FA-7962_42202_CA_IAR_20190603

An Equal Opportunity Employer

June 3, 2019

Mr. Kenneth Currie
North Carolina Department of Environmental Quality
Fayetteville Regional Office
Division of Waste Management – UST Section
225 Green Street, Suite 714
Fayetteville, NC 28301

Subject: UST CLOSURE AND
INITIAL ABATEMENT ACTION REPORT
SPEEDWAY 6993
670 NORTH REILLY ROAD
FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA
INCIDENT NO.: 42202
FACILITY ID: 00-0-0015515

Dear Mr. Currie:

Speedway LLC is pleased to submit the enclosed UST Closure and Initial Abatement Action
Report for the Speedway 6993 facility located at 670 N. Reilly Road in Fayetteville, North
Carolina. The attached report documents the results of the underground storage tank closure
and initial abatement actions for the above-referenced facility. If you have any questions, please
feel free to contact me at [phone] or Patrick Kelly with Mid-Atlantic Associates, Inc. at
[phone].

Sincerely,

SPEEDWAY LLC
Charles A. Chiara
Environmental Representative

Speedway LLC

Speedway Office
P.O. Box 1500
Springfield, OH 45501
Telephone [phone]

UST CLOSURE AND INITIAL ABATEMENT ACTION REPORT
SPEEDWAY 6993
670 N. REILLY ROAD
FAYETTEVILLE, CUMBERLAND COUNTY, NORTH CAROLINA
INCIDENT NO.: 42202
FACILITY I.D. NO.: 0-00-15515
MID-ATLANTIC JOB NO. 000R3243.00

UST Section Risk Classification: Unassigned
Land Use: Unassigned
Latitude: N 35.099832
Longitude: W -78.010845
Date Discovered: March 1, 2019
Estimated Quantity of Release: Unknown
Cause/Source of Release: Diesel

Prepared For:

Mr. Charles A. Chiara
Speedway LLC
500 Speedway Drive
Enon, OH 45323

Prepared By:

Mid-Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610

June 3, 2019

TABLE OF CONTENTS

List of Acronyms

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................. 1
1.1 Introduction ......................................................................................................... 1
1.2 Owner/Operator of the UST ................................................................................ 1
1.3 Property Owner .................................................................................................. 1
1.4 Facility Information ............................................................................................. 1
1.5 Contacts ............................................................................................................. 1
1.6 UST Information ................................................................................................. 2
1.7 Site Characteristics............................................................................................. 2

2.0 UST CLOSURE PROCEDURES ...................................................................................... 3
2.1 Pre-Closure Procedures ..................................................................................... 3
2.2 Excavation Procedures ....................................................................................... 3
2.3 Excavated Soil .................................................................................................... 4
2.4 Sampling Procedures ......................................................................................... 4
2.5 Quality Control Measures ................................................................................... 5
2.6 Investigative Results ........................................................................................... 5
2.7 Backfilling Procedures ........................................................................................ 5

3.0 INITIAL RESPONSE AND ABATEMENT ACTION .......................................................... 5

4.0 EXCAVATION OF PETROLEUM-IMPACTED SOIL ........................................................ 6
4.1 Over-Excavation and Sampling Activities ........................................................... 6
4.2 Backfilling Procedures ........................................................................................ 6
4.3 Quality Control Measures ................................................................................... 6
4.4 Investigative Results ........................................................................................... 7

5.0 REGULATORY STATUS .................................................................................................. 7

6.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS ............................................ 7

DRAWINGS

Drawing 1.1 Topographic Site Map
Drawing 1.2 Site Map
Drawing 1.3 Soil Sample Location Map
Drawing 2.1 UST Closure Soil Analytical Results – February 27 through March 5, 2019
Drawing 4.1 Over Excavation Soil Analytical Results – March 6, 2019

TABLES

Table 2.1 Summary of Soil Sampling – UVF Results
Table 4.1 Summary of Soil Sampling - Risk-Based Analytical Results

TABLE OF CONTENTS (Cont.)

APPENDICES

Appendix A UST-3, UST-61 & UST-2A Forms
Appendix B Tank Removal and Waste Disposal Documentation
Appendix C Mid-Atlantic Soil Sampling Procedure
Appendix D Laboratory Analytical Report and Chain-of-Custody Record

i
LIST OF ACRONYMS

AFVR Aggressive Fluid-Vapor Recovery
AS Air Sparge
AST Aboveground Storage Tank

BQL Below (Laboratory Practical) Quantitation Limit
BLS Below Land Surface BTEX Benzene, Toluene, Ethylbenzene, Xylenes

CAP Corrective Action Plan
cm Centimeter
COC Constituents of Concern
CSA Comprehensive Site Assessment

DIPE Diisopropyl Ether (also IPE: Isopropyl Ether)
DNAPL Dense Non-Aqueous Phase Liquids
DO Dissolved Oxygen
DPT Direct Push Technology
DRO Diesel Range Organics
DSCA North Carolina Dry-Cleaning Solvent Act
DTW Depth to Water
DWM Division of Waste Management
DWR Division of Water Resources

EDB Ethylene di-bromide
EPA Environmental Protection Agency
EPH Extractable Petroleum Hydrocarbons

FID Flame Ionization Detector
FT Feet

GCL Gross Contamination Level
GIS Geographic Information System
GPM Gallons Per Minute
GPS Global Positioning System
GRO Gasoline Range Organics

Guidelines Underground Storage Tank Section Guidelines for
Assessment and Corrective Action For UST
Releases, DENR, Division of Waste Management
UST Section (most recent version)

ID Identification
IDW Investigation Derived Waste
IGQS Interim Groundwater Quality Standards

LSA Limited Site Assessment
LUST Leaking Underground Storage Tank

m Meter
MADEP Massachusetts Department of Environmental
Protection
Mid-Atlantic Mid-Atlantic Associates, Inc.
MDL Method Detection Limit
mg/Kg Milligrams per Kilogram
mg/L Milligrams per Liter
MMP Minimum Management Practices
MMPE Mobile Multi-Phase Extraction
MNA Monitored Natural Attenuation
MSCC Maximum Soil Contaminant Concentration
MSL Mean Sea Level

MTBE Methyl tertiary butyl ether
g/Kg Micrograms per Kilogram
g/L Micrograms per Liter

NA Not Analyzed
N/A Not Applicable
NC North Carolina
NCAC North Carolina Administrative Code
NCDENR North Carolina Department of Environment
and Natural Resources
NCDEQ North Carolina Department of Environmental
Quality
NCDOT North Carolina Department of
Transportation
NCGQS North Carolina Groundwater Quality
Standards
NCSWQS North Carolina Surface Water Quality
Standards
ND Not Detected
NM Not Measured
NORR Notice of Regulatory Requirements
NOV Notice of Violation
NS Not Sampled

OVA Organic Vapor Analyzer

PA Prioritization Assessment
PAA Prioritization Assessment Agreement
PAH Polynuclear Aromatic Hydrocarbons
Pb Lead
PCBs Polychlorinated Biphenyls
PCE Perchloroethylene (also tetrachloroethene)
PPB Parts Per Billion
PPM Parts Per Million
PID Photo Ionization Detector
POTW Publicly Owned Treatment Works
PQL Practical Quantitation Limit
PRF Prioritization Ranking Form
PVC Polyvinyl chloride

RBCA Risk-Based Corrective Action
RCRA Resource Conservation and Recovery Act
ROI Radius of Influence

s Seconds
SAR Soil Assessment Report
SOW Scope of Work
STG Soil-to-Groundwater
SVE Soil Vapor Extraction
SVOC Semi-Volatile Organic Compound

TDHF Toxicologically Defined Hydrocarbon
Fractions
TCLP Toxicity Characteristic Leaching Procedure
TIC Tentatively Identified Compound
TOC Top of Casing
TPH Total Petroleum Hydrocarbons

US United States
USCS Unified Soil Classification System
USGS United States Geological Survey
UST Underground Storage Tank
UT Unnamed Tributary
VOC Volatile Organic Compounds
VPH Volatile Petroleum Hydrocarbons
yr Year

1.0 SITE HISTORY AND CHARACTERIZATION

1.1 Introduction

The site is the Speedway Store 6993 located at 670 N. Reilly Road, Fayetteville, Cumberland
County, North Carolina (Drawings 1.1 & 1.2). The site is a petroleum retail facility and convenience
store and contained four underground storage tanks (USTs) total: three 10,000 gallon capacity
USTs (regular gasoline, premium gasoline, and diesel fuel) and one 6,000 gallon capacity UST
(kerosene). The three 10,000 gallon capacity USTs were located to the north of the building and
dispensers, and the one 6,000 gallon capacity UST was located to the east.

The objective of this report was to document the removal of four USTs located on the subject
site, as Speedway is selling this property. This report presents background information, the
laboratory analytical results, and our findings, conclusions and recommendations. The opinions
included herein are based on our experience and the information obtained during the study. This
report is based on limited observations made on the dates noted using the procedures described
herein. If additional information becomes available, we request the opportunity to review the
information, reassess the potential environmental concerns and modify our conclusions and
recommendations, if appropriate.

1.2 Owner/Operator of the UST

Speedway LLC
500 Speedway Drive
Enon, Ohio 45323

1.3 Property Owner

Wilcohess LLC (who was purchased by Speedway LLC in 2014)
539 S Main Street
Findlay, Ohio 45840

1.4 Facility Information

Speedway 6993
670 N. Reilly Road
Fayetteville, North Carolina 28303

1.5 Contacts

Primary Contacts: Mr. Charles A. Chiara, Speedway LLC
500 Speedway Drive
Enon, OH 45323
[phone]

Closure Contractor: A&D Environmental Services
PO Box 484
High Point, North Carolina 27263
[phone]
UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 2
Fayetteville, North Carolina

Consultant: Mid-Atlantic Associates, Inc.
1125 E. Morehead St. Suite 104
Charlotte, North Carolina 28204
Mr. Patrick Kelly, P.G.

Laboratory: RED Lab
5598 Marvin Moss Lane
MARBIONC Building, Suite 2003
Wilmington, North Carolina 28409
[phone]

Pace National
12065 Lebanon Road
Mt. Juliet, Tennessee 37122
[phone]

1.6 UST Information

Three registered 10,000-gallon and one registered 6,000-gallon steel tanks existed on the
property prior to closure. Refer to Drawing 1.3 for the former location of the tanks, with applicable
UST information summarized below:

UST ID
Number
Previous
Contents
Capacity
(Gallons)
Tank
Dimensions
Construction
Details
Date
Installed
Status of
UST
Release
Associated
with
System
1 Gasoline 10,000 Approximately
10’ x 17’
Single-
walled steel 1979 Removed
2/27/19 No
2 Gasoline 10,000 Approximately
10’ x 17’
Single-
walled steel 1979 Removed
2/27/19 No
3 Diesel 10,000 Approximately
10’ x 17’
Single-
walled steel 1979 Removed
2/27/19 Yes
4 Kerosene 6,000 Approximately
8’ x 16’
Single-
walled steel 1979 Removed
2/27/19 No

1.7 Site Characteristics

According to the Cumberland County, North Carolina GIS website, the owner of the site is listed as
WilcoHess, LLC. On October 1, 2014, Speedway, LLC purchased the site from Hess Corporation,
who had previously purchased the site from WilcoHess, LLC. The site has been a retail petroleum
UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 3
Fayetteville, North Carolina

station since 1979, when the tanks were reportedly installed. The site operated as a retail petroleum
station until September 2018 when the store was closed. The nearest downgradient surface water
body is located approximately 1,500 feet to the west of the property. Surface drainage and
groundwater flow, determined based on topography (Drawing 1.1) is expected to be generally
towards the west.

2.0 UST CLOSURE PROCEDURES

2.1 Pre-Closure Procedures

Prior to the commencement of UST closure activities, Mid-Atlantic submitted a UST-3 Notice of
Intent: UST Permanent Closure or Change In Service (UST-3) form to NCDEQ on February 11,
2019. A copy of the UST-3 form is included in Appendix A. Mid-Atlantic Associates (MAA) mobilized
to the site on February 25, 2019 to oversee the excavation activities for the UST removal. Tanks 1,
2, and 4 did not contain liquids prior to cleaning. Tank 3 had approximately one inch of residual
diesel fuel. On February 26, 2019, A&D Environmental Services (A&D), a contractor for Speedway,
power-washed the inside of the tanks and removed a total of approximately 330 gallons of wash
water and sludge from the USTs. A&D then transported the liquid off-site to their facility for disposal.
A copy of the disposal manifest is provided in Appendix B.

2.2 Excavation Procedures

A&D obtained a UST removal permit prior to removal of the tanks. The assistant Fire Marshal from
the Cumberland County Fire Marshal’s Office (Mr. J. Naylor) was onsite and approved removal of
the tanks.

A&D uncovered the USTs, excavated the tanks, and transported petroleum-contaminated soil to a
certified disposal facility. The top of all four USTs were located approximately 3 feet below land
surface (BLS). After approval by the Fire Marshal, the USTs were removed from the ground. As the
USTs were uncovered, soils were screened with a Mini-Rae 3000 Photo-Ionization Detector (PID)
and were segregated into separate soil stockpiles for later evaluation or disposal. All four tanks
appeared to be in good condition with minor corrosion and pitting observed, but no obvious holes.
Petroleum impact was identified in the soils overlaying the three, 10,000-gallon tanks. This material
was stockpiled onsite and was later transported to Earthtec of NC, Inc. (Earthtec) in Sanford,
North Carolina for disposal. No petroleum impacts to soil were observed in the overburden soils at
the 6,000-gallon kerosene UST.

The approximate locations of the former USTs and the approximate excavation areas are shown on
Drawing 1.3. The 10,000-gallon tanks measured approximately 10 feet in diameter by 17 feet long,
and the 6,000-gallon UST measured approximately 8 feet by 16 feet. The disposal manifest for the
tanks is provided in Appendix B.

UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 4
Fayetteville, North Carolina

2.3 Excavated Soil

During excavation activities, soils were routinely screened for the presence of volatile organic
vapors with a PID. Excavated clean soils above the tanks and product lines were placed to the
side of the excavations to be used as clean fill. Based on the PID readings and olfactory
observations, the soils above Tanks 1, 2, and 3 were impacted with petroleum, and were
therefore removed for disposal. Approximately 14 tons excavated petroleum-impacted soils
were stockpiled onsite on plastic, and were subsequently taken to Earthtec for disposal. No
impacts were detected above the North Carolina TPH Action Levels in the soils below Tanks 1,
2, or 3. No impacts were observed in the soils at Tank-4. The PID readings of the UST closure
confirmation sample locations are documented in Table 2.1.

The All four steel tanks were removed on February 27, 2019 and transported by Solis
Transportation of Fayetteville, North Carolina to Omni Recycling in Fayetteville, North Carolina.
Documentation of disposal is provided in Appendix B.

2.4 Sampling Procedures

Upon removal, UST closure samples were collected according to procedures outlined in the
NCDEQ’s Underground Storage Tank Section Guidelines for Site Checks, Tank Closure, and Initial
Response and Abatement. Tank pit and product line samples were collected at the locations shown
in Drawing 1.3. UST closure samples collected underneath the former Tanks 1, 2 and 3 were
collected at approximately 14 feet BLS at the north and south ends of the tank, and below former
Tank 4 at approximately 12 feet BLS at the east and west ends of the tank. Soil samples were also
collected at 10 foot intervals along the product lines, and from below the dispenser spill bucket.
Dispenser and product lines samples were collected from a depth of 3 feet BLS.

On February 26, it was noted that two types of product lines were in place at the site. Based on field
observations, the product lines were constructed of double walled flexible plastic piping and were
connected to the USTs and dispensers. In addition, an out of service single wall fiberglass piping
system was noted to be abandoned in place, suggesting that the fiberglass lines had been
historically upgraded to double-walled plastic. The fiberglass lines were noted to be dry with no
residual fuel observed. Speedway directed Mid-Atlantic and A&D to remove the abandoned
fiberglass product lines and to contact the NCDEQ to determine if soil sampling and reporting was
conducted during the product lines system upgrade. On February 27, Mid-Atlantic contacted Mr.
Ken Currie of the NCDEQ Fayetteville Regional Office UST Section to obtain information on the
product line upgrade. Mr. Currie informed Mid-Atlantic that historically, reporting and sampling of the
out of service product lines during an upgrade was only required when a release was identified. Mr.
Currie indicated that the UST Section did not have records documenting the UST system upgrade
and the UST Section inspection notes did not provide a clear date when the system was upgraded.
Mr. Currie instructed Mid-Atlantic to proceed with the line closure as planned.

The soil samples were analyzed onsite by RED Lab for Total Petroleum Hydrocarbons (TPH)
Gasoline Range and Diesel Range Organics (DRO/GRO), benzene, toluene, ethylbenzene, and
xylenes (BTEX), total aromatics, and 16 EPA polycyclic aromatic hydrocarbons (PAHs). Following
sample collection, Mid-Atlantic placed the samples into labeled zip-lock bags and handed them
UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 5
Fayetteville, North Carolina

directly to the RED Lab technician onsite for preparation and analysis for TPH-GRO and DRO using
the UVF Method.

2.5 Quality Control Measures

The UST closure soil samples were retrieved using the excavator bucket with care being taken so
that sampled soil did not have contact with the bucket. Product line, dispenser, and stockpile
samples were collected using properly decontaminated hand auger buckets. New nitrile gloves
were worn during the collection and handling of soil samples. Further quality control measures are
described in the sampling procedures outlined in Appendix C and the laboratory analytical reports
from RED Lab is included in Appendix D.

2.6 Investigative Results

A total of 50 Samples were collected during the UST closure phase. The laboratory analytical report
for the soil samples collected at the site is provided in Appendix D. As summarized in Table 2.2,
and Drawing 2.1, test results indicated the presence of TPH-GRO and TPH-DRO exceeding the
regulatory action level of 50 milligrams/kilogram (mg/kg) and 100 mg/kg, respectively, in grab soil
samples collected from beneath Dispenser-2 and the associated piping (P-5). Soil stockpile sample
SP-LP (1) had exceedances for TPH-GRO and TPH-DRO. Sample SP-LP (2) had an exceedance
for TPH-GRO. Both soil piles consisted of the impacted soils overlaying Tanks 1, 2, and 3.

The laboratory analytical report for the confirmation soil samples did not indicate the presence of
either TPH-GRO or TPH-DRO above the regulatory actions levels at any other locations during the
initial sampling activities.

2.7 Backfilling Procedures

Backfilling was conducted upon receipt of analytical data from RED Lab and typically finished
on the same day. Backfill material included clean fill removed from above the USTs and
processed fill (screenings) obtained from Henson’s of Bunnlevel, North Carolina. The backfill
was mechanically compacted using the backhoe bucket.

3.0 INITIAL RESPONSE AND ABATEMENT ACTION

Petroleum-impacted soils above Tanks 1, 2, and 3 were screened with a PID. Excavation was
conducted to uncover the USTs to facilitate UST removal and continued around the USTs until
PID measurements were less than 5 parts per million (ppm). Excavated impacted soils were
removed from the UST excavation and directly-loaded into a dump truck and transported to
Earthtec, as previously noted. The laboratory test results from analysis of the confirmation soil
samples collected from beneath the USTs indicated that impacted soils had been removed.

Laboratory analytical data indicated the presence of a release in the vicinity of the diesel
dispenser (Disp-6) and adjacent product line sample (P-5). Following the receipt of the UST
closure analytical data, a release was reported to the NCDEQ via telephone on March 1, 2019.
A “UST-61 24-hour Release and UST Leak Release” form was subsequently submitted to the
UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 6
Fayetteville, North Carolina

NCDEQ Fayetteville Regional Office on March 4, 2019. A copy of the UST-61 form is included
in Appendix A. Following the submittal of the UST-61 form, over-excavation activities were
conducted in the vicinity of UST closure samples “Disp-6” and “P-5”. The initial abatement
activities conducted on March 6, 2019 are discussed below.

4.0 EXCAVATION OF PETROLEUM-IMPACTED SOIL

4.1 Over-Excavation and Sampling Activities

Over-excavation was conducted at Dispenser-2/P-5, (Drawing 2.1) since both samples were above
the NCDEQ TPH-GRO and DRO action levels. At Mid-Atlantic’s direction, A&D excavated down to
6 feet BLS at this location. The excavation was terminated due to the close proximity to the canopy
support and the risk of undermining the support footer. During excavation activities, Mid-Atlantic
personnel screened soils using a PID and submitted samples to RED Lab for field analysis and
confirmation. Once the limits of the excavation had been reached, five confirmatory soil samples
were collected from the sidewalls (OE-DISP-2-N, OE-DISP-2-E, OE-DISP-2-S, OE-DISP-2-W) and
pit bottom (OE-DISP-2) of the over-excavation area. The samples were then submitted to RED Lab
for laboratory analysis of TPH-GRO/DRO. Additional samples were submitted to Pace National of
Mt. Juliet, Tennessee for VOCs by EPA Method 8260, SVOCs by Method 8270, and VPH and EPH
by MADEP.

The depths and locations of the five confirmatory soil samples are identified on Tables 2.2 and 4.1,
which includes a summary of laboratory analytical results for both the UST closure and over-
excavation soil sampling. A copy of the laboratory analytical reports is provided in Appendix D. The
excavated soils (approximately 1 ton) was stockpiled onsite on plastic and covered. The soils
were then containerized in drums by A&D, and transported off-site for disposal at the A&D
facility in High Point, North Carolina. Copies of the Soil Manifest and Certificate of Acceptance
and Disposal are included in Appendix B.

4.2 Backfilling Procedures

After removal of the UST, collection of closure samples, and over-excavation activities, the
excavation was backfilled. Backfill material included re-used excavated soil that did not exhibit
laboratory evidence of residual impacts, and clean imported fill.

4.3 Quality Control Measures

The over-excavation soil samples were retrieved using the excavator bucket. Samples were
collected as discussed in the Mid-Atlantic field procedures included in Appendix C. New nitrile
gloves were worn during the collection and handling of the soils. The samples were placed into pre-
labeled, laboratory-supplied glassware, placed into an ice-filled cooler and shipped under chain-of-
custody to Pace National in Mt. Juliet, Tennessee.

UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 7
Fayetteville, North Carolina

4.4 Investigative Results

The laboratory analytical report and chain-of-custody record for UST closure and over-excavation
samples are included in Appendix D and the results summarized in Tables 2.1 and 4.1, and
Drawing 4.1. The laboratory results indicate that contaminated soils still remain at concentrations
exceeding the NCDEQ soil-to-groundwater MSCCs. In addition, concentrations of C9-C22
Aromatics were identified in sample OE-DISP #2 (N) in excess of the NCDEQ residential
MSCCs. Excavation activities were limited due to canopy structural integrity concerns, and
petroleum impacted soils remain in the subsurface above the residential soils MSCC.

5.0 REGULATORY STATUS

A release from Dispenser-2 has been confirmed at the site, and petroleum impacted soil remains in
the subsurface. Mid-Atlantic submitted form UST-61, 24-Hour Release and UST Leak Reporting
Form, to the NCDEQ on March 4, 2019. Mid-Atlantic submitted a copy of the UST-2A, Site
Investigation Report for Permanent Closure or Change in Service of Registered UST to NCDEQ.
Copies of these documents are included in Appendix A.

6.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS

Summary:

 Three 10,000-gallon and one 6,000-gallon steel USTs were removed during closure
activities and transported to the Omni Recycling facility in Fayetteville, North Carolina.
Additionally piping associated with the UST system was removed and properly disposed;

 A total of 303 gallons of petroleum-impacted water generated during UST cleaning activities
was removed from the site during UST closure activities. The water was transported to the
A&D facility in High Point, North Carolina;

 A total of approximately 15 Tons of petroleum-impacted soil was removed from the site
during UST closure activities. Approximately 14 tons of soil was transported to the Earthtec
facility in Sanford, North Carolina; and approximately one ton of soil was transported to the
A&D facility in High Point, North Carolina;

 Laboratory analytical results confirm a release from overburden soils above Tanks 1, 2, and
3 with contaminant concentrations above the NCDEQ’s action level of 50 mg/kg for TPH-
GRO and 100 mg/kg for TPH-DRO. These overburden soils were removed and transported
to Earthtec for disposal; and

 Confirmation soil sample analytical results from the Dispenser-2 over-excavation confirm
the presence impacted soils above NCDEQ’s action level of 50 mg/kg for TPH-GRO and
100 mg/kg for TPH-DRO. These soils were over-excavated but excavation was limited due
to structural integrity concerns for the canopy.

UST Closure and Initial Abatement Action Report June 3, 2019
Speedway 6993 Page 8
Fayetteville, North Carolina

Conclusions:

 Closure sampling below the USTs indicates impacted soils were removed during the UST
closure activities and do not exceed regulatory limits; and

 Soil exceeding the Residential MSCC for C9-C22 Aromatics remains in the subsurface in
the vicinity of samples Disp-2 and P-5.

Recommendations:

 Mid-Atlantic recommends the completion of a Limited Site Assessment in the vicinity of
Dispenser #2; and

 We recommend the submittal of this report to the NCDEQ Fayetteville Regional Office,
DWM, UST Section for their review.

DRAWINGS

TABLES
Sample ID (Ft. BLS)Sample Depth
(FT)
Field Screening
(PPM)
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total Aromatics
(C10-C35)16 EPA PAHs
Action Level NE 50 100 NE NE NE
TANK 1 - 1 (14') 14 NM <0.64 <0.64 1.2 1.2 0.92 0.01
TANK 1 - 2 (14') 14 NM <0.63 <0.63 0.25 0.25 0.06 0.007
TANK 2 - 1 (14') 14 23.8 <0.56 <0.56 2.2 2.2 1 0.06
TANK 2 - 2 (14') 14 27.9 <0.61 <0.61 <0.24 <0.61 <0.01 <0.01
TANK 3 - 1 (14') 14 17.7 <0.66 <0.66 <0.27 <0.66 <0.01 <0.01
TANK 3 - 2 (14') 14 19.6 <0.64 <0.64 <0.26 <0.64 <0.01 <0.01
TANK 4 - 1 E (12') 12 NM <0.73 <0.73 0.17 0.17 0.16 0.008
TANK 4 - 2 W (12') 12 NM <0.65 <0.65 1.2 1.2 0.73 0.04
DISP - 1 3 2.6 <0.4 <0.4 <0.16 <0.4 <0.008 <0.008
DISP - 2 3 31 <23.2 958 7,743 8,701 1,155 41.6
DISP - 3 3 4.3 <0.44 <0.44 0.18 0.18 0.04 0.005
DISP - 4 3 1.3 <0.62 <0.62 <0.25 <0.62 <0.01 <0.01
DISP - 5 3 1.2 <0.42 <0.42 <0.17 <0.42 <0.008 <0.008
DISPENSER 6 (3-3.5') 3 NM <0.52 <0.52 0.08 0.08 0.07 0.005
FG - 1 (3-3.5') 3.5 4.1 <0.6 <0.6 0.1 0.1 0.1 0.009
FG - 10 / P - 11 3 0.6 <0.72 <0.72 <0.29 <0.72 <0.01 <0.01
FG - 11 / P - 12 3 1 <0.77 <0.77 1.1 1.1 0.63 0.04
FG - 12 / P - 13 3 1.1 <0.39 <0.39 0.05 0.05 0.05 0.01
FG - 13 / P - 14 3 1.1 <0.42 <0.42 0.07 0.07 0.06 0.007
FG - 14 / P - 15 3 0.7 <0.76 <0.76 0.08 0.08 0.08 0.009
FG - 15 / P - 20 3 0.5 <0.64 <0.64 <0.26 <0.64 <0.01 <0.01
FG - 16 3 0.7 <0.52 <0.52 0.34 0.34 0.55 0.01
FG - 17 / P - 21 3 0.6 <0.55 <0.55 0.08 0.08 0.08 0.008
FG - 18 / P - 22 3 0.9 <0.53 <0.53 <0.21 <0.53 <0.01 <0.01
FG - 2 (3-3.5') 3.5 1.2 <0.74 <0.74 0.88 0.88 0.55 0.03
FG - 3 (3-3.5') 3.5 2.2 <0.49 <0.49 0.1 0.1 0.09 0.009
FG - 4 (3-3.5') 3.5 3.3 <0.5 <0.5 <0.2 <0.5 <0.01 <0.01
FG - 5 / P - 6 3 0.6 <0.47 <0.47 0.35 0.35 0.33 0.04
FG - 6 / P - 7 3 0.9 <0.48 <0.48 <0.19 <0.48 <0.01 <0.01
FG - 7 / P - 8 3 0.3 <0.66 <0.66 <0.27 <0.66 <0.01 <0.01
FG - 8 / P - 9 3 0.8 <0.57 <0.57 0.11 0.11 0.11 0.01
FG - 9 / P - 10 3 13.6 <0.57 <0.57 0.67 0.67 0.34 0.02
P - 1 (3-3.5') 3.5 1.2 <0.53 <0.53 1.2 1.2 0.68 0.04
P - 16 3 0.2 <0.59 <0.59 2.6 2.6 1.3 0.07
P - 17 3 0.3 <0.57 <0.57 0.12 0.12 0.12 0.01
P - 18 3 0.3 <0.48 <0.48 0.46 0.46 0.59 0.009
P - 19 3 0.6 <0.57 <0.57 0.14 0.14 0.14 0.01
P - 2 (3-3.5') 3.5 1.8 <0.58 <0.58 0.92 0.92 0.48 0.02
P - 3 (3-3.5') 3.5 2.1 <0.64 <0.64 <0.25 <0.64 <0.01 <0.01
P - 4 (3-3.5') 3.5 1.5 <0.54 <0.54 0.35 0.35 0.33 0.04
P - 5 (3-3.5') 3.5 34.6 <27.2 1,040 7,776 8,816 1,171 42.1
SP - FG - 10 THRU F6 - 18 / P - 11 THRU P - 22 (A) NA NM <1.5 <1.5 41.5 41.5 20.5 1.1
SP - FG - 10 THRU F6 - 18 / P - 11 THRU P - 22 (B) NA NM <0.43 <0.43 25.7 25.7 13.4 0.71
SP - G NA NM <0.73 1.6 4.4 6 1.4 0.06
SP - K1 NA NM <0.77 <0.77 2.2 2.2 1.2 0.07
SP - LP (1) NA NM <2.3 377.7 1,575 1,953 283.7 10.5
SP - LP (2) NA NM <0.64 62.4 30.2 92.6 5.7 0.29
SP - P - 4 THRU P - 8 / F6 - 1 THRU F6 - 9 (A) NA NM <0.62 <0.62 4.3 4.3 2.4 0.14
SP - P - 4 THRU P - 8 / F6 - 1 THRU F6 - 9 (B) NA NM <0.42 <0.42 4.1 4.1 2.3 0.13
SP - P (1-4') NA NM <0.62 <0.62 2.1 2.1 1.1 0.06
OE - DISP - 2 6.5 1,218 <3.3 366.5 1,106 1,473 113.6 4.3
OE - DISP - 2 - E 6 768 <2.8 473.1 1,714 2,187 156.3 6
OE - DISP - 2 - N 6 1,200 <7.5 444.8 1,674 2,119 142.6 5.4
OE - DISP - 2 - S 6 1,113 <8.4 133.7 69 202 45.1 1.6
OE - DISP - 2 - W 6 1,028 <19.2 322.6 1,165 1,488 95.1 3.6
Notes:
FT - Feet
BLS - Below Land Surface
PPM - Parts Per Million
mg/Kg - Milligrams per Kilogram
TPH-GRO - Total Petroleum Hydrocarbons, Gasoline Range Organics
Bold values exceed the TPH Action Level of 50 mg/Kg for TPH-GRO
NA - Not Analized - Sample Lost in Transit
J - Detected below the laboratory reporting limit, but above the MDL
MDL - Method Detection Limit
SPEEDWAY 6993
MID-ATLANTIC PROJECT NO.: R3243.00
FAYETTEVILLE, NORTH CAROLINA
TABLE 2.1
SUMMARY OF SOIL SAMPLING - UVF RESULTS
NE NE NE NE NE NE NE NE NE NE NE NE NE940 4,600 0.88 620 620 313 469 46 469 939 1,500 31,000 46924,000 122,000 8 16,400 16,400 8,176 12,264 410 12,264 24,528 40,000 810,000 12,2648.2 940 0.35 290 47 0.16 56 6.6 270 68 540Health Based Level >100%31SampleSample DateSample Depth (FT)PID Measurement (PPM)Acenaphthene (mg/kg)Anthracene (mg/kg)Benzo(a)anthracene (mg/kg)Fluoranthene (mg/kg)Flourene (mg/kg)Naphthalene (mg/kg)Phenanthrene (mg/kg)Bis(2-ethylhexyl)phthalate (mg/kg)Pyrene (mg/kg)C5-C8 Aliphatics (mg/kg)C9-C18 Aliphatics (mg/kg)C19-C36 Aliphatics (mg/kg)C9-C22 Aromatics (mg/kg)OE DISP #2 (BOTTOM) 6.5' 03/06/19 6.5 1,218 0.027 J 0.0111 J 0.00532 J 0.00669 J 0.0353 J3.540.0481 ND ND304461 6.66 J441.4OE DISP #2 (E) 6' 03/06/19 6 768 0.0317 J 0.0118 J ND 0.00818 J 0.0407 ND 0.0511 ND 0.0205 J337363J 22.1366.0OE DISP #2 (N) 6' 03/06/19 6 1,200 0.0459 0.0160 J 0.00702 J 0.0102 J 0.060410.60.0747 0.0227 0.0197 J598 628.72.55 J559.0OE DISP #2 (S) 6' 03/06/19 6 1,113 0.0156 J ND ND ND 0.0179 J0.7530.0272 J ND ND87.8 J151.1J 4.84 J157.6OE DISP #2 (W) 6' 03/06/19 6 1,028 0.0366 J 0.0114 J ND 0.00795 J 0.0416 ND 0.0541 0.0206 J ND 56.3 162.4 ND127.2Notes:mg/kg - milligrams per kilogramNE - Not establishedND - Not detected at or above laboratory quantation limitsJ - The reported value is an estimate and the identification of the analyte is acceptable. J3 - The associated batch QC was outside the established quality control range for precisionMSCC-Maximum Soil Contaminant ConcentrationsBold values exceed Soil to Groundwater MSCCShaded cell values exceed Residential MSCCMADEP Semi-Volitile Organic CompoundsTABLE 4.1SUMMARY OF SOIL SAMPLING - RISK-BASED ANALYTICAL RESULTSSPEEDWAY #6993FAYETTEVILLE, NORTH CAROLINAMID-ATLANTIC PROJECT NO.: R3243.00Industrial/Commercial MSCCSoil-to-groundwater MSCCMethodAction LevelResidential MSCC

APPENDIX A

UST-3, UST-61, & UST-2A FORMS

APPENDIX B

TANK REMOVAL AND WASTE
DISPOSAL DOCUMENTATION

APPENDIX C

MID-ATLANTIC SOIL SAMPLING PROCEDURE
Soil Sampling Procedures

I. Sample Collection

Direct Push Technology (DPT, or “Geoprobe”)

DPT uses a truck-mounted hydraulic rig to push a steel sampling probe into the
subsurface to collect soil and/or groundwater samples. The sampling device used to
collect the soil samples during this investigation was the “macrocore” sampler. This
sampler consists of a four-foot long, two-inch diameter stainless steel spoon containing a
clear, acetate liner. When the macrocore sampler is driven into the subsurface, the soil is
collected into the acetate liner and then retrieved to the land surface. The liner is then cut
open and the soil lithology is characterized and soil samples are collected.

Split Spoon Sampling

This method of soil sampling is typically used during advancement of hollowstem augers
for the construction of monitoring wells. Soil samples are obtained from the borings by
driving a prewashed, 1-3/8-inch inner-diameter split-spoon sampler at five foot intervals to
termination in general accordance with ASTM D-1586 (Standard Penetration Test)
specifications. Blow counts for each six inches of split-spoon penetration are recorded
during advancement of the spoon. Samples are then retrieved to the land surface, the
split-spoon is opened, and the soil lithology is characterized and soil samples are
collected.

Hand Augering

This method is typically used for shallow sampling in areas where access is limited or
underground obstacles such as utilities may be present. A pre-washed, three-inch
diameter steel auger bucket is attached to extension rods and manually turned to
penetrate the subsurface to the desired sampling depth. Samples are then retrieved to the
land surface and the soil lithology is characterized and soil samples are collected directly
from the hand auger bucket.

Excavator Bucket Sampling

This method is typically used during UST excavation and soil excavation projects. The soil
samples are collected from the excavator bucket when it is not safe to collect the samples
by other means. Care is taken when collecting samples from the bucket to avoid soil that
has come in contact with the bucket itself to avoid cross contamination.

II. Headspace Field Screening

A portion of each sample is removed from the sampling device and placed in a pre-
labeled, plastic "ziploc" bag. After several minutes, the gas contained in the "headspace"
or void area within the bag is tested with a photoionization detection (PID) and/or Flame
Ionization Detector (FID). These are useful as scanning devices to detect the presence of
volatile organic compounds (VOCs) but are not relied upon to determine specific levels of
contamination. Typically, the samples exhibiting the highest headspace readings will be
submitted to the laboratory for analysis.

III. Preparation for Laboratory Analysis

The sample collector dons new nitrile sampling gloves prior to handling each sample. The
samples are placed into laboratory-prepared, pre-labeled, sampling containers, packed in
ice, and shipped to a certified laboratory under chain-of-custody control. The sampler
places an executed custody seal on the cooler prior to leaving the sampler’s custody.
Laboratory analyses to be performed on the samples, along with other sampling
information, are specified on the chain-of-custody, which is placed in the cooler with the
samples.

APPENDIX D

LABORATORY ANALYTICAL REPORT
AND CHAIN-OF-CUSTODY RECORD
ANALYTICAL REPORT
April 09, 2019
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1076982
Samples Received:03/08/2019
Project Number:
Description:Speedway #6993
Site:6993
Report To:Mr. Patrick Kelly
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
April 09, 2019
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
April 09, 2019
T. Alan Harvill
Project Manager
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
OE DISP#2 (BOTTOM) 6.5' L1076982-01 6
OE DISP#2 (E) 6' L1076982-02 9
OE DISP#2 (N) 6' L1076982-03 12
OE DISP#2 (S) 6' L1076982-04 15
OE DISP#2 (W) 6' L1076982-05 18
Qc: Quality Control Summary 21
Total Solids by Method 2540 G-2011 21
Volatile Petroleum Hydrocarbons by Method MADEPV 22
Volatile Organic Compounds (GC/MS) by Method 8260D 23
Semi-Volatile Organic Compounds (GC) by Method MADEPE 34
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 36
Gl: Glossary of Terms 41
Al: Accreditations & Locations 42
Sc: Sample Chain of Custody 43
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
OE DISP#2 (BOTTOM) 6.5' L1076982-01 Solid Gary A. Fischer 03/06/19 11:40 03/08/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1248621 1 03/12/19 13:10 03/12/19 13:16 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1249073 2000 03/14/19 18:39 03/14/19 18:39 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1247993 80 03/06/19 11:40 03/10/19 22:36 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1249284 80 03/06/19 11:40 03/13/19 20:26 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 03:20 AAT Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 10:11 AAT Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 1 03/12/19 21:44 03/13/19 05:51 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 10 03/12/19 21:44 03/14/19 00:59 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
OE DISP#2 (E) 6' L1076982-02 Solid Gary A. Fischer 03/06/19 11:55 03/08/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1248621 1 03/12/19 13:10 03/12/19 13:16 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1249073 2000 03/14/19 19:12 03/14/19 19:12 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1247993 80 03/06/19 11:55 03/10/19 22:55 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1249284 80 03/06/19 11:55 03/13/19 20:45 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 03:44 AAT Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 09:47 AAT Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 1 03/12/19 21:44 03/13/19 04:42 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 10 03/12/19 21:44 03/14/19 00:39 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
OE DISP#2 (N) 6' L1076982-03 Solid Gary A. Fischer 03/06/19 12:10 03/08/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1248621 1 03/12/19 13:10 03/12/19 13:16 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1249073 2000 03/14/19 19:46 03/14/19 19:46 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1247993 80 03/06/19 12:10 03/10/19 23:13 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1249284 80 03/06/19 12:10 03/13/19 21:05 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 04:08 AAT Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 09:22 AAT Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 1 03/12/19 21:44 03/13/19 03:56 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 10 03/12/19 21:44 03/13/19 23:59 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
OE DISP#2 (S) 6' L1076982-04 Solid Gary A. Fischer 03/06/19 12:25 03/08/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1248621 1 03/12/19 13:10 03/12/19 13:16 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1249073 1000 03/14/19 20:19 03/14/19 20:19 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1247993 40 03/06/19 12:25 03/10/19 23:32 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1249284 40 03/06/19 12:25 03/13/19 21:25 ACG Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 04:32 AAT Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 08:58 AAT Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 1 03/12/19 21:44 03/13/19 04:19 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 10 03/12/19 21:44 03/14/19 00:19 AO Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
OE DISP#2 (W) 6' L1076982-05 Solid Gary A. Fischer 03/06/19 12:40 03/08/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1248621 1 03/12/19 13:10 03/12/19 13:16 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1249073 100 03/14/19 20:52 03/14/19 20:52 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1248240 8 03/06/19 12:40 03/11/19 21:04 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 04:57 AAT Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method MADEPE WG1248324 1 03/11/19 14:51 03/15/19 08:34 AAT Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 1 03/12/19 21:44 03/13/19 03:10 AO Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1247945 10 03/12/19 21:44 03/13/19 23:39 AO Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1076982
OE DISP#2 (BOTTOM) 6.5'
Collected date/time: 03/06/19 11:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.1 1 03/12/2019 13:16 WG1248621
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 304 82.1 247 2000 03/14/2019 18:39 WG1249073
Unadjusted C9-C12 Aliphatics 316 82.1 247 2000 03/14/2019 18:39 WG1249073
Unadjusted C9-C10 Aromatics 360 82.1 247 2000 03/14/2019 18:39 WG1249073
Total VPH 980 B 82.1 247 2000 03/14/2019 18:39 WG1249073
(S) 2,5-Dibromotoluene(FID)94.0 70.0-130 03/14/2019 18:39 WG1249073
(S) 2,5-Dibromotoluene(PID)93.2 70.0-130 03/14/2019 18:39 WG1249073
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.0493 0.247 80 03/10/2019 22:36 WG1247993
1,1,1-Trichloroethane U 0.0271 0.247 80 03/10/2019 22:36 WG1247993
1,1,2,2-Tetrachloroethane U 0.0385 0.247 80 03/10/2019 22:36 WG1247993
1,1,2-Trichloroethane U 0.0870 0.247 80 03/10/2019 22:36 WG1247993
1,1-Dichloroethane U 0.0567 0.247 80 03/10/2019 22:36 WG1247993
1,1-Dichloroethene U 0.0493 0.247 80 03/10/2019 22:36 WG1247993
1,1-Dichloropropene U 0.0690 0.247 80 03/10/2019 22:36 WG1247993
1,2,3-Trichlorobenzene U 0.0616 0.247 80 03/10/2019 22:36 WG1247993
1,2,3-Trichloropropane U 0.503 1.23 80 03/10/2019 22:36 WG1247993
1,2,4-Trichlorobenzene U 0.476 1.23 80 03/10/2019 22:36 WG1247993
1,2,4-Trimethylbenzene 87.6 0.114 0.493 80 03/10/2019 22:36 WG1247993
1,2-Dibromo-3-Chloropropane U 0.503 2.47 80 03/10/2019 22:36 WG1247993
1,2-Dibromoethane U 0.0518 0.247 80 03/10/2019 22:36 WG1247993
1,2-Dichlorobenzene U 0.143 0.493 80 03/10/2019 22:36 WG1247993
1,2-Dichloroethane U 0.0468 0.247 80 03/10/2019 22:36 WG1247993
1,2-Dichloropropane U 0.126 0.493 80 03/10/2019 22:36 WG1247993
1,3,5-Trimethylbenzene 31.0 0.106 0.493 80 03/10/2019 22:36 WG1247993
1,3-Dichlorobenzene U 0.168 0.493 80 03/10/2019 22:36 WG1247993
1,3-Dichloropropane U 0.173 0.493 80 03/10/2019 22:36 WG1247993
1,4-Dichlorobenzene U 0.195 0.493 80 03/10/2019 22:36 WG1247993
2,2-Dichloropropane U 0.0781 0.247 80 03/10/2019 22:36 WG1247993
2-Butanone (MEK)U 1.23 2.47 80 03/10/2019 22:36 WG1247993
2-Chlorotoluene U 0.0907 0.247 80 03/10/2019 22:36 WG1247993
4-Chlorotoluene U 0.111 0.493 80 03/10/2019 22:36 WG1247993
4-Methyl-2-pentanone (MIBK)U 0.986 2.47 80 03/10/2019 22:36 WG1247993
Acetone U 1.36 2.47 80 03/10/2019 22:36 WG1247993
Acrylonitrile U 0.187 1.23 80 03/10/2019 22:36 WG1247993
Benzene 0.0686 J 0.0394 0.0986 80 03/10/2019 22:36 WG1247993
Bromobenzene U J4 0.104 1.23 80 03/10/2019 22:36 WG1247993
Bromodichloromethane U 0.0777 0.247 80 03/10/2019 22:36 WG1247993
Bromoform U 0.589 2.47 80 03/10/2019 22:36 WG1247993
Bromomethane U 0.365 1.23 80 03/10/2019 22:36 WG1247993
Carbon tetrachloride U 0.106 0.493 80 03/10/2019 22:36 WG1247993
Chlorobenzene U 0.0565 0.247 80 03/10/2019 22:36 WG1247993
Chlorodibromomethane U 0.0444 0.247 80 03/10/2019 22:36 WG1247993
Chloroethane U 0.106 0.493 80 03/13/2019 20:26 WG1249284
Chloroform U 0.0409 0.247 80 03/10/2019 22:36 WG1247993
Chloromethane U 0.137 1.23 80 03/10/2019 22:36 WG1247993
Dichlorodifluoromethane U 0.0806 0.247 80 03/10/2019 22:36 WG1247993
Di-isopropyl ether U 0.0345 0.0986 80 03/10/2019 22:36 WG1247993
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1076982
OE DISP#2 (BOTTOM) 6.5'
Collected date/time: 03/06/19 11:40
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 12.4 0.0523 0.247 80 03/10/2019 22:36 WG1247993
Isopropylbenzene 3.47 0.0851 0.247 80 03/10/2019 22:36 WG1247993
Methyl tert-butyl ether U 0.0291 0.0986 80 03/10/2019 22:36 WG1247993
Methylene Chloride U 0.655 2.47 80 03/10/2019 22:36 WG1247993
Naphthalene 11.8 0.308 1.23 80 03/10/2019 22:36 WG1247993
Styrene U 0.269 1.23 80 03/10/2019 22:36 WG1247993
Tetrachloroethene U 0.0690 0.247 80 03/10/2019 22:36 WG1247993
Toluene 3.06 0.123 0.493 80 03/10/2019 22:36 WG1247993
Trichloroethene U 0.0394 0.0986 80 03/13/2019 20:26 WG1249284
Trichlorofluoromethane U 0.0493 0.247 80 03/10/2019 22:36 WG1247993
Vinyl chloride U 0.0673 0.247 80 03/10/2019 22:36 WG1247993
Xylenes, Total 66.8 0.471 0.641 80 03/10/2019 22:36 WG1247993
cis-1,2-Dichloroethene U 0.0680 0.247 80 03/10/2019 22:36 WG1247993
cis-1,3-Dichloropropene U 0.0668 0.247 80 03/10/2019 22:36 WG1247993
n-Butylbenzene 3.96 0.378 1.23 80 03/10/2019 22:36 WG1247993
n-Propylbenzene 14.6 0.116 0.493 80 03/10/2019 22:36 WG1247993
p-Isopropyltoluene 0.978 0.229 0.493 80 03/10/2019 22:36 WG1247993
sec-Butylbenzene 1.60 0.249 1.23 80 03/10/2019 22:36 WG1247993
tert-Butylbenzene U 0.153 0.493 80 03/10/2019 22:36 WG1247993
trans-1,2-Dichloroethene U 0.141 0.493 80 03/10/2019 22:36 WG1247993
trans-1,3-Dichloropropene U 0.150 0.493 80 03/10/2019 22:36 WG1247993
(S) Toluene-d8 105 75.0-131 03/10/2019 22:36 WG1247993
(S) Toluene-d8 93.6 75.0-131 03/13/2019 20:26 WG1249284
(S) 4-Bromofluorobenzene 98.8 67.0-138 03/10/2019 22:36 WG1247993
(S) 4-Bromofluorobenzene 92.0 67.0-138 03/13/2019 20:26 WG1249284
(S) 1,2-Dichloroethane-d4 96.7 70.0-130 03/10/2019 22:36 WG1247993
(S) 1,2-Dichloroethane-d4 112 70.0-130 03/13/2019 20:26 WG1249284
Sample Narrative:
L1076982-01 WG1247993: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 145 2.67 8.01 1 03/15/2019 03:20 WG1248324
Unadjusted C19-C36 Aliphatics 6.66 J 2.67 8.01 1 03/15/2019 03:20 WG1248324
Unadjusted C11-C22 Aromatics 81.4 2.67 8.01 1 03/15/2019 10:11 WG1248324
Unadjusted Total Petroleum
Hydrocarbons 233 2.67 8.01 1 03/15/2019 10:11 WG1248324
(S) o-Terphenyl 70.9 40.0-140 03/15/2019 10:11 WG1248324
(S) 1-Chloro-octadecane 77.1 40.0-140 03/15/2019 03:20 WG1248324
(S) 2-Fluorobiphenyl 90.6 40.0-140 03/15/2019 10:11 WG1248324
(S) 2-Bromonaphthalene 85.0 40.0-140 03/15/2019 10:11 WG1248324
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0270 J 0.00791 0.0410 1 03/13/2019 05:51 WG1247945
Acenaphthylene U 0.00827 0.0410 1 03/13/2019 05:51 WG1247945
Benzidine U 0.0785 0.410 1 03/13/2019 05:51 WG1247945
Benzo(a)anthracene 0.00532 J 0.00528 0.0410 1 03/13/2019 05:51 WG1247945
Benzo(b)fluoranthene U 0.00857 0.0410 1 03/13/2019 05:51 WG1247945
Benzo(k)fluoranthene U 0.00717 0.0410 1 03/13/2019 05:51 WG1247945
Benzo(g,h,i)perylene U 0.00889 0.0410 1 03/13/2019 05:51 WG1247945
Benzo(a)pyrene U 0.00675 0.0410 1 03/13/2019 05:51 WG1247945
Bis(2-chlorethoxy)methane U 0.0949 4.10 10 03/14/2019 00:59 WG1247945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 7 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 7 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1076982
OE DISP#2 (BOTTOM) 6.5'
Collected date/time: 03/06/19 11:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroethyl)ether U 0.110 4.10 10 03/14/2019 00:59 WG1247945
Bis(2-chloroisopropyl)ether U 0.0937 4.10 10 03/14/2019 00:59 WG1247945
4-Bromophenyl-phenylether U 0.0141 0.410 1 03/13/2019 05:51 WG1247945
2-Chloronaphthalene U 0.00788 0.0410 1 03/13/2019 05:51 WG1247945
Chrysene U 0.00684 0.0410 1 03/13/2019 05:51 WG1247945
Dibenz(a,h)anthracene U 0.0101 0.0410 1 03/13/2019 05:51 WG1247945
3,3-Dichlorobenzidine U 0.0979 0.410 1 03/13/2019 05:51 WG1247945
2,4-Dinitrotoluene U 0.00748 0.410 1 03/13/2019 05:51 WG1247945
2,6-Dinitrotoluene U 0.00908 0.410 1 03/13/2019 05:51 WG1247945
Fluoranthene 0.00669 J 0.00611 0.0410 1 03/13/2019 05:51 WG1247945
Fluorene 0.0353 J 0.00841 0.0410 1 03/13/2019 05:51 WG1247945
Hexachlorobenzene U 0.0106 0.410 1 03/13/2019 05:51 WG1247945
Hexachloro-1,3-butadiene U 0.123 4.10 10 03/14/2019 00:59 WG1247945
Hexachlorocyclopentadiene U J0 0.0724 0.410 1 03/13/2019 05:51 WG1247945
Hexachloroethane U 0.165 4.10 10 03/14/2019 00:59 WG1247945
Indeno(1,2,3-cd)pyrene U 0.00952 0.0410 1 03/13/2019 05:51 WG1247945
Isophorone U 0.0643 4.10 10 03/14/2019 00:59 WG1247945
Naphthalene 3.54 0.110 0.410 10 03/14/2019 00:59 WG1247945
Nitrobenzene U 0.0857 4.10 10 03/14/2019 00:59 WG1247945
n-Nitrosodimethylamine U 0.798 4.10 10 03/14/2019 00:59 WG1247945
n-Nitrosodiphenylamine U 0.111 0.410 1 03/13/2019 05:51 WG1247945
n-Nitrosodi-n-propylamine U 0.112 4.10 10 03/14/2019 00:59 WG1247945
Phenanthrene 0.0481 0.00651 0.0410 1 03/13/2019 05:51 WG1247945
Benzylbutyl phthalate U 0.0127 0.410 1 03/13/2019 05:51 WG1247945
Bis(2-ethylhexyl)phthalate U 0.0148 0.410 1 03/13/2019 05:51 WG1247945
Di-n-butyl phthalate U 0.0134 0.410 1 03/13/2019 05:51 WG1247945
Diethyl phthalate U 0.00852 0.410 1 03/13/2019 05:51 WG1247945
Dimethyl phthalate U 0.00666 0.410 1 03/13/2019 05:51 WG1247945
Di-n-octyl phthalate U 0.0112 0.410 1 03/13/2019 05:51 WG1247945
Pyrene U 0.0152 0.0410 1 03/13/2019 05:51 WG1247945
1,2,4-Trichlorobenzene U 0.108 4.10 10 03/14/2019 00:59 WG1247945
4-Chloro-3-methylphenol U 0.0588 4.10 10 03/14/2019 00:59 WG1247945
2-Chlorophenol U 0.102 4.10 10 03/14/2019 00:59 WG1247945
2,4-Dichlorophenol U 0.0920 4.10 10 03/14/2019 00:59 WG1247945
2,4-Dimethylphenol U J0 0.581 4.10 10 03/14/2019 00:59 WG1247945
4,6-Dinitro-2-methylphenol U 0.153 0.410 1 03/13/2019 05:51 WG1247945
2-Nitrophenol U 0.160 4.10 10 03/14/2019 00:59 WG1247945
4-Nitrophenol U 0.0647 0.410 1 03/13/2019 05:51 WG1247945
Pentachlorophenol U 0.0592 0.410 1 03/13/2019 05:51 WG1247945
Phenol U 0.0857 4.10 10 03/14/2019 00:59 WG1247945
2,4,6-Trichlorophenol U 0.00960 0.410 1 03/13/2019 05:51 WG1247945
(S) 2-Fluorophenol 79.0 12.0-120 03/14/2019 00:59 WG1247945
(S) 2-Fluorophenol 88.9 12.0-120 03/13/2019 05:51 WG1247945
(S) Phenol-d5 77.3 10.0-120 03/13/2019 05:51 WG1247945
(S) Phenol-d5 78.7 10.0-120 03/14/2019 00:59 WG1247945
(S) Nitrobenzene-d5 106 10.0-122 03/14/2019 00:59 WG1247945
(S) Nitrobenzene-d5 110 10.0-122 03/13/2019 05:51 WG1247945
(S) 2-Fluorobiphenyl 64.3 15.0-120 03/13/2019 05:51 WG1247945
(S) 2-Fluorobiphenyl 69.8 15.0-120 03/14/2019 00:59 WG1247945
(S) 2,4,6-Tribromophenol 55.6 10.0-127 03/14/2019 00:59 WG1247945
(S) 2,4,6-Tribromophenol 91.9 10.0-127 03/13/2019 05:51 WG1247945
(S) p-Terphenyl-d14 78.4 10.0-120 03/14/2019 00:59 WG1247945
(S) p-Terphenyl-d14 80.8 10.0-120 03/13/2019 05:51 WG1247945
Sample Narrative:
L1076982-01 WG1247945: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 8 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 8 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1076982
OE DISP#2 (E) 6'
Collected date/time: 03/06/19 11:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.7 1 03/12/2019 13:16 WG1248621
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 337 79.6 239 2000 03/14/2019 19:12 WG1249073
Unadjusted C9-C12 Aliphatics 235 J 79.6 239 2000 03/14/2019 19:12 WG1249073
Unadjusted C9-C10 Aromatics 299 79.6 239 2000 03/14/2019 19:12 WG1249073
Total VPH 871 B 79.6 239 2000 03/14/2019 19:12 WG1249073
(S) 2,5-Dibromotoluene(FID)93.5 70.0-130 03/14/2019 19:12 WG1249073
(S) 2,5-Dibromotoluene(PID)93.1 70.0-130 03/14/2019 19:12 WG1249073
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.0478 0.239 80 03/10/2019 22:55 WG1247993
1,1,1-Trichloroethane U 0.0263 0.239 80 03/10/2019 22:55 WG1247993
1,1,2,2-Tetrachloroethane U 0.0373 0.239 80 03/10/2019 22:55 WG1247993
1,1,2-Trichloroethane U 0.0843 0.239 80 03/10/2019 22:55 WG1247993
1,1-Dichloroethane U 0.0549 0.239 80 03/10/2019 22:55 WG1247993
1,1-Dichloroethene U 0.0478 0.239 80 03/10/2019 22:55 WG1247993
1,1-Dichloropropene U 0.0669 0.239 80 03/10/2019 22:55 WG1247993
1,2,3-Trichlorobenzene U 0.0597 0.239 80 03/10/2019 22:55 WG1247993
1,2,3-Trichloropropane U 0.487 1.19 80 03/10/2019 22:55 WG1247993
1,2,4-Trichlorobenzene U 0.461 1.19 80 03/10/2019 22:55 WG1247993
1,2,4-Trimethylbenzene 28.7 0.111 0.478 80 03/10/2019 22:55 WG1247993
1,2-Dibromo-3-Chloropropane U 0.487 2.39 80 03/10/2019 22:55 WG1247993
1,2-Dibromoethane U 0.0502 0.239 80 03/10/2019 22:55 WG1247993
1,2-Dichlorobenzene U 0.139 0.478 80 03/10/2019 22:55 WG1247993
1,2-Dichloroethane U 0.0454 0.239 80 03/10/2019 22:55 WG1247993
1,2-Dichloropropane U 0.122 0.478 80 03/10/2019 22:55 WG1247993
1,3,5-Trimethylbenzene 14.0 0.103 0.478 80 03/10/2019 22:55 WG1247993
1,3-Dichlorobenzene U 0.162 0.478 80 03/10/2019 22:55 WG1247993
1,3-Dichloropropane U 0.167 0.478 80 03/10/2019 22:55 WG1247993
1,4-Dichlorobenzene U 0.189 0.478 80 03/10/2019 22:55 WG1247993
2,2-Dichloropropane U 0.0757 0.239 80 03/10/2019 22:55 WG1247993
2-Butanone (MEK)U 1.19 2.39 80 03/10/2019 22:55 WG1247993
2-Chlorotoluene U 0.0879 0.239 80 03/10/2019 22:55 WG1247993
4-Chlorotoluene U 0.108 0.478 80 03/10/2019 22:55 WG1247993
4-Methyl-2-pentanone (MIBK)U 0.956 2.39 80 03/10/2019 22:55 WG1247993
Acetone U 1.31 2.39 80 03/10/2019 22:55 WG1247993
Acrylonitrile U 0.182 1.19 80 03/10/2019 22:55 WG1247993
Benzene U 0.0382 0.0956 80 03/10/2019 22:55 WG1247993
Bromobenzene U J4 0.100 1.19 80 03/10/2019 22:55 WG1247993
Bromodichloromethane U 0.0753 0.239 80 03/10/2019 22:55 WG1247993
Bromoform U 0.571 2.39 80 03/10/2019 22:55 WG1247993
Bromomethane U 0.354 1.19 80 03/10/2019 22:55 WG1247993
Carbon tetrachloride U 0.103 0.478 80 03/10/2019 22:55 WG1247993
Chlorobenzene U 0.0547 0.239 80 03/10/2019 22:55 WG1247993
Chlorodibromomethane U 0.0430 0.239 80 03/10/2019 22:55 WG1247993
Chloroethane U 0.103 0.478 80 03/13/2019 20:45 WG1249284
Chloroform U 0.0397 0.239 80 03/10/2019 22:55 WG1247993
Chloromethane U 0.133 1.19 80 03/10/2019 22:55 WG1247993
Dichlorodifluoromethane U 0.0781 0.239 80 03/10/2019 22:55 WG1247993
Di-isopropyl ether U 0.0334 0.0956 80 03/10/2019 22:55 WG1247993
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 9 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 9 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1076982
OE DISP#2 (E) 6'
Collected date/time: 03/06/19 11:55
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 1.37 0.0506 0.239 80 03/10/2019 22:55 WG1247993
Isopropylbenzene 1.17 0.0824 0.239 80 03/10/2019 22:55 WG1247993
Methyl tert-butyl ether U 0.0282 0.0956 80 03/10/2019 22:55 WG1247993
Methylene Chloride U 0.634 2.39 80 03/10/2019 22:55 WG1247993
Naphthalene 0.948 J 0.299 1.19 80 03/10/2019 22:55 WG1247993
Styrene U 0.260 1.19 80 03/10/2019 22:55 WG1247993
Tetrachloroethene U 0.0669 0.239 80 03/10/2019 22:55 WG1247993
Toluene 0.272 J 0.119 0.478 80 03/10/2019 22:55 WG1247993
Trichloroethene U 0.0382 0.0956 80 03/13/2019 20:45 WG1249284
Trichlorofluoromethane U 0.0478 0.239 80 03/10/2019 22:55 WG1247993
Vinyl chloride U 0.0652 0.239 80 03/10/2019 22:55 WG1247993
Xylenes, Total 7.20 0.456 0.621 80 03/10/2019 22:55 WG1247993
cis-1,2-Dichloroethene U 0.0659 0.239 80 03/10/2019 22:55 WG1247993
cis-1,3-Dichloropropene U 0.0647 0.239 80 03/10/2019 22:55 WG1247993
n-Butylbenzene 3.22 0.367 1.19 80 03/10/2019 22:55 WG1247993
n-Propylbenzene 6.35 0.113 0.478 80 03/10/2019 22:55 WG1247993
p-Isopropyltoluene 0.639 0.222 0.478 80 03/10/2019 22:55 WG1247993
sec-Butylbenzene 1.30 0.241 1.19 80 03/10/2019 22:55 WG1247993
tert-Butylbenzene U 0.148 0.478 80 03/10/2019 22:55 WG1247993
trans-1,2-Dichloroethene U 0.136 0.478 80 03/10/2019 22:55 WG1247993
trans-1,3-Dichloropropene U 0.146 0.478 80 03/10/2019 22:55 WG1247993
(S) Toluene-d8 104 75.0-131 03/10/2019 22:55 WG1247993
(S) Toluene-d8 94.0 75.0-131 03/13/2019 20:45 WG1249284
(S) 4-Bromofluorobenzene 95.8 67.0-138 03/10/2019 22:55 WG1247993
(S) 4-Bromofluorobenzene 86.1 67.0-138 03/13/2019 20:45 WG1249284
(S) 1,2-Dichloroethane-d4 96.4 70.0-130 03/10/2019 22:55 WG1247993
(S) 1,2-Dichloroethane-d4 113 70.0-130 03/13/2019 20:45 WG1249284
Sample Narrative:
L1076982-02 WG1247993: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 128 2.59 7.76 1 03/15/2019 03:44 WG1248324
Unadjusted C19-C36 Aliphatics 22.1 2.59 7.76 1 03/15/2019 03:44 WG1248324
Unadjusted C11-C22 Aromatics 67.0 2.59 7.76 1 03/15/2019 09:47 WG1248324
Unadjusted Total Petroleum
Hydrocarbons 217 2.59 7.76 1 03/15/2019 09:47 WG1248324
(S) o-Terphenyl 71.1 40.0-140 03/15/2019 09:47 WG1248324
(S) 1-Chloro-octadecane 78.9 40.0-140 03/15/2019 03:44 WG1248324
(S) 2-Fluorobiphenyl 89.5 40.0-140 03/15/2019 09:47 WG1248324
(S) 2-Bromonaphthalene 83.8 40.0-140 03/15/2019 09:47 WG1248324
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0317 J 0.00767 0.0398 1 03/13/2019 04:42 WG1247945
Acenaphthylene U 0.00801 0.0398 1 03/13/2019 04:42 WG1247945
Benzidine U 0.0761 0.398 1 03/13/2019 04:42 WG1247945
Benzo(a)anthracene U 0.00511 0.0398 1 03/13/2019 04:42 WG1247945
Benzo(b)fluoranthene U 0.00830 0.0398 1 03/13/2019 04:42 WG1247945
Benzo(k)fluoranthene U 0.00695 0.0398 1 03/13/2019 04:42 WG1247945
Benzo(g,h,i)perylene U 0.00861 0.0398 1 03/13/2019 04:42 WG1247945
Benzo(a)pyrene U 0.00655 0.0398 1 03/13/2019 04:42 WG1247945
Bis(2-chlorethoxy)methane U 0.0920 3.98 10 03/14/2019 00:39 WG1247945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 10 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 10 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1076982
OE DISP#2 (E) 6'
Collected date/time: 03/06/19 11:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroethyl)ether U 0.107 3.98 10 03/14/2019 00:39 WG1247945
Bis(2-chloroisopropyl)ether U 0.0908 3.98 10 03/14/2019 00:39 WG1247945
4-Bromophenyl-phenylether U 0.0136 0.398 1 03/13/2019 04:42 WG1247945
2-Chloronaphthalene U 0.00763 0.0398 1 03/13/2019 04:42 WG1247945
Chrysene U 0.00663 0.0398 1 03/13/2019 04:42 WG1247945
Dibenz(a,h)anthracene U 0.00981 0.0398 1 03/13/2019 04:42 WG1247945
3,3-Dichlorobenzidine U 0.0948 0.398 1 03/13/2019 04:42 WG1247945
2,4-Dinitrotoluene U 0.00725 0.398 1 03/13/2019 04:42 WG1247945
2,6-Dinitrotoluene U 0.00880 0.398 1 03/13/2019 04:42 WG1247945
Fluoranthene 0.00818 J 0.00592 0.0398 1 03/13/2019 04:42 WG1247945
Fluorene 0.0407 0.00815 0.0398 1 03/13/2019 04:42 WG1247945
Hexachlorobenzene U 0.0102 0.398 1 03/13/2019 04:42 WG1247945
Hexachloro-1,3-butadiene U 0.119 3.98 10 03/14/2019 00:39 WG1247945
Hexachlorocyclopentadiene U J0 0.0701 0.398 1 03/13/2019 04:42 WG1247945
Hexachloroethane U 0.160 3.98 10 03/14/2019 00:39 WG1247945
Indeno(1,2,3-cd)pyrene U 0.00922 0.0398 1 03/13/2019 04:42 WG1247945
Isophorone U 0.0624 3.98 10 03/14/2019 00:39 WG1247945
Naphthalene U 0.106 0.398 10 03/14/2019 00:39 WG1247945
Nitrobenzene U 0.0830 3.98 10 03/14/2019 00:39 WG1247945
n-Nitrosodimethylamine U 0.773 3.98 10 03/14/2019 00:39 WG1247945
n-Nitrosodiphenylamine U 0.108 0.398 1 03/13/2019 04:42 WG1247945
n-Nitrosodi-n-propylamine U 0.108 3.98 10 03/14/2019 00:39 WG1247945
Phenanthrene 0.0511 0.00631 0.0398 1 03/13/2019 04:42 WG1247945
Benzylbutyl phthalate U 0.0123 0.398 1 03/13/2019 04:42 WG1247945
Bis(2-ethylhexyl)phthalate U 0.0143 0.398 1 03/13/2019 04:42 WG1247945
Di-n-butyl phthalate U 0.0130 0.398 1 03/13/2019 04:42 WG1247945
Diethyl phthalate U 0.00825 0.398 1 03/13/2019 04:42 WG1247945
Dimethyl phthalate U 0.00645 0.398 1 03/13/2019 04:42 WG1247945
Di-n-octyl phthalate U 0.0108 0.398 1 03/13/2019 04:42 WG1247945
Pyrene 0.0205 J 0.0147 0.0398 1 03/13/2019 04:42 WG1247945
1,2,4-Trichlorobenzene U 0.105 3.98 10 03/14/2019 00:39 WG1247945
4-Chloro-3-methylphenol U 0.0570 3.98 10 03/14/2019 00:39 WG1247945
2-Chlorophenol U 0.0993 3.98 10 03/14/2019 00:39 WG1247945
2,4-Dichlorophenol U 0.0891 3.98 10 03/14/2019 00:39 WG1247945
2,4-Dimethylphenol U J0 0.563 3.98 10 03/14/2019 00:39 WG1247945
4,6-Dinitro-2-methylphenol U 0.148 0.398 1 03/13/2019 04:42 WG1247945
2-Nitrophenol U 0.155 3.98 10 03/14/2019 00:39 WG1247945
4-Nitrophenol U 0.0627 0.398 1 03/13/2019 04:42 WG1247945
Pentachlorophenol U 0.0573 0.398 1 03/13/2019 04:42 WG1247945
Phenol U 0.0830 3.98 10 03/14/2019 00:39 WG1247945
2,4,6-Trichlorophenol U 0.00931 0.398 1 03/13/2019 04:42 WG1247945
(S) 2-Fluorophenol 71.5 12.0-120 03/14/2019 00:39 WG1247945
(S) 2-Fluorophenol 84.7 12.0-120 03/13/2019 04:42 WG1247945
(S) Phenol-d5 75.2 10.0-120 03/13/2019 04:42 WG1247945
(S) Phenol-d5 70.8 10.0-120 03/14/2019 00:39 WG1247945
(S) Nitrobenzene-d5 89.4 10.0-122 03/14/2019 00:39 WG1247945
(S) Nitrobenzene-d5 95.5 10.0-122 03/13/2019 04:42 WG1247945
(S) 2-Fluorobiphenyl 65.0 15.0-120 03/14/2019 00:39 WG1247945
(S) 2-Fluorobiphenyl 71.6 15.0-120 03/13/2019 04:42 WG1247945
(S) 2,4,6-Tribromophenol 93.1 10.0-127 03/13/2019 04:42 WG1247945
(S) 2,4,6-Tribromophenol 59.4 10.0-127 03/14/2019 00:39 WG1247945
(S) p-Terphenyl-d14 90.3 10.0-120 03/13/2019 04:42 WG1247945
(S) p-Terphenyl-d14 78.2 10.0-120 03/14/2019 00:39 WG1247945
Sample Narrative:
L1076982-02 WG1247945: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 11 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 11 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1076982
OE DISP#2 (N) 6'
Collected date/time: 03/06/19 12:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.4 1 03/12/2019 13:16 WG1248621
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 598 76.2 229 2000 03/14/2019 19:46 WG1249073
Unadjusted C9-C12 Aliphatics 557 76.2 229 2000 03/14/2019 19:46 WG1249073
Unadjusted C9-C10 Aromatics 515 76.2 229 2000 03/14/2019 19:46 WG1249073
Total VPH 1670 76.2 229 2000 03/14/2019 19:46 WG1249073
(S) 2,5-Dibromotoluene(FID)96.0 70.0-130 03/14/2019 19:46 WG1249073
(S) 2,5-Dibromotoluene(PID)95.7 70.0-130 03/14/2019 19:46 WG1249073
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.0458 0.229 80 03/10/2019 23:13 WG1247993
1,1,1-Trichloroethane U 0.0252 0.229 80 03/10/2019 23:13 WG1247993
1,1,2,2-Tetrachloroethane U 0.0357 0.229 80 03/10/2019 23:13 WG1247993
1,1,2-Trichloroethane U 0.0808 0.229 80 03/10/2019 23:13 WG1247993
1,1-Dichloroethane U 0.0526 0.229 80 03/10/2019 23:13 WG1247993
1,1-Dichloroethene U 0.0458 0.229 80 03/10/2019 23:13 WG1247993
1,1-Dichloropropene U 0.0641 0.229 80 03/10/2019 23:13 WG1247993
1,2,3-Trichlorobenzene U 0.0572 0.229 80 03/10/2019 23:13 WG1247993
1,2,3-Trichloropropane U 0.467 1.14 80 03/10/2019 23:13 WG1247993
1,2,4-Trichlorobenzene U 0.442 1.14 80 03/10/2019 23:13 WG1247993
1,2,4-Trimethylbenzene 82.1 0.106 0.458 80 03/10/2019 23:13 WG1247993
1,2-Dibromo-3-Chloropropane U 0.467 2.29 80 03/10/2019 23:13 WG1247993
1,2-Dibromoethane U 0.0480 0.229 80 03/10/2019 23:13 WG1247993
1,2-Dichlorobenzene U 0.133 0.458 80 03/10/2019 23:13 WG1247993
1,2-Dichloroethane U 0.0435 0.229 80 03/10/2019 23:13 WG1247993
1,2-Dichloropropane U 0.117 0.458 80 03/10/2019 23:13 WG1247993
1,3,5-Trimethylbenzene 28.3 0.0988 0.458 80 03/10/2019 23:13 WG1247993
1,3-Dichlorobenzene U 0.156 0.458 80 03/10/2019 23:13 WG1247993
1,3-Dichloropropane U 0.160 0.458 80 03/10/2019 23:13 WG1247993
1,4-Dichlorobenzene U 0.181 0.458 80 03/10/2019 23:13 WG1247993
2,2-Dichloropropane U 0.0725 0.229 80 03/10/2019 23:13 WG1247993
2-Butanone (MEK)U 1.14 2.29 80 03/10/2019 23:13 WG1247993
2-Chlorotoluene U 0.0842 0.229 80 03/10/2019 23:13 WG1247993
4-Chlorotoluene U 0.103 0.458 80 03/10/2019 23:13 WG1247993
4-Methyl-2-pentanone (MIBK)U 0.915 2.29 80 03/10/2019 23:13 WG1247993
Acetone U 1.26 2.29 80 03/10/2019 23:13 WG1247993
Acrylonitrile U 0.174 1.14 80 03/10/2019 23:13 WG1247993
Benzene 0.176 0.0366 0.0915 80 03/10/2019 23:13 WG1247993
Bromobenzene U J4 0.0961 1.14 80 03/10/2019 23:13 WG1247993
Bromodichloromethane U 0.0721 0.229 80 03/10/2019 23:13 WG1247993
Bromoform U 0.547 2.29 80 03/10/2019 23:13 WG1247993
Bromomethane U 0.339 1.14 80 03/10/2019 23:13 WG1247993
Carbon tetrachloride U 0.0988 0.458 80 03/10/2019 23:13 WG1247993
Chlorobenzene U 0.0524 0.229 80 03/10/2019 23:13 WG1247993
Chlorodibromomethane U 0.0412 0.229 80 03/10/2019 23:13 WG1247993
Chloroethane U 0.0988 0.458 80 03/13/2019 21:05 WG1249284
Chloroform U 0.0380 0.229 80 03/10/2019 23:13 WG1247993
Chloromethane U 0.127 1.14 80 03/10/2019 23:13 WG1247993
Dichlorodifluoromethane U 0.0748 0.229 80 03/10/2019 23:13 WG1247993
Di-isopropyl ether U 0.0320 0.0915 80 03/10/2019 23:13 WG1247993
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 12 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 12 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1076982
OE DISP#2 (N) 6'
Collected date/time: 03/06/19 12:10
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 23.7 0.0485 0.229 80 03/10/2019 23:13 WG1247993
Isopropylbenzene 3.34 0.0789 0.229 80 03/10/2019 23:13 WG1247993
Methyl tert-butyl ether U 0.0270 0.0915 80 03/10/2019 23:13 WG1247993
Methylene Chloride U 0.607 2.29 80 03/10/2019 23:13 WG1247993
Naphthalene 18.0 0.286 1.14 80 03/10/2019 23:13 WG1247993
Styrene U 0.249 1.14 80 03/10/2019 23:13 WG1247993
Tetrachloroethene U 0.0641 0.229 80 03/10/2019 23:13 WG1247993
Toluene 11.9 0.114 0.458 80 03/10/2019 23:13 WG1247993
Trichloroethene U 0.0366 0.0915 80 03/13/2019 21:05 WG1249284
Trichlorofluoromethane U 0.0458 0.229 80 03/10/2019 23:13 WG1247993
Vinyl chloride U 0.0625 0.229 80 03/10/2019 23:13 WG1247993
Xylenes, Total 126 0.437 0.595 80 03/10/2019 23:13 WG1247993
cis-1,2-Dichloroethene U 0.0631 0.229 80 03/10/2019 23:13 WG1247993
cis-1,3-Dichloropropene U 0.0620 0.229 80 03/10/2019 23:13 WG1247993
n-Butylbenzene 3.73 0.351 1.14 80 03/10/2019 23:13 WG1247993
n-Propylbenzene 13.5 0.108 0.458 80 03/10/2019 23:13 WG1247993
p-Isopropyltoluene 0.794 0.213 0.458 80 03/10/2019 23:13 WG1247993
sec-Butylbenzene U 0.231 1.14 80 03/10/2019 23:13 WG1247993
tert-Butylbenzene U 0.142 0.458 80 03/10/2019 23:13 WG1247993
trans-1,2-Dichloroethene U 0.130 0.458 80 03/10/2019 23:13 WG1247993
trans-1,3-Dichloropropene U 0.140 0.458 80 03/10/2019 23:13 WG1247993
(S) Toluene-d8 108 75.0-131 03/10/2019 23:13 WG1247993
(S) Toluene-d8 91.8 75.0-131 03/13/2019 21:05 WG1249284
(S) 4-Bromofluorobenzene 97.5 67.0-138 03/10/2019 23:13 WG1247993
(S) 4-Bromofluorobenzene 92.6 67.0-138 03/13/2019 21:05 WG1249284
(S) 1,2-Dichloroethane-d4 95.5 70.0-130 03/10/2019 23:13 WG1247993
(S) 1,2-Dichloroethane-d4 115 70.0-130 03/13/2019 21:05 WG1249284
Sample Narrative:
L1076982-03 WG1247993: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 71.7 2.48 7.44 1 03/15/2019 04:08 WG1248324
Unadjusted C19-C36 Aliphatics 2.55 J 2.48 7.44 1 03/15/2019 04:08 WG1248324
Unadjusted C11-C22 Aromatics 44.0 2.48 7.44 1 03/15/2019 09:22 WG1248324
Unadjusted Total Petroleum
Hydrocarbons 118 2.48 7.44 1 03/15/2019 09:22 WG1248324
(S) o-Terphenyl 58.8 40.0-140 03/15/2019 09:22 WG1248324
(S) 1-Chloro-octadecane 65.8 40.0-140 03/15/2019 04:08 WG1248324
(S) 2-Fluorobiphenyl 88.7 40.0-140 03/15/2019 09:22 WG1248324
(S) 2-Bromonaphthalene 83.1 40.0-140 03/15/2019 09:22 WG1248324
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0459 0.00734 0.0381 1 03/13/2019 03:56 WG1247945
Acenaphthylene U 0.00768 0.0381 1 03/13/2019 03:56 WG1247945
Benzidine U 0.0729 0.381 1 03/13/2019 03:56 WG1247945
Benzo(a)anthracene 0.00702 J 0.00490 0.0381 1 03/13/2019 03:56 WG1247945
Benzo(b)fluoranthene U 0.00795 0.0381 1 03/13/2019 03:56 WG1247945
Benzo(k)fluoranthene U 0.00666 0.0381 1 03/13/2019 03:56 WG1247945
Benzo(g,h,i)perylene U 0.00825 0.0381 1 03/13/2019 03:56 WG1247945
Benzo(a)pyrene U 0.00627 0.0381 1 03/13/2019 03:56 WG1247945
Bis(2-chlorethoxy)methane U 0.0881 3.81 10 03/13/2019 23:59 WG1247945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 13 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 13 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1076982
OE DISP#2 (N) 6'
Collected date/time: 03/06/19 12:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroethyl)ether U 0.102 3.81 10 03/13/2019 23:59 WG1247945
Bis(2-chloroisopropyl)ether U 0.0869 3.81 10 03/13/2019 23:59 WG1247945
4-Bromophenyl-phenylether U 0.0130 0.381 1 03/13/2019 03:56 WG1247945
2-Chloronaphthalene U 0.00731 0.0381 1 03/13/2019 03:56 WG1247945
Chrysene U 0.00635 0.0381 1 03/13/2019 03:56 WG1247945
Dibenz(a,h)anthracene U 0.00939 0.0381 1 03/13/2019 03:56 WG1247945
3,3-Dichlorobenzidine U 0.0908 0.381 1 03/13/2019 03:56 WG1247945
2,4-Dinitrotoluene U 0.00694 0.381 1 03/13/2019 03:56 WG1247945
2,6-Dinitrotoluene U 0.00843 0.381 1 03/13/2019 03:56 WG1247945
Fluoranthene 0.0102 J 0.00567 0.0381 1 03/13/2019 03:56 WG1247945
Fluorene 0.0604 0.00780 0.0381 1 03/13/2019 03:56 WG1247945
Hexachlorobenzene U 0.00979 0.381 1 03/13/2019 03:56 WG1247945
Hexachloro-1,3-butadiene U 0.114 3.81 10 03/13/2019 23:59 WG1247945
Hexachlorocyclopentadiene U J0 0.0672 0.381 1 03/13/2019 03:56 WG1247945
Hexachloroethane U 0.153 3.81 10 03/13/2019 23:59 WG1247945
Indeno(1,2,3-cd)pyrene U 0.00883 0.0381 1 03/13/2019 03:56 WG1247945
Isophorone U 0.0597 3.81 10 03/13/2019 23:59 WG1247945
Naphthalene 10.6 0.102 0.381 10 03/13/2019 23:59 WG1247945
Nitrobenzene U 0.0795 3.81 10 03/13/2019 23:59 WG1247945
n-Nitrosodimethylamine U 0.740 3.81 10 03/13/2019 23:59 WG1247945
n-Nitrosodiphenylamine U 0.103 0.381 1 03/13/2019 03:56 WG1247945
n-Nitrosodi-n-propylamine U 0.104 3.81 10 03/13/2019 23:59 WG1247945
Phenanthrene 0.0747 0.00604 0.0381 1 03/13/2019 03:56 WG1247945
Benzylbutyl phthalate U 0.0118 0.381 1 03/13/2019 03:56 WG1247945
Bis(2-ethylhexyl)phthalate 0.0227 J 0.0137 0.381 1 03/13/2019 03:56 WG1247945
Di-n-butyl phthalate U 0.0125 0.381 1 03/13/2019 03:56 WG1247945
Diethyl phthalate U 0.00790 0.381 1 03/13/2019 03:56 WG1247945
Dimethyl phthalate U 0.00618 0.381 1 03/13/2019 03:56 WG1247945
Di-n-octyl phthalate U 0.0104 0.381 1 03/13/2019 03:56 WG1247945
Pyrene 0.0197 J 0.0141 0.0381 1 03/13/2019 03:56 WG1247945
1,2,4-Trichlorobenzene U 0.100 3.81 10 03/13/2019 23:59 WG1247945
4-Chloro-3-methylphenol U 0.0546 3.81 10 03/13/2019 23:59 WG1247945
2-Chlorophenol U 0.0951 3.81 10 03/13/2019 23:59 WG1247945
2,4-Dichlorophenol U 0.0853 3.81 10 03/13/2019 23:59 WG1247945
2,4-Dimethylphenol U J0 0.539 3.81 10 03/13/2019 23:59 WG1247945
4,6-Dinitro-2-methylphenol U 0.142 0.381 1 03/13/2019 03:56 WG1247945
2-Nitrophenol U 0.149 3.81 10 03/13/2019 23:59 WG1247945
4-Nitrophenol U 0.0601 0.381 1 03/13/2019 03:56 WG1247945
Pentachlorophenol U 0.0549 0.381 1 03/13/2019 03:56 WG1247945
Phenol U 0.0795 3.81 10 03/13/2019 23:59 WG1247945
2,4,6-Trichlorophenol U 0.00891 0.381 1 03/13/2019 03:56 WG1247945
(S) 2-Fluorophenol 78.9 12.0-120 03/13/2019 23:59 WG1247945
(S) 2-Fluorophenol 88.1 12.0-120 03/13/2019 03:56 WG1247945
(S) Phenol-d5 89.5 10.0-120 03/13/2019 23:59 WG1247945
(S) Phenol-d5 78.0 10.0-120 03/13/2019 03:56 WG1247945
(S) Nitrobenzene-d5 110 10.0-122 03/13/2019 23:59 WG1247945
(S) Nitrobenzene-d5 106 10.0-122 03/13/2019 03:56 WG1247945
(S) 2-Fluorobiphenyl 68.4 15.0-120 03/13/2019 23:59 WG1247945
(S) 2-Fluorobiphenyl 60.9 15.0-120 03/13/2019 03:56 WG1247945
(S) 2,4,6-Tribromophenol 93.1 10.0-127 03/13/2019 03:56 WG1247945
(S) 2,4,6-Tribromophenol 59.2 10.0-127 03/13/2019 23:59 WG1247945
(S) p-Terphenyl-d14 80.6 10.0-120 03/13/2019 23:59 WG1247945
(S) p-Terphenyl-d14 81.9 10.0-120 03/13/2019 03:56 WG1247945
Sample Narrative:
L1076982-03 WG1247945: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 14 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 14 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1076982
OE DISP#2 (S) 6'
Collected date/time: 03/06/19 12:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.8 1 03/12/2019 13:16 WG1248621
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 87.8 J 39.3 118 1000 03/14/2019 20:19 WG1249073
Unadjusted C9-C12 Aliphatics 96.7 J 39.3 118 1000 03/14/2019 20:19 WG1249073
Unadjusted C9-C10 Aromatics 123 39.3 118 1000 03/14/2019 20:19 WG1249073
Total VPH 307 B 39.3 118 1000 03/14/2019 20:19 WG1249073
(S) 2,5-Dibromotoluene(FID)93.7 70.0-130 03/14/2019 20:19 WG1249073
(S) 2,5-Dibromotoluene(PID)93.2 70.0-130 03/14/2019 20:19 WG1249073
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.0236 0.118 40 03/10/2019 23:32 WG1247993
1,1,1-Trichloroethane U J3 0.0130 0.118 40 03/10/2019 23:32 WG1247993
1,1,2,2-Tetrachloroethane U 0.0184 0.118 40 03/10/2019 23:32 WG1247993
1,1,2-Trichloroethane U 0.0416 0.118 40 03/10/2019 23:32 WG1247993
1,1-Dichloroethane U J3 0.0271 0.118 40 03/10/2019 23:32 WG1247993
1,1-Dichloroethene U J3 0.0236 0.118 40 03/10/2019 23:32 WG1247993
1,1-Dichloropropene U J3 0.0330 0.118 40 03/10/2019 23:32 WG1247993
1,2,3-Trichlorobenzene U 0.0295 0.118 40 03/10/2019 23:32 WG1247993
1,2,3-Trichloropropane U 0.241 0.590 40 03/10/2019 23:32 WG1247993
1,2,4-Trichlorobenzene U 0.228 0.590 40 03/10/2019 23:32 WG1247993
1,2,4-Trimethylbenzene 21.5 0.0547 0.236 40 03/10/2019 23:32 WG1247993
1,2-Dibromo-3-Chloropropane U 0.241 1.18 40 03/10/2019 23:32 WG1247993
1,2-Dibromoethane U 0.0248 0.118 40 03/10/2019 23:32 WG1247993
1,2-Dichlorobenzene U 0.0684 0.236 40 03/10/2019 23:32 WG1247993
1,2-Dichloroethane U 0.0224 0.118 40 03/10/2019 23:32 WG1247993
1,2-Dichloropropane U 0.0599 0.236 40 03/10/2019 23:32 WG1247993
1,3,5-Trimethylbenzene 8.01 0.0510 0.236 40 03/10/2019 23:32 WG1247993
1,3-Dichlorobenzene U J3 0.0802 0.236 40 03/10/2019 23:32 WG1247993
1,3-Dichloropropane U 0.0826 0.236 40 03/10/2019 23:32 WG1247993
1,4-Dichlorobenzene U 0.0929 0.236 40 03/10/2019 23:32 WG1247993
2,2-Dichloropropane U J3 0.0374 0.118 40 03/10/2019 23:32 WG1247993
2-Butanone (MEK)U 0.590 1.18 40 03/10/2019 23:32 WG1247993
2-Chlorotoluene U J3 0.0434 0.118 40 03/10/2019 23:32 WG1247993
4-Chlorotoluene U 0.0533 0.236 40 03/10/2019 23:32 WG1247993
4-Methyl-2-pentanone (MIBK)U 0.472 1.18 40 03/10/2019 23:32 WG1247993
Acetone U 0.646 1.18 40 03/10/2019 23:32 WG1247993
Acrylonitrile U 0.0896 0.590 40 03/10/2019 23:32 WG1247993
Benzene U J3 0.0189 0.0472 40 03/10/2019 23:32 WG1247993
Bromobenzene U J4 0.0495 0.590 40 03/10/2019 23:32 WG1247993
Bromodichloromethane U 0.0372 0.118 40 03/10/2019 23:32 WG1247993
Bromoform U 0.282 1.18 40 03/10/2019 23:32 WG1247993
Bromomethane U J3 0.175 0.590 40 03/10/2019 23:32 WG1247993
Carbon tetrachloride U J3 0.0510 0.236 40 03/10/2019 23:32 WG1247993
Chlorobenzene U 0.0270 0.118 40 03/10/2019 23:32 WG1247993
Chlorodibromomethane U 0.0212 0.118 40 03/10/2019 23:32 WG1247993
Chloroethane U 0.0510 0.236 40 03/13/2019 21:25 WG1249284
Chloroform U 0.0196 0.118 40 03/10/2019 23:32 WG1247993
Chloromethane U J3 0.0656 0.590 40 03/10/2019 23:32 WG1247993
Dichlorodifluoromethane U J3 0.0386 0.118 40 03/10/2019 23:32 WG1247993
Di-isopropyl ether U 0.0165 0.0472 40 03/10/2019 23:32 WG1247993
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 15 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 15 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1076982
OE DISP#2 (S) 6'
Collected date/time: 03/06/19 12:25
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 1.14 0.0250 0.118 40 03/10/2019 23:32 WG1247993
Isopropylbenzene 0.647 J3 0.0407 0.118 40 03/10/2019 23:32 WG1247993
Methyl tert-butyl ether U 0.0139 0.0472 40 03/10/2019 23:32 WG1247993
Methylene Chloride U 0.314 1.18 40 03/10/2019 23:32 WG1247993
Naphthalene 1.92 0.147 0.590 40 03/10/2019 23:32 WG1247993
Styrene U 0.129 0.590 40 03/10/2019 23:32 WG1247993
Tetrachloroethene U J3 0.0330 0.118 40 03/10/2019 23:32 WG1247993
Toluene 0.164 J J3 0.0590 0.236 40 03/10/2019 23:32 WG1247993
Trichloroethene U 0.0189 0.0472 40 03/13/2019 21:25 WG1249284
Trichlorofluoromethane U J3 0.0236 0.118 40 03/10/2019 23:32 WG1247993
Vinyl chloride U J3 0.0322 0.118 40 03/10/2019 23:32 WG1247993
Xylenes, Total 6.75 0.225 0.307 40 03/10/2019 23:32 WG1247993
cis-1,2-Dichloroethene U J3 0.0326 0.118 40 03/10/2019 23:32 WG1247993
cis-1,3-Dichloropropene U 0.0320 0.118 40 03/10/2019 23:32 WG1247993
n-Butylbenzene 1.23 0.182 0.590 40 03/10/2019 23:32 WG1247993
n-Propylbenzene 3.11 0.0557 0.236 40 03/10/2019 23:32 WG1247993
p-Isopropyltoluene U 0.110 0.236 40 03/10/2019 23:32 WG1247993
sec-Butylbenzene 0.465 J J3 0.119 0.590 40 03/10/2019 23:32 WG1247993
tert-Butylbenzene U J3 0.0731 0.236 40 03/10/2019 23:32 WG1247993
trans-1,2-Dichloroethene U J3 0.0675 0.236 40 03/10/2019 23:32 WG1247993
trans-1,3-Dichloropropene U 0.0722 0.236 40 03/10/2019 23:32 WG1247993
(S) Toluene-d8 105 75.0-131 03/10/2019 23:32 WG1247993
(S) Toluene-d8 92.4 75.0-131 03/13/2019 21:25 WG1249284
(S) 4-Bromofluorobenzene 96.2 67.0-138 03/10/2019 23:32 WG1247993
(S) 4-Bromofluorobenzene 87.1 67.0-138 03/13/2019 21:25 WG1249284
(S) 1,2-Dichloroethane-d4 96.9 70.0-130 03/10/2019 23:32 WG1247993
(S) 1,2-Dichloroethane-d4 114 70.0-130 03/13/2019 21:25 WG1249284
Sample Narrative:
L1076982-04 WG1247993: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 54.4 2.56 7.67 1 03/15/2019 04:32 WG1248324
Unadjusted C19-C36 Aliphatics 4.84 J 2.56 7.67 1 03/15/2019 04:32 WG1248324
Unadjusted C11-C22 Aromatics 34.6 2.56 7.67 1 03/15/2019 08:58 WG1248324
Unadjusted Total Petroleum
Hydrocarbons 93.8 2.56 7.67 1 03/15/2019 08:58 WG1248324
(S) o-Terphenyl 78.0 40.0-140 03/15/2019 08:58 WG1248324
(S) 1-Chloro-octadecane 88.9 40.0-140 03/15/2019 04:32 WG1248324
(S) 2-Fluorobiphenyl 88.9 40.0-140 03/15/2019 08:58 WG1248324
(S) 2-Bromonaphthalene 83.5 40.0-140 03/15/2019 08:58 WG1248324
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0156 J 0.00757 0.0393 1 03/13/2019 04:19 WG1247945
Acenaphthylene U 0.00791 0.0393 1 03/13/2019 04:19 WG1247945
Benzidine U 0.0751 0.393 1 03/13/2019 04:19 WG1247945
Benzo(a)anthracene U 0.00505 0.0393 1 03/13/2019 04:19 WG1247945
Benzo(b)fluoranthene U 0.00820 0.0393 1 03/13/2019 04:19 WG1247945
Benzo(k)fluoranthene U 0.00686 0.0393 1 03/13/2019 04:19 WG1247945
Benzo(g,h,i)perylene U 0.00850 0.0393 1 03/13/2019 04:19 WG1247945
Benzo(a)pyrene U 0.00646 0.0393 1 03/13/2019 04:19 WG1247945
Bis(2-chlorethoxy)methane U 0.0908 3.93 10 03/14/2019 00:19 WG1247945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 16 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 16 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1076982
OE DISP#2 (S) 6'
Collected date/time: 03/06/19 12:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Bis(2-chloroethyl)ether U 0.106 3.93 10 03/14/2019 00:19 WG1247945
Bis(2-chloroisopropyl)ether U 0.0896 3.93 10 03/14/2019 00:19 WG1247945
4-Bromophenyl-phenylether U 0.0134 0.393 1 03/13/2019 04:19 WG1247945
2-Chloronaphthalene U 0.00754 0.0393 1 03/13/2019 04:19 WG1247945
Chrysene U 0.00655 0.0393 1 03/13/2019 04:19 WG1247945
Dibenz(a,h)anthracene U 0.00968 0.0393 1 03/13/2019 04:19 WG1247945
3,3-Dichlorobenzidine U 0.0937 0.393 1 03/13/2019 04:19 WG1247945
2,4-Dinitrotoluene U 0.00716 0.393 1 03/13/2019 04:19 WG1247945
2,6-Dinitrotoluene U 0.00869 0.393 1 03/13/2019 04:19 WG1247945
Fluoranthene U 0.00585 0.0393 1 03/13/2019 04:19 WG1247945
Fluorene 0.0179 J 0.00804 0.0393 1 03/13/2019 04:19 WG1247945
Hexachlorobenzene U 0.0101 0.393 1 03/13/2019 04:19 WG1247945
Hexachloro-1,3-butadiene U 0.118 3.93 10 03/14/2019 00:19 WG1247945
Hexachlorocyclopentadiene U J0 0.0692 0.393 1 03/13/2019 04:19 WG1247945
Hexachloroethane U 0.158 3.93 10 03/14/2019 00:19 WG1247945
Indeno(1,2,3-cd)pyrene U 0.00911 0.0393 1 03/13/2019 04:19 WG1247945
Isophorone U 0.0616 3.93 10 03/14/2019 00:19 WG1247945
Naphthalene 0.753 0.105 0.393 10 03/14/2019 00:19 WG1247945
Nitrobenzene U 0.0820 3.93 10 03/14/2019 00:19 WG1247945
n-Nitrosodimethylamine U 0.763 3.93 10 03/14/2019 00:19 WG1247945
n-Nitrosodiphenylamine U 0.106 0.393 1 03/13/2019 04:19 WG1247945
n-Nitrosodi-n-propylamine U 0.107 3.93 10 03/14/2019 00:19 WG1247945
Phenanthrene 0.0272 J 0.00623 0.0393 1 03/13/2019 04:19 WG1247945
Benzylbutyl phthalate U 0.0121 0.393 1 03/13/2019 04:19 WG1247945
Bis(2-ethylhexyl)phthalate U 0.0142 0.393 1 03/13/2019 04:19 WG1247945
Di-n-butyl phthalate U 0.0129 0.393 1 03/13/2019 04:19 WG1247945
Diethyl phthalate U 0.00815 0.393 1 03/13/2019 04:19 WG1247945
Dimethyl phthalate U 0.00637 0.393 1 03/13/2019 04:19 WG1247945
Di-n-octyl phthalate U 0.0107 0.393 1 03/13/2019 04:19 WG1247945
Pyrene U 0.0145 0.0393 1 03/13/2019 04:19 WG1247945
1,2,4-Trichlorobenzene U 0.103 3.93 10 03/14/2019 00:19 WG1247945
4-Chloro-3-methylphenol U 0.0563 3.93 10 03/14/2019 00:19 WG1247945
2-Chlorophenol U 0.0980 3.93 10 03/14/2019 00:19 WG1247945
2,4-Dichlorophenol U 0.0880 3.93 10 03/14/2019 00:19 WG1247945
2,4-Dimethylphenol U J0 0.556 3.93 10 03/14/2019 00:19 WG1247945
4,6-Dinitro-2-methylphenol U 0.146 0.393 1 03/13/2019 04:19 WG1247945
2-Nitrophenol U 0.153 3.93 10 03/14/2019 00:19 WG1247945
4-Nitrophenol U 0.0619 0.393 1 03/13/2019 04:19 WG1247945
Pentachlorophenol U 0.0566 0.393 1 03/13/2019 04:19 WG1247945
Phenol U 0.0820 3.93 10 03/14/2019 00:19 WG1247945
2,4,6-Trichlorophenol U 0.00919 0.393 1 03/13/2019 04:19 WG1247945
(S) 2-Fluorophenol 85.9 12.0-120 03/14/2019 00:19 WG1247945
(S) 2-Fluorophenol 84.8 12.0-120 03/13/2019 04:19 WG1247945
(S) Phenol-d5 77.8 10.0-120 03/14/2019 00:19 WG1247945
(S) Phenol-d5 76.9 10.0-120 03/13/2019 04:19 WG1247945
(S) Nitrobenzene-d5 75.3 10.0-122 03/14/2019 00:19 WG1247945
(S) Nitrobenzene-d5 90.3 10.0-122 03/13/2019 04:19 WG1247945
(S) 2-Fluorobiphenyl 74.7 15.0-120 03/14/2019 00:19 WG1247945
(S) 2-Fluorobiphenyl 72.5 15.0-120 03/13/2019 04:19 WG1247945
(S) 2,4,6-Tribromophenol 62.8 10.0-127 03/14/2019 00:19 WG1247945
(S) 2,4,6-Tribromophenol 91.2 10.0-127 03/13/2019 04:19 WG1247945
(S) p-Terphenyl-d14 84.1 10.0-120 03/14/2019 00:19 WG1247945
(S) p-Terphenyl-d14 80.6 10.0-120 03/13/2019 04:19 WG1247945
Sample Narrative:
L1076982-04 WG1247945: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 17 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 17 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1076982
OE DISP#2 (W) 6'
Collected date/time: 03/06/19 12:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 88.3 1 03/12/2019 13:16 WG1248621
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 56.3 3.77 11.3 100 03/14/2019 20:52 WG1249073
Unadjusted C9-C12 Aliphatics 45.4 3.77 11.3 100 03/14/2019 20:52 WG1249073
Unadjusted C9-C10 Aromatics 72.4 3.77 11.3 100 03/14/2019 20:52 WG1249073
Total VPH 174 3.77 11.3 100 03/14/2019 20:52 WG1249073
(S) 2,5-Dibromotoluene(FID)98.9 70.0-130 03/14/2019 20:52 WG1249073
(S) 2,5-Dibromotoluene(PID)93.4 70.0-130 03/14/2019 20:52 WG1249073
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,1,2-Tetrachloroethane U 0.00453 0.0226 8 03/11/2019 21:04 WG1248240
1,1,1-Trichloroethane U 0.00249 0.0226 8 03/11/2019 21:04 WG1248240
1,1,2,2-Tetrachloroethane U 0.00353 0.0226 8 03/11/2019 21:04 WG1248240
1,1,2-Trichloroethane U 0.00800 0.0226 8 03/11/2019 21:04 WG1248240
1,1-Dichloroethane U 0.00521 0.0226 8 03/11/2019 21:04 WG1248240
1,1-Dichloroethene U 0.00453 0.0226 8 03/11/2019 21:04 WG1248240
1,1-Dichloropropene U 0.00634 0.0226 8 03/11/2019 21:04 WG1248240
1,2,3-Trichlorobenzene U 0.00566 0.0226 8 03/11/2019 21:04 WG1248240
1,2,3-Trichloropropane U 0.0462 0.113 8 03/11/2019 21:04 WG1248240
1,2,4-Trichlorobenzene U 0.0437 0.113 8 03/11/2019 21:04 WG1248240
1,2,4-Trimethylbenzene 11.4 0.0105 0.0453 8 03/11/2019 21:04 WG1248240
1,2-Dibromo-3-Chloropropane U 0.0462 0.226 8 03/11/2019 21:04 WG1248240
1,2-Dibromoethane U 0.00476 0.0226 8 03/11/2019 21:04 WG1248240
1,2-Dichlorobenzene U 0.0131 0.0453 8 03/11/2019 21:04 WG1248240
1,2-Dichloroethane U 0.00430 0.0226 8 03/11/2019 21:04 WG1248240
1,2-Dichloropropane U 0.0116 0.0453 8 03/11/2019 21:04 WG1248240
1,3,5-Trimethylbenzene 4.74 0.00978 0.0453 8 03/11/2019 21:04 WG1248240
1,3-Dichlorobenzene U 0.0154 0.0453 8 03/11/2019 21:04 WG1248240
1,3-Dichloropropane U 0.0159 0.0453 8 03/11/2019 21:04 WG1248240
1,4-Dichlorobenzene U 0.0179 0.0453 8 03/11/2019 21:04 WG1248240
2,2-Dichloropropane U 0.00718 0.0226 8 03/11/2019 21:04 WG1248240
2-Butanone (MEK)U 0.113 0.226 8 03/11/2019 21:04 WG1248240
2-Chlorotoluene U 0.00834 0.0226 8 03/11/2019 21:04 WG1248240
4-Chlorotoluene U 0.0102 0.0453 8 03/11/2019 21:04 WG1248240
4-Methyl-2-pentanone (MIBK)U 0.0906 0.226 8 03/11/2019 21:04 WG1248240
Acetone U J0 0.125 0.226 8 03/11/2019 21:04 WG1248240
Acrylonitrile U 0.0172 0.113 8 03/11/2019 21:04 WG1248240
Benzene U 0.00362 0.00906 8 03/11/2019 21:04 WG1248240
Bromobenzene U 0.00951 0.113 8 03/11/2019 21:04 WG1248240
Bromodichloromethane U 0.00713 0.0226 8 03/11/2019 21:04 WG1248240
Bromoform U J4 0.0541 0.226 8 03/11/2019 21:04 WG1248240
Bromomethane U 0.0335 0.113 8 03/11/2019 21:04 WG1248240
Carbon tetrachloride U 0.00978 0.0453 8 03/11/2019 21:04 WG1248240
Chlorobenzene U 0.00519 0.0226 8 03/11/2019 21:04 WG1248240
Chlorodibromomethane U 0.00408 0.0226 8 03/11/2019 21:04 WG1248240
Chloroethane U 0.00978 0.0453 8 03/11/2019 21:04 WG1248240
Chloroform U 0.00376 0.0226 8 03/11/2019 21:04 WG1248240
Chloromethane U 0.0126 0.113 8 03/11/2019 21:04 WG1248240
Dichlorodifluoromethane U J4 0.00741 0.0226 8 03/11/2019 21:04 WG1248240
Di-isopropyl ether U 0.00317 0.00906 8 03/11/2019 21:04 WG1248240
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 18 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 18 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1076982
OE DISP#2 (W) 6'
Collected date/time: 03/06/19 12:40
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 0.213 0.00480 0.0226 8 03/11/2019 21:04 WG1248240
Isopropylbenzene 0.488 0.00781 0.0226 8 03/11/2019 21:04 WG1248240
Methyl tert-butyl ether U 0.00267 0.00906 8 03/11/2019 21:04 WG1248240
Methylene Chloride U 0.0601 0.226 8 03/11/2019 21:04 WG1248240
Naphthalene 0.160 0.0283 0.113 8 03/11/2019 21:04 WG1248240
Styrene U 0.0247 0.113 8 03/11/2019 21:04 WG1248240
Tetrachloroethene U 0.00634 0.0226 8 03/11/2019 21:04 WG1248240
Toluene U 0.0113 0.0453 8 03/11/2019 21:04 WG1248240
Trichloroethene U 0.00362 0.00906 8 03/11/2019 21:04 WG1248240
Trichlorofluoromethane U 0.00453 0.0226 8 03/11/2019 21:04 WG1248240
Vinyl chloride U 0.00618 0.0226 8 03/11/2019 21:04 WG1248240
Xylenes, Total 0.479 0.0433 0.0589 8 03/11/2019 21:04 WG1248240
cis-1,2-Dichloroethene U J4 0.00625 0.0226 8 03/11/2019 21:04 WG1248240
cis-1,3-Dichloropropene U 0.00614 0.0226 8 03/11/2019 21:04 WG1248240
n-Butylbenzene 2.16 0.0348 0.113 8 03/11/2019 21:04 WG1248240
n-Propylbenzene 2.26 0.0107 0.0453 8 03/11/2019 21:04 WG1248240
p-Isopropyltoluene U 0.0211 0.0453 8 03/11/2019 21:04 WG1248240
sec-Butylbenzene 0.666 0.0229 0.113 8 03/11/2019 21:04 WG1248240
tert-Butylbenzene U 0.0140 0.0453 8 03/11/2019 21:04 WG1248240
trans-1,2-Dichloroethene U 0.0129 0.0453 8 03/11/2019 21:04 WG1248240
trans-1,3-Dichloropropene U 0.0138 0.0453 8 03/11/2019 21:04 WG1248240
(S) Toluene-d8 110 75.0-131 03/11/2019 21:04 WG1248240
(S) 4-Bromofluorobenzene 102 67.0-138 03/11/2019 21:04 WG1248240
(S) 1,2-Dichloroethane-d4 85.6 70.0-130 03/11/2019 21:04 WG1248240
Sample Narrative:
L1076982-05 WG1248240: Non-target compounds too high to run at a lower dilution.
Semi-Volatile Organic Compounds (GC) by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 117 2.46 7.36 1 03/15/2019 04:57 WG1248324
Unadjusted C19-C36 Aliphatics U 2.46 7.36 1 03/15/2019 04:57 WG1248324
Unadjusted C11-C22 Aromatics 54.8 2.46 7.36 1 03/15/2019 08:34 WG1248324
Unadjusted Total Petroleum
Hydrocarbons 171 2.46 7.36 1 03/15/2019 08:34 WG1248324
(S) o-Terphenyl 69.9 40.0-140 03/15/2019 08:34 WG1248324
(S) 1-Chloro-octadecane 80.8 40.0-140 03/15/2019 04:57 WG1248324
(S) 2-Fluorobiphenyl 85.9 40.0-140 03/15/2019 08:34 WG1248324
(S) 2-Bromonaphthalene 79.5 40.0-140 03/15/2019 08:34 WG1248324
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0366 J 0.00727 0.0377 1 03/13/2019 03:10 WG1247945
Acenaphthylene U 0.00760 0.0377 1 03/13/2019 03:10 WG1247945
Benzidine U 0.0721 0.377 1 03/13/2019 03:10 WG1247945
Benzo(a)anthracene U 0.00485 0.0377 1 03/13/2019 03:10 WG1247945
Benzo(b)fluoranthene U 0.00787 0.0377 1 03/13/2019 03:10 WG1247945
Benzo(k)fluoranthene U 0.00659 0.0377 1 03/13/2019 03:10 WG1247945
Benzo(g,h,i)perylene U 0.00817 0.0377 1 03/13/2019 03:10 WG1247945
Benzo(a)pyrene U 0.00621 0.0377 1 03/13/2019 03:10 WG1247945
Bis(2-chlorethoxy)methane U 0.0872 3.77 10 03/13/2019 23:39 WG1247945
Bis(2-chloroethyl)ether U 0.101 3.77 10 03/13/2019 23:39 WG1247945
Bis(2-chloroisopropyl)ether U 0.0861 3.77 10 03/13/2019 23:39 WG1247945
4-Bromophenyl-phenylether U 0.0129 0.377 1 03/13/2019 03:10 WG1247945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:12 19 of 48
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC L1076982 04/09/19 09:18 19 of 48
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1076982
OE DISP#2 (W) 6'
Collected date/time: 03/06/19 12:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2-Chloronaphthalene U 0.00724 0.0377 1 03/13/2019 03:10 WG1247945
Chrysene U 0.00629 0.0377 1 03/13/2019 03:10 WG1247945
Dibenz(a,h)anthracene U 0.00930 0.0377 1 03/13/2019 03:10 WG1247945
3,3-Dichlorobenzidine U 0.0899 0.377 1 03/13/2019 03:10 WG1247945
2,4-Dinitrotoluene U 0.00687 0.377 1 03/13/2019 03:10 WG1247945
2,6-Dinitrotoluene U 0.00835 0.377 1 03/13/2019 03:10 WG1247945
Fluoranthene 0.00795 J 0.00562 0.0377 1 03/13/2019 03:10 WG1247945
Fluorene 0.0416 0.00772 0.0377 1 03/13/2019 03:10 WG1247945
Hexachlorobenzene U 0.00969 0.377 1 03/13/2019 03:10 WG1247945
Hexachloro-1,3-butadiene U 0.113 3.77 10 03/13/2019 23:39 WG1247945
Hexachlorocyclopentadiene U J0 0.0665 0.377 1 03/13/2019 03:10 WG1247945
Hexachloroethane U 0.152 3.77 10 03/13/2019 23:39 WG1247945
Indeno(1,2,3-cd)pyrene U 0.00874 0.0377 1 03/13/2019 03:10 WG1247945
Isophorone U 0.0591 3.77 10 03/13/2019 23:39 WG1247945
Naphthalene U 0.101 0.377 10 03/13/2019 23:39 WG1247945
Nitrobenzene U 0.0787 3.77 10 03/13/2019 23:39 WG1247945
n-Nitrosodimethylamine U 0.733 3.77 10 03/13/2019 23:39 WG1247945
n-Nitrosodiphenylamine U 0.102 0.377 1 03/13/2019 03:10 WG1247945
n-Nitrosodi-n-propylamine U 0.103 3.77 10 03/13/2019 23:39 WG1247945
Phenanthrene 0.0541 0.00598 0.0377 1 03/13/2019 03:10 WG1247945
Benzylbutyl phthalate U 0.0117 0.377 1 03/13/2019 03:10 WG1247945
Bis(2-ethylhexyl)phthalate 0.0206 J 0.0136 0.377 1 03/13/2019 03:10 WG1247945
Di-n-butyl phthalate U 0.0123 0.377 1 03/13/2019 03:10 WG1247945
Diethyl phthalate U 0.00783 0.377 1 03/13/2019 03:10 WG1247945
Dimethyl phthalate U 0.00612 0.377 1 03/13/2019 03:10 WG1247945
Di-n-octyl phthalate U 0.0103 0.377 1 03/13/2019 03:10 WG1247945
Pyrene U 0.0139 0.0377 1 03/13/2019 03:10 WG1247945
1,2,4-Trichlorobenzene U 0.0992 3.77 10 03/13/2019 23:39 WG1247945
4-Chloro-3-methylphenol U 0.0540 3.77 10 03/13/2019 23:39 WG1247945
2-Chlorophenol U 0.0941 3.77 10 03/13/2019 23:39 WG1247945
2,4-Dichlorophenol U 0.0845 3.77 10 03/13/2019 23:39 WG1247945
2,4-Dimethylphenol U J0 0.533 3.77 10 03/13/2019 23:39 WG1247945
4,6-Dinitro-2-methylphenol U 0.140 0.377 1 03/13/2019 03:10 WG1247945
2-Nitrophenol U 0.147 3.77 10 03/13/2019 23:39 WG1247945
4-Nitrophenol U 0.0595 0.377 1 03/13/2019 03:10 WG1247945
Pentachlorophenol U 0.0544 0.377 1 03/13/2019 03:10 WG1247945
Phenol U 0.0787 3.77 10 03/13/2019 23:39 WG1247945
2,4,6-Trichlorophenol U 0.00882 0.377 1 03/13/2019 03:10 WG1247945
(S) 2-Fluorophenol 78.3 12.0-120 03/13/2019 23:39 WG1247945
(S) 2-Fluorophenol 78.5 12.0-120 03/13/2019 03:10 WG1247945
(S) Phenol-d5 73.0 10.0-120 03/13/2019 03:10 WG1247945
(S) Phenol-d5 76.7 10.0-120 03/13/2019 23:39 WG1247945
(S) Nitrobenzene-d5 101 10.0-122 03/13/2019 23:39 WG1247945
(S) Nitrobenzene-d5 91.6 10.0-122 03/13/2019 03:10 WG1247945
(S) 2-Fluorobiphenyl 65.7 15.0-120 03/13/2019 03:10 WG1247945
(S) 2-Fluorobiphenyl 65.1 15.0-120 03/13/2019 23:39 WG1247945
(S) 2,4,6-Tribromophenol 60.4 10.0-127 03/13/2019 23:39 WG1247945
(S) 2,4,6-Tribromophenol 88.3 10.0-127 03/13/2019 03:10 WG1247945
(S) p-Terphenyl-d14 80.1 10.0-120 03/13/2019 03:10 WG1247945
(S) p-Terphenyl-d14 75.0 10.0-120 03/13/2019 23:39 WG1247945
Sample Narrative:
L1076982-05 WG1247945: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248621
Total Solids by Method 2540 G-2011 L1076982-01,02,03,04,05
Method Blank (MB)
(MB) R3391089-1 03/12/19 13:16
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1076982-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1076982-02 03/12/19 13:16 • (DUP) R3391089-3 03/12/19 13:16
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 83.7 83.6 1 0.116 10
Laboratory Control Sample (LCS)
(LCS) R3391089-2 03/12/19 13:16
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1249073
Volatile Petroleum Hydrocarbons by Method MADEPV L1076982-01,02,03,04,05
Method Blank (MB)
(MB) R3391884-3 03/14/19 12:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics U 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Total VPH 2.11 J 1.67 5.00
(S) 2,5-Dibromotoluene(FID)91.8 70.0-130
(S) 2,5-Dibromotoluene(PID)90.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3391884-1 03/14/19 10:08 • (LCSD) R3391884-2 03/14/19 10:41
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.20 1.15 1.17 95.9 97.2 70.0-130 1.38 25
Unadjusted C9-C12 Aliphatics 1.40 1.44 1.45 103 104 70.0-130 0.761 25
Unadjusted C9-C10 Aromatics 0.200 0.210 0.209 105 104 70.0-130 0.860 25
Total VPH 2.80 2.80 2.83 100 101 70.0-130 1.03 25
(S) 2,5-Dibromotoluene(FID) 97.6 100 70.0-130
(S) 2,5-Dibromotoluene(PID) 99.2 103 70.0-130
L1076994-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076994-01 03/14/19 21:25 • (MS) R3391884-4 03/15/19 02:54 • (MSD) R3391884-5 03/15/19 03:27
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.32 U 63.6 60.1 96.5 91.2 50 70.0-130 5.66 25
Unadjusted C9-C12 Aliphatics 1.54 17.5 82.5 95.8 84.4 102 50 70.0-130 14.9 25
Unadjusted C9-C10 Aromatics 0.220 33.5 50.6 50.5 154 154 50 70.0-130 J5 J5 0.113 25
Total VPH 3.08 51.0 197 206 94.6 101 50 70.0-130 4.80 25
(S) 2,5-Dibromotoluene(FID) 95.3 104 70.0-130
(S) 2,5-Dibromotoluene(PID) 44.0 49.6 70.0-130 J2 J2
Sample Narrative:
OS: Surrogate failure due to matrix interference.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
Method Blank (MB)
(MB) R3391185-2 03/10/19 16:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Isopropylbenzene U 0.000863 0.00250
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)U 0.0125 0.0250
Methylene Chloride U 0.00664 0.0250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
Method Blank (MB)
(MB) R3391185-2 03/10/19 16:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
4-Methyl-2-pentanone (MIBK)U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,2,3-Trichlorobenzene U 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 106 75.0-131
(S) 4-Bromofluorobenzene 98.3 67.0-138
(S) 1,2-Dichloroethane-d4 96.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3391185-1 03/10/19 15:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.799 128 10.0-160
Acrylonitrile 0.625 0.685 110 45.0-153
Benzene 0.125 0.104 83.2 70.0-123
Bromobenzene 0.125 0.156 124 73.0-121 J4
Bromodichloromethane 0.125 0.135 108 73.0-121
Bromoform 0.125 0.133 106 64.0-132
Bromomethane 0.125 0.105 84.3 56.0-147
n-Butylbenzene 0.125 0.101 80.5 68.0-135
sec-Butylbenzene 0.125 0.112 89.8 74.0-130
tert-Butylbenzene 0.125 0.0954 76.3 75.0-127
Carbon tetrachloride 0.125 0.119 95.1 66.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3391185-1 03/10/19 15:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Chlorobenzene 0.125 0.127 102 76.0-128
Chlorodibromomethane 0.125 0.149 119 74.0-127
Chloroform 0.125 0.122 97.5 72.0-123
Chloromethane 0.125 0.156 125 51.0-138
2-Chlorotoluene 0.125 0.112 89.3 75.0-124
4-Chlorotoluene 0.125 0.114 91.5 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.141 113 59.0-130
1,2-Dibromoethane 0.125 0.129 103 74.0-128
1,2-Dichlorobenzene 0.125 0.120 96.0 76.0-124
1,3-Dichlorobenzene 0.125 0.101 80.8 76.0-125
1,4-Dichlorobenzene 0.125 0.110 88.1 77.0-121
Dichlorodifluoromethane 0.125 0.136 109 43.0-156
1,1-Dichloroethane 0.125 0.140 112 70.0-127
1,2-Dichloroethane 0.125 0.107 85.8 65.0-131
1,1-Dichloroethene 0.125 0.102 81.5 65.0-131
cis-1,2-Dichloroethene 0.125 0.0929 74.3 73.0-125
trans-1,2-Dichloroethene 0.125 0.103 82.0 71.0-125
1,2-Dichloropropane 0.125 0.134 108 74.0-125
1,1-Dichloropropene 0.125 0.119 95.3 73.0-125
1,3-Dichloropropane 0.125 0.146 117 80.0-125
cis-1,3-Dichloropropene 0.125 0.116 93.1 76.0-127
trans-1,3-Dichloropropene 0.125 0.126 101 73.0-127
2,2-Dichloropropane 0.125 0.135 108 59.0-135
Di-isopropyl ether 0.125 0.127 102 60.0-136
Ethylbenzene 0.125 0.122 97.8 74.0-126
Isopropylbenzene 0.125 0.101 81.1 72.0-127
p-Isopropyltoluene 0.125 0.107 85.6 72.0-133
2-Butanone (MEK)0.625 0.606 96.9 30.0-160
Methylene Chloride 0.125 0.0957 76.5 68.0-123
4-Methyl-2-pentanone (MIBK)0.625 0.559 89.5 56.0-143
Methyl tert-butyl ether 0.125 0.117 93.8 66.0-132
Naphthalene 0.125 0.142 113 59.0-130
n-Propylbenzene 0.125 0.109 86.9 74.0-126
Styrene 0.125 0.130 104 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.121 97.1 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.130 104 68.0-128
Tetrachloroethene 0.125 0.126 101 70.0-136
Toluene 0.125 0.0994 79.5 75.0-121
1,2,3-Trichlorobenzene 0.125 0.119 94.8 59.0-139
1,2,4-Trichlorobenzene 0.125 0.127 101 62.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3391185-1 03/10/19 15:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
1,1,1-Trichloroethane 0.125 0.111 88.7 69.0-126
1,1,2-Trichloroethane 0.125 0.104 82.9 78.0-123
Trichlorofluoromethane 0.125 0.136 109 61.0-142
1,2,3-Trichloropropane 0.125 0.116 92.9 67.0-129
1,2,4-Trimethylbenzene 0.125 0.102 81.3 70.0-126
1,3,5-Trimethylbenzene 0.125 0.118 94.4 73.0-127
Vinyl chloride 0.125 0.137 110 63.0-134
Xylenes, Total 0.375 0.333 88.8 72.0-127
(S) Toluene-d8 103 75.0-131
(S) 4-Bromofluorobenzene 94.9 67.0-138
(S) 1,2-Dichloroethane-d4 103 70.0-130
L1076982-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076982-04 03/10/19 23:32 • (MS) R3391185-3 03/10/19 23:51 • (MSD) R3391185-4 03/11/19 00:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.737 U 26.3 27.6 89.3 93.7 40 10.0-160 4.80 40
Acrylonitrile 0.737 U 21.5 23.3 72.8 78.9 40 10.0-160 8.08 40
Benzene 0.147 U 3.50 2.22 59.4 37.6 40 10.0-149 J3 44.9 37
Bromobenzene 0.147 U 5.56 4.09 94.2 69.3 40 10.0-156 30.5 38
Bromodichloromethane 0.147 U 4.67 3.65 79.2 62.0 40 10.0-143 24.4 37
Bromoform 0.147 U 4.56 4.13 77.3 70.0 40 10.0-146 9.90 36
Bromomethane 0.147 U 3.56 2.35 60.4 39.8 40 10.0-149 J3 41.1 38
n-Butylbenzene 0.147 1.23 4.99 3.39 63.8 36.7 40 10.0-160 38.2 40
sec-Butylbenzene 0.147 0.465 4.95 3.02 76.0 43.4 40 10.0-159 J3 48.3 39
tert-Butylbenzene 0.147 U 3.74 2.21 63.5 37.5 40 10.0-156 J3 51.4 39
Carbon tetrachloride 0.147 U 4.02 2.26 68.1 38.3 40 10.0-145 J3 56.1 37
Chlorobenzene 0.147 U 4.73 3.24 80.2 54.9 40 10.0-152 37.6 39
Chlorodibromomethane 0.147 U 5.27 4.49 89.4 76.1 40 10.0-146 16.1 37
Chloroform 0.147 U 4.17 2.89 70.7 49.0 40 10.0-146 36.3 37
Chloromethane 0.147 U 4.76 2.88 80.7 48.8 40 10.0-159 J3 49.3 37
2-Chlorotoluene 0.147 U 4.52 2.72 76.7 46.1 40 10.0-159 J3 49.9 38
4-Chlorotoluene 0.147 U 3.98 2.74 67.5 46.4 40 10.0-155 37.0 39
1,2-Dibromo-3-Chloropropane 0.147 U 5.03 4.92 85.2 83.3 40 10.0-151 2.23 39
1,2-Dibromoethane 0.147 U 4.40 4.09 74.7 69.4 40 10.0-148 7.30 34
1,2-Dichlorobenzene 0.147 U 4.54 3.43 77.0 58.2 40 10.0-155 27.8 37
1,3-Dichlorobenzene 0.147 U 3.83 2.48 64.9 42.1 40 10.0-153 J3 42.5 38
1,4-Dichlorobenzene 0.147 U 4.00 2.92 67.9 49.5 40 10.0-151 31.3 38
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
L1076982-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076982-04 03/10/19 23:32 • (MS) R3391185-3 03/10/19 23:51 • (MSD) R3391185-4 03/11/19 00:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Dichlorodifluoromethane 0.147 U 3.33 2.11 56.4 35.9 40 10.0-160 J3 44.5 35
1,1-Dichloroethane 0.147 U 5.04 3.37 85.4 57.1 40 10.0-147 J3 39.7 37
1,2-Dichloroethane 0.147 U 3.51 2.96 59.6 50.2 40 10.0-148 17.1 35
1,1-Dichloroethene 0.147 U 3.61 2.00 61.3 33.9 40 10.0-155 J3 57.5 37
cis-1,2-Dichloroethene 0.147 U 3.16 2.08 53.6 35.2 40 10.0-149 J3 41.6 37
trans-1,2-Dichloroethene 0.147 U 3.33 1.96 56.5 33.3 40 10.0-150 J3 51.8 37
1,2-Dichloropropane 0.147 U 4.91 3.80 83.3 64.4 40 10.0-148 25.6 37
1,1-Dichloropropene 0.147 U 4.02 2.25 68.1 38.2 40 10.0-153 J3 56.2 35
1,3-Dichloropropane 0.147 U 5.28 4.68 89.6 79.4 40 10.0-154 12.1 35
cis-1,3-Dichloropropene 0.147 U 4.19 3.13 71.0 53.1 40 10.0-151 28.9 37
trans-1,3-Dichloropropene 0.147 U 4.41 3.74 74.8 63.3 40 10.0-148 16.6 37
2,2-Dichloropropane 0.147 U 4.76 2.66 80.8 45.2 40 10.0-138 J3 56.5 36
Di-isopropyl ether 0.147 U 4.44 3.65 75.3 61.8 40 10.0-147 19.6 36
Ethylbenzene 0.147 1.14 5.45 3.87 73.1 46.2 40 10.0-160 34.0 38
Isopropylbenzene 0.147 0.647 4.59 3.08 66.9 41.2 40 10.0-155 J3 39.6 38
p-Isopropyltoluene 0.147 U 5.18 3.67 87.9 62.3 40 10.0-160 34.1 40
2-Butanone (MEK)0.737 U 19.9 21.8 67.6 74.0 40 10.0-160 8.99 40
Methylene Chloride 0.147 U 3.46 2.60 58.7 44.0 40 10.0-141 28.5 37
4-Methyl-2-pentanone (MIBK)0.737 U 18.7 20.0 63.3 67.8 40 10.0-160 6.85 35
Methyl tert-butyl ether 0.147 U 4.05 3.75 68.7 63.6 40 11.0-147 7.85 35
Naphthalene 0.147 1.92 6.89 6.42 84.2 76.3 40 10.0-160 6.96 36
n-Propylbenzene 0.147 3.11 7.05 5.46 66.8 39.9 40 10.0-158 25.4 38
Styrene 0.147 U 4.75 3.43 80.5 58.1 40 10.0-160 32.3 40
1,1,1,2-Tetrachloroethane 0.147 U 4.73 3.33 80.3 56.5 40 10.0-149 34.7 39
1,1,2,2-Tetrachloroethane 0.147 U 4.36 4.04 73.9 68.5 40 10.0-160 7.52 35
Tetrachloroethene 0.147 U 4.62 2.59 78.4 43.9 40 10.0-156 J3 56.4 39
Toluene 0.147 0.164 3.68 2.33 59.7 36.7 40 10.0-156 J3 45.1 38
1,2,3-Trichlorobenzene 0.147 U 4.28 3.77 72.6 64.0 40 10.0-160 12.7 40
1,2,4-Trichlorobenzene 0.147 U 4.89 3.72 83.0 63.0 40 10.0-160 27.4 40
1,1,1-Trichloroethane 0.147 U 3.85 2.20 65.4 37.3 40 10.0-144 J3 54.7 35
1,1,2-Trichloroethane 0.147 U 3.88 3.57 65.7 60.6 40 10.0-160 8.09 35
Trichlorofluoromethane 0.147 U 4.46 2.22 75.7 37.6 40 10.0-160 J3 67.2 40
1,2,3-Trichloropropane 0.147 U 4.18 3.92 70.8 66.4 40 10.0-156 6.44 35
1,2,4-Trimethylbenzene 0.147 21.5 24.3 23.7 47.6 37.3 40 10.0-160 2.52 36
1,3,5-Trimethylbenzene 0.147 8.01 12.1 10.7 69.7 46.4 40 10.0-160 12.0 38
Vinyl chloride 0.147 U 4.10 2.24 69.5 38.0 40 10.0-160 J3 58.6 37
Xylenes, Total 0.442 6.75 18.4 14.9 66.0 45.9 40 10.0-160 21.4 38
(S) Toluene-d8 104 105 75.0-131
(S) 4-Bromofluorobenzene 95.4 95.4 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247993
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
L1076982-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076982-04 03/10/19 23:32 • (MS) R3391185-3 03/10/19 23:51 • (MSD) R3391185-4 03/11/19 00:10
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
(S) 1,2-Dichloroethane-d4 96.9 98.1 70.0-130
Sample Narrative:
OS: Non-target compounds too high to run at a lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248240
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-05
Method Blank (MB)
(MB) R3391131-2 03/11/19 15:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Isopropylbenzene U 0.000863 0.00250
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)U 0.0125 0.0250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248240
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-05
Method Blank (MB)
(MB) R3391131-2 03/11/19 15:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Methylene Chloride 0.00738 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,2,3-Trichlorobenzene 0.00145 J 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 113 75.0-131
(S) 4-Bromofluorobenzene 96.8 67.0-138
(S) 1,2-Dichloroethane-d4 74.0 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3391131-1 03/11/19 13:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.943 151 10.0-160
Acrylonitrile 0.625 0.738 118 45.0-153
Benzene 0.125 0.127 102 70.0-123
Bromobenzene 0.125 0.101 81.1 73.0-121
Bromodichloromethane 0.125 0.101 81.1 73.0-121
Bromoform 0.125 0.181 145 64.0-132 J4
Bromomethane 0.125 0.104 83.1 56.0-147
n-Butylbenzene 0.125 0.102 81.5 68.0-135
sec-Butylbenzene 0.125 0.100 80.3 74.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248240
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-05
Laboratory Control Sample (LCS)
(LCS) R3391131-1 03/11/19 13:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
tert-Butylbenzene 0.125 0.104 83.6 75.0-127
Carbon tetrachloride 0.125 0.130 104 66.0-128
Chlorobenzene 0.125 0.123 98.2 76.0-128
Chlorodibromomethane 0.125 0.145 116 74.0-127
Chloroethane 0.125 0.120 96.3 61.0-134
Chloroform 0.125 0.126 101 72.0-123
Chloromethane 0.125 0.129 103 51.0-138
2-Chlorotoluene 0.125 0.120 96.4 75.0-124
4-Chlorotoluene 0.125 0.0950 76.0 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.122 97.5 59.0-130
1,2-Dibromoethane 0.125 0.122 97.2 74.0-128
1,2-Dichlorobenzene 0.125 0.102 81.6 76.0-124
1,3-Dichlorobenzene 0.125 0.102 81.5 76.0-125
1,4-Dichlorobenzene 0.125 0.101 80.7 77.0-121
Dichlorodifluoromethane 0.125 0.228 182 43.0-156 J4
1,1-Dichloroethane 0.125 0.136 109 70.0-127
1,2-Dichloroethane 0.125 0.121 96.9 65.0-131
1,1-Dichloroethene 0.125 0.101 80.4 65.0-131
cis-1,2-Dichloroethene 0.125 0.181 145 73.0-125 J4
trans-1,2-Dichloroethene 0.125 0.133 106 71.0-125
1,2-Dichloropropane 0.125 0.128 102 74.0-125
1,1-Dichloropropene 0.125 0.117 94.0 73.0-125
1,3-Dichloropropane 0.125 0.130 104 80.0-125
cis-1,3-Dichloropropene 0.125 0.115 91.8 76.0-127
trans-1,3-Dichloropropene 0.125 0.136 109 73.0-127
2,2-Dichloropropane 0.125 0.148 119 59.0-135
Di-isopropyl ether 0.125 0.121 96.6 60.0-136
Ethylbenzene 0.125 0.134 107 74.0-126
Isopropylbenzene 0.125 0.131 105 72.0-127
p-Isopropyltoluene 0.125 0.112 90.0 72.0-133
2-Butanone (MEK)0.625 0.852 136 30.0-160
Methylene Chloride 0.125 0.131 105 68.0-123
4-Methyl-2-pentanone (MIBK)0.625 0.715 114 56.0-143
Methyl tert-butyl ether 0.125 0.131 105 66.0-132
Naphthalene 0.125 0.105 84.2 59.0-130
n-Propylbenzene 0.125 0.103 82.4 74.0-126
Styrene 0.125 0.135 108 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.146 117 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.148 118 68.0-128
Tetrachloroethene 0.125 0.119 94.8 70.0-136
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248240
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-05
Laboratory Control Sample (LCS)
(LCS) R3391131-1 03/11/19 13:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Toluene 0.125 0.111 88.8 75.0-121
1,2,3-Trichlorobenzene 0.125 0.140 112 59.0-139
1,2,4-Trichlorobenzene 0.125 0.111 88.5 62.0-137
1,1,1-Trichloroethane 0.125 0.100 80.3 69.0-126
1,1,2-Trichloroethane 0.125 0.123 98.2 78.0-123
Trichloroethene 0.125 0.105 84.3 76.0-126
Trichlorofluoromethane 0.125 0.126 101 61.0-142
1,2,3-Trichloropropane 0.125 0.116 93.1 67.0-129
1,2,4-Trimethylbenzene 0.125 0.0963 77.1 70.0-126
1,3,5-Trimethylbenzene 0.125 0.0914 73.1 73.0-127
Vinyl chloride 0.125 0.144 115 63.0-134
Xylenes, Total 0.375 0.349 93.1 72.0-127
(S) Toluene-d8 108 75.0-131
(S) 4-Bromofluorobenzene 107 67.0-138
(S) 1,2-Dichloroethane-d4 93.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1249284
Volatile Organic Compounds (GC/MS) by Method 8260D L1076982-01,02,03,04
Method Blank (MB)
(MB) R3391260-2 03/13/19 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Chloroethane U 0.00108 0.00500
Trichloroethene U 0.000400 0.00100
(S) Toluene-d8 95.2 75.0-131
(S) 4-Bromofluorobenzene 89.7 67.0-138
(S) 1,2-Dichloroethane-d4 99.9 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3391260-1 03/13/19 09:50
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Chloroethane 0.125 0.152 121 61.0-134
Trichloroethene 0.125 0.121 96.6 76.0-126
(S) Toluene-d8 94.7 75.0-131
(S) 4-Bromofluorobenzene 95.7 67.0-138
(S) 1,2-Dichloroethane-d4 108 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248324
Semi-Volatile Organic Compounds (GC) by Method MADEPE L1076982-01,02,03,04,05
Method Blank (MB)
(MB) R3391885-1 03/15/19 00:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) 1-Chloro-octadecane 88.5 40.0-140
Method Blank (MB)
(MB) R3391885-4 03/15/19 01:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics 2.22 J 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) o-Terphenyl 81.8 40.0-140
(S) 2-Fluorobiphenyl 91.0 40.0-140
(S) 2-Bromonaphthalene 85.9 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3391885-2 03/15/19 00:55 • (LCSD) R3391885-3 03/15/19 01:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 28.5 28.6 71.4 71.7 40.0-140 0.350 25
Unadjusted C19-C36 Aliphatics 53.2 44.8 45.5 84.2 85.5 40.0-140 1.55 25
(S) 1-Chloro-octadecane 88.0 84.8 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3391885-5 03/15/19 02:07 • (LCSD) R3391885-6 03/15/19 02:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 93.6 99.4 82.8 88.0 40.0-140 6.01 25
(S) o-Terphenyl 78.0 82.5 40.0-140
(S) 2-Fluorobiphenyl 90.8 89.3 40.0-140
(S) 2-Bromonaphthalene 85.3 85.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1248324
Semi-Volatile Organic Compounds (GC) by Method MADEPE L1076982-01,02,03,04,05
L1076976-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076976-04 03/15/19 13:24 • (MS) R3391885-7 03/15/19 13:48 • (MSD) R3391885-8 03/15/19 14:12
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 49.0 ND 28.7 30.5 58.6 62.2 1 40.0-140 5.81 50
Unadjusted C19-C36 Aliphatics 65.3 340 302 351 0.000 16.9 1 40.0-140 V V 15.0 50
(S) 1-Chloro-octadecane 74.2 71.6 40.0-140
L1076976-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076976-04 03/15/19 13:24 • (MS) R3391885-10 03/15/19 15:01 • (MSD) R3391885-9 03/15/19 14:37
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 139 116 173 235 41.5 85.8 1 40.0-140 30.1 50
(S) o-Terphenyl 64.5 61.1 40.0-140
(S) 2-Fluorobiphenyl 85.7 86.5 40.0-140
(S) 2-Bromonaphthalene 82.0 83.5 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1076982-01,02,03,04,05
Method Blank (MB)
(MB) R3391266-3 03/13/19 02:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0333
Acenaphthylene U 0.00671 0.0333
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0333
Benzo(b)fluoranthene U 0.00695 0.0333
Benzo(k)fluoranthene U 0.00582 0.0333
Benzo(g,h,i)perylene U 0.00721 0.0333
Benzo(a)pyrene U 0.00548 0.0333
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0333
Chrysene U 0.00555 0.0333
Dibenz(a,h)anthracene U 0.00821 0.0333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0333
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0333
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0333
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0333
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0333
1,2,4-Trichlorobenzene U 0.00876 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1076982-01,02,03,04,05
Method Blank (MB)
(MB) R3391266-3 03/13/19 02:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 68.2 10.0-122
(S) 2-Fluorobiphenyl 63.7 15.0-120
(S) p-Terphenyl-d14 78.7 10.0-120
(S) Phenol-d5 64.1 10.0-120
(S) 2-Fluorophenol 72.7 12.0-120
(S) 2,4,6-Tribromophenol 78.7 10.0-127
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3391266-1 03/13/19 02:00 • (LCSD) R3391266-2 03/13/19 02:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.666 0.525 0.544 78.8 81.7 38.0-120 3.55 22
Acenaphthylene 0.666 0.565 0.584 84.8 87.7 40.0-120 3.31 22
Benzidine 1.33 0.123 0.154 9.25 11.6 1.00-120 22.4 40
Benzo(a)anthracene 0.666 0.619 0.630 92.9 94.6 44.0-120 1.76 20
Benzo(b)fluoranthene 0.666 0.588 0.605 88.3 90.8 43.0-120 2.85 22
Benzo(k)fluoranthene 0.666 0.576 0.589 86.5 88.4 44.0-120 2.23 21
Benzo(g,h,i)perylene 0.666 0.676 0.680 102 102 43.0-120 0.590 22
Benzo(a)pyrene 0.666 0.588 0.604 88.3 90.7 45.0-120 2.68 20
Bis(2-chlorethoxy)methane 0.666 0.422 0.436 63.4 65.5 20.0-120 3.26 23
Bis(2-chloroethyl)ether 0.666 0.522 0.548 78.4 82.3 16.0-120 4.86 31
Bis(2-chloroisopropyl)ether 0.666 0.511 0.547 76.7 82.1 23.0-120 6.81 30
4-Bromophenyl-phenylether 0.666 0.577 0.597 86.6 89.6 40.0-120 3.41 21
2-Chloronaphthalene 0.666 0.498 0.515 74.8 77.3 35.0-120 3.36 24
Chrysene 0.666 0.579 0.589 86.9 88.4 43.0-120 1.71 20
Dibenz(a,h)anthracene 0.666 0.638 0.643 95.8 96.5 44.0-120 0.781 22
3,3-Dichlorobenzidine 1.33 0.883 0.924 66.4 69.5 28.0-120 4.54 23
2,4-Dinitrotoluene 0.666 0.639 0.667 95.9 100 45.0-120 4.29 21
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1076982-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3391266-1 03/13/19 02:00 • (LCSD) R3391266-2 03/13/19 02:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
2,6-Dinitrotoluene 0.666 0.583 0.603 87.5 90.5 42.0-120 3.37 21
Fluoranthene 0.666 0.637 0.640 95.6 96.1 44.0-120 0.470 21
Fluorene 0.666 0.574 0.588 86.2 88.3 41.0-120 2.41 22
Hexachlorobenzene 0.666 0.591 0.603 88.7 90.5 39.0-120 2.01 21
Hexachloro-1,3-butadiene 0.666 0.492 0.500 73.9 75.1 15.0-120 1.61 28
Hexachlorocyclopentadiene 0.666 0.482 0.491 72.4 73.7 15.0-120 1.85 31
Hexachloroethane 0.666 0.570 0.592 85.6 88.9 17.0-120 3.79 31
Indeno(1,2,3-cd)pyrene 0.666 0.642 0.654 96.4 98.2 45.0-120 1.85 21
Isophorone 0.666 0.467 0.484 70.1 72.7 23.0-120 3.58 23
Naphthalene 0.666 0.451 0.465 67.7 69.8 18.0-120 3.06 24
Nitrobenzene 0.666 0.447 0.469 67.1 70.4 17.0-120 4.80 26
n-Nitrosodimethylamine 0.666 0.673 0.718 101 108 10.0-125 6.47 33
n-Nitrosodiphenylamine 0.666 0.547 0.563 82.1 84.5 40.0-120 2.88 21
n-Nitrosodi-n-propylamine 0.666 0.531 0.566 79.7 85.0 26.0-120 6.38 27
Phenanthrene 0.666 0.578 0.588 86.8 88.3 42.0-120 1.72 20
Benzylbutyl phthalate 0.666 0.659 0.662 98.9 99.4 40.0-120 0.454 21
Bis(2-ethylhexyl)phthalate 0.666 0.701 0.705 105 106 41.0-120 0.569 21
Di-n-butyl phthalate 0.666 0.653 0.652 98.0 97.9 43.0-120 0.153 20
Diethyl phthalate 0.666 0.607 0.634 91.1 95.2 43.0-120 4.35 21
Dimethyl phthalate 0.666 0.573 0.596 86.0 89.5 43.0-120 3.93 22
Di-n-octyl phthalate 0.666 0.694 0.701 104 105 40.0-120 1.00 21
Pyrene 0.666 0.609 0.619 91.4 92.9 41.0-120 1.63 21
1,2,4-Trichlorobenzene 0.666 0.443 0.456 66.5 68.5 17.0-120 2.89 26
4-Chloro-3-methylphenol 0.666 0.533 0.539 80.0 80.9 28.0-120 1.12 20
2-Chlorophenol 0.666 0.561 0.591 84.2 88.7 28.0-120 5.21 28
2,4-Dichlorophenol 0.666 0.493 0.508 74.0 76.3 25.0-120 3.00 21
2,4-Dimethylphenol 0.666 0.498 0.525 74.8 78.8 15.0-120 5.28 26
4,6-Dinitro-2-methylphenol 0.666 0.573 0.619 86.0 92.9 16.0-120 7.72 33
2-Nitrophenol 0.666 0.496 0.511 74.5 76.7 20.0-120 2.98 25
4-Nitrophenol 0.666 0.557 0.576 83.6 86.5 27.0-120 3.35 24
Pentachlorophenol 0.666 0.544 0.562 81.7 84.4 29.0-120 3.25 25
Phenol 0.666 0.503 0.534 75.5 80.2 28.0-120 5.98 27
2,4,6-Trichlorophenol 0.666 0.527 0.545 79.1 81.8 37.0-120 3.36 24
(S) Nitrobenzene-d5 67.0 68.5 10.0-122
(S) 2-Fluorobiphenyl 76.9 79.9 15.0-120
(S) p-Terphenyl-d14 90.1 89.8 10.0-120
(S) Phenol-d5 78.4 81.2 10.0-120
(S) 2-Fluorophenol 89.2 92.0 12.0-120
(S) 2,4,6-Tribromophenol 100 100 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1076982-01,02,03,04,05
L1076982-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076982-02 03/13/19 04:42 • (MS) R3391266-4 03/13/19 05:05 • (MSD) R3391266-5 03/13/19 05:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.791 0.0317 0.600 0.563 71.8 66.9 1 18.0-120 6.37 32
Acenaphthylene 0.791 U 0.610 0.560 77.2 70.6 1 25.0-120 8.57 32
Benzidine 1.58 U 0.625 0.640 39.6 40.3 1 1.00-120 2.46 40
Benzo(a)anthracene 0.791 U 0.670 0.639 84.7 80.6 1 25.0-120 4.74 29
Benzo(b)fluoranthene 0.791 U 0.601 0.585 76.0 73.8 1 19.0-122 2.62 31
Benzo(k)fluoranthene 0.791 U 0.607 0.576 76.7 72.6 1 23.0-120 5.25 30
Benzo(g,h,i)perylene 0.791 U 0.735 0.707 92.9 89.2 1 10.0-120 3.81 33
Benzo(a)pyrene 0.791 U 0.622 0.603 78.7 76.1 1 24.0-120 3.12 30
Bis(2-chlorethoxy)methane 0.791 U 0.750 0.674 94.9 84.9 1 10.0-120 10.7 34
Bis(2-chloroethyl)ether 0.791 U 0.590 0.517 74.6 65.2 1 10.0-120 13.2 40
Bis(2-chloroisopropyl)ether 0.791 U 0.0185 0.575 2.34 72.4 1 10.0-120 J6 J3 188 40
4-Bromophenyl-phenylether 0.791 U 0.624 0.582 78.9 73.3 1 27.0-120 6.94 30
2-Chloronaphthalene 0.791 U 0.594 0.541 75.1 68.2 1 20.0-120 9.26 32
Chrysene 0.791 U 0.631 0.577 79.8 72.7 1 21.0-120 8.90 29
Dibenz(a,h)anthracene 0.791 U 0.680 0.659 86.0 83.1 1 10.0-120 3.03 32
3,3-Dichlorobenzidine 1.58 U 1.02 1.01 64.6 63.5 1 10.0-120 0.942 34
2,4-Dinitrotoluene 0.791 U 0.731 0.706 92.4 89.0 1 30.0-120 3.49 31
2,6-Dinitrotoluene 0.791 U 0.637 0.653 80.5 82.4 1 25.0-120 2.59 31
Fluoranthene 0.791 0.00818 0.769 0.729 96.2 90.8 1 18.0-126 5.42 32
Fluorene 0.791 0.0407 0.653 0.608 77.5 71.5 1 25.0-120 7.20 30
Hexachlorobenzene 0.791 U 0.631 0.579 79.8 73.0 1 27.0-120 8.49 28
Hexachloro-1,3-butadiene 0.791 U 0.628 0.552 79.5 69.6 1 10.0-120 13.0 38
Hexachlorocyclopentadiene 0.791 U 0.514 0.460 65.0 58.0 1 10.0-120 11.0 40
Hexachloroethane 0.791 U 6.78 6.31 858 795 1 10.0-120 E J5 E J5 7.30 40
Indeno(1,2,3-cd)pyrene 0.791 U 0.692 0.672 87.5 84.8 1 10.0-120 2.80 32
Isophorone 0.791 U 0.626 0.553 79.2 69.7 1 13.0-120 12.4 34
Naphthalene 0.791 U 1.02 0.922 129 116 1 10.0-120 J5 10.3 35
Nitrobenzene 0.791 U 0.822 0.751 104 94.7 1 10.0-120 8.96 36
n-Nitrosodimethylamine 0.791 U 0.775 0.675 98.0 85.1 1 10.0-127 13.8 40
n-Nitrosodiphenylamine 0.791 U 0.657 0.608 83.1 76.7 1 17.0-120 7.74 29
n-Nitrosodi-n-propylamine 0.791 U 0.696 0.601 88.1 75.8 1 10.0-120 14.7 37
Phenanthrene 0.791 0.0511 0.678 0.624 79.3 72.2 1 17.0-120 8.44 31
Benzylbutyl phthalate 0.791 U 0.708 0.668 89.6 84.2 1 23.0-120 5.90 30
Bis(2-ethylhexyl)phthalate 0.791 U 0.762 0.720 96.4 90.8 1 17.0-126 5.64 30
Di-n-butyl phthalate 0.791 U 0.719 0.693 90.9 87.3 1 30.0-120 3.72 29
Diethyl phthalate 0.791 U 0.692 0.651 87.5 82.1 1 26.0-120 6.05 28
Dimethyl phthalate 0.791 U 0.632 0.645 79.9 81.3 1 25.0-120 2.06 29
Di-n-octyl phthalate 0.791 U 0.692 0.676 87.5 85.2 1 21.0-123 2.27 29
Pyrene 0.791 0.0205 0.657 0.629 80.5 76.8 1 16.0-121 4.27 32
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1247945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1076982-01,02,03,04,05
L1076982-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1076982-02 03/13/19 04:42 • (MS) R3391266-4 03/13/19 05:05 • (MSD) R3391266-5 03/13/19 05:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,2,4-Trichlorobenzene 0.791 U 0.565 0.500 71.5 63.1 1 12.0-120 12.1 37
4-Chloro-3-methylphenol 0.791 U 0.665 0.645 84.1 81.3 1 15.0-120 3.10 30
2-Chlorophenol 0.791 U 0.637 0.553 80.5 69.7 1 15.0-120 14.1 37
2,4-Dichlorophenol 0.791 U 0.674 0.602 85.2 75.9 1 20.0-120 11.2 31
2,4-Dimethylphenol 0.791 U 0.736 0.655 93.1 82.5 1 10.0-120 11.7 33
4,6-Dinitro-2-methylphenol 0.791 U 0.776 0.700 98.2 88.3 1 10.0-120 10.4 39
2-Nitrophenol 0.791 U 0.705 0.618 89.1 77.9 1 12.0-120 13.2 39
4-Nitrophenol 0.791 U 0.714 0.677 90.3 85.4 1 10.0-137 5.32 32
Pentachlorophenol 0.791 U 0.688 0.662 87.0 83.4 1 10.0-160 3.89 31
Phenol 0.791 U 0.545 0.481 68.9 60.7 1 12.0-120 12.3 38
2,4,6-Trichlorophenol 0.791 U 0.573 0.529 72.5 66.7 1 19.0-120 8.02 32
(S) Nitrobenzene-d5 87.3 77.4 10.0-122
(S) 2-Fluorobiphenyl 77.9 69.3 15.0-120
(S) p-Terphenyl-d14 79.5 74.7 10.0-120
(S) Phenol-d5 78.7 66.7 10.0-120
(S) 2-Fluorophenol 85.2 71.8 12.0-120
(S) 2,4,6-Tribromophenol 95.2 87.0 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J0 J0: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met method criteria.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 1 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:O:937-863-3000 x6507 Fax #:Fax: [phone]
Speedway Proj. Mgr: Mr Bryan Matthew Witt **INVOICE TO SPEEDWAY**
AFE #:190004 Work Order #:1103358557

COC ID # 00050804
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Raleigh, NC
Project Mgr: Patrick Kelly
Address:1125 E. Morehead Street, Suite 104, Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:Gary Fischer
Shipped:FedExp
Tracking #:475750882873
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
OE DISP#2 (BOTTOM) 6.5'03/06/2019 11:40am S 6 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
OE DISP#2 (E) 6'03/06/2019 11:55am S 6 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
OE DISP#2 (N) 6'03/06/2019 12:10pm S 6 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
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Page 2 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006993 Facility ID 0000015515
Address:670 N Reilly Rd
City:Fayetteville State:NC
Phone #:O:937-863-3000 x6507 Fax #:Fax: [phone]
Speedway Proj. Mgr: Mr Bryan Matthew Witt **INVOICE TO SPEEDWAY**
AFE #:190004 Work Order #:1103358557

COC ID # 00050804
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Mid-Atlantic Associates, Inc. - Raleigh, NC
Project Mgr: Patrick Kelly
Address:1125 E. Morehead Street, Suite 104, Charlotte, NC 28204-2849
Phone #:Fax #:
Sampler:Gary Fischer
Shipped:FedExp
Tracking #:475750882873
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
OE DISP#2 (S) 6'03/06/2019 12:25pm S 6 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
OE DISP#2 (W) 6'03/06/2019 12:40pm S 6 4 OZ NONE EPH MADEP EPH
40 MIL AMBER VIAL MEOH/NAHSO48260D 8260D
4 OZ NONE Semi Volatile 8270E 8270E
40 MIL AMBER VIAL MEOH VPH MADEP VPH
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 50804 Printed: 05/25/2019
Analysis Name: 8260D ( Soil )
Analysis Description / Method:VOCs by 8260D / 8260D
Container Type / Preservative:40 MIL AMBER VIAL / MEOH/NAHSO4
Analytes: 1,1,1,2-Tetrachloroethane mg/Kg, 1,1,1-Trichloroethane mg/Kg, 1,1,2,2-Tetrachloroethane mg/Kg, 1,1,2-Trichloroethane mg/Kg, 1,1-Dichloroethane mg/Kg, 1,1-Dichloroethene mg/Kg, 1,1-Dichloropropene
mg/Kg, 1,2,3-Trichlorobenzene mg/Kg, 1,2,3-Trichloropropane mg/Kg, 1,2,4-Trichlorobenzene mg/Kg, 1,2,4-Trimethylbenzene mg/Kg, 1,2-Dibromo-3-chloropropane mg/Kg, 1,2-Dibromoethane mg/Kg,
1,2-Dichlorobenzene mg/Kg, 1,2-Dichloroethane mg/Kg, 1,2-Dichloropropane mg/Kg, 1,3,5-Trimethylbenzene mg/Kg, 1,3-Dichlorobenzene mg/Kg, 1,3-Dichloropropane mg/Kg, 1,4-Dichlorobenzene mg/Kg,
2,2-Dichloropropane mg/Kg, 2-Butanone mg/Kg, 2-Chlorotoluene mg/Kg, 4-Chlorotoluene mg/Kg, 4-Methyl-2-pentanone mg/Kg, Acetone mg/Kg, Acrylonitrile mg/Kg, Benzene mg/Kg, Bromobenzene mg/Kg,
Bromodichloromethane mg/Kg, Bromoform mg/Kg, Bromomethane mg/Kg, Carbon tetrachloride mg/Kg, Chlorobenzene mg/Kg, Chlorodibromomethane mg/Kg, Chloroethane mg/Kg, Chloroform mg/Kg, Chloromethane
mg/Kg, Dibromoethane mg/Kg, Dichlorodifluoromethane mg/Kg, Diisopropyl ether mg/Kg, Ethylbenzene mg/Kg, Isopropylbenzene mg/Kg, Methyl tert butyl ether mg/Kg, Methylene chloride mg/Kg, Naphthalene mg/Kg,
Styrene mg/Kg, Tetrachloroethene mg/Kg, Toluene mg/Kg, Total Xylenes mg/Kg, Trichloroethene mg/Kg, Trichlorofluoromethane mg/Kg, Vinyl chloride mg/Kg, cis-1,2-Dichloroethene mg/Kg, cis-1,3-Dichloropropene
mg/Kg, n-Butylbenzene mg/Kg, n-Propylbenzene mg/Kg, p-Isopropyltoluene mg/Kg, sec-Butylbenzene mg/Kg, tert-Butylbenzene mg/Kg, trans-1,2-Dichloroethene mg/Kg, trans-1,3-Dichloropropene mg/Kg

Analysis Name: EPH ( Soil )
Analysis Description / Method:EPH in soil / MADEP EPH
Container Type / Preservative:4 OZ / NONE
Analytes: C11-C22 Aromatics mg/Kg, C19-C36 Aliphatics mg/Kg, C9-C18 Aliphatics mg/Kg, Extractable Petroleum Hydrocarbons mg/Kg

Analysis Name: Semi Volatile 8270E ( Soil )
Analysis Description / Method:SVOCs by 8270E / 8270E
Container Type / Preservative:4 OZ / NONE
Analytes: 1,2,4-Trichlorobenzene mg/Kg, 2,4,6-Trichlorophenol mg/Kg, 2,4-Dichlorophenol mg/Kg, 2,4-Dimethylphenol mg/Kg, 2,4-Dinitrotoluene mg/Kg, 2,6-Dinitrotoluene mg/Kg, 2-Chloronaphthalene mg/Kg,
Speedway LLC.1/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 50804 Printed: 05/25/2019
2-Chlorophenol mg/Kg, 2-Nitrophenol mg/Kg, 3,3'-Dichlorobenzidine mg/Kg, 4,6-Dinitro-2-methylphenol mg/Kg, 4-Bromophenyl phenyl ether mg/Kg, 4-Chloro-3-methylphenol mg/Kg, 4-Nitrophenol mg/Kg, Acenaphthene
mg/Kg, Acenaphthylene mg/Kg, Benzidine mg/Kg, Benzo(a)anthracene mg/Kg, Benzo(a)pyrene mg/Kg, Benzo(b)fluoranthene mg/Kg, Benzo(g,h,I)perylene mg/Kg, Benzo(k)fluoranthene mg/Kg,
Bis(2-chloroethoxy)methane mg/Kg, Bis(2-chloroisopropyl)ether mg/Kg, Bis(2-ethylhexyl)phthalate mg/Kg, Butyl benzyl phthalate mg/Kg, Chrysene mg/Kg, Di-n-butyl phthalate mg/Kg, Di-n-octyl phthalate mg/Kg,
Dibenz(a,h)anthracene mg/Kg, Diethyl phthalate mg/Kg, Dimethyl phthalate mg/Kg, Fluoranthene mg/Kg, Fluorene mg/Kg, Hexachlorobenzene mg/Kg, Hexachlorocyclopentadiene mg/Kg, Hexachloroethane mg/Kg,
Hexchloro-1,3-butadiene mg/Kg, Indeno(1,2,3-cd)pyrene mg/Kg, Isophorone mg/Kg, N-Nitroso-di-n-propylamine mg/Kg, N-Nitrosodimethylamine mg/Kg, N-Nitrosodiphenylamine mg/Kg, Naphthalene mg/Kg, Nitrobenzene
mg/Kg, Pentachlorophenol mg/Kg, Phenanthrene mg/Kg, Phenol mg/Kg, Pyrene mg/Kg, bis(2-Chloroethyl)ether mg/Kg

Analysis Name: VPH ( Soil )
Analysis Description / Method:MADEP VPH soil / MADEP VPH
Container Type / Preservative:40 MIL AMBER VIAL / MEOH
Analytes: C5-C8 Aliphatics mg/Kg, C9-C10 Aromatics mg/Kg, C9-C12 Aliphatics mg/Kg, Total Volatile Hydrocarbons mg/Kg

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