23052_Southern Steel_Final Grade Sampling Report_20230308

#C-1269 Engineering
#C-245 Geology

Final Grade Soil Sampling Report

Southern Steel Brownfields Property
Brownfields Project ID No. 23052-19-060

3015 Wilkinson Boulevard
Charlotte, North Carolina

H&H Job No. ANR-007
March 8, 2023

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Final Grade Soil Sampling Report
Southern Steel Brownfields Property
3015 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 23052-19-060
H&H Job No. ANR-007

Table of Contents

1.0 Introduction .............................................................................................................................1 
2.0 Final Grade Sampling Activities.............................................................................................2 
2.1 Soil Sampling Methodology ..................................................................................................2 
2.2 Soil Sampling Results ............................................................................................................3 
2.3 Risk Calculations ...................................................................................................................5 
3.0 Summary and Conclusions ....................................................................................................6 

List of Tables

Table 1 Final Grade Soil Sample Lithology
Table 2 Final Grade Soil Sample Analytical Summary

List of Figures

Figure 1 Site Location Map
Figure 2 Final Grade Soil Sample Location Map

List of Appendices

Appendix A Laboratory Analytical Report
Appendix B DEQ Calculator Input/Output Forms
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Final Grade Soil Sampling Report
Southern Steel Brownfields Property
3015 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 23052-19-060
H&H Job No. ANR-007

1.0 Introduction

On behalf of Wilkinson Steel Yard, LLC, Hart & Hickman, P.C. (H&H) has prepared this Final
Grade Soil Sampling Report to summarize post-development final grade soil sampling activities
at the Southern Steel Brownfields property (Brownfields Project No. 23052-19-060) located at
3015 Wilkinson Boulevard in Charlotte, Mecklenburg County, North Carolina (Site). A Site
location map is provided as Figure 1.

The Site consists of one parcel of industrial land (Mecklenburg County Parcel Identification
Number [PIN] 11701118) that is approximately 5.2 acres. A Norfolk Southern railroad right-of-
way is present along the southern portion of the Site. To date, redevelopment at the Site includes
the construction of Building C, a 20,077-square foot warehouse building, on the eastern portion
of the Site with associated landscaped areas, asphalt and concrete parking/driveways, and
concrete loading docks/walkways. Timing for the development of the central and western
portions of the Site (Buildings A and B) is unknown at this time. The current and proposed
building locations are shown on Figure 2.

In accordance with the DEQ-approved Environmental Management Plan (EMP) dated March 4,
2021 and the DEQ-approved Final Grade Sampling Work Plan dated February 7, 2023, H&H
conducted final grade soil sampling at locations in the vicinity of Building C that are not covered
with buildings, concrete or asphaltic paved (hardscape) surfaces, or other impervious surfaces.
The final grade soil sampling activities are detailed in Section 2.0 below.
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2.0 Final Grade Sampling Activities

On February 20, 2023, H&H conducted final grade soil sampling activities at the Site to evaluate
the potential for impacts in shallow soil that may pose unacceptable exposure risks to
industrial/commercial occupants. The soil sampling activities were conducted in general
accordance with the DEQ Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment
and Cleanup (Guidelines) dated September 2022 and the most recent versions of U.S.
Environmental Protection Agency (EPA) Region IV Laboratory Services and Applied Science
Division (LSASD) Field Branches Quality System and Technical Procedures guidance.

2.1 Soil Sampling Methodology

Prior to conducting field work, H&H contacted North Carolina 811, the public utility locator, to
mark subsurface utilities located on the Site. H&H also coordinated with the Site construction
manager to determine if any utilities had been recently installed at the Site that could interfere
with the proposed sample collections.

Based on review of the Site landscaping plan and observations at the Site, landscaped areas were
divided into five final grade evaluation areas (FG 1 through FG-5). Soil borings were advanced
in each final grade evaluation area for collection of aliquot soil samples. The final grade
evaluation areas and soil boring locations are shown on Figure 2.

H&H advanced four to six soil borings in each composite sample area using a decontaminated
stainless-steel hand auger to a depth of approximately two feet below ground surface (ft bgs).
Soil samples were collected from 0-1 ft bgs and 1-2 ft bgs, observed for lithologic description,
odor, and staining, and field screened for volatile organic vapors using a calibrated
photoionization detector (PID). H&H observed primarily brown silts and clays with some sands.
PID readings from the soil samples ranged from 1.2 to 8.1 parts per million (ppm). Field
personnel did not identify obvious evidence of soil impacts in the aliquot soil samples. Soil
sampling lithology and field screening results are summarized in Table 1.
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Based on field screening results, H&H collected one grab soil sample from each of the sample
areas for laboratory analysis of volatile organic compounds (VOCs) by EPA Method 8260. Each
grab sample was collected from an undisturbed portion of an aliquot sample in each final grade
evaluation area.

A composite soil sample was generated from aliquots collected from each of the soil borings
within a designated composite sample area. The soil sample aliquots were homogenized within a
designated plastic bag prior to placement into laboratory glassware. The composite soil samples
were analyzed for semi-VOCs (SVOCs) by EPA Method 8270, hexavalent chromium by EPA
Method 7199, and RCRA metals (arsenic, barium, cadmium, total chromium, lead, mercury,
selenium, and silver) by EPA Methods 6020/7471.

For quality assurance/quality control (QA/QC) purposes, H&H also collected one duplicate
composite soil sample and one duplicate grab sample from area FG-1 for the same analyses as
the parent samples.

Upon collection, the soil samples were labeled with the sample identification, date, time, and
requested analyses then placed in a laboratory-supplied cooler with ice. The grab and composite
soil samples were delivered to Waypoint Analytical for laboratory analysis under standard chain
of custody protocol.

Following sampling activities, the soil borings were properly abandoned with hydrated bentonite.
Additionally, the soil boring locations were estimated using a hand-held global positioning
system unit. A discussion of the results of the laboratory analyses is provided below.

2.2 Soil Sampling Results

The laboratory analytical results for the surficial final grade soil samples are summarized in
Table 2, and the laboratory report is included in Appendix A. The laboratory analytical results
were compared to the DEQ Residential and Industrial/Commercial health-based Preliminary Soil
Remediation Goals (PSRGs). In addition to the PSRGs, metals concentrations were compared to
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regional background levels published in Elements in North American Soils by Dragun and
Chekiri, 2005.

VOCs
Laboratory analytical results indicated the presence of the VOCs acetone, carbon disulfide,
n-hexane, and methylene chloride at estimated (J-flag) concentrations above the laboratory
method detection limits (MDLs) but below the reporting limits in one or more final grade soil
evaluation areas. No VOCs were detected above their respective Residential or
Industrial/Commercial PSRGs.

SVOCs
One or more polynuclear aromatic hydrocarbons (PAHs) were detected at estimated (J-flag)
concentrations above the laboratory MDLs in each composite soil sample. Benzo(a)pyrene was
detected in samples FG-4 (0.509 J mg/kg) and FG-5 (0.575 J mg/kg) at concentrations above the
Residential PSRG of 0.11 mg/kg but below the Industrial/Commercial PSRG of 2.1 mg/kg. The
remaining PAH detections are below the Residential and Industrial/Commercial PSRGs.

Metals
Several metals were detected at concentrations above laboratory MDLs in the final grade soil
samples collected at the Site. Arsenic was detected at concentrations ranging from 1.87 mg/kg to
3.52 mg/kg, which exceed its Residential PSRG of 0.68 mg/kg. The detections in the FG-1
duplicate sample FG-DUP (3.01 mg/kg), FG-3 (3.34 mg/kg), and FG-4 (3.52 mg/kg) also exceed
the Industrial/Commercial PSRG of 3.0 mg/kg. However, the arsenic concentrations are below
the published average background concentration of 4.8 mg/kg for North Carolina soils and are
likely naturally occurring. Hexavalent chromium was not detected above the laboratory MDLs
in any of the final grade soil samples. The remaining metals detections are below the PSRGs
and/or generally consistent with published background levels.
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2.3 Risk Calculations

The DEQ health-based PSRGs are very conservative and based on the lower of a Target
Carcinogenic Risk (TCR) of 1 x 10-6 for potential carcinogenic risks and a Target Hazard
Quotient (THQ) of 0.2 for potential non-carcinogenic risks. The DEQ and EPA acceptable risks
for potential carcinogenic risks is a cumulative lifetime incremental carcinogenic risk (LICR) of
1 x 10-4 or less and a cumulative hazard index (HI) of 1.0 or less for non-carcinogenic risks.
Therefore, H&H utilized the DEQ Risk Calculator (January 2023) to further evaluate cumulative
risks to occupants and workers based on the final grade soil sample analytical results.

The highest concentration of each compound detected in any final grade soil sample was used to
model a hypothetical worst-case exposure risk under the residential, non-residential worker, and
construction worker scenarios. Results of risk calculations are presented in the table below:

Exposure Scenario Cumulative LICR Cumulative HI Risk Exceeded?
Residential 1.2 x 10-5 0.16 No
Non-Residential Worker 1.5 x 10-6 0.012 No
Construction Worker 2.4 x 10-7 0.16 No

As shown in the table above, the results of the risk calculations indicate that the calculated
cumulative carcinogenic and non-carcinogenic risks are below the DEQ and EPA acceptable
levels for residential, non-residential worker, and construction worker scenarios. The DEQ Risk
Calculator input/output forms are provided as Appendix B.

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3.0 Summary and Conclusions

On February 20, 2023, H&H completed final grade soil assessment activities at the Southern
Steel Brownfields property (Brownfields Project No. 23052-19-060) located at 3015 Wilkinson
Boulevard in Charlotte, North Carolina. Final grade soil sampling was performed at locations in
the vicinity of Building C in the eastern portion of the Site in accordance with the DEQ-approved
EMP dated March 4, 2021 and the DEQ-approved Final Grade Sampling Work Plan dated
February 7, 2023. The schedule for construction of Buildings A and B is unknown at this time.
Final grade soil sampling will be performed in those areas at a later date.

Laboratory analytical results indicate the presence of benzo(a)pyrene and arsenic at
concentrations above the DEQ Residential PSRGs. The concentration of arsenic in three
composite soil samples also exceeds the Industrial/Commercial PSRG. However, the detected
arsenic concentrations in the final grade soil samples are consistent with naturally occurring
levels in North Carolina soils.

H&H utilized the DEQ Risk Calculator to further evaluate cumulative risks to occupants and
workers based on the highest concentration of each compound detected in any final grade
evaluation area at the Site. Results of the hypothetical worst-case risk calculations indicate that
cumulative carcinogenic and non-carcinogenic risks are below the DEQ and EPA acceptable
levels for the residential, non-residential worker, and construction worker exposure scenarios.

The eastern portion of the Site near Building C has been redeveloped for its intended use in
accordance with the DEQ-approved EMP and the recorded Brownfields Agreement.

Table 1
Summary of Final Grade Soil Sample Lithology
Southern Steel Brownfields Property
3015 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 23052-19-060
H&H Project No. ANR-007
Composite
Sample Area
Composite
Sample Aliquot
Sample
Date
Aliquot Selected
for VOC Analysis
Depth
(ft bgs)
Moisture
Content Stiffness Color Lithology PID Readings(1)
A --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Light Brown
Light Brown
Clayey Silt with some Fine Sand, rocks
Clayey Silt with some Fine Sand, rocks
4.7
5.2
B --
--
0-1
1-2
Moist
Moist
Loose
Loose
Light Brown
Light Brown
Silty Sand, rocks
Silty Sand, rocks
4.9
4.6
C --
--
0-1
1-2
Moist
Moist
Loose
Loose
Light Brown
Light Brown
Silty Sand, rocks
Silty Sand, rocks
5.2
4.1
D --
x
0-1
1-2
Moist
Moist
Loose
Loose
Light Brown
Light Brown
Silty Sand
Silty Clay
4.6
5.5
E --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Light Brown to White
Light Brown to White
Silty Clay
Silty Clay
6.7
3.1
A --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Light Brown with White
Light Brown with White
Clayey Silt with some Fine Sand
Clayey Silt with some Fine Sand
3.8
4.4
B --
--
0-1
1-2
Moist
Moist
Loose
Loose
Light Brown with White
Light Brown with White
Silty Sand with few Clay
Silty Sand with few Clay
3.6
4.7
C --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Clayey Silt with few Sand, rocks
Clayey Silt with few Sand, rocks
6.1
7.4
D --
x
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Red-Brown
Clayey Silt with few Sand
Clayey Silt
4.5
8.1
A --
--
0-1
1-2
Wet
Wet
Medium Stiff
Medium Stiff
Light Brown
Light Brown
Silty Clay with some Sand
Silty Clay with some Sand
1.6
2.9
B --
x
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Grey
Grey
Silty Clay with some Sand, rocks & debris
Silty Clay with some Sand, rocks & debris
3.4
6.9
C --
--
0-1
1-2
Moist
Moist
Loose
Loose
Grey
Grey
Silty Sand with few Clay, rocks, debris & concrete
Silty Sand with few Clay, rocks, debris & concrete
2.9
1.8
A --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Clayey Silt with some Sand, rocks & debris
Clayey Silt with some Sand, rocks & debris
2.8
3.7
B --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Grey-Brown
Grey-Brown
Clayey Silt with some Sand, rocks & debris
Clayey Silt with some Sand, rocks & debris
4.5
5.3
C --
x
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Silty Sand with some Clay, rocks & debris
Silty Sand with some Clay, rocks & debris
2.8
6.1
D --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown with White
Brown with White
Silty Sand with some Clay, rocks & debris
Silty Sand with some Clay, rocks & debris
4.6
6.3
E --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Grey-Brown
Grey-Brown
Silty Sand with few Clay, rocks & debris
Silty Sand with few Clay, rocks & debris
5.3
4.8
F --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Silty Sand with some Clay, rocks
Silty Sand with some Clay, rocks
4.7
5.2
A --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Silty Sand with few Clay, rocks
Silty Sand with few Clay, rocks
1.6
1.2
B --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Silty Sand with some Clay, rocks
Silty Sand with some Clay, rocks
3.6
4.4
C --
--
0-1
1-2
Moist
Moist
Medium Stiff
Medium Stiff
Brown
Brown
Clayey Silt with some Sand, rocks
Silty Clay with few Sand, rocks
3.9
4.8
D --
x
0-1
1-2
Moist
Moist
Stiff
Stiff
Brown
Brown
Silty Clay with few Sand, rocks
Silty Clay with few Sand, rocks
4.9
5.1
FG-1*
Notes:
1) Background PID readings were 0.0 ppm.
* = selected for duplicate sample (FG-DUP); -- = not applicable
VOC= Volatile Organic Compound; ft bgs = feet below the ground surface; PID = Photoionization Detector
FG-2
FG-3
FG-4
FG-5
2/20/2023
2/20/2023
2/20/2023
2/20/2023
2/20/2023
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Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Final Grade Soil Sample Analytical Summary
Southern Steel Brownfields Property
3015 Wilkinson Boulevard
Charlotte, North Carolina
Brownfields Project No. 23052-19-060
H&H Project No. ANR-007
Range Mean
VOCs by EPA 8260 (mg/kg)
Acetone <0.003 0.008 J 0.005 J 0.006 J 0.005 J 0.015 J 14,000 210,000 ----
Carbon Disulfide <0.0008 <0.0008 <0.0008 <0.0008 <0.0007 0.0009 J 160 740 ----
n-Hexane <0.0008 <0.0008 <0.0008 0.003 J <0.0007 <0.0008 130 540 ----
Methylene Chloride 0.002 J <0.001 0.001 J <0.001 <0.001 <0.001 58 650 ----
SVOCs by EPA Method 8270 (mg/kg)
Benzo(a)anthracene <0.174 <0.176 <0.167 <0.174 0.455 J 0.507 J 1.1 21 ----
Benzo(a)pyrene <0.184 <0.186 <0.177 <0.184 0.509 J 0.575 J 0.11 2.1 ----
Benzo(b)fluoranthene <0.182 <0.185 0.227 J 0.191 J 0.647 J 0.787 J 1.1 21 ----
Benzo(g,h,i)perylene <0.170 <0.172 <0.164 <0.170 0.323 J 0.364 J NS NS ----
Benzo(k)fluoranthene <0.171 <0.174 <0.165 <0.171 0.246 J 0.246 J 11 210 ----
Chrysene <0.177 <0.180 <0.171 <0.178 0.441 J 0.505 J 110 2,100 ----
Fluoranthene 0.159 J <0.156 0.219 J 0.171 J 0.654 J 0.469 J 480 6,000 ----
Indeno(1,2,3-cd)pyrene <0.224 <0.227 <0.216 <0.224 0.332 J 0.379 J 1.1 21 ----
Phenanthrene <0.260 <0.264 <0.251 <0.260 0.370 J <0.250 NS NS ----
Pyrene <0.167 <0.170 0.218 J 0.188 J 0.704 J 0.588 J 360 4,500 ----
Metals by EPA Methods 6020/7199/7471 (mg/kg)
Arsenic 1.87 3.01 2.75 3.34 3.52 2.21 0.68 3.0 1.0 - 18 4.8
Barium 46.4 50.8 36.7 67.0 79.8 58.8 3,100 47,000 50 - 1,000 356
Cadmium 0.0561 J 0.145 J 0.0410 J 0.0657 J 0.0936 J 0.0819 J 1.4 20 1.0 - 10 4.3
Total Chromium 20.4 43.2 13.4 30.7 21.6 29.7 NS NS 7.0 - 300 65
Chromium (III)20.4 43.2 13.4 30.7 21.6 29.7 23,000 350,000 NS NS
Chromium (VI)<0.176 <0.181 <0.175 <0.176 <0.157 <0.172 0.31 6.5 NS NS
Lead 57.9 179 30.8 74.5 65.0 36.9 400 800 ND - 50 16
Mercury (Total)<0.0279 <0.0248 <0.0260 <0.0281 <0.0254 0.0579 J 4.7 70 0.03 - 0.52 0.121
Selenium 0.639 0.851 1.16 1.01 0.643 0.796 78 1,200 <0.1 - 0.8 0.42
Silver 0.0177 J 0.0202 J 0.0142 J 0.0233 J 0.0299 J 0.0259 J 78 1,200 ND - 5.0 NS
Notes:
1) NC Department of Environmental Quality (DEQ) Health Based Preliminary Soil Remediation Goals (PSRGs) dated January 2023 and based upon a carcinogenic total risk of 1.0E-06 and a
non-carcinogenic target hazard quotient of 0.1.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. North Carolina values are generally shown;
however, southeastern and conterminous US soil values are shown for cadmium and silver.
Composite soil samples collected from 0-2 feet below ground surface (ft bgs). VOC samples collected as a grab sample from the 1-2 ft bgs interval.
Refer to Figure 2 for sample locations.
With the exception of metals, only constituents detected in at least one sample are shown.
Compounds concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Bold values exceed the Residential Health-Based PSRG.
VOCs = volatile organic compounds; SVOCs = semi-VOCs
NS = not specified; ND = not detected.
J = Estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limit
2/20/2023
Regional Background Metal
Concentrations (2)
(mg/kg)
2/20/2023Sample Date
FG-2 FG-3 FG-4
2/20/2023 2/20/2023 2/20/2023
Sample ID Health Based PSRGs(1)
(mg/kg)FG-5
Residential Industrial/
Commercial
FG-1/FG-DUP
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Table 2 (Page 1 of 1)
Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed June, 2022.
SITE LOCATION MAP
SOUTHERN STEEL BROWNFIELDS PROPERTY3015 WILKINSON BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE: 1-30-23
JOB NO: ANR-007
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
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U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2022
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
ANDREW JACKSON HIGHWAY
ASHLEY ROAD
ASHLEY ROAD
WILKINSON BOULEVARD
AS
H
L
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R
O
A
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REVISION NO. 0
JOB NO. ANR-007
DATE: 3-3-23
FIGURE NO. 2
SOUTHERN STEEL BROWNFIELDS PROPERTY
3015 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
RAILROAD TRACKS
AS BUILT BUILDING FOOTPRINT
PROPOSED BUILDING FOOTPRINT
FG-1 SOIL ALIQUOT SAMPLE
LOCATION
FG-2 SOIL ALIQUOT SAMPLE
LOCATION
FG-3 SOIL ALIQUOT SAMPLE
LOCATION
FG-4 SOIL ALIQUOT SAMPLE
LOCATION
FG-5 SOIL ALIQUOT SAMPLE
LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FG-1A
FG-1B
FG-1C
FG-1D
FG-1E
FG-2A
FG-2B
FG-2C
FG-2D
FG-3B
FG-3A
FG-3C
FG-4BFG-4DFG-4F
FG-4E FG-4C FG-4A
FG-5A
FG-5B
FG-5C
FG-5D
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2021).
2. COMPOSITE SOIL SAMPLE AREAS INCLUDE GRASS AND
LANDSCAPED AREAS.
PROPOSED
BUILDING A
PROPOSED
BUILDING B BUILDING C
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Appendix A
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/28/2023
Hart & Hickman (Charlotte) Bo Cappleman
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-051-0030 Client Project Description: ANR.007
Dear Bo Cappleman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/20/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 82
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-051-0030
Page 2 of 82
Report Number:
Sample Summary Table
Client Project Description:
23-051-0030
ANR.007
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
02/20/2023 10:45Solids 89221 FG-1 02/20/2023 16:39
02/20/2023 10:45Solids 89221 FG-1 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 10:45Solids 89221 FG-1 02/20/2023 16:39 7471A WP MTN -
02/20/2023 10:45Solids 89221 FG-1 02/20/2023 16:39 6020B WP MTN -
02/20/2023 12:45Solids 89222 FG-2 02/20/2023 16:39
02/20/2023 12:45Solids 89222 FG-2 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 12:45Solids 89222 FG-2 02/20/2023 16:39 7471A WP MTN -
02/20/2023 12:45Solids 89222 FG-2 02/20/2023 16:39 6020B WP MTN -
02/20/2023 13:45Solids 89223 FG-3 02/20/2023 16:39
02/20/2023 13:45Solids 89223 FG-3 02/20/2023 16:39 7471A WP MTN -
02/20/2023 13:45Solids 89223 FG-3 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 13:45Solids 89223 FG-3 02/20/2023 16:39 6020B WP MTN -
02/20/2023 14:55Solids 89224 FG-4 02/20/2023 16:39
02/20/2023 14:55Solids 89224 FG-4 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 14:55Solids 89224 FG-4 02/20/2023 16:39 6020B WP MTN -
02/20/2023 14:55Solids 89224 FG-4 02/20/2023 16:39 7471A WP MTN -
02/20/2023 16:15Solids 89225 FG-5 02/20/2023 16:39
02/20/2023 16:15Solids 89225 FG-5 02/20/2023 16:39 7471A WP MTN -
02/20/2023 16:15Solids 89225 FG-5 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 16:15Solids 89225 FG-5 02/20/2023 16:39 6020B WP MTN -
02/20/2023 10:45Solids 89226 FG-DUP 02/20/2023 16:39
02/20/2023 10:45Solids 89226 FG-DUP 02/20/2023 16:39 7471A WP MTN -
02/20/2023 10:45Solids 89226 FG-DUP 02/20/2023 16:39 SW-7199 WP MTN -
02/20/2023 10:45Solids 89226 FG-DUP 02/20/2023 16:39 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 82
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-051-0030
Report Limit
Project:ANR.007
V 89221FG-1
1.87 02/27/2023 23:396020BArsenicmg/Kg - dry 0.107
46.4 02/27/2023 23:396020BBariummg/Kg - dry 0.053
J0.0561 02/27/2023 23:396020BCadmiummg/Kg - dry 0.0324
20.4 02/27/2023 23:396020BChromiummg/Kg - dry 0.145
57.9 02/27/2023 23:396020BLeadmg/Kg - dry 0.0388
0.639 02/27/2023 23:396020BSeleniummg/Kg - dry 0.129
J0.0177 02/27/2023 23:396020BSilvermg/Kg - dry 0.0084
J0.002 02/21/2023 17:518260DMethylene Chloride mg/Kg - dry 0.001
J0.159 02/27/2023 13:198270EFluoranthenemg/Kg - dry 0.154
20.2 02/21/2023 17:11SW-DRYWT Moisture %
V 89222FG-2
2.75 02/27/2023 23:436020BArsenicmg/Kg - dry 0.103
36.7 02/27/2023 23:436020BBariummg/Kg - dry 0.051
J0.0410 02/27/2023 23:436020BCadmiummg/Kg - dry 0.0312
13.4 02/27/2023 23:436020BChromiummg/Kg - dry 0.140
30.8 02/27/2023 23:436020BLeadmg/Kg - dry 0.0374
1.16 02/27/2023 23:436020BSeleniummg/Kg - dry 0.124
J0.0142 02/27/2023 23:436020BSilvermg/Kg - dry 0.0081
J0.005 02/21/2023 18:188260DAcetonemg/Kg - dry 0.002
J0.001 02/21/2023 18:188260DMethylene Chloride mg/Kg - dry 0.001
J0.227 02/27/2023 13:428270EBenzo(b)fluoranthene mg/Kg - dry 0.176
J0.219 02/27/2023 13:428270EFluoranthenemg/Kg - dry 0.148
J0.218 02/27/2023 13:428270EPyrenemg/Kg - dry 0.161
17.2 02/21/2023 17:11SW-DRYWT Moisture %
V 89223FG-3
3.34 02/27/2023 23:466020BArsenicmg/Kg - dry 0.107
67.0 02/27/2023 23:466020BBariummg/Kg - dry 0.053
J0.0657 02/27/2023 23:466020BCadmiummg/Kg - dry 0.0324
30.7 02/27/2023 23:466020BChromiummg/Kg - dry 0.145
74.5 02/27/2023 23:466020BLeadmg/Kg - dry 0.0388
1.01 02/27/2023 23:466020BSeleniummg/Kg - dry 0.129
J0.0233 02/27/2023 23:466020BSilvermg/Kg - dry 0.0084
J0.006 02/21/2023 18:458260DAcetonemg/Kg - dry 0.003
J0.003 02/21/2023 18:458260Dn-Hexane mg/Kg - dry 0.0008
J0.191 02/27/2023 14:048270EBenzo(b)fluoranthene mg/Kg - dry 0.183
J0.171 02/27/2023 14:048270EFluoranthenemg/Kg - dry 0.154
Page 4 of 82
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-051-0030
Report Limit
Project:ANR.007
V 89223FG-3
J0.188 02/27/2023 14:048270EPyrenemg/Kg - dry 0.168
20.3 02/21/2023 17:11SW-DRYWT Moisture %
V 89224FG-4
3.52 02/27/2023 23:506020BArsenicmg/Kg - dry 0.0953
79.8 02/27/2023 23:506020BBariummg/Kg - dry 0.047
J0.0936 02/27/2023 23:506020BCadmiummg/Kg - dry 0.0288
21.6 02/27/2023 23:506020BChromiummg/Kg - dry 0.129
65.0 02/27/2023 23:506020BLeadmg/Kg - dry 0.0345
0.643 02/27/2023 23:506020BSeleniummg/Kg - dry 0.114
J0.0299 02/27/2023 23:506020BSilvermg/Kg - dry 0.0075
J0.005 02/21/2023 19:138260DAcetonemg/Kg - dry 0.002
J0.455 02/27/2023 14:278270EBenzo(a)anthracene mg/Kg - dry 0.154
J0.509 02/27/2023 14:278270EBenzo(a)pyrene mg/Kg - dry 0.163
J0.647 02/27/2023 14:278270EBenzo(b)fluoranthene mg/Kg - dry 0.162
J0.323 02/27/2023 14:278270EBenzo(g,h,i)perylene mg/Kg - dry 0.151
J0.246 02/27/2023 14:278270EBenzo(k)fluoranthene mg/Kg - dry 0.152
J0.441 02/27/2023 14:278270EChrysenemg/Kg - dry 0.158
J0.654 02/27/2023 14:278270EFluoranthenemg/Kg - dry 0.137
J0.332 02/27/2023 14:278270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.199
J0.370 02/27/2023 14:278270EPhenanthrenemg/Kg - dry 0.231
J0.704 02/27/2023 14:278270EPyrenemg/Kg - dry 0.149
10.3 02/21/2023 17:11SW-DRYWT Moisture %
V 89225FG-5
2.21 02/28/2023 00:016020BArsenicmg/Kg - dry 0.103
58.8 02/28/2023 00:016020BBariummg/Kg - dry 0.051
J0.0819 02/28/2023 00:016020BCadmiummg/Kg - dry 0.0311
29.7 02/28/2023 00:016020BChromiummg/Kg - dry 0.139
36.9 02/28/2023 00:016020BLeadmg/Kg - dry 0.0373
0.796 02/28/2023 00:016020BSeleniummg/Kg - dry 0.123
J0.0259 02/28/2023 00:016020BSilvermg/Kg - dry 0.0081
J0.0579 02/27/2023 12:537471AMercury (Total)mg/Kg - dry 0.0267
J0.015 02/21/2023 19:408260DAcetonemg/Kg - dry 0.002
J0.0009 02/21/2023 19:408260DCarbon Disulfide mg/Kg - dry 0.0008
J0.507 02/27/2023 14:508270EBenzo(a)anthracene mg/Kg - dry 0.167
J0.575 02/27/2023 14:508270EBenzo(a)pyrene mg/Kg - dry 0.176
J0.787 02/27/2023 14:508270EBenzo(b)fluoranthene mg/Kg - dry 0.175
Page 5 of 82
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-051-0030
Report Limit
Project:ANR.007
V 89225FG-5
J0.364 02/27/2023 14:508270EBenzo(g,h,i)perylene mg/Kg - dry 0.163
J0.246 02/27/2023 14:508270EBenzo(k)fluoranthene mg/Kg - dry 0.164
J0.505 02/27/2023 14:508270EChrysenemg/Kg - dry 0.170
J0.469 02/27/2023 14:508270EFluoranthenemg/Kg - dry 0.148
J0.379 02/27/2023 14:508270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.215
J0.588 02/27/2023 14:508270EPyrenemg/Kg - dry 0.161
16.9 02/21/2023 17:11SW-DRYWT Moisture %
V 89226FG-DUP
3.01 02/28/2023 00:276020BArsenicmg/Kg - dry 0.109
50.8 02/28/2023 00:276020BBariummg/Kg - dry 0.054
J0.145 02/28/2023 00:276020BCadmiummg/Kg - dry 0.0329
43.2 02/28/2023 00:276020BChromiummg/Kg - dry 0.147
179 02/28/2023 00:276020BLeadmg/Kg - dry 0.0393
0.851 02/28/2023 00:276020BSeleniummg/Kg - dry 0.130
J0.0202 02/28/2023 00:276020BSilvermg/Kg - dry 0.0085
J0.008 02/21/2023 20:078260DAcetonemg/Kg - dry 0.003
21.3 02/21/2023 17:11SW-DRYWT Moisture %
Page 6 of 82

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: Former Southern Steel Lab Report Number: 23-051-0030
Date: 2/28/2023
Metals Analyses Method 6020B Sample 89225 (FG-5) Analyte: Arsenic
QC Batch No: L666608/L666092 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89225 (FG-5)
Analyte: Barium QC Batch No: L666608/L666092
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89225 (FG-5)
Analyte: Chromium QC Batch No: L666608/L666092
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89225 (FG-5) Analyte: Lead QC Batch No: L666608/L666092
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 89225 (FG-5)
Analyte: Selenium QC Batch No: L666608/L666092 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 89246 (SP-02) Analyte: Arsenic QC Batch No: L666608/L666093 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89246 (SP-02) Analyte: Barium QC Batch No: L666608/L666093 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Page 7 of 82

Sample 89246 (SP-02)
Analyte: Cadmium QC Batch No: L666608/L666093
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 89246 (SP-02) Analyte: Chromium
QC Batch No: L666608/L666093 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 89246 (SP-02) Analyte: Lead
QC Batch No: L666608/L666093 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 89246 (SP-02) Analyte: Selenium
QC Batch No: L666608/L666093 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 Sample 89221 (FG-1) Analyte: Hexavalent Chromium QC Batch No: L666151/L665758 Insoluble Hexavalent Chromium spike data. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Aniline QC Batch No: V30176/V30122
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Sample 89624 (B4 0-5) Analyte: Aniline
QC Batch No: V30176/V30122 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89221 (FG-1) Analyte: Benzo(a)pyrene QC Batch No: V30176/V30122 CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte. Sample 89222 (FG-2) Analyte: Benzo(a)pyrene QC Batch No: V30176/V30122
Page 8 of 82

CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte.
Sample 89223 (FG-3)
Analyte: Benzo(a)pyrene QC Batch No: V30176/V30122
CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte.
Sample 89224 (FG-4) Analyte: Benzo(a)pyrene
QC Batch No: V30176/V30122 CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte.
Sample 89225 (FG-5)
Analyte: Benzo(a)pyrene QC Batch No: V30176/V30122
CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte.
Sample 89226 (FG-DUP) Analyte: Benzo(a)pyrene
QC Batch No: V30176/V30122 CCV result is above range for Benzo (A) Pyrene. Sample result should be considered high bias for this analyte.
Sample 89624 (B4 0-5) Analyte: Benzoic Acid QC Batch No: V30176/V30122
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 89624 (B4 0-5) Analyte: N-Nitrosodiphenylamine QC Batch No: V30176/V30122 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.

Page 9 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.2 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.176 mg/Kg - dry 0.176 0.250Chromium, Hexavalent 1 02/27/23 12:15 SW-7199SAR
1.87 mg/Kg - dry 0.107 0.313Arsenic 5 02/27/23 23:39 6020BCPW
46.4 mg/Kg - dry 0.053 0.313Barium 5 02/27/23 23:39 6020BCPW
0.0561 J mg/Kg - dry 0.0324 0.313Cadmium 5 02/27/23 23:39 6020BCPW
20.4 mg/Kg - dry 0.145 0.313
Chromium 5 02/27/23 23:39 6020BCPW
57.9 mg/Kg - dry 0.0388 0.313Lead 5 02/27/23 23:39 6020BCPW
<0.0279 mg/Kg - dry 0.0279 0.232Mercury (Total)1 02/27/23 12:45 7471AFDS
0.639 mg/Kg - dry 0.129 0.313Selenium 5 02/27/23 23:39 6020BCPW
0.0177 J mg/Kg - dry 0.0084 0.313Silver 5 02/27/23 23:39 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.003 mg/Kg - dry 0.003 0.025Acetone 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 02/21/23 17:51 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/21/23 17:51 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/21/23 17:51 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/21/23 17:51 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/21/23 17:51 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/21/23 17:51 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/21/23 17:51 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/21/23 17:51 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/21/23 17:51 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/21/23 17:51 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 02/21/23 17:51 V29996TBL
<0.017 mg/Kg - dry 0.017 0.313Ethanol 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 17:51 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 02/21/23 17:51 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/21/23 17:51 V29996TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 02/21/23 17:51 V29996TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/21/23 17:51 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 02/21/23 17:51 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/21/23 17:51 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/21/23 17:51 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/21/23 17:51 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/21/23 17:51 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/21/23 17:51 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/21/23 17:51 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/21/23 17:51 V29996
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%02/21/23 17:511 TBL V29996
Surrogate: Dibromofluoromethane 105 Limits: 84-123%02/21/23 17:511 TBL V29996
Surrogate: Toluene-d8 98.6 Limits: 76-129%02/21/23 17:511 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.145 mg/Kg - dry 0.145 0.827Acenaphthene 1 02/27/23 13:19 V30176JMV
<0.131 mg/Kg - dry 0.131 0.827Acenaphthylene 1 02/27/23 13:19 V30176JMV
<0.190 mg/Kg - dry 0.190 0.827Aniline 1 02/27/23 13:19 V30176JMV
<0.179 mg/Kg - dry 0.179 0.827Anthracene 1 02/27/23 13:19 V30176JMV
<0.174 mg/Kg - dry 0.174 0.827
Benzo(a)anthracene 1 02/27/23 13:19 V30176JMV
<0.184 mg/Kg - dry 0.184 0.827Benzo(a)pyrene 1 02/27/23 13:19 V30176JMV
<0.182 mg/Kg - dry 0.182 0.827Benzo(b)fluoranthene 1 02/27/23 13:19 V30176JMV
<0.170 mg/Kg - dry 0.170 0.827Benzo(g,h,i)perylene 1 02/27/23 13:19 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.171 mg/Kg - dry 0.171 0.827Benzo(k)fluoranthene 1 02/27/23 13:19 V30176JMV
<0.726 mg/Kg - dry 0.726 2.51Benzoic Acid 1 02/27/23 13:19 V30176JMV
<0.131 mg/Kg - dry 0.131 0.827Benzyl alcohol 1 02/27/23 13:19 V30176JMV
<0.147 mg/Kg - dry 0.147 0.827Bis(2-Chloroethoxy)methane 1 02/27/23 13:19 V30176JMV
<0.134 mg/Kg - dry 0.134 0.827Bis(2-Chloroethyl)ether 1 02/27/23 13:19 V30176JMV
<0.170 mg/Kg - dry 0.170 0.413Bis(2-Chloroisopropyl)ether 1 02/27/23 13:19 V30176JMV
<0.150 mg/Kg - dry 0.150 0.827Bis(2-ethylhexyl)phthalate 1 02/27/23 13:19 V30176JMV
<0.136 mg/Kg - dry 0.136 0.8274-Bromophenyl phenyl ether 1 02/27/23 13:19 V30176JMV
<0.141 mg/Kg - dry 0.141 0.413
Butyl benzyl phthalate 1 02/27/23 13:19 V30176JMV
<0.115 mg/Kg - dry 0.115 0.8274-Chloro-3-methylphenol 1 02/27/23 13:19 V30176JMV
<0.140 mg/Kg - dry 0.140 0.4134-Chloroaniline 1 02/27/23 13:19 V30176JMV
<0.145 mg/Kg - dry 0.145 0.8272-Chloronaphthalene 1 02/27/23 13:19 V30176JMV
<0.123 mg/Kg - dry 0.123 0.8272-Chlorophenol 1 02/27/23 13:19 V30176JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 02/27/23 13:19 V30176JMV
<0.177 mg/Kg - dry 0.177 0.827Chrysene 1 02/27/23 13:19 V30176JMV
<0.288 mg/Kg - dry 0.288 0.827
Dibenz(a,h)anthracene 1 02/27/23 13:19 V30176JMV
<0.149 mg/Kg - dry 0.149 0.827Dibenzofuran 1 02/27/23 13:19 V30176JMV
<0.118 mg/Kg - dry 0.118 0.8271,2-Dichlorobenzene 1 02/27/23 13:19 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8271,3-Dichlorobenzene 1 02/27/23 13:19 V30176JMV
<0.122 mg/Kg - dry 0.122 0.4131,4-Dichlorobenzene 1 02/27/23 13:19 V30176JMV
<0.184 mg/Kg - dry 0.184 0.8273,3'-Dichlorobenzidine 1 02/27/23 13:19 V30176JMV
<0.120 mg/Kg - dry 0.120 0.8272,4-Dichlorophenol 1 02/27/23 13:19 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.225 mg/Kg - dry 0.225 0.827Diethyl phthalate 1 02/27/23 13:19 V30176JMV
<0.218 mg/Kg - dry 0.218 0.827Dimethyl phthalate 1 02/27/23 13:19 V30176JMV
<0.135 mg/Kg - dry 0.135 0.4132,4-Dimethylphenol 1 02/27/23 13:19 V30176JMV
<0.134 mg/Kg - dry 0.134 0.827Di-n-butyl phthalate 1 02/27/23 13:19 V30176JMV
<0.300 mg/Kg - dry 0.300 1.884,6-Dinitro-2-methylphenol 1 02/27/23 13:19 V30176JMV
<0.651 mg/Kg - dry 0.651 1.882,4-Dinitrophenol 1 02/27/23 13:19 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8272,4-Dinitrotoluene 1 02/27/23 13:19 V30176JMV
<0.135 mg/Kg - dry 0.135 0.8272,6-Dinitrotoluene 1 02/27/23 13:19 V30176JMV
<0.179 mg/Kg - dry 0.179 0.413
Di-n-Octyl Phthalate 1 02/27/23 13:19 V30176JMV
0.159 J mg/Kg - dry 0.154 0.827Fluoranthene 1 02/27/23 13:19 V30176JMV
<0.160 mg/Kg - dry 0.160 0.827Fluorene 1 02/27/23 13:19 V30176JMV
<0.132 mg/Kg - dry 0.132 0.827Hexachlorobenzene 1 02/27/23 13:19 V30176JMV
<0.122 mg/Kg - dry 0.122 0.827Hexachlorobutadiene 1 02/27/23 13:19 V30176JMV
<0.196 mg/Kg - dry 0.196 0.827Hexachlorocyclopentadiene 1 02/27/23 13:19 V30176JMV
<0.099 mg/Kg - dry 0.099 0.827Hexachloroethane 1 02/27/23 13:19 V30176JMV
<0.224 mg/Kg - dry 0.224 0.827
Indeno(1,2,3-cd)pyrene 1 02/27/23 13:19 V30176JMV
<0.239 mg/Kg - dry 0.239 0.827Isophorone 1 02/27/23 13:19 V30176JMV
<0.132 mg/Kg - dry 0.132 0.8271-Methylnaphthalene 1 02/27/23 13:19 V30176JMV
<0.125 mg/Kg - dry 0.125 0.8272-Methylnaphthalene 1 02/27/23 13:19 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8272-Methylphenol 1 02/27/23 13:19 V30176JMV
<0.106 mg/Kg - dry 0.106 0.8273&4 Methylphenol 1 02/27/23 13:19 V30176JMV
<0.180 mg/Kg - dry 0.180 0.827Naphthalene 1 02/27/23 13:19 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-1
89221 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.121 mg/Kg - dry 0.121 0.8272-Nitroaniline 1 02/27/23 13:19 V30176JMV
<0.150 mg/Kg - dry 0.150 0.8273-Nitroaniline 1 02/27/23 13:19 V30176JMV
<0.116 mg/Kg - dry 0.116 0.4134-Nitroaniline 1 02/27/23 13:19 V30176JMV
<0.145 mg/Kg - dry 0.145 0.413Nitrobenzene 1 02/27/23 13:19 V30176JMV
<0.111 mg/Kg - dry 0.111 0.8272-Nitrophenol 1 02/27/23 13:19 V30176JMV
<0.146 mg/Kg - dry 0.146 0.8274-Nitrophenol 1 02/27/23 13:19 V30176JMV
<0.329 mg/Kg - dry 0.329 0.827N-Nitrosodimethylamine 1 02/27/23 13:19 V30176JMV
<0.226 mg/Kg - dry 0.226 0.827N-Nitrosodiphenylamine 1 02/27/23 13:19 V30176JMV
<0.147 mg/Kg - dry 0.147 0.827
N-Nitroso-di-n-propylamine 1 02/27/23 13:19 V30176JMV
<0.434 mg/Kg - dry 0.434 1.25Pentachlorophenol 1 02/27/23 13:19 V30176JMV
<0.260 mg/Kg - dry 0.260 0.827Phenanthrene 1 02/27/23 13:19 V30176JMV
<0.140 mg/Kg - dry 0.140 0.827Phenol 1 02/27/23 13:19 V30176JMV
<0.167 mg/Kg - dry 0.167 0.827Pyrene 1 02/27/23 13:19 V30176JMV
<0.099 mg/Kg - dry 0.099 0.413Pyridine 1 02/27/23 13:19 V30176JMV
<0.134 mg/Kg - dry 0.134 0.8271,2,4-Trichlorobenzene 1 02/27/23 13:19 V30176JMV
<0.120 mg/Kg - dry 0.120 0.827
2,4,5-Trichlorophenol 1 02/27/23 13:19 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8272,4,6-Trichlorophenol 1 02/27/23 13:19 V30176JMV
8270ESurrogate: Phenol-d5 92.2 Limits: 34-121%02/27/23 13:191 JMV
Surrogate: 2-Fluorobiphenyl 94.6 Limits: 44-115%02/27/23 13:191 JMV V30176
Surrogate: 2-Fluorophenol 90.1 Limits: 35-115%02/27/23 13:191 JMV V30176
Surrogate: Nitrobenzene-d5 91.0 Limits: 37-122%02/27/23 13:191 JMV V30176
Surrogate: 4-Terphenyl-d14 109 Limits: 54-127%02/27/23 13:191 JMV V30176
Surrogate: 2,4,6-Tribromophenol 99.4 Limits: 39-132%02/27/23 13:191 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.2 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.175 mg/Kg - dry 0.175 0.248Chromium, Hexavalent 1 02/27/23 13:24 SW-7199SAR
2.75 mg/Kg - dry 0.103 0.302Arsenic 5 02/27/23 23:43 6020BCPW
36.7 mg/Kg - dry 0.051 0.301Barium 5 02/27/23 23:43 6020BCPW
0.0410 J mg/Kg - dry 0.0312 0.302Cadmium 5 02/27/23 23:43 6020BCPW
13.4 mg/Kg - dry 0.140 0.301
Chromium 5 02/27/23 23:43 6020BCPW
30.8 mg/Kg - dry 0.0374 0.302Lead 5 02/27/23 23:43 6020BCPW
<0.0260 mg/Kg - dry 0.0260 0.215Mercury (Total)1 02/27/23 12:46 7471AFDS
1.16 mg/Kg - dry 0.124 0.301Selenium 5 02/27/23 23:43 6020BCPW
0.0142 J mg/Kg - dry 0.0081 0.302Silver 5 02/27/23 23:43 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.005 J mg/Kg - dry 0.002 0.024Acetone 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 02/21/23 18:18 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/21/23 18:18 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/21/23 18:18 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/21/23 18:18 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/21/23 18:18 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/21/23 18:18 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/21/23 18:18 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/21/23 18:18 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/21/23 18:18 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/21/23 18:18 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/21/23 18:18 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/21/23 18:18 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/21/23 18:18 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/21/23 18:18 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 02/21/23 18:18 V29996TBL
<0.016 mg/Kg - dry 0.016 0.301Ethanol 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 18:18 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 02/21/23 18:18 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 02/21/23 18:18 V29996TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 02/21/23 18:18 V29996TBL
0.001 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/21/23 18:18 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 02/21/23 18:18 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/21/23 18:18 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/21/23 18:18 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/21/23 18:18 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/21/23 18:18 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/21/23 18:18 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/21/23 18:18 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/21/23 18:18 V29996
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%02/21/23 18:181 TBL V29996
Surrogate: Dibromofluoromethane 110 Limits: 84-123%02/21/23 18:181 TBL V29996
Surrogate: Toluene-d8 93.8 Limits: 76-129%02/21/23 18:181 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.140 mg/Kg - dry 0.140 0.797Acenaphthene 1 02/27/23 13:42 V30176JMV
<0.126 mg/Kg - dry 0.126 0.797Acenaphthylene 1 02/27/23 13:42 V30176JMV
<0.183 mg/Kg - dry 0.183 0.797Aniline 1 02/27/23 13:42 V30176JMV
<0.172 mg/Kg - dry 0.172 0.797Anthracene 1 02/27/23 13:42 V30176JMV
<0.167 mg/Kg - dry 0.167 0.797
Benzo(a)anthracene 1 02/27/23 13:42 V30176JMV
<0.177 mg/Kg - dry 0.177 0.797Benzo(a)pyrene 1 02/27/23 13:42 V30176JMV
0.227 J mg/Kg - dry 0.176 0.797Benzo(b)fluoranthene 1 02/27/23 13:42 V30176JMV
<0.164 mg/Kg - dry 0.164 0.797Benzo(g,h,i)perylene 1 02/27/23 13:42 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.165 mg/Kg - dry 0.165 0.797Benzo(k)fluoranthene 1 02/27/23 13:42 V30176JMV
<0.700 mg/Kg - dry 0.700 2.42Benzoic Acid 1 02/27/23 13:42 V30176JMV
<0.126 mg/Kg - dry 0.126 0.797Benzyl alcohol 1 02/27/23 13:42 V30176JMV
<0.142 mg/Kg - dry 0.142 0.797Bis(2-Chloroethoxy)methane 1 02/27/23 13:42 V30176JMV
<0.129 mg/Kg - dry 0.129 0.797Bis(2-Chloroethyl)ether 1 02/27/23 13:42 V30176JMV
<0.164 mg/Kg - dry 0.164 0.398Bis(2-Chloroisopropyl)ether 1 02/27/23 13:42 V30176JMV
<0.144 mg/Kg - dry 0.144 0.797Bis(2-ethylhexyl)phthalate 1 02/27/23 13:42 V30176JMV
<0.131 mg/Kg - dry 0.131 0.7974-Bromophenyl phenyl ether 1 02/27/23 13:42 V30176JMV
<0.136 mg/Kg - dry 0.136 0.398
Butyl benzyl phthalate 1 02/27/23 13:42 V30176JMV
<0.111 mg/Kg - dry 0.111 0.7974-Chloro-3-methylphenol 1 02/27/23 13:42 V30176JMV
<0.135 mg/Kg - dry 0.135 0.3984-Chloroaniline 1 02/27/23 13:42 V30176JMV
<0.140 mg/Kg - dry 0.140 0.7972-Chloronaphthalene 1 02/27/23 13:42 V30176JMV
<0.118 mg/Kg - dry 0.118 0.7972-Chlorophenol 1 02/27/23 13:42 V30176JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 02/27/23 13:42 V30176JMV
<0.171 mg/Kg - dry 0.171 0.797Chrysene 1 02/27/23 13:42 V30176JMV
<0.277 mg/Kg - dry 0.277 0.797
Dibenz(a,h)anthracene 1 02/27/23 13:42 V30176JMV
<0.143 mg/Kg - dry 0.143 0.797Dibenzofuran 1 02/27/23 13:42 V30176JMV
<0.114 mg/Kg - dry 0.114 0.7971,2-Dichlorobenzene 1 02/27/23 13:42 V30176JMV
<0.117 mg/Kg - dry 0.117 0.7971,3-Dichlorobenzene 1 02/27/23 13:42 V30176JMV
<0.117 mg/Kg - dry 0.117 0.3981,4-Dichlorobenzene 1 02/27/23 13:42 V30176JMV
<0.177 mg/Kg - dry 0.177 0.7973,3'-Dichlorobenzidine 1 02/27/23 13:42 V30176JMV
<0.115 mg/Kg - dry 0.115 0.7972,4-Dichlorophenol 1 02/27/23 13:42 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.217 mg/Kg - dry 0.217 0.797Diethyl phthalate 1 02/27/23 13:42 V30176JMV
<0.210 mg/Kg - dry 0.210 0.797Dimethyl phthalate 1 02/27/23 13:42 V30176JMV
<0.130 mg/Kg - dry 0.130 0.3982,4-Dimethylphenol 1 02/27/23 13:42 V30176JMV
<0.129 mg/Kg - dry 0.129 0.797Di-n-butyl phthalate 1 02/27/23 13:42 V30176JMV
<0.289 mg/Kg - dry 0.289 1.814,6-Dinitro-2-methylphenol 1 02/27/23 13:42 V30176JMV
<0.628 mg/Kg - dry 0.628 1.812,4-Dinitrophenol 1 02/27/23 13:42 V30176JMV
<0.116 mg/Kg - dry 0.116 0.7972,4-Dinitrotoluene 1 02/27/23 13:42 V30176JMV
<0.130 mg/Kg - dry 0.130 0.7972,6-Dinitrotoluene 1 02/27/23 13:42 V30176JMV
<0.172 mg/Kg - dry 0.172 0.398
Di-n-Octyl Phthalate 1 02/27/23 13:42 V30176JMV
0.219 J mg/Kg - dry 0.148 0.797Fluoranthene 1 02/27/23 13:42 V30176JMV
<0.154 mg/Kg - dry 0.154 0.797Fluorene 1 02/27/23 13:42 V30176JMV
<0.128 mg/Kg - dry 0.128 0.797Hexachlorobenzene 1 02/27/23 13:42 V30176JMV
<0.117 mg/Kg - dry 0.117 0.797Hexachlorobutadiene 1 02/27/23 13:42 V30176JMV
<0.189 mg/Kg - dry 0.189 0.797Hexachlorocyclopentadiene 1 02/27/23 13:42 V30176JMV
<0.095 mg/Kg - dry 0.095 0.797Hexachloroethane 1 02/27/23 13:42 V30176JMV
<0.216 mg/Kg - dry 0.216 0.797
Indeno(1,2,3-cd)pyrene 1 02/27/23 13:42 V30176JMV
<0.230 mg/Kg - dry 0.230 0.797Isophorone 1 02/27/23 13:42 V30176JMV
<0.128 mg/Kg - dry 0.128 0.7971-Methylnaphthalene 1 02/27/23 13:42 V30176JMV
<0.120 mg/Kg - dry 0.120 0.7972-Methylnaphthalene 1 02/27/23 13:42 V30176JMV
<0.117 mg/Kg - dry 0.117 0.7972-Methylphenol 1 02/27/23 13:42 V30176JMV
<0.102 mg/Kg - dry 0.102 0.7973&4 Methylphenol 1 02/27/23 13:42 V30176JMV
<0.173 mg/Kg - dry 0.173 0.797Naphthalene 1 02/27/23 13:42 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-2
89222 Matrix:
2/20/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.116 mg/Kg - dry 0.116 0.7972-Nitroaniline 1 02/27/23 13:42 V30176JMV
<0.144 mg/Kg - dry 0.144 0.7973-Nitroaniline 1 02/27/23 13:42 V30176JMV
<0.112 mg/Kg - dry 0.112 0.3984-Nitroaniline 1 02/27/23 13:42 V30176JMV
<0.140 mg/Kg - dry 0.140 0.398Nitrobenzene 1 02/27/23 13:42 V30176JMV
<0.107 mg/Kg - dry 0.107 0.7972-Nitrophenol 1 02/27/23 13:42 V30176JMV
<0.141 mg/Kg - dry 0.141 0.7974-Nitrophenol 1 02/27/23 13:42 V30176JMV
<0.317 mg/Kg - dry 0.317 0.797N-Nitrosodimethylamine 1 02/27/23 13:42 V30176JMV
<0.218 mg/Kg - dry 0.218 0.797N-Nitrosodiphenylamine 1 02/27/23 13:42 V30176JMV
<0.142 mg/Kg - dry 0.142 0.797
N-Nitroso-di-n-propylamine 1 02/27/23 13:42 V30176JMV
<0.419 mg/Kg - dry 0.419 1.21Pentachlorophenol 1 02/27/23 13:42 V30176JMV
<0.251 mg/Kg - dry 0.251 0.797Phenanthrene 1 02/27/23 13:42 V30176JMV
<0.135 mg/Kg - dry 0.135 0.797Phenol 1 02/27/23 13:42 V30176JMV
0.218 J mg/Kg - dry 0.161 0.797Pyrene 1 02/27/23 13:42 V30176JMV
<0.095 mg/Kg - dry 0.095 0.398Pyridine 1 02/27/23 13:42 V30176JMV
<0.129 mg/Kg - dry 0.129 0.7971,2,4-Trichlorobenzene 1 02/27/23 13:42 V30176JMV
<0.116 mg/Kg - dry 0.116 0.797
2,4,5-Trichlorophenol 1 02/27/23 13:42 V30176JMV
<0.116 mg/Kg - dry 0.116 0.7972,4,6-Trichlorophenol 1 02/27/23 13:42 V30176JMV
8270ESurrogate: Phenol-d5 107 Limits: 34-121%02/27/23 13:421 JMV
Surrogate: 2-Fluorobiphenyl 102 Limits: 44-115%02/27/23 13:421 JMV V30176
Surrogate: 2-Fluorophenol 109 Limits: 35-115%02/27/23 13:421 JMV V30176
Surrogate: Nitrobenzene-d5 109 Limits: 37-122%02/27/23 13:421 JMV V30176
Surrogate: 4-Terphenyl-d14 113 Limits: 54-127%02/27/23 13:421 JMV V30176
Surrogate: 2,4,6-Tribromophenol 104 Limits: 39-132%02/27/23 13:421 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.3 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.176 mg/Kg - dry 0.176 0.250Chromium, Hexavalent 1 02/27/23 12:47 SW-7199SAR
3.34 mg/Kg - dry 0.107 0.314Arsenic 5 02/27/23 23:46 6020BCPW
67.0 mg/Kg - dry 0.053 0.313Barium 5 02/27/23 23:46 6020BCPW
0.0657 J mg/Kg - dry 0.0324 0.314Cadmium 5 02/27/23 23:46 6020BCPW
30.7 mg/Kg - dry 0.145 0.313
Chromium 5 02/27/23 23:46 6020BCPW
74.5 mg/Kg - dry 0.0388 0.314Lead 5 02/27/23 23:46 6020BCPW
<0.0281 mg/Kg - dry 0.0281 0.233Mercury (Total)1 02/27/23 12:47 7471AFDS
1.01 mg/Kg - dry 0.129 0.313Selenium 5 02/27/23 23:46 6020BCPW
0.0233 J mg/Kg - dry 0.0084 0.314Silver 5 02/27/23 23:46 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.006 J mg/Kg - dry 0.003 0.025Acetone 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 02/21/23 18:45 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/21/23 18:45 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/21/23 18:45 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/21/23 18:45 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/21/23 18:45 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/21/23 18:45 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/21/23 18:45 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/21/23 18:45 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/21/23 18:45 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/21/23 18:45 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 02/21/23 18:45 V29996TBL
<0.017 mg/Kg - dry 0.017 0.313Ethanol 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 18:45 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 02/21/23 18:45 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.003 J mg/Kg - dry 0.0008 0.012n-Hexane 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/21/23 18:45 V29996TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/21/23 18:45 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 02/21/23 18:45 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/21/23 18:45 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/21/23 18:45 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/21/23 18:45 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/21/23 18:45 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/21/23 18:45 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/21/23 18:45 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/21/23 18:45 V29996
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%02/21/23 18:451 TBL V29996
Surrogate: Dibromofluoromethane 108 Limits: 84-123%02/21/23 18:451 TBL V29996
Surrogate: Toluene-d8 97.8 Limits: 76-129%02/21/23 18:451 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.145 mg/Kg - dry 0.145 0.828Acenaphthene 1 02/27/23 14:04 V30176JMV
<0.131 mg/Kg - dry 0.131 0.828Acenaphthylene 1 02/27/23 14:04 V30176JMV
<0.190 mg/Kg - dry 0.190 0.828Aniline 1 02/27/23 14:04 V30176JMV
<0.179 mg/Kg - dry 0.179 0.828Anthracene 1 02/27/23 14:04 V30176JMV
<0.174 mg/Kg - dry 0.174 0.828
Benzo(a)anthracene 1 02/27/23 14:04 V30176JMV
<0.184 mg/Kg - dry 0.184 0.828Benzo(a)pyrene 1 02/27/23 14:04 V30176JMV
0.191 J mg/Kg - dry 0.183 0.828Benzo(b)fluoranthene 1 02/27/23 14:04 V30176JMV
<0.170 mg/Kg - dry 0.170 0.828Benzo(g,h,i)perylene 1 02/27/23 14:04 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.171 mg/Kg - dry 0.171 0.828Benzo(k)fluoranthene 1 02/27/23 14:04 V30176JMV
<0.727 mg/Kg - dry 0.727 2.51Benzoic Acid 1 02/27/23 14:04 V30176JMV
<0.131 mg/Kg - dry 0.131 0.828Benzyl alcohol 1 02/27/23 14:04 V30176JMV
<0.148 mg/Kg - dry 0.148 0.828Bis(2-Chloroethoxy)methane 1 02/27/23 14:04 V30176JMV
<0.134 mg/Kg - dry 0.134 0.828Bis(2-Chloroethyl)ether 1 02/27/23 14:04 V30176JMV
<0.170 mg/Kg - dry 0.170 0.414Bis(2-Chloroisopropyl)ether 1 02/27/23 14:04 V30176JMV
<0.150 mg/Kg - dry 0.150 0.828Bis(2-ethylhexyl)phthalate 1 02/27/23 14:04 V30176JMV
<0.136 mg/Kg - dry 0.136 0.8284-Bromophenyl phenyl ether 1 02/27/23 14:04 V30176JMV
<0.141 mg/Kg - dry 0.141 0.414
Butyl benzyl phthalate 1 02/27/23 14:04 V30176JMV
<0.115 mg/Kg - dry 0.115 0.8284-Chloro-3-methylphenol 1 02/27/23 14:04 V30176JMV
<0.140 mg/Kg - dry 0.140 0.4144-Chloroaniline 1 02/27/23 14:04 V30176JMV
<0.145 mg/Kg - dry 0.145 0.8282-Chloronaphthalene 1 02/27/23 14:04 V30176JMV
<0.123 mg/Kg - dry 0.123 0.8282-Chlorophenol 1 02/27/23 14:04 V30176JMV
<0.158 mg/Kg - dry 0.158 1.254-Chlorophenyl phenyl ether 1 02/27/23 14:04 V30176JMV
<0.178 mg/Kg - dry 0.178 0.828Chrysene 1 02/27/23 14:04 V30176JMV
<0.288 mg/Kg - dry 0.288 0.828
Dibenz(a,h)anthracene 1 02/27/23 14:04 V30176JMV
<0.149 mg/Kg - dry 0.149 0.828Dibenzofuran 1 02/27/23 14:04 V30176JMV
<0.118 mg/Kg - dry 0.118 0.8281,2-Dichlorobenzene 1 02/27/23 14:04 V30176JMV
<0.122 mg/Kg - dry 0.122 0.8281,3-Dichlorobenzene 1 02/27/23 14:04 V30176JMV
<0.122 mg/Kg - dry 0.122 0.4141,4-Dichlorobenzene 1 02/27/23 14:04 V30176JMV
<0.184 mg/Kg - dry 0.184 0.8283,3'-Dichlorobenzidine 1 02/27/23 14:04 V30176JMV
<0.120 mg/Kg - dry 0.120 0.8282,4-Dichlorophenol 1 02/27/23 14:04 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.225 mg/Kg - dry 0.225 0.828Diethyl phthalate 1 02/27/23 14:04 V30176JMV
<0.218 mg/Kg - dry 0.218 0.828Dimethyl phthalate 1 02/27/23 14:04 V30176JMV
<0.135 mg/Kg - dry 0.135 0.4142,4-Dimethylphenol 1 02/27/23 14:04 V30176JMV
<0.134 mg/Kg - dry 0.134 0.828Di-n-butyl phthalate 1 02/27/23 14:04 V30176JMV
<0.301 mg/Kg - dry 0.301 1.884,6-Dinitro-2-methylphenol 1 02/27/23 14:04 V30176JMV
<0.652 mg/Kg - dry 0.652 1.882,4-Dinitrophenol 1 02/27/23 14:04 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8282,4-Dinitrotoluene 1 02/27/23 14:04 V30176JMV
<0.135 mg/Kg - dry 0.135 0.8282,6-Dinitrotoluene 1 02/27/23 14:04 V30176JMV
<0.179 mg/Kg - dry 0.179 0.414
Di-n-Octyl Phthalate 1 02/27/23 14:04 V30176JMV
0.171 J mg/Kg - dry 0.154 0.828Fluoranthene 1 02/27/23 14:04 V30176JMV
<0.160 mg/Kg - dry 0.160 0.828Fluorene 1 02/27/23 14:04 V30176JMV
<0.132 mg/Kg - dry 0.132 0.828Hexachlorobenzene 1 02/27/23 14:04 V30176JMV
<0.122 mg/Kg - dry 0.122 0.828Hexachlorobutadiene 1 02/27/23 14:04 V30176JMV
<0.196 mg/Kg - dry 0.196 0.828Hexachlorocyclopentadiene 1 02/27/23 14:04 V30176JMV
<0.099 mg/Kg - dry 0.099 0.828Hexachloroethane 1 02/27/23 14:04 V30176JMV
<0.224 mg/Kg - dry 0.224 0.828
Indeno(1,2,3-cd)pyrene 1 02/27/23 14:04 V30176JMV
<0.239 mg/Kg - dry 0.239 0.828Isophorone 1 02/27/23 14:04 V30176JMV
<0.132 mg/Kg - dry 0.132 0.8281-Methylnaphthalene 1 02/27/23 14:04 V30176JMV
<0.125 mg/Kg - dry 0.125 0.8282-Methylnaphthalene 1 02/27/23 14:04 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8282-Methylphenol 1 02/27/23 14:04 V30176JMV
<0.106 mg/Kg - dry 0.106 0.8283&4 Methylphenol 1 02/27/23 14:04 V30176JMV
<0.180 mg/Kg - dry 0.180 0.828Naphthalene 1 02/27/23 14:04 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-3
89223 Matrix:
2/20/2023 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.121 mg/Kg - dry 0.121 0.8282-Nitroaniline 1 02/27/23 14:04 V30176JMV
<0.150 mg/Kg - dry 0.150 0.8283-Nitroaniline 1 02/27/23 14:04 V30176JMV
<0.117 mg/Kg - dry 0.117 0.4144-Nitroaniline 1 02/27/23 14:04 V30176JMV
<0.145 mg/Kg - dry 0.145 0.414Nitrobenzene 1 02/27/23 14:04 V30176JMV
<0.111 mg/Kg - dry 0.111 0.8282-Nitrophenol 1 02/27/23 14:04 V30176JMV
<0.146 mg/Kg - dry 0.146 0.8284-Nitrophenol 1 02/27/23 14:04 V30176JMV
<0.329 mg/Kg - dry 0.329 0.828N-Nitrosodimethylamine 1 02/27/23 14:04 V30176JMV
<0.227 mg/Kg - dry 0.227 0.828N-Nitrosodiphenylamine 1 02/27/23 14:04 V30176JMV
<0.148 mg/Kg - dry 0.148 0.828
N-Nitroso-di-n-propylamine 1 02/27/23 14:04 V30176JMV
<0.435 mg/Kg - dry 0.435 1.25Pentachlorophenol 1 02/27/23 14:04 V30176JMV
<0.260 mg/Kg - dry 0.260 0.828Phenanthrene 1 02/27/23 14:04 V30176JMV
<0.140 mg/Kg - dry 0.140 0.828Phenol 1 02/27/23 14:04 V30176JMV
0.188 J mg/Kg - dry 0.168 0.828Pyrene 1 02/27/23 14:04 V30176JMV
<0.099 mg/Kg - dry 0.099 0.414Pyridine 1 02/27/23 14:04 V30176JMV
<0.134 mg/Kg - dry 0.134 0.8281,2,4-Trichlorobenzene 1 02/27/23 14:04 V30176JMV
<0.120 mg/Kg - dry 0.120 0.828
2,4,5-Trichlorophenol 1 02/27/23 14:04 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8282,4,6-Trichlorophenol 1 02/27/23 14:04 V30176JMV
8270ESurrogate: Phenol-d5 80.8 Limits: 34-121%02/27/23 14:041 JMV
Surrogate: 2-Fluorobiphenyl 80.1 Limits: 44-115%02/27/23 14:041 JMV V30176
Surrogate: 2-Fluorophenol 81.7 Limits: 35-115%02/27/23 14:041 JMV V30176
Surrogate: Nitrobenzene-d5 81.3 Limits: 37-122%02/27/23 14:041 JMV V30176
Surrogate: 4-Terphenyl-d14 90.4 Limits: 54-127%02/27/23 14:041 JMV V30176
Surrogate: 2,4,6-Tribromophenol 80.8 Limits: 39-132%02/27/23 14:041 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.3 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.157 mg/Kg - dry 0.157 0.224Chromium, Hexavalent 1 02/27/23 12:58 SW-7199SAR
3.52 mg/Kg - dry 0.0953 0.279Arsenic 5 02/27/23 23:50 6020BCPW
79.8 mg/Kg - dry 0.047 0.278Barium 5 02/27/23 23:50 6020BCPW
0.0936 J mg/Kg - dry 0.0288 0.279Cadmium 5 02/27/23 23:50 6020BCPW
21.6 mg/Kg - dry 0.129 0.278
Chromium 5 02/27/23 23:50 6020BCPW
65.0 mg/Kg - dry 0.0345 0.279Lead 5 02/27/23 23:50 6020BCPW
<0.0254 mg/Kg - dry 0.0254 0.211Mercury (Total)1 02/27/23 12:52 7471AFDS
0.643 mg/Kg - dry 0.114 0.278Selenium 5 02/27/23 23:50 6020BCPW
0.0299 J mg/Kg - dry 0.0075 0.279Silver 5 02/27/23 23:50 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.005 J mg/Kg - dry 0.002 0.022Acetone 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 02/21/23 19:13 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 02/21/23 19:13 V29996TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 02/21/23 19:13 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 02/21/23 19:13 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 02/21/23 19:13 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 02/21/23 19:13 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 02/21/23 19:13 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 02/21/23 19:13 V29996TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 02/21/23 19:13 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 02/21/23 19:13 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 02/21/23 19:13 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 02/21/23 19:13 V29996TBL
<0.015 mg/Kg - dry 0.015 0.278Ethanol 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 19:13 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 02/21/23 19:13 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 02/21/23 19:13 V29996TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 02/21/23 19:13 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 02/21/23 19:13 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 02/21/23 19:13 V29996TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 02/21/23 19:13 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 02/21/23 19:13 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 02/21/23 19:13 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 02/21/23 19:13 V29996TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 02/21/23 19:13 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 02/21/23 19:13 V29996
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%02/21/23 19:131 TBL V29996
Surrogate: Dibromofluoromethane 109 Limits: 84-123%02/21/23 19:131 TBL V29996
Surrogate: Toluene-d8 95.9 Limits: 76-129%02/21/23 19:131 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.129 mg/Kg - dry 0.129 0.735Acenaphthene 1 02/27/23 14:27 V30176JMV
<0.117 mg/Kg - dry 0.117 0.735Acenaphthylene 1 02/27/23 14:27 V30176JMV
<0.169 mg/Kg - dry 0.169 0.735Aniline 1 02/27/23 14:27 V30176JMV
<0.159 mg/Kg - dry 0.159 0.735Anthracene 1 02/27/23 14:27 V30176JMV
0.455 J
mg/Kg - dry 0.154 0.735
Benzo(a)anthracene 1 02/27/23 14:27 V30176JMV
0.509 J mg/Kg - dry 0.163 0.735Benzo(a)pyrene 1 02/27/23 14:27 V30176JMV
0.647 J mg/Kg - dry 0.162 0.735Benzo(b)fluoranthene 1 02/27/23 14:27 V30176JMV
0.323 J mg/Kg - dry 0.151 0.735Benzo(g,h,i)perylene 1 02/27/23 14:27 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
0.246 J mg/Kg - dry 0.152 0.735Benzo(k)fluoranthene 1 02/27/23 14:27 V30176JMV
<0.646 mg/Kg - dry 0.646 2.23Benzoic Acid 1 02/27/23 14:27 V30176JMV
<0.117 mg/Kg - dry 0.117 0.735Benzyl alcohol 1 02/27/23 14:27 V30176JMV
<0.131 mg/Kg - dry 0.131 0.735Bis(2-Chloroethoxy)methane 1 02/27/23 14:27 V30176JMV
<0.119 mg/Kg - dry 0.119 0.735Bis(2-Chloroethyl)ether 1 02/27/23 14:27 V30176JMV
<0.151 mg/Kg - dry 0.151 0.367Bis(2-Chloroisopropyl)ether 1 02/27/23 14:27 V30176JMV
<0.133 mg/Kg - dry 0.133 0.735Bis(2-ethylhexyl)phthalate 1 02/27/23 14:27 V30176JMV
<0.121 mg/Kg - dry 0.121 0.7354-Bromophenyl phenyl ether 1 02/27/23 14:27 V30176JMV
<0.125 mg/Kg - dry 0.125 0.367
Butyl benzyl phthalate 1 02/27/23 14:27 V30176JMV
<0.103 mg/Kg - dry 0.103 0.7354-Chloro-3-methylphenol 1 02/27/23 14:27 V30176JMV
<0.124 mg/Kg - dry 0.124 0.3674-Chloroaniline 1 02/27/23 14:27 V30176JMV
<0.129 mg/Kg - dry 0.129 0.7352-Chloronaphthalene 1 02/27/23 14:27 V30176JMV
<0.109 mg/Kg - dry 0.109 0.7352-Chlorophenol 1 02/27/23 14:27 V30176JMV
<0.140 mg/Kg - dry 0.140 1.114-Chlorophenyl phenyl ether 1 02/27/23 14:27 V30176JMV
0.441 J mg/Kg - dry 0.158 0.735Chrysene 1 02/27/23 14:27 V30176JMV
<0.256 mg/Kg - dry 0.256 0.735
Dibenz(a,h)anthracene 1 02/27/23 14:27 V30176JMV
<0.132 mg/Kg - dry 0.132 0.735Dibenzofuran 1 02/27/23 14:27 V30176JMV
<0.105 mg/Kg - dry 0.105 0.7351,2-Dichlorobenzene 1 02/27/23 14:27 V30176JMV
<0.108 mg/Kg - dry 0.108 0.7351,3-Dichlorobenzene 1 02/27/23 14:27 V30176JMV
<0.108 mg/Kg - dry 0.108 0.3671,4-Dichlorobenzene 1 02/27/23 14:27 V30176JMV
<0.163 mg/Kg - dry 0.163 0.7353,3'-Dichlorobenzidine 1 02/27/23 14:27 V30176JMV
<0.106 mg/Kg - dry 0.106 0.7352,4-Dichlorophenol 1 02/27/23 14:27 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.200 mg/Kg - dry 0.200 0.735Diethyl phthalate 1 02/27/23 14:27 V30176JMV
<0.193 mg/Kg - dry 0.193 0.735Dimethyl phthalate 1 02/27/23 14:27 V30176JMV
<0.120 mg/Kg - dry 0.120 0.3672,4-Dimethylphenol 1 02/27/23 14:27 V30176JMV
<0.119 mg/Kg - dry 0.119 0.735Di-n-butyl phthalate 1 02/27/23 14:27 V30176JMV
<0.267 mg/Kg - dry 0.267 1.674,6-Dinitro-2-methylphenol 1 02/27/23 14:27 V30176JMV
<0.579 mg/Kg - dry 0.579 1.672,4-Dinitrophenol 1 02/27/23 14:27 V30176JMV
<0.107 mg/Kg - dry 0.107 0.7352,4-Dinitrotoluene 1 02/27/23 14:27 V30176JMV
<0.120 mg/Kg - dry 0.120 0.7352,6-Dinitrotoluene 1 02/27/23 14:27 V30176JMV
<0.159 mg/Kg - dry 0.159 0.367
Di-n-Octyl Phthalate 1 02/27/23 14:27 V30176JMV
0.654 J mg/Kg - dry 0.137 0.735Fluoranthene 1 02/27/23 14:27 V30176JMV
<0.142 mg/Kg - dry 0.142 0.735Fluorene 1 02/27/23 14:27 V30176JMV
<0.118 mg/Kg - dry 0.118 0.735Hexachlorobenzene 1 02/27/23 14:27 V30176JMV
<0.108 mg/Kg - dry 0.108 0.735Hexachlorobutadiene 1 02/27/23 14:27 V30176JMV
<0.175 mg/Kg - dry 0.175 0.735Hexachlorocyclopentadiene 1 02/27/23 14:27 V30176JMV
<0.088 mg/Kg - dry 0.088 0.735Hexachloroethane 1 02/27/23 14:27 V30176JMV
0.332 J
mg/Kg - dry 0.199 0.735
Indeno(1,2,3-cd)pyrene 1 02/27/23 14:27 V30176JMV
<0.212 mg/Kg - dry 0.212 0.735Isophorone 1 02/27/23 14:27 V30176JMV
<0.118 mg/Kg - dry 0.118 0.7351-Methylnaphthalene 1 02/27/23 14:27 V30176JMV
<0.111 mg/Kg - dry 0.111 0.7352-Methylnaphthalene 1 02/27/23 14:27 V30176JMV
<0.108 mg/Kg - dry 0.108 0.7352-Methylphenol 1 02/27/23 14:27 V30176JMV
<0.094 mg/Kg - dry 0.094 0.7353&4 Methylphenol 1 02/27/23 14:27 V30176JMV
<0.160 mg/Kg - dry 0.160 0.735Naphthalene 1 02/27/23 14:27 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-4
89224 Matrix:
2/20/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.107 mg/Kg - dry 0.107 0.7352-Nitroaniline 1 02/27/23 14:27 V30176JMV
<0.133 mg/Kg - dry 0.133 0.7353-Nitroaniline 1 02/27/23 14:27 V30176JMV
<0.104 mg/Kg - dry 0.104 0.3674-Nitroaniline 1 02/27/23 14:27 V30176JMV
<0.129 mg/Kg - dry 0.129 0.367Nitrobenzene 1 02/27/23 14:27 V30176JMV
<0.098 mg/Kg - dry 0.098 0.7352-Nitrophenol 1 02/27/23 14:27 V30176JMV
<0.130 mg/Kg - dry 0.130 0.7354-Nitrophenol 1 02/27/23 14:27 V30176JMV
<0.293 mg/Kg - dry 0.293 0.735N-Nitrosodimethylamine 1 02/27/23 14:27 V30176JMV
<0.201 mg/Kg - dry 0.201 0.735N-Nitrosodiphenylamine 1 02/27/23 14:27 V30176JMV
<0.131 mg/Kg - dry 0.131 0.735
N-Nitroso-di-n-propylamine 1 02/27/23 14:27 V30176JMV
<0.386 mg/Kg - dry 0.386 1.11Pentachlorophenol 1 02/27/23 14:27 V30176JMV
0.370 J mg/Kg - dry 0.231 0.735Phenanthrene 1 02/27/23 14:27 V30176JMV
<0.124 mg/Kg - dry 0.124 0.735Phenol 1 02/27/23 14:27 V30176JMV
0.704 J mg/Kg - dry 0.149 0.735Pyrene 1 02/27/23 14:27 V30176JMV
<0.088 mg/Kg - dry 0.088 0.367Pyridine 1 02/27/23 14:27 V30176JMV
<0.119 mg/Kg - dry 0.119 0.7351,2,4-Trichlorobenzene 1 02/27/23 14:27 V30176JMV
<0.107 mg/Kg - dry 0.107 0.735
2,4,5-Trichlorophenol 1 02/27/23 14:27 V30176JMV
<0.107 mg/Kg - dry 0.107 0.7352,4,6-Trichlorophenol 1 02/27/23 14:27 V30176JMV
8270ESurrogate: Phenol-d5 95.5 Limits: 34-121%02/27/23 14:271 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%02/27/23 14:271 JMV V30176
Surrogate: 2-Fluorophenol 93.4 Limits: 35-115%02/27/23 14:271 JMV V30176
Surrogate: Nitrobenzene-d5 94.0 Limits: 37-122%02/27/23 14:271 JMV V30176
Surrogate: 4-Terphenyl-d14 111 Limits: 54-127%02/27/23 14:271 JMV V30176
Surrogate: 2,4,6-Tribromophenol 85.0 Limits: 39-132%02/27/23 14:271 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.9 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.172 mg/Kg - dry 0.172 0.245Chromium, Hexavalent 1 02/27/23 13:09 SW-7199SAR
2.21 mg/Kg - dry 0.103 0.301Arsenic 5 02/28/23 00:01 6020BCPW
58.8 mg/Kg - dry 0.051 0.300Barium 5 02/28/23 00:01 6020BCPW
0.0819 J mg/Kg - dry 0.0311 0.301Cadmium 5 02/28/23 00:01 6020BCPW
29.7 mg/Kg - dry 0.139 0.300
Chromium 5 02/28/23 00:01 6020BCPW
36.9 mg/Kg - dry 0.0373 0.301Lead 5 02/28/23 00:01 6020BCPW
0.0579 J mg/Kg - dry 0.0267 0.221Mercury (Total)1 02/27/23 12:53 7471AFDS
0.796 mg/Kg - dry 0.123 0.300Selenium 5 02/28/23 00:01 6020BCPW
0.0259 J mg/Kg - dry 0.0081 0.301Silver 5 02/28/23 00:01 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.015 J mg/Kg - dry 0.002 0.024Acetone 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 02/21/23 19:40 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/21/23 19:40 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/21/23 19:40 V29996TBL
0.0009 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 02/21/23 19:40 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/21/23 19:40 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/21/23 19:40 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/21/23 19:40 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/21/23 19:40 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/21/23 19:40 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/21/23 19:40 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/21/23 19:40 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/21/23 19:40 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/21/23 19:40 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 02/21/23 19:40 V29996TBL
<0.016 mg/Kg - dry 0.016 0.300Ethanol 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 19:40 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 02/21/23 19:40 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/21/23 19:40 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 02/21/23 19:40 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 02/21/23 19:40 V29996TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/21/23 19:40 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/21/23 19:40 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012
1,2,3-Trichlorobenzene 1 02/21/23 19:40 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/21/23 19:40 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/21/23 19:40 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/21/23 19:40 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/21/23 19:40 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/21/23 19:40 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/21/23 19:40 V29996
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%02/21/23 19:401 TBL V29996
Surrogate: Dibromofluoromethane 104 Limits: 84-123%02/21/23 19:401 TBL V29996
Surrogate: Toluene-d8 96.7 Limits: 76-129%02/21/23 19:401 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.139 mg/Kg - dry 0.139 0.795Acenaphthene 1 02/27/23 14:50 V30176JMV
<0.126 mg/Kg - dry 0.126 0.795Acenaphthylene 1 02/27/23 14:50 V30176JMV
<0.182 mg/Kg - dry 0.182 0.795Aniline 1 02/27/23 14:50 V30176JMV
<0.172 mg/Kg - dry 0.172 0.795Anthracene 1 02/27/23 14:50 V30176JMV
0.507 J
mg/Kg - dry 0.167 0.795
Benzo(a)anthracene 1 02/27/23 14:50 V30176JMV
0.575 J mg/Kg - dry 0.176 0.795Benzo(a)pyrene 1 02/27/23 14:50 V30176JMV
0.787 J mg/Kg - dry 0.175 0.795Benzo(b)fluoranthene 1 02/27/23 14:50 V30176JMV
0.364 J mg/Kg - dry 0.163 0.795Benzo(g,h,i)perylene 1 02/27/23 14:50 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
0.246 J mg/Kg - dry 0.164 0.795Benzo(k)fluoranthene 1 02/27/23 14:50 V30176JMV
<0.697 mg/Kg - dry 0.697 2.41Benzoic Acid 1 02/27/23 14:50 V30176JMV
<0.126 mg/Kg - dry 0.126 0.795Benzyl alcohol 1 02/27/23 14:50 V30176JMV
<0.141 mg/Kg - dry 0.141 0.795Bis(2-Chloroethoxy)methane 1 02/27/23 14:50 V30176JMV
<0.128 mg/Kg - dry 0.128 0.795Bis(2-Chloroethyl)ether 1 02/27/23 14:50 V30176JMV
<0.163 mg/Kg - dry 0.163 0.398Bis(2-Chloroisopropyl)ether 1 02/27/23 14:50 V30176JMV
<0.144 mg/Kg - dry 0.144 0.795Bis(2-ethylhexyl)phthalate 1 02/27/23 14:50 V30176JMV
<0.131 mg/Kg - dry 0.131 0.7954-Bromophenyl phenyl ether 1 02/27/23 14:50 V30176JMV
<0.135 mg/Kg - dry 0.135 0.398
Butyl benzyl phthalate 1 02/27/23 14:50 V30176JMV
<0.111 mg/Kg - dry 0.111 0.7954-Chloro-3-methylphenol 1 02/27/23 14:50 V30176JMV
<0.134 mg/Kg - dry 0.134 0.3984-Chloroaniline 1 02/27/23 14:50 V30176JMV
<0.139 mg/Kg - dry 0.139 0.7952-Chloronaphthalene 1 02/27/23 14:50 V30176JMV
<0.118 mg/Kg - dry 0.118 0.7952-Chlorophenol 1 02/27/23 14:50 V30176JMV
<0.151 mg/Kg - dry 0.151 1.204-Chlorophenyl phenyl ether 1 02/27/23 14:50 V30176JMV
0.505 J mg/Kg - dry 0.170 0.795Chrysene 1 02/27/23 14:50 V30176JMV
<0.276 mg/Kg - dry 0.276 0.795
Dibenz(a,h)anthracene 1 02/27/23 14:50 V30176JMV
<0.143 mg/Kg - dry 0.143 0.795Dibenzofuran 1 02/27/23 14:50 V30176JMV
<0.113 mg/Kg - dry 0.113 0.7951,2-Dichlorobenzene 1 02/27/23 14:50 V30176JMV
<0.117 mg/Kg - dry 0.117 0.7951,3-Dichlorobenzene 1 02/27/23 14:50 V30176JMV
<0.117 mg/Kg - dry 0.117 0.3981,4-Dichlorobenzene 1 02/27/23 14:50 V30176JMV
<0.176 mg/Kg - dry 0.176 0.7953,3'-Dichlorobenzidine 1 02/27/23 14:50 V30176JMV
<0.115 mg/Kg - dry 0.115 0.7952,4-Dichlorophenol 1 02/27/23 14:50 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.216 mg/Kg - dry 0.216 0.795Diethyl phthalate 1 02/27/23 14:50 V30176JMV
<0.209 mg/Kg - dry 0.209 0.795Dimethyl phthalate 1 02/27/23 14:50 V30176JMV
<0.129 mg/Kg - dry 0.129 0.3982,4-Dimethylphenol 1 02/27/23 14:50 V30176JMV
<0.128 mg/Kg - dry 0.128 0.795Di-n-butyl phthalate 1 02/27/23 14:50 V30176JMV
<0.288 mg/Kg - dry 0.288 1.814,6-Dinitro-2-methylphenol 1 02/27/23 14:50 V30176JMV
<0.625 mg/Kg - dry 0.625 1.812,4-Dinitrophenol 1 02/27/23 14:50 V30176JMV
<0.116 mg/Kg - dry 0.116 0.7952,4-Dinitrotoluene 1 02/27/23 14:50 V30176JMV
<0.129 mg/Kg - dry 0.129 0.7952,6-Dinitrotoluene 1 02/27/23 14:50 V30176JMV
<0.172 mg/Kg - dry 0.172 0.398
Di-n-Octyl Phthalate 1 02/27/23 14:50 V30176JMV
0.469 J mg/Kg - dry 0.148 0.795Fluoranthene 1 02/27/23 14:50 V30176JMV
<0.154 mg/Kg - dry 0.154 0.795Fluorene 1 02/27/23 14:50 V30176JMV
<0.127 mg/Kg - dry 0.127 0.795Hexachlorobenzene 1 02/27/23 14:50 V30176JMV
<0.117 mg/Kg - dry 0.117 0.795Hexachlorobutadiene 1 02/27/23 14:50 V30176JMV
<0.188 mg/Kg - dry 0.188 0.795Hexachlorocyclopentadiene 1 02/27/23 14:50 V30176JMV
<0.095 mg/Kg - dry 0.095 0.795Hexachloroethane 1 02/27/23 14:50 V30176JMV
0.379 J
mg/Kg - dry 0.215 0.795
Indeno(1,2,3-cd)pyrene 1 02/27/23 14:50 V30176JMV
<0.229 mg/Kg - dry 0.229 0.795Isophorone 1 02/27/23 14:50 V30176JMV
<0.127 mg/Kg - dry 0.127 0.7951-Methylnaphthalene 1 02/27/23 14:50 V30176JMV
<0.120 mg/Kg - dry 0.120 0.7952-Methylnaphthalene 1 02/27/23 14:50 V30176JMV
<0.116 mg/Kg - dry 0.116 0.7952-Methylphenol 1 02/27/23 14:50 V30176JMV
<0.102 mg/Kg - dry 0.102 0.7953&4 Methylphenol 1 02/27/23 14:50 V30176JMV
<0.173 mg/Kg - dry 0.173 0.795Naphthalene 1 02/27/23 14:50 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-5
89225 Matrix:
2/20/2023 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.116 mg/Kg - dry 0.116 0.7952-Nitroaniline 1 02/27/23 14:50 V30176JMV
<0.144 mg/Kg - dry 0.144 0.7953-Nitroaniline 1 02/27/23 14:50 V30176JMV
<0.112 mg/Kg - dry 0.112 0.3984-Nitroaniline 1 02/27/23 14:50 V30176JMV
<0.139 mg/Kg - dry 0.139 0.398Nitrobenzene 1 02/27/23 14:50 V30176JMV
<0.106 mg/Kg - dry 0.106 0.7952-Nitrophenol 1 02/27/23 14:50 V30176JMV
<0.140 mg/Kg - dry 0.140 0.7954-Nitrophenol 1 02/27/23 14:50 V30176JMV
<0.316 mg/Kg - dry 0.316 0.795N-Nitrosodimethylamine 1 02/27/23 14:50 V30176JMV
<0.217 mg/Kg - dry 0.217 0.795N-Nitrosodiphenylamine 1 02/27/23 14:50 V30176JMV
<0.141 mg/Kg - dry 0.141 0.795
N-Nitroso-di-n-propylamine 1 02/27/23 14:50 V30176JMV
<0.417 mg/Kg - dry 0.417 1.20Pentachlorophenol 1 02/27/23 14:50 V30176JMV
<0.250 mg/Kg - dry 0.250 0.795Phenanthrene 1 02/27/23 14:50 V30176JMV
<0.134 mg/Kg - dry 0.134 0.795Phenol 1 02/27/23 14:50 V30176JMV
0.588 J mg/Kg - dry 0.161 0.795Pyrene 1 02/27/23 14:50 V30176JMV
<0.095 mg/Kg - dry 0.095 0.398Pyridine 1 02/27/23 14:50 V30176JMV
<0.128 mg/Kg - dry 0.128 0.7951,2,4-Trichlorobenzene 1 02/27/23 14:50 V30176JMV
<0.115 mg/Kg - dry 0.115 0.795
2,4,5-Trichlorophenol 1 02/27/23 14:50 V30176JMV
<0.116 mg/Kg - dry 0.116 0.7952,4,6-Trichlorophenol 1 02/27/23 14:50 V30176JMV
8270ESurrogate: Phenol-d5 102 Limits: 34-121%02/27/23 14:501 JMV
Surrogate: 2-Fluorobiphenyl 100 Limits: 44-115%02/27/23 14:501 JMV V30176
Surrogate: 2-Fluorophenol 101 Limits: 35-115%02/27/23 14:501 JMV V30176
Surrogate: Nitrobenzene-d5 102 Limits: 37-122%02/27/23 14:501 JMV V30176
Surrogate: 4-Terphenyl-d14 114 Limits: 54-127%02/27/23 14:501 JMV V30176
Surrogate: 2,4,6-Tribromophenol 96.1 Limits: 39-132%02/27/23 14:501 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.3 %Moisture 1 02/21/23 17:11 SW-DRYWTAMB
<0.181 mg/Kg - dry 0.181 0.257Chromium, Hexavalent 1 02/27/23 13:56 SW-7199SAR
3.01 mg/Kg - dry 0.109 0.318Arsenic 5 02/28/23 00:27 6020BCPW
50.8 mg/Kg - dry 0.054 0.317Barium 5 02/28/23 00:27 6020BCPW
0.145 J mg/Kg - dry 0.0329 0.318Cadmium 5 02/28/23 00:27 6020BCPW
43.2 mg/Kg - dry 0.147 0.317
Chromium 5 02/28/23 00:27 6020BCPW
179 mg/Kg - dry 0.0393 0.318Lead 5 02/28/23 00:27 6020BCPW
<0.0248 mg/Kg - dry 0.0248 0.206Mercury (Total)1 02/27/23 13:05 7471AFDS
0.851 mg/Kg - dry 0.130 0.317Selenium 5 02/28/23 00:27 6020BCPW
0.0202 J mg/Kg - dry 0.0085 0.318Silver 5 02/28/23 00:27 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
0.008 J mg/Kg - dry 0.003 0.025Acetone 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 02/21/23 20:07 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 02/21/23 20:07 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 02/21/23 20:07 V29996TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 02/21/23 20:07 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 02/21/23 20:07 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 02/21/23 20:07 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 02/21/23 20:07 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 02/21/23 20:07 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 02/21/23 20:07 V29996TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 02/21/23 20:07 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 02/21/23 20:07 V29996TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 02/21/23 20:07 V29996TBL
<0.017 mg/Kg - dry 0.017 0.317Ethanol 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 02/21/23 20:07 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 02/21/23 20:07 V29996TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 02/21/23 20:07 V29996TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 02/21/23 20:07 V29996TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 02/21/23 20:07 V29996TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 02/21/23 20:07 V29996TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 02/21/23 20:07 V29996TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V29995 02/21/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 02/21/23 20:07 V29996TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 02/21/23 20:07 V29996TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 02/21/23 20:07 V29996TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 02/21/23 20:07 V29996
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%02/21/23 20:071 TBL V29996
Surrogate: Dibromofluoromethane 108 Limits: 84-123%02/21/23 20:071 TBL V29996
Surrogate: Toluene-d8 98.4 Limits: 76-129%02/21/23 20:071 TBL V29996
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.147 mg/Kg - dry 0.147 0.838Acenaphthene 1 02/27/23 15:12 V30176JMV
<0.133 mg/Kg - dry 0.133 0.838Acenaphthylene 1 02/27/23 15:12 V30176JMV
<0.193 mg/Kg - dry 0.193 0.838Aniline 1 02/27/23 15:12 V30176JMV
<0.181 mg/Kg - dry 0.181 0.838Anthracene 1 02/27/23 15:12 V30176JMV
<0.176 mg/Kg - dry 0.176 0.838
Benzo(a)anthracene 1 02/27/23 15:12 V30176JMV
<0.186 mg/Kg - dry 0.186 0.838Benzo(a)pyrene 1 02/27/23 15:12 V30176JMV
<0.185 mg/Kg - dry 0.185 0.838Benzo(b)fluoranthene 1 02/27/23 15:12 V30176JMV
<0.172 mg/Kg - dry 0.172 0.838Benzo(g,h,i)perylene 1 02/27/23 15:12 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.174 mg/Kg - dry 0.174 0.838Benzo(k)fluoranthene 1 02/27/23 15:12 V30176JMV
<0.736 mg/Kg - dry 0.736 2.54Benzoic Acid 1 02/27/23 15:12 V30176JMV
<0.133 mg/Kg - dry 0.133 0.838Benzyl alcohol 1 02/27/23 15:12 V30176JMV
<0.149 mg/Kg - dry 0.149 0.838Bis(2-Chloroethoxy)methane 1 02/27/23 15:12 V30176JMV
<0.135 mg/Kg - dry 0.135 0.838Bis(2-Chloroethyl)ether 1 02/27/23 15:12 V30176JMV
<0.172 mg/Kg - dry 0.172 0.419Bis(2-Chloroisopropyl)ether 1 02/27/23 15:12 V30176JMV
<0.152 mg/Kg - dry 0.152 0.838Bis(2-ethylhexyl)phthalate 1 02/27/23 15:12 V30176JMV
<0.138 mg/Kg - dry 0.138 0.8384-Bromophenyl phenyl ether 1 02/27/23 15:12 V30176JMV
<0.143 mg/Kg - dry 0.143 0.419
Butyl benzyl phthalate 1 02/27/23 15:12 V30176JMV
<0.117 mg/Kg - dry 0.117 0.8384-Chloro-3-methylphenol 1 02/27/23 15:12 V30176JMV
<0.142 mg/Kg - dry 0.142 0.4194-Chloroaniline 1 02/27/23 15:12 V30176JMV
<0.147 mg/Kg - dry 0.147 0.8382-Chloronaphthalene 1 02/27/23 15:12 V30176JMV
<0.124 mg/Kg - dry 0.124 0.8382-Chlorophenol 1 02/27/23 15:12 V30176JMV
<0.160 mg/Kg - dry 0.160 1.274-Chlorophenyl phenyl ether 1 02/27/23 15:12 V30176JMV
<0.180 mg/Kg - dry 0.180 0.838Chrysene 1 02/27/23 15:12 V30176JMV
<0.292 mg/Kg - dry 0.292 0.838
Dibenz(a,h)anthracene 1 02/27/23 15:12 V30176JMV
<0.151 mg/Kg - dry 0.151 0.838Dibenzofuran 1 02/27/23 15:12 V30176JMV
<0.119 mg/Kg - dry 0.119 0.8381,2-Dichlorobenzene 1 02/27/23 15:12 V30176JMV
<0.123 mg/Kg - dry 0.123 0.8381,3-Dichlorobenzene 1 02/27/23 15:12 V30176JMV
<0.123 mg/Kg - dry 0.123 0.4191,4-Dichlorobenzene 1 02/27/23 15:12 V30176JMV
<0.186 mg/Kg - dry 0.186 0.8383,3'-Dichlorobenzidine 1 02/27/23 15:12 V30176JMV
<0.121 mg/Kg - dry 0.121 0.8382,4-Dichlorophenol 1 02/27/23 15:12 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.228 mg/Kg - dry 0.228 0.838Diethyl phthalate 1 02/27/23 15:12 V30176JMV
<0.221 mg/Kg - dry 0.221 0.838Dimethyl phthalate 1 02/27/23 15:12 V30176JMV
<0.137 mg/Kg - dry 0.137 0.4192,4-Dimethylphenol 1 02/27/23 15:12 V30176JMV
<0.135 mg/Kg - dry 0.135 0.838Di-n-butyl phthalate 1 02/27/23 15:12 V30176JMV
<0.304 mg/Kg - dry 0.304 1.914,6-Dinitro-2-methylphenol 1 02/27/23 15:12 V30176JMV
<0.660 mg/Kg - dry 0.660 1.912,4-Dinitrophenol 1 02/27/23 15:12 V30176JMV
<0.122 mg/Kg - dry 0.122 0.8382,4-Dinitrotoluene 1 02/27/23 15:12 V30176JMV
<0.137 mg/Kg - dry 0.137 0.8382,6-Dinitrotoluene 1 02/27/23 15:12 V30176JMV
<0.181 mg/Kg - dry 0.181 0.419
Di-n-Octyl Phthalate 1 02/27/23 15:12 V30176JMV
<0.156 mg/Kg - dry 0.156 0.838Fluoranthene 1 02/27/23 15:12 V30176JMV
<0.162 mg/Kg - dry 0.162 0.838Fluorene 1 02/27/23 15:12 V30176JMV
<0.134 mg/Kg - dry 0.134 0.838Hexachlorobenzene 1 02/27/23 15:12 V30176JMV
<0.124 mg/Kg - dry 0.124 0.838Hexachlorobutadiene 1 02/27/23 15:12 V30176JMV
<0.199 mg/Kg - dry 0.199 0.838Hexachlorocyclopentadiene 1 02/27/23 15:12 V30176JMV
<0.100 mg/Kg - dry 0.100 0.838Hexachloroethane 1 02/27/23 15:12 V30176JMV
<0.227 mg/Kg - dry 0.227 0.838
Indeno(1,2,3-cd)pyrene 1 02/27/23 15:12 V30176JMV
<0.242 mg/Kg - dry 0.242 0.838Isophorone 1 02/27/23 15:12 V30176JMV
<0.134 mg/Kg - dry 0.134 0.8381-Methylnaphthalene 1 02/27/23 15:12 V30176JMV
<0.127 mg/Kg - dry 0.127 0.8382-Methylnaphthalene 1 02/27/23 15:12 V30176JMV
<0.123 mg/Kg - dry 0.123 0.8382-Methylphenol 1 02/27/23 15:12 V30176JMV
<0.107 mg/Kg - dry 0.107 0.8383&4 Methylphenol 1 02/27/23 15:12 V30176JMV
<0.182 mg/Kg - dry 0.182 0.838Naphthalene 1 02/27/23 15:12 V30176JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 82
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-051-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 02/20/2023
ANR.007
Report Date : 02/28/2023
Sample ID :
Lab No :
Sampled:FG-DUP
89226 Matrix:
2/20/2023 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30122 02/24/23 10:30
<0.122 mg/Kg - dry 0.122 0.8382-Nitroaniline 1 02/27/23 15:12 V30176JMV
<0.152 mg/Kg - dry 0.152 0.8383-Nitroaniline 1 02/27/23 15:12 V30176JMV
<0.118 mg/Kg - dry 0.118 0.4194-Nitroaniline 1 02/27/23 15:12 V30176JMV
<0.147 mg/Kg - dry 0.147 0.419Nitrobenzene 1 02/27/23 15:12 V30176JMV
<0.112 mg/Kg - dry 0.112 0.8382-Nitrophenol 1 02/27/23 15:12 V30176JMV
<0.148 mg/Kg - dry 0.148 0.8384-Nitrophenol 1 02/27/23 15:12 V30176JMV
<0.334 mg/Kg - dry 0.334 0.838N-Nitrosodimethylamine 1 02/27/23 15:12 V30176JMV
<0.229 mg/Kg - dry 0.229 0.838N-Nitrosodiphenylamine 1 02/27/23 15:12 V30176JMV
<0.149 mg/Kg - dry 0.149 0.838
N-Nitroso-di-n-propylamine 1 02/27/23 15:12 V30176JMV
<0.440 mg/Kg - dry 0.440 1.27Pentachlorophenol 1 02/27/23 15:12 V30176JMV
<0.264 mg/Kg - dry 0.264 0.838Phenanthrene 1 02/27/23 15:12 V30176JMV
<0.142 mg/Kg - dry 0.142 0.838Phenol 1 02/27/23 15:12 V30176JMV
<0.170 mg/Kg - dry 0.170 0.838Pyrene 1 02/27/23 15:12 V30176JMV
<0.100 mg/Kg - dry 0.100 0.419Pyridine 1 02/27/23 15:12 V30176JMV
<0.135 mg/Kg - dry 0.135 0.8381,2,4-Trichlorobenzene 1 02/27/23 15:12 V30176JMV
<0.122 mg/Kg - dry 0.122 0.838
2,4,5-Trichlorophenol 1 02/27/23 15:12 V30176JMV
<0.122 mg/Kg - dry 0.122 0.8382,4,6-Trichlorophenol 1 02/27/23 15:12 V30176JMV
8270ESurrogate: Phenol-d5 103 Limits: 34-121%02/27/23 15:121 JMV
Surrogate: 2-Fluorobiphenyl 109 Limits: 44-115%02/27/23 15:121 JMV V30176
Surrogate: 2-Fluorophenol 105 Limits: 35-115%02/27/23 15:121 JMV V30176
Surrogate: Nitrobenzene-d5 104 Limits: 37-122%02/27/23 15:121 JMV V30176
Surrogate: 4-Terphenyl-d14 117 Limits: 54-127%02/27/23 15:121 JMV V30176
Surrogate: 2,4,6-Tribromophenol 105 Limits: 39-132%02/27/23 15:121 JMV V30176
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 57 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Metals Analyses
6020B
L666608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L666092
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225
LRB-L666092 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/27/23 22:220.2500.0855<0.0855mg/KgArsenic
02/27/23 22:220.2500.042<0.042mg/KgBarium
02/27/23 22:220.2500.0259<0.0259mg/KgCadmium
02/27/23 22:220.2500.116<0.116mg/KgChromium
02/27/23 22:220.2500.0310<0.0310mg/KgLead
02/27/23 22:220.2500.103<0.103mg/KgSelenium
02/27/23 22:220.2500.0067<0.0067mg/KgSilver
LCS-L666092Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.02.122.50mg/KgArsenic 80-120
87.04.365.00mg/KgBarium 80-120
84.00.4210.500mg/KgCadmium 80-120
89.04.445.00mg/KgChromium 80-120
91.02.272.50mg/KgLead 80-120
88.04.405.00mg/KgSelenium 80-120
84.00.4200.500mg/KgSilver 80-120
V 89225-MS-L666092 V 89225-MSD-L666092Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3.67 78.03.302.482.361.84mg/KgArsenic 59.0*75-125 10.6 80
74.9 551*57.44.964.7248.9mg/KgBarium 171*75-125 26.4 80
0.486 89.00.4950.4960.4720.0681mg/KgCadmium 86.0 75-125 1.8 80
30.5 12321.54.964.7224.7mg/KgChromium -65*75-125 34.6 80
Page 1 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 58 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Metals Analyses
6020B
L666608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L666092
V 89225-MS-L666092 V 89225-MSD-L666092Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
45.0 606*32.52.482.3630.7mg/KgLead 73.0*75-125 32.2 80
3.81 67.0*3.794.964.720.662mg/KgSelenium 63.0*75-125 0.5 80
0.427 86.00.4420.4960.4720.0216mg/KgSilver 85.0 75-125 3.4 80
V 89225-PDS-L666092Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/28/23 00:1294.01.27mg/KgArsenic
02/28/23 00:121037.42mg/KgBarium
02/28/23 00:1293.00.224mg/KgCadmium
02/28/23 00:1292.04.44mg/KgChromium
02/28/23 00:1296.04.07mg/KgLead
02/28/23 00:1292.02.20mg/KgSelenium
02/28/23 00:1289.00.209mg/KgSilver
Page 2 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 59 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Metals Analyses
6020B
L666608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L666093
Associated Lab Samples: 89226
LRB-L666093 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/28/23 00:190.2500.0855<0.0855mg/KgArsenic
02/28/23 00:190.2500.042<0.042mg/KgBarium
02/28/23 00:190.2500.0259<0.0259mg/KgCadmium
02/28/23 00:190.2500.1160.182mg/KgChromium
02/28/23 00:190.2500.03100.0313mg/KgLead
02/28/23 00:190.2500.103<0.103mg/KgSelenium
02/28/23 00:190.2500.0067<0.0067mg/KgSilver
LCS-L666093Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.02.252.50mg/KgArsenic 80-120
97.04.845.00mg/KgBarium 80-120
89.00.4450.500mg/KgCadmium 80-120
99.04.955.00mg/KgChromium 80-120
96.02.412.50mg/KgLead 80-120
84.04.225.00mg/KgSelenium 80-120
96.00.4790.500mg/KgSilver 80-120
V 89246-MS-L666093 V 89246-MSD-L666093Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.39 48.0*2.322.422.481.19mg/KgArsenic 47.0*75-125 2.9 80
91.4 483*88.04.844.9567.5mg/KgBarium 424*75-125 3.7 80
0.451 66.0*0.4360.4840.4950.126mg/KgCadmium 64.0*75-125 3.3 80
32.2 48.0*33.44.844.9529.8mg/KgChromium 74.0*75-125 3.6 80
Page 3 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 60 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Metals Analyses
6020B
L666608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L666093
V 89246-MS-L666093 V 89246-MSD-L666093Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
8.76 77.08.032.422.486.85mg/KgLead 49.0*75-125 8.6 80
3.77 60.0*3.834.844.950.784mg/KgSelenium 63.0*75-125 1.5 80
0.430 80.00.4020.4840.4950.0346mg/KgSilver 76.0 75-125 6.7 80
V 89246-PDS-L666093Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/28/23 00:4993.01.26mg/KgArsenic
02/28/23 00:491059.73mg/KgBarium
02/28/23 00:4996.00.249mg/KgCadmium
02/28/23 00:4995.05.17mg/KgChromium
02/28/23 00:4996.01.85mg/KgLead
02/28/23 00:4991.02.33mg/KgSelenium
02/28/23 00:4987.00.218mg/KgSilver
Page 4 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 61 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L666460QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L666122
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225
LRB-L666122 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/27/23 12:170.1920.0232<0.0232mg/KgMercury (Total)
LCS-L666122Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.00.3940.400mg/KgMercury (Total)80-120
V 89225-MS-L666122 V 89225-MSD-L666122Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.464 1170.4110.3450.3980.0481mg/KgMercury (Total)119 80-120 12.1 20
V 89225-PDS-L666122Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/27/23 12:591090.829mg/KgMercury (Total)
Page 5 of 23Date:02/28/2023 02:33 PM
Page 62 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L666460QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L666129
Associated Lab Samples: 89226
LRB-L666129 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/27/23 13:000.1920.0232<0.0232mg/KgMercury (Total)
LCS-L666129Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1050.4210.400mg/KgMercury (Total)80-120
L 89841-MS-L666129 L 89841-MSD-L666129Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.408 1110.4520.3890.369<0.0214mg/KgMercury (Total)116 80-120 10.2 20
L 89841-PDS-L666129Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
02/27/23 13:261070.841mg/KgMercury (Total)
Page 6 of 23Date:02/28/2023 02:33 PM
Page 63 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V29995 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/21/23 11:300.0200.002<0.002mg/KgAcetone
02/21/23 11:300.0200.001<0.001mg/KgAcrolein
02/21/23 11:300.0200.0008<0.0008mg/KgAcrylonitrile
02/21/23 11:300.0050.0006<0.0006mg/KgBenzene
02/21/23 11:300.0050.0005<0.0005mg/KgBromobenzene
02/21/23 11:300.0050.0008<0.0008mg/KgBromochloromethane
02/21/23 11:300.0050.001<0.001mg/KgBromodichloromethane
02/21/23 11:300.0050.001<0.001mg/KgBromoform
02/21/23 11:300.0100.001<0.001mg/KgBromomethane
02/21/23 11:300.0050.0005<0.0005mg/Kgn-Butylbenzene
02/21/23 11:300.0050.0006<0.0006mg/Kgsec-Butyl benzene
02/21/23 11:300.0050.0005<0.0005mg/Kgtert-Butyl benzene
02/21/23 11:300.0050.0006<0.0006mg/KgCarbon Disulfide
02/21/23 11:300.0050.001<0.001mg/KgCarbon Tetrachloride
02/21/23 11:300.0050.0007<0.0007mg/KgChlorobenzene
02/21/23 11:300.0050.0009<0.0009mg/KgChlorodibromomethane
02/21/23 11:300.0100.0009<0.0009mg/KgChloroethane
02/21/23 11:300.0050.001<0.001mg/KgChloroform
02/21/23 11:300.0100.0006<0.0006mg/KgChloromethane
02/21/23 11:300.0050.0005<0.0005mg/Kg2-Chlorotoluene
02/21/23 11:300.0050.0004<0.0004mg/Kg4-Chlorotoluene
02/21/23 11:300.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
02/21/23 11:300.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
02/21/23 11:300.0050.0006<0.0006mg/Kg1,2-Dibromoethane
02/21/23 11:300.0050.0006<0.0006mg/KgDibromomethane
02/21/23 11:300.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
02/21/23 11:300.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 7 of 23Date:02/28/2023 02:33 PM
Page 64 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V29995 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/21/23 11:300.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
02/21/23 11:300.0100.001<0.001mg/KgDichlorodifluoromethane
02/21/23 11:300.0050.0008<0.0008mg/Kg1,1-Dichloroethane
02/21/23 11:300.0050.001<0.001mg/Kg1,2-Dichloroethane
02/21/23 11:300.0050.0007<0.0007mg/Kg1,1-Dichloroethene
02/21/23 11:300.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
02/21/23 11:300.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
02/21/23 11:300.0050.0004<0.0004mg/Kg1,2-Dichloropropane
02/21/23 11:300.0050.0006<0.0006mg/Kg1,3-Dichloropropane
02/21/23 11:300.0050.001<0.001mg/Kg2,2-Dichloropropane
02/21/23 11:300.0050.0008<0.0008mg/Kg1,1-Dichloropropene
02/21/23 11:300.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
02/21/23 11:300.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
02/21/23 11:300.2500.014<0.014mg/KgEthanol
02/21/23 11:300.0050.0006<0.0006mg/KgEthylbenzene
02/21/23 11:300.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
02/21/23 11:300.0100.0008<0.0008mg/KgHexachlorobutadiene
02/21/23 11:300.0100.0007<0.0007mg/Kgn-Hexane
02/21/23 11:300.0200.0006<0.0006mg/Kg2-Hexanone
02/21/23 11:300.0050.0005<0.0005mg/KgIsopropylbenzene
02/21/23 11:300.0050.001<0.001mg/Kg4-Isopropyl toluene
02/21/23 11:300.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
02/21/23 11:300.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
02/21/23 11:300.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
02/21/23 11:300.0100.001<0.001mg/KgMethylene Chloride
02/21/23 11:300.0100.0010<0.0010mg/KgNaphthalene
02/21/23 11:300.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 8 of 23Date:02/28/2023 02:33 PM
Page 65 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V29995 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/21/23 11:300.0050.001<0.001mg/KgStyrene
02/21/23 11:300.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
02/21/23 11:300.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
02/21/23 11:300.0050.0009<0.0009mg/KgTetrachloroethene
02/21/23 11:300.0050.0007<0.0007mg/KgToluene
02/21/23 11:300.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
02/21/23 11:300.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
02/21/23 11:300.0050.001<0.001mg/Kg1,1,1-Trichloroethane
02/21/23 11:300.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
02/21/23 11:300.0050.0009<0.0009mg/KgTrichloroethene
02/21/23 11:300.0100.002<0.002mg/KgTrichlorofluoromethane
02/21/23 11:300.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
02/21/23 11:300.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
02/21/23 11:300.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
02/21/23 11:300.0100.0005<0.0005mg/KgVinyl Acetate
02/21/23 11:300.0100.0005<0.0005mg/KgVinyl Chloride
02/21/23 11:300.0050.0005<0.0005mg/Kgo-Xylene
02/21/23 11:300.0100.001<0.001mg/Kgm,p-Xylene
02/21/23 11:304-Bromofluorobenzene (S)102 70-130
02/21/23 11:30Dibromofluoromethane (S)101 84-123
02/21/23 11:30Toluene-d8 (S)101 76-129
LCS-V29995 LCSD-V29995Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.101 1011020.1020.100mg/KgAcetone 29-198 0.9 20
Page 9 of 23Date:02/28/2023 02:33 PM
Page 66 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
LCS-V29995 LCSD-V29995Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.096 96.497.90.0970.100mg/KgAcrolein 70-130 1.5 20
0.101 1011050.1050.100mg/KgAcrylonitrile 65-134 3.8 20
0.043 86.092.60.0460.050mg/KgBenzene 74-127 7.3 20
0.044 89.297.40.0480.050mg/KgBromobenzene 73-125 8.7 20
0.040 81.085.20.0420.050mg/KgBromochloromethane 72-134 5.0 20
0.046 92.088.80.0440.050mg/KgBromodichloromethane 75-122 3.5 20
0.043 86.886.60.0430.050mg/KgBromoform 66-135 0.2 20
0.046 92.81120.0560.050mg/KgBromomethane 20-180 18.7 20
0.042 85.492.80.0460.050mg/Kgn-Butylbenzene 65-135 8.3 20
0.042 85.092.00.0460.050mg/Kgsec-Butyl benzene 66-131 7.9 20
0.043 86.693.80.0460.050mg/Kgtert-Butyl benzene 67-132 7.9 20
0.042 85.690.60.0450.050mg/KgCarbon Disulfide 61-129 5.6 20
0.043 87.290.80.0450.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.044 88.890.00.0450.050mg/KgChlorobenzene 74-118 1.3 20
0.045 90.488.60.0440.050mg/KgChlorodibromomethane 73-122 2.0 20
0.043 87.697.60.0480.050mg/KgChloroethane 33-149 10.7 20
0.048 96.091.40.0450.050mg/KgChloroform 73-127 4.9 20
0.048 96.01030.0510.050mg/KgChloromethane 45-143 7.4 20
0.042 85.290.40.0450.050mg/Kg2-Chlorotoluene 67-124 5.9 20
0.042 85.290.60.0450.050mg/Kg4-Chlorotoluene 71-126 6.1 20
0.046 92.092.00.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.0 20
0.041 82.487.40.0430.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.8 20
0.045 90.889.40.0440.050mg/Kg1,2-Dibromoethane 70-132 1.5 20
0.042 85.888.20.0440.050mg/KgDibromomethane 74-133 2.7 20
0.043 87.089.20.0440.050mg/Kg1,2-Dichlorobenzene 72-123 2.4 20
0.042 84.689.00.0440.050mg/Kg1,3-Dichlorobenzene 71-120 5.0 20
Page 10 of 23Date:02/28/2023 02:33 PM
Page 67 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
LCS-V29995 LCSD-V29995Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.039 78.688.60.0440.050mg/Kg1,4-Dichlorobenzene 71-123 11.9 20
0.053 1061080.0530.050mg/KgDichlorodifluoromethane 26-146 1.4 20
0.044 89.495.20.0470.050mg/Kg1,1-Dichloroethane 74-127 6.2 20
0.044 89.492.00.0460.050mg/Kg1,2-Dichloroethane 68-128 2.8 20
0.041 83.691.80.0450.050mg/Kg1,1-Dichloroethene 67-149 9.3 20
0.043 87.691.40.0450.050mg/Kgcis-1,2-Dichloroethene 76-134 4.2 20
0.044 88.090.00.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 2.2 20
0.045 91.090.20.0450.050mg/Kg1,2-Dichloropropane 73-130 0.8 20
0.046 93.691.80.0450.050mg/Kg1,3-Dichloropropane 75-124 1.9 20
0.044 88.693.80.0460.050mg/Kg2,2-Dichloropropane 50-142 5.7 20
0.043 87.890.80.0450.050mg/Kg1,1-Dichloropropene 71-130 3.3 20
0.046 93.498.00.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 4.8 20
0.048 96.899.20.0490.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.4 20
1.18 94.486.41.081.25mg/KgEthanol 70-130 8.8 20
0.043 87.690.20.0450.050mg/KgEthylbenzene 74-128 2.9 20
0.093 93.192.20.0920.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.043 86.890.40.0450.050mg/KgHexachlorobutadiene 64-125 4.0 20
0.044 89.898.60.0490.050mg/Kgn-Hexane 70-130 9.3 20
0.047 94.488.20.0440.050mg/Kg2-Hexanone 61-157 6.7 20
0.043 87.089.80.0440.050mg/KgIsopropylbenzene 68-126 3.1 20
0.043 87.293.00.0460.050mg/Kg4-Isopropyl toluene 68-129 6.4 20
0.049 99.699.40.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.2 20
0.045 90.288.60.0440.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.7 20
0.048 97.891.00.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 7.2 20
0.044 89.291.00.0450.050mg/KgMethylene Chloride 74-129 1.9 20
0.044 89.090.00.0450.050mg/KgNaphthalene 57-157 1.1 20
Page 11 of 23Date:02/28/2023 02:33 PM
Page 68 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V29996QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V29995
LCS-V29995 LCSD-V29995Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.290.40.0450.050mg/Kgn-Propylbenzene 67-130 5.9 20
0.045 91.294.40.0470.050mg/KgStyrene 77-121 3.4 20
0.044 88.488.60.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.2 20
0.045 90.685.40.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 5.9 20
0.043 87.887.40.0430.050mg/KgTetrachloroethene 68-130 0.4 20
0.043 86.290.60.0450.050mg/KgToluene 71-129 4.9 20
0.044 88.688.60.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.0 20
0.047 94.696.20.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.6 20
0.043 86.692.60.0460.050mg/Kg1,1,1-Trichloroethane 67-131 6.6 20
0.045 90.888.00.0440.050mg/Kg1,1,2-Trichloroethane 70-133 3.1 20
0.044 89.497.20.0480.050mg/KgTrichloroethene 75-133 8.3 20
0.045 90.495.80.0470.050mg/KgTrichlorofluoromethane 44-146 5.8 20
0.044 88.878.00.0390.050mg/Kg1,2,3-Trichloropropane 60-137 12.9 20
0.042 84.890.80.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 6.8 20
0.042 85.490.40.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.6 20
0.050 1001040.0520.050mg/KgVinyl Acetate 60-140 3.9 20
0.048 96.61080.0540.050mg/KgVinyl Chloride 48-147 11.3 20
0.044 88.291.00.0450.050mg/Kgo-Xylene 74-126 3.1 20
0.087 87.891.40.0910.100mg/Kgm,p-Xylene 75-124 4.0 20
1021024-Bromofluorobenzene (S)70-130
10397.0Dibromofluoromethane (S)84-123
102100Toluene-d8 (S)76-129
Page 12 of 23Date:02/28/2023 02:33 PM
Page 69 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V30122 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/27/23 12:350.6600.116<0.116mg/KgAcenaphthene
02/27/23 12:350.6600.105<0.105mg/KgAcenaphthylene
02/27/23 12:350.6600.152<0.152mg/KgAniline
02/27/23 12:350.6600.143<0.143mg/KgAnthracene
02/27/23 12:350.6600.139<0.139mg/KgBenzo(a)anthracene
02/27/23 12:350.6600.147<0.147mg/KgBenzo(a)pyrene
02/27/23 12:350.6600.146<0.146mg/KgBenzo(b)fluoranthene
02/27/23 12:350.6600.136<0.136mg/KgBenzo(g,h,i)perylene
02/27/23 12:350.6600.137<0.137mg/KgBenzo(k)fluoranthene
02/27/23 12:352.000.580<0.580mg/KgBenzoic Acid
02/27/23 12:350.6600.105<0.105mg/KgBenzyl alcohol
02/27/23 12:350.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
02/27/23 12:350.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
02/27/23 12:350.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
02/27/23 12:350.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
02/27/23 12:350.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
02/27/23 12:350.3300.113<0.113mg/KgButyl benzyl phthalate
02/27/23 12:350.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
02/27/23 12:350.3300.112<0.112mg/Kg4-Chloroaniline
02/27/23 12:350.6600.116<0.116mg/Kg2-Chloronaphthalene
02/27/23 12:350.6600.098<0.098mg/Kg2-Chlorophenol
02/27/23 12:351.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
02/27/23 12:350.6600.142<0.142mg/KgChrysene
02/27/23 12:350.6600.230<0.230mg/KgDibenz(a,h)anthracene
02/27/23 12:350.6600.119<0.119mg/KgDibenzofuran
02/27/23 12:350.6600.094<0.094mg/Kg1,2-Dichlorobenzene
02/27/23 12:350.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 13 of 23Date:02/28/2023 02:33 PM
Page 70 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V30122 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/27/23 12:350.3300.097<0.097mg/Kg1,4-Dichlorobenzene
02/27/23 12:350.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
02/27/23 12:350.6600.095<0.095mg/Kg2,4-Dichlorophenol
02/27/23 12:350.6600.180<0.180mg/KgDiethyl phthalate
02/27/23 12:350.6600.174<0.174mg/KgDimethyl phthalate
02/27/23 12:350.3300.108<0.108mg/Kg2,4-Dimethylphenol
02/27/23 12:350.6600.107<0.107mg/KgDi-n-butyl phthalate
02/27/23 12:351.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
02/27/23 12:351.500.520<0.520mg/Kg2,4-Dinitrophenol
02/27/23 12:350.6600.096<0.096mg/Kg2,4-Dinitrotoluene
02/27/23 12:350.6600.108<0.108mg/Kg2,6-Dinitrotoluene
02/27/23 12:350.3300.143<0.143mg/KgDi-n-Octyl Phthalate
02/27/23 12:350.6600.123<0.123mg/KgFluoranthene
02/27/23 12:350.6600.128<0.128mg/KgFluorene
02/27/23 12:350.6600.106<0.106mg/KgHexachlorobenzene
02/27/23 12:350.6600.097<0.097mg/KgHexachlorobutadiene
02/27/23 12:350.6600.157<0.157mg/KgHexachlorocyclopentadiene
02/27/23 12:350.6600.079<0.079mg/KgHexachloroethane
02/27/23 12:350.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
02/27/23 12:350.6600.191<0.191mg/KgIsophorone
02/27/23 12:350.6600.106<0.106mg/Kg1-Methylnaphthalene
02/27/23 12:350.6600.100<0.100mg/Kg2-Methylnaphthalene
02/27/23 12:350.6600.097<0.097mg/Kg2-Methylphenol
02/27/23 12:350.6600.084<0.084mg/Kg3&4 Methylphenol
02/27/23 12:350.6600.144<0.144mg/KgNaphthalene
02/27/23 12:350.6600.096<0.096mg/Kg2-Nitroaniline
02/27/23 12:350.6600.120<0.120mg/Kg3-Nitroaniline
Page 14 of 23Date:02/28/2023 02:33 PM
Page 71 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-V30122 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/27/23 12:350.3300.093<0.093mg/Kg4-Nitroaniline
02/27/23 12:350.3300.116<0.116mg/KgNitrobenzene
02/27/23 12:350.6600.088<0.088mg/Kg2-Nitrophenol
02/27/23 12:350.6600.117<0.117mg/Kg4-Nitrophenol
02/27/23 12:350.6600.263<0.263mg/KgN-Nitrosodimethylamine
02/27/23 12:350.6600.181<0.181mg/KgN-Nitrosodiphenylamine
02/27/23 12:350.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
02/27/23 12:351.000.347<0.347mg/KgPentachlorophenol
02/27/23 12:350.6600.208<0.208mg/KgPhenanthrene
02/27/23 12:350.6600.112<0.112mg/KgPhenol
02/27/23 12:350.6600.134<0.134mg/KgPyrene
02/27/23 12:350.3300.079<0.079mg/KgPyridine
02/27/23 12:350.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
02/27/23 12:350.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
02/27/23 12:350.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
02/27/23 12:352-Fluorobiphenyl (S)101 44-115
02/27/23 12:352-Fluorophenol (S)101 35-115
02/27/23 12:35Nitrobenzene-d5 (S)97.6 37-122
02/27/23 12:354-Terphenyl-d14 (S)106 54-127
02/27/23 12:352,4,6-Tribromophenol (S)98.4 39-132
02/27/23 12:35Phenol-d5 (S)98.1 34-121
LCS-V30122Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.21.591.67mg/KgAcenaphthene 40-123
94.01.571.67mg/KgAcenaphthylene 32-132
Page 15 of 23Date:02/28/2023 02:33 PM
Page 72 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
LCS-V30122Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
249*4.161.67mg/KgAniline 12-197
98.21.641.67mg/KgAnthracene 47-123
95.81.601.67mg/KgBenzo(a)anthracene 49-126
1161.941.67mg/KgBenzo(a)pyrene 45-129
1071.781.67mg/KgBenzo(b)fluoranthene 45-132
1011.691.67mg/KgBenzo(g,h,i)perylene 43-134
1071.781.67mg/KgBenzo(k)fluoranthene 47-132
40.50.6771.67mg/KgBenzoic Acid 10-83
90.41.511.67mg/KgBenzyl alcohol 29-122
89.81.501.67mg/KgBis(2-Chloroethoxy)methane 36-121
88.61.481.67mg/KgBis(2-Chloroethyl)ether 31-120
99.41.661.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1071.791.67mg/KgBis(2-ethylhexyl)phthalate 51-133
95.81.601.67mg/Kg4-Bromophenyl phenyl ether 46-124
1121.871.67mg/KgButyl benzyl phthalate 48-132
82.01.371.67mg/Kg4-Chloro-3-methylphenol 45-122
87.41.461.67mg/Kg4-Chloroaniline 17-106
95.21.591.67mg/Kg2-Chloronaphthalene 41-114
86.81.451.67mg/Kg2-Chlorophenol 34-121
92.21.541.67mg/Kg4-Chlorophenyl phenyl ether 45-121
99.41.661.67mg/KgChrysene 50-124
1021.701.67mg/KgDibenz(a,h)anthracene 45-134
92.21.541.67mg/KgDibenzofuran 44-120
83.81.401.67mg/Kg1,2-Dichlorobenzene 33-117
80.81.351.67mg/Kg1,3-Dichlorobenzene 30-115
80.21.341.67mg/Kg1,4-Dichlorobenzene 31-115
76.61.281.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 16 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 73 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
LCS-V30122Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.81.351.67mg/Kg2,4-Dichlorophenol 40-122
96.41.611.67mg/KgDiethyl phthalate 50-124
94.61.581.67mg/KgDimethyl phthalate 48-124
85.01.421.67mg/Kg2,4-Dimethylphenol 30-127
1051.751.67mg/KgDi-n-butyl phthalate 51-128
92.21.541.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
88.61.481.67mg/Kg2,4-Dinitrophenol 27-129
95.81.601.67mg/Kg2,4-Dinitrotoluene 48-126
99.41.661.67mg/Kg2,6-Dinitrotoluene 46-124
1151.921.67mg/KgDi-n-Octyl Phthalate 45-140
95.21.591.67mg/KgFluoranthene 50-127
94.61.581.67mg/KgFluorene 43-125
97.61.631.67mg/KgHexachlorobenzene 45-122
76.01.271.67mg/KgHexachlorobutadiene 32-123
77.21.291.67mg/KgHexachlorocyclopentadiene 32-117
81.41.361.67mg/KgHexachloroethane 28-117
99.41.661.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
79.61.331.67mg/KgIsophorone 30-122
83.21.391.67mg/Kg1-Methylnaphthalene 40-119
77.21.291.67mg/Kg2-Methylnaphthalene 38-122
89.81.501.67mg/Kg2-Methylphenol 32-122
79.61.331.67mg/Kg3&4 Methylphenol 34-119
80.81.351.67mg/KgNaphthalene 35-123
98.21.641.67mg/Kg2-Nitroaniline 44-127
95.21.591.67mg/Kg3-Nitroaniline 33-119
90.41.511.67mg/Kg4-Nitroaniline 63-147
83.81.401.67mg/KgNitrobenzene 34-122
Page 17 of 23Date:02/28/2023 02:33 PM
Page 74 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
LCS-V30122Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.21.341.67mg/Kg2-Nitrophenol 36-123
1091.821.67mg/Kg4-Nitrophenol 30-132
83.21.391.67mg/KgN-Nitrosodimethylamine 10-146
1202.011.67mg/KgN-Nitrosodiphenylamine 38-127
91.01.521.67mg/KgN-Nitroso-di-n-propylamine 36-120
1091.821.67mg/KgPentachlorophenol 25-133
97.01.621.67mg/KgPhenanthrene 50-121
92.21.541.67mg/KgPhenol 34-121
1011.691.67mg/KgPyrene 47-127
65.81.101.67mg/KgPyridine 10-80
77.81.301.67mg/Kg1,2,4-Trichlorobenzene 34-118
90.41.511.67mg/Kg2,4,5-Trichlorophenol 41-124
89.81.501.67mg/Kg2,4,6-Trichlorophenol 39-126
97.02-Fluorobiphenyl (S)44-115
91.82-Fluorophenol (S)35-115
82.0Nitrobenzene-d5 (S)37-122
1054-Terphenyl-d14 (S)54-127
97.52,4,6-Tribromophenol (S)39-132
92.1Phenol-d5 (S)34-121
V 89624-MS-V30122 V 89624-MSD-V30122Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.65 98.81.711.671.67<0.116mg/KgAcenaphthene 102 40-123 3.5 20
1.64 98.21.701.671.67<0.105mg/KgAcenaphthylene 102 32-132 3.5 20
3.40 204*3.481.671.67<0.152mg/KgAniline 208*12-197 2.3 20
Page 18 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 75 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
V 89624-MS-V30122 V 89624-MSD-V30122Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.77 1061.801.671.67<0.143mg/KgAnthracene 108 47-123 1.6 20
1.77 1061.781.671.67<0.139mg/KgBenzo(a)anthracene 107 49-126 0.5 20
2.03 1222.071.671.67<0.147mg/KgBenzo(a)pyrene 124 45-129 1.9 20
1.84 1101.881.671.67<0.146mg/KgBenzo(b)fluoranthene 113 45-132 2.1 20
1.83 1101.881.671.67<0.136mg/KgBenzo(g,h,i)perylene 113 43-134 2.6 20
1.81 1081.851.671.67<0.137mg/KgBenzo(k)fluoranthene 111 47-132 2.1 20
1.59 95.2*1.511.671.67<0.580mg/KgBenzoic Acid 90.4*10-83 5.1 20
1.74 1041.781.671.67<0.105mg/KgBenzyl alcohol 107 29-122 2.2 20
1.59 95.21.601.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 95.8 36-121 0.6 20
1.62 97.01.641.671.67<0.107mg/KgBis(2-Chloroethyl)ether 98.2 31-120 1.2 20
1.84 1101.861.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 111 33-131 1.0 20
1.98 1191.991.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 119 51-133 0.5 20
1.76 1051.761.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 105 46-124 0.0 20
2.11 1262.161.671.67<0.113mg/KgButyl benzyl phthalate 129 48-132 2.3 20
1.48 88.61.461.671.67<0.092mg/Kg4-Chloro-3-methylphenol 87.4 45-122 1.3 20
1.29 77.21.291.671.67<0.112mg/Kg4-Chloroaniline 77.2 17-106 0.0 20
1.67 1001.731.671.67<0.116mg/Kg2-Chloronaphthalene 104 41-114 3.5 20
1.61 96.41.641.671.67<0.098mg/Kg2-Chlorophenol 98.2 34-121 1.8 20
1.62 97.01.671.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 100 45-121 3.0 20
1.79 1071.831.671.67<0.142mg/KgChrysene 110 50-124 2.2 20
1.80 1081.851.671.67<0.230mg/KgDibenz(a,h)anthracene 111 45-134 2.7 20
1.62 97.01.701.671.67<0.119mg/KgDibenzofuran 102 44-120 4.8 20
1.55 92.81.561.671.67<0.094mg/Kg1,2-Dichlorobenzene 93.4 33-117 0.6 20
1.52 91.01.541.671.67<0.097mg/Kg1,3-Dichlorobenzene 92.2 30-115 1.3 20
1.52 91.01.541.671.67<0.097mg/Kg1,4-Dichlorobenzene 92.2 31-115 1.3 20
1.27 76.01.241.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 74.2 22-121 2.3 20
Page 19 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 76 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
V 89624-MS-V30122 V 89624-MSD-V30122Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.48 88.61.461.671.67<0.095mg/Kg2,4-Dichlorophenol 87.4 40-122 1.3 20
1.73 1041.781.671.67<0.180mg/KgDiethyl phthalate 107 50-124 2.8 20
1.67 1001.761.671.67<0.174mg/KgDimethyl phthalate 105 48-124 5.2 30
1.62 97.01.641.671.67<0.108mg/Kg2,4-Dimethylphenol 98.2 30-127 1.2 20
1.92 1151.961.671.67<0.107mg/KgDi-n-butyl phthalate 117 51-128 2.0 20
1.47 88.01.481.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 88.6 29-132 0.6 20
1.47 88.01.501.671.67<0.520mg/Kg2,4-Dinitrophenol 89.8 27-129 2.0 20
1.73 1041.771.671.67<0.096mg/Kg2,4-Dinitrotoluene 106 48-126 2.2 20
1.76 1051.801.671.67<0.108mg/Kg2,6-Dinitrotoluene 108 46-124 2.2 20
1.98 1192.011.671.67<0.143mg/KgDi-n-Octyl Phthalate 120 45-140 1.5 20
1.71 1021.731.671.67<0.123mg/KgFluoranthene 104 50-127 1.1 20
1.68 1011.721.671.67<0.128mg/KgFluorene 103 43-125 2.3 20
1.74 1041.751.671.67<0.106mg/KgHexachlorobenzene 105 45-122 0.5 20
1.43 85.61.421.671.67<0.097mg/KgHexachlorobutadiene 85.0 32-123 0.7 20
0.819 49.00.7641.671.67<0.157mg/KgHexachlorocyclopentadiene 45.7 32-117 6.9 20
1.47 88.01.521.671.67<0.079mg/KgHexachloroethane 91.0 28-117 3.3 20
1.80 1081.821.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 109 45-133 1.1 20
1.43 85.61.431.671.67<0.191mg/KgIsophorone 85.6 30-122 0.0 20
1.48 88.61.461.671.67<0.106mg/Kg1-Methylnaphthalene 87.4 40-119 1.3 20
1.40 83.81.421.671.67<0.100mg/Kg2-Methylnaphthalene 85.0 38-122 1.4 20
1.67 1001.721.671.67<0.097mg/Kg2-Methylphenol 103 32-122 2.9 20
1.46 87.41.491.671.67<0.084mg/Kg3&4 Methylphenol 89.2 34-119 2.0 20
1.46 87.41.461.671.67<0.144mg/KgNaphthalene 87.4 35-123 0.0 20
1.75 1051.771.671.67<0.096mg/Kg2-Nitroaniline 106 44-127 1.1 20
1.58 94.61.591.671.67<0.120mg/Kg3-Nitroaniline 95.2 33-119 0.6 20
1.54 92.21.621.671.67<0.093mg/Kg4-Nitroaniline 97.0 63-147 5.0 20
Page 20 of 23Date:02/28/2023 02:33 PM
Page 77 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30122
V 89624-MS-V30122 V 89624-MSD-V30122Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.51 90.41.511.671.67<0.116mg/KgNitrobenzene 90.4 34-122 0.0 20
1.43 85.61.481.671.67<0.088mg/Kg2-Nitrophenol 88.6 32-123 3.4 20
1.75 1051.861.671.67<0.117mg/Kg4-Nitrophenol 111 30-132 6.0 20
1.49 89.21.481.671.67<0.263mg/KgN-Nitrosodimethylamine 88.6 10-146 0.6 30
2.21 132*2.241.671.67<0.181mg/KgN-Nitrosodiphenylamine 134*38-127 1.3 20
1.63 97.61.661.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 99.4 36-120 1.8 20
2.21 1322.201.671.67<0.347mg/KgPentachlorophenol 132 25-133 0.4 20
1.77 1061.801.671.67<0.208mg/KgPhenanthrene 108 50-121 1.6 20
1.68 1011.731.671.67<0.112mg/KgPhenol 104 34-121 2.9 20
1.88 1131.921.671.67<0.134mg/KgPyrene 115 47-127 2.1 20
1.03 61.61.061.671.67<0.079mg/KgPyridine 63.4 10-80 2.8 20
1.41 84.41.431.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 85.6 34-118 1.4 20
1.61 96.41.711.671.67<0.096mg/Kg2,4,5-Trichlorophenol 102 41-124 6.0 20
1.63 97.61.681.671.67<0.096mg/Kg2,4,6-Trichlorophenol 101 39-126 3.0 20
1022-Fluorobiphenyl (S)104 44-115
1042-Fluorophenol (S)103 35-115
89.8Nitrobenzene-d5 (S)89.2 37-122
1184-Terphenyl-d14 (S)116 54-127
1072,4,6-Tribromophenol (S)106 39-132
103Phenol-d5 (S)101 34-121
Page 21 of 23* QC Fail Date:02/28/2023 02:33 PM
Page 78 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L666151QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L665758
Associated Lab Samples: 89221, 89222, 89223, 89224, 89225, 89226
LRB-L665758 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
02/27/23 11:420.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L665758Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1184.704.00mg/KgChromium, Hexavalent 80-120
V 89221-DUP-L665758Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/27/23 12:040.4<0.201< 0.201mg/KgChromium, Hexavalent
V 89221-MS-L665758Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
32.2 79.540.5< 0.141mg/KgChromium, Hexavalent 75-125
Page 22 of 23Date:02/28/2023 02:33 PM
Page 79 of 82
Quality Control Data
23-051-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ANR.007
Dry Weight Determination
SW-DRYWT
V29993QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89244-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/21/23 17:114.723.722.6%Moisture
V 89261-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/21/23 17:110.033.833.8%Moisture
Page 23 of 23Date:02/28/2023 02:33 PM
Page 80 of 82
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-051-0030
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Asia Blakeborough Date & Time:02/20/2023 17:23:37
Special precautions or instructions included?
Comments:
Page 81 of 82
Pa
g
e

8
2

o
f

8
2

Appendix B
DEQ Risk Calculator Input/Output Forms
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Soil Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Southern Steel Brownfields Property
3015 Wilkinson Boulevard
DEQ DWM Brownfields Program
ANR-007
January 2023
November 2022 EPA RSL Table
3/6/2023
Prepared By:Hart and Hickman
Hart and Hickman
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes: CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.015 67-64-1 Acetone mg/kg
3.52 7440-38-2 Arsenic, Inorganic mg/kg
79.8 7440-39-3 Barium mg/kg
0.145 7440-43-9 Cadmium (Diet)mg/kg
0.0009 75-15-0 Carbon Disulfide mg/kg
43.2 16065-83-1 Chromium(III), Insoluble Salts mg/kg
0.003 110-54-3 Hexane, N-mg/kg
179 7439-92-1 ~Lead and Compounds mg/kg
0.0579 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.002 75-09-2 Methylene Chloride mg/kg
0.507 56-55-3 ~Benz[a]anthracene mg/kg
0.575 50-32-8 ~Benzo[a]pyrene mg/kg
0.787 205-99-2 ~Benzo[b]fluoranthene mg/kg
0.246 207-08-9 ~Benzo[k]fluoranthene mg/kg
0.505 218-01-9 ~Chrysene mg/kg
0.654 206-44-0 ~Fluoranthene mg/kg
0.379 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
0.704 129-00-0 ~Pyrene mg/kg
1.16 7782-49-2 Selenium mg/kg
0.0299 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 1.2E-05 1.6E-01 NO
Groundwater Use* NC NC NC
Soil 1.5E-06 1.2E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil 2.4E-07 1.6E-01 NO
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
Sitewide Risk Output Form 1B
Version Date: January 2023 NOTE: If any changes were made, select "Update Sitewide Risk Values" to obtain updated values.
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
Receptor Pathway
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Check box to
include in site-
wide risk
calculations
Carcinogenic
Risk Hazard Index
Soil 1.2E-05 1.6E-01 NM NM
Groundwater Use* NM NM NM NM
Soil 1.5E-06 1.2E-02 NM NM
Groundwater Use*NM NM NM NM
Construction Worker Soil 2.4E-07 1.6E-01
Soil NM NM
Surface Water Use*NM NM
Groundwater to Indoor Air NM NM NM NM
Soil Gas to Indoor Air NM NM NM NM
Indoor Air NMNM NMNM
Groundwater to Indoor Air NM NM NM NM
Soil Gas to Indoor Air NM NM NM NM
Indoor Air NM NM NM NM
1.2E-05 1.6E-01 0.0E+00 0.0E+00 1.5E-06 1.2E-02 0.0E+00 0.0E+00 2.4E-07 1.6E-01 0.0E+00 0.0E+00
3. NM = Not Modeled
4. NC = Pathway not calculated
Resident
Non-Residential Worker
Recreator/Trespasser
VAPOR INTRUSION CALCULATORS
DIRECT CONTACT SOIL AND WATER CALCULATORS
Non-Residential Worker - Future Scenario Construction Worker Recreator/TrespasserResident - Current Scenario Resident - Future Scenario Non-Residential Worker - Current Scenario
TOTAL SITEWIDE RISK FOR EACH RECEPTOR
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure.
Resident
Non-Residential Worker
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.015 0.015 0.015 2.1E-07 2.1E-07
7440-38-2 Arsenic, Inorganic 3.52 3.52 3.52 4.6E-06 6.4E-07 9.1E-11 5.2E-06 9.0E-02 1.1E-02 3.8E-06 1.0E-01
7440-39-3 Barium 79.8 79.8 79.8 5.1E-03 2.6E-06 5.1E-03
7440-43-9 Cadmium (Diet) 0.145 0.145 0.145 1.6E-12 1.6E-12 1.9E-02 1.8E-03 2.3E-07 2.0E-02
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 1.2E-07 3.9E-07 5.1E-07
16065-83-1 Chromium(III), Insoluble Salts 43.2 43.2 43.2 3.7E-04 3.7E-04
110-54-3 Hexane, N- 0.003 0.003 0.003 1.3E-06 1.3E-06
7439-92-1 ~Lead and Compounds 179 179 179 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0579 0.0579 0.0579 2.5E-03 3.1E-09 2.5E-03
75-09-2 Methylene Chloride 0.002 0.002 0.002 2.6E-11 6.3E-12 3.2E-11 4.3E-06 1.0E-06 5.3E-06
56-55-3 ~Benz[a]anthracene 0.507 0.507 0.507 3.3E-07 1.1E-07 6.4E-09 4.5E-07
50-32-8 ~Benzo[a]pyrene 0.575 0.575 0.575 3.8E-06 1.3E-06 5.7E-12 5.0E-06 2.5E-02 7.6E-03 4.6E-06 3.2E-02
205-99-2 ~Benzo[b]fluoranthene 0.787 0.787 0.787 5.1E-07 1.7E-07 7.9E-13 6.9E-07
207-08-9 ~Benzo[k]fluoranthene 0.246 0.246 0.246 1.6E-08 5.4E-09 2.5E-14 2.1E-08
218-01-9 ~Chrysene 0.505 0.505 0.505 3.3E-09 1.1E-09 5.0E-15 4.4E-09
206-44-0 ~Fluoranthene 0.654 0.654 0.654 2.1E-04 6.4E-05 2.7E-04
193-39-5 ~Indeno[1,2,3-cd]pyrene 0.379 0.379 0.379 2.5E-07 8.3E-08 3.8E-13 3.3E-07
129-00-0 ~Pyrene 0.704 0.704 0.704 3.0E-04 9.3E-05 3.9E-04
7782-49-2 Selenium 1.16 1.16 1.16 3.0E-03 9.4E-10 3.0E-03
7440-22-4 Silver 0.0299 0.0299 0.0299 7.6E-05 7.6E-05
Cumulative: 1.2E-05 1.6E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.015 0.015 0.015 1.4E-08 1.4E-08
7440-38-2 Arsenic, Inorganic 3.52 3.52 3.52 9.7E-07 2.0E-07 2.1E-11 1.2E-06 6.0E-03 1.3E-03 9.0E-07 7.3E-03
7440-39-3 Barium 79.8 79.8 79.8 3.4E-04 6.1E-07 3.4E-04
7440-43-9 Cadmium (Diet) 0.145 0.145 0.145 3.6E-13 3.6E-13 1.2E-03 2.1E-04 5.6E-08 1.5E-03
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 7.7E-09 9.3E-08 1.0E-07
16065-83-1 Chromium(III), Insoluble Salts 43.2 43.2 43.2 2.5E-05 2.5E-05
110-54-3 Hexane, N- 0.003 0.003 0.003 3.1E-07 3.1E-07
7439-92-1 ~Lead and Compounds 179 179 179 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0579 0.0579 0.0579 1.7E-04 7.4E-10 1.7E-04
75-09-2 Methylene Chloride 0.002 0.002 0.002 1.2E-12 5.2E-13 1.7E-12 2.9E-07 2.4E-07 5.3E-07
56-55-3 ~Benz[a]anthracene 0.507 0.507 0.507 1.6E-08 8.5E-09 5.3E-10 2.5E-08
50-32-8 ~Benzo[a]pyrene 0.575 0.575 0.575 1.8E-07 9.7E-08 4.7E-13 2.7E-07 1.6E-03 9.0E-04 1.1E-06 2.5E-03
205-99-2 ~Benzo[b]fluoranthene 0.787 0.787 0.787 2.4E-08 1.3E-08 6.5E-14 3.7E-08
207-08-9 ~Benzo[k]fluoranthene 0.246 0.246 0.246 7.5E-10 4.1E-10 2.0E-15 1.2E-09
218-01-9 ~Chrysene 0.505 0.505 0.505 1.5E-10 8.5E-11 4.2E-16 2.4E-10
206-44-0 ~Fluoranthene 0.654 0.654 0.654 1.4E-05 7.7E-06 2.2E-05
193-39-5 ~Indeno[1,2,3-cd]pyrene 0.379 0.379 0.379 1.2E-08 6.4E-09 3.1E-14 1.8E-08
129-00-0 ~Pyrene 0.704 0.704 0.704 2.0E-05 1.1E-05 3.1E-05
7782-49-2 Selenium 1.16 1.16 1.16 2.0E-04 2.2E-10 2.0E-047440-22-4 Silver 0.0299 0.0299 0.0299 5.1E-06 5.1E-06
Cumulative: 1.5E-06 1.2E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: ANR-007
Exposure Unit ID: Soil Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.015 0.015 0.015 7.4E-08 7.4E-08
7440-38-2 Arsenic, Inorganic 3.52 3.52 3.52 1.3E-07 2.0E-08 4.7E-08 1.9E-07 2.1E-02 3.3E-03 5.3E-02 7.7E-02
7440-39-3 Barium 79.8 79.8 79.8 1.2E-03 3.6E-03 4.8E-03
7440-43-9 Cadmium (Diet) 0.145 0.145 0.145 8.0E-10 8.0E-10 8.5E-04 1.1E-04 3.3E-03 4.2E-03
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 2.7E-08 1.2E-06 1.2E-06
16065-83-1 Chromium(III), Insoluble Salts 43.2 43.2 43.2 8.5E-05 1.9E-03 2.0E-03
110-54-3 Hexane, N- 0.003 0.003 0.003 2.9E-08 1.9E-06 2.0E-06
7439-92-1 ~Lead and Compounds 179 179 179 <SL** <SL** <SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0579 0.0579 0.0579 5.7E-05 4.3E-05 1.0E-04
75-09-2 Methylene Chloride 0.002 0.002 0.002 1.6E-13 1.3E-13 2.9E-13 9.8E-08 9.3E-07 1.0E-06
56-55-3 ~Benz[a]anthracene 0.507 0.507 0.507 2.0E-09 8.5E-10 1.9E-10 3.1E-09
50-32-8 ~Benzo[a]pyrene 0.575 0.575 0.575 2.3E-08 9.7E-09 1.1E-09 3.4E-08 5.6E-03 2.4E-03 6.5E-02 7.3E-02
205-99-2 ~Benzo[b]fluoranthene 0.787 0.787 0.787 3.2E-09 1.3E-09 1.5E-10 4.6E-09
207-08-9 ~Benzo[k]fluoranthene 0.246 0.246 0.246 9.9E-11 4.1E-11 4.5E-12 1.5E-10
218-01-9 ~Chrysene 0.505 0.505 0.505 2.0E-11 8.5E-12 9.3E-13 3.0E-11
206-44-0 ~Fluoranthene 0.654 0.654 0.654 1.9E-05 8.0E-06 2.7E-05
193-39-5 ~Indeno[1,2,3-cd]pyrene 0.379 0.379 0.379 1.5E-09 6.4E-10 7.0E-11 2.2E-09
129-00-0 ~Pyrene 0.704 0.704 0.704 6.9E-06 2.9E-06 9.8E-06
7782-49-2 Selenium 1.16 1.16 1.16 6.8E-04 1.3E-05 7.0E-04
7440-22-4 Silver 0.0299 0.0299 0.0299 1.8E-05 1.8E-05
Cumulative: 2.4E-07 1.6E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator