FA-864_16314_CA_LSA_20070221

I I I I I I I I I I I I I I I I I I I Limited Site Assessment Report A. Site Identification DATE OF REPORT: February 21, 2007 Facility I.D.: 0-011304 UST Incident Number (if known): Site Name: The Pantry #3022 (flea Quick Stop #67) Site Location: 2326 Owen Drive Nearest Cityffown: Fayetteville, North Carolina County: Cumberland UST Owner: The Pantry. Inc. Address: Post Office Box 1410. Sanford, North Carolina 27330 Phone: [phone] UST Operator: The Pantry, Inc Address: Post Office Box 1410, Sanford. North Carolina 27330 Phone: [phone] Property Owner: Marilyn Nelson, c/o The Pantry, Inc. Address: Post Office Box 1410, Sanford, North Carolina 27330 Phone: [phone] Property Occupant:_T=h=e,....,P,._,an=try..,_ . ....,In=c ______________________ _ Address: . Post Office Box 1410, Sanford. North Carolina 27330 Phone: [phone] Consultant/Contractor: SEI Professional Services, P.C. Address: 130 Penmarc Drive. Suite 108. Raleigh, North Carolina 27603 Phone: [phone] Release Information Date Discovered: February 27, 1996 Latitude: N 35.0198° Longitude: __ ...,W'--78=•aa..91 .... 7-=0--· _____ _ Estimated Quantity of Release: ____ u=nkn=o~wn~-----------Cause of Release:_U=S=T"-"'-sy_s=te=m~---------------Source of Release (e.g., Piping/UST):~U~S~T~-------------------Sizes and contents of UST system(s) from which the release occurred): ___________ _ (2) 12.000-gallon gasoline USTs, (1) 6,000-gallon gasoline UST. and {l) 6,000-gallon diesel UST Complete and include in report items B through J in the order listed. I, Chris L. Boggs, P. r; Licensed Geologist (License# 1418) for SEI Professional Services, P.C., do certify that the inform~io~ contai d in this report is correct and accurate to the best of my knowledge. I,·/: / ;;i / / f 1./ I . , . 1-l11 _/ ., .,. ~j. ;. ,· .. :•r·, -. ;: __ .. .., • :, "' ... , . . . . --~-
I I I I I I I I I I I I I I I I I I I B. Risk Characterization Submit the following questionnaire in its entirety. Answer all questions completely. Attach additional pages as needed to fully explain answers. Base answers/explanations on information known or required to be obtained during the Limited Site Assessment. NOTE: Source area means point of release from a UST system. Limited Site Assessment Risk Classification and Land Use Form Part I-Groundwater/Surface WaterNapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non-drinkin~ purposes? YESJNO/ 2. Is a water supply well used for drinking water located within 1,000 feet of the source ~the release? ~/NO There are at least sixteen water supply wells within 1,000 feet that are used for drinking water. 3. Is a water supply well not used for drinking water ( e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of th=~ Water wells within 250 feet have multi-functional use. 4. Does groundwater within 500 feet of the source area of the release have the potential for~ use (there is no other source of water supply other than the groundwater)? llS.'NO However, Cumberland County PWC water mains run along Owen Drive and Cumberland Road. 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? YE@ If yes, describe 6. Are there any other factors that would cause the release to pose an imminent danger to publi~ health, public safety, or the environment? YE~ If yes, describe. Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release? If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YES/NO 8. Is the source area of the release located within an approved or planned wellhead protection are~ definedin42 USC 300h-7(e)? YE~ If yes, describe. 9. Is the release located in the Coastal Plain physiographic region as designated on a map en~ "Geology of North Carolina" published by the Department in 1985? ~O The source area is Black Creek Formation of the Coastal Plain physiographic region, which is considered to be confined. If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of..<.:::::\ drinking water? YE~ 07-DVB-506016, The Pantry #3022, Phase I Limited Site Assessment, February 2007 2
I I I I I I I I I I I I I I I I I I I If YES, describe. 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamin~ levels (see Table 9) established by the Department? YE~ Part II -Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or YE~ temporary)? ~ Describe. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation are~ church, nursing home, or other place of public assembly? YE~ Describe. 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial ( e.g., manufacturing, utilities, industrial research and development, chemica1/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the 1~ undeveloped? ~/NO Describe. Retail asoline and convenience store and active carwash. 4. Do children visit the property? Explain. Children visit the property for short periods while accompanying parents who are making retail purchases or using the carwash. Is access to the property reliably restricted consistent with its use (e.g., by fences, security ~ personnel or both)? YE~ Explain. The ro is an active retail location and does not re uire restricted access. Do pavement, buildings, or other structures cap the contaminated soil? /NO Describe. The parking lot is paved with concrete and asphalt. If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? The property is located in a commercial zone and will likely to remain a retail store requiring paved parking. 5. What is the zoning status of the property? The site is zoned C3 -Hea Commercial 6. Is the use of the property likely to change in the next 20 years? YE Explain. The site will likely remain an active retail store of some type. 07-DVB-506016, The Pantry#3022, Phase I Limited Site Assessment, February 2007 3
I I I I I I I I I I I I I I I I I Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release ( excludes property containing source area of the release): 1. What is the distance from the source area of the release to the nearest prim.my or secondary residence (permanent or tempormy)? Aru,roximately 330 feet southwest to 2939 Cumberland Road and approximately 330 feet southeast to 928 W Mountain Road. 2. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? Approximately 500 feet east to United Pentacostal Youth Center (2403 Owen Drive). 3. What is the zoning status of properties in the surrounding area? C3 -Heavy Commercial District to the north and R6 -Residential to the south. 4. Briefly characterize the use and activities of the land in the surrounding area. The area is a mixed use area of commercial, residential, and vacant lots in the commercial and residential zones. C. Receptor Information 1. Water Suru,ly Wells At least twenty-five water supply wells exist within 1,000 feet of the site; eight water su1mly wells used for drinking are located within 500 feet. Table B-5 summarizes water suwly well information and Appendix C includes the water supply well survey forms. 2. Public Water Supplies Are public water supplies available within 1,500 feet of the source area of the release?@/No If yes, where is the location of the nearest public water lines and the source(s) of the public water supply.(indicate on map) The Cumberland County PWC supplies water to the subject site and surrounding area. Public water mains run along Cumberland Road, Owen Drive, and off select secondary roads. PWC obtains water from Cape Fear River and Glenville Lake. Both sources are beyond 1,500 feet. 3. Surface Water Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the source area of the release. This information must be shown on the USGS topographic map. An unnamed pond is located aru,roximately 1,000 feet northwest of the subject property. 4. Wellhead Protection Areas Identify all planned or approved wellhead protection areas (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the source area of the release. This information must be shown on the USGS topographic map. Wellhead protection areas are defined in 42 USC 300h-7(e). No aru,roved or planned wellhead protection areas were noted within 1,500 feet. 5. Describe Deep Aquifers in the Coastal Plain Physiographic Region (refer to page 19 of the guidelines): The subject site is within the Cretaceous aquifer of the Coastal Plain Physiographic Region, which is considered to be confined. 6. Describe Subsurface Structures (refer to page 19 of the guidelines): There were no basements noted. Subsurface utilities are common in this area. 7. Property Owners and Occupants Attach Table B-6, listing the names and addresses of property owners and occupants within or contiguous to the area containing contamination and all property owners and occupants within or contiguous to the area where the contamination is expected to migrate. Table 6 summarizes property owners and occupants contiguous to the subiect property. D. Site Geology and Hydrogeology Describe the soil and geology encountered at the site. Discuss the effects of soil and geological characteristics on the migration and attenuation of contaminants. Include information obtained during assessment activities (e.g., lithologic descriptions made during drilling, probe surveys, tank closure, 07-DVB-506016, The Pantry #3022, Phase I Limited Site Assessment, February 2007 4
I I I I I I I I I ii I I I I I etc). If a Phase II investigation is required include a discussion of groundwater flow direction and hydraulic gradient (vertical and horizontal). The source area is in the Black Creek Formation of the Coastal Plain physiographic region, which is considered to be confined. According to the Geologic Mm;> of North Carolina {Brown, et al., 1985), the Cretaceous aquifer of the Black Creek Formation is characterized by clay, gray to black, lignitic: contains thin bed and laminae of fine-grained micaceous sand and thick lenses of cross-bedded sand. During the installation of monitoring well MW-1, soil samples were collected every five feet using a properly decontaminated s;plit s;poon. The soil encountered while performing the soil boring was white, tan, gray, and orange silty sand to twenty feet below land surface (bls). Groundwater was encountered at m,proximately thirteen feet bls. Table B-8 is a groundwater elevation map from the January 22, 2007, groundwater sampling event E. Sampling Results Phase I and Phase II Investigation I. Describe all soil sampling performed during the installation of the source well(s) (use maps and tables whenever possible). On January 18, 2007, during the installation of monitoring well MW-1, two soil samples (SS-1 (5') and SS-1 (10')) were collected for laboratory analysis. The samples were placed into a laboratory supplied, clean container, sealed with a Teflon lined cm,, placed in an iced cooler, and maintained at 4 °C. The soil samples were submitted under chain-of-custody procedures to Accutest Laboratories, Southeast in Orlando, Florida, for laboratory analysis. The soil samples were analyzed by EPA methods 8260 and 8270 and MADEP methods VPH and EPH. Petroleum constituents were not detected at concentrations above laboratory detection limits. Figure 4 presents a site map showing soil sample analytical results and summarized in Table B-3. A copy of the laboratory report and chain-of-custody form is included in Appendix C. 2. Describe any groundwater sampling from the source area monitoring well(s). Use maps and tables whenever possible. On January 22, 2007, groundwater monitoring well MW-1 was sampled. Prior to sampling. the monitoring well was gauged with an electronic oil/water interface probe to measure depth to water and to detect any free product Free product was not detected in the monitoring well. The monitoring well was purged prior to sampling by removing a minimum of three well volumes of 07-DVB-506016, The Pantry #3022, Phase I Limited Site Assessment, February 2007 5
I I I I I I I ·I I I I I I water, or until the well went dry. After allowing sufficient time for recharge, representative groundwater samples were collected using new, di§Posable Teflon® hailers. Samples were placed into laborat01y supplied containers, sealed and labeled, maintained at 4 ° Celsius and submitted under proper chain-of-custody procedures to Accutest Laboratories, Southeast in Orlando, Florida for analysis. The groundwater samples were analyzed by EPA methods 601, 602 (with IPE and MTBE}, 625 BNA + TICs, and 504.1 for EDB, MADEP methods VPH and EPH, and standard method 3030c for lead. Petroleum constituents were not detected above laboratory detection limits in monitoring well MW-1. Monitoring well MW-3 contained the highest concentration of carbon tetrachloride (7.6 µg/L) for which there is not an established limit. Monitoring well MW-1 contained concentrations of bromodichloromethane (1.6 µg/L), dibromochloromethane (0.63 µg/L), and p-isopropyltoluene (2. 7 µg/L) for which there are not established limits. Lead was not detected above laboratory detection limits. Figure 4 presents a site map showing groundwater sample analytical results and summarized in Table B-4. A copy of the laboratory report and chain-of-custody form is included in Appendix C. 3. Monitoring well construction information On January 18, 2007, one (MW.I) type Il monitoring well was installed. Monitoring well MW-1 was installed to a depth of twenty feet bls and completed with ten feet of 2 inch Schedule 40 PVC casing and ten feet of 0.010-inch slot PVC screen. The annulus of the type II well was filled with a sand filter pack to two feet above the top of the screened interval. A two-foot thick bentonite seal was placed above the sand filter pack and hydrated with water. The remaining well bore was filled with grout to the surface. The well was completed flush to grade with a locking cap, watertight seal, and a bolt-down manhole. Table B-7 summarizes monitoring well construction infonnation. Boring Logs and Monitoring Well Construction Records are included in Appendix A. F. Conclusions and Recommendations Discuss the risk criteria that apply to the release and identify any other site-specific factors related to the release that may pose a risk to human health and the environment. Also, discuss any site-specific conditions or possible actions that could result in lowering the level of risk posed by the release. The subject property is zoned C3 -Heavy Commercial District and potential future use indicates that it will remain at that status. A 1,500-foot radius potable well search was performed, which revealed 07-DVB-506016, The Pantry #3022, Phase I Limited Site Assessment, February 2007 6
I I I I I I I I I I I I I I I I I I I the presence of at least twenty-five water supply wells exist within 1,000 feet of the site: eight water supply wells used for drinking are located within 500 feet. Cumberland County PWC supplies public water to the site and the surrounding area. During the January 18 2007, soil sampling event, petroleum constituents were not detected above laboratory detection limits. During the Janumy 22. 2007, groundwater sampling event, petroleum constituents were not detected above laboratory detection limits. Based on the information presented above, the subject site should be ranked high risk and have a residential land use classification. SEI Professional Services, P.C. recommends that a Notice of No Further Action. G. Free Product Investigation/Recovery (if applicable) If free product is still present or is discovered during the limited site assessment, continue or begin free product recovery immediately in accordance with 15A NCAC 2N. 0705 and submit an up-to-date Free Product Recovery Report (Report B-4). Free product was not detected on site during limited site assessment activities. H. Site History: According to a June 4. 1998, Phase I Environmental Site Assessment Report (ESA): "A review of NCDENR files indicates that a gasoline release was reported on Februmy 27. 1996 during construction in the NCDOT right-of-way. Four USTs, installed in 1983, were removed as part of the construction activities. Petroleum contaminated groundwater was encountered, and incident number 16314 was assigned to the site. The site has been ranked 50/E. The most recent report in the file was a UST Closure Report dated January 7, 1997, indicating soil contamination." A copy of the February 12, 1996, Preliminmy Assessment Report was included in the Phase I ESA. The DOT collected 14 soil samples that came back BDL and one contaminated groundwater sample. A copy of the January 7, 1997, UST Closure Report was included in the Phase I ESA. The DOT collected 12 soil samples. Four were above reportable concentrations. On December 7, 2006, NCDENR issued a Notice of Regulatory Requirement <NORR) requesting a Limited Site Assessment LSA. On January 18, 2007, SEI Environmental Inc. installed a groundwater monitoring well in the source area of the release. Soil samples were collected every five feet until encountering groundwater. Petroleum constituents were not detected above laboratory detection limits in neither soil nor groundwater samples. 07-DVB-506016, The Pantty #3022, Phase I Limited Site Assessment, February 2007 7
I I Table B-1 summarizes UST system information and Table B-2 presents UST owner/operator information. Table B-6 list surrounding property owners and tenants contiguous with the subject property. L Figures (Please attach the following figures) FIGURE 1 FIGURE2 FIGURE3 FIGURE4 FIGURE 5 USGS Quadrangle Map Vicinity Map Site Map Surrounding Property Owners Soil and Groundwater Laboratory Analytical Results I J. Other Information (Please attach the following information) I I I I I I I I TABLES TABLEB-1 TABLEB-2 TABLEB-3 TABLEB-4 TABLEB-5 TABLEB-6 TABLEB-7 TABLEB-8 APPENDICES APPENDIX A APPENDIXB APPENDIXC Site History -UST System Information Site History -UST Owner/Operator Information Soil Sample Analytical Results Groundwater Analytical Results Water Supply Well Information Property Owners/Occupants Monitoring Well Construction Summary Groundwater Elevation Data Boring Logs and Well Construction Records Water Supply Well Surveys Laboratory Analytical Reports 07-DVB-506016, The Pantry #3022, Phase I Limited Site Assessment, February 2007 8
I I I I 0 ._: rt) ...J ~ ~ • • • • • • • • • • /e / • • • • \ \ \ \ \ \ \ --------LEGEND: • WATER SUPPLY WELL 200 400 FT. SE I Professional Services, P. C. 5100 Reagan Dr., Suite 5, Charlotte, NC 28206, Ph# 704-597-4022 FIGURE 2: VICINITY MAP QUICK STOP #67(AKA THE PANTRY #3022) 2326 OWEN DR. FAYETTEVILLE, NC w.o. #: 506016 DWG #: PA3022F1 DATE: 2/19/07 DRAWN BY: JCJ
I I (I) DUMPSTE □ STORE ~POWER POLE W/TRANSFORMER ASPHALT \_ CURRENT UST PIT r--.r-•r--i.r---, 1 ,, Ii 11 I I\ \\ I\ I Ii Ii \J I I \\ Ii \\ I 10110011 I I Ii Ii Ii I 1..._11..._11..._11..._1 D DD DISPENSERS D DD CANOPY I I I I \ I I \ I I I I I I I I \ \ I I I \ \ I \ I \ \ I \ I \J CUMBERLAND ROAD 0 20 40FT. APPROXIMATE SCALE SEI Professional Services, P.C. 5100 Reagan Dr., Suite 5, Charlotte, NC 28206, Ph# 704-597-4022 FIGURE 3: SITE MAP THE PANTRY #3022 2326 OWEN DR. FAYETTEVILLE NC WO #506016 DWG #PA3022F3C DATE: 1 /22/07 DRAWN BY: JCJ
I I / / / / LEGEND: -----• WATER SUPPLY WELL 0 100 200 FT. ----------WOODS SE I Professional Services, P. C. 5100 Reagan Dr., Suite 5, Charlotte, NC 28206, Ph# 704-597-4022 FIGURE 4: SURROUNDING PROPERTIES QUICK STOP #67(AKA THE PANTRY #3022) 2326 OWEN DR. FAYETTEVILLE, NC w.o. #: 506016 DWG #: PA3022F4 DATE: 2/19/07 DRAWN BY: JCJ
I (I) DUMPSTE DRAIN~ □ STORE \_ POWER POLE W/TRANSFORMER CARWASH ASPHALT \ \_ CURRENT UST PIT r--ir--,r--ir--. 11 11 Ii I I Ii II ii I I II II II I I II Ii II I 10110011 I I II II Ii I L._IL.-IL...-IL..._I D DD DISPENSERS \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ I \ I \~ \~ ,-P \~ \~ \ \ \ \ \ \ I \ I \ \ \ I I I \ \ I \ \ \ \ \ \ I \ I I I I \ I \ DOT GW SAMPLE B 499 ug/L T 379 ug/L E 422 ug/L X 683 ug/L 02/1996 \ I \ I \ \ \ \ I \ \ I \ \J \ \ \ \ \ ' I I I I I \ \ ___ S~O_IL __ --1GROUND r--+--'5--'-F--'-T-'---. -----+--..:....:1 O'""'F---'T--'---. --1--'W:...:..:...:AT.:....:E:.:R--'----< DIESE B <0.0023 <0.0022 <0.50 DISP D DD T <0.0023 <0.0022 <0.50 E <0.0023 <0.0022 <0.50 X <0.0058 <0.0166 <1.0 MW-CANOPY HIGHEST CONC. SOIL SAMPLE ._: ', \ GRO 4600 mg/kg '-, , '-\ ORO 385 mg/kg v '-':.._, ) \ 11/20/1996 / '-, '-V \ / '-/ -=======GRASS======-===--_ ( FIBEROPTIC ____ ~--------,_ __________ _,, WATER LINE~------------)--------------/ FORMER UST PIT \ ------------------I CUMBERLAND ROAD NOTE: SOIL SAMPLED 1-18-07, UNITS ARE mg/kg. GROUNDWATER SAMPLED 1-22-07, UNITS ARE.ug/L. 0 20 40FT. APPROXIMATE SCALE SE I Professional Services, P. C. 5100 Reagan Dr., Suite 5, Charlotte, NC 28206, Ph# 704-597-4022 FIGURE 5: SOIL AND GROUNDWATER ANALYTICAL DAT THE PANTRY #3022 2326 OWEN DR. FAYETTEVILLE NC WO #506016 DATE: 1/22/07 DWG #PA3022F4C DRAWN BY: JCJ
I I I I I I I I I I ·I I I I I I I I I . USTID Number 1 2 3 4 5 6 7 8 TABLEB-1 .. , .,, -, .. ,., ,, .. ', ,-·-.·' Site History US'f Systemlnforrtuttion ' . . . Quick ~top.~617.(aka The Pantry #3022) .. . . . . Z,3ZfQwen I>rive \. . .. . .. ·. · Fayetteville, Cu~befland .Counzy, North <;aro_lina28306 · , Facilit)r,IJ> N)1JJ1ber: ~01qo4 · ·. Incid.ent Number; 16314 SEI ProJect~umbef: 506016 .• Product Capacity Date Permanent W~s ·Rele~se (gallons) Installed Closure Date Associated. Witll . ·or UST System~ Curre._~Iy in.Use (YIN) Gasoline 12,000 05/07/1983 11/20/1996 y Gasoline 12,000 05/07/1983 11/20/1996 y Gasoline 6,000 05/07/1983 11/20/1996 y Diesel 6,000 05/07/1983 11/20/1996 y Gasoline 10,000 09/01/1996 In Use N Gasoline 10,000 09/01/1996 In Use N Gasoline 10,000 09/01/1996 In Use N Diesel 10,000 09/01/1996 In Use N
I I I I jl I II I II 11 II I I I I I I I I I TABLEB-2 s~~e IIi~tory lJSt ()wlier/Operatorlnformation Quick Stop #67 (ak21 The fantry #3022) 2326 Owen.Drive Fayetteville, C11m1>~r,~n~ (:)c,11J1t)', :N()fth _Carolina. 2~306 Faci)ifl' lJlN11mber: ()-011394 · Ipcident Nu111ber:l6314 SEl Pro~ect Numl>er: 50()016 UST ID .Pates of Name of Owner Ol'_ Operator' ' Nwnber · 0w:nersliip / Operation 1 05/07/83 to 11/20/96 Quick Stop Food Mart, Inc. Address·-· POBox2427 Fayetteville, North Carolina 28302 , l,JSJ?-ffi -D~t~~-pf ---, N'~h;et _ QWbetship'/ Opertttion 2 05/07/83 to 11/20/96 Quick Stop Food Mart, Inc. Address POBox2427 Fayetteville, North Carolina 28302 usrip oaie$,,,qt · -Nullibef __ Own~rsliibf()neralti.011. 3 05/07 /83 to 11/20/96 Quick Stop Food Mart, Inc. POBox2427 Fayetteville, North Carolina 28302 JJST-1:1) Dttt~:~t Number. _ Own~rshfo l Oi>eration _ 4 05/07/83 to 11/20/96 Quick Stop Food Mart, Inc. POBox2427 Fayetteville, North Carolina 28302 us:rm Number Oat~$ i>f ----Nijm.e c,f ~~t gl'(;)p~ri,.t<ir OwnersJiipJ Onet-•tion __ 5 09/01/06 to Present The Pantrv, Inc. PO Box 1410 Sanford, North Carolina 27330 Owner or Operator? Both [phone] Both [phone] Both [phone] Both [phone] Both [phone]
I I I I ·1 ii I 1• I I I I I I I I TABLE B-2 (continued) Site Histo,ry UST Own.er/Operator Information Quick Stop #67 (a~ The Pantry #3022) .·• . .·.··. 2326/Qwenurii'~i. . .. ·· . · · Faye~evilfo, (J~in.berl~nd:Cou11ty,North Carolina ~8JQ6 : F~cwty 'Ill Nt1niber: O-OH304 _ . . ''. . USTID Number 6 usrnf N UJJibef 7 :Oates of Qwn,ershi 09/01/06 to t>ides~J Ownenln 09/01/06 to · usT m.-Qj.~~ ijf t~iunber. . . Qwijtl;Sm 8 09/01/06 to In.cidentNumber: 163. l.4. S~I Pr()Jkct Nlimber:506016 Owner or Q~ehttor? .. Present The Pan , Inc. Attaies$ PO Box 1410 Sanford, North Carolina 27330 Present The Pan , Inc. Both -iactr$s , -Tete hone N'-.mber PO Box 1410 [phone] Sanford, North Carolina 27330 Present The Pan , Inc. Both A:id~~s$ •• · 'I'ei~ b.ort~ Nimtb~t · PO Box 1410 [phone] Sanford, North Carolina 27330
-------------------I• TABLE B-3 Soil Sample AnalyticalResults Quick Stop#67 (aka ThePantry#3022) 23260:wen ·.fitive Fayetteville, Cumberland County/North CaroUna.28306 FacilitfJUNuJtlb~r: (E0J,1304 -Incident Number: 16314 SEI Project Number:•506016 ,Dat~ Sampled: JanuarylS,.2007 l --~• -~ "'-I G.I. .~ = i=. 4,1,;-,.;. ;-5~ _Jil~ -~ -Q,I ... 0 0·.~ ll ~i r:,i, =l i=. :c 41 l ==···~ r-it ffi 5 Q,I Q,I ~! -~ =r ,c: .DJ) ~ Cl) e.= a 171 0 =---;. a -; a . ~-! .~ I ~--= --.... .._,,,,, -..... 0 171 J;i;l ~ I SS-1 5 <0.0023 <0.0023 <0.0023 <0.0058 <0.0023 <0.0023 <0.0023 10 <0.0022 <0.0022 <0.0022 <0.0166 <0.0022 <0.0022 <0.0022 Soil-to-Groundwater 0.0056 7.3 4.6 5.0 0.92 0.37 0.000002 MSCCs Residential MSCCs 18 3,200 1,560 3,129 213 156 0.0075 ppm -parts per million mg/kg -milligrams per kilogram Bold denotes concentrations above the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCC) CI -Considered immobile 41 ~·: ·c ·o :a· .. · U•~ 41 t 5 a i-41 .. ~. r,J "'-I r,J ~ ~ ~ :c :c :c =i: = .. = -= -i.-,••=t-fi.~.· -~1.· ...•••. ~.i. QC a M S OIO a-u'-' ..... --..-I'-' -... u . u Ir) ·rJ... r.J..· u u u 0.0186 <3.3 I <2.5 I <7.0 0.0184 <3.3 I <2.5 I <7.1 0.02 72 3,300 85 939 9,386 C ~ ,,:: :c = =·-. ;:I .. -· . e -Q. 'o! .. 0 :Cll :-=!. ·-~.·-."" ~ • -< .~ < Cl) -.e· •ei = a ~·· ..e ..-I -U· U .. I I 0'I al ... ·u u . C :c = ~ii-·., ... ·•--<,· ,,_ N er O= I .-I .-I u <7.0 I <0.82 I <7.0 <7.1 I <0.82 I <7.1 CI 34 93,860 469
-------------------·aa r= "ai a= = ~ .vi .• ...;i ~·. 5~ .mi! =--~ Q,l -=~ l ! = ·-E-i ,_ :S 1f ~-· ,s ~ TABLEB-4 Groundwater .Analytical.Results Quick Stop #67 (aka The Pantry #3022) .2326 OwenDrive Fayetteville, Cumberland County, North Carolinal8306 Facility ID Number: 0-011304 IncidentNumbet: 16314 SElProjecfNumber: ·506016 .'I-" ·~ = ~-~···~· ~· bJ) -:s. = -¢ E-DateSainpled:.January 22,2007 =~ E-t· bJ) ~~· -t: ~ "'"' :s. -=-~··~ ·~·•-o "Cl.,...., =~ Q,l bJ) ~ :s. -"'-l ·CJ ·-= ,a_ ~.• .. ~ ~ ! oc-u .Ji u "'-l -~ -:c J ~•;,-,.. ~·~ N ::::l. 1""(-u rJ.. u "'-l ~ of ;,Cf, ~·•··~ 00 :s. .... -t ~ -:c J ~-•• ~i~ · 1.0' :s. f")-~ .... u MW-1 <0.50 I <0.50 <0.50 <1.0 <0.50 <0.50 I <0.0093 <5.0 <50 <30 I <190 I <190 2L Standards 1.0 I 1,000 550 530 200 70 I 0.0004 10x2L Standards 10 10,000 I s,sso I s,Joo I 2,000 700 GCLs I 5,000 I 257,500 I 84,500 I 87,500 I 200,000 I 70,000 µg/L -micrograms per liter Bold denotes concentration is greater than the 15A NCAC 2L Standard GCL • Gross Contamination Level NE -Not established 0.004 50 15 420 4,200 I 42,000 150 4,200 42,000 420,000 15,000 NE NE NE "'-l I-~ = .e =-:a...~ ~ bJ) = ,:S. ..... -u I rJ.. 'U "'-l w ',C a = -· <~ ~.~ u I .... .... u <10 I <140 210 2,100 NE
-------------------TABLE B-5 Water Supply Well Information . Quick Stop #67 (aka ThePantry#3022) i• 2326 Owen Drive · I• Fayetteville, Cumberland County, North Carolina 28306 I·-Facility IDNumber:0-011304 Incident Number: 16314 SElProjectNumber: 506016 · .. '. ' ~ ~ .·• _,s. ~ = ,r,.,. ' Q., i:-::s ~ = 4,1 i .~ .· .: lo. .c' ~ =·o,) --~ -·~ -,4,1· .c ~--;.-.. ..... o,) ~ = .o,), § 4,1_ ..,._,_ ---~-~:i a,~ -•--1 :ft; I·: ~ o,) fr.!4 ·"'2 ~-.!: j;;;) ·Oil-= I: .. ~e 'S .·· et.c = .c = r. ... at:a ·4,1 I : "d z = .. , ... 2Lt J:; .... t ... ---·~ =· -~ .. 4,1 4,1 = t ~ ·"' •4,1 ~ = e . ;.:Et_ . ~--= -~ ·--~e C. -~•-·.•·~ --i~ .4,1 ~<-~ ~ ; = i Q ..... = 4,1 "f •'·c!::·· .. ;.C1 ~ = i s; c.. .· ~ 0# ~ s u ,, .· .· 5 . Martha Faye Koonce 2939 Cumberland Rd 910-485-6253 Drink UK UK UK UK ~330 SW 12 Tim Pittman 927 W Mountain Dr UK Drink UK UK UK UK ---440 SW 13 Jose V alvere 925 W Mountain Dr 910-425-7960 Drink UK UK UK UK ~460 SW 14 ThyWell Tyler 923 W Mountain Dr UK Drink UK UK UK UK ~560 SW 15 Henry & Sarah Goins Life Estate 928 W Mountain Dr 910-433-0722 Drink UK UK UK UK ~330 SE 16* Champ Goins, c/o Mary Myers 926 W Mountain Dr UK Drink UK UK UK UK ~370 s 17* Henrv Fairfax 924 W Mountain Dr 910-485-6895 Drink UK UK UK UK ---440 s 18* Bienvenido & Nancy Mendez 922 W Mountain Dr 910-485-3613 Drink UK UK UK UK ~540 s 20 Zonnie Mae & Aretice Wright 3012 Dyke St 910-483-3664 Drink UK UK UK UK ~440 SE 21 James & Clara Barton 3016 Dyke St UK Drink UK UK UK UK ---480 SE UK -Property owner does not know information or information not available. * Data obtained from The Pantry #3170 (Incident 3559) December 18, 2006, Groundwater Monitoring Report and verified by site visit.
-------------------TABLEB-6 Property Owners/Occupants I QuickStop#67(aka The Pantry #3()22) ,, ' 2326 Owen Drive Fayetteville, CumberlaiJ.d County;North Carolina:28306 · . .• Facility ID Numb.er: o .. 011304 Indde:n.fNumber:16314 Parcel ID N ufubers begin 0426 SElPtoject NUlllbet: 506016 . . .
. .· ... ; ·. Map#. J>arcfl Property· PtopertyOwner/ Tenant . ID# Address . MaiJine.Addt.ess .. .· Sub 41-9941 2326 Owen Drive Marilyn Nelson, c/o The Pantrv, Inc., P.O. Box 1410, Sanford, NC 27330 The Pantry #3022 1 52-5774 2830 Cumberland Road Carolina Power & Light Co., P.O. Box 1551, Raleigh, NC 27602 Progress Energy Substation 2 51-5895 2403 Owen Drive United Pentecostal Church of Fayetteville, Inc., P.O. Box 64277, Fayetteville, NC 28306 Youth Center 3 51-3722 Owen Drive Global Development Corp., P.O. Box 47, Fayetteville, NC 28302 Parking 4 51-1657 W Mountain Drive Metes & Bounds, LLC, 401 Forest Lake Rd, Fayetteville, NC 28305 Vacant Lot 5 41-8680 2939 Cumberland Road Martha Faye Koonce, 2939 Cumberland Rd, Fayetteville, NC 28306 Same 6 41-7906 2940 Cumberland Road James P & Esther Dees, 2944 Cumberland Road, Fayetteville, NC 28306 Same 7 41-7812 2952 Cumberland Road Sue H. Lockamy, P.O. Box 42551 Fayetteville, NC 28309 Residential 8 41-6729 2960 Cumberland Road Shirley Dees & JL Trogdon, 3112 Cumberland Rd, Fayetteville, NC 28306 Residential 9 41-5907 2968 Cumberland Road Lewis G. & Harriett F. Carventer, 3116 Cumberland Rd, Fayetteville, NC 28306-2426 Residential 10 41-7568 2951 Cumberland Road Derb S. Carter, 417 Devane St, Fayetteville, NC 28305 Vacant Lot 11 41-7459 3103 Bolton Street Malgram D. & E. Hutchinson, 3103 Bolton St, Fayetteville, NC 28306-2814 Residential 12 41-9510 927 W Mountain Drive Tim Pittman, 927 W Mountain Dr., Fayetteville, NC 28306 Residential 13 41-9414 925 W Mountain Drive Jose Valvere, 925 W Mountain Dr., Fayetteville, NC 28306 Residential 14 41-9318 923 W Mountain Drive Thywell Tyler, 923 W Mountain Dr, Fayetteville, NC 28306-2812 Residential 15 51-1556 928 W Mountain Drive Henrv N & Sarah J Goins Life Estate, 2419 Downing Rd, Fayetteville, NC 28301 Residential 16 51-1449 926 W Mountain Drive Champ Goins, c/o Marv Myers, 2517 Cumberland Rd, Fayetteville, NC 28306 Residential 17 51-1442 924 W Mountain Drive Henry Fairfax, 924 W Mountain Dr., Fayetteville, NC 28306-2813 Residential 18 51-1334 922 W Mountain Drive Bienvenido M. & Nancy T. Mendez, 922 W Mountain Dr., Fayetteville, NC 28304 Upholstery 19 51-3631 2400 Owen Drive Global Development Com., P.O. Box 47, Fayetteville, NC 28302 Advance Auto 20 51-3439 3012 Dyke Street Zonnie Mae & Aretice Wrililit, 3012 Dyke St., Fayetteville, NC 28306 Same 21 51-3337 3016 Dyke Street James P & Clara G Barton, 3016 Dyke St, Fayetteville, NC 28306-2807 Residential 22 51-5556 2410 Owen Drive DS Carter, 417 Devane St., Fayetteville, NC 28305-5204 The Pantry #3170
I I I I I I I I I I I I I I I I I I I TABLEB-7 . Monitor1iig.Weff.C<,mitr11ction Sutrimary . Quick StQp ##(>7 (11lqlJ'he ):la~try #30i2) . 23260wenDrive . .. · F~yetteville,· {;1JJI1IJerla~A Coqnty, Nprt,ll CarQlina 28306 FaciJityJI) l~u)ll.ber: 0-911304 • In~ide,tNumb.er: 16314 .. · ~EI Project :N"uPlb~r: 506016 Date Total ·Screen · .Date Monitoring Well Installed Depth Interval Abandoned feet bis. feet bl~ MW-1 01/18/07 20 10-20 NA
I I I I I I I I I I I I I I I I I I I Well Location MW-1 TABLEB-8 His.toric.·• al Qtoundwitter Elevation Data ', .. ,· .. : , .... , . ,· ' . . . ... :•. Q11icllStop ~67(aka. T.11.f 1>antry#3oi2) .· .· .. ·•·. 2326 OwenD.rive < · ..... · Fayetteville, Cu1J1b~rlan4 County, N~rth-Carolina 28306 Facility ll) Nu111~er: -~011304 Jnc~~ent Number: 16314 . . Sa01ple Date 01/22/07 SEI Project Nuni~er: ~06016 . · Top of Casing Elevation (feet)* 100.00 Depth, to Groundwater (feet) 11.17 Gro·undwater l:levation (feet) 88.83 * Based on arbitrary datum of 100 feet
I I I I I I I I APPENDIXA I I I I : I i i JI i I I I ;I I
- --... 11111 ---- --------Boring Log and Type 11 Well Construction Details WELL IDENTIFICATION: MW-1 DATE DRILLED: 01/16107 STATE PERMIT#: ________ WORK ORDER#: 506016 PROJECT NAME: Quick Stop #67 (aka The Pantry #3022) SITE ADDRESS: 2326 Owen Drive, Fayetteville, NC LATITUDE: _______ LONGITUDE: _______ _ TOP OF CASING ELEV.: ____ LAND SURFACE ELEV.:~--r DEPTH TO WATER ....:12.n. SCH 40 PVC RISER REMOVEABLE STEEL COVER 1,, ,>-\' b 1,.,_:, -c-:~ ·~· [P·; .,; ·---. 7..2...FT. 2... FT. y 1>:1=-=T ly ::>:::· ~---~ :::•>: Ls,N. 21N. TOTAL DEPTH OF WELL 20 FT. DRILLING METHOD:~ ~H~ol~low_S_t_em~A~ug_e_r __________ _ SAMPLING METHOD:_S....:.pl_it_S....:.poo_n ____________ _ GRAVEL PACK SIZE:_,2=0"-(4=0_,S°"il=ica=-=s=an""'d'-------------SLOT SIZE: 0.010 inches COMMENTS: ---------------------? :r Ii: 0 SAMPLE BLOW t) ► OVA UNIFIED DESCRIPTIVE LOG Ul NUMBER COUNT UJ It: (ppm) METHOD C Cl: Ul Asohalt· tan sand fill 5 White & tan sand 10 Gray & tan sand 15 Tan & orange sand 20 End of bore 25 - -I I
I I I I I I I I I I I I I I I I I I I NoN REs1DHNTIAL WELLc.oNsnuCTioN RECo:a» North Carolina Dq:,artment or Em1ironme1n and Natural Rm>u~-Division of WIJJ:r Quality ·WELL CONTRACTORCERTlFICATJON # 2428 ..;;..;,;;.;;.. _______ _ 1. WEU. CONT~CTOR: Ray Rogers Well Cantrador (Individual) Name SEI Environmental, Inc. Well Contractor Company Name STREET ADDRESS· 130 Penmarc Dr., Suite 108 Raleigh NC 27603 City or Town Stale ZlpCode 1 919, >-832-2535 Alea coae-Phone number Z. WELL INFORMATION: srr~ we:LL 10 "(11 applicat)lel M W -\ STATE WELL PERMIT#(U applie:able.,_ _______ _ DWQ or OT.HER PERMIT #{if appir:able) ______ _ WEU. USE.(CheokAppllc:able BQQc) Mcnitoring ~ Mt.sn~blic 0 lndustrial/CommerclalO AgriaultutalO Recawiyo lryectianO lrrigliliPllCl Other O {list USlt) ________ _ CATE DRILLS> I · IS· 01 TIME COMPL....e-reD. ______ AMO PM□ 3. Wet..L LOCATION; CITY: J:'(.\ '# E:I't}; " I L..L€cou . ~ (S,,-eet Name. Numllltni, Commul!ily, Subdivlllion, Lot No,, Pall:iil. Zip Coda) TOPOGRAPHIC/ LANO SETTING: □Slope □Vaiey ~ ORidge Cl 01her _____ _ {chedt ~riate bc1cj LATITUDE J.. 5_ 0/ 'ff!; Mayb¢m~ ininutes, seconds Of l..ONG1TUDE ::J_ Ji 'if 70° inadecimaHorma1 Latitude/longitude sourci:: 1'0PS □Topographic map (location of_, must be sh~ ona USGS topo map 1111d attached to this fOml I" net using GPS) 4,. FACIJ..fTY.,. a.-otlhil DIMillNll-tdil&ftll •-· FAClUTYlO#(ll'appRcable) D: 011304 NAME OF FACILITY Uh:, 'rfr4TR.':f 302. '-STREET ADDRESS 7,g 2 /9 ~£1J 1::£. FA'I c.:n:e;v 1µ.e: N c. Cify or Town Sta1e Zip Code CONTACTPERSON'J<6N~ ~S MAILING AOORess:r:tts: P&,J11Z-'1 , Po &ox t'-k 0 :Qg..\ij:,(23> · b)c.. ' -ZZ3to City or Town Stat.9 Zip Code ,q 19 r774-lo700 Al1l2 eocie • Phone number 5. WELL OET Alt.S: ,.,D I a. TOTAL DEPTH:_...:;~__,;;;,_... __ b, DOES WeU. REPUCE !OOSTING WEJ..L'? YES □ NCC c: .• WATl'=...R LeVeL Below Top of casing; / ?:/ FT. . {Un•+• If Above Top'Of Casiog) d. TOP OF CASING IS Q ·FT. AtxMi IJlnd Surface• "Top of casing ermin:aUlld al:lcr below land sUlfce may requn a variance in ~wltt'I 15ANCAC 2C .ll118. e. YtELo tgpm): METHOD OF TEST f. D!SlNFeCTlc»f: Ty~ Amount g. WATER ZONES (depth}: Frtm __ fo __ From __ To From __ Tc __ Fram __ .To Fram __ To __ From_. __ To __ 6. CASING: Thickness/ Depth Diameter Wtilgnt Mat«lal From_O_·Tc~Ft. 2" Sch.40 --Ftom_. -· _To __ Ft, 6" --Sch.40 Frcm __ To __ FL -7~ GROUT.: Oep1h Material Me.thocf Frarn_Q_ ro__L Ft. Frcm ___ ,o_Ft. Frcm __ To_Fl 8. SCRSEH: Depth Diameter SllltSiZe Malerial From-1.SL To 2 0 Ft._2_in. 0..:Q.!Q_ in. Sch. 40 Fn:xT1 __ To __ Fl __ in. in. From_ ro_Ft. __ in •. __ ii\, !!. SAMOIGRAVEl. PACK: Depth ~ t.tatena1 From ~ Tc 2.D Ft ~ Fra-n To __ .,=i Fnim_To __ Fl 10. I>RIWNG LOG From To Fonnatlon Description tt ~~t-~·~ eze....., l TibJ s o-J)a ~~~c.~ 2:0 H. RSM.ARKS: ~'-!,, :6~~ -rn 11.:h ' c:: I 00 MER£9YCERTIFY THAT Tl1IS WEU. WAS C0NSTIUJC1a),t ACCORIW(C£WJTM 1$A 1¢1,C 20. WW.~ STAHt)Ml'JS. ANOTKAT #, CCPV OF Tl4IS R!eoRO HAS8£!H FRO'IIIOE.0'101HE Wl!U. OWHeR. SIGNATURE OF CERTIFIED WEU. CONTRACTOR DATE Ray Rogers PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Ouaflty within 30 days. Attn: Information Mgt., 1617 Mail Service c.nter-Raleign, NC 2.7699-1$17 Phone No. [phone] ext 568. FormGW•1b Rev. 7/05
I I I I I I I I APPENDIXB I I 11 I I I I I I I 1· I
Sl>f:> (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendine; Incident Name: The Pantry #3022 --., I I I I I I I I I I I I I I I I I I I Please Provide the Followin~ Information (to the best of your knowled2,e) Name and telephone number of person completing the survey T'ft: ~'1i2-L( Address of property receiving survey ~ -Z.:Z.u, Ot,je)J "T)f: City 'C', ·ne County Cumberland --Wh~f source ~~ur drinking water? _, Public Water ater Supply Well/ Stream Intuce / Other(:please explain below) ~ / '" ---Is there a water supply well on this property? Yes /No)If"No" disregard remaining questions and return survey '--"' .. · Name and address of owner(s) of property with water suoply well How many water supply wells are on your property? ,What is the well(s) used for? (check all that apply) Drinking -• Irrigation , Swimming Pool . Water Livestock , Other (specify) , y OU do not use the Well How many residences are connected to the well (list addresses below)? --How deep is the well( s )? Date well was installed? What is the casing depth of the well{s)? What is the screen interval of the well( s )? Additional water supply well information: . (This part to be completed by Responsible Party or their representative) ' . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to ( Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleimi, North Carolina 27603-24 70 ·'3. Telephone t'Consultane's Telephone Number) · [phone] or {800) 474-7049 4. E-mail to (Consultant's E-mail Address) dparker/alsei-environmental. com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] ·-.. ~ ,, . ~--
5 (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendine: Incident Name: The Pantry #3022 -; Please Provide the FQJ.lowi.rullnformation (to the best of your kno}Vle~e) Name and telephone number of person completing the survey AM; Y t:r,.J ~ ("!1 o V-fB'S ... 1,;y;~ Address of property receiving survey 2. q 3 q t'.A hv\~~ ' / City Fayetteville -. County Cumberland / -~ ,. What is the source ~ drinking wjer? Public Water/. ater Suooly We / Stream Intake/ Other (olease exolain below) \ / '----~ Is there a water supply well on this property? Yes ~No If"No" disregard remaining questions and return survey . ~r I I I I I I I I I I I I I I I I \._/ Name and address of owner( s) of property with water supply well How many water supply wells are on your property? r t ,What is the well(s) used for? (pheck all that apply) Drinking iL_, Irrigation ✓ .• .. Swimmi°'g Pool ' Water Livestock , Other (specify) , You do not use the Well How many residences are connected to the well (list addresses below)? , --How deep is the well(s)? Date well was installed? ~-/7"::>U~ What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: ,· .. . (This part to be completed by Responsible Party or their representative) I ... Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) (9f9) 832-5914 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 .. ·'3: 7e1ephone tConsuitant~s Telephone Numner) · [phone] or(800') 474-7049 I 4. E-mail to (Consultant's E-mail Address) dparkerra>.sei-environmental.com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] I .. ~. • .. .. ; " ~:· ',·
1------------------_,,,__.-;.w(/'-..... (This line to be completed by Responsible Party or their representative) PARCEL ID #: I Incident Number: Pendin2 Incident Name: The Pantry #3022 _, Please Provide the Following Information (to the best of v.our knowledeel Name and telephone number of person completing the survey ~e;S t" ~c--3 ',1, ~ ":-'&,4o I I ~~~ .:-::= y'perty receiving survey --!:::~=--'11.-l/.1... '4--1--·-_..i...,s..(', 'u.:t-.A:..i,.f'Z)~-t::J=:::.:fl='.U'\-',J:::.:....L;._..c:))'------------------1 Citv · ___ F!:!.vef ~ville County Cumberland /'Wlfat is #le·-s6itce of your drinking water? I .. { Public Water/ Water Supply Well/ Stream Intake/ Other (please explain below) '-....____ ____ ./ 11---------.,,....;;a~~----------1 Is there a water suooly well on this prooertv? Yes/Nd If "No" disregard remaining questions and return survey -L/ I Name and address of owner( s) of propertv with water suooly well I How many water suooly wells are on your property? _,What is the well(s) used for? (check all that apply) Drinking _, Irrigation . ~ Swimming Pool _ __,,, I Water Livestock , Other (specify) · , You do not use the Well How many residences are connected to the well (list addresses below)? l.~-~~-~----~-----1 .. I How deep is the well(s)? What is the casing deoth of the well(s)? Date well was installed? What is the screen interval of the well(s)? I Additional water sunnlv well information: 1------------------t 1·t------------------t I (This part to be completed by Responsible Party ortheir representative) , . Please return completed survey to SEI Environmental, Inc, by ___ using one of the following methods: 11-----,-------------t L Fax to (Consultants Fax Number) [phone] 2, Mail to . (Consulting Firm Name and SEI Environmental, Inc, Address) 130 Penmarc Drive, Suite 108 Ralei!ili, North Carolina 27603-2470 ·'3·. Te1etinone (Consuitant.,,s Telephone Nunfoei) · (919') 832-2535 or (800') 474-7049 I 4. E-mail to (Consultant's E-mail Address) [e-mail] I I If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone]
7 (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendin2 Incident Name: The Pantry #3022 I I I I I . .... Please Provide the Following Information (to the best of v.our knowle~~l Name and telephone number of person completing the survey Address of property receiving survey ~~2-f 1) M.,,(:\ttiZ' .a.. \) City Fayetteville County Cumberland What is the source of your drinking water? Public Water/ Water Sup-ply Well/ Stream Intake/ Other (please explain below} Is there a water supply well on this property? Yes/ No If"No" disregard remaining questions and return survey ' ,,,. :I II Name and address of owner( s) of property with water supply well How many water supply wells are on your property? ,What is the well(s) used for? (check all that apply) Drinking -• Irrigation . . Swimming Pool · Water Livestock , Other (specify)· . . , y OU do not use the Well How many residences are connected to the well (list addresses below)? .. How deep is the well( s )? Date well was installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: I I A -t--1-?.--l'" _} W{t-.-,,I BV--. ' ---ON ~ 1(._.QJ\ , . (This part to be completed by Responsible Party or their representative) I . I I I I I I I I I .· . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 .. ··3-_ Yeletitione t'Constiftanf"s Tefephone Number) · t'9T9) 832-7535 or (800') 474-70'49 I 4. E-mail to (Consultant's E-mail Address) dparker@.sei-environmental.com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] -.· I .. ~ 'ti• .• ,. ~-~' i-',·
9-(This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendine: Incident Name: The Pantry #3022 I I I I -.,-Plea.s.e Provide the FQllowiru!Inform:ation (to the best of your knowlewreJ Name and telephone number of person completing the survey Address of property receiving survey 2-q (pc, C!,,ut,..'\,~\;> City Fayetteville County Cumberland What is the source of your drinking water? .,...,, Public Water/ Water Sup\)ly Well/ Stream Intake/ Other(please explain below) Is there a water suooly well on this property? Yes / No If "No" disregard remaining questions and return survey 11 I I I I I I . ',t 'I :I 11 11 · Name and address of owner(s) of property with water supply well How many water supply wells are on your property? _,What is the well(s) used for? (check all that apply) Drinking -• Irrigation . , Swimming Pool -'---' · Water Livestock , Other (specify) · · · , You do not use the Well ·· How many residences are connected to the well (list addresses below)? ... How deep is the well(s)? Date well was installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information:· 1.1\ ft'\ ,./l ~1-v M -i-'-" 't' V I t:::--f ........ I I ~ c---,_ ---~ CJ71J 11'----L.J ~ 0/'--t (This part to be completed by Responsible Party or their representative) I . Please return completed survey to SEI Environmental~ Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 I I ,. 3: 1'eleptione tConsultant~s Telephone Number) · [phone] or (8ffl)') 474-7049 4. E-mail to (Consultant's E-mail Address) [e-mail] .. b •1: ~-; ,.. -.;:. i ··'-· -----------, r· If you have any que~tions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] I
9 I (This line to be completed by Responsible Party or their representative) PARCEL ID #: I ·-,: Incident Number: Pendine: Incident Name: The Pantry #3022 Please Provide the Followim!lnformation (to the best ofvour knowled2.~) Name and telephone number of person completing the survey 11 Address of property receiving survey 291,,..,p., (' .,v tV\ ~ t-AN \) City Fayetteville County Cumberland What is the source of your drinking water? I -~ Public Water/ Water Supply Well/ Stream Intake/ Other (please explain below) 11 Is there a water supply well on this property? Yes/ No If "No" disregard remaining questions and return survey I · '·Name and address of owner( s) of property with water supply well I How manv water supply wells are on your property? ,What is the well(s) used for? (check all that apply:) Drinking _, Irrigation __ . Swimmin_g Pool _ __,. · Water Livestock , Other (specify) · · , You do not use the Well · · I How manv residences are connected to the well (list addresses below)? I,----_-------... How deep is the well( s )? Date well was installed? I 1--Wh_a_t 1_· s_th_e_c_a_si--'ng...__de .... ~p_th_o_f_t_he_w_el__,l(._;_.s)'-?-------------------------1 What is the screen interval of the well(s)? I Additional water supply well information: IJ-----------------1· . I (This part to be completed by Responsible Party or their representative) , . Please return completed survey to SEI Environmental, Inc. by ___ using one of the following methods: I 1. Fax to 2. Mail to (Consultants Fax Number) [phone] (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 I Raleigh, North Carolina 27603-2470 ·· '3•. :Teletfnone (Consuitanf"s Tefephone Number)· {919) 832-2535 or {800') 474-7049 I 4. E-mail to (Consultant's E-mail Address) [e-mail] If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional I Office at [phone] I
lo (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendine; Incident Name: The Pantry #3022 ' ·~· Please Provide the Followin2 lnform.ation (to the best of vour kn.owlech!e) Name and telephone number of person completing the survey Address of property receiving survey City Fayetteville County Cumberland What is the source of your drinking water? ,. ~ Public Water I Water Sup-oly Well/ Stream Intake/ Other (please exP,lain below) Is there a water supply well on this propertv? Yes / No If '"No" disregard remaining questions and return survey .-.. Name and address of owner(s) of property with water suooly well How many water suooly wells are on your property? I I I I I I I I I I I I I I I I I I .,What is the well(s) used for? (.check all that appl)'.) Drinking _, Irrigation • Swimming Pool . Water Livestock , Other (specify) , You do not use the Well How many residences are connected to the well (list addresses below)? .,,_, How deep is the well(s)? Date well was installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: ,/ f\ AA. r•t \ I\ I ' \/,(\_\ ... / \ i'\""' ~ I L)\ -(This part to be completed by Responsible Party or their representative) I . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Finn Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 " ;3: :-r-eleptione (Cbnsu1tant,;,s Telephone NumbeiJ t9T9) 832-2535 or (800) 474-70'49 4. E-mail to (Consultant's E-mail Address) dparker(@,sei-environmental.com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] ·' I .. ,. ~:-· ~.; .. ... ,
J3 (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pending Incident Name: The Pantry #3022 I I I I I I I I I I I I I '·,; Please Provide the Followiru! Information (to the best ofvour knowled.2~) Name and telephone number of person cor~lleting the survey _lo<&: v A\-v ~ &tJo-4-ZS•?'lldo Address of property receiving survey 12..t:; LI .... J,.,,, .. .tn\,~ ~ . City Fayetteville ,r ------County Cumberland What is the source of ~te;drinking' wate~~1 ,,, Public Water/ W er Supply Well/ S earn Intake/ Other (please explain below) '-----_/ ~ Is there a water suoolv well on this propertv1Yes ~ No If "No" disregard remaining questions and return survey '--""" ·, Name and address of owner(s) of property with water suoolv well -A~.a-How many water suooly wells are on your propertv? l "What is the well(s) used for? (check all that apply) Drinking _ ✓~ Irrigation ✓-. Swimmi~g Pool . Water Livestock , Other (specify) · , You do not use the Well How many residences are connected to the well (list addresses below)? -How deep is the well(s)? { 1"1~ Date well was installed? t)...J \l. What is the casing depth of the well( s )? What is the screen interval of the well(s)? Additional water suoolv well information: I (This part to be completed by Responsible Party or their representative) I . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: I 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. I Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 ·· ·'3·_ Telephone t'Consultanf'-'s Telephone Number) · [phone] or (800) 474~'7tr49 I 4. E-mail to (Consultant's E-mail Address) dparkerra2sei-environmental. com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional I Office at [phone] I j : r-,·
/~ (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendin2 Incident Name: The Pantry #3022 I I I I I I I I I I I I I I I .. ~· Pleas.e Provide the Followin2 Information (to the best ofy,our knowled!!el Name and telephone number of person completing the survey J\f (. /4A1Z..C-i' A-t/--;~07 t"L. Address ofproperty receiving survey c:p 9 P, lA\ • IV\ mJ.JTll I JI..\ 1'\~ . City Fayetteville ~ -County Cumberland What is the source of yont'drinkmg ;titer? ,., Public Water/ Wa~er Supply W. 11 / Stream Intake I Other (please explain below} \. / --.•·~ Is there a water supply well on this property'? Yes I/No If'"No" disregard remaining questions and return survey ; l_/ Name and address of owner( s) of property with water supply well How many water suooly wells are on your property? / ,.What is the well(s) used for? (_check all that applY,) Drinking ./ • Irrigation . Swimming Pool . . Water Livestock , Other (specify) . . . , y OU do not use the Well .. How many residences are connected to the well (list addresses below)? How deep is the well(s)? Date well was installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: . (This part to be completed by Responsible Party or their representative) ; Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. I Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-2470 3·. ~elephone (Consuitanf''s Telephone Number) · t9T9) 832-1535 or (&10') 474-7049 4. E-mail to (Consultant's E-mail Address) [e-mail] If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional I Office at [phone] ·' I ' ~. ·:.-~-' r· "
I !I 1• I '' . ,·• /q (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendin2 Incident Name: The Pantry #3022 Please Provide the Followin~ Information (to the best of vour knowlede:e) .. Name and telephone number of person completing the survey I-, ~t>\J~ ~ 11\viO ?~T S Address of property receiving survey a 400 Or \C°J'.. City Fayetteville County Cumberland What i~ ~t~ of your drinking water? P lie Wat / Water Suoply Well/ Stream Intake/ Other (please ext)lain below) ' l / ---· Is there a water supply well on this property? Yes / )(i o lf "No" disregard remaining questions and return survey '-"" .. I ii . ·•: I I 11 ' I ii I I I I I I I I I Name and address of owner( s) of property with water supply well How many water supp}y wells are on your property? ,What is the well{s) used for? (.check all that apply:) Drinking _, Irrigation ... Swimmin_,s Pool , Water Livestock , Other (specify) , You do not use the Well How many residences are connected to the-well (list addresses below)? How deep is the well(s)? Date well was installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: .. . (This part to be completed by Responsible Party or their representative) ; . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: . . 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleigh, North Carolina 27603-24 70 "'3·. Telephone (Consu1tanrs Telephone Number) · (919') 832-2535 or(8t:Jtr) 474-70'49 4. E-mail to (Consultant's E-mail Address) dparker(@sei-environmental.com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] .,. ._; ,. . ~;-.,
(This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendin Incident Name: The Pan Please Provide the Full.ow' Information (t Name and telephone number of person completing the I I I I Address of property receiving survey _ _,c_0~-=2.==-_..:::::.....i...c:...!:=--..,<C~---------------1 G . rl~ r? Public Water Stream Intake/ Other (olease explain below) I :\· I How man water su 1 wells are on our ro e ? _,What is the well(s) used for? (check all that applY,) Drinking __:_, Irrigation .. , Swimming Pool --'--' · Water Livestock , Other (s eci ) · , You do not use the Well I How man residences are connected to the well list addresses below ? a-=--:.--=:~~~=-=--=-:..:..::~~--'----1--------1 1--!,F----.. ·. -~~~~-----___,.._------------i. I How dee is the well(s)? What is the casin de th of the well s ? Date well was installed? What is the screen interval of the well( s ? I · • Additional water su 1 well information: I -----------~~--.a..:-----1 I 1---------~~~~~ I (This part to be completed by Responsible Party or their representative) , ... Please return completed survey to SEI Environmental, Inc. by ___ using one of the following methods: I 1. Fax to 2. Mail to Consultants Fax Number) 919 832-5914 (Consulting Firm Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 ··•cs.Tele hone (Consuftan!'s Tefe bone Numliei Ra!~ ~;:5 ::= ~~~~!70 I 4. E-mail to Consultant's E-mail Address d arker sei-environmental.com If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional ,_Office at [phone] I r·
I I I I .I 1, ii I I I I I (This line to be completed by Responsible Party or their representative) PARCEL ID#: Incident Number: Pendin2 Incident Name: The Pantry #3022 ..... Please Provide the Followi02 Information (to the best ofv.our knowled2e) . .. . . . . ' . Name and telephone number of person completing the survey Address of property receiving survey ~c.? //,,., 't)-{~C---:-. .;.:. \ City Fayetteville -County Cumberland What is the source of your drinking water? ,,..-i Public Water/ Water Supply Well/ Stream Intake/ Other (please explain below) Is there a water supply well on this property? Yes/ No If "No" disregard remaining questions and return survey . ~'. Name and address of owner(s) of property with water supply well How many water supply wells are on your property? _,What is the well(s) used for? (check all that apply) Drinking _, Irrigation , Swimming Pool ' Water Livestock , Other (specify) , y OU do not use the Well How many residences are connected to the well (list addresses below)? . How deep is the well(s)? Date well was installed? What is the casing depth of the well( s )? What is the screen interval of the well(s)? Additional water supply well information: -1 I -I\ A ~0t----l...l 1 u I • -I _..,-,(_./' ' \ oll\~J ... .,\ ( ) \ . UN ,,-'-,µ ~../ \ L-"10 ~ . .... \,,~,..L-· ,'-,/ -r::~ E' ( k-(This part to be completed by Responsible Party or their representative) ''-"' I . Please return completed survey to SEI Environmental, Inc. by using one of the following methods: 1. Fax to (Consultants Fax Number) [phone] 2. Mail to (Consulting Finn Name and SEI Environmental, Inc. Address) 130 Penmarc Drive, Suite 108 Raleicll, North Carolina 27603-2470 I I I I I I I · '3·. ·1'e1eplione tConsuJtanf"s Tefepftone Nmrtber) · (919') 832.:7535 or [phone]' 4. E-mail to (Consultant's E-mail Address) [e-mail] If you have any questions, please contact the consultant indicated above or the UST Section Fayetteville Regional Office at [phone] .• .. ., .,. .. ...
I SEI ~ I I I I I I I I I I I I I I I I I I Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474. 7049 919.832.2535 Fax [phone] February 1, 2007 J aines & Clara Barton 3 016 Dyke Street Fayetteville, North Carolina 28306 · RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Mr. or Ms. Barton, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of · Environment and Natural Resources (NCDENR), Division of Waste . Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather inf onnation concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 51-3337, located at 3016 Dyke Street, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 James & Clara Barton 3016 Dyke Street Fayetteville, NC 28306 ~;· 0431s·:irJ10·124 ,,,,.,ttf W c , v,. v-uf~~tf~ ~ ·ff'o 390~ •~ i=, ,IA. ~ " ~-'ii, .,..,,. "l1tt ··-(fl ~ 02/0'1/:2007 ,,,fi!~~ ~ Ma!!ed From27603.,fffri~~:J -------------------
I I I I I-· I I I I I I I I \I I I I I I SEI ~ Environmental, Inc. ,130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800. 47 4.7049 919.832.2535 Fax [phone] February 1, 2007 Sue Lockamy POBox42551 Fayetteville, North Carolina 28309 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Ms. Lockamy, SEI Environmental, Inc. bas been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources · (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41-7812, located at 2952 Cumberland Road, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. . (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 I {"\ ·1· .· """ . , ,,1i½ Sue Lockamy s ' S ·s·"' ,li,.,.. PO Box42551 Fayetteville, NC 28309 .,_. . ~ttW ~ 043J83010324 4i f.!J 0 t.f~~ ~ o.. a-o 390~-"'~ ..... t"\ .;Jt . ... . -~'t .<'Y '" ~ =-0 Qi ~ 02/01/2007 ~ Mai!'2d Frnrn :2760'3 a. <n :, -------------------
I SEI ~ I I I I I I I I I I I I I I I I I I Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.2535 Fax [phone] February 1, 2007 Shirley Dees 3112 Cumberland Road Fayetteville, North Carolina 28306 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Ms. Dees, SEI Environmental, Inc. bas been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41.-6729, located at 2960 Cumberland Road, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The state requires the survey even if no water supply weUs are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 I l~ Shirley Dees ~ . ~> 3112 Cumberland Road Fayetteville, North Carolina 28306 .;..1 n;1 ·~ , ,, ,.,,,.<-;··f LU r.,; , .• 3J8-:i0 !03,,,4 ,A/[5 (!) o u&t;'ii<,ifu <t ~ $0 390~ = l-e .. --~:... _.? r..r, ~ ----~o P 0?/01/?007 "~~:,-0.. !!!a, --. '1~~1 Cf) ~ r,fo!!,ecf From27603-;;td':~::> -------------------
I I I I II 11 11 ·I I I I I I I I SEI~ Environmental, Inc. · 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.25.35 Fax [phone] February 1, 2007 Lewis & Harriet Carpenter 3116 Cumberland Road Fayetteville, North Carolina 28306 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Mr. or Ms. Carpenter, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41-5907, located at 2968 Cumberland Road, within 1,000 feetof the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The. state requires the survey even if no water supply· wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 :1~ I ~ ..... m,1.,,:r;. '"1.···'el, 'f··,,. ... , ·~. C l:,i S C1 ~Cs,•" . '\,;~ Lewis & Harriet Carpenter,. 3116 Cumberland Road Fayetteville, NC 28306 ; 043J83010324 0 Os tl'Q "90~~·. (:> <!t .1) -":__ IU ~ 02/01/2007 ~ Mailed From27603 l.U C) ~ l_f) 0 n. lf) ::> -------------------
I I I I I I I I I I I I I ·1 I I I I I SEI~ -Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.2535 Fax [phone] February 1, 2007 Malgram & E. Hutchinson 3103 Bolton Street Fayetteville, North Carolina 28306 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Mr. or Ms. Hutchinson, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by. parcel ID: 41-7459, located at 3103 Bolton Street, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 I s \:~:c. Malgram & E. Hutchinson 3103 Bolton Street Fayetteville, NC 28306 ~ 043.)83010324 . .;,;r,r;·~ 0 · ~~iii; ct; o. w . o="• ,.,_ • ,,., ,p() •. 39_ ~; .~ f~ ;) .~ 0 ~Cl 02/01/2007 llti:\ fl. ,. ,.. l:~'\1l¾!1~t! fl) M;illed From27o03·\ i'~\1&i:::J -------------------
I I I I 11 \I I I I I \1 I 1, i1 I I I I I SEI ~ Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.2535 Fax [phone] February I, 2007 Tim Pittman 927 West Mountain Drive Fayetteville, North Carolina 28306 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Mr. Pittman, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41-9510, located at 927 West Mountain Drive, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, , SEI Environmental, Inc. David Brewster Staff Scientist Enclosure Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 I t•r·I.·.·~ .·i it'= s i,~:,.· Tim Pittman 927 West Mountain Drive Fayetteville, NC 28306 ,.,\ .' ,g'LU ~ 043J83010324 ,dii,.'f't'!f{· c, 0 ----lb{,~\~,( °' $ ~.,,,,,.., A O. 39Q~; ; ,;; -~ ~l • ~-Q :~ . i:.l 02/0'1/2007 ~-~ 0.. ~-~;:~11 fl) ~ Ma!f~d From27603·{~~~:) -------------------
I I I I I I I I I I I I I I I I I I SEI~ Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.2535 Fax [phone] February 1, 2007 Thywell Tyler 923 West Mountain Drive Fayetteville, North Carolina 28306 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Mr. Tyler, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41-9318, located at 923 West Mountain Drive, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the stamped envelope provided. (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at [phone] or me at [phone]. Thank you in advance for your assistance. Sincerely, Enclosure I Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 Thywell Tyler 923 West Mountain Drive Fayetteville, North Carolina 28306 -;J .. e!J'lU .-,_, 0~3J83010324 ,,,dJsf{t (.;) 0 ·-----[1:_,.l:L~· ~ °" n,-0 3 o•"';, ·-.-t-o ill, . 9_ ~i,,F if) (I.' ' ~ 0 ~ 02/01/2007 ·111t~ a. 'tifi.t Mrii!ect Fmm27603(~Jl~ - - - - - - - - - -·-- - - - - - - -
I I I I I ii I I I I I I I I I I I I SEI~ Environmental, Inc. 130 Penmarc Drive Suite 108 Raleigh, NC 27603-2470 800.474.7049 919.832.2535 Fax [phone] February 1, 2007 David K. Goins 3976 Mission Hills Road Hope Mills, North Carolina 28348 RE: Quick Stop #67 (aka The Pantry #3022) 2326 Owen Drive Fayetteville, Cumberland County, North Carolina 27306 Wrr. Goins, SEI Environmental, Inc. has been contracted by The Pantry, Inc. to complete a North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management, UST Section required Limited Site Assessment (LSA) at the above referenced site. As a standard part of the LSA, SEI Environmental, Inc. is required to gather information concerning potential water supply wells located within 1,000 feet of the property. SEI Environmental Inc. understands that you are the property owner of land identified by parcel ID: 41-9414, located at 925 West Mountain Drive, within 1,000 feet of the above referenced site. As such, please complete the attached survey and return in the st.amped envelope provided. (NOTE: The state requires the survey even if no water supply wells are present on the properties indicated). If you have any questions regarding the survey, you may call the UST Section, Fayetteville Regional Office at (910) 486~1541 or me at [phone]. Thank you in advance for your assistance. Sincerely, Enclosure I Charlotte, NC • Columbia, SC • Knoxville, TN • Nashville, TN • Raleigh, NC
SEI Environmental, Inc 130 Penmarc Drive Suite 108 Raleigh, NC 27603 David K. Goins 3976 Mission Hills Road Hope Mills, North Carolina 28348 _.., ® 043JS:30'l0324 <"~tr !if 0 -----/;@\ti'>'·' {l) ~ !if--·•~',:( 0 $0 .. 3~0~} -~ t,~ al . ·7 (/) !:l O'''/ . ~ 0 ~ uL (11/2007 ~·' fl., ~m"it'i!: ribi!fid Frnn• '.)7r-;03'!i'·ttit-1@ ff.I " -. .•. ~ ;""' "'\\ :,) ~! -------------------
I I I I I I I .I I I I I I I . I I I I I APPENDIXC
I i !1 I II I 11 II I I .I I I I I I I I ~ Southeast IIACCUIESi. ACCUTEST LABORATORIES "l-956-2006 SEI Environmental-Raleigh Pantry 3022; Fayetteville, NC 506016 Accutest Job Number: F46687 Sampling Date: 01/18/07 Report to: SEI Environmental-Raleigh 130 Penmarc Dr. Suite 108 Raleigh, NC 27603 A TI'N: Douglas Parker Total number of pages in report: 54 ~ ~ H : Test results cootalned within this data package meet the requirements of the National Environmental Laboratory Accredllatlon Confereace and/or stite specific certification programs as applicable. e-Hardcopy 2. 0 Automated Report .~-Harty Behzadi, Ph.D. Laboratory Director Certifications: FL (DOH E83510), NC (573), NJ (FL002), MA (FL9"6), IA (366), IA (03051). KS (E-10327), SC, AK This report shall not be reproduced, except in its entirety. without the written approval of Accutest Laboratories. Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com &ID 1 of54 laACa • res r. F46687 1 " b "i-... ,. ;;_ -, ;; ,. 1'" ;
I I I I I I II I I I I I I I I I I I I I I I Table of Contents -1-Sections: Section 1: Sample Summary ................................................................................................... 3 Section 2: Sample. Results ·········•·o-••··············· ...................... *........................................................... 4 2.1: F46687-1: SS-1 (5) ....................................................................................................... 5 2.2: F46687-2: SS-1 (10) ..................................................................................................... 13 : Chain of Custody ................. ......... ... .. .. ......... ........ ... .... .. .. ..... .. .. ..... .. .. .. ... .. .. ....... .... . . .. ... . 22 Section 4: GC/MS Volatiles -QC Data Summaries ............................................................... 24 4.1: Method Blank Summary .. .... ... .... .. .... .. . .. .... ..... .. .. .. .. . .. .. .. .. ..... .. .. .. . . ... .. ............. ..... .. .. .. .. .. 25 4.2: Blank Spike Summary ......................... ......... ............... ......... ......... ...... ... .. ..................... 28 4.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 31 S ~, -GC/'l.l!'L' C • ·1 "I QC' 1) ,.., . • 34 , ec1:1on :,: · · . ,vh., ,:,enu-vo atl,es -, . , ,1: ata ~,unu:nanes ..................................................... , : Method Blank Summary ................................................................................................ 35 Blank Spike Summary ......................... .................... .... ........................ ..... .. .. ........... ...... 38 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 41 Section. 6: c;.c Volatiles -QC Data Summaries ..................................................................... 44 6J: Method Blank Summary ...........•....... ....... .... ........................... ........... .. .................. .. ...... 45 6.2: Blank Spike Summary ................................................................................................... 46 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 47 6.4: Duplicate Summary ....................................................................................................... 48 Section 7: GC Semi-volatiles -QC Data Summaries ............................................................ 49 7.1: Method Blank Summary ................................................................................................ 50 7.2: Blank Spike Summary................................................................................................... 52 7.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 53 7.4: Duplicate Summary....................................................................................................... 54 I I IJ I I I I 811!1 2of54 IIACCUIEST. F46687 ! ;1h,'."/l'"f;i◊i"i1::,
I I I I I I I I I I I I I I I I I I I Accutest Laboratories SEI Environmental-Raleigh Panny 3022; Fayetteville, NC Project No: 506016 Sample Summary Sam.pk, Number ~in~1fji:::r:'\,::\Y,• Matrix Date Time By Received Code Type 01/20/07 SO Soil 01/20/07 so Soil Job No: Client Sample ID Soil samples reported on a dry weight basis unless otherwise indicated on result page. I F46687
I I I , I I ii !I II I I I I II 11 II I I I I gm s. outheast IIACCUiESI. L;ibora.tor1es Report of Analysis Section2 I Ill 4of54 (iACCU ii ESE. F46687 t. ~ b',·,r;,tf,_,r:t,'
I I I I I I I I I I I I I I I I I Accutest Laboratories Client Sample ID: Lab Sample ID: Matrix: Method: Project: SS-1 (5) F46687-1 SO -Soil SW8468260B Report of Analysis Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94.6 Panny 3022; Fayetteville, NC Page 1 of3 File ID IRun #1 a F019396.D DF 1 Analyzed By Prep Date n/a Prep Batch Analytical Batch 1Run12 Initial Weight 4.50 g 01/22/07 WJ VOA 8260 List CAS No. Compound Result RL 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 104-51-8 135-98-8 98-06-6 108-90-7 75-00-3 67-66-3 95-49-8 106-43-4 75-15-0 56-23-5 75-34-3 75-35-4 563-58-6 96-12-8 106-93-4 107-06-2 78-87-5 142-28-9 108-20-3 594-20-7 124-48-1 75-71-8 156-59-2 10061-01-5 541-73-1 95-50-1 Acetone 'l'sID >,\, < ... 0.059 Benzene NI).;, · 0.0059 Bromobenzene NI) 0.0059 Bromocbloromethane ND' . ·. 0.0059 Bromodicblorometbane Ni:)'< : 0.0059 Bromofonn ~• : 0.0059 n-Butylbenzene NJ? i . ·•·• 0.0059 sec-Butylbenzene m:>. •·•.·. .. 0.0059 tert-Butylbenzene ND · 0.0059 Chlorobenzene ND; 0.0059 g:::!':e '.~{:, <: ~:::: o-Chlorotoluene :NI)·; ; > · · · · 0. 0059 p-Cblorotoluene ND · • .. ·. · 0.0059 Carbon disulfide Nif 0. 0059 Carbon tetrachloride •Nl:> 0.0059 1,1-Dicbloroethane NJ>' · ... 0.0059 1,1-Dicbloroetbylene l\J'p,' , >. 0.0059 1,1-Dicbloropropene ·.~ · · ·, 0.0059 1,2-Dibromo-3-cbloropropane N'D: 0.0059 1,2-Dibromoetbane 1IW\, .. ·. ··. 0.0059 1,2-Dicbloroetbane ND,: · 0.0059 1,2-Dicbloropropane · ·ND' · 0.0059 1,3-Dicbloropropane ~.{ ', · :; 0.0059 Di-Isopropyl ether .~ ·: i · .· 0.0059 2,2-Dicbloropropane NJ?, ;i • ,·., · '' 0.0059 Dibromocblorometbane ND <: 0.0059 Dichlorodifluorometbane J\JD 0.0059 ds-1,2-Dicbloroetbylene NO .. ! ··.• 0.0059 ds-1,3-Dicbloropropene NJ)· , : 0.0059 m-Dicblorobenzene NPo, · ·. :. 0.0059 o-Dicblorobenzene J\fi)),(. \ > 0.0059 n/a VF284 MDL Units Q 0.029 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N == Indicates presumptive evidence of a compound ...., :.... II 111!1 5of54 liACDiiESl. F46687 1 ,,·t-, i; . ., r·,.. 1 r:,.: \..,'
I I I I I I I I I I I I I I I I I I I Accutest Laboratories I\) :... Report of Analysis Page 2 of3 II Client Sample ID: Lab Sample ID: Matrix: Method: SS-1 (5) F46687-1 SO -Soil SW846 8260B Project: Panny 3022; Fayetteville, NC VOA 8260 List CASNo. 106-46-7 156-60-5 10061-02-6 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 108-10-1 74-83-9 74-87-3 74-95-3 75-09-2 78-93-3 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 71-55-6 79-34-5 79-00-5 87-61-6 96-18-4 120-82-1 95-63-6 108-67-8 127-18-4 108-88-3 79-01-6 75-69-4 75-01-4 Compound p-Dichlorobenzene trans-1,2-Dichloroethylene trans-1,3-Dichloropropene Etbylbenzene 2-Hexanone Hexachlorobutadiene Isopropylbell7.elle p-Isopropyltoluene 4-Methyl-2-pentanone Methyl bromide Methyl chloride Methylene bromide Methylene chloride b Methyl ethyl ketone Methyl Tert Butyl Ether Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1, 1-Trichloroethane 1, 1,2,2-Tetrachloroethane 1, 1,2-Trichloroethane 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Tetracbloroethylene Toluene Tricbloroethylene Tricblorofluoromethane Vinyl chloride m,p-Xylene o-Xylene Resuh RL Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94.6 MDL Units Q 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.012 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.012 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0059 mg/kg B 0.012 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg . 0.0023 mg/kg 0.0023 mg/kg 0.0029 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0023 mg/kg 0.0035 mg/kg 0.0023 mg/kg 95-47-6 CASNo. 1868-53-7 2037-26-5 460-00-4 Surrogate Recoveries Dibromofluorometbane Toluene-DB 4-Bromofluorobenzene Run# I J14% 92%, !JS%'. Run#2 Limits ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range 80-121% 71-130% 59-148% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 11!1 6of54 11ACD IIES .. F46687 r r. h o·r ti i ~· r i ~ ~
I I I I I I I I I I I I Accutest Laboratories Report of Analysis Client Sample ID: Lab Sample ID: Matrix: Method: SS-1 {5) F46687-1 SO -Soil SW8468260B Project: Panny 3022; Fayetteville, NC VOA 8260 List CAS No. Surrogate Recoveries Run# 1 · 17060-07-0 1,2-Dichloroethane-D4 Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94. 6 Run# 2 Limits 77-123% {a) Sample was received in a bulk container but was not preserved within 48 hours of sampling. (b) Suspected laboratory contaminant. ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value Page 3 of3 I RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 11n 7of54 liACX, I I ESI. F.46687 1 f! b i'l r ;:, I n r·; :~ -~
I !'> ..... I Accutest Laboratories I Report of Analysis Page 1 of3 I Client Sample ID: SS-1 (5) Lab Sample ID: F46687-1 Date Sampled: 01/18/07 Matrix: SO -Soil Date Received: 01/20/07 I Method: SW846 8270C SW846 3550B Percent Solids: 94.6 Project: Pantry 3022; Fayetteville, NC File ID DF Analyn,d By Prep Date Prep Batch Analytical Batch I Run#l 1035510.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 Run#2 I ~II Initial Weight Final Volume 30.6g 1.0ml Run#2 I ABN Full List CASNo. Compound Result RL MDL Units Q I 65-85-0 Benzoic acid 0.86 0.35 mg/kg 95-57-8 2-Chlorophenol 0.17 0.035 mg/kg 59-50-7 4-Chloro-3-methyl phenol 0.17 0.035 mg/kg I 120-83-2 2,4-Dichlorophenol 0.17 0.035 mg/kg 105-67-9 2,4-Dimethylphenol 0.17 0.035 mg/kg 51-28-5 2,4-Dinitrophenol 0.86 0.35 mg/kg 534-52-1 4 ,6-Dinitro-o--cresol 0.35 0.069 mg/kg I 95-48-7 2-Methylphenol 0.17 0.035 mg/kg 3&4-Methylphenol 0.17 0.035 mg/kg 88-75-5 2-Nitrophenol 0.17 0.035 mg/kg 100-02-7 4-Nitrophenol 0.86 0.35 mg/kg I 87-86-5 Pentachlorophenol 0.86 0.35 mg/kg 108-95-2 Phenol 0.17 0.035 mg/kg 95-95-4 2,4,5-Trichlorophenol 0.17 0.035 mg/kg I 88-06-2 2,4,6-Trichlorophenol 0.17 0.035 mg/kg 83-32-9 Acenaphthene 0.17 0.035 mg/kg 208-96-8 Acenaphthylene 0.17 0.035 mg/kg 62-53-3 Aniline 0.35 0.17 mg/kg I 120-12-7 Anthracene 0.17 0.035 mg/kg 92-87-5 Benzidine 1.7 0.86 mg/kg 56-55-3 Benzo(a)anthracene 0.17 0.035 mg/kg I 50-32-8 Benzo(a)pyrene 0.17 0.035 mg/kg 205-99-2 Benzo(b)fluoranthene 0.17 0.035 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.17 0.069 mg/kg 207-08-9 Benzo(k)fluoranthene 0.17 0.035 mg/kg I 101-55-3 4-Bromophenyl phenyl ether 0.17 0.035 mg/kg 85-68-7 Butyl benzyl phthalate 0.35 0.086 mg/kg 100-51-6 Benzyl Alcohol 0.17 0.035 mg/kg 91-58-7 2-Chloronaphthalene 0.17 0.035 mg/kg I 106-47-8 4-Chloroaniline 0.35 0.14 mg/kg 86-74-8 Carbazole 0.17 0.035 mg/kg 218-01-9 Chrysene 0.17 0.035 mg/kg I ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank I E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Im! 8of54 liA.CCfiJiJESi. I F46687 I. ;i h' i: i· t.•. t ;--
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of .Analysis Page 2 of 3 Client Sample ID: Lab Sample ID: Matrix: SS-1 (5) F46687-1 SO-Soil Method: Project: SW846 8270C SW846 3550B Pantry 3022; Fayetteville, NC ABN Full List CAS No. Compound 111-91-1 111-44-4 108-60-1 7005-72-3 95-50-1 122-66-7 541-73-1 106-46-7 121-14-2 606-20-2 91-94-1 53-70-3 132-64-9 84-74-2 117-84-0 84-66-2 131-11-3 117-81-7 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 90-12-0 91-57-6 88-74-4 99-09-2 100-01-6 91-20-3 98-95-3 62-75-9 621-64-7 86-30-6 85-01-8 129-00-0 110-86-1 120-82-1 bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Chloroisopropyl)ether 4-Chlorophenyl phenyl ether 1,2-Dichlorobenzene 1,2-Diphenylhydrazine 1,3-Dichlorobenzene 1,4-Dichlorobenz.ene 2, 4-Dinitrotoluene 2,6-Dinitrotoluene 3,3' -Dichlorobenzidine Dibenz.o(a,h)anthracene Dibenz.ofuran Di-n-butyl phthalate Di-n-octyl phthalate Diethyl phthalate Dbnethyl phthalate bis(2-Ethylhexyl)pbthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(l ,2,3-cd)pyrene Isophorone 1-Methylnaphthalene 2-Methylnaphthalene 2-Nitroaniline 3-Nitroanlline 4-Nitroaniline Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Phenanthrene Pyrene Pyridine 1,2,4-Trichlorobenzene Result RL l}\i~irn ·:NI).· , 0.17 •NJ). 0.17 ND 0.17 Ntf'. 0.17 ~< '0.17 ~< ·; · /',. 0.35 Np:'. 0.17 m;: ·<> ~:~! ~.. 0.35 ~Ill. . 0.35 ~i 0.35 ND 0.35 'NQ 0.17 ,~\Y• · ... ,• ~:~~ •~. .· >0.17 Nl)i . <> ..•. 0.17 Nii >.· 0.11 Nif. . 0.11 ND ··. 0.17 ND 0.17 !$). 0.17 ·~·\ 0.35 ,NU··\,>:, . o.35 NJ;) .... '. 0.35 NJ?i .·.·:., 0.17 NP . ,· 0.11 NQ 0.35 ~ 0.17 :ND 0.17 M?i: 0.17 ND''' 0.17 ~,.. ··.• 0.35 NQ :.· ... ·•. 0.17 ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94.6 MDL Units Q 0.035 0.069 0.035 0.035 0.035 0.035 0.035 0.035 0.069 0.069 0.17 0.069 0.035 0.086 0.17 0.086 0.086 0.17 0.035 0.035 0.035 0.069 0.069 0.069 0.069 0.035 0.035 0.035 0.086 0.086 0.12 0.035 0.035 0.14 0.069 0.035 0.035 0.069 0.17 0.035 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg . mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presmnptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 3 of 3 I Client Sample ID: Lab Sample ID: Matrix: Method: Project: ABN Full List SS-1 (5) F46687-l SO -Soil SW846 8270C SW846 3550B Pantry 3022; Fayetteville, NC Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94. 6 CASNo. 367-12-4 4165-62-2 118-79-6 4165-60-0 321-60-8 1718-51-0 Surrogate Recoveries 2-Fluorophenol Phenol-d5 2,4,6-Tribromophenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-dl 4 Run# 1 Run# 2 Limits 40-102% 41-100% 42-108% 40-105% 43-107% 45-119% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceem calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■D . 10 of 54 Ci'jACO I I ES 1. F46687 r 11·1i·i', 1--,i.·t ;~ :-i ,: ~
I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Client Sample ID: SS-1 (5) Lab Sample ID: F46687-1 Matrix: SO -Soil Method: MADEPVPH Project: Pantry 3022; Fayetteville, NC File ID DF Analp.ed By Run #1 a UV025609.D 1 01/24/07 MM Run#2 Initial Weight Final Volume Methanol Aliquot IRun n Run#2 3.27 g 5.1 ml 100 td MADEP VPH List CASNo. Compound Resuh C5-C8 Aliphatics (Unadj.) C9-C12 Alipbatics (Unadj.) C9-ClO Aromatics (Unadj.) CASNo. Surrogate Recoveries Run#l 460-00-4 BFB ··112%·· 460-00-4 BFB 108% RL 6.2 4.5 1.6 Run#2 Date Sampled: Date Received: Percent Solids: Prep Date n/a MDL Units 3.3 mg/kg 2.5 mg/kg 0.82 mg/kg Limits 70-130% 70-130% 01/18/07 01/20/07 94.6 Prep Batch n/a Q (a) Sample was received in a buJk container but was not preserved within 48 hours of sampling. ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value Page 1 of 1 II Analytical Batch GUV1472 RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 1111!!1 11 of 54 IIACaii EST. F46687 l'. n·1;··,::~·r·f ~--2 ;,-; :': ~
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: Lab Sample ID: Matrix: Method: Project: SS-1 (5) F46687-1 SO-Soil MADEP-EPH-98-1 SW846 3550B Pantry 3022; Fayetteville, NC File ID ZF22538.D DF 1 Analp.ed By Run #1 Run #2 01/31/07 AC Initial Weight Final Vohune 30.3 g 2.0 ml MAEPHList CASNo. Compound Result RL Cll-C22 Aromatics (Unadj.) 7.0 C9-C18 Aliphatics 7.0 C19-C36 Aliphatics 7.0 Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 94.6 Prep Date 01/25/07 MDL Units 7.0 mg/kg 7.0 mg/kg 7.0 mg/kg Prep Batch Analytical Batch OP19287 GZF1055 Q CASNo. Surrogate Recoveries Run# 1 Run#2 Limits 3386-33-2 1-Chlorooctadecane 66% 580-13-2 2-Bromonaphthalene 69% 84-15-1 o-Terphenyl 50% 321-60-8 2-Fluorobiphenyl 56% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range 40-140% 40-140% 40-140% 40-140% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Client Sample ID: Lab Sample ID: Matrix: Method: SS-1 (10) F46687-2 SO -Soil SW846 8260B Project: Pantry 3022; Fayetteville, NC File ID Run #1 a F019397 .D DF 1 IRun 12 Initial Weight 4.80 g VOA 8260 List CASNo. Compound 67-64-1 Acetone 71-43-2 Benzene 108-86-1 Bromobenzene 74-97-5 Bromocblormne1hane 75-27-4 Bromodicbloromethane 75-25-2 Bromoform 104-51-8 n-Butylbenzene 135-98-8 sec-Butylbenzene 98-06-6 tert-Butylbenzene 108-90-7 Chlorobenzene 75-00-3 Chloroe1hane 67-66-3 Chloroform 95-49-8 o-Chlorotoluene 106-43-4 p-Chlorotoluene 75-15-0 Carbon disulfide 56-23-5 Carbon tetrachloride 75-34-3 1, 1-Dichloroetbane 75-35-4 1,1-Dichloroethylene 563-58-6 1, 1-Dicbloropropene Analp.ed By 01/22/07 WJ Result RL Nll .. \ 0.056 ND> 0.0056 f( .' ~· /: 0.0056 ND· ·, ·,' 0.0056 ~.: 0.0056 :Nb 0.0056 Ni>< 0.0056 ~:·: 0.0056 Ni>' .• 0.0056 oo· ;,.' :, 0.0056 ND 0.0056 I\JI); i>. 0.0056 Ni>'.: <<>• 0.0056 ND. 0.0056 ND· \ 0.0056 Nb . 0.0056 'ND 0.0056 ND .... 0.0056 ,NI) , 0.0056 96-12-8 1,2-Dibromo-3-cbloropropane w:r: · .. · · 0.0056 106-93-4 1,2-Dibromoetbane ND>· 0.0056 107-06-2 1,2-Dichloroetbane :N'll)i':, 0.0056 78-87-5 1,2-Dichloropropane ~·· .. 0.0056 142-28-9 1,3-Dichloropropane ND . 0.0056 108-20-3 Di-Isopropyl ether ND··•.·· . ·• 0.0056 594-20-7 2 ,2-Dicbloropropane ND ,' 0.0056 124-48-1 Dlbromocbloromethane ~.<' 0.0056 75-71-8 Dichlorodifluorometbaoe ~< 0.0056 156-59-2 cis-1,2-Dichloroethylene ,NI) 0.0056 10061-01-5 cis-1,3-Dicbloropropene NI) 0.0056 541-73-1 m-Dichlorobenzene ND 0.0056 95-50-1 o-Dicblorobenzene M'. 0.0056 Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2 Prep Date n/a MDL Units 0.028 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0034 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0034 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0034 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0034 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg 0.0022 mg/kg Prep Batch n/a Q ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value Page 1 of3 Analytical Batch VF284 RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound II
I I I I ii I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 2 of3 Client Sample ID: Lab Sample ID: Matrix: Method: SS-1 (10) F46687-2 SO-Soil SW8468260B Project: Pantry 3022; Fayetteville, NC VOA 8260 List CAS No. Compound 106-46-7 156-60-5 10061-02-6 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 108-10-1 74-83-9 74-87-3 74-95-3 75-09-2 78-93-3 1634-04-4 91-20-3 103-65-1 100-42-5 630-20-6 71-55-6 79-34-5 79-00-5 87-61-6 96-18-4 120-82-1 95~63-6 108-67-8 127-18-4 108-88-3 79-01-6 75-69-4 75-01-4 95-47-6 CASNo. 1868-53-7 2037-26-5 460-00-4 p-Dichlorobenzene trans-1,2-Dichloroethylene trans-1,3-Dicbloropropene Ethylbenzene 2-Hexanone Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene 4-Metbyl-2-pentanone Methyl bromide Methyl chloride Methylene bromide Methylene chloride b Methyl ethyl ketone Methyl Tert Butyl Ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1, 1, I-Trichloroethane 1, 1,2,2-Tetracbloroethane 1, 1,2-Trichloroethane 1,2,3-Trichlorobenzene 1,2 ,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2 ,4-Trimethylbenzene 1,3,5-Trimethylbenzene Tetrachloroethylene Toluene Trichloroethylene Trichlorofluoromethane Vinyl chloride m,p-Xylene o-Xylene Surrogate Recoveries Dibromofluorometbane Toluene-DB 4-Bromofluorobenzene Resuh Run# 1 gs9fi ... 91% too.¾· ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL 0.0056 0.0056 0.0056 0.0056 0.028 0.0056 0.0056 0.0056 0.028 0.0056 0.0056 0.0056 0.011 0.028 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.0056 0.011 0.0056 Run#2 Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2. MDL Units Q 0.0022 0.0022 0.0022 0.0022 0.011 0.0022 0.0022 0.0022 0.011 0.0022 0.0022 0.0022 0.0056 0.011 0.0022 0.0022 0.0022 0.0022 0.0022 0.0022 0.0022 0.0022 0.0022 0.0028 0.0022 0.0034 0.0022 0.0022 0.0022 0.0022 0.0022 0.0022 0.0034 0.0022 mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg B mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Limits 80-121% 71-130% 59-148% J = Indicates an estimated value B = Indicates aoalyte found in associated method blank N = Indicates preswnptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Client Sample ID: Lab Sample ID: Matrix: Method: SS-1 (10) F46687-2 SO -Soil SW8468260B Project: Pantry 3022; Fayetteville, NC VOA 8260 List CAS No. Surrogate Recoveries 17060-07-0 1,2-Dichloroethane-D4 Run# I Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2 Run# 2 Limits 77-123% (a) Sample was received in a bulk container but was not preserved within 48 hours of sampling. (b) Suspected laboratory contaminant. ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value Page 3 of3 RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 1 of3 Client Sample ID: Lab Sample ID: Matrix: SS-1 (10) F46687-2 so -Soil ' Method: Project: SW846 8270C SW846 3550B Pantry 3022; Fayetteville, NC File ID L035511.D DF Analyml By NJ Runfl lwn#2 1 01/25/07 r" un#2 Initial Weight 30.5 g Final Volume 1.0ml ABN Full List CAS No. Compound 65-85-0 95-57-8 59-50-7 120-83-2 105-67-9 51-28-5 534-52-1 95-48-7 88-75-5 100-02-7 87-86-5 108-95-2 95-95-4 88-06-2 83-32-9 208-96-8 62-53-3 120-12-7 92-87-5 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 101-55-3 85-68-7 100-51-6 91-58-7 106-47-8 86-74-8 218-01-9 Benzoicadd 2-Chlorophenol 4-Chloro-3-methyl phenol 2, 4-Dichlorophenol 2, 4-Dimethylphenol 2,4-Dinitrophenol 4, 6-Dinitro-o-cresol 2-Methylphenol 3&4-Methylphenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,5-Trichlorophenol 2, 4 ,6-Trichlorophenol Acenaphthene Acenaphthylene Aniline Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)peryleoe Benzo(k)fluoranthene 4-Bromophenyl phenyl ether Butyl beozyl phthalate Benzyl Alcohol 2-Chloronaphthalene 4-Chloroaniline Carbazole Cbrysene Result RL =,· ~:~ 'l\JQ · 0.18 ~; 0.18 ;I;::-.i .. i i:ii .Nr> . 0.18 i·,::,; ~:!: ND .0.88 !I.r::· rn NP/ • 0.18 ~: 0.18 Nt> • i 0.35 Nb 0.18 Nri 1.8 :ND:_·-_::, .. {_-:: ~:!: 0.18 ~: __ ._ 0.18 Ng; ,0.18 NP 0.18 Ii" ,;rn Nti.. o.35 1'tJ) 0.18 N'lf' 0.18 ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Date Sampled: 01/18/07 Date Receiwd: 01/20/07 Percent Solids: 93.2 Prep Date 01/24/07 Prep Batch OP19264 MDL Units Q 0.35 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.35 mg/kg 0.070 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.35 mg/kg 0.35 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.18 mg/kg 0.035 mg/kg 0.88 mg/kg 0.035 mg/kg 0.035 mg/kg 0.035 mg/kg 0.070 mg/kg 0.035 mg/kg 0.035 mg/kg 0.088 mg/kg 0.035 mg/kg 0.035 mg/kg 0.14 mg/kg 0.035 mg/kg 0.035 mg/kg J = Indicates an estimated value Analytical Batch SL1820 B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I N N I Accutest Laboratories I Report of Analysis Page 2 of 3 I Client Sample ID: SS-1 (10) Lab Sample ID: F46687-2 Date Sampled: 01/18/07 Matrix: SO -Soil Date Received: 01/20/07 I Method: SW8468270C SW846 3550B Percent Solids: 93.2 Project: Pantry 3022; Fayetteville, NC ABN Full List I CASNo. Compound Result RL MDL Units Q I 111-91-1 bis(2-Chloroethoxy)methane 0.18 0.035 mg/kg 111-44-4 bis(2-Chloroethyl)ether 0.18 0.070 mg/kg 108-60-1 bis(2-Chloroisopropyl)ether 0.18 0.035 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether 0.18 0.035 mg/kg I 95-50-1 1,2-Dichlorobenzene 0.18 0.035 mg/kg 122-66-7 1,2-Diphenylhydrazine 0.18 0.035 mg/kg 541-73-1 1,3-Dichlorobenzene 0.18 0.035 mg/kg I 106-46-7 1,4-Dichlorobenzene 0.18 0.035 mg/kg 121-14-2 2,4-Dinitrotoluene 0.18 0.070 mg/kg 606-20-2 2,6-Dinitrotoluene 0.18 0.070 mg/kg 91-94-1 3,3' -Dichlorobenzidine 0.35 0.18 mg/kg I 53-70-3 Dibenzo(a,h)anthracene 0.18 0.070 mg/kg 132-64-9 Dibenzofuran 0.18 0.035 mg/kg 84-74-2 Di-n-butyl phthalate 0.35 0.088 mg/kg 117-84-0 Di-n-octyl phthalate 0.35 0.18 mg/kg I 84-66-2 Diethyl phthalate 0.35 0.088 mg/kg 131-11-3 Dimethyl phthalate 0.35 0.088 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate 0.35 0.18 mg/kg I 206-44-0 Fluoranthene 0.18 0.035 mg/kg 86-73-7 Fluorene 0.18 0.035 mg/kg 118-74-1 Hexachlorobenzene 0.18 0.035 mg/kg 87-68-3 Hexachlorobutadiene 0.18 0.070 mg/kg I 77-47-4 Hexachlorocyclopentadiene 0.18 0.070 mg/kg 67-72-1 Hexachloroethane 0.18 0.070 mg/kg 193-39-5 lndeno(l ,2,3-cd)pyrene 0.18 0.070 mg/kg I 78-59-1 Isophorone 0.18 0.035 mg/kg 90-12-0 1-Methylnaphthalene 0.18 0.035 mg/kg 91-57-6 2-Methylnaphthalene 0.18 0.035 mg/kg 88-74-4 2-Nitroaniline 0.35 0.088 mg/kg I 99-09-2 3-Nitroaniline 0.35 0.088 mg/kg 100-01-6 4-Nitroaniline 0.35 0.12 mg/kg 91-20-3 Naphthalene 0.18 0.035 mg/kg 98-95-3 Nitrobenzene 0.18 0.035 mg/kg I 62-75-9 N-Nitrosodimethylamine 0.35 0.14 mg/kg 621-64-7 N-Nitroso-di-n-propylamine 0.18 0.070 mg/kg 86-30-6 N-Nitrosodiphenylamine 0.18 0.035 mg/kg I 85-01-8 Phenanthrene 0.18 0.035 mg/kg 129-00-0 Pyrene 0.18 0.070 mg/kg 110-86-1 Pyridine 0.35 0.18 mg/kg 120-82-1 1,2 ,4-Trichlorobenzene 0.18 0.035 mg/kg I ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank I E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 54 IEST. I F46687 I. ~ b .:;: r ;.· t ,-; rt :-a
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 3 of3 Client Sample ID: Lab Sample ID: Matrix: Method: Project: ABN Full List SS-1 (10) F46687-2 SO -Soll SW846 8270C SW846 3550B Pantry 3022; Fayetteville, NC Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2 CASNo. 367-12-4 4165-62-2 118-79-6 4165-60-0 321-60-8 1718-51-0 Surrogate Recoveries 2-Fluorophenol Phenol-d5 2,4,6-Trlbromophenol Nitrobenzene-d5 2-Fluoroblphenyl Terphenyl-d14 Run# 1 Run# 2 Limits 40-102% 41-1000"6 42-108% 40-105% 43-107% 45-119% '~~~ .,., M~;)ii•···· ?6.~/•: .. ~g~,>· 63% 1~% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates preswnptlve evidence of a compound I
I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Client Sample ID: SS-1 (10) F46687-2 SO-Soil MADEPVPH Lab Sample ID: Matrix: Method: Project: Run#! a Run#2 Run#! Run#2 Pantry 3022; Fayetteville, NC File ID UV025610.D Initial Weight 3.32 g DF AnalY7-C'(l By 1 01/24/07 MM: Final Volume Methanol Aliquot 5.1 ml 100 ul MADEP VPH List CASNo. Compound Resuh RL CS-C8 Aliphatics (Unadj.) 6.2 C9-C12 Aliphatics (Una<lj.) 4.5 C9-Cl0 Aromatics (Unadj.) 1.6 CASNo. Surrogate Recoveries Run# 1 Run#2 460-00-4 BFB 19~.% 460-00-4 BFB 107% Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2 Prep Date n/a MDL Units 3.3 mg/kg 2.5 mg/kg 0.82 mg/kg Limits 70-130% 70-130% Prep Batch n/a Q (a) Sample was received in a bulk container but was not preseived within 48 hours of sampling. ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value Page 1 of 1 Analytical Batch GUV1472 I RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ill 19of54 liACD ,;m:. F46687 ' , h .•,c , " ,· ; C. •
I I I I I I I I I I I I I .I I I I I I Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: Lab Sample ID: Matrix: Method: Project: SS-1 (10) F46687-2 SO -Soil MADEP-EPH-98-1 SW846 3550B Pantry 3022; Fayetteville, NC File ID ZF22532.D DF 1 Analy7.ed By Run#l Run#2 01/30/07 AC r. #1 Run#2 Initial Weight Final Volume 30.1 g 2.0 ml MAEPHList CASNo. Compound Resuh RL Cll-C22 Aromatics (Unadj.) 7.1 C9-C18 Aliphatics 7.1 C19-C36 Aliphatics 7.1 Date Sampled: 01/18/07 Date Received: 01/20/07 Percent Solids: 93.2 Prep Date 01/25/07 MDL Units 7.1 mg/kg 7.1 mg/kg 7.1 mg/kg Prep Batch OP19287 Q Analytical Batch GZF1054 CASNo. Surrogate Recoveries Run# 1 Run#2 Limits 3386-33-2 1-Chlorooctadecane 66% 580-13-2 2-Bromonaphthalene 51% 84-15-1 o-Terphenyl .47% 321-60-8 2-Fluorobiphenyl 52% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range 40-140% 40-140% 40-140% 40-140% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I 111!1 Southeast ■ACCUiESla Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody
I I I I I I I I I I I I I I I I I I Ill IIACCUTEST. CHAIN OF CUSTODY 44G, V....._,M., SaiteCl5 Odoado. FL 32811 407.425.6700, Ju 407.42'.0707 F .... ...,__ 11!1 env,--Inc: PA31122 --1ao..,._0r .... 1oe ~--Zip -NC 27IIOS P,afoctNo. IICII011 PAXI: •-lecllon F1eld In/ Point Of Coledlon 0.. l,_ 8ou;,t""d -, 88-1 I S I 01111W7 1t35 oe 10 J IS.11 10 I 01/18/07 1145 DB IO --lly. □N,1-@11--0 141loy 01Do,,.------□NJFal ------1□ PIIU.CLP 011111or ___ (Daya) ------1□ -.-NC . ., -• 4 -TATls!DrMX-□ -..-ri. -1 '--j ------Ni n1,.,,I J//J1-f/ ,r,/01 /pli) •~--,=-)( II I Rev!Rd0W2006RS I I i V I J o-~•A• □-.-□-~· □--I .. I ' .. I § -• lt JI JI □ --,: r 1/ I I .:-;._"": __ ., I~ f .,. -;; T"'" -,-•-Of'.JH i·--• 0t.9-, --~ z t.J~II.. ·-·--· r-...,-. 4 F46687: Chain of Custody Page 1 of 2
I I I I I I I I I I I I I I I I I I I ACCJITEST IABQRATQBJES SAMPLE RECEIPT CQNFIBMATION ACCll"l1.t81"8 JOB NUMBER: f:41,/p ft: CUElff: ( t / tNYAw,f, PR.OJEC'f:,_.L.{,!.l..f/___,3~o,.IC.,l'-=-~----DATr.tmm RECEIVE1):,.::,:0c.,.( 41-P...,P'--_,Q ..... l _ __.()jf....._.:pp __ f OF COOLERS RECEIVED:.J_ COOU!2l TEMPS:, __ ...,2::..;•:.,,::9 _____ _ M&TIIOD OF DEIJ\11!:RY: (!£DEX) UPS ACCU'l'BST COURIER GREYHOUND AIRBW.NOIIBER8:: _______ J8L:~~<i~6:..._~~..!,;f6,(~r.~ful~2:___ _____________ _ DELIVERY ,OTHER CQQJEP INll'QRMATIQN C'08TODr SEAL NOT PIIE8ENT Oil NOT INTACT CHAIN OF CUSTODY NOT RECEIVED (OOCJ :l'8IS Rl:Qt.JE81ED IS lJJIICLEAR OR IIIS811'0 SAMPLE DATES OR TDIES UNCLEAR OR. MISSING mMPERATUBE CIUTERIA NOT M&T IP BLAlQ; fflPQBM&TXQN BIAlUt l'ROVID!:I> MISC fflFORM:!'.DQ!! l'IUIIBBR OF ltNCORBe ? 'l52. l'IUIIBBR OI' ISOSe FJBU> BlT8 ., 1,). IRllDma OR LAB ll'JLTEIUCD METALS ? l2 S:!:MPIB JNFQBMATIQN 8AIIPLE IABEL8 NOT PRESENT ON ALL IIOTTLES RRECT RUMBER OF CONTAINERS Um:D ~ RECEIV£D IMPllOP£RLY PRESERVED INSm'PICIENT VOWME FOR ANALYSIS 1"IJl!tS ON COC DOES NOT MATCH LABl!:L(S) ID'S ON COC DOES NOT MATCH IABBL(8J voe VIALS HAVE HJtADSPAClt IMACIIO BUBBLl:S) BOTTLE6 RECEIVED BUT AKALYSI8 NOT REQlJE8TED NO BOTTLB8 RECEIVED FOR ANALYSfS REQUESTED UNCLEAR. FILTERING Il'fSTRUCTION8 CU!:A1l OOMPO&Ulnu lN8TRUC110l'fS SAMPLE CONTAINER(SJ RECElVED BROm 'lb SOLIDS JAR NOT BECEIVE:D 9085 nEU> IDT NOT FROZEN Wl'l'IDl'I 48 HOUR'S RE8D>11AL cm.oanu: PR£8El'n' ( APPi.i~ TO EPA 800 8BIUE8 OR NORTH CAROLDIA ORGANICS) SUIDWtYOFOOJIID'Bl'8:...a.,u(yC~{ut&Y.EP:a---'E'-"'(l..'-'-----5.L.c.A~~~R~l~f4;z__~1e:~,'---4~N~e~~=-=~:__ _ __::O~.U=v~t-~-,~H~1~e~----n,A-eru.4,tlt,6 Fol: ,1,Al S mcemCIAN SIGllfAT1lRE/DATE ~iltfai 1/;,p 01-ll-tJr"l"BQIMCJAN SlONATURJt/DATE, ________ _,_A,,,s,..e..,o..:,:10,._,/0_,,3/,,.,,06,._ F46687: Chaln of Custody Page 2 of 2 ■.l!I.· • 23 of 54 ;"d.ACC.JieSI. F466S7 l ~ h ,.,_ r-ic, 1 r: ~ i ,. '
I I I I I I I I !I I I I I I I I I I QC Data Summaries Includes the following where applicable: • Method Blank Swmnaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries II 24 of 54 IES·ie F46667 1 H " ,-,, "' " "' ,,
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Samp]e VF284-MB File ID DF F019378.D 1 Analyzed 01/22/07 By WJ The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. Compound Result RL 67-64-1 Acetone 50 71-43-2 Benzene 5.0 108-86-1 Bromobenzene 5.0 74-97-5 Bromochloromethane 5.0 75-27-4 Bromodicbloromethane 5.0 75-25-2 Bromofonn 5.0 104-51-8 n-Butylbenzene 5.0 135-98-8 sec-Butylbenzene 5.0 98-06-6 tert-Butylbenzene 5.0 108-90-7 Chlorobenzene 5.0 75-00-3 Cbloroethane 5.0 67-66-3 Chloroform 5.0 95-49-8 o-Chlorotoluene 5.0 106-43-4 p-Chlorotoluene 5.0 75-15-0 Carbon disulfide 5.0 56-23-5 Carbon tetrachloride 5.0 75-34-3 1, 1-Dichloroethane 5.0 75-35-4 1,1-Dichloroethylene 5.0 563-58-6 1, 1-Dichloropropene 5.0 96-12-8 1,2-Dibromo-3-chloropropane 5.0 106-93-4 1,2-Dibromoethane 5.0 107-06-2 1,2-Dkhloroethane 5.0 78-87-5 1,2-Dichloropropane 5.0 142-28-9 1,3-Dichloropropane 5.0 108-20-3 Di-Isopropyl ether 5.0 594-20-7 2,2-Dichloropropane 5.0 124-48-1 Dibromochloromethane 5.0 75-71-8 Dichlorodifluorometbane 5.0 156-59-2 cis-1,2-Dichloroethylene 5.0 10061-01-5 cis-1,3-Dichloropropene 5.0 541-73-1 m-Dichlorobenzene 5.0 95-50-1 o-Dichlorobenzene 5.0 106-46-7 p-Dichlorobenzene 5.0 156-60-5 trans-1,2-Dichloroethylene 5.0 10061-02-6 trans-1,3-Dichloropropene 5.0 100-41-4 Ethyl benzene 5.0 Prep Date n/a Prep Batch n/a Page 1 of 3 Analytical Batch VF284 Method: SW846 8260B I MDL Units Q 25 2.0 2.0 2.0 2.0 2.0 3.0 2.0 2.0 2.0 3.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 3.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 3.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ll!J 25of54 A.C.:CI i I ES I. F46687 1 ' b· ,·. ' ' •'
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sam.p]e VF284-MB File ID DF F019378.D 1 Analyz.ed By 01/22/07 WJ The QC reported here applies to the following sampJes: F46687-1, F46687-2 CASNo. Compound Result RL 591-78-6 2-Hexanone 25 87-68-3 Hexachlorobutadiene 5.0 98-82-8 Isopropylbenzene 5.0 99-87-6 p-Isopropyltoluene 5.0 108-10-1 4-Methyl-2-pentanone 25 74-83-9 Methyl bromide 5.0 74-87-3 Methyl chloride 5.0 74-95-3 Methylene bromide 5.0 75-09-2 Methylene chloride 10 78-93-3 Methyl ethyl ketone 25 1634-04-4 Methyl Tert Butyl Ether 5.0 91-20-3 Naphthalene 5.0 103-65-1 n-Propylbenzene 5.0 100-42-5 Styrene 5.0 630-20-6 1, 1, 1,2-Tetrachloroethane 5.0 71-55-6 1,1,1-Trichloroethane 5.0 79-34-5 1,1,2,2-Tetrachloroethane 5.0 79-00-5 1, 1,2-Trichloroethane 5.0 87-61-6 1,2,3-Trichlorobenzene 5.0 96-18-4 1,2,3-Trichloropropane 5.0 120-82-1 1,2,4-Trichlorobenzene 5.0 95-63-6 1,2 ,4-Trimethylbenzene 5.0 108-67-8 1,3, 5-Trimethylbenzene 5.0 127-18-4 Tetrachloroethylene 5.0 108-88-3 Toluene 5.0 79-01-6 Trichloroethylene 5.0 75-69-4 Trichlorofluoromethane 5.0 75-01-4 Vinyl chloride 5.0 m,p-Xylene 10 95-47-6 o-Xylene 5.0 CASNo. Surrogate Recoveries Limits Page 2 of 3 Prep Date n/a Prep Batch Analytical Batch n/a VFZ84 Method: SW846 8260B MDL Units Q 10 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 10 ug/kg· 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 5.0 ug/kg J 10 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.5 ug/kg 2.0 ug/kg 3.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 2.0 ug/kg 3.0 ug/kg 2.0 ug/kg I 1868-53-7 Dibromofluoromethane 106% 80-121% 2037-26-5 Toluene-OS !M% 71-130% m 26of54 faACa.JiESI. f46687 I a b " ,. ,, I i ,. i " ,
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VF284-MB File ID DF F019378.D 1 · Anal)7.ed By 01/22/07 WJ The QC reported here applies to the following samples: F46687-l, F46687-2 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 .98%>. 91l% Limits 59-148% 77-123% Prep Date n/a Page 3 of 3 Prep Batch Analytical Batch n/a VF284 Method: SW846 8260B I
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VF284-BS File ID DF F019377.D 1 Anal)'7.C(l 01/22/07 By WJ The QC reported here applies to the following samples: F46687-1, F46687-2 Spike BSP CASNo. Compound ug/kg ug/kg 67-64-1 Acetone 250 293 71-43-2 Benzene 50 55.6 108-86-1 Bromobenzene 50 53.6 74-97-5 Bromochloromethane 50 51.2 75-27-4 Bromodichloromethane 50 52.9 75-25-2 Bromoform 50 53.7 104-51-8 n-Butylbenzene 50 56.9 135-98-8 sec-Butylbenzene 50 56.9 98-06-6 tert-Butylbenzene 50 55.7 108-90-7 Chlorobenzene 50 53.5 75-00-3 Cbloroethane 50 48.3 67-66-3 Chloroform 50 55.4 95-49-8 o-Chlorotoluene 50 53.3 106-43-4 p-Chlorotoluene 50 54.8 75-15-0 Carbon disulfide 50 56.3 56-23-5 Carbon tetrachloride 50 56.1 75-34-3 1, 1-Dichloroethane 50 55.1 75-35-4 1, 1-Dichloroethylene 50 54.5 563-58-6 1, 1-Dicbloropropene 50 57.5 96-12-8 l ,2-Dibromo-3-chloropropane 50 54.8 106-93-4 1,2-Dibromoethane 50 52.9 107-06-2 1,2-Dichloroethane 50 55.6 78-87-5 1,2-Dichloropropane 50 56.3 142-28-9 1,3-Dichloropropane 50 52.5 108-20-3 Di-Isopropyl ether 50 55.4 594-20-7 2 ,2-Dichloropropane 50 56.3 124-48-1 Dibromochloromethane 50 51.8 75-71-8 Dichlorodifluoromethane 50 52.4 156-59-2 cis-1, 2-Dichloroethylene 50 53.1 10061-01-5 cis-1, 3-Dichloropropene 50 57.9 541-73-1 m-Dichlorobenzene 50 54.6 95-50-1 o-Dichlorobenzene 50 55.4 106-46-7 p-Dichlorobenzene 50 54.8 156-60-5 trans-1,2-Dichloroethylene 50 54.7 10061-02-6 trans-1,3-Dichloropropene 50 58.3 100-41-4 Ethylbenzene 50 53.1 Prep Date n/a BSP % Limits ~f7 61-144 in 78-130 19? 78-123 102 '• 72-122 106 73-122 107 70-139 114 80-138 ll4 .• · 82-132 ·•11·1••·•.·.i·••········ 79-130 107•/. 83-122 97 61-153 lll 79-129 107 •. 77-123 llQ•.·· 78-129 H3. 61-142 112 79-135 110 77-132 1()9 66-132 vs 81-133 110 67-129 ... ., ·, 106 77-126 111 78-129 113 74-127 105 78-118 ·lll 75-131 113 . 80-137 104 78-117 105 35-162 106 74-123 gG••·•· 79-130 W9 82-126 111 ··•. 83-123 110 84-124 109 77-129 111· 87-131 106 82-124 Prep Batch n/a Page 1 of 3 Analytical Batch VF284 I Method: SW846 8260B IID .. 2s of 54 (IACCUTEST. F46687 !;ih,,·1,:.it:ri,!
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample VF284-BS File ID DF F019377.D 1 Analp.ed 01/22/07 By WJ Prep Date n/a The QC reported here applies to the following samples: F46687-l, F46687-2 Spike BSP BSP CASNo. Compound ug/kg ug/kg % Limits 591-78-6 2-He:xanone 250 326 !3Q 67-130 87-68-3 Hexacblorobutadiene 50 57.9 116 77-150 98-82-8 Isopropylbenzene 50 56.8 114 82-133 99-87-6 p-lsopropyltoluene 50 56.7 1~3\·•·· 82-132 108-10-1 4-Methyl-2-pentanone 250 302 l?l 69-125 74-83-9 Methyl bromide 50 47.7 95 60-146 74-87-3 Methyl chloride 50 67.8 136 58-163 74-95-3 Methylene bromide 50 56.7 113 75-128 75-09-2 Methylene chloride 50 65.1 13(f 62-140 78-93-3 Methyl ethyl ketone 250 321 128. 66-134 1634-04-4 Methyl Tert Butyl Ether 50 54.9 110 70-131 91-20-3 Naphthalene 50 57.2 114 59-143 103-65-1 n-Propylbenzene 50 54.7 MW 78-129 100-42-5 Styrene 50 53.5 JOT 79-123 630-20~6 1,1,1,2-Tetrachloroethane 50 52.2 104. 81-121 71-55-6 1, 1, I-Trichloroethane 50 55.2 110 80-133 79-34-5 1,1,2,2-Tetrachloroethane 50 55.8 112 70-128 79-00-5 1,1,2-Trichloroethane 50 52.7 lQ.& 76-118 87-61-6 1,2,3-Trichlorobenzene 50 56.9 l14 78-136 96-18-4 1,2 ,3-Trichloropropane 50 55.0 110 74-125 120-82-1 1,2,4-Trichlorobenzene 50 56.9 114 82-137 95-63-6 1,2,4-Trimethylbenzene 50 54.7 109 77-129 108-67-8 1,3,5-Trimethylbenzene 50 55.6 111 79-129 127-18-4 Tetrachloroethylene 50 50.2 100 79-132 108-88-3 Toluene 50 52.1 104 80-123 79-01-6 Trichloroethylene 50 56.9 114 78-132 75-69-4 Trichlorofluoromethane 50 49.2 98· 67-149 75-01-4 Vinyl chloride 50 49.9 '}@ 60-145 m,p-Xylene 100 107 107 82-128 95-47-6 o-Xylene 50 54.3 109 82-126 CASNo. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 104% 80-121% 2037-26-5 Toluene-DB I~&% 71-130% Prep Batch n/a Page 2 of3 Analytical Batch VF284 Method: SW846 8260B I
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VF284-BS File ID DF F019377.D 1 Analyzed By 01/22/07 WJ The QC reported here applies to the following samples: F46687-1, F46687-2 CAS No. Surrogate Recove:ries 460-00-4 4--Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 BSP 100% W~% Limits 59-148% 77-123% Prep Date n/a Page 3 of 3 Prep Batch Analytical Batch n/a VF284 Method: SW846 8260B I
I I I I I I -I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46687 Page 1 of 3 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample F46556-1MS F46556-1MSD F46556-1 a File ID DF F019383.D 1 F019384.D 1 F019382.D 1 Analyzed 01/22/07 01/22/07 01/22/07 By WJ WJ WJ The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. Compound 67-64-1 Acetone 71-43-2 Benzene 108-86-1 Bromobenzene 74-97-5 Bromochlorometbane 75-27-4 Bromodichlorometbane 75-25-2 Bromoform 104-51-8 n-Butylbenzene 135-98-8 sec-Butylbenzene 98-06-6 tert-Butylbenzene 108-90-7 Chlorobenzene 75-00-3 Chloroethane 67-66-3 Chloroform 95-49-8 o-Chlorotoluene 106-43-4 p-Chlorotoluene 75-15-0 Carbon disulfide 56-23-5 Carbon tetrachloride 75-34-3 1, 1-Dichloroethane 75-35-4 1, 1-Dichloroethylene 563-58-6 1, 1-Dichloropropene 96-12-8 1,2-Dibromo-3-chloropropane 106-93-4 1,2-Dibromoetbane 107-06-2 1,2-Dlchloroethane 78-87-5 1,2-Dichloropropane 142-28-9 1,3-Dichloropropane 108-20-3 Di-Isopropyl ether 594-20-7 2,2-Dichloropropane 124-48-1 Dibromochloromethane 75-71-8 Dichlorodifl.uoromethane 156-59-2 ds-1,2-Dichloroetbylene 10061-01-5 ds-1,3-Dichloropropene 541-73-1 m-Dichlorobenzene 95-50-1 o-Dichlorobenzene 106-46-7 p-Dichlorobenzene 156-60-5 trans-1,2-Dichloroethylene 10061-02-6 trans-1,3-Dichloropropene 100-41-4 Ethylbenzene F46S56-1 Spike ug/kg Q ug/kg 35.3 I 296 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 5.9U 59.2 Prep Date n/a n/a n/a MS MS ug/kg % Prep Batch n/a n/a n/a Analytical Batch VF284 VF284 VF284 Method: SW846 8260B MSD MSD Limits ug/kg % RPD Rec/RPD I 244 •i1i· ....•. · .. ·_.·. 285 84::?:-. 61-144/29 111 J.os 66.0 62.3 63.0 106 59.7 56.2 95 53.4 62.4 105 56.3 51.5 87. 46.6 59.3 ~00 52.5 64.2 10s.<· .. 57.4 65.8 111·•··. 60.6 64.8 109 60.0 62.4 105 55.9 68.5 116 62.5 64.3 109 59.0 66.4 l:fa 61.4 67.6 H•·•· 62.5 71.8 121 .. i 63.5 65.4 110 62.0 67.4 114 63.2 69.4 117 63.6 45.7 77 41.0 53.0 gq 49.1 59.0 1()() .. 53.3 62.7 106 61.5 54.8 93 50.0 60.1 102 60.0 66.8 113 59.7 57.4 97 . 51.7 68.0 ,1M 59.1 62.0 ··105 59.6 63.7 ·108 59.3 64.1 108 59.6 62.5 106 57.9 64.1 108 59.6 66.0 111 62.8 60.4 102 ·. 57.2 65.0 llQ 59.1 100 90 94 .18·· ·88 . -.~~ .. ··.• .. •·. 102 101 94 105 99 103. !Qf-1()7 104 106 107 69 82 89.< 103 84 101 100 87 99 ... 1()0 }()() 100 97 100 105 96 rut 9 0 11 78-130/25 78-123/30 72-122/23 73-122/25 70-139/26 80-138/31 82-132/29 79-130/29 83-122/23 61-153/31 79-129/27 77-123/31 78-129/29 61-142/27 79-135/29 77-132/26 66-132/27 81-133/26 67-129/29 77-126/24 78-129/24 74-127/27 78-118/26 75-131/24 80-137/28 78-117/27 35-162/30 74-123/26 79-130/23 82-126/29 83-123/28 84-124/28 77-129/27 87-131/27 82-124/25 31 of 54 ~·•iESl. F466S.7 i. " i'; ('i I' fi, t ·,: ~ : (": ,
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Page 2 of3 Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch F46556-1MS F019383.D 1 01/22/07 WJ n/a n/a VF284 F46556-1MSD F019384.D 1 01/22/07 WJ n/a n/a VF284 F46556-1 a F019382.D 1 01/22/07 WJ n/a n/a VF284 The QC reported here applies to the follow:ing samples: Method: SW846 8260B F46687-1, F46687-2 F46556-1 Spilce MS MS MSD MSD Limits CASNo. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD 591-78-6 2-Hexanone 29U 296 244 82 224 75 9 67-130/29 87-68-3 Hexachlorobutadiene 5.9U 59.2 43.9 :74~ 38.1 &1r: .: 14. 77-150/36 98-82-8 Isopropylbenzene 5.9U 59.2 69.2 ,:1_17, .· 61.0 102 1:r· / 82-133/27 99-87-6 p-lsopropyltoluene 5.9U 59.2 63.8 108 57.0 96: '·,· ... Jf,, . 82-132/29 t: 108-10-1 4-Methyl-2-pentanone 29U 296 234 79 222 15,< 5. 69-125/24 74-83-9 Methyl bromide 5.9U 59.2 65.3 Ho 56.5 95 14 60-146/31 74-87-3 Methyl chloride 5.9U 59.2 84.2 142, . 80.6 135 4 •.' 58-163/26 74-95-3 Methylene bromide 5.9U 59.2 57.9 98, . 52.6 88, 10, .... , " 75-128/26 75-09-2 Methylene chloride 41.3 V 59.2 89.6 82 100 ~s•··• 11 62-140/25 78-93-3 Methyl ethyl ketone 29U 296 213 1t 207 69 3 66-134/23 1634~04-4 Methyl Tert Butyl Ether 5.9U 59.2 52.4 39·· 49.8 84 5 70-131/25 91-20-3 Naphthalene 5.9U 59.2 49.6 84 44.3 74 11· 59-143/31 103-65-1 n-Propylbenzene 5.9U 59.2 65.3 110, 59.0 99' 10 78-129/29 100-42-5 Styrene 5.9U 59.2 61.9 '105 55.0 92 .· 12 79-123/28 630-20-6 1,1,1,2-Tetrachloroetbane 5.9U 59.2 62.3 105' :,:_,. 56.7 95. ,,,JJ''·:'' 81-121/25 71-55-6 1, 1, I-Trichloroethane 5.9U 59.2 71.0 120, 62.6 105 13 .,•·· 80-133/27 79-34-5 1,1,2,2-Tetrachloroethane 5.9U 59.2 49.1 83· 46.5 78 5 70-128/30 79-00-5 1, 1,2-Trichloroethane 5.9U 59.2 53.4 90 49.4 83 '8 76-118/28 87-61-6 1,2 ,3-Trichlorobenzene 5.9U 59.2 55.0 ,93 ,:' 49.5 8r, 11 78-136/34 96-18-4 1,2 ,3-Trichloropropane 5.9U 59.2 49.6 34/•:,•;· 46.4 7~ t 74-125/30 120-82-1 1,2,4-Trichlorobenzene 5.9U 59.2 56.9 ~6< : 51.6 8,7 1() ,_ 82-137/32 95-63-6 1,2,4-Trimethylbenzene 5.9U 59.2 65.7 111 59.2 99 10 77-129/29 108-67-8 1,3,5-Trimethylbenzene 5.9U 59.2 66.0 111 60.7 102 s· 79-129/31 127-18-4 Tetrachloroethylene 5.9U 59.2 86.3 146* 85.8 144* 79-132/27 108-88-3 Toluene 5.9 U 59.2 61.0 103/:' 59.6 l!)()< 2 80-123/26 79-01-6 Trichloroethylene 5.9U 59.2 71.5 121 64.0 .iot '11 ... '' 78-132/28 75-69-4 Trichlorofluorometbane 5.9U 59.2 68.6 116 '57.4 96.'' JS. 67-149/29 75-01-4 Vinyl chloride 5.9U 59.2 62.8 io6 56.8 95 10 60-145/29 m,p0Xylene 12U 118 133 112 118 99 12 82-128/25 95-47-6 o-Xylene 5.9U 59.2 67.2 114 60.0 101 u 82-126/25 CASNo. Surrogate Recoveries MS MSD F46556-l Limits 1868-53-7 Dibromofluoromethane ioi% 99% ,, 113%' 80-121% 2037-26-5 Toluene-OS ~% '·1-1?·:, '~% ,9t%' 71-130% ,fl,. w I
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46687 Account: SEINCR SEI Environment.al-Raleigh Project: Pantry 3022; Fayetteville, NC Sample F46556-1MS F46556-1MSD F46556-l a File ID DF F019383.D 1 F019384.D 1 F019382.D 1 Analyz.ed 01/22/07 01/22/07 01/22/07 By WJ WJ WJ Prep Date n/a n/a n/a Prep Batch n/a n/a n/a Page 3 of3 Analytical Batch VF284 VF284 VF284 The QC reported here applies to the following samples: Method: SW846 8260B F46687-1, F46687-2 CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 MS ,98% !i(96' MSD 99!¾. ' i'.¾> F465S6-1 Limits ltii% . 59-148% ill%.·· 11-123% (a) Sample was received in a bulk container and preserved within 48 hours of sampling. II
I I I I I I I I I I I I I I I I I I I llml· Southeast 1'iACCU1e&r. ~ 0''-Section 5 QC Data Summaries Includes the following where applicable: • Method Blank Swnmaries • Blank Spike Summaries • Matrix Spilce and Duplicate Summaries
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19264-MB L035507 .D 1 Analyzed 01/25/07 By NJ The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. Compound Result RL 65-85-0 Benzoic acid NO'. 830 ._,·::-.; 95-57-8 2-Cblorophenol ND ... 170 59-50-7 4-Cbloro-3-methyl phenol ·~··, .. 170 120-83-2 2,4-Dichlorophenol ·'l'ffi ' 170 105-67-9 2 ,4-Dimethylpheool Nil 170 51-28-5 2 ,4-Dinitropbeool Nti 830 534-52-1 4,6-Dinitro-o-cresol Ni?>: .......... •· .. ' 330 95-48-7 2-Methylphenol •ND··: .. ,· .• 170 I·,:·:,•.'.''.·,.:,,··.·,, 3&4-Methylphenol ND.··•.···•·•> .. ·· i 170 88-75-5 2-Nitropheool NI)'•.•· .. \ 170 100-02-7 4-Nitrophenol NI)i',·•.·< 830 87-86-5 Pentachlorophenol ·•NP 830 108-95-2 Phenol ND .170 95-95-4 2,4, 5-Trichlorophenol ND· 170 88-06-2 2,4,6-Trichlorophenol ·$> 170 83-32-9 Acenaphthene mr 170 208-96-8 Acenaphthylene ND·.·. 170 62-53-3 Aniline NIL ,·· 330 120-12-7 Anthracene ~ii. 170 92-87-5 Benzidine ·,·1700 56-55-3 Benzo(a)anthracene NP.· 170 50-32-8 Benzo(a)pyrene ND 170 205-99-2 Benzo(b)fluoranthene ND 170 191-24-2 Benzo(g,h,i)perylene NP,· 170 207-08-9 Benzo(k)fluoranthene !ID,' 170 101-55-3 4-Bromophenyl phenyl ether ND 170 85-68-7 Butyl benzyl phthalate ND 330 100-51-6 Benzyl Alcohol Ni) 170 91-58-7 2-Chloronaphthalene Nb•··•< 170 106-47-8 4-Chloroaniline ·NP·· 330 86-74-8 Carbazole NJ) ' 170 218-01-9 Chrysene ND' 170 111-91-1 bis(2-Chloroetho:xy)methane ND 170 111-44-4 bis(2-Chloroethyl)ether ND 170 108-60-1 bis(2-Chloroisopropyl)ether ND 170 Nii '' 7005-72-3 4-Chloropbenyl phenyl ether ,' 170 Prep Date 01/24/07 MDL Units 330 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 330 ug/kg 67 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 330 ug/kg 330 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 170 ug/kg 33 ug/kg 830 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 67 ug/kg 33 ug/kg 33 ug/kg 83 ug/kg 33 ug/kg 33 ug/kg 130 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 67 ug/kg 33 ug/kg 33 ug/kg Prep Batch OP19264 Page 1 of3 Analytical Batch SL1820 Method: SW846 8270C I Q ll!rl .. · · ... 35 of54 ACCUl·ESM.
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19264-MB L035507.D 1 Analyzed 01/25/07 By NJ The QC reported here applies to the following samples: F46687-l, F46687-2 CASNo. Compound Result RL 95-50-1 1,2-Dichlorobenzene •NP•. 170 122-66-7 1, 2-Dipbenylhydrazine ··l'\!lI)>·\· 170 541-73-1 1, 3-Dichlorobenzene . NP:: . 170 106-46-7 1,4-Dichlorobenzene ND 170 121-14-2 2,4-Dinitrotoluene ND 170 606-20-2 2,6-Dinitrotoluene ND 170 91-94-1 3, 3' -Dichlorobenzidine ND 330 53-70-3 Dibenzo(a,b)antbracene ·•:NR···•· 170 132-64-9 Dibenzofuran NQ< 170 84-74-2 Di-n-butyl pbtbalate ND 330 117-84-0 Di-n-octyl pbtbalate ND 330 84-66-2 Diethyl phtbalate ND 330 131-11-3 Dimethyl phthalate M? 330 117-81-7 bis(2-Ethylhexyl)phtbalate 1'1p .•. 330 206-44-0 Fluorantbene •NI) 170 86-73-7 Fluorene ND 170 118-74-1 Hexachlorobenzene ND 170 87-68-3 Hexacblorobutadiene ND 170 77-47-4 Hexachlorocyclopentadiene ·M).· 170 67-72-1 Hexacbloroetbane m.>. 170 193-39-5 Indeno(l,2,3-cd)pyrene ND•···•. .· 170 78-59-1 lsophorone ND. 170 90-12-0 1-Methylnaphtbalene ND 170 91-57-6 2-Methylnaphthalene ND 170 88-74-4 2-Nitroaniline ND 330 99-09-2 3-Nitroaniline ND·. 330 100-01-6 4-Nitroaniline ND<• 330 91-20-3 Naphthalene ND 170 98-95-3 Nitrobenzene ND 170 62-75-9 N-Nitrosodimetbylamine ND 330 621-64-7 N-Nitroso-di-n-propylamine .NP.••·•·i<···· 170 86-30-6 N-Nitrosodipbenylamine NJ>··· 170 85-01-8 Phenanthrene ND 170 129-00-0 Pyrene ND 170 110-86-1 Pyridine ND 330 120-82-1 1,2 ,4-Trichlorobenzene l'-,j;p 170 Prep Date 01/24/07 MDL Units 33 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 67 ug/kg 67 ug/kg 170 ug/kg 67 ug/kg 33 ug/kg 83 ug/kg 170 ug/kg 83 ug/kg 83 ug/kg 170 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 67 ug/kg 67 ug/kg 67 ug/kg 67 ug/kg 33 ug/kg 33 ug/kg 33 ug/kg 83 ug/kg 83 ug/kg 120 ug/kg 33 ug/kg 33 ug/kg 130 ug/kg 67 ug/kg 33 ug/kg 33 ug/kg 67 ug/kg 170 ug/kg 33 ug/kg Prep Batch OP19264 Page 2 of 3 Analytical Batch SL1820 Method: SW846 8270C Q
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19264-MB 1.035507.D 1 Analyzed 01/25/07 By NJ The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 53% , 40-102% 4165-62-2 Phenol-d5 52%' 41-1000/4 118-79-6 2 ,4, 6-Tribromophenol 71'% · 42-108% ·, ~ 4165-60-0 Nitrobenzene-d5 5l%' 40-105% 321-60-8 2-Fluorobiphenyl 52%0 . 43-107% 1718-51-0 Terphenyl-dl4 86% 45-119% Prep Date 01/24/07 Prep Batch OP19264 Page 3 of 3 Analytical Batch SL1820 Method: SW846 8270C tlmi 37of54 CiACO iiESi. F46687 t'.1b,',i"rtt)r·\~:~
I I Blank Spike Summary Page 1 of 3 Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh I Project: Pantry 3022; Fayetteville, NC Sample File ID OF Analy:t.ed By Prep Date Prep Batch Analytical Batch OP19264-BS L035506.D 1 01/25/07 NJ 01/24/07 . OP19264 SL1820 I tr. N I The QC reported here applies to the following samples: Method: SW846 8270C I F46687-1, F46687-2 I Spike BSP BSP I CASNo. Compound ug/kg ug/kg % Limits 65-85-0 Benzoic acid 3330 2480 :S7-J. 44-116 95-57-8 2-Chlorophenol 1670 1110 57> 54-97 I 59-50-7 4-Chloro-3-melhyl phenol 1670 1310 79. 59-102 120-83-2 2,4-Dichlorophenol 1670 1170 ··10 60-101 105-67-9 2,4-Dimethylphenol 1670 1000 60,' 49-89 51-28-5 2,4-Dinitrophenol 3330 1740 52 39-107 I 534-52-1 4,6-Dinitro-o-cresol 3330 2750 83 58-109 95-48-7 2-Methylphenol 1670 1080 6~\ 53-94 3&4-Methylphenol 3330 2190 66 .. < 54-95 I 88-75-5 2-Nitrophenol 1670 1150 69 55-96 I 100-02-7 4-Nitrophenol 3330 2320 70 56-106 87-86-5 Pentachlorophenol 3330 2670 80 50-115 108-95-2 Phenol 1670 1090 65 55-99 I 95-95-4 2 ,4, 5-Trichlorophenol 1670 1320 ,7p 60-101 88-06-2 2,4, 6-Trichlorophenol 1670 1300 78 60-100 83-32-9 Acenaphthene 1670 1230 74 59-97 208-96-8 Acenaphthylene 1670 1280 71 58-98 I I 62-53-3 Aniline 1670 925 56/i 38-92 120-12-7 Anlhracene 1670 1370 8~. 61-104 56-55-3 Benzo(a)anthracene 1670 1420 Mi'' 60-106 I 50-32-8 Benzo(a)pyrene 1670 1410 85 59-102 205-99-2 Benzo(b)fluoranthene 1670 1430 86 60-107 191-24-2 Benzo(g,h,i)perylene 1670 1310 79 56-103 207-08-9 Benzo(k)tluoranthene 1670 1420 85 61-107 I 101-55-3 4-Bromophenyl phenyl ether 1670 1340 a() 60-104 85-68-7 Butyl benzyl phthalate 1670 1520 9L 57-110 100-51-6 Benzyl Alcohol 1670 1100 66 51-102 I 91-58-7 2-Chloronaphthalene 1670 1170 70 57-95 106-47-8 4-Chloroaniline 1670 817 49 19-85 86-74-8 Carbazole 1670 1370 82 60-106 218-01-9 Chrysene 1670 1420 85 ·.• 60-107 I 111-91-1 bis(2-Chloroethoxy)methane 1670 1050 63 51-89 111-44-4 bis(2-Chloroethyl)ether 1670 1070 64. 50-96 108-60-1 bis(2-Chloroisopropynether 1670 1040 62. 44-94 I 7005-72-3 4-Chlorophenyl phenyl ether 1670 1260 76 60-101 95-50-1 1,2-Dichlorobenzene 1670 1030 &2 . 47-91 I ll!i 38 of 54 I At".O i i ES I. F46687 i .'J 1~ ... ,:..~ t a ,: i i-. ~
I I Blank Spike Summary Page 2 of3 Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh I Project: Pantry 3022; Fayetteville, NC Sample File ID DF Analyz.ed By Prep Date Prep Batch Analytical Batch OP19264-BS L035506.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 I U1 N I The QC reported here applies to the following samples: Method: SW846 8270C I F46687-1, F-46687-2 I Spike BSP BSP I CASNo. Compound ug/kg ug/kg % Limits 122-66-7 1,2-Diphenylhydrazine 1670 1350 $ii 58-104 541-73-1 1,3-Dicblorobenzene 1670 983 59 45-86 I 106-46-7 1,4-Dichlorobenzene 1670 991 _59 45-88 121-14-2 2,4-Dinitrotoluene 1670 1400 84 59-103 606-20-2 2,6-Dinitrotoluene '1670 1300 78 57-99 91-94-1 3,3' -Dichlorobenzidine 1670 967 58 34-88 I 53-70-3 Dibenzo(a,h)anthracene 1670 1350 sf 57-105 132-64-9 Dibenzofuran 1670 1210 73.-58-103 84-74-2 Di-n-butyl phthalate 1670 1390 sa:i·-59-105 I 117-84-0 Di-n-octyl phthalate 1670 1500 90 59-117 84-66-2 Diethyl phthalate 1670 1240 74·. 59-106 131-11-3 Dimethyl phthalate 1670 1360 82 60-100 117-81-7 bis(2-Ethylhexyl)phthalate 1670 1520 9f 57-111 I 206-44-0 Fluoranthene 1670 1410 85 60-110 86-73~7 Fluorene 1670 1310 7~ 60-99 118-74-1 Hexachlorobenzene 1670 1340 80 58-103 87-68-3 Hexachlorobutadiene 1670 1070 64 49-95 I 77-47-4 Hexachlorocyclopentadiene 1670 922 :55:, 36-94 67-72-1 Hexacbloroethane 1670 966 58 44-89 193-39-5 lndeno(l ,2,3-cd)pyrene 1670 1400 84 57-104 I 78-59-1 Isopborone 1670 1210 73, 58-97 90-12-0 1-Methylnaphthalene 1670 1110 67 55-93 91-57-6 2-Methylnaphthalene 1670 1100 66 57-103 88-74-4 2-Nitroaniline 1670 1260 75··· 53-106 I 99-09-2 3-Nitroaniline 1670 922 55 29-85 100-01-6 4-Nitroaniline 1670 1260 76, -49-104 91-20-3 Naphthalene 1670 1090 65 54-93 I 98-95-3 Nitro benzene 1670 1090 '.65, 53-92 62-75-9 N-Nitrosodimethylamine 1670 919 55 37-88 621-64-7 N-Nitroso-di-n-propylamine 1670 1060 64 49-94 86-30-6 N-Nitrosodiphenylamine 1670 1290 77 53-107 I 85-01-8 Phenanthrene 1670 1370 82 61-103 129-00-0 Pyrene 1670 1470 88 58-109 110-86-1 Pyridine 1670 643 39·• 30-68 I 120-82-1 1,2,4-Tricblorobenzene 1670 1100 66 · 52-93 I -~~~;,;~ I F466ll7 l A I"• b 1· 1-1" ,_·, r; (': .~
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantcy 3022; Fayetteville, NC Sam.pk File ID DF OP19264-BS L035506.D 1 Analyzed 01/25/07 By NJ The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol .. ~.<ki. 40-102% 4165-62-2 Phenol-d5 .64% 41-100% 118-79-6 2, 4, 6-Tribromophenol 75% 42-108% 4165-60-0 Nitrobenzene-d5 6!% .. 40-105% 321-60-8 2-Fluorobiphenyl 64% 43-107% 1718-51-0 Terpbenyl-d14 81% 45-119% Prep Date 01/24/07 Prep Batch OP19264 Page 3 of3 Analytical Batch S11820 Method: SW846 8270C I
I I Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh I Project: Pantry 3022; Fayetteville, NC Sample File ID DF Analyn,d By Prep Date Prep Batch Analytical Batch OP19264-MS L035517.D 1 01/25/07 NJ 01/24/07 OP19264 S11820 I OP19264-MSD 1035518.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 O'l F46676-5 L035516.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 "' I The QC reported here applies to the following samples: Method: SW846 8270C I F46687-l, F46687-2 I F46676-S Spike MS MS MSD MSD Limits CASNo. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD I 65-85-0 Benzoic acid 850U 3430 2120 .62 ·. 1600 46': ,28 44-116/36 85 <.' ;-9· 54-97/31 95-57-8 2-Chloropheool 170 U 1720 1460 1340 :1s.·. I 59-50-7 4-Chloro-3-methyl phenol 170U 1720 1520 89 1420 82 7 59-102/27 120-83-2 2, 4-Dichlorophenol 170U 1720 1540 ~,' 1430 83 7 60-101/30 105-67-9 2, 4-Dimethylphenol 170 U 1720 1320 .77 ·: 1220 11:: ,8 49-89/31 51-28-5 2, 4-Dinitrophenol 850 U 3430 1180 34* ' 928 2!*• :· .24' 39-107/40 I 534-52-1 4, 6-Dinitro-o-cresol 340U 3430 2070 60 1730 50* · is . 58-109/37 95-48-7 2-Methylphenol 170 U 1720 1460 85 1340 78 9 53-94/29 3&4-Methylphenol 170U 3430 2920 ~?•.•. 2670 .77 ·, 9 54-95/31 I 88-75-5 2-Nitrophenol 170U 1720 1430 83 1350 78 5•··.:· 55-96/30 100-02-7 4-Nitrophenol 850U 3430 2550 74: 2410 70 .. 6 56-106/29 87-86-5 Pentachlorophenol 850U 3430 2800 82 2550 .74 9 50-115/33 108-95-2 Phenol 170U 1720 1410 ~2, 1320 7~. ·7 55-99/28 I 95-95-4 2,4 ,5-Trichlorophenol 170 U 1720 1560 w 1460 85 ;7· "· 60-101/28 88-06-2 2, 4, 6-Trichlorophenol 170U 1720 1540 90 • 1470 .~5 5 60-100/27 83-32-9 Acenaphthene 170U 1720 1500 87 1380 ~o 8, 59-97/29 208-96-8 Acenaphthylene 170U 1720 1530 '89 1430 83 ·. '!//,'·'·:'. 58-98/30 I 62-53-3 Aniline 340U 1720 1220 'it 1180 68 .. J\ 38-92/38 9() ·,. ;·-120-12-7 Anthracene 170U 1720 1550 1470 85 5 61-104/29 92-87-5 Benzidine 1700 U 1720 941 55 1000 58 6 10-151/50 I 56-55-3 Benzo(a)anthracene 170U 1720 1560 .91··, 1500 87 4··, 60-106/31 50-32-8 Benzo(a)pyrene 170U 1720 1600 93 ,: , • 1530 89/ ~: 59-102/32 205-99-2 Benzo(b)fluoranthene 170U 1720 1640 96' 1540 89· ' 6 60-107/31 191-24-2 Benzo(g,h,i)perylene 170U 1720 1550 9Q 1490 86 4 56-103/32 I 207-08-9 Benzo(k)fluoraothene 170U 1720 1610 ,9,4, 1530 89 5 61-107/30 101-55-3 4-Bromophenyl phenyl ether 170U 1720 1530 89i 1450 84\ 5•, 60-104/26 85-68-7 Butyl benzyl phthalate 340U 1720 1720 ioo, 1640 ,95 ·•··5 57-110/28 I 100-51-6 Benzyl Alcohol 170U 1720 1460 ;85 1330 ·rr· 9 · 51-102/34 91-58-7 2-Chloronaphthalene 170U 1720 1460 85· 1350 78 Si. 57-95/28 106-47-8 4-Chloroaoiline 340U 1720 1070 62 1010 59 6 19-85/34 86-74-8 Carbazole 170U 1720 1560 91 1530 89 2 60-106/30 I 218-01-9 Chrysene 170 U 1720 1550 :90 1480 86 5, 60-107/31 111-91-1 bis(2-Chloroethoxy)methane 170U 1720 1360 79 1260 73 8 51-89/30 111-44-4 bis(2-Chloroethyl)ether 170 U 1720 1400 82 1340 78 4 50-96/33 108-60-1 bis(2-Chloroisopropyl)ether 170U 1720 1360 79· ... 1260 73 8 .. 44-94/32 I 7005-72-3 4-Chlorophenyl phenyl ether 170U 1720 1470 86 1350 78 9. 60-101/26 I 11!1 41 of54 ACCUIESF: I F46687 i .~ h ,1 i• > I. c: r i ;•, ~
I I Matrix Spike/Matrix Spike Du.plicate Summary Page 2 of3 Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh I Project: Pantry 3022; Fayetteville, NC Sample File ID DF Anal}'7,e(i By Prep Date Prep Batch Analytical Batch OP19264-MS L035517.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 I OP19264-MSD L035518.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 c, F46676-5 L035516.D 1 01/25/07 NJ 01/24/07 OP19264 SL1820 t.,.> I The QC reported here applies to the following samples: Method: SW846 8270C I F46687-1, F46687-2 I F46676-S Spike MS MS MSD MSD Limits I CASNo. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD 95-50-1 1,2-Dichlorobenzene 170 U 1720 1320 17/ 1250 72 47-91/35 122-66-7 1,2-Diphenylhydrazine 170 U 1720 1550 ~' 1460 85 58-104/27 I 541-73-1 1,3-Dichlorobenzene 170U 1720 1250 1180 "68 -45-86/36 106-46-7 1,4-Dichlorobenzene 170U 1720 1250 if 1190 69i_.-. 45-88/36 121-14-2 2 ,4-Dinitrotoluene 170U 1720 1570 92-i. :_,. 1440 8~ :· --59-103/30 606-20-2 2,6-Dinitrotoluene 170U 1720 1510 88 --1420 '82 57-99/30 I 91-94-1 3,3 '-Dichlorobenzidine 340U 1720 1440 M 1390 81 34-88/31 53-70-3 Dibenzo(a,h)anthracene 170U 1720 1630 95>-. 1500 ·s1 57-105/29 132-64-9 Dibenzofuran 170U 1720 1430 sf•••-1330 .11· 58-103/27 Di-n-butyl pbthalate 340U I'"·• 86 59-105/27 I 84-74-2 1720 1560 91 1490 117-84-0 Di-n-octyl phthalate 340U 1720 1810 106-1680 97 59-117/28 84-66-2 Diethyl phthalate 340U 1720 1400 -82,: 1320 76 59-106/27 131-11-3 Dimethyl phthalate 340U 1720 1510 88 • 1440 8~: 60-100/26 I 117-81-7 bis(2-Ethylbexyl)phthalate 340U 1720 1690 9!)\,--· 1600 93 57-111/29 206-44-0 Fluoranthene 170U 1720 1570 92 1500 87 60-110/32 86-73-7 Fluorene 170U 1720 1500 .87, --1420 82 60-99/30 I 118-74-1 Hexacblorobenzene 170U 1720 1510 :~." 1440 •83 58-103/27 87-68-3 He.xacblorobutadiene 170U 1720 1340 -78, 1220 71·. 49-95/33 77-47-4 Hexachlorocyclopentadiene 170U 1720 686 ,40 , 632 37· 36-94/41 ., 67-72-1 Hexachloroethane 170U 1720 1210 71 lllO 64 44-89/38 193-39-5 Indeno(l ,2,3-cd)pyrene 170U ,' :, 1580 57-104/33 I 1720 1650 96 -._ 92 78-59-1 lsophorone 170U 1720 1510 ·88 1410 82 · --_ 58-97/30 90-12-0 1-Methylnaphtbalene 170U 1720 1400 '8Z: 1290 75 8_' 55-93/33 91-57-6 2-Methylnaphthalene 170U 1720 1460 85·-1350 78 8 57-103/32 I 88-74-4 2-Nitroaniline 340U 1720 1450 8li 1400 81 4 53-106/29 99-09-2 3-Nitroaniline 340U 1720 1100 64i 1060 61 4 -29-85/31 100-01-6 4-Nitroaniline 340U 1720 1370 -'.so: , 1280 74,···· 1_ 49-104/31 I 91-20-3 Naphthalene 170U 1720 1420 '83 1310 :76 -.g-54-93/32 98-95-3 Nitro benzene 170U 1720 1350 .79 · 1280 ,74 5 53-92/32 62-75-9 N-Nitrosodimethylamine 340U 1720 1140 66 1080 63 5 -37-88/34 621-64-7 N-Nitroso-di-n-propylamine 170U 1720 1380 80 1310 76 5 /, 49-94/28 I 86-30-6 N-Nitrosodiphenylamine 170U 1720 1460 85' 1420 ,s2· :,f· -53-107/28 85-01-8 Phenanthrene 170U 1720 1550 90,_ ----1470 85 5 -61-103/32 129-00-0 Pyrene 170U 1720 1650 96 1590 92. 4 58-109/33 I ll0-86-1 Pyridine 340U 1720 863 50 761 44 13 30-68/38 120-82-1 1,2,4-Trichlorobenzene 170U 1720 1370 8P 1280 '11. 1 52-93/32 I • 42 of 54 I •==•·· F46&87 j '! f",-,~• j' ;._ 1" ,; (' I I'": ~
I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19264-MS L035517.D 1 OP19264-MSD L035518.D 1 F46676-5 L035516.D 1 Anal)'7.C(i By 01/25/07 NJ 01/25/07 NJ 01/25/07 NJ Prep Date 01/24/07 01/24/07 01/24/07 Prep Batch OP19264 OP19264 OP19264 Page 3 of3 Analytical Batch SL1820 SL1820 SL1820 The QC reported here applies to the following samples: Method: SW846 8270C F46687-1, F46687-2 CASNo. 367-12--4 4165-62-2 118-79-6 4165-60-0 321-60-8 1718-51-0 Surrogate Recoveries 2-Fluorophenol Phenol-d5 2,4,6-Tribromophenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14 MS MSD F 4667~5 Limits -s2%,• :16% ; · . Tl.% 40-102% ), .,. ..,,,•, ,• s,~/<•··•.·•.· ··· .75%,) < 704¼ ·... 41-100% 85'X) 7~~ \ . ·•.·· ::1~¾ > , \ 42-108% 75% . 6,9% · . 66% .> 40-105% 78% JI% ., . · .· 67% 43-107% ~1% 84%. . . 18% 45-119% I
I I I I I I I I I I I I I I I I I I I tin. . Southeast IIACCU I ES I. ""' QC Data Summaries Includes the following where applicable: • MeiliodBlankSwnmaries • Blank Spike Smnmaries • Matrix Spike and Duplicate Summaries I
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Samp:le File ID DF GUV1472-MB UV025604.D1 Analyzed 01/24/07 By MM Prep Date n/a The QC reported here applies to the following samples: F46687-l, F46687-2 CASNo. Compound Result RL MDL Units C5-C8 Aliphatics (Unadj.) 3800 2000 ug/kg C9-C12 Aliphatics (Unadj.) 2800 1500 ug/kg C9-CIO Aromatics (Unadj.) 1000 510 ug/kg CASNo. Surrogate Recoveries Limits 460-00-4 BFB 119% 70-130% 460-00-4 BFB ~9§.%. 70-130% Prep Batch n/a Page 1 of 1 Analytical Batch GUV1472 Method: MADEP VPH Q} :..,. Q I 81!1 45of54 lii.ACCUTEST. F46687 ' " " ,; ,· ' ' '' · ' "
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF GlN1472-BS W025603.D1 Analyzed 01/24/07 By MM Prep Date n/a The QC reported here applies to the following samples: F46687-l, F46687-2 Spike BSP BSP CASNo. Compound ug/kg ug/kg % Limits C5-C8 Aliphatics (Unadj.) 25000 26300 iQ~'. 70-130 C9-C12 Aliphatics (Unadj.) 25000 27100 fo!f 70-130 C9-Cl0 Aromatics (Unadj.) 4160 4690 ii~ 70-130 CASNo. Surrogate Recoveries BSP Limits 460-00-4 BFB 122% 70-130% 460-00-4 BFB 119%'··. 70-130% Prep Batch n/a Page 1 of 1 Analytical Batch GUV1472 Method: MADEP VPH I 11n 46of54 l3A.t:a I , ES I. F46687 isb-.ir."l,:;:rcr,
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF F46687-2MS UV025612.Dl F46687-2MSD UV025613.Dl F46687-2 a UV025610.Dl Analy7.ed By 01/24/07 MM 01/24/07 MM 01/24/07 MM The QC reported here applies to the following samples: F46687-1, F46687-2 F46687-2 Spike CASNo. Compound ug/kg Q ug/kg C5-C8 Aliphatics (Unadj.) ND 40300 C9-C12 Alipbatics (Unadj.) ND 40300 C9-ClO Aromatics (Unadj.) ND 6720 CASNo. Surrogate Recoveries MS MSD 460-00-4 BFB 11,% 118% 460-00-4 BFB 116% 11.3% Prep Date n/a n/a n/a MS MS ug/kg % 37800 94 39300 97 7220 101·. F46687-2 109% tor% Prep Batch n/a n/a n/a Page 1 of 1 Analytical Batch GUV1472 GUV1472 GUV1472 Method: MADEP VPH MSD MSD Limits ug/kg % RPD Rec/RPD 34400 85 70-130/50 38100 94 70-130/50 7000 lQ1 70-130/50 Limits 70-130% 70-130% I (a) Sample was received in a bulk container but was not preserved within 48 hours of sampling. 11'!1 47of54 l'(jACCUTEST. F46687 ' " " .., ' ·· ' '' ·· ' ...
I I I I I I I I I I I I I I I I I I I Duplicate Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF F46687-1DUP UV025611.Dl F46687-l 8 UV025609.D1 Analyzed 01/24/07 01/24/07 By MM MM Prep Date n/a n/a Prep Batch n/a n/a Page 1 of 1 Analytical Batch GW1472 GW1472 The QC reported here applies to the following samples: Method: MADEP VPH F46687-1, F46687-2 F46687-l DUP CASNo. Compound ug/kg Q ug/kg Q RPD Limits C5-C8 Aliphatics (Unadj.) ND ND C9-Cl2 Aliphatics (Unadj.) ND ND C9-ClO Aromatics (Unaclj.) ND ND CASNo. Surrogate Recoveries DUP F46687-l Lim.its 460-00-4 BFB 117% u2%> 70-130% 460-00-4 BFB 1}$% 108% 70-130% (a) Sample was received in a bulk container but was not preserved within 48 hours of sampling. I 111!1 48 of 54 flAcce S i EST. F46687 ' ' " ,· ' ·' ,· ' ' '
I I I I I I I I I I I I I I I I I I I fin Southeast QAccui\ESic QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spilce and Duplicate Summaries Section 7 I Im') 49of54 Ii.A.Ca i I EST. F46687 1 il h 11 1' l,,. ! () i' ' !' 'i
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC SampJe File ID DF OP19287-MB ZF22528.D 1 Analyzed 01/30/07 By AC Prep Date 01/25/07 The QC reported here applies to the following samples: F46687-1, F46687-2 CASNo. CASNo. 3386-33-2 580-13-2 84-15-1 321-60-8 Compound Cll-C22 Aromatics (Unadj.) C9-C18 Aliphatics C19-C36 Aliphatics Surrogate Recoveries 1-Chlorooctadecane 2-Bromonaphtbalene o-Terphenyl 2-Fluorobiphenyl Result RL MDL ND , .• , .... ;· 6700 6700 r-w . 6700 6700 ·, , · '6700 ND 6700 Limits 6~96 . , •· ·., 40-140% 44% ' 40-140% 58% i 40-140% 66%> 40-140% Units ug/kg ug/kg ug/kg Prep Batch OP19287 Page 1 of 1 Analytical Batch GZF1054 Method: MADEP-EPH-98-1 Q -..I :... II
I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19287 -MB ZF22537 .D 1 Analy7.ed 01/31/07 By AC Prep Date 01/25/07 The QC reported here applies to the following samples: F46687-l, F46687-2 CASNo. Compound Result RL MDL Units Cll-C22 Aromatics (Unadj.) 1'Ip .. . 6700 6700 ug/kg C9-Cl8 Aliphatics :t4p ..••..... •· 6700 6700 ug/kg Cl9-C36 Aliphatics iP < 6700 6700 ug/kg CASNo. Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane ~%/ 40-140% 580-13-2 2-Bromonaphthalene 42% 40-140% 84-15-1 o-Terphenyl 56% 40-140% 321-60-8 2-Fluorobiphenyl 64% 40-140% Prep Batch OP19287 Page 1 of 1 Analytical Batch GZF1055 Method: MADEP-EPH-98-1 Q II lffl 51 of 54 BACCY ti EST. F46687 ! :i 1)'',1 r"l 1 ,·. •·1 :: ~
I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46687 Account: SEINCR SEI Environmental-Raleigh Project: Pantty 3022; Fayetteville, NC Sample File ID DF Analyzed By OP19287 -BS ZF22527 .D 1 01/30/07 AC The QC reported here applies to the following samples: F46687-l, F46687-2 Page 1 of 1 Prep Date Prep Batch Analytical Batch 01/25/07 OP19287 GZF1054 Method: MADEP-EPH-98-1 Spike BSP BSP CASNo. Compound ug/kg ug/kg % Limits Cll-C22 Aromatics (Unadj.) 56700 33500 5ij 40-140 C9-C18 Aliphatics 20000 16500 82 . · 40-140 CI9-C36 Aliphatics 26700 23100 tJT' < 40-140 CASNo. Surrogate Recoveries BSP Limits 3386-33-2 1-Chlorooctadecane 7Q%> 40-140% 580-13-2 2-Bromonaphthalene 5~~···· 40-140% 84-15-1 o-Terphenyl 56%/! ' 40-140% 321-60-8 2-Fluorobiphenyl 58% . 40-140% -..I ;.., II
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Du.plicate Summary Job Number: F46687 Page 1 of 1 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sampk: File ID DF OP19287-MS ZF22539.D 1 OP19287-MSD ZF22540.D 1 F46687-l ZF22538.D 1 Anafy7.ed By 01/31/07 AC 01/31/07 AC 01/31/07 AC The QC reported here applies to the following samples: F46687-l, F46687-2 CAS No. Compound Cll-C22 Aromatics (Unadj.) C9-Cl8 Aliphatics Cl9-C36 Aliphatics CASNo. Surrogate Recoveries 3386-33-2 1-Chlorooctadecane 580-13-2 2-Bromonaphthalene 84-15-1 o-Terphenyl 321-60-8 2-Fluorobiphenyl F46687-l Spike uglkg Q ug/kg ND 59500 ND 21000 ND 28000 MS MSD 75% 72% 49% 68% .. a':::,: .. ,.:·., 59% 50% / 5~% ~~% Prep Date 01/25/07 01/25/07 01/25/07 Prep Batch OP19287 OP19287 OP19287 Analytical Batch GZF1055 GZF1055 GZF1055 Method: MADEP-EPH-98-1 ...., C,,,) MS ug/kg MS MSD MSD Limits -% ug/kg % RPD Rec/RPD .. 35100 c:~9 · .. ·. 32100 sf .9( 40-140/50 19100 ·.i~~ 18600 89 ···3 40-140/50 \/:i:; ·tr 29700 27300 w 40-140/50 F46687-1 Limits 66%> 40-140% .. ·59% • 40-140% 50%. 40-140% 56% 40-140%
I I I I I I I I I I I I I I I I I I I Duplicate Summary Job Number: F46687 Accollilt: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC SampJe File ID DF OP19287-DUP ZF22533.D 1 F46687-2 ZF22532.D 1 Analyz.ed 01/30/07 01/30/07 By AC AC Prep Date 01/25/07 01/25/07 Prep Batch OP19287 OP19287 Page 1 of 1 Analytical Batch GZF1054 GZF1054 The QC reported here applies to the following samples: Method: MADEP-EPH-98-1 F46687-1, F46687-2 F46687-2 CASNo. Compound ug/kg Q Cll-C22 Aromatics (Unadj.) ND C9-C18 Aliphatics ND C19-C36 Aliphatics ND CASNo. Surrogate Recoveries DUP 3386-33-2 1-Chlorooctadecane 14% 580-13-2 2-Bromonaphthalene 56% 84-15-1 o-Terphenyl 55% 321-60-8 2-Fluorobiphenyl 60% DUP ug/kg Q ND ND ND F46687-2 66%· ... • 51% 47% 52% RPD Limits Limits 40-140% 40-140% 40-140% 40-140% I 111.'j 54of54 ;'i.ACC:U i EST. r'46687 !. :, l:i ,~, r·· 1, 1· r.: ,· ; ::: ·;
I I I I I I I I I I I I I I I I I I I Im ·. . Southeast l'jAccu i ES I. ACCUTEST LABORATORIES '1956-2006 SEI Environmental-Raleigh Pantry 3022; Fayetteville, NC 506016 Accutest Job Number: F46745 Sampling Date: 01/22/07 Report to: [e-mail] A TIN: Distribution6 Total nwnber of pages in report: 53 Test results contained within this data package meet the requirements of the National Enviromnental Laboratory Accreditation Conference and/or state specific certification programs as applicable. e-Hardcopy 2. 0 Automated Report Certlficatlom: FL (DOH E83510), NC (573), NJ (FL002), MA (FL946), lA (366), LA (03051), KS (E-10327), SC, AK This report shall not be reproduced, except In Its eotirety, without the written approval of Accutest Laboratories. Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutestrom 811!!1 1 of 53 laAJ:::0 I i ES L. F46745 I. ,, h ,, .. ', t ,, " C '
I I I I I I I I I I I I I I I I I I I Sections: Table of Contents -1-Section 1: Sample Summary ............................................................................................ ....... 3 Section 2; Sampl.e Results ............. ......................................................... ..........................• ....... 4 2.1: F46745-1: MW-1 .......................................................................................................... 5 2.2: F46745-2: TRIP BL.ANK ............................................................................................. 14 ''. Chain of Custody .. .. .. .. ... .. .......... .... .... .. .. .. .. ...... .... .... .. .... .. ... .. .... .............. ................. ..... . 17 Section 4: GC/MS Volatiles -QC Data Summaries .............................................................. 19 4.1: Method Blank Summary ................................................................................................ 20 4.2: Blank Spike Summary ... ............................ ......... ....... ......... ...... ..... .. ........................ ...... 22 4.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 24 : Method Blank Summary .. .. .. .. ..... .. .. ............. ... .. .. ......... .... ..... .. .. .. ..... .. ..... .. .. .. .. .. ..... .. ...... 27 Blank Spike Summary ... ..... ...... .. ........... .... ... .. .. .. .. ..... .. .... ... .. .... ... .. ................. ... .... .. .. .... 30 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 33 Si~cti.on 6: GC Volatiles -QC Dafa Summaries ............................. no,,,.................................. 36 Method Blank Summary ................................................................................................ 37 Blank Spike Summary ... ...... ......... ..... .... ....... ...... ...................... ..... .. .. ......... .. ................. 39 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 42 6,4: Duplicate Summary ....................................................................................................... 44 Section 7: GC Semi-volatiles -QC Data Summaries ............................................................ 45 7.1: Method Blank Summary ................................................................................................ 46 7.2: Blank Spike Summary................................................................................................... 47 7.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 48 Section 8: Metals Analysis -QC Data Summa.rit~s ................................................................ 49 8.1: Prep QC MPl 1100: Pb.................................................................................................. 50 I I I I II I Mn 2of53 IIACCU1ES£. F46745 ' ., h ., 1 •
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 SEI Environmental-Raleigh Pantry 3022; Fayetteville, NC Project No: 506016 Sample Summary Sample Number i~~)::/f '1,:::/:.·.... Matrix Date Time By Received Code Type /~IZI:$.¥~: . ·; 01/22/07 12:00 NA TE 01/24/07 AQ Ground Water .f'/l.6t4'$+,Z .· 01/22/07 00:00 NATE 01/24/07 AQ Trip Blank Water Job No: Client Sample ID I F46745
I I I I I I I I I I I I I I I I I I I 111!1. Sou. th. east IIACcUTesT. !...<1bor.l:tor12'.i Report of Analysis
I I I I I I I I I I I I I I I I I I I / Accutest Laboratories Report of Analysis Page 1 of2 Client Sample ID: Lab Sample ID: Matrix: Method: MW-1 F46745-1 AQ -Ground Water EPA624 Project: Pantry 3022; Fayetteville, NC File ID DF Analyzed Run#l N0016750.D 1 01/24/07 Run#2 ~fl Purge Volume 5.0ml Run#2 VOA PPL List CASNo. Compound Resuh 71-43-2 Benzene ND: ,;,-.•: .. ~ .. : ., 75-27-4 Bromodichlorometbane ND 75-25-2 Bromofonn Nil 108-90-7 Chlorobenzene ND· 75-00-3 Chloroethane Nt,/.· .• ,· .. ·. 67-66-3 Chloroform NI), 110-75-8 2-Chloroethyl vinyl ether ND 56-23-5 Carbon tetrachloride :.ND 75-34-3 1, 1-Dichloroethane ·NJ? 75-35-4 1, 1-Dichloroethylene ND 107-06-2 1,2-Dichloroethane ND 78-87-5 1,2-Dichloropropane w·•. 108-20-3 Di-Isopropyl ether ·NJ.) 124-48-1 Dibromochloromethane ND 75-71-8 Dichlorodifluoromethane ND 156-59-2 cis-1,2-Dicbloroethylene 'NP 10061-01-5 cis-1,3-Dichloropropene ND 541-73-1 m-Dichlorobenzene ND 95-50-1 o-Dichlorobenzene ND 106-46-7 p-Dichlorobenzene ND 156-60-5 trans-1,2-Dichloroethylene ~; 10061-02-6 trans-1,3-Dichloropropene Nb···· 100-41-4 Ethylbenzene ND 74-83-9 Methyl bromide ND 74-87-3 Methyl chloride .ND·• 75-09-2 Methylene chloride 1'11) 1634-04-4 Methyl Tert Butyl Ether ND 71-55-6 1, 1, I-Trichloroethane ND 79-34-5 1,1,2,2-Tetrachloroethane ND 79-00-5 1,1,2-Trichloroethane ND 127-18-4 Tetrachloroethylene ND 108-88-3 Toluene ND By cs RL 1.0 1.0 1.0 1.0 2.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 .· 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 2.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date n/a MDL Units 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 1.0 ug/1 0.50 ug/1 2.5 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/l 0.50 ug/1 0.50 ug/1 0.40 ug/1 0.50 ug/1 0.50 ug/1 0.30 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.30 ug/1 0.50 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 0.50 ug/1 0.50 ug/1 0.40 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 Prep Batch Analytical Batch n/a VN711 Q J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest Laboratories Report of Analysis Page 2 of2 Client Sample ID: Lab Sample ID: Matrix: Method: MW-1 F46745-1 AQ -Ground Water EPA 624 Project: Panny 3022; Fayetteville, NC VOA PPL List CASNo. Compound Result 79-01-6 Trichloroethylene ND' 75-69-4 Trichlorofluoromethane ·NP. 75-01-4 Vinyl chloride ·~.'.i•.••·· 1330-20-7 Xylene (total) Nlf CASNo. Surrogate Recoveries Run# 1 1868-53-7 Dibromofluoromethane '102% 17060-07-0 1,2-Dichloroethane-D4 io2% 2037-26-5 Toluene-OS 90%· 460-00-4 4-BroDlOfluorobenzene -96% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL 1.0 2.0 1.0 3.0 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a MDL Units Q 0.50 ug/1 0.50 ug/1 0.50 ug/1 1.0 ug/1 Run#2 Limits 87-116% 76-127% 86-112% 84-120% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound II
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 Report of Analysis Page 1 of3 Client Sample ID: MW-1 Lab Sample ID: F46745-l Matrix: AQ -Ground Water Method: EPA 625 EPA 625 Project: Pantry 3022; Fayetteville, NC File ID DF Analyzed By RIDI 11 1.035546.D 1 01/31/07 RB Run#2 Initial Vohune Final Vohune 1050ml LO ml ABNTCL List CAS No. Compound 65-85-0 95-57-8 59-50-7 120-83-2 105-67-9 51-28-5 534-52-1 95-48-7 88-75-5 100-02-7 87-86-5 108-95-2 95-95-4 88-06-2 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 101-55-3 85-68-7 100-51-6 91-58-7 106-47-8 86-74-8 218-01-9 111-91-1 111-44-4 Benzoic Acid 2-Chlorophenol 4-Chloro-3-methyl phenol 2, 4-Dichlorophenol 2, 4-Dimethylphenol 2,4-Dinitrophenol 4,6-Dinitro-o-cresol 2-Methylphenol 3&4-Methylphenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4 ,5-Trichlorophenol 2,4 ,6-Tricbloropheno) Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h ,i)perylene Benzo(k)fluorantbene 4-Bromophenyl phenyl ether Butyl benzyl phtbalate Benzyl Alcohol 2-Chloronaphthalene 4-Chloroaniline Carbazole Chrysene bis(2-Chloroethoxy)methaoe bis(2-Chloroethyl)ether Resuh RL ND , 24 ND .· 4.8 NI): ,;.. 4.8 1'J:Q' .. 4.8 \ 4.8 ND .. ·.·•.···.· ... · .. ·.·.·.·.·.··.··•, ND, < 24 ND > 9.5 Nb\ .. 4.s ·NDND, . . 4.8 4.8 fm 24 ,Ni) 24 ND '4.8 ·ND· 4.s lllp( i 4.8 ND.• •4.8 Nb 4.8 w· •····4.s ND' 4.8 ND 4.8 No· , 4.8 ND . 4.8 1'ID ..... ·, 4.8 'NI)<,·, 4.8 ND 4.8 ND , · 4.8 Nb · · ... 4.8 :l\11?,, · ,: 9.5 ND ' · 4.8 'rill... : 4.8 ND 4.8 ~ . 4.8 ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Date Sampled:· 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 01/29/07 OP19321 SL1822 MDL Units Q 9.5 ug/1 1.9 ug/1 1.9 ug/1 1.9 ug/1 1.9 ug/1 9.5 ug/1 4.8 ug/1 1.9 ug/1 1.9 ug/1 1.9 ug/1 9.5 ug/1 9.5 ug/1 1.9 ug/1 1.9 ug/1 1.9 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 1.9 ug/1 0.95 ug/1 0.95 ug/1 1.9 ug/1 0.95 ug/1 0.95 ug/1 3.8 ug/l 0.95 ug/l 0.95 ug/1 0.95 ug/l 1.9 ug/l J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I~ F46745 I ;i' I;·~),: r,, ·,1 ,: i r: ·,
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 Report of Analysis Page 2 of3 I Client Sample ID: Lab Sample ID: Matrix: Method: MW-1 F46745-1 AQ -Ground Water EPA 625 EPA 625 Project: Pantry 3022; Fayetteville, NC ABNTCL List CASNo. Compound Result 108-60-1 bis(2-Chloroisopropyl)ether ii,·• 7005-72-3 4-Chlorophenyl phenyl ether 95-50-1 1,2-Dichlorobenzene NI) 541-73-1 1,3-Dichlorobenzene ND 106-46-7 1,4-Dichlorobenzene ND ;.: .. ,., ...... , 121-14-2 2, 4-Dinitrotoluene •NP< 606-20-2 2,6-Dinitrotoluene NJ;>> •. 91-94-1 3,3' -Dichlorobenzidine No···.·•.·.•·. 53-70-3 Dibenzo(a,h)anthracene NI). 132-64-9 Dibenzofuran ND 84-74-2 Di-n-butyl phthalate ND 117-84-0 Di-n-octyl phthalate NI) 84-66-2 Diethyl phthalate ND··.· .. 131-11-3 Dimethyl phthalate ND 117-81-7 bis(2-Ethylhexyl)phthalate ND 206-44-0 Fluoranthene ND 86-73-7 Flnorene ND 118-74-1 Hexachlorobenzene ND 87-68-3 Hexachlorobutadiene NI) .. ·.· 77-47-4 Hexacblorocyclopentadiene mr. 67-72-1 Hexachloroethane ·Nb .. 193-39-5 Indeno(l,2,3-cd)pyrene ND 78-59-1 lsophorone ND 91-57-6 2-Methylnaphthalene ND 88-74-4 2-Nitroaniline ND·•· 99-09-2 3-Nitroaniline NO 100-01-6 4-Nitroaniline ND 91-20-3 Naphthalene ND 98-95-3 Nitrobenzene ND 621-64-7 N-Nitroso-di-n-propylamine ND 86-30-6 N-Nitrosodiphenylamine ~ ... 85-01-8 Phenanthrene ND 129-00-0 Pyrene ND 120-82-1 1,2 ,4-Trichlorobenzene ND CASNo. Surrogate Recoveries Run# 1 367-12-4 2-Fluorophenol •36% 4165-62-2 Phenol-d5 22%·· 118-79-6 2 ,4 ,6-Tribromophenol 73% RL 4.8 ·.•·• 4.8 4.8 4.8 4.8 4.8 4.8 9.5 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 9.5 9.5 9.5 4.8 4.8 4.8 4.8 4.8 4.8 4.8 Run#2 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a MDL Units Q 0.95 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/1 1.9 ug/1 1.9 ug/1 4.8 ug/1 1.9 ug/1 0.95 ug/1 1.9 ug/1 2.4 ug/1 1.9 ug/1 1.9 ug/1 2.4 ug/1 0.95 ug/l 0.95 ug/1 0.95 ug/1 1.9 ug/1 1.9 ug/1 1.9 ug/l 1.9 ug/1 0.95 ug/l 0.95 ug/1 3.8 ug/1 3.8 ug/1 3.8 ug/1 0.95 ug/1 0.95 ug/1 1.9 ug/1 1.9 ug/1 0.95 ug/1 0.95 ug/1 0.95 ug/l Limits 19-90% 10-68% 36-137% ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presmnptive evidence of a compound 111!1 8 of 53 l;iACCU I ES 1: F4G745 ' ., b ,, ,, ,. ' ,, •. ' '
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 Report of Analysis Page 3 of3 I Client Sample ID: Lab Sample ID: Matrix: Method: MW-1 F46745-l AQ -Ground Water EPA 625 EPA 625 Project: Pantry 3022; Fayetteville, NC ABNTCL List CASNo. Surrogate Recoveries Run# 1 4165-60-0 Nitrobenzene-d5 64.% 321-60-8 2-Fluorobiphenyl 67% 1718-51-0 Terphenyl-d14 67% ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Run#2 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Limits 49-119% 45-118% 46-135% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 111m .. 9of53 QACDJTEST. F46i,45 ; 'I h ,_', ;' f. ! (: (it:
I I I I I I I I I I I I I I I I I I I Accutest LabLink@ 15:42 05-Feb-2007 Report of Analysis Page I of 1 I Client Sample ID: Lab Sample ID: Matrix: Method: MW-1 F46745-1 AQ -Ground Water MADEPVPH Pr(!iect: Pantry 3022; Fayetteville, NC File ID OF UV025621.D 1 Purge Volume 5.0ml MADEP VPH List CAS No. Compound Analy;,.ed 01/25/07 Resuh CS-CS Aliphatics (Unadj.) ND C9-Cl2 Alipbatics (Unadj.) ND. C9-CIO Aromatics (Unadj.) ND·· CAS No. Surrogate Recoveries 460-00-4 BFB 460-00-4 BFB Run# I )f01% ,95% By MM RL 75 55 20 Run#2 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date n/a MDL Units 50 ug/1 30 ug/1 10 ug/1 Limits 70-130% 70-130% Prep Batch n/a Q Analytical Batch GUV1473 ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■l!!I 1 O of 53 g'dACClhESl. F46745 1 " 11 ,~, '" ; 1 '' r' ~ :;
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 Report of Analysis Page 1 of 1 Client Sample ID: MW-I Lab Sample ID: F46745-l Matrix: AQ -Ground Water Method: EPA 504.1 EPA 504 Project: Pantry 3022; Fayetteville, NC Run#l Run#2 File ID DD37683.D DF 1 Ana1)'7.Cd 01/26/07 Initial Volume Final Volume 37.8 ml 2.0 ml CAS No. Compound Resuh 106-93-4 1,2-Dibromoethane ;INQ CAS No. Surrogate Recoveries Run# 1 460-00-4 4-Bromofluorobenzene :~i% By NJ RL . 0.019 Run#2 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date 01/25/07 MDL Units 0.0093 ug/1 Limits 63-137% Prep Batch OP19286 Q Analytical Batch GDD1029 ND= Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found In associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest LabLink@15:42 05-Feb-2007 Report of Analysis Page 1 of 1 I Client Sample ID: MW-1 Lab Sample ID: F46745-1 Matrix: AQ -Ground Water Method: MADEP-EPH-98-1 SW846 3510C Project: Pantry 3022; Fayetteville, NC File ID DF Analy:,.ed Runfl ZF22522.D 1 01/30/07 Runf2 Initial Volume Final Volume 1050 ml 2.0 ml MAEPHList CAS No. Compound Cll-C22 Aromatics (Unadj.) C9-C18 Aliphatics C19-C36 Aliphatics Resuh By AC RL 190 190 190 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 01/26/07 OP19299 GZF1054 MDL Units Q 140 ug/1 190 ug/1 190 ug/1 CASNo. Surrogate Recoveries Run# I Run#2 Limits 3386-33-2 1-Chlorooctadecane 69% 580-13-2 2-Bromonaphthalene 64% 84-15-1 o-Terphenyl 64% 321-60-8 2-Fluorobiphenyl Q7%. ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range 40-140% 40-140% 40-140% 40-140% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound II!) .. 12of53 lfACCU" fEST. F46745 ' ' "" ' ;·. ' ,, · ' ' '
I I I I I I I I I I I I I I I I I I I Accutest LabLink@l5:42 05-Feb-2007 Client Sample ID: MW-1 Lab Sample ID: F46745-1 Matrix: AQ -Ground Water Report of Analysis Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Project: Pantry 3022; Fayetteville, NC Metals Analysis Analyte Result Lead RL 5.0 (1) Instrwnent QC Batch: MA5462 (2) Prep QC Batch: MPlllOO RL = Reporting Limit Units DF Prep Anal)'7.Cd By Method ug/1 01/25/07 01/25/07 RS SW8(6 60108 l Page 1 of 1 Prep Method SM3030C 2 I litf!I 13 of 53 liACD·PLESi. F46745 I rih·~·i·i.:·1..::/i::c..:
I I I I I I I I I I I I I I I I I I I Accutest LabLlnk@15:42 05-Feb-2007 Report of Analysis Page 1 of 2 Client Sample ID: TRIP BLANK Lab Sample ID: F46745-2 Matrix: AQ -Trip Blank Water Method: EPA 624 Project: Pantry 3022; Fayetteville, NC Run#l Run#2 File ID N0016749.D Purge Volume 5.0ml DF 1 VOAPPLList CAS No. Compound 71-43-2 75-27-4 75-25-2 108-90-7 75-00-3 67-66-3 110-75-8 56-23-5 75-34-3 75-35-4 107-06-2 78-87-5 124-48-1 75-71-8 156-59-2 10061-01-5 541-73-1 95-50-1 106-46-7 156-60-5 10061-02-6 100-41-4 74-83-9 74-87-3 75-09-2 1634-04-4 71-55-6 79-34-5 79-00-5 127-18-4 108-88-3 79-01-6 Benzene Bromodicbloromethane Bromoform Cblorobenzene Chloroethane Chloroform 2-Cbloroethyl vinyl ether Carbon tetrachloride 1, 1-Dichloroethane 1, 1-Dichloroethylene 1,2-Dichloroethane 1,2-Dichloropropane Dibromochloromethane Dichlorodifluoromethane cis-1,2-Dichloroethylene cis-1,3-Dichloropropene m-Dichlorobenzene o-Dichlorobenzene p-Dichlorobenzene trans-1,2-Dichloroethylene trans-1,3-Dichloropropene Ethylbenzene Methyl bromide Methyl chloride Methylene chloride Methyl Tert Butyl Ether 1, 1, I-Trichloroethane 1, 1,2, 2-Tetracbloroethane 1,1,2-Trichloroethane Tetracbloroethyleoe Toluene Trichloroethylene Analy7.ed 01/24/07 Result ND ND ND ND.· .. ND Nb· ND ND ND ND NP ND ND ND ND ND ND ND.· ND·• ND ND ND ND ND Nb.·. ND ND ND ND ND ND .. Nri By cs RL 1.0 1.0 1.0 1.0 2.0 .. 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 2.0 < 5.0 1.0 1.0 1.0 LO 1.0 1.0 1.0 ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/a Prep Date Prep Batch Analytical Batch n/a n/a VN711 MDL Units Q 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 1.0 ug/1 0.50 ug/1 2.5 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.40 ug/1 0.50 ug/1 0.50 ug/1 0.30 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.30 ug/1 0.50 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 0.50 ug/1 0.50 ug/1 0.40 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound I
I I I I I I I I I I I I I I I I I I I Accutest LabLink.@15:42 05-Feb-2007 Report of Analysis Page 2 of2 I Client Sample ID: Lab Sample ID: Matrix: Method: TRIP BLANK F46745-2 AQ -Trip Blank Water EPA 624 Project: Pantry 3022; Fayetteville, NC VOA PPL List CASNo. 75-69-4 75-01-4 1330-20-7 CASNo. 1868-53-7 17060-07-0 2037-26-5 460-00-4 Compound Trichlorofluoromethane Vinyl chloride Xylene (total) Surrogate Recoveries Dibromofluoromethane l ,2-Dichloroethane-04 Toluene-D8 4-Bromofluorobenzene Resuh Run# 1 i01% :1.02%•·· 90%' 96%:•·•· ND = Not detected MDL -Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL 2.0 1.0 3.0 Date Sampled: 01/22/07 Date Received: 01/24/07 Percent Solids: n/ a MDL Units Q 0.50 ug/1 0.50 ug/1 1.0 ug/1 Run#2 Limits 87-116% 76-127% 86-112% 84-120% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 111!.1 15 of 53 gACCUTEST. F46745 t ,,. 1,· ,.:.;_ r· h I o"/ !" i ~ '
I I I I I I I I I I I I I I I I I I I Ill . Southeast l'iACCUTES-r: Misc",Fottns Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody
I I I I I I I I I -I I I I I I I I I I ■l!I CHAIN OF CUSTODY ■AcguTEST. +«16 IIINl!I.AM> ~ • SUITE C-15 ORLANDO, Ft 3811 Laboratories TEI.: 407~7r10 • FAX: [phone]f17 I CLIENT INl'OftMATION I I FACILITY INFOIIIIATION I ~ ErJv',~N1~L '?A ":;{oQ.:2 ] NAME j:'.~M<AIU.'_ ~Ulle /~:)_ '"t:Q_ f-A 'if,; Z i E,.I( 1 U-6 i b) C, j AIIOR~ LOCATION 50~ 0{ ~ ~(. 2]{eOJ ~ _L..t::JG,d:l. CITY, STATE ZII' PROJICTNO. --~ (..5. ~m.:tl:Cit "' _j ...... PHONI!• -1~-K:3-Z.-z.~ l'AXf COW!CT10N I !I Rtit, ... -~ ACCUTEST ~ SAIIIPl.E• PIELD D f POINI' OF COU5C'TIOII OATE TWE ~ ..,, ---= ,.--.,~---,_ ACCIITUf QUOTU: r f"' .,. 'f !) ANALYTICAi. INFOAMATION JIIATIIIX COOES I ---·-i~ ---i ·---·-~ WATER IO· IIOIL -~ ..... ----'-.i Ill• OIL -UQ--0 --~ ---1 ~ -LU USE ONLY w :... \) V\I• \-\ J/11/A'J ,,, IA.fl 1-.1 r;, r-,., II.I, y X irJ.. 'I. X ?..) -n<..l? C:,1.-A-rJ'l, >---.----! DATA TURNAROUND INFORMATION I DATA Dl!UVERAIII.£ INFORIIATION I COMMl!NTIIRl!IIARKS ~ STANDARD APPROVED IY: 0 8TANCWIO -48HOUIIRUSH □ C011M1ERCtAL ·r C 2& HOUR £Ml!f!CleNCY ~ Dl&I( DliLIV&RA8L& 0 OTHER D STATE FOAIIII EMEAGENC:f OR -IS FAX DATA 0 ontlYI (IPl!Clf'Y) utllHS PIIEVIOUSI.Y A-0 ( '-,,-,II ( I \SAMPLE CUS'TODY 1111118T ■I! DOCUll&NTID UI.OW iACH '11111 IAIIPLI& ClfANCII P0■81!81011, INCLUDING COUAIIR IIILIVIRY I -~~o,,,--:L. ~ 'Ollfl:1111E: llacatvaD■Y; MUNaUaaD lrf; . -) YI I /1.~ H£b-, Jno 1. a. ----... DIIV: o.t.ft,..: _.., _.,, 3. 3. 4.. IIIB.~ID O: DAffTIMI: tnlC8IIID n: -· 5. I. ...... .,,_ -11'1; a. ....,,,_, _.., 4. ---GNICI! ~ □ D F46745: Chain of Custody Pagel of 2 llll!!I 11 of 53 liACCU i ES i. F46745 ' _, h ·" ',, ' •O' 1 '-'
I I I I I I I I I I I I I I I I ACCJITEST LABQRATQRJES $AMPLE RECEIPT CONFIRMATION ACClJTZST's JOB rm: ,:;. 41, 9:y <;; CUEttT: 5 Et 8'11,&1J.fN, PROJECT: f 4 1" 1 :,.. DATE/TDm RECElVED: 0 I -'t '-l -fl-D1 ;.,. 11 OF COOL&RS RECEIVED:_! COOLER TEMPS: __ :;,;;._..,?-..;_ _____ _ MZTIIOD OF Dl:UVERY: ~ UPS A0CtlTEST COURIER GREYHOUND DELIVERY 'OTBF.R AlRBILLK1JM81tRS: __________________________________ _ COOLltR, INFQRM&TION ~CU8TODY SEAL l'f<n: PJiCESE1'fT OR NOT INTACT CBAll'f OF CUSTODY NOT RECEIV£D (COC) ANALYSIS RltQU]t8TED l8 UNCLEAR OR MISSING 8AIIPUt DATES OR TDIES UNCLEAR OR MISSJl'fG 1'1tMl'ltRA'nJRE CRJ.TERJA NOT M&T ~:lltlCEl1l'lmWATER TRIP BlAN1t RECEIVED eon. TRIP IILANK IQSC. INFOBH6TIQN NmlBm OF ENCORES ? NlJJIBBR OF BOSS ll11tLD KITS ? NUMB!a Oil LAB l'IL1'BRED METALS Y O'WQRMATIQN LAB&LS l'IOT PRE6ENT ON AU, BOT'l'LES RRECT NU11BER 01!" COlff.AINERS 08BD T'IJ4S ON COC DOES NOT MA'I'CH LABB:L(S) ID'S ON COC DOES NOT MATCH LABEL(SJ VOC VIALS HAVE IIEADSPACE (l(ACRO JIUBBUt8) BOTTLES RECEIV&D Btrr ANALYSIS NOT BEQUltSTED NO BOT'l1Z8 RECE1VED Jl'OR ANALTlll8 REQUESTED UNCLEAlt FILTERING INSTRUCTIONS Ul'fctEAR COIIP081TING INSTRUCTIONS SAMPLE CONTAJNER(SJ RECEIVED IIROEEN 'K> SOUDS JAR NOT RECEIVED 8035 FDtLD KIT NOT ntoza:N WlTBl5 48 BOOR'S Rlt8IDUAL CHLORINE PRESENT ( .APPUCABI.& TO EPA 600 SERIES OR NOR.TH CAROLINA ORGAl'UC8) smowrrOFCOlllmml, $A""'-fl( ::t:1,: \ t~c.EUJ@ {~ Hu v,AlS A.v11 'IB.f-l! E l>6 t1J11L$ vVtT1<e11r t.M[l,4; j "1\.->t> 8,lfo Av"'\6otS Wlffl.buf k~ ))AI{ ot, JIM£"° tN (..lff_Et... j e£c."1veA Ou~ ~SeAv~ rl1So~ A ...... ,,tA.{MW-lb\:i,c~(I@ Q_,,.I! l'dl!$t;.(yeD H;iSoy A~ {. Mw-11,) j tJvt f-<(Se~Jq.D Hf'o :i 0,1HE' /'1....,-,) j A-Mt,f4,S ANO )--tg7ju,.. hofTLr; TECIOOCIAII SIGNATURE/DATE wf..u!,_ Of~ -r,1, '1'ltCB1UCINI SIGNATURE/DATE ASBD 1003/06 F46745: Chain of Custody Page 2 of 2 F46745 ';,,,,, . .,' oc,c'
I I I I I I I I I I I I I I I I I I I fin . . . Southeast 11.Accu I EST. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 4 I ■l!i• 19 of53 lilACa ,. EST.. F46745 I ,i I'; it,·,../<. I (1 r' ! r: -t:
I I I I I I I I I I I I I I I I I I I Method Blank Summary J'ob Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VN711-MB File ID DF N0016748.D 1 AnalY7,Cd By 01/24/07 cs The QC reported here applies to the following samples: F46745-1, F46745-2 CASNo. Compound Result RL 71-43-2 Benzene ND 1.0 75-27-4 Bromodichloromethane NP• 1.0 75-25-2 Bromoform .~ 1.0 108-90-7 Chlorobenzene '·ND 1.0 75-00-3 Chloroethane ND 2.0 67-66-3 Chloroform ND 1.0 110-75-8 2-Chloroethyl vinyl ether ND 5.0 56-23-5 Carbon tetrachloride ND 1.0 75-34-3 1, 1-Dichloroethane ND 1.0 75-35-4 l, 1-Dichloroethylene ND 1.0 107-06-2 1,2-Dichloroethane ND 1.0 78-87-5 1,2-Dichloropropane ND 1.0 124-48-1 Dibromochloromethane NJ? 1.0 75-71-8 Dichlorodifluoromethane ··r-w. 1.0 156-59-2 cis-1,2-Dichloroethylene ND 1.0 10061-01-5 cis-1,3-Dichloropropene ND 1.0 541-73-1 m-Dichlorobenzene ND 1.0 95-50-1 o-Dichlorobenzene ND 1.0 106-46-7 p-Dichlorobenzene ND 1.0 156-60-5 trans-1,2-Dichloroethylene ·.~ 1.0 10061-02-6 trans-1,3-Dichloropropene ND 1.0 100-41-4 Ethylbenzene ND 1.0 74-83-9 Methyl bromide ND 2.0 74-87-3 Methyl chloride ND. 2.0 75-09-2 Methylene chloride ND 5.0 1634-04-4 Methyl Tert Butyl Ether ND 1.0 71-55-6 1, 1, 1-Tricbloroethane ND 1.0 79-34-5 1, 1,2,2-Tetrachloroethane ND LO 79-00-5 1, 1,2-Trichloroethane ND 1.0 127-18-4 Tetrachloroethylene Nb 1.0 108-88-3 Toluene Nif 1.0 79-01-6 Trichloroethylene ND 1.0 75-69-4 Trichlorofluoromethane ND 2.0 75-01-4 Vinyl chloride ND 1.0 1330-20-7 Xylene (total) NP 3.0 Prep Date n/a MDL Units 0.50 ug/l 0.50 ug/1 0.50 ug/1 0.50 ug/1 1.0 ug/1 0.50 ug/1 2.5 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.40 ug/l 0.50 ug/1 0.50 ug/1 0.30 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 . ug/1 0.30 ug/1 0.50 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 0.50 ug/1 0.50 ug/1 0.40 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 0.50 ug/1 1.0 ug/1 Page 1 of 2 Prep Batch Analytical Batch n/a VN711 I Method: EPA 624 Q
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VN711-MB File ID DF Anal)'7.Cd By N0016748.D 1 01/24/07 cs The QC reported here applies to the following samples: F46745-l, F46745-2 CAS No. Surrogate Recoveries 1868-53-7 Dibromofluorometbane 17060-07-0 1,2-Dichloroetbane-D4 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene 102% 103% 91% -~&% Limits 87-116% 76-127% 86-112% 84-120% Prep Date n/a Page 2 of2 Prep Batch Analytical Batch n/a VN711 Method: EPA 624 I 111!1 21 of53 (d.ACCUTEST. F46745 : ,, "" ' '' ,, '' ,, '
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample VN711-BS File ID DF N0016747.D 1 Anal}'7,Cd 01/24/07 By cs The QC reported here applies to the following samples: F46745-1, F46745-2 Spike BSP CASNo. Compound ug/1 ug/1 71-43-2 Benzene 25 26.7 75-27-4 Bromodichlorornethane 25 24.5 75-25-2 Bromoforrn 25 22.7 108-90-7 Chlorobenzene 25 26.3 75-00-3 Chloroethane 25 22.7 67-66-3 Chloroform 25 26.7 110-75-8 2-Chloroethyl vinyl ether 125 130 56-23-5 Carbon tetrachloride 25 23.5 75-34-3 1,1-Dichloroethane 25 27.4 75-35-4 1, 1-Dichloroethylene 25 20.4 107-06-2 1,2-Dichloroethane 25 25.7 78-87-5 1,2-Dichloropropane 25 25.9 124-48-1 Dibrornochloromethane 25 21.3 75-71-8 Dichlorodifluoromethane 25 28.2 156-59-2 cis-1,2-Dichloroethylene 25 25.0 10061-01-5 cis-1,3-Dichloropropene 25 24.9 541-73-1 m-Dichlorobenzene 25 26.2 95-50-1 o-Dichlorobenzene 25 26.3 106-46-7 p-Dichlorobenzene 25 26.3 156-60-5 trans-1,2-Dichloroethylene 25 27.5 10061-02-6 trans-1,3-Dichloropropene 25 25.3 100-41-4 Ethyl benzene 25 25.4 74-83-9 Methyl bromide 25 19.3 74-87-3 Methyl chloride 25 34.0 75-09-2 Methylene chloride 25 24.2 1634-04-4 Methyl Tert Butyl Ether 25 23.9 71-55-6 1, 1, 1-Trichloroethane 25 27.8 79-34-5 1, 1,2,2-Tetrachloroethane 25 23.5 79-00-5 1,1,2-Trichloroethane 25 24.4 127-18-4 Tetrachloroethylene 25 25.8 108-88-3 Toluene 25 26.0 79-01-6 Trichloroethylene 25 28.8 75-69-4 Tricblorofluorometbane 25 25.3 75-01-4 Vinyl chloride 25 24.1 1330-20-7 Xylene (total) 75 77.3 Prep Date n/a BSP % Limits ·101 .. ·· 83-124 ,•·,-.: .·",";"• 98• 76-116 ,ti~'.'' 68-128 87-115 :91··· .. 54-166 -107 85-123 104 .. 63-125 ~\i 74-139 ll(l 82-127 82 75-133 103 76-122 104 i 81-120 85 74-116 u3. · 34-158 100' .·';{'. 81-114 100' 83-119 105 ,. 86-115 105 85-115 105 87-113 110 .·. 82-126 ,.,·,·,,•,,: 101 87-123 102 · 87-118 77< 55-151 ~: _; .. ' ·. 136 .. 55-173 97> . 69-125 96,'· 75-116 111 . · 79-133 94> 71-120 98 80-114 103 80-131 '104 86-116 U5 85-124 101 66-156 96 57-153 103 86-120 Prep Batch n/a Page 1 of2 Analytical Batch VN711 II Method: EPA 624 fin .·· 22of53 IIACCUTEST.
I I I I I I I I I I I I I I I I I I I BJank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample VN711-BS File ID DF N0016747.D 1 Analp.ed 01/24/07 By cs The QC reported here applies to the following samples: F46745-1, F46745-2 CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 17060-07-0 1,2-Dichloroethane-D4 2037 -26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene BSP ,i0:1%·. ·100% 98% .· ~991) Limits 87-116% 76-127% 86-112% 84-120% Prep Date n/a Prep Batch n/a Page 2 of2 Analytical Batch VN711 Method: EPA 624 I
I I Matrix Spiko'Matrix Spike Duplicate Summary Page 1 of2 Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh I Project: Panny 3022; Fayetteville, NC Prep Batch Analytical Batch ,,.. SampJe File ID DF Analyud By Prep Date c.., F46745-1MS N0016751.D l 01/24/07 cs n/a n/a VN711 I I F46745-1MSD N0016752.D 1 01/24/07 cs n/a n/a VN711 F46745-1 N0016750.D 1 01/24/07 cs n/a n/a VN711 I The QC reported here applies to the following samples: Method: EPA624 F46745-l, F46745-2 I F46745-1 Spike MS MS MSD MSD Limits CASNo. Compound ug/1 Q ug/1 ug/1 % ug/1 % RPD Rec/RPD I 71-43-2 Benzene ND 25 26.6 106 26.3 105 1 83-124/11 75-27-4 Bromodicbloromethane ND 25 24.3 9T 24.6 98 1 76-116/10 I 75-25-2 Bromofonn ND 25 22.7 91 22.7 91 0 68-128/11 108-90-7 Chlorobenzene ND 25 26.0 104 25.9 104 0 87-115/9 75-00-3 Chloroethane ND 25 21.2 85 22.7 91 7 54-166/20 67-66-3 Chloroform ND 25 26.6 106 26.4 106 l 85-123/10 I 110-75-8 2-Chloroethyl vinyl ether ND 125 ND O*. ND 0* DC 63-125/24 56-23-5 Carbon tetrachloride ND 25 26.5 106 26.5 JO~ o• 74-139/13 75-34-3 1, 1-Dicbloroethane ND 25 26.8 107 26.6 105· 1 82-127/10 I 75-35-4 1, 1-Dichloroethylene ND 25 26.4 106 20.6 82 25* . 75-133/13 107-06-2 1,2-Dichloroethane ND 25 25.7 103 25.6 102 0 76-122/11 78-87-5 1,2-Dichloropropane ND 25 25.2 101 25.5 102 1 81-120/U 124-48-1 Dibromochloromethane ND 25 21.3 85 21.l 84 1 74-116/11 I 75-71-8 Dichlorodifluoromethane ND 25 28.4 '114 29.0 1:16 2 34-158/22 156-59-2 cis-1, 2-Dichloroethylene ND 25 24.8 99 24.8 ~9 0 81-114/10 10061-01-5 ds-1,3-Dichloropropene ND 25 24.4 98 25.4 102 4 83-119/10 541-73-1 m-Dicblorobenzene ND 25 26.5 106 26.4 106 0 86-115/9 I 95-50-1 o-Dichlorobenzene ND 25 26.1 104 26.1 104 0 85-115/9 106-46-7 p-Dichlorobenzene ND 25 26.1 104 26.3 l9~ 1 87-113/10 156-60-5 trans-1,2-Dichloroethylene ND 25 26.7 iO'l 26.7 107 0 82-126/10 I 10061-02-6 trans-1,3-Dichloropropene ND 25 26.1 104·. 25.4 102 3 87-123/10 100-41-4 Ethylbenzene ND 25 25.0 100 25.0 100 0 87-118/10 74-83-9 Methyl bromide ND 25 18.9 76 19.9 80 5 55-151/21 74-87-3 Methyl chloride ND 25 33.2 133 .••. 34.6 138 4 55-173/22 I 75-09-2 Methylene chloride ND 25 23.5 94 23.6 94 0 69-125/11 1634-04-4 Methyl Tert Butyl Ether ND 25 23.7 95 23.4 94· 1 75-116/10 71-55-6 1, 1, I-Trichloroethane ND 25 27.8 111 27.9 112·· 0 79-133/11 I 79-34-5 1, 1,2,2-Tetrachloroethane ND 25 25.7 103 24.7 99 4 71-120/11 79-00-5 1, 1,2-Tricbloroethane ND 25 23.8 95 23.5 94 1 80-114/11 12',:-18-4 Tetracbloroethylene ND 25 25.2 101 . 25.6 102 2 80-131/12 108-88-3 Toluene ND 25 25.7 103 25.6 :102 ·o 86-116/10 I 79-01-6 Trichloroethylene ND 25 27.1 lOS 26.8 107 l 85-124/10 75-69-4 Trichlorofluoromethane ND 25 25.0 1.()(J 25.2 101 1 66-156/15 75-01-4 Vinyl chloride ND 25 22.9 92 24.1 96 5 57-153/22 1330-20-7 Xylene (total) ND 75 76.5 102 75.9 101 1 86-120/10 I I 24 of 53 IF5T. I F46745 ! ::i l~ (., i' ;/, I ,-,, ·,-, i ::: ,;
I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF F46745-1MS N0016751.D 1 F46745-1MSD N0016752.D 1 F46745-1 N0016750.D 1 Anafy2:ed By 01/24/07 cs 01/24/07 cs 01/24/07 cs The QC reported here applies to the following samples: F46745-l, F46745-2 CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 17060-07-0 1,2-Dichloroethane-D4 2037 -26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene MS MSD tot¾, ,,. ::to1¾ loo% .loo%• 96% :96% 98% ''),~% · Prep Date n/a n/a n/a F4674S-1 ,··. ,ip~% · 102% 909tt· '~%· Prep Batch n/a n/a n/a Page 2 of2 Analytical Batch VN711 VN711 VN711 · I Method: EPA 624 Limits 87-116% . 76-127% 86-112% 84-120% llm!i 25of53 l'aACCUimT. F46745 I.. ~·h i·i ,.:;,·1 h :· j ~ '.
I I I I I I I I I I I I I I I I I I I 1111!1 Southeast IIACCUIESi& QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Swnmaries • Matrix Spike and Duplicate Summaries F46745 I. ;, b 1•, ,· "· 1 f) I'' C: ·;
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19321-MB 1035545.D 1 Analymd 01/31/07 By RB The QC reported here applies to the following samples: F46745-1 CASNo. Compound Result RL 65-85-0 Benzoic Acid 'ND···. ''; 25 95-57-8 2-Chlorophenol NI)' 5.0 • ;<-~· ,-;; ' 59-50-7 4-Chloro-3-metbyl phenol "ND 5.0 --.-;..: . '.•": 120-83-2 2,4-Dichlorophenol :-ND:;;. 5.0 105-67-9 2,4.-Dimethylphenol •~fr·' 5.0 51-28-5 2 ,4-Dinitrophenol ND . 25 534-52-1 4 ,6-Dinitro-o-cresol ND 10 95-48-7 2-Methylphenol !NJ.?ii ii< 5.0 3&4-Methylphenol '1'l);)) ': ·•·• :, 5.0 88-75-5 2-Nitrophenol NP 5.0 100-02-7 4-Nitrophenol ND 25 87-86-5 Pentachlorophenol .t,m:• 25 108-95-2 Phenol I":·. 5.0 95-95-4 2, 4 ,5-Trichlorophenol 5.0 88-06-2 2,4,6-Trichlorophenol ND·•·· 5.0 83-32-9 Acenaphthene ,~,-• 5.0 208-96-8 Acenaphthylene ·~-· .: .·,: 5.0 120-12-7 Antbracene , .. ,,., 5.0 56-55-3 Benzo(a)anthracene Ni:> 5.0 50-32-8 Benzo(a)pyrene ND 5.0 ....... , 205-99-2 Benzo(b)fluoranthene -~ Ci 5.0 191-24-2 Benzo(g,h,i)perylene ND< '" 5.0 207-08-9 Benzo(k)fluoranthene ·Nb:·-· 5.0 101-55-3 4-Bromophenyl phenyl ether ~\ 5.0 85-68-7 Butyl benzyl phthalate ND': 5.0 100-51-6 Benzyl Alcohol 'ND' 5.0 91-58-7 2-Chloronaphthalene NI>' 5.0 106-47-8 4-Chloroaniline ND 10 86-74-8 Carbazole ND 5.0 218-01-9 Cbrysene NP. 5.0 111-91-1 bis(2-Chloroethoxy)methane Nfi/' 5.0 111-44-4 bis(2-Chloroethyl)ether ND 5.0 108-60-1 bis(2-Chloroisopropyl)ether ND 5.0 7005-72-3 4-Chlorophenyl phenyl ether ND. 5.0 95-50-1 1,2-Dichlorobenzene Nb''., 5.0 541-73-1 1,3-Dichlorobenzene NP 5.0 Prep Date 01/29/07 MDL Units 10 ug/1 2.0 ug/1 2.0 ug/1 2.0 ug/1 2.0 ug/1 10 ug/1 5.0 ug/1 2.0 ug/1 2.0 ug/1 2.0 ug/1 10 ug/1 10 ug/1 2.0 ug/1 2.0 ug/1 2.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 2.0 ug/l 1.0 ug/1 1.0 ug/1 2.0 ug/1 1.0 ug/1 1.0 ug/l 4.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 2.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 Prep Batch OP19321 Page 1 of 3 Analytical Batch SL1822 Method: EPA 625 Q
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Pr~ect: Pantry 3022; Fayetteville, NC Sample File ID DF Anal)'7.Cd By OP19321-MB L035545.D 1 01/31/07 RB The QC reported here applies to the following samples: F46745-1 CASNo. Compound Result RL 106-46-7 1,4-Dicblorobenzene ND 5.0 121-14-2 2,4-Dinitrotoluene •·NJ;) 5.0 606-20-2 2,6-Dinitrotoluene ,ND . ,5.0 '.,·, 91-94-1 3,3' -Dicblorobenzidine :ND· 10 53-70-3 Dibenzo(a,h)anthracene NP 5.0 132-64-9 Dibenzofuran ND 5.0 84-74-2 Di-n-butyl phthalate Ml: 5.0 117-84-0 Di-n-octyl phthalate N.D·· 5.0 84-66-2 Diethyl phthalate ND ··.· 5.0 131-11-3 Dimethyl phthalate ND··· ·,·.· 5.0 117-81-7 bis(2-Ethylhexyl)phthalate .ND 5.0 206-44-0 Fluoranthene ,Ni)i> 5.0 86-73-7 Fluorene NP 5.0 118-74-1 Hexachlorobenzene Nt;,:\ .• 5.0 87-68-3 Hexachlorobutadiene NO ;,:; ' 5.0 77-47-4 Hexachlorocyclopentadiene .Nri . ·. 5.0 67-72-1 Hexachloroethane ND 5.0 193-39-5 Indeno(l,2,3-cd)pyrene ND 5.0 .NJ)·.· :-\ 78-59-1 lsophorone 5.0 91-57-6 2-Methylnaphthalene NP\ . . ···•·.·. 5.0 88-74-4 2-Nitroaniline NI) .. · ....... · .. 10 99-09-2 3-Nitroaniline NI). 10 100-01-6 4-Nitroaniline Nt>< 10 91-20-3 Naphthalene ND 5.0 98-95-3 Nitrobenzene ND>. 5.0 621-64-7 N-Nitroso-di-n-propylamine NP 5.0 86-30-6 N-Nitrosodiphenylamine ND 5.0 85-01-8 Phenanthrene ND 5.0 129-00-0 Pyrene ·ND 5.0 120-82-1 1,2 ,4-Trichlorobenzene ·N,I>.<'·. 5.0 CASNo. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol ~~% 19-90% 4165-62-2 Phenol-d5 ·~'1:% 10-68% Page 2 of 3 Prep Date Prep Batch Analytical Batch 01/29/07 OP19321 S11822 . Method: EPA 625 I MDL Units Q 1.0 ug/1 2.0 ug/1 2.0 ug/1 5.0 ug/1 2.0 ug/1 1.0 ug/1 2.0 ug/1 2.5 ug/1 2.0 ug/1 2.0 ug/1 2.5 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1 2.0 ug/J 2.0 ug/J 2.0 ug/1 2.0 ug/1 1.0 ug/1 1.0 ug/1 4.0 ug/1 4.0 ug/1 4.0 ug/1 1.0 ug/1 1.0 ug/1 2.0 ug/1 2.0 ug/1 1.0 ug/1 1.0 ug/1 1.0 ug/1
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19321-MB L035545.D 1 Anal)'7.ed 01/31/07 By RB The QC reported here applies to the following samples: F46745-l CASNo. Surrogate Recoveries Limits 118-79-6 2,4,6-Tribromophenol 63% 36-137% 4165-60-0 Nitrobenzene-d5 57% 49-119% 321-60-8 2-Fluorobiphenyl 58% 45-118% 1718-51-0 Terphenyl-dl 4 68%·• 46-135% Prep Date 01/29/07 Prep Batch OP19321 Page 3 of3 Analytical Batch SL1822 Method: EPA 625 Ami 29of53 l3ACCUIESI. F46745 ' 'I. L c-1· i' 1 t. · . ,. ·
I I Blank Spike Summary Page 1 of3 Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC I Sample File ID DF Anal)'7-ed By Prep Date Prep Batch .Analytical Batch OP19321-BS L035544.D 1 01/31/07 RB 01/29/07 OP19321 SL1822 I (.fl i-v I I The QC reported here applies to the following samples: Method: EPA 625 F46745-l I Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits I 65-85-0 Benzoic Acid 100 22.0 10-50 95-57-8 2-Chlorophenol 50 31.3 57-100 59-50-7 4-Chloro-3-methyl phenol 50 36.0 63-105 I 120-83-2 2, 4-Dichlorophenol 50 34.9 65-106 105-67-9 2 ,4-Dimethylphenol 50 25.5 49-90 51-28-5 2, 4-Dinitrophenol 100 60.4 60 26-125 I 534-52-1 4,6-Dinitro-o-cresol 100 81.8 .s:f ..•. 56-121 95-48-7 2-Methylphenol 50 27.9 55·.· .··· 48-90 3&4-Methylphenol 100 50.4 50 43-94 88-75-5 2-Nitrophenol 50 35.2 70. 62-107 I 100-02-7 4-Nitrophenol 100 23.7 24. 19-66 87-86-5 Pentachlorophenol 100 67.6 68 62-120 108-95-2 Phenol 50 11.5 23 .. 20-65 95-95-4 2 ,4 ,5-Trichlorophenol 50 39.0 1s···· ... 67-103 I 88-06-2 2,4,6-Trichlorophenol 50 37.7 75 68-104 83-32-9 Acenaphthene 50 36.6 73 67-101 208-96-8 Acenapbthylene 50 38.6 ;17· 65-100 I 120-12-7 Anthracene 50 38.2 7~ 71-103 56-55-3 Benzo(a)anthracene 50 39.0 78 71-105 50-32-8 Benzo(a)pyrene 50 38.7 Tl) 67-106 205-99-2 Benzo(b)fluoranthene 50 38.9 78 .. 68-108 I 191-24-2 Benzo(g,h,i)perylene 50 38.1 76 65-110 207-08-9 Benzo(k)fluoranthene 50 38.4 77 69-110 101-55-3 4-Bromophenyl phenyl ether 50 36.6 73····· .. · .. 71-106 I 85-68-7 Butyl benzyl pbthalate 50 39.2 11r 66-110 100-51-6 Benzyl Alcohol 50 29.9 l,iO 36-101 ',• 91-58-7 2-Chloronaphthalene 50 35.1 70 .. 62-99 106-47-8 4-Chloroaniline 50 34.9 10·· .. ···. 58-101 I 86-74-8 Carbazole 50 41.2 82,.· .. 73-106 218-01-9 Cbrysene 50 39.1 J~,, 71-105 111-91-1 bis(2-Cbloroethoxy)methane 50 31.4 ,63<· ·, 56-101 111-44-4 bis(2-Chloroethyl)ether 50 34.1 ·68 60-108 I 108-60-1 bis(2-Chloroisopropyl)etber 50 31.1 62 49-108 7005-72-3 4-Chlorophenyl phenyl ether 50 36.2 72 69-106 95-50-1 1,2-Dichlorobenzene 50 33.3 67 48-98 I 541-73-1 1,3-Dichlorobenzene 50 32.3 ~5 44-95 I I~~:.~ I F46745 I . :~ h ,i," ( ~ ·1· \~· r 1 :': ;
Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP19321-BS L035544.D 1 01/31/07 RB 01/29/07 OP19321 SL1822 The QC reported here applies to the following samples: Method: EPA 625 F46745-1 Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits 106-46-7 1,4-Dicblorobenzene 50 32.5 65 46-96 121-14-2 2, 4-Dioitrotoluene 50 39.7 7!f. 64-107 606-20-2 2, 6-Dioitrotoluene 50 38.8 7,· .• 64-102 91-94-1 3,3' -Dicblorobeozidioe 50 38.9 7~0 ,··. 54-109 53-70-3 Dibenzo(a,h)anthracene 50 39.5 79 61-112 132-64-9 Dibenzofman 50 36.7 73 70-102 84-74-2 Di-n-butyl phthalate 50 37.6 i75' 69-109 117-84-0 Di-n-octyl phthalate 50 39.6 1t 63-125 84-66-2 Diethyl phthalate 50 34.4 69'.••·•······ 66-111 131-11-3 Dimethyl phthaJate 50 37.5 75•.··•··. 66-109 117-81-7 bis(2-Ethylhexyl)phthalate 50 39.4 79. 66-114 206-44-0 Fluoranthene 50 40.3 81 · 71-108 86-73-7 Fluorene 50 38.7 77 68-102 118-74-1 Hexachlorobeozene 50 36.1 72 69-103 87-68-3 Hexacblorobutadiene 50 30.1 60 48-100 77-47-4 Hexachlorocyclopentadiene 50 16.9 34 20-85 67-72-1 Hexachloroethaoe 50 30.8 62 41-98 193-39-5 Indeno(l ,2,3-cd)pyreoe 50 41.0 82 .. 66-112 78-59-1 Isophorooe 50 36.2 ni ·.··• 62-105 91-57-6 2-Methylnaphthalene 50 35.8 12< 62-105 88-74-4 2-Nitroaniline 50 39.0 78 66-105 99-09-2 · 3-Nitroaniline 50 39.3 79 56-104 100-01-6 4-Nitroaoiline 50 41.5 83 62-110 91-20-3 Naphthalene 50 33.8 6$> 56-99 98-95-3 Nitrobenzene 50 32.5 ss,·· 60-102 621-64-7 N-Nitrmo-di-n-propylamine 50 32.2 ,64 56-101 86-30-6 N-Nitrosodiphenylamine 50 35.8 72 69-106 85-01-8 Phenanthrene 50 37.9 76 71-104 129-00-0 Pyrene 50 38.6 77 67-108 120-82-1 1,2 ,4-Trichlorobenzeoe 50 32.7 6~ 52-99 CASNo. Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 37%• 19-90% 4165-62-2 Phenol-d5 23% 10-68% t..l'l M II
Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sam.pk File ID DF Analyzed By OP19321-BS L035544.D 1 01/31/07 RB The QC reported here applies to the following samples: F46745-1 CASNo. Surrogate Recoveries BSP Limits 118-79-6 2,4 ,6-Tribromophenol JI%·· 36-137% 4165-60-0 Nitrobenzene-d5 62% 49-119% 321-60-8 2-Fluorobiphenyl 66% 45-118% 1718-51-0 Terphenyl-d14 13%· J 46-135% Page 3 of 3 Prep Date Prep Batch Analytical Batch 01/29/07 OP19321 SL1822 \'J'I N Method: EPA 625 I
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number: F46745 Aocount: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP19321-MS L035547.D 1 01/31/07 RB 01/29/07 OP19321-MSD L035548.D 1 01/31/07 RB 01/29/07 F46745-l L035546.D 1 01/31/07 RB 01/29/07 The QC reported here applies to the following samples: F46745-l F46745-l Spike MS CASNo. Compound ug/1 Q ug/1 ug/1 65-85-0 BenzoicAdd ND 192 66.6 95-57-8 2-Chloropbenol ND 96.2 70.1 59-50-7 4-Cbloro-3-methyl phenol ND 96.2 78.4 120-83-2 2,4-Dichlorophenol ND 96.2 75.2 105-67-9 2,4-Dimethylphenol ND 96.2 57.2 51-28-5 2 ,4-Dinitrophenol ND 192 132 534-52-1 4 ,6-Dinitro-o-cresol ND 192 176 95-48-7 2-Metbylphenol ND 96.2 63.8 3&4-Methylphenol ND 192 126 88-75-5 2-Nitrophenol ND 96.2 73.9 100-02-7 4-Nitrophenol ND 192 76.1 87-86-5 Pentachlorophenol ND 192 139 108-95-2 Phenol ND 96.2 41.0 95-95-4 2 ,4, 5-Trichloropbenol ND 96.2 79.6 88-06-2 2, 4, 6-Tricblorophenol ND 96.2 77.8 83-32-9 Acenaphthene ND 96.2 76.3 208-96-8 Acenaphthylene ND 96.2 76.5 120-12-7 Anthracene ND 96.2 81.1 56-55-3 Benzo(a)anthracene ND 96.2 83.5 50-32-8 Benzo(a)pyrene ND 96.2 83.5 205-99-2 Benzo(b)fluoranthene ND 96.2 85.3 191-24-2 Benzo(g,h,i)perylene ND 96.2 81.2 207-08-9 Benzo(k)fluorantbene ND 96.2 80.2 101-55-3 4-Bromophenyl phenyl ether ND 96.2 76.1 85-68-7 Butyl benzyl phtbalate ND 96.2 84.3 100-51-6 Benzyl Alcohol ND 96.2 67.7 91-58-7 2-Chloronaphthalene ND 96.2 71.3 106-47-8 4-Chloroaoiline ND 96.2 69.4 86-74-8 Carbazole ND 96.2 87.4 218-01-9 Cbrysene ND 96.2 82.3 111-91-1 bis(2-Chloroethoxy) methane ND 96.2 67.2 111-44-4 bis(2-Chloroethyl)ether ND 96.2 75.0 108-60-1 bis(2-Cbloroisopropyl)etber ND 96.2 67.5 7005-72-3 4-Chlorophenyl phenyl ether ND 96.2 76.3 95-50-1 1,2-Dicblorobenzene ND 96.2 70.2 541-73-1 1,3-Dichlorobenzene ND 96.2 68.5 OP19321 OP19321 OP19321 Method: MS MSD % ug/1 35 69.2 73 .·. 66.9 st 72.7 '78·'' · 70.6 59 52.7 '' 69 · 125 92,' 165 66 61.7 66 122 77,· 72.0 .fQ' ' 71.1 .tt: 129 43·;•· ,, 40.6 83 75.4 81, 73.2 79,; 73.1 so,. 75.3 84' 75.9 87 76.5 s1;/ 75.7 89 75.2 84· 74.3 ·,83···· 74.4 79 71.3 :88 75.8 10··, '., 67.4 ?4 70.5 J? 59.5 91 80.5 ,i~i 74.6 70'·.··, ... 64.6 ,73';· 71.9 ,70 66.7 79•_· .. 71.5 73 69.9 7i. 68.4 SL1822 SL1822 ~-SL1822 w EPA 625 MSD Limits % RPD Rec/R.PD ,36' 70 . w· : ·:,.·".,: 73' 55 65 '·· 86\ fi4 ·,' ,63 75: 37 57 ··_ ..• 42 78 .. 76 76 78 79 > · 80. 79·.: 78 77 77, 74 79 70 73 62 84 78 67' 75 69 74 7~ 11 4 10-80/45 5 43-109/27 •....• 8 ,' 57-109/20 '6' 49-114/23 .. ,8 32-103/24 5,, 20-131/28 6' 46-130/23 3' 40-102/25 3 ... , 39-97/24 '3' 46-115/26 7 28-81/30 7 53-128/22 r•· 19-81/33 ,5 56-110/19 6 · 55-112/19 4''·' 58-109/18 ··2··.·. 7 9 10,. 13, 9 8 ·'l • lL. 0 ' -1 ! '., 15' :8 10·•.,. 4 ,f •· 1 6 Q •(j 59-103/18 65-108/16 68-106/17 61-108/18 65-109/18 60-114/19 66-111/17 68-108/17 64-111/18 44-105/26 >, 57-102/20 37-106/27 68-111/16 69-106/17 46-106/24 48-114/28 43-110/26 66-107/17 45-103/24 42-100/24 fin 33of53 CJACCll • i ES i. F46745 / -1 (: c"' r .~ t r. -, j t; ;
Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Page 2 of 3 Sample File ID DF Analy7.ed By Prep Date Prep Batch Analytical Batch OP19321-MS 1..035547.D 1 01/31/07 RB OP19321-MSD L035548.D 1 01/31/07 RB F46745-1 1..035546.D 1 01/31/07 RB The QC reported here applies to the following samples: F46745-l F46745-l Spike CASNo. Compound ug/1 Q ug/1 106-46-7 1,.t-Dichlorobenzene ND 96.2 121-14-2 2, 4-Dinitrotoluene ND 96.2 606--20-2 2, 6-Dinitrotoluene ND 96.2 91-94-1 3,3' -Dichlorobeozidine ND 96.2 53-70-3 Dibenzo(a,h)anthracene ND 96.2 132-64-9 Dibenzofurao ND 96.2 84-74-2 Di-n-butyl phthalate ND 96.2 117-84-0 Di-n-octyl phthalate ND 96.2 84-66-2 Diethyl phthalate ND 96.2 131-11-3 Dimethyl phthalate ND 96.2 117-81-7 bis(2-Ethylhexyl)phthalate ND 96.2 206--44-0 Fluorantheoe ND 96.2 86-73-7 Fluorene ND 96.2 118-74-1 Hexachlorobenzene ND 96.2 87-68-3 Hexachlorobutadieoe ND 96.2 77-47-4 Hexachlorocyclopentadiene ND 96.2 67-72-1 Hexachloroethane ND 96.2 193-39-5 Indeno(l ,2,3-cd)pyrene ND 96.2 78-59-1 Isophorooe ND 96.2 91-57-6 2-Methyloaphthaleoe ND 96.2 88-74-4 2-Nitroanilioe ND 96.2 99-09-2 3-Nitroaoilioe ND 96.2 100-01-6 4-Nitroaoiline ND 96.2 91-20-3 Naphthalene ND 96.2 98-95-3 Nitrobeozene ND 96.2 621-64-7 N-Nitroso--di-o-propylamine ND 96.2 86-30-6 N-Nitrosodiphenylamioe ND 96.2 85-01-8 Pbeoaothrene ND 96.2 129-00-0 Pyrene ND 96.2 120-82-1 1,2 ,4-Trichlorobeozene ND 96.2 CASNo. Surrogate Recoveries MS MSD 367-12-4 2-Fluoropbeool 'S?Jfo. 52% 4165-62-2 Phenol-d5 $~ 33% 01/29/07 OP19321 SL1822 01/29/07 OP19321 SL1822 5ft. 01/29/07 OP19321 SL1822 w Method: EPA 625 MS MS MSD ug/1 % ug/1 69.0 72 , 67.1 83.4 87,: . ·, 76.9 78.4 ~2 73.8 63.9 66 67.3 83.7 81. 76.4 75.5 79 72.5 80.2 83_ ·. 73.9 84.1 87 73.9 73.2 75: ,, 66.8 78.5 82 '.· >_ 74.1 83.7 :8-1 75.1 86.5 90 · 79.3 79.3 )J2 75.1 77.9 81 71.3 66.4 69. · 64.2 31.3 ~:f 38.3 65.7 '68 · •. 65.9 86.8 90. it' 79.8 76.6 80 73.1 75.3 r~i:.-71.9 78.6 ~2-.' ' 74.4 77.9 .8_1 68.7 85.9 8~ 77.6 71.4 74 . 69.2 69.2 72 66.6 68.5 n 66.6 73.2 76 • 69.8 80.9 84.-·. 75.5 83.1 86-''. 76.7 70.2 13 67.2 F46745-1 Limits 36% 19-90% 2?,% 10-68% MSD % '.10. ·so 77 70 79 75·: 77 ,77 :59_·. 11··._· 78 · 82, · is.·. 74 -67 40-69 83 ' 75' 75_: 77 71 81 72' 69: 69'••·. 73:; 79 80' 70 Limits RPD RedR.PD ,.3_. 43-102/24 8 60-108/18 6 59-105/18 5,'. 21-120/24 9 59-112/18 4·· 65-105/17 8. 68-109/18 13 59-127/23 9, ,··· 64-111/18 6 11 9 5 9 3· . , 20 -·. O' .8 5· 5 5 J3· tO. 3.··. 4 3 5 7 :3 4 63-109/17 58-119/21 68-110/18 62-106/17 66-106/16 46-107/26 16-84/31 39-105/25 61-115/19 54-107/22 53-112/22 60-108/18 43-103/23 55-110/19 49-104/24 _ 50-107/25 47-104/23 63-110/17 67-108/17 65-108/18 49-104/25 1111!1 34of53 Q.ACC:1 • 2 ES I. F46745 1 ' ,., 0 ,· ,, 1 " '· ' '
Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Prqject: Pantry 3022; Fayetteville, NC Samp~ File ID DF OP19321-MS 1035547.D 1 OP19321-MSD 1035548.D 1 F46745-1 1035546.D 1 Analyzed By 01/31/07 RB 01/31/07 RB 01/3.1/07 RB The QC reported here applies to the following samples: F46745-1 Prep Date 01/29/07 01/29/07 01/29/07 Prep Batch OP19321 OP19321 OP19321 Page 3 of 3 Analytical Batch SL1822 SL1822 SL1822 Method: EPA 625 CAS No. Surrogate Recoveries MS .11%./ '67%: MSD F4674S-l Limits 118-79-6 4165-60-0 321-60-8 1718-51-0 2,4,6-Tribromopbenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14 68%. 77% II) 35of53 ;J~ieST. F46745 '"" ·,,,., ,,, '
f111D Southeast IIACCU I EST. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 6 I
Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC SampJe File ID DF Analymd By GUV1473-MB UV025619.D1 01/25/07 MM The QC reported here applies to the following samples: F46745-l CASNo. Compound Result RL CS-C8 Aliphatics (Unadj.) ~Jfi._ 75 C9-C12 Alipbatics (Unadj.) ~\. 55 C9-CI0 Aromatics (Unadj.) 20 ~ '"· -·~ CASNo. Surrogate Recoveries Limits Page 1 of 1 Prep Date Prep Batch Analytical Batch n/a n/a GUV1473 Method: MADEP VPH I MDL Units Q 50 ug/1 30 ug/l 10 ug/1 460-00-4 BFB 97% 70-130% 460-00-4 BFB 93~¾/ 70-130% 111!1 37 of 53 CiACCUTEST. F-46745 l ;i h i~· 1·, t "r ! ~ !,.
Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF Analyzed By OP19286-MB DD37682.D 1 01/26/07 NJ The QC reported here applies to the following samples: F46745-1 CAS No. Compound Result RL 106-93-4 1,2-Dibromoethane CAS No. Surrogate Recoveries Limits Page 1 of 1 Prep Date Prep Batch Ana.lytical Batch 01/25/07 OP19286 GDD1029 Method: EPA 504.l I MDL Units Q 460-00-4 4-Bromofluorobenzene 63-137% 111 3Sof53 gACX:u • esr. F46745 l. ;-1 h '' 1· ;,; r ,:: ,. ; :: "·
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Samp:le File ID DF GUV1473-BS UV025620.D 1 Analymi 01/25/07 By MM Prep Date n/a The QC reported here applies to the following samples: F46745-1 Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits CS-C8 Aliphatics (Unadj.) 480 445 93 70-130 C9-C12 Alipbatics (Unadj.) 480 495 103 70-130 C9-Cl0 Aromatics (Unadj.) 80 81.8 102; 70-130 CASNo. Surrogate Recoveries BSP Limits 460-00-4 BFB 118% < 70-130% 460-00-4 BFB it[% 70-130% Prep Batch n/a Page 1 of 1 Analytical Batch GUV1473 Method: MADEP VPH I 111!! 39 of 53 (IACCliieSM. F46745 I 11 I) ,":-· r .,,. r f,-~·, :: ,
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample File ID DF OP19286-BS DO37680.D 1 Anafy?.ed 01/26/07 By NJ Prep Date 01/25/07 The QC reported here applies to the following samples: F46745-1 Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits 106-93-4 1,2-Dibromoethane 0.25 0.25 i(l(} 70-130 CASNo. Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 105% 63-137% Prep Batch OP19286 Page 1 of 1 Analytical Batch GDD1029 Method: EPA 504.1 I
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sample File ID DF OP19286-BS2 OD37681.D 1 Analyzed 01/26/07 By NJ Prep Date 01/25/07 The QC reported here applies to the following samples: F46745-1 Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits 106-93-4 1,2-Dibromoetbane 0.25 0.25 t0.q.••· 70-130 CASNo. Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 102% 63-137% Prep Batch OP19286 Page 1 of 1 Analytical Batch GDD1029 Method: EPA 504.1 m 111!1 41 of53 1\1.ACCIIVESI. F46745 I. i1 h ,-,, ·:· y; ' i1· ,. ; r: ,:
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary lob Number: F46745 .Acco1U1t: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Samp:le F46745-1MS F46745-1MSD F46745-1 File ID DF UV025624.D1 UV025625 .D 1 UV025621.D 1 Analyzed 01/25/07 01/25/07 01/25/07 By MM MM MM Prep Date n/a n/a n/a Prep Batch n/a n/a n/a Page 1 of 1 Analytical Batch GUV1473 GUV1473 GUV1473 en The QC reported here applies to the following samples: Method: MADEP VPH t., F46745-1 F46745-1 CASNo. Compound ug/1 Q CS-C8 Aliphatics (Unadj.) ND C9-C12 Aliphatics (Unadj.) ND C9-ClO Aromatics (Unadj.) ND CASNo. Surrogate Recoveries MS 460-00-4 BFB Ho%•···. 460-00-4 BFB Hl9<>. Spike ug/1 480 480 80 MSD 109% .. mti MS ug/1 MS MSD MSD Limits % ug/1 % RPD Rec/RPD 426 .89 ; < 430 00 . 462 96 .. ·. 457 95 77.4 -~1--· 76.9 ~ J. 70-130/50 1. . 70-130/50 ,1,· 70-130/50 F46745-1 Limits Joi% 10-130% 9~9(, · 70-130% I
I I I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample File ID DF OP19286-MS DO37686.D 1 OP19286-MSD DO37687 .D 1 F46618-2 DO37685.D 1 Analyzed By 01/26/07 NJ 01/26/07 NJ 01/26/07 NJ The QC reported here applies to the following samples: F46745-1 F46618-2 Spike CAS No. Compound ug/1 Q ug/1 106-93-4 1,2-Dibromoethane 0.019 U 0.233 Prep Date 01/25/07 01/25/07 01/25/07 MS MS ug/1 % 0.20 Jtf Prep Batch OP19286 OP19286 OP19286 Page 1 of 1 Analytical Batch GDD1029 GDD1029 GDD1029 a, Method: EPA 504.1 w I MSD MSD Limits ug/1 % RPD Rec/RPD 0.21 CAS No. Surrogate Recoveries MS 1Q2% MSD F46618-2 Limits 460-00-4 4-Bromofluorobenzene 98.%. 107% 63-137%
I I I I I I I I I I I I I I I I I I I Duplicate Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Sampre File ID DF F46683-1DUP UV025623.Dl F46683-l UV025622.Dl Analy7.ed 01/25/07 01/25/07 By MM MM Prep Date n/a n/a Prep Batch n/a n/a Page 1 of 1 Analytical Batch GUV1473 GUV1473 The QC reported here applies to the following samples: Method: MADEP VPH F46745-l F46683-1 CASNo. Compound ug/1 Q C5-C8 Aliphatics (Unadj.) ND C9-Cl2 Aliphatics (Unadj.) ND C9-ClO Aromatics (Unadj.) ND CASNo. Surrogate Recoveries DUP 460-00-4 BFB ~% 460-00-4 BFB 91%< DUP ug/1 Q ND ND ND F46683-l ~9~ ~:% RPD Limits Lun.its 70-130% 70-130% I llffll 44of53 IIACCl Bi ES,. F46745 \ ,, b ,; r ;. ·1· \·:··,; i ;-:: a
I I I I I I I I I I I I I I I I I I I 1111!/1 . Southeast IIACCUIESf~ QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Splice Summaries • Matrix Splice and Duplicate Summaries II ..
I I I I I I I I I I I I I I I I I I I Method Blank Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC Page 1 of 1 Sample File ID DF Anal)'7.Cld By Prep Date Prep Batch Analytical Batch OP19299-MB ZF22521.D 1 01/30/07 AC 01/26/07 OP19299 GZF1054 The QC reported here applies to the following samples: Method: MADEP-EPH-98-1 F46745-1 CASNo. Compound Result Cll-C22 Aromatics (Unadj.) «s·> . . C9-Cl8 Aliphatics ND, ... C19-C36 Aliphatics NPi CASNo. Surrogate Recoveries 3386-33-2 1-Cblorooctadecane 78,% 580-13-2 2-Bromonaphthalene 86% • .. ·.;',•I,,', 84-15-1 o-Terphenyl 90% ..... ,.•, 321-60-8 2-Fluorobiphenyl 91% RL MDL 200 150 200 200 200 200 Limits 40-140% 40-140% 40-140% 40-140% Units Q ug/1 ug/1 ug/1 ..... :... II 46 of 53 EEST. F46745 t ;] h fr i· ~. I ,-; (; •• ,.
I I I I I I I I I I I I I I I I I I I Blank Spike Summary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC SampJe File ID DF OP19299-BS ZF22520.D 1 Analyzed 01/30/07 By AC Prep Date 01/26/07 The QC reported here applies to the following samples: F46745-l Spike BSP BSP CASNo. Compound ug/1 ug/1 % Limits Cll-C22 Aromatics (Unadj.) 1700 900 53 :',' 40-140 ,. C9-C18 Aliphatics 600 558 93 40-140 C19-C36 Aliphatics 800 687 ~.~ 40-140 CASNo. Surrogate Recoveries BSP Limits 3386-33-2 1-Chlorooctadecaoe 1-7% ,, .·. 40-140% 580-13-2 2-Bromonaphthalene 46?(, .. 40-140% 84-15-1 o-Terphenyl 53%· 40-1400/4 321-60-8 2-Fluorobiphenyl 55%. 40-140% Prep Batch OP19299 Page 1 of 1 Analytical Batch GZF1054 Method: MADEP-EPH-98-1 ...., iv I 111!1 47 of 53 QACCl i l"ES'I. F46745 ! H h ,:, ·, . .::.'1 r; !' ! :: ·;
I I I I I I I I I I I I I I I I I Matrix Spike/Matrix Spike Duplicate S11mmary Job Number: F46745 Account: SEINCR SEI Environmental-Raleigh Project: Panny 3022; Fayetteville, NC Sample File ID DF OP19299-MS ZF22523.D 1 OP19299-MSD ZF22524.D 1 F46745-1 ZF22522.D 1 Analyzed By 01/30/07 AC 01/30/07 AC 01/30/07 AC The QC reported here applies to the following samples: F46745-1 F46745-1 Spike CASNo. Compound ug/1 Q ug/1 Cll-C22 Aromatics (Unadj.) ND 3270 C9-C18 Aliphatics ND 1150 CI9-C36 Aliphatics ND 1540 Prep Date 01/26/07 01/26/07 01/26/07 MS ug/1 1830 1060 1450 MS % Prep Batch OP19299 OP19299 OP19299 Page 1 of 1 Analytical Batch GZF1054 GZF1054 GZF1054 Method: MADEP-EPH-98-1 ""' w MSD MSD Limits II ug/1 % RPD Rec/RPD 2320 71 1120 97 1600 104 40-140/50 40-140/50 40-140/50 CASNo. Surrogate Recoveries MS MSD F46745-1 Limits 3386-33-2 1-Chlorooctadecane 74% 580-13-2 2-Bromonaphthalene 64% 84-15-1 o-Terphenyl 55% 321-60-8 2-Fluorobiphenyl 56% ~~% 68% 73% 68% 6!}% 64% 64% 67% 40-140% 40-140% 40-140% 40-140% IUf!I 48of53 IIACCU ii ES,. F46745 ''" ""'"'''··
I I I I I I I I I I I I I I I I I I I 111!1 . Southeast CiAccuiESI., QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries I m.. 49of53 liACalieSI. F46745 i ;; h ,; r 1: t ,~ ~ , c: ·,
I I I I I I I I I I I I I I I I I I I QC Batch ID: MPlllOO Matrix Type: AQUEOUS Prep Date: !Metal RL Aluminum 200 Antimony 6.0 ArSenic 10 Barium 200 Beryllium 4.0 Cadmium 5.0 Calcium 1000 Chromium 10 Cobalt 50 Copper 25 Iron 300 Lead 5.0 Magnesium 5000 Manganese 15 Molybdenum 50 Nickel 40 Potassium 10000 Selenium 10 Silver 10 Sodium 10000 Thallium 10 Tin 50 Vanadium 50 Zinc 20 IDL J.8 3.4 2.8 5 l l 42 .6 l .9 12 J..? 4.3 .6 1.3 l 10 2 .9 500 2.3 3.1 .6 1.3 BLANK RESULTS SUMMARY Part 2 -Method Blanks Login Number: F46?45 Account: SEINCR -SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC MB raw final Methods: SW846 6010B Units: ug/1 Associated samples MPllJ.00: F46?45-l Results< IDL are shown as zero for calculation purposes (*) outside of QC limits (anr) Analyte not requested Pagel I
I I I I I I I I I I I I I I I I I I I MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: F46745 Accowit: SEINCR -SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC QC Batch ID: MPlll00 Matril< Type: AQUEOUS Prep Date: AluminUlll Antimony Arsenic Bariwn BerylliUlll Cadmium Calcium Chromium Cobalt Copper Iron Lead 4.2 Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Vanadium Zinc 5.0 Associated samples MPlll00: F46745•1 0-20 4.2 Results< IDL are shown as zero for calculation purposes (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested Pagel Methods: SW846 6010B units: ug/1 502 500 80-120 I 1111!1 51 of53 gAca • 11 es 1. F46745 l il.h n r ;, f i'
I I I I I I I I I I I I I I I I I I I SPIKE BLANK AND I..AB CONTROL SAMPLE SUMMARY Login Number: F46745 Account: SEINCR -SEI Environmental-Raleigh Project: Pantry 3022; Fayetteville, NC QC Batch ID: MPlll00 Matrix Type: AQUEOUS Prep Date: Metal Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Vanadium Zinc BSP Result 502 Spikelot MPFLICPl 't Rec 500 Associated samples MPlll00: F46745-l QC Limits 80-120 Results< IDL are shown as zero for calculation purposes {*) Outside of QC limits (anr) Analyte not requested Pagel Methods: SW846 6010B units: ug/1 I tlf!.I 52of53 ■ACCUT"EST.
I I I I I I I I I I I I I I I I I I I SERIAt. DILUI'ION RESULTS SUMMARY Login Number: F46745 Account: SEINCR -SEI Environmental-Raleigh Project, Pantry 3022; Fayetteville, NC QC Batch ID: MPlllOO Matrix Type: AQUEOUS Prep Date: F46745-l lil/:ZS/07 Metal Original SDL l:5 RPD Aluminum Antimony 'Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Vanadium Zinc 4.18 0.00 Associated samples MPlllOO: F46745-l QC Limits 0-10 Results< IDL are shown as zero for calculation purposes (*) outside of QC limits (anr) Analyte not requested Methods: SW846 60lOB Units: ug/1 (a) Percent difference acceptable due to low initial sample concentration (< SO times IDL). Pagel lill!I 53of53 liACCUT=ST. F467-45 l · 11 Ii ,:, 1· i ! 1':: ·r : c: ,