23057_CharlotteVan&Storage_Soil Export Options SP8-SP9 Package_20211229

December 29, 2021
Sent Via E-mail
Mr. Jeffrey W. Harris
Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202 [e-mail]

Subject: Brownfields Soil Management Options for SP-8 and SP-9 Charlotte Van & Storage Co. Brownfield Property Charlotte, Mecklenburg County Brownfields Project No. 23057-19-060

Dear Mr. Harris: The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received a request to export soil from the Charlotte Van & Storage Co. Brownfields Property. This request
was submitted on your behalf by Ms. Haley Martin, PG of Hart & Hickman, PC via email on
December 28, 2021, and requests approval to export approximately 1,500 cubic yards of soil to a beneficial fill reuse site known as the Fleet Maintenance facility in Mt. Holly, North Carolina. DEQ Brownfields provided letters approving soil export options on September 7 and 15, October 11, and November 18, 2021, in response to previous requests.

For this request, DEQ Brownfields reviewed the December 28, 2021, Data Summary Package which includes analytical results for stockpile soil samples SP-8 and SP-9, as well as soil analytical data from the proposed Fleet Maintenance receiving facility.
Based on our review of the data, the DEQ Brownfield determines that soils may be exported as
outlined in the table below. Please note that the “Beneficial Fill” option listed in the table below is specifically approved for the Fleet Maintenance facility in Mt. Holly, NC. Other Beneficial Fill and Land Clearing & Inert Debris Landfill (LCID) options may be available; however, DEQ requires that the receiving facility be identified and approved prior to export. The receiving
facility should have metals concentrations which are consistent with those from the Brownfields
Property. Similarly, many site soils, including those with impacts, may be suitable for use at another Brownfields Property that has similar impacts.
Mr. Jeffery Harris December 29, 2021 Page 2

Upon determination of the export facility, whether another Brownfields Property, LCID, or
another beneficial fill reuse, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
LOCATION ID DEPTH (Ft)1 MANAGEMENT OPTIONS2
SP-8 stockpile BFILL, LCID, CDLF, MSWLF
SP-9 stockpile BFILL, LCID, CDLF, MSWLF
Notes: 1) Depth listed is total depth of available analytical data. Additional sampling would potentially
be required beyond these depths prior to export. 2) BFILL= Beneficial Fill; LCID = Land Clearing & Inert Debris Landfill; CDLF = Construction & Demolition landfill; MSWLF = Municipal Solid Waste landfill (MSWLF) facility. Per the Charlotte Van & Storage Co.’s approved Environmental Management Plan (EMP), the soils are to be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease
transfer until appropriate characterization can be completed. In addition, and also in accordance with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail].
Sincerely,
Peter L. Doorn, Project Manager
Brownfields Program Ec: Haley Martin, Hart & Hickman, PC Ralph McGee, Hart & Hickman, PC Tracy Wahl, DEQ Brownfields
1
Doorn, Peter L
From:Haley Martin <[e-mail]>
Sent:Tuesday, December 28, 2021 10:55 AM
To:Doorn, Peter L
Cc:Ralph McGee
Subject:[External] Charlotte Van and Storage - Soil Management Options
Attachments:Charlotte Van & Storage Co. - December 2021 Stockpile - Data Package.pdf
Follow Up Flag:Follow up
Flag Status:Completed
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Report Spam.

Pete,

Results of recent grading activities completed at the Charlotte Van and Storage Brownfields
Property generated one 500-cubic yard stockpile and one 1,000-cubic yard stockpile of excess soil that
cannot be re-used on-Site and will need to be exported. Therefore, H&H collected one 5-point composite
soil sample from 500-cubic yard stockpile (SP-8) and one 5-point composite soil sample from 1,000-cubic
yard stockpile (SP-9) to characterize the material and assist in determining the most suitable facility for
final disposition of the approximately 1,500 cubic yards of soil planned for export. We have received the
stockpile soil sample laboratory analytical and prepared the attached data summary package which
includes a tabular summary of the analytical data in comparison to the PSRGs and results of soil samples
collected at the Fleet facility. Below is a brief summary of the sampling activities and results.

The composite stockpile soil samples selected for laboratory analyses were collected directly into
dedicated laboratory supplied sample containers, labeled with the date, time, and sample identification,
and placed in a laboratory supplied sample cooler with ice. The samples were submitted to Waypoint
Analytical (Waypoint) under standard chain of custody protocols for analysis of semi volatile organic
compounds (SVOCs) by EPA Method 8270 and Resource Conservation and Recovery Act (RCRA) metals
plus hexavalent chromium by EPA Methods 6020/7471/7199. In addition to the composite soil samples
described above, one representative grab soil sample was collected from each stockpile. The grab soil
samples were collected from an undisturbed portion of soil directly into laboratory supplied glassware and
submitted to Waypoint under standard chain of custody protocols for analysis of VOCs by EPA Method
8260.

As noted in the attached data summary package, the analytical results for SP-8 and SP-9 did not identify
organic compounds at concentrations above the Preliminary Soil Remediation Goals
(PSRGs) and metals concentrations appear to generally be consistent with background concentrations for
the Site and the Fleet Maintenance facility. The PD would like to transport the approximate the
approximate 1,500 cubic yards of stockpiled soil to the Fleet Maintenance facility.

We appreciate your reviewing this data to assist in keeping the construction schedule on track. Please let
us know if you have any questions or concerns.
2

Thanks,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

Table 1
Summary of Soil Analytical Data
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID BG-1 BG-2 SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab
Depth (ft bgs)2-4 0-2
Date Range Range Mean
Units
VOCs (8260D)
Acetone NA 0.007 J NA 0.005 J NA NA NA NA NA 25 12,000 140,000 -- -- --
SVOCs (8270E)ALL BDL NA ALL BDL NA NA NA NA NA NA -- -- -- -- -- --
Metals (6020/7471/7199)
Arsenic 1.77 NA 0.523 J NA 3.03 1.28 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 114 NA 146 NA 38.1 94.6 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium <0.0756 NA <0.0759 NA 0.434 J <0.122 <0.0655 <0.0649 0.207 J 3.0 14 200 ND - 0.434 1.0 - 10* 4.3
Chromium (total) 150 NA 57.0 NA 59.9 47.1 80.8 30.9 25.7 ---- --47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium 1.40 NA 1.14 NA 0.540 J <0.388 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 148.6 NA 55.86 NA 59.4 47.1 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 4.90 NA 3.11 NA 11.6 7.33 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0578 NA <0.0166 NA 0.0502 0.0365 J 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium <1.24 NA <1.24 NA 1.04 0.586 J 10.8 J <1.06 <1.47 J 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.0563 NA <0.0566 NA <0.202 <0.236 <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; BDL = below detection limit
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
SP-9
Sample Location Fleet Maintenance Facility
Protection of
Groundwater
PSRGs (1)
Grab Grab
1-3
12/2/2019 8/27/2021
Screening Criteria
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals
Background
Metals (2)
mg/kg
SP-8
500 cubic yard stockpile 1,000 cubic yard stockpile Background
--
12/6/2021
mg/kg
C:\Users\hmartin\Desktop\Charlotte Van & Storage Co. (LEN‐008) Stockpile
12/28/2021
Table 1 (Page 1 of 1)
Hart & Hickman, PC

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/22/2021
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-340-0007 Client Project Description: LEN-008
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/6/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 71
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-340-0007
Page 2 of 71
Report Number:
Sample Summary Table
Client Project Description:
21-340-0007
LEN-008
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
12/06/2021 09:40Solids 89937 SP-8 12/06/2021 10:57
12/06/2021 09:40Solids 89937 SP-8 12/06/2021 10:57 7199 ALS
12/06/2021 10:20Solids 89938 SP-9 12/06/2021 10:57
12/06/2021 10:20Solids 89938 SP-9 12/06/2021 10:57 7199 ALS
12/06/2021 09:40TCLP 91005 SP-8 12/06/2021 10:57
ALS: ALS Environmental - Rochester, Rochester, NY
Page 3 of 71
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-340-0007
Report Limit
Project:LEN-008
V 89937SP-8
1.77 12/08/2021 18:566020BArsenicmg/Kg - dry 0.129
114 12/08/2021 18:566020BBariummg/Kg - dry 1.93
150 12/08/2021 18:566020BChromiummg/Kg - dry 0.398
4.90 12/08/2021 18:566020BLeadmg/Kg - dry 0.193
0.0578 12/07/2021 14:567471BMercury (Total)mg/Kg - dry 0.0165
J0.007 12/07/2021 12:588260DAcetonemg/Kg - dry 0.003
27.3 12/06/2021 12:35SW-DRYWT Moisture %
V 89938SP-9
J0.523 12/08/2021 19:026020BArsenicmg/Kg - dry 0.130
146 12/08/2021 19:026020BBariummg/Kg - dry 1.93
57.0 12/08/2021 19:026020BChromiummg/Kg - dry 0.400
3.11 12/08/2021 19:026020BLeadmg/Kg - dry 0.193
J0.005 12/07/2021 13:268260DAcetonemg/Kg - dry 0.003
27.6 12/06/2021 12:35SW-DRYWT Moisture %
V 91005SP-8
Leachate 12/21/2021 16:30SW-1311 TCLP Metals Extraction
Page 4 of 71

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: LEN-008 Lab Report Number: 21-340-0007
Date: 12/22/2021
Metals Analyses Method 6020B Sample 89953 Analyte: Barium
QC Batch No: V12608/V12577 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Chromium
QC Batch No: V12608/V12577 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Chromium QC Batch No: V12608/V12577
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Lead QC Batch No: V12608/V12577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dinitrophenol QC Batch No: V12781/V12619
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1310 ug/kg which calculates to a recovery of 78% which is within the acceptable recovery range.
Sample 89903 Analyte: 2,4-Dinitrophenol QC Batch No: V12781/V12619
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1060 ug/kg which calculates to a recovery of 63.6% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol QC Batch No: V12781/V12619 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 1170 ug/kg which calculates to a recovery of 70% which is within the acceptable recovery range.
Analyte: 3,3`-Dichlorobenzidine QC Batch No: V12781/V12619 Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits. Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V12781/V12619
Page 5 of 71

Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1350 ug/kg which calculates to a recovery of 81% which is within the acceptable recovery range.
Sample 89903 Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V12781/V12619 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1100 ug/kg which calculates to a recovery of 65.8% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V12781/V12619
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1140 ug/kg which calculates to a recovery of 68.6% which is within the acceptable recovery range.
Analyte: Aniline
QC Batch No: V12781/V12619 Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid
QC Batch No: V12781/V12619 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1010 ug/kg which calculates to a recovery of 60% which is within the acceptable recovery range. Sample 89903 Analyte: Benzoic Acid
QC Batch No: V12781/V12619 Benzoic Acid did not recover in the MSD.
Analyte: Benzoic Acid QC Batch No: V12781/V12619 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 29.2 ug/kg which calculates to a recovery of 1.7% which is below the acceptable recovery range.
Analyte: Bis(2-chloroethyl)ether QC Batch No: V12781/V12619
Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits. Analyte: Indeno(1,2,3-cd)pyrene QC Batch No: V12781/V12619 Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits.
Analyte: Pyridine QC Batch No: V12781/V12619 Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits.
Page 6 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.3 %Moisture 1 12/06/21 12:35 SW-DRYWTCLB
1.77 mg/Kg - dry 0.129 1.38Arsenic 10 12/08/21 18:56 6020BEDV
114 mg/Kg - dry 1.93 13.8Barium 10 12/08/21 18:56 6020BEDV
<0.0756 mg/Kg - dry 0.0756 0.688Cadmium 10 12/08/21 18:56 6020BEDV
150 mg/Kg - dry 0.398 1.38Chromium 10 12/08/21 18:56 6020BEDV
4.90 mg/Kg - dry 0.193 1.38
Lead 10 12/08/21 18:56 6020BEDV
0.0578 mg/Kg - dry 0.0165 0.0413Mercury (Total)1 12/07/21 14:56 7471BEDV
<1.24 mg/Kg - dry 1.24 2.75Selenium 10 12/08/21 18:56 6020BEDV
<0.0563 mg/Kg - dry 0.0563 0.688Silver 10 12/08/21 18:56 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 7 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
0.007 J mg/Kg - dry 0.003 0.027Acetone 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/07/21 12:58 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/07/21 12:58 V12543TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/07/21 12:58 V12543TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 12/07/21 12:58 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/07/21 12:58 V12543TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/07/21 12:58 V12543TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/07/21 12:58 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/07/21 12:58 V12543TBL
<0.019 mg/Kg - dry 0.019 0.343Ethanol 1 12/07/21 12:58 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.068Ethyl Tertiary Butyl Ether (ETBE)1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/07/21 12:58 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 12/07/21 12:58 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 12/07/21 12:58 V12543TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 12/07/21 12:58 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/07/21 12:58 V12543TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 12/07/21 12:58 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/07/21 12:58 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/07/21 12:58 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/07/21 12:58 V12543TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/07/21 12:58 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/07/21 12:58 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/07/21 12:58 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/07/21 12:58 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/07/21 12:58 V12543
Surrogate: 4-Bromofluorobenzene 98.3 Limits: 70-130%12/07/21 12:581 TBL V12543
Surrogate: Dibromofluoromethane 99.4 Limits: 84-123%12/07/21 12:581 TBL V12543
Surrogate: Toluene-d8 90.1 Limits: 76-129%12/07/21 12:581 TBL V12543
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.159 mg/Kg - dry 0.159 0.907Acenaphthene 1 12/11/21 02:12 V12781JMV
<0.144 mg/Kg - dry 0.144 0.907Acenaphthylene 1 12/11/21 02:12 V12781JMV
<0.209 mg/Kg - dry 0.209 0.907Aniline 1 12/11/21 02:12 V12781JMV
<0.196 mg/Kg - dry 0.196 0.907Anthracene 1 12/11/21 02:12 V12781JMV
<0.191 mg/Kg - dry 0.191 0.907
Benzo(a)anthracene 1 12/11/21 02:12 V12781JMV
<0.202 mg/Kg - dry 0.202 0.907Benzo(a)pyrene 1 12/11/21 02:12 V12781JMV
<0.200 mg/Kg - dry 0.200 0.907Benzo(b)fluoranthene 1 12/11/21 02:12 V12781JMV
<0.187 mg/Kg - dry 0.187 0.907Benzo(g,h,i)perylene 1 12/11/21 02:12 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.188 mg/Kg - dry 0.188 0.907Benzo(k)fluoranthene 1 12/11/21 02:12 V12781JMV
<0.797 mg/Kg - dry 0.797 2.75Benzoic Acid 1 12/11/21 02:12 V12781JMV
<0.144 mg/Kg - dry 0.144 0.907Benzyl alcohol 1 12/11/21 02:12 V12781JMV
<0.162 mg/Kg - dry 0.162 0.907Bis(2-Chloroethoxy)methane 1 12/11/21 02:12 V12781JMV
<0.147 mg/Kg - dry 0.147 0.907Bis(2-Chloroethyl)ether 1 12/11/21 02:12 V12781JMV
<0.187 mg/Kg - dry 0.187 0.453Bis(2-Chloroisopropyl)ether 1 12/11/21 02:12 V12781JMV
<0.165 mg/Kg - dry 0.165 0.907Bis(2-ethylhexyl)phthalate 1 12/11/21 02:12 V12781JMV
<0.149 mg/Kg - dry 0.149 0.9074-Bromophenyl phenyl ether 1 12/11/21 02:12 V12781JMV
<0.155 mg/Kg - dry 0.155 0.453
Butyl benzyl phthalate 1 12/11/21 02:12 V12781JMV
<0.127 mg/Kg - dry 0.127 0.9074-Chloro-3-methylphenol 1 12/11/21 02:12 V12781JMV
<0.154 mg/Kg - dry 0.154 0.4534-Chloroaniline 1 12/11/21 02:12 V12781JMV
<0.159 mg/Kg - dry 0.159 0.9072-Chloronaphthalene 1 12/11/21 02:12 V12781JMV
<0.135 mg/Kg - dry 0.135 0.9072-Chlorophenol 1 12/11/21 02:12 V12781JMV
<0.173 mg/Kg - dry 0.173 1.384-Chlorophenyl phenyl ether 1 12/11/21 02:12 V12781JMV
<0.195 mg/Kg - dry 0.195 0.907Chrysene 1 12/11/21 02:12 V12781JMV
<0.316 mg/Kg - dry 0.316 0.907
Dibenz(a,h)anthracene 1 12/11/21 02:12 V12781JMV
<0.163 mg/Kg - dry 0.163 0.907Dibenzofuran 1 12/11/21 02:12 V12781JMV
<0.129 mg/Kg - dry 0.129 0.9071,2-Dichlorobenzene 1 12/11/21 02:12 V12781JMV
<0.133 mg/Kg - dry 0.133 0.9071,3-Dichlorobenzene 1 12/11/21 02:12 V12781JMV
<0.134 mg/Kg - dry 0.134 0.4531,4-Dichlorobenzene 1 12/11/21 02:12 V12781JMV
<0.202 mg/Kg - dry 0.202 0.9073,3'-Dichlorobenzidine 1 12/11/21 02:12 V12781JMV
<0.131 mg/Kg - dry 0.131 0.9072,4-Dichlorophenol 1 12/11/21 02:12 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.247 mg/Kg - dry 0.247 0.907Diethyl phthalate 1 12/11/21 02:12 V12781JMV
<0.239 mg/Kg - dry 0.239 0.907Dimethyl phthalate 1 12/11/21 02:12 V12781JMV
<0.148 mg/Kg - dry 0.148 0.4532,4-Dimethylphenol 1 12/11/21 02:12 V12781JMV
<0.147 mg/Kg - dry 0.147 0.907Di-n-butyl phthalate 1 12/11/21 02:12 V12781JMV
<0.330 mg/Kg - dry 0.330 2.064,6-Dinitro-2-methylphenol 1 12/11/21 02:12 V12781JMV
<0.715 mg/Kg - dry 0.715 2.062,4-Dinitrophenol 1 12/11/21 02:12 V12781JMV
<0.132 mg/Kg - dry 0.132 0.9072,4-Dinitrotoluene 1 12/11/21 02:12 V12781JMV
<0.148 mg/Kg - dry 0.148 0.9072,6-Dinitrotoluene 1 12/11/21 02:12 V12781JMV
<0.196 mg/Kg - dry 0.196 0.453
Di-n-Octyl Phthalate 1 12/11/21 02:12 V12781JMV
<0.169 mg/Kg - dry 0.169 0.907Fluoranthene 1 12/11/21 02:12 V12781JMV
<0.176 mg/Kg - dry 0.176 0.907Fluorene 1 12/11/21 02:12 V12781JMV
<0.145 mg/Kg - dry 0.145 0.907Hexachlorobenzene 1 12/11/21 02:12 V12781JMV
<0.134 mg/Kg - dry 0.134 0.907Hexachlorobutadiene 1 12/11/21 02:12 V12781JMV
<0.215 mg/Kg - dry 0.215 0.907Hexachlorocyclopentadiene 1 12/11/21 02:12 V12781JMV
<0.108 mg/Kg - dry 0.108 0.907Hexachloroethane 1 12/11/21 02:12 V12781JMV
<0.246 mg/Kg - dry 0.246 0.907
Indeno(1,2,3-cd)pyrene 1 12/11/21 02:12 V12781JMV
<0.262 mg/Kg - dry 0.262 0.907Isophorone 1 12/11/21 02:12 V12781JMV
<0.145 mg/Kg - dry 0.145 0.9071-Methylnaphthalene 1 12/11/21 02:12 V12781JMV
<0.137 mg/Kg - dry 0.137 0.9072-Methylnaphthalene 1 12/11/21 02:12 V12781JMV
<0.133 mg/Kg - dry 0.133 0.9072-Methylphenol 1 12/11/21 02:12 V12781JMV
<0.116 mg/Kg - dry 0.116 0.9073&4 Methylphenol 1 12/11/21 02:12 V12781JMV
<0.198 mg/Kg - dry 0.198 0.907Naphthalene 1 12/11/21 02:12 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.133 mg/Kg - dry 0.133 0.9072-Nitroaniline 1 12/11/21 02:12 V12781JMV
<0.165 mg/Kg - dry 0.165 0.9073-Nitroaniline 1 12/11/21 02:12 V12781JMV
<0.128 mg/Kg - dry 0.128 0.4534-Nitroaniline 1 12/11/21 02:12 V12781JMV
<0.159 mg/Kg - dry 0.159 0.453Nitrobenzene 1 12/11/21 02:12 V12781JMV
<0.122 mg/Kg - dry 0.122 0.9072-Nitrophenol 1 12/11/21 02:12 V12781JMV
<0.160 mg/Kg - dry 0.160 0.9074-Nitrophenol 1 12/11/21 02:12 V12781JMV
<0.361 mg/Kg - dry 0.361 0.907N-Nitrosodimethylamine 1 12/11/21 02:12 V12781JMV
<0.248 mg/Kg - dry 0.248 0.907N-Nitrosodiphenylamine 1 12/11/21 02:12 V12781JMV
<0.162 mg/Kg - dry 0.162 0.907
N-Nitroso-di-n-propylamine 1 12/11/21 02:12 V12781JMV
<0.477 mg/Kg - dry 0.477 1.38Pentachlorophenol 1 12/11/21 02:12 V12781JMV
<0.286 mg/Kg - dry 0.286 0.907Phenanthrene 1 12/11/21 02:12 V12781JMV
<0.154 mg/Kg - dry 0.154 0.907Phenol 1 12/11/21 02:12 V12781JMV
<0.184 mg/Kg - dry 0.184 0.907Pyrene 1 12/11/21 02:12 V12781JMV
<0.108 mg/Kg - dry 0.108 0.453Pyridine 1 12/11/21 02:12 V12781JMV
<0.147 mg/Kg - dry 0.147 0.9071,2,4-Trichlorobenzene 1 12/11/21 02:12 V12781JMV
<0.132 mg/Kg - dry 0.132 0.907
2,4,5-Trichlorophenol 1 12/11/21 02:12 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
89937 Matrix:
12/6/2021 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.132 mg/Kg - dry 0.132 0.9072,4,6-Trichlorophenol 1 12/11/21 02:12 V12781JMV
Surrogate: Phenol-d5 76.0 Limits: 34-121%12/11/21 02:121 JMV V12781
Surrogate: 2-Fluorobiphenyl 81.4 Limits: 44-115%12/11/21 02:121 JMV V12781
Surrogate: 2-Fluorophenol 79.0 Limits: 35-115%12/11/21 02:121 JMV V12781
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%12/11/21 02:121 JMV V12781
Surrogate: 4-Terphenyl-d14 84.4 Limits: 54-127%12/11/21 02:121 JMV V12781
Surrogate: 2,4,6-Tribromophenol 79.6 Limits: 39-132%12/11/21 02:121 JMV V12781
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.6 %Moisture 1 12/06/21 12:35 SW-DRYWTCLB
0.523 J mg/Kg - dry 0.130 1.38Arsenic 10 12/08/21 19:02 6020BEDV
146 mg/Kg - dry 1.93 13.8Barium 10 12/08/21 19:02 6020BEDV
<0.0759 mg/Kg - dry 0.0759 0.691Cadmium 10 12/08/21 19:02 6020BEDV
57.0 mg/Kg - dry 0.400 1.38Chromium 10 12/08/21 19:02 6020BEDV
3.11 mg/Kg - dry 0.193 1.38
Lead 10 12/08/21 19:02 6020BEDV
<0.0166 mg/Kg - dry 0.0166 0.0414Mercury (Total)1 12/07/21 14:59 7471BEDV
<1.24 mg/Kg - dry 1.24 2.76Selenium 10 12/08/21 19:02 6020BEDV
<0.0566 mg/Kg - dry 0.0566 0.691Silver 10 12/08/21 19:02 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 16 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
0.005 J mg/Kg - dry 0.003 0.027Acetone 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/07/21 13:26 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/07/21 13:26 V12543TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/07/21 13:26 V12543TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 12/07/21 13:26 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/07/21 13:26 V12543TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/07/21 13:26 V12543TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/07/21 13:26 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/07/21 13:26 V12543TBL
<0.019 mg/Kg - dry 0.019 0.345Ethanol 1 12/07/21 13:26 V12543TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/07/21 13:26 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 12/07/21 13:26 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 12/07/21 13:26 V12543TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 12/07/21 13:26 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/07/21 13:26 V12543TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 12/07/21 13:26 V12543TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/07/21 13:26 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/07/21 13:26 V12543TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/07/21 13:26 V12543TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/07/21 13:26 V12543TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12542 12/07/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/07/21 13:26 V12543TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/07/21 13:26 V12543TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/07/21 13:26 V12543TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/07/21 13:26 V12543
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%12/07/21 13:261 TBL V12543
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/07/21 13:261 TBL V12543
Surrogate: Toluene-d8 90.6 Limits: 76-129%12/07/21 13:261 TBL V12543
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.160 mg/Kg - dry 0.160 0.912Acenaphthene 1 12/11/21 02:34 V12781JMV
<0.145 mg/Kg - dry 0.145 0.912Acenaphthylene 1 12/11/21 02:34 V12781JMV
<0.209 mg/Kg - dry 0.209 0.912Aniline 1 12/11/21 02:34 V12781JMV
<0.197 mg/Kg - dry 0.197 0.912Anthracene 1 12/11/21 02:34 V12781JMV
<0.191 mg/Kg - dry 0.191 0.912
Benzo(a)anthracene 1 12/11/21 02:34 V12781JMV
<0.203 mg/Kg - dry 0.203 0.912Benzo(a)pyrene 1 12/11/21 02:34 V12781JMV
<0.201 mg/Kg - dry 0.201 0.912Benzo(b)fluoranthene 1 12/11/21 02:34 V12781JMV
<0.187 mg/Kg - dry 0.187 0.912Benzo(g,h,i)perylene 1 12/11/21 02:34 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.189 mg/Kg - dry 0.189 0.912Benzo(k)fluoranthene 1 12/11/21 02:34 V12781JMV
<0.801 mg/Kg - dry 0.801 2.76Benzoic Acid 1 12/11/21 02:34 V12781JMV
<0.145 mg/Kg - dry 0.145 0.912Benzyl alcohol 1 12/11/21 02:34 V12781JMV
<0.162 mg/Kg - dry 0.162 0.912Bis(2-Chloroethoxy)methane 1 12/11/21 02:34 V12781JMV
<0.147 mg/Kg - dry 0.147 0.912Bis(2-Chloroethyl)ether 1 12/11/21 02:34 V12781JMV
<0.187 mg/Kg - dry 0.187 0.457Bis(2-Chloroisopropyl)ether 1 12/11/21 02:34 V12781JMV
<0.165 mg/Kg - dry 0.165 0.912Bis(2-ethylhexyl)phthalate 1 12/11/21 02:34 V12781JMV
<0.150 mg/Kg - dry 0.150 0.9124-Bromophenyl phenyl ether 1 12/11/21 02:34 V12781JMV
<0.156 mg/Kg - dry 0.156 0.457
Butyl benzyl phthalate 1 12/11/21 02:34 V12781JMV
<0.127 mg/Kg - dry 0.127 0.9124-Chloro-3-methylphenol 1 12/11/21 02:34 V12781JMV
<0.154 mg/Kg - dry 0.154 0.4574-Chloroaniline 1 12/11/21 02:34 V12781JMV
<0.160 mg/Kg - dry 0.160 0.9122-Chloronaphthalene 1 12/11/21 02:34 V12781JMV
<0.135 mg/Kg - dry 0.135 0.9122-Chlorophenol 1 12/11/21 02:34 V12781JMV
<0.174 mg/Kg - dry 0.174 1.384-Chlorophenyl phenyl ether 1 12/11/21 02:34 V12781JMV
<0.196 mg/Kg - dry 0.196 0.912Chrysene 1 12/11/21 02:34 V12781JMV
<0.317 mg/Kg - dry 0.317 0.912
Dibenz(a,h)anthracene 1 12/11/21 02:34 V12781JMV
<0.164 mg/Kg - dry 0.164 0.912Dibenzofuran 1 12/11/21 02:34 V12781JMV
<0.130 mg/Kg - dry 0.130 0.9121,2-Dichlorobenzene 1 12/11/21 02:34 V12781JMV
<0.134 mg/Kg - dry 0.134 0.9121,3-Dichlorobenzene 1 12/11/21 02:34 V12781JMV
<0.135 mg/Kg - dry 0.135 0.4571,4-Dichlorobenzene 1 12/11/21 02:34 V12781JMV
<0.203 mg/Kg - dry 0.203 0.9123,3'-Dichlorobenzidine 1 12/11/21 02:34 V12781JMV
<0.132 mg/Kg - dry 0.132 0.9122,4-Dichlorophenol 1 12/11/21 02:34 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.248 mg/Kg - dry 0.248 0.912Diethyl phthalate 1 12/11/21 02:34 V12781JMV
<0.240 mg/Kg - dry 0.240 0.912Dimethyl phthalate 1 12/11/21 02:34 V12781JMV
<0.149 mg/Kg - dry 0.149 0.4572,4-Dimethylphenol 1 12/11/21 02:34 V12781JMV
<0.147 mg/Kg - dry 0.147 0.912Di-n-butyl phthalate 1 12/11/21 02:34 V12781JMV
<0.331 mg/Kg - dry 0.331 2.074,6-Dinitro-2-methylphenol 1 12/11/21 02:34 V12781JMV
<0.718 mg/Kg - dry 0.718 2.072,4-Dinitrophenol 1 12/11/21 02:34 V12781JMV
<0.133 mg/Kg - dry 0.133 0.9122,4-Dinitrotoluene 1 12/11/21 02:34 V12781JMV
<0.149 mg/Kg - dry 0.149 0.9122,6-Dinitrotoluene 1 12/11/21 02:34 V12781JMV
<0.197 mg/Kg - dry 0.197 0.457
Di-n-Octyl Phthalate 1 12/11/21 02:34 V12781JMV
<0.169 mg/Kg - dry 0.169 0.912Fluoranthene 1 12/11/21 02:34 V12781JMV
<0.176 mg/Kg - dry 0.176 0.912Fluorene 1 12/11/21 02:34 V12781JMV
<0.146 mg/Kg - dry 0.146 0.912Hexachlorobenzene 1 12/11/21 02:34 V12781JMV
<0.134 mg/Kg - dry 0.134 0.912Hexachlorobutadiene 1 12/11/21 02:34 V12781JMV
<0.216 mg/Kg - dry 0.216 0.912Hexachlorocyclopentadiene 1 12/11/21 02:34 V12781JMV
<0.109 mg/Kg - dry 0.109 0.912Hexachloroethane 1 12/11/21 02:34 V12781JMV
<0.247 mg/Kg - dry 0.247 0.912
Indeno(1,2,3-cd)pyrene 1 12/11/21 02:34 V12781JMV
<0.263 mg/Kg - dry 0.263 0.912Isophorone 1 12/11/21 02:34 V12781JMV
<0.146 mg/Kg - dry 0.146 0.9121-Methylnaphthalene 1 12/11/21 02:34 V12781JMV
<0.138 mg/Kg - dry 0.138 0.9122-Methylnaphthalene 1 12/11/21 02:34 V12781JMV
<0.134 mg/Kg - dry 0.134 0.9122-Methylphenol 1 12/11/21 02:34 V12781JMV
<0.117 mg/Kg - dry 0.117 0.9123&4 Methylphenol 1 12/11/21 02:34 V12781JMV
<0.198 mg/Kg - dry 0.198 0.912Naphthalene 1 12/11/21 02:34 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.133 mg/Kg - dry 0.133 0.9122-Nitroaniline 1 12/11/21 02:34 V12781JMV
<0.165 mg/Kg - dry 0.165 0.9123-Nitroaniline 1 12/11/21 02:34 V12781JMV
<0.129 mg/Kg - dry 0.129 0.4574-Nitroaniline 1 12/11/21 02:34 V12781JMV
<0.160 mg/Kg - dry 0.160 0.457Nitrobenzene 1 12/11/21 02:34 V12781JMV
<0.122 mg/Kg - dry 0.122 0.9122-Nitrophenol 1 12/11/21 02:34 V12781JMV
<0.161 mg/Kg - dry 0.161 0.9124-Nitrophenol 1 12/11/21 02:34 V12781JMV
<0.363 mg/Kg - dry 0.363 0.912N-Nitrosodimethylamine 1 12/11/21 02:34 V12781JMV
<0.250 mg/Kg - dry 0.250 0.912N-Nitrosodiphenylamine 1 12/11/21 02:34 V12781JMV
<0.162 mg/Kg - dry 0.162 0.912
N-Nitroso-di-n-propylamine 1 12/11/21 02:34 V12781JMV
<0.479 mg/Kg - dry 0.479 1.38Pentachlorophenol 1 12/11/21 02:34 V12781JMV
<0.287 mg/Kg - dry 0.287 0.912Phenanthrene 1 12/11/21 02:34 V12781JMV
<0.154 mg/Kg - dry 0.154 0.912Phenol 1 12/11/21 02:34 V12781JMV
<0.185 mg/Kg - dry 0.185 0.912Pyrene 1 12/11/21 02:34 V12781JMV
<0.109 mg/Kg - dry 0.109 0.457Pyridine 1 12/11/21 02:34 V12781JMV
<0.147 mg/Kg - dry 0.147 0.9121,2,4-Trichlorobenzene 1 12/11/21 02:34 V12781JMV
<0.133 mg/Kg - dry 0.133 0.912
2,4,5-Trichlorophenol 1 12/11/21 02:34 V12781JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-9
89938 Matrix:
12/6/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12619 12/09/21 09:02
<0.133 mg/Kg - dry 0.133 0.9122,4,6-Trichlorophenol 1 12/11/21 02:34 V12781JMV
Surrogate: Phenol-d5 85.0 Limits: 34-121%12/11/21 02:341 JMV V12781
Surrogate: 2-Fluorobiphenyl 83.2 Limits: 44-115%12/11/21 02:341 JMV V12781
Surrogate: 2-Fluorophenol 89.2 Limits: 35-115%12/11/21 02:341 JMV V12781
Surrogate: Nitrobenzene-d5 79.6 Limits: 37-122%12/11/21 02:341 JMV V12781
Surrogate: 4-Terphenyl-d14 86.2 Limits: 54-127%12/11/21 02:341 JMV V12781
Surrogate: 2,4,6-Tribromophenol 88.9 Limits: 39-132%12/11/21 02:341 JMV V12781
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 71
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-340-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/06/2021
LEN-008
Report Date : 12/22/2021
Sample ID :
Lab No :
Sampled:SP-8
91005 Matrix:
12/6/2021 9:40
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 12/21/21 16:30 SW-1311JMC
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A_6020B
6020B Prep Batch(es):V13144 12/22/21 09:44
<0.019 mg/L 0.019 0.050TCLP Chromium 5 12/22/21 16:05 V13146EDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 71
December 20, 2021 Service Request No:R2112804
Angela OvercashPrism Laboratories, Inc.
P.O. Box 240543Charlotte, NC 28224-0543
All testing was performed according to our laboratory’s quality assurance program and met the requirements of the TNI standards except as noted in the case narrative report. Any testing not included in the lab's accreditation is identified on a Non-Certified Analytes report. All results are
intended to be considered in their entirety. ALS Environmental is not responsible for use of less than
the complete report. Results apply only to the individual samples submitted to the lab for analysis, as listed in the report. The measurement uncertainty of the results included in this report is within that expected when using the prescribed method(s), and represented by Laboratory Control Sample control limits. Any events, such as QC failures or Holding Time exceedances, which may add to the
uncertainty are explained in the report narrative or are flagged with qualifiers. The flags are explained
in the Report Qualifiers and Definitions page of this report.
For your reference, these analyses have been assigned our service request numberEnclosed are the results of the sample(s) submitted to our laboratory
Laboratory Results for:21-340-0007
Dear Angela,
December 07, 2021R2112804.
Please contact me if you have any questions. My extension is 7475. You may also contact me via email at [e-mail].
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Meghan Pedro
Project Manager
dba ALS Environmental
ALS Group USA, Corp.
ADDRESS
FAXPHONE
1565 J efferson Road, Building 300, Suite 360, Rochester, NY 14623
[phone]+1 585 288 5380 |
Page 1 of 24
Page 26 of 71
Narrative Documents
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 2 of 24
Page 27 of 71
CASE NARRATIVE
Client:
Project:
Sample Matrix:
Service Request:
Date Received:
Waypoint Analytical formerly Prism Laboratories, Inc.
21-340-0007
Soil
R2112804
12/07/2021
All  analyses were performed consistent with the quality assurance program of ALS  Environmental.  This report contains  analytical results for samples for the Tier II level requested by the client.
Sample Receipt:
Two soil samples were received for analysis at ALS Environmental on 12/07/2021. Any discrepancies upon initial sample inspection are annotated on the sample receipt and preservation form included within this report.  The samples were stored at minimum in accordance with the analytical method requirements. General Chemistry:
No significant anomalies were noted with this analysis.
1565 Jefferson Rd, Building 300, Rochester, NY 14623 | 585-288-5380 | www.alsglobal.com
Approved by Date 12/20/2021
Page 3 of 24
Page 28 of 71
CLIENT ID:SP-8 Lab ID:R2112804-001
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 1.40 0.06 0.55 mg/Kg 7199
Total Solids 70.0 Percent ALS SOP
CLIENT ID:SP-9 Lab ID:R2112804-002
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 1.14 0.06 0.54 mg/Kg 7199
Total Solids 72.5 Percent ALS SOP
SAMPLE DETECTION SUMMARY
Page 4 of 24
Page 29 of 71
Sample Receipt Information
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 5 of 24
Page 30 of 71
SP-8R2112804-001 12/6/2021 0940
SP-9R2112804-002 12/6/2021 1020
Client:Waypoint Analytical formerly Prism Laboratories, Inc.Service Request:R2112804
Project:21-340-0007/1090EXP
SAMPLE CROSS-REFERENCE
SAMPLE #CLIENT SAMPLE ID DATE TIME
Printed 12/20/2021 4:47:24 PM Sample SummaryPage 6 of 24
Page 31 of 71
"
I
'I,
I
'I
"
i
'I','
"Waypoint
ANALYTICAL
12/06/202111:23:25
Export Batch Report
Export Batch Id : 1090EXP
To:ALS Environm ental - Rochester
1565 Jefferson Rd, Bid, 300 Ste, 360
Rochester, NY 14623
585-288-5380
-------------------------,
449 Springbrook Rd, Charlolle, NC 28217
Main 704.529.6364
www.waypolntanalytfcal.com
Page 1 of 1
Created:12/6/202111:23:03
,Com puter: W PALM S-056
User: Angela D Overcash
Project M anager: Angela D Overcash
From :W aypoint Analytical, LLC (Charlotte)
449 Springbrook Road
Charlotte, NC 28217
704-529-6364
IiI,
I
Repprt Np Due pate
21-340-0007 12{13{2021
21-340-0007 12{13{2021
Sam ple Date Custpm er Sam ple Np
12{06{2021 09:40 SP-8
12{06{2021 10:20 SP-9
*Use Custom er ID for Sam ple IO
*Report to M OL on dry weight basis
*Need 4 day TAT
Rush Y!!U'tl! M ethod No
89937 SW-7199
89938 SW-7199
FeeCode Description
Hexavalent Chrom ium 7199 (S~B)
Hexavalent Chrom ium 7199 (SUB)
I
!
I
Sam pled By
Rem arks
Relinquished By (sign)
Relinquished By (sign)
M ethod of Shipm ent Blank { Cooter Tem p,
, Date / Tim e
Date {nm e
j;01/tJkJ
(R2f12804 ~"5-i
Unli~,illlliiiiiill\I1111111111 11111 11111111 ~
Page 7 of 24
Page 32 of 71
Cooler Receipt and Preservation Check Form
Were Custody seals on outside of cooler?Y 5a
2 Custody papers properly completed (ink, signed)?Y N 5b
3 Did all bottlesarrive in good condition (unbroken)?Y N 6
4 Circle:.et Ie ry Ice Gel packs present?Y N 7
j
R2112804 5Prllm L.boretorl •• ,Inc.ilffii~i11111111111111111111111111111111111111
Folder Number .
COURIER: ALS UPS ~ VELOCITY CLIENT
Perchlorate samples have required headspace? Y . N
Did VOA vials, Alk,or Sulfide have sig' bubbles? Y N
Where did the bottlesoriginate?ALSIROC [
SoilVOA received as: Bulk Encore 5035set
by:eProject/Client h }1tr1
Cool~r receivedon ,~;;/
Y N
Y N
Saroe Day Rule
Y N
Y N
Y N
Y N
Y N
Y N
ID: IR#7 (IR"#Ij)
Y N
Y N
Y N
Y N
Time:lOlL.
y
If out of Temperature, note packinglice condition: ~[c •.melted Poorly Packed (described below)
&Client Approval to Run Samples: Slanding Approval Client aware at drop-off Client notified by: _
8. Temperature Readings
Observed Temp (0C)
Within 0-6°C?
If <O°C,were samples frozen?
All saroples held in storage location:
5035 samples placed in storagolocation:
by ....,ec<---on/)-.9.at /03..\
by on at within 48.hours of saropling? Y N--- ---
Cooler BreakdownlPreservation Check": Date:/J.7 Time:~/~$f~r~O__ ~_b-y:~@~~ _
9. Were all bottle labels complete (i.e.analysis, preservation; etc.)? ~ NO
10. Didall bottle labels and tags agree with custody papers?~ NO
11. Were correct containers used for the tests indicated? ~ NO
12.Were 5035 vialsacceptable-(nb extra labels, not leaking)?YES NO
~13.Air Samoles: Cassettes i Tubes Intact Y / N with MS Y / N Canisters Pressurized Tedlar@ Bags Intlated
pH Lot Oftest Reagent Preserved?Lot Received Exp Sarople ID Vol. Lot Adde""""Final
paper Yes No Adjusted Added pH
>12 NaOH
<2 HNO,
:s2 H2SO4
<4 NaHS04
5-9 For608pest No Notiryfor3day
Residual ForCN,If +,contact PM to add
Chlorine Phenol, 625,
N",S,O,(625,608,
(,)6080est 522
eN),ascorbic (phenol).
Na2S20)
ZnAcetate - -
"VOAs and 1664 Not to be tested before analysis.
HCI ""Otherwise, all bottles of all samples with chemical preservatives
are checked (not iust reDresentativ~t
Bottle lotnumbers:~a.J~~~-~_
Explain all Discrepanciesl Other Comments:
HPROD BULK
lITR FLDT
SUB HGFB
ALS LL354\
Labels secondary reviewed by:~~~ _
PC Secondary Review: _
P:\rNTRANET\QAQC\Fonns Controlled\Cooler Receipt rt9.doc
'significant air bubbles: VOA > 5-6 mm : WC >I in. diaroeter
03/0212021
Page 8 of 24
Page 33 of 71
Miscellaneous Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 9 of 24
Page 34 of 71

RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\QUALIF_routine rev 6.doc 9/30/21
REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
J Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
DoD: concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
“Notes” column of the Form I, this qualifier
denotes analysis was performed out of
Holding Time.
H Analysis was performed out of hold time for
tests that have an “immediate” hold time
criteria.
# Spike was diluted out.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post-Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% difference between the two
GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesticide/Aroclor is not
confirmed (≥100% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value derived
from a study designed to provide the lowest
concentration that will be detected 99% of the time.
Values between the MDL and MRL are estimated
(see J qualifier).
LOD Limit of Detection. A value at or above the MDL
which has been verified to be detectable.
ND Non-Detect. Analyte was not detected at the
concentration listed. Same as U qualifier.

Rochester Lab ID # for State Accreditations¹

¹ Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements of the current NELAP/TNI standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited. For a specific list of accredited analytes, contact the laboratory or go to
https://www.alsglobal.com/locations/americas/north-america/usa/new-york/rochester-environmental

NELAP States
Florida ID # E87674
New Hampshire ID # 2941
New York ID # 10145
Pennsylvania ID# 68-786
Virginia #460167
Non-NELAP States
Connecticut ID #PH0556
Delaware Approved
Maine ID #NY01587
North Carolina #36701
North Carolina #676
Rhode Island LAO00333
Page 10 of 24
Page 35 of 71
ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources BoardCAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental QualityDHSDepartment of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation ProgramGCGas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LUFT Leaking Underground Fuel Tank
M Modified
MCL Maximum Contaminant Level is the highest permissible concentration of a substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable NumberMRLMethod Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not DetectedNIOSHNational Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum HydrocarbonstrTrace level is the concentration of an analyte that is less than the PQL but greater than or equal to the MDL.
Acronyms
ALS Laboratory Group
Page 11 of 24
Page 36 of 71
ALS SOP Total SolidsSoil
ALS Group USA, Corp.
dba ALS Environmental
Client:
Analyte
New York Department of HealthCertifying Agency:
Non-Certified Analytes
Matrix
Project:
Waypoint Analytical formerly Prism Laboratories, Inc.
21-340-0007/1090EXP
Service Request:R2112804
Method
21-0000612477 rev 00Superset Reference:Printed 12/20/2021 4:48:07 PM
Page 12 of 24
Page 37 of 71
12/7/21Date Received:
Date Collected:
SoilSample Matrix:
12/6/21
Extracted/Digested ByAnalysis Method Analy]ed By
SP-8Sample Name:
Lab Code:R2112804-001
7199 KAWONG KWONG
ALS SOP KAWONG
12/7/21Date Received:
Date Collected:
SoilSample Matrix:
12/6/21
Extracted/Digested ByAnalysis Method Analy]ed By
SP-8Sample Name:
Lab Code:R2112804-001.R01
7199 KAWONG KWONG
12/7/21Date Received:
Date Collected:
SoilSample Matrix:
12/6/21
Extracted/Digested ByAnalysis Method Analy]ed By
SP-9Sample Name:
Lab Code:R2112804-002
7199 KAWONG KWONG
ALS SOP KAWONG
12/7/21Date Received:
Date Collected:
SoilSample Matrix:
12/6/21
Extracted/Digested ByAnalysis Method Analy]ed By
SP-9Sample Name:
Lab Code:R2112804-002.R01
7199 KAWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Project:
R2112804
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 13 of 24
Page 38 of 71

RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev 2.doc 12/20/19

INORGANIC PREPARATION METHODS
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.

Water/Liquid Matrix Solid/Soil/Non-Aqueous Matrix

Analytical Method Preparation Method Analytical Method Preparation
Method
200.7 200.2 6010C 3050B
200.8 200.2 6020A 3050B
6010C 3005A/3010A 6010C TCLP (1311)
extract
3005A/3010A
6020A ILM05.3 6010 SPLP (1312) extract 3005A/3010A
9034 Sulfide Acid Soluble 9030B 7199 3060A
SM 4500-CN-E Residual
Cyanide
SM 4500-CN-G 300.0 Anions/ 350.1/
353.2/ SM 2320B/ SM
5210B/ 9056A Anions
DI extraction
SM 4500-CN-E WAD
Cyanide
SM 4500-CN-I For analytical methods not listed, the preparation
method is the same as the analytical method
reference.

Page 14 of 24
Page 39 of 71
Sample Results
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 15 of 24
Page 40 of 71
General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 16 of 24
Page 41 of 71
Client:
12/07/21 10:20
R2112804
Date Received:
Date Collected:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:12/06/21 09:40
Inorganic Parameters
Basis:Dry
Analysis MethodAnalyte Name QDate Analy]ed Date ExtractedDil.MDLMRLResultUnits
Sample Name:SP-8
Lab Code:R2112804-001
Chromium, Hexavalent 12/12/21 17:16 12/09/2110.060.551.407199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 17 of 24
Page 42 of 71
Client:
12/07/21 10:20
R2112804
Date Received:
Date Collected:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:12/06/21 09:40
Inorganic Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate Analy]ed Date ExtractedDil.MDLMRLResultUnits
Sample Name:SP-8
Lab Code:R2112804-001
Total Solids 12/09/21 07:30 NA1--70.0ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 18 of 24
Page 43 of 71
Client:
12/07/21 10:20
R2112804
Date Received:
Date Collected:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:12/06/21 10:20
Inorganic Parameters
Basis:Dry
Analysis MethodAnalyte Name QDate Analy]ed Date ExtractedDil.MDLMRLResultUnits
Sample Name:SP-9
Lab Code:R2112804-002
Chromium, Hexavalent 12/12/21 17:32 12/09/2110.060.541.147199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 19 of 24
Page 44 of 71
Client:
12/07/21 10:20
R2112804
Date Received:
Date Collected:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:12/06/21 10:20
Inorganic Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate Analy]ed Date ExtractedDil.MDLMRLResultUnits
Sample Name:SP-9
Lab Code:R2112804-002
Total Solids 12/09/21 07:30 NA1--72.5ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 20 of 24
Page 45 of 71
QC Summary Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 21 of 24
Page 46 of 71
General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 22 of 24
Page 47 of 71
Client:
NA
R2112804
Date Received:
Date Collected:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:Dry
Analysis MethodAnalyte Name QDate Analy]ed Date ExtractedDil.MDLMRLResultUnits
Sample Name:Method Blank
Lab Code:R2112804-MB
Chromium, Hexavalent 12/12/21 13:16 12/09/2110.050.40 U0.407199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 12/20/2021 4:47:25 PM 21-0000612477 rev 00Superset Reference:
Page 23 of 24
Page 48 of 71
Analyte Name
R2112804
Date Analy]ed:
Service Request:
Soil
21-340-0007/1090EXP
Waypoint Analytical formerly Prism Laboratories, Inc.
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
General Chemistry Parameters
Dry
mg/Kg
Basis:
Units:
Lab Control Sample
R2112804-LCS
12/12/21
Spike AmountResult  Rec  Rec LimitsAnalytical Method
dba ALS Environmental
ALS Group USA, Corp.
QA/QC Report
Chromium, Hexavalent 80-120103 643662 7199
21-0000612477 rev 00Superset Reference:Printed 12/20/2021 4:47:25 PM
Page 24 of 24
Page 49 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V12608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V12577
Associated Lab Samples: 89937, 89938
LRB-V12577 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/08/21 17:501.000.0940<0.0940mg/KgArsenic
12/08/21 17:5010.01.40<1.40mg/KgBarium
12/08/21 17:500.5000.0550<0.0550mg/KgCadmium
12/08/21 17:501.000.290<0.290mg/KgChromium
12/08/21 17:501.000.140<0.140mg/KgLead
12/08/21 17:502.000.900<0.900mg/KgSelenium
12/08/21 17:500.5000.0410<0.0410mg/KgSilver
LCS-V12577Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.011.912.5mg/KgArsenic 80-120
94.011.812.5mg/KgBarium 80-120
10012.512.5mg/KgCadmium 80-120
10212.812.5mg/KgChromium 80-120
99.012.412.5mg/KgLead 80-120
92.011.512.5mg/KgSelenium 80-120
84.04.215.00mg/KgSilver 80-120
V 89953-MS-V12577 V 89953-MSD-V12577Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.2 98.011.312.512.50.631mg/KgArsenic 90.0 75-125 7.6 20
33.5 -310*28.412.512.574.2mg/KgBarium -350*75-125 16.4 20
13.0 10411.612.512.5<0.0550mg/KgCadmium 93.0 75-125 11.3 20
36.5 -170*52.012.512.559.9mg/KgChromium -63*75-125 35.0*20
Page 1 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 50 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V12608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V12577
V 89953-MS-V12577 V 89953-MSD-V12577Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
22.2 -35*21.112.512.526.6mg/KgLead -44*75-125 5.0 20
11.8 94.011.412.512.5<0.900mg/KgSelenium 91.0 75-125 3.4 20
4.31 86.03.905.005.00<0.0410mg/KgSilver 78.0 75-125 9.9 20
V 89953-PDS-V12577Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/08/21 18:2398.012.3mg/KgArsenic
12/08/21 18:2397.048.3mg/KgBarium
12/08/21 18:2396.011.9mg/KgCadmium
12/08/21 18:2310142.9mg/KgChromium
12/08/21 18:2398.025.2mg/KgLead
12/08/21 18:2398.012.3mg/KgSelenium
12/08/21 18:2394.011.7mg/KgSilver
Page 2 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 51 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analysis (TCLP)
6020B
V13146QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3010A_6020B
QC Prep:V13144
Associated Lab Samples: 91005
LRB-V13144 Matrix: TCLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/22/21 15:440.0500.019<0.019mg/LTCLP Chromium
LCS-V13144Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.02.312.50mg/LTCLP Chromium 80-120
Page 3 of 20Date:12/22/2021 04:36 PM
Page 52 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V12529QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V12506
Associated Lab Samples: 89937, 89938
LRB-V12506 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/07/21 13:350.03000.0120<0.0120mg/KgMercury (Total)
LCS-V12506Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.00.4100.417mg/KgMercury (Total)80-120
V 89966-MS-V12506 V 89966-MSD-V12506Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.402 96.00.4000.4170.417<0.0120mg/KgMercury (Total)96.0 80-120 0.4 20
V 89966-PDS-V12506Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/07/21 13:5399.00.206mg/KgMercury (Total)
Page 4 of 20Date:12/22/2021 04:36 PM
Page 53 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
Associated Lab Samples: 89937, 89938
LRB-V12542 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/07/21 12:300.0200.002<0.002mg/KgAcetone
12/07/21 12:300.0200.001<0.001mg/KgAcrolein
12/07/21 12:300.0200.0008<0.0008mg/KgAcrylonitrile
12/07/21 12:300.0050.0006<0.0006mg/KgBenzene
12/07/21 12:300.0050.0005<0.0005mg/KgBromobenzene
12/07/21 12:300.0050.0008<0.0008mg/KgBromochloromethane
12/07/21 12:300.0050.001<0.001mg/KgBromodichloromethane
12/07/21 12:300.0050.001<0.001mg/KgBromoform
12/07/21 12:300.0100.001<0.001mg/KgBromomethane
12/07/21 12:300.0050.0005<0.0005mg/Kgn-Butylbenzene
12/07/21 12:300.0050.0006<0.0006mg/Kgsec-Butyl benzene
12/07/21 12:300.0050.0005<0.0005mg/Kgtert-Butyl benzene
12/07/21 12:300.0050.0006<0.0006mg/KgCarbon Disulfide
12/07/21 12:300.0050.001<0.001mg/KgCarbon Tetrachloride
12/07/21 12:300.0050.0007<0.0007mg/KgChlorobenzene
12/07/21 12:300.0050.0009<0.0009mg/KgChlorodibromomethane
12/07/21 12:300.0100.0009<0.0009mg/KgChloroethane
12/07/21 12:300.0050.001<0.001mg/KgChloroform
12/07/21 12:300.0100.0006<0.0006mg/KgChloromethane
12/07/21 12:300.0050.0005<0.0005mg/Kg2-Chlorotoluene
12/07/21 12:300.0050.0004<0.0004mg/Kg4-Chlorotoluene
12/07/21 12:300.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
12/07/21 12:300.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
12/07/21 12:300.0050.0006<0.0006mg/Kg1,2-Dibromoethane
12/07/21 12:300.0050.0006<0.0006mg/KgDibromomethane
12/07/21 12:300.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
12/07/21 12:300.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 5 of 20Date:12/22/2021 04:36 PM
Page 54 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
Associated Lab Samples: 89937, 89938
LRB-V12542 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/07/21 12:300.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
12/07/21 12:300.0100.001<0.001mg/KgDichlorodifluoromethane
12/07/21 12:300.0050.0008<0.0008mg/Kg1,1-Dichloroethane
12/07/21 12:300.0050.001<0.001mg/Kg1,2-Dichloroethane
12/07/21 12:300.0050.0007<0.0007mg/Kg1,1-Dichloroethene
12/07/21 12:300.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
12/07/21 12:300.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
12/07/21 12:300.0050.0004<0.0004mg/Kg1,2-Dichloropropane
12/07/21 12:300.0050.0006<0.0006mg/Kg1,3-Dichloropropane
12/07/21 12:300.0050.001<0.001mg/Kg2,2-Dichloropropane
12/07/21 12:300.0050.0008<0.0008mg/Kg1,1-Dichloropropene
12/07/21 12:300.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
12/07/21 12:300.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
12/07/21 12:300.2500.014<0.014mg/KgEthanol
12/07/21 12:300.0050.0006<0.0006mg/KgEthylbenzene
12/07/21 12:300.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
12/07/21 12:300.0100.0008<0.0008mg/KgHexachlorobutadiene
12/07/21 12:300.0100.0007<0.0007mg/Kgn-Hexane
12/07/21 12:300.0200.0006<0.0006mg/Kg2-Hexanone
12/07/21 12:300.0050.0005<0.0005mg/KgIsopropylbenzene
12/07/21 12:300.0050.001<0.001mg/Kg4-Isopropyl toluene
12/07/21 12:300.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
12/07/21 12:300.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
12/07/21 12:300.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
12/07/21 12:300.0100.001<0.001mg/KgMethylene Chloride
12/07/21 12:300.0100.0010<0.0010mg/KgNaphthalene
12/07/21 12:300.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 6 of 20Date:12/22/2021 04:36 PM
Page 55 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
Associated Lab Samples: 89937, 89938
LRB-V12542 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/07/21 12:300.0050.001<0.001mg/KgStyrene
12/07/21 12:300.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
12/07/21 12:300.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
12/07/21 12:300.0050.0009<0.0009mg/KgTetrachloroethene
12/07/21 12:300.0050.0007<0.0007mg/KgToluene
12/07/21 12:300.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
12/07/21 12:300.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
12/07/21 12:300.0050.001<0.001mg/Kg1,1,1-Trichloroethane
12/07/21 12:300.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
12/07/21 12:300.0050.0009<0.0009mg/KgTrichloroethene
12/07/21 12:300.0100.002<0.002mg/KgTrichlorofluoromethane
12/07/21 12:300.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
12/07/21 12:300.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
12/07/21 12:300.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
12/07/21 12:300.0100.0005<0.0005mg/KgVinyl Acetate
12/07/21 12:300.0100.0005<0.0005mg/KgVinyl Chloride
12/07/21 12:300.0050.0005<0.0005mg/Kgo-Xylene
12/07/21 12:300.0100.001<0.001mg/Kgm,p-Xylene
12/07/21 12:304-Bromofluorobenzene (S)97.4 70-130
12/07/21 12:30Dibromofluoromethane (S)96.8 84-123
12/07/21 12:30Toluene-d8 (S)92.4 76-129
LCS-V12542 LCSD-V12542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.100 1001090.1090.100mg/KgAcetone 29-198 8.6 20
Page 7 of 20Date:12/22/2021 04:36 PM
Page 56 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
LCS-V12542 LCSD-V12542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101240.1240.100mg/KgAcrolein 70-130 11.9 20
0.105 1051170.1170.100mg/KgAcrylonitrile 65-134 10.8 20
0.047 95.81050.0520.050mg/KgBenzene 74-127 9.1 20
0.042 85.290.40.0450.050mg/KgBromobenzene 73-125 5.9 20
0.051 1031080.0540.050mg/KgBromochloromethane 72-134 4.9 20
0.048 97.21030.0510.050mg/KgBromodichloromethane 75-122 5.9 20
0.047 95.698.60.0490.050mg/KgBromoform 66-135 3.0 20
0.042 85.299.00.0490.050mg/KgBromomethane 20-180 14.9 20
0.044 88.096.60.0480.050mg/Kgn-Butylbenzene 65-135 9.3 20
0.043 86.293.40.0460.050mg/Kgsec-Butyl benzene 66-131 8.0 20
0.042 84.892.40.0460.050mg/Kgtert-Butyl benzene 67-132 8.5 20
0.045 91.61030.0510.050mg/KgCarbon Disulfide 61-129 11.3 20
0.047 94.41060.0530.050mg/KgCarbon Tetrachloride 64-143 11.5 20
0.045 90.895.20.0470.050mg/KgChlorobenzene 74-118 4.7 20
0.046 92.296.20.0480.050mg/KgChlorodibromomethane 73-122 4.2 20
0.050 1001070.0530.050mg/KgChloroethane 33-149 6.5 20
0.046 93.61020.0500.050mg/KgChloroform 73-127 8.1 20
0.050 1001110.0550.050mg/KgChloromethane 45-143 10.7 20
0.043 86.490.80.0450.050mg/Kg2-Chlorotoluene 67-124 4.9 20
0.042 85.291.20.0450.050mg/Kg4-Chlorotoluene 71-126 6.8 20
0.049 99.61060.0530.050mg/KgDi-Isopropyl Ether (DIPE)59-159 6.4 20
0.046 92.099.60.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 7.9 20
0.046 93.898.80.0490.050mg/Kg1,2-Dibromoethane 70-132 5.1 20
0.049 99.61080.0540.050mg/KgDibromomethane 74-133 8.0 20
0.042 85.891.80.0450.050mg/Kg1,2-Dichlorobenzene 72-123 6.7 20
0.043 86.691.20.0450.050mg/Kg1,3-Dichlorobenzene 71-120 5.1 20
Page 8 of 20Date:12/22/2021 04:36 PM
Page 57 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
LCS-V12542 LCSD-V12542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.291.40.0450.050mg/Kg1,4-Dichlorobenzene 71-123 7.0 20
0.048 97.81120.0560.050mg/KgDichlorodifluoromethane 26-146 13.5 20
0.048 96.81040.0510.050mg/Kg1,1-Dichloroethane 74-127 6.9 20
0.049 98.41080.0530.050mg/Kg1,2-Dichloroethane 68-128 9.1 20
0.046 93.81050.0520.050mg/Kg1,1-Dichloroethene 67-149 10.8 20
0.048 96.41050.0520.050mg/Kgcis-1,2-Dichloroethene 76-134 8.1 20
0.048 96.01040.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 8.3 20
0.049 98.81050.0520.050mg/Kg1,2-Dichloropropane 73-130 6.0 20
0.046 93.297.00.0480.050mg/Kg1,3-Dichloropropane 75-124 3.9 20
0.047 95.61070.0530.050mg/Kg2,2-Dichloropropane 50-142 11.6 20
0.047 95.21070.0530.050mg/Kg1,1-Dichloropropene 71-130 11.2 20
0.050 1001060.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 5.6 20
0.050 1011090.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 7.4 20
1.27 1021131.411.25mg/KgEthanol 70-130 10.4 20
0.044 89.294.00.0470.050mg/KgEthylbenzene 74-128 5.2 20
0.103 1031100.1100.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 6.5 20
0.043 87.692.80.0460.050mg/KgHexachlorobutadiene 64-125 5.7 20
0.047 95.81080.0540.050mg/Kgn-Hexane 70-130 12.1 20
0.054 1081180.0580.050mg/Kg2-Hexanone 61-157 8.4 20
0.042 85.092.40.0460.050mg/KgIsopropylbenzene 68-126 8.3 20
0.044 88.095.00.0470.050mg/Kg4-Isopropyl toluene 68-129 7.6 20
0.051 1031180.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 13.3 20
0.049 99.81080.0530.050mg/KgMethyl tert-butyl ether (MTBE)70-130 7.5 20
0.052 1051170.0580.050mg/Kg4-Methyl-2-Pentanone 57-162 10.7 20
0.042 85.292.20.0460.050mg/KgMethylene Chloride 74-129 7.8 20
0.044 89.297.20.0480.050mg/KgNaphthalene 57-157 8.5 20
Page 9 of 20Date:12/22/2021 04:36 PM
Page 58 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12542
LCS-V12542 LCSD-V12542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.493.00.0460.050mg/Kgn-Propylbenzene 67-130 8.5 20
0.046 92.296.60.0480.050mg/KgStyrene 77-121 4.6 20
0.045 90.493.80.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.6 20
0.043 87.094.60.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 8.3 20
0.047 94.21060.0520.050mg/KgTetrachloroethene 68-130 11.4 20
0.047 94.61030.0510.050mg/KgToluene 71-129 8.6 20
0.043 86.491.60.0450.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.8 20
0.044 88.693.80.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.7 20
0.046 93.81040.0510.050mg/Kg1,1,1-Trichloroethane 67-131 9.9 20
0.046 93.297.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 4.6 20
0.048 96.81060.0520.050mg/KgTrichloroethene 75-133 8.6 20
0.050 1001150.0570.050mg/KgTrichlorofluoromethane 44-146 14.2 20
0.043 87.094.60.0470.050mg/Kg1,2,3-Trichloropropane 60-137 8.3 20
0.043 87.092.00.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 5.5 20
0.043 86.693.20.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.3 20
0.052 1041180.0590.050mg/KgVinyl Acetate 60-140 12.6 20
0.048 97.01090.0540.050mg/KgVinyl Chloride 48-147 11.6 20
0.045 91.095.80.0470.050mg/Kgo-Xylene 74-126 5.1 20
0.091 91.697.20.0970.100mg/Kgm,p-Xylene 75-124 5.9 20
99.898.04-Bromofluorobenzene (S)70-130
95.498.2Dibromofluoromethane (S)84-123
94.691.0Toluene-d8 (S)76-129
Page 10 of 20Date:12/22/2021 04:36 PM
Page 59 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
Associated Lab Samples: 89937, 89938
LRB-V12619 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/10/21 20:380.6600.116<0.116mg/KgAcenaphthene
12/10/21 20:380.6600.105<0.105mg/KgAcenaphthylene
12/10/21 20:380.6600.152<0.152mg/KgAniline
12/10/21 20:380.6600.143<0.143mg/KgAnthracene
12/10/21 20:380.6600.139<0.139mg/KgBenzo(a)anthracene
12/10/21 20:380.6600.147<0.147mg/KgBenzo(a)pyrene
12/10/21 20:380.6600.146<0.146mg/KgBenzo(b)fluoranthene
12/10/21 20:380.6600.136<0.136mg/KgBenzo(g,h,i)perylene
12/10/21 20:380.6600.137<0.137mg/KgBenzo(k)fluoranthene
12/10/21 20:382.000.580<0.580mg/KgBenzoic Acid
12/10/21 20:380.6600.105<0.105mg/KgBenzyl alcohol
12/10/21 20:380.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
12/10/21 20:380.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
12/10/21 20:380.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
12/10/21 20:380.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
12/10/21 20:380.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
12/10/21 20:380.3300.113<0.113mg/KgButyl benzyl phthalate
12/10/21 20:380.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
12/10/21 20:380.3300.112<0.112mg/Kg4-Chloroaniline
12/10/21 20:380.6600.116<0.116mg/Kg2-Chloronaphthalene
12/10/21 20:380.6600.098<0.098mg/Kg2-Chlorophenol
12/10/21 20:381.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
12/10/21 20:380.6600.142<0.142mg/KgChrysene
12/10/21 20:380.6600.230<0.230mg/KgDibenz(a,h)anthracene
12/10/21 20:380.6600.119<0.119mg/KgDibenzofuran
12/10/21 20:380.6600.094<0.094mg/Kg1,2-Dichlorobenzene
12/10/21 20:380.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 11 of 20Date:12/22/2021 04:36 PM
Page 60 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
Associated Lab Samples: 89937, 89938
LRB-V12619 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/10/21 20:380.3300.097<0.097mg/Kg1,4-Dichlorobenzene
12/10/21 20:380.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
12/10/21 20:380.6600.095<0.095mg/Kg2,4-Dichlorophenol
12/10/21 20:380.6600.180<0.180mg/KgDiethyl phthalate
12/10/21 20:380.6600.174<0.174mg/KgDimethyl phthalate
12/10/21 20:380.3300.108<0.108mg/Kg2,4-Dimethylphenol
12/10/21 20:380.6600.107<0.107mg/KgDi-n-butyl phthalate
12/10/21 20:381.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
12/10/21 20:381.500.520<0.520mg/Kg2,4-Dinitrophenol
12/10/21 20:380.6600.096<0.096mg/Kg2,4-Dinitrotoluene
12/10/21 20:380.6600.108<0.108mg/Kg2,6-Dinitrotoluene
12/10/21 20:380.3300.143<0.143mg/KgDi-n-Octyl Phthalate
12/10/21 20:380.6600.123<0.123mg/KgFluoranthene
12/10/21 20:380.6600.128<0.128mg/KgFluorene
12/10/21 20:380.6600.106<0.106mg/KgHexachlorobenzene
12/10/21 20:380.6600.097<0.097mg/KgHexachlorobutadiene
12/10/21 20:380.6600.157<0.157mg/KgHexachlorocyclopentadiene
12/10/21 20:380.6600.079<0.079mg/KgHexachloroethane
12/10/21 20:380.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
12/10/21 20:380.6600.191<0.191mg/KgIsophorone
12/10/21 20:380.6600.106<0.106mg/Kg1-Methylnaphthalene
12/10/21 20:380.6600.100<0.100mg/Kg2-Methylnaphthalene
12/10/21 20:380.6600.097<0.097mg/Kg2-Methylphenol
12/10/21 20:380.6600.084<0.084mg/Kg3&4 Methylphenol
12/10/21 20:380.6600.144<0.144mg/KgNaphthalene
12/10/21 20:380.6600.096<0.096mg/Kg2-Nitroaniline
12/10/21 20:380.6600.120<0.120mg/Kg3-Nitroaniline
Page 12 of 20Date:12/22/2021 04:36 PM
Page 61 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
Associated Lab Samples: 89937, 89938
LRB-V12619 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/10/21 20:380.3300.093<0.093mg/Kg4-Nitroaniline
12/10/21 20:380.3300.116<0.116mg/KgNitrobenzene
12/10/21 20:380.6600.088<0.088mg/Kg2-Nitrophenol
12/10/21 20:380.6600.117<0.117mg/Kg4-Nitrophenol
12/10/21 20:380.6600.263<0.263mg/KgN-Nitrosodimethylamine
12/10/21 20:380.6600.181<0.181mg/KgN-Nitrosodiphenylamine
12/10/21 20:380.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
12/10/21 20:381.000.347<0.347mg/KgPentachlorophenol
12/10/21 20:380.6600.208<0.208mg/KgPhenanthrene
12/10/21 20:380.6600.112<0.112mg/KgPhenol
12/10/21 20:380.6600.134<0.134mg/KgPyrene
12/10/21 20:380.3300.079<0.079mg/KgPyridine
12/10/21 20:380.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
12/10/21 20:380.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
12/10/21 20:380.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
12/10/21 20:382-Fluorobiphenyl (S)83.8 44-115
12/10/21 20:382-Fluorophenol (S)81.6 35-115
12/10/21 20:38Nitrobenzene-d5 (S)76.0 37-122
12/10/21 20:384-Terphenyl-d14 (S)89.8 54-127
12/10/21 20:382,4,6-Tribromophenol (S)79.5 39-132
12/10/21 20:38Phenol-d5 (S)81.9 34-121
LCS-V12619Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.21.441.67mg/KgAcenaphthene 40-123
89.21.491.67mg/KgAcenaphthylene 32-132
Page 13 of 20Date:12/22/2021 04:36 PM
Page 62 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
LCS-V12619Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.21.291.67mg/KgAniline 12-197
89.81.501.67mg/KgAnthracene 47-123
86.81.451.67mg/KgBenzo(a)anthracene 49-126
1071.781.67mg/KgBenzo(a)pyrene 45-129
94.01.571.67mg/KgBenzo(b)fluoranthene 45-132
88.61.481.67mg/KgBenzo(g,h,i)perylene 43-134
91.61.531.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.011.67mg/KgBenzoic Acid 10-83
85.61.431.67mg/KgBenzyl alcohol 29-122
83.81.401.67mg/KgBis(2-Chloroethoxy)methane 36-121
89.21.491.67mg/KgBis(2-Chloroethyl)ether 31-120
86.21.441.67mg/KgBis(2-Chloroisopropyl)ether 33-131
94.61.581.67mg/KgBis(2-ethylhexyl)phthalate 51-133
89.21.491.67mg/Kg4-Bromophenyl phenyl ether 46-124
88.01.471.67mg/KgButyl benzyl phthalate 48-132
83.21.391.67mg/Kg4-Chloro-3-methylphenol 45-122
67.01.121.67mg/Kg4-Chloroaniline 17-106
85.61.431.67mg/Kg2-Chloronaphthalene 41-114
83.81.401.67mg/Kg2-Chlorophenol 34-121
86.81.451.67mg/Kg4-Chlorophenyl phenyl ether 45-121
89.81.501.67mg/KgChrysene 50-124
82.01.371.67mg/KgDibenz(a,h)anthracene 45-134
86.81.451.67mg/KgDibenzofuran 44-120
76.61.281.67mg/Kg1,2-Dichlorobenzene 33-117
74.81.251.67mg/Kg1,3-Dichlorobenzene 30-115
74.81.251.67mg/Kg1,4-Dichlorobenzene 31-115
78.41.311.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 14 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 63 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
LCS-V12619Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
81.41.361.67mg/Kg2,4-Dichlorophenol 40-122
88.01.471.67mg/KgDiethyl phthalate 50-124
88.01.471.67mg/KgDimethyl phthalate 48-124
87.41.461.67mg/Kg2,4-Dimethylphenol 30-127
97.61.631.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.351.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.311.67mg/Kg2,4-Dinitrophenol 27-129
92.81.551.67mg/Kg2,4-Dinitrotoluene 48-126
93.41.561.67mg/Kg2,6-Dinitrotoluene 46-124
87.41.461.67mg/KgDi-n-Octyl Phthalate 45-140
90.41.511.67mg/KgFluoranthene 50-127
89.21.491.67mg/KgFluorene 43-125
92.21.541.67mg/KgHexachlorobenzene 45-122
71.81.201.67mg/KgHexachlorobutadiene 32-123
62.21.041.67mg/KgHexachlorocyclopentadiene 32-117
76.61.281.67mg/KgHexachloroethane 28-117
86.81.451.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
70.61.181.67mg/KgIsophorone 30-122
70.01.171.67mg/Kg1-Methylnaphthalene 40-119
72.41.211.67mg/Kg2-Methylnaphthalene 38-122
89.81.501.67mg/Kg2-Methylphenol 32-122
80.21.341.67mg/Kg3&4 Methylphenol 34-119
70.61.181.67mg/KgNaphthalene 35-123
91.01.521.67mg/Kg2-Nitroaniline 44-127
84.41.411.67mg/Kg3-Nitroaniline 33-119
82.61.381.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 15 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 64 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
LCS-V12619Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
73.61.231.67mg/Kg2-Nitrophenol 36-123
97.61.631.67mg/Kg4-Nitrophenol 30-132
67.61.131.67mg/KgN-Nitrosodimethylamine 10-146
1041.741.67mg/KgN-Nitrosodiphenylamine 38-127
83.21.391.67mg/KgN-Nitroso-di-n-propylamine 36-120
1051.761.67mg/KgPentachlorophenol 25-133
88.61.481.67mg/KgPhenanthrene 50-121
83.21.391.67mg/KgPhenol 34-121
92.21.541.67mg/KgPyrene 47-127
52.50.8781.67mg/KgPyridine 10-80
70.61.181.67mg/Kg1,2,4-Trichlorobenzene 34-118
86.81.451.67mg/Kg2,4,5-Trichlorophenol 41-124
89.21.491.67mg/Kg2,4,6-Trichlorophenol 39-126
82.62-Fluorobiphenyl (S)44-115
82.52-Fluorophenol (S)35-115
68.8Nitrobenzene-d5 (S)37-122
89.24-Terphenyl-d14 (S)54-127
86.72,4,6-Tribromophenol (S)39-132
79.5Phenol-d5 (S)34-121
V 89903-MS-V12619 V 89903-MSD-V12619Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.491.671.67<0.116mg/KgAcenaphthene 89.2 40-123 4.1 20
1.43 85.61.501.671.67<0.105mg/KgAcenaphthylene 89.8 32-132 4.7 20
1.25 74.80.9211.671.67<0.152mg/KgAniline 55.1 12-197 30.3*20
Page 16 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 65 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
V 89903-MS-V12619 V 89903-MSD-V12619Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.45 86.81.521.671.67<0.143mg/KgAnthracene 91.0 47-123 4.7 20
1.38 82.61.481.671.67<0.139mg/KgBenzo(a)anthracene 88.6 49-126 6.9 20
1.75 1051.831.671.67<0.147mg/KgBenzo(a)pyrene 110 45-129 4.4 20
1.61 96.41.721.671.67<0.146mg/KgBenzo(b)fluoranthene 103 45-132 6.6 20
1.44 86.21.561.671.67<0.136mg/KgBenzo(g,h,i)perylene 93.4 43-134 8.0 20
1.54 92.21.681.671.67<0.137mg/KgBenzo(k)fluoranthene 101 47-132 8.6 20
<0.580 0.0*<0.5801.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.38 82.61.501.671.67<0.105mg/KgBenzyl alcohol 89.8 29-122 8.3 20
1.99 1192.021.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 121 36-121 1.4 20
1.07 64.01.351.671.67<0.107mg/KgBis(2-Chloroethyl)ether 80.8 31-120 23.1*20
1.26 75.41.381.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 82.6 33-131 9.0 20
1.64 98.21.681.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 101 51-133 2.4 20
1.37 82.01.541.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 92.2 46-124 11.6 20
1.64 98.21.601.671.67<0.113mg/KgButyl benzyl phthalate 95.8 48-132 2.4 20
1.55 92.81.631.671.67<0.092mg/Kg4-Chloro-3-methylphenol 97.6 45-122 5.0 20
1.11 66.41.201.671.67<0.112mg/Kg4-Chloroaniline 71.8 17-106 7.7 20
1.48 88.61.561.671.67<0.116mg/Kg2-Chloronaphthalene 93.4 41-114 5.2 20
1.03 61.61.121.671.67<0.098mg/Kg2-Chlorophenol 67.0 34-121 8.3 20
1.45 86.81.461.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 87.4 45-121 0.6 20
1.43 85.61.481.671.67<0.142mg/KgChrysene 88.6 50-124 3.4 20
1.31 78.41.441.671.67<0.230mg/KgDibenz(a,h)anthracene 86.2 45-134 9.4 20
1.42 85.01.471.671.67<0.119mg/KgDibenzofuran 88.0 44-120 3.4 20
1.15 68.81.241.671.67<0.094mg/Kg1,2-Dichlorobenzene 74.2 33-117 7.5 20
1.16 69.41.231.671.67<0.097mg/Kg1,3-Dichlorobenzene 73.6 30-115 5.8 20
1.16 69.41.231.671.67<0.097mg/Kg1,4-Dichlorobenzene 73.6 31-115 5.8 20
0.779 46.60.9691.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 58.0 22-121 21.7*20
Page 17 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 66 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
V 89903-MS-V12619 V 89903-MSD-V12619Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.34 80.21.531.671.67<0.095mg/Kg2,4-Dichlorophenol 91.6 40-122 13.2 20
1.49 89.21.461.671.67<0.180mg/KgDiethyl phthalate 87.4 50-124 2.0 20
1.39 83.21.481.671.67<0.174mg/KgDimethyl phthalate 88.6 48-124 6.2 30
1.61 96.41.731.671.67<0.108mg/Kg2,4-Dimethylphenol 104 30-127 7.1 20
1.60 95.81.691.671.67<0.107mg/KgDi-n-butyl phthalate 101 51-128 5.4 20
1.10 0.0*1.141.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.17 0.0*1.061.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.46 87.41.531.671.67<0.096mg/Kg2,4-Dinitrotoluene 91.6 48-126 4.6 20
1.43 85.61.531.671.67<0.108mg/Kg2,6-Dinitrotoluene 91.6 46-124 6.7 20
1.72 1031.681.671.67<0.143mg/KgDi-n-Octyl Phthalate 101 45-140 2.3 20
1.42 85.01.511.671.67<0.123mg/KgFluoranthene 90.4 50-127 6.1 20
1.52 91.01.511.671.67<0.128mg/KgFluorene 90.4 43-125 0.6 20
1.34 80.21.531.671.67<0.106mg/KgHexachlorobenzene 91.6 45-122 13.2 20
1.36 81.41.451.671.67<0.097mg/KgHexachlorobutadiene 86.8 32-123 6.4 20
1.02 61.01.121.671.67<0.157mg/KgHexachlorocyclopentadiene 67.0 32-117 9.3 20
20.7 1240*19.51.671.67<0.079mg/KgHexachloroethane 1170*28-117 5.9 20
1.39 83.20.3491.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 0.0*45-133 71.2*20
1.30 77.81.331.671.67<0.191mg/KgIsophorone 79.6 30-122 2.2 20
10.2 39.5*9.581.671.679.54mg/Kg1-Methylnaphthalene 2.3*40-119 6.2 20
20.0 -120*18.71.671.6722.3mg/Kg2-Methylnaphthalene -200*38-122 6.7 20
1.74 1041.831.671.67<0.097mg/Kg2-Methylphenol 110 32-122 5.0 20
1.31 78.41.371.671.67<0.084mg/Kg3&4 Methylphenol 82.0 34-119 4.4 20
16.3 -240*15.91.671.6720.6mg/KgNaphthalene -280*35-123 2.4 20
1.51 90.41.561.671.67<0.096mg/Kg2-Nitroaniline 93.4 44-127 3.2 20
1.19 71.21.301.671.67<0.120mg/Kg3-Nitroaniline 77.8 33-119 8.8 20
1.42 85.01.421.671.67<0.093mg/Kg4-Nitroaniline 85.0 63-147 0.0 20
Page 18 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 67 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V12781QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12619
V 89903-MS-V12619 V 89903-MSD-V12619Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.79 1071.791.671.67<0.116mg/KgNitrobenzene 107 34-122 0.0 20
1.42 85.01.511.671.67<0.088mg/Kg2-Nitrophenol 90.4 32-123 6.1 20
1.82 1091.831.671.67<0.117mg/Kg4-Nitrophenol 110 30-132 0.5 20
1.02 61.01.051.671.67<0.263mg/KgN-Nitrosodimethylamine 62.8 10-146 2.8 30
1.69 1011.841.671.67<0.181mg/KgN-Nitrosodiphenylamine 110 38-127 8.4 20
1.87 1121.921.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 115 36-120 2.6 20
1.57 94.01.721.671.67<0.347mg/KgPentachlorophenol 103 25-133 9.1 20
1.51 90.41.591.671.67<0.208mg/KgPhenanthrene 95.2 50-121 5.1 20
1.31 78.41.411.671.67<0.112mg/KgPhenol 84.4 34-121 7.3 20
1.51 90.41.581.671.67<0.134mg/KgPyrene 94.6 47-127 4.5 20
1.16 69.40.9401.671.67<0.079mg/KgPyridine 56.2 10-80 20.9*20
1.30 77.81.381.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 82.6 34-118 5.9 20
1.35 80.81.461.671.67<0.096mg/Kg2,4,5-Trichlorophenol 87.4 41-124 7.8 20
1.37 82.01.501.671.67<0.096mg/Kg2,4,6-Trichlorophenol 89.8 39-126 9.0 20
80.82-Fluorobiphenyl (S)82.0 44-115
61.52-Fluorophenol (S)62.7 35-115
93.4Nitrobenzene-d5 (S)89.8 37-122
86.24-Terphenyl-d14 (S)86.2 54-127
81.62,4,6-Tribromophenol (S)84.3 39-132
77.4Phenol-d5 (S)77.4 34-121
Page 19 of 20* QC Fail Date:12/22/2021 04:36 PM
Page 68 of 71
Quality Control Data
21-340-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
Dry Weight Determination
SW-DRYWT
V12464QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89891-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/06/21 12:350.013.813.8%Moisture
V 89893-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/06/21 12:357.84.504.16%Moisture
Page 20 of 20Date:12/22/2021 04:36 PM
Page 69 of 71
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-340-0007
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 6.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:12/06/2021 11:02:25
Special precautions or instructions included?
Comments:
Page 70 of 71
Page 71 of 71