AS-4431_41488_CA_LAB_20221027

#=CL#
November 02, 2022
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92633456
92633456
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
Crown Food Mart 10/27
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on October 28, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Lab ID Sample ID Matrix Date Collected Date Received
92633456001 MW-16 Water 10/27/22 10:41 10/28/22 09:24
92633456002 MW-6A Water 10/27/22 12:25 10/28/22 09:24
92633456003 SW-14 Water 10/27/22 12:52 10/28/22 09:24
92633456004 SW-11 Water 10/27/22 12:56 10/28/22 09:24
92633456005 SW-13 Water 10/27/22 13:17 10/28/22 09:24
92633456006 SW-12 Water 10/27/22 13:22 10/28/22 09:24
92633456007 MW-8 Water 10/27/22 13:37 10/28/22 09:24
92633456008 MW-13 Water 10/27/22 15:15 10/28/22 09:24
92633456009 SW-01-185 Water 10/27/22 15:10 10/28/22 09:24
92633456010 SW-02-185 Water 10/27/22 15:25 10/28/22 09:24
92633456011 SW-03-185 Water 10/27/22 15:40 10/28/22 09:24
92633456012 MW-14 Water 10/27/22 16:45 10/28/22 09:24
92633456013 DUPE Water 10/27/22 00:00 10/28/22 09:24
92633456014 DUP 2 Water 10/27/22 00:00 10/28/22 09:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92633456001 MW-16 SM 6200B 63 PASI-CSAS
92633456002 MW-6A SM 6200B 63 PASI-CSAS
92633456003 SW-14 SM 6200B 63 PASI-CSAS
92633456004 SW-11 SM 6200B 63 PASI-CSAS
92633456005 SW-13 SM 6200B 63 PASI-CSAS
92633456006 SW-12 SM 6200B 63 PASI-CSAS
92633456007 MW-8 SM 6200B 63 PASI-CSAS
92633456008 MW-13 SM 6200B 63 PASI-CSAS
92633456009 SW-01-185 SM 6200B 63 PASI-CSAS
92633456010 SW-02-185 SM 6200B 63 PASI-CSAS
92633456011 SW-03-185 SM 6200B 63 PASI-CSAS
92633456012 MW-14 SM 6200B 63 PASI-CSAS
92633456013 DUPE SM 6200B 63 PASI-CSAS
92633456014 DUP 2 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-16 Lab ID:92633456001 Collected:10/27/22 10:41 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/22 16:17 71-43-22.5 1.7 5
Bromobenzene ND ug/L 11/01/22 16:17 108-86-12.5 1.4 5
Bromochloromethane ND ug/L 11/01/22 16:17 74-97-52.5 2.3 5
Bromodichloromethane ND ug/L 11/01/22 16:17 75-27-42.5 1.5 5
Bromoform ND ug/L 11/01/22 16:17 75-25-22.5 1.7 5
Bromomethane ND ug/L 11/01/22 16:17 74-83-925.0 8.3 5
n-Butylbenzene ND ug/L 11/01/22 16:17 104-51-82.5 2.4 5
sec-Butylbenzene ND ug/L 11/01/22 16:17 135-98-82.5 2.0 5
tert-Butylbenzene ND ug/L 11/01/22 16:17 98-06-62.5 1.6 5
Carbon tetrachloride ND ug/L 11/01/22 16:17 56-23-52.5 1.7 5
Chlorobenzene ND ug/L 11/01/22 16:17 108-90-72.5 1.4 5
Chloroethane ND ug/L 11/01/22 16:17 75-00-35.0 3.2 5
Chloroform ND ug/L 11/01/22 16:17 67-66-32.5 2.2 5
Chloromethane ND ug/L 11/01/22 16:17 74-87-35.0 2.7 5
2-Chlorotoluene ND ug/L 11/01/22 16:17 95-49-82.5 1.6 5
4-Chlorotoluene ND ug/L 11/01/22 16:17 106-43-42.5 1.6 5
1,2-Dibromo-3-chloropropane ND ug/L 11/01/22 16:17 96-12-85.0 1.7 5
Dibromochloromethane ND ug/L 11/01/22 16:17 124-48-12.5 1.8 5
1,2-Dibromoethane (EDB)ND ug/L 11/01/22 16:17 106-93-42.5 1.4 5
Dibromomethane ND ug/L 11/01/22 16:17 74-95-32.5 2.0 5
1,2-Dichlorobenzene ND ug/L 11/01/22 16:17 95-50-12.5 1.7 5
1,3-Dichlorobenzene ND ug/L 11/01/22 16:17 541-73-12.5 1.7 5
1,4-Dichlorobenzene ND ug/L 11/01/22 16:17 106-46-72.5 1.7 5
Dichlorodifluoromethane ND ug/L 11/01/22 16:17 75-71-82.5 1.7 5
1,1-Dichloroethane ND ug/L 11/01/22 16:17 75-34-32.5 1.8 5
1,2-Dichloroethane ND ug/L 11/01/22 16:17 107-06-22.5 1.6 5
1,1-Dichloroethene ND ug/L 11/01/22 16:17 75-35-42.5 1.7 5
cis-1,2-Dichloroethene ND ug/L 11/01/22 16:17 156-59-22.5 1.9 5
trans-1,2-Dichloroethene ND ug/L 11/01/22 16:17 156-60-52.5 2.0 5
1,2-Dichloropropane ND ug/L 11/01/22 16:17 78-87-52.5 1.8 5
1,3-Dichloropropane ND ug/L 11/01/22 16:17 142-28-92.5 1.4 5
2,2-Dichloropropane ND ug/L 11/01/22 16:17 594-20-72.5 1.9 5
1,1-Dichloropropene ND ug/L 11/01/22 16:17 563-58-62.5 2.1 5
cis-1,3-Dichloropropene ND ug/L 11/01/22 16:17 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 11/01/22 16:17 10061-02-62.5 1.8 5
Diisopropyl ether ND ug/L 11/01/22 16:17 108-20-32.5 1.5 5
Ethylbenzene 282 ug/L 11/01/22 16:17 100-41-42.5 1.5 5
Hexachloro-1,3-butadiene ND ug/L 11/01/22 16:17 87-68-310.0 7.6 5
Isopropylbenzene (Cumene)43.7 ug/L 11/01/22 16:17 98-82-82.5 1.7 5
Methylene Chloride ND ug/L 11/01/22 16:17 75-09-210.0 9.8 5
Methyl-tert-butyl ether ND ug/L 11/01/22 16:17 1634-04-42.5 2.1 5
Naphthalene 38.5 ug/L 11/01/22 16:17 91-20-310.0 3.2 5
n-Propylbenzene 129 ug/L 11/01/22 16:17 103-65-12.5 1.7 5
Styrene ND ug/L 11/01/22 16:17 100-42-52.5 1.5 5
1,1,1,2-Tetrachloroethane ND ug/L 11/01/22 16:17 630-20-62.5 1.6 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-16 Lab ID:92633456001 Collected:10/27/22 10:41 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 11/01/22 16:17 79-34-52.5 1.1 5
Tetrachloroethene ND ug/L 11/01/22 16:17 127-18-42.5 1.5 5
Toluene 310 ug/L 11/01/22 16:17 108-88-32.5 1.2 5
1,2,3-Trichlorobenzene ND ug/L 11/01/22 16:17 87-61-610.0 4.0 5
1,2,4-Trichlorobenzene ND ug/L 11/01/22 16:17 120-82-110.0 3.2 5
1,1,1-Trichloroethane ND ug/L 11/01/22 16:17 71-55-62.5 1.7 5
1,1,2-Trichloroethane ND ug/L 11/01/22 16:17 79-00-52.5 1.6 5
Trichloroethene ND ug/L 11/01/22 16:17 79-01-62.5 1.9 5
Trichlorofluoromethane ND ug/L 11/01/22 16:17 75-69-45.0 1.5 5
1,2,3-Trichloropropane ND ug/L 11/01/22 16:17 96-18-42.5 1.3 5
1,2,4-Trimethylbenzene 637 ug/L 11/01/22 16:17 95-63-62.5 2.5 5
1,3,5-Trimethylbenzene 147 ug/L 11/01/22 16:17 108-67-82.5 1.7 5
Vinyl chloride ND ug/L 11/01/22 16:17 75-01-45.0 1.9 5
m&p-Xylene 1030 ug/L 11/01/22 16:17 179601-23-15.0 3.5 5
o-Xylene 307 ug/L 11/01/22 16:17 95-47-62.5 1.7 5
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/01/22 16:17 17060-07-070-130 5
4-Bromofluorobenzene (S)102 %11/01/22 16:17 460-00-470-130 5
Toluene-d8 (S)99 %11/01/22 16:17 2037-26-570-130 5
Sample:MW-6A Lab ID:92633456002 Collected:10/27/22 12:25 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 18:15 71-43-210.0 6.9 20
Bromobenzene ND ug/L 10/31/22 18:15 108-86-110.0 5.8 20
Bromochloromethane ND ug/L 10/31/22 18:15 74-97-510.0 9.4 20
Bromodichloromethane ND ug/L 10/31/22 18:15 75-27-410.0 6.1 20
Bromoform ND ug/L 10/31/22 18:15 75-25-210.0 6.8 20
Bromomethane ND ug/L 10/31/22 18:15 74-83-910033.2 20
n-Butylbenzene ND ug/L 10/31/22 18:15 104-51-810.0 9.8 20
sec-Butylbenzene ND ug/L 10/31/22 18:15 135-98-810.0 8.0 20
tert-Butylbenzene ND ug/L 10/31/22 18:15 98-06-610.0 6.5 20
Carbon tetrachloride ND ug/L 10/31/22 18:15 56-23-510.0 6.7 20
Chlorobenzene ND ug/L 10/31/22 18:15 108-90-710.0 5.7 20
Chloroethane ND ug/L 10/31/22 18:15 75-00-320.0 13.0 20
Chloroform ND ug/L 10/31/22 18:15 67-66-310.0 8.6 20
Chloromethane ND ug/L 10/31/22 18:15 74-87-320.0 10.8 20
2-Chlorotoluene ND ug/L 10/31/22 18:15 95-49-810.0 6.4 20
4-Chlorotoluene ND ug/L 10/31/22 18:15 106-43-410.0 6.5 20
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 18:15 96-12-820.0 6.8 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-6A Lab ID:92633456002 Collected:10/27/22 12:25 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 10/31/22 18:15 124-48-110.0 7.2 20
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 18:15 106-93-410.0 5.4 20
Dibromomethane ND ug/L 10/31/22 18:15 74-95-310.0 7.9 20
1,2-Dichlorobenzene ND ug/L 10/31/22 18:15 95-50-110.0 6.8 20
1,3-Dichlorobenzene ND ug/L 10/31/22 18:15 541-73-110.0 6.8 20
1,4-Dichlorobenzene ND ug/L 10/31/22 18:15 106-46-710.0 6.7 20
Dichlorodifluoromethane ND ug/L 10/31/22 18:15 75-71-810.0 6.9 20
1,1-Dichloroethane ND ug/L 10/31/22 18:15 75-34-310.0 7.3 20
1,2-Dichloroethane ND ug/L 10/31/22 18:15 107-06-210.0 6.4 20
1,1-Dichloroethene ND ug/L 10/31/22 18:15 75-35-410.0 7.0 20
cis-1,2-Dichloroethene ND ug/L 10/31/22 18:15 156-59-210.0 7.7 20
trans-1,2-Dichloroethene ND ug/L 10/31/22 18:15 156-60-510.0 7.9 20
1,2-Dichloropropane ND ug/L 10/31/22 18:15 78-87-510.0 7.1 20
1,3-Dichloropropane ND ug/L 10/31/22 18:15 142-28-910.0 5.7 20
2,2-Dichloropropane ND ug/L 10/31/22 18:15 594-20-710.0 7.8 20
1,1-Dichloropropene ND ug/L 10/31/22 18:15 563-58-610.0 8.5 20
cis-1,3-Dichloropropene ND ug/L 10/31/22 18:15 10061-01-510.0 7.3 20
trans-1,3-Dichloropropene ND ug/L 10/31/22 18:15 10061-02-610.0 7.3 20
Diisopropyl ether ND ug/L 10/31/22 18:15 108-20-310.0 6.2 20
Ethylbenzene 909 ug/L 10/31/22 18:15 100-41-410.0 6.1 20
Hexachloro-1,3-butadiene ND ug/L 10/31/22 18:15 87-68-340.0 30.6 20
Isopropylbenzene (Cumene)124 ug/L 10/31/22 18:15 98-82-810.0 6.7 20
Methylene Chloride ND ug/L 10/31/22 18:15 75-09-240.0 39.0 20
Methyl-tert-butyl ether ND ug/L 10/31/22 18:15 1634-04-410.0 8.4 20
Naphthalene 160 ug/L 10/31/22 18:15 91-20-340.0 12.9 20
n-Propylbenzene 326 ug/L 10/31/22 18:15 103-65-110.0 6.8 20
Styrene ND ug/L 10/31/22 18:15 100-42-510.0 5.8 20
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 18:15 630-20-610.0 6.2 20
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 18:15 79-34-510.0 4.5 20
Tetrachloroethene ND ug/L 10/31/22 18:15 127-18-410.0 5.8 20
Toluene 53.0 ug/L 10/31/22 18:15 108-88-310.0 4.8 20
1,2,3-Trichlorobenzene ND ug/L 10/31/22 18:15 87-61-640.0 16.1 20
1,2,4-Trichlorobenzene ND ug/L 10/31/22 18:15 120-82-140.0 12.8 20
1,1,1-Trichloroethane ND ug/L 10/31/22 18:15 71-55-610.0 6.6 20
1,1,2-Trichloroethane ND ug/L 10/31/22 18:15 79-00-510.0 6.5 20
Trichloroethene ND ug/L 10/31/22 18:15 79-01-610.0 7.7 20
Trichlorofluoromethane ND ug/L 10/31/22 18:15 75-69-420.0 6.0 20
1,2,3-Trichloropropane ND ug/L 10/31/22 18:15 96-18-410.0 5.2 20
1,2,4-Trimethylbenzene 2070 ug/L 10/31/22 18:15 95-63-610.0 9.9 20
1,3,5-Trimethylbenzene 468 ug/L 10/31/22 18:15 108-67-810.0 6.6 20
Vinyl chloride ND ug/L 10/31/22 18:15 75-01-420.0 7.7 20
m&p-Xylene 3080 ug/L 10/31/22 18:15 179601-23-120.0 14.2 20
o-Xylene 347 ug/L 10/31/22 18:15 95-47-610.0 6.8 20
Surrogates
1,2-Dichloroethane-d4 (S)95 %10/31/22 18:15 17060-07-070-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-6A Lab ID:92633456002 Collected:10/27/22 12:25 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)96 %10/31/22 18:15 460-00-470-130 20
Toluene-d8 (S)102 %10/31/22 18:15 2037-26-570-130 20
Sample:SW-14 Lab ID:92633456003 Collected:10/27/22 12:52 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 15:15 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 15:15 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 15:15 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 15:15 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 15:15 75-25-20.50 0.34 1
Bromomethane ND ug/L 10/31/22 15:15 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 15:15 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 15:15 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 15:15 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 15:15 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 15:15 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 15:15 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 15:15 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 15:15 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 15:15 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 15:15 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 15:15 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 15:15 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 15:15 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 15:15 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 15:15 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 15:15 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 10/31/22 15:15 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 15:15 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 15:15 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 15:15 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 15:15 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 15:15 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 15:15 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 15:15 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 15:15 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 15:15 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 15:15 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-14 Lab ID:92633456003 Collected:10/27/22 12:52 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 10/31/22 15:15 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 15:15 10061-02-60.50 0.36 1
Diisopropyl ether 0.31J ug/L 10/31/22 15:15 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 15:15 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 15:15 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 15:15 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 15:15 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.57 ug/L 10/31/22 15:15 1634-04-40.50 0.42 1
Naphthalene 2.6 ug/L 10/31/22 15:15 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 15:15 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 15:15 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 15:15 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 15:15 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 15:15 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 15:15 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 15:15 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 15:15 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/31/22 15:15 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 15:15 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 15:15 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 15:15 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 15:15 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 18.5 ug/L 10/31/22 15:15 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 24.3 ug/L 10/31/22 15:15 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 15:15 75-01-41.0 0.39 1
m&p-Xylene 5.5 ug/L 10/31/22 15:15 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 15:15 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %10/31/22 15:15 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %10/31/22 15:15 460-00-470-130 1
Toluene-d8 (S)101 %10/31/22 15:15 2037-26-570-130 1
Sample:SW-11 Lab ID:92633456004 Collected:10/27/22 12:56 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 15:33 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 15:33 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 15:33 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 15:33 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 15:33 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-11 Lab ID:92633456004 Collected:10/27/22 12:56 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 10/31/22 15:33 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 15:33 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 15:33 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 15:33 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 15:33 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 15:33 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 15:33 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 15:33 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 15:33 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 15:33 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 15:33 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 15:33 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 15:33 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 15:33 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 15:33 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 15:33 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 15:33 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 10/31/22 15:33 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 15:33 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 15:33 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 15:33 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 15:33 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 15:33 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 15:33 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 15:33 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 15:33 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 15:33 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 15:33 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/31/22 15:33 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 15:33 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 10/31/22 15:33 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 15:33 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 15:33 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 15:33 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 15:33 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 10/31/22 15:33 1634-04-40.50 0.42 1
Naphthalene 7.7 ug/L 10/31/22 15:33 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 15:33 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 15:33 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 15:33 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 15:33 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 15:33 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 15:33 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 15:33 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 15:33 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-11 Lab ID:92633456004 Collected:10/27/22 12:56 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 10/31/22 15:33 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 15:33 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 15:33 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 15:33 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 15:33 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 69.5 ug/L 10/31/22 15:33 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 97.0 ug/L 10/31/22 15:33 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 15:33 75-01-41.0 0.39 1
m&p-Xylene 19.6 ug/L 10/31/22 15:33 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 15:33 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %10/31/22 15:33 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %10/31/22 15:33 460-00-470-130 1
Toluene-d8 (S)98 %10/31/22 15:33 2037-26-570-130 1
Sample:SW-13 Lab ID:92633456005 Collected:10/27/22 13:17 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 18:33 71-43-26.2 4.3 12.5
Bromobenzene ND ug/L 10/31/22 18:33 108-86-16.2 3.6 12.5
Bromochloromethane ND ug/L 10/31/22 18:33 74-97-56.2 5.8 12.5
Bromodichloromethane ND ug/L 10/31/22 18:33 75-27-46.2 3.8 12.5
Bromoform ND ug/L 10/31/22 18:33 75-25-26.2 4.3 12.5
Bromomethane ND ug/L 10/31/22 18:33 74-83-962.5 20.8 12.5
n-Butylbenzene ND ug/L 10/31/22 18:33 104-51-86.2 6.1 12.5
sec-Butylbenzene ND ug/L 10/31/22 18:33 135-98-86.2 5.0 12.5
tert-Butylbenzene ND ug/L 10/31/22 18:33 98-06-66.2 4.0 12.5
Carbon tetrachloride ND ug/L 10/31/22 18:33 56-23-56.2 4.2 12.5
Chlorobenzene ND ug/L 10/31/22 18:33 108-90-76.2 3.6 12.5
Chloroethane ND ug/L 10/31/22 18:33 75-00-312.5 8.1 12.5
Chloroform ND ug/L 10/31/22 18:33 67-66-36.2 5.4 12.5
Chloromethane ND ug/L 10/31/22 18:33 74-87-312.5 6.8 12.5
2-Chlorotoluene ND ug/L 10/31/22 18:33 95-49-86.2 4.0 12.5
4-Chlorotoluene ND ug/L 10/31/22 18:33 106-43-46.2 4.0 12.5
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 18:33 96-12-812.5 4.2 12.5
Dibromochloromethane ND ug/L 10/31/22 18:33 124-48-16.2 4.5 12.5
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 18:33 106-93-46.2 3.4 12.5
Dibromomethane ND ug/L 10/31/22 18:33 74-95-36.2 4.9 12.5
1,2-Dichlorobenzene ND ug/L 10/31/22 18:33 95-50-16.2 4.2 12.5
1,3-Dichlorobenzene ND ug/L 10/31/22 18:33 541-73-16.2 4.2 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-13 Lab ID:92633456005 Collected:10/27/22 13:17 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 10/31/22 18:33 106-46-76.2 4.2 12.5
Dichlorodifluoromethane ND ug/L 10/31/22 18:33 75-71-86.2 4.3 12.5
1,1-Dichloroethane ND ug/L 10/31/22 18:33 75-34-36.2 4.6 12.5
1,2-Dichloroethane ND ug/L 10/31/22 18:33 107-06-26.2 4.0 12.5
1,1-Dichloroethene ND ug/L 10/31/22 18:33 75-35-46.2 4.4 12.5
cis-1,2-Dichloroethene ND ug/L 10/31/22 18:33 156-59-26.2 4.8 12.5
trans-1,2-Dichloroethene ND ug/L 10/31/22 18:33 156-60-56.2 5.0 12.5
1,2-Dichloropropane ND ug/L 10/31/22 18:33 78-87-56.2 4.4 12.5
1,3-Dichloropropane ND ug/L 10/31/22 18:33 142-28-96.2 3.6 12.5
2,2-Dichloropropane ND ug/L 10/31/22 18:33 594-20-76.2 4.8 12.5
1,1-Dichloropropene ND ug/L 10/31/22 18:33 563-58-66.2 5.3 12.5
cis-1,3-Dichloropropene ND ug/L 10/31/22 18:33 10061-01-56.2 4.6 12.5
trans-1,3-Dichloropropene ND ug/L 10/31/22 18:33 10061-02-66.2 4.5 12.5
Diisopropyl ether ND ug/L 10/31/22 18:33 108-20-36.2 3.8 12.5
Ethylbenzene 65.6 ug/L 10/31/22 18:33 100-41-46.2 3.8 12.5
Hexachloro-1,3-butadiene ND ug/L 10/31/22 18:33 87-68-325.0 19.1 12.5
Isopropylbenzene (Cumene)26.9 ug/L 10/31/22 18:33 98-82-86.2 4.2 12.5
Methylene Chloride ND ug/L 10/31/22 18:33 75-09-225.0 24.4 12.5
Methyl-tert-butyl ether ND ug/L 10/31/22 18:33 1634-04-46.2 5.3 12.5
Naphthalene 126 ug/L 10/31/22 18:33 91-20-325.0 8.1 12.5
n-Propylbenzene 20.9 ug/L 10/31/22 18:33 103-65-16.2 4.2 12.5
Styrene ND ug/L 10/31/22 18:33 100-42-56.2 3.6 12.5
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 18:33 630-20-66.2 3.9 12.5
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 18:33 79-34-56.2 2.8 12.5
Tetrachloroethene ND ug/L 10/31/22 18:33 127-18-46.2 3.6 12.5
Toluene ND ug/L 10/31/22 18:33 108-88-36.2 3.0 12.5
1,2,3-Trichlorobenzene ND ug/L 10/31/22 18:33 87-61-625.0 10.1 12.5
1,2,4-Trichlorobenzene ND ug/L 10/31/22 18:33 120-82-125.0 8.0 12.5
1,1,1-Trichloroethane ND ug/L 10/31/22 18:33 71-55-66.2 4.2 12.5
1,1,2-Trichloroethane ND ug/L 10/31/22 18:33 79-00-56.2 4.1 12.5
Trichloroethene ND ug/L 10/31/22 18:33 79-01-66.2 4.8 12.5
Trichlorofluoromethane ND ug/L 10/31/22 18:33 75-69-412.5 3.7 12.5
1,2,3-Trichloropropane ND ug/L 10/31/22 18:33 96-18-46.2 3.3 12.5
1,2,4-Trimethylbenzene 2140 ug/L 10/31/22 18:33 95-63-66.2 6.2 12.5
1,3,5-Trimethylbenzene 573 ug/L 10/31/22 18:33 108-67-86.2 4.2 12.5
Vinyl chloride ND ug/L 10/31/22 18:33 75-01-412.5 4.8 12.5
m&p-Xylene 736 ug/L 10/31/22 18:33 179601-23-112.5 8.9 12.5
o-Xylene ND ug/L 10/31/22 18:33 95-47-66.2 4.2 12.5
Surrogates
1,2-Dichloroethane-d4 (S)96 %10/31/22 18:33 17060-07-070-130 12.5
4-Bromofluorobenzene (S)97 %10/31/22 18:33 460-00-470-130 12.5
Toluene-d8 (S)102 %10/31/22 18:33 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-12 Lab ID:92633456006 Collected:10/27/22 13:22 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 17:03 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 17:03 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 17:03 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 17:03 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 17:03 75-25-20.50 0.34 1
Bromomethane ND ug/L 10/31/22 17:03 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 17:03 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 17:03 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 17:03 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 17:03 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 17:03 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 17:03 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 17:03 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 17:03 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 17:03 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 17:03 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 17:03 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 17:03 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 17:03 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 17:03 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 17:03 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 17:03 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 10/31/22 17:03 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 17:03 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 17:03 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 17:03 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 17:03 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 17:03 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 17:03 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 17:03 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 17:03 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 17:03 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 17:03 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/31/22 17:03 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 17:03 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 10/31/22 17:03 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 17:03 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 17:03 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 17:03 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 17:03 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 10/31/22 17:03 1634-04-40.50 0.42 1
Naphthalene ND ug/L 10/31/22 17:03 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 17:03 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 17:03 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 17:03 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-12 Lab ID:92633456006 Collected:10/27/22 13:22 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 17:03 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 17:03 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 17:03 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 17:03 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 17:03 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/31/22 17:03 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 17:03 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 17:03 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 17:03 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 17:03 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 10/31/22 17:03 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 24.2 ug/L 10/31/22 17:03 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 17:03 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/31/22 17:03 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 17:03 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %10/31/22 17:03 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %10/31/22 17:03 460-00-470-130 1
Toluene-d8 (S)99 %10/31/22 17:03 2037-26-570-130 1
Sample:MW-8 Lab ID:92633456007 Collected:10/27/22 13:37 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.8J ug/L 11/01/22 16:35 71-43-22.5 1.7 5
Bromobenzene ND ug/L 11/01/22 16:35 108-86-12.5 1.4 5
Bromochloromethane ND ug/L 11/01/22 16:35 74-97-52.5 2.3 5
Bromodichloromethane ND ug/L 11/01/22 16:35 75-27-42.5 1.5 5
Bromoform ND ug/L 11/01/22 16:35 75-25-22.5 1.7 5
Bromomethane ND ug/L 11/01/22 16:35 74-83-925.0 8.3 5
n-Butylbenzene ND ug/L 11/01/22 16:35 104-51-82.5 2.4 5
sec-Butylbenzene ND ug/L 11/01/22 16:35 135-98-82.5 2.0 5
tert-Butylbenzene ND ug/L 11/01/22 16:35 98-06-62.5 1.6 5
Carbon tetrachloride ND ug/L 11/01/22 16:35 56-23-52.5 1.7 5
Chlorobenzene ND ug/L 11/01/22 16:35 108-90-72.5 1.4 5
Chloroethane ND ug/L 11/01/22 16:35 75-00-35.0 3.2 5
Chloroform ND ug/L 11/01/22 16:35 67-66-32.5 2.2 5
Chloromethane ND ug/L 11/01/22 16:35 74-87-35.0 2.7 5
2-Chlorotoluene ND ug/L 11/01/22 16:35 95-49-82.5 1.6 5
4-Chlorotoluene ND ug/L 11/01/22 16:35 106-43-42.5 1.6 5
1,2-Dibromo-3-chloropropane ND ug/L 11/01/22 16:35 96-12-85.0 1.7 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-8 Lab ID:92633456007 Collected:10/27/22 13:37 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 11/01/22 16:35 124-48-12.5 1.8 5
1,2-Dibromoethane (EDB)ND ug/L 11/01/22 16:35 106-93-42.5 1.4 5
Dibromomethane ND ug/L 11/01/22 16:35 74-95-32.5 2.0 5
1,2-Dichlorobenzene ND ug/L 11/01/22 16:35 95-50-12.5 1.7 5
1,3-Dichlorobenzene ND ug/L 11/01/22 16:35 541-73-12.5 1.7 5
1,4-Dichlorobenzene ND ug/L 11/01/22 16:35 106-46-72.5 1.7 5
Dichlorodifluoromethane ND ug/L 11/01/22 16:35 75-71-82.5 1.7 5
1,1-Dichloroethane ND ug/L 11/01/22 16:35 75-34-32.5 1.8 5
1,2-Dichloroethane ND ug/L 11/01/22 16:35 107-06-22.5 1.6 5
1,1-Dichloroethene ND ug/L 11/01/22 16:35 75-35-42.5 1.7 5
cis-1,2-Dichloroethene ND ug/L 11/01/22 16:35 156-59-22.5 1.9 5
trans-1,2-Dichloroethene ND ug/L 11/01/22 16:35 156-60-52.5 2.0 5
1,2-Dichloropropane ND ug/L 11/01/22 16:35 78-87-52.5 1.8 5
1,3-Dichloropropane ND ug/L 11/01/22 16:35 142-28-92.5 1.4 5
2,2-Dichloropropane ND ug/L 11/01/22 16:35 594-20-72.5 1.9 5
1,1-Dichloropropene ND ug/L 11/01/22 16:35 563-58-62.5 2.1 5
cis-1,3-Dichloropropene ND ug/L 11/01/22 16:35 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 11/01/22 16:35 10061-02-62.5 1.8 5
Diisopropyl ether ND ug/L 11/01/22 16:35 108-20-32.5 1.5 5
Ethylbenzene 117 ug/L 11/01/22 16:35 100-41-42.5 1.5 5
Hexachloro-1,3-butadiene ND ug/L 11/01/22 16:35 87-68-310.0 7.6 5
Isopropylbenzene (Cumene)53.7 ug/L 11/01/22 16:35 98-82-82.5 1.7 5
Methylene Chloride ND ug/L 11/01/22 16:35 75-09-210.0 9.8 5
Methyl-tert-butyl ether ND ug/L 11/01/22 16:35 1634-04-42.5 2.1 5
Naphthalene 37.2 ug/L 11/01/22 16:35 91-20-310.0 3.2 5
n-Propylbenzene 158 ug/L 11/01/22 16:35 103-65-12.5 1.7 5
Styrene ND ug/L 11/01/22 16:35 100-42-52.5 1.5 5
1,1,1,2-Tetrachloroethane ND ug/L 11/01/22 16:35 630-20-62.5 1.6 5
1,1,2,2-Tetrachloroethane ND ug/L 11/01/22 16:35 79-34-52.5 1.1 5
Tetrachloroethene ND ug/L 11/01/22 16:35 127-18-42.5 1.5 5
Toluene 8.1 ug/L 11/01/22 16:35 108-88-32.5 1.2 5
1,2,3-Trichlorobenzene ND ug/L 11/01/22 16:35 87-61-610.0 4.0 5
1,2,4-Trichlorobenzene ND ug/L 11/01/22 16:35 120-82-110.0 3.2 5
1,1,1-Trichloroethane ND ug/L 11/01/22 16:35 71-55-62.5 1.7 5
1,1,2-Trichloroethane ND ug/L 11/01/22 16:35 79-00-52.5 1.6 5
Trichloroethene ND ug/L 11/01/22 16:35 79-01-62.5 1.9 5
Trichlorofluoromethane ND ug/L 11/01/22 16:35 75-69-45.0 1.5 5
1,2,3-Trichloropropane ND ug/L 11/01/22 16:35 96-18-42.5 1.3 5
1,2,4-Trimethylbenzene 930 ug/L 11/01/22 16:35 95-63-62.5 2.5 5
1,3,5-Trimethylbenzene 258 ug/L 11/01/22 16:35 108-67-82.5 1.7 5
Vinyl chloride ND ug/L 11/01/22 16:35 75-01-45.0 1.9 5
m&p-Xylene 338 ug/L 11/01/22 16:35 179601-23-15.0 3.5 5
o-Xylene 82.8 ug/L 11/01/22 16:35 95-47-62.5 1.7 5
Surrogates
1,2-Dichloroethane-d4 (S)90 %11/01/22 16:35 17060-07-070-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-8 Lab ID:92633456007 Collected:10/27/22 13:37 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)98 %11/01/22 16:35 460-00-470-130 5
Toluene-d8 (S)104 %11/01/22 16:35 2037-26-570-130 5
Sample:MW-13 Lab ID:92633456008 Collected:10/27/22 15:15 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 19:09 71-43-25.0 3.4 10
Bromobenzene ND ug/L 10/31/22 19:09 108-86-15.0 2.9 10
Bromochloromethane ND ug/L 10/31/22 19:09 74-97-55.0 4.7 10
Bromodichloromethane ND ug/L 10/31/22 19:09 75-27-45.0 3.1 10
Bromoform ND ug/L 10/31/22 19:09 75-25-25.0 3.4 10
Bromomethane ND ug/L 10/31/22 19:09 74-83-950.0 16.6 10
n-Butylbenzene ND ug/L 10/31/22 19:09 104-51-85.0 4.9 10
sec-Butylbenzene ND ug/L 10/31/22 19:09 135-98-85.0 4.0 10
tert-Butylbenzene ND ug/L 10/31/22 19:09 98-06-65.0 3.2 10
Carbon tetrachloride ND ug/L 10/31/22 19:09 56-23-55.0 3.3 10
Chlorobenzene ND ug/L 10/31/22 19:09 108-90-75.0 2.8 10
Chloroethane ND ug/L 10/31/22 19:09 75-00-310.0 6.5 10
Chloroform ND ug/L 10/31/22 19:09 67-66-35.0 4.3 10
Chloromethane ND ug/L 10/31/22 19:09 74-87-310.0 5.4 10
2-Chlorotoluene ND ug/L 10/31/22 19:09 95-49-85.0 3.2 10
4-Chlorotoluene ND ug/L 10/31/22 19:09 106-43-45.0 3.2 10
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 19:09 96-12-810.0 3.4 10
Dibromochloromethane ND ug/L 10/31/22 19:09 124-48-15.0 3.6 10
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 19:09 106-93-45.0 2.7 10
Dibromomethane ND ug/L 10/31/22 19:09 74-95-35.0 3.9 10
1,2-Dichlorobenzene ND ug/L 10/31/22 19:09 95-50-15.0 3.4 10
1,3-Dichlorobenzene ND ug/L 10/31/22 19:09 541-73-15.0 3.4 10
1,4-Dichlorobenzene ND ug/L 10/31/22 19:09 106-46-75.0 3.3 10
Dichlorodifluoromethane ND ug/L 10/31/22 19:09 75-71-85.0 3.5 10
1,1-Dichloroethane ND ug/L 10/31/22 19:09 75-34-35.0 3.7 10
1,2-Dichloroethane ND ug/L 10/31/22 19:09 107-06-25.0 3.2 10
1,1-Dichloroethene ND ug/L 10/31/22 19:09 75-35-45.0 3.5 10
cis-1,2-Dichloroethene ND ug/L 10/31/22 19:09 156-59-25.0 3.8 10
trans-1,2-Dichloroethene ND ug/L 10/31/22 19:09 156-60-55.0 4.0 10
1,2-Dichloropropane ND ug/L 10/31/22 19:09 78-87-55.0 3.6 10
1,3-Dichloropropane ND ug/L 10/31/22 19:09 142-28-95.0 2.8 10
2,2-Dichloropropane ND ug/L 10/31/22 19:09 594-20-75.0 3.9 10
1,1-Dichloropropene ND ug/L 10/31/22 19:09 563-58-65.0 4.3 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-13 Lab ID:92633456008 Collected:10/27/22 15:15 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 10/31/22 19:09 10061-01-55.0 3.6 10
trans-1,3-Dichloropropene ND ug/L 10/31/22 19:09 10061-02-65.0 3.6 10
Diisopropyl ether ND ug/L 10/31/22 19:09 108-20-35.0 3.1 10
Ethylbenzene 287 ug/L 10/31/22 19:09 100-41-45.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 10/31/22 19:09 87-68-320.0 15.3 10
Isopropylbenzene (Cumene)72.3 ug/L 10/31/22 19:09 98-82-85.0 3.3 10
Methylene Chloride ND ug/L 10/31/22 19:09 75-09-220.0 19.5 10
Methyl-tert-butyl ether ND ug/L 10/31/22 19:09 1634-04-45.0 4.2 10
Naphthalene 63.1 ug/L 10/31/22 19:09 91-20-320.0 6.4 10
n-Propylbenzene 210 ug/L 10/31/22 19:09 103-65-15.0 3.4 10
Styrene ND ug/L 10/31/22 19:09 100-42-55.0 2.9 10
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 19:09 630-20-65.0 3.1 10
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 19:09 79-34-55.0 2.2 10
Tetrachloroethene ND ug/L 10/31/22 19:09 127-18-45.0 2.9 10
Toluene 20.6 ug/L 10/31/22 19:09 108-88-35.0 2.4 10
1,2,3-Trichlorobenzene ND ug/L 10/31/22 19:09 87-61-620.0 8.1 10
1,2,4-Trichlorobenzene ND ug/L 10/31/22 19:09 120-82-120.0 6.4 10
1,1,1-Trichloroethane ND ug/L 10/31/22 19:09 71-55-65.0 3.3 10
1,1,2-Trichloroethane ND ug/L 10/31/22 19:09 79-00-55.0 3.2 10
Trichloroethene ND ug/L 10/31/22 19:09 79-01-65.0 3.8 10
Trichlorofluoromethane ND ug/L 10/31/22 19:09 75-69-410.0 3.0 10
1,2,3-Trichloropropane ND ug/L 10/31/22 19:09 96-18-45.0 2.6 10
1,2,4-Trimethylbenzene 1380 ug/L 10/31/22 19:09 95-63-65.0 5.0 10
1,3,5-Trimethylbenzene 375 ug/L 10/31/22 19:09 108-67-85.0 3.3 10
Vinyl chloride ND ug/L 10/31/22 19:09 75-01-410.0 3.9 10
m&p-Xylene 794 ug/L 10/31/22 19:09 179601-23-110.0 7.1 10
o-Xylene 199 ug/L 10/31/22 19:09 95-47-65.0 3.4 10
Surrogates
1,2-Dichloroethane-d4 (S)97 %10/31/22 19:09 17060-07-070-130 10
4-Bromofluorobenzene (S)98 %10/31/22 19:09 460-00-470-130 10
Toluene-d8 (S)101 %10/31/22 19:09 2037-26-570-130 10
Sample:SW-01-185 Lab ID:92633456009 Collected:10/27/22 15:10 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 15:51 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 15:51 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 15:51 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 15:51 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 15:51 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-01-185 Lab ID:92633456009 Collected:10/27/22 15:10 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 10/31/22 15:51 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 15:51 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 15:51 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 15:51 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 15:51 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 15:51 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 15:51 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 15:51 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 15:51 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 15:51 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 15:51 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 15:51 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 15:51 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 15:51 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 15:51 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 15:51 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 15:51 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 10/31/22 15:51 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 15:51 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 15:51 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 15:51 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 15:51 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 15:51 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 15:51 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 15:51 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 15:51 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 15:51 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 15:51 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/31/22 15:51 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 15:51 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 10/31/22 15:51 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 15:51 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 15:51 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 15:51 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 15:51 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 10/31/22 15:51 1634-04-40.50 0.42 1
Naphthalene ND ug/L 10/31/22 15:51 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 15:51 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 15:51 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 15:51 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 15:51 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 15:51 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 15:51 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 15:51 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 15:51 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-01-185 Lab ID:92633456009 Collected:10/27/22 15:10 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 10/31/22 15:51 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 15:51 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 15:51 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 15:51 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 15:51 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 10/31/22 15:51 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 10/31/22 15:51 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 15:51 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/31/22 15:51 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 15:51 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %10/31/22 15:51 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %10/31/22 15:51 460-00-470-130 1
Toluene-d8 (S)100 %10/31/22 15:51 2037-26-570-130 1
Sample:SW-02-185 Lab ID:92633456010 Collected:10/27/22 15:25 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 16:09 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 16:09 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 16:09 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 16:09 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 16:09 75-25-20.50 0.34 1
Bromomethane ND ug/L 10/31/22 16:09 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 16:09 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 16:09 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 16:09 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 16:09 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 16:09 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 16:09 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 16:09 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 16:09 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 16:09 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 16:09 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 16:09 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 16:09 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 16:09 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 16:09 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 16:09 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 16:09 541-73-10.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-02-185 Lab ID:92633456010 Collected:10/27/22 15:25 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 10/31/22 16:09 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 16:09 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 16:09 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 16:09 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 16:09 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 16:09 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 16:09 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 16:09 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 16:09 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 16:09 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 16:09 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/31/22 16:09 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 16:09 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 10/31/22 16:09 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 16:09 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 16:09 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 16:09 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 16:09 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 10/31/22 16:09 1634-04-40.50 0.42 1
Naphthalene ND ug/L 10/31/22 16:09 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 16:09 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 16:09 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 16:09 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 16:09 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 16:09 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 16:09 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 16:09 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 16:09 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/31/22 16:09 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 16:09 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 16:09 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 16:09 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 16:09 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 10/31/22 16:09 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 10/31/22 16:09 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 16:09 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/31/22 16:09 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 16:09 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %10/31/22 16:09 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %10/31/22 16:09 460-00-470-130 1
Toluene-d8 (S)99 %10/31/22 16:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-03-185 Lab ID:92633456011 Collected:10/27/22 15:40 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 16:27 71-43-20.50 0.34 1
Bromobenzene ND ug/L 10/31/22 16:27 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 10/31/22 16:27 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 10/31/22 16:27 75-27-40.50 0.31 1
Bromoform ND ug/L 10/31/22 16:27 75-25-20.50 0.34 1
Bromomethane ND ug/L 10/31/22 16:27 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 10/31/22 16:27 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 10/31/22 16:27 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 10/31/22 16:27 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 10/31/22 16:27 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 10/31/22 16:27 108-90-70.50 0.28 1
Chloroethane ND ug/L 10/31/22 16:27 75-00-31.0 0.65 1
Chloroform ND ug/L 10/31/22 16:27 67-66-30.50 0.43 1
Chloromethane ND ug/L 10/31/22 16:27 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 10/31/22 16:27 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 10/31/22 16:27 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 16:27 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 10/31/22 16:27 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 16:27 106-93-40.50 0.27 1
Dibromomethane ND ug/L 10/31/22 16:27 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 10/31/22 16:27 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 10/31/22 16:27 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 10/31/22 16:27 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 10/31/22 16:27 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 10/31/22 16:27 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 10/31/22 16:27 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 10/31/22 16:27 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 10/31/22 16:27 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 10/31/22 16:27 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 10/31/22 16:27 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 10/31/22 16:27 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 10/31/22 16:27 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 10/31/22 16:27 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 10/31/22 16:27 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 10/31/22 16:27 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 10/31/22 16:27 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 10/31/22 16:27 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 10/31/22 16:27 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 10/31/22 16:27 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 10/31/22 16:27 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 10/31/22 16:27 1634-04-40.50 0.42 1
Naphthalene ND ug/L 10/31/22 16:27 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 10/31/22 16:27 103-65-10.50 0.34 1
Styrene ND ug/L 10/31/22 16:27 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 16:27 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:SW-03-185 Lab ID:92633456011 Collected:10/27/22 15:40 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 16:27 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 10/31/22 16:27 127-18-40.50 0.29 1
Toluene ND ug/L 10/31/22 16:27 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/31/22 16:27 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 10/31/22 16:27 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 10/31/22 16:27 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 10/31/22 16:27 79-00-50.50 0.32 1
Trichloroethene ND ug/L 10/31/22 16:27 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 10/31/22 16:27 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 10/31/22 16:27 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 10/31/22 16:27 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 10/31/22 16:27 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 10/31/22 16:27 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 10/31/22 16:27 179601-23-11.0 0.71 1
o-Xylene ND ug/L 10/31/22 16:27 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %10/31/22 16:27 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %10/31/22 16:27 460-00-470-130 1
Toluene-d8 (S)103 %10/31/22 16:27 2037-26-570-130 1
Sample:MW-14 Lab ID:92633456012 Collected:10/27/22 16:45 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3.6J ug/L 10/31/22 19:27 71-43-25.0 3.4 10
Bromobenzene ND ug/L 10/31/22 19:27 108-86-15.0 2.9 10
Bromochloromethane ND ug/L 10/31/22 19:27 74-97-55.0 4.7 10
Bromodichloromethane ND ug/L 10/31/22 19:27 75-27-45.0 3.1 10
Bromoform ND ug/L 10/31/22 19:27 75-25-25.0 3.4 10
Bromomethane ND ug/L 10/31/22 19:27 74-83-950.0 16.6 10
n-Butylbenzene ND ug/L 10/31/22 19:27 104-51-85.0 4.9 10
sec-Butylbenzene ND ug/L 10/31/22 19:27 135-98-85.0 4.0 10
tert-Butylbenzene ND ug/L 10/31/22 19:27 98-06-65.0 3.2 10
Carbon tetrachloride ND ug/L 10/31/22 19:27 56-23-55.0 3.3 10
Chlorobenzene ND ug/L 10/31/22 19:27 108-90-75.0 2.8 10
Chloroethane ND ug/L 10/31/22 19:27 75-00-310.0 6.5 10
Chloroform ND ug/L 10/31/22 19:27 67-66-35.0 4.3 10
Chloromethane ND ug/L 10/31/22 19:27 74-87-310.0 5.4 10
2-Chlorotoluene ND ug/L 10/31/22 19:27 95-49-85.0 3.2 10
4-Chlorotoluene ND ug/L 10/31/22 19:27 106-43-45.0 3.2 10
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 19:27 96-12-810.0 3.4 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-14 Lab ID:92633456012 Collected:10/27/22 16:45 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 10/31/22 19:27 124-48-15.0 3.6 10
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 19:27 106-93-45.0 2.7 10
Dibromomethane ND ug/L 10/31/22 19:27 74-95-35.0 3.9 10
1,2-Dichlorobenzene ND ug/L 10/31/22 19:27 95-50-15.0 3.4 10
1,3-Dichlorobenzene ND ug/L 10/31/22 19:27 541-73-15.0 3.4 10
1,4-Dichlorobenzene ND ug/L 10/31/22 19:27 106-46-75.0 3.3 10
Dichlorodifluoromethane ND ug/L 10/31/22 19:27 75-71-85.0 3.5 10
1,1-Dichloroethane ND ug/L 10/31/22 19:27 75-34-35.0 3.7 10
1,2-Dichloroethane ND ug/L 10/31/22 19:27 107-06-25.0 3.2 10
1,1-Dichloroethene ND ug/L 10/31/22 19:27 75-35-45.0 3.5 10
cis-1,2-Dichloroethene ND ug/L 10/31/22 19:27 156-59-25.0 3.8 10
trans-1,2-Dichloroethene ND ug/L 10/31/22 19:27 156-60-55.0 4.0 10
1,2-Dichloropropane ND ug/L 10/31/22 19:27 78-87-55.0 3.6 10
1,3-Dichloropropane ND ug/L 10/31/22 19:27 142-28-95.0 2.8 10
2,2-Dichloropropane ND ug/L 10/31/22 19:27 594-20-75.0 3.9 10
1,1-Dichloropropene ND ug/L 10/31/22 19:27 563-58-65.0 4.3 10
cis-1,3-Dichloropropene ND ug/L 10/31/22 19:27 10061-01-55.0 3.6 10
trans-1,3-Dichloropropene ND ug/L 10/31/22 19:27 10061-02-65.0 3.6 10
Diisopropyl ether ND ug/L 10/31/22 19:27 108-20-35.0 3.1 10
Ethylbenzene 348 ug/L 10/31/22 19:27 100-41-45.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 10/31/22 19:27 87-68-320.0 15.3 10
Isopropylbenzene (Cumene)75.3 ug/L 10/31/22 19:27 98-82-85.0 3.3 10
Methylene Chloride ND ug/L 10/31/22 19:27 75-09-220.0 19.5 10
Methyl-tert-butyl ether ND ug/L 10/31/22 19:27 1634-04-45.0 4.2 10
Naphthalene 82.7 ug/L 10/31/22 19:27 91-20-320.0 6.4 10
n-Propylbenzene 219 ug/L 10/31/22 19:27 103-65-15.0 3.4 10
Styrene ND ug/L 10/31/22 19:27 100-42-55.0 2.9 10
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 19:27 630-20-65.0 3.1 10
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 19:27 79-34-55.0 2.2 10
Tetrachloroethene ND ug/L 10/31/22 19:27 127-18-45.0 2.9 10
Toluene 7.7 ug/L 10/31/22 19:27 108-88-35.0 2.4 10
1,2,3-Trichlorobenzene ND ug/L 10/31/22 19:27 87-61-620.0 8.1 10
1,2,4-Trichlorobenzene ND ug/L 10/31/22 19:27 120-82-120.0 6.4 10
1,1,1-Trichloroethane ND ug/L 10/31/22 19:27 71-55-65.0 3.3 10
1,1,2-Trichloroethane ND ug/L 10/31/22 19:27 79-00-55.0 3.2 10
Trichloroethene ND ug/L 10/31/22 19:27 79-01-65.0 3.8 10
Trichlorofluoromethane ND ug/L 10/31/22 19:27 75-69-410.0 3.0 10
1,2,3-Trichloropropane ND ug/L 10/31/22 19:27 96-18-45.0 2.6 10
1,2,4-Trimethylbenzene 1560 ug/L 10/31/22 19:27 95-63-65.0 5.0 10
1,3,5-Trimethylbenzene 393 ug/L 10/31/22 19:27 108-67-85.0 3.3 10
Vinyl chloride ND ug/L 10/31/22 19:27 75-01-410.0 3.9 10
m&p-Xylene 873 ug/L 10/31/22 19:27 179601-23-110.0 7.1 10
o-Xylene 56.1 ug/L 10/31/22 19:27 95-47-65.0 3.4 10
Surrogates
1,2-Dichloroethane-d4 (S)91 %10/31/22 19:27 17060-07-070-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:MW-14 Lab ID:92633456012 Collected:10/27/22 16:45 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)97 %10/31/22 19:27 460-00-470-130 10
Toluene-d8 (S)102 %10/31/22 19:27 2037-26-570-130 10
Sample:DUPE Lab ID:92633456013 Collected:10/27/22 00:00 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/31/22 19:45 71-43-210.0 6.9 20
Bromobenzene ND ug/L 10/31/22 19:45 108-86-110.0 5.8 20
Bromochloromethane ND ug/L 10/31/22 19:45 74-97-510.0 9.4 20
Bromodichloromethane ND ug/L 10/31/22 19:45 75-27-410.0 6.1 20
Bromoform ND ug/L 10/31/22 19:45 75-25-210.0 6.8 20
Bromomethane ND ug/L 10/31/22 19:45 74-83-910033.2 20
n-Butylbenzene ND ug/L 10/31/22 19:45 104-51-810.0 9.8 20
sec-Butylbenzene ND ug/L 10/31/22 19:45 135-98-810.0 8.0 20
tert-Butylbenzene ND ug/L 10/31/22 19:45 98-06-610.0 6.5 20
Carbon tetrachloride ND ug/L 10/31/22 19:45 56-23-510.0 6.7 20
Chlorobenzene ND ug/L 10/31/22 19:45 108-90-710.0 5.7 20
Chloroethane ND ug/L 10/31/22 19:45 75-00-320.0 13.0 20
Chloroform ND ug/L 10/31/22 19:45 67-66-310.0 8.6 20
Chloromethane ND ug/L 10/31/22 19:45 74-87-320.0 10.8 20
2-Chlorotoluene ND ug/L 10/31/22 19:45 95-49-810.0 6.4 20
4-Chlorotoluene ND ug/L 10/31/22 19:45 106-43-410.0 6.5 20
1,2-Dibromo-3-chloropropane ND ug/L 10/31/22 19:45 96-12-820.0 6.8 20
Dibromochloromethane ND ug/L 10/31/22 19:45 124-48-110.0 7.2 20
1,2-Dibromoethane (EDB)ND ug/L 10/31/22 19:45 106-93-410.0 5.4 20
Dibromomethane ND ug/L 10/31/22 19:45 74-95-310.0 7.9 20
1,2-Dichlorobenzene ND ug/L 10/31/22 19:45 95-50-110.0 6.8 20
1,3-Dichlorobenzene ND ug/L 10/31/22 19:45 541-73-110.0 6.8 20
1,4-Dichlorobenzene ND ug/L 10/31/22 19:45 106-46-710.0 6.7 20
Dichlorodifluoromethane ND ug/L 10/31/22 19:45 75-71-810.0 6.9 20
1,1-Dichloroethane ND ug/L 10/31/22 19:45 75-34-310.0 7.3 20
1,2-Dichloroethane ND ug/L 10/31/22 19:45 107-06-210.0 6.4 20
1,1-Dichloroethene ND ug/L 10/31/22 19:45 75-35-410.0 7.0 20
cis-1,2-Dichloroethene ND ug/L 10/31/22 19:45 156-59-210.0 7.7 20
trans-1,2-Dichloroethene ND ug/L 10/31/22 19:45 156-60-510.0 7.9 20
1,2-Dichloropropane ND ug/L 10/31/22 19:45 78-87-510.0 7.1 20
1,3-Dichloropropane ND ug/L 10/31/22 19:45 142-28-910.0 5.7 20
2,2-Dichloropropane ND ug/L 10/31/22 19:45 594-20-710.0 7.8 20
1,1-Dichloropropene ND ug/L 10/31/22 19:45 563-58-610.0 8.5 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:DUPE Lab ID:92633456013 Collected:10/27/22 00:00 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 10/31/22 19:45 10061-01-510.0 7.3 20
trans-1,3-Dichloropropene ND ug/L 10/31/22 19:45 10061-02-610.0 7.3 20
Diisopropyl ether ND ug/L 10/31/22 19:45 108-20-310.0 6.2 20
Ethylbenzene 904 ug/L 10/31/22 19:45 100-41-410.0 6.1 20
Hexachloro-1,3-butadiene ND ug/L 10/31/22 19:45 87-68-340.0 30.6 20
Isopropylbenzene (Cumene)121 ug/L 10/31/22 19:45 98-82-810.0 6.7 20
Methylene Chloride ND ug/L 10/31/22 19:45 75-09-240.0 39.0 20
Methyl-tert-butyl ether ND ug/L 10/31/22 19:45 1634-04-410.0 8.4 20
Naphthalene 148 ug/L 10/31/22 19:45 91-20-340.0 12.9 20
n-Propylbenzene 316 ug/L 10/31/22 19:45 103-65-110.0 6.8 20
Styrene ND ug/L 10/31/22 19:45 100-42-510.0 5.8 20
1,1,1,2-Tetrachloroethane ND ug/L 10/31/22 19:45 630-20-610.0 6.2 20
1,1,2,2-Tetrachloroethane ND ug/L 10/31/22 19:45 79-34-510.0 4.5 20
Tetrachloroethene ND ug/L 10/31/22 19:45 127-18-410.0 5.8 20
Toluene 46.0 ug/L 10/31/22 19:45 108-88-310.0 4.8 20
1,2,3-Trichlorobenzene ND ug/L 10/31/22 19:45 87-61-640.0 16.1 20
1,2,4-Trichlorobenzene ND ug/L 10/31/22 19:45 120-82-140.0 12.8 20
1,1,1-Trichloroethane ND ug/L 10/31/22 19:45 71-55-610.0 6.6 20
1,1,2-Trichloroethane ND ug/L 10/31/22 19:45 79-00-510.0 6.5 20
Trichloroethene ND ug/L 10/31/22 19:45 79-01-610.0 7.7 20
Trichlorofluoromethane ND ug/L 10/31/22 19:45 75-69-420.0 6.0 20
1,2,3-Trichloropropane ND ug/L 10/31/22 19:45 96-18-410.0 5.2 20
1,2,4-Trimethylbenzene 2010 ug/L 10/31/22 19:45 95-63-610.0 9.9 20
1,3,5-Trimethylbenzene 450 ug/L 10/31/22 19:45 108-67-810.0 6.6 20
Vinyl chloride ND ug/L 10/31/22 19:45 75-01-420.0 7.7 20
m&p-Xylene 3060 ug/L 10/31/22 19:45 179601-23-120.0 14.2 20
o-Xylene 339 ug/L 10/31/22 19:45 95-47-610.0 6.8 20
Surrogates
1,2-Dichloroethane-d4 (S)94 %10/31/22 19:45 17060-07-070-130 20
4-Bromofluorobenzene (S)98 %10/31/22 19:45 460-00-470-130 20
Toluene-d8 (S)103 %10/31/22 19:45 2037-26-570-130 20
Sample:DUP 2 Lab ID:92633456014 Collected:10/27/22 00:00 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/22 15:05 71-43-20.50 0.34 1
Bromobenzene ND ug/L 11/01/22 15:05 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 11/01/22 15:05 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 11/01/22 15:05 75-27-40.50 0.31 1
Bromoform ND ug/L 11/01/22 15:05 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:DUP 2 Lab ID:92633456014 Collected:10/27/22 00:00 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 11/01/22 15:05 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 11/01/22 15:05 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 11/01/22 15:05 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 11/01/22 15:05 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 11/01/22 15:05 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 11/01/22 15:05 108-90-70.50 0.28 1
Chloroethane ND ug/L 11/01/22 15:05 75-00-31.0 0.65 1
Chloroform ND ug/L 11/01/22 15:05 67-66-30.50 0.43 1
Chloromethane ND ug/L 11/01/22 15:05 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 11/01/22 15:05 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 11/01/22 15:05 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/22 15:05 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 11/01/22 15:05 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/22 15:05 106-93-40.50 0.27 1
Dibromomethane ND ug/L 11/01/22 15:05 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 11/01/22 15:05 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 11/01/22 15:05 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 11/01/22 15:05 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 11/01/22 15:05 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 11/01/22 15:05 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 11/01/22 15:05 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 11/01/22 15:05 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 11/01/22 15:05 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 11/01/22 15:05 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 11/01/22 15:05 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 11/01/22 15:05 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 11/01/22 15:05 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 11/01/22 15:05 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 11/01/22 15:05 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 11/01/22 15:05 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 11/01/22 15:05 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 11/01/22 15:05 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 11/01/22 15:05 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 11/01/22 15:05 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 11/01/22 15:05 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.44J ug/L 11/01/22 15:05 1634-04-40.50 0.42 1
Naphthalene 1.4J ug/L 11/01/22 15:05 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 11/01/22 15:05 103-65-10.50 0.34 1
Styrene ND ug/L 11/01/22 15:05 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/22 15:05 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/22 15:05 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 11/01/22 15:05 127-18-40.50 0.29 1
Toluene ND ug/L 11/01/22 15:05 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/01/22 15:05 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 11/01/22 15:05 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Sample:DUP 2 Lab ID:92633456014 Collected:10/27/22 00:00 Received:10/28/22 09:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 11/01/22 15:05 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 11/01/22 15:05 79-00-50.50 0.32 1
Trichloroethene ND ug/L 11/01/22 15:05 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 11/01/22 15:05 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 11/01/22 15:05 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 11/01/22 15:05 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 7.0 ug/L 11/01/22 15:05 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 11/01/22 15:05 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 11/01/22 15:05 179601-23-11.0 0.71 1
o-Xylene ND ug/L 11/01/22 15:05 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/01/22 15:05 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %11/01/22 15:05 460-00-470-130 1
Toluene-d8 (S)104 %11/01/22 15:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
733838
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92633456002, 92633456003, 92633456004, 92633456005, 92633456006, 92633456008, 92633456009,
92633456010, 92633456011, 92633456012, 92633456013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3819632
Associated Lab Samples:92633456002, 92633456003, 92633456004, 92633456005, 92633456006, 92633456008, 92633456009,
92633456010, 92633456011, 92633456012, 92633456013
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/31/22 11:210.31
1,1,1-Trichloroethane ug/L ND 0.50 10/31/22 11:210.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/31/22 11:210.22
1,1,2-Trichloroethane ug/L ND 0.50 10/31/22 11:210.32
1,1-Dichloroethane ug/L ND 0.50 10/31/22 11:210.37
1,1-Dichloroethene ug/L ND 0.50 10/31/22 11:210.35
1,1-Dichloropropene ug/L ND 0.50 10/31/22 11:210.43
1,2,3-Trichlorobenzene ug/L ND 2.0 10/31/22 11:210.81
1,2,3-Trichloropropane ug/L ND 0.50 10/31/22 11:210.26
1,2,4-Trichlorobenzene ug/L ND 2.0 10/31/22 11:210.64
1,2,4-Trimethylbenzene ug/L ND 0.50 10/31/22 11:210.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/31/22 11:210.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/31/22 11:210.27
1,2-Dichlorobenzene ug/L ND 0.50 10/31/22 11:210.34
1,2-Dichloroethane ug/L ND 0.50 10/31/22 11:210.32
1,2-Dichloropropane ug/L ND 0.50 10/31/22 11:210.36
1,3,5-Trimethylbenzene ug/L ND 0.50 10/31/22 11:210.33
1,3-Dichlorobenzene ug/L ND 0.50 10/31/22 11:210.34
1,3-Dichloropropane ug/L ND 0.50 10/31/22 11:210.28
1,4-Dichlorobenzene ug/L ND 0.50 10/31/22 11:210.33
2,2-Dichloropropane ug/L ND 0.50 10/31/22 11:210.39
2-Chlorotoluene ug/L ND 0.50 10/31/22 11:210.32
4-Chlorotoluene ug/L ND 0.50 10/31/22 11:210.32
Benzene ug/L ND 0.50 10/31/22 11:210.34
Bromobenzene ug/L ND 0.50 10/31/22 11:210.29
Bromochloromethane ug/L ND 0.50 10/31/22 11:210.47
Bromodichloromethane ug/L ND 0.50 10/31/22 11:210.31
Bromoform ug/L ND 0.50 10/31/22 11:210.34
Bromomethane ug/L ND 5.0 10/31/22 11:211.7
Carbon tetrachloride ug/L ND 0.50 10/31/22 11:210.33
Chlorobenzene ug/L ND 0.50 10/31/22 11:210.28
Chloroethane ug/L ND 1.0 10/31/22 11:210.65
Chloroform ug/L ND 0.50 10/31/22 11:210.43
Chloromethane ug/L ND 1.0 10/31/22 11:210.54
cis-1,2-Dichloroethene ug/L ND 0.50 10/31/22 11:210.38
cis-1,3-Dichloropropene ug/L ND 0.50 10/31/22 11:210.36
Dibromochloromethane ug/L ND 0.50 10/31/22 11:210.36
Dibromomethane ug/L ND 0.50 10/31/22 11:210.39
Dichlorodifluoromethane ug/L ND 0.50 10/31/22 11:210.35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3819632
Associated Lab Samples:92633456002, 92633456003, 92633456004, 92633456005, 92633456006, 92633456008, 92633456009,
92633456010, 92633456011, 92633456012, 92633456013
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 10/31/22 11:210.31
Ethylbenzene ug/L ND 0.50 10/31/22 11:210.30
Hexachloro-1,3-butadiene ug/L ND 2.0 10/31/22 11:211.5
Isopropylbenzene (Cumene)ug/L ND 0.50 10/31/22 11:210.33
m&p-Xylene ug/L ND 1.0 10/31/22 11:210.71
Methyl-tert-butyl ether ug/L ND 0.50 10/31/22 11:210.42
Methylene Chloride ug/L ND 2.0 10/31/22 11:212.0
n-Butylbenzene ug/L ND 0.50 10/31/22 11:210.49
n-Propylbenzene ug/L ND 0.50 10/31/22 11:210.34
Naphthalene ug/L ND 2.0 10/31/22 11:210.64
o-Xylene ug/L ND 0.50 10/31/22 11:210.34
sec-Butylbenzene ug/L ND 0.50 10/31/22 11:210.40
Styrene ug/L ND 0.50 10/31/22 11:210.29
tert-Butylbenzene ug/L ND 0.50 10/31/22 11:210.32
Tetrachloroethene ug/L ND 0.50 10/31/22 11:210.29
Toluene ug/L ND 0.50 10/31/22 11:210.24
trans-1,2-Dichloroethene ug/L ND 0.50 10/31/22 11:210.40
trans-1,3-Dichloropropene ug/L ND 0.50 10/31/22 11:210.36
Trichloroethene ug/L ND 0.50 10/31/22 11:210.38
Trichlorofluoromethane ug/L ND 1.0 10/31/22 11:210.30
Vinyl chloride ug/L ND 1.0 10/31/22 11:210.39
1,2-Dichloroethane-d4 (S)%97 70-130 10/31/22 11:21
4-Bromofluorobenzene (S)%101 70-130 10/31/22 11:21
Toluene-d8 (S)%101 70-130 10/31/22 11:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3819633LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 49.950 100 60-140
1,1,2,2-Tetrachloroethane ug/L 50.950 102 60-140
1,1,2-Trichloroethane ug/L 50.850 102 60-140
1,1-Dichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethene ug/L 50.450 101 60-140
1,1-Dichloropropene ug/L 52.150 104 60-140
1,2,3-Trichlorobenzene ug/L 55.450 111 60-140
1,2,3-Trichloropropane ug/L 50.950 102 60-140
1,2,4-Trichlorobenzene ug/L 54.450 109 60-140
1,2,4-Trimethylbenzene ug/L 52.550 105 60-140
1,2-Dibromo-3-chloropropane ug/L 49.150 98 60-140
1,2-Dibromoethane (EDB)ug/L 53.650 107 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 47.650 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3819633LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 51.350 103 60-140
1,3,5-Trimethylbenzene ug/L 52.350 105 60-140
1,3-Dichlorobenzene ug/L 51.550 103 60-140
1,3-Dichloropropane ug/L 52.150 104 60-140
1,4-Dichlorobenzene ug/L 50.350 101 60-140
2,2-Dichloropropane ug/L 50.350 101 60-140
2-Chlorotoluene ug/L 49.950 100 60-140
4-Chlorotoluene ug/L 49.950 100 60-140
Benzene ug/L 48.950 98 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 50.350 101 60-140
Bromodichloromethane ug/L 47.450 95 60-140
Bromoform ug/L 52.050 104 60-140
Bromomethane ug/L 42.350 85 60-140
Carbon tetrachloride ug/L 50.050 100 60-140
Chlorobenzene ug/L 52.350 105 60-140
Chloroethane ug/L 36.650 73 60-140
Chloroform ug/L 49.550 99 60-140
Chloromethane ug/L 49.650 99 60-140
cis-1,2-Dichloroethene ug/L 50.850 102 60-140
cis-1,3-Dichloropropene ug/L 50.350 101 60-140
Dibromochloromethane ug/L 52.150 104 60-140
Dibromomethane ug/L 49.750 99 60-140
Dichlorodifluoromethane ug/L 50.050 100 60-140
Diisopropyl ether ug/L 50.750 101 60-140
Ethylbenzene ug/L 52.650 105 60-140
Hexachloro-1,3-butadiene ug/L 52.450 105 60-140
Isopropylbenzene (Cumene)ug/L 51.150 102 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 53.850 108 60-140
Methylene Chloride ug/L 48.350 97 60-140
n-Butylbenzene ug/L 52.750 105 60-140
n-Propylbenzene ug/L 51.750 103 60-140
Naphthalene ug/L 54.550 109 60-140
o-Xylene ug/L 51.850 104 60-140
sec-Butylbenzene ug/L 50.650 101 60-140
Styrene ug/L 51.850 104 60-140
tert-Butylbenzene ug/L 43.750 87 60-140
Tetrachloroethene ug/L 50.850 102 60-140
Toluene ug/L 49.950 100 60-140
trans-1,2-Dichloroethene ug/L 51.550 103 60-140
trans-1,3-Dichloropropene ug/L 50.650 101 60-140
Trichloroethene ug/L 51.950 104 60-140
Trichlorofluoromethane ug/L 42.750 85 60-140
Vinyl chloride ug/L 53.650 107 60-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3819633LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3819634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92632293004
3819635
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 800 105 60-140118 11 30800ND839941
1,1,1-Trichloroethane ug/L 800 104 60-140111 6 30800ND836888
1,1,2,2-Tetrachloroethane ug/L 800 103 60-140114 10 30800ND822909
1,1,2-Trichloroethane ug/L 800 106 60-140111 4 30800ND849888
1,1-Dichloroethane ug/L 800 104 60-140110 6 30800ND833883
1,1-Dichloroethene ug/L 800 110 60-140118 7 30800ND882942
1,1-Dichloropropene ug/L 800 108 60-140115 6 30800ND866919
1,2,3-Trichlorobenzene ug/L 800 113 60-140113 0 30800ND907904
1,2,3-Trichloropropane ug/L 800 103 60-140112 9 30800ND824899
1,2,4-Trichlorobenzene ug/L 800 107 60-140108 1 30800ND860865
1,2,4-Trimethylbenzene ug/L 800 111 60-140119 3 30800143023102370
1,2-Dibromo-3-
chloropropane ug/L 800 102 60-140108 5 30800ND820866
1,2-Dibromoethane (EDB)ug/L 800 107 60-140120 11 30800ND859958
1,2-Dichlorobenzene ug/L 800 105 60-140114 8 30800ND843909
1,2-Dichloroethane ug/L 800 97 60-140107 9 3080077.0 855 933
1,2-Dichloropropane ug/L 800 108 60-140118 9 30800ND863941
1,3,5-Trimethylbenzene ug/L 800 111 60-140118 5 3080023611201180
1,3-Dichlorobenzene ug/L 800 103 60-140109 6 30800ND824871
1,3-Dichloropropane ug/L 800 108 60-140115 7 30800ND863924
1,4-Dichlorobenzene ug/L 800 99 60-140104 5 30800ND796835
2,2-Dichloropropane ug/L 800 94 60-140100 6 30800ND752798
2-Chlorotoluene ug/L 800 109 60-140108 2 30800ND875861
4-Chlorotoluene ug/L 800 109 60-140108 2 30800ND875861
Benzene ug/L 800 89 60-14091 0 30800471054205430
Bromobenzene ug/L 800 100 60-140109 9 30800ND802876
Bromochloromethane ug/L 800 106 60-140117 10 30800ND845933
Bromodichloromethane ug/L 800 98 60-140107 9 30800ND780858
Bromoform ug/L 800 105 60-140112 7 30800ND842900
Bromomethane ug/L 800 91 60-14098 8 30800ND727785
Carbon tetrachloride ug/L 800 108 60-140117 8 30800ND863932
Chlorobenzene ug/L 800 109 60-140118 8 30800ND869942
Chloroethane ug/L 800 100 60-140102 2 30800ND797814
Chloroform ug/L 800 108 60-140113 5 30800ND863904
Chloromethane ug/L 800 102 60-140105 2 30800ND818838
cis-1,2-Dichloroethene ug/L 800 106 60-140112 6 30800ND848898
cis-1,3-Dichloropropene ug/L 800 102 60-140110 7 30800ND820879
Dibromochloromethane ug/L 800 107 60-140116 8 30800ND854927
Dibromomethane ug/L 800 105 60-140114 8 30800ND838910
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3819634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92632293004
3819635
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 800 98 60-140107 8 30800ND788857
Diisopropyl ether ug/L 800 99 60-140109 9 3080067.2 861 942
Ethylbenzene ug/L 800 112 60-140121 4 30800101019101980
Hexachloro-1,3-butadiene ug/L 800 107 60-140107 0 30800ND853854
Isopropylbenzene
(Cumene)
ug/L 800 106 60-140114 6 3080068.5 919 978
m&p-Xylene ug/L 1600 113 60-140119 2 301600358053805490
Methyl-tert-butyl ether ug/L M180013460-140149 2 30800383049105030
Methylene Chloride ug/L 800 101 60-140107 6 30800ND808858
n-Butylbenzene ug/L 800 107 60-140110 3 30800ND858884
n-Propylbenzene ug/L 800 105 60-140113 6 3080018010201080
Naphthalene ug/L 800 113 60-140119 3 3080046513701410
o-Xylene ug/L 800 106 60-140117 4 30800141022502340
sec-Butylbenzene ug/L 800 107 60-140113 6 30800ND858907
Styrene ug/L 800 104 60-140114 9 30800ND834908
tert-Butylbenzene ug/L 800 91 60-14096 5 30800ND728765
Tetrachloroethene ug/L 800 98 60-140110 12 30800ND781881
Toluene ug/L 800 100 60-140109 5 3080078115801650
trans-1,2-Dichloroethene ug/L 800 106 60-140114 8 30800ND844911
trans-1,3-Dichloropropene ug/L 800 102 60-140109 7 30800ND815872
Trichloroethene ug/L 800 111 60-140120 7 30800ND890958
Trichlorofluoromethane ug/L 800 99 60-140104 5 30800ND789831
Vinyl chloride ug/L 800 111 60-140117 6 30800ND887938
1,2-Dichloroethane-d4 (S)%92 70-13092
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
734009
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92633456001, 92633456007, 92633456014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3820331
Associated Lab Samples:92633456001, 92633456007, 92633456014
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/01/22 10:170.31
1,1,1-Trichloroethane ug/L ND 0.50 11/01/22 10:170.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/01/22 10:170.22
1,1,2-Trichloroethane ug/L ND 0.50 11/01/22 10:170.32
1,1-Dichloroethane ug/L ND 0.50 11/01/22 10:170.37
1,1-Dichloroethene ug/L ND 0.50 11/01/22 10:170.35
1,1-Dichloropropene ug/L ND 0.50 11/01/22 10:170.43
1,2,3-Trichlorobenzene ug/L ND 2.0 11/01/22 10:170.81
1,2,3-Trichloropropane ug/L ND 0.50 11/01/22 10:170.26
1,2,4-Trichlorobenzene ug/L ND 2.0 11/01/22 10:170.64
1,2,4-Trimethylbenzene ug/L ND 0.50 11/01/22 10:170.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/01/22 10:170.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/01/22 10:170.27
1,2-Dichlorobenzene ug/L ND 0.50 11/01/22 10:170.34
1,2-Dichloroethane ug/L ND 0.50 11/01/22 10:170.32
1,2-Dichloropropane ug/L ND 0.50 11/01/22 10:170.36
1,3,5-Trimethylbenzene ug/L ND 0.50 11/01/22 10:170.33
1,3-Dichlorobenzene ug/L ND 0.50 11/01/22 10:170.34
1,3-Dichloropropane ug/L ND 0.50 11/01/22 10:170.28
1,4-Dichlorobenzene ug/L ND 0.50 11/01/22 10:170.33
2,2-Dichloropropane ug/L ND 0.50 11/01/22 10:170.39
2-Chlorotoluene ug/L ND 0.50 11/01/22 10:170.32
4-Chlorotoluene ug/L ND 0.50 11/01/22 10:170.32
Benzene ug/L ND 0.50 11/01/22 10:170.34
Bromobenzene ug/L ND 0.50 11/01/22 10:170.29
Bromochloromethane ug/L ND 0.50 11/01/22 10:170.47
Bromodichloromethane ug/L ND 0.50 11/01/22 10:170.31
Bromoform ug/L ND 0.50 11/01/22 10:170.34
Bromomethane ug/L ND 5.0 11/01/22 10:171.7
Carbon tetrachloride ug/L ND 0.50 11/01/22 10:170.33
Chlorobenzene ug/L ND 0.50 11/01/22 10:170.28
Chloroethane ug/L ND 1.0 11/01/22 10:170.65
Chloroform ug/L ND 0.50 11/01/22 10:170.43
Chloromethane ug/L ND 1.0 11/01/22 10:170.54
cis-1,2-Dichloroethene ug/L ND 0.50 11/01/22 10:170.38
cis-1,3-Dichloropropene ug/L ND 0.50 11/01/22 10:170.36
Dibromochloromethane ug/L ND 0.50 11/01/22 10:170.36
Dibromomethane ug/L ND 0.50 11/01/22 10:170.39
Dichlorodifluoromethane ug/L ND 0.50 11/01/22 10:170.35
Diisopropyl ether ug/L ND 0.50 11/01/22 10:170.31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3820331
Associated Lab Samples:92633456001, 92633456007, 92633456014
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 11/01/22 10:170.30
Hexachloro-1,3-butadiene ug/L ND 2.0 11/01/22 10:171.5
Isopropylbenzene (Cumene)ug/L ND 0.50 11/01/22 10:170.33
m&p-Xylene ug/L ND 1.0 11/01/22 10:170.71
Methyl-tert-butyl ether ug/L ND 0.50 11/01/22 10:170.42
Methylene Chloride ug/L ND 2.0 11/01/22 10:172.0
n-Butylbenzene ug/L ND 0.50 11/01/22 10:170.49
n-Propylbenzene ug/L ND 0.50 11/01/22 10:170.34
Naphthalene ug/L ND 2.0 11/01/22 10:170.64
o-Xylene ug/L ND 0.50 11/01/22 10:170.34
sec-Butylbenzene ug/L ND 0.50 11/01/22 10:170.40
Styrene ug/L ND 0.50 11/01/22 10:170.29
tert-Butylbenzene ug/L ND 0.50 11/01/22 10:170.32
Tetrachloroethene ug/L ND 0.50 11/01/22 10:170.29
Toluene ug/L ND 0.50 11/01/22 10:170.24
trans-1,2-Dichloroethene ug/L ND 0.50 11/01/22 10:170.40
trans-1,3-Dichloropropene ug/L ND 0.50 11/01/22 10:170.36
Trichloroethene ug/L ND 0.50 11/01/22 10:170.38
Trichlorofluoromethane ug/L ND 1.0 11/01/22 10:170.30
Vinyl chloride ug/L ND 1.0 11/01/22 10:170.39
1,2-Dichloroethane-d4 (S)%93 70-130 11/01/22 10:17
4-Bromofluorobenzene (S)%100 70-130 11/01/22 10:17
Toluene-d8 (S)%101 70-130 11/01/22 10:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3820332LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.050 112 60-140
1,1,1-Trichloroethane ug/L 51.850 104 60-140
1,1,2,2-Tetrachloroethane ug/L 54.750 109 60-140
1,1,2-Trichloroethane ug/L 53.750 107 60-140
1,1-Dichloroethane ug/L 52.250 104 60-140
1,1-Dichloroethene ug/L 55.250 110 60-140
1,1-Dichloropropene ug/L 55.550 111 60-140
1,2,3-Trichlorobenzene ug/L 54.850 110 60-140
1,2,3-Trichloropropane ug/L 52.150 104 60-140
1,2,4-Trichlorobenzene ug/L 56.450 113 60-140
1,2,4-Trimethylbenzene ug/L 57.450 115 60-140
1,2-Dibromo-3-chloropropane ug/L 52.650 105 60-140
1,2-Dibromoethane (EDB)ug/L 56.650 113 60-140
1,2-Dichlorobenzene ug/L 54.850 110 60-140
1,2-Dichloroethane ug/L 50.950 102 60-140
1,2-Dichloropropane ug/L 55.450 111 60-140
1,3,5-Trimethylbenzene ug/L 57.150 114 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3820332LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 56.650 113 60-140
1,3-Dichloropropane ug/L 55.450 111 60-140
1,4-Dichlorobenzene ug/L 53.250 106 60-140
2,2-Dichloropropane ug/L 53.650 107 60-140
2-Chlorotoluene ug/L 58.150 116 60-140
4-Chlorotoluene ug/L 58.150 116 60-140
Benzene ug/L 51.950 104 60-140
Bromobenzene ug/L 54.250 108 60-140
Bromochloromethane ug/L 54.850 110 60-140
Bromodichloromethane ug/L 50.350 101 60-140
Bromoform ug/L 54.950 110 60-140
Bromomethane ug/L 38.350 77 60-140
Carbon tetrachloride ug/L 54.450 109 60-140
Chlorobenzene ug/L 56.750 113 60-140
Chloroethane ug/L 38.450 77 60-140
Chloroform ug/L 53.650 107 60-140
Chloromethane ug/L 49.750 99 60-140
cis-1,2-Dichloroethene ug/L 53.950 108 60-140
cis-1,3-Dichloropropene ug/L 54.650 109 60-140
Dibromochloromethane ug/L 55.650 111 60-140
Dibromomethane ug/L 53.450 107 60-140
Dichlorodifluoromethane ug/L 52.250 104 60-140
Diisopropyl ether ug/L 51.750 103 60-140
Ethylbenzene ug/L 56.150 112 60-140
Hexachloro-1,3-butadiene ug/L 56.450 113 60-140
Isopropylbenzene (Cumene)ug/L 54.750 109 60-140
m&p-Xylene ug/L 114100 114 60-140
Methyl-tert-butyl ether ug/L 55.050 110 60-140
Methylene Chloride ug/L 50.850 102 60-140
n-Butylbenzene ug/L 57.150 114 60-140
n-Propylbenzene ug/L 56.250 112 60-140
Naphthalene ug/L 54.650 109 60-140
o-Xylene ug/L 54.850 110 60-140
sec-Butylbenzene ug/L 54.850 110 60-140
Styrene ug/L 55.150 110 60-140
tert-Butylbenzene ug/L 48.450 97 60-140
Tetrachloroethene ug/L 54.650 109 60-140
Toluene ug/L 53.850 108 60-140
trans-1,2-Dichloroethene ug/L 54.750 109 60-140
trans-1,3-Dichloropropene ug/L 53.450 107 60-140
Trichloroethene ug/L 56.050 112 60-140
Trichlorofluoromethane ug/L 45.850 92 60-140
Vinyl chloride ug/L 56.550 113 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3820333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92633456001
3820334
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 116 60-140110 5 30100ND116110
1,1,1-Trichloroethane ug/L 100 115 60-140107 7 30100ND115107
1,1,2,2-Tetrachloroethane ug/L 100 113 60-140111 2 30100ND113111
1,1,2-Trichloroethane ug/L 100 117 60-140113 3 30100ND117113
1,1-Dichloroethane ug/L 100 115 60-140107 7 30100ND115107
1,1-Dichloroethene ug/L 100 122 60-140115 6 30100ND122115
1,1-Dichloropropene ug/L 100 121 60-140113 7 30100ND121113
1,2,3-Trichlorobenzene ug/L 100 103 60-140106 3 30100ND103106
1,2,3-Trichloropropane ug/L 100 104 60-140111 7 30100ND104111
1,2,4-Trichlorobenzene ug/L 100 107 60-140106 1 30100ND107106
1,2,4-Trimethylbenzene ug/L 100 113 60-140110 1 30100637750746
1,2-Dibromo-3-
chloropropane ug/L 100 105 60-140103 2 30100ND105103
1,2-Dibromoethane (EDB)ug/L 100 118 60-140116 2 30100ND118116
1,2-Dichlorobenzene ug/L 100 111 60-140105 5 30100ND111105
1,2-Dichloroethane ug/L 100 108 60-140101 7 30100ND108101
1,2-Dichloropropane ug/L 100 119 60-140116 3 30100ND119116
1,3,5-Trimethylbenzene ug/L 100 119 60-140111 3 30100147266257
1,3-Dichlorobenzene ug/L 100 111 60-140106 5 30100ND111106
1,3-Dichloropropane ug/L 100 117 60-140113 4 30100ND117113
1,4-Dichlorobenzene ug/L 100 103 60-140101 2 30100ND103101
2,2-Dichloropropane ug/L 100 110 60-140101 9 30100ND110101
2-Chlorotoluene ug/L 100 111 60-140102 9 30100ND111102
4-Chlorotoluene ug/L 100 111 60-140102 9 30100ND111102
Benzene ug/L 100 115 60-140109 5 30100ND115109
Bromobenzene ug/L 100 110 60-140105 5 30100ND110105
Bromochloromethane ug/L 100 118 60-140112 6 30100ND118112
Bromodichloromethane ug/L 100 110 60-140104 6 30100ND110104
Bromoform ug/L 100 113 60-140109 3 30100ND113109
Bromomethane ug/L 100 84 60-14080 5 30100ND84.1 80.1
Carbon tetrachloride ug/L 100 120 60-140116 4 30100ND120116
Chlorobenzene ug/L 100 118 60-140111 6 30100ND118111
Chloroethane ug/L 100 105 60-14098 7 30100ND10597.6
Chloroform ug/L 100 117 60-140111 6 30100ND117111
Chloromethane ug/L 100 103 60-14098 5 30100ND10397.5
cis-1,2-Dichloroethene ug/L 100 115 60-140110 5 30100ND115110
cis-1,3-Dichloropropene ug/L 100 117 60-140111 6 30100ND117111
Dibromochloromethane ug/L 100 115 60-140112 2 30100ND115112
Dibromomethane ug/L 100 118 60-140113 4 30100ND118113
Dichlorodifluoromethane ug/L 100 109 60-140102 7 30100ND109102
Diisopropyl ether ug/L 100 111 60-140104 6 30100ND111104
Ethylbenzene ug/L 100 116 60-140114 1 30100282397395
Hexachloro-1,3-butadiene ug/L 100 105 60-140108 2 30100ND105108
Isopropylbenzene(Cumene)ug/L 100 117 60-140112 3 3010043.7 161 156
m&p-Xylene ug/L 200 100 60-14098 0 30200103012301230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3820333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92633456001
3820334
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 100 115 60-140111 4 30100ND115111
Methylene Chloride ug/L 100 112 60-140105 7 30100ND112105
n-Butylbenzene ug/L 100 135 60-140137 1 30100ND135137
n-Propylbenzene ug/L 100 114 60-140109 2 30100129243238
Naphthalene ug/L 100 105 60-140111 4 3010038.5 144 149
o-Xylene ug/L 100 110 60-140110 0 30100307416416
sec-Butylbenzene ug/L 100 126 60-140122 3 30100ND126122
Styrene ug/L 100 116 60-140110 5 30100ND116110
tert-Butylbenzene ug/L 100 99 60-14097 2 30100ND98.7 96.7
Tetrachloroethene ug/L 100 114 60-140109 4 30100ND114109
Toluene ug/L 100 124 60-140120 1 30100310434430
trans-1,2-Dichloroethene ug/L 100 118 60-140110 7 30100ND118110
trans-1,3-Dichloropropene ug/L 100 113 60-140110 3 30100ND113110
Trichloroethene ug/L 100 123 60-140115 6 30100ND123115
Trichlorofluoromethane ug/L 100 110 60-140101 9 30100ND110101
Vinyl chloride ug/L 100 118 60-140113 5 30100ND118113
1,2-Dichloroethane-d4 (S)%92 70-13090
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92633456
Crown Food Mart 10/27
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92633456001 734009MW-16 SM 6200B
92633456002 733838MW-6A SM 6200B
92633456003 733838SW-14 SM 6200B
92633456004 733838SW-11 SM 6200B
92633456005 733838SW-13 SM 6200B
92633456006 733838SW-12 SM 6200B
92633456007 734009MW-8 SM 6200B
92633456008 733838MW-13 SM 6200B
92633456009 733838SW-01-185 SM 6200B
92633456010 733838SW-02-185 SM 6200B
92633456011 733838SW-03-185 SM 6200B
92633456012 733838MW-14 SM 6200B
92633456013 733838DUPESM 6200B
92633456014 734009DUP 2 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/02/2022 04:32 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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