 8 07/18/2019 16:59 WG1313610
cis-1,2-Dichloroethene U 0.00665 0.0241 8 07/18/2019 16:59 WG1313610
cis-1,3-Dichloropropene U 0.00653 0.0241 8 07/18/2019 16:59 WG1313610
n-Butylbenzene 0.359 0.0370 0.121 8 07/18/2019 16:59 WG1313610
n-Propylbenzene 1.48 0.0114 0.0482 8 07/18/2019 16:59 WG1313610
p-Isopropyltoluene 0.0718 0.0224 0.0482 8 07/18/2019 16:59 WG1313610
sec-Butylbenzene 0.131 0.0243 0.121 8 07/18/2019 16:59 WG1313610
tert-Butylbenzene U 0.0149 0.0482 8 07/18/2019 16:59 WG1313610
trans-1,2-Dichloroethene U 0.0137 0.0482 8 07/18/2019 16:59 WG1313610
trans-1,3-Dichloropropene U 0.0147 0.0482 8 07/18/2019 16:59 WG1313610
(S) Toluene-d8 97.9 75.0-131 07/18/2019 16:59 WG1313610
(S) 4-Bromofluorobenzene 95.1 67.0-138 07/18/2019 16:59 WG1313610
(S) 1,2-Dichloroethane-d4 101 70.0-130 07/18/2019 16:59 WG1313610
TPH by Method MADEPE
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 8.16 J 7.85 23.5 3 07/17/2019 14:59 WG1312529
Unadjusted C19-C36 Aliphatics U 7.85 23.5 3 07/17/2019 14:59 WG1312529
Unadjusted C11-C22 Aromatics 11.8 B J 7.85 23.5 3 07/17/2019 16:05 WG1312529
Unadjusted Total Petroleum
Hydrocarbons 19.9 J 7.85 23.5 3 07/17/2019 16:05 WG1312529
(S) o-Terphenyl 81.3 40.0-140 07/17/2019 16:05 WG1312529
(S) 1-Chloro-octadecane 91.9 40.0-140 07/17/2019 14:59 WG1312529
(S) 2-Fluorobiphenyl 85.6 40.0-140 07/17/2019 16:05 WG1312529
(S) 2-Bromonaphthalene 80.6 40.0-140 07/17/2019 16:05 WG1312529
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0182 J 0.00774 0.0401 1 07/19/2019 03:37 WG1313771
Acenaphthylene U 0.00809 0.0401 1 07/19/2019 03:37 WG1313771
Anthracene U 0.00762 0.0401 1 07/19/2019 03:37 WG1313771
Benzidine U 0.0768 0.401 1 07/19/2019 03:37 WG1313771
Benzo(a)anthracene U 0.00516 0.0401 1 07/19/2019 03:37 WG1313771
Benzo(b)fluoranthene U 0.00838 0.0401 1 07/19/2019 03:37 WG1313771
Benzo(k)fluoranthene U 0.00702 0.0401 1 07/19/2019 03:37 WG1313771
Benzo(g,h,i)perylene U 0.00869 0.0401 1 07/19/2019 03:37 WG1313771
Benzo(a)pyrene U 0.00661 0.0401 1 07/19/2019 03:37 WG1313771
Bis(2-chlorethoxy)methane U 0.00928 0.401 1 07/19/2019 03:37 WG1313771
Bis(2-chloroethyl)ether U 0.0108 0.401 1 07/19/2019 03:37 WG1313771
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 6 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1118060
MW-1 (10')
Collected date/time: 07/10/19 15:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroisopropyl)ether U 0.00916 0.401 1 07/19/2019 03:37 WG1313771
4-Bromophenyl-phenylether U 0.0137 0.401 1 07/19/2019 03:37 WG1313771
2-Chloronaphthalene U 0.00770 0.0401 1 07/19/2019 03:37 WG1313771
4-Chlorophenyl-phenylether U 0.00756 0.401 1 07/19/2019 03:37 WG1313771
Chrysene U 0.00669 0.0401 1 07/19/2019 03:37 WG1313771
Dibenz(a,h)anthracene U 0.00990 0.0401 1 07/19/2019 03:37 WG1313771
3,3-Dichlorobenzidine U 0.0957 0.401 1 07/19/2019 03:37 WG1313771
2,4-Dinitrotoluene U 0.00732 0.401 1 07/19/2019 03:37 WG1313771
2,6-Dinitrotoluene U 0.00888 0.401 1 07/19/2019 03:37 WG1313771
Fluoranthene U 0.00598 0.0401 1 07/19/2019 03:37 WG1313771
Fluorene 0.0182 J 0.00822 0.0401 1 07/19/2019 03:37 WG1313771
Hexachlorobenzene U 0.0103 0.401 1 07/19/2019 03:37 WG1313771
Hexachloro-1,3-butadiene U 0.0121 0.401 1 07/19/2019 03:37 WG1313771
Hexachlorocyclopentadiene U 0.0708 0.401 1 07/19/2019 03:37 WG1313771
Hexachloroethane U J3 J5 0.0162 0.401 1 07/19/2019 03:37 WG1313771
Indeno(1,2,3-cd)pyrene U 0.00931 0.0401 1 07/19/2019 03:37 WG1313771
Isophorone U 0.00629 0.401 1 07/19/2019 03:37 WG1313771
Naphthalene 2.89 J3 0.0536 0.201 5 07/19/2019 10:45 WG1313771
Nitrobenzene U 0.00838 0.401 1 07/19/2019 03:37 WG1313771
n-Nitrosodimethylamine U 0.0780 0.401 1 07/19/2019 03:37 WG1313771
n-Nitrosodiphenylamine U 0.108 0.401 1 07/19/2019 03:37 WG1313771
n-Nitrosodi-n-propylamine U 0.0109 0.401 1 07/19/2019 03:37 WG1313771
Phenanthrene 0.0289 J 0.00636 0.0401 1 07/19/2019 03:37 WG1313771
Benzylbutyl phthalate U 0.0124 0.401 1 07/19/2019 03:37 WG1313771
Bis(2-ethylhexyl)phthalate U 0.0145 0.401 1 07/19/2019 03:37 WG1313771
Di-n-butyl phthalate U 0.0131 0.401 1 07/19/2019 03:37 WG1313771
Diethyl phthalate U 0.00833 0.401 1 07/19/2019 03:37 WG1313771
Dimethyl phthalate U 0.00651 0.401 1 07/19/2019 03:37 WG1313771
Di-n-octyl phthalate U 0.0109 0.401 1 07/19/2019 03:37 WG1313771
Pyrene U 0.0148 0.0401 1 07/19/2019 03:37 WG1313771
1,2,4-Trichlorobenzene U 0.0106 0.401 1 07/19/2019 03:37 WG1313771
4-Chloro-3-methylphenol U 0.00575 0.401 1 07/19/2019 03:37 WG1313771
2-Chlorophenol U 0.0100 0.401 1 07/19/2019 03:37 WG1313771
2,4-Dichlorophenol U 0.00899 0.401 1 07/19/2019 03:37 WG1313771
2,4-Dimethylphenol U 0.0568 0.401 1 07/19/2019 03:37 WG1313771
4,6-Dinitro-2-methylphenol U 0.149 0.401 1 07/19/2019 03:37 WG1313771
2,4-Dinitrophenol U 0.118 0.401 1 07/19/2019 03:37 WG1313771
2-Nitrophenol U 0.0157 0.401 1 07/19/2019 03:37 WG1313771
4-Nitrophenol U 0.0633 0.401 1 07/19/2019 03:37 WG1313771
Pentachlorophenol U 0.0579 0.401 1 07/19/2019 03:37 WG1313771
Phenol U 0.00838 0.401 1 07/19/2019 03:37 WG1313771
2,4,6-Trichlorophenol U 0.00939 0.401 1 07/19/2019 03:37 WG1313771
(S) 2-Fluorophenol 81.3 12.0-120 07/19/2019 03:37 WG1313771
(S) 2-Fluorophenol 64.4 12.0-120 07/19/2019 10:45 WG1313771
(S) Phenol-d5 71.3 10.0-120 07/19/2019 03:37 WG1313771
(S) Phenol-d5 58.6 10.0-120 07/19/2019 10:45 WG1313771
(S) Nitrobenzene-d5 51.9 10.0-122 07/19/2019 10:45 WG1313771
(S) Nitrobenzene-d5 64.2 10.0-122 07/19/2019 03:37 WG1313771
(S) 2-Fluorobiphenyl 56.5 15.0-120 07/19/2019 10:45 WG1313771
(S) 2-Fluorobiphenyl 68.2 15.0-120 07/19/2019 03:37 WG1313771
(S) 2,4,6-Tribromophenol 73.1 10.0-127 07/19/2019 10:45 WG1313771
(S) 2,4,6-Tribromophenol 86.6 10.0-127 07/19/2019 03:37 WG1313771
(S) p-Terphenyl-d14 89.8 10.0-120 07/19/2019 03:37 WG1313771
(S) p-Terphenyl-d14 67.6 10.0-120 07/19/2019 10:45 WG1313771
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 7 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 7 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1118060
MW-1 (15')
Collected date/time: 07/10/19 15:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 88.4 1 07/18/2019 14:53 WG1313450
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 33.1 1.88 5.65 50 07/19/2019 02:35 WG1313524
Unadjusted C9-C12 Aliphatics 25.0 1.88 5.65 50 07/19/2019 02:35 WG1313524
Unadjusted C9-C10 Aromatics 13.1 1.88 5.65 50 07/19/2019 02:35 WG1313524
Total VPH 71.2 1.88 5.65 50 07/19/2019 02:35 WG1313524
(S) 2,5-Dibromotoluene(FID) 94.5 70.0-130 07/19/2019 02:35 WG1313524
(S) 2,5-Dibromotoluene(PID) 88.2 70.0-130 07/19/2019 02:35 WG1313524
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.000565 0.00283 1 07/18/2019 15:04 WG1313610
1,1,1-Trichloroethane U 0.000311 0.00283 1 07/18/2019 15:04 WG1313610
1,1,2,2-Tetrachloroethane U 0.000441 0.00283 1 07/18/2019 15:04 WG1313610
1,1,2-Trichloroethane U 0.000998 0.00283 1 07/18/2019 15:04 WG1313610
1,1,2-Trichlorotrifluoroethane U J0 0.000763 0.00283 1 07/18/2019 15:04 WG1313610
1,1-Dichloroethane U 0.000650 0.00283 1 07/18/2019 15:04 WG1313610
1,1-Dichloroethene U 0.000565 0.00283 1 07/18/2019 15:04 WG1313610
1,1-Dichloropropene U 0.000791 0.00283 1 07/18/2019 15:04 WG1313610
1,2,3-Trichlorobenzene U 0.000707 0.00283 1 07/18/2019 15:04 WG1313610
1,2,3-Trichloropropane U 0.00577 0.0141 1 07/18/2019 15:04 WG1313610
1,2,3-Trimethylbenzene 2.37 0.00130 0.00565 1 07/18/2019 15:04 WG1313610
1,2,4-Trichlorobenzene U 0.00545 0.0141 1 07/18/2019 15:04 WG1313610
1,2,4-Trimethylbenzene 2.89 0.0262 0.113 20 07/19/2019 13:19 WG1314146
1,2-Dibromo-3-Chloropropane U 0.00577 0.0283 1 07/18/2019 15:04 WG1313610
1,2-Dibromoethane U 0.000594 0.00283 1 07/18/2019 15:04 WG1313610
1,2-Dichlorobenzene U 0.00164 0.00565 1 07/18/2019 15:04 WG1313610
1,2-Dichloroethane U 0.000537 0.00283 1 07/18/2019 15:04 WG1313610
1,2-Dichloropropane U 0.00144 0.00565 1 07/18/2019 15:04 WG1313610
1,3,5-Trimethylbenzene 2.42 0.00122 0.00565 1 07/18/2019 15:04 WG1313610
1,3-Dichlorobenzene U 0.00192 0.00565 1 07/18/2019 15:04 WG1313610
1,3-Dichloropropane U 0.00198 0.00565 1 07/18/2019 15:04 WG1313610
1,4-Dichlorobenzene 0.00818 0.00223 0.00565 1 07/18/2019 15:04 WG1313610
2,2-Dichloropropane U 0.000897 0.00283 1 07/18/2019 15:04 WG1313610
2-Butanone (MEK)U 0.0141 0.0283 1 07/18/2019 15:04 WG1313610
2-Chlorotoluene U 0.00104 0.00283 1 07/18/2019 15:04 WG1313610
4-Chlorotoluene U 0.00128 0.00565 1 07/18/2019 15:04 WG1313610
4-Methyl-2-pentanone (MIBK) U 0.0113 0.0283 1 07/18/2019 15:04 WG1313610
Acetone U 0.0155 0.0283 1 07/18/2019 15:04 WG1313610
Acrylonitrile U 0.00215 0.0141 1 07/18/2019 15:04 WG1313610
Benzene 0.656 0.000452 0.00113 1 07/18/2019 15:04 WG1313610
Bromobenzene U 0.00119 0.0141 1 07/18/2019 15:04 WG1313610
Bromodichloromethane U 0.000891 0.00283 1 07/18/2019 15:04 WG1313610
Bromoform U 0.00676 0.0283 1 07/18/2019 15:04 WG1313610
Bromomethane U 0.00418 0.0141 1 07/18/2019 15:04 WG1313610
Carbon tetrachloride U 0.00122 0.00565 1 07/18/2019 15:04 WG1313610
Chlorobenzene U 0.000648 0.00283 1 07/18/2019 15:04 WG1313610
Chlorodibromomethane U 0.000509 0.00283 1 07/18/2019 15:04 WG1313610
Chloroethane U J0 0.00122 0.00565 1 07/18/2019 15:04 WG1313610
Chloroform U 0.000469 0.00283 1 07/18/2019 15:04 WG1313610
Chloromethane U 0.00157 0.0141 1 07/18/2019 15:04 WG1313610
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 8 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 8 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1118060
MW-1 (15')
Collected date/time: 07/10/19 15:25
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Dibromomethane U 0.00113 0.00565 1 07/18/2019 15:04 WG1313610
Dichlorodifluoromethane U 0.000925 0.00283 1 07/18/2019 15:04 WG1313610
Di-isopropyl ether U 0.000396 0.00113 1 07/18/2019 15:04 WG1313610
Ethylbenzene 2.51 0.000599 0.00283 1 07/18/2019 15:04 WG1313610
Hexachloro-1,3-butadiene U 0.0144 0.0283 1 07/18/2019 15:04 WG1313610
Isopropylbenzene 0.299 0.000976 0.00283 1 07/18/2019 15:04 WG1313610
Methyl tert-butyl ether U 0.000334 0.00113 1 07/18/2019 15:04 WG1313610
Methylene Chloride U 0.00751 0.0283 1 07/18/2019 15:04 WG1313610
Naphthalene 1.35 0.00353 0.0141 1 07/18/2019 15:04 WG1313610
Styrene U 0.00309 0.0141 1 07/18/2019 15:04 WG1313610
Tetrachloroethene U 0.000791 0.00283 1 07/18/2019 15:04 WG1313610
Toluene 4.43 0.0283 0.113 20 07/19/2019 13:19 WG1314146
Trichloroethene U 0.000452 0.00113 1 07/18/2019 15:04 WG1313610
Trichlorofluoromethane U 0.000565 0.00283 1 07/18/2019 15:04 WG1313610
Vinyl chloride U 0.000772 0.00283 1 07/18/2019 15:04 WG1313610
Xylenes, Total 12.6 0.00540 0.00735 1 07/18/2019 15:04 WG1313610
cis-1,2-Dichloroethene U 0.000780 0.00283 1 07/18/2019 15:04 WG1313610
cis-1,3-Dichloropropene U 0.000767 0.00283 1 07/18/2019 15:04 WG1313610
n-Butylbenzene 0.445 0.00434 0.0141 1 07/18/2019 15:04 WG1313610
n-Propylbenzene 1.35 0.00133 0.00565 1 07/18/2019 15:04 WG1313610
p-Isopropyltoluene 0.0751 0.00263 0.00565 1 07/18/2019 15:04 WG1313610
sec-Butylbenzene 0.149 0.00286 0.0141 1 07/18/2019 15:04 WG1313610
tert-Butylbenzene U 0.00175 0.00565 1 07/18/2019 15:04 WG1313610
trans-1,2-Dichloroethene U 0.00162 0.00565 1 07/18/2019 15:04 WG1313610
trans-1,3-Dichloropropene U 0.00173 0.00565 1 07/18/2019 15:04 WG1313610
(S) Toluene-d8 95.5 75.0-131 07/18/2019 15:04 WG1313610
(S) Toluene-d8 102 75.0-131 07/19/2019 13:19 WG1314146
(S) 4-Bromofluorobenzene 93.7 67.0-138 07/18/2019 15:04 WG1313610
(S) 4-Bromofluorobenzene 98.5 67.0-138 07/19/2019 13:19 WG1314146
(S) 1,2-Dichloroethane-d4 104 70.0-130 07/18/2019 15:04 WG1313610
(S) 1,2-Dichloroethane-d4 114 70.0-130 07/19/2019 13:19 WG1314146
TPH by Method MADEPE
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 121 7.36 22.0 3 07/17/2019 15:21 WG1312529
Unadjusted C19-C36 Aliphatics U 7.36 22.0 3 07/17/2019 15:21 WG1312529
Unadjusted C11-C22 Aromatics 68.3 7.36 22.0 3 07/17/2019 15:43 WG1312529
Unadjusted Total Petroleum
Hydrocarbons 189 7.36 22.0 3 07/17/2019 15:43 WG1312529
(S) o-Terphenyl 73.1 40.0-140 07/17/2019 15:43 WG1312529
(S) 1-Chloro-octadecane 86.3 40.0-140 07/17/2019 15:21 WG1312529
(S) 2-Fluorobiphenyl 81.9 40.0-140 07/17/2019 15:43 WG1312529
(S) 2-Bromonaphthalene 76.9 40.0-140 07/17/2019 15:43 WG1312529
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0239 J 0.00726 0.0377 1 07/19/2019 04:35 WG1313771
Acenaphthylene U 0.00759 0.0377 1 07/19/2019 04:35 WG1313771
Anthracene U 0.00715 0.0377 1 07/19/2019 04:35 WG1313771
Benzidine U 0.0720 0.377 1 07/19/2019 04:35 WG1313771
Benzo(a)anthracene U 0.00484 0.0377 1 07/19/2019 04:35 WG1313771
Benzo(b)fluoranthene U 0.00786 0.0377 1 07/19/2019 04:35 WG1313771
Benzo(k)fluoranthene U 0.00658 0.0377 1 07/19/2019 04:35 WG1313771
Benzo(g,h,i)perylene U 0.00815 0.0377 1 07/19/2019 04:35 WG1313771
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 9 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 9 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1118060
MW-1 (15')
Collected date/time: 07/10/19 15:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Benzo(a)pyrene U 0.00620 0.0377 1 07/19/2019 04:35 WG1313771
Bis(2-chlorethoxy)methane U 0.00871 0.377 1 07/19/2019 04:35 WG1313771
Bis(2-chloroethyl)ether U 0.0101 0.377 1 07/19/2019 04:35 WG1313771
Bis(2-chloroisopropyl)ether U 0.00859 0.377 1 07/19/2019 04:35 WG1313771
4-Bromophenyl-phenylether U 0.0129 0.377 1 07/19/2019 04:35 WG1313771
2-Chloronaphthalene U 0.00722 0.0377 1 07/19/2019 04:35 WG1313771
4-Chlorophenyl-phenylether U 0.00709 0.377 1 07/19/2019 04:35 WG1313771
Chrysene U 0.00628 0.0377 1 07/19/2019 04:35 WG1313771
Dibenz(a,h)anthracene U 0.00928 0.0377 1 07/19/2019 04:35 WG1313771
3,3-Dichlorobenzidine U 0.0898 0.377 1 07/19/2019 04:35 WG1313771
2,4-Dinitrotoluene U 0.00686 0.377 1 07/19/2019 04:35 WG1313771
2,6-Dinitrotoluene U 0.00833 0.377 1 07/19/2019 04:35 WG1313771
Fluoranthene 0.00589 J 0.00561 0.0377 1 07/19/2019 04:35 WG1313771
Fluorene 0.0270 J 0.00771 0.0377 1 07/19/2019 04:35 WG1313771
Hexachlorobenzene U 0.00968 0.377 1 07/19/2019 04:35 WG1313771
Hexachloro-1,3-butadiene U 0.0113 0.377 1 07/19/2019 04:35 WG1313771
Hexachlorocyclopentadiene U 0.0664 0.377 1 07/19/2019 04:35 WG1313771
Hexachloroethane U 0.0152 0.377 1 07/19/2019 04:35 WG1313771
Indeno(1,2,3-cd)pyrene U 0.00873 0.0377 1 07/19/2019 04:35 WG1313771
Isophorone U 0.00590 0.377 1 07/19/2019 04:35 WG1313771
Naphthalene 4.43 0.0503 0.189 5 07/19/2019 11:05 WG1313771
Nitrobenzene U 0.00786 0.377 1 07/19/2019 04:35 WG1313771
n-Nitrosodimethylamine U 0.0732 0.377 1 07/19/2019 04:35 WG1313771
n-Nitrosodiphenylamine U 0.102 0.377 1 07/19/2019 04:35 WG1313771
n-Nitrosodi-n-propylamine U 0.0102 0.377 1 07/19/2019 04:35 WG1313771
Phenanthrene 0.0367 J 0.00597 0.0377 1 07/19/2019 04:35 WG1313771
Benzylbutyl phthalate U 0.0116 0.377 1 07/19/2019 04:35 WG1313771
Bis(2-ethylhexyl)phthalate U 0.0136 0.377 1 07/19/2019 04:35 WG1313771
Di-n-butyl phthalate U 0.0123 0.377 1 07/19/2019 04:35 WG1313771
Diethyl phthalate U 0.00781 0.377 1 07/19/2019 04:35 WG1313771
Dimethyl phthalate U 0.00611 0.377 1 07/19/2019 04:35 WG1313771
Di-n-octyl phthalate U 0.0103 0.377 1 07/19/2019 04:35 WG1313771
Pyrene U 0.0139 0.0377 1 07/19/2019 04:35 WG1313771
1,2,4-Trichlorobenzene U 0.00990 0.377 1 07/19/2019 04:35 WG1313771
4-Chloro-3-methylphenol U 0.00539 0.377 1 07/19/2019 04:35 WG1313771
2-Chlorophenol U 0.00940 0.377 1 07/19/2019 04:35 WG1313771
2,4-Dichlorophenol U 0.00843 0.377 1 07/19/2019 04:35 WG1313771
2,4-Dimethylphenol U 0.0533 0.377 1 07/19/2019 04:35 WG1313771
4,6-Dinitro-2-methylphenol U 0.140 0.377 1 07/19/2019 04:35 WG1313771
2,4-Dinitrophenol U 0.111 0.377 1 07/19/2019 04:35 WG1313771
2-Nitrophenol U 0.0147 0.377 1 07/19/2019 04:35 WG1313771
4-Nitrophenol U 0.0594 0.377 1 07/19/2019 04:35 WG1313771
Pentachlorophenol U 0.0543 0.377 1 07/19/2019 04:35 WG1313771
Phenol U 0.00786 0.377 1 07/19/2019 04:35 WG1313771
2,4,6-Trichlorophenol U 0.00881 0.377 1 07/19/2019 04:35 WG1313771
(S) 2-Fluorophenol 64.0 12.0-120 07/19/2019 11:05 WG1313771
(S) 2-Fluorophenol 75.8 12.0-120 07/19/2019 04:35 WG1313771
(S) Phenol-d5 69.5 10.0-120 07/19/2019 04:35 WG1313771
(S) Phenol-d5 57.8 10.0-120 07/19/2019 11:05 WG1313771
(S) Nitrobenzene-d5 55.5 10.0-122 07/19/2019 11:05 WG1313771
(S) Nitrobenzene-d5 61.0 10.0-122 07/19/2019 04:35 WG1313771
(S) 2-Fluorobiphenyl 62.2 15.0-120 07/19/2019 04:35 WG1313771
(S) 2-Fluorobiphenyl 54.3 15.0-120 07/19/2019 11:05 WG1313771
(S) 2,4,6-Tribromophenol 76.5 10.0-127 07/19/2019 04:35 WG1313771
(S) 2,4,6-Tribromophenol 63.7 10.0-127 07/19/2019 11:05 WG1313771
(S) p-Terphenyl-d14 61.3 10.0-120 07/19/2019 11:05 WG1313771
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 10 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 10 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1118060
MW-1 (15')
Collected date/time: 07/10/19 15:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
(S) p-Terphenyl-d14 75.0 10.0-120 07/19/2019 04:35 WG1313771
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 11 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 11 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1118060
MW-01
Collected date/time: 07/11/19 07:25
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 38200 6660 20000 200 07/17/2019 21:57 WG1313062
Unadjusted C9-C12 Aliphatics 31300 6660 20000 200 07/17/2019 21:57 WG1313062
Unadjusted C9-C10 Aromatics 13600 J 6660 20000 200 07/17/2019 21:57 WG1313062
Total VPH 83100 6660 20000 200 07/17/2019 21:57 WG1313062
(S) 2,5-Dibromotoluene(FID) 90.2 70.0-130 07/17/2019 21:57 WG1313062
(S) 2,5-Dibromotoluene(PID) 85.0 70.0-130 07/17/2019 21:57 WG1313062
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 2650 33.1 100 100 07/18/2019 11:03 WG1313111
Di-isopropyl ether U 32.0 100 100 07/18/2019 11:03 WG1313111
Ethylbenzene 2690 38.4 100 100 07/18/2019 11:03 WG1313111
Methyl tert-butyl ether U 36.7 100 100 07/18/2019 11:03 WG1313111
Naphthalene 798 100 500 100 07/18/2019 11:03 WG1313111
Toluene 14200 41.2 100 100 07/18/2019 11:03 WG1313111
m&p-Xylenes 9520 71.9 200 100 07/18/2019 11:03 WG1313111
o-Xylene 4580 34.1 100 100 07/18/2019 11:03 WG1313111
(S) Toluene-d8 109 80.0-120 07/18/2019 11:03 WG1313111
(S) 4-Bromofluorobenzene 98.9 77.0-126 07/18/2019 11:03 WG1313111
(S) 1,2-Dichloroethane-d4 89.9 70.0-130 07/18/2019 11:03 WG1313111
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 530 34.6 104 1.04 07/16/2019 14:19 WG1311838
Unadjusted C19-C36 Aliphatics U 34.6 104 1.04 07/16/2019 14:19 WG1311838
Unadjusted C11-C22 Aromatics 1420 34.6 104 1.04 07/16/2019 14:41 WG1311838
Unadjusted Total Petroleum
Hydrocarbons 1950 34.6 104 1.04 07/16/2019 14:41 WG1311838
(S) o-Terphenyl 55.8 40.0-140 07/16/2019 14:41 WG1311838
(S) 1-Chloro-octadecane 52.6 40.0-140 07/16/2019 14:19 WG1311838
(S) 2-Fluorobiphenyl 84.7 40.0-140 07/16/2019 14:41 WG1311838
(S) 2-Bromonaphthalene 79.3 40.0-140 07/16/2019 14:41 WG1311838
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,2,4-Trichlorobenzene U J4 0.355 10.0 1 07/19/2019 01:44 WG1311664
1,2-Dichlorobenzene U J4 3.29 10.0 1 07/19/2019 01:44 WG1311664
1,3-Dichlorobenzene U J4 0.383 10.0 1 07/19/2019 01:44 WG1311664
1,4-Dichlorobenzene U J4 0.401 10.0 1 07/19/2019 01:44 WG1311664
2,4-Dinitrotoluene U 1.65 10.0 1 07/19/2019 01:44 WG1311664
2,6-Dinitrotoluene U 0.279 10.0 1 07/19/2019 01:44 WG1311664
2-Chloronaphthalene U J4 0.330 1.00 1 07/19/2019 01:44 WG1311664
3,3-Dichlorobenzidine U 2.02 10.0 1 07/19/2019 01:44 WG1311664
4-Bromophenyl-phenylether U 0.335 10.0 1 07/19/2019 01:44 WG1311664
4-Chlorophenyl-phenylether U 0.303 10.0 1 07/19/2019 01:44 WG1311664
Acenaphthene U J4 0.316 1.00 1 07/19/2019 01:44 WG1311664
Acenaphthylene U 0.309 1.00 1 07/19/2019 01:44 WG1311664
Anthracene U 0.291 1.00 1 07/19/2019 01:44 WG1311664
Benzidine U J3 4.32 10.0 1 07/19/2019 01:44 WG1311664
Benzo(a)anthracene U 0.0975 1.00 1 07/19/2019 01:44 WG1311664
Benzo(a)pyrene U 0.340 1.00 1 07/19/2019 01:44 WG1311664
Benzo(b)fluoranthene U 0.0896 1.00 1 07/19/2019 01:44 WG1311664
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 12 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 12 of 45
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1118060
MW-01
Collected date/time: 07/11/19 07:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzo(g,h,i)perylene U 0.161 1.00 1 07/19/2019 01:44 WG1311664
Benzo(k)fluoranthene U 0.355 1.00 1 07/19/2019 01:44 WG1311664
Bis(2-chlorethoxy)methane U 0.329 10.0 1 07/19/2019 01:44 WG1311664
Bis(2-chloroisopropyl)ether U J4 0.445 10.0 1 07/19/2019 01:44 WG1311664
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 07/19/2019 01:44 WG1311664
Benzylbutyl phthalate U 0.275 3.00 1 07/19/2019 01:44 WG1311664
Chrysene U 0.332 1.00 1 07/19/2019 01:44 WG1311664
Di-n-butyl phthalate U 0.266 3.00 1 07/19/2019 01:44 WG1311664
Di-n-octyl phthalate U 0.278 3.00 1 07/19/2019 01:44 WG1311664
Dibenz(a,h)anthracene U 0.279 1.00 1 07/19/2019 01:44 WG1311664
Diethyl phthalate U 0.282 3.00 1 07/19/2019 01:44 WG1311664
Dimethyl phthalate U 0.283 3.00 1 07/19/2019 01:44 WG1311664
Fluoranthene U 0.310 1.00 1 07/19/2019 01:44 WG1311664
Fluorene U J4 0.323 1.00 1 07/19/2019 01:44 WG1311664
Hexachlorobenzene U 0.341 1.00 1 07/19/2019 01:44 WG1311664
Hexachloro-1,3-butadiene U J4 0.329 10.0 1 07/19/2019 01:44 WG1311664
Hexachlorocyclopentadiene U 2.33 10.0 1 07/19/2019 01:44 WG1311664
Hexachloroethane U J4 0.365 10.0 1 07/19/2019 01:44 WG1311664
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 07/19/2019 01:44 WG1311664
Isophorone U 0.272 10.0 1 07/19/2019 01:44 WG1311664
n-Nitrosodi-n-propylamine U 0.403 10.0 1 07/19/2019 01:44 WG1311664
n-Nitrosodimethylamine U 1.26 10.0 1 07/19/2019 01:44 WG1311664
n-Nitrosodiphenylamine U 1.19 10.0 1 07/19/2019 01:44 WG1311664
Naphthalene 206 0.372 1.00 1 07/19/2019 01:44 WG1311664
Nitrobenzene U J4 0.367 10.0 1 07/19/2019 01:44 WG1311664
Phenanthrene U 0.366 1.00 1 07/19/2019 01:44 WG1311664
Pyrene U 0.330 1.00 1 07/19/2019 01:44 WG1311664
(S) 2-Fluorophenol 13.7 10.0-120 07/19/2019 01:44 WG1311664
(S) Phenol-d5 11.9 8.00-424 07/19/2019 01:44 WG1311664
(S) Nitrobenzene-d5 25.9 15.0-314 07/19/2019 01:44 WG1311664
(S) 2-Fluorobiphenyl 34.0 22.0-127 07/19/2019 01:44 WG1311664
(S) 2,4,6-Tribromophenol 54.2 10.0-153 07/19/2019 01:44 WG1311664
(S) p-Terphenyl-d14 67.1 29.0-141 07/19/2019 01:44 WG1311664
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier MDL RDL Dilution Analysis Batch CAS #
Analyte ug/l ug/l ug/l date / time
Toluene 613 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000108-88-3
P-Xylene 466 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000106-42-3
Benzene, 1,2,3-Trimethyl- 453 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000526-73-8
Benzene, 1-Ethyl-2-Methyl- 365 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000611-14-3
Ethylbenzene 318 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000100-41-4
Benzene 127 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000071-43-2
Benzene, Propyl-81.5 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000103-65-1
Unknown-02 32.4 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000077-74-7
Cyclopentanol, 1-Methyl- 28.1 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 001462-03-9
Benzene, (1-Methylethyl)- 27.4 J N 0.000 0.000 1 07/19/2019 01:44 WG1311664 000098-82-8
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313450
Total Solids by Method 2540 G-2011 L1118060-01,02
Method Blank (MB)
(MB) R3432208-1 07/18/19 14:53
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1118064-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1118064-04 07/18/19 14:53 • (DUP) R3432208-3 07/18/19 14:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 90.3 89.8 1 0.553 10
Laboratory Control Sample (LCS)
(LCS) R3432208-2 07/18/19 14:53
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313062
Volatile Petroleum Hydrocarbons by Method MADEPV L1118060-03
Method Blank (MB)
(MB) R3431947-3 07/17/19 13:12
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 90.0 70.0-130
(S) 2,5-Dibromotoluene(PID) 84.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431947-1 07/17/19 11:00 • (LCSD) R3431947-2 07/17/19 11:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1110 1070 92.4 89.2 70.0-130 3.61 25
Unadjusted C9-C12 Aliphatics 1400 1440 1400 103 99.9 70.0-130 3.17 25
Unadjusted C9-C10 Aromatics 200 187 182 93.3 91.0 70.0-130 2.46 25
Total VPH 2800 2740 2650 97.8 94.7 70.0-130 3.15 25
(S) 2,5-Dibromotoluene(FID) 93.9 94.0 70.0-130
(S) 2,5-Dibromotoluene(PID) 90.9 91.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313524
Volatile Petroleum Hydrocarbons by Method MADEPV L1118060-01,02
Method Blank (MB)
(MB) R3432273-3 07/19/19 02:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics U 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Total VPH 2.33 J 1.67 5.00
(S) 2,5-Dibromotoluene(FID) 93.7 70.0-130
(S) 2,5-Dibromotoluene(PID) 86.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3432273-1 07/18/19 23:17 • (LCSD) R3432273-2 07/18/19 23:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.20 1.14 1.09 95.3 90.7 70.0-130 4.97 25
Unadjusted C9-C12 Aliphatics 1.40 1.55 1.51 110 108 70.0-130 2.36 25
Unadjusted C9-C10 Aromatics 0.200 0.195 0.191 97.3 95.6 70.0-130 1.82 25
Total VPH 2.80 2.88 2.79 103 99.7 70.0-130 2.97 25
(S) 2,5-Dibromotoluene(FID) 96.0 96.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 90.5 91.0 70.0-130
L1118060-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1118060-01 07/19/19 03:07 • (MS) R3432273-4 07/19/19 03:40 • (MSD) R3432273-5 07/19/19 04:14
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.45 491 512 574 14.9 57.4 100 70.0-130 J6 J6 11.3 25
Unadjusted C9-C12 Aliphatics 1.69 376 417 518 24.3 84.3 100 70.0-130 J6 21.6 25
Unadjusted C9-C10 Aromatics 0.241 233 229 245 0.000 51.3 100 70.0-130 V E V 6.83 25
Total VPH 3.38 1100 1160 1340 17.5 70.4 100 70.0-130 J6 14.3 25
(S) 2,5-Dibromotoluene(FID) 101 104 70.0-130
(S) 2,5-Dibromotoluene(PID) 86.0 88.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313111
Volatile Organic Compounds (GC/MS) by Method 602MS L1118060-03
Method Blank (MB)
(MB) R3431987-3 07/18/19 10:03
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
Toluene U 0.412 1.00
o-Xylene U 0.341 1.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 98.3 77.0-126
(S) 1,2-Dichloroethane-d4 92.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431987-1 07/18/19 08:44 • (LCSD) R3431987-2 07/18/19 09:04
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 22.1 22.3 88.6 89.1 70.0-123 0.633 20
Di-isopropyl ether 25.0 23.8 23.6 95.4 94.4 58.0-138 1.07 20
Ethylbenzene 25.0 23.9 24.1 95.6 96.3 79.0-123 0.743 20
Methyl tert-butyl ether 25.0 23.7 23.6 94.7 94.4 68.0-125 0.318 20
Naphthalene 25.0 21.4 22.4 85.8 89.4 54.0-135 4.19 20
Toluene 25.0 24.2 24.2 97.0 96.8 79.0-120 0.176 20
o-Xylene 25.0 24.0 24.3 95.8 97.4 80.0-122 1.62 20
m&p-Xylenes 50.0 48.1 48.4 96.1 96.9 80.0-122 0.768 20
(S) Toluene-d8 107 107 80.0-120
(S) 4-Bromofluorobenzene 96.6 99.5 77.0-126
(S) 1,2-Dichloroethane-d4 95.3 97.6 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
Method Blank (MB)
(MB) R3432007-2 07/18/19 14:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone 0.0190 J 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
Dibromomethane U 0.00100 0.00500
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Hexachloro-1,3-butadiene U 0.0127 0.0250
Isopropylbenzene U 0.000863 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
Method Blank (MB)
(MB) R3432007-2 07/18/19 14:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)0.0154 J 0.0125 0.0250
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000675 0.00250
1,2,3-Trichlorobenzene U 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,3-Trimethylbenzene U 0.00115 0.00500
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 99.2 75.0-131
(S) 4-Bromofluorobenzene 95.9 67.0-138
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3432007-1 07/18/19 12:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.629 101 10.0-160
Acrylonitrile 0.625 0.631 101 45.0-153
Benzene 0.125 0.121 97.1 70.0-123
Bromobenzene 0.125 0.129 103 73.0-121
Bromodichloromethane 0.125 0.128 102 73.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
Laboratory Control Sample (LCS)
(LCS) R3432007-1 07/18/19 12:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.101 80.6 64.0-132
Bromomethane 0.125 0.102 81.9 56.0-147
n-Butylbenzene 0.125 0.136 109 68.0-135
sec-Butylbenzene 0.125 0.129 104 74.0-130
tert-Butylbenzene 0.125 0.127 102 75.0-127
Carbon tetrachloride 0.125 0.126 101 66.0-128
Chlorobenzene 0.125 0.125 99.8 76.0-128
Chlorodibromomethane 0.125 0.127 101 74.0-127
Chloroethane 0.125 0.0946 75.7 61.0-134
Chloroform 0.125 0.125 99.9 72.0-123
Chloromethane 0.125 0.120 95.6 51.0-138
2-Chlorotoluene 0.125 0.130 104 75.0-124
4-Chlorotoluene 0.125 0.129 103 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.127 101 59.0-130
1,2-Dibromoethane 0.125 0.118 94.3 74.0-128
Dibromomethane 0.125 0.127 102 75.0-122
1,2-Dichlorobenzene 0.125 0.129 103 76.0-124
1,3-Dichlorobenzene 0.125 0.127 102 76.0-125
1,4-Dichlorobenzene 0.125 0.126 101 77.0-121
Dichlorodifluoromethane 0.125 0.122 97.6 43.0-156
1,1-Dichloroethane 0.125 0.121 96.9 70.0-127
1,2-Dichloroethane 0.125 0.127 101 65.0-131
1,1-Dichloroethene 0.125 0.109 87.1 65.0-131
cis-1,2-Dichloroethene 0.125 0.116 93.1 73.0-125
trans-1,2-Dichloroethene 0.125 0.112 89.6 71.0-125
1,2-Dichloropropane 0.125 0.120 96.1 74.0-125
1,1-Dichloropropene 0.125 0.126 101 73.0-125
1,3-Dichloropropane 0.125 0.131 105 80.0-125
cis-1,3-Dichloropropene 0.125 0.125 100 76.0-127
trans-1,3-Dichloropropene 0.125 0.131 104 73.0-127
2,2-Dichloropropane 0.125 0.119 94.8 59.0-135
Di-isopropyl ether 0.125 0.133 107 60.0-136
Ethylbenzene 0.125 0.118 94.3 74.0-126
Hexachloro-1,3-butadiene 0.125 0.111 88.8 57.0-150
Isopropylbenzene 0.125 0.121 97.1 72.0-127
p-Isopropyltoluene 0.125 0.132 105 72.0-133
2-Butanone (MEK)0.625 0.744 119 30.0-160
Methylene Chloride 0.125 0.111 88.9 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.759 121 56.0-143
Methyl tert-butyl ether 0.125 0.115 91.8 66.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
Laboratory Control Sample (LCS)
(LCS) R3432007-1 07/18/19 12:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.121 97.1 59.0-130
n-Propylbenzene 0.125 0.130 104 74.0-126
Styrene 0.125 0.120 95.8 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.130 104 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.136 109 68.0-128
Tetrachloroethene 0.125 0.114 91.3 70.0-136
Toluene 0.125 0.122 97.9 75.0-121
1,1,2-Trichlorotrifluoroethane 0.125 0.0937 75.0 61.0-139
1,2,3-Trichlorobenzene 0.125 0.109 87.2 59.0-139
1,2,4-Trichlorobenzene 0.125 0.113 90.2 62.0-137
1,1,1-Trichloroethane 0.125 0.128 103 69.0-126
1,1,2-Trichloroethane 0.125 0.121 96.9 78.0-123
Trichloroethene 0.125 0.115 92.3 76.0-126
Trichlorofluoromethane 0.125 0.105 84.0 61.0-142
1,2,3-Trichloropropane 0.125 0.140 112 67.0-129
1,2,3-Trimethylbenzene 0.125 0.133 107 74.0-124
1,2,4-Trimethylbenzene 0.125 0.128 102 70.0-126
1,3,5-Trimethylbenzene 0.125 0.131 104 73.0-127
Vinyl chloride 0.125 0.100 80.4 63.0-134
Xylenes, Total 0.375 0.363 96.8 72.0-127
(S) Toluene-d8 97.1 75.0-131
(S) 4-Bromofluorobenzene 92.7 67.0-138
(S) 1,2-Dichloroethane-d4 103 70.0-130
L1119490-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1119490-03 07/18/19 21:49 • (MS) R3432007-3 07/18/19 22:34 • (MSD) R3432007-4 07/18/19 22:55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 ND 0.484 0.397 74.7 60.8 1 10.0-160 19.7 40
Acrylonitrile 0.625 ND 0.629 0.576 101 92.1 1 10.0-160 8.86 40
Benzene 0.125 ND 0.0559 0.0992 44.3 78.9 1 10.0-149 J3 55.9 37
Bromobenzene 0.125 ND 0.0898 0.133 71.9 106 1 10.0-156 J3 38.4 38
Bromodichloromethane 0.125 ND 0.0781 0.116 62.5 92.4 1 10.0-143 J3 38.7 37
Bromoform 0.125 ND 0.0937 0.101 75.0 80.4 1 10.0-146 7.04 36
Bromomethane 0.125 ND 0.0259 0.0448 20.7 35.8 1 10.0-149 J3 53.5 38
n-Butylbenzene 0.125 ND 0.0651 0.116 52.1 92.9 1 10.0-160 J3 56.2 40
sec-Butylbenzene 0.125 ND 0.0639 0.117 51.1 93.5 1 10.0-159 J3 58.6 39
tert-Butylbenzene 0.125 ND 0.0654 0.118 52.3 94.7 1 10.0-156 J3 57.6 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
L1119490-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1119490-03 07/18/19 21:49 • (MS) R3432007-3 07/18/19 22:34 • (MSD) R3432007-4 07/18/19 22:55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.125 ND 0.0424 0.0932 34.0 74.5 1 10.0-145 J3 74.8 37
Chlorobenzene 0.125 ND 0.0687 0.112 54.9 89.9 1 10.0-152 J3 48.3 39
Chlorodibromomethane 0.125 ND 0.102 0.121 81.7 96.9 1 10.0-146 17.0 37
Chloroethane 0.125 ND 0.0228 0.0478 18.2 38.2 1 10.0-146 J3 70.9 40
Chloroform 0.125 ND 0.0599 0.104 47.9 83.2 1 10.0-146 J3 53.8 37
Chloromethane 0.125 ND 0.0366 0.0749 29.3 60.0 1 10.0-159 J3 68.8 37
2-Chlorotoluene 0.125 ND 0.0759 0.131 60.7 104 1 10.0-159 J3 53.0 38
4-Chlorotoluene 0.125 ND 0.0734 0.125 58.7 99.8 1 10.0-155 J3 51.9 39
1,2-Dibromo-3-Chloropropane 0.125 ND 0.129 0.113 103 90.8 1 10.0-151 12.7 39
1,2-Dibromoethane 0.125 ND 0.104 0.116 82.9 93.1 1 10.0-148 11.7 34
Dibromomethane 0.125 ND 0.0969 0.116 77.5 92.7 1 10.0-147 17.9 35
1,2-Dichlorobenzene 0.125 ND 0.0930 0.128 74.4 102 1 10.0-155 31.5 37
1,3-Dichlorobenzene 0.125 ND 0.0789 0.124 63.1 99.3 1 10.0-153 J3 44.5 38
1,4-Dichlorobenzene 0.125 ND 0.0842 0.127 67.4 102 1 10.0-151 J3 40.8 38
Dichlorodifluoromethane 0.125 ND 0.0330 0.0908 26.4 72.6 1 10.0-160 J3 93.2 35
1,1-Dichloroethane 0.125 ND 0.0527 0.0943 42.2 75.4 1 10.0-147 J3 56.6 37
1,2-Dichloroethane 0.125 ND 0.0906 0.112 72.5 89.3 1 10.0-148 20.8 35
1,1-Dichloroethene 0.125 ND 0.0205 0.0531 16.4 42.5 1 10.0-155 J3 88.8 37
cis-1,2-Dichloroethene 0.125 ND 0.0585 0.102 46.8 81.2 1 10.0-149 J3 53.8 37
trans-1,2-Dichloroethene 0.125 ND 0.0384 0.0804 30.7 64.3 1 10.0-150 J3 70.7 37
1,2-Dichloropropane 0.125 ND 0.0679 0.110 54.3 87.7 1 10.0-148 J3 47.1 37
1,1-Dichloropropene 0.125 ND 0.0394 0.0948 31.5 75.9 1 10.0-153 J3 82.6 35
1,3-Dichloropropane 0.125 ND 0.106 0.122 84.6 97.5 1 10.0-154 14.2 35
cis-1,3-Dichloropropene 0.125 ND 0.0794 0.113 63.5 90.5 1 10.0-151 35.1 37
trans-1,3-Dichloropropene 0.125 ND 0.0971 0.126 77.7 101 1 10.0-148 26.3 37
2,2-Dichloropropane 0.125 ND 0.0361 0.0754 28.9 60.3 1 10.0-138 J3 70.5 36
Di-isopropyl ether 0.125 ND 0.0868 0.123 69.4 98.7 1 10.0-147 34.8 36
Ethylbenzene 0.125 ND 0.0542 0.106 43.3 84.7 1 10.0-160 J3 64.6 38
Hexachloro-1,3-butadiene 0.125 ND 0.0386 0.0661 30.9 52.9 1 10.0-160 J3 52.6 40
Isopropylbenzene 0.125 ND 0.0519 0.108 41.5 86.5 1 10.0-155 J3 70.3 38
p-Isopropyltoluene 0.125 ND 0.0627 0.116 50.1 92.7 1 10.0-160 J3 59.6 40
2-Butanone (MEK)0.625 ND 0.741 0.703 116 110 1 10.0-160 5.27 40
Methylene Chloride 0.125 ND 0.0644 0.0959 51.5 76.7 1 10.0-141 J3 39.3 37
4-Methyl-2-pentanone (MIBK) 0.625 ND 0.742 0.712 119 114 1 10.0-160 4.20 35
Methyl tert-butyl ether 0.125 ND 0.0858 0.102 68.6 81.9 1 11.0-147 17.6 35
Naphthalene 0.125 ND 0.128 0.150 103 120 1 10.0-160 15.6 36
n-Propylbenzene 0.125 ND 0.0639 0.126 51.1 101 1 10.0-158 J3 65.6 38
Styrene 0.125 ND 0.0709 0.114 56.7 91.2 1 10.0-160 J3 46.6 40
1,1,1,2-Tetrachloroethane 0.125 ND 0.0828 0.122 66.3 97.7 1 10.0-149 38.4 39
1,1,2,2-Tetrachloroethane 0.125 ND 0.132 0.149 106 119 1 10.0-160 11.8 35
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 22 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 22 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313610
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-01,02
L1119490-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1119490-03 07/18/19 21:49 • (MS) R3432007-3 07/18/19 22:34 • (MSD) R3432007-4 07/18/19 22:55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Tetrachloroethene 0.125 0.00885 0.114 0.186 84.5 141 1 10.0-156 J3 47.4 39
Toluene 0.125 ND 0.0567 0.104 45.3 83.4 1 10.0-156 J3 59.1 38
1,1,2-Trichlorotrifluoroethane 0.125 ND 0.0211 0.0594 16.9 47.5 1 10.0-160 J3 95.0 36
1,2,3-Trichlorobenzene 0.125 ND 0.0711 0.0892 56.9 71.4 1 10.0-160 22.6 40
1,2,4-Trichlorobenzene 0.125 ND 0.0658 0.0937 52.6 75.0 1 10.0-160 35.0 40
1,1,1-Trichloroethane 0.125 ND 0.0434 0.0945 34.7 75.6 1 10.0-144 J3 74.1 35
1,1,2-Trichloroethane 0.125 ND 0.103 0.123 82.3 98.1 1 10.0-160 17.6 35
Trichloroethene 0.125 ND 0.0749 0.109 59.9 87.5 1 10.0-156 37.4 38
Trichlorofluoromethane 0.125 ND 0.0259 0.0626 20.7 50.0 1 10.0-160 J3 82.9 40
1,2,3-Trichloropropane 0.125 ND 0.159 0.145 128 116 1 10.0-156 9.55 35
1,2,3-Trimethylbenzene 0.125 ND 0.0874 0.132 70.0 105 1 10.0-160 J3 40.3 36
1,2,4-Trimethylbenzene 0.125 ND 0.0813 0.133 64.0 106 1 10.0-160 J3 48.5 36
1,3,5-Trimethylbenzene 0.125 ND 0.0691 0.128 55.3 102 1 10.0-160 J3 59.8 38
Vinyl chloride 0.125 ND 0.0240 0.0676 19.2 54.1 1 10.0-160 J3 95.2 37
Xylenes, Total 0.375 ND 0.177 0.325 47.3 86.7 1 10.0-160 J3 58.8 38
(S) Toluene-d8 100 103 75.0-131
(S) 4-Bromofluorobenzene 96.0 96.7 67.0-138
(S) 1,2-Dichloroethane-d4 98.2 98.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 23 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 23 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1314146
Volatile Organic Compounds (GC/MS) by Method 8260D L1118060-02
Method Blank (MB)
(MB) R3432369-3 07/19/19 07:16
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Toluene U 0.00125 0.00500
1,2,4-Trimethylbenzene U 0.00116 0.00500
(S) Toluene-d8 101 75.0-131
(S) 4-Bromofluorobenzene 100 67.0-138
(S) 1,2-Dichloroethane-d4 112 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3432369-1 07/19/19 05:54 • (LCSD) R3432369-2 07/19/19 06:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Toluene 0.125 0.102 0.105 81.9 84.0 75.0-121 2.51 20
1,2,4-Trimethylbenzene 0.125 0.102 0.109 81.3 87.4 70.0-126 7.27 20
(S) Toluene-d8 98.6 99.6 75.0-131
(S) 4-Bromofluorobenzene 103 102 67.0-138
(S) 1,2-Dichloroethane-d4 119 117 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 24 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 24 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1311838
TPH by Method MADEPE L1118060-03
Method Blank (MB)
(MB) R3431176-1 07/16/19 12:08
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics 35.0 J 33.3 100
(S) 1-Chloro-octadecane 55.3 40.0-140
Method Blank (MB)
(MB) R3431176-4 07/16/19 13:14
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 80.4 40.0-140
(S) 2-Fluorobiphenyl 86.6 40.0-140
(S) 2-Bromonaphthalene 81.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431176-2 07/16/19 12:30 • (LCSD) R3431176-3 07/16/19 12:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 390 406 65.0 67.7 40.0-140 4.02 25
Unadjusted C19-C36 Aliphatics 800 713 750 89.1 93.8 40.0-140 5.06 25
(S) 1-Chloro-octadecane 56.0 60.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431176-5 07/16/19 13:36 • (LCSD) R3431176-6 07/16/19 13:58
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1400 1500 82.4 88.2 40.0-140 6.90 25
(S) o-Terphenyl 76.8 85.8 40.0-140
(S) 2-Fluorobiphenyl 84.7 89.8 40.0-140
(S) 2-Bromonaphthalene 80.4 85.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 25 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 25 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1312529
TPH by Method MADEPE L1118060-01,02
Method Blank (MB)
(MB) R3431889-1 07/17/19 12:48
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) 1-Chloro-octadecane 86.1 40.0-140
Method Blank (MB)
(MB) R3431889-4 07/17/19 13:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics 2.39 J 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) o-Terphenyl 75.4 40.0-140
(S) 2-Fluorobiphenyl 83.1 40.0-140
(S) 2-Bromonaphthalene 78.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431889-2 07/17/19 13:10 • (LCSD) R3431889-3 07/17/19 13:32
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 27.1 28.8 67.9 72.2 40.0-140 6.08 25
Unadjusted C19-C36 Aliphatics 53.2 45.9 46.2 86.3 86.8 40.0-140 0.651 25
(S) 1-Chloro-octadecane 80.8 82.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3431889-5 07/17/19 14:15 • (LCSD) R3431889-6 07/17/19 14:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 86.4 89.8 76.5 79.5 40.0-140 3.86 25
(S) o-Terphenyl 75.6 73.3 40.0-140
(S) 2-Fluorobiphenyl 81.6 83.3 40.0-140
(S) 2-Bromonaphthalene 79.5 80.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 26 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 26 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1312529
TPH by Method MADEPE L1118060-01,02
L1117642-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1117642-01 07/18/19 14:44 • (MS) R3432546-1 07/18/19 15:06 • (MSD) R3432546-2 07/18/19 15:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 42.8 50.8 74.9 63.2 56.4 29.1 12.5 40.0-140 J6 16.9 50
Unadjusted C19-C36 Aliphatics 57.0 452 480 412 48.9 0.000 12.5 40.0-140 V 15.4 50
(S) 1-Chloro-octadecane 79.5 76.2 40.0-140
L1117642-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1117642-01 07/18/19 14:44 • (MS) R3432546-4 07/18/19 16:12 • (MSD) R3432546-3 07/18/19 15:50
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 121 U 243 223 47.8 31.0 12.5 40.0-140 J6 8.74 50
(S) o-Terphenyl 77.3 77.7 40.0-140
(S) 2-Fluorobiphenyl 88.7 87.4 40.0-140
(S) 2-Bromonaphthalene 84.2 84.2 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 27 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 27 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1311664
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1118060-03
Method Blank (MB)
(MB) R3432436-3 07/19/19 01:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
1,2-Dichlorobenzene U 3.29 10.0
1,3-Dichlorobenzene U 0.383 10.0
1,4-Dichlorobenzene U 0.401 10.0
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 28 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 28 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1311664
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1118060-03
Method Blank (MB)
(MB) R3432436-3 07/19/19 01:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
(S) Nitrobenzene-d5 23.5 15.0-314
(S) 2-Fluorobiphenyl 28.3 22.0-127
(S) p-Terphenyl-d14 76.6 29.0-141
(S) Phenol-d5 11.8 8.00-424
(S) 2-Fluorophenol 19.4 10.0-120
(S) 2,4,6-Tribromophenol 41.2 10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3432436-1 07/19/19 00:55 • (LCSD) R3432436-2 07/19/19 01:17
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 21.5 24.3 43.0 48.6 47.0-145 J4 12.2 48
Acenaphthylene 50.0 21.2 24.2 42.4 48.4 33.0-145 13.2 74
Anthracene 50.0 32.2 34.2 64.4 68.4 27.0-133 6.02 66
Benzidine 100 12.3 5.08 12.3 5.08 1.00-120 J3 83.1 36
Benzo(a)anthracene 50.0 37.5 39.1 75.0 78.2 33.0-143 4.18 53
Benzo(b)fluoranthene 50.0 36.5 37.7 73.0 75.4 24.0-159 3.23 71
Benzo(k)fluoranthene 50.0 37.4 37.9 74.8 75.8 11.0-162 1.33 63
Benzo(g,h,i)perylene 50.0 36.4 38.2 72.8 76.4 1.00-219 4.83 97
Benzo(a)pyrene 50.0 35.1 36.2 70.2 72.4 17.0-163 3.09 72
Bis(2-chlorethoxy)methane 50.0 16.0 17.8 32.0 35.6 1.00-219 10.7 54
Bis(2-chloroisopropyl)ether 50.0 13.0 15.1 26.0 30.2 36.0-166 J4 J4 14.9 76
4-Bromophenyl-phenylether 50.0 32.6 35.6 65.2 71.2 53.0-127 8.80 43
2-Chloronaphthalene 50.0 17.6 20.3 35.2 40.6 60.0-120 J4 J4 14.2 24
4-Chlorophenyl-phenylether 50.0 28.0 30.5 56.0 61.0 25.0-158 8.55 61
Chrysene 50.0 36.8 37.6 73.6 75.2 17.0-168 2.15 87
Dibenz(a,h)anthracene 50.0 35.2 37.3 70.4 74.6 1.00-227 5.79 126
3,3-Dichlorobenzidine 100 43.3 47.6 43.3 47.6 1.00-262 9.46 108
2,4-Dinitrotoluene 50.0 33.9 35.6 67.8 71.2 39.0-139 4.89 42
2,6-Dinitrotoluene 50.0 30.2 31.6 60.4 63.2 50.0-158 4.53 48
Fluoranthene 50.0 34.4 35.8 68.8 71.6 26.0-137 3.99 66
Fluorene 50.0 27.1 29.6 54.2 59.2 59.0-121 J4 8.82 38
Hexachlorobenzene 50.0 34.1 36.4 68.2 72.8 1.00-152 6.52 55
Hexachloro-1,3-butadiene 50.0 9.44 10.5 18.9 21.0 24.0-120 J4 J4 10.6 62
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 29 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 29 of 45
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1311664
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1118060-03
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3432436-1 07/19/19 00:55 • (LCSD) R3432436-2 07/19/19 01:17
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Hexachlorocyclopentadiene 50.0 11.9 14.4 23.8 28.8 10.0-120 19.0 31
Hexachloroethane 50.0 8.13 8.93 16.3 17.9 40.0-120 J4 J4 9.38 52
Indeno(1,2,3-cd)pyrene 50.0 34.9 37.3 69.8 74.6 1.00-171 6.65 99
Isophorone 50.0 17.0 19.4 34.0 38.8 21.0-196 13.2 93
Naphthalene 50.0 12.2 13.9 24.4 27.8 21.0-133 13.0 65
Nitrobenzene 50.0 13.0 15.3 26.0 30.6 35.0-180 J4 J4 16.3 62
n-Nitrosodimethylamine 50.0 10.6 11.4 21.2 22.8 10.0-120 7.27 34
n-Nitrosodiphenylamine 50.0 23.8 25.1 47.6 50.2 44.0-120 5.32 21
n-Nitrosodi-n-propylamine 50.0 16.1 18.1 32.2 36.2 1.00-230 11.7 87
Phenanthrene 50.0 32.0 33.2 64.0 66.4 54.0-120 3.68 39
Benzylbutyl phthalate 50.0 34.2 35.0 68.4 70.0 1.00-152 2.31 60
Bis(2-ethylhexyl)phthalate 50.0 34.4 35.1 68.8 70.2 8.00-158 2.01 82
Di-n-butyl phthalate 50.0 34.3 35.0 68.6 70.0 1.00-120 2.02 47
Diethyl phthalate 50.0 31.7 32.2 63.4 64.4 1.00-120 1.56 100
Dimethyl phthalate 50.0 30.7 31.6 61.4 63.2 1.00-120 2.89 183
Di-n-octyl phthalate 50.0 30.0 31.0 60.0 62.0 4.00-146 3.28 69
Pyrene 50.0 35.4 36.8 70.8 73.6 52.0-120 3.88 49
1,2,4-Trichlorobenzene 50.0 10.8 12.5 21.6 25.0 44.0-142 J4 J4 14.6 50
1,2-Dichlorobenzene 50.0 9.82 11.2 19.6 22.4 27.0-120 J4 J4 13.1 30
1,3-Dichlorobenzene 50.0 8.94 10.1 17.9 20.2 26.0-120 J4 J4 12.2 31
1,4-Dichlorobenzene 50.0 9.28 10.6 18.6 21.2 26.0-120 J4 J4 13.3 30
(S) Nitrobenzene-d5 21.8 26.0 15.0-314
(S) 2-Fluorobiphenyl 37.1 44.3 22.0-127
(S) p-Terphenyl-d14 68.6 71.4 29.0-141
(S) Phenol-d5 11.1 13.2 8.00-424
(S) 2-Fluorophenol 16.9 20.8 10.0-120
(S) 2,4,6-Tribromophenol 63.0 73.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313771
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1118060-01,02
Method Blank (MB)
(MB) R3432372-2 07/19/19 01:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0333
Acenaphthylene U 0.00671 0.0333
Anthracene U 0.00632 0.0333
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0333
Benzo(b)fluoranthene U 0.00695 0.0333
Benzo(k)fluoranthene U 0.00582 0.0333
Benzo(g,h,i)perylene U 0.00721 0.0333
Benzo(a)pyrene U 0.00548 0.0333
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0333
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0333
Dibenz(a,h)anthracene U 0.00821 0.0333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0333
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0333
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0333
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0333
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313771
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1118060-01,02
Method Blank (MB)
(MB) R3432372-2 07/19/19 01:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.0123 0.0333
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 63.1 10.0-122
(S) 2-Fluorobiphenyl 77.5 15.0-120
(S) p-Terphenyl-d14 89.5 10.0-120
(S) Phenol-d5 74.8 10.0-120
(S) 2-Fluorophenol 86.3 12.0-120
(S) 2,4,6-Tribromophenol 78.1 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3432372-1 07/19/19 01:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.498 74.8 38.0-120
Acenaphthylene 0.666 0.520 78.1 40.0-120
Anthracene 0.666 0.530 79.6 42.0-120
Benzidine 1.33 0.305 22.9 10.0-120
Benzo(a)anthracene 0.666 0.592 88.9 44.0-120
Benzo(b)fluoranthene 0.666 0.612 91.9 43.0-120
Benzo(k)fluoranthene 0.666 0.630 94.6 44.0-120
Benzo(g,h,i)perylene 0.666 0.608 91.3 43.0-120
Benzo(a)pyrene 0.666 0.606 91.0 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.349 52.4 20.0-120
Bis(2-chloroethyl)ether 0.666 0.443 66.5 16.0-120
Bis(2-chloroisopropyl)ether 0.666 0.400 60.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.556 83.5 40.0-120
2-Chloronaphthalene 0.666 0.486 73.0 35.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313771
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1118060-01,02
Laboratory Control Sample (LCS)
(LCS) R3432372-1 07/19/19 01:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.564 84.7 40.0-120
Chrysene 0.666 0.568 85.3 43.0-120
Dibenz(a,h)anthracene 0.666 0.595 89.3 44.0-120
3,3-Dichlorobenzidine 1.33 1.13 85.0 28.0-120
2,4-Dinitrotoluene 0.666 0.566 85.0 45.0-120
2,6-Dinitrotoluene 0.666 0.536 80.5 42.0-120
Fluoranthene 0.666 0.541 81.2 44.0-120
Fluorene 0.666 0.534 80.2 41.0-120
Hexachlorobenzene 0.666 0.549 82.4 39.0-120
Hexachloro-1,3-butadiene 0.666 0.372 55.9 15.0-120
Hexachlorocyclopentadiene 0.666 0.477 71.6 15.0-120
Hexachloroethane 0.666 0.390 58.6 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.587 88.1 45.0-120
Isophorone 0.666 0.346 52.0 23.0-120
Naphthalene 0.666 0.355 53.3 18.0-120
Nitrobenzene 0.666 0.337 50.6 17.0-120
n-Nitrosodimethylamine 0.666 0.387 58.1 10.0-125
n-Nitrosodiphenylamine 0.666 0.500 75.1 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.428 64.3 26.0-120
Phenanthrene 0.666 0.517 77.6 42.0-120
Benzylbutyl phthalate 0.666 0.562 84.4 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.535 80.3 41.0-120
Di-n-butyl phthalate 0.666 0.523 78.5 43.0-120
Diethyl phthalate 0.666 0.560 84.1 43.0-120
Dimethyl phthalate 0.666 0.535 80.3 43.0-120
Di-n-octyl phthalate 0.666 0.533 80.0 40.0-120
Pyrene 0.666 0.555 83.3 41.0-120
1,2,4-Trichlorobenzene 0.666 0.370 55.6 17.0-120
4-Chloro-3-methylphenol 0.666 0.423 63.5 28.0-120
2-Chlorophenol 0.666 0.469 70.4 28.0-120
2,4-Dichlorophenol 0.666 0.419 62.9 25.0-120
2,4-Dimethylphenol 0.666 0.374 56.2 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.460 69.1 16.0-120
2,4-Dinitrophenol 0.666 0.401 60.2 10.0-120
2-Nitrophenol 0.666 0.374 56.2 20.0-120
4-Nitrophenol 0.666 0.548 82.3 27.0-120
Pentachlorophenol 0.666 0.505 75.8 29.0-120
Phenol 0.666 0.455 68.3 28.0-120
2,4,6-Trichlorophenol 0.666 0.584 87.7 37.0-120
(S) Nitrobenzene-d5 51.7 10.0-122
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313771
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1118060-01,02
Laboratory Control Sample (LCS)
(LCS) R3432372-1 07/19/19 01:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 72.7 15.0-120
(S) p-Terphenyl-d14 86.2 10.0-120
(S) Phenol-d5 67.6 10.0-120
(S) 2-Fluorophenol 76.4 12.0-120
(S) 2,4,6-Tribromophenol 89.9 10.0-127
L1118060-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1118060-01 07/19/19 03:37 • (MS) R3432372-3 07/19/19 03:56 • (MSD) R3432372-4 07/19/19 04:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.803 0.0182 0.392 0.409 46.5 48.6 1 18.0-120 4.22 32
Acenaphthylene 0.803 U 0.395 0.405 49.2 50.5 1 25.0-120 2.41 32
Anthracene 0.803 U 0.499 0.533 62.2 66.4 1 22.0-120 6.54 29
Benzidine 1.60 U 0.887 0.781 55.3 48.7 1 10.0-120 12.7 40
Benzo(a)anthracene 0.803 U 0.602 0.595 74.9 74.2 1 25.0-120 1.01 29
Benzo(b)fluoranthene 0.803 U 0.627 0.622 78.1 77.5 1 19.0-122 0.772 31
Benzo(k)fluoranthene 0.803 U 0.627 0.617 78.1 76.9 1 23.0-120 1.55 30
Benzo(g,h,i)perylene 0.803 U 0.610 0.622 76.0 77.5 1 10.0-120 1.96 33
Benzo(a)pyrene 0.803 U 0.620 0.615 77.2 76.6 1 24.0-120 0.781 30
Bis(2-chlorethoxy)methane 0.803 U 0.363 0.342 45.2 42.6 1 10.0-120 5.81 34
Bis(2-chloroethyl)ether 0.803 U 0.360 0.354 44.9 44.1 1 10.0-120 1.69 40
Bis(2-chloroisopropyl)ether 0.803 U 0.291 0.292 36.2 36.3 1 10.0-120 0.414 40
4-Bromophenyl-phenylether 0.803 U 0.463 0.507 57.7 63.2 1 27.0-120 9.19 30
2-Chloronaphthalene 0.803 U 0.351 0.366 43.7 45.6 1 20.0-120 4.37 32
4-Chlorophenyl-phenylether 0.803 U 0.445 0.474 55.4 59.0 1 24.0-120 6.30 29
Chrysene 0.803 U 0.573 0.562 71.3 70.0 1 21.0-120 1.91 29
Dibenz(a,h)anthracene 0.803 U 0.593 0.611 73.9 76.1 1 10.0-120 3.00 32
3,3-Dichlorobenzidine 1.60 U 1.20 1.24 74.8 77.4 1 10.0-120 3.46 34
2,4-Dinitrotoluene 0.803 U 0.546 0.540 68.0 67.3 1 30.0-120 1.11 31
2,6-Dinitrotoluene 0.803 U 0.477 0.491 59.5 61.1 1 25.0-120 2.74 31
Fluoranthene 0.803 U 0.570 0.577 71.0 71.9 1 18.0-126 1.26 32
Fluorene 0.803 0.0182 0.448 0.468 53.6 56.0 1 25.0-120 4.21 30
Hexachlorobenzene 0.803 U 0.482 0.510 60.1 63.5 1 27.0-120 5.59 28
Hexachloro-1,3-butadiene 0.803 U 0.210 0.266 26.1 33.2 1 10.0-120 23.8 38
Hexachlorocyclopentadiene 0.803 U 0.295 0.311 36.8 38.7 1 10.0-120 5.17 40
Hexachloroethane 0.803 U 1.77 1.09 221 136 1 10.0-120 J5 J3 J5 47.4 40
Indeno(1,2,3-cd)pyrene 0.803 U 0.592 0.612 73.7 76.3 1 10.0-120 3.40 32
Isophorone 0.803 U 0.336 0.319 41.9 39.8 1 13.0-120 5.15 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1313771
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1118060-01,02
L1118060-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1118060-01 07/19/19 03:37 • (MS) R3432372-3 07/19/19 03:56 • (MSD) R3432372-4 07/19/19 04:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.803 3.70 2.23 1.41 0.000 0.000 1 10.0-120 E V J3 V 45.0 35
Nitrobenzene 0.803 U 0.336 0.310 41.9 38.6 1 10.0-120 8.21 36
n-Nitrosodimethylamine 0.803 U 0.368 0.347 45.8 43.2 1 10.0-127 5.73 40
n-Nitrosodiphenylamine 0.803 U 0.451 0.498 56.2 62.0 1 17.0-120 9.91 29
n-Nitrosodi-n-propylamine 0.803 U 0.429 0.383 53.5 47.7 1 10.0-120 11.3 37
Phenanthrene 0.803 0.0289 0.505 0.528 59.3 62.2 1 17.0-120 4.43 31
Benzylbutyl phthalate 0.803 U 0.586 0.580 73.0 72.2 1 23.0-120 1.03 30
Bis(2-ethylhexyl)phthalate 0.803 U 0.552 0.540 68.8 67.3 1 17.0-126 2.21 30
Di-n-butyl phthalate 0.803 U 0.546 0.551 68.0 68.6 1 30.0-120 0.879 29
Diethyl phthalate 0.803 U 0.524 0.522 65.3 65.0 1 26.0-120 0.461 28
Dimethyl phthalate 0.803 U 0.509 0.488 63.4 60.8 1 25.0-120 4.11 29
Di-n-octyl phthalate 0.803 U 0.561 0.538 69.8 67.0 1 21.0-123 4.17 29
Pyrene 0.803 U 0.568 0.568 70.7 70.7 1 16.0-121 0.000 32
1,2,4-Trichlorobenzene 0.803 U 0.231 0.268 28.8 33.3 1 12.0-120 14.5 37
4-Chloro-3-methylphenol 0.803 U 0.412 0.416 51.4 51.8 1 15.0-120 0.873 30
2-Chlorophenol 0.803 U 0.445 0.403 55.4 50.2 1 15.0-120 9.96 37
2,4-Dichlorophenol 0.803 U 0.410 0.395 51.1 49.2 1 20.0-120 3.59 31
2,4-Dimethylphenol 0.803 U 0.409 0.379 50.9 47.1 1 10.0-120 7.66 33
4,6-Dinitro-2-methylphenol 0.803 U 0.568 0.599 70.7 74.6 1 10.0-120 5.37 39
2,4-Dinitrophenol 0.803 U 0.620 0.603 77.2 75.1 1 10.0-121 2.76 40
2-Nitrophenol 0.803 U 0.347 0.371 43.2 46.2 1 12.0-120 6.71 39
4-Nitrophenol 0.803 U 0.646 0.603 80.5 75.1 1 10.0-137 6.95 32
Pentachlorophenol 0.803 U 0.580 0.634 72.2 79.0 1 10.0-160 8.94 31
Phenol 0.803 U 0.507 0.440 63.2 54.8 1 12.0-120 14.2 38
2,4,6-Trichlorophenol 0.803 U 0.494 0.503 61.6 62.6 1 19.0-120 1.69 32
(S) Nitrobenzene-d5 34.8 36.0 10.0-122
(S) 2-Fluorobiphenyl 43.8 44.7 15.0-120
(S) p-Terphenyl-d14 73.9 72.1 10.0-120
(S) Phenol-d5 63.5 55.9 10.0-120
(S) 2-Fluorophenol 65.2 56.5 12.0-120
(S) 2,4,6-Tribromophenol 70.4 77.0 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J0 J0: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met method criteria.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Qualifier Description
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual
concentration present in the sample.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/25/19 16:24 38 of 45
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0A L1118060 07/30/19 15:41 38 of 45
Page 1 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190004 Work Order #:1103358557

COC ID # 00051459
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Raleigh, NC
Project Mgr: Patrick Kelly
Address:1125 E. Morehead Street, Suite 104, Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:Gary Fischer
Shipped:FedExp
Tracking #:107001979734
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-01 07/11/2019 07:25am W 10 40 ML AMBER VOA HCL VPH MADEP VPH
VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
100 ML AMBER GLASS NONE SVOCs/BNA/TICs 625
1LG HCL EPH MADEP EPH
MW-1 (10')07/10/2019 03:15pm S 5 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
MW-1 (15')07/10/2019 03:25pm S 5 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/2 https://www.speedway-ids.com
Page 2 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190004 Work Order #:1103358557

COC ID # 00051459
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Raleigh, NC
Project Mgr: Patrick Kelly
Address:1125 E. Morehead Street, Suite 104, Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:Gary Fischer
Shipped:FedExp
Tracking #:107001979734
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51459 Printed: 09/09/2019
Analysis Name: 8260D ( Soil )
Analysis Description / Method:VOCs by 8260D / 8260D
Container Type / Preservative:40 MIL AMBER VIAL / MEOH/NAHSO4
Analytes: 1,1,1,2-Tetrachloroethane mg/Kg, 1,1,1-Trichloroethane mg/Kg, 1,1,2,2-Tetrachloroethane mg/Kg, 1,1,2-Trichloroethane mg/Kg, 1,1-Dichloroethane mg/Kg, 1,1-Dichloroethene mg/Kg, 1,1-Dichloropropene
mg/Kg, 1,2,3-Trichlorobenzene mg/Kg, 1,2,3-Trichloropropane mg/Kg, 1,2,4-Trichlorobenzene mg/Kg, 1,2,4-Trimethylbenzene mg/Kg, 1,2-Dibromo-3-chloropropane mg/Kg, 1,2-Dibromoethane mg/Kg,
1,2-Dichlorobenzene mg/Kg, 1,2-Dichloroethane mg/Kg, 1,2-Dichloropropane mg/Kg, 1,3,5-Trimethylbenzene mg/Kg, 1,3-Dichlorobenzene mg/Kg, 1,3-Dichloropropane mg/Kg, 1,4-Dichlorobenzene mg/Kg,
2,2-Dichloropropane mg/Kg, 2-Butanone mg/Kg, 2-Chlorotoluene mg/Kg, 4-Chlorotoluene mg/Kg, 4-Methyl-2-pentanone mg/Kg, Acetone mg/Kg, Acrylonitrile mg/Kg, Benzene mg/Kg, Bromobenzene mg/Kg,
Bromodichloromethane mg/Kg, Bromoform mg/Kg, Bromomethane mg/Kg, Carbon tetrachloride mg/Kg, Chlorobenzene mg/Kg, Chlorodibromomethane mg/Kg, Chloroethane mg/Kg, Chloroform mg/Kg, Chloromethane
mg/Kg, Dibromoethane mg/Kg, Dichlorodifluoromethane mg/Kg, Diisopropyl ether mg/Kg, Ethylbenzene mg/Kg, Isopropylbenzene mg/Kg, Methyl tert butyl ether mg/Kg, Methylene chloride mg/Kg, Naphthalene mg/Kg,
Styrene mg/Kg, Tetrachloroethene mg/Kg, Toluene mg/Kg, Total Xylenes mg/Kg, Trichloroethene mg/Kg, Trichlorofluoromethane mg/Kg, Vinyl chloride mg/Kg, cis-1,2-Dichloroethene mg/Kg, cis-1,3-Dichloropropene
mg/Kg, n-Butylbenzene mg/Kg, n-Propylbenzene mg/Kg, p-Isopropyltoluene mg/Kg, sec-Butylbenzene mg/Kg, tert-Butylbenzene mg/Kg, trans-1,2-Dichloroethene mg/Kg, trans-1,3-Dichloropropene mg/Kg

Analysis Name: BTEX/MTBE/IPE/Naph ( Water )
Analysis Description / Method:EPA Modified 602 / 602
Container Type / Preservative:VOA - 40 MILL / HCL
Analytes: Benzene ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Methyl tert butyl ether ug/L, Naphthalene ug/L, Toluene ug/L, m,p-Xylene ug/L, o-Xylene ug/L

Analysis Name: EPH ( Water )
Analysis Description / Method:Extractable Petroleum Hydrocarbons / MADEP EPH
Container Type / Preservative:1LG / HCL
Analytes: C11-C22 Aromatics ug/L, C19-C36 Aliphatics ug/L, C9-C18 Aliphatics ug/L, Extractable Petroleum Hydrocarbons ug/L

Speedway LLC.1/3 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51459 Printed: 09/09/2019
Analysis Name: EPH ( Soil )
Analysis Description / Method:EPH in soil / MADEP EPH
Container Type / Preservative:4 OZ / NONE
Analytes: C11-C22 Aromatics mg/Kg, C19-C36 Aliphatics mg/Kg, C9-C18 Aliphatics mg/Kg, Extractable Petroleum Hydrocarbons mg/Kg

Analysis Name: SVOCs/BNA/TICs ( Water )
Analysis Description / Method:Base Neutral Acid Extractables and Tentatively Identified Compounds / 625
Container Type / Preservative:100 ML AMBER GLASS / NONE
Analytes: 1,2,4-Trichlorobenzene ug/L, 1,2-Dichlorobenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,4-Dichlorobenzene ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L,
3,3'-Dichlorobenzidine ug/L, 4-Bromophenyl phenyl ether ug/L, 4-Chlorophenyl phenyl ether ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzidine ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene
ug/L, Benzo(b)fluoranthene ug/L, Benzo(g,h,I)perylene ug/L, Benzo(k)fluoranthene ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-chloroisopropyl)ether ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl phthalate ug/L,
Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenz(a,h)anthracene ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L, Hexachlorobenzene ug/L,
Hexachlorobutadiene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodimethylamine ug/L,
N-Nitrosodiphenylamine ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Phenanthrene ug/L, Pyrene ug/L

Analysis Name: Semi Volatile 8270E ( Soil )
Analysis Description / Method:SVOCs by 8270E / 8270E
Container Type / Preservative:4 OZ / NONE
Analytes: 1,2,4-Trichlorobenzene mg/Kg, 2,4,6-Trichlorophenol mg/Kg, 2,4-Dichlorophenol mg/Kg, 2,4-Dimethylphenol mg/Kg, 2,4-Dinitrotoluene mg/Kg, 2,6-Dinitrotoluene mg/Kg, 2-Chloronaphthalene mg/Kg,
2-Chlorophenol mg/Kg, 2-Nitrophenol mg/Kg, 3,3'-Dichlorobenzidine mg/Kg, 4,6-Dinitro-2-methylphenol mg/Kg, 4-Bromophenyl phenyl ether mg/Kg, 4-Chloro-3-methylphenol mg/Kg, 4-Nitrophenol mg/Kg, Acenaphthene
mg/Kg, Acenaphthylene mg/Kg, Benzidine mg/Kg, Benzo(a)anthracene mg/Kg, Benzo(a)pyrene mg/Kg, Benzo(b)fluoranthene mg/Kg, Benzo(g,h,I)perylene mg/Kg, Benzo(k)fluoranthene mg/Kg,
Bis(2-chloroethoxy)methane mg/Kg, Bis(2-chloroisopropyl)ether mg/Kg, Bis(2-ethylhexyl)phthalate mg/Kg, Butyl benzyl phthalate mg/Kg, Chrysene mg/Kg, Di-n-butyl phthalate mg/Kg, Di-n-octyl phthalate mg/Kg,
Speedway LLC.2/3 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51459 Printed: 09/09/2019
Dibenz(a,h)anthracene mg/Kg, Diethyl phthalate mg/Kg, Dimethyl phthalate mg/Kg, Fluoranthene mg/Kg, Fluorene mg/Kg, Hexachlorobenzene mg/Kg, Hexachlorocyclopentadiene mg/Kg, Hexachloroethane mg/Kg,
Hexchloro-1,3-butadiene mg/Kg, Indeno(1,2,3-cd)pyrene mg/Kg, Isophorone mg/Kg, N-Nitroso-di-n-propylamine mg/Kg, N-Nitrosodimethylamine mg/Kg, N-Nitrosodiphenylamine mg/Kg, Naphthalene mg/Kg, Nitrobenzene
mg/Kg, Pentachlorophenol mg/Kg, Phenanthrene mg/Kg, Phenol mg/Kg, Pyrene mg/Kg, bis(2-Chloroethyl)ether mg/Kg

Analysis Name: VPH ( Water )
Analysis Description / Method:Volatile Petroleum Hydrocarbons / MADEP VPH
Container Type / Preservative:40 ML AMBER VOA / HCL
Analytes: C5-C8 Aliphatics ug/L, C9-C10 Aromatics ug/L, C9-C12 Aliphatics ug/L, Total Volatile Hydrocarbons ug/L

Analysis Name: VPH ( Soil )
Analysis Description / Method:MADEP VPH soil / MADEP VPH
Container Type / Preservative:40 MIL AMBER VIAL / MEOH
Analytes: C5-C8 Aliphatics mg/Kg, C9-C10 Aromatics mg/Kg, C9-C12 Aliphatics mg/Kg, Total Volatile Hydrocarbons mg/Kg

Speedway LLC.3/3 https://www.speedway-ids.com
ANALYTICAL REPORT
January 07, 2020
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1173532
Samples Received:12/21/2019
Project Number:R3243.0B
Description:Speedway 6993
Site:6993
Report To:Mr. Troy Holzschuh
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
January 07, 2020
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 1 of 25
January 07, 2020
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 1 of 25
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 L1173532-01 5
MW-2 L1173532-02 7
Qc: Quality Control Summary 9
Volatile Petroleum Hydrocarbons by Method MADEPV 9
Volatile Organic Compounds (GC/MS) by Method 602MS 11
TPH by Method MADEPE 13
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 15
Gl: Glossary of Terms 19
Al: Accreditations & Locations 20
Sc: Sample Chain of Custody 21
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 2 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 2 of 25
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1173532-01 GW Reina Clark 12/20/19 11:11 12/21/19 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1401684 25 12/23/19 16:57 12/23/19 16:57 ACG Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1404112 25 12/30/19 19:45 12/30/19 19:45 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1403188 25 12/27/19 16:39 12/27/19 16:39 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1403692 500 12/29/19 16:54 12/29/19 16:54 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1403804 1 12/29/19 06:02 12/30/19 15:33 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1403804 1 12/29/19 06:02 12/30/19 16:21 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1402077 1 12/24/19 15:51 12/26/19 18:47 LEA Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1402077 10 12/24/19 15:51 12/26/19 20:48 LEA Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1173532-02 GW Reina Clark 12/20/19 11:28 12/21/19 10:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1401684 1 12/23/19 16:24 12/23/19 16:24 ACG Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1404112 1 12/30/19 20:18 12/30/19 20:18 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1403692 1 12/29/19 17:14 12/29/19 17:14 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1404817 1.01 12/31/19 15:02 01/02/20 15:46 KLM Mt. Juliet, TN
TPH by Method MADEPE WG1404817 1.01 12/31/19 15:02 01/02/20 20:08 KLM Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1402077 1 12/24/19 15:51 12/26/19 19:07 LEA Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 3 of 25
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 4 of 25
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 4 of 25
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1173532
MW-1
Collected date/time: 12/20/19 11:11
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 77300 833 2500 25 12/23/2019 16:57 WG1401684
Unadjusted C9-C12 Aliphatics 49600 833 2500 25 12/23/2019 16:57 WG1401684
Unadjusted C9-C10 Aromatics 6440 833 2500 25 12/30/2019 19:45 WG1404112
Total VPH 127000 833 2500 25 12/23/2019 16:57 WG1401684
(S) 2,5-Dibromotoluene(FID) 91.3 70.0-130 12/23/2019 16:57 WG1401684
(S) 2,5-Dibromotoluene(FID) 101 70.0-130 12/30/2019 19:45 WG1404112
(S) 2,5-Dibromotoluene(PID) 73.8 70.0-130 12/23/2019 16:57 WG1401684
(S) 2,5-Dibromotoluene(PID) 85.4 70.0-130 12/30/2019 19:45 WG1404112
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 7770 166 500 500 12/29/2019 16:54 WG1403692
Di-isopropyl ether U 8.00 25.0 25 12/27/2019 16:39 WG1403188
Ethylbenzene 3240 9.60 25.0 25 12/27/2019 16:39 WG1403188
Methyl tert-butyl ether U 9.18 25.0 25 12/27/2019 16:39 WG1403188
Naphthalene 899 25.0 125 25 12/27/2019 16:39 WG1403188
Toluene 26900 206 500 500 12/29/2019 16:54 WG1403692
m&p-Xylenes 9980 18.0 50.0 25 12/27/2019 16:39 WG1403188
o-Xylene 5330 170 500 500 12/29/2019 16:54 WG1403692
(S) Toluene-d8 102 80.0-120 12/27/2019 16:39 WG1403188
(S) Toluene-d8 105 80.0-120 12/29/2019 16:54 WG1403692
(S) 4-Bromofluorobenzene 99.7 77.0-126 12/27/2019 16:39 WG1403188
(S) 4-Bromofluorobenzene 99.6 77.0-126 12/29/2019 16:54 WG1403692
(S) 1,2-Dichloroethane-d4 93.1 70.0-130 12/27/2019 16:39 WG1403188
(S) 1,2-Dichloroethane-d4 99.7 70.0-130 12/29/2019 16:54 WG1403692
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 465 33.3 100 1 12/30/2019 15:33 WG1403804
Unadjusted C19-C36 Aliphatics 43.5 J 33.3 100 1 12/30/2019 15:33 WG1403804
Unadjusted C11-C22 Aromatics 794 33.3 100 1 12/30/2019 16:21 WG1403804
Unadjusted Total Petroleum
Hydrocarbons 1300 33.3 100 1 12/30/2019 16:21 WG1403804
(S) o-Terphenyl 39.0 J2 40.0-140 12/30/2019 16:21 WG1403804
(S) 1-Chloro-octadecane 26.9 J2 40.0-140 12/30/2019 15:33 WG1403804
(S) 2-Fluorobiphenyl 73.0 40.0-140 12/30/2019 16:21 WG1403804
(S) 2-Bromonaphthalene 69.1 40.0-140 12/30/2019 16:21 WG1403804
Sample Narrative:
L1173532-01 WG1403804: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 12/26/2019 18:47 WG1402077
Acenaphthylene U 0.309 1.00 1 12/26/2019 18:47 WG1402077
Anthracene U 0.291 1.00 1 12/26/2019 18:47 WG1402077
Benzidine U 4.32 10.0 1 12/26/2019 18:47 WG1402077
Benzo(a)anthracene U 0.0975 1.00 1 12/26/2019 18:47 WG1402077
Benzo(b)fluoranthene U 0.0896 1.00 1 12/26/2019 18:47 WG1402077
Benzo(k)fluoranthene U 0.355 1.00 1 12/26/2019 18:47 WG1402077
Benzo(g,h,i)perylene U 0.161 1.00 1 12/26/2019 18:47 WG1402077
Benzo(a)pyrene U 0.340 1.00 1 12/26/2019 18:47 WG1402077
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 5 of 25
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1173532
MW-1
Collected date/time: 12/20/19 11:11
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Bis(2-chlorethoxy)methane U 0.329 10.0 1 12/26/2019 18:47 WG1402077
Bis(2-chloroethyl)ether U 1.62 10.0 1 12/26/2019 18:47 WG1402077
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 12/26/2019 18:47 WG1402077
4-Bromophenyl-phenylether U 0.335 10.0 1 12/26/2019 18:47 WG1402077
2-Chloronaphthalene U 0.330 1.00 1 12/26/2019 18:47 WG1402077
4-Chlorophenyl-phenylether U 0.303 10.0 1 12/26/2019 18:47 WG1402077
Chrysene U 0.332 1.00 1 12/26/2019 18:47 WG1402077
Dibenz(a,h)anthracene U 0.279 1.00 1 12/26/2019 18:47 WG1402077
3,3-Dichlorobenzidine U 2.02 10.0 1 12/26/2019 18:47 WG1402077
2,4-Dinitrotoluene U 1.65 10.0 1 12/26/2019 18:47 WG1402077
2,6-Dinitrotoluene U 0.279 10.0 1 12/26/2019 18:47 WG1402077
Fluoranthene U 0.310 1.00 1 12/26/2019 18:47 WG1402077
Fluorene U 0.323 1.00 1 12/26/2019 18:47 WG1402077
Hexachlorobenzene U 0.341 1.00 1 12/26/2019 18:47 WG1402077
Hexachloro-1,3-butadiene U 0.329 10.0 1 12/26/2019 18:47 WG1402077
Hexachlorocyclopentadiene U 2.33 10.0 1 12/26/2019 18:47 WG1402077
Hexachloroethane U 0.365 10.0 1 12/26/2019 18:47 WG1402077
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/26/2019 18:47 WG1402077
Isophorone U 0.272 10.0 1 12/26/2019 18:47 WG1402077
Naphthalene 594 3.72 10.0 10 12/26/2019 20:48 WG1402077
Nitrobenzene U 0.367 10.0 1 12/26/2019 18:47 WG1402077
n-Nitrosodimethylamine U 1.26 10.0 1 12/26/2019 18:47 WG1402077
n-Nitrosodiphenylamine U 1.19 10.0 1 12/26/2019 18:47 WG1402077
n-Nitrosodi-n-propylamine U 0.403 10.0 1 12/26/2019 18:47 WG1402077
Phenanthrene U 0.366 1.00 1 12/26/2019 18:47 WG1402077
Benzylbutyl phthalate U 0.275 3.00 1 12/26/2019 18:47 WG1402077
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 12/26/2019 18:47 WG1402077
Di-n-butyl phthalate 0.387 J 0.266 3.00 1 12/26/2019 18:47 WG1402077
Diethyl phthalate U 0.282 3.00 1 12/26/2019 18:47 WG1402077
Dimethyl phthalate U 0.283 3.00 1 12/26/2019 18:47 WG1402077
Di-n-octyl phthalate U 0.278 3.00 1 12/26/2019 18:47 WG1402077
Pyrene U 0.330 1.00 1 12/26/2019 18:47 WG1402077
1,2,4-Trichlorobenzene U 0.355 10.0 1 12/26/2019 18:47 WG1402077
(S) Nitrobenzene-d5 15.4 15.0-314 12/26/2019 18:47 WG1402077
(S) Nitrobenzene-d5 16.7 15.0-314 12/26/2019 20:48 WG1402077
(S) 2-Fluorobiphenyl 68.2 22.0-127 12/26/2019 20:48 WG1402077
(S) 2-Fluorobiphenyl 74.5 22.0-127 12/26/2019 18:47 WG1402077
(S) p-Terphenyl-d14 73.2 29.0-141 12/26/2019 20:48 WG1402077
(S) p-Terphenyl-d14 83.3 29.0-141 12/26/2019 18:47 WG1402077
(S) Phenol-d5 36.2 8.00-424 12/26/2019 18:47 WG1402077
(S) Phenol-d5 39.6 8.00-424 12/26/2019 20:48 WG1402077
(S) 2-Fluorophenol 85.2 10.0-120 12/26/2019 18:47 WG1402077
(S) 2-Fluorophenol 11.7 10.0-120 12/26/2019 20:48 WG1402077
(S) 2,4,6-Tribromophenol 83.0 10.0-153 12/26/2019 20:48 WG1402077
(S) 2,4,6-Tribromophenol 104 10.0-153 12/26/2019 18:47 WG1402077
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 6 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 6 of 25
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1173532
MW-2
Collected date/time: 12/20/19 11:28
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 12/23/2019 16:24 WG1401684
Unadjusted C9-C12 Aliphatics U 33.3 100 1 12/23/2019 16:24 WG1401684
Unadjusted C9-C10 Aromatics U 33.3 100 1 12/30/2019 20:18 WG1404112
Total VPH U J 33.3 100 1 12/23/2019 16:24 WG1401684
(S) 2,5-Dibromotoluene(FID) 91.6 70.0-130 12/23/2019 16:24 WG1401684
(S) 2,5-Dibromotoluene(FID) 98.3 70.0-130 12/30/2019 20:18 WG1404112
(S) 2,5-Dibromotoluene(PID) 72.5 70.0-130 12/23/2019 16:24 WG1401684
(S) 2,5-Dibromotoluene(PID) 83.5 70.0-130 12/30/2019 20:18 WG1404112
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.331 1.00 1 12/29/2019 17:14 WG1403692
Di-isopropyl ether U 0.320 1.00 1 12/29/2019 17:14 WG1403692
Ethylbenzene U 0.384 1.00 1 12/29/2019 17:14 WG1403692
Methyl tert-butyl ether U 0.367 1.00 1 12/29/2019 17:14 WG1403692
Naphthalene U 1.00 5.00 1 12/29/2019 17:14 WG1403692
Toluene U 0.412 1.00 1 12/29/2019 17:14 WG1403692
m&p-Xylenes U 0.719 2.00 1 12/29/2019 17:14 WG1403692
o-Xylene U 0.341 1.00 1 12/29/2019 17:14 WG1403692
(S) Toluene-d8 106 80.0-120 12/29/2019 17:14 WG1403692
(S) 4-Bromofluorobenzene 97.3 77.0-126 12/29/2019 17:14 WG1403692
(S) 1,2-Dichloroethane-d4 99.1 70.0-130 12/29/2019 17:14 WG1403692
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 55.5 B J 33.6 101 1.01 01/02/2020 15:46 WG1404817
Unadjusted C19-C36 Aliphatics U 33.6 101 1.01 01/02/2020 15:46 WG1404817
Unadjusted C11-C22 Aromatics 53.0 B J 33.6 101 1.01 01/02/2020 20:08 WG1404817
Unadjusted Total Petroleum
Hydrocarbons 109 33.6 101 1.01 01/02/2020 20:08 WG1404817
(S) o-Terphenyl 69.4 40.0-140 01/02/2020 20:08 WG1404817
(S) 1-Chloro-octadecane 54.8 40.0-140 01/02/2020 15:46 WG1404817
(S) 2-Fluorobiphenyl 78.1 40.0-140 01/02/2020 20:08 WG1404817
(S) 2-Bromonaphthalene 71.8 40.0-140 01/02/2020 20:08 WG1404817
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 12/26/2019 19:07 WG1402077
Acenaphthylene U 0.309 1.00 1 12/26/2019 19:07 WG1402077
Anthracene U 0.291 1.00 1 12/26/2019 19:07 WG1402077
Benzidine U 4.32 10.0 1 12/26/2019 19:07 WG1402077
Benzo(a)anthracene U 0.0975 1.00 1 12/26/2019 19:07 WG1402077
Benzo(b)fluoranthene U 0.0896 1.00 1 12/26/2019 19:07 WG1402077
Benzo(k)fluoranthene U 0.355 1.00 1 12/26/2019 19:07 WG1402077
Benzo(g,h,i)perylene U 0.161 1.00 1 12/26/2019 19:07 WG1402077
Benzo(a)pyrene U 0.340 1.00 1 12/26/2019 19:07 WG1402077
Bis(2-chlorethoxy)methane U 0.329 10.0 1 12/26/2019 19:07 WG1402077
Bis(2-chloroethyl)ether U 1.62 10.0 1 12/26/2019 19:07 WG1402077
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 12/26/2019 19:07 WG1402077
4-Bromophenyl-phenylether U 0.335 10.0 1 12/26/2019 19:07 WG1402077
2-Chloronaphthalene U 0.330 1.00 1 12/26/2019 19:07 WG1402077
4-Chlorophenyl-phenylether U 0.303 10.0 1 12/26/2019 19:07 WG1402077
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 7 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 7 of 25
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1173532
MW-2
Collected date/time: 12/20/19 11:28
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Chrysene U 0.332 1.00 1 12/26/2019 19:07 WG1402077
Dibenz(a,h)anthracene U 0.279 1.00 1 12/26/2019 19:07 WG1402077
3,3-Dichlorobenzidine U 2.02 10.0 1 12/26/2019 19:07 WG1402077
2,4-Dinitrotoluene U 1.65 10.0 1 12/26/2019 19:07 WG1402077
2,6-Dinitrotoluene U 0.279 10.0 1 12/26/2019 19:07 WG1402077
Fluoranthene U 0.310 1.00 1 12/26/2019 19:07 WG1402077
Fluorene U 0.323 1.00 1 12/26/2019 19:07 WG1402077
Hexachlorobenzene U 0.341 1.00 1 12/26/2019 19:07 WG1402077
Hexachloro-1,3-butadiene U 0.329 10.0 1 12/26/2019 19:07 WG1402077
Hexachlorocyclopentadiene U 2.33 10.0 1 12/26/2019 19:07 WG1402077
Hexachloroethane U 0.365 10.0 1 12/26/2019 19:07 WG1402077
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/26/2019 19:07 WG1402077
Isophorone U 0.272 10.0 1 12/26/2019 19:07 WG1402077
Naphthalene U 0.372 1.00 1 12/26/2019 19:07 WG1402077
Nitrobenzene U 0.367 10.0 1 12/26/2019 19:07 WG1402077
n-Nitrosodimethylamine U 1.26 10.0 1 12/26/2019 19:07 WG1402077
n-Nitrosodiphenylamine U 1.19 10.0 1 12/26/2019 19:07 WG1402077
n-Nitrosodi-n-propylamine U 0.403 10.0 1 12/26/2019 19:07 WG1402077
Phenanthrene U 0.366 1.00 1 12/26/2019 19:07 WG1402077
Benzylbutyl phthalate U 0.275 3.00 1 12/26/2019 19:07 WG1402077
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 12/26/2019 19:07 WG1402077
Di-n-butyl phthalate 0.403 J 0.266 3.00 1 12/26/2019 19:07 WG1402077
Diethyl phthalate U 0.282 3.00 1 12/26/2019 19:07 WG1402077
Dimethyl phthalate U 0.283 3.00 1 12/26/2019 19:07 WG1402077
Di-n-octyl phthalate U 0.278 3.00 1 12/26/2019 19:07 WG1402077
Pyrene U 0.330 1.00 1 12/26/2019 19:07 WG1402077
1,2,4-Trichlorobenzene U 0.355 10.0 1 12/26/2019 19:07 WG1402077
(S) Nitrobenzene-d5 63.4 15.0-314 12/26/2019 19:07 WG1402077
(S) 2-Fluorobiphenyl 73.1 22.0-127 12/26/2019 19:07 WG1402077
(S) p-Terphenyl-d14 78.2 29.0-141 12/26/2019 19:07 WG1402077
(S) Phenol-d5 26.1 8.00-424 12/26/2019 19:07 WG1402077
(S) 2-Fluorophenol 42.4 10.0-120 12/26/2019 19:07 WG1402077
(S) 2,4,6-Tribromophenol 93.0 10.0-153 12/26/2019 19:07 WG1402077
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 8 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 8 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1401684
Volatile Petroleum Hydrocarbons by Method MADEPV L1173532-01,02
Method Blank (MB)
(MB) R3486950-2 12/23/19 12:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 89.1 70.0-130
(S) 2,5-Dibromotoluene(PID) 81.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3486950-1 12/23/19 10:54 • (LCSD) R3486950-3 12/23/19 18:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1370 1320 114 110 70.0-130 3.72 25
Unadjusted C9-C12 Aliphatics 1400 1810 1800 129 129 70.0-130 0.554 25
Total VPH 2800 3440 3350 123 120 70.0-130 2.65 25
(S) 2,5-Dibromotoluene(FID) 97.0 96.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 89.7 78.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 9 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 9 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1404112
Volatile Petroleum Hydrocarbons by Method MADEPV L1173532-01,02
Method Blank (MB)
(MB) R3487138-3 12/30/19 17:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C10 Aromatics U 33.3 100
(S) 2,5-Dibromotoluene(FID) 89.8 70.0-130
(S) 2,5-Dibromotoluene(PID) 77.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3487138-1 12/30/19 15:21 • (LCSD) R3487138-2 12/30/19 15:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C10 Aromatics 200 170 173 85.0 86.5 70.0-130 1.75 25
(S) 2,5-Dibromotoluene(FID) 103 103 70.0-130
(S) 2,5-Dibromotoluene(PID) 88.1 87.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 10 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 10 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1403188
Volatile Organic Compounds (GC/MS) by Method 602MS L1173532-01
Method Blank (MB)
(MB) R3486584-2 12/27/19 11:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 98.9 80.0-120
(S) 4-Bromofluorobenzene 96.1 77.0-126
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3486584-1 12/27/19 11:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Di-isopropyl ether 5.00 4.85 97.0 58.0-138
Ethylbenzene 5.00 4.62 92.4 79.0-123
Methyl tert-butyl ether 5.00 4.89 97.8 68.0-125
Naphthalene 5.00 4.58 91.6 54.0-135
m&p-Xylenes 10.0 9.29 92.9 80.0-122
(S) Toluene-d8 99.1 80.0-120
(S) 4-Bromofluorobenzene 96.9 77.0-126
(S) 1,2-Dichloroethane-d4 99.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 11 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 11 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1403692
Volatile Organic Compounds (GC/MS) by Method 602MS L1173532-01,02
Method Blank (MB)
(MB) R3486883-3 12/29/19 14:59
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
Toluene U 0.412 1.00
o-Xylene U 0.341 1.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 97.6 77.0-126
(S) 1,2-Dichloroethane-d4 98.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3486883-1 12/29/19 13:58 • (LCSD) R3486883-2 12/29/19 14:18
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 5.41 5.25 108 105 70.0-123 3.00 20
Di-isopropyl ether 5.00 5.19 5.17 104 103 58.0-138 0.386 20
Ethylbenzene 5.00 5.08 4.92 102 98.4 79.0-123 3.20 20
Methyl tert-butyl ether 5.00 4.90 4.74 98.0 94.8 68.0-125 3.32 20
Naphthalene 5.00 4.47 4.49 89.4 89.8 54.0-135 0.446 20
Toluene 5.00 5.58 5.40 112 108 79.0-120 3.28 20
o-Xylene 5.00 4.76 4.77 95.2 95.4 80.0-122 0.210 20
m&p-Xylenes 10.0 10.1 9.82 101 98.2 80.0-122 2.81 20
(S) Toluene-d8 106 106 80.0-120
(S) 4-Bromofluorobenzene 96.9 96.3 77.0-126
(S) 1,2-Dichloroethane-d4 99.6 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 12 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 12 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1403804
TPH by Method MADEPE L1173532-01
Method Blank (MB)
(MB) R3486959-1 12/30/19 08:47
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 36.2 J 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 43.9 40.0-140
Method Blank (MB)
(MB) R3486959-4 12/30/19 09:58
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 41.7 J 33.3 100
(S) o-Terphenyl 54.1 40.0-140
(S) 2-Fluorobiphenyl 88.5 40.0-140
(S) 2-Bromonaphthalene 83.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3486959-2 12/30/19 09:11 • (LCSD) R3486959-6 12/30/19 15:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 324 290 54.0 48.3 40.0-140 11.1 25
Unadjusted C19-C36 Aliphatics 800 500 423 62.5 52.9 40.0-140 16.7 25
(S) 1-Chloro-octadecane 55.6 47.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3486959-3 12/30/19 10:22 • (LCSD) R3486959-5 12/30/19 10:46
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1030 931 60.6 54.8 40.0-140 10.1 25
(S) o-Terphenyl 54.1 47.1 40.0-140
(S) 2-Fluorobiphenyl 79.7 79.4 40.0-140
(S) 2-Bromonaphthalene 75.4 74.5 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:32 13 of 25
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R3243.0B L1173532 01/07/20 09:43 13 of 25
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1404817
TPH by Method MADEPE L1173532-02
Method Blank (MB)
(MB) R3487847-1 01/02/20 13:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 47.6 J 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 73.8 40.0-140
Method Blank (MB)
(MB) R3487847-4 01/02/20 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 50.4 J 33.3 100
(S) o-Terphenyl 71.6 40.0-140
(S) 2-Fluorobiphenyl 78.3 40.0-140
(S) 2-Bromonaphthalene 72.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3487847-2 01/02/20 13:47 • (LCSD) R3487847-3 01/02/20 14:11
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 348 357 58.0 59.5 40.0-140 2.55 25
Unadjusted C19-C36 Aliphatics 800 633 633 79.1 79.1 40.0-140 0.000 25
(S) 1-Chloro-octadecane 76.8 77.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3487847-5 01/02/20 14:59 • (LCSD) R3487847-6 01/02/20 15:23
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1240 1310 72.9 77.1 40.0-140 5.49 25
(S) o-Terphenyl 69.0 71.5 40.0-140
(S) 2-Fluorobiphenyl 67.5 77.4 40.0-140
(S) 2-Bromonaphthalene 64.6 72.8 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402077
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1173532-01,02
Method Blank (MB)
(MB) R3486133-2 12/26/19 11:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402077
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1173532-01,02
Method Blank (MB)
(MB) R3486133-2 12/26/19 11:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
(S) Nitrobenzene-d5 52.3 15.0-314
(S) 2-Fluorobiphenyl 65.6 22.0-127
(S) p-Terphenyl-d14 81.5 29.0-141
(S) Phenol-d5 29.1 8.00-424
(S) 2-Fluorophenol 41.8 10.0-120
(S) 2,4,6-Tribromophenol 72.5 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3486133-1 12/26/19 11:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 33.7 67.4 47.0-145
Acenaphthylene 50.0 36.6 73.2 33.0-145
Anthracene 50.0 39.1 78.2 27.0-133
Benzidine 100 17.5 17.5 1.00-120
Benzo(a)anthracene 50.0 39.6 79.2 33.0-143
Benzo(b)fluoranthene 50.0 43.6 87.2 24.0-159
Benzo(k)fluoranthene 50.0 40.6 81.2 11.0-162
Benzo(g,h,i)perylene 50.0 42.2 84.4 1.00-219
Benzo(a)pyrene 50.0 44.3 88.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 29.5 59.0 1.00-219
Bis(2-chloroethyl)ether 50.0 30.9 61.8 33.0-185
Bis(2-chloroisopropyl)ether 50.0 31.7 63.4 36.0-166
4-Bromophenyl-phenylether 50.0 39.7 79.4 53.0-127
2-Chloronaphthalene 50.0 32.8 65.6 60.0-120
4-Chlorophenyl-phenylether 50.0 37.7 75.4 25.0-158
Chrysene 50.0 40.6 81.2 17.0-168
Dibenz(a,h)anthracene 50.0 37.6 75.2 1.00-227
3,3-Dichlorobenzidine 100 80.2 80.2 1.00-262
2,4-Dinitrotoluene 50.0 41.6 83.2 39.0-139
2,6-Dinitrotoluene 50.0 39.2 78.4 50.0-158
Fluoranthene 50.0 42.5 85.0 26.0-137
Fluorene 50.0 37.3 74.6 59.0-121
Hexachlorobenzene 50.0 38.4 76.8 1.00-152
Hexachloro-1,3-butadiene 50.0 28.8 57.6 24.0-120
Hexachlorocyclopentadiene 50.0 28.5 57.0 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402077
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1173532-01,02
Laboratory Control Sample (LCS)
(LCS) R3486133-1 12/26/19 11:03
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Hexachloroethane 50.0 28.1 56.2 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 38.2 76.4 1.00-171
Isophorone 50.0 29.8 59.6 21.0-196
Naphthalene 50.0 28.1 56.2 21.0-133
Nitrobenzene 50.0 28.1 56.2 35.0-180
n-Nitrosodimethylamine 50.0 18.8 37.6 10.0-120
n-Nitrosodiphenylamine 50.0 39.1 78.2 44.0-120
n-Nitrosodi-n-propylamine 50.0 32.6 65.2 1.00-230
Phenanthrene 50.0 38.4 76.8 54.0-120
Benzylbutyl phthalate 50.0 39.3 78.6 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 38.8 77.6 8.00-158
Di-n-butyl phthalate 50.0 45.7 91.4 1.00-120
Diethyl phthalate 50.0 41.6 83.2 1.00-120
Dimethyl phthalate 50.0 39.7 79.4 1.00-120
Di-n-octyl phthalate 50.0 40.5 81.0 4.00-146
Pyrene 50.0 39.5 79.0 52.0-120
1,2,4-Trichlorobenzene 50.0 28.3 56.6 44.0-142
(S) Nitrobenzene-d5 47.0 15.0-314
(S) 2-Fluorobiphenyl 72.0 22.0-127
(S) p-Terphenyl-d14 82.0 29.0-141
(S) Phenol-d5 27.1 8.00-424
(S) 2-Fluorophenol 39.0 10.0-120
(S) 2,4,6-Tribromophenol 84.0 10.0-153
L1173568-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173568-16 12/26/19 13:50 • (MS) R3486133-3 12/26/19 14:11 • (MSD) R3486133-4 12/26/19 14:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Bis(2-chlorethoxy)methane 50.0 U 33.4 30.3 66.8 60.6 1 33.0-184 9.73 54
Bis(2-chloroethyl)ether 50.0 U 34.7 31.1 69.4 62.2 1 12.0-158 10.9 108
Bis(2-chloroisopropyl)ether 50.0 U 35.9 32.0 71.8 64.0 1 36.0-166 11.5 76
4-Bromophenyl-phenylether 50.0 U 43.2 40.2 86.4 80.4 1 53.0-127 7.19 43
4-Chlorophenyl-phenylether 50.0 U 42.7 38.4 85.4 76.8 1 25.0-158 10.6 61
3,3-Dichlorobenzidine 100 U 70.6 62.7 70.6 62.7 1 1.00-262 11.9 108
2,4-Dinitrotoluene 50.0 U 43.6 41.6 87.2 83.2 1 39.0-139 4.69 42
2,6-Dinitrotoluene 50.0 U 43.2 39.8 86.4 79.6 1 50.0-158 8.19 48
Hexachloro-1,3-butadiene 50.0 U 32.5 29.8 65.0 59.6 1 24.0-120 8.67 62
Hexachlorocyclopentadiene 50.0 U 33.8 24.8 67.6 49.6 1 10.0-146 30.7 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402077
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1173532-01,02
L1173568-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173568-16 12/26/19 13:50 • (MS) R3486133-3 12/26/19 14:11 • (MSD) R3486133-4 12/26/19 14:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Hexachloroethane 50.0 U 45.5 40.7 91.0 81.4 1 40.0-120 11.1 52
Isophorone 50.0 U 33.9 31.3 67.8 62.6 1 21.0-196 7.98 93
Nitrobenzene 50.0 U 32.4 29.7 64.8 59.4 1 35.0-180 8.70 62
n-Nitrosodiphenylamine 50.0 U 42.6 40.1 85.2 80.2 1 16.0-160 6.05 28
n-Nitrosodi-n-propylamine 50.0 U 37.7 33.3 75.4 66.6 1 1.00-230 12.4 87
Benzylbutyl phthalate 50.0 U 42.1 40.3 84.2 80.6 1 1.00-152 4.37 60
Bis(2-ethylhexyl)phthalate 50.0 U 40.5 37.1 81.0 74.2 1 8.00-158 8.76 82
Di-n-butyl phthalate 50.0 0.312 47.1 45.5 93.6 90.4 1 1.00-120 3.46 47
Diethyl phthalate 50.0 U 43.8 42.0 87.6 84.0 1 1.00-120 4.20 100
Dimethyl phthalate 50.0 U 42.6 40.4 85.2 80.8 1 1.00-120 5.30 183
Di-n-octyl phthalate 50.0 U 41.8 37.9 83.6 75.8 1 4.00-146 9.79 69
Acenaphthene 50.0 U 38.5 34.4 77.0 68.8 1 47.0-145 11.2 48
Acenaphthylene 50.0 U 41.8 37.0 83.6 74.0 1 33.0-145 12.2 74
Anthracene 50.0 U 41.2 39.1 82.4 78.2 1 27.0-133 5.23 66
Benzidine 100 U ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 40
Benzo(a)anthracene 50.0 U 41.2 38.7 82.4 77.4 1 33.0-143 6.26 53
Benzo(b)fluoranthene 50.0 U 44.1 41.4 88.2 82.8 1 24.0-159 6.32 71
Benzo(k)fluoranthene 50.0 U 42.4 39.9 84.8 79.8 1 11.0-162 6.08 63
Benzo(g,h,i)perylene 50.0 U 46.1 42.1 92.2 84.2 1 1.00-219 9.07 97
Benzo(a)pyrene 50.0 0.125 45.6 41.9 91.0 83.6 1 17.0-163 8.46 72
2-Chloronaphthalene 50.0 U 37.9 34.3 75.8 68.6 1 60.0-120 9.97 24
Chrysene 50.0 U 41.4 39.6 82.8 79.2 1 17.0-168 4.44 87
Dibenz(a,h)anthracene 50.0 U 39.7 36.7 79.4 73.4 1 1.00-227 7.85 126
Fluoranthene 50.0 U 43.8 42.2 87.6 84.4 1 26.0-137 3.72 66
Fluorene 50.0 U 41.8 38.1 83.6 76.2 1 59.0-121 9.26 38
Indeno(1,2,3-cd)pyrene 50.0 U 40.7 37.1 81.4 74.2 1 1.00-171 9.25 99
Hexachlorobenzene 50.0 U 41.9 38.7 83.8 77.4 1 1.00-152 7.94 55
Naphthalene 50.0 U 31.9 29.2 63.8 58.4 1 21.0-133 8.84 65
n-Nitrosodimethylamine 50.0 U 21.8 20.6 43.6 41.2 1 10.0-120 5.66 40
Phenanthrene 50.0 U 41.1 38.3 82.2 76.6 1 54.0-120 7.05 39
Pyrene 50.0 U 43.0 40.5 86.0 81.0 1 52.0-120 5.99 49
1,2,4-Trichlorobenzene 50.0 U 31.9 29.3 63.8 58.6 1 44.0-142 8.50 50
(S) Nitrobenzene-d5 53.7 46.8 15.0-314
(S) 2-Fluorobiphenyl 82.2 73.3 22.0-127
(S) p-Terphenyl-d14 88.6 82.2 29.0-141
(S) Phenol-d5 35.0 32.0 8.00-424
(S) 2-Fluorophenol 48.2 44.5 10.0-120
(S) 2,4,6-Tribromophenol 92.5 84.0 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 1

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190112 Work Order #:1103701744

COC ID # 00052444
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Charlotte, NC
Project Mgr: Troy Holzschuh
Address:1125 E Moorehead Street Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:Reina Clark
Shipped:FedExp
Tracking #:114522400031
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-01 12/20/2019 11:11am W 8 40 ML AMBER VOA HCL VPH MADEP VPH
VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
100 ML AMBER GLASS NONE SVOCs/BNA/TICs 625
1LG HCL EPH MADEP EPH
MW-02 12/20/2019 11:28am W 8 40 ML AMBER VOA HCL VPH MADEP VPH
VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
100 ML AMBER GLASS NONE SVOCs/BNA/TICs 625
1LG HCL EPH MADEP EPH
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/1 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52444 Printed: 02/21/2020
Analysis Name: BTEX/MTBE/IPE/Naph ( Water )
Analysis Description / Method:EPA Modified 602 / 602
Container Type / Preservative:VOA - 40 MILL / HCL
Analytes: Benzene ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Methyl tert butyl ether ug/L, Naphthalene ug/L, Toluene ug/L, m,p-Xylene ug/L, o-Xylene ug/L

Analysis Name: EPH ( Water )
Analysis Description / Method:Extractable Petroleum Hydrocarbons / MADEP EPH
Container Type / Preservative:1LG / HCL
Analytes: C11-C22 Aromatics ug/L, C19-C36 Aliphatics ug/L, C9-C18 Aliphatics ug/L, Extractable Petroleum Hydrocarbons ug/L

Analysis Name: SVOCs/BNA/TICs ( Water )
Analysis Description / Method:Base Neutral Acid Extractables and Tentatively Identified Compounds / 625
Container Type / Preservative:100 ML AMBER GLASS / NONE
Analytes: 1,2,4-Trichlorobenzene ug/L, 1,2-Dichlorobenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,4-Dichlorobenzene ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L,
3,3'-Dichlorobenzidine ug/L, 4-Bromophenyl phenyl ether ug/L, 4-Chlorophenyl phenyl ether ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzidine ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene
ug/L, Benzo(b)fluoranthene ug/L, Benzo(g,h,I)perylene ug/L, Benzo(k)fluoranthene ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-chloroisopropyl)ether ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl phthalate ug/L,
Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenz(a,h)anthracene ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L, Hexachlorobenzene ug/L,
Hexachlorobutadiene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodimethylamine ug/L,
N-Nitrosodiphenylamine ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Phenanthrene ug/L, Pyrene ug/L

Analysis Name: VPH ( Water )
Analysis Description / Method:Volatile Petroleum Hydrocarbons / MADEP VPH
Speedway LLC.1/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52444 Printed: 02/21/2020
Container Type / Preservative:40 ML AMBER VOA / HCL
Analytes: C5-C8 Aliphatics ug/L, C9-C10 Aromatics ug/L, C9-C12 Aliphatics ug/L, Total Volatile Hydrocarbons ug/L

Speedway LLC.2/2 https://www.speedway-ids.com
ANALYTICAL REPORT
February 28, 2020
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1189272
Samples Received:02/13/2020
Project Number:
Description:Speedway 6993
Site:6993
Report To:Mr. Troy Holzschuh
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
February 28, 2020
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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March 04, 2020
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 03/04/20 15:08 1 of 28
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-03R L1189272-01 5
MW-04R L1189272-02 7
TRIP BLANK L1189272-03 9
Qc: Quality Control Summary 10
Volatile Petroleum Hydrocarbons by Method MADEPV 10
Volatile Organic Compounds (GC/MS) by Method 602MS 11
TPH by Method MADEPE 12
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 14
Gl: Glossary of Terms 21
Al: Accreditations & Locations 22
Sc: Sample Chain of Custody 23
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-03R L1189272-01 GW John Sherrill 02/12/20 10:15 02/13/20 09:40
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1427563 1 02/14/20 07:29 02/14/20 07:29 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1428444 1 02/15/20 12:57 02/15/20 12:57 JLB Mt. Juliet, TN
TPH by Method MADEPE WG1428114 1 02/14/20 06:52 02/17/20 23:51 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1428114 1 02/14/20 06:52 02/18/20 01:50 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1429997 1 02/18/20 11:01 02/20/20 11:31 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1429997 1 02/18/20 11:01 02/20/20 16:42 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1428895 1 02/17/20 15:57 02/17/20 23:38 JF Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-04R L1189272-02 GW John Sherrill 02/12/20 09:50 02/13/20 09:40
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1427563 1 02/14/20 08:02 02/14/20 08:02 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1428444 1 02/15/20 13:17 02/15/20 13:17 JLB Mt. Juliet, TN
TPH by Method MADEPE WG1428114 1 02/14/20 06:52 02/18/20 00:15 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1428114 1 02/14/20 06:52 02/18/20 01:26 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1429997 1 02/18/20 11:01 02/20/20 11:57 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1429997 1 02/18/20 11:01 02/20/20 16:18 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1429926 1 02/19/20 15:05 02/19/20 23:13 JF Mt. Juliet, TN
Collected by Collected date/time Received date/time
TRIP BLANK L1189272-03 GW John Sherrill 02/12/20 00:00 02/13/20 09:40
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 602MS WG1428444 1 02/15/20 10:59 02/15/20 10:59 JLB Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 02/28/20 16:38 4 of 28
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 03/04/20 15:08 4 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1189272
MW-03R
Collected date/time: 02/12/20 10:15
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 02/14/2020 07:29 WG1427563
Unadjusted C9-C12 Aliphatics U 33.3 100 1 02/14/2020 07:29 WG1427563
Unadjusted C9-C10 Aromatics U 33.3 100 1 02/14/2020 07:29 WG1427563
Total VPH U 33.3 100 1 02/14/2020 07:29 WG1427563
(S) 2,5-Dibromotoluene(FID) 90.7 70.0-130 02/14/2020 07:29 WG1427563
(S) 2,5-Dibromotoluene(PID) 84.2 70.0-130 02/14/2020 07:29 WG1427563
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene 0.807 J 0.331 1.00 1 02/15/2020 12:57 WG1428444
Di-isopropyl ether U 0.320 1.00 1 02/15/2020 12:57 WG1428444
Ethylbenzene U 0.384 1.00 1 02/15/2020 12:57 WG1428444
Methyl tert-butyl ether U 0.367 1.00 1 02/15/2020 12:57 WG1428444
Naphthalene U 1.00 5.00 1 02/15/2020 12:57 WG1428444
Toluene U 0.412 1.00 1 02/15/2020 12:57 WG1428444
m&p-Xylenes U 0.719 2.00 1 02/15/2020 12:57 WG1428444
o-Xylene 1.66 0.341 1.00 1 02/15/2020 12:57 WG1428444
(S) Toluene-d8 90.7 80.0-120 02/15/2020 12:57 WG1428444
(S) 4-Bromofluorobenzene 88.1 77.0-126 02/15/2020 12:57 WG1428444
(S) 1,2-Dichloroethane-d4 96.0 70.0-130 02/15/2020 12:57 WG1428444
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 02/17/2020 23:51 WG1428114
Unadjusted C9-C18 Aliphatics U 33.3 100 1 02/20/2020 11:31 WG1429997
Unadjusted C19-C36 Aliphatics 43.1 B J 33.3 100 1 02/17/2020 23:51 WG1428114
Unadjusted C19-C36 Aliphatics U 33.3 100 1 02/20/2020 11:31 WG1429997
Unadjusted C11-C22 Aromatics 206 33.3 100 1 02/18/2020 01:50 WG1428114
Unadjusted C11-C22 Aromatics U 33.3 100 1 02/20/2020 16:42 WG1429997
Unadjusted Total Petroleum
Hydrocarbons 249 33.3 100 1 02/18/2020 01:50 WG1428114
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100 1 02/20/2020 16:42 WG1429997
(S) o-Terphenyl 68.7 40.0-140 02/18/2020 01:50 WG1428114
(S) o-Terphenyl 54.0 40.0-140 02/20/2020 16:42 WG1429997
(S) 1-Chloro-octadecane 10.6 J2 40.0-140 02/17/2020 23:51 WG1428114
(S) 1-Chloro-octadecane 25.1 J2 40.0-140 02/20/2020 11:31 WG1429997
(S) 2-Fluorobiphenyl 88.2 40.0-140 02/18/2020 01:50 WG1428114
(S) 2-Fluorobiphenyl 66.5 40.0-140 02/20/2020 16:42 WG1429997
(S) 2-Bromonaphthalene 83.5 40.0-140 02/18/2020 01:50 WG1428114
(S) 2-Bromonaphthalene 62.4 40.0-140 02/20/2020 16:42 WG1429997
Sample Narrative:
L1189272-01 WG1428114, WG1429997: Duplicate Analysis performed due to surrogate failure. Results don't confirm; both analyses reported
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,2,4-Trichlorobenzene U 0.355 10.0 1 02/17/2020 23:38 WG1428895
1,2-Dichlorobenzene U 0.340 10.0 1 02/17/2020 23:38 WG1428895
1,3-Dichlorobenzene U 0.365 10.0 1 02/17/2020 23:38 WG1428895
1,4-Dichlorobenzene U 0.322 10.0 1 02/17/2020 23:38 WG1428895
2,4-Dinitrotoluene U 1.65 10.0 1 02/17/2020 23:38 WG1428895
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 02/28/20 16:38 5 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 03/04/20 15:08 5 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1189272
MW-03R
Collected date/time: 02/12/20 10:15
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
2,6-Dinitrotoluene U 0.279 10.0 1 02/17/2020 23:38 WG1428895
2-Chloronaphthalene U J4 0.330 1.00 1 02/17/2020 23:38 WG1428895
3,3-Dichlorobenzidine U 2.02 10.0 1 02/17/2020 23:38 WG1428895
4-Bromophenyl-phenylether U 0.335 10.0 1 02/17/2020 23:38 WG1428895
4-Chlorophenyl-phenylether U 0.303 10.0 1 02/17/2020 23:38 WG1428895
Acenaphthene U 0.316 1.00 1 02/17/2020 23:38 WG1428895
Acenaphthylene U 0.309 1.00 1 02/17/2020 23:38 WG1428895
Anthracene U 0.291 1.00 1 02/17/2020 23:38 WG1428895
Benzidine U 4.32 10.0 1 02/17/2020 23:38 WG1428895
Benzo(a)anthracene U 0.0975 1.00 1 02/17/2020 23:38 WG1428895
Benzo(a)pyrene U 0.340 1.00 1 02/17/2020 23:38 WG1428895
Benzo(b)fluoranthene U 0.0896 1.00 1 02/17/2020 23:38 WG1428895
Benzo(g,h,i)perylene U 0.161 1.00 1 02/17/2020 23:38 WG1428895
Benzo(k)fluoranthene U 0.355 1.00 1 02/17/2020 23:38 WG1428895
Bis(2-chlorethoxy)methane U 0.329 10.0 1 02/17/2020 23:38 WG1428895
2,2-Oxybis(1-Chloropropane) U 0.445 10.0 1 02/17/2020 23:38 WG1428895
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 02/17/2020 23:38 WG1428895
Benzylbutyl phthalate U 0.275 3.00 1 02/17/2020 23:38 WG1428895
Chrysene U 0.332 1.00 1 02/17/2020 23:38 WG1428895
Di-n-butyl phthalate U 0.266 3.00 1 02/17/2020 23:38 WG1428895
Di-n-octyl phthalate U 0.278 3.00 1 02/17/2020 23:38 WG1428895
Dibenz(a,h)anthracene U 0.279 1.00 1 02/17/2020 23:38 WG1428895
Diethyl phthalate U 0.282 3.00 1 02/17/2020 23:38 WG1428895
Dimethyl phthalate U 0.283 3.00 1 02/17/2020 23:38 WG1428895
Fluoranthene U 0.310 1.00 1 02/17/2020 23:38 WG1428895
Fluorene U 0.323 1.00 1 02/17/2020 23:38 WG1428895
Hexachlorobenzene U 0.341 1.00 1 02/17/2020 23:38 WG1428895
Hexachloro-1,3-butadiene U 0.329 10.0 1 02/17/2020 23:38 WG1428895
Hexachlorocyclopentadiene U 2.33 10.0 1 02/17/2020 23:38 WG1428895
Hexachloroethane U 0.365 10.0 1 02/17/2020 23:38 WG1428895
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 02/17/2020 23:38 WG1428895
Isophorone U 0.272 10.0 1 02/17/2020 23:38 WG1428895
n-Nitrosodi-n-propylamine U 0.403 10.0 1 02/17/2020 23:38 WG1428895
n-Nitrosodimethylamine U 1.26 10.0 1 02/17/2020 23:38 WG1428895
n-Nitrosodiphenylamine U 1.19 10.0 1 02/17/2020 23:38 WG1428895
Naphthalene U 0.372 1.00 1 02/17/2020 23:38 WG1428895
Nitrobenzene U 0.367 10.0 1 02/17/2020 23:38 WG1428895
Phenanthrene U 0.366 1.00 1 02/17/2020 23:38 WG1428895
Pyrene U 0.330 1.00 1 02/17/2020 23:38 WG1428895
(S) Nitrobenzene-d5 59.0 15.0-314 02/17/2020 23:38 WG1428895
(S) 2-Fluorobiphenyl 61.3 22.0-127 02/17/2020 23:38 WG1428895
(S) p-Terphenyl-d14 68.0 29.0-141 02/17/2020 23:38 WG1428895
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 02/28/20 16:38 6 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 03/04/20 15:08 6 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1189272
MW-04R
Collected date/time: 02/12/20 09:50
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 02/14/2020 08:02 WG1427563
Unadjusted C9-C12 Aliphatics U 33.3 100 1 02/14/2020 08:02 WG1427563
Unadjusted C9-C10 Aromatics U 33.3 100 1 02/14/2020 08:02 WG1427563
Total VPH U 33.3 100 1 02/14/2020 08:02 WG1427563
(S) 2,5-Dibromotoluene(FID) 90.0 70.0-130 02/14/2020 08:02 WG1427563
(S) 2,5-Dibromotoluene(PID) 80.9 70.0-130 02/14/2020 08:02 WG1427563
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.331 1.00 1 02/15/2020 13:17 WG1428444
Di-isopropyl ether U 0.320 1.00 1 02/15/2020 13:17 WG1428444
Ethylbenzene U 0.384 1.00 1 02/15/2020 13:17 WG1428444
Methyl tert-butyl ether U 0.367 1.00 1 02/15/2020 13:17 WG1428444
Naphthalene U 1.00 5.00 1 02/15/2020 13:17 WG1428444
Toluene U 0.412 1.00 1 02/15/2020 13:17 WG1428444
m&p-Xylenes U 0.719 2.00 1 02/15/2020 13:17 WG1428444
o-Xylene U 0.341 1.00 1 02/15/2020 13:17 WG1428444
(S) Toluene-d8 92.2 80.0-120 02/15/2020 13:17 WG1428444
(S) 4-Bromofluorobenzene 92.4 77.0-126 02/15/2020 13:17 WG1428444
(S) 1,2-Dichloroethane-d4 96.2 70.0-130 02/15/2020 13:17 WG1428444
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 02/18/2020 00:15 WG1428114
Unadjusted C9-C18 Aliphatics U 33.3 100 1 02/20/2020 11:57 WG1429997
Unadjusted C19-C36 Aliphatics 67.7 B J 33.3 100 1 02/18/2020 00:15 WG1428114
Unadjusted C19-C36 Aliphatics U 33.3 100 1 02/20/2020 11:57 WG1429997
Unadjusted C11-C22 Aromatics 41.9 J 33.3 100 1 02/18/2020 01:26 WG1428114
Unadjusted C11-C22 Aromatics U 33.3 100 1 02/20/2020 16:18 WG1429997
Unadjusted Total Petroleum
Hydrocarbons 110 33.3 100 1 02/18/2020 01:26 WG1428114
Unadjusted Total Petroleum
Hydrocarbons U 33.3 100 1 02/20/2020 16:18 WG1429997
(S) o-Terphenyl 64.9 40.0-140 02/18/2020 01:26 WG1428114
(S) o-Terphenyl 52.0 40.0-140 02/20/2020 16:18 WG1429997
(S) 1-Chloro-octadecane 18.6 J2 40.0-140 02/18/2020 00:15 WG1428114
(S) 1-Chloro-octadecane 33.4 J2 40.0-140 02/20/2020 11:57 WG1429997
(S) 2-Fluorobiphenyl 88.0 40.0-140 02/18/2020 01:26 WG1428114
(S) 2-Fluorobiphenyl 68.9 40.0-140 02/20/2020 16:18 WG1429997
(S) 2-Bromonaphthalene 82.8 40.0-140 02/18/2020 01:26 WG1428114
(S) 2-Bromonaphthalene 64.9 40.0-140 02/20/2020 16:18 WG1429997
Sample Narrative:
L1189272-02 WG1428114, WG1429997: Duplicate Analysis performed due to surrogate failure. Results don't confirm; both analyses reported
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,2,4-Trichlorobenzene U 0.355 10.0 1 02/19/2020 23:13 WG1429926
1,2-Dichlorobenzene U 0.340 10.0 1 02/19/2020 23:13 WG1429926
1,3-Dichlorobenzene U 0.365 10.0 1 02/19/2020 23:13 WG1429926
1,4-Dichlorobenzene U 0.322 10.0 1 02/19/2020 23:13 WG1429926
2,4-Dinitrotoluene U 1.65 10.0 1 02/19/2020 23:13 WG1429926
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 02/28/20 16:38 7 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1189272 03/04/20 15:08 7 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1189272
MW-04R
Collected date/time: 02/12/20 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
2,6-Dinitrotoluene U 0.279 10.0 1 02/19/2020 23:13 WG1429926
2-Chloronaphthalene U 0.330 1.00 1 02/19/2020 23:13 WG1429926
3,3-Dichlorobenzidine U 2.02 10.0 1 02/19/2020 23:13 WG1429926
4-Bromophenyl-phenylether U 0.335 10.0 1 02/19/2020 23:13 WG1429926
4-Chlorophenyl-phenylether U 0.303 10.0 1 02/19/2020 23:13 WG1429926
Acenaphthene U 0.316 1.00 1 02/19/2020 23:13 WG1429926
Acenaphthylene U 0.309 1.00 1 02/19/2020 23:13 WG1429926
Anthracene U 0.291 1.00 1 02/19/2020 23:13 WG1429926
Benzidine U 4.32 10.0 1 02/19/2020 23:13 WG1429926
Benzo(a)anthracene U 0.0975 1.00 1 02/19/2020 23:13 WG1429926
Benzo(a)pyrene U 0.340 1.00 1 02/19/2020 23:13 WG1429926
Benzo(b)fluoranthene U 0.0896 1.00 1 02/19/2020 23:13 WG1429926
Benzo(g,h,i)perylene U 0.161 1.00 1 02/19/2020 23:13 WG1429926
Benzo(k)fluoranthene U 0.355 1.00 1 02/19/2020 23:13 WG1429926
Bis(2-chlorethoxy)methane U 0.329 10.0 1 02/19/2020 23:13 WG1429926
2,2-Oxybis(1-Chloropropane) U 0.445 10.0 1 02/19/2020 23:13 WG1429926
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 02/19/2020 23:13 WG1429926
Benzylbutyl phthalate U 0.275 3.00 1 02/19/2020 23:13 WG1429926
Chrysene U 0.332 1.00 1 02/19/2020 23:13 WG1429926
Di-n-butyl phthalate 0.523 J 0.266 3.00 1 02/19/2020 23:13 WG1429926
Di-n-octyl phthalate U 0.278 3.00 1 02/19/2020 23:13 WG1429926
Dibenz(a,h)anthracene U 0.279 1.00 1 02/19/2020 23:13 WG1429926
Diethyl phthalate U 0.282 3.00 1 02/19/2020 23:13 WG1429926
Dimethyl phthalate U 0.283 3.00 1 02/19/2020 23:13 WG1429926
Fluoranthene U 0.310 1.00 1 02/19/2020 23:13 WG1429926
Fluorene U 0.323 1.00 1 02/19/2020 23:13 WG1429926
Hexachlorobenzene U 0.341 1.00 1 02/19/2020 23:13 WG1429926
Hexachloro-1,3-butadiene U 0.329 10.0 1 02/19/2020 23:13 WG1429926
Hexachlorocyclopentadiene U 2.33 10.0 1 02/19/2020 23:13 WG1429926
Hexachloroethane U 0.365 10.0 1 02/19/2020 23:13 WG1429926
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 02/19/2020 23:13 WG1429926
Isophorone U 0.272 10.0 1 02/19/2020 23:13 WG1429926
n-Nitrosodi-n-propylamine U 0.403 10.0 1 02/19/2020 23:13 WG1429926
n-Nitrosodimethylamine U 1.26 10.0 1 02/19/2020 23:13 WG1429926
n-Nitrosodiphenylamine U 1.19 10.0 1 02/19/2020 23:13 WG1429926
Naphthalene U 0.372 1.00 1 02/19/2020 23:13 WG1429926
Nitrobenzene U 0.367 10.0 1 02/19/2020 23:13 WG1429926
Phenanthrene 0.444 J 0.366 1.00 1 02/19/2020 23:13 WG1429926
Pyrene U 0.330 1.00 1 02/19/2020 23:13 WG1429926
(S) Nitrobenzene-d5 77.8 15.0-314 02/19/2020 23:13 WG1429926
(S) 2-Fluorobiphenyl 81.2 22.0-127 02/19/2020 23:13 WG1429926
(S) p-Terphenyl-d14 84.8 29.0-141 02/19/2020 23:13 WG1429926
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1189272
TRIP BLANK
Collected date/time: 02/12/20 00:00
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzene U 0.331 1.00 1 02/15/2020 10:59 WG1428444
Di-isopropyl ether U 0.320 1.00 1 02/15/2020 10:59 WG1428444
Ethylbenzene U 0.384 1.00 1 02/15/2020 10:59 WG1428444
Methyl tert-butyl ether U 0.367 1.00 1 02/15/2020 10:59 WG1428444
Naphthalene U 1.00 5.00 1 02/15/2020 10:59 WG1428444
Toluene U 0.412 1.00 1 02/15/2020 10:59 WG1428444
m&p-Xylenes U 0.719 2.00 1 02/15/2020 10:59 WG1428444
o-Xylene U 0.341 1.00 1 02/15/2020 10:59 WG1428444
(S) Toluene-d8 91.0 80.0-120 02/15/2020 10:59 WG1428444
(S) 4-Bromofluorobenzene 89.6 77.0-126 02/15/2020 10:59 WG1428444
(S) 1,2-Dichloroethane-d4 96.5 70.0-130 02/15/2020 10:59 WG1428444
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1427563
Volatile Petroleum Hydrocarbons by Method MADEPV L1189272-01,02
Method Blank (MB)
(MB) R3501241-3 02/13/20 22:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 81.5 70.0-130
(S) 2,5-Dibromotoluene(PID) 78.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3501241-1 02/13/20 20:29 • (LCSD) R3501241-2 02/13/20 21:02
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1130 1170 94.2 97.5 70.0-130 3.48 25
Unadjusted C9-C12 Aliphatics 1400 1500 1550 107 111 70.0-130 3.28 25
Unadjusted C9-C10 Aromatics 200 207 211 104 105 70.0-130 1.91 25
Total VPH 2800 2840 2930 101 105 70.0-130 3.12 25
(S) 2,5-Dibromotoluene(FID) 99.4 96.7 70.0-130
(S) 2,5-Dibromotoluene(PID) 96.9 93.6 70.0-130
L1189188-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1189188-02 02/14/20 03:05 • (MS) R3501241-4 02/14/20 09:08 • (MSD) R3501241-5 02/14/20 10:02
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 U 876 792 73.0 66.0 1 70.0-130 J6 10.1 25
Unadjusted C9-C12 Aliphatics 1400 U 989 870 70.6 62.1 1 70.0-130 J6 12.8 25
Unadjusted C9-C10 Aromatics 200 U 131 116 65.5 58.0 1 70.0-130 J6 J6 12.1 25
Total VPH 2800 U 2000 1780 71.4 63.6 1 70.0-130 J6 11.6 25
(S) 2,5-Dibromotoluene(FID) 95.5 97.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 85.8 90.6 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1428444
Volatile Organic Compounds (GC/MS) by Method 602MS L1189272-01,02,03
Method Blank (MB)
(MB) R3501267-2 02/15/20 07:29
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
Toluene U 0.412 1.00
o-Xylene U 0.341 1.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 89.8 80.0-120
(S) 4-Bromofluorobenzene 89.4 77.0-126
(S) 1,2-Dichloroethane-d4 96.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3501267-1 02/15/20 06:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 4.75 95.0 70.0-123
Di-isopropyl ether 5.00 6.00 120 58.0-138
Ethylbenzene 5.00 4.40 88.0 79.0-123
Methyl tert-butyl ether 5.00 5.63 113 68.0-125
Naphthalene 5.00 4.87 97.4 54.0-135
Toluene 5.00 4.56 91.2 79.0-120
o-Xylene 5.00 4.54 90.8 80.0-122
m&p-Xylenes 10.0 9.14 91.4 80.0-122
(S) Toluene-d8 87.4 80.0-120
(S) 4-Bromofluorobenzene 88.0 77.0-126
(S) 1,2-Dichloroethane-d4 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1428114
TPH by Method MADEPE L1189272-01,02
Method Blank (MB)
(MB) R3501390-3 02/17/20 11:11
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 67.4 40.0-140
(S) 2-Fluorobiphenyl 88.1 40.0-140
(S) 2-Bromonaphthalene 82.5 40.0-140
Method Blank (MB)
(MB) R3501390-6 02/17/20 12:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 41.5 J 33.3 100
Unadjusted C19-C36 Aliphatics 52.0 J 33.3 100
(S) 1-Chloro-octadecane 40.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3501390-1 02/17/20 10:24 • (LCSD) R3501390-2 02/17/20 10:47
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 354 366 59.0 61.0 40.0-140 3.33 25
Unadjusted C19-C36 Aliphatics 800 573 583 71.6 72.9 40.0-140 1.73 25
(S) 1-Chloro-octadecane 39.0 40.5 40.0-140 J2
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3501390-4 02/17/20 11:35 • (LCSD) R3501390-5 02/17/20 11:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1280 1300 75.3 76.5 40.0-140 1.55 25
(S) o-Terphenyl 69.5 69.0 40.0-140
(S) 2-Fluorobiphenyl 89.4 89.5 40.0-140
(S) 2-Bromonaphthalene 84.0 84.0 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1429997
TPH by Method MADEPE L1189272-01,02
Method Blank (MB)
(MB) R3501324-1 02/19/20 12:21
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics U 33.3 100
(S) 1-Chloro-octadecane 46.4 40.0-140
Method Blank (MB)
(MB) R3501324-4 02/19/20 13:33
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 62.8 40.0-140
(S) 2-Fluorobiphenyl 85.5 40.0-140
(S) 2-Bromonaphthalene 80.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3501324-2 02/19/20 12:45 • (LCSD) R3501324-3 02/19/20 13:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 351 312 58.5 52.0 40.0-140 11.8 25
Unadjusted C19-C36 Aliphatics 800 553 483 69.1 60.4 40.0-140 13.5 25
(S) 1-Chloro-octadecane 54.5 52.3 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3501324-5 02/19/20 13:57 • (LCSD) R3501324-6 02/19/20 14:21
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 968 1030 56.9 60.6 40.0-140 6.21 25
(S) o-Terphenyl 53.5 60.0 40.0-140
(S) 2-Fluorobiphenyl 73.0 86.9 40.0-140
(S) 2-Bromonaphthalene 68.8 81.4 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1428895
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-01
Method Blank (MB)
(MB) R3500645-2 02/17/20 23:58
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
2,2-Oxybis(1-Chloropropane) U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
1,2-Dichlorobenzene U 0.340 10.0
1,3-Dichlorobenzene U 0.365 10.0
1,4-Dichlorobenzene U 0.322 10.0
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1428895
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-01
Method Blank (MB)
(MB) R3500645-2 02/17/20 23:58
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
(S) Nitrobenzene-d5 40.4 15.0-314
(S) 2-Fluorobiphenyl 45.7 22.0-127
(S) p-Terphenyl-d14 62.5 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3500645-1 02/17/20 23:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 28.3 56.6 47.0-145
Acenaphthylene 50.0 30.3 60.6 33.0-145
Anthracene 50.0 30.3 60.6 27.0-133
Benzidine 100 19.6 19.6 1.00-120
Benzo(a)anthracene 50.0 31.5 63.0 33.0-143
Benzo(b)fluoranthene 50.0 32.8 65.6 24.0-159
Benzo(k)fluoranthene 50.0 32.0 64.0 11.0-162
Benzo(g,h,i)perylene 50.0 30.8 61.6 1.00-219
Benzo(a)pyrene 50.0 33.4 66.8 17.0-163
Bis(2-chlorethoxy)methane 50.0 27.7 55.4 1.00-219
2,2-Oxybis(1-Chloropropane) 50.0 28.9 57.8 36.0-166
4-Bromophenyl-phenylether 50.0 30.4 60.8 53.0-127
2-Chloronaphthalene 50.0 26.3 52.6 60.0-120 J4
4-Chlorophenyl-phenylether 50.0 31.2 62.4 25.0-158
Chrysene 50.0 31.2 62.4 17.0-168
Dibenz(a,h)anthracene 50.0 31.0 62.0 1.00-227
1,2-Dichlorobenzene 50.0 27.3 54.6 27.0-120
1,3-Dichlorobenzene 50.0 27.2 54.4 26.0-120
1,4-Dichlorobenzene 50.0 26.8 53.6 26.0-120
3,3-Dichlorobenzidine 100 62.5 62.5 1.00-262
2,4-Dinitrotoluene 50.0 32.7 65.4 39.0-139
2,6-Dinitrotoluene 50.0 30.8 61.6 50.0-158
Fluoranthene 50.0 32.4 64.8 26.0-137
Fluorene 50.0 30.7 61.4 59.0-121
Hexachlorobenzene 50.0 28.8 57.6 1.00-152
Hexachloro-1,3-butadiene 50.0 24.3 48.6 24.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1428895
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-01
Laboratory Control Sample (LCS)
(LCS) R3500645-1 02/17/20 23:37
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Hexachlorocyclopentadiene 50.0 24.8 49.6 10.0-120
Hexachloroethane 50.0 26.9 53.8 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 30.4 60.8 1.00-171
Isophorone 50.0 30.4 60.8 21.0-196
Naphthalene 50.0 24.9 49.8 21.0-133
Nitrobenzene 50.0 26.5 53.0 35.0-180
n-Nitrosodimethylamine 50.0 20.5 41.0 10.0-120
n-Nitrosodiphenylamine 50.0 29.8 59.6 44.0-120
n-Nitrosodi-n-propylamine 50.0 34.8 69.6 1.00-230
Phenanthrene 50.0 30.2 60.4 54.0-120
Benzylbutyl phthalate 50.0 33.7 67.4 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 33.6 67.2 8.00-158
Di-n-butyl phthalate 50.0 34.6 69.2 1.00-120
Diethyl phthalate 50.0 34.2 68.4 1.00-120
Dimethyl phthalate 50.0 32.0 64.0 1.00-120
Di-n-octyl phthalate 50.0 32.1 64.2 4.00-146
Pyrene 50.0 32.0 64.0 52.0-120
1,2,4-Trichlorobenzene 50.0 24.3 48.6 44.0-142
(S) Nitrobenzene-d5 47.0 15.0-314
(S) 2-Fluorobiphenyl 54.8 22.0-127
(S) p-Terphenyl-d14 66.4 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1429926
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-02
Method Blank (MB)
(MB) R3501438-2 02/19/20 23:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
2,2-Oxybis(1-Chloropropane) U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
1,2-Dichlorobenzene U 0.340 10.0
1,3-Dichlorobenzene U 0.365 10.0
1,4-Dichlorobenzene U 0.322 10.0
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1429926
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-02
Method Blank (MB)
(MB) R3501438-2 02/19/20 23:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
(S) Nitrobenzene-d5 60.9 15.0-314
(S) 2-Fluorobiphenyl 70.6 22.0-127
(S) p-Terphenyl-d14 83.1 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3501438-1 02/19/20 23:26
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 38.2 76.4 47.0-145
Acenaphthylene 50.0 40.6 81.2 33.0-145
Anthracene 50.0 39.1 78.2 27.0-133
Benzidine 100 24.4 24.4 1.00-120
Benzo(a)anthracene 50.0 41.3 82.6 33.0-143
Benzo(b)fluoranthene 50.0 43.9 87.8 24.0-159
Benzo(k)fluoranthene 50.0 40.8 81.6 11.0-162
Benzo(g,h,i)perylene 50.0 39.0 78.0 1.00-219
Benzo(a)pyrene 50.0 43.3 86.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 33.5 67.0 1.00-219
2,2-Oxybis(1-Chloropropane) 50.0 35.8 71.6 36.0-166
4-Bromophenyl-phenylether 50.0 39.8 79.6 53.0-127
2-Chloronaphthalene 50.0 36.9 73.8 60.0-120
4-Chlorophenyl-phenylether 50.0 40.5 81.0 25.0-158
Chrysene 50.0 39.5 79.0 17.0-168
Dibenz(a,h)anthracene 50.0 41.1 82.2 1.00-227
1,2-Dichlorobenzene 50.0 35.7 71.4 27.0-120
1,3-Dichlorobenzene 50.0 34.7 69.4 26.0-120
1,4-Dichlorobenzene 50.0 34.7 69.4 26.0-120
3,3-Dichlorobenzidine 100 80.0 80.0 1.00-262
2,4-Dinitrotoluene 50.0 43.6 87.2 39.0-139
2,6-Dinitrotoluene 50.0 42.0 84.0 50.0-158
Fluoranthene 50.0 42.1 84.2 26.0-137
Fluorene 50.0 40.2 80.4 59.0-121
Hexachlorobenzene 50.0 39.8 79.6 1.00-152
Hexachloro-1,3-butadiene 50.0 32.3 64.6 24.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1429926
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-02
Laboratory Control Sample (LCS)
(LCS) R3501438-1 02/19/20 23:26
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Hexachlorocyclopentadiene 50.0 27.5 55.0 10.0-120
Hexachloroethane 50.0 33.5 67.0 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 40.3 80.6 1.00-171
Isophorone 50.0 35.8 71.6 21.0-196
Naphthalene 50.0 33.0 66.0 21.0-133
Nitrobenzene 50.0 33.2 66.4 35.0-180
n-Nitrosodimethylamine 50.0 25.2 50.4 10.0-120
n-Nitrosodiphenylamine 50.0 39.2 78.4 44.0-120
n-Nitrosodi-n-propylamine 50.0 40.1 80.2 1.00-230
Phenanthrene 50.0 39.6 79.2 54.0-120
Benzylbutyl phthalate 50.0 43.8 87.6 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 43.0 86.0 8.00-158
Di-n-butyl phthalate 50.0 43.9 87.8 1.00-120
Diethyl phthalate 50.0 43.2 86.4 1.00-120
Dimethyl phthalate 50.0 41.2 82.4 1.00-120
Di-n-octyl phthalate 50.0 42.5 85.0 4.00-146
Pyrene 50.0 41.8 83.6 52.0-120
1,2,4-Trichlorobenzene 50.0 32.3 64.6 44.0-142
(S) Nitrobenzene-d5 56.9 15.0-314
(S) 2-Fluorobiphenyl 76.3 22.0-127
(S) p-Terphenyl-d14 84.6 29.0-141
L1189427-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1189427-05 02/20/20 00:47 • (MS) R3501438-3 02/20/20 01:08 • (MSD) R3501438-4 02/20/20 01:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 ND 35.5 38.2 71.0 76.4 1 47.0-145 7.33 48
Acenaphthylene 50.0 ND 38.1 41.3 76.2 82.6 1 33.0-145 8.06 74
Anthracene 50.0 ND 38.4 39.7 76.8 79.4 1 27.0-133 3.33 66
Benzidine 100 ND 59.7 22.4 59.7 22.4 1 1.00-120 J3 90.9 40
Benzo(a)anthracene 50.0 ND 40.6 42.4 81.2 84.8 1 33.0-143 4.34 53
Benzo(b)fluoranthene 50.0 ND 42.3 42.8 84.6 85.6 1 24.0-159 1.18 71
Benzo(k)fluoranthene 50.0 ND 39.4 41.1 78.8 82.2 1 11.0-162 4.22 63
Benzo(g,h,i)perylene 50.0 ND 38.0 39.9 76.0 79.8 1 1.00-219 4.88 97
Benzo(a)pyrene 50.0 ND 42.2 43.6 84.4 87.2 1 17.0-163 3.26 72
Bis(2-chlorethoxy)methane 50.0 ND 31.4 33.1 62.8 66.2 1 33.0-184 5.27 54
2,2-Oxybis(1-Chloropropane) 50.0 ND 33.4 34.3 66.8 68.6 1 36.0-166 2.66 76
4-Bromophenyl-phenylether 50.0 ND 38.5 39.8 77.0 79.6 1 53.0-127 3.32 43
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1429926
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1189272-02
L1189427-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1189427-05 02/20/20 00:47 • (MS) R3501438-3 02/20/20 01:08 • (MSD) R3501438-4 02/20/20 01:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
2-Chloronaphthalene 50.0 ND 34.8 38.5 69.6 77.0 1 60.0-120 10.1 24
4-Chlorophenyl-phenylether 50.0 ND 37.5 40.7 75.0 81.4 1 25.0-158 8.18 61
Chrysene 50.0 ND 37.9 39.8 75.8 79.6 1 17.0-168 4.89 87
Dibenz(a,h)anthracene 50.0 ND 39.4 41.8 78.8 83.6 1 1.00-227 5.91 126
3,3-Dichlorobenzidine 100 ND 79.2 81.3 79.2 81.3 1 1.00-262 2.62 108
2,4-Dinitrotoluene 50.0 ND 41.6 44.8 83.2 89.6 1 39.0-139 7.41 42
2,6-Dinitrotoluene 50.0 ND 39.4 42.4 78.8 84.8 1 50.0-158 7.33 48
Fluoranthene 50.0 ND 41.5 42.8 83.0 85.6 1 26.0-137 3.08 66
Fluorene 50.0 ND 37.6 40.9 75.2 81.8 1 59.0-121 8.41 38
Hexachlorobenzene 50.0 ND 38.2 40.0 76.4 80.0 1 1.00-152 4.60 55
Hexachloro-1,3-butadiene 50.0 ND 32.2 33.9 64.4 67.8 1 24.0-120 5.14 62
Hexachlorocyclopentadiene 50.0 ND 27.7 30.1 55.4 60.2 1 10.0-146 8.30 34
Hexachloroethane 50.0 ND 33.5 34.5 67.0 69.0 1 40.0-120 2.94 52
Indeno(1,2,3-cd)pyrene 50.0 ND 39.1 40.7 78.2 81.4 1 1.00-171 4.01 99
Isophorone 50.0 ND 33.4 35.3 66.8 70.6 1 21.0-196 5.53 93
Naphthalene 50.0 ND 31.3 33.1 62.6 66.2 1 21.0-133 5.59 65
Nitrobenzene 50.0 ND 31.9 33.7 63.8 67.4 1 35.0-180 5.49 62
n-Nitrosodimethylamine 50.0 ND 25.6 26.0 51.2 52.0 1 10.0-120 1.55 40
n-Nitrosodiphenylamine 50.0 ND 37.8 39.1 75.6 78.2 1 16.0-160 3.38 28
n-Nitrosodi-n-propylamine 50.0 ND 36.0 38.2 72.0 76.4 1 1.00-230 5.93 87
Phenanthrene 50.0 ND 39.2 40.3 78.4 80.6 1 54.0-120 2.77 39
Benzylbutyl phthalate 50.0 ND 42.2 43.4 84.4 86.8 1 1.00-152 2.80 60
Bis(2-ethylhexyl)phthalate 50.0 ND 40.8 42.0 81.6 84.0 1 8.00-158 2.90 82
Di-n-butyl phthalate 50.0 ND 42.8 43.3 85.6 86.6 1 1.00-120 1.16 47
Diethyl phthalate 50.0 ND 40.5 42.6 81.0 85.2 1 1.00-120 5.05 100
Dimethyl phthalate 50.0 ND 39.1 41.0 78.2 82.0 1 1.00-120 4.74 183
Di-n-octyl phthalate 50.0 ND 40.6 42.5 81.2 85.0 1 4.00-146 4.57 69
Pyrene 50.0 ND 40.6 41.2 81.2 82.4 1 52.0-120 1.47 49
1,2,4-Trichlorobenzene 50.0 ND 31.6 32.9 63.2 65.8 1 44.0-142 4.03 50
(S) Nitrobenzene-d5 53.1 56.7 15.0-314
(S) 2-Fluorobiphenyl 71.2 78.1 22.0-127
(S) p-Terphenyl-d14 82.6 83.5 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190112 Work Order #:1103701744

COC ID # 00052759
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Charlotte, NC
Project Mgr: Troy Holzschuh
Address:1125 E Moorehead Street Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:John Sherrill
Shipped:FedExp
Tracking #:arrived
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-03R 02/12/2020 10:15am W 13 40 ML AMBER VOA HCL VPH MADEP VPH
VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
100 ML AMBER GLASS NONE SVOCs/BNA/TICs 625
1LG HCL EPH MADEP EPH
MW-04R 02/12/2020 09:50am W 13 40 ML AMBER VOA HCL VPH MADEP VPH
VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
100 ML AMBER GLASS NONE SVOCs/BNA/TICs 625
1LG HCL EPH MADEP EPH
TRIP BLANK 02/12/2020 12:00am W 1 VOA - 40 MILL HCL BTEX/MTBE/IPE/Naph 602
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/2 https://www.speedway-ids.com
Page 2 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190112 Work Order #:1103701744

COC ID # 00052759
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Charlotte, NC
Project Mgr: Troy Holzschuh
Address:1125 E Moorehead Street Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:John Sherrill
Shipped:FedExp
Tracking #:arrived
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52759 Printed: 04/13/2020
Analysis Name: BTEX/MTBE/IPE/Naph ( Water )
Analysis Description / Method:EPA Modified 602 / 602
Container Type / Preservative:VOA - 40 MILL / HCL
Analytes: Benzene ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Methyl tert butyl ether ug/L, Naphthalene ug/L, Toluene ug/L, m,p-Xylene ug/L, o-Xylene ug/L

Analysis Name: EPH ( Water )
Analysis Description / Method:Extractable Petroleum Hydrocarbons / MADEP EPH
Container Type / Preservative:1LG / HCL
Analytes: C11-C22 Aromatics ug/L, C19-C36 Aliphatics ug/L, C9-C18 Aliphatics ug/L, Extractable Petroleum Hydrocarbons ug/L

Analysis Name: SVOCs/BNA/TICs ( Water )
Analysis Description / Method:Base Neutral Acid Extractables and Tentatively Identified Compounds / 625
Container Type / Preservative:100 ML AMBER GLASS / NONE
Analytes: 1,2,4-Trichlorobenzene ug/L, 1,2-Dichlorobenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,4-Dichlorobenzene ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L,
3,3'-Dichlorobenzidine ug/L, 4-Bromophenyl phenyl ether ug/L, 4-Chlorophenyl phenyl ether ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzidine ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene
ug/L, Benzo(b)fluoranthene ug/L, Benzo(g,h,I)perylene ug/L, Benzo(k)fluoranthene ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-chloroisopropyl)ether ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl phthalate ug/L,
Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenz(a,h)anthracene ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L, Hexachlorobenzene ug/L,
Hexachlorobutadiene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodimethylamine ug/L,
N-Nitrosodiphenylamine ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Phenanthrene ug/L, Pyrene ug/L

Analysis Name: VPH ( Water )
Analysis Description / Method:Volatile Petroleum Hydrocarbons / MADEP VPH
Speedway LLC.1/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52759 Printed: 04/13/2020
Container Type / Preservative:40 ML AMBER VOA / HCL
Analytes: C5-C8 Aliphatics ug/L, C9-C10 Aromatics ug/L, C9-C12 Aliphatics ug/L, Total Volatile Hydrocarbons ug/L

Speedway LLC.2/2 https://www.speedway-ids.com

APPENDIX E
MID-ATLANTIC FIELD PROCEDURES
Monitoring Well Installation Procedures I. Shallow Type II Monitoring Wells These wells are typically constructed in a borehole made by a power auger and penetrate the top portion of the shallow water table. The wells are typically constructed of two-inch
diameter (although they can be larger), Schedule 40 PVC casing with 0.010-inch mechanically slotted well screen placed in the bottom of the well. These wells are constructed such that the well screen intersects the water table at the time of construction. A gravel pack (typically clean washed sand) is used to fill the borehole annular space around the screened interval and is usually terminated one to two feet
above the top of the screen. A typically two-foot thick layer of bentonite is then placed in
the annular space above the sand pack, and the remainder of the annular space is filled from bottom to top with a Portland cement/bentonite mixture pumped through a tremie pipe. The monitoring wells are equipped with locking caps and fitted with flush-mounted protective manhole covers or above-ground “stick-up” protectors.

Note: for site-specific well construction details, refer to Well Construction Records II. Deep Type III Monitoring Wells
Deep, Type III monitoring wells are constructed with two “telescoping” casings, an inner
casing and an outer casing. The outer casing is larger in diameter (typically six-inch diameter Schedule 40 PVC) and typically extends from land surface to bedrock or a confining unit. The bottom of this casing is typically firmly set into the top of bedrock or other confining layer and then tremie-grouted into the borehole. After the grout has
cured, the borehole is then advanced below the bottom of the outer casing by drilling
through the outer casing to the desired depth. The inner casing (typically two-inch diameter Schedule 40 PVC) is constructed with a screened interval that monitors water within bedrock fractures or other deeper water-bearing zones. The borehole annulus is then filled with gravel pack, bentonite, and grout and finished at land surface as
described above.
Note: for site-specific well construction details, refer to Well Construction Records
Soil Sampling Procedures

I. Sample Collection

Direct Push Technology (DPT, or “Geoprobe”)

DPT uses a truck-mounted hydraulic rig to push a steel sampling probe into the
subsurface to collect soil and/or groundwater samples. The sampling device used to
collect the soil samples during this investigation was the “macrocore” sampler. This
sampler consists of a four-foot long, two-inch diameter stainless steel spoon containing a
clear, acetate liner. When the macrocore sampler is driven into the subsurface, the soil is
collected into the acetate liner and then retrieved to the land surface. The liner is then cut
open and the soil lithology is characterized and soil samples are collected.

Split Spoon Sampling

This method of soil sampling is typically used during advancement of hollowstem augers
for the construction of monitoring wells. Soil samples are obtained from the borings by
driving a prewashed, 1-3/8-inch inner-diameter split-spoon sampler at five foot intervals to
termination in general accordance with ASTM D-1586 (Standard Penetration Test)
specifications. Blow counts for each six inches of split-spoon penetration are recorded
during advancement of the spoon. Samples are then retrieved to the land surface, the
split-spoon is opened, and the soil lithology is characterized and soil samples are
collected.

Hand Augering

This method is typically used for shallow sampling in areas where access is limited or
underground obstacles such as utilities may be present. A pre-washed, three-inch
diameter steel auger bucket is attached to extension rods and manually turned to
penetrate the subsurface to the desired sampling depth. Samples are then retrieved to the
land surface and the soil lithology is characterized and soil samples are collected directly
from the hand auger bucket.

Excavator Bucket Sampling

This method is typically used during UST excavation and soil excavation projects. The soil
samples are collected from the excavator bucket when it is not safe to collect the samples
by other means. Care is taken when collecting samples from the bucket to avoid soil that
has come in contact with the bucket itself to avoid cross contamination.

II. Headspace Field Screening

A portion of each sample is removed from the sampling device and placed in a pre-
labeled, plastic "ziploc" bag. After several minutes, the gas contained in the "headspace"
or void area within the bag is tested with a photoionization detection (PID) and/or Flame
Ionization Detector (FID). These are useful as scanning devices to detect the presence of
volatile organic compounds (VOCs) but are not relied upon to determine specific levels of
contamination. Typically, the samples exhibiting the highest headspace readings will be
submitted to the laboratory for analysis.

III. Preparation for Laboratory Analysis

The sample collector dons new nitrile sampling gloves prior to handling each sample. The
samples are placed into laboratory-prepared, pre-labeled, sampling containers, packed in
ice, and shipped to a certified laboratory under chain-of-custody control. The sampler
places an executed custody seal on the cooler prior to leaving the sampler’s custody.
Laboratory analyses to be performed on the samples, along with other sampling
information, are specified on the chain-of-custody, which is placed in the cooler with the
samples.

Groundwater Sampling Procedures

I. Sample Collection

A. Monitoring Wells

Prior to sample collection, each well is purged of three to five standing well volumes or to
dryness to remove stagnant water from the well and well bore in an effort to collect
samples that are representative of the water quality in the formation surrounding each
well. Purging is performed either with a new, polyethylene bailer dedicated to each well, or
with a decontaminated pump. Samples are retrieved from the monitoring well using the
dedicated bailer. New nylon string is used on each dedicated bailer, and new nitrile
sampling gloves are donned prior to purging and sampling of each well.

B. Geoprobe “Screen Point Sampler”

The screen point sampler is a “grab” sampling device that is driven into the saturated zone
and a surrounding metal sheath is retracted, exposing a screen. Groundwater entering the
screen is then drawn to land surface through disposable tubing that is placed through the
hollow push rods. The sample is collected from the tubing into the appropriate sampling
glassware.

C. Water-Supply Wells

Water samples are typically collected from the available spigot that is nearest to the well.
The water is allowed to run at a high flow from the spigot for approximately 10 to 15
minutes to allow the water in the delivery lines to be purged. The sample flow is then
reduced and the samples are collected directly into pre-labeled containers as described
below. New nitrile sampling gloves are donned prior to sampling of each well.

D. Treatment System Influent/Effluent

Samples are typically collected from the influent or effluent of pump-and-treat groundwater
remediation systems using designated sampling ports in the influent and effluent water
transport lines. The water is typically allowed to run for several seconds to clear potential
debris in the sampling port. The sample is then collected directly into sampling containers
as described below. New nitrile sampling gloves are donned prior to sample collection.

II. Preparation for Laboratory Analysis

Groundwater samples are decanted directly into laboratory-prepared, pre-labeled, sampling
containers, packed in ice, and shipped to a certified laboratory under chain-of-custody control.
Laboratory analyses performed on the samples are specified on the chain-of-custody.