6004_DukeMcGuire_LF1_REV1_WQMR_Q1_012022_FID1773553_20230216

(' DUKE
ENERGY-.
February 16, 2023
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 28778
Attn: Ms. Sarah Moutos (submitted electronically)
Re: Semi -Annual Water Quality Monitoring Report — January 2022 (Revision 1)
Duke Energy Carolinas, LLC
McGuire Nuclear Station
Landfill No. 1 (Unlined), Permit #60-04
Dear Ms. Moutos:
526 South Church St.
Charlotte, NC 28202
Mailing Address
P.O. Box 1006
Mail Code EC 13K.
Charlotte, NC 28201-1006
Duke Energy is providing a revised semi-annual water quality monitoring report for the January 24-26, 2022,
sampling event conducted at the Duke Energy Carolinas, McGuire, Landfill No. 1 (Unlined), located near
Huntersville, North Carolina.
The original report was dated May 11, 2022. This revision to the report includes updates to Table 4, Table 5,
and Table 6. A revision log is included with a detailed description of the revisions.
The groundwater sampling field and analytical results are summarized in Table 4. The analytical results for
the constituents are compared to the groundwater standards found in Title 15A NCAC 02L .0202 (2L
Standards). Results with values that attain or exceed the 2L Standards (or outside of 2L Standard range for
pH) are indicated on Table 4 by yellow highlighting. A summary of the analytical results that attain or exceed
the 2L Standards (or outside of 2L Standard range for pH) and a preliminary analysis of the cause and
significance of such occurrences are presented in Table 5.
The surface water field and analytical results are summarized in Table 6. The analytical results for the
constituents are compared to the surface water standards found in Title 15A NCAC 02B .0211 (213 Standard)
for Class C WS-IV waters. No 213 Standards were exceeded during the January 2022 monitoring event.
If you need additional information regarding this revised submittal, please contact Ashley Healy at
Ashley.Healy(cDduke-eneray.com or [phone].
Respectfully,
Ashley Healy, P.G.
Environmental Services
Attachments: Semi -Annual Water Quality Monitoring Report (Revision 1) January 2022 Sampling Event —
Duke Energy Carolinas, McGuire, Landfill No. 1 (Unlined) Permit No. 6004
www.duke-energy.com Page 1 of 1

DENR USE ONLY ❑Paper Report ❑Electronic Data -Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
S&ME, Inc. (Consultant for Duke Energy)
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Julie P. Robertson, P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006)
Duke Energy Carolinas, LL 12700 Hagers Ferry Road
CMcGuire, Landfill No. 1 Huntersville, NC 28078 6004-INDUS .0500 June 1 - 2, 2020
(Unlined)
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring �X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
RX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Julie P. Robertson, P.G. Principal Project Mgr/Group Leader 704-523-4726
Facility Representative Name (Print) Title (Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
Signature Date
9751 Southern Pine Blvd., Charlotte, NC 28273
Facility Representative Address
S&ME Engineering License # F-0176, S&ME Geology License # C-145
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

Semi -Annual Water Quality Monitoring Report (Revision 1)
January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1
(Unlined) Permit No. 6004
Mecklenburg County, North Carolina
S&ME Project No. 21350075, Ph. 01

REPORT VERIFICATION
PROJECT: SEMI-ANNUAL WATER QUALITY MONITORING REPORT (Revision 1)
DUKE ENERGY CAROLINAS, McGUIRE, LANDFILL NO. 1
(UNLINED) PERMIT NO. 6004
S&ME PROJECT NO. 21350075, PH. 01
TITLE: JANUARY 2022 SAMPLING EVENT
This document has been reviewed for accuracy and quality commensurate with the intended
application.
Prepared by: Date: 2/13/23 (Original 5/11/22)
Approved by,2/13/23 (Original 5/11/22)
Project Manager: Julie P. Robertson, PG
Licensed Geologist Seal:
��Ry;,s:/ ti Flea;fd�
. __.AL
S&ME, Inc.
2016 Ayrsley Town Blvd., Suite 2-A
Charlotte, North Carolina 28273
North Carolina Geological Corporation Number C-145
S&ME, Inc. 12016 Ayrsley Town Blvd., Suite 2-A I Charlotte, NC 282731 p 704.523.4726 1 www.smeinc.com

REVISION LOG
Semi -Annual Water Quality Monitoring Report
January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No.1
REVISIONDATE
• OF •
0
5/11/2022
Semi -Annual WQMR - January 2022
Initial Issuance to Duke Energy.
Sampling Event
Corrected formatting errors with column
headings, added correct well location
labels to each column, updated notes to
Table 4: Groundwater Field and
reflect current NCAC 2L Standards,
Analytical Results
corrected the order of wells (moved the
MW-4D data column to display before the
MW-4R data column), corrected
significant digits for MDL values of 2-
hexanone, acetone, and carbon disulfide.
Corrected minor formatting errors,
1
2/13/2023
Table 5: Results that Equal or Exceed
corrected the order of wells (moved the
15A NCAC 2L Groundwater Standards
MW-4D data row to display above the
MW-4R data row).
Corrected formatting errors with column
headings, formatted notes and updated to
Table 6: Surface Water Field and
reflect current NCAC 2B Standards,
Analytical Results
updated NCAC 2B Standards for Arsenic
(dissolved), Chromium (total), and Lead
(total).

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1 �R
(Unlined) Permit No. 6004 rt
S&ME Project No. 21350075, Ph. 01 I I
Table of Contents
1.0 Background........................................................................................................................1
1.1 Site Description...............................................................................................................................1
1.2 Hydrologic Setting.........................................................................................................................1
1.3 Monitoring Program......................................................................................................................1
2.0 Methods..............................................................................................................................2
2.1 Sampling and Analysis Methods.................................................................................................2
2.1.1 Groundwater and Surface Water......................................................................................................2
2.1.2 Radiological Samples.........................................................................................................................3
2.2 Statement of Work..........................................................................................................................3
3.0 Results.................................................................................................................................3
3.1 Site Groundwater Flow.................................................................................................................4
3.2 Analytical Results...........................................................................................................................4
3.2.1 Groundwater.....................................................................................................................................4
3.2.2 Surface Water....................................................................................................................................4
3.2.3 Radiological Samples.........................................................................................................................5
3.2.4 Quality Assurance / Quality Control..............................................................................................5
February 13, 2023 (Original Report Date May 11, 2022)

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1
(Unlined) Permit No. 6004
S&ME Project No. 21350075, Ph. 01
Appendices
Appendix I — Figures
Figure 1
Figure 2
Figure 3
Appendix II — Tables
Table 1
Table 2
Table 3
Table 4
Table 5
Table 6
Table 7
Site Location Map
Sample Locations
Shallow Groundwater Contour Map
Well Construction Information
Groundwater Flow Velocities
Field Data Parameters
Groundwater Field and Analytical Results
Results that Equal or Exceed 15A NCAC 2L Groundwater Standards
Surface Water Field and Analytical Results
Radiological Analytical Results
Appendix III — Field Sampling Forms
Appendix IV — Laboratory Reports and Chain -of -Custody Forms
s
0
February 13, 2023 (Original Report Date May 11, 2022)

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1
(Unlined) Permit No. 6004 I s
S&ME Project No. 213S007S, Ph. 01
1.0 Background
1.1 Site Description
The Duke Energy Carolinas, McGuire, Landfill #1 (unlined)' is located at the McGuire Nuclear Station in
Mecklenburg County, North Carolina. The landfill is permitted under North Carolina Department of Environmental
Quality (NCDEQ) Solid Waste Permit No. 6004 and is closed and no longer accepts waste. The landfill and
surrounding area are shown on Figure 1 in Appendix I. The approximate limit of waste is shown on Figures 2
and 3 in Appendix I.
1.2 Hydrologic Setting
The closed landfill is located south of North Carolina (NC) Highway 73, east of the Catawba River, and west of
Cashion Road. Cashion Road runs along a topographic divide with topography sloping away from the road to the
northwest and to the southeast. Surface water northwest of Cashion Road, in the vicinity of the landfill, drains
toward the Catawba River. The Catawba River is classified as a Water Supply -IV water source (WS-IV). There is one
surface water drainage feature north of the landfill that drains northwest to the Catawba River as depicted on
Figure 2 in Appendix I.
1.3 Monitoring Program
As described in the Sampling and Analysis Plan (SAP) dated December 11, 2019, the current monitoring system at
the landfill consists of the following:
Monitoring Wells: MW-1
MW-4D
MW-1 D
MW-4R
MW-2A
MW-4DR
MW-2D
MW-11
MW-3
MW-11 D
MW-3D
MW-12
MW-4
MW-12D
Surface Water Sample Location: SW-1
In response to the North Carolina Division of Public Health, Radiation Protection Section, November 17, 2006
letter to Duke Energy, LLC, Duke Energy offered to indicate the landfill as (unlined) in reports.
February 13, 2023 (Original Report Date May 11, 2022)

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1
(Unlined) Permit No. 6004
S&ME Project No. 21350075, Ph. 01
Monitoring wells were installed as well pairs, consisting of one shallow well and one deep well. Shallow wells were
installed with screened intervals set to bracket the water table at the time of installation. Deep wells were
constructed so that the bottom of the screen is located within residual soils just above auger refusal. Wells with
"D" designations represent the deeper well within each well pair. Wells with "R" designations are replacement
wellsz.
Surface water sample location SW-1 is collected from the unnamed stream (north of the landfill), upstream of the
confluence with the surface water drainage feature that ultimately discharges to the Catawba River. SW-1 is the
designated background sampling location for this monitoring program.
The monitoring wells and the surface water sample location are shown on Figure 2 in Appendix I. Well
construction information for the landfill monitoring wells is presented in Table 1 in Appendix II.
2.0 Methods
2.1 Sampling and Analysis Methods
Groundwater and surface water sampling activities were performed by Duke Energy Groundwater Science Group
(Duke Energy Carolinas Field Certification #99046001), in general accordance with the North Carolina Solid Waste
Management Guidelines. Copies of the January 2022 field sampling forms are included in Appendix III. The
parameters and constituents reported were selected in accordance with the SAP and the NCDEQ Division of Waste
Management, Solid Waste Section Guidelines. Groundwater and surface water samples were analyzed by the Duke
Energy Analytical Laboratory (North Carolina Laboratory Certification #248), Pace Analytical Services (North
Carolina Laboratory Certification #329), and EnRad Laboratories. The laboratory reports and chain -of -custody
forms are included in Appendix IV.
2.1.1 Groundwater and Surface Water
The groundwater and surface water samples were analyzed for the following parameters using the following
analytical methods in accordance with the SAP:
• Barium, calcium, magnesium, potassium, and sodium using Solid Waste (SW)-846 Method 6010D
• Arsenic, cadmium, chromium, lead, selenium, and silver using SW-846 Method 6020B
• Mercury using SW-846 Method 7470A
Z Please note that monitoring wells MW-4R and MW-4DR were installed in December 2013 to replace wells MW-4
and MW-4D, which are approximately 15 feet outside of the waste boundary and near the review boundary. At the
request of the NCDEQ Solid Waste Section, wells MW-4 and MW-4D continue to be sampled even though
replacement wells have been installed.
February 13, 2023 (Original Report Date May 11, 2022)

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1
(Unlined) Permit No. 6004
S&ME Project No. 21350075, Ph. 01
• Sulfate and Chloride using SW-846 Method 9056A
• Alkalinity using Method SM2320B
• Volatile organic compounds (VOCs) using SW-846 Method 8260
The surface water sample was also field -filtered using a 0.45-micron in -line filter and dissolved analyses were
performed for the following constituents:
• Barium using SW-846 Method 6010D
• Arsenic, cadmium, chromium, lead, and silver using SW-846 Method 6020B
2.1.2 Radiological Samples
In accordance with the requirements of the Radioactive Materials License No. 060-0379-7 issued by the North
Carolina Department of Health and Human Services Radiation Protection Section, the following radiological
analyses were performed on groundwater and surface water samples:
• Gross alpha and beta radioactivity using EPA Method 900
• Tritium using EPA Method 906.0 Modified
• Gamma radioactivity for select isotopes
2.2 Statement of Work
S&ME completed the following tasks:
Received field sampling data from Duke Energy (performed by Duke Energy Groundwater Sciences Group)
for monitoring wells MW-1, MW-1 D, MW-2A, MW-2D, MW-3, MW-3D, MW-4, MW-4D, MW-4R, MW-
4DR, MW-11, MW-11 D, MW-12, and MW12D. Data was also received for surface water sample location
SW-1. The samples were collected between January 24t" and 261", 2022, and S&ME received the data
from Duke Energy via e-mail correspondence from Ashley Healy (Duke Energy) to Julie Robertson and Erin
Kinsey (S&ME) on April 511, 2022.
• Reviewed the laboratory analytical results and the Electronic Data Deliverables (EDDs) provided by Duke
Energy for the samples noted above.
• Developed a shallow groundwater contour map and calculated groundwater flow velocities using survey
data and groundwater levels measured by Duke Energy Groundwater Sciences Group.
February 13, 2023 (Original Report Date May 11, 2022)

Semi -Annual Water Quality Monitoring Report (Revision 1) - January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1 �R
(Unlined) Permit No. 6004
S&ME Project No. 21350075, Ph. 01 '-
3.0 Results
3.1 Site Groundwater Flow
Shallow groundwater surface contours and groundwater flow direction in the vicinity of the landfill are shown on
Figure 3 in Appendix I. These contours were developed using the depth to groundwater measurements in the
shallow wells3 on the date of sampling and top of well casing elevations. Calculated groundwater flow velocities
are presented on Table 2 in Appendix II.
Based on groundwater elevations calculated for the January 2022 sampling event, groundwater flow is generally
from the southeast to the north and northwest toward MW-3, MW-4, and MW-4R.
3.2 Analytical Results
3.2.1 Groundwater
Laboratory results for groundwater samples were compared to the Title 15A NCAC Subchapter 2L Standards (2L
Standards) to evaluate compliance with NCDEQ groundwater quality standards. Concentrations greater than the
2L Standards were reported in one or more wells for the following constituents: pH, methylene chloride,
tetrachloroethylene (PCE), trichloroethene (TCE), and vinyl chloride. The concentrations greater than the standard,
with the exception of pH, were detected in MW-4, MW-4D, and MW-4R which are located proximate to the landfill
waste boundary.
A summary of field data parameters recorded prior to sample collection is presented in Table 3 in Appendix II. A
summary of groundwater analytical results for the current sampling event is presented in Table 4 in Appendix II.
A summary of the groundwater analytical results that equal or exceed the 2L Standards and a comparison to
historical concentration ranges are presented in Table 5 in Appendix II.
3.2.2 Surface Water
Laboratory results for the surface water sample (SW-1) were compared to the Title 15A NCAC Subchapter 2B
Standards (2B Standards) for Class WS-IV waters to evaluate compliance with established criteria. No constituents
exceeded 2B Standards in the surface water sample collected during the January 2022 sampling event. A summary
of field data parameters recorded prior to sample collection is presented in Table 3 in Appendix II. A summary of
surface water analytical results for the January 2022 sampling event is presented in Table 6 in Appendix II.
3 Please note that periodically shallow monitoring well MW-12 is not used to produce groundwater contours.
Historically, MW-12 has experienced water level elevation fluctuations not typical of normal seasonal variations.
Duke Energy is currently evaluating the water level data and the need for future abandonment and replacement.
February 13, 2023 (Original Report Date May 11, 2022) 4

Semi -Annual Water Quality Monitoring Report (Revision 1) — January 2022 Sampling Event
Duke Energy Carolinas, McGuire, Landfill No. 1 �R "
(Unlined) Permit No. 6004
S&ME Project No. 21350075, Ph. 01
3.2.3 Radiological Samples
The results of the radiological analyses are presented in Table 7 in Appendix II. A copy of the laboratory report
has been submitted to the North Carolina Department of Health and Human Services Radiation Protection Section
for reference and is also included in this report in Appendix IV. S&ME did not evaluate this data.
3.2.4 Quality Assurance / Quality Control
Field -performed quality assurance and quality control (QA/QC) consisted of the collection and analysis of four
field blanks (one each on January 24t" and 251", and two on January 261") to evaluate if contamination was
imparted to the samples by the sample container, preservative, or other exogenous sources. Samples for the
monitoring wells and surface water were submitted to the Duke Energy Analytical Laboratories on January 27tn
2-Butanone, Acetone, and Ethylbenzene were detected in the field blank collected on January 24t". 2-Hexanone
and Acetone were detected in the field blank collected on January 25t". 2-Butanone, 2-Hexanone and Acetone can
be laboratory artifacts and were not detected in the monitoring wells or surface water sample at concentrations
above the laboratory Method Reporting Limit (MRL).
Two field duplicate samples were collected on January 25' and 261" to estimate sampling and laboratory
precision. No constituents were detected in the field duplicate sampled collected on January 25tn
Two Trip Blanks were transported with the VOC samples to evaluate the effects of shipping and laboratory sources
of contamination. 2-Hexanone and Acetone were detected in the trip blank collected on January 24t". No other
constituents were detected at concentrations above the laboratory Method Detection Limit (MDL) in either of the
trip blank samples. As stated previously, 2-Hexanone and Acetone can be laboratory artifacts and were not
detected in the monitoring wells or surface water sample at concentrations above the laboratory Method
Reporting Limit (MRL).
Select samples were diluted, as is normal laboratory practice, to bring samples within the calibrated range of the
analysis. Specifics regarding the samples that were diluted, including the dilution amount, are reported in the lab
report. Additional QA/QC data, laboratory analyses, and chain -of -custody forms are included in Appendix IV.
February 13, 2023 (Original Report Date May 11, 2022)

Appendices

Appendix I - Figures

_yw
(01 670.46'00*1
s
.,;
MW-4* (. ' "f%W-4 ems/
000,
677' !_e 675.12' 00
0O t
e\vooay--- MW-
Q 2A',
-
e 6 687.72'
,Olee
e0000
e i LANDFILL
NO. �/ 1
e
o
0 0 0
• �_.. QMW-1'1 I
0� 691.18' MW-1
,,e ®�o
700.480000
SEE NOTES O /
1000,
1001,
still,
0 nI-_,
'►' e -' _ .
NOTES: d
- a
MW-12 JANUARY 2022 GROUNDWATER ELEVATION (REPORTED AS 714.26') WAS NOT USED TO
0 200 400 � n
GENERATE SHALLOW GROUNDWATER CONTOURS.
GIS BASE LAYERS WERE OBTAINED FROM THE OWNER AND NC ONE MAP. THIS MAP IS FOR
INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY GRAPHIC SCALE (IN FEET) ym
ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
y r ,•,
• y.� w�� w� w I
j
LEGEND
0 SHALLOW GROUNDWATER MONITORING LOCATION
0 -►-►STREAMS WITH FLOW DIRECTION
-► GROUNDWATER FLOW
• GROUNDWATER CONTOUR - JANUARY 2022
LANDFILL NO. 1 COMPLIANCE BOUNDARY
LANDFILL NO. 1 LIMITS OF WASTE
LANDFILL NO. 1 REVIEW BOUNDARY
DUKE ENERGY PROPERTY BOUNDARY
STREETS
2' CONTOURS
10' CONTOURS
0
zz
LZ
w z
U � z
w �°
oQ
z V
J
J �
Q o p
Z z z
o Q�
wz
z
C7 o
V
z z
J J
Cn < V
N w
V �
O �
SCALE:
1=200'
DATE:
5-4-2022
PROJECT NUMBER:
21350075, PH. 01
FIGURE NO
c

Appendix II - Tables

Table 1: Well Construction Information
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station
S&ME Project No: 21350075, Ph. 01
MW-1
Install Date
..
07/18/89
Coordinates
LongitudeGround
Latitude
35.41146' 80.94761°
Survey Elevations
729.58 730.23
Well
Stick-up
Height
Above
Surface
0.65
January 24-26, 2022
DTW - TOC GW ELEV.
29.75 700.48
Total Well
Depth
Below
Top of
Casing
68.55
Screen Interval
i .010 Slot, Sch. 40
•
58.55 to 68.55
Geology in
Screen
Interval
SAP
Well
Diameter
2
Casing
TypeGPS
PVC
MW-1 D
07/20/89
35.41147'
-80.94760'
729.75
730.61
0.86
30.79
699.82
88.22
78.22
to 88.22
SAP
2
PVC
MW-2A
07/21/89
35.41306°
-80.94905'
736.96
739.67
2.71
51.95
687.72
77.57
67.57
to
77.57
SAP
2
PVC
MW-2D
07/20/89
35.41308°
-80.94909'
737.41
740.77
3.36
53.52
687.25
108.82
98.82
to
108.82
PWR
2
PVC
MW-3
1 07/10/89
35.41407'
-80.95049'
724.98
728.43
3.45
57.97
670.46
73.64
63.64
to
73.64
SAP
2
PVC
MW-3D
07/10/89
35.41407'
-80.95050'
724.98
728.39
3.41
57.75
670.64
90.19
80.19
to
90.19
PWR
2
PVC
MW-4
07/06/89
35.41349'
-80.95115'
738.40
741.13
2.73
66.01
675.12
74.15
64.15
to
74.15
SAP
2
PVC
MW-4D
07/06/89
35.41348'
-80.95117'
738.25
740.58
2.33
66.25
674.33
102.24
92.24
to
102.24
SAP/PWR
2
PVC
MW-4R
12/04/13
35.41341°
-80.95161'
711.15
713.87
2.72
41.20
672.67
45.73
30.73
to 45.73
SAP
2
PVC
MW-4DR
12/04/13
35.41340'
-80.95162'
711.15
713.75
2.60
40.81
672.94
90.40
75.40
to 90.40
SAP
2
PVC
MW-11
12/15/04
35.41138'
-80.95050'
720.10
722.60
2.50
31.42
691.18
38.45
23.45
to 38.45
SAP
2
PVC
MW-11 D
12/15/04
35.41139°
-80.95047'
720.84
723.14
2.30
32.58
690.56
101.55
91.55
to
101.55
SAP
2
PVC
MW-12
12/15/04
35.41100°
-80.94917°
722.21
724.81
2.60
10.55
714.26
29.49
14.49
to
29.49
SAP
2
PVC
MW-12D
12/15/04
35.41101°
-80.94921'
722.21
724.77
2.56
27.12
697.65
68.42
58.42
1 to
68.42
PWR
2
PVC
Notes:
(1)
0.010 Slot
0.010-Inch Machine -Slotted Pipe
(2)
DTW
Depth to Water
(3)
Ground
Ground Surface
(4)
GW ELEV.
Groundwater Elevation
(5)
PVC
Polyvinyl Chloride
(6)
PWR
Partially Weathered Rock
(7)
TOC
Top of Casing
(8)
SAP
Saprolite
(9)
Sch. 40
Schedule 40 Pipe
(10) Total well depths from 2015 well depth confirmation
(11) Elevations based on NAVD88 vertical datum.
(12) Horizontal coordinates based on NAD83 datum.
(13) Top of casing and ground surface elevations from Jan 2015 re -survey by Providence Land Group.

Table 2: Groundwater Flow Velocities
Landfill No. 1 (Unlined) Permit No. 6004-INDUS n
Duke Energy Carolinas McGuire Nuclear Station I I 1
S&ME Project No: 21350075, Ph. 01
Notes•
(1) Hydraulic gradient calculated by measuring linear distance through monitoring wells (generally perpendicular) from selected
groundwater contours.
(2) Hydraulic gradients and groundwater velocities are approximate.
(3) Hydraulic Conductivity and effective porosity are mean values for soil/saprolite taken from "Groundwater Protection Initiative Site
Characterization Report" for McGuire Nuclear Station dated June 30, 2008 by S&ME, Inc.
(4) Seepage velocity equation used to calculate groundwater flow velocity v = (K*i)/ne

Table 3: Field Data Parameters
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station
S&ME Project No: 21350075, Ph. 01
tAn- 3
III
Well ID
MW-1
Date
1/25/2022
Well
Depth
Below
•
68.55
Depth to
Water
Below •
29.75
Groundwater
Elevation
700.48
Appearance
Normal
Odor
None
Purge
..
LF
Average
Pump Rate
440
Well
Volume
6.33
EVAC
Volume
4.55
EVAC
No
Temperature
16.17
Specific
Conductivity
114
PH
6.11
Turbidity
9.8
ORP
239
Dissolved
Oxygen
0.68
MW-1 D
1/25/2022
88.22
30.79
699.82
Normal
None
LF
360
9.37
1.60
No
16.12
105
6.15
9.3
251
0.87
MW-2A
1/25/2022
77.57
51.95
687.72
Normal
None
LF
240
4.18
3.40
No
17.21
124
6.50
1.5
384
6.31
MW-2D
1/25/2022
108.82
53.52
687.25
Normal
None
EOP
NA
9.02
0.75
No
19.46
60
6.87
3.5
367
9.23
MW-3
1/26/2022
73.64
57.97
670.46
Normal
None
LF
330
2.56
3.05
No
14.81
74
6.27
1.0
399
5.48
MW-3D
1/26/2022
90.19
57.75
670.64
Normal
None
LF
420
5.29
2.70
No
15.01
152
6.55
1.0
253
3.18
MW-4
1/26/2022
74.15
66.01
675.12
Normal
None
EOP
NA
1.33
0.55
No
12.81
72
6.06
0.7
376
3.90
MW-41D
1/26/2022
102.24
66.25
674.33
Normal
None
LF
200
5.87
1.85
No
14.70
160
5.58
1.6
255
0.51
MW-4R
1/26/2022
45.73
41.20
672.67
Normal
None
EOP
NA
0.74
0.39
No
12.46
73
5.73
8.8
319
2.78
MW-4DR
1/26/2022
90.40
40.81
672.94
Normal
None
LF
210
8.09
2.25
No
11.66
81
6.09
0.8
356
2.98
MW-11
1/24/2022
38.45
31.42
691.18
Normal
None
EOP
NA
1.15
0.35
No
13.60
138
6.24
9.0
188
1.27
MW-11 D
1/24/2022
101.55
32.58
690.56
Normal
None
LF
400
11.25
11.50
No
13.68
32
5.80
44.3
378
7.15
MW-12
1/24/2022
29.49
10.55
714.26
Normal
None
LF
220
3.09
1.55
No
14.16
26
5.08
7.7
422
7.91
MW-12D
1/24/2022
68.42
27.12
697.65
Normal
None
LF
240
6.74
1.90
No
14.65
91
6.35
5.4
346
7.72
SW-1
1 1/25/20221
NA
I NA
I NA
I Normal
I None
I SWS
I NA
I NA
I NA
I NA
1 12.79
1 93
1 6.92
1 19.2
1 268
1 8.85
Notes•
(1)
°C
degrees Celsius
(2)
ft
feet
(3)
gal
gallons
(4)
µu/cm
micromhos per centimeter
(5)
mg/L
milligrams per liter
(6)
mL/min
milliliters per minute
(7)
mV-NHE
millivolts - normal hydrogen electrode
(8)
NA
not applicable
(9)
NTU
nephelometric turbidity unit
(10)
SU
standard units
(11)
TOC
top of casing
(12) Elevations based on NAVD88 vertical datum
(13) Purge methods: LF = Low Flow (average pump rate applicable to LF purging only); EOP = Equipment Only Purge; SWS = Surface Water Sample.
(14) EVAC indicates whether the water level in the well was drawn down to the level of the pump during purging and also the total amount purged from the well.
(15) Field sampling performed by Duke Energy Groundwater Science Group.

Table 4: Groundwater Field and Analytical Results
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station
S&ME Project No: 21350075, Ph. 01
Field Parameter
Field pH
Units
SU
MW-1
6.11
MW-111)
6.15
MW-2A
6.50
JUNION
6.87
6.27
6.55
6.06
rW-4D
5.58
=MW4R
5.73
=MW4DR
6.09
WMW11
6.24
MW-11D
5.80
MW-12
5.08
MW-12D
6.35
MDL
- - -
SWS
Groundwater
Protection
Standard
NE
15A NCAC
21.
Standard
6.5 - 8.5
Federal
MCL
6.5 - 8.5*
Specific Conductance
µu/cm
114
105
124
60.0
74.0
152
72.0
160.0
73.0
81.0
138
32.0
26.0
91.0
- - -
NE
NE
NE
Temperature
°C
16.17
16.12
17.21
1 19.46
14.81
15.01
12..91
14.70
12.46
11.66
13.60
13.68
14.16
14.65
- - -
NE
NE
NE
EPA Appendix I Volatile Organic Compounds Method
1,1-Dichloroethane
8260B
pg/L
and 8260B
0.40 U
SIM
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
6
NE
1,4-Dioxane
pg/L
1.0U
1.0U
1.0U
1.0U
1.0U
1.0U
1.0U
1.2J
2.2J
1.0U
1.0U
1.0U
1.0U
1.0U
1.0
NE
3
NE
cis-1,2,-Dichloroethylene
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
3.5
0.40 U
25
33
0.78 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
70
NE
2-Hexanone
pg/L
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0
NE
40
NE
Acetone
pg/L
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0U
5.0
NE
6000
NE
Benzene
pg/L
0.40 U
1 0.40 U
0.40 U
0.40 U
0.40 U
0.39 J
0.40 U
0.60 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
1
NE
Carbon Disulfide
pg/L
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0U
2.0
NE
700
NE
Methylene Chloride
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
2.7 J
0.40 U
6.5
2.0 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
5
NE
Tetrachloroethylene
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.48 J
1.3
1.0
0.91 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
0.7
NE
Toluene
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.51 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
600
NE
Trichloroethylene
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
1.3
0.40 U
4.7
0.53 J
0.56 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
3
NE
Vinyl Chloride
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.72 J
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40
NE
0.03
NE
Xylenes (total)
pg/L
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.44 J
0.40 U
11
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0.40 U
0A0
NE
500
NE
Mercury pg/L 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01U 0.01 NE 1.0 NE
Alkalinity(CaCO3) pg/L 53000 49000 74000 24500 36000 73000 69000 130000 66000 69000 49200 11300 2320J 39000 1700 NE NE NE
Chloride
pg/7
2100
2100
1300
1200
1200
1500
2900
1900
2800
1700
2200
1300
4100
3500
15.4
NE
250000
250000'
Sulfate
pg/L
330
400
680
360
560
740
700
310
250
920
890
580
350
80.0J
42.8
NE
250000
250000'
Arsenic
pg/L
0.138 J
0.180 J
0.111 U
0.111 U
0.111 U
0.111 U
0.111 U
0.164 J
0.111 U
0.111 U
0.438 J
0.111 U
0.111 U
0.111 U
0.111
NE
10
10
Cadmium
pg/L
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032 U
0.032
NE
2
5
Chromium
pg/L
0.214 J
0.240 J
0.860 J
1.26
0.397 J
0.625 J
1.11
0.232 J
0.897 J
1.53
0.326 J
0.810 J
0.287 J
0.394 J
0.185
NE
10
100
Lead
pg/L
0.052 J
0.037 U
1.39
0.138 J
3.61
0.039 J
0.037 U
0.037 U
0.070 J
0.197 J
0.088 J
0.350 J
0.156 J
0.053 J
0.037
NE
15
15
Selenium
pg/L
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193 U
0.193
NE
20
50
Silver
pg/L
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035 U
0.035
NE
20
100*
Total Recoverable Metals Method SW 0.
Barium
pg/L
227
107
52.0
14.0
44.0
36.0
67.0
51.0
10.0
15.0
11.0
33.0
11.0
10.0
2
NE
700
2000
Calcium
pg/L
7400
7690
1870
5130
6770
16600
11000
27300
12100
15800
3310
2010
1140
9130
12
NE
NE
NE
Magnesium
pg/L
3250
2600
4920
1480
2830
5310
10700
13500
8980
4720
3110
1430
558
1340
8
NE
NE
NE
Potassium
pg/L
1640
1100
1910
427
2010
990
454
763
346
758
312
379
421
321
31
NE
NE
NE
Sodium
pg/L
6360
6450
7790
5090
3980
6820
2130
4420
2830
6900
6100
3270
184
7500
17
NE
NE
NE
Notes.•
(1) Samples were collected by Duke Energy Groundwater Sciences Group.
(2) MDL refers to the laboratory Method Detection Limit.
(3) SWS Groundwater Protection Standard (GWPS) refers to the North Carolina Groundwater Protected Standards calculated by North Carolina Department of Environmental
Quality (NCDEQ), Solid Waste Section (SWS) for constituents with no established 15A NCAC 2L Standard (last amended on October 15, 2018).
(4) 15A NCAC 2L Standard refers to Class GA Standards as found in 15A NCAC 02L .0202 Groundwater Quality Standards (last amended on April 1, 2022).
(5) Federal Maximum Contaminant Level (MCL) as found in National Primary Drinking Water Regulations, 40 CFR, Subpart G, §141.62.
(6) * Concentration listed is a secondary MCL (MCL) as found in National Secondary Drinking Water Regulations, 40 CFR, Subpart A, §143.3.
(7) NE = Not Established.
(8) Yellow highlighted cells indicate concentrations equal to or greater than the 15A NCAC 2L Standard (for pH yellow highlighting indicates a measurement outside the 15A NCAC
(9) Bolded values indicate concentrations equal to or greater than the Federal MCL (for PH bolded values indicate a measurement outside of the Federal MCL range).
(10) J = estimated concentrations which are greater than the MDL but are less than the laboratory Method Reporting Limit (MRL).
(11) U = constituent detected at or below the laboratory MDL.
(12) SU = Standard Units.
03) µiS/cm = micromhos per centimeter.
(14) °C = degrees Celsius.
(15) µg/L = micrograms per liter.

Table 5: Results that Equal or Exceed 15A NCAC 2L Groundwater Standards
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station
S&ME Project No: 21350075, Ph. 01
Notes:
(1) SU = Standard units.
(2) 15A NCAC 2L Standard refers to Class GA Standards as found in 15A NCAC 02L .0202 Groundwater Quality Standards (last amended on April 1, 2022).
(3) J = estimated concentrations which are greater than the laboratory method detection limit (MDL), but less than the laboratory method reporting limit (MRL).
(4) Historical results based on data in Duke Energy Carolinas, LLC (Duke Energy) analytical results database.
(5) Ng/L = micrograms per liter.

Table 6: Surface Water Field and Analytical Results
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station I I
S&ME Project No: 21350075, Ph. 01
January 2022 MDL 15A NCAC Federal MCL
Field Parameters Units d1hoffig-J... AL 2B
Field pH SU 6.92 1 - - 6.0 - 9.0 6.5 - 8.5*
Specific Conductance µu/cm 93 NE NE
Temperature °C 12.79 1 NE NE
• 0: 0:
Volatile organic compounds were not detected in January 2022
Alkalinity (CaCo3) µg/L 41000 1700 NE NE
Chloride
µg/L
3100
15.4
250000 250000*
Sulfate
µg/L
2200
42.8
250000 250000*
Mercu µg/L 0.01 U
0.01 0.012
2
Arsenic
µg/L
0.114 J
0.111
10
10
Arsenic, dissolved
µg/L
0.154 J
0.111
150
10
Cadmium
µg/L
0.032 U
0.032
NE
5
Chromium
µg/L
0.185 U
0.185
183A
100
Lead
µg/L
0.037 U
0.037
14A
15
Lead, dissolved
ITotal Recoverable Metals Method SW i 0D
Barium
1µg/L
µg/L
0.195 J
25
0.037
2
0.54A
1000
15
2000
Barium, dissolved
µg/L
25
2
NE
NE
Calcium
µg/L
8610
12
NE
NE
Magnesium
µg/L
3470
8
NE
NE
Potassium
µg/L
1040
31
NE
NE
Sodium
µg/L
1 5210
17
1 NE
NE
Notes:
(1) Yellow highlighted cells indicate concentrations equal to or greater than the 15A NCAC 2B Standard (for pH
highlighting indicates a measurement outside the range).
(2) Bolded values indicate concentrations equal to or greater than the MCL (for PH bold indicates a measurement
outside of the range)
(3) Samples were collected by Duke Energy Groundwater Sciences Group.
(4) MDL is the laboratory Method Detection Limit. The MDL values presented are for samples not diluted by the laboratory
during analysis.
(5) 15A NCAC 2B Standard (last amended on July 26, 2021) refers to 15A NCAC 02B 0.0211 Fresh Surface Water Quality
Standards for Class C Waters, and 15A NCAC 02B 0.0216 - Fresh Surface Water Quality Standards for Class WS-IV Waters.
(6) MCL is the Federal Maximum Contaminant Level as found in 40 CFR, Subpart G §141.62.
(7) * Concentration listed is a secondary MCL (SMCL); SMCLs are established by EPA in the National Secondary Drinking
Water Regulations as found in 40 CFR §143.3.
(8) NE = not established
(9) °C = degrees Celsius
(10) J = estimated concentrations which are greater than the MDL but are less than the laboratory Method Reporting Limit
(M RL).
(11) U = concentrations less than or equal to the laboratory's MDL.
(13) SU = Standard Units
(14) µU/cm = micromhos per centimeter
(15) µg/L = micrograms per liter
(16) A = Hardness -dependent 15A NCAC 2B Standards derived using equations specified in the 15 NCAC 02B Standards
Table (last amended on July 26, 2021). The values shown rely upon an assumed in -stream default hardness of 25
milligrams per liter (mg/L) for the chronic standard. An exceedance of the criterion shown does not establish that an in -
stream exceedance has occurred.

Table 7: Radiological Analytical Results
Landfill No. 1 (Unlined) Permit No. 6004-INDUS
Duke Energy Carolinas McGuire Nuclear Station
S&ME Project No: 21350075, Ph. 01
=0
Measured in
Liter (pCi/Q
Alpha
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
5.30E-01
<
.R
5.30E-01
<
5.00E-01
<
-5.00E-01
<
5.00E-01
<
5.00E-01
<
5.00E-01
Ba-La-140
<
6.63E+00
<
8.14E+00
<
5.88E+00
<
4.13E+00
<
5.57E+00
<
4.86E+00
<
8.97E+00
<
9.64E+00
<
8.77E+00
<
6.29E+00
<
6.24E+00
<
8.43E+00
<
7.78E+00
<
9.54E+00
<
8.38E+00
Be-7
<
5.73E+01
<
5.23E+01
<
5.49E+01
<
3.38E+01
<
5.26E+01
<
4.55E+01
<
5.06E+01
<
4.01 E+01
<
5.88E+01
<
4.80E+01
<
5.25E+01
<
4.08E+01
<
5.53E+01
<
4.59E+01
<
4.48E+01
Beta
4.75E+00
<
3.22E+00
<
3.22E+00
<
3.22E+00
3.24E+00
<
3.22E+00
<
3.22E+00
<
3.22E+00
<
3.22E+00
<
3.22E+00
<
3.19E+00
<
3.19E+00
<
3.19E+00
<
3.19E+00
<
3.19E+00
Co-58
<
6.78E+00
<
6.82E+00
<
4.83E+00
<
5.19E+00
<
6.16E+00
<
5.97E+00
<
5.13E+00
<
5.75E+00
<
5.50E+00
<
5.84E+00
<
4.88E+00
<
5.02E+00
<
5.59E+00
<
6.15E+00
<
6.17E+00
Co-60
<
8.18E+00
<
6.20E+00
<
5.41 E+00
<
6.00E+00
<
5.58E+00
<
6.31 E+00
<
4.41 E+00
<
5.54E+00
<
5.50E+00
<
5.90E+00
<
6.55E+00
<
3.13E+00
<
5.57E+00
<
6.51 E+00
<
7.05E+00
Cs-134
<
8.17E+00
<
8.04E+00
<
5.69E+00
<
6.55E+00
<
7.20E+00
<
6.91 E+00
<
7.39E+00
<
7.53E+00
<
5.79E+00
<
7.23E+00
<
6.16E+00
<
5.34E+00
<
6.78E+00
<
7.05E+00
<
7.16E+00
Cs-137
<
7.39E+00
<
7.27E+00
<
5.36E+00
<
4.14E+00
<
6.95E+00
<
6.23E+00
<
5.27E+00
<
6.71 E+00
<
7.66E+00
<
6.93E+00
<
5.55E+00
<
5.12E+00
<
6.32E+00
<
5.64E+00
<
6.55E+00
Fe-59
<
1.39E+01
<
1.39E+01
<
1.13E+01
<
1.12E+01
<
1.13E+01
<
1.13E+01
<
1.28E+01
<
9.29E+00
<
1.27E+01
<
1.31 E+01
<
1.15E+01
<
1.02E+01
<
1.14E+01
<
1.09E+01
<
8.76E+00
1-131
<
7.52E+00
<
7.32E+00
<
6.09E+00
<
5.70E+00
<
7.53E+00
<
5.84E+00
<
6.40E+00
<
6.35E+00
<
6.07E+00
<
5.91 E+00
<
6.81 E+00
<
7.49E+00
<
8.06E+00
<
6.76E+00
<
6.19E+00
K-40
1.53E+02
6.20E+01
1.59E+02
9.51 E+01
1.74E+02
2.27E+02
<
1.12E+02
<
1.26E+02
2.02E+02
1.66E+02
1.22E+02
<
8.31 E+01
2.65E+02
1.16E+02
<
1.18E+02
Mn-54
<
7.68E+00
<
7.00E+00
<
5.84E+00
<
4.49E+00
<
6.70E+00
<
6.43E+00
<
5.38E+00
<
5.61 E+00
<
6.30E+00
<
6.90E+00
<
5.86E+00
<
6.03E+00
<
5.68E+00
<
6.60E+00
<
5.62E+00
Nb-95
<
7.30E+00
<
6.32E+00
<
5.49E+00
<
5.65E+00
<
7.82E+00
<
6.49E+00
<
5.96E+00
<
7.24E+00
<
4.69E+00
<
5.79E+00
<
4.32E+00
<
6.49E+00
<
6.69E+00
<
5.87E+00
<
6.65E+00
Tritium (H3GW)
<
-2.60E+01
<
3.03E+01
<
-2.80E+01
<
-5.90E+01
<
-6.30E+01
<
-1.90E+01
<
-2.80E+01
<
-1.10E+02
<
3.49E+01
<
-9.80E+01
<
-1.90E+01
<
-4.90E+01
<
-4.70E+00
<
-6.30E+01
<
-7.00E+00
Zn-65
<
1.29E+01
<
1.21E+01
<
1.15E+01
<
1.18E+01
<
1.19E+01
<
1.07E+01
<
1.53E+01
<
1.05E+01
<
1.39E+01
<
1.33E+01
<
1.27E+01
<
1.46E+01
<
1.22E+01
<
1.54E+01
<
1.40E+01
Zr-95
<
1.12E+01
<
1.19E+01
<
7.56E+00
<
1.11E+01
<
1.19E+01
<
1.19E+01
<
8.90E+00
<
9.29E+00
<
1.17E+01
<
1.07E+01
<
7.19E+00
<
1.02E+01
<
1.18E+01
<
9.44E+00
<
1.04E+01
Notes:
(1) pCi/L = picocuries per liter
(2) < = less than

Appendix III - Field Sampling Forms

FIELD SAMPLING CALIBRATION FORM
STUDY:
MCGUIRE NUCLEAR STATION - NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
DATE (s):
January 24-26, 2022
SURFACE UNIT READER: EHS
COLLECTORS: EHS
SURFACE UNIT SERIAL #: 950
ANALYZER MODEL#: ST MP
ANALYZER SERIAL #: 767668
OTHER EQUIPMENT: TURBIDIMETER NO.3 - WR-00070
WEATHER CONDITIONS:
30s-40s, sunny
EHS 1/27/22
HYDROLAB PROCEDURE #:
3210.7
VALIDATED BY:
Calibration Date / Time
DATE:
24-Jan-22
TIME:
7:00
DATE:
25-Jan-22
TIME:
7:00
CALIBRATION BP (mmHg)
733.32
CALIBRATION BP (mmHg)
736.57
Calibation
Instrument
Standard
Instrument
Standard
Parameter
Calibration Results
Calibration Results
Standard
Value
Value
Value
Value
SS
0.0 -►
0.0
INSTRUMENT ZEROED
0.0 -/-►
0.0
INSTRUMENT ZEROED
SPEC. COND.
SS
710.3 -►
720
CALIBRATION ACCEPTED
1 732.1 -/-►
720
CALIBRATION ACCEPTED
(US/cm)
SS
226.8 -/-►
227
CALIBRATION ACCEPTED
228.1 -/-►
227
CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
SS
-/-►
1410
-/-►
1410
CHECK (uS/cm)
SS
B (7.00)
7.08 -►
7.04
CALIBRATION ACCEPTED
7.05 -/-►
7.04
CALIBRATION ACCEPTED
pH
B (4.00)
4.05 -►
3.99
CALIBRATION ACCEPTED
4.00 -/-►
3.99
CALIBRATION ACCEPTED
(units)
B (10.00)
10.13 -/-►
10.09
CALIBRATION ACCEPTED
10.09 -/-►
10.09
CALIBRATION ACCEPTED
Buffer Temp.
16.68
Buffer Temp.
16.70
pH Check
B (7.00)
-►
Buffer Temp.
7.13
0.00
Time:
448 -►
449
CALIBRATION ACCEPTED
448.0 -/-►
449
CALIBRATION ACCEPTED
ORP
N/A -/-►
N/A
N/A -/-►
N/A
Zobell's
ORP Temp.
16.68
ORP Temp.
16.68
0
TEMP (C°)
16.72
16.66
BP (mmHg)
733.32
736.57
COND
0.00
0.00
DO
100 % mg/L
9.41 -►
9.37
CALIBRATION ACCEPTED
9.32 -/-►
9.43
CALIBRATION ACCEPTED
(mg/L)
After Cal
9.38
100.06
After Cal % SAT
9.32
98.85
After Cal % SAT
LCS
9.38
100.06
CALIBRATION PASS
9.32
98.85
CALIBRATION PASS
LCSD
9.38
0.00
CALIBRATION PASS
9.32
0.00
CALIBRATION PASS
OTURB
(UR
ntuTemp
SS
10.0 -/-►
10.0
CALIBRATION ACCEPTED
10.0 -/-►
10.0
CALIBRATION ACCEPTED
Cert Device #
TEMP
NIST
N/A -/-►
N/A
Adjustment Not Available
N/A -/-►
N/A
Adjustment Not Available
(deg C)
INSTRUMENT MAINTENANCE
DATE / TIME
Conductance Subsystem
pH Subsystem
❑
Cleaned Electrodes
❑
Cleaned Electrodes
❑
Tested - OK
❑
Replaced ref Electrode KCL
❑
See Notes
❑
Replaced Ref. Electrode Tip
❑
Tested - OK
❑ See Notes
Oxidation Reduction Subsystem
Temperature Subsystem
❑
Cleaned Electrode
❑
Cleaned Electrode
❑
Tested - OK ❑
See Notes
❑
Tested - OK ❑ See Notes
Dissolved Oxygen Subsystem
❑
Replaced Teflon Membrane
❑
Cleaned Electrode
❑
Replaced DO electrolyte
❑
See Notes
Field Barometric Pressure
Beginning BP
(mmHg)
Ending BP
(mmHg)
KEY:
B = Butter
LCS = Lab ControlStandard
-► =Adjusted I o
SS = Standard solution
LCSD = Lab Control Standard Duplicate
-/-►= Not Adjusted To
N/A = Not Applicable
W = Winkler
BP = Barometric Pressure
AW = Average Winkler
NOTES:
G1720B, K2820A, 200388, 197914, 197602, 1015

FIELD SAMPLING CALIBRATION FORM
STUDY:
MCGUIRE NUCLEAR STATION - NUCLEAR LANDFILL 1 GROUNDWATER MONITORING
PROGRAM
DATE (s):
January 24-26, 2022
SURFACE UNIT READER: EHS
COLLECTORS: EHS
SURFACE UNIT SERIAL #: 950
ANALYZER MODEL#: ST MP
ANALYZER SERIAL #: 767668
OTHER EQUIPMENT: TURBIDIMETER NO.3 - WR-00070
WEATHER CONDITIONS:
EHS 1/27/22
HYDROLAB PROCEDURE #:
3210.7
VALIDATED BY:
Calibration Date / Time
DATE:
25-Jan-22
TIME:
7:00
DATE:
26-Jan-22
TIME:
7:00
CALIBRATION BP (mmHg)
736.57
CALIBRATION BP (mmHg)
734.68
Calibation
Instrument
Standard
Instrument
Standard
Parameter
Calibration Results
Calibration Results
Standard
Value
Value
Value
Value
SS
0.0 -/-►
0.0
INSTRUMENT ZEROED
0.0 -/-►
0.0
INSTRUMENT ZEROED
SPEC. COND.
SS
732.1 -►
720
CALIBRATION ACCEPTED
1 722.4 -/-►
720
CALIBRATION ACCEPTED
(US/cm)
SS
228.1 -/-►
227
CALIBRATION ACCEPTED
227.2 -/-►
227
CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
SS
-/-►
1410
-/-►
1410
CHECK (uS/cm)
SS
B (7.00)
7.05 -►
7.04
CALIBRATION ACCEPTED
7.05 -/-►
7.04
CALIBRATION ACCEPTED
pH
B (4.00)
4.00 -►
3.99
CALIBRATION ACCEPTED
4.00 -/-►
3.99
CALIBRATION ACCEPTED
(units)
B (10.00)
10.09 -/-►
10.09
CALIBRATION ACCEPTED
10.11 -/-►
10.09
CALIBRATION ACCEPTED
Buffer Temp.
16.70
Buffer Temp.
16.98
pH Check
B (7.00)
-►
Buffer Temp.
7.13
0.00
Time:
448 -►
449
CALIBRATION ACCEPTED
448.0 -/-►
449
CALIBRATION ACCEPTED
ORP
N/A -/-►
N/A
N/A -/-►
N/A
Zobell's
ORP Temp.
16.68
ORP Temp.
16.68
0
TEMP (Co)
16.66
16.80
BP (mmHg)
736.57
734.68
COND
0.00
0.00
DO
100 % mg/L
9.32 -►
9.43
CALIBRATION ACCEPTED
9.42 -/-►
9.38
CALIBRATION ACCEPTED
(mg/L)
After Cal
9.32
98.85
After Cal % SAT
9.41
100.36
After Cal % SAT
LCS
9.32
98.85
CALIBRATION PASS
9.41
100.36
CALIBRATION PASS
LCSD
9.32
0.00
CALIBRATION PASS
9.41
0.00
CALIBRATION PASS
OTURB
(UR
ntuTemp
SS
10.0 -/-►
10.0
CALIBRATION ACCEPTED
10.0 -/-►
10.0
CALIBRATION ACCEPTED
Cert Device #
TEMP
NIST
N/A -/-►
N/A
Adjustment Not Available
N/A -/-►
N/A
Adjustment Not Available
(deg C)
INSTRUMENT MAINTENANCE
DATE / TIME
Conductance Subsystem
pH Subsystem
❑
Cleaned Electrodes
❑
Cleaned Electrodes
❑
Tested - OK
❑
Replaced ref Electrode KCL
❑
See Notes
❑
Replaced Ref. Electrode Tip
❑
Tested - OK
❑ See Notes
Oxidation Reduction Subsystem
Temperature Subsystem
❑
Cleaned Electrode
❑
Cleaned Electrode
❑
Tested - OK ❑
See Notes
❑
Tested - OK ❑ See Notes
Dissolved Oxygen Subsystem
❑
Replaced Teflon Membrane
❑
Cleaned Electrode
❑
Replaced DO electrolyte
❑
See Notes
Field Barometric Pressure
Beginning BP
(mmHg)
Ending BP
(mmHg)
KEY:
B = Butter
LCS = Lab ControlStandard
-► =Adjusted I o
SS = Standard solution
LCSD = Lab Control Standard Duplicate
-/-►= Not Adjusted To
N/A = Not Applicable
W = Winkler
BP = Barometric Pressure
AW = Average Winkler
NOTES:
G1720B, K2820A, 200388, 197914, 197602, 1015

FIELD SAMPLING CALIBRATION FORM
STUDY:
MCGUIRE NUCLEAR STATION - NUCLEAR LANDFILL 1 GROUNDWATER MONITORING
PROGRAM
DATE (s):
January 24-26, 2022
SURFACE UNIT READER: EHS
COLLECTORS: EHS
SURFACE UNIT SERIAL #: 950
ANALYZER MODEL#: ST MP
ANALYZER SERIAL #: 767668
OTHER EQUIPMENT: TURBIDIMETER NO.3 - WR-00070
WEATHER CONDITIONS:
20s-40s, sunny
EHS 1/27/22
HYDROLAB PROCEDURE #:
3210.7
VALIDATED BY:
Calibration Date / Time
DATE:
26-Jan-22
TIME:
7:00
DATE:
26-Jan-22
TIME:
4:30
CALIBRATION BP (mmHg)
734.68
CALIBRATION BP (mmHg)
735.12
Calibation
Instrument
Standard
Instrument
Standard
Parameter
Calibration Results
Calibration Results
Standard
Value
Value
Value
Value
SS
0.0 -/-►
0.0
INSTRUMENT ZEROED
0.0 -/-►
0.0
INSTRUMENT ZEROED
SPEC. COND.
SS
722.4 -►
720
CALIBRATION ACCEPTED
1 727.2 -►
720
CALIBRATION ACCEPTED
(US/cm)
SS
227.2 -/-►
227
CALIBRATION ACCEPTED
229.9 -/-►
227
CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
SS
-/-►
1410
-/-►
1410
CHECK (uS/cm)
SS
B (7.00)
7.05 -►
7.04
CALIBRATION ACCEPTED
7.08 -►
7.04
CALIBRATION ACCEPTED
pH
B (4.00)
4.00 -►
3.99
CALIBRATION ACCEPTED
4.01 -►
3.99
CALIBRATION ACCEPTED
(units)
B (10.00)
10.11 -/-►
10.09
CALIBRATION ACCEPTED
10.13 -/-►
10.09
CALIBRATION ACCEPTED
Buffer Temp.
16.98
Buffer Temp.
17.12
pH Check
B (7.00)
-►
Buffer Temp.
7.13
0.00
Time:
448 -►
449
CALIBRATION ACCEPTED
448 -►
448
CALIBRATION ACCEPTED
ORP
N/A -/-►
N/A
N/A -/-►
N/A
Zobell's
ORP Temp.
16.68
ORP Temp.
17.04
0
TEMP (Co)
16.80
16.97
BP (mmHg)
734.68
735.12
COND
0.00
0.00
DO
100 % mg/L
9.42 -►
9.38
CALIBRATION ACCEPTED
9.39 -►
9.35
CALIBRATION ACCEPTED
(mg/L)
After Cal
9.41
100.36
After Cal % SAT
9.40
100.55
After Cal % SAT
LCS
9.41
100.36
CALIBRATION PASS
9.40
100.55
CALIBRATION PASS
LCSD
9.41
0.00
CALIBRATION PASS
9.40
0.00
CALIBRATION PASS
OTURB
(UR
ntuTemp
SS
10.0 -/-►
10.0
CALIBRATION ACCEPTED
10.1 -/-►
10.0
CALIBRATION ACCEPTED
Cert Device #
TEMP
NIST
N/A -/-►
N/A
Adjustment Not Available
N/A -/-►
N/A
Adjustment Not Available
(deg C)
INSTRUMENT MAINTENANCE
DATE / TIME
Conductance Subsystem
pH Subsystem
❑
Cleaned Electrodes
❑
Cleaned Electrodes
❑
Tested - OK
❑
Replaced ref Electrode KCL
❑
See Notes
❑
Replaced Ref. Electrode Tip
❑
Tested - OK
❑ See Notes
Oxidation Reduction Subsystem
Temperature Subsystem
❑
Cleaned Electrode
❑
Cleaned Electrode
❑
Tested - OK ❑
See Notes
❑
Tested - OK ❑ See Notes
Dissolved Oxygen Subsystem
❑
Replaced Teflon Membrane
❑
Cleaned Electrode
❑
Replaced DO electrolyte
❑
See Notes
Field Barometric Pressure
Beginning BP
(mmHg)
Ending BP
(mmHg)
KEY:
B = Butter
LCS = Lab ControlStandard
-► =Adjusted I o
SS = Standard solution
LCSD = Lab Control Standard Duplicate
-/-►= Not Adjusted To
N/A = Not Applicable
W = Winkler
BP = Barometric Pressure
AW = Average Winkler
NOTES:
G1720B, K2820A, 200388, 197914, 197602, 1015

FIELD SAMPLING CALIBRATION FORM
STUDY:
MCGUIRE NUCLEAR STATION - NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
DATE (s):
January 26, 2022
SURFACE UNIT READER: CJZ
COLLECTORS: CJZ
SURFACE UNIT SERIAL #: 950
ANALYZER MODEL#: ST MP
ANALYZER SERIAL #: 763574
OTHER EQUIPMENT: TURBIDIMETER No.5 - WR-00070
WEATHER CONDITIONS:
20s-40s, sunny
EHS 1/27/22
HYDROLAB PROCEDURE #:
3210.7
VALIDATED BY:
Calibration Date / Time
DATE:
26-Jan-22
TIME:
8:45
DATE:
26-Jan-22
TIME:
2:05
CALIBRATION BP (mmHg)
750.22
CALIBRATION BP (mmHg)
750.53
Calibation
Instrument
Standard
Instrument
Standard
Parameter
Calibration Results
Calibration Results
Standard
Value
Value
Value
Value
SS
0.0 -►
0.0
INSTRUMENT ZEROED
0.0 -/-►
0.0
INSTRUMENT ZEROED
SPEC. COND.
SS
1409.2 -►
1410
CALIBRATION ACCEPTED
1 1410.4 -/-►
1410
CALIBRATION ACCEPTED
(US/cm)
SS
226.6 -/-►
227
CALIBRATION ACCEPTED
228.8 -/-►
227
CALIBRATION ACCEPTED
Specifc conductance checkpoint (used if sampled well is outside of initial calibration range).
SPEC. COND.
SS
-/-►
1410
-/-►
1410
CHECK (uS/cm)
SS
B (7.00)
7.07 -►
7.09
CALIBRATION ACCEPTED
7.06 -/-►
7.07
CALIBRATION ACCEPTED
pH
B (4.00)
3.93 -►
3.99
CALIBRATION ACCEPTED
3.96 -/-►
4.00
CALIBRATION ACCEPTED
(units)
B (10.00)
10.26 -/-►
10.22
CALIBRATION ACCEPTED
10.10 -/-►
10.18
CALIBRATION ACCEPTED
Buffer Temp.
7.22
Buffer Temp.
11.01
pH Check
B (7.00)
7.08 -►
Buffer Temp.
7.09
6.90
Calibration Accepted
Time:
0
475 -►
476
CALIBRATION ACCEPTED
465 -/-►
463
CALIBRATION ACCEPTED
ORP
N/A -/-►
N/A
N/A -/-►
N/A
Zobell's
ORP Temp.
5.26
ORP Temp.
10.99
0
TEMP (C°)
4.90
10.89
BP (mmHg)
750.22
750.53
COND
0.00
0.00
DO
100 % mg/L
12.80 -►
12.64
CALIBRATION ACCEPTED
10.84 -/-►
10.92
CALIBRATION ACCEPTED
(mg/L)
After Cal
12.85
101.68
After Cal % SAT
10.85
99.40
After Cal % SAT
LCS
12.85
101.68
CALIBRATION PASS
10.85
99.40
CALIBRATION PASS
LCSD
12.85
0.00
CALIBRATION PASS
10.85
0.00
CALIBRATION PASS
OTURB
(UR
ntuTemp
SS
10.0 -/-►
10.0
CALIBRATION ACCEPTED
10.0 -/-►
10.0
CALIBRATION ACCEPTED
Cert Device #
TEMP
NIST
N/A -/-►
N/A
Adjustment Not Available
N/A -/-►
N/A
Adjustment Not Available
(deg C)
INSTRUMENT MAINTENANCE
DATE / TIME
Conductance Subsystem
pH Subsystem
❑
Cleaned Electrodes
❑
Cleaned Electrodes
❑
Tested - OK
❑
Replaced ref Electrode KCL
❑
See Notes
❑
Replaced Ref. Electrode Tip
❑
Tested - OK
❑ See Notes
Oxidation Reduction Subsystem
Temperature Subsystem
❑
Cleaned Electrode
❑
Cleaned Electrode
❑
Tested - OK ❑
See Notes
❑
Tested - OK ❑ See Notes
Dissolved Oxygen Subsystem
❑
Replaced Teflon Membrane
❑
Cleaned Electrode
❑
Replaced DO electrolyte
❑
See Notes
Field Barometric Pressure
Beginning BP
(mmHg)
Ending BP
(mmHg)
KEY:
B = Butter
LCS = Lab ControlStandard
-► =Adjusted I o
SS = Standard solution
LCSD = Lab Control Standard Duplicate
-/-►= Not Adjusted To
N/A = Not Applicable
W = Winkler
BP = Barometric Pressure
AW = Average Winkler
NOTES:
G1720B, K2820A, 200388, 197914, 197602, 1015

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
I 24-Ian-2022 25-Ian-2022 Ll 26-Ian-2022 Ll
WELL/LOCATION NAME
MW-1
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
730.23
MIDDLE OF WETTED SCREEN (ft toc)
63.55
WELL DEPTH (ft TOC) 68.55
GS ELEV (ft msl)
729.58
PUMP INTAKE DEPTH (ft TOC)
05
�-68 -.
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
58.55
TO
68.55
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
(sec)
DISCHARGE
a (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
29.75
11WATER
COLUMN (ft)
1 38.80
WATER ELEVATION (ft msl)
700.48
WELL VOLUME
(gal)
6.33 ]j
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
1:23
31.25
440
16.21
113
6.11
15.7
239
0.66
N/A
1:26
31.25
440
16.18
113
6.11
12.7
239
0.68
N/A
1:29
31.25
440
16.16
113
6.11
11.6
239
0.78
N/A
1:32
31.25
440
16.17
114
6.11
9.8
239
0.68
N/A
DRAW -DOWN
1.50
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
3.50
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
4.55
(gal)
1/25/2022 @ 1335
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
❑24-Ian-2022 ❑25-Ian-2022 ❑26-Ian-2022 ❑
WELL/LOCATION NAME
MW-1D
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
730.61
MIDDLE OF WETTED SCREEN (ft toc)
83.22
WELL DEPTH (ft TOC) 88.22
GS ELEV (ft msl)
729.75
PUMP INTAKE DEPTH (ft TOC)
�-87 . —
72
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
78.22
TO
88.22
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iu
(sec)
DISCHARGE
5
(sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
30.79
11WATER
COLUMN (ft)
1 57.43
WATER ELEVATION (ft msl)
1 699.82
11WELLVOLUME
(gal)
1 9.37
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
2:03
32.20
360
16.16
105
6.16
21.9
251
0.79
N/A
2:06
32.20
360
16.12
104
6.15
14.2
252
0.85
N/A
2:09
32.20
360
16.12
105
6.15
9.3
251
0.87
N/A
DRAW -DOWN
1.41
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
1.00
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
�1/25/2
CHLORINE (mg/I)
TOTAL PURGE VOLUME
1.60
(gal)
0 22 @ 1415
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
I 24-Ian-2022 25-Ian-2022 Ll 26-Ian-2022 Ll
WELL/LOCATION NAME
MW-2A
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
739.67
MIDDLE OF WETTED SCREEN (ft toc)
72.57
WELL DEPTH (ft TOC) 77.57
GS ELEV (ft msl)
736.96
PUMP INTAKE DEPTH (ft TOC)
�-77 -.
07
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
67.57
TO
77.57
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iu
(sec)
DISCHARGE
to (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
51.95
11WATER
COLUMN (ft)
1 25.62
WATER ELEVATION (ft msl)
687.72
WELL VOLUME
(gal)
4.18 ]l
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
11:36
60.80
240
17.55
127
6.53
3.7
345
6.34
N/A
11:39
60.80
240
17.33
123
6.52
1.7
372
6.45
N/A
11:42
60.80
240
17.21
124
6.50
1.5
384
6.31
N/A
DRAW -DOWN
8.85
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
3.00
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
3.40
(gal)
1/25/2022 @ 1145
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
IM NS_FD-20220125-1
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

, DIME DUKE ENERGY
ENERGY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR EQUIPMENT PURGE ONLY SAMPLING
.(' DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
24-Ian-2022 El 25-Ian-2022 26-Jan-2022
7WELL/LOCATION NAME
MW-ZD
MONITORING WELL INFORMATION
WELL DIAMETER (in)
2.00
TOC ELEV (ft msl)
740.77
MIDDLE OF WETTED SCREEN (ft toc)
103.82
WELL DEPTH (ft TOC)
108.82
GS ELEV (ft msl)
737.41
PUMP INTAKE DEPTH (ft TOC)
108.32
SCREEN LENGTH (ft)
10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
98.82
TO
108.82
F— EQUIPMENT INFORMATION
LEVEL METER SERIAL# I 0965-T2
SAMPLING EQUIPMENT QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
(sec)
I DISCHARGE
(sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELT
NUCLEAR LANDFILL
Equip. Only Purge
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
53.52
WATER COLUMN (ft)
55.30
WATER ELEVATION (ft msl)
687.25
WELL VOLUME (gal) 9.02
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
INITIAL
WATER LEVEL
(ft)
FLOW
RATE
(ml/min)
FINAL
WATER LEVEL
(ft)
TEMP
(deg C)
SPECIFIC
COND.
(umho/cm)
pH
(su)
TURBIDITY
(NTU)
ORP
(mV -NEH)
DISSOLVED
OXYGEN
(mg/L)
5 3.5 2
100
58.09
19.46
60
6.87
3.5
367
9.23
N/A
If Evacuated And It Is Requiered To Return To Sample, Enter The Date, Time, And
Water Level To The Right Before Sampling to Determine Recharge.
L r:
TIME:
WATER LEVEL:
Well Vol.:
Evacuated:
N/A
N/A
Sample:
Tubing Volume
2353
(ml) I INITIAL PURGE VOL. EQUIPMENT PURGE ONLY SAMPLE
CHLORINE (mg/1)
Pump (Bladder) Volume
495
(ml) 1.00 SAMPLE COLLECTED BY
(ml) 1 - 1 0.75 1 (gal) EHS
DATE TIME
Total Purge Volume
2848
1/25/2022
@
1215
0
:QC:By: EHS 1/27/22
Sample preservation verified to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 [:]BORON ❑ SR 89/90 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,Cl- ❑ ALPHA SPEC
0 METALS q F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD Good Condition I lWell Impacted By Silting: I NO
WELL CAPS
WELL CASING
ACCESS TO WELLS
PROTECTIVE CASING
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well cap in good conditon
Good Condition
Access cleared into well
Casing in good condition
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES
Normally pump at 420 ml/min but pump will only go to 100 ml/min.

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
I 24-Ian-2022 11 25-Ian-2022 21 26-Ian-2022 Ll
WELL/LOCATION NAME
MW-3
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
728.43
MIDDLE OF WETTED SCREEN (ft toc)
68.64
WELL DEPTH (ft TOC) 73.64
GS ELEV (ft msl)
724.98
PUMP INTAKE DEPTH (ft TOC)
�-73 -.
14
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
63.64
TO
73.64
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iu
(sec)
DISCHARGE
to (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
57.97
11WATER
COLUMN (ft)
1 15.67
WATER ELEVATION (ft msl)
670.46
WELL VOLUME
(gal)
2.56 ]j
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑�
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
12:26
61.85
330
14.82
75
6.27
1.1
405
5.66
N/A
12:29
61.85
330
14.86
74
6.27
1.0
401
5.60
N/A
12:32
61.85
330
14.81
74
6.27
1.0
399
5.48
N/A
DRAW -DOWN
3.88
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
2.50
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
3.05
(gal)
1/26/2022 @ 1235
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
11 JLl
I 24-Ian-2022 25-Ian-2022 26-Ian-2022
WELL/LOCATION NAME
MW-3D
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
728.39
MIDDLE OF WETTED SCREEN (ft toc)
85.19
WELL DEPTH (ft TOC) 90.19
GS ELEV (ft msl)
724.98
PUMP INTAKE DEPTH (ft TOC)
89.69
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
80.19
TO
90.19
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
14
(sec)
DISCHARGE
a (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
57.75
11WATER
COLUMN (ft)
1 32.44
WATER ELEVATION (ft msl)
1 670.64
11WELLVOLUME
(gal)
1 5.29
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
11:53
58.45
420
14.98
150
6.56
2.3
246
3.30
N/A
11:56
58.45
420
15.04
150
6.55
1.0
249
3.28
N/A
11:59
58.45
420
15.01
152
6.55
1.0
253
3.18
N/A
DRAW -DOWN
0.70
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
2.00
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
�1/26/2
CHLORINE (mg/I)
TOTAL PURGE VOLUME
2.70
(gal)
0 22 @ 1200
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

, DIME DUKE ENERGY
ENERGY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR EQUIPMENT PURGE ONLY SAMPLING
.(' DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
CJZ
SAMPLING DATE(s)
❑26-Ian-2022 ❑ ❑
�E]
7WELL/LOCATION NAME
MW-4
MONITORING WELL INFORMATION
WELL DIAMETER (in)
2.00
TOC ELEV (ft msl)
741.13
MIDDLE OF WETTED SCREEN (ft toc)
70.08
WELL DEPTH (ft TOC)
74.15
GS ELEV (ft msl)
738.40
PUMP INTAKE DEPTH (ft TOC)
73.65
SCREEN LENGTH (ft)
10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
64.15
TO
74.15
F— EQUIPMENT INFORMATION
LEVEL METER SERIAL# I 0957-T2
SAMPLING EQUIPMENT QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
1 45
(sec)
DISCHARGE
15 (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELT
NUCLEAR LANDFILL
Equip. Only Purge
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
66.01
WATER COLUMN (ft)
8.14
WATER ELEVATION (ft msl)
675.12
WELL VOLUME (gal) 1.33
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
INITIAL
WATER LEVEL
(ft)
FLOW
RATE
(ml/min)
FINAL
WATER LEVEL
(ft)
TEMP
(deg C)
SPECIFIC
COND.
(umho/cm)
pH
(su)
TURBIDITY
(NTU)
ORP
(mV -NEH)
DISSOLVED
OXYGEN
(mg/L)
66.01
270
67.98
12.81
72
6.06
0.7
376
3.90
N/A
If Evacuated And It Is Required To Return To Sample, Enter The Date, Time, And Water
Level To The Right Before Sampling to Determine Recharge.
L r:
TIME:
WATER LEVEL:
Well Vol.:
Evacuated:
N/A
N/A
Sampled:
Tubing Volume
1600
(ml) I INITIAL PURGE VOL. EQUIPMENT PURGE ONLY SAMPLE
CHLORINE (mg/1)
Pump (Bladder) Volume
495
(ml) 0.75 SAMPLE COLLECTED BY
(ml) 1 - 1 0.55 1 (gal) CJZ
DATE TIME
Total Purge Volume
2095
1/26/2022
@
1100
N/A
amp a preservation verl le to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 [:]BORON ❑ SR 89/90 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,Cl- ❑ ALPHA SPEC
0 METALS ❑ F_ALK [21 CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD Good Condition I lWell Impacted By Silting: I NO
WELL CAPS
WELL CASING
ACCESS TO WELLS
PROTECTIVE CASING
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
N
Well cap in good conditon
Good Condition
Access cleared into well
Casing in good condition
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
CJZ
SAMPLING DATE(s)
❑26-Ian-2022 ❑ ❑ ❑
WELL/LOCATION NAME
MW-4D
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
740.58
MIDDLE OF WETTED SCREEN (ft toc)
WELL DEPTH (ft TOC) 102.24
GS ELEV (ft msl)
738.25
PUMP INTAKE DEPTH (ft TOC)
�_97.24
101 .74
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
92.24
TO
102.24
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0957-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iu
(sec)
DISCHARGE
to (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
66.25
11WATER
COLUMN (ft)
1 35.99
WATER ELEVATION (ft msl)
674.33
WELL VOLUME
(gal)
5.87
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑r
TEMP
(deg Q
❑✓
SPECIFIC
COND.
(umho/cm)
❑r
pH
(SU)
❑✓
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
11:17
66.70
200
13.34
145
6.12
2.4
351
5.50
N/A
11:20
66.77
200
13.78
152
5.70
1.9
261
2.38
N/A
11:23
66.77
200
14.23
157
5.60
2.0
255
0.66
N/A
11:26
66.77
200
14.77
159
5.58
2.2
253
0.57
N/A
11:29
66.77
200
14.70
160
5.58
1.6
255
0.51
N/A
DRAW -DOWN
0.52
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
1.20
(gal)
SAMPLE COLLECTED BY
CJZ
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
1.85
(gal)
1/26/2022 @ 1130
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

, DIME DUKE ENERGY
ENERGY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR EQUIPMENT PURGE ONLY SAMPLING
.(' DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
CJZ
SAMPLING DATE(s)
❑26-Ian-2022 ❑ ❑
7WELL/LOCATION NAME
MW-4R
MONITORING WELL INFORMATION
WELL DIAMETER (in)
2.00
TOC ELEV (ft msl)
713.87
MIDDLE OF WETTED SCREEN (ft toc)
43.47
WELL DEPTH (ft TOC)
45.73
GS ELEV (ft msl)
711.15
PUMP INTAKE DEPTH (ft TOC)
45.23
SCREEN LENGTH (ft)
15
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
30.73
TO
45.73
F— EQUIPMENT INFORMATION
LEVEL METER SERIAL# I 0957-T2
SAMPLING EQUIPMENT QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
13
(sec)
DISCHARGE
(sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELT
NUCLEAR LANDFILL
Equip. Only Purge
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
41.20
WATER COLUMN (ft)
4.53
WATER ELEVATION (ft msl)
672.67
WELL VOLUME (gal) 0.74
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
INITIAL
WATER LEVEL
(ft)
FLOW
RATE
(ml/min)
FINAL
WATER LEVEL
(ft)
TEMP
(deg C)
SPECIFIC
COND.
(umho/cm)
pH
(su)
TURBIDITY
(NTU)
ORP
(mV -NEH)
DISSOLVED
OXYGEN
(mg/L)
41.20
300
42.73
12.46
73
5.73
8.8
319
2.78
N/A
If Evacuated And It Is Requiered To Return To Sample, Enter The Date, Time, And
Water Level To The Right Before Sampling to Determine Recharge.
b FE:
TIME:
WATER LEVEL:
Well Vol.:
Evacuated:
N/A
N/A
Sample:
Tubing Volume
982
(ml) I INITIAL PURGE VOL. EQUIPMENT PURGE ONLY SAMPLE
CHLORINE (mg/1)
Pump (Bladder) Volume
495
(ml) 0.50 SAMPLE COLLECTED BY
(ml) 1 - 1 0.39 1 (gal) CJZ
DATE TIME
Total Purge Volume
1477
1/26/2022
@
1220
0
:QC:By: EHS 1/27/22
Sample preservation verified to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 [:]BORON ❑ SR 89/90 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,Cl- ❑ ALPHA SPEC
0 METALS q F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD Good Condition I lWell Impacted By Silting: I NO
WELL CAPS
WELL CASING
ACCESS TO WELLS
PROTECTIVE CASING
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
N
Well cap in good conditon
Good Condition
Access cleared into well
Casing in good condition
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
CJZ
SAMPLING DATE(s)
❑26-Ian-2022 ❑ ❑ ❑
WELL/LOCATION NAME
MW-4Da
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
713.75
MIDDLE OF WETTED SCREEN (ft toc)
82.90
WELL DEPTH (ft TOC) 90.40
GS ELEV (ft msl)
711.15
PUMP INTAKE DEPTH (ft TOC)
�-89.90
SCREEN LENGTH (ft) 15
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
75.40
TO
90.40
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0957-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iL,
(sec)
DISCHARGE
5 (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
40.81
11WATER
COLUMN (ft)
1 49.59
WATER ELEVATION (ft msl)
672.94
WELL VOLUME
(gal)
8.09
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑r
TEMP
(deg Q
❑✓
SPECIFIC
COND.
(umho/cm)
❑r
pH
(SU)
❑✓
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
13:18
41.22
210
9.62
84
6.25
0.6
352
6.25
N/A
13:21
41.22
210
11.24
81
6.04
0.9
354
3.47
N/A
13:24
41.22
210
11.50
80
6.09
1.0
355
3.01
N/A
13:27
41.22
210
11.67
80
6.10
0.6
355
2.97
N/A
13:30
41.22
210
11.66
81
6.09
0.8
356
2.98
N/A
DRAW -DOWN
0.41
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
1.55
(gal)
SAMPLE COLLECTED BY
CJZ
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
2.25
(gal)
1/26/2022 @ 1330
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

, DIME DUKE ENERGY
ENERGY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR EQUIPMENT PURGE ONLY SAMPLING
.(' DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
JEl
24-Ian-2022 25-Ian-2022 26-Jan-2022
7WELL/LOCATION NAME
—t
MW-11
MONITORING WELL INFORMATION
WELL DIAMETER (in)
2.00
TOC ELEV (ft msl)
722.60
MIDDLE OF WETTED SCREEN (ft toc)
34.94
WELL DEPTH (ft TOC)
38.45
GS ELEV (ft msl)
720.10
PUMP INTAKE DEPTH (ft TOC)
37.95
SCREEN LENGTH (ft)
15
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
23.45
TO
38.45
F— EQUIPMENT INFORMATION
LEVEL METER SERIAL# I 0965-T2
SAMPLING EQUIPMENT QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
13
(sec)
I DISCHARGE
(sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELT
NUCLEAR LANDFILL
Equip. Only Purge
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
31.42
WATER COLUMN (ft)
7.03
WATER ELEVATION (ft msl)
691.18
WELL VOLUME (gal) 1.15
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
INITIAL
WATER LEVEL
(ft)
FLOW
RATE
(ml/min)
FINAL
WATER LEVEL
(ft)
TEMP
(deg Q
SPECIFIC
COND.
(umho/cm)
pH
(su)
TURBIDITY
(NTU)
ORP
(mV -NEH)
DISSOLVED
OXYGEN
(mg/L)
31.42
240
34.45
13.60
138
6.24
9.0
188
1.27
N/A
If Evacuated And It Is Requiered To Return To Sample, Enter The Date, Time, And
Water Level To The Right Before Sampling to Determine Recharge.
L r:
TIME:
WATER LEVEL:
Well Vol.:
Evacuated:
N/A
N/A
Sample:
Tubing Volume
824
(ml) I INITIAL PURGE VOL. EQUIPMENT PURGE ONLY SAMPLE
CHLORINE (mg/1)
Pump (Bladder) Volume
495
(ml) 0.50 SAMPLE COLLECTED BY
(ml) 1 - 1 0.35 1 (gal) EHS
DATE TIME
Total Purge Volume
1319
1/24/2022
@
1100
0
:QC:By: EHS 1/27/22
Sample preservation verified to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 [:]BORON ❑ SR 89/90 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,Cl- ❑ ALPHA SPEC
0 METALS q F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD Good Condition I lWell Impacted By Silting: I NO
WELL CAPS
WELL CASING
ACCESS TO WELLS
PROTECTIVE CASING
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
N
Well cap in good conditon
Good Condition
Access cleared into well
Casing in good condition
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
❑24-Ian-2022 ❑25-Ian-2022 ❑26-Ian-2022 ❑
WELL/LOCATION NAME
MW-11D
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
723.14
MIDDLE OF WETTED SCREEN (ft toc)
WELL DEPTH (ft TOC) 101.55
GS ELEV (ft msl)
720.84
PUMP INTAKE DEPTH (ft TOC)
�_96.55
101.05
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
91.55
TO
101.55
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iL,
(sec)
DISCHARGE
5 (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
32.58
11WATER
COLUMN (ft)
1 68.97
WATER ELEVATION (ft msl)
690.56
11WELLVOLUME
(gal)
1 11.25
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Turbid
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
9:55
44.80
400
13.28
32
5.78
40.0
369
7.29
N/A
10:00
44.80
400
13.56
32
5.78
46.2
375
7.15
N/A
10:05
44.80
400
13.68
32
5.76
36.9
378
7.10
N/A
10:10
44.80
400
13.86
32
5.79
43.4
377
7.09
N/A
10:13
44.80
400
13.87
32
5.79
39.2
376
7.11
N/A
10:16
44.80
400
13.91
32
5.80
38.0
376
7.12
N/A
10:19
44.80
400
13.83
33
5.79
45.2
379
7.14
N/A
10:22
44.80
400
13.81
32
5.79
54.0
378
7.15
N/A
10:25
44.80
400
13.72
33
5.80
50.7
376
7.18
N/A
10:28
44.80
400
13.68
32
5.80
44.3
378
7.15
N/A
DRAW -DOWN
12.22
(ft)
INITIAL PURGE VOLUME
8.00
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
�1/24/2
CHLORINE (mg/1)
TOTAL PURGE VOLUME
11.50
(gal)
0 22 @ 1030
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES
After initial well volume is removed - WL drops to 65 ft - recalculate well volume and use for subsequent readings.

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
24-Ian-2022 25-Ian-2022 Ll 26-Ian-2022 Ll
WELL/LOCATION NAME
MW-12
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
724.81
MIDDLE OF WETTED SCREEN (ft toc)
21.99
WELL DEPTH (ft TOC) 29.49
GS ELEV (ft msl)
722.21
PUMP INTAKE DEPTH (ft TOC)
28.99
SCREEN LENGTH (ft) 15
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
14.49
TO
29.49
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
14
(sec)
DISCHARGE
a (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
10.55
11WATER
COLUMN (ft)
1 18.94
WATER ELEVATION (ft msl)
714.26
WELL VOLUME
(gal)
3.09 ]j
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
12:34
12.28
220
14.03
26
5.08
14.9
429
7.97
N/A
12:39
12.28
220
14.08
26
5.08
11.5
426
7.93
N/A
12:43
12.28
220
14.16
26
5.08
7.7
422
7.91
N/A
DRAW -DOWN
1.73
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
1.00
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
CHLORINE (mg/1)
TOTAL PURGE VOLUME
1.55
(gal)
1/24/2022 @ 1245
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

�. DUDE DUKE ENERGY
ENERGY GY GROUNDWATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR LOW FLOW SAMPLING
r�� DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
❑24-Ian-2022 ❑25-Ian-2022 ❑26-Ian-2022 ❑
WELL/LOCATION NAME
MW-12D
MONITORING WELL INFORMATION
WELL DIAMETER (in) 2.00
TOC ELEV (ft msl)
724.77
MIDDLE OF WETTED SCREEN (ft toc)
63.42
WELL DEPTH (ft TOC) 68.42
GS ELEV (ft msl)
722.21
PUMP INTAKE DEPTH (ft TOC)
�-67 -.
92
SCREEN LENGTH (ft) 10
ELEV REF
NAVD 88
SCREEN INTERVAL (ft TOC)
58.42
TO
68.42
EQUIPMENT INFORMATION
LEVEL METER SERIAL#
I 0965-T2
SAMPLING EQUIPMENT
QED T1200
TUBING DIAMETER (in)
1/2 OD
PUMP CONTROLLER SETTINGS
PRESSURE
(psi)
RECHARGE
iu
(sec)
DISCHARGE
to (sec)
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
STICK UP WELL
MONITORING WELL
NUCLEAR LANDFILL
Low Flow
SAMPLING INFORMATION
INITIAL DEPTH TO WATER (ft TOC)
27.12
11WATER
COLUMN (ft)
1 41.30
WATER ELEVATION (ft msl)
697.65
11WELLVOLUME
(gal)
1 6.74
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
TIME
(hh:mm)
WATER
LEVEL
(ft)
FLOWRATE
(ml/min)
❑�
TEMP
(deg Q
❑�
SPECIFIC
COND.
(umho/cm)
❑�
pH
(SU)
❑�
TURBIDITY
(NTU)
❑
ORP
(mV-NHE)
❑
DISSOLVED
OXYGEN
(mg/L)
❑ (gal)
WELL VOL
(recalculates on
current water level)
1:22
29.27
240
14.64
91
6.35
8.9
348
7.72
N/A
1:25
29.27
240
14.64
89
6.36
5.0
346
7.71
N/A
1:28
29.27
240
14.65
91
6.35
5.4
346
7.72
N/A
DRAW -DOWN
2.15
(ft)
COLLECT SAMPLE
- SAMPLE CRITERIA SATISFIED
INITIAL PURGE VOLUME
1.50
(gal)
SAMPLE COLLECTED BY
EHS
DATE TIME
CHLORINE (mg/I)
TOTAL PURGE VOLUME
1.90
(gal)
1/24/2022 @ 1330
0
QC By: EHS 1/27/22
Sample preservation verl ie to p
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 0 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 0 SO4,CL ❑ ALPHA SPEC
❑ METALS ❑ F_ALK ❑ CO2 ❑ RSK 175 0 VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑ TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD
Good Condition
Well Impacted By Silting:
NO
WELL CAPS
Well cap in good conditon
WELL CASING
Good Condition
ACCESS TO WELLS
Access cleared into well
PROTECTIVE CASING
Casing in good condition
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Well tag in good condition
Access cleared around well
Well found locked
Lock in good condition
SAMPLING NOTES

, DIME DUKE ENERGY
ENERGY SURFACE WATER MONITORING DATA SHEET
SAMPLING PROCEDURE NO. 3175.4
FOR SURFACE WATER SAMPLING
.(' DUKE
� ENERGY
SITE NAME
MCGUIRE NUCLEAR STATION
PERMIT #
60-04
SITE ID
N/A
PROJECT NAME
NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM
FIELD CREW
EHS
SAMPLING DATE(s)
❑24-Ian-2022 ❑25-Ian-2022 026-Jan-2022
❑
7WELL/LOCATION NAME
sW-1
SURFACE WATER LOCATION
INFORMATION
LOCATION TYPE:
STREAM
WAS WATER PRESENT:
YES
WAS THERE A NOTICABLE FLOW: YES
SAMPLING METHOD:
PERISTALTIC PUMP
LOCATION ENVIRONMENT:
WOODED
WELL/SAMPLING INFORMATION
WELL TYPE
WELL INFORMATION
WELL USE
PURGE METHOD
Surface Water Sample
SAMPLING INFORMATION
DETECTED ODOR
None
ODOR STRENGTH
None
APPEARANCE
Normal
DEPTH OF
INTAKE
(METERS)
❑'
TEMP
(degQ
❑J
SPECIFIC
COND.
(umho/cm)
❑'
pH
(su)
❑'
TURBIDITY
(NTU)
❑
ORP
(mV-NEH)
❑
DISSOLVED
OXYGEN
(mg/L)
❑
0.01
12.79
93
6.92
19.2
268
8.85
N/A
FLOW
CONDITIONS:
Flowing, 3.00 gallons removed
SURFACE
WATER SAMPLE
CHLORINE (mg/1)
SAMPLE COLLECTED BY
EHS
DATE TIME
1/25/2022
@
1515
0
:QC:By: EHS 1/27/22
Sample preservation verified to p
'0
(units)
SAMPLE LIST CHECK IF SAMPLES WERE COLLECTED
0 GAMMA 0 H3 ❑ BORON ❑ SR 89/90 F11 GROSS ALPH/BETA ❑ Fe 55 ❑ Ni 63 ❑ IODINE 131 ❑ SO4,CL ❑ ALPHA SPEC
❑ METALS P/1 F_ALK ❑ CO2 ❑ RSK 175 ❑ VOC's ❑ TPH-DRO
❑ METALS ❑ NO3-N, CL, F, SO4, F_ALK ❑TDS
❑ METALS ❑ NO3-N, CL, SO4 ❑ F_ALK ❑ TDS/TSS ❑ RADIUM 226/228
WELL CONDITION ADDITIONAL WELL CONDITION NOTES
WELL PAD I I lWell Impacted By Silting: I N/A
WELL CAPS
WELL CASING
ACCESS TO WELLS
PROTECTIVE CASING
FLUSH MOUNT WELLS
WELL TAG
ACCESS AROUND WELL
WELL SECURITY
WELL LOCK CONDITION
Access cleared into well
Access cleared around well
SAMPLING NOTES

NORTH CAROLINA GROUNDWATER SAMPLING SITE CHECK LIST
SITE: MCGUIRE NUCLEAR STATION SAMPLE DATE January 24-26, 2022
PROJECT: NUCLEAR LANDFILL 1 GROUNDWATER MONITORING PROGRAM FIELD CREW EHS
SITE CONTACT John Ballard
1/24/2022 30s-40s,sunny 1/25/2022
WEATHER
1/26/2022 20s-40s, sunny
PAGE 1 OF 1
MW-1
MW-1D
MW-2A
MW-2D
MW-3
MW-3D
MW-4
MW-4D
MW-4R
MW-4DR
MW-11
MW-11D
MW-12
MW-12D
SW-1
ACCESS TO WELLS
Access cleared into well
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Access cleared around well
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Tall grass or weeds - needs mowing
Road washing out / muddy / needs grading
Fallen tree blocking access
WELL DEPTH
Well impacted by silting
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
N/A
WELL SECURITY
Well found locked
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Well found unlocked
WELL LOCK CONDITION
Lock in good condition
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Lock rusted, difficult to open / needs replacing
Replaced damaged lock
WELL CASINGS
Casing in good condition
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Damaged casing / still functional
Damaged casing / repair required
CONCRETE PADS
Pad in good condition
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Minor cracks
Major cracks / broken / repair required
Undermined / washing out
Fire ants around concrete pad
WELL PROTECTIVE CASINGS
Casing in good condition
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Damaged casing / still functional
Damaged casing / repair required
Broken hinge on protective lid
Wasp nest inside protective casing
Ants inside protective casing
WELL CAPS
Well cap in good conditon
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Damaged / needs replacement
Replaced damaged well cap
FLUSH MOUNT WELLS
Vault in good condition
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Water inside vault
Vault bolt holes broken or stripped
Bolts stripped
Vault lid cracked or broken
WELL ID TAGS
Well tag in good condition
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
N/A
Well tag missing
Well tag damaged / illegible
Lacks required information - Driller Reg #
Lacks required information - Completion date
Lacks required information -Total well depth
Lacks required information - Depth to screen
Lacks required info - Casing depth / diam.
Lacks required information - Screen interval
Lacks required information - Static WL / date
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Lacks required information - Non potable tag
NOTE:

MCGUIRE NUCLEAR STATION
NUCLEAR
LANDFILL 1 GROUNDWATER MONITORING PROGRAM
GROUNDWATER MONITORING FIELD
DATA
PERMIT # 60-04
Purge Methods
LF
= Low Flow
C
= Connventional
EOP = Equip. Only Purge
LO = Level Only NP = No Purge
LF(M) = Low Flow (Mod.)
* = Applicable to LF & LF(M) Purging Only
WELL
DEPTH TO
WATER
PUMP WELL
EVAC
SPECIFIC
DATE
WELL
DEPTH
WATER
ELEV.
APPEARANCE
ODOR
PURGE RATE VOL.
VOL.
EVAC
TEMP.
CONDUCTANCE
pH
TURBIDITY
ORP
DO
NO
(ft -'roc)
(ft - TOC)
(ft)
METHOD (MI/Min) (gal)
(gal)
(YES/NO)
(deg. C)
(umho/cm)
(units)
(NTU's)
(mV-NHE)
(mg/L)
1/25/2022
MW-1
68.55
29.75
700.48
Normal
None
LF 440.00 6.33
4.55
N/A
16.17
114
6.11
9.8
239
0.68
1/25/2022
MW-1D
88.22
30.79
699.82
Normal
None
LF 360.00 9.37
1.60
N/A
16.12
105
6.15
9.3
251
0.87
1/25/2022
MW-2A
77.57
51.95
687.72
Normal
None
LF 240.00 4.18
3.40
N/A
17.21
124
6.50
1.5
384
6.31
1/25/2022
MW-2D
108.82
53.52
687.25
Normal
None
EOP N/A 9.02
1.00
N/A
19.46
60
6.87
3.5
367
9.23
1/26/2022
MW-3
73.64
57.97
670.46
Normal
None
LF 330.00 2.56
3.05
N/A
14.81
74
6.27
1.0
399
5.48
1/26/2022
MW-31D
90.19
57.75
670.64
Normal
None
LF 420.00 5.29
2.70
N/A
15.01
152
6.55
1.0
253
3.18
1/26/2022
MW-4
74.15
66.01
675.12
Normal
None
EOP N/A 1.33
0.75
N/A
12.81
72
6.06
0.7
376
3.90
1/26/2022
MW-41D
102.24
66.25
674.33
Normal
None
LF 200.00 5.87
1.85
N/A
14.70
160
5.58
1.6
255
0.51
1/26/2022
MW-4R
45.73
41.20
672.67
Normal
None
EOP N/A 0.74
0.50
N/A
12.46
73
5.73
8.8
319
2.78
1/26/2022
MW-41DR
90.40
40.81
672.94
Normal
None
LF 210.00 8.09
2.25
N/A
11.66
81
6.09
0.8
356
2.98
1/24/2022
MW-11
38.45
31.42
691.18
Normal
None
EOP N/A 1.15
0.50
N/A
13.60
138
6.24
9.0
188
1.27
1/24/2022
MW-11D
101.55
32.58
690.56
Turbid
None
LF 400.00 11.25
11.50
N/A
13.68
32
5.80
44.3
378
7.15
1/24/2022
MW-12
29.49
10.55
714.26
Normal
None
LF 220.00 3.09
1.55
N/A
14.16
26
5.08
7.7
422
7.91
1/24/2022
MW-12D
68.42
27.12
697.65
Normal
None
LF 240.00 6.74
1.90
N/A
14.65
91
6.35
5.4
346
7.72
1/25/2022
SW-1
0.00
Normal
None
SWS N/A
N/A
N/A
12.79
93
6.92
19.2
268
8.85

Appendix IV - Laboratory Reports and Chain -of -Custody Forms

y , DUKE
"
Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number:
J22010014
Project Name:
MCGUIRE - GW LF1
Task Code:
LF
Customer Name(s):
C Murphy, B Moeller,D Obrien,J Stowe, E Smith
Customer Address:
McGuire Nuclear Station
13225 Hagers Ferry Rd
Mail Code: MG01CH
Huntersville, NC 28078-8985
Lab Contact:
Peggy Kendall Phone: [phone]
Report Authorized By:
Date: 2/18/2022
(Signature)
Pegg endall
Page 1 of 151
Program Comments:
8260 QC Notes:
There were several MS/MSD exceedances for FD-20220126-1; results for three compounds, 1,1 dichloroethane/cis 1,2-
dichloroethene/methylene chloride should be considered estimates. All other compounds were non -detect; see the vendor report
for the complete list of MS/MSD exceedances.
MW-1 D had several MS/MSD exceedances; see vendor report for the complete list. All results were non -detect.
Methylene chloride detections were observed in MW-3D, MW-4D, MW-313R, and MW-413R. This analyte is a possible lab
contaminant, not present in the method blank.
Acetone and MEK were detected in TB-20220124-0930, FB-20220124-1600, and FB-20220125-1230; these analytes are
possible lab contaminants, not present in the method blank.
Four qualifiers were applied to several results. They are IK (recalculated concentration of the calibration stds did not meet
method acceptance limits), v1 (continuing calibration verification was above the method acceptance limit, result may be biased
high). v3(continuing calibration verification was below the method acceptance limit, result may be biased low). IH (analyte
exceeded secondary source verification criteria high for the initial calibration). Associated results were non -detect. Please refer
to the Pace report to see the specific sample results.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)

uertincation:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carge
olinaof 151
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 3 of 151
Sample ID
Plant/Station
Collection
Date and Time
Collected By
Sample Description
2022000054
MCGUIRE
25-Jan-22
1:35 PM
Ethan Smith
MNS MW-1
2022000055
MCGUIRE
25-Jan-22
2:15 PM
Ethan Smith
MNS MW-1D
2022000056
MCGUIRE
25-Jan-22
11:45 AM
Ethan Smith
MNS MW-2A
2022000057
MCGUIRE
25-Jan-22
12:15 PM
Ethan Smith
MNS MW-2D
2022000058
MCGUIRE
26-Jan-22
12:35 PM
Ethan Smith
MNS MW-3
2022000059
MCGUIRE
26-Jan-22
12:00 PM
Ethan Smith
MNS MW-3D
2022000060
MCGUIRE
26-Jan-22
11:00 AM
Connor Zahora
MNS MW-4
2022000061
MCGUIRE
26-Jan-22
11:30 AM
Connor Zahora
MNS MW-4D
2022000062
MCGUIRE
24-Jan-22
11:00 AM
Ethan Smith
MNS MW-11
2022000063
MCGUIRE
24-Jan-22
10:30 AM
Ethan Smith
MNS MW-11D
2022000064
MCGUIRE
24-Jan-22
12:45 PM
Ethan Smith
MNS MW-12
2022000065
MCGUIRE
24-Jan-22
1:30 PM
Ethan Smith
MNS MW-12D
2022000066
MCGUIRE
25-Jan-22
3:15 PM
Ethan Smith
MNS SW-1
2022000067
MCGUIRE
26-Jan-22
12:20 PM
Connor Zahora
MNS MW-4R
2022000068
MCGUIRE
26-Jan-22
1:30 PM
Connor Zahora
MNS MW-4DR
2022000069
MCGUIRE
26-Jan-22
11:05 AM
Ethan Smith
MNS MW-3BR
2022000070
MCGUIRE
26-Jan-22
10:10 AM
Connor Zahora
MNS MW-4BR
2022000071
MCGUIRE
26-Jan-22
1:55 PM
Connor Zahora
MNS MW-4BRR
2022000072
MCGUIRE
26-Jan-22
9:50AM
Ethan Smith
MNS MW-11BR
2022000073
MCGUIRE
26-Jan-22
2:00 PM
Ethan Smith
MNS MW-13D
2022000074
MCGUIRE
26-Jan-22
1:30 PM
Ethan Smith
MNS MW-13BR
2022000075
MCGUIRE
26-Jan-22
8:00 AM
Connor Zahora
MNS TB-20220126-0800
2022000076
MCGUIRE
26-Jan-22
11:00 AM
Connor Zahora
MNS FB-20220126-1100
2022000078
MCGUIRE
26-Jan-22
Ethan Smith
MNS FD-20220126-1
2022000079
MCGUIRE
24-Jan-22
9:30 AM
Ethan Smith
MNS TB-20220124-0930
2022000081
MCGUIRE
26-Jan-22
11:45 AM
Connor Zahora
MNS FB-20210126-1145
2022000082
MCGUIRE
24-Jan-22
4:00 PM
Ethan Smith
MNS FB-20220124-1600
2022000083
MCGUIRE
25-Jan-22
12:30 PM
Ethan Smith
MNS FB-20220125-1230
2022000084
MCGUIRE
25-Jan-22
Ethan Smith
MNS FD-20220125-1
29 Total Samples

Page 4 of 151
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals❑ Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
d❑ Job Summary Report
❑ Sample Identification
❑ Technical Validation of Data Package
d❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑ Chain of Custody
❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 2/18/2022

Certificate of Laboratory Analysis Page 5 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-1 Sample #: 2022000054
Collection Date: 01/25/2022 01:35 PM Loc code: MNS MW-1 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 53 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.1
mg/L
0.1
0.0154
1
Sulfate
0.33
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.227
mg/L
0.005
0.002
1
Calcium (Ca)
7.40
mg/L
0.05
0.012
1
Magnesium (Mg)
3.25
mg/L
0.02
0.008
1
Potassium (K)
1.64
mg/L
0.1
0.031
1
Sodium (Na)
6.36
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.138 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.214 J
ug/L
1
0.185
1
Lead (Pb)
0.052 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:34 EBATIAN
EPA 9056A
01/27/2022 13:43
BGN9034
EPA 9056A
01/27/2022 13:43
BGN9034
EPA 7470A
02/02/2022 13:47
JAA5429
SW 6010D
02/08/2022 15:11
DMFRANC
SW 6010D
02/08/2022 15:11
DMFRANC
SW 601OD
02/08/2022 15:11
DMFRANC
SW 6010D
02/08/2022 15:11
DMFRANC
SW 6010D
02/08/2022 15:11
DMFRANC
SW 6020B
02/01/2022 19:27
CWSPEN3
SW 6020B
02/01/2022 19:27
CWSPEN3
SW 6020B
02/01/2022 19:27
CWSPEN3
SW 6020B
02/01/2022 19:27
CWSPEN3
SW 6020B
02/01/2022 19:27
CWSPEN3
SW 6020B
02/01/2022 19:27
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 6 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-1 D Sample #: 2022000055
Collection Date: 01/25/2022 02:15 PM Loc code: MNS MW-1 D Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 49 mg/L 20 1.7 1 SM 2320B 01/28/2022 13:41 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.1
mg/L
0.1
0.0154
1
Sulfate
0.40
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.107
mg/L
0.005
0.002
1
Calcium (Ca)
7.69
mg/L
0.05
0.012
1
Magnesium (Mg)
2.60
mg/L
0.02
0.008
1
Potassium (K)
1.10
mg/L
0.1
0.031
1
Sodium (Na)
6.45
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.18 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.24 J
ug/L
1
0.185
1
Lead (Pb)
0.037 U
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
EPA 9056A
01/27/2022 14:27
BGN9034
EPA 9056A
01/27/2022 14:27
BGN9034
EPA 7470A
02/02/2022 13:54
JAA5429
SW 6010D
02/08/2022 15:25
DMFRANC
SW 6010D
02/08/2022 15:25
DMFRANC
SW 601OD
02/08/2022 15:25
DMFRANC
SW 6010D
02/08/2022 15:25
DMFRANC
SW 6010D
02/08/2022 15:25
DMFRANC
SW 6020B
02/01/2022 19:01
CWSPEN3
SW 6020B
02/01/2022 19:01
CWSPEN3
SW 6020B
02/01/2022 19:01
CWSPEN3
SW 6020B
02/01/2022 19:01
CWSPEN3
SW 6020B
02/01/2022 19:01
CWSPEN3
SW 6020B
02/01/2022 19:01
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-2A
Collection Date: 01/25/2022 11:45 AM Loc code: MNS MW-2A
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 74 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.3
mg/L
0.1
0.0154
1
Sulfate
0.68
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.052
mg/L
0.005
0.002
1
Calcium (Ca)
18.7
mg/L
0.05
0.012
1
Magnesium (Mg)
4.92
mg/L
0.02
0.008
1
Potassium (K)
1.91
mg/L
0.1
0.031
1
Sodium (Na)
7.79
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.86 J
ug/L
1
0.185
1
Lead (Pb)
1.39
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Sample #: 2022000056
Matrix: GW RCRA
Page 7 of 151
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:45 EBATIAN
EPA 9056A
01/27/2022 14:42
BGN9034
EPA 9056A
01/27/2022 14:42
BGN9034
EPA 7470A
02/02/2022 13:56
JAA5429
SW 6010D
02/08/2022 15:30
DMFRANC
SW 6010D
02/08/2022 15:30
DMFRANC
SW 601OD
02/08/2022 15:30
DMFRANC
SW 6010D
02/08/2022 15:30
DMFRANC
SW 6010D
02/08/2022 15:30
DMFRANC
SW 6020B
02/01/2022 19:36
CWSPEN3
SW 6020B
02/01/2022 19:36
CWSPEN3
SW 6020B
02/01/2022 19:36
CWSPEN3
SW 6020B
02/01/2022 19:36
CWSPEN3
SW 6020B
02/01/2022 19:36
CWSPEN3
SW 6020B
02/01/2022 19:36
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 8 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-2D Sample #: 2022000057
Collection Date: 01/25/2022 12:15 PM Loc code: MNS MW-2D Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 24.5 mg/L 5 1.7 1 SM 232064d 01/28/2022 16:45 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.2
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 14:57
BGN9034
Sulfate
0.36
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 14:57
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 13:58
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.014
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 15:34
DMFRANC
Calcium (Ca)
5.13
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 15:34
DMFRANC
Magnesium (Mg)
1.48
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 15:34
DMFRANC
Potassium (K)
0.427
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 15:34
DMFRANC
Sodium (Na)
5.09
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 15:34
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Chromium (Cr)
1.26
ug/L
1
0.185
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Lead (Pb)
0.138 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 19:44
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-3
Collection Date: 01/26/2022 12:35 PM Loc code: MNS MW-3
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 36 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.2
mg/L
0.1
0.0154
1
Sulfate
0.56
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.044
mg/L
0.005
0.002
1
Calcium (Ca)
6.77
mg/L
0.05
0.012
1
Magnesium (Mg)
2.83
mg/L
0.02
0.008
1
Potassium (K)
2.01
mg/L
0.1
0.031
1
Sodium (Na)
3.98
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.397 J
ug/L
1
0.185
1
Lead (Pb)
3.61
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Sample #: 2022000058
Matrix: GW RCRA
Page 9 of 151
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:48 EBATIAN
EPA 9056A
01/27/2022 15:12
BGN9034
EPA 9056A
01/27/2022 15:12
BGN9034
EPA 7470A
02/02/2022 14:01
JAA5429
SW 6010D
02/08/2022 15:39
DMFRANC
SW 6010D
02/08/2022 15:39
DMFRANC
SW 601OD
02/08/2022 15:39
DMFRANC
SW 6010D
02/08/2022 15:39
DMFRANC
SW 6010D
02/08/2022 15:39
DMFRANC
SW 6020B
02/01/2022 19:52
CWSPEN3
SW 6020B
02/01/2022 19:52
CWSPEN3
SW 6020B
02/01/2022 19:52
CWSPEN3
SW 6020B
02/01/2022 19:52
CWSPEN3
SW 6020B
02/01/2022 19:52
CWSPEN3
SW 6020B
02/01/2022 19:52
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-3D
Collection Date: 01/26/2022 12:00 PM Loc code: MNS MW-3D
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 73 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.5
mg/L
0.1
0.0154
1
Sulfate
0.74
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.036
mg/L
0.005
0.002
1
Calcium (Ca)
16.6
mg/L
0.05
0.012
1
Magnesium (Mg)
5.31
mg/L
0.02
0.008
1
Potassium (K)
0.990
mg/L
0.1
0.031
1
Sodium (Na)
6.82
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.625 J
ug/L
1
0.185
1
Lead (Pb)
0.039 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 10 of 151
Sample #: 2022000059
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:51 EBATIAN
EPA 9056A
01/27/2022 18:26
BGN9034
EPA 9056A
01/27/2022 18:26
BGN9034
EPA 7470A
02/02/2022 14:03
JAA5429
SW 6010D
02/08/2022 15:43
DMFRANC
SW 6010D
02/08/2022 15:43
DMFRANC
SW 601OD
02/08/2022 15:43
DMFRANC
SW 6010D
02/08/2022 15:43
DMFRANC
SW 6010D
02/08/2022 15:43
DMFRANC
SW 6020B
02/01/2022 20:01
CWSPEN3
SW 6020B
02/01/2022 20:01
CWSPEN3
SW 6020B
02/01/2022 20:01
CWSPEN3
SW 6020B
02/01/2022 20:01
CWSPEN3
SW 6020B
02/01/2022 20:01
CWSPEN3
SW 6020B
02/01/2022 20:01
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4
Collection Date: 01/26/2022 11:00 AM Loc code: MNS MW-4
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 69 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.9
mg/L
0.1
0.0154
1
Sulfate
0.70
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.067
mg/L
0.005
0.002
1
Calcium (Ca)
11.0
mg/L
0.05
0.012
1
Magnesium (Mg)
10.7
mg/L
0.02
0.008
1
Potassium (K)
0.454
mg/L
0.1
0.031
1
Sodium (Na)
2.13
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
1.11
ug/L
1
0.185
1
Lead (Pb)
0.037 U
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 11 of 151
Sample #: 2022000060
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:55 EBATIAN
EPA 9056A
01/27/2022 18:41
BGN9034
EPA 9056A
01/27/2022 18:41
BGN9034
EPA 7470A
02/02/2022 14:05
JAA5429
SW 6010D
02/08/2022 15:48
DMFRANC
SW 6010D
02/08/2022 15:48
DMFRANC
SW 601OD
02/08/2022 15:48
DMFRANC
SW 6010D
02/08/2022 15:48
DMFRANC
SW 6010D
02/08/2022 15:48
DMFRANC
SW 6020B
02/01/2022 20:09
CWSPEN3
SW 6020B
02/01/2022 20:09
CWSPEN3
SW 6020B
02/01/2022 20:09
CWSPEN3
SW 6020B
02/01/2022 20:09
CWSPEN3
SW 6020B
02/01/2022 20:09
CWSPEN3
SW 6020B
02/01/2022 20:09
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4D
Collection Date: 01/26/2022 11:30 AM Loc code: MNS MW-4D
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 130 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.9
mg/L
0.1
0.0154
1
Sulfate
0.31
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.051
mg/L
0.005
0.002
1
Calcium (Ca)
27.3
mg/L
0.05
0.012
1
Magnesium (Mg)
13.5
mg/L
0.02
0.008
1
Potassium (K)
0.763
mg/L
0.1
0.031
1
Sodium (Na)
4.42
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.164 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.232 J
ug/L
1
0.185
1
Lead (Pb)
0.037 U
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 12 of 151
Sample #: 2022000061
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 13:59 EBATIAN
EPA 9056A
01/27/2022 19:11
BGN9034
EPA 9056A
01/27/2022 19:11
BGN9034
EPA 7470A
02/02/2022 14:08
JAA5429
SW 6010D
02/08/2022 15:53
DMFRANC
SW 6010D
02/08/2022 15:53
DMFRANC
SW 601OD
02/08/2022 15:53
DMFRANC
SW 6010D
02/08/2022 15:53
DMFRANC
SW 6010D
02/08/2022 15:53
DMFRANC
SW 6020B
02/01/2022 20:17
CWSPEN3
SW 6020B
02/01/2022 20:17
CWSPEN3
SW 6020B
02/01/2022 20:17
CWSPEN3
SW 6020B
02/01/2022 20:17
CWSPEN3
SW 6020B
02/01/2022 20:17
CWSPEN3
SW 6020B
02/01/2022 20:17
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 13 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-11 Sample #: 2022000062
Collection Date: 01/24/2022 11:00 AM Loc code: MNS MW-11 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 49.2 mg/L 5 1.7 1 SM 232064d 01/28/2022 16:59 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.2
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 17:11
BGN9034
Sulfate
0.89
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 17:11
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 14:10
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.011
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 15:57
DMFRANC
Calcium (Ca)
3.31
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 15:57
DMFRANC
Magnesium (Mg)
3.11
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 15:57
DMFRANC
Potassium (K)
0.312
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 15:57
DMFRANC
Sodium (Na)
6.10
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 15:57
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.438 J
ug/L
1
0.111
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Chromium (Cr)
0.326 J
ug/L
1
0.185
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Lead (Pb)
0.088 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 20:52
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-11 D
Collection Date: 01/24/2022 10:30 AM Loc code: MNS MW-11D
Analyte Result Units Qualifiers RDL MDL DF
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 11.3 mg/L 5 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.3
mg/L
0.1
0.0154
1
Sulfate
0.58
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.033
mg/L
0.005
0.002
1
Calcium (Ca)
2.01
mg/L
0.05
0.012
1
Magnesium (Mg)
1.43
mg/L
0.02
0.008
1
Potassium (K)
0.379
mg/L
0.1
0.031
1
Sodium (Na)
3.27
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.81 J
ug/L
1
0.185
1
Lead (Pb)
0.35 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 14 of 151
Sample #: 2022000063
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 232064d 01/28/2022 17:07 EBATIAN
EPA 9056A
01/27/2022 17:26
BGN9034
EPA 9056A
01/27/2022 17:26
BGN9034
EPA 7470A
02/02/2022 14:12
JAA5429
SW 6010D
02/08/2022 16:02
DMFRANC
SW 6010D
02/08/2022 16:02
DMFRANC
SW 601OD
02/08/2022 16:02
DMFRANC
SW 6010D
02/08/2022 16:02
DMFRANC
SW 6010D
02/08/2022 16:02
DMFRANC
SW 6020B
02/01/2022 21:00
CWSPEN3
SW 6020B
02/01/2022 21:00
CWSPEN3
SW 6020B
02/01/2022 21:00
CWSPEN3
SW 6020B
02/01/2022 21:00
CWSPEN3
SW 6020B
02/01/2022 21:00
CWSPEN3
SW 6020B
02/01/2022 21:00
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 15 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-12 Sample #: 2022000064
Collection Date: 01/24/2022 12:45 PM Loc code: MNS MW-12 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 2.32 J mg/L 5 1.7 1 SM 232064d 01/28/2022 17:13 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
4.1
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 17:41
BGN9034
Sulfate
0.35
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 17:41
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 14:19
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.011
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 16:14
DMFRANC
Calcium (Ca)
1.14
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 16:14
DMFRANC
Magnesium (Mg)
0.558
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 16:14
DMFRANC
Potassium (K)
0.421
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 16:14
DMFRANC
Sodium (Na)
1.84
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 16:14
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Chromium (Cr)
0.287 J
ug/L
1
0.185
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Lead (Pb)
0.156 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 21:08
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-12D
Collection Date: 01/24/2022 01:30 PM Loc code: MNS MW-12D
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 39 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
3.5
mg/L
0.1
0.0154
1
Sulfate
0.08 J
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.010
mg/L
0.005
0.002
1
Calcium (Ca)
9.13
mg/L
0.05
0.012
1
Magnesium (Mg)
1.34
mg/L
0.02
0.008
1
Potassium (K)
0.321
mg/L
0.1
0.031
1
Sodium (Na)
7.50
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.394 J
ug/L
1
0.185
1
Lead (Pb)
0.053 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 16 of 151
Sample #: 2022000065
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:02 EBATIAN
EPA 9056A
01/27/2022 17:56
BGN9034
EPA 9056A
01/27/2022 17:56
BGN9034
EPA 7470A
02/02/2022 14:26
JAA5429
SW 6010D
02/08/2022 16:19
DMFRANC
SW 6010D
02/08/2022 16:19
DMFRANC
SW 601OD
02/08/2022 16:19
DMFRANC
SW 6010D
02/08/2022 16:19
DMFRANC
SW 6010D
02/08/2022 16:19
DMFRANC
SW 6020B
02/01/2022 21:17
CWSPEN3
SW 6020B
02/01/2022 21:17
CWSPEN3
SW 6020B
02/01/2022 21:17
CWSPEN3
SW 6020B
02/01/2022 21:17
CWSPEN3
SW 6020B
02/01/2022 21:17
CWSPEN3
SW 6020B
02/01/2022 21:17
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS SW-1
Collection Date: 01/25/2022 03:15 PM Loc code: MNS SW-1
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 41 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
3.1
mg/L
0.1
0.0154
1
Sulfate
2.2
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED) - Q22010468
Barium (Ba)
0.025
mg/L
0.005
0.002
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.025
mg/L
0.005
0.002
1
Calcium (Ca)
8.61
mg/L
0.05
0.012
1
Magnesium (Mg)
3.47
mg/L
0.02
0.008
1
Potassium (K)
1.04
mg/L
0.1
0.031
1
Sodium (Na)
5.21
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
- Q22010477
Arsenic (As)
0.114 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.185 U
ug/L
1
0.185
1
Lead (Pb)
0.037 U
ug/L
1
0.037
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.154 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.669 J
ug/L
1
0.185
1
Lead (Pb)
0.195 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed
by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 17 of 151
Sample #: 2022000066
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:06 EBATIAN
EPA 9056A
01/27/2022 15:27
BGN9034
EPA 9056A
01/27/2022 15:27
BGN9034
EPA 7470A
02/02/2022 14:28
JAA5429
SW 6010D
02/08/2022 17:05
DMFRANC
SW 6010D
02/08/2022 16:23
DMFRANC
SW 6010D
02/08/2022 16:23
DMFRANC
SW 601OD
02/08/2022 16:23
DMFRANC
SW 601OD
02/08/2022 16:23
DMFRANC
SW 601OD
02/08/2022 16:23
DMFRANC
SW 6020B
02/02/2022 16:25
CWSPEN3
SW 6020B
02/02/2022 16:25
CWSPEN3
SW 6020B
02/02/2022 16:25
CWSPEN3
SW 6020B
02/02/2022 16:25
CWSPEN3
SW 6020B
02/02/2022 16:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
SW 6020B
02/01/2022 21:25
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4R
Collection Date: 01/26/2022 12:20 PM Loc code: MNS MW-4R
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 66 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.8
mg/L
0.1
0.0154
1
Sulfate
0.25
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.010
mg/L
0.005
0.002
1
Calcium (Ca)
12.1
mg/L
0.05
0.012
1
Magnesium (Mg)
8.98
mg/L
0.02
0.008
1
Potassium (K)
0.346
mg/L
0.1
0.031
1
Sodium (Na)
2.83
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.897 J
ug/L
1
0.185
1
Lead (Pb)
0.07 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 18 of 151
Sample #: 2022000067
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:09 EBATIAN
EPA 9056A
01/27/2022 20:25
BGN9034
EPA 9056A
01/27/2022 20:25
BGN9034
EPA 7470A
02/02/2022 14:30
JAA5429
SW 6010D
02/08/2022 16:28
DMFRANC
SW 6010D
02/08/2022 16:28
DMFRANC
SW 601OD
02/08/2022 16:28
DMFRANC
SW 6010D
02/08/2022 16:28
DMFRANC
SW 6010D
02/08/2022 16:28
DMFRANC
SW 6020B
02/01/2022 21:33
CWSPEN3
SW 6020B
02/01/2022 21:33
CWSPEN3
SW 6020B
02/01/2022 21:33
CWSPEN3
SW 6020B
02/01/2022 21:33
CWSPEN3
SW 6020B
02/01/2022 21:33
CWSPEN3
SW 6020B
02/01/2022 21:33
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4DR
Collection Date: 01/26/2022 01:30 PM Loc code: MNS MW-4DR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 69 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.7
mg/L
0.1
0.0154
1
Sulfate
0.92
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.015
mg/L
0.005
0.002
1
Calcium (Ca)
15.8
mg/L
0.05
0.012
1
Magnesium (Mg)
4.72
mg/L
0.02
0.008
1
Potassium (K)
0.758
mg/L
0.1
0.031
1
Sodium (Na)
6.90
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
1.53
ug/L
1
0.185
1
Lead (Pb)
0.197 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 19 of 151
Sample #: 2022000068
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:13 EBATIAN
EPA 9056A
01/27/2022 20:40
BGN9034
EPA 9056A
01/27/2022 20:40
BGN9034
EPA 7470A
02/02/2022 14:32
JAA5429
SW 6010D
02/08/2022 16:33
DMFRANC
SW 6010D
02/08/2022 16:33
DMFRANC
SW 601OD
02/08/2022 16:33
DMFRANC
SW 6010D
02/08/2022 16:33
DMFRANC
SW 6010D
02/08/2022 16:33
DMFRANC
SW 6020B
02/01/2022 21:42
CWSPEN3
SW 6020B
02/01/2022 21:42
CWSPEN3
SW 6020B
02/01/2022 21:42
CWSPEN3
SW 6020B
02/01/2022 21:42
CWSPEN3
SW 6020B
02/01/2022 21:42
CWSPEN3
SW 6020B
02/01/2022 21:42
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-3BR
Collection Date: 01/26/2022 11:05 AM Loc code: MNS MW-3BR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 110 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.0
mg/L
0.1
0.0154
1
Sulfate
3.7
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.088
mg/L
0.005
0.002
1
Calcium (Ca)
25.6
mg/L
0.05
0.012
1
Magnesium (Mg)
6.19
mg/L
0.02
0.008
1
Potassium (K)
6.01
mg/L
0.1
0.031
1
Sodium (Na)
11.3
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.421 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.262 J
ug/L
1
0.185
1
Lead (Pb)
0.147 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 20 of 151
Sample #: 2022000069
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:16 EBATIAN
EPA 9056A
01/27/2022 20:55
BGN9034
EPA 9056A
01/27/2022 20:55
BGN9034
EPA 7470A
02/02/2022 14:35
JAA5429
SW 6010D
02/08/2022 16:37
DMFRANC
SW 6010D
02/08/2022 16:37
DMFRANC
SW 601OD
02/08/2022 16:37
DMFRANC
SW 6010D
02/08/2022 16:37
DMFRANC
SW 6010D
02/08/2022 16:37
DMFRANC
SW 6020B
02/01/2022 21:50
CWSPEN3
SW 6020B
02/01/2022 21:50
CWSPEN3
SW 6020B
02/01/2022 21:50
CWSPEN3
SW 6020B
02/01/2022 21:50
CWSPEN3
SW 6020B
02/01/2022 21:50
CWSPEN3
SW 6020B
02/01/2022 21:50
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4BR
Collection Date: 01/26/2022 10:10 AM Loc code: MNS MW-4BR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 110 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
3.5
mg/L
0.1
0.0154
1
Sulfate
33
mg/L
1
0.0428
10
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.012
mg/L
0.005
0.002
1
Calcium (Ca)
6.48
mg/L
0.05
0.012
1
Magnesium (Mg)
2.99
mg/L
0.02
0.008
1
Potassium (K)
27.0
mg/L
2
0.031
20
Sodium (Na)
44.9
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
0.67 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
1.32
ug/L
1
0.185
1
Lead (Pb)
0.077 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 21 of 151
Sample #: 2022000070
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:20 EBATIAN
EPA 9056A
01/28/2022 00:53
BGN9034
EPA 9056A
01/28/2022 00:53
BGN9034
EPA 7470A
02/02/2022 14:37
JAA5429
SW 6010D
02/08/2022 16:42
DMFRANC
SW 6010D
02/08/2022 16:42
DMFRANC
SW 601OD
02/08/2022 16:42
DMFRANC
SW 6010D
02/08/2022 16:42
DMFRANC
SW 6010D
02/08/2022 16:42
DMFRANC
SW 6020B
02/01/2022 21:58
CWSPEN3
SW 6020B
02/01/2022 21:58
CWSPEN3
SW 6020B
02/01/2022 21:58
CWSPEN3
SW 6020B
02/01/2022 21:58
CWSPEN3
SW 6020B
02/01/2022 21:58
CWSPEN3
SW 6020B
02/01/2022 21:58
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-4BRR
Collection Date: 01/26/2022 01:55 PM Loc code: MNS MW-4BRR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 540 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
43
mg/L
2
0.0154
20
Sulfate
1000
mg/L
20
0.0428
200
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010440
Barium (Ba)
0.086
mg/L
0.005
0.002
1
Calcium (Ca)
8.05
mg/L
0.05
0.012
1
Magnesium (Mg)
0.169
mg/L
0.02
0.008
1
Potassium (K)
159
mg/L
2
0.031
20
Sodium (Na)
629
mg/L
1
0.017
20
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010448
Arsenic (As)
6.46
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
1.22
ug/L
1
0.185
1
Lead (Pb)
0.214 J
ug/L
1
0.037
1
Selenium (Se)
0.4 J
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 22 of 151
Sample #: 2022000071
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:24 EBATIAN
EPA 9056A
01/28/2022 01:37
BGN9034
EPA 9056A
01/28/2022 01:37
BGN9034
EPA 7470A
02/02/2022 14:39
JAA5429
SW 6010D
02/08/2022 16:46
DMFRANC
SW 6010D
02/08/2022 16:46
DMFRANC
SW 601OD
02/08/2022 16:46
DMFRANC
SW 6010D
02/08/2022 16:46
DMFRANC
SW 6010D
02/08/2022 16:46
DMFRANC
SW 6020B
02/01/2022 22:07
CWSPEN3
SW 6020B
02/01/2022 22:07
CWSPEN3
SW 6020B
02/01/2022 22:07
CWSPEN3
SW 6020B
02/01/2022 22:07
CWSPEN3
SW 6020B
02/01/2022 22:07
CWSPEN3
SW 6020B
02/01/2022 22:07
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-11 BR
Collection Date: 01/26/2022 09:50 AM Loc code: MNS MW-11 BR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 54 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.5
mg/L
0.1
0.0154
1
Sulfate
3.0
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.010
mg/L
0.005
0.002
1
Calcium (Ca)
8.65
mg/L
0.05
0.012
1
Magnesium (Mg)
2.02
mg/L
0.02
0.008
1
Potassium (K)
2.52
mg/L
0.1
0.031
1
Sodium (Na)
12.4
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.116 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
1.02
ug/L
1
0.185
1
Lead (Pb)
0.125 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 23 of 151
Sample #: 2022000072
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:31 EBATIAN
EPA 9056A
01/28/2022 01:08
BGN9034
EPA 9056A
01/28/2022 01:08
BGN9034
EPA 7470A
02/02/2022 14:41
JAA5429
SW 6010D
02/08/2022 13:55
DMFRANC
SW 6010D
02/08/2022 13:55
DMFRANC
SW 601OD
02/08/2022 13:55
DMFRANC
SW 6010D
02/08/2022 13:55
DMFRANC
SW 6010D
02/08/2022 13:55
DMFRANC
SW 6020B
02/01/2022 17:02
CWSPEN3
SW 6020B
02/01/2022 17:02
CWSPEN3
SW 6020B
02/01/2022 17:02
CWSPEN3
SW 6020B
02/01/2022 17:02
CWSPEN3
SW 6020B
02/01/2022 17:02
CWSPEN3
SW 6020B
02/01/2022 17:02
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-13D
Collection Date: 01/26/2022 02:00 PM Loc code: MNS MW-13D
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 47 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.4
mg/L
0.1
0.0154
1
Sulfate
0.66
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.018
mg/L
0.005
0.002
1
Calcium (Ca)
9.98
mg/L
0.05
0.012
1
Magnesium (Mg)
3.63
mg/L
0.02
0.008
1
Potassium (K)
0.641
mg/L
0.1
0.031
1
Sodium (Na)
5.27
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.173 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.57 J
ug/L
1
0.185
1
Lead (Pb)
0.13 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 24 of 151
Sample #: 2022000073
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:35 EBATIAN
EPA 9056A
01/27/2022 22:24
BGN9034
EPA 9056A
01/27/2022 22:24
BGN9034
EPA 7470A
02/02/2022 14:44
JAA5429
SW 6010D
02/08/2022 14:13
DMFRANC
SW 6010D
02/08/2022 14:13
DMFRANC
SW 601OD
02/08/2022 14:13
DMFRANC
SW 6010D
02/08/2022 14:13
DMFRANC
SW 6010D
02/08/2022 14:13
DMFRANC
SW 6020B
02/01/2022 16:28
CWSPEN3
SW 6020B
02/01/2022 16:28
CWSPEN3
SW 6020B
02/01/2022 16:28
CWSPEN3
SW 6020B
02/01/2022 16:28
CWSPEN3
SW 6020B
02/01/2022 16:28
CWSPEN3
SW 6020B
02/01/2022 16:28
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS MW-13BR
Collection Date: 01/26/2022 01:30 PM Loc code: MNS MW-13BR
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 92 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.2
mg/L
0.1
0.0154
1
Sulfate
9.7
mg/L
0.5
0.0428
5
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.004 J
mg/L
0.005
0.002
1
Calcium (Ca)
23.5
mg/L
0.05
0.012
1
Magnesium (Mg)
4.87
mg/L
0.02
0.008
1
Potassium (K)
2.52
mg/L
0.1
0.031
1
Sodium (Na)
10.6
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.271 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.635 J
ug/L
1
0.185
1
Lead (Pb)
0.264 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 25 of 151
Sample #: 2022000074
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:38 EBATIAN
EPA 9056A
01/28/2022 01:23
BGN9034
EPA 9056A
01/28/2022 01:23
BGN9034
EPA 7470A
02/02/2022 14:55
JAA5429
SW 6010D
02/08/2022 14:17
DMFRANC
SW 6010D
02/08/2022 14:17
DMFRANC
SW 601OD
02/08/2022 14:17
DMFRANC
SW 6010D
02/08/2022 14:17
DMFRANC
SW 6010D
02/08/2022 14:17
DMFRANC
SW 6020B
02/01/2022 17:11
CWSPEN3
SW 6020B
02/01/2022 17:11
CWSPEN3
SW 6020B
02/01/2022 17:11
CWSPEN3
SW 6020B
02/01/2022 17:11
CWSPEN3
SW 6020B
02/01/2022 17:11
CWSPEN3
SW 6020B
02/01/2022 17:11
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS_TB-20220126-0800 Trip Blank
Collection Date: 01/26/2022 08:00 AM Loc code: MNS TB
Analyte Result Units Qualifiers RDL MDL DF
Miscellaneous Tests by a Vendor Laboratory - (Analysis Performed bV Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene Complete
Page 26 of 151
Sample #: 2022000075
Matrix: GW RCRA
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis Page 27 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS FB-20220126-1100 Field Blank Sample #: 2022000076
Collection Date: 01/26/2022 11:00 AM Loc code: MNS QA Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 1.7 U mg/L 5 1.7 1 SM 232064d 01/28/2022 17:19 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
0.04 J
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 23:53
BGN9034
Sulfate
0.0428 U
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 23:53
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 15:02
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.002 U
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 14:22
DMFRANC
Calcium (Ca)
0.012 U
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 14:22
DMFRANC
Magnesium (Mg)
0.008 U
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 14:22
DMFRANC
Potassium (K)
0.031 U
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 14:22
DMFRANC
Sodium (Na)
0.017 U
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 14:22
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Chromium (Cr)
0.185 U
ug/L
1
0.185
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Lead (Pb)
0.133 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 17:19
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS_FD-20220126-1 Duplicate
Collection Date: 01/26/2022 Loc code: MNS FD
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 110 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
2.1
mg/L
1
0.0154
10
Sulfate
3.1
mg/L
1
0.0428
10
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.085
mg/L
0.005
0.002
1
Calcium (Ca)
24.4
mg/L
0.05
0.012
1
Magnesium (Mg)
5.97
mg/L
0.02
0.008
1
Potassium (K)
6.82
mg/L
0.1
0.031
1
Sodium (Na)
11.3
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.388 J
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.55 J
ug/L
1
0.185
1
Lead (Pb)
0.201 J
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 28 of 151
Sample #: 2022000078
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:42 EBATIAN
EPA 9056A
01/28/2022 00:38
BGN9034
EPA 9056A
01/28/2022 00:38
BGN9034
EPA 7470A
02/02/2022 15:04
JAA5429
SW 6010D
02/08/2022 14:27
DMFRANC
SW 6010D
02/08/2022 14:27
DMFRANC
SW 601OD
02/08/2022 14:27
DMFRANC
SW 6010D
02/08/2022 14:27
DMFRANC
SW 6010D
02/08/2022 14:27
DMFRANC
SW 6020B
02/01/2022 17:27
CWSPEN3
SW 6020B
02/01/2022 17:27
CWSPEN3
SW 6020B
02/01/2022 17:27
CWSPEN3
SW 6020B
02/01/2022 17:27
CWSPEN3
SW 6020B
02/01/2022 17:27
CWSPEN3
SW 6020B
02/01/2022 17:27
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS_TB-20220124-0930 Trip Blank
Collection Date: 01/24/2022 09:30 AM Loc code: MNS TB
Analyte Result Units Qualifiers RDL MDL DF
Miscellaneous Tests by a Vendor Laboratory - (Analysis Performed bV Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene Complete
Page 29 of 151
Sample #: 2022000079
Matrix: GW RCRA
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis Page 30 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS FB-20210126-1145 Field Blank Sample #: 2022000081
Collection Date: 01/26/2022 11:45 AM Loc code: MNS QA Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 1.7 U mg/L 5 1.7 1 SM 232064d 01/28/2022 17:48 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
0.07 J
mg/L
0.1
0.0154
1
EPA 9056A
01/28/2022 00:08
BGN9034
Sulfate
0.0428 U
mg/L
0.1
0.0428
1
EPA 9056A
01/28/2022 00:08
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 15:06
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.002 U
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 14:31
DMFRANC
Calcium (Ca)
0.012 U
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 14:31
DMFRANC
Magnesium (Mg)
0.008 U
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 14:31
DMFRANC
Potassium (K)
0.031 U
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 14:31
DMFRANC
Sodium (Na)
0.017 U
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 14:31
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Chromium (Cr)
0.185 U
ug/L
1
0.185
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Lead (Pb)
0.125 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 17:36
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 31 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS FB-20220124-1600 Field Blank Sample #: 2022000082
Collection Date: 01/24/2022 04:00 PM Loc code: MNS QA Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 1.7 U mg/L 5 1.7 1 SM 232064d 01/28/2022 17:52 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
0.0154 U
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 18:11
BGN9034
Sulfate
0.0428 U
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 18:11
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 15:08
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.002 U
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 14:36
DMFRANC
Calcium (Ca)
0.012 U
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 14:36
DMFRANC
Magnesium (Mg)
0.008 U
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 14:36
DMFRANC
Potassium (K)
0.031 U
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 14:36
DMFRANC
Sodium (Na)
0.017 U
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 14:36
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Chromium (Cr)
0.185 U
ug/L
1
0.185
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Lead (Pb)
0.111 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 17:44
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis Page 32 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS FB-20220125-1230 Field Blank Sample #: 2022000083
Collection Date: 01/25/2022 12:30 PM Loc code: MNS QA Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
LOW LEVEL ALKALINITY (FIXED END POINT) - Q22010451
Total Alkalinity as CaCO3 1.7 U mg/L 5 1.7 1 SM 232064d 01/28/2022 17:57 EBATIAN
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
0.0154 U
mg/L
0.1
0.0154
1
EPA 9056A
01/27/2022 15:42
BGN9034
Sulfate
0.0428 U
mg/L
0.1
0.0428
1
EPA 9056A
01/27/2022 15:42
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
EPA 7470A
02/02/2022 15:11
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.002 U
mg/L
0.005
0.002
1
SW 6010D
02/08/2022 14:40
DMFRANC
Calcium (Ca)
0.012 U
mg/L
0.05
0.012
1
SW 6010D
02/08/2022 14:40
DMFRANC
Magnesium (Mg)
0.008 U
mg/L
0.02
0.008
1
SW 601OD
02/08/2022 14:40
DMFRANC
Potassium (K)
0.031 U
mg/L
0.1
0.031
1
SW 6010D
02/08/2022 14:40
DMFRANC
Sodium (Na)
0.017 U
mg/L
0.05
0.017
1
SW 6010D
02/08/2022 14:40
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.111 U
ug/L
1
0.111
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Chromium (Cr)
0.185 U
ug/L
1
0.185
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Lead (Pb)
0.111 J
ug/L
1
0.037
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Selenium (Se)
0.193 U
ug/L
1
0.193
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
02/01/2022 17:53
CWSPEN3
Miscellaneous Tests by
a Vendor Laboratory
- (Analysis Performed by Pace Laboratories)
Vendor Parameter
Complete
Vendor Method
V_PACE
VOLATILES - (Analysis Performed by Pace Laboratories)
Benzene
Complete
Vendor Method
V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22010014
Site: MNS_FD-20220125-1 Duplicate
Collection Date: 01/25/2022 Loc code: MNS FD
Analyte Result Units Qualifiers RDL MDL DF
ALKALINITY (FIXED END POINT 4.5) - Q22010424
Total Alkalinity as CaCO3 79 mg/L 20 1.7 1
(CaCO3)
INORGANIC IONS BY IC - Q22010416
Chloride
1.4
mg/L
0.1
0.0154
1
Sulfate
0.73
mg/L
0.1
0.0428
1
MERCURY (COLD VAPOR) IN WATER - Q22020098
Mercury (Hg)
0.01 U
ug/L
0.05
0.01
1
TOTAL RECOVERABLE METALS BY ICP - Q22010439
Barium (Ba)
0.052
mg/L
0.005
0.002
1
Calcium (Ca)
18.8
mg/L
0.05
0.012
1
Magnesium (Mg)
4.93
mg/L
0.02
0.008
1
Potassium (K)
1.98
mg/L
0.1
0.031
1
Sodium (Na)
7.77
mg/L
0.05
0.017
1
TOTAL RECOVERABLE METALS BY ICP-MS - Q22010447
Arsenic (As)
0.111 U
ug/L
1
0.111
1
Cadmium (Cd)
0.032 U
ug/L
1
0.032
1
Chromium (Cr)
0.697 J
ug/L
1
0.185
1
Lead (Pb)
1.53
ug/L
1
0.037
1
Selenium (Se)
0.193 U
ug/L
1
0.193
1
Silver (Ag)
0.035 U
ug/L
1
0.035
1
Miscellaneous Tests by
a Vendor Laboratory
- (Analvsis Performed by Pace Laboratories)
Vendor Parameter Complete
VOLATILES - (Analysis Performed by Pace Laboratories
Benzene Complete
Page 33 of 151
Sample #: 2022000084
Matrix: GW RCRA
Method Analysis Date/Time Analyst
SM 2320B 01/28/2022 14:45 EBATIAN
EPA 9056A
01/27/2022 16:56
BGN9034
EPA 9056A
01/27/2022 16:56
BGN9034
EPA 7470A
02/02/2022 15:13
JAA5429
SW 6010D
02/08/2022 14:45
DMFRANC
SW 6010D
02/08/2022 14:45
DMFRANC
SW 601OD
02/08/2022 14:45
DMFRANC
SW 6010D
02/08/2022 14:45
DMFRANC
SW 6010D
02/08/2022 14:45
DMFRANC
SW 6020B
02/01/2022 18:01
CWSPEN3
SW 6020B
02/01/2022 18:01
CWSPEN3
SW 6020B
02/01/2022 18:01
CWSPEN3
SW 6020B
02/01/2022 18:01
CWSPEN3
SW 6020B
02/01/2022 18:01
CWSPEN3
SW 6020B
02/01/2022 18:01
CWSPEN3
Vendor Method
V_PACE
Vendor Method
V_PACE
Qualifiers:
J Analyte detected above the MDL, but below the RL. Analyte concentration should be considered an estimate.

Certificate of Laboratory Analysis Page 34 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
022010424 ALK FIX4.5 ALKALINITY (FIXED END POINT 4.5)
Duplicate # 1
Parameter Measured Final
Total Alkalinity as CaCO3 53.4
LCS # 1
Parameter Measured Final
Total Alkalinity as CaCO3 104
LCS # 2
Parameter Measured Final
Total Alkalinity as CaCO3 97.3
LCS # 3
Parameter Measured Final
Total Alkalinity as CaCO3 97
LCS # 4
Parameter Measured Final
Total Alkalinity as CaCO3 96.9
LCS # 5
Parameter Measured Final
Total Alkalinity as CaCO3 96.8
Parent Sample: J22010014 -- 2022000054
Units Dil MDL RPD Qualifier
mg/L 1 1.7 1.22
(CaCO3)
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
1.7
95.5
109
85
115
(CaCO3)
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
1.7
95.5
102
85
115
(CaCO3)
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
1.7
95.5
102
85
115
(CaCO3)
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
1.7
95.5
101
85
115
(CaCO3)
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
1.7
95.5
101
85
115
(CaCO3)

Certificate of Laboratory Analysis Page 35 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010451 ALK_LL_Fix LOW LEVEL ALKALINITY (FIXED END POINT)
Duplicate # 1
Parent Sample: J22010014 -- 2022000057
Parameter Measured
Final
Units
Dil
MDL RPD Qualifier
Total Alkalinity as CaCO3
24.7
mg/L
1
1.7 0.935
LCS # 1
Parameter Measured
Final
Units
Dil
MDL Spike % Recovery LCL UCL Qualifier
Total Alkalinity as CaCO3
48.4
mg/L
1
1.7 50.9 95.1 85 115
(CaCO3)

Certificate of Laboratory Analysis Page 36 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010416 Dionex INORGANIC IONS BY IC
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Chloride
0
0
mg/L
1
0.0154
0.1
< MDL
Sulfate
0
0
mg/L
1
0.0428
0.1
< MDL
LCS # 1
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Chloride
5.01
5.01
mg/L
1
0.0154
5
100
90 110
Sulfate
4.79
4.79
mg/L
1
0.0428
5
95.8
90 110
MS # 1
Parent Sample:
J22010014 -- 2022000054
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL UCL
Qualifier
Chloride
4.33
4.33
mg/L
1
0.0154
2
111
80 120
Sulfate
2.42
2.42
mg/L
1
0.0428
2
104
80 120
MSD # 1
Parent Sample:
J22010014 -- 2022000054
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL UCL RPD
Qualifier
Chloride
4.39
4.39
mg/L
1
0.0154
2
114
80 120 2.85
Sulfate
2.46
2.46
mg/L
1
0.0428
2
106
80 120 1.95
MS # 2
Parent Sample:
J22010014 -- 2022000069
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Chloride
4.05
4.05
mg/L
1
0.0154
2
101
80 120
Sulfate
5.74
5.74
mg/L
1
0.0428
2
99.8
80 120
MSD # 2
Parent Sample:
J22010014 -- 2022000069
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL RPD
Qualifier
Chloride
4.07
4.07
mg/L
1
0.0154
2
103
80 120 1.18
Sulfate
5.77
5.77
mg/L
1
0.0428
2
102
80 120 1.79

Certificate of Laboratory Analysis Page 37 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22020098 HG 7470 MERCURY (COLD VAPOR) IN WATER
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
-0.025
-0.025
ug/L
1
0.01
0.05
< MDL
Blank # 2
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
-0.02
-0.02
ug/L
1
0.01
0.05
< MDL
Blank # 3
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
-0.024
-0.024
ug/L
1
0.01
0.05
< MDL
Blank # 4
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
-0.032
-0.032
ug/L
1
0.01
0.05
< MDL
LCS # 1
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery LCL UCL
Qualifier
Mercury (Hg)
1.98
1.98
ug/L
1
0.01
2
98.8 85 115
LCS # 2
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
1.96
1.96
ug/L
1
0.01
2
98
85 115
MS # 1
Parent Sample:
J22010014 -- 2022000054
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.927
0.927
ug/L
1
0.01
1
92.7
75 125
MSD # 1
Parent Sample:
J22010014 -- 2022000054
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL RPD
Qualifier
Mercury (Hg)
0.939
0.939
ug/L
1
0.01
1
93.9
75 125 1.29
MS # 2
Parent Sample:
J22010014 -- 2022000064
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.948
0.948
ug/L
1
0.01
1
94.8
75 125
MSD # 2
Parent Sample:
J22010014 -- 2022000064
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL RPD
Qualifier
Mercury (Hg)
0.93
0.93
ug/L
1
0.01
1
93
75 125 1.92
MS # 3
Parent Sample:
J22010014 -- 2022000074
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.908
0.908
ug/L
1
0.01
1
90.8
75 125

Certificate of Laboratory Analysis Page 38 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22020098 HG 7470 MERCURY (COLD VAPOR) IN WATER
MSD # 3 Parent Sample: J22010014 -- 2022000074
Parameter Measured Final Units Dil MDL Spike % Recovery LCL UCL RPD Qualifier
Mercury (Hg) 0.916 0.916 ug/L 1 0.01 1 91.6 75 125 0.877

Certificate of Laboratory Analysis Page 39 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010468 ICP_DIS_TRM TOTAL RECOVERABLE METALS BY ICP (DISSOLVED)
Blank # 1
LCS # 1
Parameter Measured Final
Barium (Ba)-0.000177-0.000177
Parameter Measured Final
Barium (Ba) 5.14 5.14
LCSD # 1
Parameter Measured Final
Barium (Ba) 5.16 5.16
Units Dil MDL RDL Relative Concentration
mg/L 1 0.002 0.005 < MDL
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 0.002 5 103 80 120
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 0.002 5 103 80 120
Qualifier
Qualifier
RPD Qualifier
0.446

Certificate of Laboratory Analysis Page 40 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010439 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units
Barium (Ba)
-0.000117
-0.000117
mg/L
Calcium (Ca)
0.00188
0.00188
mg/L
Magnesium (Mg)
-0.00144
-0.00144
mg/L
Potassium (K)
0.00571
0.00571
mg/L
Sodium (Na)
0.00829
0.00829
mg/L
LCS # 1
MS # 1
Parameter
Measured
Final
Units
Barium (Ba)
5.04
5.04
mg/L
Calcium (Ca)
4.89
4.89
mg/L
Magnesium (Mg)
4.95
4.95
mg/L
Potassium (K)
4.98
4.98
mg/L
Sodium (Na)
4.94
4.94
mg/L
Parameter
Measured
Final
Units
Barium (Ba)
5.06
5.06
mg/L
Calcium (Ca)
13.7
13.7
mg/L
Magnesium (Mg)
6.88
6.88
mg/L
Potassium (K)
7.46
7.46
mg/L
Sodium (Na)
16.6
16.6
mg/L
MSD # 1
Parameter
Measured
Final
Units
Barium (Ba)
5.09
5.09
mg/L
Calcium (Ca)
13.8
13.8
mg/L
Magnesium (Mg)
6.92
6.92
mg/L
Potassium (K)
7.52
7.52
mg/L
Sodium (Na)
16.7
16.7
mg/L
Dil
MDL
RDL
Relative Concentration
1
0.002
0.005
< MDL
1
0.012
0.05
< MDL
1
0.008
0.02
< MDL
1
0.031
0.1
< MDL
1
0.017
0.05
< MDL
Dil
MDL
S ike
% Recovery
LCL
UCL
1
0.002
5
101
80
120
1
0.012
5
97.7
80
120
1
0.008
5
98.9
80
120
1
0.031
5
99.6
80
120
1
0.017
5
98.8
80
120
Parent Sample:
J22010014 -- 2022000072
DiI
MDL
Spike
% Recovery
LCL
UCL
1
0.002
5
101
75
125
1
0.012
5
102
75
125
1
0.008
5
97.1
75
125
1
0.031
5
98.8
75
125
1
0.017
5
84.5
75
125
Parent Sample:
J22010014 -- 2022000072
Dil
MDL
S ike
% Recovery
LCL
UCL
RPD
1
0.002
5
102
75
125
0.67
1
0.012
5
104
75
125
0.725
1
0.008
5
98
75
125
0.696
1
0.031
5
99.9
75
125
0.748
1
0.017
5
87.4
75
125
0.888
Qualifier
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 41 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010440 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units
Barium (Ba)
-0.00012
-0.00012
mg/L
Calcium (Ca)
0.00224
0.00224
mg/L
Magnesium (Mg)
-0.00246
-0.00246
mg/L
Potassium (K)
0.00134
0.00134
mg/L
Sodium (Na)
0.015
0.015
mg/L
LCS # 1
MS # 1
Parameter
Measured
Final
Units
Barium (Ba)
5.14
5.14
mg/L
Calcium (Ca)
4.92
4.92
mg/L
Magnesium (Mg)
5
5
mg/L
Potassium (K)
5.05
5.05
mg/L
Sodium (Na)
4.99
4.99
mg/L
Parameter
Measured
Final
Units
Barium (Ba)
5.28
5.28
mg/L
Calcium (Ca)
12.5
12.5
mg/L
Magnesium (Mg)
8.12
8.12
mg/L
Potassium (K)
6.6
6.6
mg/L
Sodium (Na)
11.2
11.2
mg/L
MSD # 1
Parameter
Measured
Final
Units
Barium (Ba)
5.31
5.31
mg/L
Calcium (Ca)
12.5
12.5
mg/L
Magnesium (Mg)
8.09
8.09
mg/L
Potassium (K)
6.62
6.62
mg/L
Sodium (Na)
11.3
11.3
mg/L
Dil
MDL
RDL
Relative Concentration
1
0.002
0.005
< MDL
1
0.012
0.05
< MDL
1
0.008
0.02
< MDL
1
0.031
0.1
< MDL
1
0.017
0.05
< MDL
Dil
MDL
S ike
% Recovery
LCL
UCL
1
0.002
5
103
80
120
1
0.012
5
98.3
80
120
1
0.008
5
100
80
120
1
0.031
5
101
80
120
1
0.017
5
99.8
80
120
Parent Sample:
J22010014 -- 2022000054
DiI
MDL
Spike
% Recovery
LCL
UCL
1
0.002
5
101
75
125
1
0.012
5
102
75
125
1
0.008
5
97.3
75
125
1
0.031
5
99.1
75
125
1
0.017
5
97.6
75
125
Parent Sample:
J22010014 -- 2022000054
Dil
MDL
S ike
% Recovery
LCL
UCL
RPD
1
0.002
5
102
75
125
0.548
1
0.012
5
101
75
125
0.16
1
0.008
5
96.8
75
125
0.333
1
0.031
5
99.4
75
125
0.212
1
0.017
5
98
75
125
0.16
Qualifier
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 42 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010477 IMS_DIS_TRM TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Blank # 1
LCS # 1
Parameter
Measured
Final
Arsenic (As)
0.002
0.002
Cadmium (Cd)
0.007
0.007
Chromium (Cr)
0.14
0.14
Lead (Pb)
-0.007
-0.007
Silver (Ag)
-0.002
-0.002
Parameter
Measured
Final
Arsenic (As)
50.9
50.9
Cadmium (Cd)
49.9
49.9
Chromium (Cr)
48.6
48.6
Lead (Pb)
50.7
50.7
Silver (Ag)
49.6
49.6
LCSD # 1
Units
Dil
MDL
RDL
Relative Concentration
ug/L
1
0.111
1
< MDL
ug/L
1
0.032
1
< MDL
ug/L
1
0.185
1
< MDL
ug/L
1
0.037
1
< MDL
ug/L
1
0.035
1
< MDL
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
ug/L
1
0.111
50
102
80
120
ug/L
1
0.032
50
99.8
80
120
ug/L
1
0.185
50
97.1
80
120
ug/L
1
0.037
50
101
80
120
ug/L
1
0.035
50
99.3
80
120
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
RPD
Arsenic (As)
50.5
50.5
ug/L
1
0.111
50
101
80
120
0.84
Cadmium (Cd)
50
50
ug/L
1
0.032
50
99.9
80
120
0.134
Chromium (Cr)
48.7
48.7
ug/L
1
0.185
50
97.3
80
120
0.237
Lead (Pb)
50.5
50.5
ug/L
1
0.037
50
101
80
120
0.342
Silver (Ag)
49.9
49.9
ug/L
1
0.035
50
99.8
80
120
0.498
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 43 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010447 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
LCS # 1
MS # 1
MSD # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Arsenic (As)
-0.01
-0.01
ug/L
1
0.111
1
< MDL
Cadmium (Cd)
-0.005
-0.005
ug/L
1
0.032
1
< MDL
Chromium (Cr)
0.01
0.01
ug/L
1
0.185
1
< MDL
Lead (Pb)
-0.016
-0.016
ug/L
1
0.037
1
< MDL
Selenium (Se)
-0.015
-0.015
ug/L
1
0.193
1
< MDL
Silver (Ag)
0.002
0.002
ug/L
1
0.035
1
< MDL
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Arsenic (As)
53.1
53.1
ug/L
1
0.111
50
106
80
120
Cadmium (Cd)
52.8
52.8
ug/L
1
0.032
50
106
80
120
Chromium (Cr)
51.8
51.8
ug/L
1
0.185
50
104
80
120
Lead (Pb)
53.1
53.1
ug/L
1
0.037
50
106
80
120
Selenium (Se)
49.3
49.3
ug/L
1
0.193
50
98.6
80
120
Silver (Ag)
50.9
50.9
ug/L
1
0.035
50
102
80
120
Parent Sample:
J22010014 -- 2022000073
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Arsenic (As)
51.7
51.7
ug/L
1
0.111
50
103
75
125
Cadmium (Cd)
52.6
52.6
ug/L
1
0.032
50
105
75
125
Chromium (Cr)
52.7
52.7
ug/L
1
0.185
50
104
75
125
Lead (Pb)
52.4
52.4
ug/L
1
0.037
50
105
75
125
Selenium (Se)
48.8
48.8
ug/L
1
0.193
50
97.5
75
125
Silver (Ag)
50.3
50.3
ug/L
1
0.035
50
101
75
125
Parent Sample:
J22010014 -- 2022000073
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
RPD
Arsenic (As)
52.4
52.4
ug/L
1
0.111
50
104
75
125
1.33
Cadmium (Cd)
52.8
52.8
ug/L
1
0.032
50
106
75
125
0.47
Chromium (Cr)
53.1
53.1
ug/L
1
0.185
50
105
75
125
0.688
Lead (Pb)
53.2
53.2
ug/L
1
0.037
50
106
75
125
1.51
Selenium (Se)
49.2
49.2
ug/L
1
0.193
50
98.4
75
125
0.984
Silver (Ag)
50.7
50.7
ug/L
1
0.035
50
101
75
125
0.776
Qualifier
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 44 of 151
This report shall not be reproduced, except in full.
Order # J22010014
Level II QC Summary
Q22010448 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
LCS # 1
MS # 1
MSD # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Arsenic (As)
-0.005
-0.005
ug/L
1
0.111
1
< MDL
Cadmium (Cd)
-0.004
-0.004
ug/L
1
0.032
1
< MDL
Chromium (Cr)
-0.008
-0.008
ug/L
1
0.185
1
< MDL
Lead (Pb)
-0.013
-0.013
ug/L
1
0.037
1
< MDL
Selenium (Se)
-0.023
-0.023
ug/L
1
0.193
1
< MDL
Silver (Ag)
-0.001
-0.001
ug/L
1
0.035
1
< MDL
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Arsenic (As)
52.4
52.4
ug/L
1
0.111
50
105
80
120
Cadmium (Cd)
52.7
52.7
ug/L
1
0.032
50
105
80
120
Chromium (Cr)
51.9
51.9
ug/L
1
0.185
50
104
80
120
Lead (Pb)
53.2
53.2
ug/L
1
0.037
50
106
80
120
Selenium (Se)
49.1
49.1
ug/L
1
0.193
50
98.2
80
120
Silver (Ag)
51.4
51.4
ug/L
1
0.035
50
103
80
120
Parent Sample:
J22010014 -- 2022000055
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Arsenic (As)
50.5
50.5
ug/L
1
0.111
50
101
75
125
Cadmium (Cd)
51.1
51.1
ug/L
1
0.032
50
102
75
125
Chromium (Cr)
51.5
51.5
ug/L
1
0.185
50
103
75
125
Lead (Pb)
51.9
51.9
ug/L
1
0.037
50
104
75
125
Selenium (Se)
48.1
48.1
ug/L
1
0.193
50
96.3
75
125
Silver (Ag)
49.4
49.4
ug/L
1
0.035
50
98.9
75
125
Parent Sample:
J22010014 -- 2022000055
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
RPD
Arsenic (As)
50.7
50.7
ug/L
1
0.111
50
101
75
125
0.262
Cadmium (Cd)
51.2
51.2
ug/L
1
0.032
50
102
75
125
0.209
Chromium (Cr)
51.4
51.4
ug/L
1
0.185
50
102
75
125
0.326
Lead (Pb)
51.5
51.5
ug/L
1
0.037
50
103
75
125
0.79
Selenium (Se)
48.5
48.5
ug/L
1
0.193
50
96.9
75
125
0.689
Silver (Ag)
49.7
49.7
ug/L
1
0.035
50
99.5
75
125
0.583
Qualifier
Qualifier
Qualifier
Qualifier

leAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
P989041� YOe. Suite 100
Huntersville, NC 28078
[phone]
February 02, 2022
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg.7405 MG30A2
Huntersville, NC 28078
RE: Project: J22010014 MNS LF
Pace Project No.: 92584910
Dear Program Manager:
Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4 a'0-�
Nicole D'Oleo
nicole.d'[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 102

leAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
PdaR041� yoe. Suite 100
Huntersville, NC 28078
[phone]
Project: J22010014 MNS LF
Pace Project No.: 92584910
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 102

leAnalytical
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Pace Analytical Services, LLC
P989041 WeYOe. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: J22010014 MNS LF
Pace Project No.: 92584910
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92584910001
MW-1
Water
01 /25/22 13:35
01/27/22 13:30
92584910002
M W-1 D
Water
01 /25/22 14:15
01/27/22 13:30
92584910003
MW-2A
Water
01/25/2211:45
01/27/22 13:30
92584910004
MW-21)
Water
01/25/2212:15
01/27/22 13:30
92584910005
MW-3
Water
01/26/22 12:35
01/27/22 13:30
92584910006
MW-313
Water
01/26/2212:00
01/27/22 13:30
92584910007
MW-4
Water
01/26/2211:00
01/27/22 13:30
92584910008
MW-41)
Water
01/26/2211:30
01/27/22 13:30
92584910009
MW-11
Water
01/24/2211:00
01/27/22 13:30
92584910010
MW-11 D
Water
01 /24/22 10:30
01/27/22 13:30
92584910011
MW-12
Water
01 /24/22 12:45
01/27/22 13:30
92584910012
MW-12D
Water
01/24/2213:30
01/27/22 13:30
92584910013
SW-1
Water
01 /25/22 15:15
01/27/22 13:30
92584910014
MW-4R
Water
01/26/2212:20
01/27/22 13:30
92584910015
MW-4DR
Water
01/26/22 13:30
01/27/22 13:30
92584910016
MW-313R
Water
01/26/2211:05
01/27/22 13:30
92584910017
MW-413R
Water
01/26/2210:10
01/27/22 13:30
92584910018
MW-413RR
Water
01/26/2213:55
01/27/22 13:30
92584910019
MW-11 BR
Water
01/26/22 09:50
01/27/22 13:30
92584910020
MW-13D
Water
01/26/2214:00
01/27/22 13:30
92584910021
MW-13BR
Water
01/26/22 13:30
01/27/22 13:30
92584910022
MNS TB-20220126-0800
Water
01/26/22 08:00
01/27/22 13:30
92584910023
MNS FB-20220126-1100
Water
01/26/2211:00
01/27/22 13:30
92584910024
MNS FD-20220126-1
Water
01/26/22 00:00
01/27/22 13:30
92584910025
MNS TB-20220124-0930
Water
01/24/22 09:30
01/27/22 13:30
92584910026
MNS FB-20220126-1145
Water
01/26/2211:45
01/27/22 13:30
92584910027
MNS FB-20220124-1600
Water
01/24/2216:00
01/27/22 13:30
92584910028
MNS FB-20220125-1230
Water
01/25/2212:30
01/27/22 13:30
92584910029
MNS FD-20220125-1
Water
01/25/22 00:00
01/27/22 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 102

leAnalytical
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Pace Analytical Services, LLC
P989041 WeYOe. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
J22010014 MNS LF
92584910
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92584910001
MW-1
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910002
MW-1 D
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910003
MW-2A
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910004
MW-21)
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910005
MW-3
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910006
MW-31)
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910007
MW-4
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910008
MW-41)
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910009
MW-11
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910010
MW-11 D
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910011
MW-12
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910012
MW-12D
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910013
SW-1
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910014
MW-4R
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910015
MW-4DR
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910016
MW-313R
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910017
MW-413R
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910018
MW-413RR
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910019
MW-11BR
EPA 8260D
CL
50
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 102

leAnalytical
www.pacelabsxom
Pace Analytical Services, LLC
P989041 WeYOe. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
J22010014 MNS LF
Pace Project No.:
92584910
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 8260D Mod.
LMB
3
PASI-C
92584910020
MW-13D
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910021
MW-13BR
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910022
MNS TB-20220126-0800
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910023
MNS FB-20220126-1100
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910024
MNS FD-20220126-1
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910025
MNS TB-20220124-0930
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910026
MNS FB-20220126-1145
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910027
MNS FB-20220124-1600
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910028
MNS FB-20220125-1230
EPA 8260D
CL
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92584910029
MNS FD-20220125-1
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 102

leAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
P���05t Wy0e. Suite 100
�J Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
J22010014 MNS LF
92584910
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92584910006
MW-313
EPA 8260D
Benzene
0.39J
ug/L
1.0
01/29/22 03:47
EPA 8260D
cis-1,2-Dichloroethene
3.5
ug/L
1.0
01/29/22 03:47
EPA 8260D
Methylene Chloride
2.7J
ug/L
5.0
01/29/22 03:47
C7
EPA 8260D
Tetrachloroethene
0.48J
ug/L
1.0
01/29/22 03:47
EPA 8260D
Trichloroethene
1.3
ug/L
1.0
01/29/22 03:47
EPA 8260D
Xylene (Total)
0.44J
ug/L
1.0
01/29/22 03:47
92584910007
MW-4
EPA 8260D
Tetrachloroethene
1.3
ug/L
1.0
01/29/22 04:06
92584910008
MW-411)
EPA 8260D
Benzene
0.60J
ug/L
1.0
01/29/22 04:24
EPA 8260D
cis-1,2-Dichloroethene
25.3
ug/L
1.0
01/29/22 04:24
EPA 8260D
Methylene Chloride
6.5
ug/L
5.0
01/29/22 04:24
C7
EPA 8260D
Tetrachloroethene
1.0
ug/L
1.0
01/29/22 04:24
EPA 8260D
Trichloroethene
4.7
ug/L
1.0
01/29/22 04:24
EPA 8260D
Xylene (Total)
11.4
ug/L
1.0
01/29/22 04:24
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
1.2J
ug/L
2.0
01/28/22 01:51
92584910014
MW-4R
EPA 8260D
Tetrachloroethene
0.91 J
ug/L
1.0
01/29/22 06:14
EPA 8260D
Trichloroethene
0.53J
ug/L
1.0
01/29/22 06:14
92584910015
MW-4DR
EPA 8260D
cis-1,2-Dichloroethene
0.78J
ug/L
1.0
01/29/2206:33
EPA 8260D
Trichloroethene
0.56J
ug/L
1.0
01/29/22 06:33
92584910016
MW-3BR
EPA 8260D
Benzene
0.65J
ug/L
1.0
01/29/22 06:51
EPA 8260D
1,1-Dichloroethane
0.72J
ug/L
1.0
01/29/22 06:51
EPA 8260D
cis-1,2-Dichloroethene
3.5
ug/L
1.0
01/29/22 06:51
EPA 8260D
Methylene Chloride
9.7
ug/L
5.0
01/29/22 06:51
C7
EPA 8260D
Trichloroethene
1.2
ug/L
1.0
01/29/22 06:51
EPA 8260D
Xylene (Total)
58.1
ug/L
1.0
01/29/22 06:51
92584910017
MW-4BR
EPA 8260D
Carbon disulfide
3.3
ug/L
2.0
01/29/22 07:10
EPA 8260D
1,1-Dichloroethane
0.42J
ug/L
1.0
01/29/22 07:10
EPA 8260D
cis-1,2-Dichloroethene
4.4
ug/L
1.0
01/29/22 07:10
EPA 8260D
Methylene Chloride
4.5J
ug/L
5.0
01/29/22 07:10
C7
EPA 8260D
Xylene (Total)
5.3
ug/L
1.0
01/29/22 07:10
92584910018
MW-4BRR
EPA 8260D
Acetone
15AJ
ug/L
25.0
01/29/22 07:28
EPA 8260D
Carbon disulfide
13.4
ug/L
2.0
01/29/22 07:28
EPA 8260D
cis-1,2-Dichloroethene
0.85J
ug/L
1.0
01/29/22 07:28
EPA 8260D
Xylene (Total)
0.34J
ug/L
1.0
01/29/22 07:28
92584910021
MW-13BR
EPA 8260D
cis-1,2-Dichloroethene
1.9
ug/L
1.0
01/29/2208:23
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 6 of 102

leAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
Pdago5 r6fygfe. Suite 100
�J Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
J22010014 MNS LF
92584910
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92584910021
MW-13BR
EPA 8260D
2-Hexanone
0.79J
ug/L
5.0
01/29/22 08:23
EPA 8260D
Trichloroethene
0.57J
ug/L
1.0
01/29/22 08:23
EPA 8260D
Xylene (Total)
10.1
ug/L
1.0
01/29/22 08:23
92584910024
MNS FD-20220126-1
EPA 8260D
Benzene
0.74J
ug/L
1.0
01/29/22 09:16
EPA 8260D
1,1-Dichloroethane
0.77J
ug/L
1.0
01/29/22 09:16
M1
EPA 8260D
cis-1,2-Dichloroethene
4.0
ug/L
1.0
01/29/22 09:16
M1
EPA 8260D
Methylene Chloride
12.4
ug/L
5.0
01/29/22 09:16
M1,v3
EPA 8260D
Tetrachloroethene
0.48J
ug/L
1.0
01/29/22 09:16
EPA 8260D
Trichloroethene
1.4
ug/L
1.0
01/29/22 09:16
EPA 8260D
Xylene (Total)
75.1
ug/L
1.0
01/29/22 09:16
92584910025
MNS TB-20220124-0930
EPA 8260D
Acetone
12.6J
ug/L
25.0
01/31/2215:05
C7
EPA 8260D
2-Hexanone
0.79J
ug/L
5.0
01/31/2215:05
92584910027
MNS FB-20220124-1600
EPA 8260D
Acetone
12.3J
ug/L
25.0
01/31/2215:23
C7
EPA 8260D
2-Butanone (MEK)
4.OJ
ug/L
5.0
01/31/22 15:23
C7
EPA 8260D
2-Hexanone
0.83J
ug/L
5.0
01/31/2215:23
92584910028
MNS FB-20220125-1230
EPA 8260D
Acetone
12.5J
ug/L
25.0
01/31/2215:42
C7
EPA 8260D
2-Hexanone
0.83J
ug/L
5.0
01/31/2215:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PARYWy0e. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
General Information:
29 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: 674609
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3530850)
• Chloroethane
• LCS (Lab ID: 3530851)
• Chloroethane
• MS (Lab ID: 3530852)
• Chloroethane
• MSD (Lab ID: 3530853)
• Chloroethane
• MW-1 (Lab ID: 92584910001)
• Chloroethane
QC Batch: 674643
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3531118)
• Chloroethane
• LCS (Lab ID: 3531119)
• Chloroethane
• MNS_FB-20220126-1100 (Lab ID: 92584910023)
• Chloroethane
• MNS_FB-20220126-1145 (Lab ID: 92584910026)
• Chloroethane
• MNS_FD-20220125-1 (Lab ID: 92584910029)
• Chloroethane
• MNS_FD-20220126-1 (Lab ID: 92584910024)
• Chloroethane
• MNS_TB-20220126-0800 (Lab ID: 92584910022)
• Chloroethane
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 8 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAR%Ywyoe. Suite 100
�J Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
QC Batch: 674609
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3530850)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• LCS (Lab ID: 3530851)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MS (Lab ID: 3530852)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MSD (Lab ID: 3530853)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MW-1 (Lab ID: 92584910001)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
QC Batch: 674641
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3531103)
• trans-1,4-Dichloro-2-butene
• LCS (Lab ID: 3531104)
• trans-1,4-Dichloro-2-butene
• MS (Lab ID: 3531105)
• trans-1,4-Dichloro-2-butene
• MSD (Lab ID: 3531106)
• trans-1,4-Dichloro-2-butene
• MW-11 (Lab ID: 92584910009)
• trans-1,4-Dichloro-2-butene
• MW-11BR (Lab ID: 92584910019)
• trans-1,4-Dichloro-2-butene
• MW-11D (Lab ID: 92584910010)
• trans-1,4-Dichloro-2-butene
• MW-12 (Lab ID: 92584910011)
• trans-1,4-Dichloro-2-butene
• MW-12D (Lab ID: 92584910012)
• trans-1,4-Dichloro-2-butene
• MW-13BR (Lab ID: 92584910021)
• trans-1,4-Dichloro-2-butene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdag0Aiirpyoe. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
QC Batch: 674641
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• MW-13D (Lab ID: 92584910020)
• trans-1,4-Dichloro-2-butene
• MW-1D (Lab ID: 92584910002)
• trans-1,4-Dichloro-2-butene
• MW-2A (Lab ID: 92584910003)
• trans-1,4-Dichloro-2-butene
• MW-21D (Lab ID: 92584910004)
• trans-1,4-Dichloro-2-butene
• MW-3 (Lab ID: 92584910005)
• trans-1,4-Dichloro-2-butene
• MW-3BR (Lab ID: 92584910016)
• trans-1,4-Dichloro-2-butene
• MW-31D (Lab ID: 92584910006)
• trans-1,4-Dichloro-2-butene
• MW-4 (Lab ID: 92584910007)
• trans-1,4-Dichloro-2-butene
• MW-4BR (Lab ID: 92584910017)
• trans-1,4-Dichloro-2-butene
• MW-4BRR (Lab ID: 92584910018)
• trans-1,4-Dichloro-2-butene
• MW-41D (Lab ID: 92584910008)
• trans-1,4-Dichloro-2-butene
• MW-4DR (Lab ID: 92584910015)
• trans-1,4-Dichloro-2-butene
• MW-4R (Lab ID: 92584910014)
• trans-1,4-Dichloro-2-butene
• SW-1 (Lab ID: 92584910013)
• trans-1,4-Dichloro-2-butene
QC Batch: 674643
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
- BLANK (Lab ID: 3531118)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• LCS (Lab ID: 3531119)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MNS_FB-20220126-1100 (Lab ID: 92584910023)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
POO Wy0e. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
QC Batch: 674643
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• MNS_FB-20220126-1145 (Lab ID: 92584910026)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MNS_FD-20220125-1 (Lab ID: 92584910029)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MNS_FD-20220126-1 (Lab ID: 92584910024)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MNS_TB-20220126-0800 (Lab ID: 92584910022)
• Bromomethane
• lodomethane
• trans-1,4-Dichloro-2-butene
• MS (Lab ID: 3531120)
• 1,2-Dibromo-3-chloropropane
• trans-1,4-Dichloro-2-butene
• MSD (Lab ID: 3531121)
• 1,2-Dibromo-3-chloropropane
• trans-1,4-Dichloro-2-butene
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• MNS_FD-20220126-1 (Lab ID: 92584910024)
• Methylene Chloride
• Trichlorofluoromethane
• MS (Lab ID: 3531120)
• Methylene Chloride
• Trichlorofluoromethane
• MSD (Lab ID: 3531121)
• Methylene Chloride
• Trichlorofluoromethane
QC Batch: 674949
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3532809)
• trans-1,4-Dichloro-2-butene
• LCS (Lab ID: 3532810)
• trans-1,4-Dichloro-2-butene
• MNS_FB-20220124-1600 (Lab ID: 92584910027)
• trans-1,4-Dichloro-2-butene
• MNS_FB-20220125-1230 (Lab ID: 92584910028)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
pdaRVirpy0e. Suite 100
��JJ Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
QC Batch: 674949
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• trans-1,4-Dichloro-2-butene
• MNS_TB-20220124-0930 (Lab ID: 92584910025)
• trans-1,4-Dichloro-2-butene
• MS (Lab ID: 3532811)
• trans-1,4-Dichloro-2-butene
• MSD (Lab ID: 3532812)
• trans-1,4-Dichloro-2-butene
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 674641
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92584910002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3531105)
• 1,1,1,2-Tetrachloroethane
• 1,1,2,2-Tetrachloroethane
• 1,2,3-Trichloropropane
• 1.2-Dichlorobenzene
• 1,4-Dichlorobenzene
• Styrene
• Tetrachloroethene
QC Batch: 674643
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92584910024
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3531120)
• Methylene Chloride
• MSD (Lab ID: 3531121)
• 1,1,1-Trichloroethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 12 of 102

leAnalytical
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Pace Analytical Services, LLC
Pdagvrwyoe. Suite 100
Huntersville, NC 28078
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PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
QC Batch: 674643
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92584910024
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• 1,1,2-Trichloroethane
• 1,1-Dichloroethane
• 1,2-Dichloroethane
• Acrylonitrile
• Bromochloromethane
• Bromodichloromethane
• Carbon disulfide
• Chloroform
• Methylene Chloride
• cis-1,2-Dichloroethene
• cis-1,3-Dichloropropene
• trans-1,2-Dichloroethene
• trans- 1,3-Dichloropropene
QC Batch: 674949
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92584635002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 3532812)
-Benzene
Additional Comments:
Analyte Comments:
QC Batch: 674641
CT Analyte is a possible laboratory contaminant (not present in method blank).
• MW-3BR (Lab ID: 92584910016)
• Methylene Chloride
• MW-3D (Lab ID: 92584910006)
• Methylene Chloride
• MW-4BR (Lab ID: 92584910017)
• Methylene Chloride
• MW-4D (Lab ID: 92584910008)
• Methylene Chloride
QC Batch: 674949
CO: Result confirmed by second analysis.
• MNS_FB-20220124-1600 (Lab ID: 92584910027)
• 4-Bromofluorobenzene (S)
• MNS_FB-20220125-1230 (Lab ID: 92584910028)
• 4-Bromofluorobenzene (S)
• MNS_TB-20220124-0930 (Lab ID: 92584910025)
• 4-Bromofluorobenzene (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 13 of 102

leAnalytical
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Pace Analytical Services, LLC
POWWy0e. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D
Description: 8260D MSV Low Level
Client: Duke Energy
Date: February 02, 2022
Analyte Comments:
QC Batch: 674949
CT Analyte is a possible laboratory contaminant (not present in method blank).
• MNS_FB-20220124-1600 (Lab ID: 92584910027)
• 2-Butanone (MEK)
• Acetone
• MNS_FB-20220125-1230 (Lab ID: 92584910028)
• 2-Butanone (MEK)
• Acetone
• MNS_TB-20220124-0930 (Lab ID: 92584910025)
• 2-Butanone (MEK)
• Acetone
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 14 of 102

leAnalytical
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Pace Analytical Services, LLC
POO Wy0e. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Method: EPA 8260D Mod.
Description: 8260D MSV SIM
Client: Duke Energy
Date: February 02, 2022
General Information:
29 samples were analyzed for EPA 8260D Mod. by Pace Analytical Services Charlotte. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 15 of 102

leAnalytical
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Pdagvrwyoe. Suite 100
�J Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-1 Lab ID: 92584910001 Collected: 01/25/22 13:35 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/28/22 20:22
67-64-1
ND
ug/L
10.0
1.8
1
01/28/22 20:22
107-13-1
ND
ug/L
1.0
0.34
1
01/28/22 20:22
71-43-2
ND
ug/L
1.0
0.47
1
01/28/22 20:22
74-97-5
ND
ug/L
1.0
0.31
1
01/28/22 20:22
75-27-4
ND
ug/L
1.0
0.34
1
01/28/22 20:22
75-25-2
ND
ug/L
2.0
1.7
1
01/28/22 20:22
74-83-9
ND
ug/L
5.0
4.0
1
01/28/22 20:22
78-93-3
ND
ug/L
2.0
0.73
1
01/28/22 20:22
75-15-0
ND
ug/L
1.0
0.33
1
01/28/22 20:22
56-23-5
ND
ug/L
1.0
0.28
1
01/28/22 20:22
108-90-7
ND
ug/L
1.0
0.65
1
01/28/22 20:22
75-00-3
ND
ug/L
1.0
0.43
1
01/28/22 20:22
67-66-3
ND
ug/L
1.0
0.54
1
01/28/22 20:22
74-87-3
ND
ug/L
2.0
0.34
1
01/28/22 20:22
96-12-8
ND
ug/L
1.0
0.36
1
01/28/22 20:22
124-48-1
ND
ug/L
1.0
0.27
1
01/28/22 20:22
106-93-4
ND
ug/L
1.0
0.39
1
01/28/22 20:22
74-95-3
ND
ug/L
1.0
0.34
1
01/28/22 20:22
95-50-1
ND
ug/L
1.0
0.33
1
01/28/22 20:22
106-46-7
ND
ug/L
1.0
0.56
1
01/28/22 20:22
110-57-6
ND
ug/L
1.0
0.37
1
01/28/22 20:22
75-34-3
ND
ug/L
1.0
0.32
1
01/28/22 20:22
107-06-2
ND
ug/L
1.0
0.35
1
01/28/22 20:22
75-35-4
ND
ug/L
1.0
0.38
1
01/28/22 20:22
156-59-2
ND
ug/L
1.0
0.40
1
01/28/22 20:22
156-60-5
ND
ug/L
1.0
0.36
1
01/28/22 20:22
78-87-5
ND
ug/L
1.0
0.36
1
01/28/22 20:22
10061-01-5
ND
ug/L
1.0
0.36
1
01/28/22 20:22
10061-02-6
ND
ug/L
1.0
0.30
1
01/28/22 20:22
100-41-4
ND
ug/L
5.0
0.48
1
01/28/22 20:22
591-78-6
ND
ug/L
20.0
9.7
1
01/28/22 20:22
74-88-4
ND
ug/L
5.0
2.0
1
01/28/22 20:22
75-09-2
ND
ug/L
5.0
2.7
1
01/28/22 20:22
108-10-1
ND
ug/L
1.0
0.29
1
01/28/22 20:22
100-42-5
ND
ug/L
1.0
0.31
1
01/28/22 20:22
630-20-6
ND
ug/L
1.0
0.22
1
01/28/22 20:22
79-34-5
ND
ug/L
1.0
0.29
1
01/28/22 20:22
127-18-4
ND
ug/L
1.0
0.48
1
01/28/22 20:22
108-88-3
ND
ug/L
1.0
0.33
1
01/28/22 20:22
71-55-6
ND
ug/L
1.0
0.32
1
01/28/22 20:22
79-00-5
ND
ug/L
1.0
0.38
1
01/28/22 20:22
79-01-6
ND
ug/L
1.0
0.30
1
01/28/22 20:22
75-69-4
ND
ug/L
1.0
0.26
1
01/28/22 20:22
96-18-4
ND
ug/L
2.0
1.3
1
01/28/22 20:22
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v1
IN
v1
v1
Page 16 of 102

leAnalytical
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Pace Analytical Services, LLC
Pdagmirpygfe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-1
Lab ID: 92584910001 Collected:
01/25/22 13:35
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/28/22 20:22
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/28/22 20:22
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/28/22 20:22
460-00-4
1,2-Dichloroethane-d4 (S)
102 % 70-130
1
01/28/22 20:22
17060-07-0
Toluene-d8 (S)
102 % 70-130
1
01/28/22 20:22
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/27/22 23:36
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 % 70-130
1
01/27/22 23:36
17060-07-0
Toluene-d8 (S)
95 % 66-133
1
01/27/22 23:36
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 102

leAnalytical
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Pace Analytical Services, LLC
P989�r6fYoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MWAD Lab ID: 92584910002 Collected: 01/25/22 14:15 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 02:34
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 02:34
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 02:34
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 02:34
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 02:34
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 02:34
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 02:34
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 02:34
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 02:34
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 02:34
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 02:34
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 02:34
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 02:34
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 02:34
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 02:34
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 02:34
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 02:34
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 02:34
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 02:34
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 02:34
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 02:34
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 02:34
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 02:34
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 02:34
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 02:34
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 02:34
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 02:34
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 02:34
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 02:34
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 02:34
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 02:34
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 02:34
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 02:34
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 02:34
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 02:34
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 02:34
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 02:34
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 02:34
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 02:34
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 02:34
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 02:34
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 02:34
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 02:34
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 02:34
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 02:34
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
M1
M1
v1
M1
M1
M1
M1
I •il
Page 18 of 102

leAnalytical
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Pace Analytical Services, LLC
P98HISr6fYoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MWAD
Lab ID: 92584910002 Collected:
01/25/22 14:15
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 02:34
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 02:34
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 02:34
460-00-4
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
01/29/22 02:34
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
01/29/22 02:34
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/27/22 23:55
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/27/22 23:55
17060-07-0
Toluene-d8(S)
94 % 66-133
1
01/27/22 23:55
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 102

leAnalytical
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Pace Analytical Services, LLC
pdagl pyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-2A Lab ID: 92584910003 Collected: 01/25/22 11:45 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 02:52
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 02:52
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 02:52
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 02:52
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 02:52
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 02:52
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 02:52
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 02:52
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 02:52
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 02:52
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 02:52
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 02:52
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 02:52
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 02:52
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 02:52
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 02:52
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 02:52
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 02:52
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 02:52
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 02:52
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 02:52
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 02:52
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 02:52
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 02:52
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 02:52
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 02:52
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 02:52
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 02:52
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 02:52
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 02:52
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 02:52
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 02:52
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 02:52
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 02:52
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 02:52
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 02:52
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 02:52
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 02:52
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 02:52
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 02:52
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 02:52
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 02:52
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 02:52
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 02:52
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 02:52
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 20 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P989%18r6fYoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-2A
Lab ID: 92584910003 Collected:
01/25/22 11:45
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 02:52
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 02:52
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 % 70-130
1
01/29/22 02:52
460-00-4
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
01/29/22 02:52
17060-07-0
Toluene-d8(S)
98 % 70-130
1
01/29/22 02:52
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 00:15
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 % 70-130
1
01/28/22 00:15
17060-07-0
Toluene-d8 (S)
95 % 66-133
1
01/28/22 00:15
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdag%larpyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-21) Lab ID: 92584910004 Collected: 01/25/22 12:15 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 03:11
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 03:11
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 03:11
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 03:11
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 03:11
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 03:11
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 03:11
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 03:11
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 03:11
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 03:11
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 03:11
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 03:11
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 03:11
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 03:11
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 03:11
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 03:11
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 03:11
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 03:11
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 03:11
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 03:11
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 03:11
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 03:11
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 03:11
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 03:11
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 03:11
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 03:11
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 03:11
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 03:11
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 03:11
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 03:11
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 03:11
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 03:11
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 03:11
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 03:11
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 03:11
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 03:11
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 03:11
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 03:11
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 03:11
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 03:11
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 03:11
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 03:11
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 03:11
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 03:11
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 03:11
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 22 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagvrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-21)
Lab ID: 92584910004 Collected:
01/25/22 12:15
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 03:11
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 03:11
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 03:11
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 03:11
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
01/29/22 03:11
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 00:34
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 % 70-130
1
01/28/22 00:34
17060-07-0
Toluene-d8 (S)
94 % 66-133
1
01/28/22 00:34
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P989�rwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-3 Lab ID: 92584910005 Collected: 01/26/22 12:35 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 03:29
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 03:29
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 03:29
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 03:29
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 03:29
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 03:29
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 03:29
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 03:29
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 03:29
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 03:29
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 03:29
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 03:29
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 03:29
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 03:29
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 03:29
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 03:29
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 03:29
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 03:29
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 03:29
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 03:29
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 03:29
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 03:29
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 03:29
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 03:29
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 03:29
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 03:29
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 03:29
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 03:29
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 03:29
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 03:29
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 03:29
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 03:29
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 03:29
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 03:29
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 03:29
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 03:29
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 03:29
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 03:29
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 03:29
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 03:29
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 03:29
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 03:29
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 03:29
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 03:29
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 03:29
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 24 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAR16r6fYoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-3
Lab ID: 92584910005 Collected:
01/26/22 12:35
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 03:29
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 03:29
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 % 70-130
1
01/29/22 03:29
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 03:29
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 03:29
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 00:53
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
88 % 70-130
1
01/28/22 00:53
17060-07-0
Toluene-d8(S)
93 % 66-133
1
01/28/22 00:53
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P98907birwyoe. Suite 100
��JJ Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-31) Lab ID: 92584910006 Collected: 01/26/22 12:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 03:47
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 03:47
107-13-1
0.39J
ug/L
1.0
0.34
1
01/29/22 03:47
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 03:47
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 03:47
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 03:47
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 03:47
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 03:47
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 03:47
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 03:47
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 03:47
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 03:47
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 03:47
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 03:47
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 03:47
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 03:47
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 03:47
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 03:47
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 03:47
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 03:47
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 03:47
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 03:47
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 03:47
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 03:47
75-35-4
3.5
ug/L
1.0
0.38
1
01/29/22 03:47
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 03:47
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 03:47
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 03:47
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 03:47
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 03:47
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 03:47
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 03:47
74-88-4
2.7J
ug/L
5.0
2.0
1
01/29/22 03:47
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 03:47
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 03:47
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 03:47
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 03:47
79-34-5
0.48J
ug/L
1.0
0.29
1
01/29/22 03:47
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 03:47
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 03:47
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 03:47
79-00-5
1.3
ug/L
1.0
0.38
1
01/29/22 03:47
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 03:47
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 03:47
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 03:47
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
C7
Page 26 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PdagoAirpygfe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-31)
Lab ID: 92584910006 Collected:
01/26/22 12:00
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 03:47
75-01-4
Xylene (Total)
0.44J ug/L 1.0
0.34
1
01/29/22 03:47
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
01/29/22 03:47
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 03:47
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
01/29/22 03:47
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 01:12
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 01:12
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 01:12
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagohrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4 Lab ID: 92584910007 Collected: 01/26/22 11:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 04:06
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 04:06
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 04:06
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 04:06
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 04:06
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 04:06
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 04:06
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 04:06
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 04:06
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 04:06
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 04:06
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 04:06
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 04:06
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 04:06
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 04:06
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 04:06
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 04:06
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 04:06
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 04:06
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 04:06
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 04:06
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 04:06
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 04:06
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 04:06
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 04:06
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 04:06
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 04:06
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 04:06
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 04:06
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 04:06
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 04:06
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 04:06
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 04:06
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 04:06
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 04:06
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 04:06
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 04:06
79-34-5
1.3
ug/L
1.0
0.29
1
01/29/22 04:06
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 04:06
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 04:06
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 04:06
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 04:06
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 04:06
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 04:06
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 04:06
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 28 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdago �irwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4
Lab ID: 92584910007 Collected:
01/26/22 11:00
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 04:06
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 04:06
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 % 70-130
1
01/29/22 04:06
460-00-4
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
01/29/22 04:06
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 04:06
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 01:31
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 01:31
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 01:31
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PdaRO�irpyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-41) Lab ID: 92584910008 Collected: 01/26/22 11:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 04:24
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 04:24
107-13-1
0.60J
ug/L
1.0
0.34
1
01/29/22 04:24
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 04:24
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 04:24
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 04:24
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 04:24
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 04:24
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 04:24
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 04:24
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 04:24
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 04:24
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 04:24
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 04:24
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 04:24
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 04:24
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 04:24
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 04:24
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 04:24
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 04:24
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 04:24
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 04:24
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 04:24
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 04:24
75-35-4
25.3
ug/L
1.0
0.38
1
01/29/22 04:24
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 04:24
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 04:24
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 04:24
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 04:24
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 04:24
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 04:24
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 04:24
74-88-4
6.5
ug/L
5.0
2.0
1
01/29/22 04:24
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 04:24
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 04:24
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 04:24
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 04:24
79-34-5
1.0
ug/L
1.0
0.29
1
01/29/22 04:24
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 04:24
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 04:24
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 04:24
79-00-5
4.7
ug/L
1.0
0.38
1
01/29/22 04:24
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 04:24
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 04:24
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 04:24
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
C7
Page 30 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagomrw Yoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-41)
Lab ID: 92584910008 Collected:
01/26/22 11:30
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 04:24
75-01-4
Xylene (Total)
11.4 ug/L 1.0
0.34
1
01/29/22 04:24
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 04:24
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 04:24
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 04:24
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1.2J ug/L 2.0
0.86
1
01/28/22 01:51
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 % 70-130
1
01/28/22 01:51
17060-07-0
Toluene-d8 (S)
92 % 66-133
1
01/28/22 01:51
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
pdaROMrpyoe. Suite 100
��JJ Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11 Lab ID: 92584910009 Collected: 01/24/22 11:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 04:43
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 04:43
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 04:43
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 04:43
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 04:43
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 04:43
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 04:43
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 04:43
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 04:43
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 04:43
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 04:43
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 04:43
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 04:43
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 04:43
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 04:43
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 04:43
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 04:43
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 04:43
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 04:43
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 04:43
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 04:43
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 04:43
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 04:43
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 04:43
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 04:43
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 04:43
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 04:43
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 04:43
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 04:43
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 04:43
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 04:43
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 04:43
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 04:43
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 04:43
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 04:43
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 04:43
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 04:43
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 04:43
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 04:43
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 04:43
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 04:43
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 04:43
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 04:43
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 04:43
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 04:43
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 32 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagonrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11
Lab ID: 92584910009 Collected:
01/24/22 11:00
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 04:43
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 04:43
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 04:43
460-00-4
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
01/29/22 04:43
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
01/29/22 04:43
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 02:10
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 02:10
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 02:10
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 33 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdago �irwYoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11D Lab ID: 92584910010 Collected: 01/24/22 10:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 05:01
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 05:01
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 05:01
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 05:01
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 05:01
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 05:01
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 05:01
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 05:01
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 05:01
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 05:01
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 05:01
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 05:01
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 05:01
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 05:01
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 05:01
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 05:01
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 05:01
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 05:01
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 05:01
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 05:01
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 05:01
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 05:01
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 05:01
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 05:01
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 05:01
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 05:01
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 05:01
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 05:01
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 05:01
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 05:01
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 05:01
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 05:01
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 05:01
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 05:01
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 05:01
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 05:01
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 05:01
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 05:01
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 05:01
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 05:01
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 05:01
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 05:01
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 05:01
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 05:01
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 05:01
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 34 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagohrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11D
Lab ID: 92584910010 Collected:
01/24/22 10:30
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 05:01
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 05:01
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 05:01
460-00-4
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
01/29/22 05:01
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/29/22 05:01
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 02:29
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 02:29
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 02:29
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagvrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-12 Lab ID: 92584910011 Collected: 01/24/22 12:45 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 05:19
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 05:19
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 05:19
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 05:19
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 05:19
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 05:19
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 05:19
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 05:19
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 05:19
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 05:19
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 05:19
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 05:19
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 05:19
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 05:19
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 05:19
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 05:19
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 05:19
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 05:19
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 05:19
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 05:19
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 05:19
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 05:19
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 05:19
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 05:19
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 05:19
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 05:19
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 05:19
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 05:19
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 05:19
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 05:19
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 05:19
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 05:19
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 05:19
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 05:19
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 05:19
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 05:19
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 05:19
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 05:19
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 05:19
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 05:19
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 05:19
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 05:19
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 05:19
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 05:19
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 05:19
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 36 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pd8R0gfir6fy&fe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-12
Lab ID: 92584910011 Collected:
01/24/22 12:45
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 05:19
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 05:19
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/29/22 05:19
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 05:19
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 05:19
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 02:48
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 02:48
17060-07-0
Toluene-d8 (S)
92 % 66-133
1
01/28/22 02:48
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 37 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAR%Ywyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-12D Lab ID: 92584910012 Collected: 01/24/22 13:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 05:38
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 05:38
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 05:38
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 05:38
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 05:38
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 05:38
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 05:38
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 05:38
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 05:38
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 05:38
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 05:38
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 05:38
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 05:38
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 05:38
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 05:38
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 05:38
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 05:38
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 05:38
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 05:38
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 05:38
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 05:38
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 05:38
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 05:38
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 05:38
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 05:38
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 05:38
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 05:38
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 05:38
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 05:38
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 05:38
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 05:38
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 05:38
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 05:38
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 05:38
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 05:38
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 05:38
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 05:38
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 05:38
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 05:38
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 05:38
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 05:38
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 05:38
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 05:38
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 05:38
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 05:38
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 38 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAR%Ywyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-12D
Lab ID: 92584910012 Collected:
01/24/22 13:30
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 05:38
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 05:38
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/29/22 05:38
460-00-4
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
01/29/22 05:38
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
01/29/22 05:38
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 03:08
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
88 % 70-130
1
01/28/22 03:08
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 03:08
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 39 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAM'irwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: SW-1 Lab ID: 92584910013 Collected: 01/25/22 15:15 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 05:56
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 05:56
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 05:56
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 05:56
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 05:56
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 05:56
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 05:56
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 05:56
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 05:56
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 05:56
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 05:56
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 05:56
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 05:56
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 05:56
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 05:56
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 05:56
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 05:56
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 05:56
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 05:56
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 05:56
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 05:56
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 05:56
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 05:56
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 05:56
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 05:56
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 05:56
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 05:56
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 05:56
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 05:56
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 05:56
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 05:56
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 05:56
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 05:56
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 05:56
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 05:56
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 05:56
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 05:56
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 05:56
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 05:56
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 05:56
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 05:56
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 05:56
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 05:56
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 05:56
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 05:56
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 40 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAMrWy0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: SW-1
Lab ID: 92584910013 Collected:
01/25/22 15:15
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 05:56
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 05:56
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
01/29/22 05:56
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 05:56
17060-07-0
Toluene-d8(S)
98 % 70-130
1
01/29/22 05:56
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 03:27
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 03:27
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 03:27
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 41 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
pdaRVirpy0e. Suite 100
��JJ Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4R Lab ID: 92584910014 Collected: 01/26/22 12:20 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 06:14
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 06:14
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 06:14
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 06:14
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 06:14
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 06:14
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 06:14
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 06:14
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 06:14
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 06:14
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 06:14
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 06:14
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 06:14
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 06:14
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 06:14
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 06:14
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 06:14
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 06:14
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 06:14
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 06:14
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 06:14
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 06:14
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 06:14
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 06:14
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 06:14
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 06:14
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 06:14
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 06:14
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 06:14
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 06:14
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 06:14
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 06:14
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 06:14
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 06:14
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 06:14
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 06:14
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 06:14
79-34-5
0.911
ug/L
1.0
0.29
1
01/29/22 06:14
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 06:14
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 06:14
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 06:14
79-00-5
0.53J
ug/L
1.0
0.38
1
01/29/22 06:14
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 06:14
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 06:14
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 06:14
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 42 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagvrwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4R
Lab ID: 92584910014 Collected:
01/26/22 12:20
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 06:14
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 06:14
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96 % 70-130
1
01/29/22 06:14
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 06:14
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 06:14
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 03:46
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 03:46
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 03:46
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 43 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAMrWy0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4DR Lab ID: 92584910015 Collected: 01/26/22 13:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 06:33
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 06:33
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 06:33
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 06:33
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 06:33
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 06:33
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 06:33
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 06:33
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 06:33
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 06:33
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 06:33
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 06:33
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 06:33
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 06:33
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 06:33
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 06:33
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 06:33
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 06:33
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 06:33
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 06:33
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 06:33
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 06:33
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 06:33
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 06:33
75-35-4
0.78J
ug/L
1.0
0.38
1
01/29/22 06:33
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 06:33
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 06:33
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 06:33
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 06:33
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 06:33
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 06:33
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 06:33
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 06:33
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 06:33
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 06:33
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 06:33
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 06:33
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 06:33
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 06:33
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 06:33
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 06:33
79-00-5
0.56J
ug/L
1.0
0.38
1
01/29/22 06:33
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 06:33
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 06:33
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 06:33
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 44 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PAMrWy0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4DR
Lab ID: 92584910015 Collected:
01/26/22 13:30
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 06:33
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 06:33
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/29/22 06:33
460-00-4
1,2-Dichloroethane-d4 (S)
96 % 70-130
1
01/29/22 06:33
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 06:33
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 04:05
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 04:05
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 04:05
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 45 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagvirwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-3BR Lab ID: 92584910016 Collected: 01/26/22 11:05 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 06:51
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 06:51
107-13-1
0.65J
ug/L
1.0
0.34
1
01/29/22 06:51
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 06:51
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 06:51
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 06:51
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 06:51
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 06:51
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 06:51
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 06:51
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 06:51
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 06:51
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 06:51
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 06:51
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 06:51
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 06:51
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 06:51
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 06:51
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 06:51
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 06:51
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 06:51
110-57-6
0.72J
ug/L
1.0
0.37
1
01/29/22 06:51
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 06:51
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 06:51
75-35-4
3.5
ug/L
1.0
0.38
1
01/29/22 06:51
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 06:51
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 06:51
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 06:51
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 06:51
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 06:51
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 06:51
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 06:51
74-88-4
9.7
ug/L
5.0
2.0
1
01/29/22 06:51
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 06:51
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 06:51
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 06:51
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 06:51
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 06:51
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 06:51
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 06:51
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 06:51
79-00-5
1.2
ug/L
1.0
0.38
1
01/29/22 06:51
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 06:51
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 06:51
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 06:51
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
C7
Page 46 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagmir6fygfe. Suite 100
��JJ Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-313R
Lab ID: 92584910016 Collected:
01/26/22 11:05
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 06:51
75-01-4
Xylene (Total)
58.1 ug/L 1.0
0.34
1
01/29/22 06:51
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 06:51
460-00-4
1,2-Dichloroethane-d4 (S)
96 % 70-130
1
01/29/22 06:51
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/29/22 06:51
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 04:24
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 04:24
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 04:24
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 47 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagld wyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4BR Lab ID: 92584910017 Collected: 01/26/22 10:10 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 07:10
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 07:10
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 07:10
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 07:10
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 07:10
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 07:10
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 07:10
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 07:10
78-93-3
3.3
ug/L
2.0
0.73
1
01/29/22 07:10
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 07:10
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 07:10
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 07:10
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 07:10
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 07:10
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 07:10
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 07:10
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 07:10
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 07:10
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 07:10
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 07:10
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 07:10
110-57-6
0.42J
ug/L
1.0
0.37
1
01/29/22 07:10
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 07:10
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 07:10
75-35-4
4.4
ug/L
1.0
0.38
1
01/29/22 07:10
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 07:10
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 07:10
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 07:10
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 07:10
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 07:10
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 07:10
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 07:10
74-88-4
4.5J
ug/L
5.0
2.0
1
01/29/22 07:10
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 07:10
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 07:10
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 07:10
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 07:10
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 07:10
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 07:10
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 07:10
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 07:10
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 07:10
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 07:10
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 07:10
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 07:10
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
C7
Page 48 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P98906r6fy0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-413R
Lab ID: 92584910017 Collected:
01/26/22 10:10
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 07:10
75-01-4
Xylene (Total)
5.3 ug/L 1.0
0.34
1
01/29/22 07:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
01/29/22 07:10
460-00-4
1,2-Dichloroethane-d4 (S)
96 % 70-130
1
01/29/22 07:10
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 07:10
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 04:44
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 % 70-130
1
01/28/22 04:44
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 04:44
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 49 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdag0Aiirpyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-4BRR Lab ID: 92584910018 Collected: 01/26/22 13:55 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
15.4J
ug/L
25.0
5.1
1
01/29/22 07:28
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 07:28
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 07:28
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 07:28
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 07:28
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 07:28
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 07:28
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 07:28
78-93-3
13.4
ug/L
2.0
0.73
1
01/29/22 07:28
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 07:28
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 07:28
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 07:28
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 07:28
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 07:28
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 07:28
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 07:28
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 07:28
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 07:28
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 07:28
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 07:28
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 07:28
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 07:28
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 07:28
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 07:28
75-35-4
0.85J
ug/L
1.0
0.38
1
01/29/22 07:28
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 07:28
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 07:28
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 07:28
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 07:28
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 07:28
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 07:28
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 07:28
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 07:28
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 07:28
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 07:28
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 07:28
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 07:28
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 07:28
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 07:28
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 07:28
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 07:28
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 07:28
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 07:28
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 07:28
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 07:28
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 50 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P9890rwYoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-413RR
Lab ID: 92584910018 Collected:
01/26/22 13:55
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 07:28
75-01-4
Xylene (Total)
0.34J ug/L 1.0
0.34
1
01/29/22 07:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
01/29/22 07:28
460-00-4
1,2-Dichloroethane-d4 (S)
94 % 70-130
1
01/29/22 07:28
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 07:28
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 05:03
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 05:03
17060-07-0
Toluene-d8 (S)
93 % 66-133
1
01/28/22 05:03
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 51 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pdagvirwyoe. Suite 100
�J Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11BR Lab ID: 92584910019 Collected: 01/26/22 09:50 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 07:47
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 07:47
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 07:47
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 07:47
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 07:47
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 07:47
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 07:47
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 07:47
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 07:47
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 07:47
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 07:47
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 07:47
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 07:47
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 07:47
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 07:47
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 07:47
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 07:47
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 07:47
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 07:47
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 07:47
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 07:47
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 07:47
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 07:47
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 07:47
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 07:47
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 07:47
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 07:47
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 07:47
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 07:47
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 07:47
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 07:47
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 07:47
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 07:47
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 07:47
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 07:47
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 07:47
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 07:47
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 07:47
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 07:47
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 07:47
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 07:47
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 07:47
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 07:47
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 07:47
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 07:47
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 52 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P9891*rwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-11BR
Lab ID: 92584910019 Collected:
01/26/22 09:50
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 07:47
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 07:47
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
01/29/22 07:47
460-00-4
1,2-Dichloroethane-d4 (S)
95 % 70-130
1
01/29/22 07:47
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 07:47
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 06:39
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 06:39
17060-07-0
Toluene-d8 (S)
92 % 66-133
1
01/28/22 06:39
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 53 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P989"Arwy0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-13D Lab ID: 92584910020 Collected: 01/26/22 14:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 08:05
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 08:05
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 08:05
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 08:05
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 08:05
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 08:05
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 08:05
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 08:05
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 08:05
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 08:05
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 08:05
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 08:05
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 08:05
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 08:05
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 08:05
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 08:05
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 08:05
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 08:05
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 08:05
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 08:05
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 08:05
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 08:05
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 08:05
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 08:05
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 08:05
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 08:05
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 08:05
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 08:05
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 08:05
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 08:05
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 08:05
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 08:05
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 08:05
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 08:05
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 08:05
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 08:05
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 08:05
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 08:05
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 08:05
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 08:05
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 08:05
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 08:05
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 08:05
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 08:05
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 08:05
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 54 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
P98906rwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-13D
Lab ID: 92584910020 Collected:
01/26/22 14:00
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 08:05
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 08:05
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/29/22 08:05
460-00-4
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
01/29/22 08:05
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 08:05
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 06:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
88 % 70-130
1
01/28/22 06:58
17060-07-0
Toluene-d8(S)
92 % 66-133
1
01/28/22 06:58
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 55 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgwrwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-13BR Lab ID: 92584910021 Collected: 01/26/22 13:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 08:23
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 08:23
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 08:23
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 08:23
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 08:23
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 08:23
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 08:23
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 08:23
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 08:23
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 08:23
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 08:23
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 08:23
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 08:23
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 08:23
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 08:23
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 08:23
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 08:23
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 08:23
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 08:23
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 08:23
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 08:23
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 08:23
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 08:23
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 08:23
75-35-4
1.9
ug/L
1.0
0.38
1
01/29/22 08:23
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 08:23
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 08:23
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 08:23
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 08:23
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 08:23
100-41-4
0.79J
ug/L
5.0
0.48
1
01/29/22 08:23
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 08:23
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 08:23
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 08:23
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 08:23
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 08:23
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 08:23
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 08:23
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 08:23
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 08:23
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 08:23
79-00-5
0.57J
ug/L
1.0
0.38
1
01/29/22 08:23
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 08:23
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 08:23
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 08:23
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v1
Page 56 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgwlir6fygfe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MW-13BR
Lab ID: 92584910021 Collected:
01/26/22 13:30
Received: 01/27/22 13:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 08:23
75-01-4
Xylene (Total)
10.1 ug/L 1.0
0.34
1
01/29/22 08:23
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
01/29/22 08:23
460-00-4
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
01/29/22 08:23
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
01/29/22 08:23
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 07:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 % 70-130
1
01/28/22 07:17
17060-07-0
Toluene-d8 (S)
94 % 66-133
1
01/28/22 07:17
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 57 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"rwy ie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_TB-20220126-0800 Lab ID: 92584910022 Collected: 01/26/22 08:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/28/22 23:58
67-64-1
ND
ug/L
10.0
1.8
1
01/28/22 23:58
107-13-1
ND
ug/L
1.0
0.34
1
01/28/22 23:58
71-43-2
ND
ug/L
1.0
0.47
1
01/28/22 23:58
74-97-5
ND
ug/L
1.0
0.31
1
01/28/22 23:58
75-27-4
ND
ug/L
1.0
0.34
1
01/28/22 23:58
75-25-2
ND
ug/L
2.0
1.7
1
01/28/22 23:58
74-83-9
ND
ug/L
5.0
4.0
1
01/28/22 23:58
78-93-3
ND
ug/L
2.0
0.73
1
01/28/22 23:58
75-15-0
ND
ug/L
1.0
0.33
1
01/28/22 23:58
56-23-5
ND
ug/L
1.0
0.28
1
01/28/22 23:58
108-90-7
ND
ug/L
1.0
0.65
1
01/28/22 23:58
75-00-3
ND
ug/L
1.0
0.43
1
01/28/22 23:58
67-66-3
ND
ug/L
1.0
0.54
1
01/28/22 23:58
74-87-3
ND
ug/L
2.0
0.34
1
01/28/22 23:58
96-12-8
ND
ug/L
1.0
0.36
1
01/28/22 23:58
124-48-1
ND
ug/L
1.0
0.27
1
01/28/22 23:58
106-93-4
ND
ug/L
1.0
0.39
1
01/28/22 23:58
74-95-3
ND
ug/L
1.0
0.34
1
01/28/22 23:58
95-50-1
ND
ug/L
1.0
0.33
1
01/28/22 23:58
106-46-7
ND
ug/L
1.0
0.56
1
01/28/22 23:58
110-57-6
ND
ug/L
1.0
0.37
1
01/28/22 23:58
75-34-3
ND
ug/L
1.0
0.32
1
01/28/22 23:58
107-06-2
ND
ug/L
1.0
0.35
1
01/28/22 23:58
75-35-4
ND
ug/L
1.0
0.38
1
01/28/22 23:58
156-59-2
ND
ug/L
1.0
0.40
1
01/28/22 23:58
156-60-5
ND
ug/L
1.0
0.36
1
01/28/22 23:58
78-87-5
ND
ug/L
1.0
0.36
1
01/28/22 23:58
10061-01-5
ND
ug/L
1.0
0.36
1
01/28/22 23:58
10061-02-6
ND
ug/L
1.0
0.30
1
01/28/22 23:58
100-41-4
ND
ug/L
5.0
0.48
1
01/28/22 23:58
591-78-6
ND
ug/L
20.0
9.7
1
01/28/22 23:58
74-88-4
ND
ug/L
5.0
2.0
1
01/28/22 23:58
75-09-2
ND
ug/L
5.0
2.7
1
01/28/22 23:58
108-10-1
ND
ug/L
1.0
0.29
1
01/28/22 23:58
100-42-5
ND
ug/L
1.0
0.31
1
01/28/22 23:58
630-20-6
ND
ug/L
1.0
0.22
1
01/28/22 23:58
79-34-5
ND
ug/L
1.0
0.29
1
01/28/22 23:58
127-18-4
ND
ug/L
1.0
0.48
1
01/28/22 23:58
108-88-3
ND
ug/L
1.0
0.33
1
01/28/22 23:58
71-55-6
ND
ug/L
1.0
0.32
1
01/28/22 23:58
79-00-5
ND
ug/L
1.0
0.38
1
01/28/22 23:58
79-01-6
ND
ug/L
1.0
0.30
1
01/28/22 23:58
75-69-4
ND
ug/L
1.0
0.26
1
01/28/22 23:58
96-18-4
ND
ug/L
2.0
1.3
1
01/28/22 23:58
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v1
IN
v1
v1
Page 58 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg rwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_TB-20220126-0800
Parameters
Lab ID: 92584910022 Collected:
Report
Results Units Limit
01/26/22 08:00
MDL DF
Received: 01/27/22 13:30 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/28/22 23:58
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/28/22 23:58
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96 % 70-130
1
01/28/22 23:58
460-00-4
1,2-Dichloroethane-d4 (S)
100 % 70-130
1
01/28/22 23:58
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/28/22 23:58
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/27/22 18:46
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/27/22 18:46
17060-07-0
Toluene-d8 (S)
95 % 66-133
1
01/27/22 18:46
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 59 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgaffl�lrwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220126-1100 Lab ID: 92584910023 Collected: 01/26/22 11:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 00:16
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 00:16
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 00:16
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 00:16
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 00:16
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 00:16
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 00:16
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 00:16
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 00:16
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 00:16
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 00:16
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 00:16
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 00:16
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 00:16
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 00:16
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 00:16
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 00:16
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 00:16
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 00:16
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 00:16
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 00:16
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 00:16
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 00:16
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 00:16
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 00:16
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 00:16
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 00:16
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 00:16
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 00:16
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 00:16
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 00:16
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 00:16
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 00:16
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 00:16
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 00:16
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 00:16
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 00:16
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 00:16
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 00:16
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 00:16
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 00:16
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 00:16
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 00:16
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 00:16
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 00:16
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v1
IN
v1
v1
Page 60 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgamrwy ie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220126-1100
Parameters
Lab ID: 92584910023 Collected:
Report
Results Units Limit
01/26/22 11:00
MDL DF
Received: 01/27/22 13:30 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 00:16
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 00:16
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 % 70-130
1
01/29/22 00:16
460-00-4
1,2-Dichloroethane-d4 (S)
100 % 70-130
1
01/29/22 00:16
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/29/22 00:16
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/27/22 19:06
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 % 70-130
1
01/27/22 19:06
17060-07-0
Toluene-d8 (S)
95 % 66-133
1
01/27/22 19:06
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 61 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgaftrwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FD-20220126-1 Lab ID: 92584910024 Collected: 01/26/22 00:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 09:16
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 09:16
107-13-1
M1
0.74J
ug/L
1.0
0.34
1
01/29/22 09:16
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 09:16
74-97-5
M 1
ND
ug/L
1.0
0.31
1
01/29/22 09:16
75-27-4
M 1
ND
ug/L
1.0
0.34
1
01/29/22 09:16
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 09:16
74-83-9
IH,v1
ND
ug/L
5.0
4.0
1
01/29/22 09:16
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 09:16
75-15-0
M1
ND
ug/L
1.0
0.33
1
01/29/22 09:16
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 09:16
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 09:16
75-00-3
IK
ND
ug/L
1.0
0.43
1
01/29/22 09:16
67-66-3
M 1
ND
ug/L
1.0
0.54
1
01/29/22 09:16
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 09:16
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 09:16
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 09:16
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 09:16
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 09:16
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 09:16
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 09:16
110-57-6
v1
0.77J
ug/L
1.0
0.37
1
01/29/22 09:16
75-34-3
M1
ND
ug/L
1.0
0.32
1
01/29/22 09:16
107-06-2
M 1
ND
ug/L
1.0
0.35
1
01/29/22 09:16
75-35-4
4.0
ug/L
1.0
0.38
1
01/29/22 09:16
156-59-2
M1
ND
ug/L
1.0
0.40
1
01/29/22 09:16
156-60-5
M 1
ND
ug/L
1.0
0.36
1
01/29/22 09:16
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 09:16
10061-01-5
M 1
ND
ug/L
1.0
0.36
1
01/29/22 09:16
10061-02-6
M 1
ND
ug/L
1.0
0.30
1
01/29/22 09:16
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 09:16
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 09:16
74-88-4
v1
12.4
ug/L
5.0
2.0
1
01/29/22 09:16
75-09-2
M 1, v3
ND
ug/L
5.0
2.7
1
01/29/22 09:16
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 09:16
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 09:16
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 09:16
79-34-5
0.48J
ug/L
1.0
0.29
1
01/29/22 09:16
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 09:16
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 09:16
71-55-6
M 1
ND
ug/L
1.0
0.32
1
01/29/22 09:16
79-00-5
M 1
1.4
ug/L
1.0
0.38
1
01/29/22 09:16
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 09:16
75-69-4
v3
ND
ug/L
1.0
0.26
1
01/29/22 09:16
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 09:16
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 62 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"rwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FD-20220126-1
Parameters
Lab ID: 92584910024 Collected:
Report
Results Units Limit
01/26/22 00:00
MDL DF
Received: 01/27/22 13:30 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 09:16
75-01-4
Xylene (Total)
75.1 ug/L 1.0
0.34
1
01/29/22 09:16
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96 % 70-130
1
01/29/22 09:16
460-00-4
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
01/29/22 09:16
17060-07-0
Toluene-d8 (S)
99 % 70-130
1
01/29/22 09:16
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 07:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
01/28/22 07:37
17060-07-0
Toluene-d8 (S)
94 % 66-133
1
01/28/22 07:37
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 63 of 102

leAnalytical
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Pace Analytical Services, LLC
Padg"rwy ie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_TB-20220124-0930 Lab ID: 92584910025 Collected: 01/24/22 09:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
12.6J
ug/L
25.0
5.1
1
01/31/2215:05
67-64-1 C7
ND
ug/L
10.0
1.8
1
01/31/2215:05
107-13-1
ND
ug/L
1.0
0.34
1
01 /31 /22 15:05
71-43-2
ND
ug/L
1.0
0.47
1
01 /31 /22 15:05
74-97-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:05
75-27-4
ND
ug/L
1.0
0.34
1
01 /31 /22 15:05
75-25-2
ND
ug/L
2.0
1.7
1
01 /31 /22 15:05
74-83-9
ND
ug/L
5.0
4.0
1
01/31/2215:05
78-93-3 C7
ND
ug/L
2.0
0.73
1
01/31/2215:05
75-15-0
ND
ug/L
1.0
0.33
1
01 /31 /22 15:05
56-23-5
ND
ug/L
1.0
0.28
1
01 /31 /22 15:05
108-90-7
ND
ug/L
1.0
0.65
1
01 /31 /22 15:05
75-00-3
ND
ug/L
1.0
0.43
1
01 /31 /22 15:05
67-66-3
ND
ug/L
1.0
0.54
1
01 /31 /22 15:05
74-87-3
ND
ug/L
2.0
0.34
1
01/31/2215:05
96-12-8
ND
ug/L
1.0
0.36
1
01/31/2215:05
124-48-1
ND
ug/L
1.0
0.27
1
01 /31 /22 15:05
106-93-4
ND
ug/L
1.0
0.39
1
01 /31 /22 15:05
74-95-3
ND
ug/L
1.0
0.34
1
01/31/2215:05
95-50-1
ND
ug/L
1.0
0.33
1
01 /31 /22 15:05
106-46-7
ND
ug/L
1.0
0.56
1
01/31/2215:05
110-57-6 v1
ND
ug/L
1.0
0.37
1
01 /31 /22 15:05
75-34-3
ND
ug/L
1.0
0.32
1
01 /31 /22 15:05
107-06-2
ND
ug/L
1.0
0.35
1
01 /31 /22 15:05
75-35-4
ND
ug/L
1.0
0.38
1
01 /31 /22 15:05
156-59-2
ND
ug/L
1.0
0.40
1
01 /31 /22 15:05
156-60-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:05
78-87-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:05
10061-01-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:05
10061-02-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:05
100-41-4
0.79J
ug/L
5.0
0.48
1
01 /31 /22 15:05
591-78-6
ND
ug/L
20.0
9.7
1
01 /31 /22 15:05
74-88-4
ND
ug/L
5.0
2.0
1
01 /31 /22 15:05
75-09-2
ND
ug/L
5.0
2.7
1
01/31/2215:05
108-10-1
ND
ug/L
1.0
0.29
1
01 /31 /22 15:05
100-42-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:05
630-20-6
ND
ug/L
1.0
0.22
1
01 /31 /22 15:05
79-34-5
ND
ug/L
1.0
0.29
1
01/31/2215:05
127-18-4
ND
ug/L
1.0
0.48
1
01 /31 /22 15:05
108-88-3
ND
ug/L
1.0
0.33
1
01 /31 /22 15:05
71-55-6
ND
ug/L
1.0
0.32
1
01 /31 /22 15:05
79-00-5
ND
ug/L
1.0
0.38
1
01 /31 /22 15:05
79-01-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:05
75-69-4
ND
ug/L
1.0
0.26
1
01/31/2215:05
96-18-4
ND
ug/L
2.0
1.3
1
01 /31 /22 15:05
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 64 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"rwyoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_TB-20220124-0930 Lab ID: 92584910025 Collected: 01/24/22 09:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L
1.0
0.39 1
01/31/22 15:05
75-01-4
Xylene (Total)
ND ug/L
1.0
0.34 1
01/31/22 15:05
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/31/22 15:05
460-00-4 CO
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/31/22 15:05
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
01/31/22 15:05
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services
- Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
0.86 1
01/27/22 19:25
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 %
70-130
1
01/27/22 19:25
17060-07-0
Toluene-d8 (S)
95 %
66-133
1
01/27/22 19:25
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 65 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgopibrwyeie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220126-1145 Lab ID: 92584910026 Collected: 01/26/22 11:45 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 00:51
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 00:51
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 00:51
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 00:51
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 00:51
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 00:51
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 00:51
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 00:51
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 00:51
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 00:51
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 00:51
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 00:51
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 00:51
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 00:51
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 00:51
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 00:51
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 00:51
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 00:51
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 00:51
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 00:51
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 00:51
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 00:51
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 00:51
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 00:51
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 00:51
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 00:51
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 00:51
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 00:51
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 00:51
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 00:51
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 00:51
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 00:51
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 00:51
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 00:51
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 00:51
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 00:51
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 00:51
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 00:51
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 00:51
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 00:51
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 00:51
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 00:51
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 00:51
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 00:51
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 00:51
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v1
IN
v1
v1
Page 66 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pad8op1y6fy&f.. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220126-1145
Parameters
Lab ID: 92584910026 Collected:
Report
Results Units Limit
01/26/22 11:45
MDL DF
Received: 01/27/22 13:30 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 00:51
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 00:51
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96 % 70-130
1
01/29/22 00:51
460-00-4
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
01/29/22 00:51
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/29/22 00:51
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/27/22 19:44
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93 % 70-130
1
01/27/22 19:44
17060-07-0
Toluene-d8 (S)
95 % 66-133
1
01/27/22 19:44
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 67 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PadgomweyAie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220124-1600 Lab ID: 92584910027 Collected: 01/24/22 16:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
12.3J
ug/L
25.0
5.1
1
01/31/2215:23
67-64-1 C7
ND
ug/L
10.0
1.8
1
01/31/2215:23
107-13-1
ND
ug/L
1.0
0.34
1
01 /31 /22 15:23
71-43-2
ND
ug/L
1.0
0.47
1
01 /31 /22 15:23
74-97-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:23
75-27-4
ND
ug/L
1.0
0.34
1
01 /31 /22 15:23
75-25-2
ND
ug/L
2.0
1.7
1
01 /31 /22 15:23
74-83-9
4.0.1
ug/L
5.0
4.0
1
01/31/22 15:23
78-93-3 C7
ND
ug/L
2.0
0.73
1
01/31/2215:23
75-15-0
ND
ug/L
1.0
0.33
1
01 /31 /22 15:23
56-23-5
ND
ug/L
1.0
0.28
1
01 /31 /22 15:23
108-90-7
ND
ug/L
1.0
0.65
1
01 /31 /22 15:23
75-00-3
ND
ug/L
1.0
0.43
1
01 /31 /22 15:23
67-66-3
ND
ug/L
1.0
0.54
1
01 /31 /22 15:23
74-87-3
ND
ug/L
2.0
0.34
1
01/31/2215:23
96-12-8
ND
ug/L
1.0
0.36
1
01/31/2215:23
124-48-1
ND
ug/L
1.0
0.27
1
01 /31 /22 15:23
106-93-4
ND
ug/L
1.0
0.39
1
01 /31 /22 15:23
74-95-3
ND
ug/L
1.0
0.34
1
01/31/2215:23
95-50-1
ND
ug/L
1.0
0.33
1
01 /31 /22 15:23
106-46-7
ND
ug/L
1.0
0.56
1
01/31/2215:23
110-57-6 v1
ND
ug/L
1.0
0.37
1
01 /31 /22 15:23
75-34-3
ND
ug/L
1.0
0.32
1
01 /31 /22 15:23
107-06-2
ND
ug/L
1.0
0.35
1
01 /31 /22 15:23
75-35-4
ND
ug/L
1.0
0.38
1
01 /31 /22 15:23
156-59-2
ND
ug/L
1.0
0.40
1
01 /31 /22 15:23
156-60-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:23
78-87-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:23
10061-01-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:23
10061-02-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:23
100-41-4
0.83J
ug/L
5.0
0.48
1
01 /31 /22 15:23
591-78-6
ND
ug/L
20.0
9.7
1
01 /31 /22 15:23
74-88-4
ND
ug/L
5.0
2.0
1
01 /31 /22 15:23
75-09-2
ND
ug/L
5.0
2.7
1
01/31/2215:23
108-10-1
ND
ug/L
1.0
0.29
1
01 /31 /22 15:23
100-42-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:23
630-20-6
ND
ug/L
1.0
0.22
1
01 /31 /22 15:23
79-34-5
ND
ug/L
1.0
0.29
1
01/31/2215:23
127-18-4
ND
ug/L
1.0
0.48
1
01 /31 /22 15:23
108-88-3
ND
ug/L
1.0
0.33
1
01 /31 /22 15:23
71-55-6
ND
ug/L
1.0
0.32
1
01 /31 /22 15:23
79-00-5
ND
ug/L
1.0
0.38
1
01 /31 /22 15:23
79-01-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:23
75-69-4
ND
ug/L
1.0
0.26
1
01/31/2215:23
96-18-4
ND
ug/L
2.0
1.3
1
01 /31 /22 15:23
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 68 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgop1lsweyeye. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220124-1600 Lab ID: 92584910027 Collected: 01/24/22 16:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L
1.0
0.39 1
01/31/22 15:23
75-01-4
Xylene (Total)
ND ug/L
1.0
0.34 1
01/31/22 15:23
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/31/22 15:23
460-00-4 CO
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
01/31/22 15:23
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
01/31/22 15:23
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services
- Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
0.86 1
01/27/22 20:03
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
01/27/22 20:03
17060-07-0
Toluene-d8 (S)
96 %
66-133
1
01/27/22 20:03
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 69 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pad8opoirwYoe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220125-1230 Lab ID: 92584910028 Collected: 01/25/22 12:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
12.5J
ug/L
25.0
5.1
1
01/31/2215:42
67-64-1 C7
ND
ug/L
10.0
1.8
1
01/31/2215:42
107-13-1
ND
ug/L
1.0
0.34
1
01 /31 /22 15:42
71-43-2
ND
ug/L
1.0
0.47
1
01 /31 /22 15:42
74-97-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:42
75-27-4
ND
ug/L
1.0
0.34
1
01 /31 /22 15:42
75-25-2
ND
ug/L
2.0
1.7
1
01 /31 /22 15:42
74-83-9
ND
ug/L
5.0
4.0
1
01/31/2215:42
78-93-3 C7
ND
ug/L
2.0
0.73
1
01/31/2215:42
75-15-0
ND
ug/L
1.0
0.33
1
01 /31 /22 15:42
56-23-5
ND
ug/L
1.0
0.28
1
01 /31 /22 15:42
108-90-7
ND
ug/L
1.0
0.65
1
01 /31 /22 15:42
75-00-3
ND
ug/L
1.0
0.43
1
01 /31 /22 15:42
67-66-3
ND
ug/L
1.0
0.54
1
01 /31 /22 15:42
74-87-3
ND
ug/L
2.0
0.34
1
01/31/2215:42
96-12-8
ND
ug/L
1.0
0.36
1
01/31/2215:42
124-48-1
ND
ug/L
1.0
0.27
1
01 /31 /22 15:42
106-93-4
ND
ug/L
1.0
0.39
1
01 /31 /22 15:42
74-95-3
ND
ug/L
1.0
0.34
1
01/31/2215:42
95-50-1
ND
ug/L
1.0
0.33
1
01 /31 /22 15:42
106-46-7
ND
ug/L
1.0
0.56
1
01/31/2215:42
110-57-6 v1
ND
ug/L
1.0
0.37
1
01 /31 /22 15:42
75-34-3
ND
ug/L
1.0
0.32
1
01 /31 /22 15:42
107-06-2
ND
ug/L
1.0
0.35
1
01 /31 /22 15:42
75-35-4
ND
ug/L
1.0
0.38
1
01 /31 /22 15:42
156-59-2
ND
ug/L
1.0
0.40
1
01 /31 /22 15:42
156-60-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:42
78-87-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:42
10061-01-5
ND
ug/L
1.0
0.36
1
01 /31 /22 15:42
10061-02-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:42
100-41-4
0.83J
ug/L
5.0
0.48
1
01 /31 /22 15:42
591-78-6
ND
ug/L
20.0
9.7
1
01 /31 /22 15:42
74-88-4
ND
ug/L
5.0
2.0
1
01 /31 /22 15:42
75-09-2
ND
ug/L
5.0
2.7
1
01/31/2215:42
108-10-1
ND
ug/L
1.0
0.29
1
01 /31 /22 15:42
100-42-5
ND
ug/L
1.0
0.31
1
01 /31 /22 15:42
630-20-6
ND
ug/L
1.0
0.22
1
01 /31 /22 15:42
79-34-5
ND
ug/L
1.0
0.29
1
01/31/2215:42
127-18-4
ND
ug/L
1.0
0.48
1
01 /31 /22 15:42
108-88-3
ND
ug/L
1.0
0.33
1
01 /31 /22 15:42
71-55-6
ND
ug/L
1.0
0.32
1
01 /31 /22 15:42
79-00-5
ND
ug/L
1.0
0.38
1
01 /31 /22 15:42
79-01-6
ND
ug/L
1.0
0.30
1
01 /31 /22 15:42
75-69-4
ND
ug/L
1.0
0.26
1
01/31/2215:42
96-18-4
ND
ug/L
2.0
1.3
1
01 /31 /22 15:42
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 70 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PadgomweyAie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FB-20220125-1230 Lab ID: 92584910028 Collected: 01/25/22 12:30 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L
1.0
0.39 1
01/31/22 15:42
75-01-4
Xylene (Total)
ND ug/L
1.0
0.34 1
01/31/22 15:42
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/31/22 15:42
460-00-4 CO
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
01/31/22 15:42
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
01/31/22 15:42
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services
- Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
0.86 1
01/27/22 20:23
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 %
70-130
1
01/27/22 20:23
17060-07-0
Toluene-d8 (S)
95 %
66-133
1
01/27/22 20:23
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 71 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Pa8gomwey0e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FD-20220125-1 Lab ID: 92584910029 Collected: 01/25/22 00:00 Received: 01/27/22 13:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Date: 02/02/2022 04:59 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
01/29/22 08:58
67-64-1
ND
ug/L
10.0
1.8
1
01/29/22 08:58
107-13-1
ND
ug/L
1.0
0.34
1
01/29/22 08:58
71-43-2
ND
ug/L
1.0
0.47
1
01/29/22 08:58
74-97-5
ND
ug/L
1.0
0.31
1
01/29/22 08:58
75-27-4
ND
ug/L
1.0
0.34
1
01/29/22 08:58
75-25-2
ND
ug/L
2.0
1.7
1
01/29/22 08:58
74-83-9
ND
ug/L
5.0
4.0
1
01/29/22 08:58
78-93-3
ND
ug/L
2.0
0.73
1
01/29/22 08:58
75-15-0
ND
ug/L
1.0
0.33
1
01/29/22 08:58
56-23-5
ND
ug/L
1.0
0.28
1
01/29/22 08:58
108-90-7
ND
ug/L
1.0
0.65
1
01/29/22 08:58
75-00-3
ND
ug/L
1.0
0.43
1
01/29/22 08:58
67-66-3
ND
ug/L
1.0
0.54
1
01/29/22 08:58
74-87-3
ND
ug/L
2.0
0.34
1
01/29/22 08:58
96-12-8
ND
ug/L
1.0
0.36
1
01/29/22 08:58
124-48-1
ND
ug/L
1.0
0.27
1
01/29/22 08:58
106-93-4
ND
ug/L
1.0
0.39
1
01/29/22 08:58
74-95-3
ND
ug/L
1.0
0.34
1
01/29/22 08:58
95-50-1
ND
ug/L
1.0
0.33
1
01/29/22 08:58
106-46-7
ND
ug/L
1.0
0.56
1
01/29/22 08:58
110-57-6
ND
ug/L
1.0
0.37
1
01/29/22 08:58
75-34-3
ND
ug/L
1.0
0.32
1
01/29/22 08:58
107-06-2
ND
ug/L
1.0
0.35
1
01/29/22 08:58
75-35-4
ND
ug/L
1.0
0.38
1
01/29/22 08:58
156-59-2
ND
ug/L
1.0
0.40
1
01/29/22 08:58
156-60-5
ND
ug/L
1.0
0.36
1
01/29/22 08:58
78-87-5
ND
ug/L
1.0
0.36
1
01/29/22 08:58
10061-01-5
ND
ug/L
1.0
0.36
1
01/29/22 08:58
10061-02-6
ND
ug/L
1.0
0.30
1
01/29/22 08:58
100-41-4
ND
ug/L
5.0
0.48
1
01/29/22 08:58
591-78-6
ND
ug/L
20.0
9.7
1
01/29/22 08:58
74-88-4
ND
ug/L
5.0
2.0
1
01/29/22 08:58
75-09-2
ND
ug/L
5.0
2.7
1
01/29/22 08:58
108-10-1
ND
ug/L
1.0
0.29
1
01/29/22 08:58
100-42-5
ND
ug/L
1.0
0.31
1
01/29/22 08:58
630-20-6
ND
ug/L
1.0
0.22
1
01/29/22 08:58
79-34-5
ND
ug/L
1.0
0.29
1
01/29/22 08:58
127-18-4
ND
ug/L
1.0
0.48
1
01/29/22 08:58
108-88-3
ND
ug/L
1.0
0.33
1
01/29/22 08:58
71-55-6
ND
ug/L
1.0
0.32
1
01/29/22 08:58
79-00-5
ND
ug/L
1.0
0.38
1
01/29/22 08:58
79-01-6
ND
ug/L
1.0
0.30
1
01/29/22 08:58
75-69-4
ND
ug/L
1.0
0.26
1
01/29/22 08:58
96-18-4
ND
ug/L
2.0
1.3
1
01/29/22 08:58
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IH.v1
IN
v1
v1
Page 72 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PadgomweyAie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J22010014 MNS LF
Pace Project No.: 92584910
Sample: MNS_FD-20220125-1
Parameters
Lab ID: 92584910029 Collected:
Report
Results Units Limit
01/25/22 00:00
MDL DF
Received: 01/27/22 13:30 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L 1.0
0.39
1
01/29/22 08:58
75-01-4
Xylene (Total)
ND ug/L 1.0
0.34
1
01/29/22 08:58
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96 % 70-130
1
01/29/22 08:58
460-00-4
1,2-Dichloroethane-d4 (S)
103 % 70-130
1
01/29/22 08:58
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
01/29/22 08:58
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
0.86
1
01/28/22 07:56
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89 % 70-130
1
01/28/22 07:56
17060-07-0
Toluene-d8(S)
92 % 66-133
1
01/28/22 07:56
2037-26-5
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 73 of 102

leAnalytical
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Pace Analytical Services, LLC
PadgomyAie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674609 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910001
METHOD BLANK: 3530850
Associated Lab Samples: 92584910001
Parameter Units
1,1,1,2-Tetrachloroethane
ug/L
1,1,1-Trichloroethane
ug/L
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2,3-Trichloropropane
ug/L
1,2-Dibromo-3-chloropropane
ug/L
1,2-Dibromoethane (EDB)
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,4-Dichlorobenzene
ug/L
2-Butanone (MEK)
ug/L
2-Hexanone
ug/L
4-Methyl-2-pentanone (MIBK)
ug/L
Acetone
ug/L
Acrylonitrile
ug/L
Benzene
ug/L
Bromochloromethane
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon disulfide
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis-1,2-Dichloroethene
ug/L
cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Dibromomethane
ug/L
Ethylbenzene
ug/L
lodomethane
ug/L
Methylene Chloride
ug/L
Styrene
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
Matrix: Water
Blank
Result
Reporting
Limit
MDL
Analyzed Qualifiers
ND
1.0
0.31
01 /28/22 11:58
ND
1.0
0.33
01 /28/22 11:58
ND
1.0
0.22
01 /28/22 11:58
ND
1.0
0.32
01 /28/22 11:58
ND
1.0
0.37
01 /28/22 11:58
ND
1.0
0.35
01 /28/22 11:58
ND
1.0
0.26
01 /28/22 11:58
ND
2.0
0.34
01 /28/22 11:58
ND
1.0
0.27
01 /28/22 11:58
ND
1.0
0.34
01 /28/22 11:58
ND
1.0
0.32
01 /28/22 11:58
ND
1.0
0.36
01 /28/22 11:58
ND
1.0
0.33
01 /28/22 11:58
ND
5.0
4.0
01 /28/22 11:58
ND
5.0
0.48
01 /28/22 11:58
ND
5.0
2.7
01 /28/22 11:58
ND
25.0
5.1
01 /28/22 11:58
ND
10.0
1.8
01 /28/22 11:58
ND
1.0
0.34
01 /28/22 11:58
ND
1.0
0.47
01 /28/22 11:58
ND
1.0
0.31
01 /28/22 11:58
ND
1.0
0.34
01 /28/22 11:58
ND
2.0
1.7
01/28/2211:58 IH,v1
ND
2.0
0.73
01 /28/22 11:58
ND
1.0
0.33
01 /28/22 11:58
ND
1.0
0.28
01 /28/22 11:58
ND
1.0
0.65
01 /28/22 11:58 I K
ND
1.0
0.43
01 /28/22 11:58
ND
1.0
0.54
01 /28/22 11:58
ND
1.0
0.38
01 /28/22 11:58
ND
1.0
0.36
01 /28/22 11:58
ND
1.0
0.36
01 /28/22 11:58
ND
1.0
0.39
01 /28/22 11:58
ND
1.0
0.30
01 /28/22 11:58
ND
20.0
9.7
01 /28/22 11:58 v1
ND
5.0
2.0
01 /28/22 11:58
ND
1.0
0.29
01 /28/22 11:58
ND
1.0
0.29
01 /28/22 11:58
ND
1.0
0.48
01 /28/22 11:58
ND
1.0
0.40
01 /28/22 11:58
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 74 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PadgomyAie. Suite 100
Huntersville, NC 28078
[phone]
Project: J22010014 MNS LF
Pace Project No.: 92584910
METHOD BLANK: 3530850
Associated Lab Samples: 92584910001
Parameter
Units
trans- 1,3-Dichloropropene
ug/L
trans-1,4-Dichloro-2-butene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
Vinyl acetate
ug/L
Vinyl chloride
ug/L
Xylene (Total)
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LABORATORY CONTROL SAMPLE: 3530851
Parameter
QUALITY CONTROL DATA
Matrix: Water
Blank
Result
Reporting
Limit
ND
1.0
ND
1.0
ND
1.0
ND
1.0
ND
2.0
ND
1.0
ND
1.0
103
70-130
99
70-130
100
70-130
MDL Analyzed
0.36
01 /28/22 11:58
0.56
01 /28/22 11:58
0.38
01 /28/22 11:58
0.30
01 /28/22 11:58
1.3
01 /28/22 11:58
0.39
01 /28/22 11:58
0.34
01 /28/22 11:58
01 /28/22 11:58
01 /28/22 11:58
01 /28/22 11:58
v1
Qualifiers
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.7
101
70-130
1,1,1-Trichloroethane
ug/L
50
50.7
101
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.3
101
70-130
1,1,2-Trichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethane
ug/L
50
51.3
103
70-130
1,1-Dichloroethene
ug/L
50
48.9
98
70-132
1,2,3-Trichloropropane
ug/L
50
50.4
101
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.9
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.7
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.3
97
70-130
1,2-Dichloroethane
ug/L
50
52.2
104
70-130
1,2-Dichloropropane
ug/L
50
51.4
103
70-130
1,4-Dichlorobenzene
ug/L
50
48.3
97
70-130
2-Butanone (MEK)
ug/L
100
95.0
95
70-133
2-Hexanone
ug/L
100
94.7
95
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
96.8
97
70-130
Acetone
ug/L
100
98.0
98
70-144
Acrylonitrile
ug/L
250
249
99
70-130
Benzene
ug/L
50
49.7
99
70-130
Bromochloromethane
ug/L
50
50.9
102
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
54.5
109
70-131
Bromomethane
ug/L
50
69.2
138
30-177lH,v1
Carbon disulfide
ug/L
50
52.2
104
70-133
Carbon tetrachloride
ug/L
50
50.9
102
70-130
Chlorobenzene
ug/L
50
49.6
99
70-130
Chloroethane
ug/L
50
48.5
97
46-131 IK
Chloroform
ug/L
50
50.1
100
70-130
Chloromethane
ug/L
50
56.8
114
49-130
cis-1,2-Dichloroethene
ug/L
50
51.7
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 75 of 102

Pace Analytical Services, LLC
ceAnalytical padi yAie. Suite100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
LABORATORY CONTROL SAMPLE:
Parameter
3530851
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,3-Dichloropropene
ug/L
50
52.8
106
70-130
Dibromochloromethane
ug/L
50
50.6
101
70-130
Dibromomethane
ug/L
50
50.8
102
70-130
Ethylbenzene
ug/L
50
49.1
98
70-130
lodomethane
ug/L
100
122
122
47-140 v1
Methylene Chloride
ug/L
50
49.0
98
68-130
Styrene
ug/L
50
51.8
104
70-130
Tetrachloroethene
ug/L
50
49.3
99
70-130
Toluene
ug/L
50
50.1
100
70-130
trans-1,2-Dichloroethene
ug/L
50
52.1
104
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.7
107
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
68.3
137
25-200 v1
Trichloroethene
ug/L
50
50.2
100
70-130
Trichlorofluoromethane
ug/L
50
45.2
90
61-130
Vinyl acetate
ug/L
100
108
108
70-140
Vinyl chloride
ug/L
50
57.3
115
59-142
Xylene (Total)
ug/L
150
148
98
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530852
MS
92584422005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3530853
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
500
500
577
542
115
108
70-135
6
30
1,1,1-Trichloroethane
ug/L
ND
500
500
558
500
112
100
70-148
11
30
1,1,2,2-Tetrachloroethane
ug/L
ND
500
500
579
545
116
109
70-131
6
30
1,1,2-Trichloroethane
ug/L
ND
500
500
582
566
116
113
70-136
3
30
1,1-Dichloroethane
ug/L
ND
500
500
539
499
108
100
70-147
8
30
1,1-Dichloroethene
ug/L
ND
500
500
533
474
107
95
70-158
12
30
1,2,3-Trichloropropane
ug/L
ND
500
500
572
535
114
107
67-137
7
30
1,2-Dibromo-3-
ug/L
ND
500
500
581
601
116
120
69-136
3
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
500
500
568
538
114
108
70-137
5
30
1,2-Dichlorobenzene
ug/L
ND
500
500
522
512
104
102
70-133
2
30
1,2-Dichloroethane
ug/L
ND
500
500
563
520
113
104
67-138
8
30
1,2-Dichloropropane
ug/L
ND
500
500
566
534
113
107
70-138
6
30
1,4-Dichlorobenzene
ug/L
ND
500
500
538
498
108
100
70-133
8
30
2-Butanone (MEK)
ug/L
ND
1000
1000
1010
1040
101
104
61-147
2
30
2-Hexanone
ug/L
ND
1000
1000
1090
1090
109
109
67-139
0
30
4-Methyl-2-pentanone
ug/L
ND
1000
1000
1100
1090
110
109
67-136
1
30
(MIBK)
Acetone ug/L
ND 1000 1000 1000 979 100 98 55-159
2 30
Acrylonitrile ug/L
ND 2500 2500 2640 2620 106 105 68-140
1 30
Benzene ug/L
ND 500 500 526 505 103 99 67-150
4 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM
without the written consent of Pace Analytical Services, LLC.
Page 76 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"IirpYo.. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530852
MS
92584422005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3530853
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Bromochloromethane
ug/L
ND
500
500
534
521
107
104
70-146
2
30
Bromodichloromethane
ug/L
ND
500
500
568
555
114
111
70-138
2
30
Bromoform
ug/L
ND
500
500
585
566
117
113
57-138
3
30
Bromomethane
ug/L
ND
500
500
587
607
117
121
10-200
3
30 IH,v1
Carbon disulfide
ug/L
ND
500
500
504
455
101
91
70-152
10
30
Carbon tetrachloride
ug/L
ND
500
500
571
491
114
98
70-147
15
30
Chlorobenzene
ug/L
ND
500
500
565
530
113
106
70-137
6
30
Chloroethane
ug/L
ND
500
500
585
528
117
106
51-166
10
30 IK
Chloroform
ug/L
ND
500
500
553
512
110
102
70-144
8
30
Chloromethane
ug/L
ND
500
500
548
511
110
102
24-161
7
30
cis-1,2-Dichloroethene
ug/L
1630
500
500
2210
2150
118
106
67-148
3
30
cis-1,3-Dichloropropene
ug/L
ND
500
500
581
548
116
110
70-142
6
30
Dibromochloromethane
ug/L
ND
500
500
554
520
111
104
68-138
6
30
Dibromomethane
ug/L
ND
500
500
543
519
109
104
70-134
5
30
Ethylbenzene
ug/L
ND
500
500
573
535
115
107
68-143
7
30
lodomethane
ug/L
ND
1000
1000
963
929
96
93
20-161
4
30 v1
Methylene Chloride
ug/L
ND
500
500
614
573
117
109
64-148
7
30
Styrene
ug/L
ND
500
500
564
538
113
108
70-136
5
30
Tetrachloroethene
ug/L
ND
500
500
556
501
111
100
70-139
10
30
Toluene
ug/L
ND
500
500
551
511
110
102
47-157
8
30
trans-1,2-Dichloroethene
ug/L
ND
500
500
549
505
110
101
70-149
8
30
trans-1,3-Dichloropropene
ug/L
ND
500
500
577
555
115
111
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
500
500
567
561
113
112
31-145
1
30 v1
Trichloroethene
ug/L
2790
500
500
3390
3340
120
111
70-149
1
30
Trichlorofluoromethane
ug/L
ND
500
500
557
414
111
83
61-154
29
30
Vinyl acetate
ug/L
ND
1000
1000
1140
1110
114
111
48-156
3
30
Vinyl chloride
ug/L
ND
500
500
591
511
114
98
55-172
14
30
Xylene (Total)
ug/L
ND
1500
1500
1710
1590
114
106
66-145
7
30
1,2-Dichloroethane-d4 (S)
%
103
100
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8 (S)
%
100
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 77 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgaphrwyoe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674641 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910002, 92584910003, 92584910004, 92584910005, 92584910006, 92584910007, 92584910008,
92584910009,92584910010,92584910011,92584910012,92584910013,92584910014,92584910015,
92584910016,92584910017,92584910018,92584910019,92584910020,92584910021
METHOD BLANK: 3531103 Matrix: Water
Associated Lab Samples: 92584910002, 92584910003, 92584910004, 92584910005, 92584910006, 92584910007, 92584910008,
92584910009,92584910010,92584910011,92584910012,92584910013,92584910014,92584910015,
92584910016,92584910017,92584910018,92584910019,92584910020,92584910021
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
01/29/22 01:02
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
01/29/22 01:02
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
01/29/22 01:02
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
01/29/22 01:02
1,1-Dichloroethane
ug/L
ND
1.0
0.37
01/29/22 01:02
1,1-Dichloroethene
ug/L
ND
1.0
0.35
01/29/22 01:02
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
01/29/22 01:02
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
01/29/22 01:02
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
01/29/22 01:02
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
01/29/22 01:02
1,2-Dichloroethane
ug/L
ND
1.0
0.32
01/29/22 01:02
1,2-Dichloropropane
ug/L
ND
1.0
0.36
01/29/22 01:02
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
01/29/22 01:02
2-Butanone (MEK)
ug/L
ND
5.0
4.0
01/29/22 01:02
2-Hexanone
ug/L
ND
5.0
0.48
01/29/22 01:02
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
01/29/22 01:02
Acetone
ug/L
ND
25.0
5.1
01/29/22 01:02
Acrylonitrile
ug/L
ND
10.0
1.8
01/29/22 01:02
Benzene
ug/L
ND
1.0
0.34
01/29/22 01:02
Bromochloromethane
ug/L
ND
1.0
0.47
01/29/22 01:02
Bromodichloromethane
ug/L
ND
1.0
0.31
01/29/22 01:02
Bromoform
ug/L
ND
1.0
0.34
01/29/22 01:02
Bromomethane
ug/L
ND
2.0
1.7
01/29/22 01:02
Carbon disulfide
ug/L
ND
2.0
0.73
01/29/22 01:02
Carbon tetrachloride
ug/L
ND
1.0
0.33
01/29/22 01:02
Chlorobenzene
ug/L
ND
1.0
0.28
01/29/22 01:02
Chloroethane
ug/L
ND
1.0
0.65
01/29/22 01:02
Chloroform
ug/L
ND
1.0
0.43
01/29/22 01:02
Chloromethane
ug/L
ND
1.0
0.54
01/29/22 01:02
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
01/29/22 01:02
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/29/22 01:02
Dibromochloromethane
ug/L
ND
1.0
0.36
01/29/22 01:02
Dibromomethane
ug/L
ND
1.0
0.39
01/29/22 01:02
Ethylbenzene
ug/L
ND
1.0
0.30
01/29/22 01:02
lodomethane
ug/L
ND
20.0
9.7
01/29/22 01:02
Methylene Chloride
ug/L
ND
5.0
2.0
01/29/22 01:02
Styrene
ug/L
ND
1.0
0.29
01/29/22 01:02
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"rwy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
METHOD BLANK: 3531103 Matrix: Water
Associated Lab Samples: 92584910002, 92584910003, 92584910004, 92584910005, 92584910006, 92584910007, 92584910008,
92584910009,92584910010,92584910011,92584910012,92584910013,92584910014,92584910015,
92584910016,92584910017,92584910018,92584910019,92584910020,92584910021
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Tetrachloroethene
ug/L
ND
1.0
0.29
01/29/22 01:02
Toluene
ug/L
ND
1.0
0.48
01/29/22 01:02
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
01/29/22 01:02
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/29/22 01:02
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
01/29/22 01:02 v1
Trichloroethene
ug/L
ND
1.0
0.38
01/29/22 01:02
Trichlorofluoromethane
ug/L
ND
1.0
0.30
01/29/22 01:02
Vinyl acetate
ug/L
ND
2.0
1.3
01/29/22 01:02
Vinyl chloride
ug/L
ND
1.0
0.39
01/29/22 01:02
Xylene (Total)
ug/L
ND
1.0
0.34
01/29/22 01:02
1,2-Dichloroethane-d4 (S)
%
98
70-130
01/29/22 01:02
4-Bromofluorobenzene (S)
%
97
70-130
01/29/22 01:02
Toluene-d8 (S)
%
97
70-130
01/29/22 01:02
LABORATORY CONTROL SAMPLE:
3531104
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.9
104
70-130
1,1,1-Trichloroethane
ug/L
50
46.0
92
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.9
98
70-130
1,1,2-Trichloroethane
ug/L
50
46.2
92
70-130
1,1-Dichloroethane
ug/L
50
44.7
89
70-130
1,1-Dichloroethene
ug/L
50
45.1
90
70-132
1,2,3-Trichloropropane
ug/L
50
53.9
108
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.2
98
70-132
1,2-Dibromoethane (EDB)
ug/L
50
48.4
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.7
101
70-130
1,2-Dichloroethane
ug/L
50
44.2
88
70-130
1,2-Dichloropropane
ug/L
50
47.3
95
70-130
1,4-Dichlorobenzene
ug/L
50
52.7
105
70-130
2-Butanone (MEK)
ug/L
100
87.2
87
70-133
2-Hexanone
ug/L
100
85.0
85
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
82.2
82
70-130
Acetone
ug/L
100
80.2
80
70-144
Acrylonitrile
ug/L
250
249
100
70-130
Benzene
ug/L
50
47.8
96
70-130
Bromochloromethane
ug/L
50
45.8
92
70-130
Bromodichloromethane
ug/L
50
45.5
91
70-130
Bromoform
ug/L
50
51.1
102
70-131
Bromomethane
ug/L
50
60.7
121
30-177
Carbon disulfide
ug/L
50
49.4
99
70-133
Carbon tetrachloride
ug/L
50
49.1
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 79 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padfftirwyoe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
LABORATORY CONTROL SAMPLE:
Parameter
3531104
Units
Spike LCS
Conc. Result
Chlorobenzene
ug/L
50
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
49.7
99
70-130
44.0
88
46-131
46.2
92
70-130
46.6
93
49-130
45.6
91
70-130
47.4
95
70-130
47.0
94
70-130
47.7
95
70-130
50.1
100
70-130
92.3
92
47-140
41.1
82
68-130
50.7
101
70-130
50.5
101
70-130
46.9
94
70-130
45.6
91
70-130
46.6
93
70-130
36.6
73
25-200 v1
49.4
99
70-130
44.3
89
61-130
94.6
95
70-140
52.0
104
59-142
150
100
70-130
102
70-130
98
70-130
97
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3531105
MS
92584910002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3531106
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
27.6
25.9
138
130
70-135
6
30 M1
1,1,1-Trichloroethane
ug/L
ND
20
20
25.6
24.1
128
121
70-148
6
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
26.4
25.0
132
125
70-131
5
30 M1
1,1,2-Trichloroethane
ug/L
ND
20
20
24.9
23.7
124
119
70-136
5
30
1,1-Dichloroethane
ug/L
ND
20
20
24.7
23.2
123
116
70-147
6
30
1,1-Dichloroethene
ug/L
ND
20
20
25.3
23.6
126
118
70-158
7
30
1,2,3-Trichloropropane
ug/L
ND
20
20
27.9
25.8
139
129
67-137
8
30 M1
1,2-Dibromo-3-
ug/L
ND
20
20
26.0
25.4
130
127
69-136
2
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
26.1
24.6
131
123
70-137
6
30
1,2-Dichlorobenzene
ug/L
ND
20
20
26.9
25.7
135
128
70-133
5
30 M1
1,2-Dichloroethane
ug/L
ND
20
20
24.4
22.9
122
114
67-138
6
30
1,2-Dichloropropane
ug/L
ND
20
20
25.7
24.1
129
120
70-138
7
30
1,4-Dichlorobenzene
ug/L
ND
20
20
27.4
26.3
137
132
70-133
4
30 M1
2-Butanone (MEK)
ug/L
ND
40
40
47.9
45.1
120
113
61-147
6
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 80 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"ifyoe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3531105
3531106
MS
MSD
92584910002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Hexanone
ug/L
ND
40
40
46.3
43.8
116
109
67-139
6
30
4-Methyl-2-pentanone
ug/L
ND
40
40
44.2
42.0
110
105
67-136
5
30
(MIBK)
Acetone
ug/L
ND
40
40
45.3
43.1
113
108
55-159
5
30
Acrylonitrile
ug/L
ND
100
100
120
120
120
120
68-140
0
30
Benzene
ug/L
ND
20
20
26.2
24.9
131
124
67-150
5
30
Bromochloromethane
ug/L
ND
20
20
25.0
23.8
125
119
70-146
5
30
Bromodichloromethane
ug/L
ND
20
20
24.5
23.7
122
119
70-138
3
30
Bromoform
ug/L
ND
20
20
26.5
24.8
132
124
57-138
6
30
Bromomethane
ug/L
ND
20
20
32.0
31.6
160
158
10-200
1
30
Carbon disulfide
ug/L
ND
20
20
27.6
25.6
138
128
70-152
7
30
Carbon tetrachloride
ug/L
ND
20
20
27.7
26.2
139
131
70-147
5
30
Chlorobenzene
ug/L
ND
20
20
27.3
25.8
137
129
70-137
6
30
Chloroethane
ug/L
ND
20
20
28.8
26.8
144
134
51-166
7
30
Chloroform
ug/L
ND
20
20
25.5
23.8
127
119
70-144
7
30
Chloromethane
ug/L
ND
20
20
25.7
24.2
129
121
24-161
6
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
24.9
23.2
125
116
67-148
7
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
25.6
24.5
128
122
70-142
4
30
Dibromochloromethane
ug/L
ND
20
20
25.1
23.2
125
116
68-138
8
30
Dibromomethane
ug/L
ND
20
20
26.1
24.8
131
124
70-134
5
30
Ethylbenzene
ug/L
ND
20
20
27.6
25.6
138
128
68-143
8
30
lodomethane
ug/L
ND
40
40
45.0
41.5
112
104
20-161
8
30
Methylene Chloride
ug/L
ND
20
20
22.1
20.8
110
104
64-148
6
30
Styrene
ug/L
ND
20
20
27.4
25.6
137
128
70-136
7
30 M1
Tetrachloroethene
ug/L
ND
20
20
28.0
26.1
140
131
70-139
7
30 M1
Toluene
ug/L
ND
20
20
26.0
24.7
130
123
47-157
5
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
25.4
24.0
127
120
70-149
6
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
25.0
23.7
125
119
70-138
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
28.6
27.1
143
135
31-145
5
30 v1
Trichloroethene
ug/L
ND
20
20
27.3
25.8
136
129
70-149
6
30
Trichlorofluoromethane
ug/L
ND
20
20
26.4
24.6
132
123
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
49.5
46.7
124
117
48-156
6
30
Vinyl chloride
ug/L
ND
20
20
28.7
27.1
143
135
55-172
6
30
Xylene (Total)
ug/L
ND
60
60
82.4
77.0
137
128
66-145
7
30
1,2-Dichloroethane-d4 (S)
%
100
100
70-130
4-Bromofluorobenzene (S)
%
99
98
70-130
Toluene-d8 (S)
%
97
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 81 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
PadffArwy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674643 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910022, 92584910023, 92584910024, 92584910026, 92584910029
METHOD BLANK: 3531118 Matrix: Water
Associated Lab Samples: 92584910022, 92584910023, 92584910024, 92584910026, 92584910029
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
01/28/22 23:22
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
01/28/22 23:22
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
01/28/22 23:22
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
01/28/22 23:22
1,1-Dichloroethane
ug/L
ND
1.0
0.37
01/28/22 23:22
1,1-Dichloroethene
ug/L
ND
1.0
0.35
01/28/22 23:22
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
01/28/22 23:22
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
01/28/22 23:22
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
01/28/22 23:22
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
01/28/22 23:22
1,2-Dichloroethane
ug/L
ND
1.0
0.32
01/28/22 23:22
1,2-Dichloropropane
ug/L
ND
1.0
0.36
01/28/22 23:22
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
01/28/22 23:22
2-Butanone (MEK)
ug/L
ND
5.0
4.0
01/28/22 23:22
2-Hexanone
ug/L
ND
5.0
0.48
01/28/22 23:22
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
01/28/22 23:22
Acetone
ug/L
ND
25.0
5.1
01/28/22 23:22
Acrylonitrile
ug/L
ND
10.0
1.8
01/28/22 23:22
Benzene
ug/L
ND
1.0
0.34
01/28/22 23:22
Bromochloromethane
ug/L
ND
1.0
0.47
01/28/22 23:22
Bromodichloromethane
ug/L
ND
1.0
0.31
01/28/22 23:22
Bromoform
ug/L
ND
1.0
0.34
01/28/22 23:22
Bromomethane
ug/L
ND
2.0
1.7
01/28/22 23:22
Carbon disulfide
ug/L
ND
2.0
0.73
01/28/22 23:22
Carbon tetrachloride
ug/L
ND
1.0
0.33
01/28/22 23:22
Chlorobenzene
ug/L
ND
1.0
0.28
01/28/22 23:22
Chloroethane
ug/L
ND
1.0
0.65
01/28/22 23:22
Chloroform
ug/L
ND
1.0
0.43
01/28/22 23:22
Chloromethane
ug/L
ND
1.0
0.54
01/28/22 23:22
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
01/28/22 23:22
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/28/22 23:22
Dibromochloromethane
ug/L
ND
1.0
0.36
01/28/22 23:22
Dibromomethane
ug/L
ND
1.0
0.39
01/28/22 23:22
Ethylbenzene
ug/L
ND
1.0
0.30
01/28/22 23:22
lodomethane
ug/L
ND
20.0
9.7
01/28/22 23:22
Methylene Chloride
ug/L
ND
5.0
2.0
01/28/22 23:22
Styrene
ug/L
ND
1.0
0.29
01/28/22 23:22
Tetrachloroethene
ug/L
ND
1.0
0.29
01/28/22 23:22
Toluene
ug/L
ND
1.0
0.48
01/28/22 23:22
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
01/28/22 23:22
Qualifiers
IH.v1
IK
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"rwyoe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
METHOD BLANK: 3531118 Matrix: Water
Associated Lab Samples: 92584910022, 92584910023, 92584910024, 92584910026, 92584910029
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/28/22 23:22
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
01/28/22 23:22
Trichloroethene
ug/L
ND
1.0
0.38
01/28/22 23:22
Trichlorofluoromethane
ug/L
ND
1.0
0.30
01/28/22 23:22
Vinyl acetate
ug/L
ND
2.0
1.3
01/28/22 23:22
Vinyl chloride
ug/L
ND
1.0
0.39
01/28/22 23:22
Xylene (Total)
ug/L
ND
1.0
0.34
01/28/22 23:22
1,2-Dichloroethane-d4 (S)
%
99
70-130
01/28/22 23:22
4-Bromofluorobenzene (S)
%
97
70-130
01/28/22 23:22
Toluene-d8 (S)
%
102
70-130
01/28/22 23:22
LABORATORY CONTROL SAMPLE: 3531119
Parameter
Qualifiers
v1
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.2
100
70-130
1,1,1-Trichloroethane
ug/L
50
50.2
100
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.5
97
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
49.3
99
70-130
1,1-Dichloroethene
ug/L
50
48.6
97
70-132
1,2,3-Trichloropropane
ug/L
50
46.5
93
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.4
107
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.4
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.5
97
70-130
1,2-Dichloroethane
ug/L
50
50.0
100
70-130
1,2-Dichloropropane
ug/L
50
48.8
98
70-130
1,4-Dichlorobenzene
ug/L
50
49.0
98
70-130
2-Butanone (MEK)
ug/L
100
88.5
89
70-133
2-Hexanone
ug/L
100
91.1
91
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
92.3
92
70-130
Acetone
ug/L
100
92.7
93
70-144
Acrylonitrile
ug/L
250
261
104
70-130
Benzene
ug/L
50
47.8
96
70-130
Bromochloromethane
ug/L
50
49.8
100
70-130
Bromodichloromethane
ug/L
50
50.5
101
70-130
Bromoform
ug/L
50
52.9
106
70-131
Bromomethane
ug/L
50
73.5
147
30-177lH,v1
Carbon disulfide
ug/L
50
49.2
98
70-133
Carbon tetrachloride
ug/L
50
50.1
100
70-130
Chlorobenzene
ug/L
50
48.5
97
70-130
Chloroethane
ug/L
50
48.1
96
46-131 IK
Chloroform
ug/L
50
48.2
96
70-130
Chloromethane
ug/L
50
57.5
115
49-130
cis-1,2-Dichloroethene
ug/L
50
51.1
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 102

Pace Analytical Services, LLC
ceAnalytical padi yAie. Suite100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
LABORATORY CONTROL SAMPLE:
Parameter
3531119
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,3-Dichloropropene
ug/L
50
51.0
102
70-130
Dibromochloromethane
ug/L
50
49.3
99
70-130
Dibromomethane
ug/L
50
47.5
95
70-130
Ethylbenzene
ug/L
50
48.5
97
70-130
lodomethane
ug/L
100
118
118
47-140 v1
Methylene Chloride
ug/L
50
47.5
95
68-130
Styrene
ug/L
50
51.3
103
70-130
Tetrachloroethene
ug/L
50
48.8
98
70-130
Toluene
ug/L
50
48.1
96
70-130
trans-1,2-Dichloroethene
ug/L
50
49.7
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
50.6
101
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
66.6
133
25-200 v1
Trichloroethene
ug/L
50
47.8
96
70-130
Trichlorofluoromethane
ug/L
50
44.7
89
61-130
Vinyl acetate
ug/L
100
104
104
70-140
Vinyl chloride
ug/L
50
55.7
111
59-142
Xylene (Total)
ug/L
150
146
97
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3531120
MS
92584910024 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3531121
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
18.7
15.2
94
76
70-135
21
30
1,1,1-Trichloroethane
ug/L
ND
20
20
15.7
13.0
78
65
70-148
18
30 M1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.4
15.7
97
78
70-131
21
30
1,1,2-Trichloroethane
ug/L
ND
20
20
16.9
13.7
84
68
70-136
21
30 M1
1,1-Dichloroethane
ug/L
0.77J
20
20
16.6
13.9
79
66
70-147
17
30 M1
1,1-Dichloroethene
ug/L
ND
20
20
17.0
14.1
85
71
70-158
18
30
1,2,3-Trichloropropane
ug/L
ND
20
20
19.9
16.7
100
83
67-137
18
30
1,2-Dibromo-3-
ug/L
ND
20
20
20.6
17.3
103
87
69-136
17
30 v1
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
19.7
15.9
98
80
70-137
21
30
1,2-Dichlorobenzene
ug/L
ND
20
20
20.8
17.6
104
88
70-133
16
30
1,2-Dichloroethane
ug/L
ND
20
20
15.0
12.3
75
61
67-138
20
30 M1
1,2-Dichloropropane
ug/L
ND
20
20
17.0
14.9
85
74
70-138
13
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.6
18.3
108
91
70-133
17
30
2-Butanone (MEK)
ug/L
ND
40
40
30.1
24.8
75
62
61-147
19
30
2-Hexanone
ug/L
ND
40
40
38.5
31.3
96
78
67-139
21
30
4-Methyl-2-pentanone
ug/L
ND
40
40
32.3
27.1
81
68
67-136
18
30
(MIBK)
Acetone ug/L
ND 40 40 30.3 26.4 76 66 55-159
14 30
Acrylonitrile ug/L
ND 100 100 76.0 62.7 76 63 68-140
19 30 M1
Benzene ug/L
0.74J 20 20 17.6 15.0 84 71 67-150
16 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM
without the written consent of Pace Analytical Services, LLC.
Page 84 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"ifyoe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3531120
MS
92584910024 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3531121
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Bromochloromethane
ug/L
ND
20
20
16.3
13.5
82
68
70-146
19
30 M1
Bromodichloromethane
ug/L
ND
20
20
17.1
13.9
86
69
70-138
21
30 M1
Bromoform
ug/L
ND
20
20
18.8
15.5
94
77
57-138
19
30
Bromomethane
ug/L
ND
20
20
16.9
13.8
85
69
10-200
21
30
Carbon disulfide
ug/L
ND
20
20
15.9
13.3
80
67
70-152
18
30 M1
Carbon tetrachloride
ug/L
ND
20
20
18.0
16.0
90
80
70-147
12
30
Chlorobenzene
ug/L
ND
20
20
19.8
16.8
99
84
70-137
17
30
Chloroethane
ug/L
ND
20
20
17.8
14.7
89
73
51-166
19
30
Chloroform
ug/L
ND
20
20
14.3
12.5
72
62
70-144
14
30 M1
Chloromethane
ug/L
ND
20
20
14.8
12.5
74
62
24-161
17
30
cis-1,2-Dichloroethene
ug/L
4.0
20
20
18.4
15.7
72
58
67-148
16
30 M1
cis-1,3-Dichloropropene
ug/L
ND
20
20
17.0
13.6
85
68
70-142
22
30 M1
Dibromochloromethane
ug/L
ND
20
20
20.0
15.9
100
79
68-138
23
30
Dibromomethane
ug/L
ND
20
20
17.3
14.6
87
73
70-134
17
30
Ethylbenzene
ug/L
ND
20
20
20.2
16.8
101
84
68-143
18
30
lodomethane
ug/L
ND
40
40
30.4
24.4
76
61
20-161
22
30
Methylene Chloride
ug/L
12.4
20
20
23.3
20.4
54
40
64-148
13
30 M1,v3
Styrene
ug/L
ND
20
20
20.2
16.7
101
84
70-136
19
30
Tetrachloroethene
ug/L
0.48J
20
20
21.0
17.3
102
84
70-139
19
30
Toluene
ug/L
ND
20
20
16.7
14.0
83
70
47-157
18
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
15.2
13.4
76
67
70-149
13
30 M1
trans-1,3-Dichloropropene
ug/L
ND
20
20
17.1
13.7
85
69
70-138
22
30 M1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.4
15.6
92
78
31-145
16
30 v1
Trichloroethene
ug/L
1.4
20
20
19.7
16.1
91
73
70-149
20
30
Trichlorofluoromethane
ug/L
ND
20
20
15.4
12.9
76
63
61-154
18
30 v3
Vinyl acetate
ug/L
ND
40
40
31.5
26.5
79
66
48-156
17
30
Vinyl chloride
ug/L
ND
20
20
16.1
13.4
81
67
55-172
18
30
Xylene (Total)
ug/L
75.1
60
60
138
125
105
83
66-145
10
30
1,2-Dichloroethane-d4 (S)
%
86
88
70-130
4-Bromofluorobenzene (S)
%
99
96
70-130
Toluene-d8 (S)
%
94
95
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 85 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"MrWy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674949 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910025, 92584910027, 92584910028
METHOD BLANK: 3532809 Matrix:
Associated Lab Samples: 92584910025, 92584910027, 92584910028
Blank
Parameter Units Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
01/31/22 12:57
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
01/31/22 12:57
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
01/31/22 12:57
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
01/31/22 12:57
1,1-Dichloroethane
ug/L
ND
1.0
0.37
01/31/22 12:57
1,1-Dichloroethene
ug/L
ND
1.0
0.35
01/31/22 12:57
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
01/31/22 12:57
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
01/31/22 12:57
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
01/31/22 12:57
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
01/31/22 12:57
1,2-Dichloroethane
ug/L
ND
1.0
0.32
01/31/22 12:57
1,2-Dichloropropane
ug/L
ND
1.0
0.36
01/31/22 12:57
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
01/31/22 12:57
2-Butanone (MEK)
ug/L
ND
5.0
4.0
01/31/22 12:57
2-Hexanone
ug/L
ND
5.0
0.48
01/31/22 12:57
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
01/31/22 12:57
Acetone
ug/L
ND
25.0
5.1
01/31/22 12:57
Acrylonitrile
ug/L
ND
10.0
1.8
01/31/22 12:57
Benzene
ug/L
ND
1.0
0.34
01/31/22 12:57
Bromochloromethane
ug/L
ND
1.0
0.47
01/31/22 12:57
Bromodichloromethane
ug/L
ND
1.0
0.31
01/31/22 12:57
Bromoform
ug/L
ND
1.0
0.34
01/31/22 12:57
Bromomethane
ug/L
ND
2.0
1.7
01/31/22 12:57
Carbon disulfide
ug/L
ND
2.0
0.73
01/31/22 12:57
Carbon tetrachloride
ug/L
ND
1.0
0.33
01/31/22 12:57
Chlorobenzene
ug/L
ND
1.0
0.28
01/31/22 12:57
Chloroethane
ug/L
ND
1.0
0.65
01/31/22 12:57
Chloroform
ug/L
ND
1.0
0.43
01/31/22 12:57
Chloromethane
ug/L
ND
1.0
0.54
01/31/22 12:57
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
01/31/22 12:57
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/31/22 12:57
Dibromochloromethane
ug/L
ND
1.0
0.36
01/31/22 12:57
Dibromomethane
ug/L
ND
1.0
0.39
01/31/22 12:57
Ethylbenzene
ug/L
ND
1.0
0.30
01/31/22 12:57
lodomethane
ug/L
ND
20.0
9.7
01/31/22 12:57
Methylene Chloride
ug/L
ND
5.0
2.0
01/31/22 12:57
Styrene
ug/L
ND
1.0
0.29
01/31/22 12:57
Tetrachloroethene
ug/L
ND
1.0
0.29
01/31/22 12:57
Toluene
ug/L
ND
1.0
0.48
01/31/22 12:57
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
01/31/22 12:57
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"lirpygfe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
METHOD BLANK: 3532809 Matrix:
Associated Lab Samples: 92584910025, 92584910027, 92584910028
Blank
Parameter Units Result
Water
Reporting
Limit
MDL
Analyzed
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
01/31/22 12:57
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
01/31/22 12:57
Trichloroethene
ug/L
ND
1.0
0.38
01/31/22 12:57
Trichlorofluoromethane
ug/L
ND
1.0
0.30
01/31/22 12:57
Vinyl acetate
ug/L
ND
2.0
1.3
01/31/22 12:57
Vinyl chloride
ug/L
ND
1.0
0.39
01/31/22 12:57
Xylene (Total)
ug/L
ND
1.0
0.34
01/31/22 12:57
1,2-Dichloroethane-d4 (S)
%
96
70-130
01/31/22 12:57
4-Bromofluorobenzene (S)
%
99
70-130
01/31/22 12:57
Toluene-d8(S)
%
98
70-130
01/31/22 12:57
LABORATORY CONTROL SAMPLE:
Parameter
3532810
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.4
103
70-130
1,1,1-Trichloroethane
ug/L
50
44.8
90
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
70-130
1,1,2-Trichloroethane
ug/L
50
47.6
95
70-130
1,1-Dichloroethane
ug/L
50
44.2
88
70-130
1,1-Dichloroethene
ug/L
50
43.6
87
70-132
1,2,3-Trichloropropane
ug/L
50
51.0
102
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.8
104
70-132
1,2-Dibromoethane (EDB)
ug/L
50
49.0
98
70-130
1,2-Dichlorobenzene
ug/L
50
51.4
103
70-130
1,2-Dichloroethane
ug/L
50
44.1
88
70-130
1,2-Dichloropropane
ug/L
50
47.3
95
70-130
1,4-Dichlorobenzene
ug/L
50
52.0
104
70-130
2-Butanone (MEK)
ug/L
100
93.3
93
70-133
2-Hexanone
ug/L
100
88.0
88
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.0
86
70-130
Acetone
ug/L
100
87.2
87
70-144
Acrylonitrile
ug/L
250
238
95
70-130
Benzene
ug/L
50
47.6
95
70-130
Bromochloromethane
ug/L
50
47.0
94
70-130
Bromodichloromethane
ug/L
50
46.7
93
70-130
Bromoform
ug/L
50
51.3
103
70-131
Bromomethane
ug/L
50
50.5
101
30-177
Carbon disulfide
ug/L
50
48.2
96
70-133
Carbon tetrachloride
ug/L
50
48.8
98
70-130
Chlorobenzene
ug/L
50
50.3
101
70-130
Chloroethane
ug/L
50
42.4
85
46-131
Chloroform
ug/L
50
45.1
90
70-130
Chloromethane
ug/L
50
45.5
91
49-130
cis-1,2-Dichloroethene
ug/L
50
45.1
90
70-130
Qualifiers
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 87 of 102

Pace Analytical Services, LLC
ceAnalytical padi yAie. Suite100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
LABORATORY CONTROL SAMPLE:
Parameter
3532810
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,3-Dichloropropene
ug/L
50
48.2
96
70-130
Dibromochloromethane
ug/L
50
47.4
95
70-130
Dibromomethane
ug/L
50
49.5
99
70-130
Ethylbenzene
ug/L
50
48.7
97
70-130
lodomethane
ug/L
100
85.5
85
47-140
Methylene Chloride
ug/L
50
40.5
81
68-130
Styrene
ug/L
50
50.8
102
70-130
Tetrachloroethene
ug/L
50
49.9
100
70-130
Toluene
ug/L
50
47.3
95
70-130
trans-1,2-Dichloroethene
ug/L
50
45.0
90
70-130
trans- 1,3-Dichloropropene
ug/L
50
48.2
96
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
69.6
139
25-200 v1
Trichloroethene
ug/L
50
49.0
98
70-130
Trichlorofluoromethane
ug/L
50
43.3
87
61-130
Vinyl acetate
ug/L
100
97.1
97
70-140
Vinyl chloride
ug/L
50
50.6
101
59-142
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3532811
MS
92584635002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3532812
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
1000
1000
1070
1060
107
106
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
1000
1000
951
927
95
93
70-148
3
30
1,1,2,2-Tetrachloroethane
ug/L
ND
1000
1000
1000
1030
100
103
70-131
2
30
1,1,2-Trichloroethane
ug/L
ND
1000
1000
958
958
96
96
70-136
0
30
1,1-Dichloroethane
ug/L
ND
1000
1000
905
888
90
89
70-147
2
30
1,1-Dichloroethene
ug/L
ND
1000
1000
902
878
90
88
70-158
3
30
1,2,3-Trichloropropane
ug/L
ND
1000
1000
1060
1070
106
107
67-137
1
30
1,2-Dibromo-3-
ug/L
ND
1000
1000
971
1050
97
105
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
1000
1000
991
998
99
100
70-137
1
30
1,2-Dichlorobenzene
ug/L
ND
1000
1000
1050
1060
105
106
70-133
2
30
1,2-Dichloroethane
ug/L
ND
1000
1000
904
909
90
91
67-138
1
30
1,2-Dichloropropane
ug/L
ND
1000
1000
954
951
95
95
70-138
0
30
1,4-Dichlorobenzene
ug/L
ND
1000
1000
1070
1080
107
108
70-133
1
30
2-Butanone (MEK)
ug/L
ND
2000
2000
1810
1880
86
89
61-147
3
30
2-Hexanone
ug/L
ND
2000
2000
1770
1870
89
93
67-139
5
30
4-Methyl-2-pentanone
ug/L
ND
2000
2000
1690
1760
85
88
67-136
4
30
(MIBK)
Acetone ug/L
ND 2000 2000 1600 1460 80 73 55-159
9 30
Acrylonitrile ug/L
ND 5000 5000 5120 5140 102 103 68-140
0 30
Benzene ug/L
5750 1000 1000 6650 6390 90 63 67-150
4 30 M1
Results presented on this page are
in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM
without the written consent of Pace Analytical Services, LLC.
Page 88 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg"Wfy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3532811
MS
92584635002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3532812
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Bromochloromethane
ug/L
ND
1000
1000
943
916
94
92
70-146
3
30
Bromodichloromethane
ug/L
ND
1000
1000
944
931
94
93
70-138
1
30
Bromoform
ug/L
ND
1000
1000
979
964
98
96
57-138
2
30
Bromomethane
ug/L
ND
1000
1000
957
918
96
92
10-200
4
30
Carbon disulfide
ug/L
ND
1000
1000
938
913
94
91
70-152
3
30
Carbon tetrachloride
ug/L
ND
1000
1000
1050
1020
105
102
70-147
3
30
Chlorobenzene
ug/L
ND
1000
1000
1060
1060
106
106
70-137
0
30
Chloroethane
ug/L
ND
1000
1000
1050
986
105
99
51-166
6
30
Chloroform
ug/L
ND
1000
1000
916
909
91
90
70-144
1
30
Chloromethane
ug/L
ND
1000
1000
892
875
89
87
24-161
2
30
cis-1,2-Dichloroethene
ug/L
ND
1000
1000
919
898
92
90
67-148
2
30
cis-1,3-Dichloropropene
ug/L
ND
1000
1000
957
957
96
96
70-142
0
30
Dibromochloromethane
ug/L
ND
1000
1000
951
937
95
94
68-138
1
30
Dibromomethane
ug/L
ND
1000
1000
1000
984
100
98
70-134
2
30
Ethylbenzene
ug/L
3030
1000
1000
4090
3920
107
90
68-143
4
30
lodomethane
ug/L
ND
2000
2000
1160
1480
58
74
20-161
24
30
Methylene Chloride
ug/L
ND
1000
1000
844
824
84
82
64-148
3
30
Styrene
ug/L
ND
1000
1000
1110
1110
111
111
70-136
0
30
Tetrachloroethene
ug/L
ND
1000
1000
1060
1080
106
108
70-139
1
30
Toluene
ug/L
1880
1000
1000
2810
2730
93
85
47-157
3
30
trans-1,2-Dichloroethene
ug/L
ND
1000
1000
923
902
92
90
70-149
2
30
trans-1,3-Dichloropropene
ug/L
ND
1000
1000
937
923
94
92
70-138
1
30
trans-1,4-Dichloro-2-butene
ug/L
ND
1000
1000
1120
1140
112
114
31-145
1
30 v1
Trichloroethene
ug/L
ND
1000
1000
1030
1010
103
101
70-149
2
30
Trichlorofluoromethane
ug/L
ND
1000
1000
940
906
94
91
61-154
4
30
Vinyl acetate
ug/L
ND
2000
2000
1770
1780
88
89
48-156
1
30
Vinyl chloride
ug/L
ND
1000
1000
964
945
96
94
55-172
2
30
Xylene (Total)
ug/L
10500
3000
3000
13500
13000
98
83
66-145
3
30
1,2-Dichloroethane-d4 (S)
%
98
98
70-130
4-Bromofluorobenzene (S)
%
96
96
70-130
Toluene-d8 (S)
%
97
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 89 of 102

leAnalytical
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Pace Analytical Services, LLC
Pa88Qtir6fy0e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674403 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910001, 92584910002, 92584910003, 92584910004, 92584910005, 92584910022, 92584910023,
92584910025,92584910026,92584910027,92584910028
METHOD BLANK: 3530129 Matrix: Water
Associated Lab Samples: 92584910001, 92584910002, 92584910003, 92584910004, 92584910005, 92584910022, 92584910023,
92584910025,92584910026,92584910027,92584910028
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 01/27/22 18:08
1,2-Dichloroethane-d4 (S) % 96 70-130 01/27/22 18:08
Toluene-d8 (S) % 96 66-133 01/27/22 18:08
LABORATORY CONTROL SAMPLE: 3530130
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 20.1 100 70-130
1,2-Dichloroethane-d4 (S) % 90 70-130
Toluene-d8 (S) % 95 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530131 3530132
Parameter
1,4-Dioxane (p-Dioxane)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
MS
92584759001 Spike
Units Result Conc.
ug/L 33.2 20
MSD
Spike MS MSD MS
MSD
% Rec
Max
Conc. Result Result % Rec
% Rec
Limits
RPD RPD Qual
20 49.1 49.5 79
81
64-141
1 30
91
93
70-130
30
94
94
66-133
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 90 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padg rWy0e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674404 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910006,92584910007,92584910008,92584910009,92584910010,92584910011,92584910012,
92584910013,92584910014,92584910015,92584910016,92584910017,92584910018
METHOD BLANK: 3530133 Matrix: Water
Associated Lab Samples: 92584910006,92584910007,92584910008,92584910009,92584910010,92584910011,92584910012,
92584910013,92584910014,92584910015,92584910016,92584910017,92584910018
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 01/27/22 18:27
1,2-Dichloroethane-d4 (S) % 92 70-130 01/27/22 18:27
Toluene-d8 (S) % 95 66-133 01/27/22 18:27
LABORATORY CONTROL SAMPLE: 3530134
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 70-130
1,2-Dichloroethane-d4 (S) % 91 70-130
Toluene-d8 (S) % 95 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530135 3530136
Parameter
1,4-Dioxane (p-Dioxane)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
MS
92584910006 Spike
Units Result Conc.
ug/L ND 20
MSD
Spike MS MSD MS
MSD
% Rec
Max
Conc. Result Result % Rec
% Rec
Limits
RPD RPD Qual
20 19.2 19.5 96
97
64-141
2 30
93
93
70-130
30
94
94
66-133
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 91 of 102

leAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
Padgwrwy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J22010014 MNS LF
Pace Project No.: 92584910
QC Batch: 674405 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92584910019, 92584910020, 92584910021, 92584910024, 92584910029
METHOD BLANK: 3530137
Matrix:
Water
Associated Lab Samples:
92584910019, 92584910020, 92584910021, 92584910024, 92584910029
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0 0.86
01/28/22 06:20
1,2-Dichloroethane-d4 (S)
%
87
70-130
01/28/22 06:20
Toluene-d8 (S)
%
92
66-133
01/28/22 06:20
LABORATORY CONTROL SAMPLE: 3530138
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 18.7 93 70-130
1,2-Dichloroethane-d4 (S) % 90 70-130
Toluene-d8 (S) % 93 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3530139
3530140
MS
MSD
92584910019 Spike
Spike MS MSD
MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result Result
% Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.0 19.8
100
99
64-141
1 30
1,2-Dichloroethane-d4 (S)
%
92
92
70-130
30
Toluene-d8 (S)
%
93
93
66-133
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC.
Page 92 of 102

Pace Analytical Services, LLC
ceAnalytical padi yAie. Suite100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: J22010014 MNS LF
Pace Project No.: 92584910
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
CO Result confirmed by second analysis.
C7 Analyte is a possible laboratory contaminant (not present in method blank).
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/02/2022 04:59 PM without the written consent of Pace Analytical Services, LLC. Page 93 of 102

aC`eAnalytical fl
www.pacelabs.com
Pace Analytical Services, LLC
Pa890ir6Py&e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Lab ID
Sample ID
QC Batch Method
QC Batch
92584910001
MW-1
EPA 8260D
674609
92584910002
MW-1D
EPA 8260D
674641
92584910003
MW-2A
EPA 8260D
674641
92584910004
MW-2D
EPA 8260D
674641
92584910005
MW-3
EPA 8260D
674641
92584910006
MW-3D
EPA 8260D
674641
92584910007
MW-4
EPA 8260D
674641
92584910008
MW-4D
EPA 8260D
674641
92584910009
MW-11
EPA 8260D
674641
92584910010
MW-11D
EPA 8260D
674641
92584910011
MW-12
EPA 8260D
674641
92584910012
MW-12D
EPA 8260D
674641
92584910013
SW-1
EPA 8260D
674641
92584910014
MW-4R
EPA 8260D
674641
92584910015
MW-4DR
EPA 8260D
674641
92584910016
MW-3BR
EPA 8260D
674641
92584910017
MW-4BR
EPA 8260D
674641
92584910018
MW-4BRR
EPA 8260D
674641
92584910019
MW-11 BR
EPA 8260D
674641
92584910020
MW-13D
EPA 8260D
674641
92584910021
MW-13BR
EPA 8260D
674641
92584910022
M NS_TB-20220126-0800
EPA 8260D
674643
92584910023
M NS_FB-20220126-1100
EPA 8260D
674643
92584910024
MNS FD-20220126-1
EPA 8260D
674643
92584910025
MNS TB-20220124-0930
EPA 8260D
674949
92584910026
MNS FB-20220126-1145
EPA 8260D
674643
92584910027
M NS_FB-20220124-1600
EPA 8260D
674949
92584910028
MNS FB-20220125-1230
EPA 8260D
674949
92584910029
MNS FD-20220125-1
EPA 8260D
674643
92584910001
MW-1
EPA 8260D Mod.
674403
92584910002
MW-1 D
EPA 8260D Mod.
674403
92584910003
MW-2A
EPA 8260D Mod.
674403
92584910004
MW-2D
EPA 8260D Mod.
674403
92584910005
MW-3
EPA 8260D Mod.
674403
92584910006
MW-31)
EPA 8260D Mod.
674404
92584910007
MW-4
EPA 8260D Mod.
674404
92584910008
MW-41)
EPA 8260D Mod.
674404
92584910009
MW-11
EPA 8260D Mod.
674404
92584910010
MW-11 D
EPA 8260D Mod.
674404
92584910011
MW-12
EPA 8260D Mod.
674404
92584910012
MW-12D
EPA 8260D Mod.
674404
92584910013
SW-1
EPA 8260D Mod.
674404
92584910014
MW-4R
EPA 8260D Mod.
674404
92584910015
MW-4DR
EPA 8260D Mod.
674404
92584910016
MW-3BR
EPA 8260D Mod.
674404
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 02/02/2022 04:59
PM
without the written consent of Pace Analytical Services, LLC.
Analytical
Analytical Method Batch
Page 94 of 102

leAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
PaWmrwy ie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J22010014 MNS LF
Pace Project No.: 92584910
Lab ID Sample ID QC Batch Method QC Batch
92584910017
MW-4BR
EPA 8260D
Mod.
674404
92584910018
MW-4BRR
EPA 8260D
Mod.
674404
92584910019
MW-11BR
EPA 8260D
Mod.
674405
92584910020
MW-13D
EPA 8260D
Mod.
674405
92584910021
MW-13BR
EPA 8260D
Mod.
674405
92584910022
MNS_TB-20220126-0800
EPA 8260D
Mod.
674403
92584910023
MNS FB-20220126-1100
EPA 8260D
Mod.
674403
92584910024
MNS FD-20220126-1
EPA 8260D
Mod.
674405
92584910025
MNS_TB-20220124-0930
EPA 8260D
Mod.
674403
92584910026
MNS_FB-20220126-1145
EPA 8260D
Mod.
674403
92584910027
MNS_FB-20220124-1600
EPA 8260D
Mod.
674403
92584910028
MINIS FB-20220125-1230
EPA 8260D
Mod.
674403
92584910029 MNS FD-20220125-1 EPA 8260D Mod. 674405
Date: 02/02/2022 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 95 of 102

Document Name:
Document Revised: November 11P.W94
aceAnalXiCal n
Sample Condition Upon Receipt JSCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.08
Pace Carolinas Quality Office
of 151
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersviiie % Raleigh❑ Mechanicsville(] Atlanta❑ Kernersville❑
conditionClient Name:Upon Receipt Project #:Wp# : 92584910
P b, �--- e , -1
Courier: ❑Fed Ex ❑UPS ❑U5P5 ❑Client
❑ Commercial ❑Pace ❑Other:
92'384510
Custody Seal Present? Oyes ❑No Seals Intact? ❑Yes 060 S
Date/initials Person Examining Contents:
Packing Material: ❑Bubble Wrap []Bubble Bags [DNone ❑ ' Other Biological Tissue Frozen?
❑Yes ❑No ❑id/A
Thermometer: [20et ❑Blue []None
[31111 Gun ID; 7�. i Type of Ice:
1� Correction Factor:
Cooler Temp: i }— L �dd/Subtract (°C) , Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples an ice, cooling process
CaalerFempforrected 4'H• ` r _ gv
USDA Regulated Solt (❑ N/A, water. sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally,
r1ai.. inrhniinoWnwaii and Puprtn Rim)? nYpt 171Nn
Comments/loiscrepan cy:
Chain of Custody Present?
❑Yes
[]NO
[]N/A
1.
Samples Arrived within Hold Time?
C: es
[]No
❑NJA
2.
Short Hold Time Analysis (<72 hr.)?
QYes
[]6o
EINJA
3.
Rush Turn Around Time Requested?
[]Yes
`
i]No
❑NJA
4.
sufficient Volume?
❑Yes
❑No
N/A
S.
Correct Containers Used?
-Pace Containers Used?
©j�
❑Yes
❑No
[]No
❑NJA
❑N/A
6.
Containers Intact?
Dies
[No
N/A
7.
Dissolved analysis: Samples Field Filtered?
Elyes
❑Na
- NIA
S.
Sample labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
ayes
❑No
❑NIA
4.
Headspace in VOA Vials >5•6mm)?
[-]Yes
❑No
❑N/A
10.
Trip Blank Present?.
Trip Blank Custody Seals Present?
❑Yes
byes
❑N6
❑No
❑NJA
❑NjA
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted: -
Project Manager SCURF Review:
Date/Time:
Lot ID of split containers:
Date:
Project Manager SRF Review: Date:
Field Data Required? ❑Yes ❑No
Page 96 of 102

Document Name: Document Revised: November IpEan1141
Sample Condition Upon Receipt (SCUR) Page 2 of 21�20Analytical- - ' Document No.: issuing Authority,
F-CAR-CS-033-Rev.08 Pace Carolinas Quality r7ff;—
". 0- A f f % +1 IA
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
51
7
Project# WOR : UZ00%V i W
PM: NMC Due Date: 02/03/22
CLIENT: 92-Dupe Ener
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Sample ID
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Lot d
Note: Whenever there is a discrepancy affecting North Carolina compliance Samples, a copy of this form will be sent to the North Carolina aEHNR Certification Office ii.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 97 of 102

Document Name:
Document Revised: November'lVfOyl,
aG8AflaljllGr l
sample Condition Upon Recelpt (SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR•CS-033-Rev.08
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DSO/Bois (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project i# WO# : 92584910
PM: NMG Due Date: 02/03/22
CLIENT: 92-Duke Ener
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Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 98 of 102

Document Name:
Document Revised: November 1 021
�ceAnalXidal' � -
Sample Condition Upon Recelpt ISCURI
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR•C5-033•Rev.08
pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 lwaterj DOC, LLHg
"Bottom half of box is to list number of bottles
Project t4 FWO#
NM MG
CLIENT:
'92584910
Due Date: 02/03/22
92-Duke Ever
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Notes Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of thls form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 99 of 102

Duke Energy Analytical Laboratory
,4-., DUKE Mae rcosaz iawwim7M6!
"'C' ENERGY
_ --------- - - ------------ -
'Project
trial 87s4w
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............ .L. -1-?----.......
Name MNS LANDFILL #1 Permit #60-04 PRan. No:
Client Ethan Smith f Bryan Moeller!
Courtney Murphy
Operating Unit: 20036 Process: BLDFLGN Account:
Proj.et: Activity to: Facility IM
MGAO
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Sample Description or ID
SAMPLE ID
i NUMBER i
202200005411 MNS_MW-1
2022000055 ; MNS_MW-1D
2022000056 MNS_Mw-2A
2022000057 MNS_MW-2D
i 2022000058 f MNS_MW-3
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2022000060 MNS_MW4
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! 2022000064 ! MNS_MW-12
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i 2022000065 MNS_MW-12D
i 2022000066 i MNS_SW-1
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Relinquished By — , / DatelTime
w
CHAIN_ OF CUSTODY RECORD AND REQUEST FORM
_._._._._._._._._.._._._._._._._-
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a,.awwrQK.a
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SAMPLE PROGRAM
44 6
Ground Water
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8
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DISTRIBUTION a
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! rat t tir Duke Energy Analytical laboratory ! i-----------------•-----------------------------------•-•------ ----Analv--- Laboratory Use Only
Page 145 of 151
fimwb� L/Vr\C 10.11God.MG03M (BWMln97405) i !OrderNJ22010014
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._._._._._._._._..,._._._._._._._._ _._._._._._, Fex: L7w)ps.l.xi-_._._._._.J I
Prgiect Name MNS LANDFILL #1 Permit NSO-04 P"Ov� NO= V.rdvr: Pave
Client Ethan Smith IBryan Moeller ;RDR
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CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM Page 146 of 151
Duke Energy Analytica] Laboratory ! i Analytical LaboratoryUse Onlys-
'�� DUKE u.acm.uG 1110MIN7fe6) Matrix WATER NC_ Page_2—of 3_ o
i iOrdertlJ22010014
1333V Hn— F. Rd s.mrl.. dh4i.p•e F— i —
ENERGY ' i 5C i DISTRIBUTION N
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pwi srsszu i i_ �7_ _ / SAMPLE PROGRAM I
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Project Name MNS LANDFILL 41 Permit 460-04 P^O N- weeder: Pao. Drinking Water � UST
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CElant Ethan Smith !Bryan Moeller I �Po a - -� -- -•-- �-• -•-•---�-----�---�-�---._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._
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5
2022000080
MNS_TB
[/?x ZZ
%
3
3
NIA
6
2022000081
MNS_FB-.r [ 0[2(v-
1145
(GNND22gIa�W4
%
3
1
3
1
NIA
8
! 2022000082 !.
MNS-FB_262Z6ia4-- IWO
f 24 �
�
� �
%
3
1
3
1
NIA
8
! 2022000063 !
i�
MNS_FBa Zlj Oi 5 _ 1a36
x
3
1
3
1
NIA
8
i 2022000094 i
�i
MNS_FD-z:yaxjL2 I
�c
--
X
3
1
3
1
NIA
e
0
1
i
0
i
D
0
i -
0
i i
0
i e
0
! 1
0
I i
0
0
rT t
0
1 1
D
TOTALS CONTAINERS
18
4 0
1 18
0
1 4
0
0
1 0
0
0
0
0
44
Relinquished By pus "DetelTime
Acce tad y: Date)Time
cl
Requested Turnaround
TotaE
Rol inquia By DatefTims
ccepted By. DataMme
- .Z7
/'
r� , U
m V
u �
21 Days
14 Days I �'
nq DatefTlmo
Accepted By: DatafTlme
b;
n
SeaOLo d BY /DatafTime
SeaiedlLock Opened By DalefTlme
C-
'7 Days
Ea
Comments �� �4Liy� ('oyjt%IL(� (-Iff� !
Q'i'L /�/�Z
a
'Other
'Add Cost Will Apply
t)

Duke Energy AmIyGca3 Wmratcry i
,Ifts DUE
ENERGY.
MAP Gods MG03A2 (MIEM 74"] j
57�e Hrer . r . ,210
Xwhnvll4. N. L. 2rar0 j
MM 176-124 I
'Project
Name---~-MNS LANDFILL 41 Permit #60-04 Fh—Ha.
Client Ethan Smith 1 Bryan Moeller 1
Courtney Murphy
OperaHng Unk: 70g36 Process: BLDFLON Account_
Project: Ac" ID: Facility 10!
yCon
Program I E4ui8 Teak Cade: Su"rograWask Code:
_ Sample Description or ID
SAMPLE ID _.. i
j NUMBER
2022000054 ; IMNS_MW-1
202MOOSS
MNS_MW-lD
•. 2022000056 '
MNS_MW-2A
! I
2022000067
MNS_MW-2D
2022000068 !
MNS MW-3
j 202200005E j
MNS_MW-3D
2022I p
2022000061 =
MNS_MVV 4
MNS MW-4D
'' 202�
MNS_MW-11
! 2022000063 !
MIN S MW-11D
? 2022000064 !
MNS_MW-12
ih
{ 2022000065
MNS_MW-12D
i 2022000066
MNS_SW-1
E 2022000067
MNs MW-4R
2022000068
MNS MW-4DR
l I
i—�
�-J
us mer w sE n a date ee o
Relinquished By L, Dateffime
Rennquis By DetaMrne
Relinquished By DaeelTlme
Sa&AAcked By Determine
Comments
CHAIN OF CUSTODY RECORD AND A_NAL_Y_SIS_ REQUEST FORM
----
_—...._...._._._._............
._.__._....---------------._._._._._._.
I - Il-ah
IOrdereJ2267OQ14
,
Alatrlx WATER—
eriow aNgn�re rran
�
Lvygsd ay
TLn
Dog e t
SAMPLE
M� PROGRMM1
.Vender: Pees
/+1'�
�f'
Grcund
0nnkinq Water_
g
UST_
RCRA Waste,._.._..__.�.._..�._
i�
Pace
Pete
I Filtration 10.45 umj
8
Unfiltered
I
Preservative
NCI- ICE
HH05
IICL, ICE
ICE
ICE
I- PO # 9172712 _ _
I Container Volume ImLj
40
600
40
wo
Soo
Contain rType
T � y
OC
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.a r
a J
ui
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s 2 i i
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a m
n
_[
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Collection Information
ems
o$•
adfva
d Y �. d
14
m LO. a
d
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-iU
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_
CI
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D&W Time
Printed Name
5 nature �3 o
S 249
f �—_' r."a C$ o
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-a ii
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Page 147 of 151
Page -1_ of
DISTRIBLMN
ORIGINAL to LAB, COPY to CLIENT
� Filtered
1
-ro-rAL / CONTAINERS
45
1 15 1 6
1 45
I 11
4
0
0
1 D
1 0
I U
1
121
AcLe y= DatmMme
m
Requested Tumaround
Tots? 727
L
E
Aceep d jr- Datemnut
< 7
C
Q -a
c
21 Days
AcWpGad By: v DstelTurre
E
14 Days
W ..
C a
SealsdiLock Opened By Oatamine
a
E 'w
7 Days
c
'Other
0
Add. Cast Will Apply
U

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM _ � __ __ _ _ __ _ _ _ _ _ _ _ _ _ p— ,dR of 1 R1
❑uka Energy Arulytical Laboratory i i
Analytical LaboratoryUlm Gnl
NC_
r
• —� _ .. _ _. . _ .
Pago_3 of 3_
wr����� MeaCe ma=RlierismgT4tal iOrtlarltJ22010014
Htl" a• G Lar'
ENERGY ""�"'°'"` �'
Maud WATER
vrp.
s�
;
I]o LAR. UTION
LAB, COPY to CLIENT
ORIGINAL COPY
Pula r�a.r
Pula
Yy
Ostt a Time
r r
ga,ppLE PRpppo,M
!
to
io±!!>��al.
Prajact NAM M N S LANDFILL #1 Permit #60-04 Brea. 9w Va der:
pros
/�+
f
Ground Water _X�
Dr nkiog WaterUST
RCRA waste
.._.._..__._..__.__._.. _.. _.._.._.. _.._..
NPOES
_.._.._.._.._..__._.___
Client Ethan Smith f Bryan Moeller f !PD
Pace
Filtration [0.45 um)
8
Unfiltered
Fl
8 lEered
Courtn Murp i
r
Opsrstirrq UnR: 2003E Process: BLOFLGN Aavourrt: `_
�� 171712
i Preservative
HCL, ICE
NN03
HCL, Mr.
ICE
ICE
_
Projed: Aodit0: Facility10:
}� 7 _.._..
_.._.._
Container Vo lu me (ML)
40
00
40
588
50D
Program I EOuIS Task Coda:. Sub-PrdgramlTask Coda:
Container Type
6'N
a
a c�v
a
w
7CU
W
Cusromer ro camplere all approprisra non-shadad
areas m
—
n r77
w
i —TV` m
K rp o, m
r
y, y
x
o
s
Sam pie Description Or IO
v••
1
Collak0jan WronnaUon
b m L¢
L
R
a m w
�
=1
SAMPLE I]
NUMBER
Printed Name
0
�
a vQ❑
Uirma
j 20200069i
MNSMW-38R
_
i
Y
x
3
1
I
3j1,��
.
2022000070
MNS_MW-48R
io 14
COVNot ?Aare"
� r
x
3
t
3
1
8
E 20230000T '
MNS_MW-4BRR
(
f�'t,
f 7j�j
�()NNC2 fapC�
%
3
1
3
1
0
S
2022000072 `
MNS MVV-11BR
x
3
1
3
1
$
2022000073 !
MNs MW-130
1
yy
14DO
6{ky, t-k
%
3
1
3
1
8
i 2022000074 i
MNS_MW-130R
i'lj2ff7OW
5"tk
%
3
1
3
1
s
i 2022D0 5
MNS Ta.24_
i
OgOO
NLfL
x
S
3
f
8
} 2022000076
MNS_FB-2A;.7eI;,(o OiD
Cu"A Z41-tCOA
%
S
1
3
1
e
2022000077
MNS FB
4/ Z
x
3
1
s
1
e
1 2022000078
MNs_FDw;Z42Z j;10 — 1
x
3
1
3
i
0
e
��
fl
r
g
0
i
0
0
0
TOTAL A CohTAnlEAS
90
8 0
30
8
S
0
O
0
6
e
e
8
7e
ustnmer to sin ante oa low
Relinquished By DatalTi
EMAC411 5m 15 47- !so
Acre
y:
DatelTlme
/ .2 -
Requested Tumaround
21 Days
Total
78
Rdlnqu had By Oatemme
Ostamms qq
c
a o
c
14 Days'_�d'
S
L�
Rolinqulshad By Dalarrime
Accepted By: free
c Y
m
c a
n u
`7 pays
SealfLocked By WtelTime
O-Wdd -k opened By nahtTime
E
-
w
�
"Add.
"del.
Lp}� rah ,/j � � � � 1 [ + � [ G !_
CvmmaMa 0' W L 6 � r rj`'4•�'L�+y� �� �/11� YR H l . �TJ W4f�'
S y Yvi y
Mw - `f�� vx
V - $.-75
1
21
0
C
Cosl Will Apply

CHAIN. OF CUSTODY RECORD AND ANALYSIS REQUEST FORM _ _ _ _ _ _ _ _ _ _ _ _ 13.. Ida of 1 R1
nuke Energy Analytical Laboratory 3 i Amll cal LaboratoryUse O P P —Z— p{ 3
DUKE J22D10Q74 Maki% WATER — —
/r� ❑u KE eaa Cea. kWOlA] Iaulldlna 7►0aY iOMer
0 aw0. &h*W%F—
n123"Mae a-c- sFic. SC— DISTRIBUTION
ENERGY ]]]9XgvsFaryRd J ;
ORIGINAL to LAB, COPY to CLIENT
r
�IJ 0-sus i Logged By pMra rlm.PROGRAM!
_ _ _ 1--------.-- _ _ ......... _ v.::• 794J-"._...._ ..........1 Ground Waler X_ POES _
'Project
Nance M N S LANDFILL #1 Permit OGO.04 Ift— Ha, 1viewar' Pau Drinking Water � UST J
r RCRA Waste
�- T �L51_.._.._
Client Ethan Smith I Bryan Aloellef I iPO a Filtration (0.46 um) 1ti Unfiltered 0 red
Courtney Murphy Pace
aparawg Unit: 20M Praceae: BLDFLON JA unt ! �{9172112r Preservative HCL, ICE HM03 ACL. ICE ICE ICE
-- --•-----------
i -- -._... PO #
Project: AcHvky ID: Faailfly In: Contalner Volume {mL} 46 500 60 600 50D
Program I E4uIS Task Code: Sub43rayramfTask Code: Container Type
�1 SN�44u c
ry
� -t- rc Nit T 1�6 N W Ca
gg p a u C N 1i L]
Customet ro romprore all approprwfr non-shedeR aroas. a W K N e 4 x d H 00 W
Sample Description a ID a 6 ya o o Q x ^ ,I� Q ..
1.5
1 SAMPLE In Collection Information ۥ Cpi 9 ,ice d x r ,$m n J y it 0 a
It
f NUMBER Date Time Printed Name Si nature U v 5 a si - ci $ v +^ y f VJ 6 L1 Q V) U Q. ~
;; 20220�00079
MNS_T8 -,Z02;k0 - jj t ?xj
; .jam
%
3
3
NIA
s
f2022000080
MNS_TS
S LL
x
3
3
NSA
E
2022000001
MNS_Fe—Fe(•I 5
21/
If 45
CM1UCZ?AI-1C"
%
3
1
3
1
WA
e
! 2022000082 !,
MNS FB_2627-61-24—600
(2 Z+LWOO
%
3
1
3
1
NIA
6
i
! 2022000083 1
1VINS_F8►z02,LoF _ 030
-
x
3
1
3
1
NIA
n
i 2022000084 ;
MNS Fa-x�1.Z rJ I
LrJ
--
]i
3
1
3
1
NIA
6
! r
0
! r
0
r
0
0
! !
0
0
0
` ;
0
� I
r i
0
i i
6
v
TOTAL 0 CONTAINERS
19
4 a
18
0
4
D
0
0
0
D
0
0
44
Lv omer to sign a oom ao row
Relinquished By DatefTi a
ADeepted4f. Datomme
Jjn, (
Ut"40I'
-� '
R
b
e
Requested Turnaround
z1 Days
Total 46
Ralktqula d By D&N lTime
IL
oe d By. DelselTlme
__
% ��
al C
a �
n
r -
nq a wtamme
Accepted By: T7atsfTime
.. E
z
p �1
t a Days p
Sep trLna lead By DatefTime
SeNedlLuck Opened By Detarrime
06y5
E 'J
E a
Comments Oo,a inlmY P y( 9
1+'1.��LZ
o
•Other
• Add. Cost Will AWgly
V

Page 150 of 151
McGuire Landfill #1
COMPOUNDS REQUIRED FOR 8260 ANALYSES NC SWSL Std. Required MRL"
* MRL must meet or be
COMPOUND
CASSNo_
below the SWSL Std.
Acetone
67-64-1
100
Acrylonitrile
107-13-1
200
Benzene
71-43-2
1
Bromochloromethane
74-97-5
3
Bromodichloromethane
75-27-4
1
Bromoform; Tribromomethane
75-25-2
3
Carbon disulfide
75-15-0
100
Carbon tetrachloride
56-23-5
1
Chlorobenzene
108-90-7
3
Chloroethane; Ethyl chloride
75-00-3
10
Chloroform; Trich loromethane
67-66-3
5
Dibromochloromethane: Chlorodibromomethane
1 24-48-1
1
1,2-Dibromo-3-chlorpropane; DBCP
96-12-8
1
1,2-Dibromoethane; Ethylene dibromide; EDB
106-93-4
1
o-Dichlorobenzene; 1,2-Dichlorobenzene
95-50-1
5
p-Dichlorobenzene; 1,4-0ichlorobenzene
1 06-46-7
1
trans-1,4-Dich1ero-2-butene
110-57-6
100
1,1-Dichloroethane: Ethylidene chloride
75-34-3
5
1.2-0ich1oroethane: Ethlyene dichloride
1 07-06-2
1
1,1-❑ichlorcethylene; 1-1-❑ichloroethene, Vinylidene chloride
75-35-4
5
cis-1,2-Dichloroethylene; cis-1,2-Dichloroethene
156-59-2
5
trans-1.2-Dichloroethylene: trans-1,2-Dichloroethene
156-60-5
5
1,2-Dichlorpropane: Propylene dichloride
78-87-5
1
cis- 1,3-DichIorpropene
10061-01-
1
trans-1,3-DichIorpropene
10061-02-
1
Ethylbenzene
100-41-4
1
2-hexanone; Methyl butyl ketone
591-78-6
50
Methyl bromide; Sromomethane
74-83-9
10
Methyl chloride. Chloromethane
74-87-3
1
Methylene bromide Dibromomethane
74-95-3
10
Methylene chloride; Dichloromethane
75-09-2
1
Methyl ethyl ketone; MEK; 2-Butanone
78-93-3
100
Methyl iodide: lodomelhane
74-88-4
10
4-Methyl-2-pentanone; Methyl isobutyl isobulyl ketone
1 08-1 0-1
100
Styrene
100-42-5
1
1,1,1.2Jet rachloroethane
630-20-6
5
1,1,2.2-Tetrachlore etharie
79-34-5
1
Tetrachloroethylene, Tetrachotorethen% Perchloroethylene
127-18-4
1
Toluene
108-88-3
1
1,1,1-Trochlore thane; M ethy I ch I o rofo rm
71-55-6
1
1,1,2-Trichlore ethane
7 9-00-5
5
Trichloroethylene; Trichlorethene
79-01-6
1
Trichlorofluoromethene; CFC-11
75-69-4
1

Page 151 of 151
1,2,3-Trichloropropane
96-18-4
1
Vinyl acetate
108-05-4
50
Vinyl chloride
75-01-4
1
xylenes
1330-20-7
4

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559065
Location:
MW-1_ML1 [MNS Landfill 1 / MW-1 (LANDFILL)]
Collection Start:
1/25/2022 13:35:00
Job:
MNSGW20221
Collection End:
1/25/2022 13:35:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta 4.75E+00 4.41 E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<7.68E+00
0.00E+00
7.68E+00
<15
<1000
LLD OK
Co-58
<6.78E+00
0.00E+00
6.78E+00
<15
<1000
LLD OK
Fe-59
<1.29E+01
0.00E+00
1.29E+01
<30
<400
LLD OK
Co-60
<8.18E+00
0.00E+00
8.18E+00
<15
<300
LLD OK
Zn-65
<1.29E+01
0.00E+00
1.29E+01
<30
<300
LLD OK
Zr-95
<1.12E+01
0.00E+00
1.12E+01
<15
<400
LLD OK
Nb-95
<7.30E+00
0.00E+00
7.30E+00
<15
<400
LLD OK
1-131
<7.52E+00
0.00E+00
7.52E+00
<15
LLD OK
Cs-134
<8.17E+00
0.00E+00
8.17E+00
<15
<30
LLD OK
Cs-137
<7.39E+00
0.00E+00
7.39E+00
<18
<50
LLD OK
Bala-140
<6.63E+00
0.00E+00
6.63E+00
<15
<200
LLD OK
Be-7
<5.73E+01
0.00E+00
5.73E+01
K-40
1.53E+02
7.00E+01
8.84E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-2.6E+01
0.00E+00
1.83E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559066
Location: MW-1D_ML1 [ MNS Landfill
1 / MWAD
( LANDFILL) ]
Collection Start: 1/25/2022
14:15:00
Job: MNSGW20221
Collection End: 1/25/2022
14:15:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<7.00E+00
0.00E+00 7.00E+00 <15
<1000 LLD OK
Co-58
<6.82E+00
0.00E+00 6.82E+00 <15
<1000 LLD OK
Fe-59
<1.39E+01
0.00E+00 1.39E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 1 of 12
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 1 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Sample #:
559066
Location: MW-1D_ML1 [MNS Landfill
1 / MW-1D
(LANDFILL)]
Collection Start:
1/25/2022
14:15:00
Job: MNSGW20221
Collection End:
1/25/2022
14:15:00
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Co-60
<6.20E+00
0.00E+00
6.20E+00
<15
<300
LLD OK
Zn-65
<1.21 E+01
0.00E+00
1.21E+01
<30
<300
LLD OK
Zr-95
<1.19E+01
0.00E+00
1.19E+01
<15
<400
LLD OK
Nb-95
<6.32E+00
0.00E+00
6.32E+00
<15
<400
LLD OK
1-131
<7.32E+00
0.00E+00
7.32E+00
<15
LLD OK
Cs-134
<8.04E+00
0.00E+00
8.04E+00
<15
<30
LLD OK
Cs-137
<7.27E+00
0.00E+00
7.27E+00
<18
<50
LLD OK
Bala-140
<8.14E+00
0.00E+00
8.14E+00
<15
<200
LLD OK
Be-7
<5.23E+01
0.00E+00
5.23E+01
K-40
6.20E+01
6.47E+01
1.04E+02
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <3.03E+01 0.00E+00 1.83E+02 <250 <20000 LLD OK
Station: MCGUIRE Sample #: 559067
Location: MW-2A ML1 [ MNS Landfill 1 / MW-2A ( LANDFILL) ] Collection Start: 1/25/2022 11:45:00
Job: MNSGW20221 Collection End: 1/25/2022 11:45:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma
Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Mn-54
<5.84E+00
0.00E+00
5.84E+00
<15
Co-58
<4.83E+00
0.00E+00
4.83E+00
<15
Fe-59
<1.13E+01
0.00E+00
1.13E+01
<30
Co-60
<5.41 E+00
0.00E+00
5.41 E+00
<15
Zn-65
<1.15E+01
0.00E+00
1.15E+01
<30
Zr-95
<7.56E+00
0.00E+00
7.56E+00
<15
Nb-95
<5.49E+00
0.00E+00
5.49E+00
<15
1-131
<6.09E+00
0.00E+00
6.09E+00
<15
Cs-134
<5.69E+00
0.00E+00
5.69E+00
<15
Cs-137
<5.36E+00
0.00E+00
5.36E+00
<18
Bala-140
<5.88E+00
0.00E+00
5.88E+00
<15
Report Generated @ 2/21/2022 15:06:06 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Fraction SLC/ODCM RPT LVL
<1000
LLD OK
<1000
LLD OK
<400
LLD OK
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
EnRad Laboratories Page 2 of 13 02/22/2022
Page 2 of 12

11D Radiological Data for MCGUIRE
Station: MCGUIRE Sample #: 559067
Location: MW-2A ML1 [ MNS Landfill 1 / MW-2A (LANDFILL)] Collection Start: 1/25/2022 11:45:00
Job: MNSGW20221 Collection End: 1/25/2022 11:45:00
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <5.49E+01 0.00E+00 5.49E+01
K-40 1.59E+02 6.99E+01 8.65E+01
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-2.8E+01 0.00E+00 1.83E+02 <250 <20000 LLD OK
Station: MCGUIRE
Sample #: 559068
Location: MW-2D_ML1 [ MNS Landfill
1 / MW-2D
( LANDFILL) ]
Collection
Start: 1/25/2022 12:15:00
Job: MNSGW20221
Collection
End: 1/25/2022 12:15:00
GW Ground Water
ALPHABETA
Gross Alpha / Beta Analysis in Water and Effluent
Filters
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Alpha
<5.30E-01
0.00E+00
5.30E-01
<3
LLD OK
Beta
<3.22E+00
0.00E+00
3.22E+00
<4
LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Mn-54
<4.49E+00
0.00E+00
4.49E+00
<15
<1000 LLD OK
Co-58
<5.19E+00
0.00E+00
5.19E+00
<15
<1000 LLD OK
Fe-59
<1.12E+01
0.00E+00
1.12E+01
<30
<400 LLD OK
Co-60
<6.00E+00
0.00E+00
6.00E+00
<15
<300 LLD OK
Zn-65
<1.18E+01
0.00E+00
1.18E+01
<30
<300 LLD OK
Zr-95
<1.11 E+01
0.00E+00
1.11E+01
<15
<400 LLD OK
Nb-95
<5.65E+00
0.00E+00
5.65E+00
<15
<400 LLD OK
1-131
<5.70E+00
0.00E+00
5.70E+00
<15
LLD OK
Cs-134
<6.55E+00
0.00E+00
6.55E+00
<15
<30 LLD OK
Cs-137
<4.14E+00
0.00E+00
4.14E+00
<18
<50 LLD OK
Bala-140
<4.13E+00
0.00E+00
4.13E+00
<15
<200 LLD OK
Be-7
<3.38E+01
0.00E+00
3.38E+01
K-40
9.51E+01
5.45E+01
7.07E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
H3GW
<-5.9E+01
0.00E+00
1.83E+02
<250
<20000 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 3 of 12
job_report_grouped_by_media
MNS
Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories
Page 3 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559069
Location:
MW-3_ML1 [ MNS Landfill 1 / MW-3 (LANDFILL)]
Collection Start:
1/26/2022 12:35:00
Job:
MNSGW20221
Collection End:
1/26/2022 12:35:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta 3.24E+00 4.38E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.70E+00
0.00E+00
6.70E+00
<15
<1000
LLD OK
Co-58
<6.16E+00
0.00E+00
6.16E+00
<15
<1000
LLD OK
Fe-59
<1.13E+01
0.00E+00
1.13E+01
<30
<400
LLD OK
Co-60
<5.58E+00
0.00E+00
5.58E+00
<15
<300
LLD OK
Zn-65
<1.19E+01
0.00E+00
1.19E+01
<30
<300
LLD OK
Zr-95
<1.19E+01
0.00E+00
1.19E+01
<15
<400
LLD OK
Nb-95
<7.82E+00
0.00E+00
7.82E+00
<15
<400
LLD OK
1-131
<7.53E+00
0.00E+00
7.53E+00
<15
LLD OK
Cs-134
<7.20E+00
0.00E+00
7.20E+00
<15
<30
LLD OK
Cs-137
<6.95E+00
0.00E+00
6.95E+00
<18
<50
LLD OK
Bala-140
<5.57E+00
0.00E+00
5.57E+00
<15
<200
LLD OK
Be-7
<5.26E+01
0.00E+00
5.26E+01
K-40
1.74E+02
6.02E+01
6.79E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-6.3E+01
0.00E+00
1.83E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559070
Location: MW-3D_ML1 [ MNS Landfill
1 / MW-3D
( LANDFILL) ]
Collection Start: 1/26/2022
12:00:00
Job: MNSGW20221
Collection End: 1/26/2022
12:00:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.43E+00
0.00E+00 6.43E+00 <15
<1000 LLD OK
Co-58
<5.97E+00
0.00E+00 5.97E+00 <15
<1000 LLD OK
Fe-59
<1.13E+01
0.00E+00 1.13E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 4 of 12
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 4 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Location: MW-3D_ML1 [MNS Landfill 1 / MW-3D (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Co-60
<6.31 E+00
0.00E+00
6.31 E+00
<15
Zn-65
<1.07E+01
0.00E+00
1.07E+01
<30
Zr-95
<1.19E+01
0.00E+00
1.19E+01
<15
Nb-95
<6.49E+00
0.00E+00
6.49E+00
<15
1-131
<5.84E+00
0.00E+00
5.84E+00
<15
Cs-134
<6.91 E+00
0.00E+00
6.91 E+00
<15
Cs-137
<6.23E+00
0.00E+00
6.23E+00
<18
Bala-140
<4.86E+00
0.00E+00
4.86E+00
<15
Be-7
<4.55E+01
0.00E+00
4.55E+01
K-40
2.27E+02
6.92E+01
7.31 E+01
H3
Units: pCi/I
H3GW
Station: MCGUIRE
Tritium Analysis of Water
559070
1 /26/2022 12:00:00
1 /26/2022 12:00:00
Fraction SLC/ODCM RPT LVL
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
<-1.9E+01 0.00E+00 1.83E+02 <250 <20000 LLD OK
Location: MW-4_ML1 [MINIS Landfill 1 / MW-4 (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
559071
1 /26/2022 11:00:00
1 /26/2022 11:00:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma
Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Mn-54
<5.38E+00
0.00E+00
5.38E+00
<15
Co-58
<5.13E+00
0.00E+00
5.13E+00
<15
Fe-59
<1.28E+01
0.00E+00
1.28E+01
<30
Co-60
<4.41 E+00
0.00E+00
4.41 E+00
<15
Zn-65
<1.53E+01
0.00E+00
1.53E+01
<30
Zr-95
<8.90E+00
0.00E+00
8.90E+00
<15
Nb-95
<5.96E+00
0.00E+00
5.96E+00
<15
1-131
<6.40E+00
0.00E+00
6.40E+00
<15
Cs-134
<7.39E+00
0.00E+00
7.39E+00
<15
Cs-137
<5.27E+00
0.00E+00
5.27E+00
<18
Bala-140
<8.97E+00
0.00E+00
8.97E+00
<15
Report Generated @ 2/21/2022 15:06:06 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Fraction SLC/ODCM RPT LVL
<1000
LLD OK
<1000
LLD OK
<400
LLD OK
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
EnRad Laboratories Page 5 of 13 02/22/2022
Page 5 of 12

11D Radiological Data for MCGUIRE
Station: MCGUIRE Sample #: 559071
Location: MW-4_ML1 [ MNS Landfill 1 / MW-4 (LANDFILL)] Collection Start: 1/26/2022 11:00:00
Job: MNSGW20221 Collection End: 1/26/2022 11:00:00
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <5.06E+01 0.00E+00 5.06E+01
K-40 <1.12E+02 0.00E+00 1.12E+02
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-2.8E+01 0.00E+00 1.83E+02 <250 <20000 LLD OK
Station: MCGUIRE
Sample #: 559073
Location: MW-4R_ML1 [ MNS Landfill
1 / MW-4R
( LANDFILL) ]
Collection
Start: 1/26/2022 12:20:00
Job: MNSGW20221
Collection
End: 1/26/2022 12:20:00
GW Ground Water
ALPHABETA
Gross Alpha / Beta Analysis in Water and Effluent
Filters
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Alpha
<5.30E-01
0.00E+00
5.30E-01
<3
LLD OK
Beta
<3.22E+00
0.00E+00
3.22E+00
<4
LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Mn-54
<6.30E+00
0.00E+00
6.30E+00
<15
<1000 LLD OK
Co-58
<5.50E+00
0.00E+00
5.50E+00
<15
<1000 LLD OK
Fe-59
<1.27E+01
0.00E+00
1.27E+01
<30
<400 LLD OK
Co-60
<5.50E+00
0.00E+00
5.50E+00
<15
<300 LLD OK
Zn-65
<1.39E+01
0.00E+00
1.39E+01
<30
<300 LLD OK
Zr-95
<1.17E+01
0.00E+00
1.17E+01
<15
<400 LLD OK
Nb-95
<4.69E+00
0.00E+00
4.69E+00
<15
<400 LLD OK
1-131
<6.07E+00
0.00E+00
6.07E+00
<15
LLD OK
Cs-134
<5.79E+00
0.00E+00
5.79E+00
<15
<30 LLD OK
Cs-137
<7.66E+00
0.00E+00
7.66E+00
<18
<50 LLD OK
Bala-140
<8.77E+00
0.00E+00
8.77E+00
<15
<200 LLD OK
Be-7
<5.88E+01
0.00E+00
5.88E+01
K-40
2.02E+02
8.59E+01
1.12E+02
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
H3GW
<3.49E+01
0.00E+00
1.83E+02
<250
<20000 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 6 of 12
job_report_grouped_by_media
MNS
Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories
Page 6 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559074
Location:
MW-4D_ML1 [MNS Landfill 1 / MW-4D (LANDFILL)]
Collection Start:
1/26/2022 11:30:00
Job:
MNSGW20221
Collection End:
1/26/2022 11:30:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<5.61 E+00
0.00E+00
5.61 E+00
<15
<1000
LLD OK
Co-58
<5.75E+00
0.00E+00
5.75E+00
<15
<1000
LLD OK
Fe-59
<9.29E+00
0.00E+00
9.29E+00
<30
<400
LLD OK
Co-60
<5.54E+00
0.00E+00
5.54E+00
<15
<300
LLD OK
Zn-65
<1.05E+01
0.00E+00
1.05E+01
<30
<300
LLD OK
Zr-95
<9.29E+00
0.00E+00
9.29E+00
<15
<400
LLD OK
Nb-95
<7.24E+00
0.00E+00
7.24E+00
<15
<400
LLD OK
1-131
<6.35E+00
0.00E+00
6.35E+00
<15
LLD OK
Cs-134
<7.53E+00
0.00E+00
7.53E+00
<15
<30
LLD OK
Cs-137
<6.71 E+00
0.00E+00
6.71 E+00
<18
<50
LLD OK
Bala-140
<9.64E+00
0.00E+00
9.64E+00
<15
<200
LLD OK
Be-7
<4.01 E+01
0.00E+00
4.01E+01
K-40
<1.26E+02
0.00E+00
1.26E+02
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-1.1E+02
0.00E+00
1.82E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559075
Location: MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR ( LANDFILL) ]
Collection Start: 1/26/2022
13:30:00
Job: MNSGW20221
Collection End: 1/26/2022 13:30:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.30E-01 0.00E+00 5.30E-01 <3 LLD OK
Beta <3.22E+00 0.00E+00 3.22E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.90E+00
0.00E+00 6.90E+00 <15
<1000 LLD OK
Co-58
<5.84E+00
0.00E+00 5.84E+00 <15
<1000 LLD OK
Fe-59
<1.31 E+01
0.00E+00 1.31E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 7 of 12
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 7 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Location: MW-4DR_ML1 [ MNS Landfill 1 / MW-4DR (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Co-60
<5.90E+00
0.00E+00
5.90E+00
<15
Zn-65
<1.33E+01
0.00E+00
1.33E+01
<30
Zr-95
<1.07E+01
0.00E+00
1.07E+01
<15
Nb-95
<5.79E+00
0.00E+00
5.79E+00
<15
1-131
<5.91 E+00
0.00E+00
5.91 E+00
<15
Cs-134
<7.23E+00
0.00E+00
7.23E+00
<15
Cs-137
<6.93E+00
0.00E+00
6.93E+00
<18
Bala-140
<6.29E+00
0.00E+00
6.29E+00
<15
Be-7
<4.80E+01
0.00E+00
4.80E+01
K-40
1.66E+02
6.34E+01
6.48E+01
H3
Units: pCi/I
H3GW
Station: MCGUIRE
Tritium Analysis of Water
559075
1 /26/2022 13:30:00
1 /26/2022 13:30:00
Fraction SLC/ODCM RPT LVL
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
<-9.8E+01 0.00E+00 1.83E+02 <250 <20000 LLD OK
Location: MW-11_ML1 [MNS Landfill 1 / MW-11 (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
559076
1/24/2022 11:00:00
1/24/2022 11:00:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta <3.19E+00 0.00E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma
Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Mn-54
<5.86E+00
0.00E+00
5.86E+00
<15
Co-58
<4.88E+00
0.00E+00
4.88E+00
<15
Fe-59
<1.15E+01
0.00E+00
1.15E+01
<30
Co-60
<6.55E+00
0.00E+00
6.55E+00
<15
Zn-65
<1.27E+01
0.00E+00
1.27E+01
<30
Zr-95
<7.19E+00
0.00E+00
7.19E+00
<15
Nb-95
<4.32E+00
0.00E+00
4.32E+00
<15
1-131
<6.81 E+00
0.00E+00
6.81 E+00
<15
Cs-134
<6.16E+00
0.00E+00
6.16E+00
<15
Cs-137
<5.55E+00
0.00E+00
5.55E+00
<18
Bala-140
<6.24E+00
0.00E+00
6.24E+00
<15
Report Generated @ 2/21/2022 15:06:06 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Fraction SLC/ODCM RPT LVL
<1000
LLD OK
<1000
LLD OK
<400
LLD OK
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
EnRad Laboratories Page 8 of 13 02/22/2022
Page 8 of 12

11D Radiological Data for MCGUIRE
Station: MCGUIRE Sample #: 559076
Location: MW-11_ML1 [MNS Landfill 1 / MW-11 (LANDFILL)] Collection Start: 1/24/2022 11:00:00
Job: MNSGW20221 Collection End: 1/24/2022 11:00:00
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <5.25E+01 0.00E+00 5.25E+01
K-40 1.22E+02 6.78E+01 9.33E+01
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.9E+01 0.00E+00 1.84E+02 <250 <20000 LLD OK
Station: MCGUIRE
Sample #: 559077
Location: MW-11D_ML1 [ MNS Landfill
1 / MW-11D
( LANDFILL) ]
Collection
Start: 1/24/2022 10:30:00
Job: MNSGW20221
Collection
End: 1/24/2022 10:30:00
GW Ground Water
ALPHABETA
Gross Alpha / Beta Analysis in Water and Effluent
Filters
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Alpha
<5.00E-01
0.00E+00
5.00E-01
<3
LLD OK
Beta
<3.19E+00
0.00E+00
3.19E+00
<4
LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Mn-54
<6.03E+00
0.00E+00
6.03E+00
<15
<1000 LLD OK
Co-58
<5.02E+00
0.00E+00
5.02E+00
<15
<1000 LLD OK
Fe-59
<1.02E+01
0.00E+00
1.02E+01
<30
<400 LLD OK
Co-60
<3.13E+00
0.00E+00
3.13E+00
<15
<300 LLD OK
Zn-65
<1.46E+01
0.00E+00
1.46E+01
<30
<300 LLD OK
Zr-95
<1.02E+01
0.00E+00
1.02E+01
<15
<400 LLD OK
Nb-95
<6.49E+00
0.00E+00
6.49E+00
<15
<400 LLD OK
1-131
<7.49E+00
0.00E+00
7.49E+00
<15
LLD OK
Cs-134
<5.34E+00
0.00E+00
5.34E+00
<15
<30 LLD OK
Cs-137
<5.12E+00
0.00E+00
5.12E+00
<18
<50 LLD OK
Bala-140
<8.43E+00
0.00E+00
8.43E+00
<15
<200 LLD OK
Be-7
<4.08E+01
0.00E+00
4.08E+01
K-40
<8.31 E+01
0.00E+00
8.31E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
H3GW
<-4.9E+01
0.00E+00
1.83E+02
<250
<20000 LLD OK
Report Generated @ 2/21/2022
15:06:06
EnRad Laboratory
Page 9 of 12
job_report_grouped_by_media
MNS
Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories
Page 9 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559078
Location:
MW-12_ML1 [ MNS Landfill 1 / MW-12 (LANDFILL)]
Collection Start:
1/24/2022 12:45:00
Job:
MNSGW20221
Collection End:
1/24/2022 12:45:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta <3.19E+00 0.00E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<5.68E+00
0.00E+00
5.68E+00
<15
<1000
LLD OK
Co-58
<5.59E+00
0.00E+00
5.59E+00
<15
<1000
LLD OK
Fe-59
<1.14E+01
0.00E+00
1.14E+01
<30
<400
LLD OK
Co-60
<5.57E+00
0.00E+00
5.57E+00
<15
<300
LLD OK
Zn-65
<1.22E+01
0.00E+00
1.22E+01
<30
<300
LLD OK
Zr-95
<1.18E+01
0.00E+00
1.18E+01
<15
<400
LLD OK
Nb-95
<6.69E+00
0.00E+00
6.69E+00
<15
<400
LLD OK
1-131
<8.06E+00
0.00E+00
8.06E+00
<15
LLD OK
Cs-134
<6.78E+00
0.00E+00
6.78E+00
<15
<30
LLD OK
Cs-137
<6.32E+00
0.00E+00
6.32E+00
<18
<50
LLD OK
Bala-140
<7.78E+00
0.00E+00
7.78E+00
<15
<200
LLD OK
Be-7
<5.53E+01
0.00E+00
5.53E+01
K-40
2.65E+02
7.58E+01
7.81E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-4.7E+00
0.00E+00
1.83E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559079
Location: MW-12D_ML1
[ MNS Landfill
1 / MW-12D ( LANDFILL) ]
Collection Start: 1/24/2022
13:30:00
Job: MNSGW20221
Collection End: 1/24/2022
13:30:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta <3.19E+00 0.00E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.60E+00
0.00E+00 6.60E+00 <15
<1000 LLD OK
Co-58
<6.15E+00
0.00E+00 6.15E+00 <15
<1000 LLD OK
Fe-59
<1.09E+01
0.00E+00 1.09E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:06:06
EnRad Laboratory
Page 10 of 12
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 10 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Location: MW-12D_ML1 [MNS Landfill 1 / MW-12D (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Co-60
<6.51 E+00
0.00E+00
6.51 E+00
<15
Zn-65
<1.54E+01
0.00E+00
1.54E+01
<30
Zr-95
<9.44E+00
0.00E+00
9.44E+00
<15
Nb-95
<5.87E+00
0.00E+00
5.87E+00
<15
1-131
<6.76E+00
0.00E+00
6.76E+00
<15
Cs-134
<7.05E+00
0.00E+00
7.05E+00
<15
Cs-137
<5.64E+00
0.00E+00
5.64E+00
<18
Bala-140
<9.54E+00
0.00E+00
9.54E+00
<15
Be-7
<4.59E+01
0.00E+00
4.59E+01
K-40
1.16E+02
5.33E+01
5.91 E+01
H3
Units: pCi/I
H3GW
Station: MCGUIRE
Tritium Analysis of Water
559079
1 /24/2022 13:30:00
1 /24/2022 13:30:00
Fraction SLC/ODCM RPT LVL
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
<-6.3E+01 0.00E+00 1.82E+02 <250 <20000 LLD OK
Location: SW-1_ML1 [MNS Landfill 1 / SW-1 (LANDFILL)]
Job: MNSGW20221
Sample M
Collection Start:
Collection End:
559080
1 /25/2022 15:15:00
1 /25/2022 15:15:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta <3.19E+00 0.00E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma
Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Mn-54
<5.62E+00
0.00E+00
5.62E+00
<15
Co-58
<6.17E+00
0.00E+00
6.17E+00
<15
Fe-59
<8.76E+00
0.00E+00
8.76E+00
<30
Co-60
<7.05E+00
0.00E+00
7.05E+00
<15
Zn-65
<1.40E+01
0.00E+00
1.40E+01
<30
Zr-95
<1.04E+01
0.00E+00
1.04E+01
<15
Nb-95
<6.65E+00
0.00E+00
6.65E+00
<15
1-131
<6.19E+00
0.00E+00
6.19E+00
<15
Cs-134
<7.16E+00
0.00E+00
7.16E+00
<15
Cs-137
<6.55E+00
0.00E+00
6.55E+00
<18
Bala-140
<8.38E+00
0.00E+00
8.38E+00
<15
Report Generated @ 2/21/2022 15:06:06 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Fraction SLC/ODCM RPT LVL
<1000
LLD OK
<1000
LLD OK
<400
LLD OK
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
Page 11 of 12
EnRad Laboratories Page 11 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Location: SW-1_ML1 [MNS Landfill 1 / SW-1 (LANDFILL)]
Job: MNSGW20221
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units: CiI/I
Sample #: 559080
Collection Start: 1/25/2022 15:15:00
Collection End: 1/25/2022 15:15:00
v Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.48E+01 0.00E+00 4.48E+01
K-40 <1.18E+02 0.00E+00 1.18E+02
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-7.0E+00 0.00E+00 1.82E+02 <250 <20000 LLD OK
Report Generated @ 2/21/2022 15:06:06 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Page 12 of 12
EnRad Laboratories Page 12 of 13 02/22/2022

r_NniN nF: MIRTODY RIPCORD AND ANALYSIS REQUEST FORM
/,� UUKt Duke Energy EnRad Laboratories 1
EnRad LaboratoryUse Only
Mail Cade MGQ3A2 {Building 7405]
ENERGY !
Page 1 of 1
DISTNAL10
LIMS # MN5GW2022'I
sample Class:
�:c.-+_.
-_
13339 Ha9ers Ferry Rd
GROUNDWATER
rripinating
From
LAB,
ORIGINAL LA
Lagged By Lynn llutada
Data d. Time 114f22 09�eB
SAMRLE PFacRAM
! Humersville• N. C. 28075 !
COPY la CL3ENT
CLIENT
[phone]
Grind Water 4
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NPDES,
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usr
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MNS LANDFILL #1 PERMIT # 60-04
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3)Client
4]Fax No:
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Bryan Moeller 1 Ethan Smith I Courtney Murphy
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14Collection Information
Date
Time
SignatureCC
a
• 13Sample Description or ID
Lab ID i
ti
559065
MNS_MW-1
{' y'
'
X
1
1
1
3
559066
MNS_MW-1 D
Lf 15
x
1
1
t
3
5590fi7 !
MNS MW-2A
5 LZ
[
x
1
1
1
3
559068
MNS_MW-2❑
i
f-7 15
x
1
1
1
3
559069
MNS_MW-3
X
1
1
1
3
559070 I M
MNS_MW-3D
j
.:Zo 1)5
x
1
1
1
3
559071 !
MNS_MW-4
x
1
1
1
3
559073 ;;
MNS_MW-4R
Z
x
1
'1
1
3
559074 ; m
MNS_MW-4❑
x
1
1
1
3
659075 i s
MNS_MW-4DR
x
1
1
1
3
559076 A
MNS_MW-11
l ,s
��
x
1
1
1
3
559077 ! d
MNS_MW-1 i D
i
Q]
x
1
1
1
3
559078 a
MNS_MW-12
{
rj
x
1
1
1
3
5s907B ; n
MNS_MW-12D
I'
i �i7
x
1
1
1
3
559080 i
MNS SW-1
i
${
x
1
1
1
3
!2
At
Customer to sign & date below
21 }Relinquished By_EHi mith
Oa elTime
�[�j� I a�
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Datelrime
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Requested Turnaround
21}Relinquish
DatoiTime
Accipted By:
DatelTime
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21)Relinqulshed By
DatelTime
Accepted By:
Datefrime
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23]SeaI1Lo(*ed By
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Add Cost WIN Apply
EnRad Laboratories Page 13 of 13 02/22/2022

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559111
Location:
MW-3BR_ML1 [ MNS Landfill 1 / MW-3BR (LANDFILL)]
Collection Start:
1/26/2022 11:05:00
Job:
MNSGW20222
Collection End:
1/26/2022 11:05:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta 7.26E+00 4.43E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.90E+00
0.00E+00
6.90E+00
<15
<1000
LLD OK
Co-58
<6.03E+00
0.00E+00
6.03E+00
<15
<1000
LLD OK
Fe-59
<1.27E+01
0.00E+00
1.27E+01
<30
<400
LLD OK
Co-60
<5.49E+00
0.00E+00
5.49E+00
<15
<300
LLD OK
Zn-65
<1.28E+01
0.00E+00
1.28E+01
<30
<300
LLD OK
Zr-95
<1.08E+01
0.00E+00
1.08E+01
<15
<400
LLD OK
Nb-95
<6.59E+00
0.00E+00
6.59E+00
<15
<400
LLD OK
1-131
<7.48E+00
0.00E+00
7.48E+00
<15
LLD OK
Cs-134
<7.04E+00
0.00E+00
7.04E+00
<15
<30
LLD OK
Cs-137
<6.31 E+00
0.00E+00
6.31 E+00
<18
<50
LLD OK
Bala-140
<1.06E+01
0.00E+00
1.06E+01
<15
<200
LLD OK
Be-7
<5.05E+01
0.00E+00
5.05E+01
K-40
1.84E+02
7.38E+01
8.78E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-1.3E+02
0.00E+00
1.91 E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559112
Location: MW-4BR_ML1 [ MNS Landfill 1 / MW-413R ( LANDFILL) ]
Collection Start: 1/26/2022
10:10:00
Job: MNSGW20222
Collection End: 1/26/2022
10:10:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha 5.60E-01 7.30E-01 5.10E-01 <3 LLD OK
Beta 2.04E+01 4.69E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.55E+00
0.00E+00 6.55E+00 <15
<1000 LLD OK
Co-58
<7.59E+00
0.00E+00 7.59E+00 <15
<1000 LLD OK
Fe-59
<1.05E+01
0.00E+00 1.05E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:07:18
EnRad Laboratory
Page 1 of 5
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 1 of 6 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Location: MW-4BR_ML1 [ MNS Landfill 1 / MW-4BR (LANDFILL)]
Job: MNSGW20222
Sample M
Collection Start:
Collection End:
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Co-60
<6.42E+00
0.00E+00
6.42E+00
<15
Zn-65
<1.47E+01
0.00E+00
1.47E+01
<30
Zr-95
<1.18E+01
0.00E+00
1.18E+01
<15
Nb-95
<6.40E+00
0.00E+00
6.40E+00
<15
1-131
<5.67E+00
0.00E+00
5.67E+00
<15
Cs-134
<8.03E+00
0.00E+00
8.03E+00
<15
Cs-137
<5.62E+00
0.00E+00
5.62E+00
<18
Bala-140
<6.15E+00
0.00E+00
6.15E+00
<15
Be-7
<5.55E+01
0.00E+00
5.55E+01
K-40
2.10E+02
8.11 E+01
9.95E+01
H3
Units: pCi/I
H3GW
Station: MCGUIRE
Tritium Analysis of Water
559112
1 /26/2022 10:10:00
1 /26/2022 10:10:00
Fraction SLC/ODCM RPT LVL
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
<-1.4E+02 0.00E+00 1.92E+02 <250 <20000 LLD OK
Location: MW-4BRRML1 [ MNS Landfill 1 / MW-4BRR (LANDFILL)]
Job: MNSGW20222
Sample M
Collection Start:
Collection End:
559113
1 /26/2022 13:55:00
1 /26/2022 13:55:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha 7.38E+00 1.15E+00 6.00E-01 <3 LLD OK
Beta 1.21 E+02 6.17E+00 3.94E+00 <4 LLD OK
GAMMAGW
Gamma
Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA SLC/ODCM LLD
Mn-54
<6.51 E+00
0.00E+00
6.51 E+00
<15
Co-58
<5.59E+00
0.00E+00
5.59E+00
<15
Fe-59
<8.40E+00
0.00E+00
8.40E+00
<30
Co-60
<6.20E+00
0.00E+00
6.20E+00
<15
Zn-65
<1.31 E+01
0.00E+00
1.31E+01
<30
Zr-95
<9.71 E+00
0.00E+00
9.71 E+00
<15
Nb-95
<6.20E+00
0.00E+00
6.20E+00
<15
1-131
<6.22E+00
0.00E+00
6.22E+00
<15
Cs-134
<6.36E+00
0.00E+00
6.36E+00
<15
Cs-137
<5.55E+00
0.00E+00
5.55E+00
<18
Bala-140
<6.23E+00
0.00E+00
6.23E+00
<15
Report Generated @ 2/21/2022 15:07:18 EnRad Laboratory
job_report_grouped_by_media MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
Fraction SLC/ODCM RPT LVL
<1000
LLD OK
<1000
LLD OK
<400
LLD OK
<300
LLD OK
<300
LLD OK
<400
LLD OK
<400
LLD OK
LLD OK
<30
LLD OK
<50
LLD OK
<200
LLD OK
EnRad Laboratories Page 2 of 6 02/22/2022
Page 2 of 5

11D Radiological Data for MCGUIRE
Station: MCGUIRE Sample #: 559113
Location: MW-4BRRML1 [ MNS Landfill 1 / MW-4BRR (LANDFILL)] Collection Start: 1/26/2022 13:55:00
Job: MNSGW20222 Collection End: 1/26/2022 13:55:00
GW Ground Water
GAMMAGW Gamma Spectroscopy Ground Water Analysis
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Be-7 <4.61 E+01 0.00E+00 4.61E+01
K-40 2.50E+02 8.74E+01 1.03E+02
H3 Tritium Analysis of Water
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW <-1.5E+02 0.00E+00 1.91 E+02 <250 <20000 LLD OK
Station: MCGUIRE
Sample #: 559114
Location: MW-11BRML1
[ MNS Landfill 1 / MW-11BR
( LANDFILL) ]
Collection
Start: 1/26/2022 09:50:00
Job: MNSGW20222
Collection
End: 1/26/2022 09:50:00
GW Ground Water
ALPHABETA
Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Alpha
<5.00E-01
0.00E+00
5.00E-01
<3
LLD OK
Beta
<3.19E+00
0.00E+00
3.19E+00
<4
LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Mn-54
<6.18E+00
0.00E+00
6.18E+00
<15
<1000 LLD OK
Co-58
<4.17E+00
0.00E+00
4.17E+00
<15
<1000 LLD OK
Fe-59
<9.33E+00
0.00E+00
9.33E+00
<30
<400 LLD OK
Co-60
<5.58E+00
0.00E+00
5.58E+00
<15
<300 LLD OK
Zn-65
<1.40E+01
0.00E+00
1.40E+01
<30
<300 LLD OK
Zr-95
<8.57E+00
0.00E+00
8.57E+00
<15
<400 LLD OK
Nb-95
<6.41 E+00
0.00E+00
6.41 E+00
<15
<400 LLD OK
1-131
<6.07E+00
0.00E+00
6.07E+00
<15
LLD OK
Cs-134
<5.86E+00
0.00E+00
5.86E+00
<15
<30 LLD OK
Cs-137
<5.72E+00
0.00E+00
5.72E+00
<18
<50 LLD OK
Bala-140
<5.80E+00
0.00E+00
5.80E+00
<15
<200 LLD OK
Be-7
<4.52E+01
0.00E+00
4.52E+01
K-40
<7.43E+01
0.00E+00
7.43E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
H3GW
<-1.7E+02
0.00E+00
1.91 E+02
<250
<20000 LLD OK
Report Generated @ 2/21/2022 15:07:18
EnRad Laboratory
Page 3 of 5
job_report_grouped_by_media
MNS
Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories
Page 3 of 6 02/22/2022

11D Radiological Data for MCGUIRE
Station:
MCGUIRE
Sample #:
559115
Location:
MW-13D_ML1 [MNS Landfill 1 / MW-13D (LANDFILL)]
Collection Start:
1/26/2022 14:00:00
Job:
MNSGW20222
Collection End:
1/26/2022 14:00:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha <5.00E-01 0.00E+00 5.00E-01 <3 LLD OK
Beta <3.19E+00 0.00E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<6.09E+00
0.00E+00
6.09E+00
<15
<1000
LLD OK
Co-58
<6.35E+00
0.00E+00
6.35E+00
<15
<1000
LLD OK
Fe-59
<1.15E+01
0.00E+00
1.15E+01
<30
<400
LLD OK
Co-60
<5.78E+00
0.00E+00
5.78E+00
<15
<300
LLD OK
Zn-65
<1.35E+01
0.00E+00
1.35E+01
<30
<300
LLD OK
Zr-95
<9.24E+00
0.00E+00
9.24E+00
<15
<400
LLD OK
Nb-95
<4.74E+00
0.00E+00
4.74E+00
<15
<400
LLD OK
1-131
<6.94E+00
0.00E+00
6.94E+00
<15
LLD OK
Cs-134
<6.47E+00
0.00E+00
6.47E+00
<15
<30
LLD OK
Cs-137
<5.64E+00
0.00E+00
5.64E+00
<18
<50
LLD OK
Bala-140
<6.18E+00
0.00E+00
6.18E+00
<15
<200
LLD OK
Be-7
<5.06E+01
0.00E+00
5.06E+01
K-40
1.55E+02
6.67E+01
7.99E+01
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
H3GW
<-1.1E+02
0.00E+00
1.91 E+02
<250
<20000
LLD OK
Station: MCGUIRE
Sample #: 559116
Location: MW-13BRML1 [ MNS Landfill 1 / MW-13BR ( LANDFILL) ]
Collection Start: 1/26/2022
13:30:00
Job: MNSGW20222
Collection End: 1/26/2022
13:30:00
GW Ground Water
ALPHABETA Gross Alpha / Beta Analysis in Water and Effluent Filters
Units: pCi/I Activity 2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Alpha 5.70E-01 7.30E-01 5.00E-01 <3 LLD OK
Beta 3.68E+00 4.35E+00 3.19E+00 <4 LLD OK
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error Calculated MDA SLC/ODCM LLD Fraction SLC/ODCM RPT LVL
Mn-54
<5.95E+00
0.00E+00 5.95E+00 <15
<1000 LLD OK
Co-58
<5.89E+00
0.00E+00 5.89E+00 <15
<1000 LLD OK
Fe-59
<1.27E+01
0.00E+00 1.27E+01 <30
<400 LLD OK
Report Generated @ 2/21/2022 15:07:18
EnRad Laboratory
Page 4 of 5
job_report_grouped_by_media
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 4 of 6 02/22/2022

11D Radiological Data for MCGUIRE
Station: MCGUIRE
Sample #: 559116
Location: MW-13BRML1 [ MNS Landfill 1 / MW-13BR (LANDFILL)]
Collection
Start: 1/26/2022
13:30:00
Job: MNSGW20222
Collection
End: 1/26/2022
13:30:00
GW Ground Water
GAMMAGW
Gamma Spectroscopy Ground Water Analysis
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
Co-60
<6.30E+00
0.00E+00
6.30E+00
<15
<300
LLD OK
Zn-65
<1.43E+01
0.00E+00
1.43E+01
<30
<300
LLD OK
Zr-95
<1.11 E+01
0.00E+00
1.11E+01
<15
<400
LLD OK
Nb-95
<7.20E+00
0.00E+00
7.20E+00
<15
<400
LLD OK
1-131
<6.80E+00
0.00E+00
6.80E+00
<15
LLD OK
Cs-134
<8.33E+00
0.00E+00
8.33E+00
<15
<30
LLD OK
Cs-137
<7.41 E+00
0.00E+00
7.41 E+00
<18
<50
LLD OK
Bala-140
<9.19E+00
0.00E+00
9.19E+00
<15
<200
LLD OK
Be-7
<4.89E+01
0.00E+00
4.89E+01
K-40
2.31 E+02
9.41 E+01
1.24E+02
H3
Tritium Analysis of Water
Units: pCi/I
Activity
2 Sigma Error
Calculated MDA
SLC/ODCM LLD
Fraction SLC/ODCM RPT LVL
H3GW
<-1.6E+02
0.00E+00
1.91 E+02
<250
<20000
LLD OK
Report Generated @ 2/21/2022 15:07:18
job_report_grouped_by_media
EnRad Laboratory
MNS Building 7405 (MG03A2)
13339 Haqers Ferry Road
Huntersville, NC 28078
[phone]
EnRad Laboratories Page 5 of 6 02/22/2022
Page 5 of 5

Ir - .., - CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
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EnRad Laboratories Page 6 of 6 02/22/2022