AS-4331_41488_CA_LAB_20221219

#=CL#
December 28, 2022
LIMS USE: FR - ROBERT MARTIN
LIMS OBJECT ID: 92643625
92643625
Project:
Pace Project No.:
RE:
Mr. Robert Martin
Martin and Slagle
24 Lookout Terrace
Black Mountain, NC 28711
CROWN FOOD MART
Dear Mr. Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Lab ID Sample ID Matrix Date Collected Date Received
92643625001 SW-01-192 Water 12/19/22 16:19 12/20/22 15:40
92643625002 SW-02-192 Water 12/19/22 14:10 12/20/22 15:40
92643625003 SW-03-192 Water 12/19/22 14:30 12/20/22 15:40
92643625004 SW-11 Water 12/19/22 16:35 12/20/22 15:40
92643625005 SW-12 Water 12/19/22 17:10 12/20/22 15:40
92643625006 SW-13 Water 12/19/22 17:02 12/20/22 15:40
92643625007 SW-14 Water 12/19/22 16:26 12/20/22 15:40
92643625008 DUP-3 Water 12/19/22 00:00 12/20/22 15:40
92643625009 MW-2 Water 12/19/22 17:07 12/20/22 15:40
92643625010 MW-16 Water 12/19/22 13:01 12/20/22 15:40
92643625011 DUP-1 Water 12/19/22 00:00 12/20/22 15:40
92643625012 MW-10 Water 12/19/22 12:07 12/20/22 15:40
92643625013 MW-12 Water 12/19/22 10:17 12/20/22 15:40
92643625014 MW-6 Water 12/19/22 15:10 12/20/22 15:40
92643625015 MW-7 Water 12/19/22 15:07 12/20/22 15:40
92643625016 MW-1 Water 12/19/22 11:20 12/20/22 15:40
92643625017 MW-3 Water 12/19/22 17:12 12/20/22 15:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92643625001 SW-01-192 SM 6200B 63 PASI-CSAS
92643625002 SW-02-192 SM 6200B 63 PASI-CSAS
92643625003 SW-03-192 SM 6200B 63 PASI-CSAS
92643625004 SW-11 SM 6200B 63 PASI-CSAS
92643625005 SW-12 SM 6200B 63 PASI-CSAS
92643625006 SW-13 SM 6200B 63 PASI-CSAS
92643625007 SW-14 SM 6200B 63 PASI-CSAS
92643625008 DUP-3 SM 6200B 63 PASI-CSAS
92643625009 MW-2 SM 6200B 63 PASI-CSAS
92643625010 MW-16 SM 6200B 63 PASI-CSAS
92643625011 DUP-1 SM 6200B 63 PASI-CSAS
92643625012 MW-10 SM 6200B 63 PASI-CSAS
92643625013 MW-12 SM 6200B 63 PASI-CSAS
92643625014 MW-6 SM 6200B 63 PASI-CSAS
92643625015 MW-7 SM 6200B 63 PASI-CSAS
92643625016 MW-1 SM 6200B 63 PASI-CSAS
92643625017 MW-3 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-01-192 Lab ID:92643625001 Collected:12/19/22 16:19 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 14:22 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 14:22 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 14:22 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 14:22 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 14:22 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 14:22 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 14:22 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 14:22 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 14:22 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 14:22 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 14:22 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 14:22 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 14:22 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 14:22 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 14:22 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 14:22 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 14:22 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 14:22 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 14:22 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 14:22 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 14:22 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 14:22 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 14:22 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 14:22 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 14:22 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 14:22 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 14:22 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 14:22 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 14:22 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 14:22 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 14:22 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 14:22 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 14:22 563-58-6 M10.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 14:22 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 14:22 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 14:22 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 14:22 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 14:22 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 14:22 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 14:22 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 14:22 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 14:22 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 14:22 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 14:22 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 14:22 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-01-192 Lab ID:92643625001 Collected:12/19/22 16:19 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 14:22 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 14:22 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 14:22 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 14:22 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 14:22 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 14:22 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 14:22 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 14:22 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 14:22 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 14:22 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 14:22 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 14:22 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 14:22 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 14:22 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 14:22 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %12/23/22 14:22 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %12/23/22 14:22 460-00-470-130 1
Toluene-d8 (S)106 %12/23/22 14:22 2037-26-570-130 1
Sample:SW-02-192 Lab ID:92643625002 Collected:12/19/22 14:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/28/22 12:02 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/28/22 12:02 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/28/22 12:02 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/28/22 12:02 75-27-40.50 0.31 1
Bromoform ND ug/L 12/28/22 12:02 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/28/22 12:02 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/28/22 12:02 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/28/22 12:02 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/28/22 12:02 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/28/22 12:02 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/28/22 12:02 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/28/22 12:02 75-00-31.0 0.65 1
Chloroform ND ug/L 12/28/22 12:02 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/28/22 12:02 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/28/22 12:02 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/28/22 12:02 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/28/22 12:02 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-02-192 Lab ID:92643625002 Collected:12/19/22 14:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/28/22 12:02 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/28/22 12:02 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/28/22 12:02 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/28/22 12:02 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/28/22 12:02 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/28/22 12:02 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/28/22 12:02 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/28/22 12:02 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/28/22 12:02 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/28/22 12:02 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/28/22 12:02 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/28/22 12:02 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/28/22 12:02 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/28/22 12:02 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/28/22 12:02 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/28/22 12:02 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/28/22 12:02 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/28/22 12:02 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/28/22 12:02 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/28/22 12:02 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/28/22 12:02 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/28/22 12:02 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/28/22 12:02 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/28/22 12:02 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/28/22 12:02 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/28/22 12:02 103-65-10.50 0.34 1
Styrene ND ug/L 12/28/22 12:02 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/28/22 12:02 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/28/22 12:02 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/28/22 12:02 127-18-40.50 0.29 1
Toluene ND ug/L 12/28/22 12:02 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/28/22 12:02 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/28/22 12:02 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/28/22 12:02 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/28/22 12:02 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/28/22 12:02 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/28/22 12:02 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/28/22 12:02 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/28/22 12:02 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/28/22 12:02 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/28/22 12:02 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/28/22 12:02 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/28/22 12:02 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %12/28/22 12:02 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-02-192 Lab ID:92643625002 Collected:12/19/22 14:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)103 %12/28/22 12:02 460-00-470-130 1
Toluene-d8 (S)105 %12/28/22 12:02 2037-26-570-130 1
Sample:SW-03-192 Lab ID:92643625003 Collected:12/19/22 14:30 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 14:40 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 14:40 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 14:40 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 14:40 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 14:40 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 14:40 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 14:40 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 14:40 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 14:40 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 14:40 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 14:40 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 14:40 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 14:40 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 14:40 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 14:40 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 14:40 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 14:40 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 14:40 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 14:40 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 14:40 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 14:40 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 14:40 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 14:40 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 14:40 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 14:40 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 14:40 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 14:40 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 14:40 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 14:40 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 14:40 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 14:40 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 14:40 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 14:40 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-03-192 Lab ID:92643625003 Collected:12/19/22 14:30 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/23/22 14:40 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 14:40 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 14:40 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 14:40 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 14:40 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 14:40 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 14:40 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 14:40 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 14:40 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 14:40 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 14:40 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 14:40 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 14:40 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 14:40 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 14:40 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 14:40 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 14:40 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 14:40 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 14:40 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 14:40 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 14:40 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 14:40 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 14:40 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 14:40 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 14:40 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 14:40 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 14:40 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %12/23/22 14:40 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %12/23/22 14:40 460-00-470-130 1
Toluene-d8 (S)106 %12/23/22 14:40 2037-26-570-130 1
Sample:SW-11 Lab ID:92643625004 Collected:12/19/22 16:35 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.81 ug/L 12/23/22 14:58 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 14:58 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 14:58 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 14:58 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 14:58 75-25-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-11 Lab ID:92643625004 Collected:12/19/22 16:35 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/23/22 14:58 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 14:58 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 14:58 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 14:58 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 14:58 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 14:58 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 14:58 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 14:58 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 14:58 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 14:58 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 14:58 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 14:58 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 14:58 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 14:58 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 14:58 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 14:58 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 14:58 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 14:58 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 14:58 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 14:58 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 14:58 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 14:58 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 14:58 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 14:58 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 14:58 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 14:58 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 14:58 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 14:58 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 14:58 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 14:58 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 14:58 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 14:58 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 14:58 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 14:58 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 14:58 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 14:58 1634-04-40.50 0.42 1
Naphthalene 9.0 ug/L 12/23/22 14:58 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 14:58 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 14:58 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 14:58 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 14:58 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 14:58 127-18-40.50 0.29 1
Toluene 0.30J ug/L 12/23/22 14:58 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 14:58 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 14:58 120-82-12.0 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-11 Lab ID:92643625004 Collected:12/19/22 16:35 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/23/22 14:58 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 14:58 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 14:58 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 14:58 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 14:58 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 14:58 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 102 ug/L 12/23/22 14:58 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 14:58 75-01-41.0 0.39 1
m&p-Xylene 2.2 ug/L 12/23/22 14:58 179601-23-11.0 0.71 1
o-Xylene 24.1 ug/L 12/23/22 14:58 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %12/23/22 14:58 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/23/22 14:58 460-00-470-130 1
Toluene-d8 (S)99 %12/23/22 14:58 2037-26-570-130 1
Sample:SW-12 Lab ID:92643625005 Collected:12/19/22 17:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 2.2 ug/L 12/28/22 12:37 71-43-21.2 0.86 2.5
Bromobenzene ND ug/L 12/28/22 12:37 108-86-11.2 0.72 2.5
Bromochloromethane ND ug/L 12/28/22 12:37 74-97-51.2 1.2 2.5
Bromodichloromethane ND ug/L 12/28/22 12:37 75-27-41.2 0.77 2.5
Bromoform ND ug/L 12/28/22 12:37 75-25-21.2 0.85 2.5
Bromomethane ND ug/L 12/28/22 12:37 74-83-912.5 4.2 2.5
n-Butylbenzene ND ug/L 12/28/22 12:37 104-51-81.2 1.2 2.5
sec-Butylbenzene ND ug/L 12/28/22 12:37 135-98-81.2 1.0 2.5
tert-Butylbenzene ND ug/L 12/28/22 12:37 98-06-61.2 0.81 2.5
Carbon tetrachloride ND ug/L 12/28/22 12:37 56-23-51.2 0.83 2.5
Chlorobenzene ND ug/L 12/28/22 12:37 108-90-71.2 0.71 2.5
Chloroethane ND ug/L 12/28/22 12:37 75-00-32.5 1.6 2.5
Chloroform ND ug/L 12/28/22 12:37 67-66-31.2 1.1 2.5
Chloromethane ND ug/L 12/28/22 12:37 74-87-32.5 1.4 2.5
2-Chlorotoluene ND ug/L 12/28/22 12:37 95-49-81.2 0.80 2.5
4-Chlorotoluene ND ug/L 12/28/22 12:37 106-43-41.2 0.81 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/28/22 12:37 96-12-82.5 0.85 2.5
Dibromochloromethane ND ug/L 12/28/22 12:37 124-48-11.2 0.90 2.5
1,2-Dibromoethane (EDB)ND ug/L 12/28/22 12:37 106-93-41.2 0.68 2.5
Dibromomethane ND ug/L 12/28/22 12:37 74-95-31.2 0.98 2.5
1,2-Dichlorobenzene ND ug/L 12/28/22 12:37 95-50-11.2 0.85 2.5
1,3-Dichlorobenzene ND ug/L 12/28/22 12:37 541-73-11.2 0.85 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-12 Lab ID:92643625005 Collected:12/19/22 17:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/28/22 12:37 106-46-71.2 0.83 2.5
Dichlorodifluoromethane ND ug/L 12/28/22 12:37 75-71-81.2 0.86 2.5
1,1-Dichloroethane ND ug/L 12/28/22 12:37 75-34-31.2 0.92 2.5
1,2-Dichloroethane ND ug/L 12/28/22 12:37 107-06-21.2 0.80 2.5
1,1-Dichloroethene ND ug/L 12/28/22 12:37 75-35-41.2 0.87 2.5
cis-1,2-Dichloroethene ND ug/L 12/28/22 12:37 156-59-21.2 0.96 2.5
trans-1,2-Dichloroethene ND ug/L 12/28/22 12:37 156-60-51.2 0.99 2.5
1,2-Dichloropropane ND ug/L 12/28/22 12:37 78-87-51.2 0.89 2.5
1,3-Dichloropropane ND ug/L 12/28/22 12:37 142-28-91.2 0.71 2.5
2,2-Dichloropropane ND ug/L 12/28/22 12:37 594-20-71.2 0.97 2.5
1,1-Dichloropropene ND ug/L 12/28/22 12:37 563-58-61.2 1.1 2.5
cis-1,3-Dichloropropene ND ug/L 12/28/22 12:37 10061-01-51.2 0.91 2.5
trans-1,3-Dichloropropene ND ug/L 12/28/22 12:37 10061-02-61.2 0.91 2.5
Diisopropyl ether ND ug/L 12/28/22 12:37 108-20-31.2 0.77 2.5
Ethylbenzene ND ug/L 12/28/22 12:37 100-41-41.2 0.76 2.5
Hexachloro-1,3-butadiene ND ug/L 12/28/22 12:37 87-68-35.0 3.8 2.5
Isopropylbenzene (Cumene)ND ug/L 12/28/22 12:37 98-82-81.2 0.83 2.5
Methylene Chloride ND ug/L 12/28/22 12:37 75-09-25.0 4.9 2.5
Methyl-tert-butyl ether ND ug/L 12/28/22 12:37 1634-04-41.2 1.1 2.5
Naphthalene 26.9 ug/L 12/28/22 12:37 91-20-35.0 1.6 2.5
n-Propylbenzene ND ug/L 12/28/22 12:37 103-65-11.2 0.85 2.5
Styrene ND ug/L 12/28/22 12:37 100-42-51.2 0.73 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/28/22 12:37 630-20-61.2 0.78 2.5
1,1,2,2-Tetrachloroethane ND ug/L 12/28/22 12:37 79-34-51.2 0.56 2.5
Tetrachloroethene ND ug/L 12/28/22 12:37 127-18-41.2 0.73 2.5
Toluene 1.1J ug/L 12/28/22 12:37 108-88-31.2 0.60 2.5
1,2,3-Trichlorobenzene ND ug/L 12/28/22 12:37 87-61-65.0 2.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/28/22 12:37 120-82-15.0 1.6 2.5
1,1,1-Trichloroethane ND ug/L 12/28/22 12:37 71-55-61.2 0.83 2.5
1,1,2-Trichloroethane ND ug/L 12/28/22 12:37 79-00-51.2 0.81 2.5
Trichloroethene ND ug/L 12/28/22 12:37 79-01-61.2 0.96 2.5
Trichlorofluoromethane ND ug/L 12/28/22 12:37 75-69-42.5 0.74 2.5
1,2,3-Trichloropropane ND ug/L 12/28/22 12:37 96-18-41.2 0.65 2.5
1,2,4-Trimethylbenzene 349 ug/L 12/28/22 12:37 95-63-61.2 1.2 2.5
1,3,5-Trimethylbenzene 313 ug/L 12/28/22 12:37 108-67-81.2 0.83 2.5
Vinyl chloride ND ug/L 12/28/22 12:37 75-01-42.5 0.96 2.5
m&p-Xylene 50.5 ug/L 12/28/22 12:37 179601-23-12.5 1.8 2.5
o-Xylene ND ug/L 12/28/22 12:37 95-47-61.2 0.84 2.5
Surrogates
1,2-Dichloroethane-d4 (S)112 %12/28/22 12:37 17060-07-070-130 2.5
4-Bromofluorobenzene (S)102 %12/28/22 12:37 460-00-470-130 2.5
Toluene-d8 (S)105 %12/28/22 12:37 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-13 Lab ID:92643625006 Collected:12/19/22 17:02 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 15:34 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 15:34 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 15:34 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 15:34 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 15:34 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 15:34 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 15:34 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 15:34 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 15:34 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 15:34 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 15:34 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 15:34 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 15:34 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 15:34 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 15:34 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 15:34 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 15:34 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 15:34 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 15:34 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 15:34 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 15:34 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 15:34 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 15:34 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 15:34 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 15:34 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 15:34 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 15:34 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 15:34 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 15:34 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 15:34 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 15:34 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 15:34 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 15:34 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 15:34 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 15:34 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 15:34 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 15:34 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 15:34 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 15:34 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 15:34 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 15:34 1634-04-40.50 0.42 1
Naphthalene 1.5J ug/L 12/23/22 15:34 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 15:34 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 15:34 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 15:34 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-13 Lab ID:92643625006 Collected:12/19/22 17:02 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 15:34 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 15:34 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 15:34 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 15:34 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 15:34 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 15:34 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 15:34 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 15:34 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 15:34 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 15:34 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 1.2 ug/L 12/23/22 15:34 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 23.7 ug/L 12/23/22 15:34 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 15:34 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 15:34 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 15:34 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %12/23/22 15:34 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %12/23/22 15:34 460-00-470-130 1
Toluene-d8 (S)104 %12/23/22 15:34 2037-26-570-130 1
Sample:SW-14 Lab ID:92643625007 Collected:12/19/22 16:26 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.56 ug/L 12/23/22 15:52 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 15:52 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 15:52 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 15:52 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 15:52 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 15:52 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 15:52 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 15:52 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 15:52 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 15:52 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 15:52 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 15:52 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 15:52 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 15:52 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 15:52 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 15:52 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 15:52 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-14 Lab ID:92643625007 Collected:12/19/22 16:26 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/23/22 15:52 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 15:52 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 15:52 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 15:52 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 15:52 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 15:52 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 15:52 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 15:52 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 15:52 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 15:52 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 15:52 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 15:52 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 15:52 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 15:52 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 15:52 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 15:52 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 15:52 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 15:52 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 15:52 108-20-30.50 0.31 1
Ethylbenzene 7.7 ug/L 12/23/22 15:52 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 15:52 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)8.8 ug/L 12/23/22 15:52 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 15:52 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.92 ug/L 12/23/22 15:52 1634-04-40.50 0.42 1
Naphthalene 7.6 ug/L 12/23/22 15:52 91-20-32.0 0.64 1
n-Propylbenzene 21.3 ug/L 12/23/22 15:52 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 15:52 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 15:52 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 15:52 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 15:52 127-18-40.50 0.29 1
Toluene 0.84 ug/L 12/23/22 15:52 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 15:52 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 15:52 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 15:52 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 15:52 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 15:52 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 15:52 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 15:52 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 164 ug/L 12/23/22 15:52 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 25.9 ug/L 12/23/22 15:52 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 15:52 75-01-41.0 0.39 1
m&p-Xylene 12.4 ug/L 12/23/22 15:52 179601-23-11.0 0.71 1
o-Xylene 13.7 ug/L 12/23/22 15:52 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/23/22 15:52 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:SW-14 Lab ID:92643625007 Collected:12/19/22 16:26 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)98 %12/23/22 15:52 460-00-470-130 1
Toluene-d8 (S)100 %12/23/22 15:52 2037-26-570-130 1
Sample:DUP-3 Lab ID:92643625008 Collected:12/19/22 00:00 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 17:04 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 17:04 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 17:04 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 17:04 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 17:04 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 17:04 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 17:04 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 17:04 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 17:04 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 17:04 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 17:04 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 17:04 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 17:04 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 17:04 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 17:04 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 17:04 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 17:04 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 17:04 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 17:04 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 17:04 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 17:04 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 17:04 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 17:04 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 17:04 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 17:04 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 17:04 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 17:04 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 17:04 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 17:04 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 17:04 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 17:04 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 17:04 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 17:04 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:DUP-3 Lab ID:92643625008 Collected:12/19/22 00:00 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/23/22 17:04 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 17:04 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 17:04 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 17:04 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 17:04 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 17:04 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 17:04 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 17:04 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 17:04 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 17:04 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 17:04 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 17:04 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 17:04 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 17:04 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 17:04 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 17:04 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 17:04 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 17:04 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 17:04 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 17:04 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 17:04 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 17:04 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 1.3 ug/L 12/23/22 17:04 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 0.45J ug/L 12/23/22 17:04 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 17:04 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 17:04 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 17:04 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/23/22 17:04 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %12/23/22 17:04 460-00-470-130 1
Toluene-d8 (S)105 %12/23/22 17:04 2037-26-570-130 1
Sample:MW-2 Lab ID:92643625009 Collected:12/19/22 17:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 163 ug/L 12/23/22 18:34 71-43-225.0 17.2 50
Bromobenzene ND ug/L 12/23/22 18:34 108-86-125.0 14.5 50
Bromochloromethane ND ug/L 12/23/22 18:34 74-97-525.0 23.4 50
Bromodichloromethane ND ug/L 12/23/22 18:34 75-27-425.0 15.4 50
Bromoform ND ug/L 12/23/22 18:34 75-25-225.0 17.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-2 Lab ID:92643625009 Collected:12/19/22 17:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/23/22 18:34 74-83-925083.0 50
n-Butylbenzene ND ug/L 12/23/22 18:34 104-51-825.0 24.5 50
sec-Butylbenzene ND ug/L 12/23/22 18:34 135-98-825.0 20.0 50
tert-Butylbenzene ND ug/L 12/23/22 18:34 98-06-625.0 16.2 50
Carbon tetrachloride ND ug/L 12/23/22 18:34 56-23-525.0 16.6 50
Chlorobenzene ND ug/L 12/23/22 18:34 108-90-725.0 14.2 50
Chloroethane ND ug/L 12/23/22 18:34 75-00-350.0 32.4 50
Chloroform ND ug/L 12/23/22 18:34 67-66-325.0 21.5 50
Chloromethane ND ug/L 12/23/22 18:34 74-87-350.0 27.0 50
2-Chlorotoluene ND ug/L 12/23/22 18:34 95-49-825.0 16.0 50
4-Chlorotoluene ND ug/L 12/23/22 18:34 106-43-425.0 16.2 50
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 18:34 96-12-850.0 17.0 50
Dibromochloromethane ND ug/L 12/23/22 18:34 124-48-125.0 18.0 50
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 18:34 106-93-425.0 13.6 50
Dibromomethane ND ug/L 12/23/22 18:34 74-95-325.0 19.7 50
1,2-Dichlorobenzene ND ug/L 12/23/22 18:34 95-50-125.0 17.0 50
1,3-Dichlorobenzene ND ug/L 12/23/22 18:34 541-73-125.0 17.0 50
1,4-Dichlorobenzene ND ug/L 12/23/22 18:34 106-46-725.0 16.6 50
Dichlorodifluoromethane ND ug/L 12/23/22 18:34 75-71-825.0 17.3 50
1,1-Dichloroethane ND ug/L 12/23/22 18:34 75-34-325.0 18.4 50
1,2-Dichloroethane ND ug/L 12/23/22 18:34 107-06-225.0 16.1 50
1,1-Dichloroethene ND ug/L 12/23/22 18:34 75-35-425.0 17.4 50
cis-1,2-Dichloroethene 32.8 ug/L 12/23/22 18:34 156-59-225.0 19.2 50
trans-1,2-Dichloroethene ND ug/L 12/23/22 18:34 156-60-525.0 19.8 50
1,2-Dichloropropane ND ug/L 12/23/22 18:34 78-87-525.0 17.8 50
1,3-Dichloropropane ND ug/L 12/23/22 18:34 142-28-925.0 14.2 50
2,2-Dichloropropane ND ug/L 12/23/22 18:34 594-20-725.0 19.4 50
1,1-Dichloropropene ND ug/L 12/23/22 18:34 563-58-625.0 21.4 50
cis-1,3-Dichloropropene ND ug/L 12/23/22 18:34 10061-01-525.0 18.2 50
trans-1,3-Dichloropropene ND ug/L 12/23/22 18:34 10061-02-625.0 18.2 50
Diisopropyl ether ND ug/L 12/23/22 18:34 108-20-325.0 15.4 50
Ethylbenzene 3090 ug/L 12/23/22 18:34 100-41-425.0 15.2 50
Hexachloro-1,3-butadiene ND ug/L 12/23/22 18:34 87-68-310076.5 50
Isopropylbenzene (Cumene)156 ug/L 12/23/22 18:34 98-82-825.0 16.6 50
Methylene Chloride ND ug/L 12/23/22 18:34 75-09-210097.5 50
Methyl-tert-butyl ether 26.0 ug/L 12/23/22 18:34 1634-04-425.0 21.1 50
Naphthalene 337 ug/L 12/23/22 18:34 91-20-310032.2 50
n-Propylbenzene 319 ug/L 12/23/22 18:34 103-65-125.0 17.0 50
Styrene ND ug/L 12/23/22 18:34 100-42-525.0 14.6 50
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 18:34 630-20-625.0 15.6 50
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 18:34 79-34-525.0 11.2 50
Tetrachloroethene ND ug/L 12/23/22 18:34 127-18-425.0 14.6 50
Toluene 7910 ug/L 12/23/22 18:34 108-88-325.0 12.0 50
1,2,3-Trichlorobenzene ND ug/L 12/23/22 18:34 87-61-610040.3 50
1,2,4-Trichlorobenzene ND ug/L 12/23/22 18:34 120-82-110032.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-2 Lab ID:92643625009 Collected:12/19/22 17:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/23/22 18:34 71-55-625.0 16.6 50
1,1,2-Trichloroethane ND ug/L 12/23/22 18:34 79-00-525.0 16.2 50
Trichloroethene ND ug/L 12/23/22 18:34 79-01-625.0 19.2 50
Trichlorofluoromethane ND ug/L 12/23/22 18:34 75-69-450.0 14.9 50
1,2,3-Trichloropropane ND ug/L 12/23/22 18:34 96-18-425.0 13.0 50
1,2,4-Trimethylbenzene 2370 ug/L 12/23/22 18:34 95-63-625.0 24.8 50
1,3,5-Trimethylbenzene 520 ug/L 12/23/22 18:34 108-67-825.0 16.6 50
Vinyl chloride ND ug/L 12/23/22 18:34 75-01-450.0 19.3 50
m&p-Xylene 11200 ug/L 12/23/22 18:34 179601-23-150.0 35.4 50
o-Xylene 4560 ug/L 12/23/22 18:34 95-47-625.0 16.9 50
Surrogates
1,2-Dichloroethane-d4 (S)97 %12/23/22 18:34 17060-07-070-130 50
4-Bromofluorobenzene (S)94 %12/23/22 18:34 460-00-470-130 50
Toluene-d8 (S)107 %12/23/22 18:34 2037-26-570-130 50
Sample:MW-16 Lab ID:92643625010 Collected:12/19/22 13:01 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.44J ug/L 12/23/22 16:28 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 16:28 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 16:28 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 16:28 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 16:28 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 16:28 74-83-95.0 1.7 1
n-Butylbenzene 10.6 ug/L 12/23/22 16:28 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 16:28 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 16:28 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 16:28 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 16:28 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 16:28 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 16:28 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 16:28 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 16:28 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 16:28 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 16:28 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 16:28 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 16:28 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 16:28 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 16:28 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 16:28 541-73-10.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-16 Lab ID:92643625010 Collected:12/19/22 13:01 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/23/22 16:28 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 16:28 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 16:28 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 16:28 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 16:28 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 16:28 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 16:28 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 16:28 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 16:28 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 16:28 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 16:28 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 16:28 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 16:28 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 16:28 108-20-30.50 0.31 1
Ethylbenzene 30.9 ug/L 12/23/22 16:28 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 16:28 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)10.7 ug/L 12/23/22 16:28 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 16:28 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.64 ug/L 12/23/22 16:28 1634-04-40.50 0.42 1
Naphthalene 7.8 ug/L 12/23/22 16:28 91-20-32.0 0.64 1
n-Propylbenzene 36.5 ug/L 12/23/22 16:28 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 16:28 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 16:28 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 16:28 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 16:28 127-18-40.50 0.29 1
Toluene 9.9 ug/L 12/23/22 16:28 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 16:28 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 16:28 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 16:28 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 16:28 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 16:28 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 16:28 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 16:28 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 152 ug/L 12/23/22 16:28 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 16.8 ug/L 12/23/22 16:28 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 16:28 75-01-41.0 0.39 1
m&p-Xylene 84.4 ug/L 12/23/22 16:28 179601-23-11.0 0.71 1
o-Xylene 30.4 ug/L 12/23/22 16:28 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/23/22 16:28 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/23/22 16:28 460-00-470-130 1
Toluene-d8 (S)98 %12/23/22 16:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:DUP-1 Lab ID:92643625011 Collected:12/19/22 00:00 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.44J ug/L 12/28/22 12:19 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/28/22 12:19 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/28/22 12:19 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/28/22 12:19 75-27-40.50 0.31 1
Bromoform ND ug/L 12/28/22 12:19 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/28/22 12:19 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/28/22 12:19 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/28/22 12:19 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/28/22 12:19 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/28/22 12:19 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/28/22 12:19 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/28/22 12:19 75-00-31.0 0.65 1
Chloroform ND ug/L 12/28/22 12:19 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/28/22 12:19 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/28/22 12:19 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/28/22 12:19 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/28/22 12:19 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/28/22 12:19 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/28/22 12:19 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/28/22 12:19 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/28/22 12:19 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/28/22 12:19 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/28/22 12:19 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/28/22 12:19 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/28/22 12:19 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/28/22 12:19 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/28/22 12:19 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/28/22 12:19 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/28/22 12:19 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/28/22 12:19 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/28/22 12:19 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/28/22 12:19 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/28/22 12:19 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/28/22 12:19 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/28/22 12:19 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/28/22 12:19 108-20-30.50 0.31 1
Ethylbenzene 29.7 ug/L 12/28/22 12:19 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/28/22 12:19 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)10.1 ug/L 12/28/22 12:19 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/28/22 12:19 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/28/22 12:19 1634-04-40.50 0.42 1
Naphthalene 6.2 ug/L 12/28/22 12:19 91-20-32.0 0.64 1
n-Propylbenzene 34.7 ug/L 12/28/22 12:19 103-65-10.50 0.34 1
Styrene ND ug/L 12/28/22 12:19 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/28/22 12:19 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:DUP-1 Lab ID:92643625011 Collected:12/19/22 00:00 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/28/22 12:19 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/28/22 12:19 127-18-40.50 0.29 1
Toluene 10.1 ug/L 12/28/22 12:19 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/28/22 12:19 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/28/22 12:19 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/28/22 12:19 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/28/22 12:19 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/28/22 12:19 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/28/22 12:19 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/28/22 12:19 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene 153 ug/L 12/28/22 12:19 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 16.0 ug/L 12/28/22 12:19 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/28/22 12:19 75-01-41.0 0.39 1
m&p-Xylene 78.5 ug/L 12/28/22 12:19 179601-23-11.0 0.71 1
o-Xylene 27.6 ug/L 12/28/22 12:19 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %12/28/22 12:19 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %12/28/22 12:19 460-00-470-130 1
Toluene-d8 (S)103 %12/28/22 12:19 2037-26-570-130 1
Sample:MW-10 Lab ID:92643625012 Collected:12/19/22 12:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 12.2 ug/L 12/28/22 12:54 71-43-21.2 0.86 2.5
Bromobenzene ND ug/L 12/28/22 12:54 108-86-11.2 0.72 2.5
Bromochloromethane ND ug/L 12/28/22 12:54 74-97-51.2 1.2 2.5
Bromodichloromethane ND ug/L 12/28/22 12:54 75-27-41.2 0.77 2.5
Bromoform ND ug/L 12/28/22 12:54 75-25-21.2 0.85 2.5
Bromomethane ND ug/L 12/28/22 12:54 74-83-912.5 4.2 2.5
n-Butylbenzene ND ug/L 12/28/22 12:54 104-51-81.2 1.2 2.5
sec-Butylbenzene ND ug/L 12/28/22 12:54 135-98-81.2 1.0 2.5
tert-Butylbenzene ND ug/L 12/28/22 12:54 98-06-61.2 0.81 2.5
Carbon tetrachloride ND ug/L 12/28/22 12:54 56-23-51.2 0.83 2.5
Chlorobenzene ND ug/L 12/28/22 12:54 108-90-71.2 0.71 2.5
Chloroethane ND ug/L 12/28/22 12:54 75-00-32.5 1.6 2.5
Chloroform ND ug/L 12/28/22 12:54 67-66-31.2 1.1 2.5
Chloromethane ND ug/L 12/28/22 12:54 74-87-32.5 1.4 2.5
2-Chlorotoluene ND ug/L 12/28/22 12:54 95-49-81.2 0.80 2.5
4-Chlorotoluene ND ug/L 12/28/22 12:54 106-43-41.2 0.81 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/28/22 12:54 96-12-82.5 0.85 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-10 Lab ID:92643625012 Collected:12/19/22 12:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/28/22 12:54 124-48-11.2 0.90 2.5
1,2-Dibromoethane (EDB)ND ug/L 12/28/22 12:54 106-93-41.2 0.68 2.5
Dibromomethane ND ug/L 12/28/22 12:54 74-95-31.2 0.98 2.5
1,2-Dichlorobenzene ND ug/L 12/28/22 12:54 95-50-11.2 0.85 2.5
1,3-Dichlorobenzene ND ug/L 12/28/22 12:54 541-73-11.2 0.85 2.5
1,4-Dichlorobenzene ND ug/L 12/28/22 12:54 106-46-71.2 0.83 2.5
Dichlorodifluoromethane ND ug/L 12/28/22 12:54 75-71-81.2 0.86 2.5
1,1-Dichloroethane ND ug/L 12/28/22 12:54 75-34-31.2 0.92 2.5
1,2-Dichloroethane ND ug/L 12/28/22 12:54 107-06-21.2 0.80 2.5
1,1-Dichloroethene ND ug/L 12/28/22 12:54 75-35-41.2 0.87 2.5
cis-1,2-Dichloroethene ND ug/L 12/28/22 12:54 156-59-21.2 0.96 2.5
trans-1,2-Dichloroethene ND ug/L 12/28/22 12:54 156-60-51.2 0.99 2.5
1,2-Dichloropropane ND ug/L 12/28/22 12:54 78-87-51.2 0.89 2.5
1,3-Dichloropropane ND ug/L 12/28/22 12:54 142-28-91.2 0.71 2.5
2,2-Dichloropropane ND ug/L 12/28/22 12:54 594-20-71.2 0.97 2.5
1,1-Dichloropropene ND ug/L 12/28/22 12:54 563-58-61.2 1.1 2.5
cis-1,3-Dichloropropene ND ug/L 12/28/22 12:54 10061-01-51.2 0.91 2.5
trans-1,3-Dichloropropene ND ug/L 12/28/22 12:54 10061-02-61.2 0.91 2.5
Diisopropyl ether 0.80J ug/L 12/28/22 12:54 108-20-31.2 0.77 2.5
Ethylbenzene 47.8 ug/L 12/28/22 12:54 100-41-41.2 0.76 2.5
Hexachloro-1,3-butadiene ND ug/L 12/28/22 12:54 87-68-35.0 3.8 2.5
Isopropylbenzene (Cumene)39.0 ug/L 12/28/22 12:54 98-82-81.2 0.83 2.5
Methylene Chloride ND ug/L 12/28/22 12:54 75-09-25.0 4.9 2.5
Methyl-tert-butyl ether ND ug/L 12/28/22 12:54 1634-04-41.2 1.1 2.5
Naphthalene 31.3 ug/L 12/28/22 12:54 91-20-35.0 1.6 2.5
n-Propylbenzene 106 ug/L 12/28/22 12:54 103-65-11.2 0.85 2.5
Styrene ND ug/L 12/28/22 12:54 100-42-51.2 0.73 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/28/22 12:54 630-20-61.2 0.78 2.5
1,1,2,2-Tetrachloroethane ND ug/L 12/28/22 12:54 79-34-51.2 0.56 2.5
Tetrachloroethene ND ug/L 12/28/22 12:54 127-18-41.2 0.73 2.5
Toluene 3.0 ug/L 12/28/22 12:54 108-88-31.2 0.60 2.5
1,2,3-Trichlorobenzene ND ug/L 12/28/22 12:54 87-61-65.0 2.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/28/22 12:54 120-82-15.0 1.6 2.5
1,1,1-Trichloroethane ND ug/L 12/28/22 12:54 71-55-61.2 0.83 2.5
1,1,2-Trichloroethane ND ug/L 12/28/22 12:54 79-00-51.2 0.81 2.5
Trichloroethene ND ug/L 12/28/22 12:54 79-01-61.2 0.96 2.5
Trichlorofluoromethane ND ug/L 12/28/22 12:54 75-69-42.5 0.74 2.5
1,2,3-Trichloropropane ND ug/L 12/28/22 12:54 96-18-41.2 0.65 2.5
1,2,4-Trimethylbenzene 271 ug/L 12/28/22 12:54 95-63-61.2 1.2 2.5
1,3,5-Trimethylbenzene 17.7 ug/L 12/28/22 12:54 108-67-81.2 0.83 2.5
Vinyl chloride ND ug/L 12/28/22 12:54 75-01-42.5 0.96 2.5
m&p-Xylene 44.8 ug/L 12/28/22 12:54 179601-23-12.5 1.8 2.5
o-Xylene ND ug/L 12/28/22 12:54 95-47-61.2 0.84 2.5
Surrogates
1,2-Dichloroethane-d4 (S)111 %12/28/22 12:54 17060-07-070-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-10 Lab ID:92643625012 Collected:12/19/22 12:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)103 %12/28/22 12:54 460-00-470-130 2.5
Toluene-d8 (S)105 %12/28/22 12:54 2037-26-570-130 2.5
Sample:MW-12 Lab ID:92643625013 Collected:12/19/22 10:17 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 17:22 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 17:22 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 17:22 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 17:22 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 17:22 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 17:22 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 17:22 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 17:22 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 17:22 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 17:22 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 17:22 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 17:22 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 17:22 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 17:22 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 17:22 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 17:22 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 17:22 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 17:22 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 17:22 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 17:22 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 17:22 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 17:22 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 17:22 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 17:22 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 17:22 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 17:22 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 17:22 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 17:22 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 17:22 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 17:22 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 17:22 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 17:22 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 17:22 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-12 Lab ID:92643625013 Collected:12/19/22 10:17 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 12/23/22 17:22 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 17:22 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 17:22 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 17:22 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 17:22 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 17:22 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 17:22 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 17:22 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 17:22 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 17:22 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 17:22 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 17:22 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 17:22 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 17:22 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 17:22 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 17:22 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 17:22 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 17:22 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 17:22 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 17:22 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 17:22 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 17:22 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 17:22 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 17:22 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 17:22 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 17:22 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 17:22 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %12/23/22 17:22 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/23/22 17:22 460-00-470-130 1
Toluene-d8 (S)105 %12/23/22 17:22 2037-26-570-130 1
Sample:MW-6 Lab ID:92643625014 Collected:12/19/22 15:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 4.6J ug/L 12/28/22 13:12 71-43-26.2 4.3 12.5
Bromobenzene ND ug/L 12/28/22 13:12 108-86-16.2 3.6 12.5
Bromochloromethane ND ug/L 12/28/22 13:12 74-97-56.2 5.8 12.5
Bromodichloromethane ND ug/L 12/28/22 13:12 75-27-46.2 3.8 12.5
Bromoform ND ug/L 12/28/22 13:12 75-25-26.2 4.3 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-6 Lab ID:92643625014 Collected:12/19/22 15:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromomethane ND ug/L 12/28/22 13:12 74-83-962.5 20.8 12.5
n-Butylbenzene ND ug/L 12/28/22 13:12 104-51-8 M16.2 6.1 12.5
sec-Butylbenzene ND ug/L 12/28/22 13:12 135-98-86.2 5.0 12.5
tert-Butylbenzene ND ug/L 12/28/22 13:12 98-06-66.2 4.0 12.5
Carbon tetrachloride ND ug/L 12/28/22 13:12 56-23-56.2 4.2 12.5
Chlorobenzene ND ug/L 12/28/22 13:12 108-90-76.2 3.6 12.5
Chloroethane ND ug/L 12/28/22 13:12 75-00-3 M112.5 8.1 12.5
Chloroform ND ug/L 12/28/22 13:12 67-66-36.2 5.4 12.5
Chloromethane ND ug/L 12/28/22 13:12 74-87-312.5 6.8 12.5
2-Chlorotoluene ND ug/L 12/28/22 13:12 95-49-86.2 4.0 12.5
4-Chlorotoluene ND ug/L 12/28/22 13:12 106-43-46.2 4.0 12.5
1,2-Dibromo-3-chloropropane ND ug/L 12/28/22 13:12 96-12-812.5 4.2 12.5
Dibromochloromethane ND ug/L 12/28/22 13:12 124-48-16.2 4.5 12.5
1,2-Dibromoethane (EDB)ND ug/L 12/28/22 13:12 106-93-46.2 3.4 12.5
Dibromomethane ND ug/L 12/28/22 13:12 74-95-36.2 4.9 12.5
1,2-Dichlorobenzene ND ug/L 12/28/22 13:12 95-50-16.2 4.2 12.5
1,3-Dichlorobenzene ND ug/L 12/28/22 13:12 541-73-16.2 4.2 12.5
1,4-Dichlorobenzene ND ug/L 12/28/22 13:12 106-46-76.2 4.2 12.5
Dichlorodifluoromethane ND ug/L 12/28/22 13:12 75-71-86.2 4.3 12.5
1,1-Dichloroethane ND ug/L 12/28/22 13:12 75-34-36.2 4.6 12.5
1,2-Dichloroethane ND ug/L 12/28/22 13:12 107-06-26.2 4.0 12.5
1,1-Dichloroethene ND ug/L 12/28/22 13:12 75-35-4 M16.2 4.4 12.5
cis-1,2-Dichloroethene ND ug/L 12/28/22 13:12 156-59-26.2 4.8 12.5
trans-1,2-Dichloroethene ND ug/L 12/28/22 13:12 156-60-56.2 5.0 12.5
1,2-Dichloropropane ND ug/L 12/28/22 13:12 78-87-56.2 4.4 12.5
1,3-Dichloropropane ND ug/L 12/28/22 13:12 142-28-96.2 3.6 12.5
2,2-Dichloropropane ND ug/L 12/28/22 13:12 594-20-76.2 4.8 12.5
1,1-Dichloropropene ND ug/L 12/28/22 13:12 563-58-6 M16.2 5.3 12.5
cis-1,3-Dichloropropene ND ug/L 12/28/22 13:12 10061-01-56.2 4.6 12.5
trans-1,3-Dichloropropene ND ug/L 12/28/22 13:12 10061-02-66.2 4.5 12.5
Diisopropyl ether ND ug/L 12/28/22 13:12 108-20-36.2 3.8 12.5
Ethylbenzene 431 ug/L 12/28/22 13:12 100-41-46.2 3.8 12.5
Hexachloro-1,3-butadiene ND ug/L 12/28/22 13:12 87-68-325.0 19.1 12.5
Isopropylbenzene (Cumene)93.1 ug/L 12/28/22 13:12 98-82-86.2 4.2 12.5
Methylene Chloride ND ug/L 12/28/22 13:12 75-09-225.0 24.4 12.5
Methyl-tert-butyl ether ND ug/L 12/28/22 13:12 1634-04-46.2 5.3 12.5
Naphthalene 106 ug/L 12/28/22 13:12 91-20-325.0 8.1 12.5
n-Propylbenzene 249 ug/L 12/28/22 13:12 103-65-16.2 4.2 12.5
Styrene ND ug/L 12/28/22 13:12 100-42-56.2 3.6 12.5
1,1,1,2-Tetrachloroethane ND ug/L 12/28/22 13:12 630-20-66.2 3.9 12.5
1,1,2,2-Tetrachloroethane ND ug/L 12/28/22 13:12 79-34-56.2 2.8 12.5
Tetrachloroethene ND ug/L 12/28/22 13:12 127-18-46.2 3.6 12.5
Toluene 25.2 ug/L 12/28/22 13:12 108-88-36.2 3.0 12.5
1,2,3-Trichlorobenzene ND ug/L 12/28/22 13:12 87-61-625.0 10.1 12.5
1,2,4-Trichlorobenzene ND ug/L 12/28/22 13:12 120-82-125.0 8.0 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-6 Lab ID:92643625014 Collected:12/19/22 15:10 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,1-Trichloroethane ND ug/L 12/28/22 13:12 71-55-66.2 4.2 12.5
1,1,2-Trichloroethane ND ug/L 12/28/22 13:12 79-00-56.2 4.1 12.5
Trichloroethene ND ug/L 12/28/22 13:12 79-01-66.2 4.8 12.5
Trichlorofluoromethane ND ug/L 12/28/22 13:12 75-69-412.5 3.7 12.5
1,2,3-Trichloropropane ND ug/L 12/28/22 13:12 96-18-46.2 3.3 12.5
1,2,4-Trimethylbenzene 1570 ug/L 12/28/22 13:12 95-63-66.2 6.2 12.5
1,3,5-Trimethylbenzene 275 ug/L 12/28/22 13:12 108-67-86.2 4.2 12.5
Vinyl chloride ND ug/L 12/28/22 13:12 75-01-412.5 4.8 12.5
m&p-Xylene 1010 ug/L 12/28/22 13:12 179601-23-112.5 8.9 12.5
o-Xylene 136 ug/L 12/28/22 13:12 95-47-66.2 4.2 12.5
Surrogates
1,2-Dichloroethane-d4 (S)111 %12/28/22 13:12 17060-07-070-130 12.5
4-Bromofluorobenzene (S)103 %12/28/22 13:12 460-00-470-130 12.5
Toluene-d8 (S)107 %12/28/22 13:12 2037-26-570-130 12.5
Sample:MW-7 Lab ID:92643625015 Collected:12/19/22 15:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 17:40 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 17:40 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 17:40 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 17:40 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 17:40 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 17:40 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 17:40 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 17:40 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 17:40 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 17:40 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 17:40 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 17:40 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 17:40 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 17:40 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 17:40 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 17:40 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 17:40 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 17:40 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 17:40 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 17:40 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 17:40 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 17:40 541-73-10.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-7 Lab ID:92643625015 Collected:12/19/22 15:07 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,4-Dichlorobenzene ND ug/L 12/23/22 17:40 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 17:40 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 17:40 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 17:40 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 17:40 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 17:40 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 17:40 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 17:40 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 17:40 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 17:40 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 17:40 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 17:40 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 17:40 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 17:40 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 17:40 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 17:40 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 17:40 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 17:40 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 17:40 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 17:40 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 17:40 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 17:40 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 17:40 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 17:40 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 17:40 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 17:40 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 17:40 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 17:40 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 17:40 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 17:40 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 17:40 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 17:40 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 17:40 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 17:40 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 17:40 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 17:40 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 17:40 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 17:40 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/23/22 17:40 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %12/23/22 17:40 460-00-470-130 1
Toluene-d8 (S)102 %12/23/22 17:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-1 Lab ID:92643625016 Collected:12/19/22 11:20 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 17:58 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 17:58 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 17:58 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 17:58 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 17:58 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 17:58 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 17:58 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 17:58 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 17:58 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 17:58 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 17:58 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 17:58 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 17:58 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 17:58 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 17:58 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 17:58 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 17:58 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 12/23/22 17:58 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 17:58 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 17:58 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 17:58 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 17:58 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 17:58 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 17:58 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 17:58 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 17:58 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 17:58 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 17:58 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 17:58 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 17:58 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 17:58 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 17:58 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 17:58 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 17:58 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 17:58 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 17:58 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 17:58 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 17:58 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 17:58 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 17:58 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 17:58 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 17:58 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 17:58 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 17:58 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 17:58 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
Page 29 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-1 Lab ID:92643625016 Collected:12/19/22 11:20 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 17:58 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 17:58 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 17:58 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 17:58 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 17:58 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 17:58 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 17:58 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 17:58 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 17:58 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 17:58 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 17:58 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 17:58 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 17:58 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 17:58 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 17:58 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %12/23/22 17:58 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/23/22 17:58 460-00-470-130 1
Toluene-d8 (S)105 %12/23/22 17:58 2037-26-570-130 1
Sample:MW-3 Lab ID:92643625017 Collected:12/19/22 17:12 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/23/22 18:16 71-43-20.50 0.34 1
Bromobenzene ND ug/L 12/23/22 18:16 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 12/23/22 18:16 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 12/23/22 18:16 75-27-40.50 0.31 1
Bromoform ND ug/L 12/23/22 18:16 75-25-20.50 0.34 1
Bromomethane ND ug/L 12/23/22 18:16 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 12/23/22 18:16 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 12/23/22 18:16 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 12/23/22 18:16 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 12/23/22 18:16 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 12/23/22 18:16 108-90-70.50 0.28 1
Chloroethane ND ug/L 12/23/22 18:16 75-00-31.0 0.65 1
Chloroform ND ug/L 12/23/22 18:16 67-66-30.50 0.43 1
Chloromethane ND ug/L 12/23/22 18:16 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 12/23/22 18:16 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 12/23/22 18:16 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 12/23/22 18:16 96-12-81.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-3 Lab ID:92643625017 Collected:12/19/22 17:12 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromochloromethane ND ug/L 12/23/22 18:16 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 12/23/22 18:16 106-93-40.50 0.27 1
Dibromomethane ND ug/L 12/23/22 18:16 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 12/23/22 18:16 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 12/23/22 18:16 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 12/23/22 18:16 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 12/23/22 18:16 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 12/23/22 18:16 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 12/23/22 18:16 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 12/23/22 18:16 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 12/23/22 18:16 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 12/23/22 18:16 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 12/23/22 18:16 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 12/23/22 18:16 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 12/23/22 18:16 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 12/23/22 18:16 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 12/23/22 18:16 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 12/23/22 18:16 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 12/23/22 18:16 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 12/23/22 18:16 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 12/23/22 18:16 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 12/23/22 18:16 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 12/23/22 18:16 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 12/23/22 18:16 1634-04-40.50 0.42 1
Naphthalene ND ug/L 12/23/22 18:16 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 12/23/22 18:16 103-65-10.50 0.34 1
Styrene ND ug/L 12/23/22 18:16 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 12/23/22 18:16 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 12/23/22 18:16 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 12/23/22 18:16 127-18-40.50 0.29 1
Toluene ND ug/L 12/23/22 18:16 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/23/22 18:16 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 12/23/22 18:16 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 12/23/22 18:16 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 12/23/22 18:16 79-00-50.50 0.32 1
Trichloroethene ND ug/L 12/23/22 18:16 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 12/23/22 18:16 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 12/23/22 18:16 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 12/23/22 18:16 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 12/23/22 18:16 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 12/23/22 18:16 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 12/23/22 18:16 179601-23-11.0 0.71 1
o-Xylene ND ug/L 12/23/22 18:16 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %12/23/22 18:16 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Sample:MW-3 Lab ID:92643625017 Collected:12/19/22 17:12 Received:12/20/22 15:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Surrogates
4-Bromofluorobenzene (S)99 %12/23/22 18:16 460-00-470-130 1
Toluene-d8 (S)104 %12/23/22 18:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
745606
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92643625001, 92643625003, 92643625004, 92643625006, 92643625007, 92643625008, 92643625009,
92643625010, 92643625013, 92643625015, 92643625016, 92643625017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3878574
Associated Lab Samples:92643625001, 92643625003, 92643625004, 92643625006, 92643625007, 92643625008, 92643625009,
92643625010, 92643625013, 92643625015, 92643625016, 92643625017
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/23/22 13:280.31
1,1,1-Trichloroethane ug/L ND 0.50 12/23/22 13:280.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/23/22 13:280.22
1,1,2-Trichloroethane ug/L ND 0.50 12/23/22 13:280.32
1,1-Dichloroethane ug/L ND 0.50 12/23/22 13:280.37
1,1-Dichloroethene ug/L ND 0.50 12/23/22 13:280.35
1,1-Dichloropropene ug/L ND 0.50 12/23/22 13:280.43
1,2,3-Trichlorobenzene ug/L ND 2.0 12/23/22 13:280.81
1,2,3-Trichloropropane ug/L ND 0.50 12/23/22 13:280.26
1,2,4-Trichlorobenzene ug/L ND 2.0 12/23/22 13:280.64
1,2,4-Trimethylbenzene ug/L ND 0.50 12/23/22 13:280.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/23/22 13:280.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/23/22 13:280.27
1,2-Dichlorobenzene ug/L ND 0.50 12/23/22 13:280.34
1,2-Dichloroethane ug/L ND 0.50 12/23/22 13:280.32
1,2-Dichloropropane ug/L ND 0.50 12/23/22 13:280.36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/23/22 13:280.33
1,3-Dichlorobenzene ug/L ND 0.50 12/23/22 13:280.34
1,3-Dichloropropane ug/L ND 0.50 12/23/22 13:280.28
1,4-Dichlorobenzene ug/L ND 0.50 12/23/22 13:280.33
2,2-Dichloropropane ug/L ND 0.50 12/23/22 13:280.39
2-Chlorotoluene ug/L ND 0.50 12/23/22 13:280.32
4-Chlorotoluene ug/L ND 0.50 12/23/22 13:280.32
Benzene ug/L ND 0.50 12/23/22 13:280.34
Bromobenzene ug/L ND 0.50 12/23/22 13:280.29
Bromochloromethane ug/L ND 0.50 12/23/22 13:280.47
Bromodichloromethane ug/L ND 0.50 12/23/22 13:280.31
Bromoform ug/L ND 0.50 12/23/22 13:280.34
Bromomethane ug/L ND 5.0 12/23/22 13:281.7
Carbon tetrachloride ug/L ND 0.50 12/23/22 13:280.33
Chlorobenzene ug/L ND 0.50 12/23/22 13:280.28
Chloroethane ug/L ND 1.0 12/23/22 13:280.65
Chloroform ug/L ND 0.50 12/23/22 13:280.43
Chloromethane ug/L ND 1.0 12/23/22 13:280.54
cis-1,2-Dichloroethene ug/L ND 0.50 12/23/22 13:280.38
cis-1,3-Dichloropropene ug/L ND 0.50 12/23/22 13:280.36
Dibromochloromethane ug/L ND 0.50 12/23/22 13:280.36
Dibromomethane ug/L ND 0.50 12/23/22 13:280.39
Dichlorodifluoromethane ug/L ND 0.50 12/23/22 13:280.35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3878574
Associated Lab Samples:92643625001, 92643625003, 92643625004, 92643625006, 92643625007, 92643625008, 92643625009,
92643625010, 92643625013, 92643625015, 92643625016, 92643625017
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 0.50 12/23/22 13:280.31
Ethylbenzene ug/L ND 0.50 12/23/22 13:280.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/23/22 13:281.5
Isopropylbenzene (Cumene)ug/L ND 0.50 12/23/22 13:280.33
m&p-Xylene ug/L ND 1.0 12/23/22 13:280.71
Methyl-tert-butyl ether ug/L ND 0.50 12/23/22 13:280.42
Methylene Chloride ug/L ND 2.0 12/23/22 13:282.0
n-Butylbenzene ug/L ND 0.50 12/23/22 13:280.49
n-Propylbenzene ug/L ND 0.50 12/23/22 13:280.34
Naphthalene ug/L ND 2.0 12/23/22 13:280.64
o-Xylene ug/L ND 0.50 12/23/22 13:280.34
sec-Butylbenzene ug/L ND 0.50 12/23/22 13:280.40
Styrene ug/L ND 0.50 12/23/22 13:280.29
tert-Butylbenzene ug/L ND 0.50 12/23/22 13:280.32
Tetrachloroethene ug/L ND 0.50 12/23/22 13:280.29
Toluene ug/L ND 0.50 12/23/22 13:280.24
trans-1,2-Dichloroethene ug/L ND 0.50 12/23/22 13:280.40
trans-1,3-Dichloropropene ug/L ND 0.50 12/23/22 13:280.36
Trichloroethene ug/L ND 0.50 12/23/22 13:280.38
Trichlorofluoromethane ug/L ND 1.0 12/23/22 13:280.30
Vinyl chloride ug/L ND 1.0 12/23/22 13:280.39
1,2-Dichloroethane-d4 (S)%101 70-130 12/23/22 13:28
4-Bromofluorobenzene (S)%98 70-130 12/23/22 13:28
Toluene-d8 (S)%103 70-130 12/23/22 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3878575LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.350 115 60-140
1,1,1-Trichloroethane ug/L 54.650 109 60-140
1,1,2,2-Tetrachloroethane ug/L 53.250 106 60-140
1,1,2-Trichloroethane ug/L 54.150 108 60-140
1,1-Dichloroethane ug/L 49.050 98 60-140
1,1-Dichloroethene ug/L 53.050 106 60-140
1,1-Dichloropropene ug/L 60.350 121 60-140
1,2,3-Trichlorobenzene ug/L 59.450 119 60-140
1,2,3-Trichloropropane ug/L 48.650 97 60-140
1,2,4-Trichlorobenzene ug/L 55.950 112 60-140
1,2,4-Trimethylbenzene ug/L 52.450 105 60-140
1,2-Dibromo-3-chloropropane ug/L 56.850 114 60-140
1,2-Dibromoethane (EDB)ug/L 57.650 115 60-140
1,2-Dichlorobenzene ug/L 55.150 110 60-140
1,2-Dichloroethane ug/L 50.950 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3878575LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 57.350 115 60-140
1,3,5-Trimethylbenzene ug/L 53.950 108 60-140
1,3-Dichlorobenzene ug/L 55.450 111 60-140
1,3-Dichloropropane ug/L 55.050 110 60-140
1,4-Dichlorobenzene ug/L 52.450 105 60-140
2,2-Dichloropropane ug/L 56.150 112 60-140
2-Chlorotoluene ug/L 56.750 113 60-140
4-Chlorotoluene ug/L 54.350 109 60-140
Benzene ug/L 51.250 102 60-140
Bromobenzene ug/L 55.450 111 60-140
Bromochloromethane ug/L 54.950 110 60-140
Bromodichloromethane ug/L 52.950 106 60-140
Bromoform ug/L 56.550 113 60-140
Bromomethane ug/L 37.650 75 60-140
Carbon tetrachloride ug/L 53.550 107 60-140
Chlorobenzene ug/L 54.450 109 60-140
Chloroethane ug/L 38.550 77 60-140
Chloroform ug/L 46.350 93 60-140
Chloromethane ug/L 48.650 97 60-140
cis-1,2-Dichloroethene ug/L 51.550 103 60-140
cis-1,3-Dichloropropene ug/L 57.150 114 60-140
Dibromochloromethane ug/L 50.650 101 60-140
Dibromomethane ug/L 56.750 113 60-140
Dichlorodifluoromethane ug/L 43.150 86 60-140
Diisopropyl ether ug/L 55.050 110 60-140
Ethylbenzene ug/L 52.750 105 60-140
Hexachloro-1,3-butadiene ug/L 56.050 112 60-140
Isopropylbenzene (Cumene)ug/L 52.750 105 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 47.850 96 60-140
Methylene Chloride ug/L 47.150 94 60-140
n-Butylbenzene ug/L 55.950 112 60-140
n-Propylbenzene ug/L 54.050 108 60-140
Naphthalene ug/L 59.550 119 60-140
o-Xylene ug/L 53.950 108 60-140
sec-Butylbenzene ug/L 52.750 105 60-140
Styrene ug/L 54.050 108 60-140
tert-Butylbenzene ug/L 44.550 89 60-140
Tetrachloroethene ug/L 54.050 108 60-140
Toluene ug/L 50.650 101 60-140
trans-1,2-Dichloroethene ug/L 52.650 105 60-140
trans-1,3-Dichloropropene ug/L 54.450 109 60-140
Trichloroethene ug/L 58.650 117 60-140
Trichlorofluoromethane ug/L 39.350 79 60-140
Vinyl chloride ug/L 48.550 97 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3878575LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3878576MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643625001
3878577
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 117 60-140131 11 3020ND23.4 26.2
1,1,1-Trichloroethane ug/L 20 118 60-140131 10 3020ND23.6 26.2
1,1,2,2-Tetrachloroethane ug/L 20 109 60-140120 10 3020ND21.9 24.1
1,1,2-Trichloroethane ug/L 20 110 60-140121 10 3020ND22.1 24.3
1,1-Dichloroethane ug/L 20 109 60-140121 10 3020ND21.8 24.1
1,1-Dichloroethene ug/L 20 118 60-140136 14 3020ND23.7 27.2
1,1-Dichloropropene ug/L M12012860-140142 10 3020ND25.6 28.3
1,2,3-Trichlorobenzene ug/L 20 115 60-140135 16 3020ND22.9 26.9
1,2,3-Trichloropropane ug/L 20 109 60-140115 5 3020ND21.9 22.9
1,2,4-Trichlorobenzene ug/L 20 108 60-140121 12 3020ND21.6 24.3
1,2,4-Trimethylbenzene ug/L 20 110 60-140122 10 3020ND22.1 24.3
1,2-Dibromo-3-
chloropropane ug/L 20 118 60-140119 1 3020ND23.6 23.8
1,2-Dibromoethane (EDB)ug/L 20 117 60-140129 10 3020ND23.5 25.8
1,2-Dichlorobenzene ug/L 20 113 60-140126 11 3020ND22.5 25.3
1,2-Dichloroethane ug/L 20 113 60-140122 8 3020ND22.6 24.4
1,2-Dichloropropane ug/L 20 123 60-140135 9 3020ND24.6 27.0
1,3,5-Trimethylbenzene ug/L 20 113 60-140126 11 3020ND22.5 25.2
1,3-Dichlorobenzene ug/L 20 114 60-140130 14 3020ND22.7 26.0
1,3-Dichloropropane ug/L 20 114 60-140128 11 3020ND22.9 25.6
1,4-Dichlorobenzene ug/L 20 108 60-140124 14 3020ND21.6 24.8
2,2-Dichloropropane ug/L 20 119 60-140134 12 3020ND23.9 26.8
2-Chlorotoluene ug/L 20 108 60-140124 14 3020ND21.6 24.9
4-Chlorotoluene ug/L 20 117 60-140127 9 3020ND23.4 25.5
Benzene ug/L 20 109 60-140120 10 3020ND21.7 24.1
Bromobenzene ug/L 20 115 60-140129 12 3020ND22.9 25.9
Bromochloromethane ug/L 20 114 60-140127 10 3020ND22.9 25.4
Bromodichloromethane ug/L 20 113 60-140122 8 3020ND22.5 24.4
Bromoform ug/L 20 111 60-140127 13 3020ND22.2 25.4
Bromomethane ug/L 20 67 60-14089 28 3020ND13.5 17.9
Carbon tetrachloride ug/L 20 118 60-140138 15 3020ND23.6 27.5
Chlorobenzene ug/L 20 117 60-140130 10 3020ND23.4 25.9
Chloroethane ug/L 20 106 60-140123 14 3020ND21.2 24.5
Chloroform ug/L 20 102 60-140113 10 3020ND20.7 22.8
Chloromethane ug/L 20 111 60-140124 11 3020ND22.3 24.8
cis-1,2-Dichloroethene ug/L 20 112 60-140123 10 3020ND22.3 24.7
cis-1,3-Dichloropropene ug/L 20 118 60-140133 12 3020ND23.6 26.6
Dibromochloromethane ug/L 20 103 60-140114 10 3020ND20.7 22.8
Dibromomethane ug/L 20 121 60-140131 8 3020ND24.1 26.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3878576MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643625001
3878577
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 20 98 60-140111 12 3020ND19.7 22.2
Diisopropyl ether ug/L 20 113 60-140122 7 3020ND22.6 24.4
Ethylbenzene ug/L 20 112 60-140127 12 3020ND22.4 25.4
Hexachloro-1,3-butadiene ug/L 20 113 60-140125 11 3020ND22.5 25.1
Isopropylbenzene
(Cumene)
ug/L 20 112 60-140125 11 3020ND22.3 25.0
m&p-Xylene ug/L 40 111 60-140127 13 3040ND44.5 50.9
Methyl-tert-butyl ether ug/L 20 98 60-140106 8 3020ND19.6 21.3
Methylene Chloride ug/L 20 102 60-140111 9 3020ND20.4 22.2
n-Butylbenzene ug/L 20 115 60-140129 12 3020ND22.9 25.9
n-Propylbenzene ug/L 20 115 60-140128 10 3020ND23.0 25.5
Naphthalene ug/L 20 110 60-140127 15 3020ND21.9 25.4
o-Xylene ug/L 20 114 60-140126 11 3020ND22.8 25.3
sec-Butylbenzene ug/L 20 112 60-140126 11 3020ND22.5 25.1
Styrene ug/L 20 112 60-140127 12 3020ND22.4 25.4
tert-Butylbenzene ug/L 20 96 60-140107 10 3020ND19.2 21.3
Tetrachloroethene ug/L 20 111 60-140124 12 3020ND22.1 24.9
Toluene ug/L 20 107 60-140120 12 3020ND21.3 24.0
trans-1,2-Dichloroethene ug/L 20 117 60-140127 8 3020ND23.3 25.3
trans-1,3-Dichloropropene ug/L 20 113 60-140126 11 3020ND22.7 25.2
Trichloroethene ug/L 20 119 60-140136 13 3020ND23.9 27.1
Trichlorofluoromethane ug/L 20 95 60-140108 13 3020ND19.0 21.6
Vinyl chloride ug/L 20 112 60-140122 9 3020ND22.4 24.5
1,2-Dichloroethane-d4 (S)%102 70-130101
4-Bromofluorobenzene (S)%97 70-13098
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746101
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92643625002, 92643625005, 92643625011, 92643625012, 92643625014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880501
Associated Lab Samples:92643625002, 92643625005, 92643625011, 92643625012, 92643625014
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/28/22 11:440.31
1,1,1-Trichloroethane ug/L ND 0.50 12/28/22 11:440.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/28/22 11:440.22
1,1,2-Trichloroethane ug/L ND 0.50 12/28/22 11:440.32
1,1-Dichloroethane ug/L ND 0.50 12/28/22 11:440.37
1,1-Dichloroethene ug/L ND 0.50 12/28/22 11:440.35
1,1-Dichloropropene ug/L ND 0.50 12/28/22 11:440.43
1,2,3-Trichlorobenzene ug/L ND 2.0 12/28/22 11:440.81
1,2,3-Trichloropropane ug/L ND 0.50 12/28/22 11:440.26
1,2,4-Trichlorobenzene ug/L ND 2.0 12/28/22 11:440.64
1,2,4-Trimethylbenzene ug/L ND 0.50 12/28/22 11:440.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/28/22 11:440.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/28/22 11:440.27
1,2-Dichlorobenzene ug/L ND 0.50 12/28/22 11:440.34
1,2-Dichloroethane ug/L ND 0.50 12/28/22 11:440.32
1,2-Dichloropropane ug/L ND 0.50 12/28/22 11:440.36
1,3,5-Trimethylbenzene ug/L ND 0.50 12/28/22 11:440.33
1,3-Dichlorobenzene ug/L ND 0.50 12/28/22 11:440.34
1,3-Dichloropropane ug/L ND 0.50 12/28/22 11:440.28
1,4-Dichlorobenzene ug/L ND 0.50 12/28/22 11:440.33
2,2-Dichloropropane ug/L ND 0.50 12/28/22 11:440.39
2-Chlorotoluene ug/L ND 0.50 12/28/22 11:440.32
4-Chlorotoluene ug/L ND 0.50 12/28/22 11:440.32
Benzene ug/L ND 0.50 12/28/22 11:440.34
Bromobenzene ug/L ND 0.50 12/28/22 11:440.29
Bromochloromethane ug/L ND 0.50 12/28/22 11:440.47
Bromodichloromethane ug/L ND 0.50 12/28/22 11:440.31
Bromoform ug/L ND 0.50 12/28/22 11:440.34
Bromomethane ug/L ND 5.0 12/28/22 11:441.7
Carbon tetrachloride ug/L ND 0.50 12/28/22 11:440.33
Chlorobenzene ug/L ND 0.50 12/28/22 11:440.28
Chloroethane ug/L ND 1.0 12/28/22 11:440.65
Chloroform ug/L ND 0.50 12/28/22 11:440.43
Chloromethane ug/L ND 1.0 12/28/22 11:440.54
cis-1,2-Dichloroethene ug/L ND 0.50 12/28/22 11:440.38
cis-1,3-Dichloropropene ug/L ND 0.50 12/28/22 11:440.36
Dibromochloromethane ug/L ND 0.50 12/28/22 11:440.36
Dibromomethane ug/L ND 0.50 12/28/22 11:440.39
Dichlorodifluoromethane ug/L ND 0.50 12/28/22 11:440.35
Diisopropyl ether ug/L ND 0.50 12/28/22 11:440.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880501
Associated Lab Samples:92643625002, 92643625005, 92643625011, 92643625012, 92643625014
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 12/28/22 11:440.30
Hexachloro-1,3-butadiene ug/L ND 2.0 12/28/22 11:441.5
Isopropylbenzene (Cumene)ug/L ND 0.50 12/28/22 11:440.33
m&p-Xylene ug/L ND 1.0 12/28/22 11:440.71
Methyl-tert-butyl ether ug/L ND 0.50 12/28/22 11:440.42
Methylene Chloride ug/L ND 2.0 12/28/22 11:442.0
n-Butylbenzene ug/L ND 0.50 12/28/22 11:440.49
n-Propylbenzene ug/L ND 0.50 12/28/22 11:440.34
Naphthalene ug/L ND 2.0 12/28/22 11:440.64
o-Xylene ug/L ND 0.50 12/28/22 11:440.34
sec-Butylbenzene ug/L ND 0.50 12/28/22 11:440.40
Styrene ug/L ND 0.50 12/28/22 11:440.29
tert-Butylbenzene ug/L ND 0.50 12/28/22 11:440.32
Tetrachloroethene ug/L ND 0.50 12/28/22 11:440.29
Toluene ug/L ND 0.50 12/28/22 11:440.24
trans-1,2-Dichloroethene ug/L ND 0.50 12/28/22 11:440.40
trans-1,3-Dichloropropene ug/L ND 0.50 12/28/22 11:440.36
Trichloroethene ug/L ND 0.50 12/28/22 11:440.38
Trichlorofluoromethane ug/L ND 1.0 12/28/22 11:440.30
Vinyl chloride ug/L ND 1.0 12/28/22 11:440.39
1,2-Dichloroethane-d4 (S)%114 70-130 12/28/22 11:44
4-Bromofluorobenzene (S)%104 70-130 12/28/22 11:44
Toluene-d8 (S)%103 70-130 12/28/22 11:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880502LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.850 114 60-140
1,1,1-Trichloroethane ug/L 60.050 120 60-140
1,1,2,2-Tetrachloroethane ug/L 56.750 113 60-140
1,1,2-Trichloroethane ug/L 56.150 112 60-140
1,1-Dichloroethane ug/L 59.150 118 60-140
1,1-Dichloroethene ug/L 62.850 126 60-140
1,1-Dichloropropene ug/L 65.350 131 60-140
1,2,3-Trichlorobenzene ug/L 53.050 106 60-140
1,2,3-Trichloropropane ug/L 56.850 114 60-140
1,2,4-Trichlorobenzene ug/L 53.950 108 60-140
1,2,4-Trimethylbenzene ug/L 56.850 114 60-140
1,2-Dibromo-3-chloropropane ug/L 52.350 105 60-140
1,2-Dibromoethane (EDB)ug/L 57.150 114 60-140
1,2-Dichlorobenzene ug/L 54.850 110 60-140
1,2-Dichloroethane ug/L 60.850 122 60-140
1,2-Dichloropropane ug/L 58.350 117 60-140
1,3,5-Trimethylbenzene ug/L 57.750 115 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880502LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 54.850 110 60-140
1,3-Dichloropropane ug/L 58.450 117 60-140
1,4-Dichlorobenzene ug/L 53.050 106 60-140
2,2-Dichloropropane ug/L 60.950 122 60-140
2-Chlorotoluene ug/L 56.450 113 60-140
4-Chlorotoluene ug/L 57.150 114 60-140
Benzene ug/L 53.350 107 60-140
Bromobenzene ug/L 54.150 108 60-140
Bromochloromethane ug/L 57.550 115 60-140
Bromodichloromethane ug/L 55.550 111 60-140
Bromoform ug/L 53.450 107 60-140
Bromomethane ug/L 56.750 113 60-140
Carbon tetrachloride ug/L 55.250 110 60-140
Chlorobenzene ug/L 54.850 110 60-140
Chloroethane ug/L 69.950 140 60-140
Chloroform ug/L 57.050 114 60-140
Chloromethane ug/L 57.050 114 60-140
cis-1,2-Dichloroethene ug/L 59.550 119 60-140
cis-1,3-Dichloropropene ug/L 58.650 117 60-140
Dibromochloromethane ug/L 55.550 111 60-140
Dibromomethane ug/L 51.150 102 60-140
Dichlorodifluoromethane ug/L 55.050 110 60-140
Diisopropyl ether ug/L 59.650 119 60-140
Ethylbenzene ug/L 54.650 109 60-140
Hexachloro-1,3-butadiene ug/L 56.750 113 60-140
Isopropylbenzene (Cumene)ug/L 53.150 106 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 59.550 119 60-140
Methylene Chloride ug/L 52.750 105 60-140
n-Butylbenzene ug/L 61.450 123 60-140
n-Propylbenzene ug/L 56.950 114 60-140
Naphthalene ug/L 55.150 110 60-140
o-Xylene ug/L 54.950 110 60-140
sec-Butylbenzene ug/L 57.450 115 60-140
Styrene ug/L 55.350 111 60-140
tert-Butylbenzene ug/L 45.150 90 60-140
Tetrachloroethene ug/L 51.050 102 60-140
Toluene ug/L 52.850 106 60-140
trans-1,2-Dichloroethene ug/L 61.950 124 60-140
trans-1,3-Dichloropropene ug/L 57.450 115 60-140
Trichloroethene ug/L 56.450 113 60-140
Trichlorofluoromethane ug/L 54.350 109 60-140
Vinyl chloride ug/L 58.350 117 60-140
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3880503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643625014
3880504
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 250 122 60-140115 6 30250ND305288
1,1,1-Trichloroethane ug/L 250 135 60-140130 4 30250ND336325
1,1,2,2-Tetrachloroethane ug/L 250 125 60-140117 7 30250ND313292
1,1,2-Trichloroethane ug/L 250 121 60-140116 4 30250ND302291
1,1-Dichloroethane ug/L 250 133 60-140127 5 30250ND333317
1,1-Dichloroethene ug/L M125014260-140134 6 30250ND355335
1,1-Dichloropropene ug/L M125014460-140141 3 30250ND361352
1,2,3-Trichlorobenzene ug/L 250 111 60-140108 3 30250ND277270
1,2,3-Trichloropropane ug/L 250 126 60-140119 6 30250ND315296
1,2,4-Trichlorobenzene ug/L 250 110 60-140107 3 30250ND276269
1,2,4-Trimethylbenzene ug/L 250 128 60-140121 1 30250157018901870
1,2-Dibromo-3-
chloropropane ug/L 250 109 60-140106 2 30250ND272266
1,2-Dibromoethane (EDB)ug/L 250 124 60-140115 7 30250ND309288
1,2-Dichlorobenzene ug/L 250 118 60-140111 6 30250ND294277
1,2-Dichloroethane ug/L 250 136 60-140130 4 30250ND339325
1,2-Dichloropropane ug/L 250 131 60-140123 7 30250ND328307
1,3,5-Trimethylbenzene ug/L 250 129 60-140124 2 30250275598585
1,3-Dichlorobenzene ug/L 250 118 60-140114 3 30250ND294284
1,3-Dichloropropane ug/L 250 130 60-140119 9 30250ND324297
1,4-Dichlorobenzene ug/L 250 115 60-140111 4 30250ND287277
2,2-Dichloropropane ug/L 250 133 60-140127 4 30250ND331317
2-Chlorotoluene ug/L 250 133 60-140130 2 30250ND332325
4-Chlorotoluene ug/L 250 126 60-140121 4 30250ND315302
Benzene ug/L 250 121 60-140115 5 302504.6J 308 292
Bromobenzene ug/L 250 117 60-140115 2 30250ND294287
Bromochloromethane ug/L 250 126 60-140120 5 30250ND314299
Bromodichloromethane ug/L 250 122 60-140114 6 30250ND304285
Bromoform ug/L 250 110 60-140103 7 30250ND275256
Bromomethane ug/L 250 93 60-140108 15 30250ND232270
Carbon tetrachloride ug/L 250 124 60-140119 4 30250ND311298
Chlorobenzene ug/L 250 123 60-140117 5 30250ND307293
Chloroethane ug/L M125015360-140144 6 30250ND383361
Chloroform ug/L 250 130 60-140124 5 30250ND326309
Chloromethane ug/L 250 115 60-140113 2 30250ND289282
cis-1,2-Dichloroethene ug/L 250 134 60-140127 5 30250ND335317
cis-1,3-Dichloropropene ug/L 250 124 60-140118 5 30250ND310296
Dibromochloromethane ug/L 250 119 60-140108 10 30250ND297270
Dibromomethane ug/L 250 114 60-140107 6 30250ND284269
Dichlorodifluoromethane ug/L 250 108 60-140104 4 30250ND269259
Diisopropyl ether ug/L 250 129 60-140121 6 30250ND321303
Ethylbenzene ug/L 250 129 60-140121 3 30250431754733
Hexachloro-1,3-butadiene ug/L 250 115 60-140113 2 30250ND288282
Isopropylbenzene(Cumene)ug/L 250 121 60-140114 5 3025093.1 396 377
m&p-Xylene ug/L 500 125 60-140113 4 30500101016401580
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3880503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92643625014
3880504
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 250 127 60-140120 6 30250ND317299
Methylene Chloride ug/L 250 119 60-140114 4 30250ND298286
n-Butylbenzene ug/L M125014760-140145 2 30250ND368362
n-Propylbenzene ug/L 250 122 60-140120 1 30250249554548
Naphthalene ug/L 250 116 60-140113 2 30250106397389
o-Xylene ug/L 250 123 60-140115 4 30250136443424
sec-Butylbenzene ug/L 250 134 60-140130 3 30250ND334324
Styrene ug/L 250 121 60-140114 6 30250ND303285
tert-Butylbenzene ug/L 250 100 60-14097 4 30250ND251242
Tetrachloroethene ug/L 250 113 60-140109 3 30250ND281272
Toluene ug/L 250 120 60-140114 5 3025025.2 325 310
trans-1,2-Dichloroethene ug/L 250 138 60-140131 5 30250ND345327
trans-1,3-Dichloropropene ug/L 250 121 60-140115 6 30250ND303286
Trichloroethene ug/L 250 126 60-140120 5 30250ND316300
Trichlorofluoromethane ug/L 250 120 60-140115 5 30250ND300286
Vinyl chloride ug/L 250 123 60-140117 5 30250ND306292
1,2-Dichloroethane-d4 (S)%118 70-130111
4-Bromofluorobenzene (S)%103 70-130101
Toluene-d8 (S)%102 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92643625
CROWN FOOD MART
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92643625
CROWN FOOD MART
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92643625001 745606SW-01-192 SM 6200B
92643625002 746101SW-02-192 SM 6200B
92643625003 745606SW-03-192 SM 6200B
92643625004 745606SW-11 SM 6200B
92643625005 746101SW-12 SM 6200B
92643625006 745606SW-13 SM 6200B
92643625007 745606SW-14 SM 6200B
92643625008 745606DUP-3 SM 6200B
92643625009 745606MW-2 SM 6200B
92643625010 745606MW-16 SM 6200B
92643625011 746101DUP-1 SM 6200B
92643625012 746101MW-10 SM 6200B
92643625013 745606MW-12 SM 6200B
92643625014 746101MW-6 SM 6200B
92643625015 745606MW-7 SM 6200B
92643625016 745606MW-1 SM 6200B
92643625017 745606MW-3 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 02:36 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 49
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