AS-4331_41488_CA_LAB_20221220

#=CL#
December 30, 2022
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92643751
92643751
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
CROWN FOOD MART 12/20/22
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 52
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 52
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Lab ID Sample ID Matrix Date Collected Date Received
92643751001 MW-4 Water 12/20/22 14:20 12/22/22 10:11
92643751002 MW-5 Water 12/20/22 15:39 12/22/22 10:11
92643751003 MW-8 Water 12/20/22 12:59 12/22/22 10:11
92643751004 MW-9 Water 12/20/22 10:43 12/22/22 10:11
92643751005 MW-11 Water 12/21/22 11:40 12/22/22 10:11
92643751006 MW-13 Water 12/20/22 13:58 12/22/22 10:11
92643751007 MW-14 Water 12/20/22 12:30 12/22/22 10:11
92643751008 MW-15 Water 12/20/22 11:23 12/22/22 10:11
92643751009 MW-17 Water 12/20/22 15:50 12/22/22 10:11
92643751010 MW-18 Water 12/20/22 10:22 12/22/22 10:11
92643751011 EW-2 Water 12/21/22 09:59 12/22/22 10:11
92643751012 EW-3 Water 12/21/22 10:07 12/22/22 10:11
92643751013 EW-4 Water 12/21/22 10:15 12/22/22 10:11
92643751014 EW-5 Water 12/21/22 10:19 12/22/22 10:11
92643751015 DUP-2 Water 12/21/22 00:00 12/22/22 10:11
92643751016 TRIP Water 12/20/22 00:00 12/22/22 10:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 52
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92643751001 MW-4 SM 6200B 63 PASI-CSAS
92643751002 MW-5 SM 6200B 63 PASI-CSAS
92643751003 MW-8 SM 6200B 63 PASI-CSAS
92643751004 MW-9 SM 6200B 63 PASI-CSAS
92643751005 MW-11 SM 6200B 63 PASI-CSAS
92643751006 MW-13 SM 6200B 63 PASI-CSAS
92643751007 MW-14 SM 6200B 63 PASI-CSAS
92643751008 MW-15 SM 6200B 63 PASI-CSAS
92643751009 MW-17 SM 6200B 63 PASI-CSAS
92643751010 MW-18 SM 6200B 63 PASI-CSAS
92643751011 EW-2 SM 6200B 63 PASI-CSAS
92643751012 EW-3 SM 6200B 63 PASI-CSAS
92643751013 EW-4 SM 6200B 63 PASI-CSAS
92643751014 EW-5 SM 6200B 63 PASI-CSAS
92643751015 DUP-2 SM 6200B 63 PASI-CSAS
92643751016 TRIP SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-4 Lab ID:92643751001 Collected:12/20/22 14:20 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.1 ug/L 12/29/22 13:07 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 13:07 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 13:07 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 13:07 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 13:07 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 13:07 74-83-95.0 1.7 1
n-Butylbenzene 7.2 ug/L 12/29/22 13:07 104-51-80.50 0.49 1
sec-Butylbenzene 12.7 ug/L 12/29/22 13:07 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 13:07 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 13:07 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 13:07 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 13:07 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 13:07 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 13:07 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 13:07 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 13:07 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 13:07 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 13:07 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 13:07 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 13:07 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 13:07 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 13:07 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 13:07 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 13:07 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 13:07 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 13:07 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 13:07 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 13:07 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 13:07 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 13:07 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 13:07 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 13:07 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 13:07 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 13:07 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 13:07 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 13:07 108-20-30.50 0.31 1
Ethylbenzene 11.8 ug/L 12/29/22 13:07 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 13:07 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)15.3 ug/L 12/29/22 13:07 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 13:07 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 13:07 1634-04-40.50 0.42 1
Naphthalene 4.3 ug/L 12/29/22 13:07 91-20-32.0 0.64 1
n-Propylbenzene 52.2 ug/L 12/29/22 13:07 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 13:07 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 13:07 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-4 Lab ID:92643751001 Collected:12/20/22 14:20 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 13:07 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 13:07 127-18-40.50 0.29 1
Toluene 0.89 ug/L 12/29/22 13:07 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 13:07 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 13:07 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 13:07 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 13:07 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 13:07 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 13:07 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 13:07 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 14.7 ug/L 12/29/22 13:07 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 1.5 ug/L 12/29/22 13:07 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 13:07 75-01-41.0 0.39 1
m&p-Xylene 15.6 ug/L 12/29/22 13:07 179601-23-11.0 0.71 1
o-Xylene 1.1 ug/L 12/29/22 13:07 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)114 %12/29/22 13:07 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %12/29/22 13:07 460-00-470-130 1
Toluene-d8 (S)104 %12/29/22 13:07 2037-26-570-130 1
Sample:MW-5 Lab ID:92643751002 Collected:12/20/22 15:39 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 17.0 ug/L 12/29/22 13:25 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 13:25 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 13:25 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 13:25 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 13:25 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 13:25 74-83-95.0 1.7 1
n-Butylbenzene 22.1 ug/L 12/29/22 13:25 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 13:25 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 13:25 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 13:25 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 13:25 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 13:25 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 13:25 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 13:25 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 13:25 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 13:25 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 13:25 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-5 Lab ID:92643751002 Collected:12/20/22 15:39 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/29/22 13:25 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 13:25 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 13:25 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 13:25 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 13:25 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 13:25 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 13:25 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 13:25 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 13:25 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 13:25 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 13:25 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 13:25 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 13:25 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 13:25 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 13:25 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 13:25 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 13:25 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 13:25 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 13:25 108-20-30.50 0.31 1
Ethylbenzene 75.2 ug/L 12/29/22 13:25 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 13:25 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)45.1 ug/L 12/29/22 13:25 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 13:25 75-09-22.0 2.0 1
Methyl-tert-butyl ether 2.1 ug/L 12/29/22 13:25 1634-04-40.50 0.42 1
Naphthalene 27.2 ug/L 12/29/22 13:25 91-20-32.0 0.64 1
n-Propylbenzene 160 ug/L 12/29/22 13:25 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 13:25 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 13:25 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 13:25 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 13:25 127-18-40.50 0.29 1
Toluene 13.9 ug/L 12/29/22 13:25 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 13:25 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 13:25 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 13:25 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 13:25 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 13:25 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 13:25 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 13:25 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 135 ug/L 12/29/22 13:25 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 9.1 ug/L 12/29/22 13:25 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 13:25 75-01-41.0 0.39 1
m&p-Xylene 81.2 ug/L 12/29/22 13:25 179601-23-11.0 0.71 1
o-Xylene 2.6 ug/L 12/29/22 13:25 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)118 %12/29/22 13:25 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-5 Lab ID:92643751002 Collected:12/20/22 15:39 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)102 %12/29/22 13:25 460-00-470-130 1
Toluene-d8 (S)103 %12/29/22 13:25 2037-26-570-130 1
Sample:MW-8 Lab ID:92643751003 Collected:12/20/22 12:59 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3.5 ug/L 12/29/22 05:45 71-43-21.0 0.69 2
Bromobenzene ND ug/L 12/29/22 05:45 108-86-11.0 0.58 2
Bromochloromethane ND ug/L 12/29/22 05:45 74-97-51.0 0.94 2
Bromodichloromethane ND ug/L 12/29/22 05:45 75-27-41.0 0.61 2
Bromoform ND ug/L 12/29/22 05:45 75-25-21.0 0.68 2
Bromomethane ND ug/L 12/29/22 05:45 74-83-910.0 3.3 2
n-Butylbenzene ND ug/L 12/29/22 05:45 104-51-81.0 0.98 2
sec-Butylbenzene ND ug/L 12/29/22 05:45 135-98-81.0 0.80 2
tert-Butylbenzene ND ug/L 12/29/22 05:45 98-06-61.0 0.65 2
Carbon tetrachloride ND ug/L 12/29/22 05:45 56-23-51.0 0.67 2
Chlorobenzene ND ug/L 12/29/22 05:45 108-90-71.0 0.57 2
Chloroethane ND ug/L 12/29/22 05:45 75-00-32.0 1.3 2
Chloroform ND ug/L 12/29/22 05:45 67-66-31.0 0.86 2
Chloromethane ND ug/L 12/29/22 05:45 74-87-32.0 1.1 2
2-Chlorotoluene ND ug/L 12/29/22 05:45 95-49-81.0 0.64 2
4-Chlorotoluene ND ug/L 12/29/22 05:45 106-43-41.0 0.65 2
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 05:45 96-12-82.0 0.68 2
Dibromochloromethane ND ug/L 12/29/22 05:45 124-48-11.0 0.72 2
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 05:45 106-93-41.0 0.54 2
Dibromomethane ND ug/L 12/29/22 05:45 74-95-31.0 0.79 2
1,2-Dichlorobenzene ND ug/L 12/29/22 05:45 95-50-11.0 0.68 2
1,3-Dichlorobenzene ND ug/L 12/29/22 05:45 541-73-11.0 0.68 2
1,4-Dichlorobenzene ND ug/L 12/29/22 05:45 106-46-71.0 0.67 2
Dichlorodifluoromethane ND ug/L 12/29/22 05:45 75-71-81.0 0.69 2
1,1-Dichloroethane ND ug/L 12/29/22 05:45 75-34-31.0 0.73 2
1,2-Dichloroethane ND ug/L 12/29/22 05:45 107-06-21.0 0.64 2
1,1-Dichloroethene ND ug/L 12/29/22 05:45 75-35-41.0 0.70 2
cis-1,2-Dichloroethene ND ug/L 12/29/22 05:45 156-59-21.0 0.77 2
trans-1,2-Dichloroethene ND ug/L 12/29/22 05:45 156-60-51.0 0.79 2
1,2-Dichloropropane ND ug/L 12/29/22 05:45 78-87-51.0 0.71 2
1,3-Dichloropropane ND ug/L 12/29/22 05:45 142-28-91.0 0.57 2
2,2-Dichloropropane ND ug/L 12/29/22 05:45 594-20-71.0 0.78 2
1,1-Dichloropropene ND ug/L 12/29/22 05:45 563-58-61.0 0.85 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-8 Lab ID:92643751003 Collected:12/20/22 12:59 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/29/22 05:45 10061-01-51.0 0.73 2
trans-1,3-Dichloropropene ND ug/L 12/29/22 05:45 10061-02-61.0 0.73 2
Diisopropyl ether ND ug/L 12/29/22 05:45 108-20-31.0 0.62 2
Ethylbenzene 27.3 ug/L 12/29/22 05:45 100-41-41.0 0.61 2
Hexachloro-1,3-butadiene ND ug/L 12/29/22 05:45 87-68-34.0 3.1 2
Isopropylbenzene (Cumene)15.8 ug/L 12/29/22 05:45 98-82-81.0 0.67 2
Methylene Chloride 4.5 ug/L 12/29/22 05:45 75-09-2 C94.0 3.9 2
Methyl-tert-butyl ether ND ug/L 12/29/22 05:45 1634-04-41.0 0.84 2
Naphthalene 12.9 ug/L 12/29/22 05:45 91-20-34.0 1.3 2
n-Propylbenzene 39.6 ug/L 12/29/22 05:45 103-65-11.0 0.68 2
Styrene ND ug/L 12/29/22 05:45 100-42-51.0 0.58 2
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 05:45 630-20-61.0 0.62 2
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 05:45 79-34-51.0 0.45 2
Tetrachloroethene ND ug/L 12/29/22 05:45 127-18-41.0 0.58 2
Toluene 3.0 ug/L 12/29/22 05:45 108-88-31.0 0.48 2
1,2,3-Trichlorobenzene ND ug/L 12/29/22 05:45 87-61-64.0 1.6 2
1,2,4-Trichlorobenzene ND ug/L 12/29/22 05:45 120-82-14.0 1.3 2
1,1,1-Trichloroethane ND ug/L 12/29/22 05:45 71-55-61.0 0.66 2
1,1,2-Trichloroethane ND ug/L 12/29/22 05:45 79-00-51.0 0.65 2
Trichloroethene ND ug/L 12/29/22 05:45 79-01-61.0 0.77 2
Trichlorofluoromethane ND ug/L 12/29/22 05:45 75-69-42.0 0.60 2
1,2,3-Trichloropropane ND ug/L 12/29/22 05:45 96-18-41.0 0.52 2
1,2,4-Trimethylbenzene 337 ug/L 12/29/22 05:45 95-63-61.0 0.99 2
1,3,5-Trimethylbenzene 79.7 ug/L 12/29/22 05:45 108-67-81.0 0.66 2
Vinyl chloride ND ug/L 12/29/22 05:45 75-01-42.0 0.77 2
m&p-Xylene 40.7 ug/L 12/29/22 05:45 179601-23-12.0 1.4 2
o-Xylene 47.9 ug/L 12/29/22 05:45 95-47-61.0 0.68 2
Surrogates
1,2-Dichloroethane-d4 (S)119 %12/29/22 05:45 17060-07-070-130 2
4-Bromofluorobenzene (S)101 %12/29/22 05:45 460-00-470-130 2
Toluene-d8 (S)108 %12/29/22 05:45 2037-26-570-130 2
Sample:MW-9 Lab ID:92643751004 Collected:12/20/22 10:43 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 03:22 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 03:22 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 03:22 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 03:22 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 03:22 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-9 Lab ID:92643751004 Collected:12/20/22 10:43 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/29/22 03:22 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 03:22 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 03:22 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 03:22 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 03:22 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 03:22 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 03:22 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 03:22 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 03:22 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 03:22 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 03:22 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 03:22 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 03:22 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 03:22 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 03:22 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 03:22 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 03:22 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 03:22 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 03:22 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 03:22 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 03:22 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 03:22 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 03:22 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 03:22 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 03:22 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 03:22 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 03:22 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 03:22 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 03:22 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 03:22 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 03:22 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 03:22 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 03:22 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/29/22 03:22 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 03:22 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 03:22 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 03:22 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 03:22 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 03:22 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 03:22 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 03:22 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 03:22 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 03:22 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 03:22 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 03:22 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-9 Lab ID:92643751004 Collected:12/20/22 10:43 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/29/22 03:22 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 03:22 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 03:22 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 03:22 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 03:22 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 03:22 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 03:22 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 03:22 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 03:22 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 03:22 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)119 %12/29/22 03:22 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/29/22 03:22 460-00-470-130 1
Toluene-d8 (S)105 %12/29/22 03:22 2037-26-570-130 1
Sample:MW-11 Lab ID:92643751005 Collected:12/21/22 11:40 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 03:40 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 03:40 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 03:40 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 03:40 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 03:40 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 03:40 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 03:40 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 03:40 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 03:40 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 03:40 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 03:40 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 03:40 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 03:40 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 03:40 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 03:40 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 03:40 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 03:40 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 03:40 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 03:40 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 03:40 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 03:40 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 03:40 541-73-10.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-11 Lab ID:92643751005 Collected:12/21/22 11:40 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/29/22 03:40 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 03:40 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 03:40 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 03:40 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 03:40 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 03:40 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 03:40 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 03:40 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 03:40 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 03:40 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 03:40 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 03:40 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 03:40 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 03:40 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 03:40 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 03:40 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/29/22 03:40 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 03:40 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 03:40 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 03:40 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 03:40 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 03:40 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 03:40 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 03:40 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 03:40 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 03:40 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 03:40 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 03:40 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 03:40 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 03:40 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 03:40 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 03:40 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 03:40 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 03:40 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 03:40 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 03:40 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 03:40 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 03:40 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/29/22 03:40 17060-07-070-130 1
4-Bromofluorobenzene (S)104 %12/29/22 03:40 460-00-470-130 1
Toluene-d8 (S)108 %12/29/22 03:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-13 Lab ID:92643751006 Collected:12/20/22 13:58 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3.7 ug/L 12/29/22 14:00 71-43-2 M12.5 1.7 5
Bromobenzene ND ug/L 12/29/22 14:00 108-86-12.5 1.4 5
Bromochloromethane ND ug/L 12/29/22 14:00 74-97-5 M12.5 2.3 5
Bromodichloromethane ND ug/L 12/29/22 14:00 75-27-4 M12.5 1.5 5
Bromoform ND ug/L 12/29/22 14:00 75-25-22.5 1.7 5
Bromomethane ND ug/L 12/29/22 14:00 74-83-925.0 8.3 5
n-Butylbenzene ND ug/L 12/29/22 14:00 104-51-8 M12.5 2.4 5
sec-Butylbenzene ND ug/L 12/29/22 14:00 135-98-8 M12.5 2.0 5
tert-Butylbenzene ND ug/L 12/29/22 14:00 98-06-62.5 1.6 5
Carbon tetrachloride ND ug/L 12/29/22 14:00 56-23-52.5 1.7 5
Chlorobenzene ND ug/L 12/29/22 14:00 108-90-72.5 1.4 5
Chloroethane ND ug/L 12/29/22 14:00 75-00-3 M15.0 3.2 5
Chloroform ND ug/L 12/29/22 14:00 67-66-3 M12.5 2.2 5
Chloromethane ND ug/L 12/29/22 14:00 74-87-3 M15.0 2.7 5
2-Chlorotoluene ND ug/L 12/29/22 14:00 95-49-8 M12.5 1.6 5
4-Chlorotoluene ND ug/L 12/29/22 14:00 106-43-4 M12.5 1.6 5
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 14:00 96-12-85.0 1.7 5
Dibromochloromethane ND ug/L 12/29/22 14:00 124-48-12.5 1.8 5
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 14:00 106-93-4 M12.5 1.4 5
Dibromomethane ND ug/L 12/29/22 14:00 74-95-32.5 2.0 5
1,2-Dichlorobenzene ND ug/L 12/29/22 14:00 95-50-12.5 1.7 5
1,3-Dichlorobenzene ND ug/L 12/29/22 14:00 541-73-12.5 1.7 5
1,4-Dichlorobenzene ND ug/L 12/29/22 14:00 106-46-72.5 1.7 5
Dichlorodifluoromethane ND ug/L 12/29/22 14:00 75-71-82.5 1.7 5
1,1-Dichloroethane ND ug/L 12/29/22 14:00 75-34-3 M12.5 1.8 5
1,2-Dichloroethane ND ug/L 12/29/22 14:00 107-06-2 M12.5 1.6 5
1,1-Dichloroethene ND ug/L 12/29/22 14:00 75-35-4 M12.5 1.7 5
cis-1,2-Dichloroethene 2.1J ug/L 12/29/22 14:00 156-59-2 M12.5 1.9 5
trans-1,2-Dichloroethene ND ug/L 12/29/22 14:00 156-60-5 M12.5 2.0 5
1,2-Dichloropropane ND ug/L 12/29/22 14:00 78-87-5 M12.5 1.8 5
1,3-Dichloropropane ND ug/L 12/29/22 14:00 142-28-9 M12.5 1.4 5
2,2-Dichloropropane ND ug/L 12/29/22 14:00 594-20-7 M12.5 1.9 5
1,1-Dichloropropene ND ug/L 12/29/22 14:00 563-58-6 M12.5 2.1 5
cis-1,3-Dichloropropene ND ug/L 12/29/22 14:00 10061-01-5 M12.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 12/29/22 14:00 10061-02-6 M12.5 1.8 5
Diisopropyl ether ND ug/L 12/29/22 14:00 108-20-3 M12.5 1.5 5
Ethylbenzene 137 ug/L 12/29/22 14:00 100-41-4 M12.5 1.5 5
Hexachloro-1,3-butadiene ND ug/L 12/29/22 14:00 87-68-310.0 7.6 5
Isopropylbenzene (Cumene)39.1 ug/L 12/29/22 14:00 98-82-82.5 1.7 5
Methylene Chloride 19.3 ug/L 12/29/22 14:00 75-09-2 C910.0 9.8 5
Methyl-tert-butyl ether ND ug/L 12/29/22 14:00 1634-04-4 M12.5 2.1 5
Naphthalene 30.4 ug/L 12/29/22 14:00 91-20-3 M110.0 3.2 5
n-Propylbenzene 122 ug/L 12/29/22 14:00 103-65-1 M12.5 1.7 5
Styrene 1.8J ug/L 12/29/22 14:00 100-42-52.5 1.5 5
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 14:00 630-20-62.5 1.6 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-13 Lab ID:92643751006 Collected:12/20/22 13:58 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 14:00 79-34-5 M12.5 1.1 5
Tetrachloroethene ND ug/L 12/29/22 14:00 127-18-42.5 1.5 5
Toluene 11.9 ug/L 12/29/22 14:00 108-88-3 M12.5 1.2 5
1,2,3-Trichlorobenzene ND ug/L 12/29/22 14:00 87-61-610.0 4.0 5
1,2,4-Trichlorobenzene ND ug/L 12/29/22 14:00 120-82-110.0 3.2 5
1,1,1-Trichloroethane ND ug/L 12/29/22 14:00 71-55-6 M12.5 1.7 5
1,1,2-Trichloroethane ND ug/L 12/29/22 14:00 79-00-5 M12.5 1.6 5
Trichloroethene ND ug/L 12/29/22 14:00 79-01-6 M12.5 1.9 5
Trichlorofluoromethane ND ug/L 12/29/22 14:00 75-69-45.0 1.5 5
1,2,3-Trichloropropane ND ug/L 12/29/22 14:00 96-18-4 M12.5 1.3 5
1,2,4-Trimethylbenzene 814 ug/L 12/29/22 14:00 95-63-6 M12.5 2.5 5
1,3,5-Trimethylbenzene 184 ug/L 12/29/22 14:00 108-67-8 M12.5 1.7 5
Vinyl chloride ND ug/L 12/29/22 14:00 75-01-4 M15.0 1.9 5
m&p-Xylene 250 ug/L 12/29/22 14:00 179601-23-1 M15.0 3.5 5
o-Xylene 112 ug/L 12/29/22 14:00 95-47-6 M12.5 1.7 5
Surrogates
1,2-Dichloroethane-d4 (S)117 %12/29/22 14:00 17060-07-070-130 5
4-Bromofluorobenzene (S)102 %12/29/22 14:00 460-00-470-130 5
Toluene-d8 (S)110 %12/29/22 14:00 2037-26-570-130 5
Sample:MW-14 Lab ID:92643751007 Collected:12/20/22 12:30 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 06:38 71-43-25.0 3.4 10
Bromobenzene ND ug/L 12/29/22 06:38 108-86-15.0 2.9 10
Bromochloromethane ND ug/L 12/29/22 06:38 74-97-55.0 4.7 10
Bromodichloromethane ND ug/L 12/29/22 06:38 75-27-45.0 3.1 10
Bromoform ND ug/L 12/29/22 06:38 75-25-25.0 3.4 10
Bromomethane ND ug/L 12/29/22 06:38 74-83-950.0 16.6 10
n-Butylbenzene ND ug/L 12/29/22 06:38 104-51-85.0 4.9 10
sec-Butylbenzene ND ug/L 12/29/22 06:38 135-98-85.0 4.0 10
tert-Butylbenzene ND ug/L 12/29/22 06:38 98-06-65.0 3.2 10
Carbon tetrachloride ND ug/L 12/29/22 06:38 56-23-55.0 3.3 10
Chlorobenzene ND ug/L 12/29/22 06:38 108-90-75.0 2.8 10
Chloroethane ND ug/L 12/29/22 06:38 75-00-3 M110.0 6.5 10
Chloroform ND ug/L 12/29/22 06:38 67-66-35.0 4.3 10
Chloromethane ND ug/L 12/29/22 06:38 74-87-310.0 5.4 10
2-Chlorotoluene ND ug/L 12/29/22 06:38 95-49-85.0 3.2 10
4-Chlorotoluene ND ug/L 12/29/22 06:38 106-43-45.0 3.2 10
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 06:38 96-12-810.0 3.4 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-14 Lab ID:92643751007 Collected:12/20/22 12:30 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/29/22 06:38 124-48-15.0 3.6 10
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 06:38 106-93-45.0 2.7 10
Dibromomethane ND ug/L 12/29/22 06:38 74-95-35.0 3.9 10
1,2-Dichlorobenzene ND ug/L 12/29/22 06:38 95-50-15.0 3.4 10
1,3-Dichlorobenzene ND ug/L 12/29/22 06:38 541-73-15.0 3.4 10
1,4-Dichlorobenzene ND ug/L 12/29/22 06:38 106-46-75.0 3.3 10
Dichlorodifluoromethane ND ug/L 12/29/22 06:38 75-71-85.0 3.5 10
1,1-Dichloroethane ND ug/L 12/29/22 06:38 75-34-35.0 3.7 10
1,2-Dichloroethane ND ug/L 12/29/22 06:38 107-06-2 M15.0 3.2 10
1,1-Dichloroethene ND ug/L 12/29/22 06:38 75-35-4 M15.0 3.5 10
cis-1,2-Dichloroethene 7.9 ug/L 12/29/22 06:38 156-59-25.0 3.8 10
trans-1,2-Dichloroethene ND ug/L 12/29/22 06:38 156-60-55.0 4.0 10
1,2-Dichloropropane ND ug/L 12/29/22 06:38 78-87-55.0 3.6 10
1,3-Dichloropropane ND ug/L 12/29/22 06:38 142-28-95.0 2.8 10
2,2-Dichloropropane ND ug/L 12/29/22 06:38 594-20-75.0 3.9 10
1,1-Dichloropropene ND ug/L 12/29/22 06:38 563-58-6 M15.0 4.3 10
cis-1,3-Dichloropropene ND ug/L 12/29/22 06:38 10061-01-55.0 3.6 10
trans-1,3-Dichloropropene ND ug/L 12/29/22 06:38 10061-02-65.0 3.6 10
Diisopropyl ether ND ug/L 12/29/22 06:38 108-20-35.0 3.1 10
Ethylbenzene 208 ug/L 12/29/22 06:38 100-41-45.0 3.0 10
Hexachloro-1,3-butadiene ND ug/L 12/29/22 06:38 87-68-320.0 15.3 10
Isopropylbenzene (Cumene)38.9 ug/L 12/29/22 06:38 98-82-85.0 3.3 10
Methylene Chloride ND ug/L 12/29/22 06:38 75-09-220.0 19.5 10
Methyl-tert-butyl ether ND ug/L 12/29/22 06:38 1634-04-45.0 4.2 10
Naphthalene 47.2 ug/L 12/29/22 06:38 91-20-320.0 6.4 10
n-Propylbenzene 110 ug/L 12/29/22 06:38 103-65-15.0 3.4 10
Styrene ND ug/L 12/29/22 06:38 100-42-55.0 2.9 10
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 06:38 630-20-65.0 3.1 10
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 06:38 79-34-55.0 2.2 10
Tetrachloroethene ND ug/L 12/29/22 06:38 127-18-45.0 2.9 10
Toluene 7.9 ug/L 12/29/22 06:38 108-88-35.0 2.4 10
1,2,3-Trichlorobenzene ND ug/L 12/29/22 06:38 87-61-620.0 8.1 10
1,2,4-Trichlorobenzene ND ug/L 12/29/22 06:38 120-82-120.0 6.4 10
1,1,1-Trichloroethane ND ug/L 12/29/22 06:38 71-55-65.0 3.3 10
1,1,2-Trichloroethane ND ug/L 12/29/22 06:38 79-00-55.0 3.2 10
Trichloroethene ND ug/L 12/29/22 06:38 79-01-65.0 3.8 10
Trichlorofluoromethane ND ug/L 12/29/22 06:38 75-69-410.0 3.0 10
1,2,3-Trichloropropane ND ug/L 12/29/22 06:38 96-18-45.0 2.6 10
1,2,4-Trimethylbenzene 915 ug/L 12/29/22 06:38 95-63-65.0 5.0 10
1,3,5-Trimethylbenzene 155 ug/L 12/29/22 06:38 108-67-85.0 3.3 10
Vinyl chloride ND ug/L 12/29/22 06:38 75-01-410.0 3.9 10
m&p-Xylene 184 ug/L 12/29/22 06:38 179601-23-110.0 7.1 10
o-Xylene 106 ug/L 12/29/22 06:38 95-47-65.0 3.4 10
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/29/22 06:38 17060-07-070-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-14 Lab ID:92643751007 Collected:12/20/22 12:30 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)103 %12/29/22 06:38 460-00-470-130 10
Toluene-d8 (S)108 %12/29/22 06:38 2037-26-570-130 10
Sample:MW-15 Lab ID:92643751008 Collected:12/20/22 11:23 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 03:58 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 03:58 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 03:58 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 03:58 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 03:58 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 03:58 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 03:58 104-51-80.50 0.49 1
sec-Butylbenzene 0.70 ug/L 12/29/22 03:58 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 03:58 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 03:58 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 03:58 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 03:58 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 03:58 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 03:58 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 03:58 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 03:58 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 03:58 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 03:58 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 03:58 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 03:58 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 03:58 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 03:58 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 03:58 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 03:58 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 03:58 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 03:58 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 03:58 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 03:58 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 03:58 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 03:58 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 03:58 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 03:58 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 03:58 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-15 Lab ID:92643751008 Collected:12/20/22 11:23 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/29/22 03:58 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 03:58 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 03:58 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 03:58 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 03:58 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)0.73 ug/L 12/29/22 03:58 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 03:58 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 03:58 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 03:58 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 03:58 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 03:58 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 03:58 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 03:58 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 03:58 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 03:58 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 03:58 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 03:58 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 03:58 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 03:58 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 03:58 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 03:58 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 03:58 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 03:58 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 03:58 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 03:58 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 03:58 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 03:58 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)116 %12/29/22 03:58 17060-07-070-130 1
4-Bromofluorobenzene (S)103 %12/29/22 03:58 460-00-470-130 1
Toluene-d8 (S)106 %12/29/22 03:58 2037-26-570-130 1
Sample:MW-17 Lab ID:92643751009 Collected:12/20/22 15:50 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 04:16 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 04:16 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 04:16 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 04:16 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 04:16 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-17 Lab ID:92643751009 Collected:12/20/22 15:50 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/29/22 04:16 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 04:16 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 04:16 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 04:16 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 04:16 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 04:16 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 04:16 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 04:16 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 04:16 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 04:16 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 04:16 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 04:16 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 04:16 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 04:16 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 04:16 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 04:16 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 04:16 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 04:16 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 04:16 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 04:16 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 04:16 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 04:16 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 04:16 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 04:16 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 04:16 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 04:16 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 04:16 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 04:16 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 04:16 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 04:16 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 04:16 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 04:16 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 04:16 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/29/22 04:16 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 04:16 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 04:16 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 04:16 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 04:16 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 04:16 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 04:16 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 04:16 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 04:16 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 04:16 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 04:16 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 04:16 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-17 Lab ID:92643751009 Collected:12/20/22 15:50 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/29/22 04:16 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 04:16 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 04:16 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 04:16 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 04:16 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 04:16 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 04:16 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 04:16 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 04:16 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 04:16 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)120 %12/29/22 04:16 17060-07-070-130 1
4-Bromofluorobenzene (S)104 %12/29/22 04:16 460-00-470-130 1
Toluene-d8 (S)105 %12/29/22 04:16 2037-26-570-130 1
Sample:MW-18 Lab ID:92643751010 Collected:12/20/22 10:22 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 04:33 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 04:33 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 04:33 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 04:33 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 04:33 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 04:33 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 04:33 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 04:33 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 04:33 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 04:33 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 04:33 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 04:33 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 04:33 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 04:33 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 04:33 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 04:33 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 04:33 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 04:33 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 04:33 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 04:33 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 04:33 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 04:33 541-73-10.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:MW-18 Lab ID:92643751010 Collected:12/20/22 10:22 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/29/22 04:33 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 04:33 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 04:33 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 04:33 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 04:33 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 04:33 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 04:33 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 04:33 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 04:33 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 04:33 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 04:33 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 04:33 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 04:33 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 04:33 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 04:33 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 04:33 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/29/22 04:33 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 04:33 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 04:33 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 04:33 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 04:33 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 04:33 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 04:33 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 04:33 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 04:33 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 04:33 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 04:33 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 04:33 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 04:33 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 04:33 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 04:33 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 04:33 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 04:33 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 04:33 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 04:33 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 04:33 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 04:33 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 04:33 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)118 %12/29/22 04:33 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/29/22 04:33 460-00-470-130 1
Toluene-d8 (S)107 %12/29/22 04:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-2 Lab ID:92643751011 Collected:12/21/22 09:59 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.2 ug/L 12/29/22 13:42 71-43-21.2 0.86 2.5
Bromobenzene ND ug/L 12/29/22 13:42 108-86-11.2 0.72 2.5
Bromochloromethane ND ug/L 12/29/22 13:42 74-97-51.2 1.2 2.5
Bromodichloromethane ND ug/L 12/29/22 13:42 75-27-41.2 0.77 2.5
Bromoform ND ug/L 12/29/22 13:42 75-25-21.2 0.85 2.5
Bromomethane ND ug/L 12/29/22 13:42 74-83-912.5 4.2 2.5
n-Butylbenzene 17.8 ug/L 12/29/22 13:42 104-51-81.2 1.2 2.5
sec-Butylbenzene ND ug/L 12/29/22 13:42 135-98-81.2 1.0 2.5
tert-Butylbenzene ND ug/L 12/29/22 13:42 98-06-61.2 0.81 2.5
Carbon tetrachloride ND ug/L 12/29/22 13:42 56-23-51.2 0.83 2.5
Chlorobenzene ND ug/L 12/29/22 13:42 108-90-71.2 0.71 2.5
Chloroethane ND ug/L 12/29/22 13:42 75-00-32.5 1.6 2.5
Chloroform ND ug/L 12/29/22 13:42 67-66-31.2 1.1 2.5
Chloromethane ND ug/L 12/29/22 13:42 74-87-32.5 1.4 2.5
2-Chlorotoluene ND ug/L 12/29/22 13:42 95-49-81.2 0.80 2.5
4-Chlorotoluene ND ug/L 12/29/22 13:42 106-43-41.2 0.81 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 13:42 96-12-82.5 0.85 2.5
Dibromochloromethane ND ug/L 12/29/22 13:42 124-48-11.2 0.90 2.5
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 13:42 106-93-41.2 0.68 2.5
Dibromomethane ND ug/L 12/29/22 13:42 74-95-31.2 0.98 2.5
1,2-Dichlorobenzene ND ug/L 12/29/22 13:42 95-50-11.2 0.85 2.5
1,3-Dichlorobenzene ND ug/L 12/29/22 13:42 541-73-11.2 0.85 2.5
1,4-Dichlorobenzene ND ug/L 12/29/22 13:42 106-46-71.2 0.83 2.5
Dichlorodifluoromethane ND ug/L 12/29/22 13:42 75-71-81.2 0.86 2.5
1,1-Dichloroethane ND ug/L 12/29/22 13:42 75-34-31.2 0.92 2.5
1,2-Dichloroethane ND ug/L 12/29/22 13:42 107-06-21.2 0.80 2.5
1,1-Dichloroethene ND ug/L 12/29/22 13:42 75-35-41.2 0.87 2.5
cis-1,2-Dichloroethene ND ug/L 12/29/22 13:42 156-59-21.2 0.96 2.5
trans-1,2-Dichloroethene ND ug/L 12/29/22 13:42 156-60-51.2 0.99 2.5
1,2-Dichloropropane ND ug/L 12/29/22 13:42 78-87-51.2 0.89 2.5
1,3-Dichloropropane ND ug/L 12/29/22 13:42 142-28-91.2 0.71 2.5
2,2-Dichloropropane ND ug/L 12/29/22 13:42 594-20-71.2 0.97 2.5
1,1-Dichloropropene ND ug/L 12/29/22 13:42 563-58-61.2 1.1 2.5
cis-1,3-Dichloropropene ND ug/L 12/29/22 13:42 10061-01-51.2 0.91 2.5
trans-1,3-Dichloropropene ND ug/L 12/29/22 13:42 10061-02-61.2 0.91 2.5
Diisopropyl ether ND ug/L 12/29/22 13:42 108-20-31.2 0.77 2.5
Ethylbenzene 47.5 ug/L 12/29/22 13:42 100-41-41.2 0.76 2.5
Hexachloro-1,3-butadiene ND ug/L 12/29/22 13:42 87-68-35.0 3.8 2.5
Isopropylbenzene (Cumene)20.1 ug/L 12/29/22 13:42 98-82-81.2 0.83 2.5
Methylene Chloride 13.8 ug/L 12/29/22 13:42 75-09-2 C95.0 4.9 2.5
Methyl-tert-butyl ether ND ug/L 12/29/22 13:42 1634-04-41.2 1.1 2.5
Naphthalene 15.9 ug/L 12/29/22 13:42 91-20-35.0 1.6 2.5
n-Propylbenzene 68.7 ug/L 12/29/22 13:42 103-65-11.2 0.85 2.5
Styrene ND ug/L 12/29/22 13:42 100-42-51.2 0.73 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 13:42 630-20-61.2 0.78 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-2 Lab ID:92643751011 Collected:12/21/22 09:59 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 13:42 79-34-51.2 0.56 2.5
Tetrachloroethene ND ug/L 12/29/22 13:42 127-18-41.2 0.73 2.5
Toluene 4.6 ug/L 12/29/22 13:42 108-88-31.2 0.60 2.5
1,2,3-Trichlorobenzene ND ug/L 12/29/22 13:42 87-61-65.0 2.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/29/22 13:42 120-82-15.0 1.6 2.5
1,1,1-Trichloroethane ND ug/L 12/29/22 13:42 71-55-61.2 0.83 2.5
1,1,2-Trichloroethane ND ug/L 12/29/22 13:42 79-00-51.2 0.81 2.5
Trichloroethene ND ug/L 12/29/22 13:42 79-01-61.2 0.96 2.5
Trichlorofluoromethane ND ug/L 12/29/22 13:42 75-69-42.5 0.74 2.5
1,2,3-Trichloropropane ND ug/L 12/29/22 13:42 96-18-41.2 0.65 2.5
1,2,4-Trimethylbenzene 346 ug/L 12/29/22 13:42 95-63-61.2 1.2 2.5
1,3,5-Trimethylbenzene 72.8 ug/L 12/29/22 13:42 108-67-81.2 0.83 2.5
Vinyl chloride ND ug/L 12/29/22 13:42 75-01-42.5 0.96 2.5
m&p-Xylene 142 ug/L 12/29/22 13:42 179601-23-12.5 1.8 2.5
o-Xylene 26.4 ug/L 12/29/22 13:42 95-47-61.2 0.84 2.5
Surrogates
1,2-Dichloroethane-d4 (S)115 %12/29/22 13:42 17060-07-070-130 2.5
4-Bromofluorobenzene (S)100 %12/29/22 13:42 460-00-470-130 2.5
Toluene-d8 (S)106 %12/29/22 13:42 2037-26-570-130 2.5
Sample:EW-3 Lab ID:92643751012 Collected:12/21/22 10:07 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 4.6 ug/L 12/29/22 04:51 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 04:51 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 04:51 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 04:51 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 04:51 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 04:51 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 04:51 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 04:51 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 04:51 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 04:51 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 04:51 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 04:51 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 04:51 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 04:51 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 04:51 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 04:51 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 04:51 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-3 Lab ID:92643751012 Collected:12/21/22 10:07 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/29/22 04:51 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 04:51 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 04:51 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 04:51 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 04:51 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 04:51 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 04:51 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 04:51 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 04:51 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 04:51 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 04:51 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 04:51 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 04:51 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 04:51 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 04:51 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 04:51 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 04:51 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 04:51 10061-02-60.50 0.36 1
Diisopropyl ether 2.5 ug/L 12/29/22 04:51 108-20-30.50 0.31 1
Ethylbenzene 7.7 ug/L 12/29/22 04:51 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 04:51 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)3.7 ug/L 12/29/22 04:51 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 04:51 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.77 ug/L 12/29/22 04:51 1634-04-40.50 0.42 1
Naphthalene 6.7 ug/L 12/29/22 04:51 91-20-32.0 0.64 1
n-Propylbenzene 3.2 ug/L 12/29/22 04:51 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 04:51 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 04:51 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 04:51 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 04:51 127-18-40.50 0.29 1
Toluene 0.53 ug/L 12/29/22 04:51 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 04:51 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 04:51 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 04:51 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 04:51 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 04:51 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 04:51 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 04:51 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 37.0 ug/L 12/29/22 04:51 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 22.9 ug/L 12/29/22 04:51 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 04:51 75-01-41.0 0.39 1
m&p-Xylene 13.3 ug/L 12/29/22 04:51 179601-23-11.0 0.71 1
o-Xylene 10.4 ug/L 12/29/22 04:51 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)119 %12/29/22 04:51 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-3 Lab ID:92643751012 Collected:12/21/22 10:07 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)103 %12/29/22 04:51 460-00-470-130 1
Toluene-d8 (S)105 %12/29/22 04:51 2037-26-570-130 1
Sample:EW-4 Lab ID:92643751013 Collected:12/21/22 10:15 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 29.2 ug/L 12/29/22 14:53 71-43-22.5 1.7 5
Bromobenzene ND ug/L 12/29/22 14:53 108-86-12.5 1.4 5
Bromochloromethane ND ug/L 12/29/22 14:53 74-97-52.5 2.3 5
Bromodichloromethane ND ug/L 12/29/22 14:53 75-27-42.5 1.5 5
Bromoform ND ug/L 12/29/22 14:53 75-25-22.5 1.7 5
Bromomethane ND ug/L 12/29/22 14:53 74-83-925.0 8.3 5
n-Butylbenzene ND ug/L 12/29/22 14:53 104-51-82.5 2.4 5
sec-Butylbenzene ND ug/L 12/29/22 14:53 135-98-82.5 2.0 5
tert-Butylbenzene ND ug/L 12/29/22 14:53 98-06-62.5 1.6 5
Carbon tetrachloride ND ug/L 12/29/22 14:53 56-23-52.5 1.7 5
Chlorobenzene ND ug/L 12/29/22 14:53 108-90-72.5 1.4 5
Chloroethane ND ug/L 12/29/22 14:53 75-00-35.0 3.2 5
Chloroform ND ug/L 12/29/22 14:53 67-66-32.5 2.2 5
Chloromethane ND ug/L 12/29/22 14:53 74-87-35.0 2.7 5
2-Chlorotoluene ND ug/L 12/29/22 14:53 95-49-82.5 1.6 5
4-Chlorotoluene ND ug/L 12/29/22 14:53 106-43-42.5 1.6 5
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 14:53 96-12-85.0 1.7 5
Dibromochloromethane ND ug/L 12/29/22 14:53 124-48-12.5 1.8 5
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 14:53 106-93-42.5 1.4 5
Dibromomethane ND ug/L 12/29/22 14:53 74-95-32.5 2.0 5
1,2-Dichlorobenzene ND ug/L 12/29/22 14:53 95-50-12.5 1.7 5
1,3-Dichlorobenzene ND ug/L 12/29/22 14:53 541-73-12.5 1.7 5
1,4-Dichlorobenzene ND ug/L 12/29/22 14:53 106-46-72.5 1.7 5
Dichlorodifluoromethane ND ug/L 12/29/22 14:53 75-71-82.5 1.7 5
1,1-Dichloroethane ND ug/L 12/29/22 14:53 75-34-32.5 1.8 5
1,2-Dichloroethane ND ug/L 12/29/22 14:53 107-06-22.5 1.6 5
1,1-Dichloroethene ND ug/L 12/29/22 14:53 75-35-42.5 1.7 5
cis-1,2-Dichloroethene ND ug/L 12/29/22 14:53 156-59-22.5 1.9 5
trans-1,2-Dichloroethene ND ug/L 12/29/22 14:53 156-60-52.5 2.0 5
1,2-Dichloropropane ND ug/L 12/29/22 14:53 78-87-52.5 1.8 5
1,3-Dichloropropane ND ug/L 12/29/22 14:53 142-28-92.5 1.4 5
2,2-Dichloropropane ND ug/L 12/29/22 14:53 594-20-72.5 1.9 5
1,1-Dichloropropene ND ug/L 12/29/22 14:53 563-58-62.5 2.1 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-4 Lab ID:92643751013 Collected:12/21/22 10:15 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/29/22 14:53 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene ND ug/L 12/29/22 14:53 10061-02-62.5 1.8 5
Diisopropyl ether 5.5 ug/L 12/29/22 14:53 108-20-32.5 1.5 5
Ethylbenzene 124 ug/L 12/29/22 14:53 100-41-42.5 1.5 5
Hexachloro-1,3-butadiene ND ug/L 12/29/22 14:53 87-68-310.0 7.6 5
Isopropylbenzene (Cumene)39.4 ug/L 12/29/22 14:53 98-82-82.5 1.7 5
Methylene Chloride 22.8 ug/L 12/29/22 14:53 75-09-2 C910.0 9.8 5
Methyl-tert-butyl ether 3.3 ug/L 12/29/22 14:53 1634-04-42.5 2.1 5
Naphthalene 36.1 ug/L 12/29/22 14:53 91-20-310.0 3.2 5
n-Propylbenzene 103 ug/L 12/29/22 14:53 103-65-12.5 1.7 5
Styrene ND ug/L 12/29/22 14:53 100-42-52.5 1.5 5
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 14:53 630-20-62.5 1.6 5
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 14:53 79-34-52.5 1.1 5
Tetrachloroethene ND ug/L 12/29/22 14:53 127-18-42.5 1.5 5
Toluene 3.9 ug/L 12/29/22 14:53 108-88-32.5 1.2 5
1,2,3-Trichlorobenzene ND ug/L 12/29/22 14:53 87-61-610.0 4.0 5
1,2,4-Trichlorobenzene ND ug/L 12/29/22 14:53 120-82-110.0 3.2 5
1,1,1-Trichloroethane ND ug/L 12/29/22 14:53 71-55-62.5 1.7 5
1,1,2-Trichloroethane ND ug/L 12/29/22 14:53 79-00-52.5 1.6 5
Trichloroethene ND ug/L 12/29/22 14:53 79-01-62.5 1.9 5
Trichlorofluoromethane ND ug/L 12/29/22 14:53 75-69-45.0 1.5 5
1,2,3-Trichloropropane ND ug/L 12/29/22 14:53 96-18-42.5 1.3 5
1,2,4-Trimethylbenzene 602 ug/L 12/29/22 14:53 95-63-62.5 2.5 5
1,3,5-Trimethylbenzene 176 ug/L 12/29/22 14:53 108-67-82.5 1.7 5
Vinyl chloride ND ug/L 12/29/22 14:53 75-01-45.0 1.9 5
m&p-Xylene 139 ug/L 12/29/22 14:53 179601-23-15.0 3.5 5
o-Xylene 20.3 ug/L 12/29/22 14:53 95-47-62.5 1.7 5
Surrogates
1,2-Dichloroethane-d4 (S)115 %12/29/22 14:53 17060-07-070-130 5
4-Bromofluorobenzene (S)101 %12/29/22 14:53 460-00-470-130 5
Toluene-d8 (S)108 %12/29/22 14:53 2037-26-570-130 5
Sample:EW-5 Lab ID:92643751014 Collected:12/21/22 10:19 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 4.8 ug/L 12/29/22 14:35 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 14:35 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 14:35 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 14:35 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 14:35 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-5 Lab ID:92643751014 Collected:12/21/22 10:19 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/29/22 14:35 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 14:35 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 14:35 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 14:35 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 14:35 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 14:35 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 14:35 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 14:35 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 14:35 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 14:35 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 14:35 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 14:35 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 14:35 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 14:35 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 14:35 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 14:35 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 14:35 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 14:35 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 14:35 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 14:35 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 14:35 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 14:35 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 14:35 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 14:35 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 14:35 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 14:35 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 14:35 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 14:35 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 14:35 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 14:35 10061-02-60.50 0.36 1
Diisopropyl ether 4.2 ug/L 12/29/22 14:35 108-20-30.50 0.31 1
Ethylbenzene 5.7 ug/L 12/29/22 14:35 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 14:35 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)2.4 ug/L 12/29/22 14:35 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 14:35 75-09-22.0 2.0 1
Methyl-tert-butyl ether 5.2 ug/L 12/29/22 14:35 1634-04-40.50 0.42 1
Naphthalene 5.2 ug/L 12/29/22 14:35 91-20-32.0 0.64 1
n-Propylbenzene 3.8 ug/L 12/29/22 14:35 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 14:35 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 14:35 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 14:35 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 14:35 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 14:35 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 14:35 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 14:35 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:EW-5 Lab ID:92643751014 Collected:12/21/22 10:19 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/29/22 14:35 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 14:35 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 14:35 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 14:35 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 14:35 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 26.3 ug/L 12/29/22 14:35 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 38.3 ug/L 12/29/22 14:35 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 14:35 75-01-41.0 0.39 1
m&p-Xylene 15.6 ug/L 12/29/22 14:35 179601-23-11.0 0.71 1
o-Xylene 7.0 ug/L 12/29/22 14:35 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)116 %12/29/22 14:35 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/29/22 14:35 460-00-470-130 1
Toluene-d8 (S)106 %12/29/22 14:35 2037-26-570-130 1
Sample:DUP-2 Lab ID:92643751015 Collected:12/21/22 00:00 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.6 ug/L 12/30/22 13:36 71-43-21.2 0.86 2.5
Bromobenzene ND ug/L 12/30/22 13:36 108-86-11.2 0.72 2.5
Bromochloromethane ND ug/L 12/30/22 13:36 74-97-51.2 1.2 2.5
Bromodichloromethane ND ug/L 12/30/22 13:36 75-27-41.2 0.77 2.5
Bromoform ND ug/L 12/30/22 13:36 75-25-21.2 0.85 2.5
Bromomethane ND ug/L 12/30/22 13:36 74-83-912.5 4.2 2.5
n-Butylbenzene ND ug/L 12/30/22 13:36 104-51-81.2 1.2 2.5
sec-Butylbenzene ND ug/L 12/30/22 13:36 135-98-81.2 1.0 2.5
tert-Butylbenzene ND ug/L 12/30/22 13:36 98-06-61.2 0.81 2.5
Carbon tetrachloride ND ug/L 12/30/22 13:36 56-23-51.2 0.83 2.5
Chlorobenzene ND ug/L 12/30/22 13:36 108-90-71.2 0.71 2.5
Chloroethane ND ug/L 12/30/22 13:36 75-00-32.5 1.6 2.5
Chloroform ND ug/L 12/30/22 13:36 67-66-31.2 1.1 2.5
Chloromethane ND ug/L 12/30/22 13:36 74-87-32.5 1.4 2.5
2-Chlorotoluene ND ug/L 12/30/22 13:36 95-49-81.2 0.80 2.5
4-Chlorotoluene ND ug/L 12/30/22 13:36 106-43-41.2 0.81 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/30/22 13:36 96-12-82.5 0.85 2.5
Dibromochloromethane ND ug/L 12/30/22 13:36 124-48-11.2 0.90 2.5
1,2-Dibromoethane (EDB)ND ug/L 12/30/22 13:36 106-93-41.2 0.68 2.5
Dibromomethane ND ug/L 12/30/22 13:36 74-95-31.2 0.98 2.5
1,2-Dichlorobenzene ND ug/L 12/30/22 13:36 95-50-11.2 0.85 2.5
1,3-Dichlorobenzene ND ug/L 12/30/22 13:36 541-73-11.2 0.85 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:DUP-2 Lab ID:92643751015 Collected:12/21/22 00:00 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/30/22 13:36 106-46-71.2 0.83 2.5
Dichlorodifluoromethane ND ug/L 12/30/22 13:36 75-71-81.2 0.86 2.5
1,1-Dichloroethane ND ug/L 12/30/22 13:36 75-34-31.2 0.92 2.5
1,2-Dichloroethane ND ug/L 12/30/22 13:36 107-06-21.2 0.80 2.5
1,1-Dichloroethene ND ug/L 12/30/22 13:36 75-35-41.2 0.87 2.5
cis-1,2-Dichloroethene ND ug/L 12/30/22 13:36 156-59-21.2 0.96 2.5
trans-1,2-Dichloroethene ND ug/L 12/30/22 13:36 156-60-51.2 0.99 2.5
1,2-Dichloropropane ND ug/L 12/30/22 13:36 78-87-51.2 0.89 2.5
1,3-Dichloropropane ND ug/L 12/30/22 13:36 142-28-91.2 0.71 2.5
2,2-Dichloropropane ND ug/L 12/30/22 13:36 594-20-71.2 0.97 2.5
1,1-Dichloropropene ND ug/L 12/30/22 13:36 563-58-61.2 1.1 2.5
cis-1,3-Dichloropropene ND ug/L 12/30/22 13:36 10061-01-51.2 0.91 2.5
trans-1,3-Dichloropropene ND ug/L 12/30/22 13:36 10061-02-61.2 0.91 2.5
Diisopropyl ether ND ug/L 12/30/22 13:36 108-20-31.2 0.77 2.5
Ethylbenzene 45.3 ug/L 12/30/22 13:36 100-41-41.2 0.76 2.5
Hexachloro-1,3-butadiene ND ug/L 12/30/22 13:36 87-68-35.0 3.8 2.5
Isopropylbenzene (Cumene)19.6 ug/L 12/30/22 13:36 98-82-81.2 0.83 2.5
Methylene Chloride ND ug/L 12/30/22 13:36 75-09-25.0 4.9 2.5
Methyl-tert-butyl ether ND ug/L 12/30/22 13:36 1634-04-41.2 1.1 2.5
Naphthalene 16.0 ug/L 12/30/22 13:36 91-20-35.0 1.6 2.5
n-Propylbenzene 60.6 ug/L 12/30/22 13:36 103-65-11.2 0.85 2.5
Styrene ND ug/L 12/30/22 13:36 100-42-51.2 0.73 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/30/22 13:36 630-20-61.2 0.78 2.5
1,1,2,2-Tetrachloroethane ND ug/L 12/30/22 13:36 79-34-51.2 0.56 2.5
Tetrachloroethene ND ug/L 12/30/22 13:36 127-18-41.2 0.73 2.5
Toluene 6.2 ug/L 12/30/22 13:36 108-88-31.2 0.60 2.5
1,2,3-Trichlorobenzene ND ug/L 12/30/22 13:36 87-61-65.0 2.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/30/22 13:36 120-82-15.0 1.6 2.5
1,1,1-Trichloroethane ND ug/L 12/30/22 13:36 71-55-61.2 0.83 2.5
1,1,2-Trichloroethane ND ug/L 12/30/22 13:36 79-00-51.2 0.81 2.5
Trichloroethene ND ug/L 12/30/22 13:36 79-01-61.2 0.96 2.5
Trichlorofluoromethane ND ug/L 12/30/22 13:36 75-69-42.5 0.74 2.5
1,2,3-Trichloropropane ND ug/L 12/30/22 13:36 96-18-41.2 0.65 2.5
1,2,4-Trimethylbenzene 305 ug/L 12/30/22 13:36 95-63-61.2 1.2 2.5
1,3,5-Trimethylbenzene 67.6 ug/L 12/30/22 13:36 108-67-81.2 0.83 2.5
Vinyl chloride ND ug/L 12/30/22 13:36 75-01-42.5 0.96 2.5
m&p-Xylene 137 ug/L 12/30/22 13:36 179601-23-12.5 1.8 2.5
o-Xylene 26.7 ug/L 12/30/22 13:36 95-47-61.2 0.84 2.5
Surrogates
1,2-Dichloroethane-d4 (S)80 %12/30/22 13:36 17060-07-070-130 2.5
4-Bromofluorobenzene (S)94 %12/30/22 13:36 460-00-470-130 2.5
Toluene-d8 (S)99 %12/30/22 13:36 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:TRIP Lab ID:92643751016 Collected:12/20/22 00:00 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/29/22 12:31 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/29/22 12:31 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/29/22 12:31 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/29/22 12:31 75-27-40.50 0.31 1
Bromoform ND ug/L 12/29/22 12:31 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/29/22 12:31 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/29/22 12:31 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/29/22 12:31 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/29/22 12:31 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/29/22 12:31 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/29/22 12:31 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/29/22 12:31 75-00-31.0 0.65 1
Chloroform ND ug/L 12/29/22 12:31 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/29/22 12:31 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/29/22 12:31 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/29/22 12:31 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/29/22 12:31 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/29/22 12:31 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/29/22 12:31 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/29/22 12:31 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/29/22 12:31 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/29/22 12:31 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/29/22 12:31 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/29/22 12:31 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/29/22 12:31 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/29/22 12:31 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/29/22 12:31 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/29/22 12:31 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/29/22 12:31 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/29/22 12:31 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/29/22 12:31 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/29/22 12:31 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/29/22 12:31 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/29/22 12:31 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/29/22 12:31 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/29/22 12:31 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/29/22 12:31 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/29/22 12:31 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/29/22 12:31 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/29/22 12:31 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/29/22 12:31 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/29/22 12:31 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/29/22 12:31 103-65-10.50 0.34 1
Styrene ND ug/L 12/29/22 12:31 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/29/22 12:31 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Sample:TRIP Lab ID:92643751016 Collected:12/20/22 00:00 Received:12/22/22 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/29/22 12:31 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/29/22 12:31 127-18-40.50 0.29 1
Toluene ND ug/L 12/29/22 12:31 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/29/22 12:31 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/29/22 12:31 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/29/22 12:31 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/29/22 12:31 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/29/22 12:31 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/29/22 12:31 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/29/22 12:31 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/29/22 12:31 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/29/22 12:31 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/29/22 12:31 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/29/22 12:31 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/29/22 12:31 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)118 %12/29/22 12:31 17060-07-070-130 1
4-Bromofluorobenzene (S)105 %12/29/22 12:31 460-00-470-130 1
Toluene-d8 (S)105 %12/29/22 12:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746186
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92643751003, 92643751004, 92643751005, 92643751007, 92643751008, 92643751009, 92643751010,
92643751012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880801
Associated Lab Samples:92643751003, 92643751004, 92643751005, 92643751007, 92643751008, 92643751009, 92643751010,
92643751012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/28/22 23:500.31
1,1,1-Trichloroethane ug/L ND 0.50 12/28/22 23:500.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/28/22 23:500.22
1,1,2-Trichloroethane ug/L ND 0.50 12/28/22 23:500.32
1,1-Dichloroethane ug/L ND 0.50 12/28/22 23:500.37
1,1-Dichloroethene ug/L ND 0.50 12/28/22 23:500.35
1,1-Dichloropropene ug/L ND 0.50 12/28/22 23:500.43
1,2,3-Trichlorobenzene ug/L ND 2.0 12/28/22 23:500.81
1,2,3-Trichloropropane ug/L ND 0.50 12/28/22 23:500.26
1,2,4-Trichlorobenzene ug/L ND 2.0 12/28/22 23:500.64
1,2,4-Trimethylbenzene ug/L ND 0.50 12/28/22 23:500.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/28/22 23:500.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/28/22 23:500.27
1,2-Dichlorobenzene ug/L ND 0.50 12/28/22 23:500.34
1,2-Dichloroethane ug/L ND 0.50 12/28/22 23:500.32
1,2-Dichloropropane ug/L ND 0.50 12/28/22 23:500.36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/28/22 23:500.33
1,3-Dichlorobenzene ug/L ND 0.50 12/28/22 23:500.34
1,3-Dichloropropane ug/L ND 0.50 12/28/22 23:500.28
1,4-Dichlorobenzene ug/L ND 0.50 12/28/22 23:500.33
2,2-Dichloropropane ug/L ND 0.50 12/28/22 23:500.39
2-Chlorotoluene ug/L ND 0.50 12/28/22 23:500.32
4-Chlorotoluene ug/L ND 0.50 12/28/22 23:500.32
Benzene ug/L ND 0.50 12/28/22 23:500.34
Bromobenzene ug/L ND 0.50 12/28/22 23:500.29
Bromochloromethane ug/L ND 0.50 12/28/22 23:500.47
Bromodichloromethane ug/L ND 0.50 12/28/22 23:500.31
Bromoform ug/L ND 0.50 12/28/22 23:500.34
Bromomethane ug/L ND 5.0 12/28/22 23:501.7
Carbon tetrachloride ug/L ND 0.50 12/28/22 23:500.33
Chlorobenzene ug/L ND 0.50 12/28/22 23:500.28
Chloroethane ug/L ND 1.0 12/28/22 23:500.65
Chloroform ug/L ND 0.50 12/28/22 23:500.43
Chloromethane ug/L ND 1.0 12/28/22 23:500.54
cis-1,2-Dichloroethene ug/L ND 0.50 12/28/22 23:500.38
cis-1,3-Dichloropropene ug/L ND 0.50 12/28/22 23:500.36
Dibromochloromethane ug/L ND 0.50 12/28/22 23:500.36
Dibromomethane ug/L ND 0.50 12/28/22 23:500.39
Dichlorodifluoromethane ug/L ND 0.50 12/28/22 23:500.35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880801
Associated Lab Samples:92643751003, 92643751004, 92643751005, 92643751007, 92643751008, 92643751009, 92643751010,
92643751012
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 12/28/22 23:500.31
Ethylbenzene ug/L ND 0.50 12/28/22 23:500.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/28/22 23:501.5
Isopropylbenzene (Cumene)ug/L ND 0.50 12/28/22 23:500.33
m&p-Xylene ug/L ND 1.0 12/28/22 23:500.71
Methyl-tert-butyl ether ug/L ND 0.50 12/28/22 23:500.42
Methylene Chloride ug/L ND 2.0 12/28/22 23:502.0
n-Butylbenzene ug/L ND 0.50 12/28/22 23:500.49
n-Propylbenzene ug/L ND 0.50 12/28/22 23:500.34
Naphthalene ug/L ND 2.0 12/28/22 23:500.64
o-Xylene ug/L ND 0.50 12/28/22 23:500.34
sec-Butylbenzene ug/L ND 0.50 12/28/22 23:500.40
Styrene ug/L ND 0.50 12/28/22 23:500.29
tert-Butylbenzene ug/L ND 0.50 12/28/22 23:500.32
Tetrachloroethene ug/L ND 0.50 12/28/22 23:500.29
Toluene ug/L ND 0.50 12/28/22 23:500.24
trans-1,2-Dichloroethene ug/L ND 0.50 12/28/22 23:500.40
trans-1,3-Dichloropropene ug/L ND 0.50 12/28/22 23:500.36
Trichloroethene ug/L ND 0.50 12/28/22 23:500.38
Trichlorofluoromethane ug/L ND 1.0 12/28/22 23:500.30
Vinyl chloride ug/L ND 1.0 12/28/22 23:500.39
1,2-Dichloroethane-d4 (S)%118 70-130 12/28/22 23:50
4-Bromofluorobenzene (S)%103 70-130 12/28/22 23:50
Toluene-d8 (S)%106 70-130 12/28/22 23:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880802LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.250 98 60-140
1,1,1-Trichloroethane ug/L 52.850 106 60-140
1,1,2,2-Tetrachloroethane ug/L 50.550 101 60-140
1,1,2-Trichloroethane ug/L 51.150 102 60-140
1,1-Dichloroethane ug/L 52.750 105 60-140
1,1-Dichloroethene ug/L 54.750 109 60-140
1,1-Dichloropropene ug/L 57.050 114 60-140
1,2,3-Trichlorobenzene ug/L 44.850 90 60-140
1,2,3-Trichloropropane ug/L 51.850 104 60-140
1,2,4-Trichlorobenzene ug/L 43.850 88 60-140
1,2,4-Trimethylbenzene ug/L 49.550 99 60-140
1,2-Dibromo-3-chloropropane ug/L 47.150 94 60-140
1,2-Dibromoethane (EDB)ug/L 50.250 100 60-140
1,2-Dichlorobenzene ug/L 47.250 94 60-140
1,2-Dichloroethane ug/L 55.550 111 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880802LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 53.550 107 60-140
1,3,5-Trimethylbenzene ug/L 50.450 101 60-140
1,3-Dichlorobenzene ug/L 46.750 93 60-140
1,3-Dichloropropane ug/L 52.250 104 60-140
1,4-Dichlorobenzene ug/L 45.550 91 60-140
2,2-Dichloropropane ug/L 49.250 98 60-140
2-Chlorotoluene ug/L 48.850 98 60-140
4-Chlorotoluene ug/L 50.050 100 60-140
Benzene ug/L 48.150 96 60-140
Bromobenzene ug/L 47.550 95 60-140
Bromochloromethane ug/L 50.450 101 60-140
Bromodichloromethane ug/L 49.250 98 60-140
Bromoform ug/L 45.050 90 60-140
Bromomethane ug/L 47.450 95 60-140
Carbon tetrachloride ug/L 48.450 97 60-140
Chlorobenzene ug/L 48.550 97 60-140
Chloroethane ug/L 60.450 121 60-140
Chloroform ug/L 51.450 103 60-140
Chloromethane ug/L 49.950 100 60-140
cis-1,2-Dichloroethene ug/L 53.950 108 60-140
cis-1,3-Dichloropropene ug/L 51.750 103 60-140
Dibromochloromethane ug/L 48.650 97 60-140
Dibromomethane ug/L 45.550 91 60-140
Dichlorodifluoromethane ug/L 46.050 92 60-140
Diisopropyl ether ug/L 54.650 109 60-140
Ethylbenzene ug/L 48.250 96 60-140
Hexachloro-1,3-butadiene ug/L 44.650 89 60-140
Isopropylbenzene (Cumene)ug/L 46.250 92 60-140
m&p-Xylene ug/L 94.6100 95 60-140
Methyl-tert-butyl ether ug/L 53.950 108 60-140
Methylene Chloride ug/L 48.350 97 60-140
n-Butylbenzene ug/L 50.050 100 60-140
n-Propylbenzene ug/L 49.750 99 60-140
Naphthalene ug/L 48.350 97 60-140
o-Xylene ug/L 47.650 95 60-140
sec-Butylbenzene ug/L 48.950 98 60-140
Styrene ug/L 48.350 97 60-140
tert-Butylbenzene ug/L 38.550 77 60-140
Tetrachloroethene ug/L 42.550 85 60-140
Toluene ug/L 47.450 95 60-140
trans-1,2-Dichloroethene ug/L 54.450 109 60-140
trans-1,3-Dichloropropene ug/L 50.750 101 60-140
Trichloroethene ug/L 49.750 99 60-140
Trichlorofluoromethane ug/L 47.950 96 60-140
Vinyl chloride ug/L 49.850 100 60-140
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880802LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3880803MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643751007
3880804
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 118 60-140115 3 30200ND236230
1,1,1-Trichloroethane ug/L 200 136 60-140129 5 30200ND272259
1,1,2,2-Tetrachloroethane ug/L 200 126 60-140123 2 30200ND251245
1,1,2-Trichloroethane ug/L 200 121 60-140116 4 30200ND242232
1,1-Dichloroethane ug/L 200 139 60-140131 6 30200ND278262
1,1-Dichloroethene ug/L M120014860-140139 7 30200ND297278
1,1-Dichloropropene ug/L M120014460-140139 4 30200ND288278
1,2,3-Trichlorobenzene ug/L 200 100 60-140102 2 30200ND200204
1,2,3-Trichloropropane ug/L 200 130 60-140125 4 30200ND259250
1,2,4-Trichlorobenzene ug/L 200 99 60-140102 3 30200ND199205
1,2,4-Trimethylbenzene ug/L 200 114 60-140111 0 3020091511401140
1,2-Dibromo-3-
chloropropane ug/L 200 106 60-140107 1 30200ND212214
1,2-Dibromoethane (EDB)ug/L 200 121 60-140118 2 30200ND241237
1,2-Dichlorobenzene ug/L 200 115 60-140112 3 30200ND229223
1,2-Dichloroethane ug/L M120014160-140135 4 30200ND282270
1,2-Dichloropropane ug/L 200 134 60-140131 3 30200ND268261
1,3,5-Trimethylbenzene ug/L 200 127 60-140124 1 30200155409404
1,3-Dichlorobenzene ug/L 200 114 60-140112 2 30200ND228223
1,3-Dichloropropane ug/L 200 126 60-140121 4 30200ND251242
1,4-Dichlorobenzene ug/L 200 110 60-140107 3 30200ND221214
2,2-Dichloropropane ug/L 200 120 60-140113 5 30200ND239227
2-Chlorotoluene ug/L 200 127 60-140125 1 30200ND253250
4-Chlorotoluene ug/L 200 125 60-140123 1 30200ND250247
Benzene ug/L 200 124 60-140120 3 30200ND248240
Bromobenzene ug/L 200 115 60-140113 2 30200ND230227
Bromochloromethane ug/L 200 130 60-140121 7 30200ND259241
Bromodichloromethane ug/L 200 124 60-140119 4 30200ND247237
Bromoform ug/L 200 102 60-14099 3 30200ND205198
Bromomethane ug/L 200 94 60-140104 10 30200ND188208
Carbon tetrachloride ug/L 200 123 60-140118 4 30200ND246236
Chlorobenzene ug/L 200 122 60-140118 3 30200ND244237
Chloroethane ug/L M120016660-140157 5 30200ND332315
Chloroform ug/L 200 138 60-140126 9 30200ND276252
Chloromethane ug/L 200 132 60-140123 7 30200ND265247
cis-1,2-Dichloroethene ug/L 200 138 60-140135 2 302007.9 283 278
cis-1,3-Dichloropropene ug/L 200 122 60-140118 3 30200ND243236
Dibromochloromethane ug/L 200 111 60-140108 2 30200ND222217
Dibromomethane ug/L 200 113 60-140108 5 30200ND226215
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3880803MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643751007
3880804
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 200 126 60-140117 8 30200ND253233
Diisopropyl ether ug/L 200 131 60-140127 3 30200ND262254
Ethylbenzene ug/L 200 123 60-140116 3 30200208454440
Hexachloro-1,3-butadiene ug/L 200 100 60-140100 0 30200ND200200
Isopropylbenzene
(Cumene)
ug/L 200 118 60-140113 3 3020038.9 274 265
m&p-Xylene ug/L 400 122 60-140117 3 30400184671653
Methyl-tert-butyl ether ug/L 200 124 60-140121 3 30200ND249241
Methylene Chloride ug/L 200 129 60-140119 7 30200ND268248
n-Butylbenzene ug/L 200 139 60-140138 1 30200ND279276
n-Propylbenzene ug/L 200 124 60-140123 1 30200110358356
Naphthalene ug/L 200 106 60-140112 5 3020047.2 260 272
o-Xylene ug/L 200 122 60-140114 4 30200106350335
sec-Butylbenzene ug/L 200 129 60-140127 1 30200ND257254
Styrene ug/L 200 120 60-140116 4 30200ND240231
tert-Butylbenzene ug/L 200 99 60-14097 2 30200ND199194
Tetrachloroethene ug/L 200 106 60-140104 2 30200ND212207
Toluene ug/L 200 124 60-140120 3 302007.9 255 247
trans-1,2-Dichloroethene ug/L 200 139 60-140135 3 30200ND277269
trans-1,3-Dichloropropene ug/L 200 119 60-140115 3 30200ND237231
Trichloroethene ug/L 200 123 60-140117 5 30200ND246235
Trichlorofluoromethane ug/L 200 125 60-140116 7 30200ND250233
Vinyl chloride ug/L 200 135 60-140124 9 30200ND271248
1,2-Dichloroethane-d4 (S)%120 70-130119
4-Bromofluorobenzene (S)%104 70-130102
Toluene-d8 (S)%104 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746393
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92643751001, 92643751002, 92643751006, 92643751011, 92643751013, 92643751014, 92643751016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3881556
Associated Lab Samples:92643751001, 92643751002, 92643751006, 92643751011, 92643751013, 92643751014, 92643751016
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/29/22 10:280.31
1,1,1-Trichloroethane ug/L ND 0.50 12/29/22 10:280.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/29/22 10:280.22
1,1,2-Trichloroethane ug/L ND 0.50 12/29/22 10:280.32
1,1-Dichloroethane ug/L ND 0.50 12/29/22 10:280.37
1,1-Dichloroethene ug/L ND 0.50 12/29/22 10:280.35
1,1-Dichloropropene ug/L ND 0.50 12/29/22 10:280.43
1,2,3-Trichlorobenzene ug/L ND 2.0 12/29/22 10:280.81
1,2,3-Trichloropropane ug/L ND 0.50 12/29/22 10:280.26
1,2,4-Trichlorobenzene ug/L ND 2.0 12/29/22 10:280.64
1,2,4-Trimethylbenzene ug/L ND 0.50 12/29/22 10:280.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/29/22 10:280.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/29/22 10:280.27
1,2-Dichlorobenzene ug/L ND 0.50 12/29/22 10:280.34
1,2-Dichloroethane ug/L ND 0.50 12/29/22 10:280.32
1,2-Dichloropropane ug/L ND 0.50 12/29/22 10:280.36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/29/22 10:280.33
1,3-Dichlorobenzene ug/L ND 0.50 12/29/22 10:280.34
1,3-Dichloropropane ug/L ND 0.50 12/29/22 10:280.28
1,4-Dichlorobenzene ug/L ND 0.50 12/29/22 10:280.33
2,2-Dichloropropane ug/L ND 0.50 12/29/22 10:280.39
2-Chlorotoluene ug/L ND 0.50 12/29/22 10:280.32
4-Chlorotoluene ug/L ND 0.50 12/29/22 10:280.32
Benzene ug/L ND 0.50 12/29/22 10:280.34
Bromobenzene ug/L ND 0.50 12/29/22 10:280.29
Bromochloromethane ug/L ND 0.50 12/29/22 10:280.47
Bromodichloromethane ug/L ND 0.50 12/29/22 10:280.31
Bromoform ug/L ND 0.50 12/29/22 10:280.34
Bromomethane ug/L ND 5.0 12/29/22 10:281.7
Carbon tetrachloride ug/L ND 0.50 12/29/22 10:280.33
Chlorobenzene ug/L ND 0.50 12/29/22 10:280.28
Chloroethane ug/L ND 1.0 12/29/22 10:280.65
Chloroform ug/L ND 0.50 12/29/22 10:280.43
Chloromethane ug/L ND 1.0 12/29/22 10:280.54
cis-1,2-Dichloroethene ug/L ND 0.50 12/29/22 10:280.38
cis-1,3-Dichloropropene ug/L ND 0.50 12/29/22 10:280.36
Dibromochloromethane ug/L ND 0.50 12/29/22 10:280.36
Dibromomethane ug/L ND 0.50 12/29/22 10:280.39
Dichlorodifluoromethane ug/L ND 0.50 12/29/22 10:280.35
Diisopropyl ether ug/L ND 0.50 12/29/22 10:280.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3881556
Associated Lab Samples:92643751001, 92643751002, 92643751006, 92643751011, 92643751013, 92643751014, 92643751016
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 12/29/22 10:280.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/29/22 10:281.5
Isopropylbenzene (Cumene)ug/L ND 0.50 12/29/22 10:280.33
m&p-Xylene ug/L ND 1.0 12/29/22 10:280.71
Methyl-tert-butyl ether ug/L ND 0.50 12/29/22 10:280.42
Methylene Chloride ug/L ND 2.0 12/29/22 10:282.0
n-Butylbenzene ug/L ND 0.50 12/29/22 10:280.49
n-Propylbenzene ug/L ND 0.50 12/29/22 10:280.34
Naphthalene ug/L ND 2.0 12/29/22 10:280.64
o-Xylene ug/L ND 0.50 12/29/22 10:280.34
sec-Butylbenzene ug/L ND 0.50 12/29/22 10:280.40
Styrene ug/L ND 0.50 12/29/22 10:280.29
tert-Butylbenzene ug/L ND 0.50 12/29/22 10:280.32
Tetrachloroethene ug/L ND 0.50 12/29/22 10:280.29
Toluene ug/L ND 0.50 12/29/22 10:280.24
trans-1,2-Dichloroethene ug/L ND 0.50 12/29/22 10:280.40
trans-1,3-Dichloropropene ug/L ND 0.50 12/29/22 10:280.36
Trichloroethene ug/L ND 0.50 12/29/22 10:280.38
Trichlorofluoromethane ug/L ND 1.0 12/29/22 10:280.30
Vinyl chloride ug/L ND 1.0 12/29/22 10:280.39
1,2-Dichloroethane-d4 (S)%118 70-130 12/29/22 10:28
4-Bromofluorobenzene (S)%103 70-130 12/29/22 10:28
Toluene-d8 (S)%106 70-130 12/29/22 10:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3881557LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.150 108 60-140
1,1,1-Trichloroethane ug/L 57.250 114 60-140
1,1,2,2-Tetrachloroethane ug/L 56.050 112 60-140
1,1,2-Trichloroethane ug/L 55.650 111 60-140
1,1-Dichloroethane ug/L 57.450 115 60-140
1,1-Dichloroethene ug/L 57.950 116 60-140
1,1-Dichloropropene ug/L 63.150 126 60-140
1,2,3-Trichlorobenzene ug/L 53.050 106 60-140
1,2,3-Trichloropropane ug/L 56.950 114 60-140
1,2,4-Trichlorobenzene ug/L 52.450 105 60-140
1,2,4-Trimethylbenzene ug/L 56.550 113 60-140
1,2-Dibromo-3-chloropropane ug/L 50.650 101 60-140
1,2-Dibromoethane (EDB)ug/L 54.850 110 60-140
1,2-Dichlorobenzene ug/L 53.050 106 60-140
1,2-Dichloroethane ug/L 62.150 124 60-140
1,2-Dichloropropane ug/L 58.750 117 60-140
1,3,5-Trimethylbenzene ug/L 57.450 115 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3881557LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 53.250 106 60-140
1,3-Dichloropropane ug/L 57.750 115 60-140
1,4-Dichlorobenzene ug/L 51.850 104 60-140
2,2-Dichloropropane ug/L 57.950 116 60-140
2-Chlorotoluene ug/L 56.350 113 60-140
4-Chlorotoluene ug/L 56.850 114 60-140
Benzene ug/L 51.050 102 60-140
Bromobenzene ug/L 52.550 105 60-140
Bromochloromethane ug/L 54.150 108 60-140
Bromodichloromethane ug/L 54.350 109 60-140
Bromoform ug/L 48.250 96 60-140
Bromomethane ug/L 50.350 101 60-140
Carbon tetrachloride ug/L 50.850 102 60-140
Chlorobenzene ug/L 53.050 106 60-140
Chloroethane ug/L 62.550 125 60-140
Chloroform ug/L 56.050 112 60-140
Chloromethane ug/L 51.250 102 60-140
cis-1,2-Dichloroethene ug/L 59.150 118 60-140
cis-1,3-Dichloropropene ug/L 57.850 116 60-140
Dibromochloromethane ug/L 52.550 105 60-140
Dibromomethane ug/L 48.850 98 60-140
Dichlorodifluoromethane ug/L 46.250 92 60-140
Diisopropyl ether ug/L 60.750 121 60-140
Ethylbenzene ug/L 53.650 107 60-140
Hexachloro-1,3-butadiene ug/L 54.250 108 60-140
Isopropylbenzene (Cumene)ug/L 52.050 104 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 58.650 117 60-140
Methylene Chloride ug/L 51.250 102 60-140
n-Butylbenzene ug/L 61.950 124 60-140
n-Propylbenzene ug/L 57.450 115 60-140
Naphthalene ug/L 55.250 110 60-140
o-Xylene ug/L 52.550 105 60-140
sec-Butylbenzene ug/L 58.050 116 60-140
Styrene ug/L 53.250 106 60-140
tert-Butylbenzene ug/L 44.650 89 60-140
Tetrachloroethene ug/L 47.350 95 60-140
Toluene ug/L 51.450 103 60-140
trans-1,2-Dichloroethene ug/L 59.050 118 60-140
trans-1,3-Dichloropropene ug/L 56.750 113 60-140
Trichloroethene ug/L 53.350 107 60-140
Trichlorofluoromethane ug/L 49.950 100 60-140
Vinyl chloride ug/L 50.950 102 60-140
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3881558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643751006
3881559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 138 60-140132 4 30100ND138132
1,1,1-Trichloroethane ug/L M110015760-140148 6 30100ND157148
1,1,2,2-Tetrachloroethane ug/L M110014260-140134 6 30100ND142134
1,1,2-Trichloroethane ug/L M110014360-140134 6 30100ND143134
1,1-Dichloroethane ug/L M110015960-140153 4 30100ND159153
1,1-Dichloroethene ug/L M110016660-140162 3 30100ND166162
1,1-Dichloropropene ug/L M110016860-140163 3 30100ND168163
1,2,3-Trichlorobenzene ug/L 100 125 60-140122 3 30100ND125122
1,2,3-Trichloropropane ug/L M110014360-140137 4 30100ND143137
1,2,4-Trichlorobenzene ug/L 100 127 60-140122 3 30100ND127122
1,2,4-Trimethylbenzene ug/L E,M110021960-140214 1 3010081410301030
1,2-Dibromo-3-
chloropropane ug/L 100 122 60-140116 5 30100ND122116
1,2-Dibromoethane (EDB)ug/L M110014160-140133 6 30100ND141133
1,2-Dichlorobenzene ug/L 100 133 60-140131 2 30100ND133131
1,2-Dichloroethane ug/L M110016360-140153 6 30100ND163153
1,2-Dichloropropane ug/L M110015760-140150 4 30100ND159152
1,3,5-Trimethylbenzene ug/L M110017660-140172 1 30100184359355
1,3-Dichlorobenzene ug/L 100 133 60-140131 1 30100ND134133
1,3-Dichloropropane ug/L M110015060-140140 7 30100ND150140
1,4-Dichlorobenzene ug/L 100 130 60-140128 2 30100ND130128
2,2-Dichloropropane ug/L M110014760-140141 4 30100ND149143
2-Chlorotoluene ug/L M110016360-140148 10 30100ND163148
4-Chlorotoluene ug/L M110014760-140146 1 30100ND147146
Benzene ug/L M110014160-140136 4 301003.7 145 140
Bromobenzene ug/L 100 133 60-140131 1 30100ND133131
Bromochloromethane ug/L M110014660-140141 3 30100ND146141
Bromodichloromethane ug/L M110014160-140136 4 30100ND141136
Bromoform ug/L 100 114 60-140111 3 30100ND114111
Bromomethane ug/L 100 93 60-140113 19 30100ND95.2 115
Carbon tetrachloride ug/L 100 135 60-140136 1 30100ND135136
Chlorobenzene ug/L 100 139 60-140137 1 30100ND139137
Chloroethane ug/L M110017560-140170 3 30100ND177173
Chloroform ug/L M110015360-140148 3 30100ND153148
Chloromethane ug/L M110014160-140138 2 30100ND141138
cis-1,2-Dichloroethene ug/L M110016060-140152 5 301002.1J 162 154
cis-1,3-Dichloropropene ug/L M110014660-140138 5 30100ND147139
Dibromochloromethane ug/L 100 130 60-140124 5 30100ND130124
Dibromomethane ug/L 100 125 60-140120 4 30100ND125120
Dichlorodifluoromethane ug/L 100 127 60-140125 2 30100ND127125
Diisopropyl ether ug/L M110016360-140150 8 30100ND163150
Ethylbenzene ug/L M110016160-140159 1 30100137299296
Hexachloro-1,3-butadiene ug/L 100 136 60-140132 3 30100ND136132
Isopropylbenzene(Cumene)ug/L 100 138 60-140136 1 3010039.1 177 175
m&p-Xylene ug/L M120017960-140165 5 30200250609579
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3881558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643751006
3881559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L M110015260-140139 9 30100ND152139
Methylene Chloride ug/L 100 138 60-140133 3 3010019.3 157 153
n-Butylbenzene ug/L M110018260-140175 4 30100ND182175
n-Propylbenzene ug/L M110015860-140156 1 30100122280278
Naphthalene ug/L M110018160-140138 23 3010030.4 212 169
o-Xylene ug/L M110016860-140154 5 30100112280266
sec-Butylbenzene ug/L M110015960-140154 3 30100ND159154
Styrene ug/L 100 134 60-140132 2 301001.8J 136 133
tert-Butylbenzene ug/L 100 118 60-140117 1 30100ND118117
Tetrachloroethene ug/L 100 124 60-140121 2 30100ND124121
Toluene ug/L M110017760-140151 15 3010011.9 189 163
trans-1,2-Dichloroethene ug/L M110016460-140156 5 30100ND164156
trans-1,3-Dichloropropene ug/L M110014260-140137 3 30100ND142137
Trichloroethene ug/L M110014260-140137 3 30100ND142137
Trichlorofluoromethane ug/L 100 135 60-140133 1 30100ND135133
Vinyl chloride ug/L M110014860-140145 3 30100ND148145
1,2-Dichloroethane-d4 (S)%123 70-130122
4-Bromofluorobenzene (S)%103 70-130104
Toluene-d8 (S)%103 70-130103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746671
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92643751015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3882614
Associated Lab Samples:92643751015
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/30/22 12:060.31
1,1,1-Trichloroethane ug/L ND 0.50 12/30/22 12:060.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/30/22 12:060.22
1,1,2-Trichloroethane ug/L ND 0.50 12/30/22 12:060.32
1,1-Dichloroethane ug/L ND 0.50 12/30/22 12:060.37
1,1-Dichloroethene ug/L ND 0.50 12/30/22 12:060.35
1,1-Dichloropropene ug/L ND 0.50 12/30/22 12:060.43
1,2,3-Trichlorobenzene ug/L ND 2.0 12/30/22 12:060.81
1,2,3-Trichloropropane ug/L ND 0.50 12/30/22 12:060.26
1,2,4-Trichlorobenzene ug/L ND 2.0 12/30/22 12:060.64
1,2,4-Trimethylbenzene ug/L ND 0.50 12/30/22 12:060.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/30/22 12:060.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/30/22 12:060.27
1,2-Dichlorobenzene ug/L ND 0.50 12/30/22 12:060.34
1,2-Dichloroethane ug/L ND 0.50 12/30/22 12:060.32
1,2-Dichloropropane ug/L ND 0.50 12/30/22 12:060.36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/30/22 12:060.33
1,3-Dichlorobenzene ug/L ND 0.50 12/30/22 12:060.34
1,3-Dichloropropane ug/L ND 0.50 12/30/22 12:060.28
1,4-Dichlorobenzene ug/L ND 0.50 12/30/22 12:060.33
2,2-Dichloropropane ug/L ND 0.50 12/30/22 12:060.39
2-Chlorotoluene ug/L ND 0.50 12/30/22 12:060.32
4-Chlorotoluene ug/L ND 0.50 12/30/22 12:060.32
Benzene ug/L ND 0.50 12/30/22 12:060.34
Bromobenzene ug/L ND 0.50 12/30/22 12:060.29
Bromochloromethane ug/L ND 0.50 12/30/22 12:060.47
Bromodichloromethane ug/L ND 0.50 12/30/22 12:060.31
Bromoform ug/L ND 0.50 12/30/22 12:060.34
Bromomethane ug/L ND 5.0 12/30/22 12:061.7
Carbon tetrachloride ug/L ND 0.50 12/30/22 12:060.33
Chlorobenzene ug/L ND 0.50 12/30/22 12:060.28
Chloroethane ug/L ND 1.0 12/30/22 12:060.65
Chloroform ug/L ND 0.50 12/30/22 12:060.43
Chloromethane ug/L ND 1.0 12/30/22 12:060.54
cis-1,2-Dichloroethene ug/L ND 0.50 12/30/22 12:060.38
cis-1,3-Dichloropropene ug/L ND 0.50 12/30/22 12:060.36
Dibromochloromethane ug/L ND 0.50 12/30/22 12:060.36
Dibromomethane ug/L ND 0.50 12/30/22 12:060.39
Dichlorodifluoromethane ug/L ND 0.50 12/30/22 12:060.35
Diisopropyl ether ug/L ND 0.50 12/30/22 12:060.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3882614
Associated Lab Samples:92643751015
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 12/30/22 12:060.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/30/22 12:061.5
Isopropylbenzene (Cumene)ug/L ND 0.50 12/30/22 12:060.33
m&p-Xylene ug/L ND 1.0 12/30/22 12:060.71
Methyl-tert-butyl ether ug/L ND 0.50 12/30/22 12:060.42
Methylene Chloride ug/L ND 2.0 12/30/22 12:062.0
n-Butylbenzene ug/L ND 0.50 12/30/22 12:060.49
n-Propylbenzene ug/L ND 0.50 12/30/22 12:060.34
Naphthalene ug/L ND 2.0 12/30/22 12:060.64
o-Xylene ug/L ND 0.50 12/30/22 12:060.34
sec-Butylbenzene ug/L ND 0.50 12/30/22 12:060.40
Styrene ug/L ND 0.50 12/30/22 12:060.29
tert-Butylbenzene ug/L ND 0.50 12/30/22 12:060.32
Tetrachloroethene ug/L ND 0.50 12/30/22 12:060.29
Toluene ug/L ND 0.50 12/30/22 12:060.24
trans-1,2-Dichloroethene ug/L ND 0.50 12/30/22 12:060.40
trans-1,3-Dichloropropene ug/L ND 0.50 12/30/22 12:060.36
Trichloroethene ug/L ND 0.50 12/30/22 12:060.38
Trichlorofluoromethane ug/L ND 1.0 12/30/22 12:060.30
Vinyl chloride ug/L ND 1.0 12/30/22 12:060.39
1,2-Dichloroethane-d4 (S)%87 70-130 12/30/22 12:06
4-Bromofluorobenzene (S)%96 70-130 12/30/22 12:06
Toluene-d8 (S)%105 70-130 12/30/22 12:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3882615LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.150 116 60-140
1,1,1-Trichloroethane ug/L 55.450 111 60-140
1,1,2,2-Tetrachloroethane ug/L 54.650 109 60-140
1,1,2-Trichloroethane ug/L 56.650 113 60-140
1,1-Dichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethene ug/L 51.650 103 60-140
1,1-Dichloropropene ug/L 59.750 119 60-140
1,2,3-Trichlorobenzene ug/L 57.550 115 60-140
1,2,3-Trichloropropane ug/L 49.950 100 60-140
1,2,4-Trichlorobenzene ug/L 56.350 113 60-140
1,2,4-Trimethylbenzene ug/L 54.750 109 60-140
1,2-Dibromo-3-chloropropane ug/L 59.350 119 60-140
1,2-Dibromoethane (EDB)ug/L 59.250 118 60-140
1,2-Dichlorobenzene ug/L 57.750 115 60-140
1,2-Dichloroethane ug/L 50.150 100 60-140
1,2-Dichloropropane ug/L 58.850 118 60-140
1,3,5-Trimethylbenzene ug/L 56.650 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3882615LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 59.950 120 60-140
1,3-Dichloropropane ug/L 55.050 110 60-140
1,4-Dichlorobenzene ug/L 55.550 111 60-140
2,2-Dichloropropane ug/L 54.650 109 60-140
2-Chlorotoluene ug/L 55.950 112 60-140
4-Chlorotoluene ug/L 56.850 114 60-140
Benzene ug/L 52.350 105 60-140
Bromobenzene ug/L 58.750 117 60-140
Bromochloromethane ug/L 57.450 115 60-140
Bromodichloromethane ug/L 53.350 107 60-140
Bromoform ug/L 57.750 115 60-140
Bromomethane ug/L 32.950 66 60-140
Carbon tetrachloride ug/L 53.850 108 60-140
Chlorobenzene ug/L 56.150 112 60-140
Chloroethane ug/L 33.250 66 60-140
Chloroform ug/L 47.550 95 60-140
Chloromethane ug/L 53.950 108 60-140
cis-1,2-Dichloroethene ug/L 53.150 106 60-140
cis-1,3-Dichloropropene ug/L 57.850 116 60-140
Dibromochloromethane ug/L 51.650 103 60-140
Dibromomethane ug/L 59.850 120 60-140
Dichlorodifluoromethane ug/L 44.350 89 60-140
Diisopropyl ether ug/L 56.650 113 60-140
Ethylbenzene ug/L 53.550 107 60-140
Hexachloro-1,3-butadiene ug/L 57.650 115 60-140
Isopropylbenzene (Cumene)ug/L 54.750 109 60-140
m&p-Xylene ug/L 108100 108 60-140
Methyl-tert-butyl ether ug/L 47.250 94 60-140
Methylene Chloride ug/L 47.250 94 60-140
n-Butylbenzene ug/L 58.650 117 60-140
n-Propylbenzene ug/L 56.850 114 60-140
Naphthalene ug/L 57.150 114 60-140
o-Xylene ug/L 57.050 114 60-140
sec-Butylbenzene ug/L 55.150 110 60-140
Styrene ug/L 57.650 115 60-140
tert-Butylbenzene ug/L 47.350 95 60-140
Tetrachloroethene ug/L 58.950 118 60-140
Toluene ug/L 52.550 105 60-140
trans-1,2-Dichloroethene ug/L 53.550 107 60-140
trans-1,3-Dichloropropene ug/L 55.250 110 60-140
Trichloroethene ug/L 61.150 122 60-140
Trichlorofluoromethane ug/L 39.050 78 60-140
Vinyl chloride ug/L 48.650 97 60-140
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%92 70-130
Toluene-d8 (S)%94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3882616MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644079004
3882617
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 8000 122 60-140127 4 308000ND976010100
1,1,1-Trichloroethane ug/L 8000 116 60-140121 4 308000ND93209690
1,1,2,2-Tetrachloroethane ug/L 8000 113 60-140111 2 308000ND90708860
1,1,2-Trichloroethane ug/L 8000 122 60-140120 2 308000ND98009630
1,1-Dichloroethane ug/L 8000 108 60-140108 0 308000ND86808670
1,1-Dichloroethene ug/L 8000 119 60-140117 1 308000ND94909360
1,1-Dichloropropene ug/L 8000 126 60-140131 4 308000ND1010010500
1,2,3-Trichlorobenzene ug/L 8000 110 60-140127 15 308000ND878010200
1,2,3-Trichloropropane ug/L 8000 91 60-140102 11 308000ND72908130
1,2,4-Trichlorobenzene ug/L 8000 111 60-140116 4 308000ND88909270
1,2,4-Trimethylbenzene ug/L 8000 103 60-140108 3 30800030901140011700
1,2-Dibromo-3-
chloropropane ug/L 8000 113 60-140117 3 308000ND90709340
1,2-Dibromoethane (EDB)ug/L 8000 119 60-140124 4 308000ND95309920
1,2-Dichlorobenzene ug/L 8000 119 60-140124 4 308000ND95509950
1,2-Dichloroethane ug/L 8000 100 60-14099 1 308000ND80307930
1,2-Dichloropropane ug/L 8000 124 60-140126 2 308000ND995010100
1,3,5-Trimethylbenzene ug/L 8000 123 60-140129 5 308000ND982010400
1,3-Dichlorobenzene ug/L 8000 121 60-140128 5 308000ND970010200
1,3-Dichloropropane ug/L 8000 110 60-140115 5 308000ND88109230
1,4-Dichlorobenzene ug/L 8000 113 60-140118 4 308000ND90609470
2,2-Dichloropropane ug/L 8000 119 60-140119 0 308000ND95509530
2-Chlorotoluene ug/L 8000 117 60-140117 0 308000ND93909360
4-Chlorotoluene ug/L 8000 115 60-140121 5 308000ND91709660
Benzene ug/L M1800013160-140158 8 308000146002510027200
Bromobenzene ug/L 8000 118 60-140129 9 308000ND946010400
Bromochloromethane ug/L 8000 123 60-140128 4 308000ND983010200
Bromodichloromethane ug/L 8000 110 60-140112 2 308000ND88208990
Bromoform ug/L 8000 116 60-140119 2 308000ND93209530
Bromomethane ug/L 8000 71 60-14083 15 308000ND56806640
Carbon tetrachloride ug/L 8000 122 60-140123 0 308000ND97909830
Chlorobenzene ug/L 8000 120 60-140124 4 308000ND95609910
Chloroethane ug/L 8000 90 60-14094 5 308000ND72007540
Chloroform ug/L 8000 106 60-140104 1 308000ND85808470
Chloromethane ug/L 8000 110 60-140111 1 308000ND87808890
cis-1,2-Dichloroethene ug/L 8000 111 60-140112 1 308000ND88508930
cis-1,3-Dichloropropene ug/L 8000 122 60-140122 0 308000ND97609790
Dibromochloromethane ug/L 8000 105 60-140110 5 308000ND83808830
Dibromomethane ug/L 8000 130 60-140132 1 308000ND1040010500
Dichlorodifluoromethane ug/L 8000 96 60-14099 3 308000ND76407890
Diisopropyl ether ug/L 8000 107 60-140120 9 30800026501120012200
Ethylbenzene ug/L 8000 113 60-140123 6 30800029501200012800
Hexachloro-1,3-butadiene ug/L 8000 127 60-140131 4 308000ND1010010500
Isopropylbenzene(Cumene)ug/L 8000 120 60-140123 2 308000ND96209830
m&p-Xylene ug/L 16000 105 60-140120 8 3016000124002920031700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3882616MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92644079004
3882617
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 8000 87 60-14095 8 30800055075108120
Methylene Chloride ug/L 8000 96 60-14096 0 30800094886708640
n-Butylbenzene ug/L 8000 118 60-140125 6 308000ND943010000
n-Propylbenzene ug/L 8000 121 60-140128 5 308000ND970010200
Naphthalene ug/L 8000 84 60-14098 12 308000212088709970
o-Xylene ug/L 8000 113 60-140126 7 30800060501510016200
sec-Butylbenzene ug/L 8000 118 60-140122 3 308000ND94609730
Styrene ug/L 8000 121 60-140124 3 308000ND96509930
tert-Butylbenzene ug/L 8000 100 60-140103 3 308000ND79908260
Tetrachloroethene ug/L 8000 126 60-140129 2 308000ND1010010300
Toluene ug/L M180008460-140153 11 308000420004870054200
trans-1,2-Dichloroethene ug/L 8000 113 60-140117 4 308000ND90409380
trans-1,3-Dichloropropene ug/L 8000 114 60-140115 1 308000ND91409200
Trichloroethene ug/L 8000 135 60-140134 1 308000ND1080010700
Trichlorofluoromethane ug/L 8000 93 60-14094 1 308000ND74107520
Vinyl chloride ug/L 8000 104 60-140107 3 308000ND82908560
1,2-Dichloroethane-d4 (S)%83 70-13083
4-Bromofluorobenzene (S)%95 70-13096
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 52
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 52
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92643751
CROWN FOOD MART 12/20/22
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92643751001 746393MW-4 SM 6200B
92643751002 746393MW-5 SM 6200B
92643751003 746186MW-8 SM 6200B
92643751004 746186MW-9 SM 6200B
92643751005 746186MW-11 SM 6200B
92643751006 746393MW-13 SM 6200B
92643751007 746186MW-14 SM 6200B
92643751008 746186MW-15 SM 6200B
92643751009 746186MW-17 SM 6200B
92643751010 746186MW-18 SM 6200B
92643751011 746393EW-2 SM 6200B
92643751012 746186EW-3 SM 6200B
92643751013 746393EW-4 SM 6200B
92643751014 746393EW-5 SM 6200B
92643751015 746671DUP-2 SM 6200B
92643751016 746393TRIPSM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/30/2022 03:46 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 52
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