23057_CharlotteVan&Storage_Soil Export Options SP3 - SP5 Package_20211011

October 11, 2021
Sent Via E-mail
Mr. Jeffrey W. Harris
Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202 [e-mail]
Subject: Brownfields Soil Management Options for Stockpiled Soil Charlotte Van & Storage Co. Brownfield Property Charlotte, Mecklenburg County Brownfields Project No. 23057-19-060
Dear Mr. Harris:
The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received a request to export soil from the Charlotte Van & Storage Co. Brownfields Property. This request
was submitted on your behalf by Ms. Haley Martin, PG of Hart & Hickman, PC via email on
October 11, 2021, and requests approval to export approximately 2,000 cubic yards of stockpiled soil generated during utility installations to a beneficial fill reuse site known as Fleet Maintenance facility in Mt. Holly, North Carolina. On September 7, 2021, DEQ Brownfields provided a letter approving soil export options for areas identified by samples EX-1 through EX-6 and SP-1, and
on September 15, 2021, for stockpiled soil identified by sample SP-2.
For this request, DEQ Brownfields reviewed the October 11, 2021, Data Summary Package which includes analytical results for soil samples SP-3, SP-4, and SP-5, as well as soil analytical data from the proposed Fleet Maintenance receiving facility.
Based on our review of the data, the DEQ Brownfield determines that soils may be exported as outlined in the table below. Please note that the “Beneficial Fill” option listed in the table below is specifically approved for the Fleet Maintenance facility in Mt. Holly, NC. Other Beneficial Fill and Land Clearing & Inert Debris Landfill (LCID) options may be available; however, DEQ
requires that the receiving facility be identified and approved prior to export. The receiving
facility should have metals concentrations which are consistent with those from the Brownfields Property. Similarly, many site soils, including those with impacts, may be suitable for use at another Brownfields Property that has similar impacts.
Mr. Jeffery Harris October 11, 2021 Page 2

Upon determination of the export facility, whether another Brownfields Property, LCID, or
another beneficial fill reuse, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
LOCATION ID DEPTH (Ft)1 MANAGEMENT OPTIONS2
SP-3 stockpile BFILL, LCID, CDLF, MSWLF
SP-4 stockpile BFILL, LCID, CDLF, MSWLF
SP-5 stockpile BFILL, LCID, CDLF, MSWLF

Notes: 1) Depth listed is total depth of available analytical data. Additional sampling would potentially be required beyond these depths prior to export. 2) BFILL= Beneficial Fill; LCID = Land Clearing & Inert Debris Landfill; CDLF = Construction
& Demolition landfill; MSWLF = Municipal Solid Waste landfill (MSWLF) facility. Per the Charlotte Van & Storage Co.’s approved Environmental Management Plan (EMP), the soils are to be field screened during excavation prior to export from the property. If unanticipated
impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, and also in accordance with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the
Redevelopment Summary Report. Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free
to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail]. Sincerely,
Peter L. Doorn, Project Manager Brownfields Program Ec: Haley Martin, Hart & Hickman, PC
Ralph McGee, Hart & Hickman, PC
Tracy Wahl, DEQ Brownfields
1
Doorn, Peter L
From:Haley Martin <[e-mail]>
Sent:Monday, October 11, 2021 9:22 AM
To:Doorn, Peter L
Cc:Ralph McGee
Subject:RE: [External] 23057-19-060 - Charlotte Van & Storage - Soil Management Options
Attachments:Charlotte Van & Storage - Data Summary Package.pdf; 23057
_CharlotteVan&Storage_Soil Export Options_Approval Letters.pdf
Follow Up Flag:Follow up
Flag Status:Completed
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good Morning Pete,

Please find the attached data summary package for the Charlotte Van and Storage Brownfields Property. On September
29, 2021, H&H collected two 5-point composite sample (SP-3 and SP-4) from an approximate 1,500 cubic yard soil
stockpile at the Charlotte Van and Storage property that was generated during installation of utilities. H&H also
collected one 5-point composite sample from an approximate 500 cubic yard stockpile (SP-5) that was generated during
deconstruction of an erosion control sediment pond. Soil sample aliquots collected from the stockpiles were
homogenized to form three composite soil sample (SP-3 through SP-5) representative of soil conditions.

The composite soil samples selected for laboratory analyses was collected directly into dedicated laboratory supplied
sample containers, labeled with the date, time, and sample identification, and placed in a laboratory supplied sample
cooler with ice. The samples were submitted to Waypoint Analytical (Waypoint) under standard chain of custody
protocols for analysis of semi volatile organic compounds (SVOCs) by EPA Method 8270 and Resource Conservation and
Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199. In addition to the composite
soil samples described above, one representative grab soil sample was collected from each stockpile. The grab soil
samples were collected from an undisturbed portion of soil directly into laboratory supplied glassware and submitted to
Waypoint under standard chain of custody protocols for analysis of VOCs by EPA Method 8260.

As noted in the attached data summary package, the analytical results for SP-3 through SP-5 did not identify organic
compounds at concentrations above the Preliminary Soil Remediation Goals (PSRGs) and metals appear to be consistent
with background concentrations for the Site and the Fleet Maintenance facility. The PD would like to transport the
approximate the approximate 1,500 cubic yard and 500 cubic yard stockpiles to the Fleet Maintenance facility that was
previously approved on September 7, 2021 and September 15, 2021. The previous approval letters are attached for
ease of reference.

As you may know, grading construction work is ongoing. We appreciate your reviewing this data to assist in keeping the
construction schedule on track. In the meantime, please let us know if you have any questions or concerns.

Thanks,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
2

www.harthickman.com

From: Doorn, Peter L <[e-mail]>
Sent: Tuesday, September 28, 2021 3:04 PM
To: Haley Martin <[e-mail]>
Cc: Ralph McGee <[e-mail]>
Subject: RE: [External] 23057-19-060 - Charlotte Van & Storage - Soil Management Options

Haley – thanks for the update on the soil stockpile. Your approach for sampling and analysis sounds appropriate.

I’ll be out next week, so if results come in next week, I will get you a response as soon as I can when I return on Oct. 11.

Pete

Peter L. Doorn
Brownfields Program/DWM/NCDEQ
Mobile: [phone]

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties.

From: Haley Martin <[e-mail]>
Sent: Tuesday, September 28, 2021 1:56 PM
To: Doorn, Peter L <[e-mail]>
Cc: Ralph McGee <[e-mail]>
Subject: [External] 23057-19-060 - Charlotte Van & Storage - Soil Management Options

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good Afternoon Pete,

The PD at the Charlotte Van and Storage Brownfields property (BPN 23057-19-060) has an approximate 1,500 cubic
yard soil stockpile generated from installation of utilities along Verbena Street that cannot be re-used on-Site. H&H will
collect two composite soil samples to assist in management of the stockpile. In accordance with the DEQ-approved EMP,
the soil stockpile will be evaluated in approximately 750 cubic yard sections and two sets of five (5) aliquot soil samples
will be collected to represent each section of the stockpile. The soil samples from each section will be combined and
homogenized to form two composite soil samples (SP-3 and SP-4) representative of soil that will be transported off-Site.

The composite soil samples selected for laboratory analysis will be placed directly into laboratory supplied glassware,
labeled with the sample identification, the date, and requested analysis and placed in a laboratory supplied cooler with
ice. The samples will be delivered to a NC certified laboratory under standard chain of custody protocols for analysis of
semi-volatile organic compounds (SVOCs) by EPA Method 8270 and RCRA metals plus hexavalent chromium by EPA
Methods 6020/7471/7199. In addition, one grab soil sample will be collected from an undisturbed portion of an aliquot
soil sample from each stockpile section and submitted to the laboratory for analysis of VOCs by EPA Method 8260.

If results of the above sampling indicate that there are no impacts above acceptable levels and metals appear consistent
with background concentrations, the PD for the Charlotte Van and Storage Brownfields property would like to request
3
approval to export the stockpile to Fleet Maintenance facility that was previously approved on September 7, 2021 and
September 15, 2021. We will send laboratory analytical results and risk calculations as soon as they are available. In the
meantime, please let us know if you have questions or require additional information.

Thank you,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

Table 1
Summary of Soil Analytical Data
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab Composite Grab
Depth (ft bgs)
Date Range Range Mean
Units
VOCs (8260D)
Acetone NA 0.006 J NA 0.009 J NA 0.005 J NA NA NA 25 12,000 140,000 -- -- --
SVOCs (8270E)ALL BDL NA ALL BDL NA ALL BDL NA NA NA NA -- -- -- -- -- --
Metals (6020/7471/7199)
Arsenic 0.676 J NA 2.44 NA 1.77 B NA 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 47.1 NA 132 NA 117 NA 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium <0.0699 NA 0.0705 J NA <0.0799 NA <0.0655 <0.0649 0.207 J 3.0 14 200 ND - 0.434 1.0 - 10* 4.3
Chromium (total) 21.9 NA 42.2 NA 78.3 NA 80.8 30.9 25.7 ---- --47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium <0.26 NA <0.23 NA 0.57 J NA 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 21.9 NA 42.2 NA 77.7 NA 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 10.7 NA 20.4 NA 13.4 NA 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0324 J NA 0.0195 J NA <0.0174 NA 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium <1.15 NA 1.23 J NA 2.30 J NA 10.8 J <1.06 <1.47 J 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.0521 NA <0.0475 NA <0.0595 NA <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit; BDL = below laboratory method detection limits
B = Compound was detected in the laboratory blank.
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
mg/kg mg/kg
1-3
9/29/2021
Background
Metals (2)Grab
--
Fleet Maintenance Facility
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals in Soil
8/27/2021
Sample Location Stockpile
Screening Criteria SP-3 SP-4 SP-5
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/Site Work/Charlotte Van & Storage Co. (LEN‐008) Data Tables aem.xlsx
10/11/2021
Table 1 (Page 1 of 1)
Hart & Hickman, PC

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/8/2021
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-272-0017 Client Project Description: LEN-008
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/29/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 68
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-272-0017
Page 2 of 68
Report Number:
Sample Summary Table
Client Project Description:
21-272-0017
LEN-008
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/29/2021 09:45Solids 96523 SP-3 09/29/2021 14:48 7199
09/29/2021 09:45Solids 96523 SP-3 09/29/2021 14:48
09/29/2021 10:20Solids 96524 SP-4 09/29/2021 14:48 7199
09/29/2021 10:20Solids 96524 SP-4 09/29/2021 14:48
09/29/2021 11:00Solids 96525 SP-5 09/29/2021 14:48 7199
09/29/2021 11:00Solids 96525 SP-5 09/29/2021 14:48
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-272-0017
Report Limit
Project:LEN-008
V 96523SP-3
J0.676 10/04/2021 23:526020BArsenicmg/Kg - dry 0.120
47.1 10/04/2021 23:526020BBariummg/Kg - dry 1.78
21.9 10/04/2021 23:526020BChromiummg/Kg - dry 0.368
10.7 10/04/2021 23:526020BLeadmg/Kg - dry 0.178
J0.0324 10/04/2021 18:217471BMercury (Total)mg/Kg - dry 0.0153
J0.006 09/30/2021 15:358260DAcetonemg/Kg - dry 0.003
21.4 10/04/2021 17:21SW-DRYWT Moisture %
V 96524SP-4
2.44 10/04/2021 23:586020BArsenicmg/Kg - dry 0.109
132 10/04/2021 23:586020BBariummg/Kg - dry 1.62
J0.0705 10/04/2021 23:586020BCadmiummg/Kg - dry 0.0638
42.2 10/04/2021 23:586020BChromiummg/Kg - dry 0.336
20.4 10/04/2021 23:586020BLeadmg/Kg - dry 0.162
J1.23 10/04/2021 23:586020BSeleniummg/Kg - dry 1.04
J0.0195 10/04/2021 18:247471BMercury (Total)mg/Kg - dry 0.0139
J0.009 09/30/2021 16:038260DAcetonemg/Kg - dry 0.002
13.8 10/04/2021 17:21SW-DRYWT Moisture %
V 96525SP-5
B1.77 10/07/2021 18:136020BArsenicmg/Kg - dry 0.137
117 10/07/2021 18:136020BBariummg/Kg - dry 2.03
78.3 10/07/2021 18:136020BChromiummg/Kg - dry 0.421
13.4 10/07/2021 18:136020BLeadmg/Kg - dry 0.203
J2.30 10/08/2021 16:086020BSeleniummg/Kg - dry 1.31
J0.005 09/30/2021 16:308260DAcetonemg/Kg - dry 0.003
31.2 10/04/2021 17:21SW-DRYWT Moisture %
Page 4 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.4 %Moisture 1 10/04/21 17:21 SW-DRYWTCEG
0.676 J mg/Kg - dry 0.120 1.27Arsenic 10 10/04/21 23:52 6020BEDV
47.1 mg/Kg - dry 1.78 12.7Barium 10 10/04/21 23:52 6020BEDV
<0.0699 mg/Kg - dry 0.0699 0.636Cadmium 10 10/04/21 23:52 6020BEDV
21.9 mg/Kg - dry 0.368 1.27Chromium 10 10/04/21 23:52 6020BEDV
10.7 mg/Kg - dry 0.178 1.27
Lead 10 10/04/21 23:52 6020BEDV
0.0324 J mg/Kg - dry 0.0153 0.0382Mercury (Total)1 10/04/21 18:21 7471BEDV
<1.15 mg/Kg - dry 1.15 2.54Selenium 10 10/04/21 23:52 6020BEDV
<0.0521 mg/Kg - dry 0.0521 0.636Silver 10 10/04/21 23:52 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 5 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
0.006 J mg/Kg - dry 0.003 0.025Acetone 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/30/21 15:35 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/30/21 15:35 V9550TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/30/21 15:35 V9550TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/30/21 15:35 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/30/21 15:35 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/30/21 15:35 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/30/21 15:35 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 6 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/30/21 15:35 V9550TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/30/21 15:35 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/30/21 15:35 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/30/21 15:35 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/30/21 15:35 V9550TBL
<0.017 mg/Kg - dry 0.017 0.318Ethanol 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/30/21 15:35 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/30/21 15:35 V9550TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/30/21 15:35 V9550TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/30/21 15:35 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/30/21 15:35 V9550TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/30/21 15:35 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/30/21 15:35 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/30/21 15:35 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/30/21 15:35 V9550TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/30/21 15:35 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/30/21 15:35 V9550
Surrogate: 4-Bromofluorobenzene 113 Limits: 70-130%09/30/21 15:351 TBL V9550
Surrogate: Dibromofluoromethane 102 Limits: 84-123%09/30/21 15:351 TBL V9550
Surrogate: Toluene-d8 91.2 Limits: 76-129%09/30/21 15:351 TBL V9550
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.147 mg/Kg - dry 0.147 0.840Acenaphthene 1 10/01/21 16:58 V9595JMV
<0.133 mg/Kg - dry 0.133 0.840Acenaphthylene 1 10/01/21 16:58 V9595JMV
<0.193 mg/Kg - dry 0.193 0.840Aniline 1 10/01/21 16:58 V9595JMV
<0.181 mg/Kg - dry 0.181 0.840Anthracene 1 10/01/21 16:58 V9595JMV
<0.176 mg/Kg - dry 0.176 0.840
Benzo(a)anthracene 1 10/01/21 16:58 V9595JMV
<0.187 mg/Kg - dry 0.187 0.840Benzo(a)pyrene 1 10/01/21 16:58 V9595JMV
<0.185 mg/Kg - dry 0.185 0.840Benzo(b)fluoranthene 1 10/01/21 16:58 V9595JMV
<0.173 mg/Kg - dry 0.173 0.840Benzo(g,h,i)perylene 1 10/01/21 16:58 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.174 mg/Kg - dry 0.174 0.840Benzo(k)fluoranthene 1 10/01/21 16:58 V9595JMV
<0.737 mg/Kg - dry 0.737 2.54Benzoic Acid 1 10/01/21 16:58 V9595JMV
<0.133 mg/Kg - dry 0.133 0.840Benzyl alcohol 1 10/01/21 16:58 V9595JMV
<0.150 mg/Kg - dry 0.150 0.840Bis(2-Chloroethoxy)methane 1 10/01/21 16:58 V9595JMV
<0.136 mg/Kg - dry 0.136 0.840Bis(2-Chloroethyl)ether 1 10/01/21 16:58 V9595JMV
<0.173 mg/Kg - dry 0.173 0.421Bis(2-Chloroisopropyl)ether 1 10/01/21 16:58 V9595JMV
<0.152 mg/Kg - dry 0.152 0.840Bis(2-ethylhexyl)phthalate 1 10/01/21 16:58 V9595JMV
<0.138 mg/Kg - dry 0.138 0.8404-Bromophenyl phenyl ether 1 10/01/21 16:58 V9595JMV
<0.143 mg/Kg - dry 0.143 0.421
Butyl benzyl phthalate 1 10/01/21 16:58 V9595JMV
<0.117 mg/Kg - dry 0.117 0.8404-Chloro-3-methylphenol 1 10/01/21 16:58 V9595JMV
<0.142 mg/Kg - dry 0.142 0.4214-Chloroaniline 1 10/01/21 16:58 V9595JMV
<0.147 mg/Kg - dry 0.147 0.8402-Chloronaphthalene 1 10/01/21 16:58 V9595JMV
<0.125 mg/Kg - dry 0.125 0.8402-Chlorophenol 1 10/01/21 16:58 V9595JMV
<0.160 mg/Kg - dry 0.160 1.274-Chlorophenyl phenyl ether 1 10/01/21 16:58 V9595JMV
<0.180 mg/Kg - dry 0.180 0.840Chrysene 1 10/01/21 16:58 V9595JMV
<0.292 mg/Kg - dry 0.292 0.840
Dibenz(a,h)anthracene 1 10/01/21 16:58 V9595JMV
<0.151 mg/Kg - dry 0.151 0.840Dibenzofuran 1 10/01/21 16:58 V9595JMV
<0.120 mg/Kg - dry 0.120 0.8401,2-Dichlorobenzene 1 10/01/21 16:58 V9595JMV
<0.123 mg/Kg - dry 0.123 0.8401,3-Dichlorobenzene 1 10/01/21 16:58 V9595JMV
<0.124 mg/Kg - dry 0.124 0.4211,4-Dichlorobenzene 1 10/01/21 16:58 V9595JMV
<0.187 mg/Kg - dry 0.187 0.8403,3'-Dichlorobenzidine 1 10/01/21 16:58 V9595JMV
<0.122 mg/Kg - dry 0.122 0.8402,4-Dichlorophenol 1 10/01/21 16:58 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.229 mg/Kg - dry 0.229 0.840Diethyl phthalate 1 10/01/21 16:58 V9595JMV
<0.221 mg/Kg - dry 0.221 0.840Dimethyl phthalate 1 10/01/21 16:58 V9595JMV
<0.137 mg/Kg - dry 0.137 0.4212,4-Dimethylphenol 1 10/01/21 16:58 V9595JMV
<0.136 mg/Kg - dry 0.136 0.840Di-n-butyl phthalate 1 10/01/21 16:58 V9595JMV
<0.305 mg/Kg - dry 0.305 1.914,6-Dinitro-2-methylphenol 1 10/01/21 16:58 V9595JMV
<0.661 mg/Kg - dry 0.661 1.912,4-Dinitrophenol 1 10/01/21 16:58 V9595JMV
<0.123 mg/Kg - dry 0.123 0.8402,4-Dinitrotoluene 1 10/01/21 16:58 V9595JMV
<0.137 mg/Kg - dry 0.137 0.8402,6-Dinitrotoluene 1 10/01/21 16:58 V9595JMV
<0.181 mg/Kg - dry 0.181 0.421
Di-n-Octyl Phthalate 1 10/01/21 16:58 V9595JMV
<0.156 mg/Kg - dry 0.156 0.840Fluoranthene 1 10/01/21 16:58 V9595JMV
<0.162 mg/Kg - dry 0.162 0.840Fluorene 1 10/01/21 16:58 V9595JMV
<0.134 mg/Kg - dry 0.134 0.840Hexachlorobenzene 1 10/01/21 16:58 V9595JMV
<0.124 mg/Kg - dry 0.124 0.840Hexachlorobutadiene 1 10/01/21 16:58 V9595JMV
<0.199 mg/Kg - dry 0.199 0.840Hexachlorocyclopentadiene 1 10/01/21 16:58 V9595JMV
<0.100 mg/Kg - dry 0.100 0.840Hexachloroethane 1 10/01/21 16:58 V9595JMV
<0.227 mg/Kg - dry 0.227 0.840
Indeno(1,2,3-cd)pyrene 1 10/01/21 16:58 V9595JMV
<0.243 mg/Kg - dry 0.243 0.840Isophorone 1 10/01/21 16:58 V9595JMV
<0.134 mg/Kg - dry 0.134 0.8401-Methylnaphthalene 1 10/01/21 16:58 V9595JMV
<0.127 mg/Kg - dry 0.127 0.8402-Methylnaphthalene 1 10/01/21 16:58 V9595JMV
<0.123 mg/Kg - dry 0.123 0.8402-Methylphenol 1 10/01/21 16:58 V9595JMV
<0.108 mg/Kg - dry 0.108 0.8403&4 Methylphenol 1 10/01/21 16:58 V9595JMV
<0.183 mg/Kg - dry 0.183 0.840Naphthalene 1 10/01/21 16:58 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.123 mg/Kg - dry 0.123 0.8402-Nitroaniline 1 10/01/21 16:58 V9595JMV
<0.152 mg/Kg - dry 0.152 0.8403-Nitroaniline 1 10/01/21 16:58 V9595JMV
<0.119 mg/Kg - dry 0.119 0.4214-Nitroaniline 1 10/01/21 16:58 V9595JMV
<0.147 mg/Kg - dry 0.147 0.421Nitrobenzene 1 10/01/21 16:58 V9595JMV
<0.113 mg/Kg - dry 0.113 0.8402-Nitrophenol 1 10/01/21 16:58 V9595JMV
<0.148 mg/Kg - dry 0.148 0.8404-Nitrophenol 1 10/01/21 16:58 V9595JMV
<0.334 mg/Kg - dry 0.334 0.840N-Nitrosodimethylamine 1 10/01/21 16:58 V9595JMV
<0.230 mg/Kg - dry 0.230 0.840N-Nitrosodiphenylamine 1 10/01/21 16:58 V9595JMV
<0.150 mg/Kg - dry 0.150 0.840
N-Nitroso-di-n-propylamine 1 10/01/21 16:58 V9595JMV
<0.441 mg/Kg - dry 0.441 1.27Pentachlorophenol 1 10/01/21 16:58 V9595JMV
<0.264 mg/Kg - dry 0.264 0.840Phenanthrene 1 10/01/21 16:58 V9595JMV
<0.142 mg/Kg - dry 0.142 0.840Phenol 1 10/01/21 16:58 V9595JMV
<0.170 mg/Kg - dry 0.170 0.840Pyrene 1 10/01/21 16:58 V9595JMV
<0.101 mg/Kg - dry 0.101 0.421Pyridine 1 10/01/21 16:58 V9595JMV
<0.136 mg/Kg - dry 0.136 0.8401,2,4-Trichlorobenzene 1 10/01/21 16:58 V9595JMV
<0.122 mg/Kg - dry 0.122 0.840
2,4,5-Trichlorophenol 1 10/01/21 16:58 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-3
96523 Matrix:
9/29/2021 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.123 mg/Kg - dry 0.123 0.8402,4,6-Trichlorophenol 1 10/01/21 16:58 V9595JMV
Surrogate: Phenol-d5 76.0 Limits: 34-121%10/01/21 16:581 JMV V9595
Surrogate: 2-Fluorobiphenyl 79.6 Limits: 44-115%10/01/21 16:581 JMV V9595
Surrogate: 2-Fluorophenol 82.6 Limits: 35-115%10/01/21 16:581 JMV V9595
Surrogate: Nitrobenzene-d5 71.9 Limits: 37-122%10/01/21 16:581 JMV V9595
Surrogate: 4-Terphenyl-d14 82.0 Limits: 54-127%10/01/21 16:581 JMV V9595
Surrogate: 2,4,6-Tribromophenol 76.0 Limits: 39-132%10/01/21 16:581 JMV V9595
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.8 %Moisture 1 10/04/21 17:21 SW-DRYWTCEG
2.44 mg/Kg - dry 0.109 1.16Arsenic 10 10/04/21 23:58 6020BEDV
132 mg/Kg - dry 1.62 11.6Barium 10 10/04/21 23:58 6020BEDV
0.0705 J mg/Kg - dry 0.0638 0.580Cadmium 10 10/04/21 23:58 6020BEDV
42.2 mg/Kg - dry 0.336 1.16Chromium 10 10/04/21 23:58 6020BEDV
20.4 mg/Kg - dry 0.162 1.16
Lead 10 10/04/21 23:58 6020BEDV
0.0195 J mg/Kg - dry 0.0139 0.0348Mercury (Total)1 10/04/21 18:24 7471BEDV
1.23 J mg/Kg - dry 1.04 2.32Selenium 10 10/04/21 23:58 6020BEDV
<0.0475 mg/Kg - dry 0.0475 0.580Silver 10 10/04/21 23:58 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
0.009 J mg/Kg - dry 0.002 0.023Acetone 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/30/21 16:03 V9550TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/30/21 16:03 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/30/21 16:03 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/30/21 16:03 V9550TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/30/21 16:03 V9550TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/30/21 16:03 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/30/21 16:03 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/30/21 16:03 V9550TBL
<0.016 mg/Kg - dry 0.016 0.290Ethanol 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/30/21 16:03 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 09/30/21 16:03 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/30/21 16:03 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 09/30/21 16:03 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/30/21 16:03 V9550TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/30/21 16:03 V9550TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 09/30/21 16:03 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/30/21 16:03 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/30/21 16:03 V9550TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/30/21 16:03 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/30/21 16:03 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/30/21 16:03 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/30/21 16:03 V9550TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/30/21 16:03 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/30/21 16:03 V9550
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/30/21 16:031 TBL V9550
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/30/21 16:031 TBL V9550
Surrogate: Toluene-d8 90.4 Limits: 76-129%09/30/21 16:031 TBL V9550
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.134 mg/Kg - dry 0.134 0.766Acenaphthene 1 10/01/21 19:16 V9595JMV
<0.121 mg/Kg - dry 0.121 0.766Acenaphthylene 1 10/01/21 19:16 V9595JMV
<0.176 mg/Kg - dry 0.176 0.766Aniline 1 10/01/21 19:16 V9595JMV
<0.165 mg/Kg - dry 0.165 0.766Anthracene 1 10/01/21 19:16 V9595JMV
<0.161 mg/Kg - dry 0.161 0.766
Benzo(a)anthracene 1 10/01/21 19:16 V9595JMV
<0.170 mg/Kg - dry 0.170 0.766Benzo(a)pyrene 1 10/01/21 19:16 V9595JMV
<0.169 mg/Kg - dry 0.169 0.766Benzo(b)fluoranthene 1 10/01/21 19:16 V9595JMV
<0.157 mg/Kg - dry 0.157 0.766Benzo(g,h,i)perylene 1 10/01/21 19:16 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.158 mg/Kg - dry 0.158 0.766Benzo(k)fluoranthene 1 10/01/21 19:16 V9595JMV
<0.672 mg/Kg - dry 0.672 2.32Benzoic Acid 1 10/01/21 19:16 V9595JMV
<0.121 mg/Kg - dry 0.121 0.766Benzyl alcohol 1 10/01/21 19:16 V9595JMV
<0.136 mg/Kg - dry 0.136 0.766Bis(2-Chloroethoxy)methane 1 10/01/21 19:16 V9595JMV
<0.124 mg/Kg - dry 0.124 0.766Bis(2-Chloroethyl)ether 1 10/01/21 19:16 V9595JMV
<0.157 mg/Kg - dry 0.157 0.382Bis(2-Chloroisopropyl)ether 1 10/01/21 19:16 V9595JMV
<0.139 mg/Kg - dry 0.139 0.766Bis(2-ethylhexyl)phthalate 1 10/01/21 19:16 V9595JMV
<0.126 mg/Kg - dry 0.126 0.7664-Bromophenyl phenyl ether 1 10/01/21 19:16 V9595JMV
<0.131 mg/Kg - dry 0.131 0.382
Butyl benzyl phthalate 1 10/01/21 19:16 V9595JMV
<0.107 mg/Kg - dry 0.107 0.7664-Chloro-3-methylphenol 1 10/01/21 19:16 V9595JMV
<0.129 mg/Kg - dry 0.129 0.3824-Chloroaniline 1 10/01/21 19:16 V9595JMV
<0.134 mg/Kg - dry 0.134 0.7662-Chloronaphthalene 1 10/01/21 19:16 V9595JMV
<0.114 mg/Kg - dry 0.114 0.7662-Chlorophenol 1 10/01/21 19:16 V9595JMV
<0.146 mg/Kg - dry 0.146 1.164-Chlorophenyl phenyl ether 1 10/01/21 19:16 V9595JMV
<0.164 mg/Kg - dry 0.164 0.766Chrysene 1 10/01/21 19:16 V9595JMV
<0.266 mg/Kg - dry 0.266 0.766
Dibenz(a,h)anthracene 1 10/01/21 19:16 V9595JMV
<0.138 mg/Kg - dry 0.138 0.766Dibenzofuran 1 10/01/21 19:16 V9595JMV
<0.109 mg/Kg - dry 0.109 0.7661,2-Dichlorobenzene 1 10/01/21 19:16 V9595JMV
<0.112 mg/Kg - dry 0.112 0.7661,3-Dichlorobenzene 1 10/01/21 19:16 V9595JMV
<0.113 mg/Kg - dry 0.113 0.3821,4-Dichlorobenzene 1 10/01/21 19:16 V9595JMV
<0.170 mg/Kg - dry 0.170 0.7663,3'-Dichlorobenzidine 1 10/01/21 19:16 V9595JMV
<0.111 mg/Kg - dry 0.111 0.7662,4-Dichlorophenol 1 10/01/21 19:16 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.208 mg/Kg - dry 0.208 0.766Diethyl phthalate 1 10/01/21 19:16 V9595JMV
<0.201 mg/Kg - dry 0.201 0.766Dimethyl phthalate 1 10/01/21 19:16 V9595JMV
<0.125 mg/Kg - dry 0.125 0.3822,4-Dimethylphenol 1 10/01/21 19:16 V9595JMV
<0.124 mg/Kg - dry 0.124 0.766Di-n-butyl phthalate 1 10/01/21 19:16 V9595JMV
<0.278 mg/Kg - dry 0.278 1.744,6-Dinitro-2-methylphenol 1 10/01/21 19:16 V9595JMV
<0.603 mg/Kg - dry 0.603 1.742,4-Dinitrophenol 1 10/01/21 19:16 V9595JMV
<0.112 mg/Kg - dry 0.112 0.7662,4-Dinitrotoluene 1 10/01/21 19:16 V9595JMV
<0.125 mg/Kg - dry 0.125 0.7662,6-Dinitrotoluene 1 10/01/21 19:16 V9595JMV
<0.165 mg/Kg - dry 0.165 0.382
Di-n-Octyl Phthalate 1 10/01/21 19:16 V9595JMV
<0.142 mg/Kg - dry 0.142 0.766Fluoranthene 1 10/01/21 19:16 V9595JMV
<0.148 mg/Kg - dry 0.148 0.766Fluorene 1 10/01/21 19:16 V9595JMV
<0.122 mg/Kg - dry 0.122 0.766Hexachlorobenzene 1 10/01/21 19:16 V9595JMV
<0.113 mg/Kg - dry 0.113 0.766Hexachlorobutadiene 1 10/01/21 19:16 V9595JMV
<0.182 mg/Kg - dry 0.182 0.766Hexachlorocyclopentadiene 1 10/01/21 19:16 V9595JMV
<0.091 mg/Kg - dry 0.091 0.766Hexachloroethane 1 10/01/21 19:16 V9595JMV
<0.207 mg/Kg - dry 0.207 0.766
Indeno(1,2,3-cd)pyrene 1 10/01/21 19:16 V9595JMV
<0.221 mg/Kg - dry 0.221 0.766Isophorone 1 10/01/21 19:16 V9595JMV
<0.122 mg/Kg - dry 0.122 0.7661-Methylnaphthalene 1 10/01/21 19:16 V9595JMV
<0.116 mg/Kg - dry 0.116 0.7662-Methylnaphthalene 1 10/01/21 19:16 V9595JMV
<0.112 mg/Kg - dry 0.112 0.7662-Methylphenol 1 10/01/21 19:16 V9595JMV
<0.098 mg/Kg - dry 0.098 0.7663&4 Methylphenol 1 10/01/21 19:16 V9595JMV
<0.167 mg/Kg - dry 0.167 0.766Naphthalene 1 10/01/21 19:16 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.112 mg/Kg - dry 0.112 0.7662-Nitroaniline 1 10/01/21 19:16 V9595JMV
<0.139 mg/Kg - dry 0.139 0.7663-Nitroaniline 1 10/01/21 19:16 V9595JMV
<0.108 mg/Kg - dry 0.108 0.3824-Nitroaniline 1 10/01/21 19:16 V9595JMV
<0.134 mg/Kg - dry 0.134 0.382Nitrobenzene 1 10/01/21 19:16 V9595JMV
<0.103 mg/Kg - dry 0.103 0.7662-Nitrophenol 1 10/01/21 19:16 V9595JMV
<0.135 mg/Kg - dry 0.135 0.7664-Nitrophenol 1 10/01/21 19:16 V9595JMV
<0.305 mg/Kg - dry 0.305 0.766N-Nitrosodimethylamine 1 10/01/21 19:16 V9595JMV
<0.209 mg/Kg - dry 0.209 0.766N-Nitrosodiphenylamine 1 10/01/21 19:16 V9595JMV
<0.136 mg/Kg - dry 0.136 0.766
N-Nitroso-di-n-propylamine 1 10/01/21 19:16 V9595JMV
<0.402 mg/Kg - dry 0.402 1.16Pentachlorophenol 1 10/01/21 19:16 V9595JMV
<0.241 mg/Kg - dry 0.241 0.766Phenanthrene 1 10/01/21 19:16 V9595JMV
<0.129 mg/Kg - dry 0.129 0.766Phenol 1 10/01/21 19:16 V9595JMV
<0.155 mg/Kg - dry 0.155 0.766Pyrene 1 10/01/21 19:16 V9595JMV
<0.091 mg/Kg - dry 0.091 0.382Pyridine 1 10/01/21 19:16 V9595JMV
<0.124 mg/Kg - dry 0.124 0.7661,2,4-Trichlorobenzene 1 10/01/21 19:16 V9595JMV
<0.111 mg/Kg - dry 0.111 0.766
2,4,5-Trichlorophenol 1 10/01/21 19:16 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-4
96524 Matrix:
9/29/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.112 mg/Kg - dry 0.112 0.7662,4,6-Trichlorophenol 1 10/01/21 19:16 V9595JMV
Surrogate: Phenol-d5 74.6 Limits: 34-121%10/01/21 19:161 JMV V9595
Surrogate: 2-Fluorobiphenyl 79.6 Limits: 44-115%10/01/21 19:161 JMV V9595
Surrogate: 2-Fluorophenol 77.8 Limits: 35-115%10/01/21 19:161 JMV V9595
Surrogate: Nitrobenzene-d5 72.5 Limits: 37-122%10/01/21 19:161 JMV V9595
Surrogate: 4-Terphenyl-d14 80.8 Limits: 54-127%10/01/21 19:161 JMV V9595
Surrogate: 2,4,6-Tribromophenol 75.4 Limits: 39-132%10/01/21 19:161 JMV V9595
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
31.2 %Moisture 1 10/04/21 17:21 SW-DRYWTCEG
1.77 B mg/Kg - dry 0.137 1.45Arsenic 10 10/07/21 18:13 6020BEDV
117 mg/Kg - dry 2.03 14.5Barium 10 10/07/21 18:13 6020BEDV
<0.0799 mg/Kg - dry 0.0799 0.727Cadmium 10 10/07/21 18:13 6020BEDV
78.3 mg/Kg - dry 0.421 1.45Chromium 10 10/07/21 18:13 6020BEDV
13.4 mg/Kg - dry 0.203 1.45
Lead 10 10/07/21 18:13 6020BEDV
<0.0174 mg/Kg - dry 0.0174 0.0436Mercury (Total)1 10/04/21 18:27 7471BEDV
2.30 J mg/Kg - dry 1.31 2.91Selenium 10 10/08/21 16:08 6020BEDV
<0.0595 mg/Kg - dry 0.0595 0.727Silver 10 10/07/21 18:13 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
0.005 J mg/Kg - dry 0.003 0.029Acetone 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.029Acrolein 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 09/30/21 16:30 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 09/30/21 16:30 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 09/30/21 16:30 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 09/30/21 16:30 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 09/30/21 16:30 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 09/30/21 16:30 V9550TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 09/30/21 16:30 V9550TBL
<0.020 mg/Kg - dry 0.020 0.363Ethanol 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.072Ethyl Tertiary Butyl Ether (ETBE)1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 09/30/21 16:30 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0010 mg/Kg - dry 0.0010 0.014n-Hexane 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0292-Hexanone 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.029Methyl Ethyl Ketone (MEK)1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 09/30/21 16:30 V9550TBL
<0.021 mg/Kg - dry 0.021 0.0294-Methyl-2-Pentanone 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 09/30/21 16:30 V9550TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 09/30/21 16:30 V9550TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.014
1,2,3-Trichlorobenzene 1 09/30/21 16:30 V9550TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 09/30/21 16:30 V9550TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 09/30/21 16:30 V9550TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 09/30/21 16:30 V9550TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V9549 09/30/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 09/30/21 16:30 V9550TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 09/30/21 16:30 V9550TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 09/30/21 16:30 V9550TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 09/30/21 16:30 V9550
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/30/21 16:301 TBL V9550
Surrogate: Dibromofluoromethane 96.7 Limits: 84-123%09/30/21 16:301 TBL V9550
Surrogate: Toluene-d8 100 Limits: 76-129%09/30/21 16:301 TBL V9550
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.168 mg/Kg - dry 0.168 0.959Acenaphthene 1 10/01/21 16:12 V9595JMV
<0.152 mg/Kg - dry 0.152 0.959Acenaphthylene 1 10/01/21 16:12 V9595JMV
<0.220 mg/Kg - dry 0.220 0.959Aniline 1 10/01/21 16:12 V9595JMV
<0.207 mg/Kg - dry 0.207 0.959Anthracene 1 10/01/21 16:12 V9595JMV
<0.202 mg/Kg - dry 0.202 0.959
Benzo(a)anthracene 1 10/01/21 16:12 V9595JMV
<0.213 mg/Kg - dry 0.213 0.959Benzo(a)pyrene 1 10/01/21 16:12 V9595JMV
<0.212 mg/Kg - dry 0.212 0.959Benzo(b)fluoranthene 1 10/01/21 16:12 V9595JMV
<0.197 mg/Kg - dry 0.197 0.959Benzo(g,h,i)perylene 1 10/01/21 16:12 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.199 mg/Kg - dry 0.199 0.959Benzo(k)fluoranthene 1 10/01/21 16:12 V9595JMV
<0.843 mg/Kg - dry 0.843 2.91Benzoic Acid 1 10/01/21 16:12 V9595JMV
<0.152 mg/Kg - dry 0.152 0.959Benzyl alcohol 1 10/01/21 16:12 V9595JMV
<0.171 mg/Kg - dry 0.171 0.959Bis(2-Chloroethoxy)methane 1 10/01/21 16:12 V9595JMV
<0.155 mg/Kg - dry 0.155 0.959Bis(2-Chloroethyl)ether 1 10/01/21 16:12 V9595JMV
<0.197 mg/Kg - dry 0.197 0.479Bis(2-Chloroisopropyl)ether 1 10/01/21 16:12 V9595JMV
<0.174 mg/Kg - dry 0.174 0.959Bis(2-ethylhexyl)phthalate 1 10/01/21 16:12 V9595JMV
<0.158 mg/Kg - dry 0.158 0.9594-Bromophenyl phenyl ether 1 10/01/21 16:12 V9595JMV
<0.164 mg/Kg - dry 0.164 0.479
Butyl benzyl phthalate 1 10/01/21 16:12 V9595JMV
<0.134 mg/Kg - dry 0.134 0.9594-Chloro-3-methylphenol 1 10/01/21 16:12 V9595JMV
<0.162 mg/Kg - dry 0.162 0.4794-Chloroaniline 1 10/01/21 16:12 V9595JMV
<0.168 mg/Kg - dry 0.168 0.9592-Chloronaphthalene 1 10/01/21 16:12 V9595JMV
<0.142 mg/Kg - dry 0.142 0.9592-Chlorophenol 1 10/01/21 16:12 V9595JMV
<0.183 mg/Kg - dry 0.183 1.454-Chlorophenyl phenyl ether 1 10/01/21 16:12 V9595JMV
<0.206 mg/Kg - dry 0.206 0.959Chrysene 1 10/01/21 16:12 V9595JMV
<0.334 mg/Kg - dry 0.334 0.959
Dibenz(a,h)anthracene 1 10/01/21 16:12 V9595JMV
<0.172 mg/Kg - dry 0.172 0.959Dibenzofuran 1 10/01/21 16:12 V9595JMV
<0.137 mg/Kg - dry 0.137 0.9591,2-Dichlorobenzene 1 10/01/21 16:12 V9595JMV
<0.141 mg/Kg - dry 0.141 0.9591,3-Dichlorobenzene 1 10/01/21 16:12 V9595JMV
<0.141 mg/Kg - dry 0.141 0.4791,4-Dichlorobenzene 1 10/01/21 16:12 V9595JMV
<0.213 mg/Kg - dry 0.213 0.9593,3'-Dichlorobenzidine 1 10/01/21 16:12 V9595JMV
<0.139 mg/Kg - dry 0.139 0.9592,4-Dichlorophenol 1 10/01/21 16:12 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.261 mg/Kg - dry 0.261 0.959Diethyl phthalate 1 10/01/21 16:12 V9595JMV
<0.252 mg/Kg - dry 0.252 0.959Dimethyl phthalate 1 10/01/21 16:12 V9595JMV
<0.156 mg/Kg - dry 0.156 0.4792,4-Dimethylphenol 1 10/01/21 16:12 V9595JMV
<0.155 mg/Kg - dry 0.155 0.959Di-n-butyl phthalate 1 10/01/21 16:12 V9595JMV
<0.348 mg/Kg - dry 0.348 2.184,6-Dinitro-2-methylphenol 1 10/01/21 16:12 V9595JMV
<0.755 mg/Kg - dry 0.755 2.182,4-Dinitrophenol 1 10/01/21 16:12 V9595JMV
<0.140 mg/Kg - dry 0.140 0.9592,4-Dinitrotoluene 1 10/01/21 16:12 V9595JMV
<0.156 mg/Kg - dry 0.156 0.9592,6-Dinitrotoluene 1 10/01/21 16:12 V9595JMV
<0.207 mg/Kg - dry 0.207 0.479
Di-n-Octyl Phthalate 1 10/01/21 16:12 V9595JMV
<0.178 mg/Kg - dry 0.178 0.959Fluoranthene 1 10/01/21 16:12 V9595JMV
<0.186 mg/Kg - dry 0.186 0.959Fluorene 1 10/01/21 16:12 V9595JMV
<0.154 mg/Kg - dry 0.154 0.959Hexachlorobenzene 1 10/01/21 16:12 V9595JMV
<0.141 mg/Kg - dry 0.141 0.959Hexachlorobutadiene 1 10/01/21 16:12 V9595JMV
<0.228 mg/Kg - dry 0.228 0.959Hexachlorocyclopentadiene 1 10/01/21 16:12 V9595JMV
<0.115 mg/Kg - dry 0.115 0.959Hexachloroethane 1 10/01/21 16:12 V9595JMV
<0.260 mg/Kg - dry 0.260 0.959
Indeno(1,2,3-cd)pyrene 1 10/01/21 16:12 V9595JMV
<0.277 mg/Kg - dry 0.277 0.959Isophorone 1 10/01/21 16:12 V9595JMV
<0.154 mg/Kg - dry 0.154 0.9591-Methylnaphthalene 1 10/01/21 16:12 V9595JMV
<0.145 mg/Kg - dry 0.145 0.9592-Methylnaphthalene 1 10/01/21 16:12 V9595JMV
<0.140 mg/Kg - dry 0.140 0.9592-Methylphenol 1 10/01/21 16:12 V9595JMV
<0.123 mg/Kg - dry 0.123 0.9593&4 Methylphenol 1 10/01/21 16:12 V9595JMV
<0.209 mg/Kg - dry 0.209 0.959Naphthalene 1 10/01/21 16:12 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.140 mg/Kg - dry 0.140 0.9592-Nitroaniline 1 10/01/21 16:12 V9595JMV
<0.174 mg/Kg - dry 0.174 0.9593-Nitroaniline 1 10/01/21 16:12 V9595JMV
<0.135 mg/Kg - dry 0.135 0.4794-Nitroaniline 1 10/01/21 16:12 V9595JMV
<0.168 mg/Kg - dry 0.168 0.479Nitrobenzene 1 10/01/21 16:12 V9595JMV
<0.129 mg/Kg - dry 0.129 0.9592-Nitrophenol 1 10/01/21 16:12 V9595JMV
<0.170 mg/Kg - dry 0.170 0.9594-Nitrophenol 1 10/01/21 16:12 V9595JMV
<0.382 mg/Kg - dry 0.382 0.959N-Nitrosodimethylamine 1 10/01/21 16:12 V9595JMV
<0.263 mg/Kg - dry 0.263 0.959N-Nitrosodiphenylamine 1 10/01/21 16:12 V9595JMV
<0.171 mg/Kg - dry 0.171 0.959
N-Nitroso-di-n-propylamine 1 10/01/21 16:12 V9595JMV
<0.504 mg/Kg - dry 0.504 1.45Pentachlorophenol 1 10/01/21 16:12 V9595JMV
<0.302 mg/Kg - dry 0.302 0.959Phenanthrene 1 10/01/21 16:12 V9595JMV
<0.162 mg/Kg - dry 0.162 0.959Phenol 1 10/01/21 16:12 V9595JMV
<0.194 mg/Kg - dry 0.194 0.959Pyrene 1 10/01/21 16:12 V9595JMV
<0.115 mg/Kg - dry 0.115 0.479Pyridine 1 10/01/21 16:12 V9595JMV
<0.155 mg/Kg - dry 0.155 0.9591,2,4-Trichlorobenzene 1 10/01/21 16:12 V9595JMV
<0.139 mg/Kg - dry 0.139 0.959
2,4,5-Trichlorophenol 1 10/01/21 16:12 V9595JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-272-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Angela D Overcash
Senior Project Manager
Received : 09/29/2021
LEN-008
Report Date : 10/08/2021
Sample ID :
Lab No :
Sampled:SP-5
96525 Matrix:
9/29/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V9503 09/30/21 10:28
<0.140 mg/Kg - dry 0.140 0.9592,4,6-Trichlorophenol 1 10/01/21 16:12 V9595JMV
Surrogate: Phenol-d5 71.3 Limits: 34-121%10/01/21 16:121 JMV V9595
Surrogate: 2-Fluorobiphenyl 73.1 Limits: 44-115%10/01/21 16:121 JMV V9595
Surrogate: 2-Fluorophenol 76.9 Limits: 35-115%10/01/21 16:121 JMV V9595
Surrogate: Nitrobenzene-d5 70.1 Limits: 37-122%10/01/21 16:121 JMV V9595
Surrogate: 4-Terphenyl-d14 77.2 Limits: 54-127%10/01/21 16:121 JMV V9595
Surrogate: 2,4,6-Tribromophenol 70.7 Limits: 39-132%10/01/21 16:121 JMV V9595
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 68
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-272-0017
Lot Number:WI30096
Date Completed:10/05/2021
10/06/2021 11:45 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 14
Page 32 of 68
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WI30096
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B,Silica EPA 200.7, Boron, Calcium,Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weightunless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 14
Page 33 of 68
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WI30096

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/29/2021 0945SP-3 Solid 09/30/2021
002 09/29/2021 1020SP-4 Solid 09/30/2021
003 09/29/2021 1100SP-5 Solid 09/30/2021
(3 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 14
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WI30096

Sample Sample ID Matrix Parameter Method Result Q Units Page
003 SP-5 Solid Hexavalent Chromium 7199 0.57 J mg/kg 7
(1 detection)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 14
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-3
WI30096-001
09/29/2021 0945
09/30/2021
Solid
% Solids:77.0 09/30/2021 2304
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 10/04/2021 1703 AMR 10/04/2021 1134 17536
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 14
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-4
WI30096-002
09/29/2021 1020
09/30/2021
Solid
% Solids:88.4 09/30/2021 2304
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 10/04/2021 1729 AMR 10/04/2021 1134 17536
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.231.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 14
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-5
WI30096-003
09/29/2021 1100
09/30/2021
Solid
% Solids:68.7 09/30/2021 2304
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 10/04/2021 1821 AMR 10/04/2021 1134 17536
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.57 J 1mg/kg0.291.5
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 14
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 14
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ17536-001
17536 3060A
10/04/2021 1134Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 10/04/2021 15331.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 14
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ17536-002
17536 3060A
10/04/2021 1134Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.1 10/04/2021 1559911080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 14
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:WI30096-001MS
17536 3060A
10/04/2021 1134Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(mg/kg) (mg/kg) (mg/kg)
Hexavalent Chromium 1200 10/04/2021 171688140075-125ND50
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 14
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 14
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 14
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 14
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V9553,V9698QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9530
Associated Lab Samples: 96523, 96524
LRB-V9530 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/30/21 19:541.000.0940<0.0940mg/KgArsenic
09/30/21 19:5410.01.40<1.40mg/KgBarium
09/30/21 19:540.5000.0550<0.0550mg/KgCadmium
09/30/21 19:541.000.290<0.290mg/KgChromium
09/30/21 19:541.000.140<0.140mg/KgLead
09/30/21 19:542.000.900<0.900mg/KgSelenium
09/30/21 19:540.5000.0410<0.0410mg/KgSilver
LCS-V9530Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.012.312.5mg/KgArsenic 80-120
10212.712.5mg/KgBarium 80-120
10513.112.5mg/KgCadmium 80-120
10312.912.5mg/KgChromium 80-120
10613.312.5mg/KgLead 80-120
10713.412.5mg/KgSelenium 80-120
1055.245.00mg/KgSilver 80-120
V 96172-MS-V9530 V 96172-MSD-V9530Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
11.5 92.011.212.512.50.705mg/KgArsenic 90.0 75-125 2.6 20
37.9 94.037.912.512.526.2mg/KgBarium 94.0 75-125 0.0 20
11.9 95.011.712.512.50.0573mg/KgCadmium 94.0 75-125 1.6 20
12.9 94.012.712.512.51.09mg/KgChromium 93.0 75-125 1.5 20
Page 1 of 21Date:10/08/2021 04:58 PM
Page 46 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V9553,V9698QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9530
V 96172-MS-V9530 V 96172-MSD-V9530Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
19.4 95.019.312.512.57.52mg/KgLead 94.0 75-125 0.5 20
13.5 84.013.812.512.52.97mg/KgSelenium 87.0 75-125 2.1 20
4.78 96.04.645.005.00<0.0410mg/KgSilver 93.0 75-125 2.9 20
V 96172-PDS-V9530Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/05/21 00:1797.012.1mg/KgArsenic
10/05/21 00:1710226.1mg/KgBarium
10/05/21 00:1798.012.2mg/KgCadmium
10/05/21 00:1796.012.5mg/KgChromium
10/05/21 00:1799.016.1mg/KgLead
10/05/21 00:1792.012.9mg/KgSelenium
10/05/21 00:1797.012.2mg/KgSilver
Page 2 of 21Date:10/08/2021 04:58 PM
Page 47 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V9881,V9935QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9795
Associated Lab Samples: 96525
LRB-V9795 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/07/21 16:551.000.09400.126mg/KgArsenic
10/07/21 16:5510.01.40<1.40mg/KgBarium
10/07/21 16:550.5000.0550<0.0550mg/KgCadmium
10/07/21 16:551.000.290<0.290mg/KgChromium
10/07/21 16:551.000.140<0.140mg/KgLead
10/08/21 15:552.000.900<0.900mg/KgSelenium
10/07/21 16:550.5000.0410<0.0410mg/KgSilver
LCS-V9795Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10212.812.5mg/KgArsenic 80-120
10012.512.5mg/KgBarium 80-120
10413.012.5mg/KgCadmium 80-120
10312.912.5mg/KgChromium 80-120
10513.112.5mg/KgLead 80-120
10813.512.5mg/KgSelenium 80-120
1035.145.00mg/KgSilver 80-120
V 96615-MS-V9795 V 96615-MSD-V9795Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.6 86.012.512.512.51.79mg/KgArsenic 86.0 75-125 0.7 20
56.9 12558.512.512.541.3mg/KgBarium 138*75-125 2.7 20
12.6 10112.712.512.50.167mg/KgCadmium 102 75-125 0.7 20
26.8 11725.912.512.512.2mg/KgChromium 110 75-125 3.4 20
Page 3 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 48 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V9881,V9935QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V9795
V 96615-MS-V9795 V 96615-MSD-V9795Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
31.1 98.031.612.512.518.8mg/KgLead 102 75-125 1.5 20
13.0 10414.712.512.51.42mg/KgSelenium 118 75-125 12.2 20
4.97 99.05.055.005.00<0.0410mg/KgSilver 101 75-125 1.5 20
V 96615-PDS-V9795Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/07/21 17:2810313.7mg/KgArsenic
10/07/21 17:2810033.3mg/KgBarium
10/07/21 17:2810112.7mg/KgCadmium
10/07/21 17:2899.018.4mg/KgChromium
10/07/21 17:2810021.9mg/KgLead
10/07/21 17:2810413.0mg/KgSelenium
10/07/21 17:2810012.5mg/KgSilver
Page 4 of 21Date:10/08/2021 04:58 PM
Page 49 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V9690QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V9672
Associated Lab Samples: 96523, 96524, 96525
LRB-V9672 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/04/21 17:080.03000.0120<0.0120mg/KgMercury (Total)
LCS-V9672Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
91.00.3790.417mg/KgMercury (Total)80-120
V 96597-MS-V9672 V 96597-MSD-V9672Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.422 1010.4150.4170.4170.0165mg/KgMercury (Total)100 80-120 1.6 20
V 96597-PDS-V9672Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/04/21 17:2698.00.204mg/KgMercury (Total)
Page 5 of 21Date:10/08/2021 04:58 PM
Page 50 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
Associated Lab Samples: 96523, 96524, 96525
LRB-V9549 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/30/21 11:530.0200.002<0.002mg/KgAcetone
09/30/21 11:530.0200.001<0.001mg/KgAcrolein
09/30/21 11:530.0200.0008<0.0008mg/KgAcrylonitrile
09/30/21 11:530.0050.0006<0.0006mg/KgBenzene
09/30/21 11:530.0050.0005<0.0005mg/KgBromobenzene
09/30/21 11:530.0050.0008<0.0008mg/KgBromochloromethane
09/30/21 11:530.0050.001<0.001mg/KgBromodichloromethane
09/30/21 11:530.0050.001<0.001mg/KgBromoform
09/30/21 11:530.0100.001<0.001mg/KgBromomethane
09/30/21 11:530.0050.0005<0.0005mg/Kgn-Butylbenzene
09/30/21 11:530.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/30/21 11:530.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/30/21 11:530.0050.0006<0.0006mg/KgCarbon Disulfide
09/30/21 11:530.0050.001<0.001mg/KgCarbon Tetrachloride
09/30/21 11:530.0050.0007<0.0007mg/KgChlorobenzene
09/30/21 11:530.0050.0009<0.0009mg/KgChlorodibromomethane
09/30/21 11:530.0100.0009<0.0009mg/KgChloroethane
09/30/21 11:530.0050.001<0.001mg/KgChloroform
09/30/21 11:530.0100.0006<0.0006mg/KgChloromethane
09/30/21 11:530.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/30/21 11:530.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/30/21 11:530.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/30/21 11:530.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/30/21 11:530.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/30/21 11:530.0050.0006<0.0006mg/KgDibromomethane
09/30/21 11:530.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/30/21 11:530.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 6 of 21Date:10/08/2021 04:58 PM
Page 51 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
Associated Lab Samples: 96523, 96524, 96525
LRB-V9549 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/30/21 11:530.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/30/21 11:530.0100.001<0.001mg/KgDichlorodifluoromethane
09/30/21 11:530.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/30/21 11:530.0050.001<0.001mg/Kg1,2-Dichloroethane
09/30/21 11:530.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/30/21 11:530.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/30/21 11:530.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/30/21 11:530.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/30/21 11:530.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/30/21 11:530.0050.001<0.001mg/Kg2,2-Dichloropropane
09/30/21 11:530.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/30/21 11:530.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/30/21 11:530.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/30/21 11:530.2500.014<0.014mg/KgEthanol
09/30/21 11:530.0050.0006<0.0006mg/KgEthylbenzene
09/30/21 11:530.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/30/21 11:530.0100.0008<0.0008mg/KgHexachlorobutadiene
09/30/21 11:530.0100.0007<0.0007mg/Kgn-Hexane
09/30/21 11:530.0200.0006<0.0006mg/Kg2-Hexanone
09/30/21 11:530.0050.0005<0.0005mg/KgIsopropylbenzene
09/30/21 11:530.0050.001<0.001mg/Kg4-Isopropyl toluene
09/30/21 11:530.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/30/21 11:530.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/30/21 11:530.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/30/21 11:530.0100.001<0.001mg/KgMethylene Chloride
09/30/21 11:530.0100.0010<0.0010mg/KgNaphthalene
09/30/21 11:530.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 7 of 21Date:10/08/2021 04:58 PM
Page 52 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
Associated Lab Samples: 96523, 96524, 96525
LRB-V9549 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/30/21 11:530.0050.001<0.001mg/KgStyrene
09/30/21 11:530.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/30/21 11:530.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/30/21 11:530.0050.0009<0.0009mg/KgTetrachloroethene
09/30/21 11:530.0050.0007<0.0007mg/KgToluene
09/30/21 11:530.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/30/21 11:530.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/30/21 11:530.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/30/21 11:530.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/30/21 11:530.0050.0009<0.0009mg/KgTrichloroethene
09/30/21 11:530.0100.002<0.002mg/KgTrichlorofluoromethane
09/30/21 11:530.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/30/21 11:530.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/30/21 11:530.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/30/21 11:530.0100.0005<0.0005mg/KgVinyl Acetate
09/30/21 11:530.0100.0005<0.0005mg/KgVinyl Chloride
09/30/21 11:530.0050.0005<0.0005mg/Kgo-Xylene
09/30/21 11:530.0100.001<0.001mg/Kgm,p-Xylene
09/30/21 11:534-Bromofluorobenzene (S)101 70-130
09/30/21 11:53Dibromofluoromethane (S)101 84-123
09/30/21 11:53Toluene-d8 (S)94.4 76-129
LCS-V9549 LCSD-V9549Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.080 80.51010.1010.100mg/KgAcetone 29-198 22.5*20
Page 8 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 53 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
LCS-V9549 LCSD-V9549Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.104 1041200.1200.100mg/KgAcrolein 70-130 14.2 20
0.101 1011220.1220.100mg/KgAcrylonitrile 65-134 18.8 20
0.041 82.41010.0500.050mg/KgBenzene 74-127 20.6*20
0.040 81.293.80.0460.050mg/KgBromobenzene 73-125 14.4 20
0.047 95.41120.0560.050mg/KgBromochloromethane 72-134 16.0 20
0.045 90.695.60.0470.050mg/KgBromodichloromethane 75-122 5.3 20
0.049 98.298.20.0490.050mg/KgBromoform 66-135 0.0 20
0.055 1101040.0520.050mg/KgBromomethane 20-180 5.7 20
0.039 79.089.00.0440.050mg/Kgn-Butylbenzene 65-135 11.9 20
0.040 80.681.40.0400.050mg/Kgsec-Butyl benzene 66-131 0.9 20
0.040 80.888.20.0440.050mg/Kgtert-Butyl benzene 67-132 8.7 20
0.040 80.294.20.0470.050mg/KgCarbon Disulfide 61-129 16.0 20
0.041 82.21030.0510.050mg/KgCarbon Tetrachloride 64-143 22.0*20
0.042 85.290.20.0450.050mg/KgChlorobenzene 74-118 5.7 20
0.046 93.697.00.0480.050mg/KgChlorodibromomethane 73-122 3.5 20
0.036 72.279.00.0390.050mg/KgChloroethane 33-149 8.9 20
0.041 83.41020.0510.050mg/KgChloroform 73-127 20.0*20
0.039 78.687.00.0430.050mg/KgChloromethane 45-143 10.1 20
0.040 80.288.60.0440.050mg/Kg2-Chlorotoluene 67-124 9.9 20
0.040 80.091.20.0450.050mg/Kg4-Chlorotoluene 71-126 13.0 20
0.042 84.21080.0530.050mg/KgDi-Isopropyl Ether (DIPE)59-159 24.4*20
0.052 1051010.0500.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.4 20
0.047 94.097.00.0480.050mg/Kg1,2-Dibromoethane 70-132 3.1 20
0.047 95.01040.0520.050mg/KgDibromomethane 74-133 9.2 20
0.043 87.290.40.0450.050mg/Kg1,2-Dichlorobenzene 72-123 3.6 20
0.042 84.285.20.0420.050mg/Kg1,3-Dichlorobenzene 71-120 1.1 20
Page 9 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 54 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
LCS-V9549 LCSD-V9549Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.088.80.0440.050mg/Kg1,4-Dichlorobenzene 71-123 4.3 20
0.036 73.878.00.0390.050mg/KgDichlorodifluoromethane 26-146 5.5 20
0.040 81.41030.0510.050mg/Kg1,1-Dichloroethane 74-127 23.4*20
0.043 86.698.60.0490.050mg/Kg1,2-Dichloroethane 68-128 12.9 20
0.040 81.693.80.0460.050mg/Kg1,1-Dichloroethene 67-149 13.9 20
0.040 81.61020.0510.050mg/Kgcis-1,2-Dichloroethene 76-134 22.4*20
0.040 81.01020.0510.050mg/Kgtrans-1,2-Dichloroethene 73-132 23.3*20
0.043 86.21030.0510.050mg/Kg1,2-Dichloropropane 73-130 17.5 20
0.044 89.493.40.0460.050mg/Kg1,3-Dichloropropane 75-124 4.3 20
0.041 82.41030.0510.050mg/Kg2,2-Dichloropropane 50-142 22.2*20
0.040 80.01020.0510.050mg/Kg1,1-Dichloropropene 71-130 24.5*20
0.045 91.61040.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 12.8 20
0.046 93.61130.0560.050mg/Kgtrans-1,3-Dichloropropene 68-123 18.6 20
1.39 1111211.511.25mg/KgEthanol 70-130 8.2 20
0.041 82.689.00.0440.050mg/KgEthylbenzene 74-128 7.4 20
0.090 90.41100.1100.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 19.5 20
0.045 91.899.60.0490.050mg/KgHexachlorobutadiene 64-125 8.1 20
0.042 85.41120.0550.050mg/Kgn-Hexane 70-130 26.7*20
0.048 96.01030.0510.050mg/Kg2-Hexanone 61-157 7.0 20
0.040 80.492.40.0460.050mg/KgIsopropylbenzene 68-126 13.8 20
0.041 82.884.80.0420.050mg/Kg4-Isopropyl toluene 68-129 2.3 20
0.045 90.41100.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 19.5 20
0.047 95.01130.0560.050mg/KgMethyl tert-butyl ether (MTBE)70-130 17.3 20
0.049 98.81220.0610.050mg/Kg4-Methyl-2-Pentanone 57-162 21.0*20
0.040 81.01010.0500.050mg/KgMethylene Chloride 74-129 21.7*20
0.051 1041040.0510.050mg/KgNaphthalene 57-157 0.1 20
Page 10 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 55 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V9550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V9549
LCS-V9549 LCSD-V9549Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.039 79.493.00.0460.050mg/Kgn-Propylbenzene 67-130 15.7 20
0.043 87.092.40.0460.050mg/KgStyrene 77-121 6.0 20
0.044 89.293.00.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.1 20
0.043 87.497.60.0480.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 11.0 20
0.044 89.01070.0530.050mg/KgTetrachloroethene 68-130 18.5 20
0.042 85.81010.0500.050mg/KgToluene 71-129 16.6 20
0.048 96.899.20.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.4 20
0.046 93.01010.0500.050mg/Kg1,2,4-Trichlorobenzene 66-125 7.8 20
0.040 81.81010.0500.050mg/Kg1,1,1-Trichloroethane 67-131 21.0*20
0.046 92.497.20.0480.050mg/Kg1,1,2-Trichloroethane 70-133 5.0 20
0.042 85.093.00.0460.050mg/KgTrichloroethene 75-133 8.9 20
0.044 88.097.60.0480.050mg/KgTrichlorofluoromethane 44-146 10.3 20
0.045 90.691.20.0450.050mg/Kg1,2,3-Trichloropropane 60-137 0.6 20
0.041 82.890.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 8.5 20
0.041 82.088.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.2 20
0.053 1071230.0610.050mg/KgVinyl Acetate 60-140 14.6 20
0.039 79.490.20.0450.050mg/KgVinyl Chloride 48-147 12.7 20
0.042 85.490.20.0450.050mg/Kgo-Xylene 74-126 5.4 20
0.085 85.591.20.0910.100mg/Kgm,p-Xylene 75-124 6.4 20
1021084-Bromofluorobenzene (S)70-130
97.0111Dibromofluoromethane (S)84-123
95.092.2Toluene-d8 (S)76-129
Page 11 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 56 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
Associated Lab Samples: 96523, 96524, 96525
LRB-V9503 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/01/21 08:540.6600.116<0.116mg/KgAcenaphthene
10/01/21 08:540.6600.105<0.105mg/KgAcenaphthylene
10/01/21 08:540.6600.152<0.152mg/KgAniline
10/01/21 08:540.6600.143<0.143mg/KgAnthracene
10/01/21 08:540.6600.139<0.139mg/KgBenzo(a)anthracene
10/01/21 08:540.6600.147<0.147mg/KgBenzo(a)pyrene
10/01/21 08:540.6600.146<0.146mg/KgBenzo(b)fluoranthene
10/01/21 08:540.6600.136<0.136mg/KgBenzo(g,h,i)perylene
10/01/21 08:540.6600.137<0.137mg/KgBenzo(k)fluoranthene
10/01/21 08:542.000.580<0.580mg/KgBenzoic Acid
10/01/21 08:540.6600.105<0.105mg/KgBenzyl alcohol
10/01/21 08:540.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
10/01/21 08:540.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
10/01/21 08:540.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
10/01/21 08:540.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
10/01/21 08:540.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
10/01/21 08:540.3300.113<0.113mg/KgButyl benzyl phthalate
10/01/21 08:540.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
10/01/21 08:540.3300.112<0.112mg/Kg4-Chloroaniline
10/01/21 08:540.6600.116<0.116mg/Kg2-Chloronaphthalene
10/01/21 08:540.6600.098<0.098mg/Kg2-Chlorophenol
10/01/21 08:541.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
10/01/21 08:540.6600.142<0.142mg/KgChrysene
10/01/21 08:540.6600.230<0.230mg/KgDibenz(a,h)anthracene
10/01/21 08:540.6600.119<0.119mg/KgDibenzofuran
10/01/21 08:540.6600.094<0.094mg/Kg1,2-Dichlorobenzene
10/01/21 08:540.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 12 of 21Date:10/08/2021 04:58 PM
Page 57 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
Associated Lab Samples: 96523, 96524, 96525
LRB-V9503 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/01/21 08:540.3300.097<0.097mg/Kg1,4-Dichlorobenzene
10/01/21 08:540.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
10/01/21 08:540.6600.095<0.095mg/Kg2,4-Dichlorophenol
10/01/21 08:540.6600.180<0.180mg/KgDiethyl phthalate
10/01/21 08:540.6600.174<0.174mg/KgDimethyl phthalate
10/01/21 08:540.3300.108<0.108mg/Kg2,4-Dimethylphenol
10/01/21 08:540.6600.107<0.107mg/KgDi-n-butyl phthalate
10/01/21 08:541.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
10/01/21 08:541.500.520<0.520mg/Kg2,4-Dinitrophenol
10/01/21 08:540.6600.096<0.096mg/Kg2,4-Dinitrotoluene
10/01/21 08:540.6600.108<0.108mg/Kg2,6-Dinitrotoluene
10/01/21 08:540.3300.143<0.143mg/KgDi-n-Octyl Phthalate
10/01/21 08:540.6600.123<0.123mg/KgFluoranthene
10/01/21 08:540.6600.128<0.128mg/KgFluorene
10/01/21 08:540.6600.106<0.106mg/KgHexachlorobenzene
10/01/21 08:540.6600.097<0.097mg/KgHexachlorobutadiene
10/01/21 08:540.6600.157<0.157mg/KgHexachlorocyclopentadiene
10/01/21 08:540.6600.079<0.079mg/KgHexachloroethane
10/01/21 08:540.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
10/01/21 08:540.6600.191<0.191mg/KgIsophorone
10/01/21 08:540.6600.106<0.106mg/Kg1-Methylnaphthalene
10/01/21 08:540.6600.100<0.100mg/Kg2-Methylnaphthalene
10/01/21 08:540.6600.097<0.097mg/Kg2-Methylphenol
10/01/21 08:540.6600.084<0.084mg/Kg3&4 Methylphenol
10/01/21 08:540.6600.144<0.144mg/KgNaphthalene
10/01/21 08:540.6600.096<0.096mg/Kg2-Nitroaniline
10/01/21 08:540.6600.120<0.120mg/Kg3-Nitroaniline
Page 13 of 21Date:10/08/2021 04:58 PM
Page 58 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
Associated Lab Samples: 96523, 96524, 96525
LRB-V9503 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/01/21 08:540.3300.093<0.093mg/Kg4-Nitroaniline
10/01/21 08:540.3300.116<0.116mg/KgNitrobenzene
10/01/21 08:540.6600.088<0.088mg/Kg2-Nitrophenol
10/01/21 08:540.6600.117<0.117mg/Kg4-Nitrophenol
10/01/21 08:540.6600.263<0.263mg/KgN-Nitrosodimethylamine
10/01/21 08:540.6600.181<0.181mg/KgN-Nitrosodiphenylamine
10/01/21 08:540.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
10/01/21 08:541.000.347<0.347mg/KgPentachlorophenol
10/01/21 08:540.6600.208<0.208mg/KgPhenanthrene
10/01/21 08:540.6600.112<0.112mg/KgPhenol
10/01/21 08:540.6600.134<0.134mg/KgPyrene
10/01/21 08:540.3300.079<0.079mg/KgPyridine
10/01/21 08:540.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
10/01/21 08:540.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
10/01/21 08:540.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
10/01/21 08:542-Fluorobiphenyl (S)97.6 44-115
10/01/21 08:542-Fluorophenol (S)104 35-115
10/01/21 08:54Nitrobenzene-d5 (S)94.6 37-122
10/01/21 08:544-Terphenyl-d14 (S)101 54-127
10/01/21 08:542,4,6-Tribromophenol (S)100 39-132
10/01/21 08:54Phenol-d5 (S)96.0 34-121
LCS-V9503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.01.421.67mg/KgAcenaphthene 40-123
89.21.491.67mg/KgAcenaphthylene 32-132
Page 14 of 21Date:10/08/2021 04:58 PM
Page 59 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
LCS-V9503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.41.511.67mg/KgAniline 12-197
89.81.501.67mg/KgAnthracene 47-123
88.61.481.67mg/KgBenzo(a)anthracene 49-126
1121.871.67mg/KgBenzo(a)pyrene 45-129
1041.731.67mg/KgBenzo(b)fluoranthene 45-132
1041.741.67mg/KgBenzo(g,h,i)perylene 43-134
93.41.561.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.121.67mg/KgBenzoic Acid 10-83
85.01.421.67mg/KgBenzyl alcohol 29-122
86.21.441.67mg/KgBis(2-Chloroethoxy)methane 36-121
84.41.411.67mg/KgBis(2-Chloroethyl)ether 31-120
75.41.261.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1011.681.67mg/KgBis(2-ethylhexyl)phthalate 51-133
85.61.431.67mg/Kg4-Bromophenyl phenyl ether 46-124
97.61.631.67mg/KgButyl benzyl phthalate 48-132
81.41.361.67mg/Kg4-Chloro-3-methylphenol 45-122
70.61.181.67mg/Kg4-Chloroaniline 17-106
88.61.481.67mg/Kg2-Chloronaphthalene 41-114
83.81.401.67mg/Kg2-Chlorophenol 34-121
88.61.481.67mg/Kg4-Chlorophenyl phenyl ether 45-121
89.81.501.67mg/KgChrysene 50-124
96.41.611.67mg/KgDibenz(a,h)anthracene 45-134
85.61.431.67mg/KgDibenzofuran 44-120
71.21.191.67mg/Kg1,2-Dichlorobenzene 33-117
73.01.221.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
80.21.341.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 15 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 60 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
LCS-V9503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.61.331.67mg/Kg2,4-Dichlorophenol 40-122
92.81.551.67mg/KgDiethyl phthalate 50-124
91.01.521.67mg/KgDimethyl phthalate 48-124
92.81.551.67mg/Kg2,4-Dimethylphenol 30-127
1011.681.67mg/KgDi-n-butyl phthalate 51-128
89.81.501.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
95.81.601.67mg/Kg2,4-Dinitrophenol 27-129
90.41.511.67mg/Kg2,4-Dinitrotoluene 48-126
90.41.511.67mg/Kg2,6-Dinitrotoluene 46-124
1051.761.67mg/KgDi-n-Octyl Phthalate 45-140
86.81.451.67mg/KgFluoranthene 50-127
88.01.471.67mg/KgFluorene 43-125
86.81.451.67mg/KgHexachlorobenzene 45-122
73.61.231.67mg/KgHexachlorobutadiene 32-123
67.01.121.67mg/KgHexachlorocyclopentadiene 32-117
69.41.161.67mg/KgHexachloroethane 28-117
97.61.631.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
72.41.211.67mg/KgIsophorone 30-122
69.41.161.67mg/Kg1-Methylnaphthalene 40-119
69.41.161.67mg/Kg2-Methylnaphthalene 38-122
85.01.421.67mg/Kg2-Methylphenol 32-122
72.41.211.67mg/Kg3&4 Methylphenol 34-119
71.21.191.67mg/KgNaphthalene 35-123
94.61.581.67mg/Kg2-Nitroaniline 44-127
90.41.511.67mg/Kg3-Nitroaniline 33-119
95.81.601.67mg/Kg4-Nitroaniline 63-147
77.21.291.67mg/KgNitrobenzene 34-122
Page 16 of 21Date:10/08/2021 04:58 PM
Page 61 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
LCS-V9503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
69.41.161.67mg/Kg2-Nitrophenol 36-123
1081.811.67mg/Kg4-Nitrophenol 30-132
83.21.391.67mg/KgN-Nitrosodimethylamine 10-146
1081.811.67mg/KgN-Nitrosodiphenylamine 38-127
77.81.301.67mg/KgN-Nitroso-di-n-propylamine 36-120
1191.991.67mg/KgPentachlorophenol 25-133
90.41.511.67mg/KgPhenanthrene 50-121
92.81.551.67mg/KgPhenol 34-121
91.01.521.67mg/KgPyrene 47-127
56.20.9401.67mg/KgPyridine 10-80
67.61.131.67mg/Kg1,2,4-Trichlorobenzene 34-118
86.21.441.67mg/Kg2,4,5-Trichlorophenol 41-124
94.61.581.67mg/Kg2,4,6-Trichlorophenol 39-126
77.82-Fluorobiphenyl (S)44-115
80.72-Fluorophenol (S)35-115
64.6Nitrobenzene-d5 (S)37-122
79.64-Terphenyl-d14 (S)54-127
75.62,4,6-Tribromophenol (S)39-132
74.4Phenol-d5 (S)34-121
V 96524-MS-V9503 V 96524-MSD-V9503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.32 79.01.191.671.67<0.116mg/KgAcenaphthene 71.2 40-123 10.3 20
1.40 83.81.281.671.67<0.105mg/KgAcenaphthylene 76.6 32-132 8.9 20
1.32 79.01.201.671.67<0.152mg/KgAniline 71.8 12-197 9.5 20
Page 17 of 21Date:10/08/2021 04:58 PM
Page 62 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
V 96524-MS-V9503 V 96524-MSD-V9503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.35 80.81.181.671.67<0.143mg/KgAnthracene 70.6 47-123 13.4 20
1.35 80.81.171.671.67<0.139mg/KgBenzo(a)anthracene 70.0 49-126 14.2 20
1.74 1041.491.671.67<0.147mg/KgBenzo(a)pyrene 89.2 45-129 15.4 20
1.63 97.61.431.671.67<0.146mg/KgBenzo(b)fluoranthene 85.6 45-132 13.0 20
1.53 91.61.341.671.67<0.136mg/KgBenzo(g,h,i)perylene 80.2 43-134 13.2 20
1.42 85.01.251.671.67<0.137mg/KgBenzo(k)fluoranthene 74.8 47-132 12.7 20
<0.580 0.0*<0.5801.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.33 79.61.421.671.67<0.105mg/KgBenzyl alcohol 85.0 29-122 6.5 20
1.38 82.61.261.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 75.4 36-121 9.0 20
1.29 77.21.171.671.67<0.107mg/KgBis(2-Chloroethyl)ether 70.0 31-120 9.7 20
1.23 73.61.081.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 64.6 33-131 12.9 20
1.61 96.41.401.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 83.8 51-133 13.9 20
1.36 81.41.151.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 68.8 46-124 16.7 20
1.61 96.41.421.671.67<0.113mg/KgButyl benzyl phthalate 85.0 48-132 12.5 20
1.26 75.41.121.671.67<0.092mg/Kg4-Chloro-3-methylphenol 67.0 45-122 11.7 20
1.05 62.80.9321.671.67<0.112mg/Kg4-Chloroaniline 55.8 17-106 11.9 20
1.42 85.01.251.671.67<0.116mg/Kg2-Chloronaphthalene 74.8 41-114 12.7 20
1.33 79.61.191.671.67<0.098mg/Kg2-Chlorophenol 71.2 34-121 11.1 20
1.30 77.81.191.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 71.2 45-121 8.8 20
1.38 82.61.171.671.67<0.142mg/KgChrysene 70.0 50-124 16.4 20
1.43 85.61.241.671.67<0.230mg/KgDibenz(a,h)anthracene 74.2 45-134 14.2 20
1.35 80.81.181.671.67<0.119mg/KgDibenzofuran 70.6 44-120 13.4 20
1.18 70.61.041.671.67<0.094mg/Kg1,2-Dichlorobenzene 62.2 33-117 12.6 20
1.15 68.80.9871.671.67<0.097mg/Kg1,3-Dichlorobenzene 59.1 30-115 15.2 20
1.13 67.61.011.671.67<0.097mg/Kg1,4-Dichlorobenzene 60.4 31-115 11.2 20
1.11 66.41.021.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 61.0 22-121 8.4 20
Page 18 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 63 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
V 96524-MS-V9503 V 96524-MSD-V9503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.23 73.61.121.671.67<0.095mg/Kg2,4-Dichlorophenol 67.0 40-122 9.3 20
1.39 83.21.251.671.67<0.180mg/KgDiethyl phthalate 74.8 50-124 10.6 20
1.38 82.61.241.671.67<0.174mg/KgDimethyl phthalate 74.2 48-124 10.6 30
1.37 82.01.131.671.67<0.108mg/Kg2,4-Dimethylphenol 67.6 30-127 19.2 20
1.56 93.41.341.671.67<0.107mg/KgDi-n-butyl phthalate 80.2 51-128 15.1 20
1.02 0.0*0.6181.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.06 0.0*0.6991.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.39 83.21.261.671.67<0.096mg/Kg2,4-Dinitrotoluene 75.4 48-126 9.8 20
1.39 83.21.241.671.67<0.108mg/Kg2,6-Dinitrotoluene 74.2 46-124 11.4 20
1.74 1041.531.671.67<0.143mg/KgDi-n-Octyl Phthalate 91.6 45-140 12.8 20
1.35 80.81.171.671.67<0.123mg/KgFluoranthene 70.0 50-127 14.2 20
1.36 81.41.221.671.67<0.128mg/KgFluorene 73.0 43-125 10.8 20
1.27 76.01.071.671.67<0.106mg/KgHexachlorobenzene 64.0 45-122 17.0 20
1.19 71.21.061.671.67<0.097mg/KgHexachlorobutadiene 63.4 32-123 11.5 20
0.316 0.0*0.2081.671.67<0.157mg/KgHexachlorocyclopentadiene 0.0*32-117 0.0 20
1.07 64.00.9291.671.67<0.079mg/KgHexachloroethane 55.6 28-117 14.1 20
1.52 91.01.341.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 80.2 45-133 12.5 20
1.11 66.41.001.671.67<0.191mg/KgIsophorone 59.8 30-122 10.4 20
1.13 67.60.9891.671.67<0.106mg/Kg1-Methylnaphthalene 59.2 40-119 13.3 20
1.12 67.00.9741.671.67<0.100mg/Kg2-Methylnaphthalene 58.3 38-122 13.9 20
1.33 79.61.171.671.67<0.097mg/Kg2-Methylphenol 70.0 32-122 12.8 20
1.13 67.61.001.671.67<0.084mg/Kg3&4 Methylphenol 59.8 34-119 12.2 20
1.17 70.01.031.671.67<0.144mg/KgNaphthalene 61.6 35-123 12.7 20
1.49 89.21.311.671.67<0.096mg/Kg2-Nitroaniline 78.4 44-127 12.8 20
1.35 80.81.231.671.67<0.120mg/Kg3-Nitroaniline 73.6 33-119 9.3 20
1.34 80.21.191.671.67<0.093mg/Kg4-Nitroaniline 71.2 63-147 11.8 20
Page 19 of 21* QC Fail Date:10/08/2021 04:58 PM
Page 64 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V9595QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V9503
V 96524-MS-V9503 V 96524-MSD-V9503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.24 74.21.071.671.67<0.116mg/KgNitrobenzene 64.0 34-122 14.7 20
1.16 69.40.9871.671.67<0.088mg/Kg2-Nitrophenol 59.1 32-123 16.1 20
1.56 93.41.381.671.67<0.117mg/Kg4-Nitrophenol 82.6 30-132 12.2 20
1.18 70.60.9831.671.67<0.263mg/KgN-Nitrosodimethylamine 58.8 10-146 18.2 30
1.64 98.21.441.671.67<0.181mg/KgN-Nitrosodiphenylamine 86.2 38-127 12.9 20
1.25 74.81.111.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 66.4 36-120 11.8 20
1.79 1071.531.671.67<0.347mg/KgPentachlorophenol 91.6 25-133 15.6 20
1.43 85.61.241.671.67<0.208mg/KgPhenanthrene 74.2 50-121 14.2 20
1.42 85.01.281.671.67<0.112mg/KgPhenol 76.6 34-121 10.3 20
1.44 86.21.301.671.67<0.134mg/KgPyrene 77.8 47-127 10.2 20
0.984 58.90.8301.671.67<0.079mg/KgPyridine 49.7 10-80 16.9 20
1.13 67.60.9741.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 58.3 34-118 14.8 20
1.40 83.81.191.671.67<0.096mg/Kg2,4,5-Trichlorophenol 71.2 41-124 16.2 20
1.37 82.01.261.671.67<0.096mg/Kg2,4,6-Trichlorophenol 75.4 39-126 8.3 20
78.42-Fluorobiphenyl (S)68.8 44-115
78.62-Fluorophenol (S)69.9 35-115
64.6Nitrobenzene-d5 (S)58.6 37-122
76.04-Terphenyl-d14 (S)66.4 54-127
68.72,4,6-Tribromophenol (S)60.3 39-132
72.9Phenol-d5 (S)64.8 34-121
Page 20 of 21Date:10/08/2021 04:58 PM
Page 65 of 68
Quality Control Data
21-272-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
Dry Weight Determination
SW-DRYWT
V9677QC Analytical Batch:
Analysis Method:
Analysis Description:
V 96732-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/04/21 17:212.321.421.9%Moisture
V 96733-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/04/21 17:211.519.219.5%Moisture
Page 21 of 21Date:10/08/2021 04:58 PM
Page 66 of 68
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-272-0017
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 5.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:09/29/2021 15:48:53
Special precautions or instructions included?
Comments:
Page 67 of 68
Page 68 of 68