Loading...
HomeMy WebLinkAbout4101_Guilford_CityHighPoint_Riverdale_MSWLF_Seaboard_MonitoringComments_FID1776825_20230313Environmental Compliance and Remediation Babb & Associates, PA. March 13, 2023 Eric B. Aufderhaar, P.G., Environmental Program Consultant North Carolina Department of Environmental Quality Division of Waste Management 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Re: 2022 Annual Water Quality Monitoring Report — Response to Comments Former Seaboard Chemical and Riverdale Drive Landfill Site EPA ID# NCD 071 574 164 and NC Solid Waste 41-01 Dear Eric: In response to the February 23, 2023 correspondence from NCDEQ regarding the October 2022 Annual Water Quality Monitoring Report, the following revisions and/or comments are provided: Comment: Site Geology - Reference a figure that shows the location of geologic features or identify well locations to orient the reader to where the features are located. Response: In order to provide a complete description of the site geology, reference will be provided to the full October 2000 RI/FS Report which is available on the NCDEQ Laserfiche website. RI/FS:Volume 1 of 3 https://edocs.deq.nc.gov/WasteManagement/DocView.aspx?id=1655021 &dbi d=0&repo=WasteManagement&searchid=dbe35611-6ca6-4c3c-8e5c- f4f07b10865e RI/FS: Volumes 2 & 3 https://edocs.deq.nc.gov/WasteManagement/DocView.aspx?id=1655015&dbi d=0&repo=WasteManagement&searchid=dbe35611-6ca6-4c3c-8e5c- f4f07b10865e Comment: Well PW-SF1 is referenced in the Section but is not shown on Figure 2. Response: This well was inadvertently omitted as it has been converted to an extraction well. The location of PW-SF1 has been included on the revised Figure 2 (attached). Comment: The third paragraph references an extraction rate/capture zone test that was completed using well PW-DR01. This well is not shown on any of the figures. Response: Well PW-DR1 is the primary extraction point located adjacent to Lift Station 1. The location of this well has been added to Figure 2 of the revised report (attached). Comment: Seaboard Group II and the City of High Point should continue to monitor the contaminant concentrations in wells across the Deep River along with well MW- 12b, in the northwest part of the plume. At well MW-12b, the contaminant concentrations have not decreased as much over the last five years. Response: Agreed. Comment: Well MW-17 (WSW-1) is listed in the table but not shown on any of the figures. Where is it located? Response: Well MW-17 is a former drinking water supply well for the landfill operations. This well was converted into a monitoring well during the RI/FS process but is not part of the Site's monitoring program. It is located between Lift Station 2 and the Soil Residue Mound. A revised 2022 Water Quality Monitoring Report which addresses the issues discussed in this correspondence is attached. If there are any other questions or comments please contact us. Respectfully, Babb & Associates, P.A. Gary D. Babb, P.G. President Attachment Cc: Jaclynne Drummond Craig Coslett •••�11111111177111!•► •. SEAL i 488 •11111l1 it 111ti11 DENR USE ONLY ❑Paper Report [:]Electronic Data -Email CD (data loaded: Yes / No Doc/Event #: NC DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Babb & Associates, P.A. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Gary D. Babb E-mail: gdbabb(c)gmail.com Phone: 919/605-4719 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) Closed Riverdale Drived Landfill 5899 Riverdale Drive 41-01 .0500 October 12-20. 2022 Jamestown, NC Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring ❑ Assessment Monitoring �X Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells X❑ Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) Annual Monitori Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Gary D. Babb Licensed Geologist 919/605-4719 Facility Representative Name (Print) Signature Title (Area Code) Telephone Number November 21, 2022 Affix NC Licensed/ Professional Geologist Seal Date Babb & Associates, P.A., 5506 Bradford Pear Ct., Raleigh, NC 27606-1379 Facility Representative Address NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Water Quality Monitoring Report Former Seaboard Chemical/Riverdale Drive Landfill 5899 Riverdale Drive Jamestown, North Carolina Permit No. 41-01 NCD 071 574 164 Prepared for: Seaboard Group II and City of High Point High Point, NC Prepared by: Babb & Associates, P.A. 5506 Bradford Pear Court Raleigh, North Carolina 27606 October 2022 FA, W� ' - � L -0 41""f Gary D. Babb, Licensed Geologist Revised 3.6.2023 Table of Contents 1.0 Introduction 1.1 Site Information 1.2 Site Geology 1.3 Site Hydrogeology 2.0 Water Quality Monitoring Program 2.1 Groundwater Monitoring Network 2.2 Surface Water Monitoring Network 3.0 Water Quality Sample Collection 3.1 Field Sample Procedures 3.2 Field Quality Assurance 3.3 Sample Delivery/Chain-of-Custody 4.0 Laboratory Analysis 5.0 Hydrogeological Conditions 6.0 Laboratory Analytical Results 6.1 Groundwater Analytical Results 6.2 Surface Water Analytical Results 6.3 Quality Control Samples 7.0 Conclusions Figure 1 Site Location Map Figure 2 Groundwater Monitoring Well Locations Figure 3 Surface Water Monitoring Locations Figure 4 Groundwater Potentiometric Map Figure 5 1,4-Dioxane Isoconcentration Map Figure 6 Total Volatile Organics Isoconcentration Map Figure 7 1,2-Dichloroethane Isoconcentration Map Figure 8 Chlorobenzene Isoconcentration Map Figure 9 Vinyl Chloride Isoconcentration Map Figure 10 PW-15D/16D Contaminant Trend Graphs Table 1 Monitoring Well Construction/Groundwater Elevations Table 2 Groundwater VOC Concentrations Table 3 Surface Water VOC Concentrations Table 4 Field Parameters Table 5 Monitoring Well Lat/Long and Elevations Appendix A ENCO Laboratory Analytical Report 1 5 7 10 11 12 17 Revised 3.6.2023 1.0 Introduction 1.1 Site Information The former Seaboard Chemical/Riverdale Drive Landfill Site (the Site) is located approximately five miles east-southeast of High Point, NC near the intersection of Riverdale Drive and Interstate 85 (Figure 1). The Site consists of two properties, the facility where the former Seaboard Chemical Corporation (Seaboard) conducted operations and the closed municipal Riverdale Drive Landfill (Landfill), as shown on Figure 2. The former Seaboard Facility is located at 5899 Riverdale Drive, Jamestown, NC and consists of approximately 13 acres. Between 1974 and 1989, Seaboard operated solvent recovery and fuel blending processes at the facility. The corporation declared bankruptcy in 1989 and was not able to fund the cost of performing the necessary site closure and remediation. Removal activities were conducted during 1990 and 1992 to remove all remaining waste materials and certain tanks and equipment from the former Seaboard Facility. The removal was conducted by Seaboard Group I which was formed by parties that may have used the services of Seaboard in the past. The adjacent Landfill, a closed unlined municipal solid waste facility, consists of approximately 150 acres and bounds the former Seaboard Facility on two sides. The Landfill was operated from the 1950's until October 1993. The Landfill was permitted by the North Carolina DEQ - Solid Waste Section in 1979. During Landfill operations, sections of the two tributary streams that cross the landfill property were piped and solid waste was used to fill the drainage valleys. The two streams are referred to as the Southern Intermittent Stream and the Northern Intermittent Stream. During filling of the Southern Intermittent Stream valley, a leachate collection system was installed adjacent to the stream channel to collect leachate migrating from the overlying solid waste. In Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 1 1989, a leachate collection system was added to control surface seeps (leachate leaks) along the slopes of the Landfill. From approximately 1966 to 1970, Landfill operations also included the disposal and open burning of spent solvents in shallow pits located just north of the former Landfill scale house (Figure 2). Periodically, these burn pits were cleaned of residue that accumulated in a mound to the south of the burn pits. Presently, this mound consists of approximately 600 cubic yards of contaminated residue capped by a synthetic liner and is referred to as the "soil residue mound". The Landfill is now capped and maintained under an approved post -closure plan. Seaboard Group II was formed in 1994 and entered into an agreement with the City of High Point (the City) to jointly perform a remedial investigation and prepare a baseline risk assessment and feasibility study for the Site, including both the former Seaboard Facility and closed Landfill properties. The Seaboard Group II and the City then entered into an Administrative Order on Consent (AOC) dated January 30, 1996 with NC DEQ to perform the remedial investigation. The feasibility study was conducted under a separate AOC dated July 22, 1997. Remedial investigations conducted at the Site have documented the presence of chlorinated and non -chlorinated volatile organic compounds (VOCs) in soils, leachate, groundwater, and surface water. The results from the remedial investigation indicate that the VOC-affected groundwater had migrated toward Randleman Lake, which adjoins the Site along the northern and eastern property boundary of the Landfill. The Randleman Lake was created by the impoundment of the Deep River in 2006 by the Randleman Lake Dam, which is located approximately 11.5 miles downstream of the Site. The Remedial Recommendation Document (February 2005) presented a remedial strategy for the impacted media at the Site based on the results of the remedial investigation, Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 2 baseline risk assessment, and feasibility study. The remedial design consisted of groundwater extraction and treatment in combination with institutional controls including site access control, recorded land use restrictions, and restriction of water supply well construction. The groundwater and surface water monitoring program is designed to evaluate the effectiveness of the remedy. The Remedial Recommendation Document was conditionally approved by the NC DEQ in September 2005. Seaboard Group II and the City entered into a Remedial Action Settlement Agreement (RASA) with NC DEQ on December 29, 2008. The RASA provides for the design and implementation of the approved remedial action program for the Site as well as completion and reporting of annual groundwater and surface water monitoring activities. 1.2 Site Geology The geology at the Site was fully evaluated during the Remedial Investigation /Feasibility Study which was completed in October 2000. The full text and figures of this evaluation can be reviewed at the following NCDEQ Laserfiche locations: RI/FS:Volume 1 of 3 https:Hedocs.deq.nc.gov/WasteManagement/DocView.aspx?id=l 655021 &dbid=0&repo= WasteManagement&searchid=dbe35611-6ca6-4c3 c-8e5c-f4f07b 10865e RI/FS: Volumes 2 & 3 https:Hedocs.deq.nc.gov/WasteManagement/DocView.aspx?id=l 655015&dbid=0&repo= WasteManagement&searchid=dbe35611-6ca6-4c3 c-8e5c-f4f07b 10865e Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 3 1.3 Site Hydrogeology The Site hydrogeology is characteristic of the regional piedmont aquifer system and consists of three aquifer units: the saprolite and partially weathered rock (PWR) aquifer, shallow bedrock aquifer, and deep bedrock aquifer. The saprolite/PWR aquifer is the uppermost aquifer across much of the Site, but is locally absent where the water table occurs below the top of bedrock. The thickness of the saprolite/PWR aquifer, where present, is generally less than 20 feet but extends to depths of 90 feet in limited areas (PW-13I). The shallow bedrock aquifer extends from the top of competent bedrock to a depth where groundwater flow becomes limited due to the lack of open fractures. The base of the shallow bedrock zone at the Site is variable but generally believed to occur at depths of 200 to 400 feet. The deep bedrock aquifer extends downward from the base of the shallow bedrock aquifer and is characterized by low permeability and limited groundwater flow. The primary zone of groundwater movement at the Site is considered to occur within the saprolite/PWR and shallow bedrock aquifer zones. The saprolite/PWR and shallow bedrock aquifers are hydraulically connected. The potentiometric surface of shallow groundwater in the saprolite/PWR aquifer is generally a subdued replica of the original topography of the Site. The saprolite/PWR aquifer is locally absent where the water table occurs below the top of bedrock (generally beneath higher topographic elevations). Groundwater flow within the shallow bedrock aquifer is primarily through fractures in the bedrock and is strongly controlled by subsurface geologic structures such as faults, fracture zones, and mafic dikes. Two constant rate discharge tests were conducted in August and September 1997. The calculated bulk hydraulic conductivity values at the Site range from 0.5 to 3 feet/day in the saprolite/PWR aquifer and 0.1 to 0.6 feet/day in the shallow bedrock aquifer. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 4 2.0 Water Quality Monitoring Program The water quality monitoring network at the Site is evaluated on an annual basis. The locations of the groundwater and surface water samples collected during the annual monitoring event are shown on Figure 2 and 3, respectively. The primary objectives of the annual groundwater and surface water monitoring program are: • Monitor VOC concentrations and migration of the VOC-affected groundwater; • Monitor groundwater elevations, hydraulic gradients and flow directions; • Monitor surface water quality in Randleman Lake, Northern Intermittent Stream, and Southern Intermittent Stream to assess water quality. The 2022 annual groundwater and surface water monitoring activities were conducted at the Site during the period of October 12-20, 2022. Groundwater level gauging was conducted at the monitoring wells to be sampled to evaluate groundwater flow patterns at the Site (Figure 4). Surface water sampling was conducted at nine surface water stations which included; four stations along Randleman Lake (SW-6, SW-7, SW-DRP-2, and SW-DRP-11), three stations on the Southern Intermittent Stream (SW-3, SW-4, and SW-5), and two monitoring stations on the Northern Intermittent Stream (SW-1 and SW-2). Please note that surface water monitoring stations SW-1 was dry during this sampling event. 2.1 Groundwater Monitoring Network The existing groundwater monitoring network consists of 24 monitoring wells which have been selected to evaluate the lateral and vertical extent of the contaminant plume as well as the effectiveness of the groundwater extraction system (Figure 2). The 24 monitoring wells sampled for subsequent laboratory analysis include: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 5 MW-1 (background) MW-3C MW-6 MW-10 MW-1 2A MW-12B MW-12D MW-15A OW-DR2 OW-LFS2 PW-31) PW-4I PW-51) PW-6I PW-61) PW-10I PW-1 OD PW-12I PW-13I PW-14D PW-15D PW-16D PW-SF 1 W-4A Monitoring well construction information and groundwater elevations for the monitoring wells at the Site are provided on Table 1. 2.2 Surface Water Monitoring Network The current surface water monitoring network consists of nine monitoring stations as shown on Figure 3. The surface water monitoring stations are located along the Northern Intermittent Stream, Southern Intermittent Stream, and on Randleman Lake. The nine surface water stations sampled for the water quality monitoring program include: SW-1 SW-3 SW-5 SW-7 SW-DRP- I I SW-2 SW-4 SW-6 SW-DRP-2 * The surface water samples collected from the Randleman Lake are collected at two discrete depths, 1' below the surface and I' above the bottom of the lake. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 6 3.0 Water Quality Sample Collection Samples of groundwater and surface water were collected in accordance with the approved Annual Monitoring Plan — 2010 dated March 17, 2010. A brief description of the sample collection procedure is provided below. The 2022 annual groundwater and surface water monitoring activities were conducted at the Site during the period of October 12-20, 2022. 3.1 Field Sample Procedures Prior to groundwater sampling, water levels were obtained from each well using an electric water level meter capable of measuring the depth to water to the nearest 0.01 feet. This information was later used to determine the elevation of the water table in each monitoring well relative to surveyed datum (Table 1). The groundwater elevations are used to develop a potentiometric map of the shallow water table (Figure 4). The monitoring wells were sampled using low -flow purge and sample procedures. The groundwater samples were collected using either a peristaltic pump or Grunfos pump with disposable poly tubing. The depth of the intake tubing is positioned at the mid -point of the well screen and the pumping rate is adjusted to match recharge and minimize drawdown in the well. Multiple field parameters, including pH, specific conductivity, temperature, dissolved oxygen, and ORP, are constantly monitored using a flow cell. The turbidity of the influent groundwater is periodically evaluated using a field meter capable of measuring turbidity to +0.01 NTU. Low -flow purging of the well continues until the field parameters have stabilized and the NTU concentration is <10 NTUs, at which time the sample is collected. The samples are collected in the following order: • VOCs and 1,4-dioxane • Field parameters (pH, conductivity, temperature, dissolved oxygen) Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 7 The samples were collected directly in the laboratory -supplied containers which were pre -filled with the appropriate preservative. No filtering of the samples was performed either in the field or laboratory. After collection, the samples were placed in a cooler on ice for overnight shipment to the analytical laboratory. Surface water samples were collected directly into the laboratory -supplied containers as grab samples. Sampling personnel wore new disposable nitrile gloves for each surface water sample collected. The surface water samples collected from the four stations along the Randleman Lake were collected at two discrete intervals: a shallow sample collected one foot below the surface, and a deeper sample collected one foot above the bottom of the Lake. The Randleman Lake water samples were collected using a stainless steel discrete -interval Kemmerer water sampler. The actual depths of the shallow and deeper Randleman Lake surface water samples are provided in Table 4. As with the groundwater samples, these samples were stored in a cooler on ice prior to overnight delivery to the analytical laboratory. 3.2 Field Quality Assurance Two trip blank samples were prepared by the analytical laboratory and accompanied the sample shipments until receipt by the laboratory. The trip blank samples were analyzed for VOCs. Temperature blanks were also provided with the sample shipments to assure the proper temperature was maintained until delivery to the analytical laboratory. 3.3 Sample Delivery/Chain of Custody All groundwater and surface water samples were stored in coolers on ice immediately after collection. Individual sample containers for each monitoring well or surface water sample were placed in zip lock plastic bags to reduce the potential for cross contamination between sample locations. Chain -of -Custody control documents were prepared and shipped with each cooler. Custody seals were also used for each cooler to Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 8 maintain sample integrity until delivery to the analytical laboratory. The sample coolers were shipped via Federal Express for next morning delivery to the analytical laboratory. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 9 4.0 Laboratory Analysis The groundwater and surface water samples were analyzed for VOCs by EPA Method 8260D and 1,4-dioxane by EPA Method 8260D SIM. The laboratory performing the water quality analysis is Environmental Conservation Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory. Internal quality control samples, including matrix spikes/matrix spike duplicates, were performed by ENCO for each set of samples. The ENCO laboratory reports, including internal quality control samples, are provided with this report in Appendix A. Field parameters (pH, specific conductivity, temperature, dissolved oxygen) were also measured by the sampling personnel for each groundwater and surface water sample using calibrated meters. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 10 5.0 Hydrogeological Conditions The depth to groundwater was measured in the 24 compliance monitoring wells during the October 2022 monitoring event. The groundwater elevations were calculated relative to the surveyed measuring point (top of casing) for each monitoring well. A groundwater potentiometric map is provided as Figure 4. This potentiometric map primarily represents groundwater flow in the uppermost aquifer. The groundwater depths and elevation data for the Site monitoring wells are summarized in Table 1. In the bedrock aquifer the general groundwater flow direction across the Site is northeastward toward Randleman Lake. The vertical hydraulic gradient in the shallow bedrock aquifer, as measured between monitoring wells MW-3C and OW-DR2 during the October 2022 monitoring event, was 0.021 feet/feet downward. An Extraction Rate/Capture Zone Test was conducted by ERM NC, PC in August 2002. This test used well PW-DR1 as the primary extraction point to determine the potential capture zone using various pumping rates. The results of this test indicated pumping at a relatively low rate of 10 - 20 gallons per minute from PW-DR1 effectively contains the contaminant plume. A pumping rate of 7 gallons per minute from PW-DR1 during operation of the system has demonstrated a drawdown of approximately 45 below top of casting which creates an effective capture zone. The filling of Randleman Lake began in 2006 and the lake level reached normal pool elevation (682 feet msl) in 2008. Consistent with prior gauging events, and confirmed with the data collected during the October 2022 monitoring event, groundwater levels at monitoring wells located adjacent to the lake have risen 10 - 12 feet as compared to pre -lake water level conditions. Inland from the lake, groundwater levels at wells located on the western portion of the Site have risen approximately 4 feet due to the lake impoundment. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 11 6.0 Laboratory Analytical Results The complete analytical results for the samples collected during the period of October 12-20, 2022 were received from the laboratory on October 28 and 31, 2022, and November 1 and 7, 2022. A summary of the analytical results are provided for groundwater (Table 2), surface water (Table 3), and field parameters (Table 4). 6.1 Groundwater Analytical Results The analytical results for selected groundwater contaminants collected during the October 2022 monitoring event are shown in a series of figures. Groundwater quality maps representing the bedrock aquifer are provided for 1,4-dioxane (Figure 5), total VOCs (Figure 6), 1,2-dichloroethane (Figure 7), chlorobenzene (Figure 8), and vinyl chloride (Figure 9). The historical groundwater analytical results for specific VOCs, including the 2022 data, are summarized in Table 2 and the ENCO laboratory reports are provided in Appendix A. Measurements of pH, temperature, and specific conductance as determined in the field during sample collection are provided in Table 4. Additional monitoring well information including the latitude/longitude of each well location is provided in Table 5. The main mass of VOC-impacted groundwater generally extends northeastward across the Site to the Randleman Lake basin. As shown on Figure 6, the highest levels of VOCs are present in the vicinity of the northeast corner of the Seaboard Facility near the location of three former surface impoundments. Prior to their closure and capping between 1984 and 1986, the area of the former impoundments served as a primary source area of VOC releases to the groundwater at the Seaboard Facility. Additionally, elevated VOC concentrations in groundwater are also present in the area of the soil residue mound, a contaminant source area located at the Landfill which has also been closed and capped with a synthetic liner. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 12 During this monitoring event, VOCs were detected in a limited area across Randleman Lake to the northeast of the Site. Minor concentrations of VOCs at levels above the North Carolina 2L Groundwater Quality Standards were detected at off -site bedrock monitoring wells PW-15D and PW-16D. These bedrock monitoring wells are located on the north side of the Randleman Lake basin from the Site. The extent of the VOC contaminant plume on the north side of Randleman Lake appears to be limited primarily to property encompassed by the Lake's buffer zone, which is maintained and regulated by the Piedmont Triad Regional Water Authority (PTRWA). Overall, the October 2022 groundwater analytical results and the general distribution of VOCs in the Site's groundwater are consistent with the historical groundwater quality monitoring results. As shown on Figure 10, a historical reduction in contaminant concentrations in the monitoring wells on the north side of Randleman Lake is evident from the groundwater VOC and 1,4-dioxane data collected during this monitoring event. 6.2 Surface Water Analytical Results Surface water sampling was conducted at the Southern Intermittent Stream, Northern Intermittent Stream, and at various locations and depths in Randleman Lake. The surface water monitoring results for VOCs and 1,4-dioxane are summarized in Table 3 and the ENCO laboratory report is provided in Appendix A. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 13 Randleman Lake The Randleman Lake surface water sampling stations include: • SW-6 — Upstream and background sample location for the Site, • SW-DRP-2 — Adjacent to the Site near Lift Station 1 and PW-DR1, • SW-7 — Downstream of the Site at the I-85 bridge, and • SW-DRP-11 —Downstream (-1 mile) at Richland Creek confluence. The laboratory analytical data indicated no VOC concentrations above the laboratory practical quantitation limits in any of Randleman Lake surface water samples. Only one Randleman Lake sample reported a concentration of 1,4- dioxane above the laboratory reporting limit. The surface sample (1' depth) collected at surface water sample location SW-DRP11 reported a concentration of 1.0 ug/l. No other Randleman Lake surface water samples reported detectable concentrations of 1,4-dioxane above the laboratory reporting limit. The locations of the surface water monitoring stations are shown on Figure 3 and a summary of the Randleman Lake surface water analytical results are provided in Table 3. Note that the SW-DRP11 surface water monitoring station is located approximately 4,000 feet downstream of the Site at the confluence with Richland Creek. There are at least two known sources of 1,4-dioxane surface water contamination on Richland Creek upgradient of this confluence. Based on field observations during the October 2022 monitoring activities, the Randleman Lake was at or near the normal pool elevation of 682 feet msl. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 14 Southern Intermittent Stream The Southern Intermittent Stream surface water sampling stations include: • SW-5 — Upstream of Seaboard Facility and downstream of City MRF, • SW-3 — Downstream of Seaboard Facility and upstream of Landfill, and • SW- 4 — Downstream of both Seaboard Facility and Landfill. The compound 1,4-dioxane was reported in all three of the Southern Intermittent Stream surface water monitoring stations. The upstream surface water monitoring station (SW-5) reported a 1,4-dioxane concentration of 1.6 ug/l. Both of the downstream surface water monitoring stations on the Southern Intermittent Stream, SW-3 and SW-4, reported detectable 1,4-dioxane concentrations of 2.1 ug/I and 14 ug/l, respectively. No other Site VOCs were reported above the laboratory reporting limits in the samples collected from surface water monitoring station SW-5. Only one VOC (cis-1,2-dichloroethene — 1.2 ug/1) was reported in surface water sample SW-3 at a concentration well below the regulatory standard of 60 ug/l. The sample collected from surface water monitoring station SW-4 reported seven VOCs above the laboratory reporting limit, with two compounds (1,2-dichloroethane and vinyl chloride) exceeding the regulatory standards. A summary of the analytical data for the Southern Intermittent Stream surface water samples is provided in Table 3. Northern Intermittent Stream The Northern Intermittent Stream surface water sampling stations include: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 15 • SW-1 Surface Water Station —Upstream of the Landfill, and • SW-2 Surface Water Station — Downstream of the Landfill. The flow path of the Northern Intermittent Stream was re-routed in 2011 and no longer passes through a pipe beneath the Landfill. Due to a limited watershed area, these two surface water monitoring stations are typically dry except during periods of heavy rainfall. The upstream surface water location (SW-1) was dry during the October 2022 monitoring event. A surface water sample was collected from the SW-2 location which reported a 1,4-dioxane concentration of 14 ug/l. No VOC compounds were reported in this sample above the laboratory reporting limits. A summary of the laboratory analytical results for October 2022 surface water monitoring event is provided on Table 3. A copy of the ENCO laboratory analytical report for the surface water samples is provided with Appendix A. 6.3 Quality Control Samples Two trip blanks were submitted and analyzed for quality assurance purposes. No VOCs were detected at a concentration equaling or exceeding its laboratory quantitation limit in either of the trip blanks. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 16 7.0 Conclusions The major findings of the annual groundwater and surface water monitoring activities for October 2022 monitoring event at the Site include the following: • The overall groundwater flow pattern at the Site continues to be toward Randleman Lake on both sides of the Lake basin (Figure 4). Operation of the extraction well PW-DR1 over the past year indicates a significant capture zone for monitoring wells along the northern section of the Landfill adjacent to Randleman Lake. The observed capture zone also extends to the bedrock wells on the north side of Randleman Lake. The capture zone can be maintained by pumping extraction well PW-DR1 at a rate of approximately 7 - 10 gallons per minute. An operational extraction rate of 7 gallons per minute from PW-DR1 during this monitoring period has demonstrated a drawdown of approximately 45 feet below top of casing which creates an effective capture zone. • In addition to the PW-DR1 extraction well, four additional extraction wells were added in June 2022 to supplement the existing remedial system. Two new extraction wells (R-1 and PW-SF1) are located immediately downgradient of the former Seaboard processing area (Pond 3). Also, two new extraction wells (RW- SIS7 and RW-SIS8) are located at the SIS Basin area. These extraction wells have proven to be very effective in removing contaminant mass from the saprolite and shallow bedrock groundwater zones. A separate report is being prepared to evaluate the effectiveness of these new extraction locations. Based on the October 2022 monitoring results and historical data, the main VOC plume extends from the Site through the Southern Intermittent Stream valley northeastward to Randleman Lake. The minor concentrations of VOCs detected on the north side of the Randleman Lake in monitoring wells PW-15D and PW- 16D represents the northern extent of the VOC plume. Based on historical Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 17 analytical results, the northern extent of Site VOCs in the groundwater north of Randleman Lake is likely restricted to the Piedmont Triad Regional Water Authority regulated buffer. • During the October 2022 monitoring event, concentrations of 1,4-dioxane above the laboratory practical quantitation limit were reported at five of the nine surface water monitoring locations. The four surface water samples collected from the Southern and Northern Intermittent Streams exceeded the laboratory quantitation limit and the established NC In -Stream Target Value of 0.35 ug/l. Of the four surface water monitoring stations on Randleman Lake, the upstream sample (SW-8), sidegradient sample (SW-DRP2), and the sample collected immediately downstream of the Site (SW-7) did not report 1,4-dioxane above the laboratory method detection limit of 0.30 ug/l. Only one of the Randleman Lake surface samples (SW-DRP11 — F depth) reported a detectable 1,4-dioxane concentration. The reported concentration of 1.0 ug/1 in this sample is slightly above the NC In -Stream Target Value of 0.35 ug/l. Note that the SW-DRP11 surface water monitoring station is located approximately 4,000 feet downstream of the Site at the confluence with Richland Creek. There are at least two known sources of 1,4-dioxane surface water contamination on Richland Creek upgradient of this confluence. • The October 2022 monitoring data indicated that groundwater levels at monitoring wells located adjacent to the Randleman Lake have risen approximately 10 to 12 feet compared to pre -lake water level conditions. Inland from the lake, the October 2022 groundwater levels at wells located on the western portion of the Site are approximately four feet higher compared to pre - lake water level conditions. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 18 • Overall, the October 2022 groundwater monitoring results are generally consistent with historical monitoring data. The pumping of extraction well PW-DR1 at a rate of 7 gallons per minute has demonstrated a significant capture zone created by the drawdown on both sides of Randleman Lake. A historical reduction in contaminant concentrations in the monitoring wells on the north side of Randleman Lake from the Site is evident from the groundwater VOC data collected during this monitoring event (Figure 10). Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report (Revised 3.6.2023) October 2022 Page 19 FIGURES -► + - Greensboro I T L --.� 8 f - High Point Seaboard/Riverdai Landfill Site' __ �. 20 is t _ fit 6 a 62 62 - - r 20 N - Site Location T t Figure 1 — Site Location Map Babb & Associates, P.A. Former Seaboard/Riverdale Drive Landfill Site 5506 Bradford Pear Court 5899 Riverdale Drive Raleigh, North Carolina 27606-1379 Jamestown, North Carolina (919) 605-4719 Scale: Prep. By: Rev. By: Date: 1" = 1.5 miles G. Babb G. Babb October 2022 Er [MW-1 ,r �4 1 , - A. N Ph y to MW-12A;,. MW-12B .,.. Zones MW-12D 1-11 Soil --, Residue Mound :.; PW-131 Lift Station 2 1i MW-15A W-4AI9bIPW-3D Mw PW-SF1 i Former Pond 3 SCC Site PW-14D PW-15D :. 4D PW-16D At PW-6D PW-61 DOW-DR2 MW-3C" PW-DR1 CD PW-5D Phyto Zones 12-16 OW-LFS2 :C PW-41 SO MW-10 PW-101 PW-10D PW-121 1 jEq.`,jr—. 4C MW-6 - f r�j J+, 4 t i SW-2 It SW-6 Located Upstream At Kivett Dr. Bridge SW-1 ~ Phyto Zones 1-11 SW-DRP2 Soil Residue, SW-4 ' Mound e 40 F r - SW-5 SW-3 Phyto Fo mer Pond 3 1 r 0 Zones 12-16 r, r SW-; ■ '•�O COO SW-DRP11 CO Located Downstream At the Confluence of Richland Creek 720 710 700* 0 r F 1*V P682.57 hyto `BMW-12A ,680.82 Zones 659.20 ; "PW-16D ULL ` PW-14D - 680.59 PW-15D \765.10 ' ,.681.39 681.31 MW-1 681.57 `DPW-131 .. ` MW-3C Soil PW-SF1 v , 650 Residue ' 658 Mound = TM*t,.* >• .. Ilk MW-15A i . # 739:12 W-LFS2 697.77 .,v PW-3D 660.00 . \I I\ PW-41 Phyto . .......... ... +, 680 .68f:1.5 ,•ID6.692.40 Zones Y 679.54 :., 16 c 12-h •_ MW-10 .............. er Pond* 3. c 720 i1 -— 710 # i I\PW-121 722.08 700 68 r \IMW 6 690 6o ` 1 696.10 6t MW-1 \4BQL N ;50 ug/I Phyto ;;. MW-12A Zones 1-11 PW-131,, 84 ug/I 170 ug/12: O Soil dh PW-5D \, Residue,, 310 ug/I hAni inrl 'L MW-15A \�830 ug/I Phyto Zones 12-16 ,DPW-41 150 ug/I 10 ug/I All \�W-4A ,DPW-3D \�180 ug/I T . �o j Former Pond 3 SCC Site ,\PW-121 \I BQL ,.45 ug/I \r PW-16D 83 ug/I \FPW-15D At PW-6D 180 ug/I CD r m 220 ug/I,. OW-LFS2\w 590 ug/I:�� PW-101 '\I MW-6„ 23 \I ug/I .ti y ;,�12 ug/I to �j�MW-12B �9 ug/I Zones .. 1-11 �kPW-14D P - 6D \I 36 ug/I 63: g/I IF PW-15D PW-6D MW-1 w w _ n rA I inli \V gym\ 101 -4, r .f. i MW-12Ai� PhytoBQL MW-12B Zones MW-126 1-11 BQL \" PW-14D BQL Igh \"PW-15D 1.4 ug/IAh $ u /I PVV-131 low g ... .. O W -DR2 \" Soil PW-SD Residue, 17 ug/I hA n 1 1 n rl,; IRb, MW-15AIRV 4 BQL !\W-4A BQL`" 12,000 ug/I \" �1h PW-41 PW3D \20 ug/I Fo mer Pond 3 AkPW-121 "BQL ��}w �. K' N _# ..BQL \"PW-16D At \I PW-6D 2.6 ug/I BQL ,k OW-LFS2\" Phyto Zones 12-16 BQ�-Ajh W PW-101 PW-10D \MW-6 �K... \I BQL P\ 7 kbw'ALI �f "' 8 ug/I Phyto . MW-12B Zones 1-11 PW-14D 1.3 ug/I 3.91hug/I 19 \FPW-15D ..MW-1 11 ug/I \ 4BQL PW-131 \F 72 ug/I ...fir' OW-DR2 IMF Soil •. I\ PW-5D Residue,, 150 ug/I Mound glk MW-15A `i ••170 ug/I Phyto Zones r • ,. W-4A 12-16 3.9 ug/I PW-3D .. PW-41 20,000 ug/I \�53 ug/I 4 5 Former Pond 3 PW-121 \I BQL } N ..50 ug/I \F PW-16D 190 PW-6D 17 ug/I m r m ..BQL \• OW-LFS2 3.3 ug/j,,. PW-101 \I . r, w yrfr" `+�► ram. r - �+* r.L . MW-12A BQL Q'i.�\ Phyto MW-12B Zones MW-12D�� 1-11 Concentration > 1( 0 Concentration >1, . Monitoring Well L( 23 Vinyl Chloride Cor V-1 \5.3 ug/I \PW-14D low PW-16D Q 1.2 u /I BQL g ,\ 'IrPW-15D At qF PW-6D 7.1 ug/I,\ 21 ug/I��\ 2.6 ug/I low OW-DR2 'IW Soil _ \PW-5D Residue,, , 6 ug/I CD nn„i ind _ MW-15A BQL m 25 u /I ,\ BQL g Phyto „OW-LFS2 a: W-4A ;; PW-3D ,\PW-41 Zones 4,200 ug/I 35 ug/I 12-16 1.7 ug/I :�� PW-101 V Former Pond 3 , 4,\PW-121 `BQL N �I Figure 10 — VOC & 1,4-Dioxane Graphs Former Seaboard/Riverdale Drive Landfill Site 5899 Riverdale Drive Jamestown, North Carolina Scale: Prep. By: No Scale G. Babb Babb & Associates, P.A. 5506 Bradford Pear Court Raleigh, North Carolina 27606-1379 (919) 605-4719 Rev. By: Date: G. Babb October 2022 TABLES TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 1 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-1 57.71 47.71-57.71 743.98-733.98 789.40 791.69 11/14/2000 27.28 764.41 9/4/2001 27.99 763.70 9/17/2002 29.55 762.14 9/11/2003 23.86 767.83 8/16/2004 25.70 765.99 12/19/2005 25.55 766.14 8/21/2006 25.97 765.72 9/24/2007 26.33 765.36 2/23/2009 25.35 766.14 3/29/2010 24.89 765.72 11/1/2011 27.69 764.00 11/16/2012 27.23 764.46 12/9/2013 28.36 763.33 12/8/2014 28.54 763.15 New Survey 788.85 790.46 10/26/2015 27.99 763.47 11/14/2016 27.50 762.96 10/11/2017 28.43 762.03 11/1/2018 29.70 760.76 9/10/2019 24.78 765.68 10/13/2020 27.67 761.18 10/26/2021 26.86 763.60 10/12/2022 25.36 765.10 MW-2A 19 4-19 709.9-694.9 711.80 713.90 11/14/2000 13.46 700.44 9/4/2001 17.43 696.47 9/17/2002 10.25 703.65 9/11/2003 10.60 703.30 8/16/2004 7.83 706.07 8/21 /2006 13.04 700.86 9/24/2007 14.17 699.73 2/23/2009 10.67 703.23 3/29/2010 6.11 707.79 11/1/2011 8.18 705.72 11/16/2012 12.90 701.00 MW-26 30 30 681.0 711.00 712.57 11/14/2000 12.78 699.79 9/4/2001 13.01 699.56 9/17/2002 10.61 701.96 9/11/2003 10.62 701.95 8/16/2004 7.75 704.82 8/21 /2006 12.25 700.32 9/24/2007 14.64 697.93 2/23/2009 10.35 702.22 3/29/2010 6.05 706.52 11/1/2011 9.16 703.41 1 /16/2012 12.21 700.36 MW-2C 48 28-48 685.56-665.56 711.40 713.56 11/14/2000 16.12 697.44 9/4/2001 14.02 699.54 9/17/2002 18.41 695.15 9/11/2003 12.78 700.78 8/16/2004 14.80 698.76 12/19/2005 NM NM 8/21 /2006 17.53 696.03 9/24/2007 16.86 696.70 2/23/2009 14.25 699.31 3/29/2010 10.97 702.59 11/1/2011 14.55 699.01 11/16/2012 15.82 697.74 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 2 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-3A 27 12-27 682.4-667.4 692.74 694.40 11/14/2000 19.62 674.78 9/4/2001 21.03 673.37 9/17/2002 20.22 674.18 9/11/2003 16.74 677.66 8/16/2004 18.60 675.80 12/19/2005 18.54 675.86 8/21/2006 20.32 674.08 9/24/2007 17.18 677.22 2/23/2009 11.00 683.40 3/29/2010 10.92 683.48 11 /1 /2011 12.34 682.06 11/16/2012 11.87 682.53 MW-36 38.83 28.83-38.83 664.76-654.76 692.32 693.59 11/14/2000 19.46 674.13 9/4/2001 21.00 672.59 9/17/2002 20.00 673.59 9/11/2003 16.32 677.27 8/16/2004 NM NM 12/19/2005 18.81 674.78 8/21/2006 20.33 673.26 9/24/2007 16.59 677.00 2/23/2009 8.48 685.11 3/29/2010 8.04 685.55 11 /1 /2011 11.27 682.32 11/16/2012 11.00 682.59 MW-3C 57 47-57 647.22-637.22 691.90 694.22 11/14/2000 19.51 674.71 9/4/2001 21.12 673.10 8/19/2002 20.57 673.65 9/16/2002 20.00 674.22 9/11/2003 16.47 677.75 8/16/2004 18.46 675.13 12/19/2005 18.96 674.63 8/21/2006 20.56 673.03 9/24/2007 16.50 677.72 2/23/2009 10.15 683.44 3/29/2010 7.86 685.73 11 /1 /2011 10.33 683.89 11/16/2012 10.88 683.34 12/11/2013 10.54 683.68 12/11/2014 20.74 673.48 New Survey 692.50 692.74 10/27/2015 17.68 675.06 11/14/2016 9.90 682.84 10/9/2017 20.46 672.28 11 /2/2018 18.31 674.43 9/11/2019 18.00 674.74 10/13/2020 17.54 674.96 10/26/2021 15.24 677.50 10/17/2022 11.17 681.57 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 3 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-4 30 20-30 664.72-654.72 683.20 684.72 11/14/2000 12.22 672.50 9/4/2001 14.18 670.54 9/ 16/2002 12.71 672.01 9/11/2003 10.62 674.10 8/16/2004 11.91 672.81 12/19/2005 17.55 667.17 8/21/2006 NM NM 9/24/2007 13.22 671.50 New TOC elevation 683.87 687.29 2/23/2009 8.02 679.27 3/29/2010 6.25 681.04 11/1/2011 6.48 680.81 11/16/2012 7.01 680.28 MW-5 30 20-30 664.4-654.4 682.00 684.40 11/14/2000 12.89 671.51 9/4/2001 14.69 669.71 9/ 16/2002 13.81 670.59 9/11/2003 9.23 675.17 8/16/2004 12.05 672.35 12/19/2005 16.59 667.81 8/21/2006 NM NM 9/24/2007 13.98 670.42 New TOC elevation; survey data pending 2/23/2009 5.82 NA 3/29/2010 4.63 NA 11/1/2011 6.18 NA 11/16/2012 6.61 NA MW-6 110 100-110 661.73-651.73 759.60 761.73 11/14/2000 65.92 695.81 9/4/2001 66.49 695.24 9/17/2002 67.21 694.52 9/11/2003 59.32 702.41 8/16/2004 63.47 698.26 12/19/2005 65.83 695.90 8/21/2006 66.46 695.27 9/24/2007 67.11 694.62 2/23/2009 62.58 699.15 3/29/2010 60.55 701.18 11/1/2011 64.36 697.37 11/16/2012 64.60 697.13 12/11/2013 64.88 696.85 12/12/2014 65.80 695.93 New Survey 759.74 761.47 10/30/2015 64.89 696.58 11/17/2016 64.38 697.09 10/10/2017 65.03 696.44 11 /2/2018 61.20 700.27 9/12/2019 62.28 699.19 10/14/2020 63.00 696.74 10/28/2021 65.11 696.36 10/19/2022 65.37 696.10 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 4 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-7A 35 15-35 726.64-706.64 739.42 741.64 11/14/2000 31.10 710.54 9/4/2001 32.34 709.30 9/17/2002 35.73 705.91 9/11/2003 22.61 719.03 8/16/2004 29.02 712.62 12/19/2005 31.13 710.51 8/21 /2006 31.19 710.45 9/24/2007 30.55 711.09 2/23/2009 28.23 713.41 3/29/2010 23.65 717.99 11/1/2011 30.61 711.03 11/16/2012 30.60 711.04 MW-713 68 58-68 682.16-672.16 738.50 740.16 11/14/2000 33.90 706.26 9/4/2001 33.15 707.01 9/17/2002 38.12 702.04 9/11/2003 24.53 715.63 8/16/2004 31.80 708.36 12/19/2005 33.74 706.42 8/21 /2006 33.36 706.80 9/24/2007 33.31 706.85 2/23/2009 30.18 709.98 3/29/2010 25.67 714.49 11/1/2011 27.93 712.23 11/16/2012 30.00 710.16 MW-8 33 13-33 721.16-701.16 731.80 734.16 11/14/2000 >30.70 - 9/4/2001 >30.70 9/17/2002 >30.70 - 9/11/2003 20.49 719.67 8/16/2004 28.35 711.81 12/19/2005 20.22 719.94 8/21 /2006 30.81 709.35 9/24/2007 32.89 701.27 2/23/2009 26.39 713.77 3/29/2010 20.51 719.65 11/1/2011 28.85 705.31 11/16/2012 30.96 703.20 MW-9 32 12-32 676.95-656.95 685.95 688.95 11/14/2000 12.36 9/4/2001 13.53 675.42 9/16/2002 13.48 675.47 9/11/2003 8.15 680.80 8/16/2004 10.78 678.17 12/19/2005 11.43 677.52 8/21 /2006 21.35 667.60 9/24/2007 NM NM 2/23/2009 5.37 683.58 3/29/2010 4.22 684.73 11/1/2011 5.97 682.98 11/16/2012 6.26 682.69 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 5 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-10 28 8-28 687.62-667.62 693.60 695.62 11/14/2000 16.91 678.71 9/4/2001 18.61 677.01 9/16/2002 17.64 677.98 9/11/2003 13.78 681.84 8/16/2004 15.06 680.56 12/19/2005 14.47 681.15 8/21 /2006 16.80 678.82 9/24/2007 17.29 678.33 2/23/2009 11.92 683.70 3/29/2010 10.57 685.05 11 /1 /2011 12.96 682.66 11/16/2012 13.18 682.44 12/10/2013 12.97 682.65 12/10/2014 13.97 681.65 New Survey 693.24 695.01 10/26/2015 12.59 682.42 11/14/2016 12.86 682.15 10/9/2017 12.95 682.06 10/31 /2018 11.53 683.48 9/10/2019 13.40 681.61 10/12/2020 14.96 678.28 10/26/2021 19.50 675.51 10/14/2022 15.47 679.54 MW-11 68 53-68 695.42-680.42 746.26 748.42 11/14/2000 38.24 710.18 9/4/2001 38.50 709.92 8/19/2002 41.06 707.36 9/16/2002 40.65 707.77 9/11/2003 28.97 719.45 8/16/2004 36.81 711.61 12/19/2005 38.51 709.91 8/21 /2006 32.91 715.51 9/24/2007 37.29 711.13 2/23/2009 28.91 719.51 3/29/2010 26.02 722.40 11/1/2011 31.13 717.29 11/16/2012 34.87 713.55 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 6 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-12A 20 5-20 688.96-673.96 691.12 693.96 11/14/2000 15.66 678.30 9/4/2001 15.87 678.09 9/16/2002 15.62 678.34 9/11/2003 11.08 682.88 8/16/2004 14.15 679.81 12/ 19/2005 11.31 682.65 8/21 /2006 14.67 679.29 9/24/2007 13.92 680.04 2/23/2009 11.11 682.85 3/29/2010 9.99 683.97 11 /1 /2011 9.26 684.70 11/16/2012 11.13 682.83 12/10/2013 9.07 684.89 12/11/2014 11.58 682.38 New Survey 690.21 693.07 10/27/2015 11.15 681.92 11 /14/2016 11.01 682.06 10/9/2017 10.98 682.09 11/1/2018 10.19 682.88 9/ 10/2019 10.41 682.66 10/13/2020 10.34 679.87 10/26/2021 11.20 681.87 10/17/2022 10.50 682.57 MW-12B 58 48-58 647-637 691.70 695.00 11/14/2000 16.49 678.51 9/4/2001 16.92 678.08 9/16/2002 16.65 678.35 9/11/2003 12.72 682.28 8/16/2004 15.03 679.97 12/19/2005 14.12 680.88 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 10.95 684.05 3/29/2010 NM NM 11 /1 /2011 10.25 684.75 11 /16/2012 10.81 684.19 12/10/2013 11.55 683.45 12/11/2014 11.65 683.35 New Survey 690.75 693.86 10/27/2015 10.67 683.19 11/14/2016 10.23 683.63 10/ 10/2017 11.21 682.65 11 /1 /2018 10.22 683.64 9/11/2019 10.76 683.10 10/13/2020 10.35 680.40 10/26/2021 11.51 682.35 10/17/2022 11.17 682.69 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 7 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-12D 202 187-202 507.93-492.93 691.81 694.93 11/14/2000 >101.50 <593 9/4/2001 48.12 646.81 9/16/2002 47.59 647.34 9/11/2003 46.06 648.87 8/16/2004 NM NM 12/19/2005 20.80 674.13 8/21/2006 NM NM 9/24/2007 14.24 680.69 2/23/2009 9.43 685.50 3/29/2010 12.62 682.31 11/1/2011 13.88 681.05 11/16/2012 43.06 651.87 12/10/2013 25.34 669.59 12/11/2014 43.02 651.91 New Survey 691.19 694.21 10/29/2015 21.96 672.25 11/18/2016 24.12 670.09 10/11/2017 53.41 640.80 11 /1 /2018 26.84 667.37 9/12/2019 3.25 690.96 10/13/2020 2.97 688.22 10/26/2021 3.90 690.31 10/17/2022 3.47 690.74 MW-14 35 20-35 746.22-731.22 763.80 766.22 11/14/2000 28.42 737.80 9/4/2001 29.33 736.89 9/17/2002 NM NM 9/11/2003 25.38 740.84 8/16/2004 26.16 740.06 8/21/2006 27.98 738.24 2/23/2009 27.27 738.95 3/29/2010 25.71 740.51 11/1/2011 27.86 738.36 11/16/2012 27.61 738.61 MW-15A 34 19-34 731.34-746.34 762.5 765.34 9/4/2001 26.70 738.64 9/17/2002 21.40 743.94 9/11/2003 NM NM 8/16/2004 22.72 742.62 12/19/2005 24.31 741.03 8/21/2006 NM NM 2/23/2009 15.21 750.13 3/29/2010 22.06 743.28 11/1/2011 25.19 740.15 11/16/2012 24.75 740.59 12/10/2013 24.69 740.65 12/8/2014 25.64 739.70 New Survey 762.57 764.33 10/27/2015 24.46 739.87 11/14/2016 27.01 737.32 10/11/2017 27.90 736.43 10/31/2018 22.72 741.61 9/10/2019 22.58 741.75 10/9/2020 22.43 740.14 10/28/2021 25.55 738.78 10/18/2022 25.21 739.12 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 8 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-16 45 30-45 749.13-734.13 779.00 779.13 11/14/2000 34.18 744.95 9/4/2001 NM NM 9/17/2002 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 11/16/2012 NM NM MW-17 (WSW-1) 250 230-250 12/19/2005 68.09 8/21/2006 NM NM 2/23/2009 66.04 3/29/2010 64.30 11 /1 /2011 66.88 11/16/2012 67.34 NM MRF-1 43.5 28.5-43.5 723.31-708.31 752.10 751.81 11/14/2000 8.45 743.36 9/4/2001 8.48 743.33 9/17/2002 8.56 743.25 9/11/2003 7.40 744.41 8/16/2004 7.59 744.22 12/19/2005 7.63 744.18 8/21/2006 8.25 743.56 9/24/2007 8.87 742.94 2/23/2009 7.56 744.25 3/29/2010 7.55 744.26 11 /1 /2011 8.01 743.80 11/16/2012 7.98 743.83 MRF-2 41.5 26.5-41.5 724.23-709.23 751.00 750.73 11/14/2000 26.06 724.67 9/4/2001 26.18 724.55 9/17/2002 26.10 724.63 9/11/2003 24.28 726.45 8/16/2004 24.10 726.63 12/19/2005 24.35 726.38 8/21/2006 25.69 725.04 9/24/2007 25.69 725.04 2/23/2009 25.22 725.51 3/29/2010 24.73 726.00 11/1/2011 25.18 725.55 11/16/2012 25.30 725.43 OW-DR1 165 49-165 648.95-532.95 695.39 697.95 11/14/2000 23.21 674.74 9/4/2001 24.72 673.23 9/16/2002 23.80 674.15 9/11/2003 20.21 677.74 8/16/2004 22.23 675.72 12/19/2005 22.91 675.04 8/21/2006 24.40 673.55 9/24/2007 20.16 677.79 2/23/2009 13.77 684.18 3/29/2010 11.42 686.53 11 /1 /2011 13.95 684.00 11/16/2012 14.64 683.31 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 9 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-DR2 186 176-186 518.4-508.4 692.61 694.40 11/14/2000 19.72 674.68 9/4/2001 21.33 673.07 8/19/2002 20.75 673.65 9/16/2002 20.25 674.15 9/11/2003 16.60 677.80 8/16/2004 18.62 675.78 12/19/2005 19.34 675.06 8/21/2006 20.79 673.61 9/24/2007 16.52 677.88 2/23/2009 10.13 684.27 3/29/2010 7.97 686.43 11/1/2011 10.32 684.08 11/16/2012 10.90 683.50 12/10/2013 10.55 683.85 12/12/2014 27.31 667.09 New Survey 692.22 695.87 10/30/2015 13.53 682.34 11/18/2016 14.28 681.59 10/ 10/2017 16.31 679.56 11 /2/2018 19.59 676.28 9/11/2019 20.24 675.63 10/13/2020 19.76 672.46 10/28/2021 17.06 678.81 10/18/2022 17.00 678.87 OW-DR3 160 77-160 626.52-543.52 703.52 704.75 8/19/2002 30.79 663.61 9/16/2002 30.40 664.00 9/11/2003 27.80 666.60 8/16/2004 29.02 665.38 12/19/2005 30.29 664.11 8/21 /2006 31.17 663.23 9/24/2007 26.32 678.43 2/23/2009 20.17 684.58 3/29/2010 18.61 686.14 11/1/2011 20.45 684.30 11/16/2012 20.75 684.00 12/10/2013 20.99 683.76 OW-DR4 165 45 - 165 667.70-547.70 712.70 713.85 8/19/2002 40.15 673.70 9/16/2002 39.72 674.13 9/11/2003 36.25 677.60 8/16/2004 38.23 675.62 12/19/2005 38.91 674.94 8/21 /2006 40.34 673.51 9/24/2007 35.99 677.86 2/23/2009 29.64 684.21 3/29/2010 22.30 691.55 11/1/2011 29.83 684.02 11/16/2012 30.30 683.55 OW-DR5 40 20-40 12/19/2005 10.50 -- 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM OW-NIS1 40 25-40 12/19/2005 10.91 2/23/2009 8.40 3/29/2010 7.59 11/1/2011 6.40 11/16/2012 7.54 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 10 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-SIS1 39 20-39 12/19/2005 24.05 8/21 /2006 24.08 9/24/2007 23.89 2/23/2009 20.89 3/29/2010 17.69 11/1/2011 22.98 11/16/2012 22.99 OW-SIS2 40 20-40 12/19/2005 5.32 2/23/2009 4.32 3/29/2010 3.29 11/1/2011 3.74 11/16/2012 7.63 OW-SIS3 45 15-45 12/19/2005 5.80 2/23/2009 5.67 3/29/2010 3.61 11/1/2011 5.22 -- 11/16/2012 7.00 OW-SF1 120 95-120 638.15-613.15 731.06 731.06 12/19/2005 26.15 704.91 8/21 /2006 26.00 705.06 9/24/2007 25.84 705.22 2/23/2009 23.03 708.03 3/29/2010 18.64 712.42 11/1/2011 25.39 705.67 11/16/2012 25.22 705.84 OW-SF2 120 80-120 651.05-611.05 728.87 731.05 8/21/2006 NM NM 9/24/2007 20.44 710.61 2/23/2009 18.47 -- 3/29/2010 14.27 716.78 11/1/2011 20.46 710.59 11/16/2012 20.68 710.37 OW-LFS1 50 30-50 698.74 12/19/2005 17.15 681.59 2/23/2009 14.45 684.29 3/29/2010 13.28 685.46 11/1/2011 14.90 683.84 11/16/2012 15.88 682.86 OW-LFS2 50 30-50 700.08 12/19/2005 21.97 678.11 2/23/2009 15.81 684.27 3/29/2010 14.66 685.42 11/1/2011 16.34 683.74 11/16/2012 16.61 683.47 12/11/2013 16.82 683.26 12/12/2014 17.44 682.64 New Survey 696.69 699.45 10/26/2015 16.48 682.97 11/14/2016 20.12 679.33 10/9/2017 25.57 673.88 10/31/2018 38.96 660.49 9/12/2019 17.20 682.25 10/12/2020 32.22 664.47 10/28/2021 16.05 683.40 10/17/2022 39.45 660.00 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 11 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-DR1 185 38-185 657.21-510.21 693.62 695.21 11/14/2000 20.51 674.70 9/4/2001 21.90 673.31 8/19/2002 21.48 673.73 9/16/2002 21.02 674.19 9/11 /2003 17.51 677.70 8/16/2004 19.55 675.66 12/19/2005 NM -- 8/21/2006 NM 9/24/2007 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM -- 11/16/2012 NM PW-SF1 120 95-120 638.15-613.15 732.14 733.15 8/21/2006 25.98 707.17 9/24/2007 25.60 707.55 2/23/2009 22.96 710.19 3/29/2010 18.62 714.53 11 /1 /2011 25.31 707.84 11/16/2012 25.50 707.64 12/9/2013 21.00 712.15 12/8/2014 26.65 706.50 New Survey 731.13 732.19 10/27/2015 26.78 705.41 11/17/2016 24.45 707.74 10/11/2017 28.21 703.98 10/31 /2018 22.17 710.02 9/10/2019 20.50 711.69 10/9/2020 21.66 709.47 10/27/2021 23.76 708.43 10/18/2022 51.36 680.83 PW-SIS1 39 19-39 695.21 8/16/2004 NM -- 12/19/2005 12.20 683.01 8/21/2006 13.95 681.26 9/24/2007 15.43 679.78 2/23/2009 12.73 682.48 3/29/2010 11.31 683.90 11 /1 /2011 13.01 682.20 11/16/2012 13.63 681.58 PW-1D 81.5 66.5-81.5 717.18-702.18 781.90 783.68 11/14/2000 54.92 728.76 9/4/2001 54.60 729.08 9/17/2002 54.65 729.03 9/11/2003 47.49 736.19 8/16/2004 NM -- 12/19/2005 51.82 731.86 8/21/2006 NM -- 2/23/2009 49.60 734.08 3/29/2010 47.86 735.82 11 /1 /2011 50.18 733.50 11/16/2012 50.30 733.38 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 12 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-21D 101 80-100 700.55-680.55 778.80 780.55 11/14/2000 45.43 735.12 9/4/2001 45.16 735.39 9/17/2002 NM -- 9/11/2003 NM -- 8/16/2004 43.45 737.10 12/19/2005 43.94 736.61 8/21 /2006 42.75 737.80 9/24/2007 44.20 736.35 2/23/2009 41.43 739.12 3/29/2010 39.30 741.25 11 /1 /2011 42.62 737.93 11/16/2012 42.20 738.35 PW-3D 209.5 179.5-209.5 578.84-548.84 756.60 758.34 11/14/2000 56.60 701.74 9/4/2001 NM -- 9/16/2002 58.62 699.72 9/11/2003 NM -- 8/16/2004 55.55 702.79 12/19/2005 NM -- 8/21/2006 56.75 701.59 2/23/2009 50.02 708.32 3/29/2010 48.12 710.22 11 /1 /2011 50.52 707.82 11/16/2012 47.90 710.44 12/17/2013 48.81 709.53 12/11/2014 49.51 708.83 New Survey 737.63 738.60 10/29/2015 48.91 689.69 11/16/2016 52.42 686.18 10/11/2017 43.99 694.61 11 /2/2018 50.71 687.89 9/11/2019 52.02 686.58 10/14/2020 51.76 685.87 10/27/2021 51.39 687.21 10/12/2022 52.45 686.15 PW-41 122 112-122 625.67-615.67 735.17 737.67 11/14/2000 43.39 694.28 9/4/2001 44.73 692.94 9/17/2002 45.94 691.73 9/11/2003 36.04 701.63 8/16/2004 42.31 695.36 12/19/2005 43.27 694.40 8/21 /2006 43.11 712.03 2/23/2009 39.35 698.32 3/29/2010 35.56 719.58 11 /1 /2011 41.23 696.44 11/16/2012 41.49 696.18 12/17/2013 42.03 695.64 12/8/2014 42.62 695.05 New Survey 732.04 737.59 10/29/2015 42.10 695.49 Corrected elevation after well repair. Removed 2.59' of casing. 735.00 11/17/2016 40.78 694.22 10/11/2017 43.80 691.20 11 /2/2018 34.04 700.96 9/11/2019 35.52 699.48 10/14/2020 36.42 695.62 10/27/2021 38.12 696.88 10/18/2022 42.60 692.40 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 13 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-5D 306.5 272-282 425.87-415.87 695.07 697.87 11/14/2000 23.52 674.35 9/4/2001 24.04 673.83 8/19/2002 24.54 673.33 9/16/2002 23.86 674.01 9/11/2003 20.37 677.50 8/16/2004 22.45 675.42 12/19/2005 23.21 674.66 8/21 /2006 24.68 673.19 9/24/2007 20.31 677.56 2/23/2009 13.85 684.02 3/29/2010 10.85 687.02 11 /1 /2011 13.98 683.89 11/16/2012 12.92 684.95 12/16/2013 10.54 687.33 12/11/2014 21.86 676.01 New Survey 693.96 696.27 10/30/2015 13.80 682.47 11/18/2016 13.73 682.54 10/ 10/2017 17.41 678.86 11 /2/2018 17.31 678.96 9/11/2019 17.42 678.85 10/13/2020 17.72 678.55 10/28/2021 16.37 679.90 10/18/2022 16.33 679.94 PW-61 76 65-76 619.19-608.19 682.27 684.19 11/14/2000 11.80 672.39 9/4/2001 13.98 670.21 8/ 19/2002 12.81 671.38 9/16/2002 12.35 671.84 9/11/2003 11.20 672.99 8/16/2004 12.00 672.19 12/19/2005 16.14 668.05 8/21/2006 NM -- 9/24/007 NM -- New TOC elevation 693.57 696.15 2/23/2009 14.75 681.40 3/29/2010 11.76 684.39 11/1/2011 13.98 682.17 11/16/2012 14.26 669.93 12/16/2013 14.29 681.86 New well 12/10/2014 17.43 679.98 New Survey 100 90-100 695.12 697.41 10/27/2015 16.15 681.26 11/17/2016 16.54 680.87 10/10/2017 17.38 680.03 11/1/2018 15.47 681.94 9/12/2019 16.00 681.41 10/13/2020 15.27 679.85 10/28/2021 16.05 681.36 10/14/2022 16.10 681.31 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 14 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-6D 275 260-275 424.77-409.77 682.22 684.77 11/14/2000 11.01 673.76 9/4/2001 12.58 672.19 8/19/2002 12.07 672.70 9/16/2002 11.57 673.20 9/11/2003 7.87 676.90 8/16/2004 9.95 674.82 12/19/2005 13.24 671.53 8/21/2006 NM -- 9/24/2007 NM -- New TOC elevation 691.53 696.33 3/12/2009 13.05 683.28 3/29/2010 11.84 684.49 11 /1 /2011 13.34 682.99 11/16/2012 14.03 682.30 12/16/2013 NA NA New well 12/10/2014 23.56 673.23 New Survey 300 270-300 695.02 696.79 10/30/2015 14.53 682.26 11/17/2016 15.02 681.77 10/10/2017 21.65 675.14 11 /1 /2018 17.33 679.46 9/12/2019 18.44 678.35 10/12/2020 16.75 678.27 10/28/2021 16.68 680.11 10/14/2022 15.92 680.87 PW-71 101 90-100 594.92-584.92 683.42 684.92 11/14/2000 12.90 672.02 9/4/2001 14.58 670.34 6/ 16/2002 12.81 672.11 8/19/2002 13.28 671.64 9/ 16/2002 12.81 672.11 9/11/2003 11.69 673.23 8/16/2004 12.92 672.00 12/19/2005 11.41 673.51 8/21 /2006 14.38 670.54 9/24/2007 9.11 675.81 New TOC elevation; survey data pending 2/23/2009 2.34 NA 3/29/2010 1.89 NA 11/1/2011 1.85 NA 11/16/2012 2.99 NA PW-8S 48 35-45 728.13-718.13 761.23 763.13 11/14/2000 42.30 720.83 9/4/2001 45.10 718.03 9/17/2002 47.33 715.80 9/11/2003 38.95 724.18 8/16/2004 40.70 722.43 12/19/2005 42.80 720.33 8/21 /2006 43.39 719.74 9/24/2007 44.57 718.56 2/23/2009 41.66 721.47 3/29/2010 27.22 735.91 11 /1 /2011 40.58 722.55 11/16/2012 40.96 722.17 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 15 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-91 100 80-100 619.07-599.07 698.07 699.07 11/14/2000 21.80 677.27 9/4/2001 22.95 676.12 9/16/2002 22.74 676.33 9/11/2003 18.04 681.03 8/16/2004 20.50 678.57 12/19/2005 20.79 678.28 8/21 /2006 11.75 687.32 9/24/2007 21.14 677.93 2/23/2009 14.18 684.89 3/29/2010 13.50 685.57 11 /1 /2011 14.61 684.46 11/16/2012 15.18 683.89 PW-101 100 80-100 616.44-596.44 695.34 696.44 11/14/2000 17.24 679.20 9/4/2001 19.08 677.36 9/16/2002 18.30 678.14 9/11/2003 14.57 681.87 8/16/2004 16.05 680.39 12/19/2005 15.53 680.91 8/21 /2006 17.68 678.76 9/24/2007 17.44 679.00 2/23/2009 12.06 684.38 3/29/2010 10.62 685.82 11/1/2011 12.32 684.12 11/16/2012 13.37 683.07 12/11/2013 13.10 683.34 12/ 10/2014 14.21 682.23 New Survey 694.63 695.97 10/29/2015 12.43 683.54 11/17/2016 13.46 682.51 10/9/2017 14.19 681.78 11 /1 /2018 11.68 684.29 9/12/2019 13.20 682.77 10/12/2020 16.82 677.81 10/26/2021 19.63 676.34 10/ 13/2022 17.51 678.46 PW-1OD 200 185-200 512.75-497.75 695.48 697.96 11/14/2000 >101.50 - 9/4/2001 39.20 658.76 9/16/2002 46.45 651.51 9/11/2003 NM NM 8/16/2004 48.04 649.92 12/19/2005 29.01 668.95 8/21 /2006 32.60 665.36 9/24/2007 18.42 679.54 2/23/2009 14.51 683.45 3/29/2010 26.38 671.58 11 /1 /2011 17.01 680.95 11/16/2012 43.21 654.75 12/11/2013 42.25 655.71 12/10/2014 34.50 663.46 New Survey 695.13 697.26 11/3/2015 35.32 661.94 11/17/2016 25.33 671.93 10/10/2017 49.55 647.71 10/31 /2018 26.28 670.98 9/12/2019 45.70 651.56 10/12/2020 22.75 672.38 10/26/2021 16.41 680.85 10/13/2022 16.00 681.26 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 16 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-111 90 75-90 710.45-695.45 784.38 785.45 11/14/2000 57.55 727.90 9/4/2001 58.00 727.45 9/17/2002 58.77 726.68 9/11/2003 53.81 731.64 8/16/2004 56.23 729.22 12/19/2005 56.65 728.80 8/21 /2006 56.73 728.72 9/24/2007 57.25 728.20 2/23/2009 55.90 729.55 3/29/2010 52.60 732.85 11 /1 /2011 55.01 730.44 11/16/2012 54.90 730.55 PW-121 105 90-105 660.54-645.54 748.07 750.54 11/14/2000 29.09 721.45 9/4/2001 32.36 718.18 2/16/2002 36.25 714.29 9/16/2002 36.25 714.29 9/11/2003 26.18 724.36 8/16/2004 27.41 723.13 12/19/2005 29.55 720.99 8/23/2006 30.15 720.39 9/24/2007 28.55 721.99 2/23/2009 28.93 721.61 3/29/2010 24.62 725.92 11/1/2011 28.18 722.36 11/16/2012 27.73 722.81 12/16/2013 28.17 722.37 12/12/2014 28.70 721.84 New Survey 746.99 749.48 10/30/2015 28.82 720.66 11/21/2016 35.73 713.75 10/11/2017 28.55 720.93 11/6/2018 29.51 719.97 9/11/2019 21.83 727.65 10/14/2020 22.94 724.05 10/28/2021 23.95 725.53 10/19/2022 27.40 722.08 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 17 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-131 250 235-250 504.9-489.9 736.58 739.90 11/14/2000 67.65 672.25 9/4/2001 69.68 670.22 8/19/2002 68.50 671.40 9/17/2002 68.12 671.78 9/11/2003 66.59 673.31 8/16/2004 67.52 672.38 12/19/2005 68.51 671.39 8/21/2006 69.64 670.26 9/24/2007 64.70 675.20 2/23/2009 57.31 682.59 3/29/2010 54.65 685.25 11 /1 /2011 57.33 682.57 11/16/2012 58.05 681.85 12/16/2013 57.20 682.70 12/12/2014 59.52 680.38 New Survey 736.23 739.01 10/26/2015 37.69 701.32 11/18/2016 58.24 680.77 10/11/2017 58.97 680.04 10/31/2018 57.15 681.86 9/11/2019 51.68 687.33 10/13/2020 56.93 679.30 10/28/2021 57.69 681.32 10/12/2022 57.62 681.39 PW-14D 198.8 183.8-198.8 505.33-490.33 686.38 689.13 10/31/2000 16.24 672.89 12/20/2000 > 150 - 9/5/2001 76.98 612.15 9/17/2002 64.16 624.97 9/11/2003 6.51 682.62 8/16/2004 56.01 633.12 12/19/2005 67.27 621.86 8/21/2006 37.29 651.84 9/24/2007 62.45 626.68 3/11/2009 37.90 651.23 3/29/2010 29.41 659.72 11/1/2011 17.63 671.50 11/16/2012 32.37 656.76 12/12/2013 56.60 632.53 12/9/2014 63.29 625.84 New Survey 685.27 686.50 11/3/2015 72.59 613.91 11/16/2016 46.02 640.48 10/12/2017 9.42 677.08 11 /5/2018 39.62 646.88 9/17/2019 87.88 598.62 10/14/2020 62.08 623.19 10/27/2021 37.36 649.14 10/13/20232 27.30 659.20 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 18 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-14S 21.5 11.5-21.5 677.09-667.09 685.96 688.59 10/30/2000 13.19 675.40 12/20/2000 13.47 675.12 9/5/2001 14.28 674.31 9/17/2002 14.55 674.04 9/11/2003 14.92 673.67 8/16/2004 10.26 678.33 12/19/2005 11.54 677.05 8/21 /2006 13.45 675.14 3/11/2009 4.34 684.25 3/29/2010 2.13 686.46 11/1/2011 4.27 684.32 11/16/2012 5.30 683.29 PW-15D 163.5 153.5-163.5 533.93-523.93 684.85 687.43 10/31/2000 13.25 674.18 12/20/2000 13.32 674.11 9/5/2001 14.79 672.64 9/17/2002 13.81 673.62 9/11/2003 10.13 677.30 8/16/2004 12.24 675.19 12/19/2005 13.03 674.40 8/21 /2006 15.80 671.63 9/24/2007 9.93 677.50 3/11/2009 3.20 684.23 3/29/2010 2.02 685.41 11/1/2011 3.25 684.18 11/16/2012 4.39 683.04 12/12/2013 4.50 682.93 12/9/2014 8.14 679.29 New Survey 684.05 685.80 10/28/2015 4.11 681.69 11/15/2016 4.54 681.26 10/12/2017 10.15 675.65 11 /5/2018 4.95 680.85 9/17/2019 6.60 679.20 10/14/2020 5.95 678.10 10/27/2021 5.38 680.42 10/13/2022 5.21 680.59 PW-15S 21.5 11.5-21.5 676.71-666.71 685.88 688.21 10/30/2000 14.87 673.34 12/20/2000 14.91 673.30 9/5/2001 16.26 671.95 9/17/2002 15.42 672.79 9/11/2003 11.61 676.60 8/16/2004 13.89 674.32 12/19/2005 14.14 674.07 8/21 /2006 14.32 673.89 9/24/2007 9.75 678.46 3/11/2009 4.65 683.56 3/29/2010 3.09 685.12 11/1/2011 4.58 683.63 11/16/2012 5.89 682.32 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 19 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-16D 179 169-179 515.98-505.98 681.46 684.98 10/31/2000 10.94 674.04 12/20/2000 10.95 674.03 9/5/2001 12.43 672.55 9/ 17/2002 11.51 673.47 9/11/2003 7.88 677.10 8/16/2004 9.91 675.07 12/19/2005 10.80 674.18 8/21 /2006 12.09 672.89 9/24/2007 11.21 673.77 New TOC elevation; survey data pending 3/11/2009 4.38 NA 3/29/2010 3.23 NA 11/1/2011 4.45 NA 11/16/2012 5.65 NA 12/12/2013 5.22 NA 12/9/2014 7.10 NA New Survey 684.07 686.68 10/28/2015 4.84 681.84 11/15/2016 5.31 681.37 10/12/2017 8.89 677.79 11 /5/2018 4.70 681.98 9/17/2019 6.77 679.91 10/14/2020 6.31 677.76 10/27/2021 6.09 680.59 10/13/2022 5.86 680.82 PW-16S 12.5 5.5-12.5 677.67-670.67 680.97 683.17 10/30/2000 8.00 675.17 12/20/2000 7.39 675.78 9/5/2001 9.82 673.35 9/17/2002 9.65 673.52 9/11/2003 6.56 676.61 8/16/2004 6.79 676.38 12/19/2005 6.21 676.96 8/21 /2006 8.44 674.73 9/24/2007 11.83 671.34 New TOC elevation; survey data pending 3/11/2009 4.93 NA 3/29/2010 4.10 NA 11/1/2011 4.64 NA 11/16/2012 5.96 NA PW-17 100 85 - 100 686.0 - 671.0 771.0 774.7 11/14/2000 43.25 731.45 12/20/2000 43.96 730.74 9/5/2001 45.55 729.15 9/16/2002 49.34 725.36 9/11/2003 37.64 737.06 8/16/2004 39.42 735.28 12/19/2005 21.09 753.61 8/21 /2006 43.19 731.51 9/24/2007 42.02 732.68 2/23/2009 42.50 732.20 3/29/2010 38.20 736.50 11/1/2011 43.50 731.20 11/16/2012 42.40 732.30 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 20 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-18 225 210 - 225 525.4 - 510.4 735.4 737.8 11/9/2000 110.06 627.74 12/7/2000 57.23 680.57 12/14/2000 57.28 680.52 12/20/2000 57.27 680.53 9/5/2001 58.50 679.30 9/17/2002 NM NM 9/11/2003 86.31? Suspect data 8/16/2004 53.18 684.62 12/19/2005 NM NM 8/21 /2006 39.32 698.48 9/24/2007 34.56 703.24 3/11/2009 37.43 700.37 3/29/2010 30.22 707.58 11/1/2011 36.15 701.65 11/16/2012 35.04 702.76 12/12/2013 34.75 703.05 12/9/2014 33.80 704.00 New Survey 734.02 736.44 10/26/2015 36.68 699.76 11/15/2016 30.73 705.71 10/16/2017 33.24 703.20 11 /7/2018 32.70 703.74 NM NM NM PW-19 260 235-250 516.6 - 501.6 751.6 754.1 11/5/2001 75.70 678.40 9/17/2002 60.16 693.94 9/11/2003 94.56? Suspect data 9/11/2003 52.75 701.35 8/16/2004 53.18 700.92 12/19/2005 54.11 699.99 8/21 /2006 54.50 699.60 9/24/007 54.15 699.95 2/25/2009 52.18 701.92 3/29/2010 50.65 703.45 11/1/2011 NM 11/16/2012 NM W-1 64.7 53.7-64.7 719.05-708.05 772.20 772.75 11/14/2000 42.08 730.67 9/4/2001 24.12 748.63 9/17/2002 48.07 724.68 9/11/2003 36.39 736.36 8/16/2004 38.00 734.75 12/19/2005 40.78 731.97 8/21 /2006 41.87 730.88 2/23/2009 41.63 731.12 3/29/2010 37.13 735.62 11/1/2011 41.53 731.22 11/16/2012 41.00 731.75 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 21 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-2 35 23-35 703-691 723.30 726.00 11/14/2000 16.51 709.49 9/4/2001 17.33 708.67 9/17/2002 18.35 707.65 9/11/2003 12.62 713.38 8/16/2004 14.05 711.95 8/21 /2006 18.56 707.44 9/224/07 16.30 709.70 2/23/2009 15.54 710.46 3/29/2010 14.75 711.25 11 /1 /2011 16.43 709.57 11/16/2012 18.10 707.90 W-4 19 9-19 703.64-693.64 710.30 712.64 11/14/2000 9.49 703.15 9/4/2001 9.84 702.80 9/17/2002 8.57 704.07 9/11/2003 6.71 705.93 8/16/2004 6.28 706.36 12/19/2005 7.74 704.90 8/21 /2006 9.09 703.55 9/24/2007 9.94 702.70 2/23/2009 6.22 706.42 3/29/2010 5.80 706.84 11 /1 /2011 6.69 705.95 11/16/2012 9.35 703.29 W-4A 38.5 28.5-38.5 684.75-674.75 712.00 713.25 11/14/2000 9.77 703.48 9/4/2001 10.12 703.13 9/17/2002 9.00 704.25 9/11/2003 7.58 705.67 8/16/2004 6.87 706.38 12/19/2005 6.91 706.34 8/21 /2006 9.49 703.76 9/24/2007 10.08 703.17 2/23/2009 6.92 706.33 3/29/2010 5.83 707.42 11 /1 /2011 6.82 706.43 11/16/2012 9.57 703.68 12/17/2013 7.39 705.86 12./8/2014 14.76 698.49 New Survey 709.86 712.64 10/27/2015 9.93 702.71 11/16/2016 11.07 701.57 10/11/2017 12.93 699.71 10/31 /2018 6.72 705.92 9/11/2019 17.60 695.04 10/9/2020 15.57 694.29 10/27/2021 15.62 697.02 10/18/2022 14.87 697.77 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 22 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-413 50 52.7 711.70 713.93 11/14/2000 10.71 703.22 9/4/2001 11.11 702.82 9/17/2002 10.27 703.66 9/11/2003 NM NM 8/16/2004 7.90 706.03 12/19/2005 7.79 706.14 8/21 /2006 10.59 703.34 9/24/2007 11.00 702.93 2/23/2009 6.50 707.43 3/29/2010 5.78 708.15 11/1/2011 7.58 706.35 11/16/2012 10.50 703.43 W-5 60 50-60 702.06-692.06 750.86 752.06 11/14/2000 32.28 719.78 9/4/2001 33.84 718.22 9/17/2002 38.61 713.45 9/11/2003 26.85 725.21 8/16/2004 29.64 722.42 12/19/2005 32.30 719.76 8/21 /2006 33.11 718.95 9/24/2007 32.50 719.56 2/23/2009 31.97 720.09 3/29/2010 27.64 724.42 11/1/2011 32.63 719.43 11/16/2012 32.35 719.71 W-6 57 42-57 701.8-686.8 742.17 743.80 11/14/2000 30.43 713.37 9/4/2001 31.59 712.21 9/17/2002 35.47 708.33 9/11/2003 22.78 721.02 8/16/2004 27.95 715.85 12/19/2005 30.36 713.44 8/21 /2006 30.81 712.99 9/24/2007 29.86 713.94 2/23/2009 28.53 715.27 3/29/2010 24.32 719.48 11/1/2011 30.13 713.67 11/16/2012 30.15 713.65 W-6A 90 80-90 664.9-654.9 742.91 744.90 11/14/2000 32.45 712.45 9/4/2001 33.70 711.20 9/17/2002 36.67 708.23 9/11/2003 24.62 720.28 8/16/2004 30.20 714.70 12/19/2005 32.51 712.39 8/21 /2006 32.85 712.05 9/24/2007 32.15 712.75 2/23/2009 30.39 714.51 3/29/2010 26.17 718.73 11/1/2011 32.99 711.91 11/16/2012 33.17 711.73 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 23 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-613 35 20-35 724.39-709.39 743.13 744.39 11/14/2000 29.75 714.64 9/4/2001 30.98 713.41 9/17/2002 33.71 710.68 9/11/2003 22.34 722.05 8/16/2004 27.00 717.39 12/19/2005 29.44 714.95 8/21/2006 29.97 714.42 9/24/2007 28.86 715.53 2/23/2009 27.99 716.40 3/29/2010 23.70 720.69 11/1/2011 28.03 716.36 11/16/2012 27.33 717.06 W-12 60 50-60 685.84-675.84 734.14 735.84 12/19/2005 21.65 714.19 8/21/2006 NM NM 9/24/2007 20.96 714.88 2/23/2009 19.83 716.01 3/29/2010 15.45 720.39 11/1/2011 21.26 714.58 11/16/2012 21.30 714.54 W-12A 25 10-25 725.74-710.74 733.62 735.74 12/19/2005 21.61 714.13 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 20.19 715.55 3/29/2010 15.93 719.81 11/1/2011 21.71 714.03 11/16/2012 21.50 714.24 W-13 20 10-20 744.4-734.7 752.40 754.70 11/14/2000 DRY -- 9/4/2001 DRY 9/17/2002 DRY -- 9/11/2003 24.25 730.45 8/16/2004 14.30 740.40 8/21/2006 DRY -- 2/23/2009 35.97 718.73 3/29/2010 4.30 750.40 11/1/2011 18.61 736.09 11/16/2012 dry W-14 23 8-23 715.9-700.9 721.3 723.90 12/19/2005 16.68 707.22 8/21/2006 NM NM 9/24/2007 13.32 710.58 2/23/2009 3.52 720.38 3/29/2010 2.56 721.34 11/1/2011 11.72 712.18 11/16/2012 12.52 711.38 W-15 55 35-55 727.36-707.36 760.0 762.36 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 40.96 721.40 11/16/2012 40.27 722.09 W-16 38 28-38 714.01-704.01 739.8 742.01 9/17/2002 29.73 712.28 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 22.53 719.48 3/29/2010 18.42 723.59 11/1/2011 23.69 718.32 11/16/2012 23.62 718.39 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 24 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-17 20.5 23 687.44 708.4 710.44 12/19/2005 6.97 703.47 8/21 /2006 9.40 701.04 9/24/2007 11.00 699.44 2/23/2009 7.80 702.64 3/29/2010 4.62 705.82 11/1/2011 9.86 700.58 11/16/2012 10.20 700.24 W-18 41.5 31.5-41.5 722.21-712.21 751.4 753.71 12/19/2005 35.01 718.70 8/21 /2006 36.45 717.26 9/24/2007 37.10 716.61 2/23/2009 36.08 717.63 3/29/2010 33.81 719.90 11/1/2011 36.69 717.02 11/16/2012 37.55 716.16 W-19 40 30-40 717.33-707.33 744.3 747.33 8/21/2006 NM NM 9/24/2007 29.14 718.19 2/23/2009 28.75 718.58 3/29/2010 24.68 722.65 11/1/2011 29.22 718.11 11/16/2012 29.00 718.33 W-20 10 5-10 712.24-707.24 715.14 717.24 12/19/2005 5.14 712.10 8/21 /2006 6.65 710.59 9/24/2007 7.10 710.14 2/23/2009 4.59 712.65 3/29/2010 4.05 713.19 11/1/2011 7.01 710.23 11/16/2012 7.61 709.63 W-21 33.4 33.4 684.78 716.00 718.18 11/14/2000 15.73 702.45 9/4/2001 16.41 701.77 9/17/2002 17.15 701.03 9/11/2003 14.00 704.18 8/16/2004 14.94 703.24 12/19/2005 14.18 704.00 8/21 /2006 15.59 702.59 9/24/2007 15.91 702.27 2/23/2009 14.60 703.58 3/29/2010 9.48 708.70 11/1/2011 15.02 703.16 11/16/2012 15.70 702.48 W-23A 75 65-75 707.66-697.66 770.18 772.66 11/14/2000 41.41 731.25 9/4/2001 42.91 729.75 9/17/2002 45.30 727.36 9/11/2003 31.29 741.37 8/16/2004 38.17 734.49 12/19/2005 42.06 730.60 8/21 /2006 40.94 731.72 9/24/2007 42.30 730.36 2/23/2009 40.10 732.56 3/29/2010 36.44 736.22 11/1/2011 41.74 730.92 11/16/2012 41.65 731.01 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 25 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-23B 55 40-55 731.89-716.89 769.60 771.89 11/14/2000 41.00 730.89 9/4/2001 42.37 729.52 9/17/2002 44.54 727.35 9/11/2003 31.29 740.60 8/16/2004 37.45 734.44 12/19/2005 41.29 730.60 8/21/2006 40.42 731.47 9/24/2007 42.57 729.32 2/23/2009 39.55 732.34 3/29/2010 35.74 736.15 11/1/2011 41.01 730.88 11/16/2012 41.40 730.49 W-24 60 45-60 721.14-706.14 765.80 766.14 11/14/2000 40.45 725.69 9/4/2001 42.61 723.53 9/17/2002 NM -- 9/11/2003 NM 8/16/2004 NM 12/19/2005 NM 8/21/2006 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM W-25 58 43-58 727.27-712.27 770.80 770.27 11/14/2000 40.58 729.69 9/4/2001 42.47 727.80 9/17/2002 46.25 724.02 9/11/2003 35.75 734.52 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-26 53 38-53 721.65-706.65 759.20 759.65 11/14/2000 NM NM 9/4/2001 NM NM 9/17/2002 40.62 719.03 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-27 58.5 43.5-58.5 721.7-706.7 765.50 765.20 11/14/2000 39.86 725.34 9/4/2001 41.37 723.83 9/17/02 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 39.05 726.15 11/16/2012 37.61 727.59 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 26 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-29 49.5 34.5-49.5 715.69-700.69 750.74 750.19 11/14/2000 28.22 721.97 9/4/2001 29.68 720.51 9/17/2002 28.01 722.18 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-30 53 38-53 722.77-707.77 761.00 760.77 11/14/2000 34.47 726.30 9/4/2001 36.59 724.18 9/17/2002 40.16 720.61 9/11/2003 30.37 730.40 8/16/2004 NM NM 12/19/2005 NM NM 8/21 /2006 34.92 725.85 9/24/2007 33.67 727.10 2/23/2009 32.79 727.98 3/29/2010 28.64 732.13 11/1/2011 33.73 727.04 11/16/2012 33.58 727.19 RW-NIS1 40 20-40 12/19/2005 10.51 -- 2/23/2009 9.43 -- 3/29/2010 8.72 -- 11/1/2011 3.79 -- 11/16/2012 5.57 RW-SIS1 50 30-50 12/19/2005 11.59 2/23/2009 NM -- 3/29/2010 NM -- 11/1/2011 NM -- 11/16/2012 NM RW-SIS2 40 20-40 12/19/2005 6.48 2/23/2009 7.47 -- 3/29/2010 6.98 -- 11/1/2011 6.11 -- 11/16/2012 8.84 RW-SIS3 40 20-40 713.60 12/19/2005 6.67 706.93 2/23/2009 5.15 708.45 3/29/2010 4.05 709.55 11/1/2011 4.82 708.78 11/16/2012 5.43 708.17 RW-SIS4 45 1545 713.16 12/19/2005 4.38 708.78 2/23/2009 9.99 703.17 3/29/2010 2.51 710.65 11/1/2011 4.27 708.89 11/16/2012 4.00 709.16 RW-SIS5 12/19/2005 9.22 -- 2/23/2009 9.22 3/29/2010 5.50 11/1/2011 9.56 11/16/2012 8.50 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 27 of 27 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) RW-SIS6 12/19/2005 5.28 2/23/2009 6.15 3/29/2010 4.70 11/1/2011 5.73 -- 11/16/2012 6.70 RW-LFS1 50 30-50 696.44 12/19/2005 14.71 681.73 2/23/2009 12.09 684.35 3/29/2010 10.97 685.47 11 /1 /2011 11.88 684.56 11/16/2012 11.74 684.70 RW-LFS2 50 30-50 697.48 12/19/2005 19.39 678.09 2/23/2009 13.16 684.32 3/29/2010 12.05 685.43 11 /1 /2011 13.49 683.99 11/16/2012 12.96 684.52 NM = Not measured BGL = Below ground level MSL = Mean sea level BTOC = Below top of well casing TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 1 of 15 VOLATILE ORGANIC COMPOUNDS (ug/L) c> °1 n Sam p le n ^' N b o ^' :° ^' Sample I.D. b q b 0 3 n n b ,� Date 0 n 0 0 c, 3 --1 n 3 c, m m n 0 n � .s O O O O O A y p O 3' p O `< fD O O O 3 S A O O O O O D W n a O O O a n O -4 O O n y p N fD fD O 0 _G 0 O 2' O O (D. .O. O 3 fD O_ fD fD S_ O x S 3' S 3' S -a x .+ N O � N =r �+ O S S N O 3' C S 3' O O O C) 3 D) 3 a) 3 O 3 a) 3 0 3 D) 3 O 3 M 3 O. CD 3 O 3 D) 3 N 3 fD 3 � CL M 3 M 3 N 3 lD 3 � O. 2) n M fD N fD N fD fD fD fD fD fD fD fD N fD fD M M N M fD N NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-1 1/28/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/5/2009 17 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 15.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 54 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 54.4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/9/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/8/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/10/2019 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/13/2020 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/12/2022 ND <1 <1 <1 <1 <1 I <1 <2 I <20 <1 <1 I <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 I <0.3 ND MW-2A 1/24/1997 4 4 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-2C 1/24/1997 620 160 ND 260 98.0 30.0 ND ND ND 7 J ND 3 J 10 J ND ND ND ND 6 J ND ND 13.0 31.0 ND 2.0 7/15/1998 600 ND 100 290 D 140 ND ND ND ND 5.0 ND ND ND ND ND ND ND 6.0 ND ND 9.0 50.0 ND ND 2/24/2009 102 <1.0 <1.0 1 41.1 <1.0 2.8 1 <1.0 49 1 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 I <1.0 <1.0 4.9 <2.0 ND MW-3A 8/6/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/29/1997 24 ND ND ND ND ND ND ND ND 3 J ND 15 ND ND ND ND ND ND ND ND ND ND ND 6 MW-3B 7/15/1998 139 ND ND ND ND ND ND 120 J ND 3 J 14 2 J ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 186 <5 <5 <5 <5 <5 <5 160 NA <5 26 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 139 <5 <5 <5 <5 <5 <5 126 <10 <5 12.6 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND MW-3C 8/6/1996 273 11 ND 150 31 5.0 ND ND 6 37 ND ND ND ND 2 J 4J ND ND 14 13 ND ND 1/28/1997 197 6 ND 92 21 3.0 ND ND ND ND 41 14 ND NA ND 1 J ND ND ND 9 10.0 ND ND 9/26/2000 138 <5 <5 41 7.2 <5 <5 <100 NA <5 32 <10 <5 21 <5 <5 <5 37 <5 <5 <10 <10 ND 9/5/2001 178 <5 <5 22.6 <5 <5 <5 117 <10 <5 24.2 <10 <5 14.6 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 152 <5 <5 18.4 <5 <5 <5 94.6 <10 <5 27.3 <10 <5 12 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 103 <5 <5 <5 <5 <5 <5 90 <10 <5 13.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 132 <5 <5 19.4 <5 <5 <5 71 <10 <5 30.0 <10 <5 12.4 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/27/2009 589 <1.0 <1.0 104 20.3 4.4 <1.0 160 <5.0 3.0 <1.0 151 32.7 <1.0 <1.0 70.1 <1.0 <1.0 1.9 <1.0 <1.0 2.5 39.4 <2.0 ND 3/30/2010 863 <1.0 <1.0 161 32.4 6.31 <1.0 186 <5.0 3.92 <1.0 249 45.7 <1.0 <1.0 108 <1.0 4.87 1.71 <1.0 <1.0 2.71 61 ND ND 11/1/2011 1,861 29.1 <0.5 396 144 14 <0.5 80 <0.5 9.94 <0.5 459 192 <0.5 <0.5 364 <0.5 <0.5 3.09 <0.5 1.15 8.74 157 <0.5 3.26 11 /20/2012 1,798 28.5 <0.5 361 106 <0.5 <0.5 268 <0.5 8.73 <0.5 386 150 <0.5 <0.5 314 <0.5 4.30 3.83 1.26 1.40 8.36 146 0.7 10.31 12/11/2013 2,268 18.6 <5 383 107 15 <5 549 <50 9 <5 559 137 <5 <5 318 <5 <5 <5 <5 <5 <5 173 <5 ND 12/11/2014 2,051 100 <1 290 170 <1 <1 311 <5.0 12 17.0 330 60 <1 <1 620 <1 <1 <1 <1 <1 11 130 <3 ND 10/27/2015 1,262 66 <1 210 100 <1 <1 308 >50 10 <1 350 40 <1 <1 410 <1 <1 <1 <1 <1 9.4 J 67 <30 ND 11/14/2016 872 67 <10 94 56 <10 <10 190 <10 5.4 J 12.0 150 <10 <10 <10 270 <10 <10 <10 <10 <10 6.0 27 <30 ND 10/10/2017 402 15 <1 57 22 1.8 <1 120 <20 2.2 <1 49 6.2 J <1 <1 100 <1 <1 0.81 J <1 0.73 J 2.0 31 <3 1.70 11/2/2018 414 6 <1 54 30 1.9 <1 110 <20 3.2 <1 66 6.3 <1 <1 110 <1 <1 0.62 J <1 0.61 J 2.3 22 <3 2.60 9/11/2019 288 <10 <10 41 17 <10 <10 94 <200 <10 <10 50 <10 <10 <10 72 <10 <10 <10 <10 <10 <10 14 <30 ND 10/13/2020 246 1.7 <1 38 13 1.5 <1 64 <20 1.6 <1 50 5.4 <1 <1 46 <1 <1 <1 0.57 J 0.55 J 1.4 23 <2 ND 10/26/2021 156 <1 <1 37 2 1.4 <1 67 <20 0.93 J <1 36 2.8 <1 <1 9.8 <1 <1 <1 <1 0.53 J <1 21 <2 ND 10/17/2022 173 <1 <1 28 5 1.3 <1 39 <20 0.97 J <1 64 <1 <1 <1 18.0 <1 <1 <1 <1 0.56 J <1 15 <3 1.51 MW-4 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 2 of 15 n v; Sample O N a CD Sample I.D. H b q b 0 3 n 0 b Date :3 0 0 0 0 n 3• 3- 0 3• n m 6 0 0 0 C ,G Q 3' 3' 3' 3' S 0 0 3' O =r O O O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O O � D Do0 a O O O a n O -4 O O n y p N fD (D O 0 _G 0 O 3 O (D .O. fD O 3 M O ( M 3 C O 3' S 3' 3' 3' -a K .r N O N S �+ S 3' N O O O y 0) 3 0) 3 0) 3 M 3 0) 3 0) 3 a) 3 O 3 (D 3 CL (D 7 0) 7 0) 3 fD 3 fD 7 7 CL CD 3 M 3 (D 7 CD 3 3 Q 2) n 3 fD M fD M fD fD M M fD M fD fD fD fD fD CD M M fD CD (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-5 2/24/2009 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 18.6 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-6 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 40 <5 <5 <5 <5 <5 <5 40.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 24 <5 <5 <5 <5 <5 <5 24.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 16 <5 <5 <5 <5 <5 <5 15.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 14 <5 <5 <5 <5 <5 <5 13.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/3/2009 75 <1.0 <1.0 5.9 <1.0 <1.0 <1.0 36.8 16.2 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 6.3 <1.0 2.4 2.9 <1.0 <1.0 1.6 2.0 <2.0 ND 3/30/2010 73 <1.0 <1.0 7.99 <1.0 <1.0 <1.0 47.9 <5.0 <1.0 <1.0 1.21 <1.0 <1.0 <1.0 7.47 <1.0 2.51 1.86 <1.0 <1.0 1.44 2.13 ND ND 11/1/2011 57 <0.5 <0.5 12.9 1.84 <0.5 <0.5 18.0 <0.5 <0.5 <0.5 3.86 2.58 <0.5 <0.5 11 <0.5 <0.5 0.52 <0.5 <0.5 1.92 3.66 <0.5 0.63 11/19/2012 58 <0.5 <0.5 13.2 <0.5 <0.5 <0.5 19.7 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 14 <0.5 <0.5 1.86 <0.5 0.68 2.46 4.87 <0.5 0.76 12/11/2013 48 <5 <5 13.8 <5 <5 <5 12.3 <50 <5 <5 6.50 <5 <5 <5 16 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 101 <1 <1 13 0.47 J <1 <1 58.4 <5 0.96 J <1 2.2 3.8 <1 <1 14 <1 <1 1.9 <1 0.65 J 1.7 4.7 <3 1.2 10/30/2015 69 <1 <1 10 <1 <1 <1 44.8 <5 0.63 J <1 2.0 J 2.2 J <1 <1 8.3 <1 <1 0.99 J <1 <1 1.2 3.2 <3 1.5 11/17/2016 90 <1 <1 12 <1 <1 <1 59 <20 0.74 J <1 1.9 J 2.1 J <1 <1 11 <1 <1 1.6 <1 0.56 J 1.6 3.2 <3 1.4 10/10/2017 53 <1 <1 7 <1 <1 <1 34 <20 15 J <1 1.7 J <1 <1 <1 6 <1 <1 <1 <1 <1 4.2 2.0 <3 ND 11/2/2018 118 <1 <1 12 <1 <1 <1 82 <20 0.63 J <1 2.7 2.1 <1 <1 13 <1 <1 0.79 J <1 0.54 J 1.1 3.3 <3 1.6 9/12/2019 67 <1 <1 5.4 <1 <1 <1 29 27.0 0.45 J <1 <1 <1 <1 <1 4.2 <1 <1 <1 <1 <1 <1 1.1 <3 ND 10/14/2020 76 <1 <1 12.0 <1 <1 <1 43 <20 0.75 J <1 2.8 2.0 <1 <1 10.0 <1 <1 0.81 J <1 0.51 J 1.7 3.0 <2 1.9 10/28/2021 51 <1 <1 7.2 <1 <1 <1 24 <20 0.63 J <1 3.2 1.8 <1 <1 8.8 <1 <1 0.85 J <1 0.41 J 2.0 2.2 <2 1.7 10/19/2022 43 <1 <1 6.2 <1 <1 <1 23 <20 0.64 J <1 2.4 2.2 <1 <1 5.5 <1 <1 <1 <1 <1 <1 2.0 <3 1.3 MW-7B 3/3/2009 244,324 2,630 <100X 25,800 10,100 9,760 <100X 28,900 12,000 <100X <100X 39,500 2,450 <100X <100X 36,100 181 48,100 522 6,020 <100X 251 15,800 1,740 4,470 MW-8 1/28/1997 119 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2 J 96 4.0 3/5/2009 47 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 10.8 15.2 6.6 <1.0 10.8 <1.0 <1.0 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-9 1/28/1997 1 ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND DUP-1 (MW-9) 1/28/1997 2 ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2/26/2009 182 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 168 6.0 <1.0 <1.0 2.7 2.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-10 1/27/1997 126 ND ND 6 ND ND ND 120 ND 2 J ND ND ND ND ND ND ND ND 1 J ND ND ND 7/14/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 258 <5 <5 7.6 <5 <5 <5 250 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 335 <5 <5 <5 <5 <5 <5 335 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 234 <5 <5 <5 <5 <5 <5 234 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 221 <5 <5 <5 <5 <5 <5 221 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 198 <5 <5 <5 <5 <5 <5 198 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 176 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 162 6.4 1.1 <1.0 4.1 <1.0 <1.0 <1.0 <1.0 <1.0 2.2 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/29/2010 184 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 166 10.6 <1.0 <1.0 3.82 1.26 <1.0 <1.0 <1.0 <1.0 2.31 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 47 <0.5 <0.5 <0.5 3.99 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.45 11/19/2012 148 <5 74 <5 <5 <5 <5 74.4 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 33 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 28.1 <5 <0.5 <0.5 2.27 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 2.7 12/10/2014 137 <1 <1 <1 <1 <1 <1 133 <5 <1 <1 2.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.2 10/26/2015 104 <1 <1 <1 <1 <1 <1 103 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.1 11/14/2016 130 <1 <1 <1 <1 <1 <1 130 <20 0.78 J <1 2.8 J <1 <1 <1 0.41 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/10/2017 150 <1 <1 <1 <1 <1 <1 150 <20 <1 <1 <1 1.8 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 160 <1 <1 <1 <1 <1 <1 160 <20 <1 <1 0.93 J 1.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/10/2019 74 <1 <1 <1 <1 <1 <1 72 <20 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 14 <1 <1 <1 <1 <1 <1 14 <20 <1 <1 0.46 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 10 <1 <1 <1 <1 <1 <1 10 <20 <1 <1 0.46 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/14/2022 12 <1 <1 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 3 of 15 n v; Sample O N a M Sample I.D. H b q b 0 3 0 0 b Date :3 0 0 n n n 3- 0 3• n m 6 n n n Q S S 3' 3' S C M p 3' O =r MO O O O O O A y p p fD O 3 S A O O O O D n O 3 n O O O n y MO p N .. fD .. O ,. O _ O 0 �p M O 3 3 M 3 (D O .O. fD - O 3 S_ O .' O ( M S C O S S S 3 S -a K N O N S �+ S S N O S C S S O O O y D) 3 D) 3 a) 3 M 3 a) 3 D) 3 D) 3 O 3 fD 3 CL N 7 N 7 c) 3 N 3 M 7 7 Q. M 3 M 3 N 7 M 3 3 CL n 3 (D M N M N N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-11 1/23/1997 84 5 J ND 4 J 3 J ND ND ND ND 4 J 9 ND ND NA 10 ND ND ND ND ND ND 2 J 47 9/28/2000 298 <5 <5 <5 <5 <5 <5 270 NA 8.6 12 <10 <5 <5 <5 7.7 <5 <5 <5 <5 <10 <10 ND 9/10/2001 314 <5 <5 <5 <5 <5 <5 288 <10 10.6 15.3 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 434 <5 <5 <5 <5 <5 <5 283 <10 11.1 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 126 9/19/2003 118 <5 <5 <5 <5 <5 <5 94.2 <10 7.4 16.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 120 <5 <5 <5 <5 <5 <5 94.1 <10 11.5 14.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 74 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 39.8 11.6 5.4 <1.0 15.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-12A 1/23/1997 11 2 J ND ND 3 J ND ND ND ND 2 J ND ND ND ND ND ND 2 J ND 2 J ND ND ND 7/10/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 12 <5 <5 <5 <5 <5 <5 <10 12.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 27 <5 <5 <5 <5 <5 <5 11.7 14.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 28 <5 <5 <5 <5 <5 <5 11.9 15.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 44 <5 <5 <5 <5 <5 <5 <10 43.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 40 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 38.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.50 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.09 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 38 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 29.0 <5 <0.5 <0.5 8.04 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.61 11/19/2012 203 <5 <5 <5 <5 <5 <5 203 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 210 <5 <5 <5 <5 <5 <5 210 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 226 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 210 8.3 <1.0 <1.0 5.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 1.7 10/27/2015 213 <1 <1 <1 <1 <1 <1 200 <5 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.2 11/14/2016 207 <1 <1 <1 <1 <1 <1 200 19 J <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.5 10/10/2017 273 <1 <1 <1 <1 <1 <1 260 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.7 11/1/2018 93 <1 <1 <1 <1 <1 <1 79 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 9/10/2019 189 <1 <1 <1 <1 <1 <1 180 16 J <1 <1 6.2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 10/13/2020 34 <1 <1 <1 <1 <1 <1 31 <20 <1 <1 1.0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 2.0 10/26/2021 188 <1 <1 <1 <1 <1 <1 180 <20 <1 <1 5.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 1.7 10/17/2022 157 <1 <1 <1 <1 <1 <1 150 <20 <1 <1 6.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND MW-12B 1/23/1997 16 6 ND 2 J ND ND ND ND ND ND 8.0 ND ND ND ND ND ND ND ND ND ND ND 7/10/1998 11 ND ND ND ND ND ND ND ND ND 11 ND ND ND ND ND ND ND ND ND ND ND 9/28/2000 567 <5 <5 <5 <5 <5 <5 510 <5 18 <10 <5 11.0 <5 28 <5 <5 <5 <5 <10 <10 ND 9/6/2001 371 <5 <5 <5 <5 <5 <5 359 <10 <5 12 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 221 <5 <5 <5 <5 <5 <5 211 <10 <5 10.2 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 262 <5 <5 <5 <5 <5 <5 250 <10 <5 12.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 196 <5 <5 <5 <5 <5 <5 182 <10 <5 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 199 17.6 <1.0 <1.0 5.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/9/2010 191 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 176 12.6 <1.0 <1.0 2.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 62 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 43 <5 <0.5 <0.5 13.0 <0.5 <0.5 <0.5 3.6 <0.5 <0.5 <0.5 <0.5 <0.5 1.5 <0.5 <0.5 1.1 11/19/2012 69 <10 <10 <10 <10 <10 <10 68.5 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 83 <5 <5 <5 <5 <5 <5 71.4 <50 <5 <5 11.3 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 158 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 132 6.3 0.64 J <1.0 12.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 0.73 J <1.0 <3 4.2 10/27/2015 123 <1 <1 <1 <1 <1 <1 117 <5 <1 <1 4.7 <1 <1 <1 1.1 J <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 164 <1 <1 <1 <1 <1 <1 150 <20 0.5 J <1 11.0 <1 <1 <1 2.7 J <1 <1 <1 <1 <1 0.58 J <1 <3 3.4 10/10/2017 181 <1 <1 <1 <1 <1 <1 170 <20 0.94 J <1 8.3 <1 <1 <1 2.3 J <1 <1 <1 <1 <1 0.61 J <1 <3 2.7 11/1/2018 112 <1 <1 <1 <1 <1 <1 95 <20 0.51 J <1 11 <1 <1 <1 2.7 <1 <1 <1 <1 <1 <1 <1 <3 3.1 9/11/2019 133 <1 <1 <1 <1 <1 <1 120 <20 0.48 J <1 10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 3.1 10/13/2020 125 <1 <1 <1 <1 <1 <1 110 <20 0.75 J <1 9.5 <1 <1 <1 2.8 <1 <1 <1 <1 <1 <1 <1 <2 3.0 10/26/2021 120 <1 <1 <1 <1 <1 <1 110 <20 0.75 J <1 7.7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 2.2 10/17/2022 111 <1 <1 <1 <1 <1 <1 99 <20 <1 <1 8 <1 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <3 2.3 TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 4 of 15 n v; Sample O N a CD Sample I.D. H b q b 0 3 n 0 b Date :3 0 0 0 0 n 3- 0 3• n m 6 0 0 0 � ,G Q 3' 3' 3' 3' S 0 0 3' O =r O O O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O O � D Do0 a O O O a n O -4 O O n y p N fD (D O 0 _G 0 fD 3 M(D :3 0.O. fD O 3 M O ( M =r C O 3' S 3' 3' 3' -a K .r N O N S �+ S 3' N O O O y 0) 3 0) 3 0) 3 M 3 0) 3 0) 3 a) 3 O 3 (D 3 CL (D 7 0) 7 0) 3 fD 3 fD 7 7 Q. M 3 M 3 fD 7 CD 3 3 CL 0 3 fD M fD M fD fD CD M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-12D 9/10/1998 ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND ND NA ND ND ND ND 9/29/2000 132 <5 <5 <5 <5 <5 <5 120 NA <5 <5 <10 <5 <5 <5 12 <5 <5 <5 <5 <10 <10 ND 9/12/2001 54 <5 <5 <5 <5 <5 <5 14.4 39.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 31 <5 <5 <5 <5 <5 <5 <10 21.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 9.5 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.58 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/3/2011 11 <0.5 <0.5 0.99 <0.5 <0.5 <0.5 3.0 <5 <0.5 <0.5 2.22 <0.5 <0.5 <0.5 1.42 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/23/2012 79 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 77.6 <5 <0.5 <0.5 1.30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2014 1740 41 2.2 29 41 770 <1.0 5.3 5.3 12 6.3 480 <1.0 <1.0 <1.0 5 <1.0 66 47 32 <1.0 180 2.2 7.1 8.6 10/25/2015 ND <1 <1 <1 <1 <1 <1 4.29 J <5 <1 <1 1.1 J <1 <1 <1 0.49 J <1 <1 <1 <1 <1 0.56 J <1 <3 ND 11/18/2016 ND <1 <1 0.48 J 0.41 J <1 <1 4.9 J <20 <1 <1 0.76 J <1 <1 <1 0.79 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 8 <1 <1 <1 <1 <1 <1 8.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 16 <1 <1 0.82 J 1.4 <1 <1 7.2 <20 <1 <1 0.95 J <1 <1 <1 4.1 <1 <1 <1 <1 <1 1.8 1.5 <3 ND 9/11/2019 4 <10 <10 <10 <10 <10 <10 3.7 <200 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND 10/13/2020 3 <1 <1 <1 <1 <1 <1 3.1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 3 <1 <1 <1 <1 <1 <1 2.9 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/17/2022 ND <1 <1 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 0.47 J <1 <1 <1 <1 <1 <3 ND MW-14 8/6/1996 147 ND ND ND ND ND ND ND ND ND 140 ND ND ND ND ND ND ND ND 7 J ND ND 1/29/1997 2,118 ND ND 1 J ND ND ND 1,700 J ND 2 J ND 180 ND ND ND ND ND ND ND ND 3 J 7 J 1 J 46 MW-15A 1/30/1997 2,266 ND ND ND ND ND ND 1,700 ND 9 J ND 520 ND ND ND ND ND ND ND ND ND ND ND 37.0 9/5/2001 3,157 <5 <5 <5 <5 <5 <5 2,640 <10 <5 517 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 2,140 <5 <5 <5 <5 <5 <5 1,500 <10 <5 635 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 2,424 <25 <25 <25 <25 <25 <25 1,910 <50 <25 514 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 8/18/2004 3,209 <25 <25 <25 <25 <25 <25 2,720 <50 <25 489 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 3/6/2009 2,238 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 1,900 <5.0 <1.0 <1.0 335 <1.0 <1.0 <1.0 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 1,211 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 1,170 <5.0 <1.0 <1.0 32.7 <1.0 <1.0 <1.0 7.48 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 940 <0.5 <0.5 <0.5 <0.5 <0.5 1.23 480 <5 1.27 <0.5 430 <0.5 <0.5 <0.5 1.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.92 14.96 11/19/2012 2,324 <10 <10 <10 <10 <10 <10 1,920 <100 <10 <10 404 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 3,308 <5 <5 <5 <5 <5 <5 2,950 <50 <5 <5 350 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.2 12/9/2014 2,405 <5 <5 <5 <5 <5 <5 1,970 <25 <5 <5 430 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 4.6 10/27/2015 2,159 <5 <5 <5 <5 <5 <5 1,740 <25 <5 <5 410 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 9.0 11/14/2016 2,334 <1 <1 <1 <1 <1 1.4 2,200 <20 0.49 J <1 110 <1 <1 <1 5.3 <1 <1 <1 <1 <1 0.45 J 0.93 J <3 17.3 10/11/2017 2,734 <1 <1 <1 <1 <1 1.8 2,600 <20 0.51 J <1 110 <1 <1 <1 5.8 <1 <1 <1 <1 <1 0.43 J 0.69 J <3 16.1 10/31/2018 1,796 <1 <1 <1 <1 <1 0.42 J 1,600 <20 0.67J <1 190 <1 <1 <1 0.45J <1 <1 <1 <1 <1 <1 <1 <3 6.2 9/10/2019 1,590 <5 <5 <5 <5 <5 <5 1,400 <100 <5 <5 190 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 ND 10/8/2020 1,449 <2 <2 7.7 9.9 <2 <2 1,100 <40 0.92 J <2 300 <2 <2 <2 17.0 <2 <2 <2 2.6 <2 <2 5.4 <4 9.0 10/28/2021 1,262 <1 <1 <1 <1 <1 <1 1,200 <20 <1 <1 60 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.9 10/18/2022 1,004 <1 <1 <1 <1 <1 0.46 J 830 <20 <1 <1 170 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 3.6 MW-15B 1/30/1997 330 ND ND ND ND ND ND 210 J ND 1 J ND 110 ND ND ND ND ND ND ND ND ND ND ND 9.0 MW-16 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-17 3/5/2009 305 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 258 30.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 5.8 <1.0 <1.0 1.7 <1.0 <1.0 5.9 3.2 <2.0 ND MRF-1 1/21/1997 63 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 63.0 ND ND ND 7/13/1998 53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 53.0 ND ND ND 2/24/2009 65 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 28.3 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 29.9 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 5 of 15 O N n v; M Sample H a 0 Sample I.D. Date 0 0 b 0 q 0 b n 0 3 n 3- 0 3• b n 0 0 0 :3 Q 3' 3' 3' 3- S 0 M 0 3' O =r m 6 O O O O O O O A y 0 0 fD O 3 S A O O O O O D n O 7 O O O i y p N fD O _ 0 M fD 3 M (D .O. fD O 3 M O ( M =r C O y 3' D) S D) 3' a) 3' M 3' a) -a D) K D) O N M O N N S N �+ S c) 3' N N M O 7 S M C M 3' N S M O 3 O O 3 3 3 3 3 3 3 3 3 3 CL 7 7 3 3 7 Q. 3 3 7 3 CL 0 (D M N M N N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MRF-2 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND OW-NIS1 3/10/2009 214 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 180 9.9 <1.0 <1.0 20.6 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND OW-DR1 9/28/2000 26,291 360 <5 4,300 1,000 150 <5 2,900 150 6,600 3,300 <5 4,100 33 310 18 420 26 14 2,400 210 ND OW-DR2 7/21/1998 11,612 400 J 1,500 D 480 J ND 3,400 J ND 150 2,900 D 1,100 D ND 40 J 460 J 22 ND 250 J 910 9/26/2000 25,240 460 <5 4,200 1,400 220 <5 4,900 NA 170 5,600 1,300 <5 3,500 25 120 19 260 77 28 2,800 161 ND 9/10/2001 27,394 695 <5 4,950 1,330 208 <5 3,450 <10 145 5,980 1,380 <5 5,700 27 107 36 271 11.3 27.8 2,880 196 ND 2/27/2009 25,306 1,230 7.3 3,550 1,580 141 1.3 4,180 46.8 113 <1.0 5,380 1,030 4.3 41.4 6,320 21.1 41.4 47.2 201 17.4 29.5 1,190 120 13.6 3/30/2010 24,982 1,330 <1.0 3,330 1,790 123 <5.0 3,910 <5.0 127 <1.0 5,510 1,090 <1.0 <1.0 6,400 <1.0 <1.0 <1.0 182 <1.0 <1.0 1,190 ND ND 11/1/2011 22,265 1,910 <25 3,000 2,050 121 <25 990 <250 101 <25 4,130 2,350 <25 <25 6,290 <25 <25 <25 153 <25 <25 1,100 38 32.0 11/23/2012 19,775 1,620 <50 2,230 1,430 <50 <50 2,180 <500 <50 <50 4,810 1,760 <50 <50 4,650 <50 <50 <50 177 <50 <50 918 <50 ND 12/11/2013 24,766 1,920 <50 2,730 1,920 120 <50 3,130 <500 154 <50 4,800 1,890 <50 <50 6,600 <50 <50 <50 172 <50 <50 1,330 <100 ND 12/12/2014 6,977 11 <100 19 15 3 <100 2,160 <5 1.1 1.8 4,500 <1.0 <1.0 <1.0 45 <100 <1.0 <100 160 <1.0 <100 13 48 ND 10/30/2015 12,595 720 <20 1,300 800 71 <20 1,630 <100 79 <20 3,400 480 <20 <20 3,200 <20 <20 24 95 14 J 22 750 24 J ND 11/18/2016 11,740 830 <20 1,300 860 150 <20 1,800 <400 65 <20 2,800 340 8.8 J <20 2,800 9.4 J <20 19 J 65 12 J 20 710 21 J ND 10/10/2017 4,103 100 <5 590 290 48 <5 990 <50 23 <100 920 45 <5 <5 840 <5 <5 5.9 5.4 4.7 J 5.4 240 4.5 J ND 11/2/2018 1,882 20 <10 250 110 16 <10 560 <200 8.9 J <10 380 13 <10 <10 430 <10 <10 <10 <10 <10 <10 94 <30 ND 9/11/2019 1,178 12 <5 200 84 11 <5 250 <100 7 <5 260 12 <5 <5 290 <5 <5 <5 <5 <5 <5 52 <15 ND 10/13/2020 1,060 10 <5 220 86 15 <5 280 <100 <5 <5 71 15 <5 <5 310 <5 <5 2.3 J <5 2.6 J <5 53 <10 ND 10/28/2021 742 5.2 <5 130 54 6 <5 250 <100 <5 <5 36 11 <5 <5 230 <5 <5 <5 <5 <5 <5 20 <10 ND 10/18/2022 529 5.2 <5 130 50 8 <5 170 <100 <5 <5 72 23 <5 <5 220 <5 <5 <5 <5 <5 <5 21 <5 ND OW-DR3 9/20/2002 3,989 <5 <5 221 <5 15.4 <5 1,050 <10 11.3 1,840 778 <5 8.9 <5 29.5 <5 <5 <5 <5 35.3 <5 ND 9/19/2003 2,815 <5 <5 201 <5 14.7 <5 690 <10 6.1 1,390 455 <5 11.1 <5 12 <5 <5 <5 <5 35.5 <5 ND 8/24/2004 4,403 <50 <50 452 <50 <50 <50 1,260 <100 <50 1,910 675 <50 <50 <50 <50 <50 <50 <50 <50 106 <50 ND 10/12/2004 3,438 <5 <5 353 <5 14.2 <5 916 <10 6.9 1,480 553 <5 26.2 <5 11.5 <5 <5 <5 <5 77.1 <5 ND 3/4/2009 2,184 <1.0 <1.0 251 5.3 25.1 <1.0 552 <5.0 3.3 <1.0 984 267 <1.0 5.8 38.7 <1.0 5.0 1.3 2.4 <1.0 2.6 40.6 <2.0 ND 11/26/2012 2,352 <0.5 <0.5 226 J 14.7 23.3 <0.5 471 <5 <0.5 <0.5 1,020 359 <0.5 <0.5 73.4 <0.5 5.5 2.06 2.16 1.21 6.55 92.8 0.61 279.57 12/10/2013 2,757 <5 <5 374 43.6 26.4 <5 793 <50 <5 <5 1,060 249 <5 <5 112.0 <5 <5 <5 <5 <5 7.70 85.3 <10 6.30 OW-DR4 9/23/2002 20,502 1,860 <5 4,320 2,010 226 <5 1,570 <10 121 323 282 <5 7,630 5.4 27.6 55.3 27.3 11.7 66.1 1,880 86.7 ND 9/22/2003 22,030 1,350 <50 4,850 1,860 181 <50 2,200 <100 107 562 311 <50 8,960 <50 <50 <50 <50 <50 65.4 1,530 53.5 ND 8/24/2004 20,516 1,840 <250 4,630 2,100 298 <250 1,480 <500 <250 608 <250 <250 7,880 <250 <250 <250 <250 <250 <250 1,680 <250 ND 10/12/2004 9,067 810 <5 3,110 1,230 167 <5 2,190 <10 77 353 <10 <5 <5 <5 <5 35.3 <5 18.8 39.3 987 50.0 ND 10/20/2004 20,733 1,700 <250 4,480 2,240 <250 <250 2,120 <500 <250 522 <500 <250 8,030 <250 <250 <250 <250 <250 <250 1,590 51.0 ND 2/25/2009 15,223 1,490 6.2 2,570 1,510 156 <1.0 1,300 56.0 96.4 <1.0 659 127 7.1 3.9 6,350 4.3 <1.0 44.9 12.9 17.7 96.3 677 38.5 ND OW-SIS-1 8/17/2004 9,885 1,770 6.0 768 1,580 201 <5 811 <10 95 111 <10 18.3 3,150 <5 160 215 <5 <5 774 213 12.8 ND 3/9/2009 16,834 2,820 11.6 1,280 2,950 256 <10.OX 1,360 107 180 <10.OX 179 54.1 29.6 <10.OX 5,200 <10.OX 146 412 <10.OX <10.OX 1,540 288 20.9 ND OW-SIS-2 2/24/2009 3,111 79.8 <1.0 579 277 26 <1.0 418 17.8 38.2 <1.0 29 14.8 <1.0 <1.0 1,030 4.9 356 3.8 36.1 2.1 3.9 167 28.2 ND OW-SIS-3 3/4/2009 41,840 9,110 14.4 4,320 4,640 172 2.7 2,540 158 167 <1.0 147 23.5 34.9 <1.0 13,600 46.2 3,330 103 132 72.6 1,620 1,400 207 ND OW-SF1 3/9/2009 57,440 2,920 48.4 4,980 5,530 1,860 <10.OX 6,670 242 89.6 <10.OX 2,160 1,840 194 <10.OX 20,400 15.7 680 437 618 40.2 1,290 7,240 185 ND OW-LFS-1 2/26/2009 782 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 723 12.8 4.5 <1.0 20.8 12.0 <1.0 <1.0 4.3 1 2.4 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 6 of 15 n v; Sample n N ^' b c N M N Sample I.D. H b q b 3 n c� b =r b Date 0 0 0 0 F 3• n 3 c, m m 0 0 0 Q 3' 3' 3' 3- 3' 0 M 0 3' O 3' 3 3 3' 3' 3' 3 MO O O O O O A y 0 0 fD O 3 S A O O O O D n O 7 O O O i y IO p N fD O _ 0 M O 3' M (D .O. fD O 3 M O M M 3' O x S S S S S -a �( N O N 3' �+ O 3' 3' N O S C 3' S O O O 0) 3 0) 3 0) 3 M 3 0) 3 0) 3 a) 3 O 3 fD 7 CL N 7 N 7 0) 3 N 3 fD 7 CL M 3 M 3 N 7 M 3 3 CL n fD M fD M fD fD M M M M M M M fD fD M M M fD M (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 OW-LFS-2 2/26/2009 363 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 329 9.0 2.4 <1.0 9.4 3.5 <1.0 <1.0 7.1 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/30/2010 281 <1.0 <1.0 2.33 <1.0 <1.0 <1.0 251 <5.0 2.17 <1.0 9.92 2.74 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.15 <1.0 ND ND 11 /1 /2011 110 <0.5 <0.5 3.23 <0.5 <0.5 <0.5 65 <5 4.52 <0.5 10.1 1.90 <0.5 <0.5 20.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 3.5 11/19/2012 276 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 274 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.12 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 421 <5 <5 <5 <5 <5 <5 391 <50 <5 <5 <5 <5 <5 <5 29.6 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 306 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 255 8.1 6.2 <1.0 15 3.8 <1.0 <1.0 12 <1.0 <1.0 <1.0 0.48 J <1.0 0.54 J 1.7 0.75 J 3.7 10/26/2015 285 <1.0 <1.0 1.8 J <1.0 <1.0 <1.0 253 <5 4.5 <1.0 11 <1.0 <1.0 <1.0 13 <1.0 <1.0 <1.0 <1.0 <1.0 0.93 J <1.0 0.45 J 3.4 11/14/2016 276 <1.0 <1.0 1.2 J <1.0 <1.0 <1.0 250 12 J 2.4 <1.0 11 0.76 J <1.0 <1.0 9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 3.2 10/10/2017 248 <1 <1 1.1 J <1 <1 <1 240 <20 1.4 <1 4.6 1.5 J <1 <1 4.6 J <1 <1 <1 <1 <1 <1 <3 0.50 J 2.0 10/31/2018 404 <1 <1 <1 <1 <1 <1 360 <20 32.0 <1 9.3 1.3 <1 <1 0.80 J <1 <1 <1 <1 <1 <1 <1 <3 1.2 9/12/2019 213 <1 <1 0.8 J <1 <1 <1 210 <20 0.48 J <1 3.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 153 <1 <1 0.74 J <1 <1 <1 150 <20 1.2 <1 2.0 0.53 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/28/2021 284 <1 <1 0.79 J <1 <1 <1 270 <20 7.0 <1 3.8 1.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.4 <2 ND 10/17/2022 223 <1 <1 0.78 J <1 <1 <1 220 <20 1.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.48 J <3 ND PW-1 D 1/24/1997 659 ND ND 1 J 1 J ND ND 530 J ND ND 7 ND ND ND ND ND ND ND ND ND 120 ND ND ND 7/15/1998 110 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 110 ND ND ND PW-2D 2/7/1997 28 ND ND 10 ND ND ND ND 10 J ND ND ND 4 J ND ND ND 4 J ND ND ND ND ND ND ND 7/18/1998 11 ND ND 9 ND ND ND ND ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND 2/26/2009 21 <1.0 <1.0 1 1.3 <1.0 <1.0 I <1.0 19.5 1 <5.0 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 <1.0 I <2.0 ND PW-3D 2/7/1997 42,680 4,100 ND 370 J 790 15,000 ND ND ND 260 J ND 16,000 ND ND ND ND 1,300 990 740 ND 3,600 ND ND 160 7/17/1998 21,462 ND 650 D ND 520 J 8,100 D ND ND ND 160 ND 8,600 3 J 2 J ND 13 680 610 D ND ND 2,000 D 54.0 49.0 21.0 4/9/2010 22,149 <1.0 <1.0 393 82.5 8,840 <1.0 39.8 18.4 5.46 <1.0 174 <1.0 <1.0 <1.0 36.1 <1.0 99.1 137.0 7.72 <1.0 419 11.6 ND ND 11/3/2011 damaged 11/27/2012 8,532 54 <50 293 203 4,830 <50 55 <500 <50 <50 2,150 <50 <50 <50 54.0 <50 <50 222 82 <50 589 <50 <50 ND 12/17/2013 27,696 993 9.0 491 1,180 12,800 <5 19.5 <50 137 <5 7,250 <5 <5 <5 59.4 <5 979 723 338 <5 2,540 58.4 12.3 106.5 12/11/2014 73,348 1,500 <200 610 2,800 14,000 <200 67.6 <100 310 240 32,000 <200 <200 <200 100 <200 1,100 8,900 1,300 <200 9,300 150 180 790 10/29/2015 67,602 2,300 <200 660 2,100 17,000 <200 112 <1000 350 <200 32,000 <200 <200 <200 380 86 J 1,000 3,300 1,400 <200 7,000 120 J >600 160 J 11/16/2016 45,170 970 <100 400 870 20,000 <100 120 <2000 190 <100 16,000 <100 <100 <100 110 <100 1,100 1,300 610 <100 3,500 <100 <300 470 J 10/11/2017 70,050 1,700 <200 730 2,000 20,000 <200 180 <4000 330 <200 31,000 <200 <200 <200 280 <200 1,700 3,700 1,200 <200 7,100 120 J 130 760 J 11/2/2018 61,400 1,600 <200 660 2,000 17,000 <200 170 <4000 320 <200 27,000 <200 <200 <200 510 <200 1,400 3,100 1,100 <200 6,100 130 J 100 J 1101 9/11/2019 31,290 860 <200 480 1,100 14,000 <200 140 <200 190 J <200 11,000 <200 <200 <200 350 <200 1,300 620 470 <200 <200 <200 <600 780 J 10/14/2020 76,030 1,700 <200 800 2,900 20,000 <200 160 <4000 450 <200 32,000 <200 <200 <200 540 <200 1,800 4,800 1,300 <200 8,400 190 210 780 10/27/2021 42,540 890 <500 660 1,500 17,000 <500 160 <10000 280 <500 18,000 <500 <500 <500 380 <500 1,800 1,200 670 <500 4,200 <500 <1500 ND 10/12/2022 43,440 620 <500 540 1,300 12,000 <500 1 180 1 <10000 240 <500 20,000 <500 <500 <500 1 380 1 <500 1,400 1 1,900 1 680 1 <500 4,200 <500 <1500 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 7 of 15 n v; Sample O N a M Sample I.D. H b q b 0 3 n 0 b . Date 3 0 0 n n n 3• � 3- 0 3• n m 6 n n n C ,C Q 3' 3' 3' 3' S p 3' n O S 3 3 3' 3' 3' 3 fD O O O O O O A y p O S p O `<_ fD O O O 3 S A O O O O O D W n a O O O a 0O O O 0y p N fD O _G 0 M fD 3 M (D .O. fD O 3 M O ( M 3 C O 3' S 3' 3' 3' -a �( N O N S �+ S 3' N O O O y D) 3 D) 3 C) 3 M 3 C) 3 D) 3 D) 3 O 3 fD 3 CL N 7 N 7 C) 3 N 3 M 7 7 Q. M 3 M 3 N 7 M 3 Q m 0 3 (D M N M N N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-41 1/29/1997 1,086 19.0 ND 440 19.0 280 ND ND ND 3 J 210 101 ND ND ND 4 J 4 J ND 7 J 100 4 J ND 7/13/1998 1,012 ND ND 240 D 26 J 200 D ND ND ND 3 J 110 J ND ND 140 J ND ND 101 2 J ND 11 J 130 DJ ND 140 9/26/2000 1,063 37.0 <5 290 28.0 200 <5 <100 <5 160 <10 <5 190 <5 <5 8 <5 <5 30 120 <10 ND 9/12/2001 1,532 47.8 <5 378 49.2 256 <5 108 <10 <5 211 <10 <5 277 <5 <5 30.6 <5 <5 47.4 127 <5 ND 9/19/2002 1,861 55.8 <15 451 64 306 <15 156 <30 <15 253 <30 <15 336 <15 <15 33.7 <15 <15 53.1 152 <15 ND 10/22/2003 1,781 95.3 <5 340 84 247 <5 232 <10 <5 228 <10 <5 361 <5 <5 18.7 <5 <5 27.5 147 <5 ND 8/26/2004 1,997 78.1 <20 359 78.9 409 <20 215 <40 <20 266 <40 <20 357 <20 <20 39.9 <20 <20 50.6 143 <20 ND 3/5/2009 1,441 45.2 <2.OX 227 66.5 192 <2.OX 204 15.4 <2.OX <2.OX 172 6.4 <2.OX <2.OX 288 <2.OX <2.OX 51.4 <2.OX <2.OX 67.2 106 <4.OX ND 4/2/2010 1,143 <1.0 <1.0 220 38.8 178 <1.0 224 8.12 2.32 <1.0 132 3.78 <1.0 <1.0 195 <1.0 3.19 21.3 <1.0 <1.0 28.5 87.6 ND ND 11/2/2011 1,077 456 <5 8.84 48.7 101 <5 44 <50 <5 <5 74.2 <5 <5 <5 204 <5 <5 17.3 <5 <5 118 4.99 <5 ND 11/20/2012 1,086 28.9 <0.5 122 65.5 135 <0.5 175 <50 <5 <5 84.3 <5 <5 <5 276 <5 <5 30 <5 <5 87.8 81.3 <5 ND 12/17/2013 1,276 62.2 <5 134 67.1 139 <5 143 <50 <5 <5 82.4 <5 <5 <5 406 <5 <5 9.4 <5 <5 110 123 <10 ND 12/8/2014 864 35 <5 73 48 87 <5 196 <25 <5 <5 63 3.1 J <5 <5 210 <5 <5 28 <5 <5 74 50 <15 ND 10/29/2015 942 33 <2 75 43 55 <2 206 <10 2.0 <2 88 <2 <2 <2 240 <2 <2 44 <2 1.3 J 95 57 <6 3.9 11/17/2016 933 59 <2 75 51 74 <2 210 <40 2.0 <2 71 <2 <2 <2 230 <2 <2 31 <2 1.5 J 80 47 <6 3.3 10/11/2017 906 46 <2 72 42 49 <2 240 <40 2.0 <2 77 3.5 J <2 <2 230 <2 <2 30 <2 1.7 J 70 45 <6 2.9 11/2/2018 853 46 <2 57 42 36 <2 220 <40 1.6 J <2 78 2.8 <2 <2 230 <2 <2 26 <2 1.3 J 64 46 <6 2.7 9/11/2019 720 32 <5 69 37 36 <5 200 <100 <5 <5 60 <5 <5 <5 230 <5 <5 13 <5 <5 <5 43 <15 ND 10/14/2020 789 30 <5 62 41 37 <5 160 <100 2.8 J <5 100 <5 <5 <5 220 <5 <5 32 2.0 J <5 65 42 <10 3.5 10/27/2021 585 26 <5 43 32 22 <5 180 <100 2.1 J <5 60 <5 <5 <5 170 <5 2.2 J 12 2.0 J <5 41 33 <10 2.6 10/18/2022 485 9 <5 39 17 20 <5 150 <100 <5 <5 53 <5 <5 <5 120 <5 <5 9 <5 <5 30 35 <15 3.0 PW-5D 1/30/1997 426 ND ND 20.0 ND 2.0 ND ND 76.0 2 J 140 33.0 8.0 NA ND 26 ND 10 ND ND 18 ND 91 7/14/1998 6,293 96 J ND 550 D ND 38.0 ND 1,300 ND 61 J 3,800 ND ND 22.0 19 J ND 9 J 260 D 3 J 5 J ND 99 J 31 9/26/2000 13,327 360 <5 2,400 500 150 <5 2,300 110 4,300 220 <5 1,600 21 6.3 17 180 31 28 1,000 104 ND 9/10/2001 13,445 437 <5 2,310 534 168 <5 1,680 <10 90.6 4,110 156 <5 2,280 19.3 11.1 31.7 205 6.6 30.8 1,270 105 ND 9/23/2002 14,201 552 <5 2,500 694 211 <5 1,920 <10 90.1 3,460 190 <5 2,900 16.9 6 27.6 169 7.5 26.2 1,330 101 ND 9/19/2003 753 <5 <5 57.6 <5 <5 <5 412 110.0 <5 164 <10 <5 9 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 12,945 534 <5 2,360 757 177 <5 1,260 <10 78.0 3,240 <10 <5 2,980 15.6 <5 32.1 131 <5 15.7 1,280 85 ND 10/12/2004 6,457 166 <5 842 235 57.4 <5 2,420 33.4 31.6 1,240 <10 <5 921 5.7 <5 9.5 44.0 <5 5.8 417 28.4 ND 2/27/2009 14,465 638 5.7 1,900 885 178 <1.0 2,390 36.4 83.4 <1.0 3,110 119 3.5 22.8 4,120 14.8 <1.0 38.3 131 12.1 26.4 672 78.7 ND 3/30/2010 12,428 481 <20.0 1,760 771 102 <20.0 2,170 <100 71.4 <20 3,070 210 <20.0 <20.0 3,040 <20.0 <20.0 <20.0 109 <20.0 <20.0 644 ND ND 11/3/2011 11,290 895 <50 1,760 925 103 <50 580 <500 <50 <50 2,440 488 <50 <50 3,450 <50 <50 <50 <50 <50 <50 649 <50 ND 11/23/2012 11,845 792 <5 1,290 896 109 <5 1,710 <50 51.9 <5 2,000 302 <5 <5 3,850 <5 <5 21.5 101 <5 22.2 602 49.8 47.6 12/16/2013 19,821 1,550 <5 2,200 2,200 181 <5 3,760 <50 121 <5 2,960 509 7.2 <5 5,300 <5 <5 <5 <5 29.7 <5 920 57.6 25.5 12/10/2014 18,168 860 <100 1,800 1,700 340 <100 1,740 <100 100 120 5,200 350 <100 <100 4,400 <100 <100 100 <100 160 <100 1,000 58 240 10/30/2015 7,514 280 <20 870 490 61 <20 1,390 <100 46 <20 2,000 52 <20 <20 1,900 <20 <20 14 J 45 8.8 J 9.2 J 380 13 J ND 11/18/2016 11,941 830 <50 1,400 960 190 <50 1,600 <1000 65 <50 3,000 240 <50 <50 2,900 <50 <50 28 J 66 <50 28 J 690 22 J ND 10/10/2017 4,536 120 <10 640 300 57 <10 1,100 <200 23 <10 830 36 <10 <10 1,200 <10 <10 5.0 J 4.0 J <10 5.1 J 230 4.1 J ND 11/2/2018 2,010 20 <10 280 110 15 <10 560 <200 11 <10 450 14 <10 <10 440 <10 <10 <10 <10 <10 <10 110 <30 ND 9/11/2019 940 7 <5 170 55 8 <5 240 <100 4.4 J <5 220 <5 <5 <5 180 <5 <5 <5 <5 <5 <5 56 <15 ND 10/13/2020 1,272 25 <5 370 21 26 <5 460 <100 9.2 <5 280 7.8 <5 <5 44 <5 <5 3.1 J 3.4 J 2.4 J <5 29 <10 ND 10/28/2021 834 7.6 <5 200 4 15 <5 400 <100 5.4 <5 180 <5 <5 <5 12 <5 <5 <5 <5 <5 <5 10 <10 ND 10/18/2022 686 7.7 <10 190 <10 17 <10 310 <200 <10 <10 150 <10 <10 <10 5 <10 <10 <10 <10 <10 <10 6 <30 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 8 of 15 n O N v; Sample a CD Sample I.D. H b q b 0 3 n 0 b Date :3 0 0 0 0 n 3- 0 3• n m 6 0 0 0 � ,G Q 3' 3' 3' 3' S 0 0 3' O =r O O O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O O 'a D W 0 a O O 3 O a n O -4 O O n y p N .. fD .. (D O ,. 0 O _G O 0 �D fD 3 3 fD 3 (D O .O. fD - O 3 3 M .' O ( M S C O 3' S 3' 3' 3' -a K .r N O N S �+ S 3' N O O O y D) 3 D) 3 O 3 fD 3 O 3 0) 3 D) 3 O 3 (D 3 CL fD 7 N 7 c) 3 fD 3 fD 7 7 CL CD 3 M 3 fD 7 CD 3 3 CL n 3 fD M fD M fD fD CD M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-6D 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/18/2009 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 31.3 <1.0 <1.0 4.9 <1.0 <1.0 <1.0 5.70 <5.0 <1.0 <1.0 15.5 <1.0 <1.0 <1.0 3.24 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 266 3.2 <1 41 16 <1 <1 43.2 <5 1.7 <1 90 <1 <1 <1 48 <1 <1 0.53J 1.1 <1 <1 20.0 1.5 ND 10/30/2015 116 2.7 <1 20 8.6 <1 <1 8.85 J <5 0.9 J <1 46 3.0 J <1 <1 31 <1 <1 <1 <1 <1 <1 7.9 <3 ND 11/17/2016 935 14.0 <5 140 59.0 5.2 <5 190 <100 5.4 <5 260 12.0 <5 <5 210 <5 <5 <5 <5 <5 <5 39 <15 ND 12/28/2016 13 NA NA NA NA NA NA 13 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2017 600 NA NA NA NA NA NA 600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/10/2017 1,626 19.0 <2 270 95 12.0 <2 450 <40 7.3 <2 320 20.0 <2 <2 370 <2 <2 1.5 <2 1.4 J 1.4 J 61 <6 ND 11/1/2018 996 7.4 <2 130 50 6.5 <2 320 <40 2.7 <2 230 6.1 <2 <2 210 <2 <2 1.3 <2 <2 1.1 J 31 <6 ND 9/12/2019 492 4.5 <1 120 42 4.7 <1 100 <20 1.4 <1 120 7.0 <1 <1 150 <1 0.84 J 0.84 J <1 1.6 <1 25 <3 ND 10/12/2020 210 <1 <1 47 1.1 3.2 <1 120 <20 0.92 J <1 27 2.3 <1 <1 6.7 <1 <1 <1 0.99 J <1 <1 3.1 <2 ND 10/28/2021 620 3.4 <5 110 38 5.3 <5 190 <100 2.2 J <5 93 5.6 <5 <5 150 <5 <5 <5 <5 <5 <5 22 <15 ND 10/14/2022 234 <1 <1 29 <1 2.6 <1 180 <20 0.54 J <1 17 <1 <1 <1 <1 <1 1.1 <1 0.75 J <1 <1 2.6 <3 ND PW-61 1/28/1997 33 ND ND 11 ND 1 J ND ND ND ND 14 4 J ND ND 1 J ND ND ND 2 J ND ND ND 7/14/1998 46 ND ND 10 ND ND ND ND ND ND 14 4 J ND 5 ND ND 5 ND ND 3 J ND ND 5 9/26/2000 29 <5 <5 12 <5 <5 <5 <100 <5 8.4 <10 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 28 <5 <5 10.7 <5 <5 <5 <10 <10 <5 7.2 <10 <5 9.9 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 31 <5 <5 12.2 <5 <5 <5 <10 <10 <5 9.0 <10 <5 9.8 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 47 <5 <5 12.1 <5 <5 <5 11.6 <10 <5 9.9 <10 <5 13 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 42 <5 <5 10.6 <5 <5 <5 11.7 <10 <5 6.2 <10 <5 13.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 8.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 2.4 <1.0 3.8 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 143.1 <1.0 <1.0 32 1.63 3.47 <1.0 22.5 <5.0 <1.0 <1.0 35.7 10.3 <1.0 <1.0 25.2 <1.0 <1.0 1.56 <1.0 <1.0 2.81 7.88 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 115 0.41 J <1 26 2.2 <1 <1 47.9 <5 <1 <1 2.2 <1 <1 <1 24 <1 1.1 0.7 J 0.7 J <1 1.1 3.3 4.8 1.9 10/27/2015 98 <1 <1 20 1.1 J 3 <1 46.7 <5 <1 <1 7.6 <1 <1 <1 18 <1 <1 0.74 J <1 <1 1.4 <1 <3 1.1 11/17/2016 132 <1 <1 19 1.1 J 11 <1 56 <20 0.47 J <1 21 <1 <1 <1 18 <1 0.53 J 1.0 <1 <1 2.5 3.6 <3 3.89 J 10/10/2017 148 <1 <1 25 0.92 J 3.6 <1 71 <20 0.52 J <1 19 <1 <1 <1 25 <1 <1 0.42 J <1 <1 1.1 3.0 <3 1.4 11/1/2018 128 <1 <1 17 1.1 3.2 0.4 J 60 <20 0.58 J <1 14 <1 <1 <1 24 <1 <1 0.8 J <1 <1 1.7 4.7 <3 1.8 9/12/2019 148 <1 <1 19 1.0 2.9 <1 79 <20 0.74 J <1 13 <1 <1 <1 26 <1 <1 0.42 J <1 <1 <1 5.3 <3 1.8 10/13/2020 137 <1 <1 20 1.4 3.3 <1 63 <20 0.74 J <1 15 <1 <1 <1 26 <1 <1 0.52 J <1 0.43 J 1.6 4.5 <2 1.8 10/28/2021 115 <1 <1 11 0.74 J 2.1 <1 69 <20 0.62 J <1 9.6 <1 <1 <1 18 <1 <1 0.50 J <1 <1 <1 3.2 <2 2.0 10/14/2022 116 <1 <1 8.3 <1 2.0 <1 86 <20 <1 <1 5.2 <1 <1 <1 12 <1 <1 <1 <1 <1 <1 1.6 <3 1.2 PW-71 2/6/1997 11 ND ND 2 J ND ND ND ND 7 J ND 1 J ND ND ND ND ND ND ND 1 J ND ND ND 7/17/1998 443 86 ND 16 37 23 ND ND ND 2 J 77 ND ND 50 ND ND 65 9 ND 21 4 J 3 J 50 9/28/2000 99 <5 <5 9.2 15 7.2 <5 <100 NA <5 18 <10 <5 36 <5 14 <5 <5 <5 <5 <10 <10 ND 9/12/2001 158 <5 <5 <5 <5 <5 <5 150 <10 <5 8.1 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 139 <5 <5 <5 <5 <5 <5 126 <10 <5 7.7 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 161 <5 <5 <5 <5 <5 <5 144 <10 <5 9.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 6.8 8/25/2004 199 <5 <5 <5 <5 <5 <5 191 <10 <5 8.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 75 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 50.5 6.8 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 2.6 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 1.8 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 9 of 15 n v; Sample O N a Sample I.D. H b q b 3 n 0 Date :3 0 0 0 0 n 3• 3- 0 3• n m 6 0 n 0 .G Q 3' 3' 3' 3' S 0 M 0 3' O O O O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O 0 D W 0 a O O 0 a C7 O O O ii y p N fD O _G 0 M O 3 O (D .O. fD O 3 M O ( M =r C O 3' S 3' 3' 3' -a K N O N S �+ S 3' N O O O y D) 3 D) 3 a) 3 M 3 a) 3 D) 3 D) 3 O 3 fD 3 CL N 7 N 7 c) 3 N 3 M 7 7 Q. M 3 M 3 N 7 M 3 3 CL 0 3 (D M N M N N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-8S 1/28/1997 670 ND ND ND ND ND ND ND 670 J ND ND ND ND ND ND ND ND ND ND ND ND ND 7/13/1998 17 ND ND ND ND ND ND ND ND ND ND ND ND 7 ND ND ND ND ND ND ND ND 10 9/27/2000 7.7 <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 7.7 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 37 <5 <5 <5 <5 <5 <5 14.5 <10 <5 6.1 <10 <5 8.1 <5 <5 <5 <5 <5 <5 <10 <5 8.7 9/17/2003 180 <5 <5 <5 <5 <5 <5 <10 163 <5 11.3 <10 <5 6.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 7.7 <5 <5 <5 <5 <5 <5 <10 <10 <5 7.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND PW-91 1/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 50 ND ND ND ND ND ND ND 50 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/12/2009 97 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 95.2 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-10D 9/10/1998 15.0 ND ND 6.0 ND ND ND ND ND ND ND 9 J NA NA NA ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 11 <5 <5 <5 <5 <5 <5 10.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 10.4 <5 <5 <5 <5 <5 <5 <10 10.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/26/2009 31 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 <2.0 29.0 3/29/2010 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.37 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 1.56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.72 <0.5 <0.5 <0.5 <0.5 ND 11 /21 /2012 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/10/2014 ND <1 <1 <1 <1 <1 <1 1.7 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.8 J ND 11/3/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/17/2016 15 1.5 <1 2.3 J 4.9 J <1 <1 <1 <20 <1 <1 2.6 J <1 <1 <1 7.8 <1 <1 0.60 J 0.49 J <1 2.4 3.3 <3 ND 10/10/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 20 0.96 J <1 1.6 2.3 <1 <1 <2 <20 <1 <1 1.1 <1 <1 <1 8.6 <1 <1 <1 0.5 J <1 2.7 3.2 <3 ND 9/12/2019 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.85 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/13/2022 1 <1 <1 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 1.3 <1 <1 <1 <1 <1 <3 ND PW-101 1/27/1997 7.0 ND ND 6 ND ND ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND 7/10/1998 8.0 ND ND 8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 14 <5 <5 14 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/11/2001 44 <5 <5 12.9 <5 <5 <5 31.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 39 <5 <5 <5 <5 <5 <5 14.7 24.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2003 126 <5 <5 17 <5 <5 <5 109 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 83 <5 <5 16.7 <5 <5 <5 61.3 <10 <5 <5 <10 <5 5.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/12/2009 150 <1.0 <1.0 12.7 <1.0 <1.0 <1.0 115 13.8 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 5.2 <1.0 1.1 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/29/2010 229 <1.0 <1.0 12.6 <1.0 <1.0 <1.0 206 <5.0 <1.0 <1.0 1.38 1.96 <1.0 <1.0 4.86 <1.0 1.49 <1.0 <1.0 <1.0 <1.0 1.14 ND ND 11/1/2011 78 <0.5 <0.5 21.7 1.65 <0.5 <0.5 36 <5 <0.5 <0.5 1.95 3.73 <0.5 <0.5 8.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3.18 <0.5 1.45 11/19/2012 440 220 <5 25.9 <5 <5 <5 183 <50 <5 <5 <5 <5 <5 <5 11.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/11/2013 276 <5 <5 19.5 <5 <5 <5 249 <50 <5 <5 <5 <5 <5 <5 7.7 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/10/2014 243 <1 <1 18 0.55 J <1 <1 205 <5 0.45 J <1 2.3 5.1 <1 <1 6.2 <1 <1 <1 <1 <1 <1 4.4 <3 1.6 10/29/2015 22 <1 <1 16 <1 <1 <1 222 <5 0.57 J <1 2.7 J 3.3 J <1 <1 4.2 J <1 <1 <1 <1 <1 <1 3.9 <3 2.3 11/17/2016 270 <1 <1 18 0.41 J <1 <1 240 <20 0.85 J <1 3.0 2.6 J <1 <1 5.2 <1 <1 <1 <1 0.45 J <1 4.1 <3 2.93 J 10/10/2017 226 <1 <1 5.7 <1 <1 <1 220 <20 <1 <1 <1 <1 <1 <1 1.4 J <1 <1 <1 <1 <1 <1 0.51 J <3 0.44 J 11/1/2018 319 <1 <1 13 <1 <1 <1 290 <20 0.96 J <1 2.5 3.7 <1 <1 4.2 <1 <1 <1 <1 <1 <1 3.4 <3 2.0 9/12/2019 292 <1 <1 12 <1 <1 <1 260 <20 1.0 <1 2.6 <1 <1 5.9 4.2 <1 <1 <1 <1 <1 <1 3.7 <3 2.4 10/12/2020 281 <1 <1 11 <1 <1 <1 250 <20 1.4 <1 2.9 4.0 <1 <1 4.5 <1 1.1 <1 <1 <1 <1 3.2 <2 2.7 10/26/2021 327 <1 <1 7 <1 <1 <1 310 <20 1.2 <1 2.2 2.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.9 <2 1.7 10/13/2022 604 <1 <1 4.9 <1 <1 <1 590 <20 1.3 <1 3.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.7 <3 3.1 TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 10of15 n v; Sample O N a CD Sample I.D. H b q b 3 0 0 b Date 3 0 0 0 0 n s 0 s n m 6 0 n 0 C ,C Q 3 3 S 2:3 0 0 S O 3 3 3 3 S 3 7 O O O O O O A y 0 O S 0 O `G fD O O O 7 S A O O O O O 'a D Do a O O 3 O a n O -4 O O n y 0 N fD (D O _G 0 O 3 M( 0 .O. fD O S_ O O (D 3 3 S 3 3 -a >< .r N O N S �+ 3 3 N O 3 C S 3 O O O y D) 3 D) N fD O 0) 3 D) O (D CL fD > N > C) fD fD 7 CL CD CD fD CD a m n fD CD fD M fD fD CD fD fD M fD fD fD fD fD CD CD M fD CD (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-111 7/22/1997 458 ND ND ND ND ND 8 J ND ND ND ND ND ND ND ND ND ND ND 450 ND ND ND 7/16/1998 354 ND ND ND ND ND ND ND ND ND ND ND ND 47 ND ND ND ND ND 260 D ND ND 47 9/29/2000 156 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 26 <5 <5 <5 <5 <5 130 <10 <10 ND 9/11/2001 254 <5 <5 <5 <5 <5 <5 14.3 <10 <5 <5 <10 <5 34.8 <5 <5 <5 <5 <5 205 <10 <5 ND 9/18/2002 274 <5 <5 <5 <5 <5 <5 22.3 <10 <5 <5 <10 <5 38.1 <5 <5 <5 <5 <5 214 <10 <5 ND 9/23/2003 516 <10 <10 <10 <10 <10 <10 50.3 <20 <10 <10 <20 <10 87.3 <10 <10 <10 <10 <10 378 <20 <10 ND 8/25/2004 365 <10 <10 21.5 <10 <10 <10 31.3 <20 <10 <10 <20 <10 82.7 <10 <10 <10 <10 <10 229 <20 <10 ND 3/5/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 13.2 8.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 36.2 <1.0 2.5 <1.0 <1.0 <1.0 162 <1.0 <5.0 ND PW-121 7/22/1997 8.0 ND ND ND ND ND ND ND 6 J ND ND ND ND ND 2 J ND ND ND ND ND ND ND 7/16/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 1.0 <5 <5 <5 <5 <5 <5 1.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/3/2009 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.69 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 8.55 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.22 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/17/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/12/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/30/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 1.3 J <1 <1 <1 0.70 J <1 <1 <1 <1 <1 <1 <1 <3 ND 11/21/2016 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/6/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/11/2019 ND <1 <1 <1 <1 <1 <1 1.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/14/2020 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.63 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/28/2021 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.63 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/19/2022 ND <1 <1 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND PW-131 7/22/1998 295 16/14 NA 77176 35/26 ND/ND NA ND/ND ND/ND 2 J/2 J 6/6 ND/4 J NA ND/ND 3 J / 2 J 8/8 NA 4 J / 4 J 34/36 ND/ND 110/110 9/29/2000 754 27 <5 240 120 12 <5 <100 NA 8.2 11.0 11.0 <5 220 <5 <5 <5 <5 5.4 6.2 93 <10 ND 9/12/2001 892 16.4 <5 275 89.0 14.1 <5 70.9 <10 7.8 10.4 10.9 <5 305 <5 <5 <5 <5 <5 5.2 87.6 <5 ND 9/20/2002 799 <15 <15 243 67.4 <15 <15 128 <30 <15 <15 <30 <15 270 <15 <15 <15 <15 <15 <15 91 <15 ND 9/23/2003 1,027 11.7 <10 321 92.2 14.3 <10 118 <20 <10 21.7 <20 <10 358 <10 <10 <10 <10 <10 <10 90.4 <10 ND 8/25/2004 1,285 <5 <5 353 116 22.2 <5 166 <10 10.7 47.0 13.4 <5 405 <5 <5 5.6 <5 <5 8.4 138 <5 ND 3/4/2009 520 <1.0 <1.0 175 39.3 8.9 <1.0 78.0 <5.0 5.6 <1.0 18.1 4.1 <1.0 <1.0 133 <1.0 <1.0 1.8 <1.0 <1.0 2.6 53.9 <2.0 ND 3/31/2010 581 <1.0 <1.0 192 41.6 8.8 <1.0 92.4 <5.0 4.96 <1.0 14.5 3.66 <1.0 <1.0 158 <1.0 <1.0 1.07 <1.0 <1.0 2.08 62 ND ND 11/3/2011 784 6.18 <0.5 214 121 11.8 <0.5 27.0 <5 8.05 <0.5 31.4 7.27 <0.5 <0.5 243 <0.5 <0.5 <0.5 <0.5 <0.5 6.26 107 <0.5 0.87 11 /23/2012 779 2.10 <0.5 137 58.5 <0.5 <0.5 332 <5 2.21 <0.5 23.1 4.98 <0.5 <0.5 147 <0.5 <0.5 1.64 <0.5 <0.5 3.26 62.1 <0.5 5.21 12/16/2013 743 <5 <5 197 56.3 11.0 <5 139 <50 <5 <5 <5 <5 <5 <5 236 <5 <5 <5 <5 <5 <5 104 <10 ND 12/12/2014 564 <2 <2 150 53 11.0 <2 91.6 <10 4.0 <2 22 <2 <2 <2 160 <2 <2 1.5 <2 <2 2.8 69 <6 2.1 10/26/2015 419 <1 <1 120 28 4.6 <1 88.6 <5 3.2 <1 18 2.0 J <1 <1 110 <1 <1 1.2 <1 <1 2.1 41 <3 2.2 11/18/2016 433 <1 <1 120 34 5.0 <1 89 <20 2.9 <1 17 1.6 J <1 <1 120 <1 <1 1.3 <1 <1 2.3 40 <3 1.9 10/11/2017 350 <1 <1 100 20 4.8 <1 88 <20 2.5 <1 11 1.7 J <1 <1 80 <1 <1 0.83 J <1 <1 1.6 40 <3 1.9 10/31/2018 322 <1 <1 82 20 4.1 <1 81 <20 2.3 <1 12 1.3 <1 <1 84 <1 <1 0.86 J <1 <1 1.7 32 <3 1.5 9/11/2019 282 <1 <1 94 18 3.6 <1 44 <20 2.4 <1 8.9 1.4 <1 <1 72 <1 <1 0.72 J <1 0.44 J <1 38 <3 ND 10/13/2020 146 <1 <1 110 1.6 4.0 <1 68 <20 2.7 <1 11.0 2.5 <1 <1 7.8 <1 <1 <1 0.65 J <1 0.51 J 6.1 <2 0.93 J 10/28/2021 171 <1 <1 87 <1 1.2 <1 70 <20 2.3 <1 9.4 1.2 <1 <1 <1 <1 <1 <1 0.53 J <1 <1 0.94 J <2 0.74 J 10/12/2022 194 <1 <1 76 1.4 1.4 <1 84 <20 2.0 <1 11.0 2.0 <1 <1 6.9 <1 <1 0.53 J 0.59 1 <1 <1 7.1 <3 0.91 1 TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 11 of 15 n v; Sample O N a M Sample I.D. H b q b 0 3 n 0 b Date :3 0 0 0 0 n 3- 0 3• n m 6 0 0 0 C ,G Q 3' 3' 3' 3- S 0 M 0 3' O 3' MO O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O O D W n a O O O a 00 O O 0y p N .. fD .. O ,. O _G O 0 M fD 3 3 M 3 (D O .O. fD - O 3 3 M .' O ( M 3 C O 3' S 3' 3' 3' -a x .+ N O N S �+ S 3' N O S C 3' S O O O y D) 3 D) 3 N 3 M 3 a) 3 D) 3 D) 3 O 3 fD 7 CL N 7 N 7 c) 3 N 3 M 7 7 Q. M 3 M 3 N 7 M 3 3 Q 2) n 3 (D M N M N M M M M M M M M N M CD M M N M N U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-14D 7/22/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/31/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 81 <5 <5 <5 <5 <5 <5 <10 73.1 <5 <5 <10 <5 <5 <5 7.6 <5 <5 <5 <5 <10 <5 ND 9/17/2003 71 <5 <5 <5 <5 <5 <5 <10 70.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 25 <5 <5 <5 <5 <5 <5 <10 25.2 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 16 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 16.3/18.1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 ND 7/26/2007 13 <1 <1 <1 <1 <1 <1 <2 12.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 14 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 13.4 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 21.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 23 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 13.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 9.2 11/27/2012 40 <0.5 <0.5 1.1 <0.5 <0.5 <0.5 35.4 <5 <0.5 <0.5 1.72 <0.5 <0.5 <0.5 2.18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 690 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 690 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/9/2014 236 8.9 <1 25 17 <1 <1 28.7 16.0 1.9 1.2 75.0 6.9 <1 <1 44 <1 <1 0.41 J 1.1 <1 <1 10 2.9 J ND 11/3/2015 10 0.53 J <1 4.2 J 1.0 J <1 <1 8.33 J 8.5 J <1 <1 4.0 <1 <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/16/2016 9 0.64 J <1 3.1 J 0.96 J <1 <1 7.6 J <20 <1 <1 4.4 <1 <1 <1 5 <1 <1 <1 <1 <1 <1 0.89 J <3 ND 10/12/2017 972 5.9 <1 100 24 0.63 J <1 640 <20 1.7 <1 83.0 4.7 J <1 <1 110 <1 <1 0.87 J <1 <1 0.59 J 7.8 <3 ND 11/5/2018 153 <1 <1 0.91 J <1 <1 <1 2.4 <20 0.71 J <1 1.5 <1 <1 <1 1.6 7.7 <1 <1 23 <1 <1 <1 59 ND 9/17/2019 19 <1 <1 0.55 J <1 <1 <1 <2 10 J <1 <1 1.4 <1 <1 <1 0.89 J 1.6 <1 <1 5.2 <1 <1 <1 11 ND 10/15/2020 16 <1 <1 0.44 J <1 <1 <1 <2 <20 <1 <1 1.4 <1 <1 <1 0.99 J 0.90 J <1 <1 2.7 <1 <1 <1 5.7 ND 10/27/2021 10 <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 0.80 J <1 <1 <1 0.76 J 0.67 J <1 <1 1.7 <1 <1 <1 4.2 ND 10/13/2022 37 <1 <1 <1 <1 <1 <1 0.49 J 15 J <1 <1 1.3 <1 3.5 <1 0.77 J 0.58 J 0.52 J <1 2.2 <1 <1 0.58 J 3.9 4.3 PW-14S 7/23/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 7/28/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/10/2009 28 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 28.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-15D 7/21/1998 841 ND 150 ND 8 320 J ND ND 14.0 220 D 75.0 3 J ND 3 J 38.0 ND 10.0 10/31/2000 9,042 46.0 <5 710 57 19 <5 1,800 NA 73.0 5,100 690 <5 220 <5 68.0 <5 25.0 5.4 6.5 200 22.0 ND 9/6/2001 12,582 <5 <5 1,150 <5 <5 <5 3,650 <10 <5 5,930 813 <5 653 <5 <5 <5 <5 <5 <5 386 <5 ND 9/16/2003 2,467 24.0 <5 349 78.2 14.1 <5 622 <10 <10 728 162 <5 352 <5 20.1 <5 <5 <5 <5 118 <5 ND 8/19/2004 507 <5 <5 105 19.7 <5 <5 126 <10 <10 107 27.0 <5 104 <5 <5 <5 <5 <5 <5 17.8 <5 ND 8/29/2006 8,571 234 <10 1,450 507 65.2 <10 1,650 <50 57.3 1,910 200 <10 1,920 <10 16.9 10.1 <10 <10 <10 550 <20 ND 9/26/2007 1.8 <1 <1 1.8 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 11,715 426 3.6 1,840 740 83.6 <1.0 1,990 37.1 69.3 <1.0 2,890 254 1.7 <1.0 2,530 1.9 7.4 20.2 31.6 8.4 7.1 713 52.2 7.4 3/30/2010 14,028 466 3.37 2,120 876 83.0 <1.0 2,230 40.1 82.1 <1.0 3,660 273 1.65 <1.0 3,360 <1.0 8.21 15.9 19.1 9.47 8.0 772 ND ND 11/7/2011 196 10.1 <5 39.4 <5 <5 <5 8 <50 <5 <5 61.9 <5 <5 <5 58.4 <5 <5 <5 <5 <5 <5 18.5 <5 ND 11/26/2012 6,608 424 1.89 1,160 612 64.6 0.59 1,180 <5 73.9 <0.5 812 J 351 <0.5 <0.5 2,070 6.56 7.23 12.0 53.2 12.0 7.48 483 37.5 50.63 12/12/2013 11,775 591 <5 1,440 593 70.5 <5 1,770 <50 67.3 88.4 2,920 536 <5 <5 2,920 <5 <5 <5 51.8 <5 <5 676 32.7 18.2 12/9/2014 12,358 520 <50 1,400 920 82.0 <50 1,930 <250 66.0 <50 3,600 470 <50 <50 2,700 <50 <50 <50 23.0 <50 <50 670 <150 ND 10/28/2015 4,734 68 <50 570 220 <50 <50 1,280 <250 28.0 <50 1,300 <50 <50 96 1,000 <50 <50 <50 <50 <50 <50 200 <150 ND 11/15/2016 3,812 63 <10 430 170 24 <10 1,300 <200 16.0 <10 910 99 <10 <10 690 <10 <10 <10 <10 <10 <10 110 <30 ND 10/12/2017 1,321 12 <1 200 66 7.9 <1 510 <20 4.2 <1 190 12 <1 <1 280 <1 <1 1.5 J <1 1.1 J 1.0 J 39 <3 ND 11/5/2018 572 3.1 <2 81 27 2.2 <2 240 <40 1.1 J <2 79 5.3 <2 <2 120 <2 <2 1.2 J <2 1.1 J <2 11 <6 ND 9/17/2019 176 <5 <5 30 8.9 <5 <5 91 <100 <5 <5 7.4 <5 <5 <5 39 <5 <5 <5 <5 <5 <5 <5 <15 ND 10/14/2020 36 <1 <1 3 6.2 <1 <1 <2 <20 <1 <1 4.7 <1 <1 <1 20 <1 <1 <1 <1 <1 <1 2.5 <2 ND 10/27/2021 106 <1 <1 18 5.2 0.53 J <1 53 <20 <1 <1 2.0 <1 <1 <1 27 <1 <1 <1 <1 <1 <1 1.1 <2 ND 10/13/2022 146 <1 <1 21 6.1 0.61 J <1 83 <20 <1 <1 3.9 <1 <1 <1 29 <1 1.0 <1 <1 <1 <1 1.2 <3 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 12 of 15 n v; Sample O N a Sample I.D. H b q b 3 n 0 Date :3 0 0 0 0 n 3- 0 3• n m 6 0 n 0 C ,G Q 3' 3' 3' 3' S 0 M 0 3' O O O O O O O O A y 0 O S 0 O `G fD O O O 7 S A O O O O O D W n a O O O a 0O O O 0y p N fD O _G 0 M fD 3 M (D .O. fD O 3 M O ( M 3 C O 3' S 3' 3' 3' -a K N O N S �+ S 3' N O O O y D) 3 D) 3 N 3 M 3 a) 3 D) 3 D) 3 O 3 fD 3 CL N 7 N 7 c) 3 N 3 M 7 7 CL M 3 M 3 N 7 M 3 3 Q 2) n 3 (D M N M N M M M M M M M M N M CD M M N M N U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-15S 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 11 <5 <5 <5 <5 <5 <5 11.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 25 <5 <5 <5 <5 <5 <5 24.6 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/25/2007 1.5 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 78 <1.0 <1.0 1 18.6 4.8 <1.0 <1.0 1 6.6 13.4 1 <1.0 <1.0 <1.0 1 4.5 <1.0 <1.0 26.5 <1.0 1 3.9 <1.0 <1.0 <1.0 <1.0 I <1.0 <2.0 ND PW-16D 7/22/1998 786 ND 130 ND 6.0 87.0 ND 7.0 380 140 ND 3 J ND 6.0 16.0 ND 11.0 11/2/2000 1,610 <120 <120 210 <120 <120 <120 <2,500 <120 1,400 <250 <120 <120 <120 <120 <120 <120 <120 <120 <250 <250 ND 9/6/2001 4,184 10.6 <5 355 12.3 8.9 <5 788 <10 29.3 2,580 250 <5 71.5 <5 22.7 <5 <5 <5 <5 55.2 <5 ND 9/17/2003 4,324 <100 <100 501 <100 <100 <100 858 <200 <100 2,680 <200 <100 285 <100 <100 <100 <100 <100 <100 <200 <100 ND 8/19/2004 2,722 <50 <50 353 <50 <50 <50 729 <100 <50 1,200 119 <50 215 <50 <50 <50 <50 <50 <50 106 <50 ND 8/29/2006 4,357 71.8 <10 732 178 31.5 <10 889 <50 31.1 1,370 78 <10 709 <10 <10 <10 <10 <10 <10 266 <20 ND 9/25/2007 5,130 <20 <20 844 247 36.5 <20 882 <100 36.8 1,700 75.5 <20 957 <20 <20 <20 <20 <20 <20 351 <40 ND 3/11/2009 6,570 110 1.5 1,160 372 50.5 <1.0 890 15.9 42.6 <1.0 1,950 93.5 <1.0 <1.0 1,400 <1.0 4.9 11.1 3.4 4.2 4.5 442 10.5 3.3 3/30/2010 6,295 88.2 <1.0 1,180 329 48.2 <1.0 1,080 27.2 39.9 <1.0 1,780 80.8 <1.0 <1.0 1,240 <1.0 4.85 4.97 1.50 3.03 3.59 384 ND ND 11/7/2011 7,345 232.0 <5 1,380 732 62.5 <5 260 <50 55.9 <5 1,770 405 <5 <5 1,740 <5 <5 <5 <5 <5 11.7 655 7.9 8.0 11/26/2012 7,820 165 1.01 1,090 543 50.4 0.52 1,260 <5 48.7 <0.5 2,100 229 <0.5 <0.5 1,680 <0.5 4.57 8.59 3.30 6.72 5.5 601 <0.5 23.1 12/12/2013 7,988 251 <5 1,360 688 65.9 <5 1,330 <50 55.2 37 1,870 245 <5 <5 1,700 <5 <5 <5 <5 <5 <5 368 5.7 12.0 12/9/2014 6,745 180 <20 920 490 60 <20 1,150 <100 36 <20 1,900 150 <20 <20 1,500 <20 <20 9.2 <20 <20 <20 350 <60 ND 10/28/2015 3,527 51 <20 480 190 18 <20 772 <100 22 <20 1,000 44 <20 <20 790 <20 <20 <20 <20 <20 <20 160 <60 ND 11/15/2016 2,461 46 <10 390 180 23 <10 650 <200 12 <10 520 <10 <10 <10 540 <10 <10 3.2 J <10 <10 2.1 J 100 <30 ND 10/12/2017 4 <1 <1 1.5 J 0.47 J <1 <1 3.9 J 13 J <1 <1 2.4 J <1 <1 <1 2.5 J <1 <1 <1 <1 <1 <1 0.66 J <3 ND 11/29/2017 2,284 21 <5 340 76 16 <5 870 <100 14 <5 490 14 <5 <5 370 <5 <5 2.4 J <5 <5 <5 73 <15 ND 11/5/2018 195 1.5 <1 40 12 0.96 J <1 84 <20 <1 <1 2.3 <1 <1 <1 53 <1 <1 <1 <1 <1 0.46 J 1.8 <3 ND 9/17/2019 99 0.51 J <1 20 4.5 <1 <1 28 <20 0.45 J <1 22 3.3 <1 <1 20 <1 <1 <1 <1 <1 <1 1.3 <3 ND 10/14/2020 68 <1 <1 4.6 9.1 <1 <1 <2 <20 <1 <1 17 1.2 <1 <1 30 <1 <1 <1 <1 <1 <1 5.8 <2 ND 10/27/2021 127 <1 <1 20.0 7.1 <1 <1 23 <20 <1 <1 40 1.5 <1 <1 32 <1 <1 <1 <1 <1 <1 3.6 <2 ND 10/13/2022 174 <1 <1 23.0 9.9 0.62 J <1 45 <20 0.7 J <1 50 <1 <1 <1 39 <1 0.53 J <1 <1 <1 <1 5.3 <3 ND PW-16S 7/22/1998 ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 6.5 <1 <1 <1 <1 <1 <1 <2 6.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/26/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND PW-17 11/3/2000 160 <5 <5 <5 <5 <5 <5 160 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 8.8 <1 <1 <1 <1 <1 <1 <2 8.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 6.3 <1 <1 <1 <1 <1 <1 <2 6.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 13 of 15 n v; Sample Sample I.D. H b q b c� c� b =r b Date 3 0 0 0 0 F 3• n c, m m 0 0 0 Q 3' 3' 3' 3' 3' 0 0 3' O =r 3 = 3' 3' 3' 3 O O O O O O O A y 0 O S 0 O `G fD O O O 3 S A O O O O O � D W 0 a O O O a n O -4 O O n y p N fD (D O _G 0 O =r fD (D � .O. fD O 3 M O ( M 3' O x S S S S S -a x .r N O N =r �+ O S S N O 3' C 3' S O O O w 01 3 0) 3 O 3 m 3 2) 3 d 3 a)O 3 3 CD 3 0: m 3 m 3 3 m 3 m 3 CL CD 3 M 3 m 3 CD 3 3 CL a� 0 fD M N M N N CD M M M M M M M M (D M M N CD M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-18 11/7/2000 19 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 19.0 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/11/2001 24 <5 <5 <5 <5 <5 <5 <10 24.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 204 <5 <5 <5 <5 <5 <5 <10 195 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.9 ND 8/19/2004 149 <5 <5 <5 <5 <5 <5 22.8 119 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 6.8 ND 10/1/2004 27 <5 <5 <5 <5 <5 <5 <10 27.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 264 <1 <1 <1 <1 <1 <1 <2 151 <1 <1 <1 < <1 1.7 <1 <1 1.2 <1 <1 <1 16.3 93.8 9/26/2007 194 <1 <1 <1 <1 <1 <1 <2 108 <1 <1 <1 < <1 1.3 <1 <1 1.2 <1 <1 <1 12.0 71.1 3/12/2009 203 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 125 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 3.5 <1.0 <1.0 <1.0 <1.0 <1.0 9.8 63.7 3/31/2010 86 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 85.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 143 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 92.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.94 48.43 11 /26/2012 91 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 36.0 30.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.86 <0.5 <0.5 0.6 <0.5 <0.5 <0.5 6.73 24.5 1/21/2013 ND <2.0 12/12/2013 31 <5 <5 <5 <5 <5 <0.5 5.05 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 25.6 2/25/2014 ND <2 12/9/2014 96 <1 <1 <1 <1 <1 <1 9.17 55 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1 <1 <1 <1 6 30.7 1/29/2015 58 <1 <1 <1 <1 <1 <1 <2 35 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.9 18 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 40 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.65 J <1 <1 <1 1.2 J 19 11/15/2016 ND <10 <10 <10 <10 <10 <10 <10 <200 <10 <10 <10 <10 8.3 J <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND 10/16/2017 ND <1 <1 <1 <1 <1 <1 <2 20 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 6.7 J 11/7/20018 35 <1 <1 0.65 J 0.91 J <1 <1 <2 20 <1 <1 0.42 J <1 <1 <1 2.8 <1 <1 <1 <1 <1 1.3 <1 0.58 J 7.3 1/10/2019 24 J <1 <1 0.65 J <1 <1 <1 <2 17 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.3 J 5.2 J 9/17/2019 Not Sampled 10/14/2020 Not Sampled 10/27/2021 Not Sampled PW-19 11/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 98 <5 <5 <5 <5 <5 <5 97.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/1/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 3.7 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 3.7 9/27/2007 5.0 <1 <1 <1 <1 <1 <1 <2 5.0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 91 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 87.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 1/29/2015 <1 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.57 J <1 <3 ND PW-DR-1 9/8/2004 248 <5 <5 10.7 <5 <5 <5 164 <10 <5 40.2 16.6 <5 16.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 9/23/2004 268 <5 <5 5.6 <5 <5 <5 209 <10 <5 31.3 13.6 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/8/2004 249 <5 <5 5.6 <5 <5 <5 213 <10 <5 30.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/25/2009 1,848 54.4 <1.0 213 98.8 7.7 <1.0 579 7.5 11.8 <1.0 400 58.3 <1.0 <1.0 314 2.2 <1.0 3.5 23.8 1.2 1.3 <1.0 71.2 ND PW-SIS1 8/25/2004 12,848 201 <5 3,370 765 223 <5 2,500 <10 69.5 39.0 <10 <5 5,060 <5 110 49.9 <5 <5 69.8 376 15.1 ND 3/9/2009 9,940 473 3.7 1,990 1,310 139 1.4 1,230 37.7 97.4 <1.0 68.1 38.8 3.7 <1.0 3,510 1 <1.0 6.0 121 3.2 49.0 263 555 39.9 ND W-1 1/29/1997 3 ND ND ND ND ND ND ND ND ND ND ND 3 J NA ND ND ND ND ND ND ND ND ND 9/27/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 <5 <5 <5 <5 <5 <5 12.4 <10 <5 <5 <10 <5 <5 <5 <5 8.4 <5 <5 <5 <10 <5 ND 9/18/2002 20 <5 <5 <5 <5 <5 <5 11.5 <10 <5 <5 <10 <5 <5 <5 <5 8.2 <5 <5 <5 <10 <5 ND 9/17/2003 86 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 76.4 <5 <5 9.7 <10 <5 ND 8/17/2004 43 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 33.7 <5 <5 9.3 <10 <5 ND 3/3/2009 25 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <2.0 7.7 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0 11.1 <1.0 <1.0 1.9 <1.0 <2.0 ND W-2 1/30/1997 87,240 30,000 ND 12,000 11,000 960 J ND ND 2,200 J 410 J ND ND 1,500 J ND ND ND 20,000 970 J 1,200 ND 1,200 5,300 500 J ND DUP-3(W-2) 1/28/1997 79,260 27,000 ND 11,000 9,500 930 J ND ND 2,300 J 410 J ND ND 1,400 J ND ND ND 19,000 910 1 1,200 ND 1,100 4,300 210 J ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 14 of 15 O N n v; Sample H a 0 CD Sample I.D. Date 3 0 n b n q n b n 0 3• 3 � 0 s 0 3• b n n n . n C Q 3' 3' 3' 3' 3'0 p 3' n O 3' m 6 ,C fD O O O O O O A y p O 3' p O `G fD O O O 3 S A O O O O O � D W n a O O O a n O -4 O O n y 0 N fD (D O _G n O 3 fD ( 0 .O. fD O S_ O O ( M 3 C O y 3' 0) 3' 0) 0) M 0) -a 0) a) 0) .r O N fD O N fD 3' 0) �+ 3' 0) 3' fD N fD O 7 3' lD C M 3' fD 3' lD O M. O O 3 3 3 3 3 3 3 3 CL > > 3 3 O CL 3 3 7 3 m 0 fD M fD M fD fD CD M fD M fD fD fD fD fD CD CD M fD M (D U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 W-4 2/6/1997 1,624 47.0 ND 640 86.0 23 J ND ND 6 J 30.0 8 J 35 J ND NA 7 J ND ND 7 J ND ND 280 5 J 450 9/27/2000 525 14.0 <5 200 57.0 8.4 <5 <100 NA 8.7 <5 <10 <5 170 <5 <5 <5 <5 6.7 <5 60.0 <10 ND 9/10/2001 49 <5 32.7 <5 <5 <5 <5 16.5 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2002 18 <5 <5 <5 <5 <5 <5 18.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 694 27.9 <5 135 56.9 10.9 <5 162 <10 <5 <5 <10 <5 248 <5 <5 <5 <5 <5 8.1 45.2 <5 ND 8/17/2004 3,157 136 <10 432 331 35.2 <10 547 <20 17.0 14.5 <20 <10 1,010 <10 <10 13.0 <10 <10 10.4 91.2 <10 ND W-4A 1/28/1997 75,370 13,000 ND 11,000 5,700 540 ND ND ND 890 J ND ND ND NA ND 39,000 ND 1,300 ND ND 2,600 280 J 1,060 9/27/2000 15,940 380 <5 4,300 1,500 160 <5 2,100 NA 230 67 50 <5 4,500 12.0 1,300 38.0 57 260 42.0 870 66.0 8.3 9/10/2001 37,215 619 <5 10,400 3,560 316 <5 2,770 <10 <5 125 111 <5 12,400 40.4 4,350 52.6 126 19.3 43.8 2,100 169 13.1 9/17/2002 31,439 515 <5 9,120 2,490 207 <5 1,950 <10 273 105 95.7 <5 10,500 24.4 3,570 38.5 59.4 10.9 28.5 2,330 122 ND 9/17/2003 5,351 83 <5 1,350 544 68.1 <5 1,090 <10 73 29.1 18.5 <5 1,740 <5 <5 16.8 15.1 <5 16 286 22.4 ND 8/17/2004 19,357 <100 <100 5,390 2,070 182 <100 1,870 <200 225 111 <100 <100 7,330 <100 831 <100 <100 <100 <100 1,230 118 ND 2/27/2009 6,307 73.4 <1.0 1,240 541 57.9 <1.0 942 13.4 98.4 <1.0 67.4 163 <1.0 3.3 2,260 7.3 78.8 8.3 11.3 6.5 12 686 36.8 ND 3/31/2010 10,920 401 <1.0 1,880 995 73.6 1.19 1,010 32.7 129 <1.0 91.9 238 <1.0 1.98 3,590 16.1 918 43.5 72.5 6.26 89 1,330 ND ND 11/2/2011 41,390 216 <50 5,340 3,750 363 <50 520 <500 861 <50 469 7,290 <50 <50 10,300 <50 1,130 <50 307 <50 83 11,000 281 ND 11/19/2012 4,144 28.7 <0.5 335 296 21.9 <0.5 1,600 <5 65.3 3.77 30 241 <0.5 0.95 693 3.28 155 1.48 16 2.87 4.27 622 20.11 3.74 12/17/2013 59,696 513 <50 7,580 3,260 318 <50 1,270 <500 843 <50 332 6,790 <50 <50 14,400 <50 15,300 <50 249 <50 <50 8,580 261 ND 12/8/2014 37,661 430 <100 4,700 2,700 360 <100 2,100 <100 560 <100 270 3,600 <100 <100 8,800 <100 6,300 <100 220 41 140 7,000 220 220 10/27/2015 8,952 270 <100 1,400 640 <100 <100 962 <500 210 <100 110 540 <100 <100 2,500 <100 <100 <100 120 <100 76 J 2,200 <300 ND 11/16/2016 9,410 380 <100 2,000 690 67 <100 660 <2000 260 <100 140 560 <100 <100 2,400 <100 220 <100 72 J <100 92 J 2,100 <300 ND 10/11/2017 2,832 24 <10 440 190 36 <10 630 <200 40 <10 39 66 <10 <10 570 <10 <10 4.3 J <10 <10 5.3 780 12 ND 10/31/2018 1,400 33 <5 260 110 7.6 <5 210 <100 14 <5 11 30 <5 <5 500 <5 <5 3.4 J <5 2.4 J 28 190 <15 ND 9/11/2019 435 12 <1 83 33 2.8 <1 54 <20 7.5 <1 4.4 13 <1 <1 130 <1 0.45 J 0.81 J <1 1.3 6 88 <3 ND 10/9/2020 344 13 <2 74 35 2.3 <2 30 <40 3.1 <2 6.7 4 <2 <2 120 <2 <2 <2 1.7 J 0.88 J 5.5 50 <4 ND 10/27/2021 513 24 <5 110 43 2.8 <5 54 <100 6.6 <5 <5 4.5 J <5 <5 170 <5 <5 <5 <5 <5 <5 98 <15 ND 10/18/2022 125 5.2 <1 31 8.8 0.93 J <1 10 <20 0.99 J <1 3.9 <1 <1 <1 34 <1 1.1 1.2 <1 0.51 J 2.1 25 <3 ND W-4B 2/4/1997 117,470 20,000 ND 13,000 8,700 810 J ND ND 4,500 J 1,200 J ND ND ND ND ND ND 61,000 550 J 2,800 ND ND 4,200 710 J ND W-5 8/7/1996 467,000 110,000 ND 27,000 21,000 ND ND 19,000 2,100 J 1,700 9,400 J ND ND ND 140,000 6,900 13,000 ND ND 36,000 3,900 J 77,000 2/24/1997 415,300 98,000 ND 26,000 19,000 2,000 ND ND 34,000 2,200 J 1,800 9,100 J ND ND 1,100 J 130,000 5,600 15,000 ND 24,000 33,000 5,200 9,300 10/30/2000 402,208 95,000 91.0 22,000 31,000 1,100 17.0 24,000 NA 1,000 1,200 2,200 190 72,000 760 100,000 3,500 8,900 340 11,000 25,000 2,540 370 9/10/2001 378,680 144,000 <5 14,000 33,300 <5 <5 13,800 <10 <5 <5 <10 <5 53,900 <5 63,200 7,710 9,270 <5 27,000 12,500 <5 ND 9/19/2002 672,790 121,000 <5,000 45,400 122,000 <5,000 <5,000 14,300 <10,000 7,780 11,100 <10,000 <5,000 74,300 5,880 93,100 28,900 35,300 <5,000 38,300 39,500 28,400 7,530 9/17/2003 367,940 135,000 <5,000 9,220 31,800 <5,000 <5,000 11,300 <10,000 <5,000 <5,000 <10,000 <5,000 56,400 <5,000 81,900 6,340 7,580 <5,000 28,400 <10,000 <5,000 ND 8/18/2004 375,700 177,000 <5000 5,290 36,600 <5000 <5,000 4,110 <10,000 <5,000 <5,000 <10,000 <5,000 41,400 <5,000 48,900 10,800 10,400 <5,000 41,200 <10,000 <5,000 ND 3/3/2009 170,238 66,700 75.8 3,720 15,500 289 <50.OX 1,860 1,380 1,420 <50 1,000 111 121 <50.OX 30,800 <50.OX 10,900 3,700 3,400 70.0 25,900 1,040 1,940 311.0 W-6 2/5/1997 123,360 23,000 ND 14,000 8,500 20,000 ND ND 3,400 J ND ND 15,000 ND ND ND ND 260 J 19,000 2,700 3,000 ND 2,400 5,100 1,400 2,800 DUP-1 (W-6 8/7/1996 143,900 27,000 ND 16,000 10,000 23,000 ND 2,800 ND ND 18,000 ND ND ND ND ND 21,000 6,200 3,300 ND 4,000 6,500 1,600 4,500 W-6A 2/5/1997 739,000 10,000 ND 65,000 16,000 48,000 ND ND 150,000 ND 21,000 ND ND ND ND 310,000 3,200 J 12,000 ND ND 6,800 J ND 97,000 9/28/2000 838,040 31,000 280 69,000 24,000 71,000 <5 81,000 <5 17,000 940 160 100,000 550 410,000 3,200 14,000 660 3,100 9,900 1,950 300 W-66 2/5/1997 238,400 59,000 ND 23,000 14,000 19,000 ND ND 14,000 ND ND 18,000 ND ND ND ND 55,000 4,700 5,700 ND 11,000 1,000 J 1,000 J 13,000 W-13A 1/31/1997 1,688 66.0 ND 230 110 6 J ND 990 120 ND ND ND 5J ND ND ND 27.0 90 ND ND 30 14J ND ND W-18 2/3/1997 6,781 500 ND 820 930 960 ND ND ND ND ND ND ND 71 J ND ND 610 1,500 ND ND 930 460 ND ND 3/5/2009 9,932 60.0 3 741 396 17.4 <1.0 1,350 19.5 9.9 7.2 4.4 11.7 77.9 <1.0 4,050 <1.0 7.2 490 <1.0 1 13.5 1,850 819 3.8 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 15of15 n v; Sample O N a M Sample I.D. H b q b 0 3 n 0 b . Date 3 0 0 0 0 n 3• � 3- 0 3• n m 6 0 0 0 C ,C Q 3' 3' 3' 3' S 0 M 0 3' O =r 3 3 3' 3' 3' 3 O O O O O O A y 0 O S 0 O `G CD O O O 3 S A O O O O O D W n a O O O Cr 0O O O 0y p N fD O _G 0 M O 3 M M .O. O O 3 M O M M 3 C O 3' S 3' 3' 3' 0 �( N O N S �+ S 3' N O O O y D) 3 D) 3 C) 3 M 3 C) 3 D) 3 D) 3 O 3 fD 3 CL N 7 N 7 C) 3 N 3 M 7 7 Q. M 3 M 3 N 7 M 3 Q m 0 3 CD fD M N M N N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 0.6 6 350 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 W-20 1/31/1997 19.0 4 J ND 4 J 4 J ND ND ND ND ND ND ND ND ND ND ND ND 5 ND ND 2 J ND ND ND W-21 1/31/1997 1,232 340 ND 130 210 110 ND 240 J ND ND ND 18 J 3 J ND ND 3 J 47.0 ND ND 54.0 77.0 ND ND 9/28/2000 1,494 190 <5 120 140 74.0 <5 520 NA <5 <5 <10 <5 220 <5 <5 97.0 <5 <5 73.0 60.0 <10 ND 9/10/2001 1,336 129 <5 101 140 57.8 <5 407 <10 <5 <5 <10 <5 271 <5 <5 116 <5 <5 72.7 41.4 <5 ND 9/17/2002 1,775 127 <5 188 163 36.2 <5 458 <10 5.2 <5 <10 <5 498 <5 <5 102 <5 <5 98.0 100 <5 ND 9/17/2003 1,890 106 <5 140 151 44.6 <5 743 <10 <5 <5 <10 <5 384 <5 <5 140 <5 <5 105 76.7 <5 ND 8/17/2004 1,761 71.2 <10 114 124 47.4 <10 821 <20 <10 <10 <20 <10 333 <10 <10 95.2 <10 <10 81.5 73.5 <10 ND 9/24/2009 3,701 313 1.2 1 518 390 38.9 1 <1.0 678 1 16.0 12.6 <1.0 1 9.8 4.9 5.3 <1.0 1,210 1 <1.0 <1.0 108 <1.0 1 3.3 170 222 1 <2.0 ND W-23A 1/30/1997 4,600 ND ND ND ND ND ND ND 4,600 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/4/2009 115 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 106 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 3.1 <1.0 <1.0 2.6 <1.0 <2.0 ND W-23B 1/22/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-24 1/31/1997 2,109 200 ND 190 330 ND ND ND ND ND ND ND ND 11 J ND ND 54 440 ND ND 710 160 14 J ND UP-2 (W-2 1/31/1997 1,921 180 ND 180 310 ND ND ND ND ND ND ND ND 10 J ND ND 49 400 ND ND 630 150 12 J ND 7/16/1998 1,943 ND 100 J 160 240 D ND ND ND ND 3 J ND ND ND 8 ND ND 12 520 D ND ND 690 D 190 20.0 ND W-25 8/7/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-29 2/5/1997 1,688,000 120,000 ND 7,400 J 29,000 580,000 ND ND 240,000 ND ND 49,000 ND ND ND ND 290,000 13,000 J 10,000 J ND 150,000 ND ND 230,000 BD-1 3/29/2010 235 <1.0 <1.0 14.7 <1.0 <1.0 <5.0 208 <5.0 <1.0 <1.0 1.74 2.28 <1.0 <1.0 5.72 <1.0 1.48 <1.0 <1.0 <1.0 <1.0 1.34 ND ND DUP-02 3/31/2010 148 <1.0 <1.0 31.0 1.60 3.45 <1.0 28.6 <5.0 <1.0 <1.0 35.4 9.90 <1.0 <1.0 24.1 <1.0 2.00 1.55 <1.0 <1.0 2.87 7.67 ND ND LCHT-COMP 3/30/2010 904 <2.0 <2.0 82.2 34.4 8.87 <2.0 416 32.4 8.00 <2.0 136 24.7 <2.0 <2.0 95.8 2.60 5.09 <2.0 6.24 <2.0 6.69 44.9 ND ND PW-SF1 4/2/2010 11,985 <2.0 <2.0 114 <2.0 <2.0 <2.0 8,410 247 20 <2.0 1,190 1,340 <2.0 <2.0 2.4 11 175 <2.0 447 4 <2.0 25 ND ND 11/3/2011 34,627 1,840 32.6 2,990 3,670 1,240 <5 1,300 57.2 32.5 <5 1,450 1,580 250 <5 13,100 <5 251 211 1,070 23.3 1,410 3,920 54.0 145.7 11/20/2012 8,577 136 <50 480 5.7 135 <50 4,310 <500 <50 <50 298 <50 <50 <50 2,230 <50 <50 <50 110 <50 123 749 <50 ND 12/9/2013 46,400 1,250 <50 3,700 6,190 1,060 <50 3,940 <500 <50 <50 1,710 1,130 276 19,900 <50 <50 <50 700 <50 1,470 4,920 <100 154 12/8/2014 43,302 1,100 <200 3,500 4,200 1,300 <200 3,510 <1000 <200 <200 2,000 1,200 200 <200 19,000 <200 <200 320 680 <200 1,700 4,500 <600 92 10/27/2015 41,479 1,100 <100 3,200 3,600 780 <100 3,550 <500 <100 <100 2,100 790 160 <100 18,000 <100 <100 420 800 <100 2,200 4,700 <300 79 J 11/17/2016 48,530 1,800 <500 4,400 4,900 780 <500 3,600 <10000 <500 <500 2,200 450 J 280 J <500 22,000 <500 <500 660 690 <500 2,800 4,700 <1500 ND 10/11/2017 43,254 1,300 <100 3,900 4,000 880 <100 3,600 <2000 <100 <100 1,900 340 180 <100 19,000 <100 <100 650 530 <100 2,900 4,000 43 J 74 10/30/2018 40,063 1,200 <100 3,400 3,600 660 <100 2,800 <2000 <100 <100 2,100 <100 110 <100 18,000 <100 <100 680 660 <100 3,100 3,600 45 J 63 J 9/10/2019 43,240 3,100 <200 3,500 4,100 600 <200 3,200 <4000 <200 <200 1,800 <200 120 <200 20,000 <200 160 830 530 <200 2,900 2,400 <600 ND 10/9/2020 42,870 130 J <200 6,400 4,300 <200 <200 2,400 <4000 <200 <200 1,900 970 <200 <200 14,000 <200 260 <200 640 <200 <200 12,000 <600 ND 10/27/2021 61,780 3,300 <500 6,200 5,300 <500 <500 2,300 <10000 <500 <500 2,100 <500 <500 <500 38,000 <500 260 J <500 720 <500 <500 3,200 <1500 400 10/18/2022 160,420 25,000 <1000 15,000 12,000 3,100 <1000 6,900 <20000 <1000 <1000 22,000 1,300 <1000 <1000 39,000 <1000 5,800 4,500 5,100 <1000 2,100 11,000 710 6,200 EB-1 4/2/2010 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 15.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND FB-1 4/2/2010 25 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 21.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.55 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND Grutchtleld (potable well 12/1/1998' ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <2.0 <0.5 <0.5 <0.5 <2.0 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 ND 3/11/2009 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND ug/1= micrograms per liter J = Estimated Value ND = Not Detected NA - Not Analyzed Bold type indicates value exceeds NC 2L ground water standard TABLE3 SURFACE WATER ANALY17CAL RESULTS - VOCs SEABOARD CHEMICWRIVERDALE DRIVE LANDFILL SITE I= G S 3 y S o o o - o o o F _ 5 Sample ID Sample Date _ - _ o = � ? - o m u/I u/I u/l u/l u/I u/I u/I u/I u/I u/I u/I u/I u/I) (uA) (u/I u/I u/I NC 2B Std. S 2500 6 300 9.90 0.35 3100 1.19 488 NE 3 60 11000 0.7 11 290 2.5 0.025 6200 20000 NOMam Imam meM Stream SW-1 4/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 15 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/15/2002 Dry -- -- -- -- -- -- -- -- ND -- -- -- -- -- -- -- -- -- 9/16/2003 <5 <5 <5 <5 <10 <10 <6 <5 <10 ND <5 <5 <5 <6 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 Dry -- -- -- -- -- -- -- -- -- -- -- .. .. .. .. .. .. .. 8/29/2006 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 9/27/2007 Dry -- -- -- -- -- -- -- -- .. .. .. .. .. .. .. .. .. .. 5/13/2009 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 12/1312013 Dry .. .. .. .. .. .. .. .. 12/8/2014 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 10/22/2015 Dry .. .. .. .. .. .. .. .. 11/17/2016 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 2/1/2017 Dry .. .. .. .. .. .. .. .. 10/13/2017 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 11/29/2017 Dry .. .. .. .. .. .. .. .. 11/7/2018 <1 <1 <i <i 12 120 <7 <1 <1 <1 <i <1 <i <i <i <i <i <3 <5 1/10/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry 10/19/2022 Dry SW-2 4/30/1997 ND ND ND ND ND ND 3J 8 ND ND ND ND ND ND ND ND ND ND ND 7/15/1998 ND ND ND ND ND ND 6 12 ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 420 NA <5 10 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 353 <10 <5 7.6 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 258 <10 <5 7.7 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 293 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 305 <10 <5 9.6 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/16/2004 <5 <5 <5 <5 233 <10 <5 8.7 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 64 14.7 <5 6.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 218 <5 <1 9.1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Spld (8270) 8/29/2006 NA NA NA NA 390 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 176 <5 <1 9.4 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 <1 <7 <1 ,1 17.1 7.1 <7 3.8 <7 <7 <1 <1 <1 <1 <1 <1 <1 <1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 <0.5 <0.5 <0.5 <0.5 6.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 Dry -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- .. .. .. .. .. .. .. .. 12/8/2014 Dry -- -- -- - -- -- -- -- -- -- -- -- -- -- -- -- -- 0/2 2/2 ry .. _ .. .. .. .. .. .. .. .. .. .. .. .. .. .. 11/17/2016 Dry -- -- -- - -- -- -- -- -- -- -- -- -- -- -- -- -- -- 2/j/2017 Dry .. .. .. .. .. .. .. .. 10/13/2017 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 .. .. .. .. .. .. .. .. 11/7/2018 <i <i <i <i 22 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 1/10/2019 <1 <1 <1 <1 15 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 15 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry 10/19/2022 <1 <1 <1 <1 14 -0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 South- Intermittent SW-3 4/30/1997 66 73 33 6 ND ND 3J ND SJ ND ND 110 4J 4J ND 21 19 ND ND 7/15/1998 ND 5 ND ND NA ND ND ND ND ND 4J ND ND ND ND ND ND ND ND 11/2/2000 24 38 14 <5 600 B NA <5 <5 <10 ND 45 10 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 281 <10 <5 <5 <10 ND <5 <5 <5 <6 <5 <5 <10 <5 ND 9/24/2002 <5 14.6 5.1 <5 69.7 <10 <5 <5 <10 ND 17.0 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 151 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/1 2003 13 42.4 16.8 <5 202 <10 <5 <5 <10 ND 50.4 7.2 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 13.3 <5 <5 546 <10 <5 8.7 16.4 ND 6.9 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 31.7 9 <5 115 <10 <5 <5 <10 ND 33.6 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 39.1 96.3 50 <5 26.3 <10 <6 <5 <10 ND 182 111 <5 <5 <5 <5 20.7 <5 <10 8/29/2006 11.8 59.3 24 3.5 327 <5 <1 <1 3.2 ND 88.6 5.2 1.1 <1 <1 1.7 7.4 <2 ND SW-3A 8/25/2004 23.8 85.4 26 <5 182 <10 <5 <5 <10 87.2 7.7 <5 <5 <5 5.8 31.2 <5 <10 SW-3B 8/25/2004 <5 <5 <5 <5 84 <10 <5 <5 <10 19.1 <5 5.3 <5 <5 7.7 <10 <5 <10 SW-108 11/2/2000 14 26 10 <6 330 NA <5 <5 <10 30 5.8 <5 <5 <5 <5 <10 <10 ND nd split of SW-3) 9/27/2007 Dry -- -- -- -- -- -- -- -- .. .. .. .. .. .. .. .. .. .. 5/13/2009 32.3 84.1 52.4 4.1 144 10.2 2.5 1.4 10.5 <1 178 7.6 2.1 <1.0 <1.0 7.8 28.5 <1 <5 4/1/2010 21.7 52.6 36.6 <1.0 66.9 8.01 1.69 1.01 11.2 <1.0 127 51 1.32 <1.0 <1.0 5.68 23.7 ND <5.0 11/3/2011 20.6 37.3 24 1.58 38 <5 <0.5 <0.5 19.9 <0.5 76.5 4.79 <0.5 <0.5 <0.5 10.6 25 <0.5 <5 11/20/2012 27.1 50.7 29.3 <0.5 115 <5 <0.5 0.62 19 <0.5 105 1.31 2.62 <0.5 0.58 14 23.2 <0.5 <5 12/11/2013 28.7 26.6 33.2 0.74 10 <5 1.83 0.73 10.4 <0.5 85.1 <0.5 1.4 <0.5 0.75 14.6 18.8 <0.5 <5 12/8/2014 8.2 22 10 <1 96.8 <5 <1 <1 8.8 <1 42 15 1.2 <1 <1 4.8 11 13 <5 10/22/2115 27 81 37 2.7 104 <5 1.181 <1 24 <1 140 81 4.8 <1 1.171 19 28 <3 <5 11/17/2016 <7 <1 <7 <1 16 28J <7 <7 <1 <7 0.44J <1 <7 <7 <7 <1 <1 <3 <5 2112017 NA NA NA NA 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 <7 <1 <7 <1 9.7J <20 <7 <1 <1 <7 <7 <1 <7 <7 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 15 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 1.2 <1 <1 13 <20 <7 <7 <1 <7 2.3 <1 <7 <7 <7 <1 <7 <3 <5 9/18/2019 <i <i <i <i 1.7 120 <7 <7 <i <7 <7 <i <7 <7 <7 <i <i <3 <i <1 0.69 J <1 <1 3.9 <20 <7 <1 <1 <7 1.6 <7 <7 <7 <7 <7 <7 <2 <1 10/22/2020 0/21/2021 0.951 2.1 <7 <7 4.6 120 <7 <i <i <7 2.6 <7 <7 <7 <7 <7 <7 <2 <i 10/19/2022 <1 0.88J <1 <1 2.1 <20 <7 <1 <1 <7 1.2 <1 <7 <7 <1 <1 <7 <3 <5 TABLE3 SURFACE WATER ANALY17CAL RESULTS -VOCa SEABOARD CHEMICWRIVERDALE DRIVE LANDFILL SITE 12=1 G S 3 y S o o D - D o o F _ 5 Sample ID Sample Date _ _ _ ii = C = ? Q _ o u 3 R z a 1 u /l Ng/I (, IQ ( u il Ng/I u n NCO) u n u /I u l NCO) u /I u n u 9 u 9 NAM u l u l u l ND 2B Std. 5 2500 6 300 9.90 0.35 3100 1.19 488 NE 3 80 11000 0.7 11 290 2.5 0.025 6200 20000 SW-4 4/30/1997 4J/5J 30/34 3J/3J 3J/4J ND/ND 12J/23J 1J/1J 62/69 15J/16J ND ND/ND 10/11 ND/ND ND/ND ND/ND ND/ND 8J/9J ND/ND ND/ND 7/20/1998 ND 16 ND 4J NA ND ND 77 36 ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 1100B NA <5 48 34 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 806 <10 <5 16.5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 480 <10 <5 19.3 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 448 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 7.7 <5 <5 118 11 <5 12.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 592 <10 <5 38.0 18.2 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 6.4 24.9 7.3 <5 172 17.3 <5 22.4 <10 ND 36.5 5.8 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 1.2 <1 <1 1040 <5 <1 9.5 8.1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Split (8270) 8/29/2006 NA NA NA NA 1200 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 24.1 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 <1 <1 <l 0 8.4 8.4 <l <1 <1 1.7 <l <1 <l <l <1 <1 <1 <1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 72 443 126 32.6 110 10.6 14.2 368 141 <0.5 440 1.21 3.24 0.74 <0.5 13.5 371 4.93 <5 11/20/2012 <0.5 2.1 <0.5 <0.5 22.7 <5 <0.5 5.9 <0.5 <0.5 1.56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/8/2014 <1 <1 <1 <1 3.3 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 10/22/2015 <1 <1 <1 <1 4.1 J <5 <1 0.82 J <1 <1 <1 <1 <1 <1 <1 <1 <1 13 <5 11/21/2016 <1 <1 <1 <1 18 <10 <1 1.3J 0.70J <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA <2.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 86 710 280 63 1700 1200 20 840 120 <10 1100 <10 6.7 J 4.8 J 4.3 J 4.1 J 1000 9.1 <50 11/29/2017 120 770 370 58 1500 <200 24 960 65 <10 1400 <10 15 6.7 4.1 22 970 14 <50 11/7/2018 <1 25 13 2.5 48 120 <1 23 2.4 <1 40 <1 <1 <1 <1 <1 45 <3 <5 9/18/2019 51 400 120 34 1800 <200 <10 820 260 <10 540 <10 4.4 4.9 J 7.1 J <1 420 7.7 J <50 10/22/2020 7.7 52 27 4.7 79 120 0.41 J 6 6.6 <1 100 <1 1 <1 <1 <1 73 0.47 J <5 10/21/2021 170 1100 670 120 1500 <20 0.41 J 1700 100 <1 3300 <1 18 11 <1 <1 1500 <1 <5 10/19/2022 1.4 12 4.2 1.1 14 120 <1 1.8 <1 <1 18 <1 <1 <1 <1 <1 19 <3 <5 SW-5 4/30/1997 ND ND ND ND ND 81 ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 12.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 51.7 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <1 <1 12 <5 <1 <1 <1 ND <l <l <l <l <1 <1 <1 <2 ND 5/13/2009 8.7 8.6 6.4 <1 25.4 5.3 <1 <1 <1 <1 39.4 <1 3.3 <1 <1 9.0 8.2 <1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 <0.5 <0.5 <0.5 <0.5 6.97 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/16/2013 <0.5 <0.5 <0.5 <0.5 13.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12/8/2014 <1 <1 <1 <1 2.26 <5 <1 <7 <1 <l <l <1 <1 <1 <1 <1 <1 <3 <5 10/22/2015 <1 <1 <1 <1 1.8 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/17/2016 <1 <1 <1 <1 3.1J <10 <1 <1 <7 <1 <l <l <l <l <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA 8.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 <1 <1 <l <1 14.0 <20 <l <l <1 <l <l <l <1 <1 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 8.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 <1 <7 <l 23.0 <20 <l <l <1 <l <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 <1 <1 <1 <1 5.8 120 <1 <1 <1 <1 0.63 J <1 <1 <1 <1 <1 0.46 J <3 <5 10/22/2020 <1 <l <1 <1 3.5 <20 <l <l <l <l <1 <1 <1 <1 <1 <1 <1 <2 <5 10/21/2021 <1 <1 <1 <1 2.2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 10/19/2022 <1 <l <1 <1 1.6 <20 <l <l <l <1 <1 <1 <1 <1 <1 <1 <1 13 <5 Randleman Lake (formerly the Dae River SW-6 5/l/1997 ND ND ND ND ND 6J ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 11.5 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 133 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 11.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Split(8270) 8/29/2006 NA NA NA NA <3.3 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 8.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 0.0 <1.0 <1.0 <1.0 4.02 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 3.73 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 9.29 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 12 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <1 <1 12 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 12 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 <2 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/l/2017 NA NA NA NA 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 13.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 14.0 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bollom 11/29/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 1V7/2018 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.6J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <t <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <1 <l <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/21/2021 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/20/2022 <1 <l <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/20/2022 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 TABLE3 SURFACE WATER ANALY17CAL RESULTS -VOCa SEABOARD CHEMICWRIVERDALE DRIVE LANDFILL SITE G S 3 y S o o - F _ � Sample ID Sample Date _ _ _ o = e = ? _ e m 3 P, R z a 1 u /I (,oil) u 1 u n (,oil) u n u l u n u /I u l u l u /I u n u n u/1 NAM u l u l u l ND 2B Std. 5 2500 6 300 9.90 0.35 3100 1.19 488 NE 3 80 11000 0.7 11 290 2.5 0.025 6200 20000 SW-7 5/211997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/3/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/13/2001 <5 <5 <5 <5 40.5 <10 <5 <5 23 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 10.7 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 4.3 <5 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9-27-200 <1 <1 <1 <1 23.2 5.0 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 0.0 <1.0 <1.0 <1.0 <2.0 5.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 7.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Surface 4/l/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 11/21/2012 <0.5 <0.5 0.88 <0.5 9.10 <5 <0.5 1.11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 9.88 <5 <0.5 0.94 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 2.38 <5 <1 1.3 <1 <1 0.42J <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 12 <5 <1 1.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <1 <1 1.43J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 1.60 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 27 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 28 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/28/2016 NA NA NA NA 10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 26.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 20.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 8.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 9.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 1117/2018 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 1117/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/21/2021 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/20/2022 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/20/2022 <1 <1 <1 <1 <0.3 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 SW-DRP-2 11/3/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND PAST 9/14/2001 <5 6.3 <5 <5 15.3 <10 <5 5.8 <10 ND 5.7 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 29.5 <5 <5 42.8 <10 <5 61.5 30.5 ND 26.4 <5 <5 <5 <5 <5 21.7 <5 ND 9/24/2002 6.6 47.0 11.8 <5 39.2 <10 <5 62.3 20.6 ND 60.3 <5 <5 <5 <5 <5 28.1 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 7.1 <5 145 <10 5.4 189 48.6 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 14.2 80.3 33.8 <5 82.1 <10 <5 66.4 17.7 ND 140 <5 <5 <5 <5 <5 36.1 <5 <10 8/29/2006 <1 2 <1 <1 <2 <5 <1 <1 <1 ND 3.1 <1 <1 <1 <1 <1 <1 <2 ND Split (8270) 8/29/2006 NA NA NA NA 13 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 23.3 <5 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 3.0 1.9 <2.0 8.0 <1.0 1.4 <1.0 ND 7.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 9.2 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 1.4 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 8.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/l/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 7.27 <5 <0.5 2.75 <0.5 <0.5 1.19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 1.86 1.4 <0.5 11.4 <5 <0.5 6.26 6.36 <0.5 2.26 <0.5 <0.5 <0.5 <0.5 <0.5 2.54 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <7 <1 <1 <1 1.2 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bollom 12/15/2014 <1 <1 <1 <1 1.62J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <7 <7 <1 <1 3.02J <5 <7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 3.11 J <5 <1 0.47 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 18 <10 <1 1.3J 0.591 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 18 <10 <1 1.3J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/28/2016 NA NA NA NA 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 19.0 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 21.0 <20 <1 0.53 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 3.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 3.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.4J 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/8/2019 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <1 <1 <1 <1 0.83J 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Sur/ace 10/21/2021 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/20/2022 <1 <1 <1 <1 <0.3 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/20/2022 <1 <1 <1 <1 <0.3 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 TABLE3 SURFACE WATER ANALY17CAL RESULTS -VOCs SEABOARD CHEMICWRIVERDALE DRIVE LANDFILL SITE ram G S 3 y S o o D - D o o F _ 5 Sample ID Sample Date _ _ _ o = e ? _ e m = P, z 3 R a 1 u /I (,oil) (' IQ ( (a/I (,oil) u /I u l u /I u /I u 1 Noll) u /I u /I u /I u /I u /I u l u l u l ND 2B Still. 5 2500 6 300 9.90 0.35 3100 1.19 488 NE 3 60 11000 0.7 11 290 2.5 0.025 6200 20000 SW-DRP4 1112/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/14/2001 <5 9.1 <5 <5 44 <10 <5 101 51.5 ND 8 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 8.5 <5 <5 30.2 <10 <5 69.4 33.3 ND 7.4 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/24/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SWT40 ND EAST@1 9/13/2001 <5 6.5 <5 <5 49.3 <10 <5 47.6 36.7 ND 5.1 <5 <5 <5 <5 <5 <10 <5 ND EAST @3.2 9/13/2001 <5 6 <5 <5 48.9 <10 <5 68.4 38.9 ND <5 <5 <5 <5 <5 <5 <10 <5 ND WEST@0.5 9/13/2001 <5 5.9 <5 <5 45.9 <10 <5 59.9 37.3 ND <5 <5 <5 <5 <5 <5 <10 <5 ND SWT-50 ND EAST @1.0 9/13/2001 <5 7 <5 <5 43.4 <10 <5 14.8 33.6 ND 5.4 <5 <5 <5 <5 <5 <10 <5 ND EAST @3.0 9/13/2001 <5 7.6 <5 <5 48.2 <10 <5 42 39.8 ND 6.1 <5 <5 <5 <5 <5 <10 <5 ND WEST@1.0 9/13/2001 <5 7 <5 <5 as <10 <5 20.2 34.3 ND 5.6 <5 <5 <5 <5 <5 <10 <5 ND 9/27/2007 <1 <1 <1 <1 24.9 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SW-DRP-10 11/2/2000 <5 7.5 <5 <5 <100 NA <5 14 17 ND 5.7 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/13/2001 <5 6 <5 <5 43.8 <10 <5 14.4 27.7 ND <5 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/13/2001 <5 6.3 <5 <5 43.5 <10 <5 19.2 30.9 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 12.6 <10 <5 7.2 7.5 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 12 <10 <5 9.1 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <10 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 4.1 <5 <1 2.9 1.1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SWT-70 ND ND ND EAST 9/13/2001 <5 <5 <5 <5 38.3 <10 <5 <5 22.5 ND <5 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/13/2001 <5 <5 <5 <5 42.2 <10 <5 5.1 22.1 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/27/2007 <1 <1 <1 <1 22A <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SW-DRP-11 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/13/2001 <5 <5 <5 <5 10.2 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 109 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 50 FT UP 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 63.6 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 20.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 3.5 5.2 <1 1.1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <7 <1 17.9 <5 <7 <7 <1 ND <1 <1 <1 <1 <7 <1 <7 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 10.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 10.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 9.93 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/16/2013 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 12/16/2013 <0.5 <0.5 <0.5 <0.5 %4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/15/2014 <1 <1 <1 <1 1.551 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 1.53J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 12 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 19 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 17 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/l/2017 NA NA NA NA 1.4 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 31.0 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 31.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom Ilf7/2018 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.3J 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <7 <I <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <1 <1 <1 <1 <2 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/21/2021 <1 <1 <1 <1 1.4J 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 <1 <1 1.2J <20 <1 <1 <7 <1 <I <7 <1 <1 <1 <1 <1 <2 <5 Surface 10/20/2022 <1 <1 <1 <1 1.0 120 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/20/2022 1 1 1 7 1 <1 I <1 I <0.3 1 <20 1 <1 I <1 I <1 I <1 <1 <1 <1 <1 <1 <1 <1 <3 1 <5 ug/I= m crvgrams per liter ND = Not Detected J= Estimated value NE = Not Established B =Acolyte detected m method blank as well as sample NA = Not Analyzed Bold type indicates value exceeds NC 2B surface water quality standard (1NS-II NC 2B Std. (M-IV) = North C-lirw 2B ... - water quality standard fr Class WS-IV waters Value separated by slush 0 indicates split sample results TABLE 4 Page 1 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification Ground Water = MRF-1 2/24/2009 17.0 6.1 900 MW-1 3/5/2009 14.8 3.9 194 3/31/2010 16.5 6.6 2840 11/2/2011 14.2 8.2 9.7 228 11/20/2012 13.6 9.4 3.5 458 12/9/2013 13.5 12.0 3.6 3 12/8/2014 12.1 7.8 4.6 352 10/26/2015 13.7 8.0 3.5 0 11/14/2016 14.5 7.3 3.4 287 10/11/2017 19.9 7.2 4.7 262 11/1/2018 17.8 8.1 10.5 324 9/10/2019 22.8 6.6 585 10/13/2020 19.7 7.4 196 10/26/2021 15.7 5.7 1.3 337 10/12/2022 16.5 5.9 1.1 482 MW-2C 2/24/2009 14.4 6.6 688 MW-313 9/26/2000 15.7 6.2 2000 9/5/2001 17.8 6.4 1930 MW-3C 9/26/2000 15.4 6.3 1520 9/5/2001 17.6 6.5 1570 9/18/2002 16.9 6.8 1820 8/17/2004 18.2 6.6 1461 2/27/2009 15.7 6.4 686 3/30/2010 17.5 7.7 2370 11/1/2011 16.4 7.8 8.3 971 11/20/2012 14.8 7.9 2.9 648 12/11/2013 11.1 6.9 19.5 4 12/11/2014 15.7 6.7 4.4 1915 10/27/2015 15.3 6.5 1.9 1284 11/14/2016 17.2 7.3 2.7 1221 10/10/2017 23.9 6.2 4.2 1096 11/2/2018 17.3 6.8 3.3 1123 9/11/2019 31.1 6.5 1555 10/13/2020 18.1 6.4 665 10/26/2021 16.6 5.5 1.2 1042 10/17/2022 16.8 5.4 4.0 804 MW-5 2/24/2009 10.5 5.2 544 MW-6 9/26/2000 15.3 6.0 559 9/6/2001 17.5 6.2 472 9/19/2002 18.1 6.5 538 8/18/2004 -- -- -- 3/3/2009 14.6 7.5 900 3/30/2010 17.4 6.9 2730 11/1/2011 17.6 8.9 7.3 40 11/19/2012 20.6 7.3 2.9 1036 12/11/2013 11.3 6.5 11.7 113 12/12/2014 14.7 6.6 3.2 1163 10/30/2015 16.0 7.1 1.3 719 11/17/2016 20.1 6.5 1.7 751 10/10/2017 22.0 7.6 3.6 692 11/2/2018 19.5 6.6 4.6 993 9/12/2019 26.7 6.9 1245 10/14/2020 19.7 6.2 579 10/28/2021 19.2 6.4 0.3 955 10/19/2022 16.9 6.4 3.2 950 MW-713 3/3/2009 16.2 5.9 4220 MW-8 3/5/2009 16.9 5.1 990 MW-9 9/26/2000 14.9 5.8 1.17 2/26/2009 12.4 8.0 1840 MW-10 9/26/2000 15.4 6.3 2.51 9/6/2001 16.0 6.3 2480 9/19/2002 16.1 6.7 2740 9/16/2003 17.0 6.7 1940 8/17/2004 16.0 6.4 2200 3/6/2009 14.9 6.2 932 3/29/2010 16.6 8.8 4510 11/1/2011 16.9 7.1 9.4 1058 11/19/2012 15.8 7.4 2.0 154 12/10/2013 12.8 6.5 7.9 302 12/10/2014 13.1 6.5 4.1 257 10/26/2015 15.9 7.0 1.8 1523 11/14/2016 16.6 6.7 2.3 1194 10/10/2017 20.2 6.0 3.9 905 10/31/2018 17.6 6.8 3.6 1591 9/10/2019 24.5 6.2 31 10/12/2020 19.1 6.4 307 10/26/2021 18.7 4.6 0.9 355 10/14/2022 16.6 6.5 3.0 467 TABLE 4 Page 2 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification MW-11 9/28/2000 17.2 6.5 5950 9/10/2001 17.3 6.7 5860 9/18/2002 16.5 7.0 5350 8/17/2004 -- -- -- 3/4/2009 14.0 6.8 2990 MW-12A 9/28/2000 17.9 6.2 747 10/30/2000 17.7 6.4 899 9/6/2001 18.7 6.5 506 9/20/2002 18.8 6.4 766 9/16/2003 21.3 6.6 521 8/18/2004 23.0 7.0 425 3/6/2009 12.1 5.0 150 4/1/2010 17.0 7.4 6660 11/2/2011 10.9 9.6 1.1 1601 11/19/2012 15.8 7.7 2.8 539 12/10/2013 12.3 6.8 7.7 317 12/11/2014 14.1 6.8 4.6 564 10/27/2015 14.7 6.8 1.6 1948 11/14/2016 16.4 7.5 3.1 1530 10/10/2017 22.2 6.4 4.4 1558 11/1/2018 18.2 6.1 1.7 1720 9/10/2019 26.7 6.5 1500 10/13/2020 19.5 6.5 1180 10/26/2021 18.6 5.9 0.8 1856 10/17/2022 18.5 5.6 0.8 1794 MW-12B 9/28/2000 16.9 6.2 2620 9/6/2001 17.7 6.4 2570 9/20/2002 18.1 6.3 2930 9/16/2003 18.3 6.7 2500 8/18/2004 -- -- -- 3/4/2009 11.9 7.8 2990 4/9/2010 16.6 6.2 412 11/2/2011 16.4 9.0 2.7 1418 11/19/2012 15.0 7.4 2.8 39 12/10/2013 14.8 6.4 18.5 295 12/11/2014 14.3 6.5 3.5 868 10/27/2015 14.0 6.5 1.7 1475 11/14/2016 15.3 6.6 2.9 1682 10/10/2017 22.4 6.5 3.5 1699 11/1/2018 22.1 6.7 7.8 990 9/11/2019 25.0 6.5 1695 10/13/2020 18.9 6.5 1230 10/26/2021 17.4 5.6 0.7 1965 10/17/2022 17.5 5.1 1.2 1767 MW-12D 9/29/2000 15.8 6.8 1110 9/12/2001 16.2 7.8 949 9/20/2002 19.5 7.6 520 3/5/2009 13.4 11.9 208 4/1/2010 19.6 9.6 91100 11/2/2011 11.2 8.4 11.5 293 11/23/2012 18.0 9.1 1.9 27 12/11/2013 12.8 7.9 18.8 379 12/11/2014 17.3 7.7 6.0 609 10/25/2015 19.3 6.7 1.8 1210 11/18/2016 14.8 8.3 3.7 358 10/11/2017 20.5 7.3 6.2 382 11/1/2018 22.2 8.7 4.7 412 9/12/2019 21.0 7.1 275 10/13/2020 18.8 7.7 113 10/26/2021 17.7 6.3 0.6 279 10/17/2022 17.7 6.0 1.0 MW-15A 9/5/2001 17.5 6.3 942 9/18/2002 15.8 6.7 1150 9/17/2003 15.8 5.9 932 8/18/2004 -- -- -- 3/6/2009 15.1 6.3 427 3/31/2010 17.7 7.7 4940 11/2/2011 14.7 7.8 7.8 265 11/19/2012 14.8 7.6 2.7 237 12/10/2013 14.9 6.1 6.9 873 12/8/2014 11.6 6.6 4.9 768 10/27/2015 14.7 6.6 1.8 478 11/14/2016 14.1 6.6 2.8 760 10/11/2017 22.9 6.6 4.7 739 10/31/2018 16.3 6.8 11.2 246 9/10/2019 24.8 6.6 1515 10/9/2020 17.9 6.3 289 10/28/2021 15.7 7.1 0.5 508 10/18/2022 15.2 9.0 1.2 508 MW-16 MW-17 3/5/2009 18.7 10.0 357 OW-DR1 9/27/2000 19.0 6.3 2120 TABLE 4 Page 3 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification OW-DR2 9/26/2000 16.0 6.3 1850 9/10/2001 15.6 6.5 1900 2/27/2009 16.2 9.9 1760 3/30/2010 17.1 8.2 4960 11/1/2011 17.0 8.4 6.3 1060 11/23/2012 14.7 7.7 1.9 789 12/11/2013 13.2 8.4 2.9 837 12/12/2014 14.4 7.0 3.1 1918 10/30/2015 12.7 9.7 0.9 1388 11/18/2016 17.0 6.9 1.0 987 10/10/2017 20.6 6.4 3.3 1500 11/2/2018 17.1 7.6 0.8 1600 9/11/2019 23.3 7.6 900 10/13/2020 18.1 7.2 372 10/28/2021 16.2 7.5 0.3 627 10/18/2022 16.0 6.7 4.3 618 OW-DR3 9/20/2002 16.7 6.3 2520 8/24/2004 17.6 6.7 643 3/4/2009 12.7 3.7 2460 11/26/2012 17.5 6.1 2.5 1713 12/10/2013 13.7 6.3 4.1 254 OW-DR4 9/23/2002 17.9 6.6 1720 8/24/2004 17.5 6.3 1288 2/25/2009 17.5 6.2 762 OW-LFS1 2/26/2009 15.2 6.0 3730 OW-LFS2 2/26/2009 14.5 5.4 3100 3/30/2010 17.3 8.2 9990 11/1/2011 16.9 7.7 6.2 141 11/19/2012 17.4 7.6 2.7 367 12/11/2013 12.2 6.4 8.4 668 12/12/2014 14.7 6.5 4.6 1722 10/26/2015 16.2 6.6 2.2 1302 11/14/2016 18.9 6.5 2.5 2036 10/10/2017 21.6 6.5 4.5 2093 10/31/2018 17.9 6.6 9.5 1403 9/12/2019 20.2 6.7 830 10/12/2020 20.4 6.5 1440 10/28/2021 17.2 6.5 0.3 2827 10/17/2022 22.8 6.6 1.5 1545 OW-NIS1 3/10/2009 20.3 4.4 2650 OW-SF1 3/9/2009 18.0 3.8 802 OW-SIS1 8/17/2004 16.2 5.8 656.4 3/9/2009 18.0 4.2 579 OW-SIS2 2/24/2009 16.0 6.1 155 OW-SIS3 3/4/2009 13.6 6.0 392 PW-2D 3/3/2009 15.2 7.8 1930 PW-3D 11/27/2012 9.3 10.0 5.0 375 12/17/2013 8.6 12.7 18.7 128 12/11/2014 14.1 8.6 1.8 572 10/25/2015 18.8 6.3 0.6 397 11/16/2016 18.1 8.5 3.7 358 10/11/2017 21.4 7.5 1.7 377 11/2/2018 19.1 7.5 1.5 457 9/11/2019 23.6 8.0 762 10/27/2021 17.0 6.9 0.4 461 10/12/2022 18.3 6.0 0.8 466 PW-41 9/28/2000 21.8 6.3 2010 9/11/2001 19.7 6.4 1710 9/19/2002 20.8 6.5 1890 8/23/2004 20.4 3.1 1719 3/5/2009 17.5 4.4 2160 4/2/2010 16.6 7.6 1860 11/2/2011 24.4 8.0 0.2 1017 11/20/2012 18.9 7.2 2.0 920 12/17/2013 12.1 6.7 19.6 807 12/8/2014 13.9 6.3 1.5 1516 10/29/2015 20.5 6.8 0.8 1675 11/17/2016 21.1 6.0 1.6 1399 10/11/2017 22.7 6.4 1.5 857 11/2/2018 21.5 6.5 1.9 1686 9/11/2019 24.2 6.4 1857 10/14/2020 21.6 6.2 1120 10/27/2021 18.3 6.9 0.3 1944 10/18/2022 15.2 9.0 1.2 508 TABLE 4 Page 4 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-5D 9/26/2000 15.8 6.4 1620 9/10/2001 16.0 6.7 1590 9/23/2002 16.3 6.8 1610 8/18/2004 16.5 6.4 1293 3/27/2009 16.3 6.3 797 3/30/2010 17.2 8.4 1690 11/3/2011 17.3 8.4 8.3 1044 11/23/2012 15.8 8.2 1.9 790 12/16/2013 10.4 6.8 18.3 995 12/11/2014 14.9 7.0 2.8 1609 10/30/2015 15.8 7.8 1.3 955 11/18/2016 15.3 6.9 1.1 927 10/10/2017 20.3 6.8 2.4 1335 11/2/2018 17.6 7.8 2.9 1658 9/11/2019 25.6 7.6 920 10/13/2020 18.0 7.4 455 10/28/2021 16.5 7.5 0.4 757 10/18/2022 16.0 7.3 1.5 770 PW-6D 10/2/2000 16.5 7.7 320 9/12/2001 15.4 8.0 472 9/19/2002 15.9 8.1 356 8/25/2004 15.7 7.9 276 3/18/2009 16.7 7.3 363 3/31/2010 17.4 7.4 408 New Well 12/10/2014 13.1 8.2 4.6 564 10/30/2015 20.5 8.2 1.2 263 11/17/2016 17.6 7.7 1.4 410 10/10/2017 19.0 7.3 4.3 1100 11/1/2018 16.6 7.6 7.1 918 9/12/2019 25.2 7.5 904 10/12/2020 17.9 8.0 241 10/28/2021 15.9 6.1 0.4 780 10/14/2022 15.8 6.4 2.3 448 PW-61 10/2/2000 15.9 6.2 573 9/12/2001 14.5 6.2 816 9/19/2002 15.3 6.3 631 8/25/2004 15.1 6.3 544 3/4/2009 13.5 6.2 404 3/31/2010 17.9 6.0 1020 New Well 12/10/2014 11.0 7.6 3.5 1521 10/27/2015 14.7 6.7 1.5 1201 11/17/2016 14.6 6.8 1.9 1155 10/10/2017 22.1 6.4 3.6 1178 11/1/2018 17.3 6.5 0.7 1157 9/12/2019 21.8 6.0 1517 10/13/2020 17.4 6.3 761 10/28/2021 15.9 6.0 0.4 1303 10/14/2022 15.8 6.4 2.3 448 PW-71 9/28/2000 19.3 6.9 2230 9/12/2001 16.6 6.6 3190 9/20/2002 16.2 6.7 3250 8/20/2004 19.6 6.6 2666 3/4/2009 13.8 5.2 3010 PW-8S 9/27/2000 15.5 6.3 1130 9/6/2001 19.0 6.5 1040 9/17/2003 17.4 6.2 2080 8/17/2004 20.0 6.3 1628 3/3/2009 14.1 9.7 1670 PW-91 9/27/2000 19.2 7.0 1860 3/12/2009 19.0 5.4 1410 PW-10D 9/26/2000 15.1 8.3 703 9/11/2001 15.5 6.9 769 9/18/2002 19.8 9.8 354 8/17/2004 18.0 9.3 235 3/29/2010 18.1 9.9 920 11/1/2011 19.3 7.7 6.8 53 11/21/2012 14.3 12.8 4.7 103 12/11/2013 13.3 12.0 4.6 120 12/10/2014 13.6 9.8 4.6 342 11/3/2015 17.7 7.1 2.7 1225 11/17/2016 17.5 9.9 2.1 259 10/10/2017 21.3 7.3 4.6 285 10/31/2018 23.3 9.9 4.9 250 9/12/2019 24.9 9.9 298 10/12/2020 19.2 10.3 130 10/26/2021 17.4 7.0 0.9 220 10/13/2022 17.9 7.0 1.6 217 TABLE 4 Page 5 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-101 9/26/2000 16.7 6.1 787 9/11/2001 15.6 6.2 1080 9/18/2002 16.0 6.4 1210 8/17/2004 15.9 6.3 1192 3/12/2009 16.5 3.7 2110 3/29/2010 15.6 7.7 3960 11/1/2011 17.4 7.9 6.1 1123 11/19/2012 15.0 7.3 1.9 1693 12/11/2013 11.9 6.5 7.2 973 12/10/2014 14.3 6.4 2.7 214 10/29/2015 19.7 8.1 2.5 1356 11/17/2016 17.3 6.2 1.7 1529 10/10/2017 22.5 6.9 2.8 930 11/1/2018 16.3 7.3 11.8 62 9/12/2019 22.2 6.2 2000 10/12/2020 17.7 6.2 1150 10/26/2021 17.5 5.3 0.9 2254 10/13/2022 17.0 5.9 2.3 2517 PW-111 9/29/2000 16.3 6.9 649 9/11/2001 17.2 7.2 722 9/18/2002 19.1 8.1 618 8/25/2004 19.1 7.8 294 3/5/2009 16.1 5.2 929 PW-121 10/2/2000 23.1 7.1 659 9/11/2001 15.9 6.5 554 9/19/2002 17.6 6.7 689 8/17/2004 17.3 5.8 525 8/22/2006 16.9 5.5 90 3/3/2009 13.9 6.1 752 3/31/2010 17.0 6.4 634 11/2/2011 21.3 8.9 1.5 47 11/20/2012 16.3 8.1 3.4 152 12/17/2013 11.8 7.0 8.8 160 12/12/2014 11.7 7.1 9.2 880 10/30/2015 15.8 7.2 2.9 650 11/21/2016 16.1 6.7 2.7 597 10/11/2017 21.3 6.5 8.9 660 11/6/2018 19.1 7.2 3.4 816 9/11/2019 25.5 6.3 1022 10/14/2020 18.0 6.4 446 10/28/2021 17.1 6.3 0.4 852 10/19/2022 21.9 6.8 1.1 763 PW-131 9/29/2000 17.5 6.7 1100 9/12/2001 18.3 6.9 937 9/20/2002 18.4 7.2 999 9/23/2003 17.8 6.3 890 8/25/2004 17.8 7.0 896 3/4/2009 16.5 6.7 483 3/31/2010 18.5 8.1 1640 11/3/2011 12.1 9.5 6.3 780 11/23/2012 19.2 8.4 1.7 1323 12/16/2013 13.1 6.8 8.7 319 12/12/2014 17.5 6.9 2.9 1450 10/26/2015 16.9 6.9 1.0 1701 11/18/2016 18.0 6.9 1.3 976 10/11/2017 19.8 6.8 3.0 791 10/31/2018 17.7 7.1 10.1 1003 9/11/2019 24.7 6.9 1247 10/13/2020 18.3 7.0 571 10/28/2021 16.2 6.9 0.4 1007 10/12/2022 17.3 6.4 2.7 562 PW-14D 10/31/2000 23.0 12.2 6.91 9/10/2001 19.3 12.7 6,720 8/19/2004 19.2 12.2 4941 8/22/2006 20.5 12.8 613 3/11/2009 18.9 9.7 6400 3/31/2010 16.0 12.0 6640 11/7/2011 14.8 9.6 7.5 1253 11/27/2012 13.3 12.7 2.8 1776 12/12/2013 9.5 7.0 2.6 629 12/9/2014 16.8 12.1 5.2 381 11/3/2015 18.1 9.1 1.7 340 11/16/2016 15.6 13.1 2.0 3999 10/12/2017 18.8 6.9 5.1 612 11/5/2018 19.2 12.7 2.0 4246 9/17/2019 26.0 12.5 365 10/14/2020 19.7 12.1 3370 10/27/2021 15.9 10.0 0.0 5677 10/13/2022 15.9 9.7 1.6 5593 PW-14S 10/30/2000 17.7 6.0 130 9/6/2001 17.8 6.3 185 8/19/2004 16.8 5.9 95 8/22/2006 16.8 5.1 185 3/10/2009 15.7 4.0 68 TABLE 4 Page 6 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-15D 10/31/2000 15.5 6.8 1.46 9/6/2001 16.8 6.7 1.68 9/16/2003 16.3 7.5 730 8/19/2004 -- -- -- 8/23/2006 16.0 6.3 1.6 3/11/2009 19.0 4.0 79 3/30/2010 15.9 6.2 1950 11/7/2011 11.1 6.3 8.1 95 11/26/2012 17.3 6.3 1.1 1204 12/12/2013 9.4 6.9 7.0 727 12/9/2014 16.1 7.0 2.8 1628 10/28/2015 18.7 7.1 1.0 966 11/15/2016 17.3 7.8 2.4 867 10/12/2017 18.1 6.9 2.8 738 11/5/2018 15.9 7.5 0.7 1360 9/17/2019 21.1 7.2 920 10/14/2020 19.6 6.4 34 10/27/2021 15.2 6.0 0.4 784 10/13/2022 16.0 6.3 2.4 790 PW-15S 10/30/2000 16.7 6.4 467 9/6/2001 16.3 7.2 648 8/19/2004 -- -- -- 8/23/2006 17.9 6.5 604 3/11/2009 17.6 4.5 432 PW-16D 11/2/2000 17.1 7.4 85.7 9/6/2001 15.7 7.3 96 8/19/2004 16.5 7.2 845 8/23/2006 15.8 6.7 125 3/11/2009 19.1 3.8 633 3/30/2010 15.4 6.6 1280 11/7/2011 16.8 8.2 6.1 460 11/26/2012 19.8 6.8 1.6 926 12/12/2013 8.4 7.8 9.7 365 12/9/2014 15.2 7.7 2.9 1327 10/28/2015 18.6 7.1 0.8 815 11/15/2016 18.0 8.4 1.7 709 10/12/2017 18.8 7.8 3.2 1364 11/5/2018 16.3 7.4 2.4 619 9/12/2019 22.5 7.2 689 10/14/2020 18.4 6.2 45 10/27/2021 16.1 6.5 0.4 604 10/13/2022 16.8 6.7 5.8 691 PW-16S 10/30/2000 17.4 6.3 347 9/6/2001 17.6 6.3 499 8/19/2004 17.2 6.3 291 8/23/2006 18.6 6.8 416 PW-17 11/3/2000 18.8 6.4 44.4 9/12/2001 18.3 6.5 364 9/18/2002 16.8 6.6 424 8/19/2004 17.3 6.6 447 3/5/2009 15.9 7.4 242 PW-18 11/3/2000 15.6 10.3 44.2 9/10/2001 17.3 11.2 853 9/16/2003 16.8 12.9 9040 8/19/2004 -- -- -- 8/22/2006 18.5 13.1 121 3/11/2009 20.3 8.7 1310 3/31 /2010 17.7 12.2 12200 11/8/2011 7.7 6.1 9.6 954 11/26/2012 15.1 12.0 3.1 393 12/12/2013 10.6 12.5 8.7 66 12/9/2014 14.1 12.2 7.6 1134 10/26/2015 15.5 12.7 4.3 1102 11/15/2016 17.2 13.5 7.3 3999 10/16/2017 16.7 12.8 7.9 1217 11/7/2018 17.5 12.7 4.8 1210 9/17/2019 Not Sampled 10/14/2020 Not Sampled 10/27/2021 Not Sampled PW-19 11/6/2001 15.3 7.2 268 9/18/2002 18.6 7.5 387 9/16/2003 11.8 8.9 483 8/17/2004 16.2 7.8 450 3/10/2009 17.1 9.2 299 PW-DR1 2/25/2009 13.6 6.2 1950 PW-SIS1 8/19/2004 15.7 6.8 536 3/9/2009 17.2 5.8 210 TABLE 4 Page 7 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-SF1 4/2/2010 17.6 8.8 3960 11/3/2011 18.6 8.7 3.4 896 11/20/2012 14.9 7.6 1.8 147 12/9/2013 14.9 6.8 11.3 39 12/8/2014 14.5 6.7 3.4 1272 10/27/2015 14.1 6.8 3.1 1656 11/17/2016 15.9 6.9 1.6 845 10/11/2017 18.3 6.4 3.3 819 10/31/2018 17.2 6.4 0.5 392 9/10/2019 24.6 6.0 218 10/9/2020 17.5 7.1 676 10/27/2021 15.6 6.3 0.5 1091 10/18/2022 15.0 8.0 2.0 1851 RW-LFS1 2/26/2009 14.8 6.0 3010 RW-LFS2 2/26/2009 15.7 6.2 2460 RW-NIS1 3/6/2009 15.0 5.1 3190 RW-SIS2 3/9/2009 17.7 3.8 160 RW-SIS3 3/4/2009 15.6 6.0 681 RW-SIS4 3/4/2009 12.7 6.1 97 RW-SIS5 3/4/2009 12.5 6.7 425 RW-SIS6 3/4/2009 15.2 6.3 322 W-1 9/27/2000 16.2 6.5 330 9/10/2001 17.5 6.6 296 9/18/2002 17.1 6.6 307 9/17/2003 17.6 6.3 448 8/17/2004 17.1 6.8 390 3/3/2009 16.4 6.9 484 W-4 9/27/2000 14.9 6.5 267 9/10/2001 16.0 6.6 263 9/17/2002 18.4 6.9 342 9/17/2003 16.5 6.1 290 8/17/2004 18.4 6.0 248 W-4A 9/27/2000 14.7 6.5 612 9/10/2001 15.1 6.5 773 9/14/2002 15.5 6.4 653 9/17/2003 14.5 6.1 434 8/17/2004 15.5 6.4 475 2/27/2009 18.6 6.2 223 3/31/2010 15.6 7.6 52100 11/2/2011 14.7 9.0 1.0 695 11/19/2012 14.5 7.6 3.4 32 12/17/2013 10.8 6.5 9.5 546 12/8/2014 12.5 6.6 4.2 1006 10/27/2015 14.3 6.7 1.8 234 11/16/2016 16.3 7.6 1.3 356 10/11/2017 21.9 6.6 4.1 383 10/31/2018 17.3 6.6 10.0 13 9/11/2019 23.2 7.1 337 10/9/2020 19.7 6.2 144 10/27/2021 15.3 6.0 0.4 270 10/18/2022 13.4 7.0 1.5 233 W-5 9/27/2000 15.7 6.4 2530 10/30/2000 15.3 6.3 2580 9/10/2001 15.9 6.4 2170 9/18/2002 16.1 6.9 2060 8/18/2004 -- -- -- 3/3/2009 14.1 6.3 556 W-6A 9/28/2000 17.1 5.9 4950 W-18 3/5/2009 14.6 6.1 361 W-21 9/28/2000 14.3 6.0 343 9/10/2001 14.8 6.6 310 9/17/2002 15.5 6.7 342 9/17/2003 14.9 6.1 360 8/17/2004 16.8 6.5 292 2/24/2009 13.4 6.6 900 W-23A 3/4/2009 11.8 6.4 426 W-24 3/5/2009 TABLE 4 Page 8 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification Surface Water = 175 SW-1 11/2/2000 10.4 6.7 9/14/2001 20.1 6.4 153 9/24/2002 Dry -- -- 9/16/2003 19.9 6.8 119 8/23/2004 20.2 7.4 59 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 Dry 11/7/2018 12.8 7.9 6.7 177 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry 10/19/2022 Dry SW-2 11/2/2000 16.6 7.2 2070 9/14/2001 21.2 7.1 1640 9/24/2002 20.9 5.8 1870 9/15/2003 21.8 7.2 2160 8/23/2004 24.8 7.3 98 8/22/2006 20.8 7.0 226 4/1/2010 15.3 7.5 103 11/3/2011 14.3 8.4 378 11/20/2012 Dry 12/11/2013 Dry 12/8/2014 Dry 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 21.7 7.8 5.3 112 11/7/2018 14.7 7.7 7.1 251 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry 10/19/2022 15.1 6.1 5.5 470 SW-3 11/2/2000 11.0 8.0 359 9/14/2001 20.1 7.3 199 9/24/2002 19.3 6.7 3450 9/16/2003 19.7 7.3 244 8/25/2004 23.1 8.1 133 8/22/2006 23.2 7.5 480 4/1/2010 15.6 7.6 6850 11/3/2011 10.6 8.9 11.1 261 11/20/2012 11.1 9.1 6.0 35 12/11/2013 5.5 9.0 1.6 144 12/8/2014 10.2 8.4 16.2 108 10/22/2015 16.6 7.5 4.8 224 11/17/2016 12.7 7.7 2.2 1577 10/13/2017 19.1 7.4 2.2 246 11/7/2018 19.2 7.9 6.6 298 9/18/2019 21.8 7.7 323 10/22/2020 20.8 8.4 4.5 281 10/21/2021 11.6 4.9 2.7 312 10/19/2022 11.2 7.2 10.2 195 SW-3A 8/25/2004 21.9 8.1 126 SW-313 8/25/2004 21.9 7.7 123 SW-4 11/2/2000 12.8 6.9 964 9/14/2001 19.9 7.2 771 9/15/2003 25.0 7.5 473 8/25/2004 22.9 7.5 452 8/22/2006 22.2 7.3 112 4/1/2010 14.9 7.7 102 11/3/2011 14.5 7.7 6.1 671 11/20/2012 11.5 9.1 5.6 22 12/13/2013 4.2 8.8 9.5 1 12/8/2014 7.2 8.3 17.4 147 10/22/2015 15.8 8.4 4.8 0 11/21/2016 9.8 8.1 4.0 206 10/13/2017 19.9 6.3 8.8 878 11/7/2018 19.5 8.1 6.3 252 9/18/2019 21.2 6.5 1285 10/22/2020 20.5 8.3 2.5 108 10/21/2021 15.0 4.7 2.1 1546 10/19/2022 15.2 7.0 3.7 156 TABLE 4 Page 9 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification SW-5 11/2/2000 14.7 6.9 415 9/14/2001 19.7 6.7 295 9/24/2002 19.7 6.7 295 9/16/2003 20.6 7.0 300 8/25/2004 21.1 7.5 168 8/22/2006 22.2 7.5 540 4/1/2010 17.1 7.4 6760 11/3/2011 11.9 9.6 9.9 212 11/20/2012 11.5 9.1 5.6 22 12/16/2013 8.7 8.5 9.7 78 12/8/2014 7.7 10.1 11.0 229 10/22/2015 16.3 7.3 4.9 199 11/17/2016 10.2 7.8 4.8 320 10/13/2017 19.0 7.4 9.2 314 11/7/2018 14.9 7.8 6.1 217 9/18/2019 22.0 9.1 311 10/22/2020 19.5 8.1 3.8 301 10/21/2021 13.3 6.1 4.1 438 10/19/2022 14.1 6.8 7.8 367 SW-6 11/2/2000 11.4 7.5 215 9/14/2001 22.4 6.9 133 9/24/2002 22.4 7.5 168 9/16/2003 21.5 7.4 117 8/25/2004 26.4 8.2 82 8/22/2006 25.7 7.7 168 4/1/2010 14.3 8.3 103 11/3/2011 14.5 10.3 6.8 326 shallow-1' 11/21/2012 8.1 9.0 5.4 8 deep - 8.5' 11/21/2012 8.7 9.3 5.2 79 shallow - 1' 12/13/2013 5.2 8.2 9.8 45 deep - 11' 12/13/2013 5.6 8.3 9.5 26 shallow - 1' 12/15/2014 9.0 8.6 13.9 212 deep - 8.6' 12/15/2014 9.1 8.7 13.3 279 shallow - 1' 10/22/2015 21.6 7.5 3.9 127 deep - 8.6' 10/22/2015 20.3 7.4 4.1 97 shallow-1' 11/21/2016 12.2 8.0 4.4 154 deep - 8.5' 11/21/2016 11.9 7.9 4.2 151 shallow - 1' 10/13/2017 22.5 9.4 13.6 303 deep - 10.2' 10/13/2017 22.0 9.2 13.3 293 shallow - 1' 11/7/2018 18.1 9.9 7.3 197 deep - 11.0' 11/7/2018 17.8 9.5 7.3 100 shallow - 1' 9/18/2019 24.4 8.1 177 deep - 10' 9/18/2019 24.6 8.6 163 shallow - 1' 10/22/2020 21.8 5.9 4.8 56 deep - 11' 10/22/2020 22.3 4.8 5.7 69 shallow - 1' 10/21/2021 16.0 5.7 2.0 150 deep - 15.3' 10/21/2021 16.2 5.3 1.7 124 shallow - 1' 10/20/2022 12.1 6.5 3.1 1415 deep - 5' 10/20/2022 10.2 6.5 3.2 1107 SW-7 11/3/2000 9.0 6.3 319 9/13/2001 20.3 6.8 220 9/24/2002 21.8 6.6 263 9/15/2003 23.8 7.0 156 8/23/2004 25.5 7.2 85 4/1/2010 13.4 7.4 103 11/3/2011 11.8 9.0 13.3 84 shallow-1' 11/21/2012 10.5 9.1 6.4 58 deep -11.5' 11/21/2012 10.7 9.0 6.8 319 shallow - 1' 12/13/2013 6.6 8.2 9.1 18 deep - 13' 12/13/2013 6.4 8.2 9.6 4 shallow - 1' 12/15/2014 10.5 8.6 13.4 186 deep - 12.3' 12/15/2014 11.1 8.4 13.8 179 shallow - 1' 10/22/2015 18.6 8.6 5.4 75 deep - 12.1' 10/22/2015 18.3 8.6 5.5 64 shallow-1' 11/21/2016 10.5 8.0 4.4 262 deep -12' 11/21/2016 9.7 9.2 5.7 276 shallow - 1' 10/13/2017 23.3 8.6 13.8 338 deep - 13.0' 10/13/2017 22.3 8.3 13.5 318 shallow - 1' 11/7/2018 17.8 8.7 6.9 82 deep - 16.0' 11/7/2018 17.8 8.7 6.4 80 shallow - 1' 9/18/2019 26.2 8.5 216 deep - 19.5' 9/18/2019 24.7 8.2 169 shallow - 1' 10/22/2020 23.0 8.2 6.4 144 deep - 11' 10/22/2020 21.6 8.2 5.2 89 shallow - 1' 10/21/2021 18.1 5.4 1.0 116 deep - 14' 10/21/2021 17.9 5.3 1.0 111 shallow - 1' 10/20/2022 12.6 2.7 137 deep -14' 10/20/2022 12.1 2.5 142 TABLE 4 Page 10 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification SW-DRP-2 11/3/2000 13.5 6.5 1870 East 9/14/2001 20.3 7.0 224 West 9/14/2001 20.5 6.9 239 9/15/2003 23.1 7.1 150 8/23/2004 22.0 3.7 386 4/1/2010 14.1 7.8 102 11/3/2011 11.5 8.8 10.9 140 shallow-1' 11/21/2012 10.2 8.9 5.9 43 deep - 12.5' 11/21/2012 9.9 9.1 5.6 67 shallow - 1' 12/13/2013 5.8 8.2 9.4 10 deep - 10' 12/13/2013 5.7 6.9 9.9 28 shallow - 1' 12/15/2014 10.2 8.7 16.5 176 deep - 12.3' 12/15/2014 10.2 8.5 16.3 176 shallow - 1' 10/22/2015 15.9 8.1 6.3 0 deep - 12.3' 10/22/2015 16.0 8.1 6.4 0 shallow-1' 11/21/2016 9.7 8.1 3.7 203 deep-12' 11/21/2016 9.6 7.9 6.6 206 shallow - 1' 10/13/2017 23.3 8.5 16.5 324 deep - 14.2' 10/13/2017 21.7 8.6 16.3 334 shallow - 1' 11/7/2018 18.9 9.1 6.7 97 deep - 12.0' 11/7/2018 17.9 8.8 6.5 83 shallow - 1' 9/18/2019 24.8 7.7 300 deep -10' 9/18/2019 25.0 8.3 159 shallow - 1' 10/22/2020 25.3 8.6 5.3 119 deep - 12' 10/22/2020 24.6 8.6 4.6 89 shallow - 1' 10/21/2021 17.8 6.2 1.9 124 deep - 11.5' 10/21/2021 17.7 5.9 1.8 113 shallow - 1' 10/20/2022 11.6 6.6 3.0 460 deep - 12' 10/20/2022 13.2 6.6 3.5 144 SW-DRP-4 11/3/2000 13.1 6.3 544 East 9/14/2001 18.8 6.1 286 West 9/14/2001 17.7 6.8 237 9/15/2003 23.4 7.1 182 SW-DRP-10 11/2/2000 12.6 6.9 306 East 9/13/2001 21.9 7.6 214 West 9/13/2001 21.4 7.2 215 9/15/2003 23.5 7.1 154 SW-DRP-11 11/2/2000 16.5 6.4 559 9/13/2001 20.4 6.4 343 9/24/2002 23.6 6.3 527 9/15/2003 25.4 6.8 357 8/23/2004 15.7 7.9 276 4/1/2010 14.0 7.3 104 11/3/2011 13.5 9.1 12.2 58 shallow-1' 11/21/2012 9.2 11.0 8.2 27 deep -9' 11/21/2012 10.3 9.3 8.3 26 shallow - 1' 12/16/2013 5.6 8.5 9.7 1 deep - 12' 12/16/2013 5.4 8.7 9.2 34 shallow - 1' 12/15/2014 7.5 8.9 16.4 164 deep - 11.6' 12/15/2014 9.3 8.8 16.9 198 shallow - 1' 10/22/2015 18.4 7.9 5.6 0 deep - 11.7' 10/22/2015 18.0 7.6 6.0 0 shallow-1' 11/21/2016 11.0 8.2 7.0 362 deep-12' 11/21/2016 11.2 8.2 2.7 398 shallow - 1' 10/13/2017 23.0 7.7 16.4 357 deep - 12.5' 10/13/2017 21.9 7.9 16.7 342 shallow - 1' 11/7/2018 17.9 8.7 6.4 87 deep - 11.5' 11/7/2018 17.8 8.9 6.7 167 shallow - 1' 9/18/2019 26.8 8.3 230 deep - 5' 9/18/2019 28.6 7.7 224 shallow - 1' 10/22/2020 23.9 8.1 6.3 195 deep - 10' 10/22/2020 23.0 7.5 4.3 149 shallow - 1' 10/21/2021 20.0 6.4 0.7 223 deep - 6.5' 10/21/2021 18.9 6.3 0.7 190 shallow - 1' 10/20/2022 14.6 6.4 2.6 178 deep - 6' 10/20/2022 15.2 6.4 1.9 180 SWT-40 East @ 1' ^ 9/13/2001 21.9 7.0 219 East @ 3.25' ^ 9/13/2001 22.0 7.0 219 West @ 0.5' ^ 9/13/2001 21.8 7.0 217 SWT-50 East @ 1' ^ 9/13/2001 21.0 7.5 217 East @ 3' ^ 9/13/2001 22.1 7.0 216 West @ 1' ^ 9/13/2001 21.6 7.0 216 SWT-70 East 9/13/2001 22.0 7.1 216 West 9/13/2001 20.8 7.2 216 RCP-1 11/2/2000 15.3 6.6 277 RCP-2 11/2/2000 15.4 6.6 248 TABLE 4 Page 10 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification SW-DRP-2 11/3/2000 13.5 6.5 1870 East 9/14/2001 20.3 7.0 224 West 9/14/2001 20.5 6.9 239 9/15/2003 23.1 7.1 150 8/23/2004 22.0 3.7 386 4/1/2010 14.1 7.8 102 11/3/2011 11.5 8.8 10.9 140 shallow-1' 11/21/2012 10.2 8.9 5.9 43 deep - 12.5' 11/21/2012 9.9 9.1 5.6 67 shallow - 1' 12/13/2013 5.8 8.2 9.4 10 deep - 10' 12/13/2013 5.7 6.9 9.9 28 shallow - 1' 12/15/2014 10.2 8.7 16.5 176 deep - 12.3' 12/15/2014 10.2 8.5 16.3 176 shallow - 1' 10/22/2015 15.9 8.1 6.3 0 deep - 12.3' 10/22/2015 16.0 8.1 6.4 0 shallow-1' 11/21/2016 9.7 8.1 3.7 203 deep-12' 11/21/2016 9.6 7.9 6.6 206 shallow - 1' 10/13/2017 23.3 8.5 16.5 324 deep - 14.2' 10/13/2017 21.7 8.6 16.3 334 shallow - 1' 11/7/2018 18.9 9.1 6.7 97 deep - 12.0' 11/7/2018 17.9 8.8 6.5 83 shallow - 1' 9/18/2019 24.8 7.7 300 deep -10' 9/18/2019 25.0 8.3 159 shallow - 1' 10/22/2020 25.3 8.6 5.3 119 deep - 12' 10/22/2020 24.6 8.6 4.6 89 shallow - 1' 10/21/2021 17.8 6.2 1.9 124 deep - 11.5' 10/21/2021 17.7 5.9 1.8 113 shallow - 1' 10/20/2022 11.6 6.6 3.0 460 deep - 12' 10/20/2022 13.2 6.6 3.5 144 SW-DRP-4 11/3/2000 13.1 6.3 544 East 9/14/2001 18.8 6.1 286 West 9/14/2001 17.7 6.8 237 9/15/2003 23.4 7.1 182 SW-DRP-10 11/2/2000 12.6 6.9 306 East 9/13/2001 21.9 7.6 214 West 9/13/2001 21.4 7.2 215 9/15/2003 23.5 7.1 154 SW-DRP-11 11/2/2000 16.5 6.4 559 9/13/2001 20.4 6.4 343 9/24/2002 23.6 6.3 527 9/15/2003 25.4 6.8 357 8/23/2004 15.7 7.9 276 4/1/2010 14.0 7.3 104 11/3/2011 13.5 9.1 12.2 58 shallow-1' 11/21/2012 9.2 11.0 8.2 27 deep -9' 11/21/2012 10.3 9.3 8.3 26 shallow - 1' 12/16/2013 5.6 8.5 9.7 1 deep - 12' 12/16/2013 5.4 8.7 9.2 34 shallow - 1' 12/15/2014 7.5 8.9 16.4 164 deep - 11.6' 12/15/2014 9.3 8.8 16.9 198 shallow - 1' 10/22/2015 18.4 7.9 5.6 0 deep - 11.7' 10/22/2015 18.0 7.6 6.0 0 shallow-1' 11/21/2016 11.0 8.2 7.0 362 deep-12' 11/21/2016 11.2 8.2 2.7 398 shallow - 1' 10/13/2017 23.0 7.7 16.4 357 deep - 12.5' 10/13/2017 21.9 7.9 16.7 342 shallow - 1' 11/7/2018 17.9 8.7 6.4 87 deep - 11.5' 11/7/2018 17.8 8.9 6.7 167 shallow - 1' 9/18/2019 26.8 8.3 230 deep - 5' 9/18/2019 28.6 7.7 224 shallow - 1' 10/22/2020 23.9 8.1 6.3 195 deep - 10' 10/22/2020 23.0 7.5 4.3 149 shallow - 1' 10/21/2021 20.0 6.4 0.7 223 deep - 6.5' 10/21/2021 18.9 6.3 0.7 190 shallow - 1' 10/20/2022 14.6 6.4 2.6 178 deep - 6' 10/20/2022 15.2 6.4 1.9 180 SWT-40 East @ 1' ^ 9/13/2001 21.9 7.0 219 East @ 3.25' ^ 9/13/2001 22.0 7.0 219 West @ 0.5' ^ 9/13/2001 21.8 7.0 217 SWT-50 East @ 1' ^ 9/13/2001 21.0 7.5 217 East @ 3' ^ 9/13/2001 22.1 7.0 216 West @ 1' ^ 9/13/2001 21.6 7.0 216 SWT-70 East 9/13/2001 22.0 7.1 216 West 9/13/2001 20.8 7.2 216 RCP-1 11/2/2000 15.3 6.6 277 RCP-2 11/2/2000 15.4 6.6 248 TABLE 5 MONITORING WELL LATITUDE/LONGITUDE, DEPTHS AND ELEVATIONS SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Facility Name Seaboard Chemical/Riverdale Drive Landfill EPA ID Number NCD 071 574 164 Well ID Type Well Use Northing Easting Reference Source of Information TOC Elevation Well Depth MW-1 well monitoring 801318.45 1729231.88 state plane coord Jamestown Engineering 790.46 57.7 MW-3C well monitoring 801265.20 1731350.08 state plane coord Jamestown Engineering 692.74 57 MW-6 well monitoring 799702.65 1731990.93 state plane coord Jamestown Engineering 761.47 110 MW-10 well monitoring 800464.20 1732378.92 state plane coord Jamestown Engineering 695.01 28 MW-12A well monitoring 801788.63 1730912.94 state plane coord Jamestown Engineering 693.07 20 MW-12B well monitoring 801780.30 1730911.77 state plane coord Jamestown Engineering 693.86 58 MW-12D well monitoring 801770.20 1730908.12 state plane coord Jamestown Engineering 694.21 202 MW-15A well monitoring 800903.23 1730181.46 state plane coord Jamestown Engineering 764.33 34 OW-DR2 well monitoring 801266.66 1731357.68 state plane coord Jamestown Engineering 695.87 186 OW-DR3 well monitoring 801185.56 1731735.15 state plane coord Jamestown Engineering 702.93 160 OW-LFS-2 well monitoring 800674.15 1732093.91 state plane coord Jamestown Engineering 699.45 50 PW-3D well monitoring 800603.04 1730831.13 state plane coord Jamestown Engineering 738.60 209.5 PW-41 well monitoring 800545.88 1731099.56 state plane coord Jamestown Engineering 735.00 ** 122 PW-5D well monitoring 801164.35 1731363.53 state plane coord Jamestown Engineering 696.27 306.5 PW-6D well monitoring 801425.12 1732032.71 state plane coord Jamestown Engineering 696.79 275 PW-61 well monitoring 801415.38 1732022.44 state plane coord Jamestown Engineering 697.41 75 PW-10D well monitoring 800446.73 1732384.15 state plane coord Jamestown Engineering 697.26 200 PW-101 well monitoring 800456.28 1732373.34 state plane coord Jamestown Engineering 695.97 100 PW-121 well monitoring 799844.10 1730816.38 state plane coord Jamestown Engineering 749.48 105 PW-131 well monitoring 801310.27 1730977.69 state plane coord Jamestown Engineering 739.01 250 PW-14D well monitoring 801653.66 1731389.41 state plane coord Jamestown Engineering 686.50 * 198.8 PW-15D well monitoring 801544.36 1731748.91 state plane coord Jamestown Engineering 685.80 163.5 PW-16D well monitoring 801711.36 1732067.64 state plane coord Jamestown Engineering 686.68 179 W-4A well monitoring 1800667.98 11730625.66 state plane coord iJamestown Engineering 1712.64 138.5 I * Elevation corrected for repairs performed on PW-14D during October 2015 monitoring event. ** Elevation corrected for repairs performed on PW-41 during November 2016 monitoring event. APPENDIX A Laboratory Report 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, November 7, 2022 Babb & Associates (BA024) Attn: Gary Babb 5506 Bradford Pear Court Raleigh, NC 27606 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Seaboard/Riverdale Landfill ENCO Workorder(s): CF14375,CF14376,CF15781 Dear Gary Babb, Enclosed is a copy of your laboratory report for test samples received by our laboratory between Saturday, October 15, 2022 and Friday, October 21, 2022. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 4P 0 ee Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 1 15 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4301-MW3C Lab ID: CF14375-01 Sampled: 10/17/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 00:18 Client ID: 4301-MW3C Lab ID: CF14375-01RE1 Sampled: 10/17/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/27/22 15:30 Analysis Date/Time(s) 10/27/22 19:51 Client ID: 4301-MW6 Lab ID: CF14375-02 Sampled: 10/19/22 08:20 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 00:46 Client ID: 4301-MW6 Lab ID: CF14375-02RE1 Sampled: 10/19/22 08:20 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/31/22 15:45 Analysis Date/Time(s) 10/31/22 21:56 Client ID: 4101-MW12A Lab ID: CF14375-03 Sampled: 10/17/22 11:30 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 01:15 Client ID: 4101-MW12B Lab ID: CF14375-04 Sampled: 10/17/22 13:15 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 01:43 Client ID: 4101-MW12D Lab ID: CF14375-05 Sampled: 10/17/22 10:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MIS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 02:12 Client ID: 4101-MW15A Lab ID: CF14375-06 Sampled: 10/18/22 10:35 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 02:41 Client ID: 4301-OWDR2 Lab ID: CF14375-07 Sampled: 10/18/22 08:40 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 03:09 Client ID: 4301-OWDR2 Lab ID: CF14375-07RE1 Sampled: 10/18/22 08:40 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/31/22 15:45 Analysis Date/Time(s) 10/31/22 22:53 Client ID: 4301-OWLFS2 Lab ID: CF14375-08 Sampled: 10/17/22 13:45 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/31/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 03:38 Client ID: 4301-PW5D Lab ID: CF14375-09 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 04:07 Client ID: 4301-PW5D Lab ID: CF14375-09RE2 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/31/22 19:13 Analysis Date/Time(s) 11/01/22 12:15 Client ID: 4301-PW4I Lab ID: CF14375-10 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 04:35 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 115 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4301-PW4I Lab ID: CF34375-30RE2 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/31/22 19:13 Analysis Date/Time(s) 11/01/22 12:44 Client ID: 4101-PW12I Lab ID: CF14375-11 Sampled: 10/19/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 05:04 Client ID: 4301-PWSF1 Lab ID: CF14375-12 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/25/22 15:56 Analysis Date/Time(s) 10/26/22 05:32 Client ID: 4101-PWSF1 Lab ID: CF14375-12RE1 Sampled: 10/18/22 09:25 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/31/22 15:45 Analysis Date/Time(s) 10/31/22 23:22 Client ID: 4301-W4A Lab ID: CF14375-13RE1 Sampled: 10/18/22 13:55 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/27/22 15:30 Analysis Date/Time(s) 10/27/22 20:20 Client ID: 4101-W4A Lab ID: CF14375-13RE2 Sampled: 10/18/22 13:55 Received: 10/20/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/01/22 Prep Date/Time(s) 10/31/22 19:13 Analysis Date/Time(s) 11/01/22 10:49 Client ID: 4101-SW2 Lab ID: CF14376-01 Sampled: 10/19/22 12:25 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MIS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/21/22 22:44 Client ID: 4301-SW3 Lab ID: CF14376-02 Sampled: 10/19/22 13:25 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/21/22 23:13 Client ID: 4301-SW4 Lab ID: CF14376-03RE2 Sampled: 10/19/22 12:50 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/25/22 19:31 Analysis Date/Time(s) 10/27/22 01:42 Client ID: 4101-SWS Lab ID: CF14376-04 Sampled: 10/19/22 13:10 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 00:10 Client ID: 4301-SW6Surface Lab ID: CF14376-05 Sampled: 10/20/22 08:40 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 00:38 Client ID: 4301-SW6Bottom Lab ID: CF14376-06 Sampled: 10/20/22 08:50 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 01:07 Client ID: 4301-SW7Bottom Lab ID: CF14376-07 Sampled: 10/20/22 10:20 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 01:35 Client ID: 4301-SW7Surface Lab ID: CF14376-08 Sampled: 10/20/22 10:10 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 02:04 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 115 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4301-SWDRP2Bottom Lab ID: CF14376-09 Sampled: 10/20/22 09:50 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 02:33 Client ID: 4301-SWDRP2Surface Lab ID: CF14376-10 Sampled: 10/20/22 09:40 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 03:01 Client ID: 4301-SWDRP11Surface Lab ID: CF14376-11 Sampled: 10/20/22 11:00 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 03:30 Client ID: 4101-SWDRP11Bottom Lab ID: CF14376-12 Sampled: 10/20/22 11:10 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/03/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/22/22 03:59 Client ID: 4301-TripBlank Lab ID: CF14376-13 Sampled: 10/19/22 12:25 Received: 10/21/22 11:00 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 11/02/22 Prep Date/Time(s) 10/21/22 15:55 Analysis Date/Time(s) 10/21/22 20:50 Client ID: 4101-MW1 Lab ID: CF15781-01 Sampled: 10/12/22 13:50 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/18/22 02:20 Client ID: 4301-MW1 Lab ID: CF15781-01RE1 Sampled: 10/12/22 13:50 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 5030B_MIS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/18/22 17:33 Analysis Date/Time(s) 10/18/22 23:21 Client ID: 4101-MW10 Lab ID: CF15781-02 Sampled: 10/14/22 10:50 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/28/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(sl 10/20/22 02:20 Client ID: 4301-PW3D Lab ID: CF15781-03 Sampled: 10/12/22 11:40 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/18/22 02:49 Client ID: 4301-PW3D Lab ID: CF15781-03RE1 Sampled: 10/12/22 11:40 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/19/22 22:46 Client ID: 4301-PW6I Lab ID: CF15781-04 Sampled: 10/14/22 12:00 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/28/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/20/22 02:49 Client ID: 4301-PW6D Lab ID: CF15781-05RE1 Sampled: 10/14/22 11:35 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/28/22 Prep Date/Time(s) 10/20/22 05:39 Analysis Date/Time(s) 10/21/22 10:13 Client ID: 4101-PW10I Lab ID: CF15781-06 Sampled: 10/13/22 13:45 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/20/22 03:51 Client ID: 4101-PW10D Lab ID: CF15781-07 Sampled: 10/13/22 14:10 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/20/22 04:24 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 115 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4101-PW13I Lab ID: CF15781-08 Sampled: 10/12/22 13:10 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/18/22 03:17 Client ID: 4101-PW13I Lab ID: CF15781-08RE1 Sampled: 10/12/22 13:10 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/19/22 21:11 Client ID: 4101-PW14D Lab ID: CF15781-09 Sampled: 10/13/22 11:20 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/20/22 04:53 Client ID: 4101-PW15D Lab ID: CF15781-10 Sampled: 10/13/22 10:35 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/18/22 03:46 Client ID: 4101-PW15D Lab ID: CF15781-30RE1 Sampled: 10/13/22 10:35 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/19/22 21:40 Client ID: 4101-PW16D Lab ID: CF15781-11 Sampled: 10/13/22 09:35 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/18/22 04:14 Client ID: 4101-PW16D Lab ID: CF15781-31RE1 Sampled: 10/13/22 09:35 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 5030B_MIS Hold Date/Time(s) 10/27/22 Prep Date/Time(s) 10/18/22 18:22 Analysis Date/Time(s) 10/19/22 22:13 Client ID: 4301-TripBlank Lab ID: CF15781-12 Sampled: 10/12/22 11:40 Received: 10/15/22 10:25 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 10/26/22 Prep Date/Time(s) 10/17/22 15:06 Analysis Date/Time(s) 10/17/22 20:37 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 115 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4301-MW3C Lab ID: CF14375-01 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 28 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 5.0 0.21 1.0 ug/L EPA 8260D 1,2-Dichlorobenzene 0.41 J 0.19 1.0 ug/L EPA 8260D 1,2-Dichloroethane 1.3 0.21 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.1 0.19 1.0 ug/L EPA 8260D Benzene 0.97 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 64 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 18 0.15 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 0.56 J 0.21 1.0 ug/L EPA 8260D Vinyl chloride 15 0.32 1.0 ug/L EPA 8260D Client ID: 4301-MW3C Lab ID: CF34375-01RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 0.44 1 0.12 1.0 ug/L EPA 8260D Client ID: 4301-MW6 Lab ID: CF14375-02 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 6.2 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.3 0.19 1.0 ug/L EPA 8260D Benzene 0.64 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 2.4 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 5.5 0.15 1.0 ug/L EPA 8260D Vinyl chloride 2.0 0.32 1.0 ug/L EPA 8260D Client ID: 4301-MW6 Lab ID: CF34375-02RE1 Analvte Results Flag MDL PQL Units Method Notes Chloroethane 2.2 0.23 1.0 uq/L EPA 8260D I Client ID: 4101-MW12A Lab ID: CF14375-03 Analvte Results Flag MDL PQL Units Method Notes Chlorobenzene 6.9 0.17 1.0 ug/L EPA 8260D Client ID: 4101-MW12B Lab ID: CF14375-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 2.3 0.19 1.0 ug/L EPA 8260D Chlorobenzene 8.0 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.5 0.15 1.0 ug/L EPA 8260D Client ID: 4101-MW12D Lab ID: CF14375-05 Analvte Results Flag MDL PQL Units Method Notes Methylene chloride 0.47 1 0.23 1.0 uq/L EPA 8260D 0-01 I Client ID: 4101-MW15A Lab ID: CF14375-06 Analvte Results Flag MDL PQL Units Method Notes 1,2-Dichlorobenzene 1.4 0.19 1.0 ug/L EPA 8260D 1,2-Dichloropropane 0.46 J 0.10 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 2.2 0.19 1.0 ug/L EPA 8260D Chlorobenzene 170 0.17 1.0 ug/L EPA 8260D Client ID: 4301-OWDR2 Lab ID: CF14375-07 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 130 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 50 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 7.8 D 1.0 5.0 ug/L EPA 8260D Chlorobenzene 72 D 0.85 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 220 D 0.75 5.0 ug/L EPA 8260D chloride 21 1.6 5.0 EPA 8260D Client ID: 4301-OWDR2 Lab ID: CF14375-07RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 5.2 D 0.60 5.0 ug/L EPA 8260D Chloroethane 23 D 1.2 5.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 115 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4301-OWLFS2 Lab ID: CF14375-08 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 0.78 J 0.13 1.0 ug/L EPA 8260D Benzene 1.6 0.15 1.0 ug/L EPA 8260D Chlorobenzene 1.4 0.17 1.0 ug/L EPA 8260D Vinyl chloride 0.48 J 0.32 1.0 ug/L EPA 8260D Client ID: 4301-PW5D Lab ID: CF14375-09 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 190 D 1.3 10 ug/L EPA 8260D 1,2-Dichloroethane 17 D 2.1 10 ug/L EPA 8260D Chlorobenzene 150 D 1.7 10 ug/L EPA 8260D cis-1,2-Dichloroethene 5.4 ]D 1.5 10 ug/L EPA 8260D Vinyl chloride 6.2 ]D 3.2 10 ug/L EPA 8260D Client ID: 4301-PW5D Lab ID: CF34375-09RE2 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 7.7 ]D 1.2 10 ug/L EPA 8260D Client ID: 4301-PW4I Lab ID: CF14375-10 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 39 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 17 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 20 D 1.0 5.0 ug/L EPA 8260D 1,4-Dichlorobenzene 3.0 ]D 0.95 5.0 ug/L EPA 8260D Chlorobenzene 53 D 0.85 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 120 D 0.75 5.0 ug/L EPA 8260D Tetrachloroethene 9.0 D 0.85 5.0 ug/L EPA 8260D Trichloroethene 30 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 35 D 1.6 5.0 ug/L EPA 8260D Client ID: 4301-PW4I Lab ID: CF34375-10RE2 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 9.0 D 0.60 5.0 ug/L EPA 8260D Client ID: 4301-PWSF1 Lab ID: CF14375-12 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 15000 D 130 1000 ug/L EPA 8260D 1,1-Dichloroethene 12000 D 210 1000 ug/L EPA 8260D 1,2-Dichloroethane 3100 D 210 1000 ug/L EPA 8260D 2-Butanone 6200 D 1300 5000 ug/L EPA 8260D Chlorobenzene 22000 D 170 1000 ug/L EPA 8260D cis-1,2-Dichloroethene 39000 D 150 1000 ug/L EPA 8260D m,p-Xylenes 710 ]D 170 2000 ug/L EPA 8260D Methylene chloride 5800 D 230 1000 ug/L EPA 8260D 0-01 Tetrachloroethene 4500 D 170 1000 ug/L EPA 8260D Toluene 5100 D 140 1000 ug/L EPA 8260D Trichloroethene 2100 D 150 1000 ug/L EPA 8260D Vinyl chloride 11000 D 320 1000 ug/L EPA 8260D Xylenes (Total) 710 ]D 450 3000 ug/L EPA 8260D Client ID: 4301-PWSF3 Lab ID: CF34375-12RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 25000 D 120 1000 ug/L EPA 8260D Chloroethane 1300 D 230 1000 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 115 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4301-W4A Lab ID: CF34375-13RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 5.2 0.12 1.0 ug/L EPA 8260D 1,1-Dichloroethane 31 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 8.8 0.21 1.0 ug/L EPA 8260D Benzene 0.99 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 3.9 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 34 0.15 1.0 ug/L EPA 8260D Methylene chloride 1.1 0.23 1.0 ug/L EPA 8260D Tetrachloroethene 1.2 0.17 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 0.51 J 0.21 1.0 ug/L EPA 8260D Trichloroethene 2.1 0.15 1.0 ug/L EPA 8260D Client ID: 4301-W4A Lab ID: CF14375-13RE2 Analvte Results Flag MDL PQL Units Method Notes 1,2-Dichloroethane 0.93 1 0.21 1.0 ug/L EPA 8260D Vinyl chloride 25 0.32 1.0 uq/L EPA 8260D I Client ID: 4301-SW3 Lab ID: CF14376-02 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 0.88 J 0.13 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.2 0.15 1.0 ug/L EPA 8260D Client ID: 4301-SW4 Lab ID: CF14376-03RE2 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 1.4 0.12 1.0 ug/L EPA 8260D 1,1-Dichloroethane 12 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 4.2 0.21 1.0 ug/L EPA 8260D 1,2-Dichloroethane 1.1 0.21 1.0 ug/L EPA 8260D 3-05 Chlorobenzene 1.8 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 18 0.15 1.0 ug/L EPA 8260D Vinyl chloride 19 0.32 1.0 ug/L EPA 8260D Client ID: 4101-MW3 Lab ID: CF35781-01RE1 Analvte Results Flag MDL PQL Units Method Notes Methylene chloride 0.98 1 0.23 1.0 ug/L EPA 8260D 0-01 Client ID: 4301-PW3D Lab ID: CF15781-03 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 620 D 60 500 ug/L EPA 8260D 1,1-Dichloroethane 540 D 65 500 ug/L EPA 8260D 1,2-Dichloroethane 12000 D 100 500 ug/L EPA 8260D Benzene 240 ]D 75 500 ug/L EPA 8260D Chlorobenzene 20000 D 85 500 ug/L EPA 8260D cis-1,2-Dichloroethene 380 ]D 75 500 ug/L EPA 8260D Tetrachloroethene 1900 D 85 500 ug/L EPA 8260D Toluene 680 D 70 500 ug/L EPA 8260D Trichloroethene 4200 D 75 500 ug/L EPA 8260D Client ID: 4301-PW3D Lab ID: CF35781-03RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 1300 D 100 500 ug/L EPA 8260D Methylene chloride 1400 D 120 500 ug/L EPA 8260D 0-01 Client ID: 4301-PW6I Lab ID: CF15781-04 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 8.3 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 2.0 0.21 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.2 0.19 1.0 ug/L EPA 8260D Chlorobenzene 5.2 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 12 0.15 1.0 ug/L EPA 8260D Vinyl chloride 1.6 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 115 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4301-PW6D Lab ID: CF35781-05RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 29 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 2.6 0.21 1.0 ug/L EPA 8260D Benzene 0.54 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 17 0.17 1.0 ug/L EPA 8260D Methylene chloride 1.1 0.23 1.0 ug/L EPA 8260D Toluene 0.75 J 0.14 1.0 ug/L EPA 8260D Vinyl chloride 2.6 0.32 1.0 ug/L EPA 8260D Client ID: 4101-PW10I Lab ID: CF15781-06 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 4.9 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 3.1 0.19 1.0 ug/L EPA 8260D Benzene 1.3 0.15 1.0 ug/L EPA 8260D Chlorobenzene 3.3 0.17 1.0 ug/L EPA 8260D chloride 1.7 0.32 1.0 uq/L EPA 8260D I Client ID: 4101-PW10D Lab ID: CF15781-07 Analvte Results Flag MDL PQL Units Method Notes Methylene chloride 1.3 0.23 1.0 ug/L EPA 8260D 0-01 Client ID: 4101-PW13I Lab ID: CF15781-08 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 76 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 1.4 0.21 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 0.91 J 0.19 1.0 ug/L EPA 8260D Benzene 2.0 0.15 1.0 ug/L EPA 8260D Chlorobenzene 11 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 6.9 0.15 1.0 ug/L EPA 8260D Tetrachloroethene 0.53 J 0.17 1.0 ug/L EPA 8260D Toluene 0.59 J 0.14 1.0 ug/L EPA 8260D chloride 7.1 0.32 1.0 uq/L EPA 8260D I Client ID: 4101-PW13I Lab ID: CF15781-08RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 1.4 0.21 1.0 ug/L EPA 8260D Chloroethane 2.0 0.23 1.0 ug/L EPA 8260D 3-04 Client ID: 4101-PW14D Lab ID: CF15781-09 Analvte Results Flag MDL PQL Units Method Notes 2-Butanone 4.3 J 1.3 5.0 ug/L EPA 8260D Acetone 15 J 10 20 ug/L EPA 8260D 0-01 Chlorobenzene 1.3 0.17 1.0 ug/L EPA 8260D Chloroform 3.5 0.18 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.77 J 0.15 1.0 ug/L EPA 8260D Ethylbenzene 0.58 J 0.13 1.0 ug/L EPA 8260D m,p-Xylenes 2.7 0.17 2.0 ug/L EPA 8260D Methylene chloride 0.52 J 0.23 1.0 ug/L EPA 8260D 0-01 o-Xylene 1.3 0.065 1.0 ug/L EPA 8260D Toluene 2.2 0.14 1.0 ug/L EPA 8260D Vinyl chloride 0.58 J 0.32 1.0 ug/L EPA 8260D 3.9 0.45 3.0 EPA 8260D Client ID: 4101-PW15D Lab ID: CF15781-10 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 21 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 0.61 J 0.21 1.0 ug/L EPA 8260D Chlorobenzene 3.9 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 29 0.15 1.0 ug/L EPA 8260D Vinyl chloride 1.2 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 115 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4101-PW15D Lab ID: CF15781-10RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 6.1 0.21 1.0 ug/L EPA 8260D Methylene chloride 1.0 0.23 1.0 ug/L EPA 8260D 0-01 Client ID: 4101-PW16D Lab ID: CF15781-11 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 23 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 0.62 J 0.21 1.0 ug/L EPA 8260D Benzene 0.70 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 50 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 39 0.15 1.0 ug/L EPA 8260D Vinyl chloride 5.3 0.32 1.0 ug/L EPA 8260D Client ID: 4101-PW16D Lab ID: CF15781-11RE1 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 9.9 0.21 1.0 ug/L EPA 8260D Methylene chloride 0.53 J 0.23 1.0 ug/L EPA 8260D 0-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW3C Lab Sample ID:CF14375-01 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1,1,1-Trichloroethane [71-55-6]A 0.44 J ug/L 1 0.12 1.0 2J27021 EPA 8260D 10/27/22 19:51 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1.1-Dichloroethane [75-34-3]A 28 ug/L 1 0.13 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY 1.1-Dichloroethene [75-35-4]A 5.0 ug/L 1 0.21 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY QV-01 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1,2-Dichlorobenzene [95-50-1]A 0.41 J ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY 1,2-Dichloroethane [107-06-2]A 1.3 ug/L 1 0.21 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY 1,4-Dichlorobenzene [106-46-7]A 1.1 ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 2125020 EPA 8260D 10/26/22 00:18 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 00:18 RKY Benzene [71-43-2]A 0.97 J ug/L 1 0.15 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY QV-01 Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY QV-01 Chlorobenzene [108-90-7]A 64 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY cis-1,2-Dichloroethene [156-59-2]A 18 ug/L 1 0.15 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 00:18 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY trans-1,2-Dichloroethene [156-60-5]A 0.56 J ug/L 1 0.21 1.0 2J25020 EPA 8260D 10/26/22 00:18 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY QV-01 Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 00:18 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 00:18 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 Of 1 1 5J (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW3C Lab Sample ID:CF14375-01 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 15 ug/L 1 0.32 1.0 2325020 EPA 8260D 10/26/22 00:18 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 00:18 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 109 % 53-136 2J25020 EPA 6260D 10126122 00:16 RKY 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 2J27021 EPA 6260D 10127122 19:51 RKY Dlbromofluoromethane 51 1 50.0 101 % 67-129 2J25020 EPA 6260D 10126122 00:16 RKY Dlbromofluoromethane 57 1 50.0 115 % 67-129 2J27021 EPA 6260D 1012712219:51 RKY Toluene-d8 49 1 50.0 98 % 59-134 2J25020 EPA 6260D 10126122 00:16 RKY Toluene-d8 53 1 50.0 107 % 59-134 2J27021 EPA 6260D 1012712219:51 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW6 Lab Sample ID:CF14375-02 Received: 10/20/22 11:00 Matrix: Water Sampled:10/19/22 08:20 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,1-Dichloroethane [75-34-3]A 6.2 ug/L 1 0.13 1.0 2J25020 EPA 8260D 10/26/22 00:46 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY QV-01 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.3 ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 00:46 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2125020 EPA 8260D 10/26/22 00:46 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 00:46 RKY Benzene [71-43-2]A 0.64 J ug/L 1 0.15 1.0 2J25020 EPA 8260D 10/26/22 00:46 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY QV-01 Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY QV-01 Chlorobenzene [108-90-7]A 2.4 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 00:46 RKY Chloroethane [75-00-3]A 2.2 ug/L 1 0.23 1.0 2J31016 EPA 8260D 10/31/22 21:56 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY cis-1,2-Dichloroethene [156-59-2]A 5.5 ug/L 1 0.15 1.0 2.125020 EPA 8260D 10/26/22 00:46 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 00:46 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 00:46 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 00:46 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW6 Lab Sample ID:CF14375-02 Received: 10/20/22 11:00 Matrix: Water Sampled:10/19/22 08:20 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 2.0 ug/L 1 0.32 1.0 2325020 EPA 8260D 10/26/22 00:46 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 00:46 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 2J25020 EPA 6260D 10126122 00:46 RKY 4-Bromofluorobenzene 62 1 60.0 103 % 53-136 2J31016 EPA 6260D 10131122 21:56 RKY Dlbromofluoromethane 54 1 50.0 108 % 67-129 2J25020 EPA 6260D 10126122 00:46 RKY Dlbromofluoromethane 71 1 60.0 119 % 67-129 2J31016 EPA 6260D 10131122 21:56 RKY Toluene-d8 53 1 50.0 105 % 59-134 2J25020 EPA 6260D 10126122 00:46 RKY Toluene-d8 64 1 60.0 107 % 59-134 2J31016 EPA 6260D 10131122 21:56 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12A Lab Sample ID:CF14375-03 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 11:30 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY QV-01 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 2125020 EPA 8260D 10/26/22 01:15 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 01:15 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY QV-01 Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY QV-01 Chlorobenzene [108-90-7]A 6.9 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 01:15 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 u ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 01:15 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY QV-01 Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 01:15 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 01:15 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12A Lab Sample ID:CF14375-03 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 11:30 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J25020 EPA 8260D 10/26/22 01:15 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 01:15 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 2J25020 EPA 6260D 10126122 01:15 RKY Dibromofluoromethane 54 1 50.0 108 % 67-129 2J25020 EPA 6260D 10126122 01:15 RKY Toluene-d8 53 1 50.0 106 % 59-134 2J25020 EPA 6260D 10126122 01:15 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12B Lab Sample ID:CF14375-04 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 13:15 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY QV-01 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY 1,4-Dichlorobenzene [306-46-7]^ 2.3 ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 01:43 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2125020 EPA 8260D 10/26/22 01:43 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 01:43 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY QV-01 Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY QV-01 Chlorobenzene [108-90-7]^ 8.0 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 01:43 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY cis-1,2-Dichloroethene [156-59-2]^ 1.5 ug/L 1 0.15 1.0 2.125020 EPA 8260D 10/26/22 01:43 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 01:43 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 01:43 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 01:43 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12B Lab Sample ID:CF14375-04 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 13:15 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J25020 EPA 8260D 10/26/22 01:43 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 01:43 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 57 1 50.0 115 % 53-136 2J25020 EPA 6260D 10126122 01:43 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 2J25020 EPA 6260D 10126122 01:43 RKY Toluene-d8 50 1 50.0 100 % 59-134 2J25020 EPA 6260D 10126122 01:43 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 S Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12D Lab Sample ID:CF14375-05 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 10:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY QV-01 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 2125020 EPA 8260D 10/26/22 02:12 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 02:12 RKY Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY QV-01 Chlorobenzene [108-90-7]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 02:12 RKY Methylene chloride [75-09-2]^ 0.47 J ug/L 1 0.23 1.0 2J25020 EPA 8260D 10/26/22 02:12 RKY 0-01 o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Styrene [100-42-5]^ 0.11 u ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 02:12 RKY Vinyl acetate [108-05-4]^ 0.95 Ll ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 02:12 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW12D Lab Sample ID:CF14375-05 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 10:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J25020 EPA 8260D 10/26/22 02:12 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 02:12 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 2J25020 EPA 6260D 10126122 02:12 RKY Dibromofluoromethane 53 1 50.0 106 % 67-129 2J25020 EPA 6260D 10126122 02:12 RKY Toluene-d8 51 1 50.0 101 % 59-134 2J25020 EPA 6260D 10126122 02:12 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW15A Lab Sample ID:CF14375-06 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 10:35 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analvte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY QV-01 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,2-Dichlorobenzene [95-50-1]A 1.4 ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 02:41 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY 1,2-Dichloropropane [78-87-5]A 0.46 J ug/L 1 0.10 1.0 2J25020 EPA 8260D 10/26/22 02:41 RKY 1,4-Dichlorobenzene [106-46-7]A 2.2 ug/L 1 0.19 1.0 2J25020 EPA 8260D 10/26/22 02:41 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 2125020 EPA 8260D 10/26/22 02:41 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 02:41 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY QV-01 Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY QV-01 Chlorobenzene [108-90-7]A 170 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 02:41 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 02:41 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY QV-01 Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 02:41 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 02:41 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW15A Lab Sample ID:CF14375-06 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 10:35 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J25020 EPA 8260D 10/26/22 02:41 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 02:41 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 2J25020 EPA 6260D 10126122 02:41 RKY Dibromofluoromethane 48 1 50.0 96 % 67-129 2J25020 EPA 6260D 10126122 02:41 RKY Toluene-d8 49 1 50.0 97 % 59-134 2J25020 EPA 6260D 10126122 02:41 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-OWDR2 Lab Sample ID:CF14375-07 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 08:40 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1,1,1-Trichloroethane [71-55-6]A 5.2 D ug/L 5 0.60 5.0 2J31016 EPA 8260D 10/31/22 22:53 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 1.4 LID ug/L 5 1.4 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1,1,2-Trichloroethane [79-00-5]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1.1-Dichloroethane [75-34-3]A 130 D ug/L 5 0.65 5.0 2J25020 EPA 8260D 10/26/22 03:09 RKY 1.1-Dichloroethene [75-35-4]A 50 D ug/L 5 1.0 5.0 2J25020 EPA 8260D 10/26/22 03:09 RKY 1,2,3-Trichloropropane [96-18-4]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 2.4 LID ug/L 5 2.4 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY QV-01 1,2-Dibromoethane [106-93-4]A 3.3 LID ug/L 5 3.3 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1,2-Dichlorobenzene [95-50-1]A 0.95 LID ug/L 5 0.95 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1.2-Dichloroethane [107-06-2]A 7.8 D ug/L 5 1.0 5.0 2J25020 EPA 8260D 10/26/22 03:09 RKY 1,2-Dichloropropane [78-87-5]A 0.50 LID ug/L 5 0.50 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 1,4-Dichlorobenzene [106-46-7]A 0.95 LID ug/L 5 0.95 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY 2-Butanone [78-93-3]A 6.5 LID ug/L 5 6.5 25 2125020 EPA 8260D 10/26/22 03:09 RKY 2-Hexanone [591-78-6]A 4.4 LID ug/L 5 4.4 25 2125020 EPA 8260D 10/26/22 03:09 RKY 4-Methyl-2-pentanone [108-10-1]A 5.5 LID ug/L 5 5.5 25 2125020 EPA 8260D 10/26/22 03:09 RKY Acetone [67-64-1]A 50 LID ug/L 5 50 100 2125020 EPA 8260D 10/26/22 03:09 RKY Acrylonitrile [107-13-1]A 18 LID ug/L 5 18 50 2125020 EPA 8260D 10/26/22 03:09 RKY Benzene[71-43-2]A 0.75 LID ug/L 5 0.75 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Bromochloromethane [74-97-5]A 2.4 LID ug/L 5 2.4 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Bromodichloromethane [75-27-4]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY QV-01 Bromoform [75-25-2]A 1.1 LID ug/L 5 1.1 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Bromomethane [74-83-9]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Carbon disulfide [75-15-0]A 7.5 LID ug/L 5 7.5 25 2125020 EPA 8260D 10/26/22 03:09 RKY Carbon tetrachloride [56-23-5]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY QV-01 Chlorobenzene [108-90-7]A 72 D ug/L 5 0.85 5.0 2J25020 EPA 8260D 10/26/22 03:09 RKY Chloroethane [75-00-3]A 23 D ug/L 5 1.2 5.0 2J31016 EPA 8260D 10/31/22 22:53 RKY Chloroform [67-66-3]A 0.90 LID ug/L 5 0.90 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Chloromethane [74-87-3]A 0.65 LID ug/L 5 0.65 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY cis-1,2-Dichloroethene [156-59-2]A 220 D ug/L 5 0.75 5.0 2J25020 EPA 8260D 10/26/22 03:09 RKY cis-1,3-Dichloropropene [10061-01-5]A 1.0 LID ug/L 5 1.0 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Dibromochloromethane [124-48-1]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Dibromomethane [74-95-3]A 1.4 LID ug/L 5 1.4 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Ethylbenzene [100-41-4]A 0.65 LID ug/L 5 0.65 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Iodomethane[74-88-4]A 8.5 LID ug/L 5 8.5 25 2125020 EPA 8260D 10/26/22 03:09 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.85 LID ug/L 5 0.85 10 2125020 EPA 8260D 10/26/22 03:09 RKY Methylene chloride [75-09-2]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY o-Xylene [95-47-6]A 0.32 LID ug/L 5 0.32 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Styrene [100-42-5]A 0.55 LID ug/L 5 0.55 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Tetrachloroethene [127-18-4]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Toluene [108-88-3]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY trans-1,2-Dichloroethene [156-60-5]A 1.0 LID ug/L 5 1.0 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.75 LID ug/L 5 0.75 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 3.5 LID ug/L 5 3.5 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY QV-01 Trichloroethene [79-01-6]A 0.75 LID ug/L 5 0.75 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Trichlorofluoromethane [75-69-4]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 03:09 RKY Vinyl acetate [108-05-4]A 4.8 LID ug/L 5 4.8 25 2125020 EPA 8260D 10/26/22 03:09 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 1 1 cJ (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-OWDR2 Lab Sample ID:CF14375-07 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 08:40 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 21 D ug/L 5 1.6 5.0 2325020 EPA 8260D 10/26/22 03:09 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 2J25020 EPA 8260D 10/26/22 03:09 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analured By Notes 4-Bromofluorobenzene 54 1 50.0 107 % 53-136 2J25020 EPA 6260D 10126122 03:09 RKY 4-Bromofluorobenzene 62 1 60.0 104 % 53-136 2J31016 EPA 6260D 10131122 22:53 RKY Dlbromofluoromethane 50 1 50.0 100 % 67-129 2J25020 EPA 6260D 10126122 03:09 RKY Dlbromofluoromethane 72 1 60.0 121 % 67-129 2J31016 EPA 6260D 10131122 22:53 RKY Toluene-d8 49 1 50.0 98 % 59-134 2J25020 EPA 6260D 10126122 03:09 RKY Toluene-d8 64 1 60.0 107 % 59-134 2J31016 EPA 6260D 10131122 22:53 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-OWLFS2 Lab Sample ID:CF14375-08 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 13:45 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,1-Dichloroethane [75-34-3]A 0.78 J ug/L 1 0.13 1.0 2J25020 EPA 8260D 10/26/22 03:38 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY QV-01 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2125020 EPA 8260D 10/26/22 03:38 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 03:38 RKY Benzene [71-43-2]A 1.6 ug/L 1 0.15 1.0 2J25020 EPA 8260D 10/26/22 03:38 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY QV-01 Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY QV-01 Chlorobenzene [108-90-7]A 1.4 ug/L 1 0.17 1.0 2J25020 EPA 8260D 10/26/22 03:38 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 03:38 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 03:38 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 03:38 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-OWLFS2 Lab Sample ID:CF14375-08 Received: 10/20/22 11:00 Matrix: Water Sampled:10/17/22 13:45 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.48 J ug/L 1 0.32 1.0 2325020 EPA 8260D 10/26/22 03:38 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 03:38 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 106 % 53-136 2J25020 EPA 6260D 10126122 03:38 RKY Dlbromofluoromethane 50 1 50.0 99 % 67-129 2J25020 EPA 6260D 10126122 03:38 RKY Toluene-d8 51 1 50.0 101 % 59-134 2J25020 EPA 6260D 10126122 0338 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW51) Lab Sample ID:CF14375-09 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 1.7 LID ug/L 10 1.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,1,1-Trichloroethane [71-55-6]A 7.7 JD ug/L 10 1.2 10 2J31017 EPA 8260D 11/01/22 12:15 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 2.8 LID ug/L 10 2.8 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,1,2-Trichloroethane [79-00-5]A 1.4 LID ug/L 10 1.4 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,1-Dichloroethane [75-34-3]A 190 D ug/L 10 1.3 10 2J25020 EPA 8260D 10/26/22 04:07 RKY 1,1-Dichloroethene [75-35-4]A 2.1 LID ug/L 10 2.1 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,2,3-Trichloropropane [96-18-4]A 2.3 LID ug/L 10 2.3 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 4.8 LID ug/L 10 4.8 10 2125020 EPA 8260D 10/26/22 04:07 RKY QV-01 1,2-Dibromoethane [106-93-4]A 6.6 LID ug/L 10 6.6 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,2-Dichlorobenzene [95-50-1]A 1.9 LID ug/L 10 1.9 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,2-Dichloroethane [107-06-2]A 17 D ug/L 10 2.1 10 2J25020 EPA 8260D 10/26/22 04:07 RKY 1,2-Dichloropropane [78-87-5]A 1.0 LID ug/L 10 1.0 10 2125020 EPA 8260D 10/26/22 04:07 RKY 1,4-Dichlorobenzene [106-46-7]A 1.9 LID ug/L 10 1.9 10 2125020 EPA 8260D 10/26/22 04:07 RKY 2-Butanone [78-93-3]A 13 LID ug/L 10 13 50 2125020 EPA 8260D 10/26/22 04:07 RKY 2-Hexanone [591-78-6]A 8.8 LID ug/L 10 8.8 50 2125020 EPA 8260D 10/26/22 04:07 RKY 4-Methyl-2-pentanone [108-10-1]A 11 LID ug/L 10 11 50 2125020 EPA 8260D 10/26/22 04:07 RKY Acetone [67-64-1]A 100 LID ug/L 10 100 200 2125020 EPA 8260D 10/26/22 04:07 RKY Acrylonitrile [107-13-1]A 35 LID ug/L 10 35 100 2125020 EPA 8260D 10/26/22 04:07 RKY Benzene[71-43-2]A 1.5 LID ug/L 10 1.5 10 2125020 EPA 8260D 10/26/22 04:07 RKY Bromochloromethane [74-97-5]A 4.8 LID ug/L 10 4.8 10 2125020 EPA 8260D 10/26/22 04:07 RKY Bromodichloromethane [75-27-4]A 1.7 LID ug/L 10 1.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY QV-01 Bromoform [75-25-2]A 2.2 LID ug/L 10 2.2 10 2125020 EPA 8260D 10/26/22 04:07 RKY Bromomethane [74-83-9]A 1.4 LID ug/L 10 1.4 10 2125020 EPA 8260D 10/26/22 04:07 RKY Carbon disulfide [75-15-0]A 15 LID ug/L 10 15 50 2125020 EPA 8260D 10/26/22 04:07 RKY Carbon tetrachloride [56-23-5]A 1.7 LID ug/L 10 1.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY QV-01 Chlorobenzene [108-90-7]A 150 D ug/L 10 1.7 10 2J25020 EPA 8260D 10/26/22 04:07 RKY Chloroethane [75-00-3]A 2.3 UD ug/L 10 2.3 10 2125020 EPA 8260D 10/26/22 04:07 RKY Chloroform [67-66-3]A 1.8 U D ug/L 10 1.8 10 2125020 EPA 8260D 10/26/22 04:07 RKY Chloromethane [74-87-3]A 1.3 LID ug/L 10 1.3 10 2125020 EPA 8260D 10/26/22 04:07 RKY cis-1,2-Dichloroethene [156-59-2]A 5.4 JD ug/L 10 1.5 10 2J25020 EPA 8260D 10/26/22 04:07 RKY cis-1,3-Dichloropropene [10061-01-5]A 2.0 LID ug/L 10 2.0 10 2125020 EPA 8260D 10/26/22 04:07 RKY Dibromochloromethane [124-48-1]A 1.7 LID ug/L 10 1.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY Dibromomethane [74-95-3]A 2.7 LID ug/L 10 2.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY Ethylbenzene [100-41-4]A 1.3 LID ug/L 10 1.3 10 2125020 EPA 8260D 10/26/22 04:07 RKY Iodomethane[74-88-4]A 17 LID ug/L 10 17 50 2125020 EPA 8260D 10/26/22 04:07 RKY m,p-Xylenes[108-38-3/106-42-3]A 1.7 LID ug/L 10 1.7 20 2125020 EPA 8260D 10/26/22 04:07 RKY Methylene chloride [75-09-2]A 2.3 LID ug/L 10 2.3 10 2125020 EPA 8260D 10/26/22 04:07 RKY o-Xylene [95-47-6]A 0.65 LID ug/L 10 0.65 10 2125020 EPA 8260D 10/26/22 04:07 RKY Styrene [100-42-5]A 1.1 LID ug/L 10 1.1 10 2125020 EPA 8260D 10/26/22 04:07 RKY Tetrachloroethene [127-18-4]A 1.7 LID ug/L 10 1.7 10 2125020 EPA 8260D 10/26/22 04:07 RKY Toluene [108-88-3]A 1.4 LID ug/L 10 1.4 10 2125020 EPA 8260D 10/26/22 04:07 RKY trans-1,2-Dichloroethene [156-60-5]A 2.1 LID ug/L 10 2.1 10 2125020 EPA 8260D 10/26/22 04:07 RKY trans-1,3-Dichloropropene [10061-02-6]A 1.5 LID ug/L 10 1.5 10 2125020 EPA 8260D 10/26/22 04:07 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 7.0 LID ug/L 10 7.0 10 2125020 EPA 8260D 10/26/22 04:07 RKY QV-01 Trichloroethene [79-01-6]A 1.5 LID ug/L 10 1.5 10 2125020 EPA 8260D 10/26/22 04:07 RKY Trichlorofluoromethane [75-69-4]A 2.4 LID ug/L 10 2.4 10 2125020 EPA 8260D 10/26/22 04:07 RKY Vinyl acetate [108-05-4]A 9.5 LID ug/L 10 9.5 50 2125020 EPA 8260D 10/26/22 04:07 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW5D Lab Sample ID:CF14375-09 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 6.2 JD ug/L 10 3.2 10 2325020 EPA 8260D 10/26/22 04:07 RKY Xylenes (Total) [1330-20-7]^ 4.5 UD ug/L 10 4.5 30 2J25020 EPA 8260D 10/26/22 04:07 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 106 % 53-136 2J25020 EPA 6260D 10126122 04:07 RKY 4-Bromofluorobenzene 62 1 60.0 104 % 53-136 2J31017 EPA 6260D 11101122 12:15 RKY Dlbromofluoromethane 53 1 50.0 105 % 67-129 2J25020 EPA 6260D 10126122 04:07 RKY Dlbromofluoromethane 71 1 60.0 119 % 67-129 2J31017 EPA 6260D 11101122 12:15 RKY Toluene-d8 51 1 50.0 101 % 59-134 2J25020 EPA 6260D 10126122 04:07 RKY Toluene-d8 64 1 60.0 107 % 59-134 2J31017 EPA 6260D 11101122 12:15 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW4I Lab Sample ID:CF14375-10 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1,1,1-Trichloroethane [71-55-6]A 9.0 D ug/L 5 0.60 5.0 2J31017 EPA 8260D 11/01/22 12:44 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 1.4 LID ug/L 5 1.4 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1,1,2-Trichloroethane [79-00-5]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1.1-Dichloroethane [75-34-3]A 39 D ug/L 5 0.65 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY 1.1-Dichloroethene [75-35-4]A 17 D ug/L 5 1.0 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY 1,2,3-Trichloropropane [96-18-4]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 2.4 LID ug/L 5 2.4 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY QV-01 1,2-Dibromoethane [106-93-4]A 3.3 LID ug/L 5 3.3 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1,2-Dichlorobenzene [95-50-1]A 0.95 LID ug/L 5 0.95 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1.2-Dichloroethane [107-06-2]A 20 D ug/L 5 1.0 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY 1,2-Dichloropropane [78-87-5]A 0.50 LID ug/L 5 0.50 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY 1.4-Dichlorobenzene [106-46-7]A 3.0 JD ug/L 5 0.95 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY 2-Butanone [78-93-3]A 6.5 LID ug/L 5 6.5 25 2125020 EPA 8260D 10/26/22 04:35 RKY 2-Hexanone [591-78-6]A 4.4 LID ug/L 5 4.4 25 2125020 EPA 8260D 10/26/22 04:35 RKY 4-Methyl-2-pentanone [108-10-1]A 5.5 LID ug/L 5 5.5 25 2125020 EPA 8260D 10/26/22 04:35 RKY Acetone [67-64-1]A 50 LID ug/L 5 50 100 2125020 EPA 8260D 10/26/22 04:35 RKY Acrylonitrile [107-13-1]A 18 LID ug/L 5 18 50 2125020 EPA 8260D 10/26/22 04:35 RKY Benzene[71-43-2]A 0.75 LID ug/L 5 0.75 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Bromochloromethane [74-97-5]A 2.4 LID ug/L 5 2.4 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Bromodichloromethane [75-27-4]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY QV-01 Bromoform [75-25-2]A 1.1 LID ug/L 5 1.1 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Bromomethane [74-83-9]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Carbon disulfide [75-15-0]A 7.5 LID ug/L 5 7.5 25 2125020 EPA 8260D 10/26/22 04:35 RKY Carbon tetrachloride [56-23-5]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY QV-01 Chlorobenzene [108-90-7]A 53 D ug/L 5 0.85 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY Chloroethane [75-00-3]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Chloroform [67-66-3]A 0.90 LID ug/L 5 0.90 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Chloromethane [74-87-3]A 0.65 LID ug/L 5 0.65 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY cis-1,2-Dichloroethene [156-59-2]A 120 D ug/L 5 0.75 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY cis-1,3-Dichloropropene [10061-01-5]A 1.0 LID ug/L 5 1.0 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Dibromochloromethane [124-48-1]A 0.85 LID ug/L 5 0.85 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Dibromomethane [74-95-3]A 1.4 LID ug/L 5 1.4 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Ethylbenzene [100-41-4]A 0.65 LID ug/L 5 0.65 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Iodomethane[74-88-4]A 8.5 LID ug/L 5 8.5 25 2125020 EPA 8260D 10/26/22 04:35 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.85 LID ug/L 5 0.85 10 2125020 EPA 8260D 10/26/22 04:35 RKY Methylene chloride [75-09-2]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY o-Xylene [95-47-6]A 0.32 LID ug/L 5 0.32 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Styrene [100-42-5]A 0.55 LID ug/L 5 0.55 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Tetrachloroethene [127-18-4]A 9.0 D ug/L 5 0.85 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY Toluene [108-88-3]A 0.70 LID ug/L 5 0.70 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY trans-1,2-Dichloroethene [156-60-5]A 1.0 LID ug/L 5 1.0 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.75 LID ug/L 5 0.75 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY trans- l,4-Dichloro-2-butene [110-57-6]A 3.5 LID ug/L 5 3.5 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY QV-01 Trichloroethene [79-01-6]A 30 D ug/L 5 0.75 5.0 2J25020 EPA 8260D 10/26/22 04:35 RKY Trichlorofluoromethane [75-69-4]A 1.2 LID ug/L 5 1.2 5.0 2125020 EPA 8260D 10/26/22 04:35 RKY Vinyl acetate [108-05-4]A 4.8 LID ug/L 5 4.8 25 2125020 EPA 8260D 10/26/22 04:35 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 1 1 cJ (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW4I Lab Sample ID:CF14375-10 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 35 D ug/L 5 1.6 5.0 2325020 EPA 8260D 10/26/22 04:35 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 2J25020 EPA 8260D 10/26/22 04:35 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analured By Notes 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 2J25020 EPA 6260D 10126122 04:35 RKY 4-Bromofluorobenzene 63 1 60.0 105 % 53-136 2J31017 EPA 6260D 11101122 12:44 RKY Dlbromofluoromethane 52 1 50.0 103 % 67-129 2J25020 EPA 6260D 10126122 04:35 RKY Dlbromofluoromethane 67 1 60.0 112 % 67-129 2J31017 EPA 6260D 11101122 12:44 RKY Toluene-d8 49 1 50.0 99 % 59-134 2J25020 EPA 6260D 10126122 04:35 RKY Toluene-d8 63 1 60.0 105 % 59-134 2J31017 EPA 6260D 11101122 12:44 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW12I Lab Sample ID:CF14375-11 Received: 10/20/22 11:00 Matrix: Water Sampled:10/19/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY QV-01 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 2125020 EPA 8260D 10/26/22 05:04 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 2125020 EPA 8260D 10/26/22 05:04 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY QV-01 Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 2125020 EPA 8260D 10/26/22 05:04 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 2125020 EPA 8260D 10/26/22 05:04 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 2125020 EPA 8260D 10/26/22 05:04 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW12I Lab Sample ID:CF14375-11 Received: 10/20/22 11:00 Matrix: Water Sampled:10/19/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J25020 EPA 8260D 10/26/22 05:04 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J25020 EPA 8260D 10/26/22 05:04 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 2J25020 EPA 6260D 10126122 05:04 RKY Dibromofluoromethane 59 1 50.0 117 % 67-129 2J25020 EPA 6260D 10126122 05:04 RKY Toluene-d8 53 1 50.0 107 % 59-134 2J25020 EPA 6260D 10126122 05:04 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PWSF1 Lab Sample ID:CF14375-12 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 170 LID ug/L 1000 170 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,1,1-Trichloroethane [71-55-6]A 25000 D ug/L 1000 120 1000 2J31016 EPA 8260D 10/31/22 23:22 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 280 LID ug/L 1000 280 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,1,2-Trichloroethane [79-00-5]^ 140 LID ug/L 1000 140 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,1-Dichloroethane [75-34-3]A 15000 D ug/L 1000 130 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY 1,1-Dichloroethene [75-35-4]A 12000 D ug/L 1000 210 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY 1,2,3-Trichloropropane[96-18-4]^ 230 LID ug/L 1000 230 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 480 LID ug/L 1000 480 1000 2125020 EPA 8260D 10/26/22 05:32 RKY QV-01 1,2-Dibromoethane[106-93-4]^ 660 LID ug/L 1000 660 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,2-Dichlorobenzene [95-50-1]^ 190 LID ug/L 1000 190 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,2-Dichloroethane [107-06-2]A 3100 D ug/L 1000 210 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY 1,2-Dichloropropane [78-87-5]^ 100 LID ug/L 1000 100 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 1,4-Dichlorobenzene [106-46-7]^ 190 LID ug/L 1000 190 1000 2125020 EPA 8260D 10/26/22 05:32 RKY 2-Butanone [78-93-3]A 6200 D ug/L 1000 1300 5000 2J25020 EPA 8260D 10/26/22 05:32 RKY 2-Hexanone [591-78-6]^ 880 LID ug/L 1000 880 5000 2125020 EPA 8260D 10/26/22 05:32 RKY 4-Methyl-2-pentanone [108-10-1]^ 1100 LID ug/L 1000 1100 5000 2125020 EPA 8260D 10/26/22 05:32 RKY Acetone [67-64-1]^ 10000 LID ug/L 1000 10000 20000 2125020 EPA 8260D 10/26/22 05:32 RKY Acrylonitrile [107-13-1]^ 3500 LID ug/L 1000 3500 10000 2125020 EPA 8260D 10/26/22 05:32 RKY Benzene[71-43-2]^ 150 LID ug/L 1000 150 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Bromochloromethane [74-97-5]^ 480 LID ug/L 1000 480 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Bromodichloromethane [75-27-4]^ 170 LID ug/L 1000 170 1000 2125020 EPA 8260D 10/26/22 05:32 RKY QV-01 Bromoform [75-25-2]^ 220 LID ug/L 1000 220 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Bromomethane[74-83-9]^ 140 LID ug/L 1000 140 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Carbon disulfide [75-15-0]^ 1500 LID ug/L 1000 1500 5000 2125020 EPA 8260D 10/26/22 05:32 RKY Carbon tetrachloride [56-23-5]^ 170 LID ug/L 1000 170 1000 2125020 EPA 8260D 10/26/22 05:32 RKY QV-01 Chlorobenzene [108-90-7]A 22000 D ug/L 1000 170 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY Chloroethane [75-00-3]A 1300 D ug/L 1000 230 1000 2J31016 EPA 8260D 10/31/22 23:22 RKY Chloroform [67-66-3]^ 180 LID ug/L 1000 180 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Chloromethane [74-87-3]^ 130 LID ug/L 1000 130 1000 2125020 EPA 8260D 10/26/22 05:32 RKY cis-1,2-Dichloroethene [156-59-2]A 39000 D ug/L 1000 150 1000 2.125020 EPA 8260D 10/26/22 05:32 RKY cis-1,3-Dichloropropene [10061-01-5]^ 200 LID ug/L 1000 200 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Dibromochloromethane [124-48-1]^ 170 LID ug/L 1000 170 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Dibromomethane[74-95-3]^ 270 LID ug/L 1000 270 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Ethylbenzene[100-41-4]^ 130 LID ug/L 1000 130 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Iodomethane[74-88-4]^ 1700 LID ug/L 1000 1700 5000 2125020 EPA 8260D 10/26/22 05:32 RKY m,p-Xylenes[308-38-3/306-42-3]^ 710 JD ug/L 1000 170 2000 2J25020 EPA 8260D 10/26/22 05:32 RKY Methylene chloride [75-09-2]^ 5800 D ug/L 1000 230 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY 0-01 o-Xylene [95-47-6]^ 65 LID ug/L 1000 65 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Styrene [100-42-5]^ 110 LID ug/L 1000 110 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Tetrachloroethene [127-18-4]^ 4500 D ug/L 1000 170 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY Toluene [108-88-3]^ 5100 D ug/L 1000 140 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY trans-1,2-Dichloroethene [156-60-5]^ 210 LID ug/L 1000 210 1000 2125020 EPA 8260D 10/26/22 05:32 RKY trans-1,3-Dichloropropene [10061-02-6]^ 150 LID ug/L 1000 150 1000 2125020 EPA 8260D 10/26/22 05:32 RKY trans- l,4-Dichloro-2-butene [110-57-6]^ 700 LID ug/L 1000 700 1000 2125020 EPA 8260D 10/26/22 05:32 RKY QV-01 Trichloroethene [79-01-6]A 2100 D ug/L 1000 150 1000 2J25020 EPA 8260D 10/26/22 05:32 RKY Trichlorofluoromethane [75-69-4]^ 240 LID ug/L 1000 240 1000 2125020 EPA 8260D 10/26/22 05:32 RKY Vinyl acetate[108-05-4]^ 950 LID ug/L 1000 950 5000 2125020 EPA 8260D 10/26/22 05:32 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 1 1 cJ (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PWSF1 Lab Sample ID:CF14375-12 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 09:25 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 11000 D ug/L 1000 320 1000 2325020 EPA 8260D 10/26/22 05:32 RKY Xylenes(Total)[1330-20-7]^ 710 JD ug/L 1000 450 3000 2325020 EPA 8260D 10/26/22 05:32 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 123 % 53-136 2J25020 EPA 6260D 10126122 05:32 RKY 4-Bromofluorobenzene 62 1 60.0 104 % 53-136 2J31016 EPA 6260D 10131122 23:22 RKY Dlbromofluoromethane 56 1 50.0 112 % 67-129 2J25020 EPA 6260D 10126122 05:32 RKY Dlbromofluoromethane 69 1 60.0 115 % 67-129 2J31016 EPA 6260D 10131122 23:22 RKY Toluene-d8 53 1 50.0 106 % 59-134 2J25020 EPA 6260D 10126122 05:32 RKY Toluene-d8 62 1 60.0 104 % 59-134 2J31016 EPA 6260D 10131122 23:22 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-W4A Lab Sample ID:CF14375-13 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 13:55 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,1,1-Trichloroethane [71-55-6]A 5.2 ug/L 1 0.12 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1.1-Dichloroethane [75-34-3]A 31 ug/L 1 0.13 1.0 2.127021 EPA 8260D 10/27/22 20:20 RKY 1.1-Dichloroethene [75-35-4]A 8.8 ug/L 1 0.21 1.0 2.127021 EPA 8260D 10/27/22 20:20 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 1,2-Dichloroethane [107-06-2]A 0.93 J ug/L 1 0.21 1.0 2J31017 EPA 8260D 11/01/22 10:49 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY A-07 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2127021 EPA 8260D 10/27/22 20:20 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2127021 EPA 8260D 10/27/22 20:20 RKY Benzene [71-43-2]A 0.99 J ug/L 1 0.15 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Chlorobenzene [108-90-7]A 3.9 ug/L 1 0.17 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY cis-1,2-Dichloroethene [156-59-2]A 34 ug/L 1 0.15 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2127021 EPA 8260D 10/27/22 20:20 RKY Methylene chloride [75-09-2]^ 1.1 ug/L 1 0.23 1.0 2.127021 EPA 8260D 10/27/22 20:20 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Tetrachloroethene [127-18-4]A 1.2 ug/L 1 0.17 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY trans-1,2-Dichloroethene [156-60-5]A 0.51 J ug/L 1 0.21 1.0 2J27021 EPA 8260D 10/27/22 20:20 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY trans- l,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Trichloroethene [79-01-6]A 2.1 ug/L 1 0.15 1.0 2.127021 EPA 8260D 10/27/22 20:20 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2127021 EPA 8260D 10/27/22 20:20 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2127021 EPA 8260D 10/27/22 20:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-W4A Lab Sample ID:CF14375-13 Received: 10/20/22 11:00 Matrix: Water Sampled:10/18/22 13:55 Work Order: CF14375 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 25 ug/L 1 0.32 1.0 2331017 EPA 8260D 11/01/22 10:49 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J27021 EPA 8260D 10/27/22 20:20 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 103 % 53-136 2J27021 EPA 6260D 10127122 20:20 RKY 4-Bromofluorobenzene 63 1 60.0 106 % 53-136 2J31017 EPA 6260D 11101122 10:49 RKY Dlbromofluoromethane 57 1 50.0 114 % 67-129 2J27021 EPA 6260D 10127122 20:20 RKY Dlbromofluoromethane 68 1 60.0 114 % 67-129 2J31017 EPA 6260D 11101122 10:49 RKY Toluene-d8 53 1 50.0 107 % 59-134 2J27021 EPA 6260D 10127122 20:20 RKY Toluene-d8 63 1 60.0 105 % 59-134 2J31017 EPA 6260D 11101122 10:49 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW2 Lab Sample ID:CF14376-01 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/21/22 22:44 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/21/22 22:44 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/21/22 22:44 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW2 Lab Sample ID:CF14376-01 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/21/22 22:44 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/21/22 22:44 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/21/22 22:44 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 58 1 50.0 115 % 53-136 2-721025 EPA 8260D 10121122 22:44 RKY Dlbromofluoromethane 53 1 50.0 107 % 67-129 2721025 EPA 8260D 10121122 22:44 RKY Toluene-& 54 1 50.0 108 % 59-134 2-721025 EPA 8260D 10121122 22:44 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW3 Lab Sample ID:CF14376-02 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 13:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,1-Dichloroethane [75-34-3]A 0.88 J ug/L 1 0.13 1.0 2121025 EPA 8260D 10/21/22 23:13 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY Acetone[67-64-1]A 10 U ug/L 1 10 20 2321025 EPA 8260D 10/21/22 23:13 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/21/22 23:13 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY cis-1,2-Dichloroethene [156-59-2]A 1.2 ug/L 1 0.15 1.0 2121025 EPA 8260D 10/21/22 23:13 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY m,p-Xylenes [108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/21/22 23:13 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW3 Lab Sample ID:CF14376-02 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 13:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/21/22 23:13 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/21/22 23:13 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/21/22 23:13 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 2721025 EPA 8260D 10121122 23:13 RKY Dlbromofluoromethane 54 1 50.0 108 % 67-129 2721025 EPA 8260D 10121122 23:13 RKY Toluene-& 54 1 50.0 108 % 59-134 2721025 EPA 8260D 10121122 23:13 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW4 Lab Sample ID:CF14376-03 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,1,1-Trichloroethane [71-55-6]^ 1.4 ug/L 1 0.12 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,1-Dichloroethane [75-34-3]^ 12 ug/L 1 0.13 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,1-Dichloroethene [75-35-4]^ 4.2 ug/L 1 0.21 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,2-Dichloroethane [107-06-2]^ 1.1 ug/L 1 0.21 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 3-05 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2325025 EPA 8260D 10/27/22 01:42 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2325025 EPA 8260D 10/27/22 01:42 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY QL-02 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Chlorobenzene [308-90-7]^ 1.8 ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY cis- 1,2-Dichloroethene [156-59-2]^ 18 ug/L 1 0.15 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2325025 EPA 8260D 10/27/22 01:42 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW4 Lab Sample ID:CF14376-03 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2325025 EPA 8260D 10/27/22 01:42 RKY Vinyl chloride [75-01-4]A 19 ug/L 1 0.32 1.0 2325025 EPA 8260D 10/27/22 01:42 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2325025 EPA 8260D 10/27/22 01:42 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 53 1 50.0 106 % 53-136 2-725025 EPA 8260D 10127122 01:42 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 2725025 EPA 8260D 10127122 01:42 RKY Toluene-& 51 1 50.0 103 % 59-134 2-725025 EPA 8260D 10127122 01:42 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW5 Lab Sample ID:CF14376-04 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 13:10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 00:10 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 00:10 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 00:10 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 43 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW5 Lab Sample ID:CF14376-04 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 13:10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 00:10 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 00:10 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 00:10 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 55 1 50.0 109 % 53-136 2-721025 EPA 8260D 10122122 00:10 RKY Dlbromofluoromethane 54 1 50.0 109 % 67-129 2721025 EPA 8260D 10122122 00:10 RKY Toluene-& 54 1 50.0 107 % 59-134 2-721025 EPA 8260D 10122122 00:10 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW6Surface Lab Sample ID:CF14376-05 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 08:40 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 00:38 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 00:38 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 00:38 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW6Surface Lab Sample ID:CF14376-05 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 08:40 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 00:38 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 00:38 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 00:38 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 ill % 53-136 2-721025 EPA 8260D 10122122 0028 RKY Dlbromofluoromethane 53 1 50.0 105 % 67-129 2721025 EPA 8260D 10122122 00:38 RKY Toluene-& 54 1 50.0 108 % 59-134 2-721025 EPA 8260D 10122122 0028 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW6Bottom Lab Sample ID:CF14376-06 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 08:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 01:07 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 01:07 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 01:07 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW6Bottom Lab Sample ID:CF14376-06 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 08:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 01:07 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 01:07 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 01:07 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 2-721025 EPA 8260D 10122122 01:07 RKY Dlbromofluoromethane 54 1 50.0 109 % 67-129 2721025 EPA 8260D 10122122 01:07 RKY Toluene-& 55 1 50.0 109 % 59-134 2-721025 EPA 8260D 10122122 01:07 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW7Bottom Lab Sample ID:CF14376-07 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 10:20 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 01:35 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 01:35 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 01:35 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW7Bottom Lab Sample ID:CF14376-07 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 10:20 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 01:35 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 01:35 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 01:35 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 2721025 EPA 8260D 10122122 01:35 RKY Dlbromofluoromethane 56 1 50.0 ill % 67-129 2721025 EPA 8260D 10122122 01:35 RKY Toluene-& 54 1 50.0 108 % 59-134 2721025 EPA 8260D 10122122 01:35 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW7Surface Lab Sample ID:CF14376-08 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 10: 10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 02:04 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 02:04 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 02:04 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SW7Surface Lab Sample ID:CF14376-08 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 10:10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 02:04 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 02:04 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 02:04 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 55 1 50.0 ill % 53-136 2-721025 EPA 8260D 10122122 02:04 RKY Dlbromofluoromethane 56 1 50.0 113 % 67-129 2721025 EPA 8260D 10122122 02:04 RKY Toluene-& 55 1 50.0 110 % 59-134 2-721025 EPA 8260D 10122122 02:04 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 52 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP2Bottom Lab Sample ID:CF14376-09 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 09:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 02:33 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 02:33 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 02:33 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP2Bottom Lab Sample ID:CF14376-09 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 09:50 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 02:33 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 02:33 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 02:33 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 58 1 50.0 116 % 53-136 2-721025 EPA 8260D 10122122 02:33 RKY Dlbromofluoromethane 55 1 50.0 110 % 67-129 2721025 EPA 8260D 10122122 02:33 RKY Toluene-& 56 1 50.0 112 % 59-134 2-721025 EPA 8260D 10122122 02:33 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 54 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP2Surface Lab Sample ID:CF14376-10 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 09:40 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 03:01 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 03:01 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 03:01 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP2Surface Lab Sample ID:CF14376-10 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 09:40 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 03:01 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 03:01 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 03:01 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 58 1 50.0 116 % 53-136 2-721025 EPA 8260D 10122122 03:01 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 2721025 EPA 8260D 10122122 03:01 RKY Toluene-& 54 1 50.0 108 % 59-134 2-721025 EPA 8260D 10122122 03:01 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 56 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP11Surface Lab Sample ID:CF14376-11 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 11:00 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 03:30 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 03:30 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 03:30 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 57 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRPllSurface Lab Sample ID:CF14376-11 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 11:00 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 03:30 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 03:30 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 03:30 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 2721025 EPA 8260D 10122122 03:30 RKY Dlbromofluoromethane 56 1 50.0 112 % 67-129 2721025 EPA 8260D 10122122 03:30 RKY Toluene-& 55 1 50.0 109 % 59-134 2721025 EPA 8260D 10122122 0320 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 58 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 410 1-SWDRP1 1 Bottom Lab Sample ID:CF14376-12 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 11:10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY Acetone[67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/22/22 03:59 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/22/22 03:59 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/22/22 03:59 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-SWDRP11Bottom Lab Sample ID:CF14376-12 Received: 10/21/22 11:00 Matrix: Water Sampled:10/20/22 11:10 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/22/22 03:59 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/22/22 03:59 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/22/22 03:59 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 113 % 53-136 2-721025 EPA 8260D 10122122 03:59 RKY Dlbromofluoromethane 55 1 50.0 110 % 67-129 2721025 EPA 8260D 10122122 03:59 RKY Toluene-& 55 1 50.0 109 % 59-134 2-721025 EPA 8260D 10122122 03:59 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-TripBlank Lab Sample ID:CF14376-13 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan Units DF MDL I'Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2321025 EPA 8260D 10/21/22 20:50 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2321025 EPA 8260D 10/21/22 20:50 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2321025 EPA 8260D 10/21/22 20:50 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-TripBlank Lab Sample ID:CF14376-13 Received: 10/21/22 11:00 Matrix: Water Sampled:10/19/22 12:25 Work Order: CF14376 Project: Seaboard/Riverdale Landfill- SW Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 2321025 EPA 8260D 10/21/22 20:50 RKY Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 2321025 EPA 8260D 10/21/22 20:50 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 2321025 EPA 8260D 10/21/22 20:50 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 2-721025 EPA 8260D 10121122 20:50 RKY Dlbromofluoromethane 56 1 50.0 112 % 67-129 2721025 EPA 8260D 10121122 20:50 RKY Toluene-& 55 1 50.0 110 % 59-134 2-721025 EPA 8260D 10121122 20:50 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 62 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW1 Lab Sample ID:CF15781-01 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 13:50 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 2117021 EPA 8260D 10/18/22 02:20 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 2117021 EPA 8260D 10/18/22 02:20 RKY Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY QV-01 Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 2117021 EPA 8260D 10/18/22 02:20 RKY Methylene chloride [75-09-2]^ 0.98 J ug/L 1 0.23 1.0 2J18026 EPA 8260D 10/18/22 23:21 RKY 0-01 o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Styrene [100-42-5]^ 0.11 u ug/L 1 0.11 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 2117021 EPA 8260D 10/18/22 02:20 RKY Vinyl acetate [108-05-4]^ 0.95 Ll ug/L 1 0.95 5.0 2117021 EPA 8260D 10/18/22 02:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW1 Lab Sample ID:CF15781-01 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 13:50 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J17021 EPA 8260D 10/18/22 02:20 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J17021 EPA 8260D 10/18/22 02:20 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 2J17021 EPA 6260D 10118122 02:20 RKY 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 2J18026 EPA 6260D 10118122 23:21 RKY Dibromofluoromethane 57 1 50.0 114 % 67-129 2J17021 EPA 6260D 10116122 02:20 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 2J18026 EPA 6260D 10116122 23:21 RKY Toluene-d8 55 1 50.0 110 % 59-134 2J17021 EPA 6260D 10116122 02:20 RKY Toluene-d8 55 1 50.0 109 % 59-134 2J18026 EPA 6260D 10/16122 23:21 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 64 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW10 Lab Sample ID:CF15781-02 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 10:50 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 2118027 EPA 8260D 10/20/22 02:20 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 2118027 EPA 8260D 10/20/22 02:20 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY QV-01 Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 2118027 EPA 8260D 10/20/22 02:20 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 2118027 EPA 8260D 10/20/22 02:20 RKY QV-01 Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 2118027 EPA 8260D 10/20/22 02:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 65 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-MW10 Lab Sample ID:CF15781-02 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 10:50 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J18027 EPA 8260D 10/20/22 02:20 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J18027 EPA 8260D 10/20/22 02:20 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 2J18027 EPA 6260D 10120122 02:20 RKY Dibromofluoromethane 55 1 50.0 109 % 67-129 2J18027 EPA 6260D 10120122 02:20 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J18027 EPA 6260D 10120122 02:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 66 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW3D Lab Sample ID:CF15781-03 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 11:40 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 85 UD ug/L 500 85 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,1,1-Trichloroethane [71-55-6]^ 620 D ug/L 500 60 500 2317021 EPA 8260D 10/18/22 02:49 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 140 UD ug/L 500 140 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,1,2-Trichloroethane [79-00-5]^ 70 UD ug/L 500 70 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,1-Dichloroethane [75-34-3]^ 540 D ug/L 500 65 500 2317021 EPA 8260D 10/18/22 02:49 RKY 1,1-Dichloroethene [75-35-4]^ 1300 D ug/L 500 100 500 2318027 EPA 8260D 10/19/22 22:46 RKY 1,2,3-Trichloropropane [96-18-4]^ 120 UD ug/L 500 120 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 240 UD ug/L 500 240 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,2-Dibromoethane[106-93-4]^ 330 UD ug/L 500 330 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,2-Dichlorobenzene [95-50-1]^ 95 UD ug/L 500 95 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,2-Dichloroethane [107-06-2]^ 12000 D ug/L 500 100 500 2317021 EPA 8260D 10/18/22 02:49 RKY 1,2-Dichloropropane [78-87-5]^ 50 UD ug/L 500 50 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 1,4-Dichlorobenzene [106-46-7]^ 95 UD ug/L 500 95 500 2J17021 EPA 8260D 10/18/22 02:49 RKY 2-Butanone [78-93-3]^ 650 UD ug/L 500 650 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY 2-Hexanone [591-78-6]^ 440 UD ug/L 500 440 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY 4-Methyl-2-pentanone [108-10-1]^ 550 UD ug/L 500 550 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY Acetone [67-64-1]^ 5000 UD ug/L 500 5000 10000 2J17021 EPA 8260D 10/18/22 02:49 RKY Acrylonitrile [107-13-1]^ 1800 UD ug/L 500 1800 5000 2J17021 EPA 8260D 10/18/22 02:49 RKY Benzene [71-43-2]^ 240 JD ug/L 500 75 500 2317021 EPA 8260D 10/18/22 02:49 RKY Bromochloromethane [74-97-5]^ 240 UD ug/L 500 240 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Bromodichloromethane [75-27-4]^ 85 UD ug/L 500 85 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Bromoform [75-25-2]^ 110 UD ug/L 500 110 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Bromomethane [74-83-9]^ 70 UD ug/L 500 70 500 2J17021 EPA 8260D 10/18/22 02:49 RKY QV-01 Carbon disulfide [75-15-0]^ 750 UD ug/L 500 750 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY Carbon tetrachloride [56-23-5]^ 85 UD ug/L 500 85 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Chlorobenzene [308-90-7]^ 20000 D ug/L 500 85 500 2317021 EPA 8260D 10/18/22 02:49 RKY Chloroethane [75-00-3]^ 120 UD ug/L 500 120 500 2J17021 EPA 8260D 10/18/22 02:49 RKY QV-01 Chloroform [67-66-3]^ 90 UD ug/L 500 90 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Chloromethane [74-87-3]^ 65 UD ug/L 500 65 500 2J17021 EPA 8260D 10/18/22 02:49 RKY cis- 1,2-Dichloroethene [156-59-2]^ 380 JD ug/L 500 75 500 2317021 EPA 8260D 10/18/22 02:49 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 100 UD ug/L 500 100 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Dibromochloromethane [124-48-1]^ 85 UD ug/L 500 85 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Dibromomethane [74-95-3]^ 140 UD ug/L 500 140 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Ethylbenzene [100-41-4]^ 65 UD ug/L 500 65 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Iodomethane[74-88-4]^ 850 UD ug/L 500 850 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY m,p-Xylenes [108-38-3/106-42-3]^ 85 UD ug/L 500 85 1000 2J17021 EPA 8260D 10/18/22 02:49 RKY Methylene chloride [75-09-2]^ 1400 D ug/L 500 120 500 2318027 EPA 8260D 10/19/22 22:46 RKY 0-01 o-Xylene [95-47-6]^ 32 UD ug/L 500 32 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Styrene [100-42-5]^ 55 UD ug/L 500 55 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Tetrachloroethene [127-18-4]^ 1900 D ug/L 500 85 500 2317021 EPA 8260D 10/18/22 02:49 RKY Toluene [108-88-3]^ 680 D ug/L 500 70 500 2317021 EPA 8260D 10/18/22 02:49 RKY trans-1,2-Dichloroethene [156-60-5]^ 100 UD ug/L 500 100 500 2J17021 EPA 8260D 10/18/22 02:49 RKY trans-1,3-Dichloropropene [10061-02-6]^ 75 UD ug/L 500 75 500 2J17021 EPA 8260D 10/18/22 02:49 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 350 UD ug/L 500 350 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Trichloroethene [79-01-6]^ 4200 D ug/L 500 75 500 2317021 EPA 8260D 10/18/22 02:49 RKY Trichlorofluoromethane [75-69-4]^ 120 UD ug/L 500 120 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Vinyl acetate [108-05-4]^ 480 UD ug/L 500 480 2500 2J17021 EPA 8260D 10/18/22 02:49 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 67 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW3D Lab Sample ID:CF15781-03 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 11:40 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 160 UD ug/L 500 160 500 2J17021 EPA 8260D 10/18/22 02:49 RKY Xylenes (Total) [1330-20-7]^ 220 UD ug/L 500 220 1500 2J17021 EPA 8260D 10/18/22 02:49 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 2J17021 EPA 6260D 10118122 02:49 RKY 4-Bromofluorobenzene 55 1 50.0 109 % 53-136 2J18027 EPA 6260D 10119122 22:46 RKY Dibromofluoromethane 56 1 50.0 111 % 67-129 2J17021 EPA 6260D 10116122 02:49 RKY Dibromofluoromethane 55 1 50.0 109 % 67-129 2J18027 EPA 6260D 10119122 22:46 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J17021 EPA 6260D 10116122 02:49 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J18027 EPA 6260D 10119122 22:46 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 68 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW6I Lab Sample ID:CF15781-04 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 12:00 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,1-Dichloroethane [75-34-3]A 8.3 ug/L 1 0.13 1.0 2J18027 EPA 8260D 10/20/22 02:49 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,2-Dichloroethane [107-06-2]A 2.0 ug/L 1 0.21 1.0 2J18027 EPA 8260D 10/20/22 02:49 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY 1,4-Dichlorobenzene [506-46-7]A 1.2 ug/L 1 0.19 1.0 2J18027 EPA 8260D 10/20/22 02:49 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2118027 EPA 8260D 10/20/22 02:49 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2118027 EPA 8260D 10/20/22 02:49 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Chlorobenzene [108-90-7]A 5.2 ug/L 1 0.17 1.0 2J18027 EPA 8260D 10/20/22 02:49 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY cis-1,2-Dichloroethene [156-59-2]A 12 ug/L 1 0.15 1.0 2J18027 EPA 8260D 10/20/22 02:49 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2118027 EPA 8260D 10/20/22 02:49 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2118027 EPA 8260D 10/20/22 02:49 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2118027 EPA 8260D 10/20/22 02:49 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 69 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW6I Lab Sample ID:CF15781-04 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 12:00 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 1.6 ug/L 1 0.32 1.0 2318027 EPA 8260D 10/20/22 02:49 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J18027 EPA 8260D 10/20/22 02:49 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 109 % 53-136 2J18027 EPA 6260D 10120122 02:49 RKY Dlbromofluoromethane 54 1 50.0 108 % 67-129 2J18027 EPA 6260D 10120122 02:49 RKY Toluene-d8 54 1 50.0 107 % 59-134 2J18027 EPA 6260D 10120122 02:49 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 70 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW6D Lab Sample ID:CF15781-05 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 11:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,1-Dichloroethane [75-34-3]A 29 ug/L 1 0.13 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2-Dichloroethane [107-06-2]A 2.6 ug/L 1 0.21 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2120026 EPA 8260D 10/21/22 10:13 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2120026 EPA 8260D 10/21/22 10:13 RKY Benzene [71-43-2]A 0.54 J ug/L 1 0.15 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Chlorobenzene [108-90-7]A 17 ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2120026 EPA 8260D 10/21/22 10:13 RKY Methylene chloride [75-09-2]^ 1.1 ug/L 1 0.23 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Toluene [108-88-3]A 0.75 J ug/L 1 0.14 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2120026 EPA 8260D 10/21/22 10:13 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2120026 EPA 8260D 10/21/22 10:13 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 71 of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW6D Lab Sample ID:CF15781-05 Received: 10/15/22 10:25 Matrix: Water Sampled:10/14/22 11:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 2.6 ug/L 1 0.32 1.0 2320026 EPA 8260D 10/21/22 10:13 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J20026 EPA 8260D 10/21/22 10:13 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analured By Notes 4-Bromofluorobenzene 55 1 50.0 111 % 53-136 2J20026 EPA 6260D 10121122 10:13 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 2J20026 EPA 6260D 1012112210:13 RKY Toluene-d8 54 1 50.0 109 % 59-134 2J20026 EPA 6260D 1012112210:13 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 72 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW10I Lab Sample ID:CF15781-06 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 13:45 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,1-Dichloroethane [75-34-3]A 4.9 ug/L 1 0.13 1.0 2J18027 EPA 8260D 10/20/22 03:51 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY 1,4-Dichlorobenzene [306-46-7]^ 3.1 ug/L 1 0.19 1.0 2J18027 EPA 8260D 10/20/22 03:51 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2118027 EPA 8260D 10/20/22 03:51 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2118027 EPA 8260D 10/20/22 03:51 RKY Benzene [71-43-2]A 1.3 ug/L 1 0.15 1.0 2J18027 EPA 8260D 10/20/22 03:51 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Chlorobenzene [108-90-7]A 3.3 ug/L 1 0.17 1.0 2J18027 EPA 8260D 10/20/22 03:51 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2118027 EPA 8260D 10/20/22 03:51 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2118027 EPA 8260D 10/20/22 03:51 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2118027 EPA 8260D 10/20/22 03:51 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 73 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW10I Lab Sample ID:CF15781-06 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 13:45 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 1.7 ug/L 1 0.32 1.0 2318027 EPA 8260D 10/20/22 03:51 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J18027 EPA 8260D 10/20/22 03:51 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 2J18027 EPA 6260D 10120122 03:51 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 2J18027 EPA 6260D 10120122 03:51 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J18027 EPA 6260D 10120122 03:51 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 74 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW10D Lab Sample ID:CF15781-07 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 14:10 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2118027 EPA 8260D 10/20/22 04:24 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2118027 EPA 8260D 10/20/22 04:24 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2118027 EPA 8260D 10/20/22 04:24 RKY Methylene chloride [75-09-2]^ 1.3 ug/L 1 0.23 1.0 2J18027 EPA 8260D 10/20/22 04:24 RKY 0-01 o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2118027 EPA 8260D 10/20/22 04:24 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2118027 EPA 8260D 10/20/22 04:24 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 75 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW10D Lab Sample ID:CF15781-07 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 14:10 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J18027 EPA 8260D 10/20/22 04:24 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J18027 EPA 8260D 10/20/22 04:24 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 56 1 50.0 111 % 53-136 2J18027 EPA 6260D 10120122 04:24 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 2J18027 EPA 6260D 10120122 04:24 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J18027 EPA 6260D 10120122 04:24 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 76 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW13I Lab Sample ID:CF15781-08 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 13:10 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,1-Dichloroethane [75-34-3]A 76 ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,1-Dichloroethene [75-35-4]A 1.4 ug/L 1 0.21 1.0 2118027 EPA 8260D 10/19/22 21:11 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,2-Dichloroethane [107-06-2]A 1.4 ug/L 1 0.21 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY 1,4-Dichlorobenzene [106-46-7]A 0.91 J ug/L 1 0.19 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2117021 EPA 8260D 10/18/22 03:17 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2117021 EPA 8260D 10/18/22 03:17 RKY Benzene [71-43-2]A 2.0 ug/L 1 0.15 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Chlorobenzene [108-90-7]A 11 ug/L 1 0.17 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY Chloroethane [75-00-3]A 2.0 ug/L 1 0.23 1.0 2J18027 EPA 8260D 10/19/22 21:11 RKY 3-04 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY cis-1,2-Dichloroethene [156-59-2]A 6.9 ug/L 1 0.15 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2117021 EPA 8260D 10/18/22 03:17 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Tetrachloroethene [127-18-4]^ 0.53 J ug/L 1 0.17 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY Toluene [108-88-3]^ 0.59 J ug/L 1 0.14 1.0 2J17021 EPA 8260D 10/18/22 03:17 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2117021 EPA 8260D 10/18/22 03:17 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2117021 EPA 8260D 10/18/22 03:17 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 77 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW13I Lab Sample ID:CF15781-08 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 13:10 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 7.1 ug/L 1 0.32 1.0 2317021 EPA 8260D 10/18/22 03:17 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J17021 EPA 8260D 10/18/22 03:17 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analured By Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 2J17021 EPA 6260D 10118122 03:17 RKY 4-Bromofluorobenzene 56 1 50.0 111 % 53-136 2J18027 EPA 6260D 10119122 21:11 RKY Dlbromofluoromethane 56 1 50.0 112 % 67-129 2J17021 EPA 6260D 10116122 03:17 RKY Dlbromofluoromethane 53 1 50.0 105 % 67-129 2J18027 EPA 6260D 10119122 21:11 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J17021 EPA 6260D 10116122 03:17 RKY Toluene-d8 54 1 50.0 107 % 59-134 2J18027 EPA 6260D 10119122 21:11 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 78 Of 115 00� www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW14D Lab Sample ID:CF15781-09 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 11:20 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY 2-Butanone [78-93-3]^ 4.3 J ug/L 1 1.3 5.0 2J18027 EPA 8260D 10/20/22 04:53 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2118027 EPA 8260D 10/20/22 04:53 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2118027 EPA 8260D 10/20/22 04:53 RKY Acetone [67-64-1]^ 15 J ug/L 1 10 20 2J18027 EPA 8260D 10/20/22 04:53 RKY 0-01 Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2118027 EPA 8260D 10/20/22 04:53 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2118027 EPA 8260D 10/20/22 04:53 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Chlorobenzene [108-90-7]^ 1.3 ug/L 1 0.17 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY QV-01 Chloroform [67-66-3]^ 3.5 ug/L 1 0.18 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.77 J ug/L 1 0.15 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Ethylbenzene [100-41-4]^ 0.58 J ug/L 1 0.13 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY Iodomethane[74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2118027 EPA 8260D 10/20/22 04:53 RKY m,p-Xylenes[108-38-3/306-42-3]^ 2.7 ug/L 1 0.17 2.0 2J18027 EPA 8260D 10/20/22 04:53 RKY Methylene chloride [75-09-2]^ 0.52 J ug/L 1 0.23 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY 0-01 o-Xylene [95-47-6]^ 1.3 ug/L 1 0.065 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Toluene [108-88-3]^ 2.2 ug/L 1 0.14 1.0 2J18027 EPA 8260D 10/20/22 04:53 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2118027 EPA 8260D 10/20/22 04:53 RKY QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2118027 EPA 8260D 10/20/22 04:53 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 79 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW14D Lab Sample ID:CF15781-09 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 11:20 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.58 J ug/L 1 0.32 1.0 2318027 EPA 8260D 10/20/22 04:53 RKY Xylenes(Total)[1330-20-7]^ 3.9 ug/L 1 0.45 3.0 2318027 EPA 8260D 10/20/22 04:53 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 109 % 53-136 2J18027 EPA 6260D 10120122 04:53 RKY Dlbromofluoromethane 54 1 50.0 108 % 67-129 2J18027 EPA 6260D 10120122 04:53 RKY Toluene-d8 55 1 50.0 109 % 59-134 2J18027 EPA 6260D 10120122 04:53 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 80 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW15D Lab Sample ID:CF15781-10 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 10:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,1-Dichloroethane [75-34-3]A 21 ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,1-Dichloroethene [75-35-4]A 6.1 ug/L 1 0.21 1.0 2118027 EPA 8260D 10/19/22 21:40 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 2118027 EPA 8260D 10/19/22 21:40 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,2-Dichloroethane [107-06-2]A 0.61 J ug/L 1 0.21 1.0 2J17021 EPA 8260D 10/18/22 03:46 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2117021 EPA 8260D 10/18/22 03:46 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 2117021 EPA 8260D 10/18/22 03:46 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2117021 EPA 8260D 10/18/22 03:46 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2117021 EPA 8260D 10/18/22 03:46 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2117021 EPA 8260D 10/18/22 03:46 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 2117021 EPA 8260D 10/18/22 03:46 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Chlorobenzene [108-90-7]A 3.9 ug/L 1 0.17 1.0 2J17021 EPA 8260D 10/18/22 03:46 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY cis-1,2-Dichloroethene [156-59-2]A 29 ug/L 1 0.15 1.0 2J17021 EPA 8260D 10/18/22 03:46 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2117021 EPA 8260D 10/18/22 03:46 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2117021 EPA 8260D 10/18/22 03:46 RKY Methylene chloride [75-09-2]A 1.0 ug/L 1 0.23 1.0 2J18027 EPA 8260D 10/19/22 21:40 RKY 0-01 o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2117021 EPA 8260D 10/18/22 03:46 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 81 Of 1 1 cJ (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW15D Lab Sample ID:CF15781-10 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 10:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2J17021 EPA 8260D 10/18/22 03:46 RKY Vinyl chloride [75-01-4]^ 1.2 ug/L 1 0.32 1.0 2317021 EPA 8260D 10/18/22 03:46 RKY Xylenes(Total)[1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 2J17021 EPA 8260D 10/18/22 03:46 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 2J17021 EPA 6260D 10118122 03:46 RKY 4-Bromofluorobenzene 54 1 50.0 107 % 53-136 2J18027 EPA 6260D 10119122 21:40 RKY Dlbromofluoromethane 57 1 50.0 113 % 67-129 2J17021 EPA 6260D 10116122 03:46 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 2J18027 EPA 6260D 10119122 21:40 RKY Toluene-d8 54 1 50.0 109 % 59-134 2J17021 EPA 6260D 10116122 03:46 RKY Toluene-d8 53 1 50.0 106 % 59-134 2J18027 EPA 8260D 10119122 21:40 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 82 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW16D Lab Sample ID:CF15781-11 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 09:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analvte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,1-Dichloroethane [75-34-3]A 23 ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,1-Dichloroethene [75-35-4]A 9.9 ug/L 1 0.21 1.0 2118027 EPA 8260D 10/19/22 22:13 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,2-Dichloroethane [107-06-2]A 0.62 J ug/L 1 0.21 1.0 2J17021 EPA 8260D 10/18/22 04:14 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 2117021 EPA 8260D 10/18/22 04:14 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 2117021 EPA 8260D 10/18/22 04:14 RKY Benzene [71-43-2]A 0.70 J ug/L 1 0.15 1.0 2J17021 EPA 8260D 10/18/22 04:14 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY QV-01 Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Chlorobenzene [108-90-7]A 50 ug/L 1 0.17 1.0 2J17021 EPA 8260D 10/18/22 04:14 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 2118027 EPA 8260D 10/19/22 22:13 RKY QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY cis-1,2-Dichloroethene [156-59-2]A 39 ug/L 1 0.15 1.0 2J17021 EPA 8260D 10/18/22 04:14 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 2117021 EPA 8260D 10/18/22 04:14 RKY Methylene chloride [75-09-2]^ 0.53 J ug/L 1 0.23 1.0 2J18027 EPA 8260D 10/19/22 22:13 RKY 0-01 o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 2117021 EPA 8260D 10/18/22 04:14 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 2117021 EPA 8260D 10/18/22 04:14 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 83 Of 1 1 5J (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-PW16D Lab Sample ID:CF15781-11 Received: 10/15/22 10:25 Matrix: Water Sampled:10/13/22 09:35 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 5.3 ug/L 1 0.32 1.0 2317021 EPA 8260D 10/18/22 04:14 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J17021 EPA 8260D 10/18/22 04:14 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analured By Notes 4-Bromofluorobenzene 53 1 50.0 105 % 53-136 2J17021 EPA 6260D 10118122 04:14 RKY 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 2J18027 EPA 6260D 10119122 22:13 RKY Dlbromofluoromethane 56 1 50.0 113 % 67-129 2J17021 EPA 6260D 10116122 04:14 RKY Dlbromofluoromethane 56 1 50.0 113 % 67-129 2J18027 EPA 6260D 10119122 22:13 RKY Toluene-d8 54 1 50.0 108 % 59-134 2J17021 EPA 6260D 10116122 04:14 RKY Toluene-d8 56 1 50.0 111 % 59-134 2J18027 EPA 6260D 10119122 22:13 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 84 Of 115 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4101-TripBlank Lab Sample ID:CF15781-12 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 11:40 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 2117021 EPA 8260D 10/17/22 20:37 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 2117021 EPA 8260D 10/17/22 20:37 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY QV-01 Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY QV-01 Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 2117021 EPA 8260D 10/17/22 20:37 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 2117021 EPA 8260D 10/17/22 20:37 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 2117021 EPA 8260D 10/17/22 20:37 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 85 Of 115 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4101-TripBlank Lab Sample ID:CF15781-12 Received: 10/15/22 10:25 Matrix: Water Sampled:10/12/22 11:40 Work Order: CF15781 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2J17021 EPA 8260D 10/17/22 20:37 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2J17021 EPA 8260D 10/17/22 20:37 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 2J17021 EPA 6260D 10117122 20:37 RKY Dibromofluoromethane 53 1 50.0 106 % 67-129 2J17021 EPA 6260D 10117122 20:37 RKY Toluene-d8 55 1 50.0 110 % 59-134 2J17021 EPA 6260D 10117122 20:37 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 86 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2JI7021 - EPA 5030B MS Blank (2117021-BLK1) Prepared: 10/17/2022 15:06 Analyzed: 10/17/2022 20:08 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 87 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2JI7021 - EPA 5030B MS - Continued Blank (2117021-BLK1) Continued Prepared: 10/17/2022 15:06 Analyzed: 10/17/2022 20:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 55 u91L 50.0 110 53-136 Dibromofluoromethane 52 u91L 50.0 105 67-129 Toluene-d8 54 u91L 50.0 108 59-134 LCS (2317021-BS1) Prepared: 10/17/2022 15:06 Analyzed: 10/17/2022 18:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 81 75-133 Benzene 18 1.0 ug/L 20.0 88 80-134 Chlorobenzene 19 1.0 ug/L 20.0 96 80-120 Toluene 18 1.0 ug/L 20.0 91 71-120 Trichloroethene 18 1.0 ug/L 20.0 91 74-120 4-Bromofluorobenzene 56 u91L 50.0 113 53-136 Dibromofluoromethane 50 u91L 50.0 101 67-129 Toluene-d8 53 u91L 50.0 105 59-134 Matrix Spike (2317021-MS1) Prepared: 10/17/2022 15:06 Analyzed: 10/17/2022 18:42 Source: CF15703-04 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 84 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 19 1.0 ug/L 20.0 0.14 U 93 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 95 74-120 4-Bromofluorobenzene 56 u91L 50.0 112 53-136 Dibromofluoromethane 51 u91L 50.0 102 67-129 Toluene-d8 53 u91L 50.0 106 59-134 Matrix Spike Dup (2317021-MSD1) Prepared: 10/17/2022 15:06 Analyzed: 10/17/2022 19:10 Source: CF15703-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 84 75-133 1 20 Benzene 18 1.0 ug/L 20.0 0.15 U 88 80-134 2 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 0.3 16 Toluene 18 1.0 ug/L 20.0 0.14 U 91 71-120 3 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 93 74-120 2 22 4-Bromofluorobenzene 57 u91L 50.0 114 53-136 Dibromofluoromethane 51 u91L 50.0 102 67-129 Toluene-d8 53 u91L 50.0 105 59-134 Batch 2-718026 - EPA 5030B MS Blank (2118026-BLK3) Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 20:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 88 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch M8026 - EPA 5030B MS - Continued Blank (2118026-BLK1) Continued Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 20:58 Analvte Result Flaq POL Units 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 55 u9/L 50.0 110 53-136 Dibromofluoromethane 55 u9/L 50.0 111 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch M8026 - EPA 5030B MS - Continued Blank (2118026-BLK1) Continued Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 20:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 55 u91L 50.0 109 59-134 LCS (2718026-BS3) Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 19:04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 79 75-133 Benzene 17 1.0 ug/L 20.0 87 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 17 1.0 ug/L 20.0 87 71-120 Trichloroethene 18 1.0 ug/L 20.0 90 74-120 4-Bromofluorobenzene 55 ug/L 50.0 110 53-136 Dibromofluoromethane 54 ug/L 50.0 107 67-129 Toluene-d8 54 ug/L 50.0 108 59-134 Matrix Spike (2118026-MS1) Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 19:32 Source: CF15354-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 0.21 U 76 75-133 Benzene 16 1.0 ug/L 20.0 0.15 U 82 80-134 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 Toluene 16 1.0 ug/L 20.0 0.14 U 81 71-120 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 85 74-120 4-Bromofluorobenzene 55 ug/L 50.0 110 53-136 Dibromofluoromethane 53 u91L 50.0 105 67-129 Toluene-d8 53 u9/L 50.0 105 59-134 Matrix Spike Dup (2718026-MSD1) Prepared: 10/18/2022 17:33 Analyzed: 10/18/2022 20:01 Source: CF15354-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 91 75-133 18 20 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 20 17 QM-11 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 102 80-120 19 16 QM-11 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 20 17 QM-11 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 100 74-120 16 22 4-Bromofluorobenzene 56 u91L 50.0 112 53-136 Dibromofluoromethane 55 u9/L 50.0 110 67-129 Toluene-& 54 u9/L 50.0 108 59-134 Batch 2718027 - EPA 5030B MS Blank (2118027-BLK3) Prepared: 10/18/2022 18:22 Analyzed: 10/19/2022 20:09 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full Page 90 of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch M8027 - EPA 5030B MS - Continued Blank (2118027-BLK1) Continued Prepared: 10/18/2022 18:22 Analyzed: 10/19/2022 20:09 Analvte Result Flaq POL Units 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 54 u9/L 50.0 108 53-136 Dibromofluoromethane 52 u9/L 50.0 104 67-129 Toluene-d8 54 u9/L 50.0 107 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 91 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch M8027 - EPA 5030B MS - Continued LCS (2318027-BS1) Prepared: 10/18/2022 18:22 Analyzed: 10/19/2022 18:05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 83 75-133 Benzene 18 1.0 ug/L 20.0 91 80-134 Chlorobenzene 19 1.0 ug/L 20.0 97 80-120 Toluene 19 1.0 ug/L 20.0 93 71-120 Trichloroethene 19 1.0 ug/L 20.0 97 74-120 4-Bromofluorobenzene 57 ug/L 50.0 113 53-136 Dibromofluoromethane 51 u9/L 50.0 102 67-129 Toluene-d8 54 u9/L 50.0 109 59-134 Matrix Spike (2318027-MS1) Prepared: 10/18/2022 18:22 Analyzed: 10/19/2022 18:38 Source: CF15703-05 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 85 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 92 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 96 74-120 4-Bromofluorobenzene 58 ug/L 50.0 116 53-136 Dibromofluoromethane 51 u9/L 50.0 102 67-129 Toluene-d8 53 ug/L 50.0 107 59-134 Matrix Spike Dup (2318027-MSD1) Prepared: 10/18/2022 18:22 Analyzed: 10/19/2022 19:07 Source: CF15703-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 82 75-133 4 20 Benzene 18 1.0 ug/L 20.0 0.15 U 89 80-134 3 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 2 16 Toluene 19 1.0 ug/L 20.0 0.14 U 93 71-120 1 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 90 74-120 6 22 4-Bromofluorobenzene 56 u9/L 50.0 113 53-136 Dibromofluoromethane 50 u9/L 50.0 100 67-129 Toluene-d8 52 u9/L 50.0 104 59-134 Batch Z720026 - EPA 5030B MS Blank (2120026-BLK3) Prepared: 10/20/2022 05:39 Analyzed: 10/21/2022 09:45 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 92 of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2120026 - EPA 5030B MS - Continued Blank (2120026-BLK1) Continued Prepared: 10/20/2022 05:39 Analyzed: 10/21/2022 09:45 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 55 ug/L 50.0 111 53-136 Dibromofluoromethane 54 ug/L 50.0 108 67-129 Toluene-d8 53 ug/L 50.0 106 59-134 LCS (2320026-BSI) Prepared: 10/20/2022 05:39 Analyzed: 10/22/2022 23:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 84 75-133 Benzene 18 1.0 ug/L 20.0 90 80-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 93 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2120026 - EPA 5030B MS - Continued LCS (2320026-BSI) Continued Prepared: 10/20/2022 05:39 Analyzed: 10/22/2022 23:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 18 1.0 ug/L 20.0 89 71-120 Trichloroethene 19 1.0 ug/L 20.0 94 74-120 4-Bromofluorobenzene 58 ug/L 50.0 116 53-136 Dibromofluoromethane 53 u91L 50.0 106 67-129 Toluene-d8 53 u91L 50.0 106 59-134 Matrix Spike (2320026-MS1) Prepared: 10/20/2022 05:39 Analyzed: 10/21/2022 08:19 Source: CF15703-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 82 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 88 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 92 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 91 74-120 4-Bromofluorobenzene 58 u91L 50.0 116 53-136 Dibromofluoromethane 51 ug/L 50.0 103 67-129 Toluene-d8 53 u91L 50.0 106 59-134 Matrix Spike Dup (2320026-MSD1) Prepared: 10/20/2022 05:39 Analyzed: 10/21/2022 08:47 Source: CF15703-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 93 75-133 12 20 Benzene 20 1.0 ug/L 20.0 0.15 U 101 80-134 14 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 101 80-120 9 16 Toluene 20 1.0 ug/L 20.0 0.14 U 98 71-120 11 17 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 102 74-120 12 22 4-Bromofluorobenzene 58 u91L 50.0 117 53-136 Dibromofluoromethane 53 u91L 50.0 105 67-129 Toluene-d8 55 u91L 50.0 109 59-134 Batch 2.721025 - EPA 5030B MS Blank (2321025-BLK3) Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 20:21 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dichloroethene 1, 2, 3-Trich I o rop ropa ne 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane FINAL Spike Source %REC Result Flaq POL Units Level Result %REC Limits 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 94 of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2121025 - EPA 5030B MS - Continued Blank (2121025-BLK1) Continued Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 20:21 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 57 u91L 50.0 113 53-136 Dibromofluoromethane 55 u91L 50.0 109 67-129 Toluene-d8 54 u91L 50.0 109 59-134 LCS (2321025-BS1) Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 18:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 82 75-133 Benzene 18 1.0 ug/L 20.0 89 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 95 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2121025 - EPA 5030B MS - Continued LCS (2323025-BS1) Continued Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 18:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 18 1.0 ug/L 20.0 88 74-120 4-Bromofluorobenzene 56 u91L 50.0 113 53-136 Dibromofluoromethane 53 u91L 50.0 105 67-129 Toluene-d8 54 u91L 50.0 108 59-134 Matrix Spike (2323025-MS1) Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 18:55 Source: CF15703-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 90 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 Toluene 19 1.0 ug/L 20.0 0.14 U 94 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 97 74-120 4-Bromofluorobenzene 57 u91L 50.0 114 53-136 Dibromofluoromethane 51 u91L 50.0 103 67-129 Toluene-d8 54 u91L 50.0 108 59-134 Matrix Spike Dup (2323025-MSD1) Prepared: 10/21/2022 15:55 Analyzed: 10/21/2022 19:23 Source: CF15703-13 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 86 75-133 4 20 Benzene 19 1.0 ug/L 20.0 0.15 U 95 80-134 1 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 2 16 Toluene 19 1.0 ug/L 20.0 0.14 U 95 71-120 1 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 94 74-120 3 22 4-Bromofluorobenzene 56 u91L 50.0 116 53-136 Dibromofluoromethane 51 u91L 50.0 101 67-129 Toluene-d8 53 u91L 50.0 106 59-134 Batch 2124024 - EPA 5030E MS Blank (2324024-BLK1) Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 08:26 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Butanone FINAL Spike Source %REC Result Flaci POL Units Level Result %REC Limits 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L 0.19 U 1.0 ug/L 1.3 U 5.0 ug/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 96 of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2124024 - EPA 5030B MS - Continued Blank (2124024-BLK1) Continued Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 08:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 64 u91L 50.0 128 53-136 Dibromofluoromethane 64 u91L 50.0 128 67-129 Toluene-d8 57 u91L 50.0 114 59-134 LCS (2724024-BS1) Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 06:32 Spike Source O/oREC RPD Analvte Result Flaq Q Units Level Result O/oREC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 112 75-133 Benzene 20 1.0 ug/L 20.0 98 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 18 1.0 ug/L 20.0 91 71-120 Trichloroethene 18 1.0 ug/L 20.0 91 74-120 4-Bromofluorobenzene 66 u91L 50.0 135 53-136 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 97 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2124024 - EPA 5030B MS - Continued LCS (2324024-BSI) Continued Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 06:32 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Dibromofluoromethane 63 u9/L 50.0 126 67-129 Toluene-& 57 u9/L 50.0 114 59-134 Matrix Spike (2J24024-MS3) Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 07:01 Source: CF15883-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 98 75-133 Benzene 21 1.0 ug/L 20.0 0.15 U 106 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 102 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 100 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 105 74-120 4-Bromofluorobenzene 51 ug/L 50.0 102 53-136 Dibromofluoromethane 55 u9/L 50.0 111 67-129 Toluene-d8 59 u9/L 50.0 118 59-134 Matrix Spike Dup (2324024-MSDI) Prepared: 10/24/2022 14:45 Analyzed: 10/25/2022 07:29 Source: CF15883-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 110 75-133 11 20 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 12 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 89 80-120 13 16 Toluene 18 1.0 ug/L 20.0 0.14 U 90 71-120 10 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 88 74-120 18 22 4-Bromofluorobenzene 68 u9/L 50.0 136 53-136 Dibromofluoromethane 63 u9/L 50.0 127 67-129 Toluene-d8 57 u9/L 50.0 113 59-134 Batch 2725020 - EPA 5030B MS Blank (2325020-BLK3) Prepared: 10/25/2022 15:56 Analyzed: 10/25/2022 22:52 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dichloroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 4-Methyl-2-pentanone FINAL Result Flaa Q Units 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L 0.19 U 1.0 ug/L 1.3 U 5.0 ug/L 0.88 U 5.0 ug/L 1.1 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 98 Of 1 1 5 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2125020 - EPA 5030B MS - Continued Blank (2125020-BLK1) Continued Prepared: 10/25/2022 15:56 Analyzed: 10/25/2022 22:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 61 ug/L 50.0 123 53-136 Dibromofluoromethane 56 ug/L 50.0 113 67-129 Toluene-d8 52 u9/L 50.0 105 59-134 LCS (2325020-BSI) Prepared: 10/25/2022 15:56 Analyzed: 10/25/2022 20:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 97 75-133 Benzene 17 1.0 ug/L 20.0 86 80-134 Chlorobenzene 17 1.0 ug/L 20.0 86 80-120 Toluene 17 1.0 ug/L 20.0 87 71-120 Trichloroethene 16 1.0 ug/L 20.0 78 74-120 4-Bromofluorobenzene 64 ug/L 50.0 128 53-136 Dibromofluoromethane 55 u9/L 50.0 110 67-129 Toluene-d8 53 u9/L 50.0 106 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 99 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2J25020 - EPA 5030B MS - Continued Matrix Spike (2325020-MS3) Prepared: 10/25/2022 15:56 Analyzed: 10/25/2022 21:26 Source: CF15883-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 100 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 89 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 91 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 91 71-120 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 83 74-120 4-Bromofluorobenzene 67 u9/L 50.0 134 53-136 Dibromofluoromethane 55 u9/L 50.0 111 67-129 Toluene-d8 51 u9/L 50.0 103 59-134 Matrix Spike Dup (2325020-MSD1) Prepared: 10/25/2022 15:56 Analyzed: 10/25/2022 21:55 Source: CF15883-09 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 95 75-133 5 20 Benzene 17 1.0 ug/L 20.0 0.15 U 87 80-134 2 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 89 80-120 2 16 Toluene 18 1.0 ug/L 20.0 0.14 U 89 71-120 2 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 79 74-120 5 22 4-Bromofluorobenzene 64 u9/L 50.0 128 53-136 Dibromofluoromethane 54 u9/L 50.0 108 67-129 Toluene-d8 52 u9/L 50.0 105 59-134 Batch 2J25025 - EPA 5030E MS Blank (2325025-BLK3) Prepared: 10/25/2022 19:31 Analyzed: 10/27/2022 00:44 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 100 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2125025 - EPA 5030B MS - Continued Blank (2325025-BLK1) Continued Prepared: 10/25/2022 19:31 Analyzed: 10/27/2022 00:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 54 u9/L 50.0 109 53-136 Dibromofluoromethane 53 u9/L 50.0 105 67-129 Toluene-d8 52 u9/L 50.0 103 59-134 LCS (2325025-BSI) Prepared: 10/25/2022 19:31 Analyzed: 10/26/2022 22:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 98 75-133 Benzene 18 1.0 ug/L 20.0 90 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 19 1.0 ug/L 20.0 93 71-120 Trichloroethene 16 1.0 ug/L 20.0 81 74-120 4-Bromofluorobenzene 63 u9/L 50.0 126 53-136 Dibromofluoromethane 57 u9/L 50.0 113 67-129 Toluene-d8 54 u9/L 50.0 108 59-134 Matrix Spike (2325025-MS3) Prepared: 10/25/2022 19:31 Analyzed: 10/26/2022 23:17 Source: CF15883-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 80 75-133 Benzene 17 1.0 ug/L 20.0 0.15 U 84 80-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 101 of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2125025 - EPA 5030B MS - Continued Matrix Spike (2325025-MS3) Continued Prepared: 10/25/2022 19:31 Analyzed: 10/26/2022 23:17 Source: CF15883-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 82 74-120 4-Bromofluorobenzene 55 u91L 50.0 110 53-136 Dibromofluoromethane 53 ug/L 50.0 107 67-129 Toluene-d8 51 u91L 50.0 102 59-134 Matrix Spike Dup (2125025-MSD1) Prepared: 10/25/2022 19:31 Analyzed: 10/26/2022 23:46 Source: CF15883-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 0.21 U 77 75-133 4 20 Benzene 16 1.0 ug/L 20.0 0.15 U 81 80-134 3 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 88 80-120 2 16 Toluene 17 1.0 ug/L 20.0 0.14 U 86 71-120 3 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 82 74-120 0.5 22 4-Bromofluorobenzene 54 ug/L 50.0 107 53-136 Dibromofluoromethane 51 u91L 50.0 103 67-129 Toluene-d8 50 u91L 50.0 100 59-134 Batch 2127021 - EPA 5030B MS Blank (2127021-BLK3) Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 19:22 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 102 of 115 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2127021 - EPA 5030E MS - Continued Blank (2327021-BLK1) Continued Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 19:22 Analvte Result Flaq POL Units Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis-1,2-Dichloroethene 0.15 U 1.0 ug/L cis-1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 60 u91L 50.0 121 53-136 Dibromofluoromethane 61 u91L 50.0 123 67-129 Toluene-d8 56 u91L 50.0 112 59-134 LCS (2127021-BS1) Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 17:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Mina Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 76 75-133 Benzene 16 1.0 ug/L 20.0 81 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 17 1.0 ug/L 20.0 86 71-120 Trichloroethene 16 1.0 ug/L 20.0 78 74-120 4-8romofluorobenzene 56 u91L 50.0 111 53-136 Dibromofluoromethane 54 u91L 50.0 109 67-129 Toluene-& 53 u91L 50.0 105 59-134 Matrix Spike (2727021-MS1) Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 17:55 Source: CF16027-07 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 79 75-133 Benzene 16 1.0 ug/L 20.0 0.15 U 80 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 89 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 89 71-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 103 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2127021 - EPA 5030B MS - Continued Matrix Spike (2327021-MS3) Continued Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 17:55 Source: CF16027-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 15 1.0 ug/L 20.0 0.15 U 76 74-120 4-Bromofluorobenzene 55 u91L 50.0 110 53-136 Dibromofluoromethane 55 u91L 50.0 110 67-129 Toluene-d8 51 u91L 50.0 103 59-134 Matrix Spike Dup (2327021-MSD1) Prepared: 10/27/2022 15:30 Analyzed: 10/27/2022 18:24 Source: CF16027-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 81 75-133 2 20 Benzene 17 1.0 ug/L 20.0 0.15 U 84 80-134 5 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 91 80-120 2 16 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 2 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 81 74-120 7 22 4-Bromofluorobenzene 56 u91L 50.0 112 53-136 Dibromofluoromethane 54 u91L 50.0 109 67-129 Toluene-d8 52 u91L 50.0 103 59-134 Batch 2.731016 - EPA 5030B MS Blank (2331016-BLK3) Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 20:00 Analvte Result Flaa Q Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 104 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2131016 - EPA 5030B MS - Continued Blank (2331016-BLK1) Continued Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 20:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromor7uorobenzene 65 u91L 60.0 108 53-136 Dibromofluoromethane 69 u91L 60.0 116 67-129 Toluene-d8 62 u91L 60.0 104 59-134 LCS (2333016-BS1) Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 18:05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 100 75-133 Benzene 19 1.0 ug/L 20.0 93 80-134 Chlorobenzene 19 1.0 ug/L 20.0 96 80-120 Toluene 21 1.0 ug/L 20.0 103 71-120 Trichloroethene 19 1.0 ug/L 20.0 94 74-120 4-Bromofluorobenzene 65 u91L 60.0 109 53-136 Dibromofluoromethane 64 u91L 60.0 106 67-129 Toluene-d8 64 u91L 60.0 107 59-134 Matrix Spike (2333016-MS1) Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 18:34 Source: CF16027-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 103 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 107 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 96 74-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 105 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2131016 - EPA 5030B MS - Continued Matrix Spike (2333016-MS3) Continued Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 18:34 Source: CF16027-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 65 ug/L 60.0 109 53-136 Dibromofluoromethane 64 ug/L 60.0 106 67-129 Toluene-d8 64 ug/L 60.0 107 59-134 Matrix Spike Dup (2333016-MSD1) Prepared: 10/31/2022 15:45 Analyzed: 10/31/2022 19:02 Source: CF16027-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 102 75-133 0.9 20 Benzene 18 1.0 ug/L 20.0 0.15 U 91 80-134 5 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 3 16 Toluene 21 1.0 ug/L 20.0 0.14 U 105 71-120 2 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 95 74-120 2 22 4-Bromofluorobenzene 64 ug/L 60.0 107 53-136 Dibromofluoromethane 64 ug/L 60.0 106 67-129 Toluene-d8 63 ug/L 60.0 104 59-134 Batch 2131017 - EPA 5030B MS Blank (2131017-BLK3) Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 08:54 Analvte Result Flao POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 106 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2131017 - EPA 5030B MS - Continued Blank (2131017-BLK1) Continued Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 08:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 64 u91L 60.0 107 53-136 Dibromofluoromethane 70 u91L 60.0 117 67-129 Toluene-d8 64 u91L 60.0 107 59-134 LCS (2331017-BS1) Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 07:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 100 75-133 Benzene 18 1.0 ug/L 20.0 90 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 20 1.0 ug/L 20.0 100 71-120 Trichloroethene 18 1.0 ug/L 20.0 91 74-120 4-Bromofluorobenzene 63 u91L 60.0 105 53-136 Dibromofluoromethane 69 u91L 60.0 115 67-129 Toluene-d8 64 u91L 60.0 107 59-134 Matrix Spike (2733017-MS1) Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 07:28 Source: CF16105-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 113 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 102 80-134 Chlorobenzene 21 1.0 ug/L 20.0 0.17 U 104 80-120 Toluene 22 1.0 ug/L 20.0 0.14 U 112 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 102 74-120 4-Bromofluorobenzene 64 u91L 60.0 106 53-136 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 107 Of 115 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 2131017 - EPA 5030B MS - Continued Matrix Spike (2333017-MS3) Continued Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 07:28 Source: CF16105-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Dibromofluoromethane 67 u91L 60.0 111 67-129 Toluene-& 63 u91L 60.0 105 59-134 Matrix Spike Dup (2]33017-MSD1) Prepared: 10/31/2022 19:13 Analyzed: 11/01/2022 07:57 Source: CF16105-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 96 75-133 16 20 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 13 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 91 80-120 13 16 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 13 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 92 74-120 10 22 4-Bromofluorobenzene 64 u91L 60.0 107 53-136 Dibromofluoromethane 67 u91L 60.0 111 67-129 Toluene-d8 64 u91L 60.0 107 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 108 Of 115 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. A-07 Analyte biased low in LCS but detected in the reporting limit standard. Since the analyte in the associated sample was not detected, there is no impact on data quality. 3-04 Result may be biased high. Associated calibration verification standard exceeded the upper control limit. 1-05 Result may be biased low. Associated calibration verification standard did not meet the minimum control limit. 0-01 This compound is a common laboratory contaminant. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 109 of 115 E g -ocm Q y j y o o (D I� E ' E E n _ a°i m m x Cn ii.i -`2 U Qi r c CD 4 � LL E z 0 � J � R U m G N S� � N m G p G d O U m 0 U m ¢ n 0 m Z Ul � m Q C E U 0 a ro al oils oo9z8' '!9;Y5 (3009'C nz? x x X x x X x x x X x x v N P d Q 4� � m � �+ C7 �a Tx V G c� m•G• xui m am a a ¢ m m c _ _c • W � � 1 � ti r o a � d L' N c��i Cv lU d eG E cr7�_^; u9 E ecim n v cd cd n 8 m c � E m m o n a a� n � V n ¢ as U a O C U J m a m d m ' 1 m � m m �E o \ o a r•- 6 V m m t m M. m a cccc ¢ a U ELK U EQ N c t a d a � E EFPage 110 of 1 Mn U 115 n O w m 0 V r. qj I cc 0 U W CC 0 0 U) M V I,L 0 Z a U LL7 Q 0 a 0 a J Z 0 i W N Z 0 U J H Z LLI Z 0r z W Q7 CD CL 0 LO w —� a '� ` N ❑ N U U cc Q E d f— m m 7C LLI m T E E E n O = n D , LL E CO f l y J CL Q N m pppC �= O U O U � a `m y 'EZ o o x m v N N al � Y 0 = N _ ch n r d d Z m 2 Q x Z O N G _ U x a N O U m 0. dO U E E E0 y 6 F C! M13 cmzs,PQPUE'i� fl09zg,mz8 X X }� '+{ ]G X >C "�` X o v � N p ` U ` `5 m CD CD SD CD CD CC C;` :O (C CD v D E ° E F U C N -o r xo d d d Q a V 1 VV a a N C7 � � m c v 3 m �✓ li ai c m Q. zmE L V im (U F O m m IL1�1Y� U O •� ai d d d Q m LC ❑c C _ L Lu 2 j \ o J �. U = = 3 m c ` ❑ cro ° m W m w �- 3 m a _ CV � � D 0 � E �a Q, CL CL d a n Ln m x c f7 LO Page 111 of 115 U ¢ t5 H rmn �n 61 [n E 3 3 cc 0 U ui Q } ❑ 0 H U LL 0 z Q U LLI cc L0 r a cc 0 cc Q J z 0 RMM lcc W N z 0 U J z uj 2 z 0 X 5 z W U � N � - m a r LO w -2 Q c ^t w m Q1 , EOL ♦ ! a a iffy} H E X c c m E E �C c a o� dyye d t c v p a � Q� r U n Q E E E � c 0 [g 4 C 8 .m 0 � ' = E m Z o w IDZ p m v O # T � E m Q m m m a y 'C N a MO m IA Y a y ¢ ¢ ¢ 2 E ¢ � U E E E v O y y o N O O m n 01 NIS 009n*P8RU9;X3 0491B'QcI3Z9 X ?C X 7G X X � o V N p C U o v E� O O _ ro � }. y O N Q U Q � CG to Er c Em {� roZM w M. LU 0 O J o C vi O m E N m m Ov vi m � Z © Hl 41 r\ m 04 C Y (71 C E c V E � _ Q b O ,aC to 0 z m a m e /� T Page 112 of 15j .fr R ro-T E �V 0 a 0 V LLi 0 0 U LL 0 z a U LLL 0 a 0 m a J z 0 R V/ z 0 U J z W 2 z 0 cc z LU aE, N .i.. G E N y S CXL a a W d � a+ N _E E E cca / \ 1cc F= m O O m 0 a q c Z Cl ¢ U 12 a ¢ I1 an 0 I c o c � u m m y p iv O m � m Z 1yfi � a z a pqq � G G n U u u ¢ U O Ir z E s` C V a N Ifl d U E E_ E 6 ~ o CO a Lti. N o I VgIS Q09ZIR i xipueddy QDF x x x x x x x x x x x x v _ n c E zE m m (O Q0 Co C.D co w CD CD w co w Q _ Ec E RC ~ U a �a¢aaaaaaa¢aaa N y 3 �� o0 m n U q m C a L' [} V U }9' 0 z a zq� m� ��m t U r ✓ m 3 w O 4, wu'L7 Q.� da/.,1 a o �' N Lr' N rZ ¢ s ¢ pm U a m �.• , `V 1 N W E N � N N C'�f �} r3 N N ^� y _y C w Z Cl a � d a, CL o00 C, (n _ Up r o u �+"� Q '"4 _vo t' t= to a a (f} IM m G] G.` i m a m ccfj _ 9 y d ty c� it7 t� t� ti M G C3 23 o m W co 0 in U) U) (n co En to w m cm r n� L E Page 113 of 115 �, I b o a7 E c m L cc�f+� N " L 'a E o $ ro �' J C vw X U a Y LLE cc O m z O Z' C T Q m c a m m N ° a � Uyy N Z N C_ G. C c� 0 QI ME sl09ze, f x!PLI" 009Ze X x X X v ot2 E ` C 1 V 75 d Ul N /r V E � `mr-, ❑ RS c 5 m u ,� E� Z Z m O1M O D d a` a r m in v r y 1 04 t� R� o E a C-4 U �t v r t� c Zm co 171 1 1 1 a � N U Ctl C N v N m tru s A ca � a C U U n Q a U m �f m m a m ¢ m CC m ff E � a ❑ C d ❑ o m r 0 m m N m m N N a m r as N Lt c S c C m U E r v E v m Q m c ia b Q m a_ `S U C E E Page 114 of 1 U m ifl N 0 N a a Q 2 O 8 LuQ jr rn } Og � I-3Ng N obi m (�¢zv LL.. p U O� Z a u n CL. O 'D FE x J P cn LU ' m ¢' 8 Y E c m m d O fI) c .0 Z � .0 J d c a 8 IL 6 0 0 U long CO ti d V C \3 V V D Iq U O V � a ' N cc •Q � '� a U pm o c 1a 4 E C U 2 -02 O �y O O wnyi Z m E � � ; E a a � ¢ m in 76 N N a y � .Q Q o z _ � HQ HQ l a R fU! m E 17 m m z F N L7. c E m m a m pC V O. U m m m ry E ' E E OO Q iz m ti m m 0 F. G s G ¢ C Q m $ E r a N v .g m s m m a Page 115 of 1 cn urofins Environment Testing ANALYTICAL REPORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 E7 Laboratory Job ID: 680-224127-1 Client Project/Site: CF14375 For: Environmental Conservation Laboratories 102 Woodwinds Industrial Ct, Suite A Cary, North Carolina 27511 IAttt�t__n'' : Mr. Bill Scott raw Authorized for release by. 1013112022 1:00:25 PM Naomi Flanagan, Project Manager (912)354-7858 Naomi.Flanagan@et.eurofinsus.com Designee for Sheila Hoffman, Project Manager II (912)250-0279 Sheila.Hoffman@et.eurofinsus.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Environmental Conservation Laboratories Sample Summary Job ID: 680-224127-1 Project/Site: CF14375 Lab Sample ID Client Sample ID Matrix Collected Received 680-224127-1 4101-MW3C Water 10/17/22 09:25 10/27/22 08:00 680-224127-2 4101-MW6 Water 10/19/22 08:20 10/27/22 08:00 680-224127-3 4101-MW12A Water 10/17/22 11:30 10/27/22 08:00 680-224127-4 4101-MW12B Water 10/17/22 13:15 10/27/22 08:00 680-224127-5 4101-MW12D Water 10/17/22 10:25 10/27/22 08:00 680-224127-6 4101-MW15A Water 10/18/22 10:35 10/27/22 08:00 680-224127-7 4101-OWDR2 Water 10/18/22 08:40 10/27/22 08:00 680-224127-8 4101-OWLFS2 Water 10/17/22 13:45 10/27/22 08:00 680-224127-9 4101-PW5D Water 10/18/22 09:25 10/27/22 08:00 680-224127-10 4101-PW41 Water 10/18/22 09:25 10/27/22 08:00 680-224127-11 4101-PW121 Water 10/19/22 09:25 10/27/22 08:00 680-224127-12 4101-PWSF1 Water 10/18/22 09:25 10/27/22 08:00 680-224127-13 4101-W4A Water 10/18/22 13:55 10/27/22 08:00 Page 2 of 36 Eurofins 9-P02 Method Summary Client: Environmental Conservation Laboratories Project/Site: CF14375 Job ID: 680-224127-1 Method Method Description Protocol Laboratory 8260D SIM Volatile Organic Compounds (GC/MS) SW846 EET PEN 5030C Purge and Trap SW846 EET PEN Protocol References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Savannah Page 3 of 36 10/31 /2022 Definitions/Glossary Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 U Qualifiers GUMS VOA Qualifier Qualifier Description F1 MS and/or MSD recovery exceeds control limits. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "Y column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present IDOL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 4 of 36 10/31 /2022 Case Narrative C Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Job ID: 680-224127-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-224127-1 Receipt The samples were received on 10/27/2022 8:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 5.4°C GC/MS VOA Method 8260D_SIM: The matrix spike duplicate (MSD) recoveries for analytical batch 400-598314 were outside control limits. Sample matrix interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits. Method 8260D_SIM: The following sample(s) was collected in a properly preserved vial; however, the pH was outside the required criteria when verified by the laboratory. The samples were analyzed outside the 7-day holding time specified for unpreserved samples but within the 14-day holding time specified for preserved samples: 4101-MW12B (680-224127-4) and 4101-OWLFS2 (680-224127-8). Method 8260D_SIM: The following sample(s) was collected in a properly preserved vial; however, the pH was outside the required criteria when verified by the laboratory. The sample was analyzed outside the 7-day holding time specified for unpreserved samples but within the 14-day holding time specified for preserved samples: 4101-OWLFS2 (680-224127-8). Method 8260D_SIM: The following samples were diluted to bring the concentration of target analytes within the calibration range: 4101-MW12A(680-224127-3), 4101-MW15A(680-224127-6), 4101-OWDR2 (680-224127-7), 4101-OWLFS2 (680-224127-8), 4101-PW5D (680-224127-9), 4101-PW41 (680-224127-10) and 4101-PWSF1 (680-224127-12). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins Savannah Page 5 of 36 10/31 /2022 Detection Summary Client: Environmental Conservation Laboratories Project/Site: CF14375 Job ID: 680-224127-1 Client Sample ID: 4101-MW3C Lab Sample ID: 680-224127-1 Cmalyte Result 1,4-Dioxane 39 Client Sample ID: 4101-MW6 Qualifier F1 RL 1.0 MDL 0.30 Unit ug/L Dil Fac D Method Prep Type 1 8260D SIM Total/NA ' Lab Sample ID: 680-224127-2 Analyte Result 1,4-Dioxane 23 Qualifier RL 1.0 MDL 0.30 Unit ug/L Dil Fac D Method Prep Type 1 8260D SIM Total/NA Client Sample ID: 4101-MW12A Lab Sample ID: 680-224127-3 CAnalyte Result 1,4-Dioxane 150 Qualifier RL 2.0 MDL 0.60 Unit ug/L Dil Fac D Method Prep Type 2 8260D SIM Total/NA Client Sample ID: 4101-MW12B Lab Sample ID: 680-224127-4 C Analyte Result 1,4-Dioxane 99 Qualifier RL 1.0 MDL 0.30 Unit ug/L Dil Fac D Method Prep Type 1 8260D SIM Total/NA Client Sample ID: 4101-MW12D Lab Sample ID: 680-224127-5 1 No Detections. Client Sample ID: 4101-MW15A Analyte Result 1,4-Dioxane 830 Qualifier RL 20 MDL 6.0 Unit ug/L Lab Sample ID: 680-224127-6 Dil Fac D Method Prep Type 20 8260D SIM Total/NA Client Sample ID: 4101-OWDR2 Lab Sample ID: 680-224127-7 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 170 5.0 1.5 ug/L 5 8260D SIM Total/NA Client Sample ID: 4101-OWLFS2 Lab Sample ID: 680-224127-8 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 220 5.0 1.5 ug/L 5 8260D SIM Total/NA Client Sample ID: 4101-PW5D Lab Sample ID: 680-224127-9 CAnalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 310 Client Sample ID: 4101-PW41 5.0 1.5 ug/L 5 8260D SIM Total/NA Lab Sample ID: 680-224127-10 Analyte Result 1,4-Dioxane 150 Client Sample ID: 4101-PW121 Qualifier RL 5.0 MDL 1.5 Unit ug/L Dil Fac D Method Prep Type 5 8260D SIM Total/NA Lab Sample ID: 680-224127-11 ENo Detections. Client Sample ID: 4101-PWSF1 Analyte Result 1,4-Dioxane 6900 Qualifier RL 100 MDL 30 Unit ug/L Lab Sample ID: 680-224127-12 Dil Fac D Method Prep Type 100 8260D SIM Total/NA This Detection Summary does not include radiochemical test results. Page 6 of 36 Eurofins Savannah 10/31 /2022 Detection Summary Client: Environmental Conservation Laboratories Project/Site: CF14375 Client Sample ID: 4101-W4A Analyte 1,4-Dioxane Result Qualifier 10 This Detection Summary does not include radiochemical test results. F Job ID: 680-224127-1 Lab Sample ID: 680-224127-13 RL MDL Unit Dil Fac D Method Prep Type 1.0 0.30 ug/L 1 8260D SIM Total/NA L Eurofins Savannah Page 7 of 36 10/31 /2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW3C Lab Sample ID: 680-224127-1 Date Collected: 10/17/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 39 F1 1.0 0.30 ug/L 10/28/2217:22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 77 50 - 150 10128122 17:22 1 Toluene-d8 (Surr) 104 50 - 150 10128122 17:22 1 4-Bromofluorobenzene 104 50 - 150 10128122 17:22 1 F Eurofins Savannah Page 8 of 36 10/31 /2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW6 Lab Sample ID: 680-224127-2 Date Collected: 10/19/22 08:20 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 23 1.0 0.30 ug/L 10/28/2219:02 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 78 50 - 150 10128122 19:02 1 Toluene-d8 (Surr) 100 50 - 150 10128122 19:02 1 4-Bromofluorobenzene 106 50 - 150 10128122 19:02 1 F Eurofins Savannah Page 9 of 36 10/31 /2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW12A Lab Sample ID: 680-224127-3 Date Collected: 10/17/22 11:30 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 150 2.0 0.60 ug/L 10/29/2218:49 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 78 50 - 150 10129122 18:49 2 Toluene-d8 (Surr) 103 50 - 150 10/29/22 18:49 2 4-Bromofluorobenzene 104 50 - 150 10/29/22 18:49 2 F Eurofins Savannah Page 10 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW12B Lab Sample ID: 680-224127-4 Date Collected: 10/17/22 13:15 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 99 1.0 0.30 ug/L 10/28/2219:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 75 50 - 150 10128122 19:52 1 Toluene-d8 (Surr) 104 50 - 150 10128122 19:52 1 4-Bromofluorobenzene 104 50 - 150 10128122 19:52 1 F Eurofins Savannah Page 11 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW12D Lab Sample ID: 680-224127-5 Date Collected: 10/17/22 10:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.30 1.0 0.30 ug/L 10/28/22 20:17 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 79 50 - 150 10128122 20:17 1 Toluene-d8 (Surr) 104 50 - 150 10128122 20:17 1 4-Bromofluorobenzene 103 50 - 150 10128122 20:17 1 F Eurofins Savannah Page 12 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW15A Lab Sample ID: 680-224127-6 Date Collected: 10/18/22 10:35 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 830 20 6.0 ug/L 10/29/22 22:10 20 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 77 50 - 150 10129122 22:10 20 Toluene-d8 (Surr) 104 50 - 150 10/29/22 22:10 20 4-Bromofluorobenzene 103 50 - 150 10/29/22 22:10 20 F Eurofins Savannah Page 13 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-OWDR2 Lab Sample ID: 680-224127-7 Date Collected: 10/18/22 08:40 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 170 5.0 1.5 ug/L 10/29/22 20:04 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 79 50 - 150 10129122 20:04 5 Toluene-d8 (Surr) 102 50 - 150 10/29/22 20:04 5 4-Bromofluorobenzene 105 50 - 150 10/29/22 20:04 5 F Eurofins Savannah Page 14 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-OWLFS2 Lab Sample ID: 680-224127-8 Date Collected: 10/17/22 13:45 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 220 5.0 1.5 ug/L 10/29/22 20:29 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 81 50 - 150 10129122 20:29 5 Toluene-d8 (Surr) 103 50 - 150 10/29/22 20:29 5 4-Bromofluorobenzene 104 50 - 150 10/29/22 20:29 5 F Eurofins Savannah Page 15 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-PW5D Lab Sample ID: 680-224127-9 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 310 5.0 1.5 ug/L 10/29/22 20:54 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 80 50 - 150 10129122 20:54 5 Toluene-d8 (Surr) 102 50 - 150 10/29/22 20:54 5 4-Bromofluorobenzene 105 50 - 150 10/29/22 20:54 5 F Eurofins Savannah Page 16 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-PW41 Lab Sample ID: 680-224127-10 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 150 5.0 1.5 ug/L 10/29/22 21:20 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 79 50 - 150 10129122 21:20 5 Toluene-d8 (Surr) 103 50 - 150 10/29/22 21:20 5 4-Bromofluorobenzene 105 50 - 150 10/29/22 21:20 5 F Eurofins Savannah Page 17 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-PW121 Lab Sample ID: 680-224127-11 Date Collected: 10/19/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.30 1.0 0.30 ug/L 10/29/2213:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 78 50 - 150 10129122 13:23 1 Toluene-d8 (Surr) 103 50 - 150 10/29/22 13:23 1 4-Bromofluorobenzene 104 50 - 150 10/29/22 13:23 1 F Eurofins Savannah Page 18 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-PWSF1 Lab Sample ID: 680-224127-12 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 6900 100 30 ug/L 10/29/22 22:35 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 77 50 - 150 10129122 22:35 100 Toluene-d8 (Surr) 104 50 - 150 10/29/22 22:35 100 4-Bromofluorobenzene 109 50 - 150 10/29/22 22:35 100 F Eurofins Savannah Page 19 of 36 10/31/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-W4A Lab Sample ID: 680-224127-13 Date Collected: 10/18/22 13:55 Matrix: Water Date Received: 10/27/22 08:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 10 1.0 0.30 ug/L 10/29/2215:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 78 50 - 150 10129122 15:28 1 Toluene-d8 (Surr) 103 50 - 150 10/29/22 15:28 1 4-Bromofluorobenzene 104 50 - 150 10/29/22 15:28 1 F Eurofins Savannah Page 20 of 36 10/31/2022 QC Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Method: 8260D SIM - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 400-598314/6 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 598314 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.30 1.0 0.30 ug/L 10/28/2216:17 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 80 50 - 150 10128122 16:17 1 Toluene-d8 (Surr) 104 50 - 150 10128122 16:17 1 4-Bromofluorobenzene 103 50 - 150 10128122 16:17 1 Lab Sample ID: LCS 400-598314/1004 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 598314 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits 1,4-Dioxane 10.0 10.3 ug/L 103 50-150 LCS LCS Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 - 150 Toluene-d8 (Surr) 108 50 - 150 4-Bromofluorobenzene 106 50 - 150 Lab Sample ID: 680-224127-1 MS Client Sample ID: 4101-MW3C Matrix: Water Prep Type: Total/NA Analysis Batch: 598314 Sample Sample Spike MS MS %Rec Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,4-Dioxane 39 F1 10.0 49.8 ug/L 109 50-150 MS MS Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 -150 Toluene-d8 (Surr) 108 50 -150 4-Bromofluorobenzene 105 50 -150 Lab Sample ID: 680-224127-1 MSD Client Sample ID: 4101-MW3C Matrix: Water Prep Type: Total/NA Analysis Batch: 598314 Sample Sample Spike MSD MSD %Rec RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,4-Dioxane 39 F1 10.0 59.7 F1 ug/L 208 50-150 18 50 MSD MSD Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 - 150 Toluene-d8 (Surr) 107 50 - 150 4-Bromofluorobenzene 106 50 - 150 Eurofins Savannah Page 21 of 36 10/31/2022 QC Sample Results Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Method: 8260D SIM - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 400-598354/6 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 598354 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.30 1.0 0.30 ug/L 10/29/2212:58 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane 79 50 - 150 10129122 12:58 1 Toluene-d8 (Surr) 104 50 - 150 10129122 12:58 1 4-Bromofluorobenzene 105 50 - 150 10129122 12:58 1 Lab Sample ID: LCS 400-598354/1004 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 598354 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits 1,4-Dioxane 10.0 9.84 ug/L 98 50 -150 LCS LCS Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 - 150 Toluene-d8 (Surr) 108 50 - 150 4-Bromofluorobenzene 105 50 - 150 Lab Sample ID: 680-224127-11 MS Client Sample ID: 4101-PW121 Matrix: Water Prep Type: Total/NA Analysis Batch: 598354 Sample Sample Spike MS MS %Rec Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,4-Dioxane <0.30 10.0 10.3 ug/L 103 50-150 MS MS Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 -150 Toluene-d8 (Surr) 107 50 -150 4-Bromofluorobenzene 105 50 -150 Lab Sample ID: 680-224127-11 MSD Client Sample ID: 4101-PW121 Matrix: Water Prep Type: Total/NA Analysis Batch: 598354 Sample Sample Spike MSD MSD %Rec RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,4-Dioxane <0.30 10.0 10.6 ug/L 106 50-150 2 50 MSD MSD Surrogate %Recovery Qualifier Limits Dibromofluoromethane 77 50 - 150 Toluene-d8 (Surr) 107 50 - 150 4-Bromofluorobenzene 107 50 - 150 Eurofins Savannah Page 22 of 36 10/31/2022 QC Association Summary Client: Environmental Conservation Laboratories Project/Site: CF14375 GC/MS VOA Analysis Batch: 598314 Lab Sample ID Client Sample ID 680-224127-1 4101-MW3C 680-224127-2 4101-MW6 680-224127-4 4101-MW12B 680-224127-5 4101-MW12D MB 400-598314/6 Method Blank LCS 400-598314/1004 Lab Control Sample 680-224127-1 MS 4101-MW3C 680-224127-1 MSD 4101-MW3C Analysis Batch: 598354 Lab Sample ID Client Sample ID 680-224127-3 4101-M W 12A 680-224127-6 4101-M W 15A 680-224127-7 4101-OWDR2 680-224127-8 4101-OWLFS2 680-224127-9 4101-PW5D 680-224127-10 4101-PW41 680-224127-11 4101-PW 121 680-224127-12 4101-PWSF1 680-224127-13 4101-W4A MB 400-598354/6 Method Blank LCS 400-598354/1004 Lab Control Sample 680-224127-11 MS 4101-PW121 680-224127-11 MSD 4101-PW121 Job ID: 680-224127-1 Prep Type Matrix Method Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Prep Type Matrix Method Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Prep Batch 0 F Prep Batch F Eurofins Savannah Page 23 of 36 10/31/2022 Lab Chronicle Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-MW3C Lab Sample ID: 680-224127-1 Date Collected: 10/17/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598314 10/28/22 17:22 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-MW6 Lab Sample ID: 680-224127-2 Date Collected: 10/19/22 08:20 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598314 10/28/22 19:02 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-MW12A Lab Sample ID: 680-224127-3 Date Collected: 10/17/22 11:30 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 2 5 mL 5 mL 598354 10/29/22 18:49 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-MW12B Lab Sample ID: 680-224127-4 Date Collected: 10/17/22 13:15 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598314 10/28/22 19:52 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-MW12D Lab Sample ID: 680-224127-5 Date Collected: 10/17/22 10:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598314 10/28/22 20:17 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-MW15A Lab Sample ID: 680-224127-6 Date Collected: 10/18/22 10:35 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 20 5 mL 5 mL 598354 10/29/22 22:10 AGW EET PEN Instrument ID: Curie Eurofins Savannah Page 24 of 36 10/31/2022 Lab Chronicle Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Client Sample ID: 4101-OWDR2 Lab Sample ID: 680-224127-7 Date Collected: 10/18/22 08:40 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 5 5 mL 5 mL 598354 10/29/22 20:04 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-OWLFS2 Lab Sample ID: 680-224127-8 Date Collected: 10/17/22 13:45 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch DII Initial Final Batch Prepared • Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 5 5 mL 5 mL 598354 10/29/22 20:29 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-PW5D Lab Sample ID: 680-224127-9 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 5 5 mL 5 mL 598354 10/29/22 20:54 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-PW41 Lab Sample ID: 680-224127-10 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 5 5 mL 5 mL 598354 10/29/22 21:20 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-PW121 Lab Sample ID: 680-224127-11 Date Collected: 10/19/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598354 10/29/22 13:23 AGW EET PEN Instrument ID: Curie Client Sample ID: 4101-PWSF1 Lab Sample ID: 680-224127-12 Date Collected: 10/18/22 09:25 Matrix: Water Date Received: 10/27/22 08:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 100 5 mL 5 mL 598354 10/29/22 22:35 AGW EET PEN Instrument ID: Curie Eurofins Savannah Page 25 of 36 10/31/2022 Lab Chronicle Client: Environmental Conservation Laboratories Project/Site: CF14375 F Job ID: 680-224127-1 Client Sample ID: 4101-W4A Date Collected: 10/18/22 13:55 Date Received: 10/27/22 08:00 Lab Sample ID: 680-224127-13 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 598354 10/29/22 15:28 AGW EET PEN Instrument ID: Curie Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 0 Eurofins Savannah Page 26 of 36 10/31/2022 SUBCONTRACT ORDER ENCO Cary CF14375 TALS Project #68024012 SENDING LABORATORY: RECEIVING LABORATORY: ENCO Cary 102-A Woodwinds Industrial Court Cary, NC 27511 Phone 919 467 3090 Fax 919 467 3515 Protect Manager Bill Scott Test America (GA) 5102 LaRoche Avenue Savannah, GA 31404 Phone •(912) 354-7858 Fax. -0 V" e Project State of Origin: North Carolina Sub Lab Ill Originating Lab ID Client Matrix Date Sampled Sample Comments Conlaineis Supplied 40mLV+HCI (D) 4101-MW3C Water 40mLV+HCI (E) 40mLV+HCI (F) 17-Oct-22 09:25 Is/ zto uriancio Sub Lab ID Originating Lab ID Client Matrix DateSamp lecl Sample Comments 4101-MW6 Water 19-Oct-22 08:20 8260D SIM ID 27-Oct-22 15 00 02-Nov-22 08 20 sub to Orlando Conwineis Supplied 40niLV-+HCI. (D) 40tnLV+I3CL.(E) 40inLV+11CI (F) Sub Lab ID Originating Lab ID Client -Matrix Date Sampled Sample Comments 4-1-0-1-MW12A Water 17-0ct-12-I-1:30 - - - - - -- -- 8260D SIM ID 27-Oct-22 1500 31-Oct-22 11 30 sub to Orlando Containers Supplied. 40mLV+HCI (D) 40mI,V+HCI (E) 40mLV+HCI (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-M W 12B Water 17-Oct-22 13:15 Analysis Due: lgx.tires - Anit1 sCuirti>Inenis' 8260D SIM 1D 27-Oct-22 15 00 31-Oct-22 13 15 sub to Orlando Containers Supplied_ 40mLV+HCI (D) 40mI V+}ICI (E) 40mLV+HCI (F) Date Sampled Sample Comments Sub Lab ID Originating Lab ID Client Matrix 4101-M W 12 D NVater 17-Oct-22 10:25 Anal sip Due .-Uivirw .... Ana# sip commetits 8260D SIM ID 27-Oct-22 15 00 31-Oct-22 10 25 ... sub to Orlando Containers Supplied 40mLV+HCI (D) 40mLV+HCI (E) 40mLV+l4CI (F) Page 27 of 36 "M/A�&22 SUBCONTRACT ORDER ENCO Cary CF14375 Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-M W 15A Water 18-Oct-22 10:35 Anal sls Due K ;ltres Anal * comments 8260D SIM Ill Containers Sapphetl 40mLV+HCI (D) 27-Oct-22 15 00 40mLV+HCI (E) 01-Nov-22 10 35 40mLV+HCI (F) sub to Orlando Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-OWDR2 Water 18-Oct-22 08:40 Anal sis Due. _ Expires n anal pis tCovmeets • 8260D SIM ID C onloweis Supplied 40mLV+l-ICI (D) 27-Oct-22 15 00 40mLV+HCI (E) 01-Nov-22 08 40 40mLV+HCI (F) sub to Orlando Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-OWLFS2 Water 17-Oct-22 13:45 Analysis Dit Expires Analysis Comments 8260D SIM ID Containers Supplied 40mLV+HCI (D) 27-Oct-22 15 00 40mLV+HCI (E) 31-Oct-22 13 45 40mLV+HCI (F) sub to Orlando Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-PW5D Water I9-Oct-22 09:25 8260D SIM ID 27-Oct-22 15 00 01 Nov-22 09 25 sub to Orlando Containers Supplied 40mLV+HCI-(D) —10mL--V+HeF(I) 40mLV+HCI (F)--- Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-PW41 Water 18-Oct-22 09:25 Analysis Onep(res .. .. Annlysls �Cgx�tmeirts 8260D SIM ID 27-Oct-22 15 00 01-Nov-22 09 25 sub to Orlando Conlameis Supplied 40niLV+I:ICI..(.D). 40ml V+H-CI(I) 40mLV+1-ICI (F). _ ._.._. Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-PW 121 Water 19-Oct-22 09:25 Analysis _ Due ides Anal s' etammenits 8260D SIM ID 27-Oc1-22 15 00 02-Nov-22 09 25 sub to Orlando Conioinei s Supplied 40mLV+1-ICI (D) 40mLV+HCI (E) 40mLV+HCI (F) Released By Dale Received By Date Released By Date Received R� Dale Page 2 o F 3 Page 28 of 36 10/31/2022 SUBCONTRACT ORDER ENCO Cary CF14375 Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-PWSFI Water 18-Oct-22 09:25 Analysis Due Expires Analysis Comments 8260D SIM ID Containers Sipphed 40mLV+I ICI (D) 27-Oct-22 15 00 40mLV+HCI (E) 01-Nov-22 09 25 40mLV+HCI (F) sub to Orlando Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101-W4A Water 18-Oct-22 13:55 Analysis Due Expires Analysis Comments 8260D SIM ID Containers Supplied 40mLV+HCI (D) 27-Oct-22 15 00 40mLV+HCI (E) 01-Nov-22 13 55 40mLV+FICI (F) sub to Orlando Released By Date Received By Date Released By Date Received By Date Page 3 of 3 Page 29 of 36 10/31/2022 (A CL 01 U) w W i5 Ice a ILL 8 15 h 12 ME 0-- (0 441- 0 < ;L bF t7 ' F I 4 z w z UJI 7, M U G jz- lh- I M `4 CC I 13 v Page 30 of 36 10/31/2022 / N th co v CL V x 0' C) w -P, LL CL + pd ti TI Lt CL J) I I L m Page 31 of 36 10/31/2022 -2 —0 ej, 0 T— cc tx tL —calk»:. cc l4i LU 2, h"I aL m 7) uj 0 Page 32 of 36 10/31 --/2022 L X C LL > C m > 1 (D � Cl) fA u O N cu m rn O -1 C o N m L = o m L W U) U) 0- d z o L oc N o m w m O m o z O m ry a u U 2 c t 2 z¢zz ,M: 2( l;E v t O G a a n Li �zoaC3� nF»3rN W N . o mU E E ci E i E (i N N U 9Z Q92 L 7 Ov N OUz d cl Cvm`m vO ' «2O UU) l zL_ Nm ZuE¢U o =c ¢Q ` N ww0 dy oy O LLL T a 0 (000 t `a Q m L) 0 wu_(72 oa F 3 d u sjaulejuo3;ojagwnNlelol n r M m m Cl) co Cl) Cl) c Eo .� Q a E; D uL N w L , m c E E E� c E£ E v w w o 1) o z m m m N c co L r o F o y N J m '� N DU C o m u �a 1 m L v L (o af+ G to 10 L 0 m d C U L E 2 E N o Li N fn Z OQ �" H p c Z `tg 11 .0 E o o c ',0 a) S rn E O m e E Q) c T C N � cS SSA coo o, m cV o U Q oN c ' u c U ° 10 /1 O L° a E o y U o E w t U 4 G b a a a E m /m�� lJ L C 'C u o 0 O O t o Z auexol0-q'L (OOW) 00£09/WIS 409Z9 X X X X X X X X X v d� yO u K x i U o m v S t f0 h a U)c ui (ON Jo SaA) 4SW/SW w�oJJad = m 8 2 E E (ON Jo ssA) aldweS pai9311.1 plel� E _ c ¢ O u a �. N Tn a O J 2 2 di (n =( - H o V N _ N _ N N N N N N N 'a 2 o d T F C w a E E E E O m m E 'u Uo U a `o d E E a„ �(°, aFl V m I I I 04 C E E .c.. c.. E i i ELo E L d m Y ca �J1 E m F O N o m N ap o m� A m� N m� O N m- O (/1 mo W 41 m- c,N (a N . nc N T N W W W W w w W W W m U O N �m N ❑ 9 y ry J C� '- y K N H m C3 Of N N Cl N N N � N N N N N N � N N � Cl N � N N � a10i z T O N .d. N .d, O c i, O N mi-11N o O N # d• 0 30 A O O O O O O O O O rn a a" E m//�� E E in to d-a ❑' F H a O o a (COo cn N d' E t T c o a o� o 0 m` E 0 m c o o d o J o J W U c � O y N � = w '� Z U) Jc _O c Q. w V ❑ uo O m F O Z N N X d (n c ,C m Q v J O v7 z ^ c o to to E`oCO c?c N o U N ^ N_ N N N_ N N `o_ 5 .-. u r _ L U C H LO C N V V V v N V N v C w C -� � .. O C > °D O N N N N N N 0 N u 'Ya o a m w m-' O �•+ ld m C •> N C .� ~ i0 U N O O O O (a - co N m A c rn o .E o E N Q 'j tT Z ul O` N = COO (v O m (�O to (cow � N (V m C d QQ N m ❑ 1Q J0 �, v` N N lL d m om'o OI .. ,� U co � mmNZ G :? m L-.-. m E oLi v m O o om toLom2'a> o cLE-y Z0 UIn UW Q (h Ua fn W aU (n V) v v V' V V V V v V za w ❑ W K K K m Page 33 of 36 10/31 /2022 Login Sample Receipt Checklist Client: Environmental Conservation Laboratories Job Number: 680-224127-1 Login Number: 224127 List Number: 1 Creator: Johnson, Corey M Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True m Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Savannah Page 34 of 36 10/31/2022 Login Sample Receipt Checklist Client: Environmental Conservation Laboratories Login Number: 224127 List Number: 2 Creator: Whitley, Adrian Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. N/A Sample custody seals, if present, are intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A 1.5, 0.8°C IR8 Job Number: 680-224127-1 List Source: Eurofins Pensacola List Creation: 10/28/22 12:04 PM Eurofins Savannah Page 35 of 36 10/31/2022 Accreditation/Certification Summary Client: Environmental Conservation Laboratories Job ID: 680-224127-1 Project/Site: CF14375 Laboratory: Eurofins Pensacola The accreditations/certifications listed below are applicable to this report Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 314 12-31-22 Eurofins Savannah Page 36 of 36 10/31/2022 urofins Environment Testing ANALYTICAL REPORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 E7 Laboratory Job ID: 680-223412-1 Client Project/Site: CF15781 For: Environmental Conservation Laboratories 102 Woodwinds Industrial Ct, Suite A Cary, North Carolina 27511 IAttt�t__n'' : Mr. Bill Scott raw Authorized for release by. 1012812022 2:23:16 PM Naomi Flanagan, Project Manager (912)354-7858 Naomi.Flanagan@et.eurofinsus.com Designee for Sheila Hoffman, Project Manager II (912)250-0279 Sheila.Hoffman@et.eurofinsus.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Environmental Conservation Laboratories Sample Summary Job ID: 680-223412-1 Project/Site: CF15781 Lab Sample ID Client Sample ID Matrix Collected Received 680-223412-1 4101-MW1 Water 10/12/22 13:50 10/18/22 07:00 680-223412-2 4101-MW10 Water 10/14/22 10:50 10/18/22 07:00 680-223412-3 4101-PW3D Water 10/14/22 11:40 10/18/22 07:00 680-223412-4 4101-PW61 Water 10/14/22 12:00 10/18/22 07:00 680-223412-5 4101-PW6D Water 10/14/22 11:35 10/18/22 07:00 680-223412-6 4101-PW101 Water 10/13/22 13:45 10/18/22 07:00 680-223412-7 4101-PW10D Water 10/13/22 14:10 10/18/22 07:00 680-223412-8 4101-PW131 Water 10/12/22 13:10 10/18/22 07:00 680-223412-9 4101-PW14D Water 10/13/22 11:20 10/18/22 07:00 680-223412-10 4101-PW15D Water 10/13/22 10:35 10/18/22 07:00 680-223412-11 4101-PW16D Water 10/13/22 09:35 10/18/22 07:00 680-223412-12 4101-Trip Blank Water 10/12/22 11:40 10/18/22 07:00 Page 2 of 32 Eurofins �+MPP02 Method Summary Client: Environmental Conservation Laboratories Project/Site: CF15781 Job ID: 680-223412-1 U Method Method Description Protocol Laboratory 8260D SIM Volatile Organic Compounds (GC/MS) SW846 EET DEN 5030C Purge and Trap SW846 EET DEN Protocol References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100 Eurofins Savannah Page 3 of 32 10/28/2022 Definitions/Glossary Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Qualifiers GUMS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "Y column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present IDOL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 4 of 32 10/28/2022 Case Narrative C Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Job ID: 680-223412-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-223412-1 Receipt The samples were received on 10/18/2022 7:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.2°C Receipt Exceptions The Chain -of -Custody (COC) was incomplete as received and/or improperly completed. ICOC received for Denver workshare not relinquished. GC/MS VOA Method 8260D_SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 280-591514. An LCS/LCSD pair was analyzed for batch precision and accuracy. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins Savannah Page 5 of 32 10/28/2022 Detection Summary Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-MW1 Lab Sample ID: 680-223412-1 Cmalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 1.0 J 1.4 0.27 ug/L 1 8260D SIM Total/NA ' Client Sample ID: 4101-MW10 Lab Sample ID: 680-223412-2 C Cmalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 12 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW3D Lab Sample ID: 680-223412-3 Cmalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 180 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW61 Lab Sample ID: 680-223412-4 C Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 86 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW6D Lab Sample ID: 680-223412-5 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 180 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW101 Lab Sample ID: 680-223412-6 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 590 14 2.7 ug/L 10 8260D SIM Total/NA Client Sample ID: 4101-PW10D Lab Sample ID: 680-223412-7 1 No Detections. Client Sample ID: 4101-PW131 Lab Sample ID: 680-223412-8 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 84 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW14D Lab Sample ID: 680-223412-9 CAnalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 0.49 J 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW15D Lab Sample ID: 680-223412-10 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 83 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-PW16D Lab Sample ID: 680-223412-11 CAnalyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type 1,4-Dioxane 45 1.4 0.27 ug/L 1 8260D SIM Total/NA Client Sample ID: 4101-Trip Blank Lab Sample ID: 680-223412-12 ENo Detections This Detection Summary does not include radiochemical test results. Page 6 of 32 Eurofins Savannah 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-MW1 Lab Sample ID: 680-223412-1 Date Collected: 10/12/22 13:50 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 1.0 J 1.4 0.27 ug/L 10/26/22 20:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 103 70 - 127 10126122 20:08 1 Dibromofluoromethane (Surr) 100 77 - 120 10126122 20:08 1 F F Eurofins Savannah Page 7 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-MW10 Lab Sample ID: 680-223412-2 Date Collected: 10/14/22 10:50 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 12 1.4 0.27 ug/L 10/26/22 23:33 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 104 70 - 127 10126122 23:33 1 Dibromofluoromethane (Surr) 100 77 - 120 10126122 23:33 1 F F Eurofins Savannah Page 8 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW3D Lab Sample ID: 680-223412-3 Date Collected: 10/14/22 11:40 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 180 1.4 0.27 ug/L 10/26/22 23:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 91 70 - 127 10126122 23:53 1 Dibromofluoromethane (Surr) 85 77 - 120 10126122 23:53 1 F F Eurofins Savannah Page 9 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW61 Lab Sample ID: 680-223412-4 Date Collected: 10/14/22 12:00 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 86 1.4 0.27 ug/L 10/27/22 00:14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 92 70 - 127 10127122 00:14 1 Dibromofluoromethane (Surr) 94 77 - 120 10127122 00:14 1 F F Eurofins Savannah Page 10 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW6D Lab Sample ID: 680-223412-5 Date Collected: 10/14/22 11:35 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 180 1.4 0.27 ug/L 10/27/22 00:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 95 70 - 127 10127122 00:34 1 Dibromofluoromethane (Surr) 96 77 - 120 10127122 00:34 1 F F Eurofins Savannah Page 11 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW101 Lab Sample ID: 680-223412-6 Date Collected: 10/13/22 13:45 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 590 14 2.7 ug/L 10/27/22 22:07 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 95 70 - 127 10127122 22:07 10 Dibromofluoromethane (Surr) 93 77 - 120 10127122 22:07 10 F F Eurofins Savannah Page 12 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW1OD Lab Sample ID: 680-223412-7 Date Collected: 10/13/22 14:10 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.27 1.4 0.27 ug/L 10/27/2217:40 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 100 70- 127 10127122 17.40 1 Dibromofluoromethane (Surr) 97 77 - 120 10127122 17.40 1 F F Eurofins Savannah Page 13 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW131 Lab Sample ID: 680-223412-8 Date Collected: 10/12/22 13:10 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 84 1.4 0.27 ug/L 10/26/22 20:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 98 70 - 127 10126122 20:28 1 Dibromofluoromethane (Surr) 97 77 - 120 10126122 20:28 1 F F Eurofins Savannah Page 14 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW14D Lab Sample ID: 680-223412-9 Date Collected: 10/13/22 11:20 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 0.49 J 1.4 0.27 ug/L 10/27/22 01:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 101 70 - 127 10127122 01:36 1 Dibromofluoromethane (Surr) 97 77 - 120 10127122 01:36 1 F F Eurofins Savannah Page 15 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW151) Lab Sample ID: 680-223412-10 Date Collected: 10/13/22 10:35 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 83 1.4 0.27 ug/L 10/27/22 01:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 101 70 - 127 10127122 01:56 1 Dibromofluoromethane (Surr) 99 77 - 120 10127122 01:56 1 F F Eurofins Savannah Page 16 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW161) Lab Sample ID: 680-223412-11 Date Collected: 10/13/22 09:35 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane 45 1.4 0.27 ug/L 10/27/22 02:17 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 100 70 - 127 10127122 02:17 1 Dibromofluoromethane (Surr) 98 77 - 120 10127122 02:17 1 F F Eurofins Savannah Page 17 of 32 10/28/2022 Client Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-Trip Blank Lab Sample ID: 680-223412-12 Date Collected: 10/12/22 11:40 Matrix: Water Date Received: 10/18/22 07:00 Method: SW846 8260D SIM - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4-Dioxane <0.27 1.4 0.27 ug/L 10/26/2219:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac 1,2-Dichloroethane-d4 (Surr) 102 70- 127 10126122 19:47 1 Dibromofluoromethane (Surr) 99 77- 120 10126122 19:47 1 F F Eurofins Savannah Page 18 of 32 10/28/2022 QC Sample Results Client: Environmental Conservation Laboratories Project/Site: CF15781 Method: 8260D SIM - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 280-591338/6 Matrix: Water Analysis Batch: 591338 MB MB Analyte Result Qualifier RL MDL Unit 1,4-Dioxane <0.27 1.4 0.27 ug/L MB MB Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 102 70- 127 Dibromofluoromethane (Surr) 99 77- 120 Lab Sample ID: LCS 280-591338/3 Matrix: Water Analysis Batch: 591338 Analyte 1,4-Dioxane LCS LCS Surrogate %Recovery Qualifier 1,2-Dichloroethane-d4 (Surr) 99 Dibromofluoromethane (Surr) 97 Lab Sample ID: LCSD 280-59133814 Matrix: Water Analysis Batch: 591338 Analyte 1,4-Dioxane Spike Added 25.0 Limits 70- 127 77- 120 Job ID: 680-223412-1 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 10/26/2219:27 1 Prepared Analyzed Dil Fac 10126122 19:27 1 10126122 19:27 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec Result Qualifier Unit D %Rec Limits 30.1 ug/L 121 25 -141 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 25.0 31.2 ug/L 125 25 -141 4 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 1, 2-Dichloroethane-d4 (Surr) 99 70 -127 Dibromofluoromethane (Surr) 98 77-120 Lab Sample ID: MB 280-591514/6 Matrix: Water Analysis Batch: 591514 MB MB Analyte Result Qualifier RL 1,4-Dioxane <0.27 1.4 MB MB Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 99 70- 127 Dibromofluoromethane (Surr) 95 77- 120 Lab Sample ID: LCS 280-591514/3 Matrix: Water Analysis Batch: 591514 Spike Analyte Added 1,4-Dioxane 50.0 Client Sample ID: Method Blank Prep Type: Total/NA MDL Unit D Prepared Analyzed Dil Fac 0.27 ug/L 10/27/2217:20 1 Prepared Analyzed Dil Fac 10127122 17:20 1 10127122 17:20 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec Result Qualifier Unit D %Rec Limits 55.8 ug/L 112 25 -141 Page 19 of 32 Eurofins Savannah 10/28/2022 QC Sample Results Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Method: 8260D SIM - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 280-591514/3 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 591514 LCS LCS Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 96 70- 127 • Dibromofluoromethane (Surr) 94 77- 120 Lab Sample ID: LCSD 280-591514/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 591514 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 1,4-Dioxane 50.0 57.4 ug/L 115 25 -141 3 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 95 70- 127 Dibromofluoromethane (Surr) 92 77 - 120 Eurofins Savannah Page 20 of 32 10/28/2022 QC Association Summary Client: Environmental Conservation Laboratories Project/Site: CF15781 GC/MS VOA Analysis Batch: 591338 Lab Sample ID Client Sample ID 680-223412-1 4101-M W 1 680-223412-2 4101-MW10 680-223412-3 4101-PW3D 680-223412-4 4101-PW61 680-223412-5 4101-PW6D 680-223412-8 4101-PW131 680-223412-9 4101-PW14D 680-223412-10 4101-PW15D 680-223412-11 4101-PW 16D 680-223412-12 4101-Trip Blank MB 280-591338/6 Method Blank LCS 280-591338/3 Lab Control Sample LCSD 280-591338/4 Lab Control Sample Dup Analysis Batch: 591514 Job ID: 680-223412-1 Prep Type Matrix Method Prep Batch Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Total/NA Water 8260D SIM Lab Sample ID Client Sample ID Prep Type Matrix Method 680-223412-6 4101-PW101 Total/NA Water 8260D SIM 680-223412-7 4101-PW10D Total/NA Water 8260D SIM MB 280-591514/6 Method Blank Total/NA Water 8260D SIM LCS 280-591514/3 Lab Control Sample Total/NA Water 8260D SIM LCSD 280-591514/4 Lab Control Sample Dup Total/NA Water 8260D SIM Prep Batch Page 21 of 32 Eurofins Savannah 10/28/2022 Lab Chronicle Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-MW1 Lab Sample ID: 680-223412-1 Date Collected: 10/12/22 13:50 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/26/22 20:08 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-MW10 Lab Sample ID: 680-223412-2 Date Collected: 10/14/22 10:50 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/26/22 23:33 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW3D Lab Sample ID: 680-223412-3 Date Collected: 10/14/22 11:40 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/26/22 23:53 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW61 Lab Sample ID: 680-223412-4 Date Collected: 10/14/22 12:00 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/27/22 00:14 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW6D Lab Sample ID: 680-223412-5 Date Collected: 10/14/22 11:35 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/27/22 00:34 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW101 Lab Sample ID: 680-223412-6 Date Collected: 10/13/22 13:45 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 10 5 mL 5 mL 591514 10/27/22 22:07 GO EET DEN Instrument ID: VMS E Eurofins Savannah Page 22 of 32 10/28/2022 Lab Chronicle Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Client Sample ID: 4101-PW1OD Lab Sample ID: 680-223412-7 Date Collected: 10/13/22 14:10 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591514 10/27/22 17:40 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW131 Lab Sample ID: 680-223412-8 Date Collected: 10/12/22 13:10 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/26/22 20:28 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW14D Lab Sample ID: 680-223412-9 Date Collected: 10/13/22 11:20 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/27/22 01:36 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW15D Lab Sample ID: 680-223412-10 Date Collected: 10/13/22 10:35 Matrix: Water Date Received: 10/18/22 07:00 Batch Batch DII Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260D SIM 1 5 mL 5 mL 591338 10/27/22 01:56 GO EET DEN Instrument ID: VMS E Client Sample ID: 4101-PW16D Date Collected: 10/13/22 09:35 Date Received: 10/18/22 07:00 Batch Batch Prep Type Type Method Total/NA Analysis 8266D SIM Instrument ID: VMS E Client Sample ID: 4101-Trip Blank Date Collected: 10/12/22 11:40 Date Received: 10/18/22 07:00 Lab Sample ID: 680-223412-11 Matrix: Water Dil Initial Final Batch Prepared Run Factor Amount Amount Number or Analyzed Analyst Lab 1 5 mL 5 mL 591338 10/27/22 02:17 GO EET DEN Batch Batch DII Initial Prep Type Type Method Run Factor Amount Total/NA Analysis 8260D SIM 1 5 mL Instrument ID: VMS E Laboratory References: EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100 Lab Sample ID: 680-223412-12 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 5 mL 591338 10/26/22 19:47 GO EET DEN Eurofins Savannah Page 23 of 32 10/28/2022 I�p�INN�WIIMI��IIVIp��680-223412 Chain of Custody SUBCONTRACT ORDER -TV CF 5781y SENDING LABORATORY: RECEIVING LABORATORY: ENCO Cary Test America (GA) 102-A Woodwinds Industrial Court 5102 LaRoche Avenue Cary, NC 27511 Savannah, GA 31404` Phone 919 467 3090 Phone (912) 354-7858 Fax. 919 467 3515 Fax, -0 Project Manager Bill Scott Project State of Origin. North Carolina 1�)pt-KIWI Water 12-Oct-2213:50 Analysis Due IgXpireta A016 rz1"M11400 8260D SIM ID 24-Oct-22 15 00 26-Oct-22 13 50 sub to Orlando Conlarners Supplied 40m1 V+FICI (D) 40mLV+NCI (F) 40ml-V+1-10 (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments f iZA 4'&Q-NIWI0 Water 14-Oct-2210:50 8260D SIM ID 24-Oct-22 IS 00 28-Oct-22 10 50 sub to Orlando Containers Supplied W�0' 40m1_V+HCI (D) 40mLV+HCI (F) 40tnlV+IICI (F) Sub Lab IU Originating Lab ID Client Matrix Date Sampled Sample Comments 4JQ 440, PW3D Water 12-Oct-2211:40 Anal sis .... Dux fires; Anal Comfits 8260D SIM ID 24-Oct-22 15 00 26-Oct-22 11 40 sub to Orlando Conlcuners Supplied 40mLV+HCI (D) 40mLV+HCI (E) 40mLV+1`ICI (I') Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4tol 441-PW61 NVatei 14-00-22 12:00 Analysis Due. ExpiresAnal fist *� dents 82600 SIM ID 24-00-22 15 00 28-Oct-22 12 00 sub to Orlando C ontnrners Supplied 40m1V+I ICI (D) 40ml-V+FICI (E) 40mLV+HCI (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 44N-PW6D Water 14-Oct 22 11:35 AnaF sis. Due Lxptres 8260D SIM ID 24-00-22 15 00 28-Oct-22 11 35 sub to Orlando Conlamers Supplied 40ml V-i-FICI () 40mLV+HCI (E) 40mLV+HCI (F) I () I I I K -7 00 Date Released By Date Recetred By Date Page I ul , Page 24 of 32 10/28/2022 SUBCONTRACT ORDER ENCO Cary Cr15781 Sub Lab ILY Originating Lab ID Client Matrix Date Sampled Sample Comments j lj l� I X01-PW 101 Water 13-Oct-22 13:45 Analysis Due Expires tlnal sis Commen s 8260D SIM ID 24-Oct-22 15 00 27-Oct-22 13 45 sub to Orlando C ontaurers Snpphed 40mLV+1 K-1 (D) 40mLV+HCI (C) 40mLV+HCI (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments u101 4XI-PWIOD Water 13-Oct-22 14: 10 Analysis _ Due Expires: Atnalysis Cotmments 8260D SIM ID 24-Oct-22 15 00 27-Oct-22 14 10 sub to Orlando Containers Supplied 40mLV+FICI (D) 40mLV+HCI (E) 40mLV+HCI (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4101 4)QI-PW131 Water 12-Oct-22 13: 10 Analysis Due ]Expires Analysis Comments 8260D SIM ID 24-Oct-22 15 00 26-Oct-22 13 10 sub to Orlando C onlamers Snpphed 40mLV+FICI (D) 40ml V+FICI (I-) 40mLV+HCI (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments Ll1 401-PW14D Water 13-Oct-2211:20 Analysis Due Expires Analysis Comments 8260D SIM ID 24-Oct-22 15 00 27-Oct-22 11 20 sub to Orlando C ontarner s Snpphed 40m1 V+FICI (D) 40mLV+FICI (E) 40tnLV+I-tCl (F) LjiO 4 4\01-PW15D Water 13-Oct-2210:35 Analysis Due Expires Analysis Comments 8260D SIM ID 24-Oct-22 15 00 27-Oct-22 10 35 sub to Orlando Containers Snpphed 40mLV+FICI (D) 40mLV+HCI (F) 40mLV+1­I0 (F) Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments L) I U 4,�)1-PW161) Water 13-Oct-22 09:35 Analysis Due Expires Analysis Comments 8260D SIM ID 24-OLt-22 15 00 27-Oct-22 09 35 sub to Orlando Containers Supplied 40mLV+IiCI (D) 40mLV+I-ICI (L) 40mLV+FICI (F) Released By Date Received By Date Released By Date Received By Date Page 2 of ; Page 25 of 32 10/28/2022 SUBCONTRACT ORDER ENCO Cary ?4 rolls CF15781 Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments 4\01-TripBlank Water 12-Oct-22 11:40 Analysis Due Expires Analysis Comments 8260D SHM ID 24-Oct-22 15 00 26-Oct-22 1 l 40 sub to Orlando C'onlantei.s Supplier! 40ml V+FIC I (C.) 4011ILV+1R-I (D) 0 Released I3y Dale Received By Date Released By Date Received Bti Dale Page 3 of ; Page 26 of 32 10/28/2022 CL 0) t, 0 Page 27 of 32 10/28/2022 r, O N z 0 o Qc m M Z � m O,O�a� c¢'o I E m x z O m m.0 a u< o G x z o Eo Zi z0 wU) »3YN N N u o mU L J U U a0 7 U i0 u¢ m R O) m m N O N V m o m 9v ua m O o m x ¢(nxs ¢ U o$ oa o w GI o z I- N N Z OG cx0 u 31-¢ m U m c m E ❑ p .. aoU v o' O� G O N x z N 2 Z Lr ¢ a= p W W o + OU a n. ° co a ¢mUOww(7x_ m« Q) sjau!e;uoo;oiagwnN!e)ol m m m m m m m m co c o E m o 2 n "A e 2 > Ly c W a� tiN d d E t o E 2 GJ E No E m >?Z z (0 N y o wco m o ` O V C ce U 2U E N p N M 7 U Az r o �,,;p �m N Q m O aci `m o o c L n N m O E ro 6 m oQ i0 ��� cc. o Q N C7 Q c m m a E Cj U c '0 j 9 c m 0 c o o m '> _c N O O O m a) U o�'- C c 2 a a n E m o C > U > U > U `v o m o Z auexoiO-b'L ((]OW)OOCOS/W!S 409Z8 X X X X X X X X X F w' N' U s E (ON Jo saA) OSW/SW wio}iad c o u o c f (ON jo saA) a!dweg pajall!d plaid E = o m < mg o. o J x W U1 x ¢ y a F c N N N N N N N Ul Ul 2i m m a tad t E E E F m O @ E o U o U o U O ad Z E m nui " E a d : d m E;u a m N G/ C NS C N� C NO c N5 C a) C NO C NO c NN C N m Y '' O N m �C E Xc, (2 oO N7 wn! w`- N�2 y NN2 i/ m � mf m� m� m� m� m� ca co m.- m ac y N a U) Lu W w W W Lu w w Lu J m W Q N N c� N N v N N v N N v N N v N N c'� N N m N N a N N o y N K N y m m N v x `- L T o f °: - N v Nc o O - .- 0 0 0 �- 0 0 r- 0 0 o U) y w v E n o C, N w i! # N N Q 3 E m o mm d E m E t m t d C m a o o a O 3 o a` (0 O m m .o E m v o -mU >c >o J W � J y m O d m w m O -. u) m .O rn L O N a+ f0 o u Q ~ O z cv- C v WFd E O U) L) Q m W G o !n C M Cf N m N N o Nm N N N m C r1 O .- M m CqO w W U.. O N N N N A�- c .00.. ONN EO - N N O NO O o c L- Za > rom co 0. C]N7E c wL Ua J U3) oO v o Q - O Q F5 Q v o E O Y oc�E�} m .. oo m m a, 2i 3 0 m Y z t t a mao ^� W M Z v^i a a a a m y r E v n °v 2 O° aj _ o ii v o 0 0 0 0 0 0 0 0 o v m o c .� E '� w U U U U) UFO a U¢ n U a m w a` U in N v v v v v v v v v z a a J 0 W o oof 0 Page 28 of 32 10/28/2022 U7 .e o m m 1p m O M m Z .• W c 0,0 m mp(A cgOo oQv x N� O o o w c0 m mMA = z¢ z z z S r¢ g a h o u u rn G O E o E 0 E° l( Vi `�ZO°.U<r to l-�> 2iYN m 9 N C o cU L J C U U U UJ N '- U A J U ¢ m 10 m N N o A v ¢ N a v« v v\ Zr NN 0x0 .. mWm i n'n = O ofco m _ G J sjauleluoa to iagwnN lelol moc o , ri E. 2c .(V "mow, mE E E E5 0 E a m� m m m v m o z N o I C E a O o o o c r z, o lu m o x rn •� ~° u N w J 10 - (0 O U C 2 m n u Qi y L m d r = O Q .. W U o N Z O J o" A y h IN0 0 w m E a Z N m t •- y •O `m N n O O E u) m m m N m A 0 o m c K U e c: C_ quo, � U Q U r ! O a' m O u c° ° > InO O U m N N cU L W 1O o C U Q G N 2 N N a N a d E F- m r m +�. O C suexoi0-l"� (pOW) 0060SIWIS ante X X X cca 2 Z o E w' m '� u w u u o U (ON JO sal.) OSW/SW w�oliad co o m d o co) y m E - a N E (ON JO saA) eldweS pajalll=l Platt XIL O m J a: t W U7 _ _ a x ° < o N - y; M hi O Ui> !U a o � m a T m a T m v o co:y > a Is E E F m � E N u U o U U m o2i `oEm O E A G do N N a m c rn~vim a m a N' o m m u N N E E E E C M 2 C_ M N C_ 7 m m S m m o n W o m o W w .- w m n tr N m J �D Q it O a m O 0 N N N c`� N N M N N N omi « o E d N 0 6 m .. n N o a � iE o - •- o c- 0 o O' m rn v Z' co E E E c N # o o E E d w d m a o a O 3 o a` m f" E c o a o 0 0 c E tO cm oo z m S o U G O J W N J c p d N n t W.�o J O ? N ♦+ o " a O U fE p and o m F' Z y X -• fq L m J ? t E O In V c o > ` _ N w m N N ° N N M V V V d' N W C O O C M M N a m G -� M O N N O� c E 01 4: L N p N ^ l0 (7 O co O m tMa m m N C Z E m � u) M Y ° E o V C N a `p U 3 N 00 •c 0 0 (om p a c a to A b Z a a a U) In >•N C C o.c E m No o r�i z� a a I- d w v y a E� E� m 6� orrS = w� E ct v y o> a g Q U N L (n o N UI- v 01 ¢ v D UQ m O nU O a-m E w 'O LL a`U n to o v 0 c o v za a O W ¢ U 0 Page 29 of 32 10/28/2022 Login Sample Receipt Checklist Client: Environmental Conservation Laboratories Job Number: 680-223412-1 Login Number: 223412 List Number: 1 Creator: Flanagan, Naomi V Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True m Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Savannah Page 30 of 32 10/28/2022 Login Sample Receipt Checklist Client: Environmental Conservation Laboratories Login Number: 223412 List Number: 2 Creator: Lee, Jerry Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. False Is the Field Sampler's name present on COC? N/A There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Job Number: 680-223412-1 List Source: Eurofins Denver List Creation: 10/25/22 04:56 PM COC not relinquished. Eurofins Savannah Page 31 of 32 10/28/2022 Accreditation/Certification Summary C Client: Environmental Conservation Laboratories Job ID: 680-223412-1 Project/Site: CF15781 Laboratory: Eurofins Denver All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. Authority Program Identification Number Expiration Date A21-A Dept. of Defense ELAP 2907.01 10-31-23 A21-A ISO/IEC 17025 2907.01 10-31-23 Alabama State Program 40730 09-30-12 Alaska (UST) State 18-001 02-08-23 Arizona State AZ0713 12-20-22 Arkansas DEQ State 19-047-0 05-31-23 California State 2513 01-08-23 Connecticut State PH-0686 09-30-22 Florida NELAP E87667-57 06-30-23 Georgia State 4025-011 01-08-23 Illinois NELAP 2000172019-1 04-30-23 Iowa State IA#370 12-02-22 Kansas NELAP E-10166 04-30-23 Kentucky (WW) State KY98047 12-31-22 Louisiana NELAP 30785 06-30-14 m Louisiana NELAP 30785 06-30-23 Minnesota NELAP 1788752 12-31-22 Nevada State CO000262020-1 07-31-23 New Hampshire NELAP 205319 04-28-23 New Jersey NELAP 190002 06-30-23 New York NELAP 59923 04-01-23 North Carolina (WW/SW) State 358 12-31-22 North Dakota State R-034 01-08-23 Oklahoma NELAP 8614 08-31-23 Oregon NELAP 4025-011 01-09-23 Pennsylvania NELAP 013 07-31-23 South Carolina State 72002001 01-08-23 Texas NELAP TX104704183-08-TX 09-30-09 Texas NELAP T104704183-21-19 09-30-23 US Fish & Wildlife US Federal Programs 058448 07-31-23 USDA US Federal Programs P330-20-00065 03-06-23 Utah NELAP QUAN5 06-30-13 Utah NELAP CO000262019-11 07-31-23 Virginia NELAP 10490 06-14-23 Washington State C583-19 08-03-23 West Virginia DEP State 354 11-30-22 Wisconsin State 999615430 08-31-23 Wyoming (UST) A21-A 2907.01 10-31-22 " Accreditation/Certification renewal pending - accreditation/certification considered valid. Eurofins Savannah Page 32 of 32 10/28/2022