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3412_Forsyth_OldSalisburyRoad_CDLF_Nov2022GW_FID1772791_20230209
ENR USE ONLY: ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form_ Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. • Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards The notification must include a preliminary analysis of the cause and significance of each value (e.g naturally occurring, off -site source, pre-existing condition, etc ). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). • Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): HDR Engineering, Inc. of the Carolinas Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: nn,rk p Fll,rrii Phone: .70AA'An-a7a� E-mail: iVla[k Filardi hhririnr rnrt'L NC Landfill Rule: Actual sampling dates (e.g.. Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Old Salisbury Road Landfill 34-12 0.0500 3336 Old Salisbury Road November 7-10, 2022 Winston-Salem, NC 27127 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring �X Assessment Monitoring Corrective Action T e of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data X Surface water monitoring data ❑XEl Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. HX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Mark P. Filardi, P.G. Southeast Remediation Lead 704-338-6787 Facility Representative Name (Print) Title Filardi Mark Digitally signed by Filardi, Mark i Date: 2023.02.09 14:14:46-05'00' Signature Date 440 South Church Street Suite 1200, Charlotte, NC 28202 Facility Representative Address (Area Code) Geologist Seal F-0116 NC PE Firm License Number (if applicable effective May 1, 2009) D—i—a aronno FN Winston-Salem / Forsyth County UtI9i 140ties Water • Wastewater • Solid Waste HDR Project No. 10347433 i Assessment Monitoring Report Groundwater and Surface Water Sampling Event — November 2022 Old Salisbury Road Landfill NCDEQ Permit NO. 34-12 Forsyth County, North Carolina February 2023 This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Contents List of Acronyms 1 Introduction......................................................................................................................... 1 1.1 Facility Background...................................................................................................... 1 1.2 Regulatory Authority.................................................................................................... 1 1.3 Assessment Monitoring................................................................................................ 1 1.4 Geologic Characteristics.............................................................................................. 1 1.4.1 Regional Geologic and Hydrogeologic Setting ...................................................... 1 1.4.2 Site Specific Topography and Drainage................................................................ 2 1.4.3 Site Specific Hydrogeology................................................................................... 2 2 Monitoring Network............................................................................................................. 2 3 Data Collection................................................................................................................... 3 3.1 Water Level Measurements......................................................................................... 3 3.2 Groundwater Flow........................................................................................................ 3 3.3 Sample Collection and Analysis................................................................................... 3 4 Analytical Results................................................................................................................ 4 4.1 Groundwater................................................................................................................4 4.2 Surface Water.............................................................................................................. 6 4.3 Landfill Gas.................................................................................................................. 6 5 Summary............................................................................................................................ 6 6 Recommendations.............................................................................................................. 7 February 2023 i Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Figures Figure 1 Groundwater contours and sample locations Figure 2 Historical groundwater elevations Figure 3 Time vs. concentration for MW-2R groundwater detections Tables Table 1 Existing groundwater monitoring well details Table 2 Sampling parameters and schedule Table 3 Groundwater measurements and elevations — November 7, 2022 Table 4 Historical groundwater elevations Table 5 Interwell flow Table 6 Summary of laboratory analytical detections — November 7 - 10, 2022 Table 7 Summary of landfill gas readings — November 7, 2022 Appendices Appendix A — Summary of Monitoring Results Al — Detections of Concern A2 — Groundwater Detections by Well Location A3 — Surface Water Detections A4 — Historical Detections by Date Appendix B — Laboratory Reports Appendix C — Field Data Appendix D — Electronic Files (Paper Copies Only) February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� List of Acronyms List of Acronyms 2B 15A NCAC Subchapter 02B — Surface Water and Wetlands Standards 2L 15A NCAC Subchapter 02L — Groundwater Classification and Standards pg/L micrograms per liter EPA United States Environmental Protection Agency FID NCDEQ File Identification HDR HDR Engineering, Inc. LEL lower explosive limit MCPP Methylchlorophenoxypropionic acid (mecoprop) MDL method detection limit NCAC North Carolina Administrative Code NCDEQ North Carolina Department of Environmental Quality NRWQC Nationally Recommended Water Quality Criteria OSR Old Salisbury Road PCE tetrachloroethene PVC polyvinyl chloride PWR Partially weathered rock SVOC semi -volatile organic compound VOC volatile organic compound USGS U.S. Geological Survey February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� List of Acronyms This page intentionally left blank. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Introduction 1 Introduction HDR Engineering, Inc. of the Carolinas (HDR), on behalf of Winston-Salem/Forsyth County Utilities (the City), is submitting this assessment monitoring report for the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North Carolina (Figure 1). 1.1 Facility Background OSR covers approximately 56 acres within a 140-acre tract north of Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The facility was issued a permit to operate on July 3, 1996, and opened in August of the same year. 1.2 Regulatory Authority OSR is currently operating under North Carolina Department of Environmental Quality (NCDEQ) facility permit number 34-12, dated February 28, 2020 (FID 1389508). Groundwater monitoring and reporting requirements are outlined in items 14 to 21 of the permit. North Carolina Solid Waste Management (SWM) Rules 15A NCAC 13B .0544(b) and .0544(c) define the requirements of groundwater and surface water monitoring plans, respectively, as applicable to OSR. The groundwater monitoring plan (FID 1388728) dated January 2020, was approved by NCDEQ on February 28, 2020. 1.3 Assessment Monitoring OSR is in assessment monitoring, as specified in 15 NCAC 02L .0202 (2L Standards), for benzene and tetrachloroethene (PCE) detected in well MW-2R in 2011. On December 9, 2011, an assessment monitoring plan for MW-2R was submitted in accordance with 15A NCAC 13B. The assessment monitoring plan can be summarized as: • Groundwater monitoring wells MW-1 R, MW-2R, MW-4R and MW-15 will be sampled semi-annually for Appendix I constituents and the previously detected Appendix II constituents, as specified in 40 CFR §258. All 14 groundwater monitoring wells (including MW-1 R, MW-2R, MW-4R and MW-15) will be sampled during every other fall event (odd years) for the entire Appendix II constituent list. Additional Appendix II constituents detected during these events will be added to the sampling program for subsequent semi-annual events. 1.4 Geologic Characteristics Regional and site -specific geology and hydrogeology were originally presented in the July 2003 Groundwater Monitoring Plan and the 2003 Design Hydrogeologic Investigation Report. The summaries that follow are taken from those reports. 1.4.1 Regional Geologic and Hydrogeologic Setting As shown on the 1985 Geologic Map of North Carolina, OSR is in the Raleigh Belt of the Piedmont Physiographic Province. This province is characterized by metamorphic and igneous rocks, which have been extensively weathered and eroded, forming an undulating topography. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network Subsurface conditions generally consist of topsoil underlain by residual soils, saprolite, partially weathered rock (PWR), and bedrock. There is generally a gradual transition between material types with varying thickness. Bedrock in the Raleigh Belt is characterized by numerous plutons with granitic to gabbroic composition that have intruded gneiss, schist, metavolcanic rocks, and metamorphosed mafic complexes (basalt, gabbro, and ultramafic rocks). Typically, bedrock is overlain by PWR and saprolite. Saprolite retains some of the original (relict) structural features of the parent rock and varies in thickness from a few feet to over 100 feet. The near surface residual soils are formed by physical and chemical weathering of the saprolite and usually do not retain the relict structural features. Groundwater is present within fractures and joints in the bedrock and within the pore spaces of the overlying saprolite and residual soils. Groundwater is primarily recharged by precipitation and commonly located within the saprolite layer. Groundwater moves laterally toward streams and surface water bodies and generally follows the surface topography. 1.4.2 Site Specific Topography and Drainage Surface drainage at OSR generally follows topography and flows toward the South Fork Muddy Creek and its tributaries. A small area on the southeast portion of the site drains south into Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow west where they converge with Muddy Creek and eventually discharge to the Yadkin River. 1.4.3 Site Specific Hydrogeology As documented in the Design Hydrogeological Investigation Report submitted by HDR on December 2, 2003, the uppermost aquifer underlying the facility is comprised of three stratigraphic units. The downward progression of the three units is saprolite transitioning into PWR, then bedrock. Groundwater flows through pore spaces within the saprolite and PWR, while groundwater flow through the bedrock is primarily through fractures. OSR was constructed within the unconsolidated micaceous silty sands and sandy silts produced by the in -situ weathering of the granodioritic parent rock. There is no evidence of discrete flow patterns resulting from relict quartz veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In general, groundwater flows from areas of higher elevation to areas of lower elevation and mimics surface topography. 2 Monitoring Network The monitoring network consists of 14 groundwater wells and 4 surface water sampling locations. Well construction details are presented in Table 1. Sampling of monitoring wells and surface water locations is conducted on a semi-annual basis, as summarized in Table 2. Groundwater monitoring well MW-1 R is located hydraulically upgradient of the landfill and is considered as the background well for the site. Upstream surface water (SW-1) and downstream surface water (SW-2) samples are obtained from the adjacent stream east of OSR. Two surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity of MW- February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 2R. Surface water sampling location SW-3 is located south of the entrance road near MW-2R; while SW-4 is located on the north side of the entrance road, downstream of SW-3. 3 Data Collection 3.1 Water Level Measurements On November 7, 2022, static groundwater level measurements were obtained from the 14 existing groundwater monitoring wells, MW-1 R through MW-5R and MW-7 through MW-15 (MW-6R was abandoned). Groundwater depths were measured to the nearest 0.01 foot from the top of the PVC casing prior to purging each well. Depth to water data was used to calculate static groundwater elevations for the current sampling event (Table 3). Historical groundwater elevations are presented in Table 4 and depicted on Figure 2. 3.2 Groundwater Flow Hydraulic gradients were calculated between representative well pairs positioned approximately perpendicular to groundwater flow. The flow velocities have been calculated based on the historical average hydraulic conductivity of 0.466 ft/day for the PWR material and an effective porosity of 25 percent, as presented in Table 2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report. Historically (based on data collected since May 2003), estimated groundwater flow velocities ranged from approximately 9 feet per year (ft/yr) from well MW-13 to MW-10 to approximately 49 ft/yr from well MW-2R to MW-15. Estimated groundwater flow velocities for this sampling event ranged from 10 ft/yr to 47 ft/yr between the same well pairs. Historical and recent groundwater flow velocities are presented in Table 5. 3.3 Sample Collection and Analysis HDR collected samples from 14 wells and 4 surface water locations between November 7 and 10, 2022. Groundwater was purged and sampled from each well using low -flow sampling techniques until stabilization of field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) was achieved. Samples were collected using dedicated QED TM MicroPurge® pumps that were installed in August 2004, except MW-15, which was sampled with a variable speed submersible pump. Field parameters were recorded and are presented in Appendix C. Surface water samples were collected from locations (SW-1 through SW-4) outside of the landfill boundary to evaluate potential groundwater to surface water interaction. Prior to sample collection, field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) were measured with a water quality meter and recorded on field data sheets (Appendix C). It should be noted that SW-1 was sampled on November 7, 2022; however, due to a transcription error on the COC, SW-1 was recorded as being sampled on November 6, 2022. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results Non -disposable sampling equipment was decontaminated after each use by washing in a Liqunox® detergent solution followed by a tap -water rinse. Purge water was discharged to the ground surface adjacent to its respective collection site (monitoring well). For quality control, equipment blank and field blank samples were collected using laboratory - provided deionized water. The field blank sample was collected and analyzed to ensure that the sample handling process did not introduce external constituents into the groundwater samples. The equipment blank sample was collected by pouring the laboratory -provided deionized water over the water -level meter, once decontaminated, to evaluate the effectiveness of field decontamination processes. Sample containers were labeled with the project name, sample ID, date, and time of collection. This same information was also recorded on a chain -of -custody form. The samples were placed in a cooler with ice, then transported under chain -of -custody protocol to Pace Analytical Services, LLC (Pace) in Huntersville, North Carolina (NC Cert. #12), Asheville, North Carolina (NC Cert. #40), Ormond Beach, Florida (NC Cert. #12710), and Mt. Juliet, Tennessee (NC Cert. #375) for laboratory analysis. 4 Analytical Results 4.1 Groundwater During this sampling event the following constituents exceeded the 2L Standards: • Concentrations of 1,4-dioxane (p-dioxane) exceeded the 2L Standard of 3 µg/L in MW- 2R, MW-4R, MW-7, MW-10, MW-12, and MW-13. • The concentration of benzene in MW-2R exceeded the 2L Standard of 1 µg/L. • Concentrations of cobalt exceeded the 2L Standard of 1 µg/L in MW-2R through MW- 4R, MW-7, and MW-10 through MW-12. • Concentrations of iron exceeded the 2L Standard of 300 µg/L in MW-1 R through MW- 4R, MW-7, MW-10 through MW-12, and MW-15. • Concentrations of manganese exceeded the 2L Standard of 50 µg/L in MW-1 R through MW-4R, MW-7, MW-10 through MW-13, and MW-15. • Concentrations of mercury exceeded the 2L Standard of 1 µg/L in MW-1 R. • pH exceeded the 2L Standard range of 6.5 — 8.5 in MW-1 R through MW-5R, MW-7 through MW-9, and MW-11 through MW-14. • Total dissolved solids exceeded the 2L Standard of 500,000 µg/L in MW-2R, MW-4R, MW-7, and MW-10. • Concentrations of vinyl chloride exceeded the 2L Standard of 0.03 µg/L in MW-2R, however, the results were greater than the method detection limit (MDL) and below the method reporting limit (MRL) (J-flagged value). February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results In 2011, concentrations of benzene and tetrachloroethene (PCE) were detected above 2L Standards in well MW-2R triggering assessment monitoring. During this event, 1,4-dioxane (p- dioxane), benzene, and vinyl chloride (as a J-flagged value) exceeded the 2L Standard in the sample collected from well MW-2R. However, the constituents that triggered assessment monitoring in 2011 (benzene and PCE) were not detected in down -gradient monitoring wells, indicating that these constituents are confined to the OSR site and do not extend to off -site properties. 1,4-dioxane was detected at concentrations slightly greater than the 2L Standard (3.0 pg/L) in the groundwater samples from several wells, including down -gradient locations MW-4R, MW-7, MW-10, MW-12, and MW-13. The highest concentration of 1,4-dioxane observed during this sampling event was in the sample collected from MW-7 (7.8 pg/L). Concentrations of 1,4- dioxane increased in MW-2R during the November 2019 monitoring event, and peaked during the November 2020 monitoring event. Since that time, it appears that the concentration trend of 1,4-dioxane has been decreasing in MW-2R, which suggests that there is not a replenishing source and down -gradient concentrations observed should not be expected to increase over time. Detections of the other VOCs analyzed at the down -gradient monitoring locations were less than the 2L Standard, and generally less than the laboratory reporting limit (J-flag). Benzene (2.7 pg/L) and vinyl chloride (0.73J pg/L) were detected in the groundwater sample collected from MW-2R at concentrations slightly greater than the respective 2L Standards. The vinyl chloride concentration is an estimated value, less the reporting limit. Estimated values of benzene less than the reporting limit (also less than the 2L Standard) were observed at down - gradient locations MW-7, MW-10, and MW-12. The remaining exceedances are naturally occurring inorganic compounds commonly found in Piedmont soils and are likely not indicative of a release from the landfill. The trends of select constituents of concern in MW-2R detected above the current standard and are shown on Figure 3. Pesticides were not detected in the groundwater samples during this monitoring event. The herbicide constituent MCPP was detected in wells MW-2R and MW-4R. It should be noted that the herbicide samples for MW-1 R, MW-2R, MW-4R, MW-15, DUP-1, equipment blank, and field blank were analyzed outside of the required method hold time due to logistical issues amongst the available laboratories in Pace's network. Confirmation sampling of the herbicide MCPP will be conducted during the Spring 2023 sampling event. Appendix II semi-volatiles were last detected in groundwater samples during the November 2017 sampling event. Concentrations of constituents detected during this sampling event are presented in Table 6. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. Field sampling data sheets are included in Appendix C. An electronic file containing the analytical data in NCDEQ electronic data deliverable format will be submitted to NCDEQ separately. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Summary 4.2 Surface Water Surface water analytical results were compared to 15A NCAC 02B (2B Standards). Note that there are no 2B Standards for 1,1-dichloroethene, 1,4-dichlorobenzene, 1,4-dioxane (p- dioxane), acetone, alkalinity, antimony, barium, benzene, cadmium, chloroform, cis-1,2- dichloroethene, cobalt, copper, dichlorodifluoromethane, ethylbenzene, iron, lead, manganese, m&p-xylenes, MCPP, o-xylene, silver, sodium, sulfide, tetrahydrofuran, total dissolved solids, trichloroethene, trichlorofluoromethane, vanadium, vinyl chloride, or zinc. Therefore, North Carolina In -Stream Target Values for Surface Water for Class C freshwater and Environmental Protection Agency Nationally Recommended Water Quality Criteria (EPA NRWQC) for Class C freshwater (Class C Standards) were applied, where applicable. • Alkalinity exceeded the EPA NRWQC standard of 20,000 µg/L in all surface water samples. Cobalt exceeded the North Carolina In -Stream Target Values for Surface Water for Class C freshwater standard of 1.6 µg/L in SW-1, SW-3, and SW-4. • Iron exceeded the EPA NRWQC standard of 1,000 µg/L in all surface water samples. A summary of surface water quality data obtained during this sampling event is shown in Table 6. Laboratory data for surface water samples collected during the current monitoring event are included in Appendix B. 4.3 Landfill Gas Landfill gas was measured at well MM-1, MW-1 R, MW-2R, MW-13, and MW-15 during the current sampling event. Measured carbon dioxide (CO2), oxygen (02), hydrogen sulfide (112S), and methane (CH4) levels are shown in Table 7. Methane concentrations in the wells and monitoring points were lower than the lower explosive limit (LEL) of 5.0 percent during this monitoring event. Gas field readings are included in Appendix C. Note that the City is responsible for quarterly sampling of all methane monitoring wells and related reporting, which is not included in this document. 5 Summary Groundwater constituent concentration exceedances consisted of 1,4-dioxane (p- dioxane), benzene, cobalt, iron, manganese, mercury, total dissolved solids, vinyl chloride (J-flagged value), and pH exceeded the 2L. Benzene was not detected in down - gradient wells. • Pesticides were not detected in groundwater samples during the November 2022 monitoring event. • The herbicide constituent MCPP was detected in wells MW-2R and MW-4R, however, all herbicide samples were analyzed outside of the required method hold time due a lab error. Confirmation sampling of the herbicide MCPP will be conducted during the Spring 2023 sampling event. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Recommendations Appendix II semi-volatiles were last detected in groundwater samples during the November 2017 sampling event. • Concentrations of alkalinity, cobalt, and iron exceeded applicable surface water criteria in one or more surface water samples. Results of limited landfill gas monitoring conducted during this event indicate that the concentration of carbon dioxide and oxygen in MM-1 and MW-13 were outside of ambient levels. Measurements for MM-1 are consistent with previous readings, however, ranges of carbon dioxide and oxygen in MW-13 exceeded atmospheric ranges for the first time since November 2017. Methane concentrations in the wells and monitoring points did not exceed the (LEL) of 5.0 percent during this event. 6 Recommendations • Based on the results of groundwater, surface water, and landfill gas monitoring conducted during this semi-annual event, chloroform and toluene will be added to the recently detected Appendix II VOCs list to be sampled semi-annually. • Due to the detection of MCPP in MW-2R and MW-4R, the recently detected herbicides list to be sampled semi-annually will include MCPP. • SVOCs and pesticides were not detected during this event and therefore will not be sampled until fall of 2023; except for the constituents listed for specific locations in Table 2 that will continue to be monitored on a semiannual reporting schedule. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Recommendations This page intentionally left blank. February 2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Figures Figures r -I Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Figures This page intentionally left blank. I . - :I ..:..... - I .. LEGEND Property Line Existing Monitoring Well Q Abandoned Monitoring Well Methane Probe t Surface Water Sample Location Groundwater Contour ski— — Groundwater Contour (Inferred) noon='s MW-1U i- 726. 8 Jo. Approximate Groundwater Flow 3VV_2 Topographic Contour MW-14 MM 1° 732.90, USGS National Hydrography MW 9 M-.-11 Dataset �739.14 728,74°" Permit/Phase Boundary r • " �� Forsyth County Parcel r,. ° __ MW-8 �� _ 743.35 MM-11 MM-a �► — 1 0 MW-12 733.66 L ° 'vo MM-12 \`1 I r vt ` - �• I MW=13 N.,MW-3R/ �— �. o 742:96 756�77 \� SW- / \ MW=15 SW-1 763.49 F)l OLD SALISBURY ROAD C&D LANDFILL GROUNDWATER CONTOURS AND SAMPLE LOCATIONS N 0 500 FEET DATE NOVEMBER 7, 2022 FIGURE FIGURE 1 Figure 2 Historical Groundwater Elevations Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina 810 800 N 790 E w 0 M 780 a w c ro 770 v w a 760 3 N v io 750 3 3 0 o 740 730 720 1� �z Nam fan �z Nam fan Nam �a� �a� Nam NO Nay a� NO Nay Nay Nam Sample Date BMW-1R fMW-2R —BMW-5R tMW-6R BMW-7 MW-15 —X—MW-4R MW-3R $MW-8 MW-13 MW-9 —a� MW-12 CIE MW-14 fMW-11 tMW-10 Figure 3 Time vs. Concentration for MW-2R VOCs of Concern Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina 4.5 4 3.5 3 J al c 2.5 0 2 c 0 U 1.5 1 0.5 01a" l.Ja\N.J1311 1 21 NIsa" N.J011 Ja1 NISa" l.Ja\NIsa" NISa" l.Ja\N.J1311 Date Collected 1,4-Dioxane (p-Dioxane) Benzene —� Tetrachloroethene Vinyl chloride Benzene 2L PCE 2L VC 2L 1,4-Dioxane 2L 2/6/2023 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Figures This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Tables Tables r -I Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Tables This page intentionally left blank. Table 1 Existing Groundwater Monitoring Well Details Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina NC State NC State Well Depth to Top Of Ground OSR LF Installed Plane Plane Diameter Well Depth (ft Top of Screened Screened Interval Casing Elevation WELL bgs) Screen Interval (ft) Geology Elevation Northing Easting (inches) (ft bgs) (ft MSL) (ft MSL) MW-1R 12/27/1995 820,411 1,622,983 2 60 45 15 Granitic saprolite 836.42 833.40 MW-2R 12/29/1995 820,974 1,622,722 2 23 8 15 Granitic saprolite 785.22 781.81 MW 2 27 12 15 Granitic saprolite 776.60 772.90 MW-4R 12/28/1995 820,435 1,621,428 2 20 5 15 Granitic saprolite 767.96 765.70 MW-5R 12/29/1995 820,137 1,622,1301& 2 32 Granitic saprolite 784.36 782.30 MW-6R 7/8/1999 821,079 1,622,430 2 60 45 15 PWR 820.40 817.80 MW-7 12/28/1995 820,886 1,621,424 2 48 Granitic saprolite 803.66 MW-8 7/7/1999 821,930 1,621,485 2 27 12 15 Granitic saprolite 762.50 759.80 MW-9 8/11/20OW 822, 1,986 2 60 4 n 90.28 788.04 MW-10 8/10/2004 822,626 1,622,699 2 21 6 15 Sand 738.21 735.70 MW-11 8/10/2004 822,307 1,622,838 2 20 5 15 Sand 732.59 730.35 MW-12 8/9/2004 821,844 1,622,955 2 16 6 10 Silt 739.07 736.41 MW-13 8/9/2004 821,500 1,622,915 2 20 5 15 Sand 751.23 749.19 MW-14 8/11/2004 822,420 1,622,260 2 60 45 15 Sand 783.88 781.44 MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58 Table 2 Sampling Parameters and Schedule Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina Surface Method Parameter(s)* Frequency Monitoring wells water EPA 300.0 Sulfate 2x/year All All EPA 6010/EPA Trace metals 2x/year All All 6020 EPA 7470 Mercury 2x/year All All Pesticides: all Fall of odd All None years (2023) Pesticides recently detected: EPA 8081 4,4'-DDD, 4,4'-DDT, aldrin, alpha-BHC, delta- MW-1 R, MW-2R, BHC, endosulfan I, endosulfan 11, endrin, endrin 2x/year MW-4, MW-7, None aldehyde, heptachlor, heptachlor epoxide & MW-10 & MW-15 methoxychlor Fall of odd EPA 8082 years (2023) All None EPA Herbicides: all Fall of odd years (2023) All None 8151/SW- Herbicides previously detected: MW-1 R, MW-2R, 846-8321 2,4,5-TP (Silvex), 2,4-D 2x/year MW-4R & MW-15 None App I VOCs, tetrahydrofuran & 2x/year All 1,4-dioxane EPA 8260 Appendix II VOCs: All Fall of odd None years (2023) Appendix II VOCs recently detected: 2x/year dichlorodifluoromethane All None SVOCs: All Fall of odd All None years (2023) EPA 8270 SVOCs recently detected: benzo(a)anthracene, MW-1 R, MW-2R, bis(2-ethylhexyl)phthalate, chrysene, 2x/year MW-3R, MW-4R SW-2 dibenz(a,h)anthracene, & indeno(1,2,3-cd)pyrene & MW-15 SM 2320B Alkalinity 2x/year All All SM 2540C Total dissolved solids 2x/year All All SM 4500 Chloride, cyanide, sulfi 2x/year All All Field Temperature, specific conductance, dissolved 2x/year All All oxygen, redox, turbidity, pH Field Total well depth, static water eve 2x/year All NA Prepared bv: CWG, QC'd b• Table 3 Groundwater Measurements and Elevations - November 7, 2022 Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina Well ID Top of Casing Elevation (ft) Ground Surface Elevation (ft) Depth to Water (ft) Groundwater Elevation (ft) MW-1 R 836.42 833.40 34.17 802.25 MW-2R 785.22 781.81 8.32 776.90 M W-3R 776.60 772.90 19.83 756.77 M W-4R 767.96 765.70 7.85 760.11 M W-5R 784.36 782.30 11.47 772.89 M W-7 803.66 802.10 34.05 769.61 M W-8 762.50 759.80 19.15 743.35 M W-9 790.28 788.04 51.14 739.14 MW-10 738.21 735.70 11.73 726.48 MW-11 732.59 730.35 3.85 728.74 MW-12 739.07 736.41 5.41 733.66 MW-13 751.23 749.19 8.27 742.96 MW-14 783.88 781.44 50.98 732.90 M W-15 802.85 800.58 39.36 763.49 Prepared by BW, QC'D by BJS Table 4 Historical Goundwater Elevations Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina Well ID Nov-17 May-18 Nov-18 May-19 Nov-19 May-20 Nov-20 May-21 Nov-21 May-22 Nov-22 MW-1R 801.59 800.85 801.34 &802.!�M803JM803.60 804.27 803.93,,_ 804.59 803.23 802.25 MW-2R 777.00 777.39 777.75 778.47 777.35 778.53 778.25 779.14 777.40 777.33 776.90 MWW 756.20 IW.57 760.08 762.49 759.64 763.59 762.36 0. 756.77 MW-4R 759.04 759.60 759.94 762.32 761.04 763.11 763.05 764.94 762.41 761.78 760.11 MW-5R 772.94 773.35 773.56 774.95 773.89 775.06 774.85 Am 774.23 774.08 772.89 MW-7 767.01 766.57 767.21 769.41 769.81 771.15 771.86 773.16 772.12 771.04 769.61 744.95 747.7 74GMI, 753.13 M&54 8.19 _ 743.35 MW-9 737.45 736.82 736.80 738.65 739.68 740.00 740.78 741.14 741.68 740.23 739.14 727.98 726.64 727.78 727.33 727.40 726.48 MW-11 728.22 728.81 729.27 728.96 728.98 729.22 729.37 730.05 728.56 728.79 728.74 - 733.77 734.13 734.26 734.52 734.46 733.90 733.66 MW-13 742.19 742.75 743.34 743.15 742.87 743.36 743.47 744.16 742.92 743.27 742.96 MW-1 733.39 733.30 733.78 3.80 MW-15 763.48 763.71 764.08 765.11 763.87 765.04 764.62 765.58 764.03 764.07 763.49 Prepared bv: CWG, QC'd bv: ZDH Table 5 Interwell Flow Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina Min. Velocity ft/ r Based on Historical Record Max. Range of Travel Time Velocity Myr (Years) May 2019 Nov 2019 May 2020 Flow Velocity (ft/yr) Nov 2020 May 2021 Nov 2021 May 2022 Nov 2022 MW-1 R to 17 19 82.6 93.4 18 18 18 18 17 18 18 18 MW-4R MW-1Rto 22 30 20.8 28.2 26 28 28 29 27 30 28 28 MW-2R MW-2R to 41 44 12.9 13.7 43 42 43 42 42 42 41 41 MW-13 MW-13 to 9 10 116.1 127.3 9 10 9 10 9 10 9 10 MW-10 MW-2R to 49 4.0 4.2 47 47 47 48 47 47 46 47 MW-15 Prepared by: CWG, QGd by: ZDH Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Tables This page intentionally left blank. Table 6 Summary of Laboratory Analytical Detections - November 7 - 10, 2022 Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth Count, North Carolina Constituents 213 Standards ... MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 Sample Locations MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 DUP-1 MW-4R EQBL FB Sulfate 250,000 250,000 790J 66,300 1,760 133,000 8,420 98,400 8,290 807J 146,000 9,830 94,600 27,300 <1,000 22,800 2,840 11,700 34,000 46,500 139,000 <1,000 <1,000 Sulfide NE NE <100 27.6J <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 Antimony 5,300 1 0.56J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Arsenic 150 10 <1.0 1.0 5.3 1.6 <1.0 0.62J <1.0 <1.0 0.901 <1.0 0.57J <1.0 <1.0 <1.0 0.71J 0.55J 2.0 0.97J 1.6 <1.0 <1.0 Barium 21,000 700 304 467 231 157 59.1 283 60.1 191 93.0 69.6 161 515 249 18.1 45.9 143 367 263 154 <1.0 <1.0 Beryllium 6.5 4 0.46 0.082J 0.063J 0.055J <0.10 0.49 0.47 0.26 0.17 0.067J 0.063J 1.8 0.69 0.049J 0.11 0.034J 0.40 0.22 0.056J <0.10 <0.10 Cadmium NE 2 0.0901 <0.10 <0.10 <0.10 <0.10 0.16 <0.10 <0.10 <0.10 <0.10 <0.10 0.072J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 Chromium 11 10 7.9 0.75J 0.69J 0.55J 6.6 0.801 3.8 0.61J 2.1 <1.0 0.77J <1.0 0.97J 1.7 2.5 0.68J 9.4 5.3 0.62J <1.0 <1.0 Cobalt Copper 1.6 NE 1 0.74J 5.3 1.5 0.39J 0.64J <1.0 0.25J 3.5 <1.0 <1.0 <1.0 0.37J 0.69J 0.27J 0.86J 0.56J 0.62J 0.27J 1.1 0.36J 3.8 1.9 4.0 1.4 0.55J 4.5 16.5 5.9 5.5 0.68J <1.0 <1.0 <1.0 0.74J 1,000 Iron 1,000 300 42.5 74.3 142 183 50.9iiiiiiiiiiie E, 6,950 4,170 37,400 10,800 <10.0 6.7J Lead NE 15 0.46J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.51J <1.0 <1.0 <1.0 <1.0 0.33J 2.4 <1.0 6.7 2.4 <1.0 <1.0 <1.0 Manganese Nickel NE 25 50 100 5.8 13.8 0.811 0 8.9 1.06575.3 1.2 5.2 0.31J 6.2 0.58J 10.5 0.67J 9.0 2.2 . 4.6 2.4 721 1.7 2,990 2.2 2,690 5.8 6,200 6.4 0 8.6 0.37J <1.0 <1.0 <1.0 Selenium 5 20 0.39J <2.0 0.23J <2.0 0.23J 0.25J 1.2J <2.0 1.4J <2.0 <2.0 <2.0 <2.0 <2.0 0.37J <2.0 1.2J 0.65J <2.0 <2.0 <2.0 Silver NE 20 0.053J <0.50 <0.50 <0.50 <0.50 0.047J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.079J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Sodium NE NE 16,200 60,500 2,480 74,000 13,300 43,900 11,200 14,600 112,000 11,900 23,700 17,800 18,000 16,800 13,100 18,800 16,800 35,500 72,000 <2,000 <2,000 Vanadium NE 7 3.0 1.3 <1.0 <1.0 5.5 1.1 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 2.1 4.7 0.991 21.4 12.7 <1.0 <1.0 <1.0 Zinc NE 1,000 15.2 6.0 <5.0 18.6 <5.0 16.9 <5.0 <5.0 <5.0 <5.0 <5.0 8.9 <5.0 9.5 22.9 <5.0 51.8 17.8 5.1 11.5 <5.0 Mercury 0.012 1 <0.20 <0.20 <0.20 <0.20 0.17J <0.20 <0.20 <0.20 <0.20 <0.20 0.15J <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 1,1-Dichloroethane NE 6 <1.0 <1.0 <1.0 <1.0 <1.0 0.87J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1,4-Dichlorobenzene NE 6 <1.0 0.59J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Acetone 2,000 6,000 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 132J <25.0 <25.0 <25.0 <25.0 Benzene NE 1 <1.0 <1.0 <1.0 <1.0 0.95J <1.0 <1.0 0.63J <1.0 0.36J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Chloroform NE 70 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.45J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 cis-1,2-Dichloroethene NE 70 0.64J 1.1 <1.0 <1.0 <1.0 1.01 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Dichlorodifluoromethane NE 1,000 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.35J <1.0 <1.0 <1.0 <1.0 3.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Ethylbenzene 97 600 0.67J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 M&p-Xylene 670 500 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 0.75J O-Xylene 600 500 <1.0 <1.0 <1.0 <1.0 <1.0 0.44J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Tetrachloroethene 0.7 0.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Tetrahydrofuran 110,000 2,000 <10.0 12.8 <10.0 10J <10.0 48.0 <10.0 <10.0 74.3 <10.0 <10.0 10.1 <10.0 <10.0 <10.0 <10.0 <10.0 5.2J 9.91 <10.0 <10.0 Toluene 11 600 0.28J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.30J 0.26J <1.0 <1.0 <1.0 <1.0 Trichloroethene NE 3 <1.0 0.61J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Trichlorofluoromethane NE 2,000 <1.0 <1.0 <1.0 <1.0 <1.0 0.96J <1.0 0.37J <1.0 <1.0 <1.0 0.45J 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Vinyl Chloride NE 0.03 <1.0 ARM <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1,4-Dioxane (p-Dioxane) NE 3 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 4.4 <2.0 5.6 <2.0 <2.0 MCPP' NE NE <2.0 5.67 NS 8.02 NS NS NS NS NS NS NS NS NS <2.0 NS NS NS NS 8.96 <2.0 <2.0 Alkalinity, Total as CaCO3 20,000 NE 90,400 879,000 130,000 552,000 33,900 265,000 29,300 29,200 919,000 106,000 294,000 84,400 63,100 83,100 41,700 140,000 234,000 351,000 544,000 <5,000 <5,000 Total Dissolved Solids NE 500,000 163,000 ��� 121,000 ��� 159,000 ��� 86,000 139,000 ffffa LI�� 173,000 496,000 272,000 158,000 255,000 88,000 245,000 312,000 511,000 � <25,000 <25,000 Chloride 230,000 250,000 11,700 39,800 2,860 46,200 14,700 32,500 3,710 3,690 51,400 8,540 28,200 47,300 3,910 54,700 19,500 27,200 20,600 43,500 45,300 <1,000 <1,000 pH 6.0-9.0 6.5-8.5 6.50 6.35 7.13 7.1 7.28 NS NS Notes: 1. Methods used for analysis include: EPA 8081 B, EPA 6010, EPA 6020, EPA 7470A, EPA 8321, EPA 8270E, EPA 8260D, EPA 8260D Mod., SM 23206-2011, SM 2540C-2015, SM 4500-S2D-2011, EPA 300.0 Rev 2.1 1993, SM 4500-CL-E-2011, SM 4500-CN-E-2016 2. All Concentrations reported in pg/L with exception of pH 3. NS = Not Sampled 4. < = Constituents not detected at concentration greater than laboratory method reporting limit (MRL) 5. ' = Not Tested within method hold time 6. Concentration exceeds 2L Standards (2022) or IMAC (2022) = 7. Concentration exceeds 213 Standards, NCDEQ In -Stream Target Values, and EPA National Recommended Water Quality Criteria for Surface Water = Yellow Highlight 8. Estimated concentration is below the Method Reporting Limit (MRL) but above the Method Detection Limit (MDL) (J-Flag) = Italics 9. Estimated concentration (J-flag) below the MRL but greater than the 2L Standards, IMAC, 213 Standards, NCDEQ In -Stream Target Values, or EPA National Recommended Water Quality Criteria for Surface Water = Prepared by: CWG, QCd by: ZDH Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Tables This page intentionally left blank. Table 7 Summary of Landfill Gas Readings - November 7, 2022 Old Salisbury Road Construction & Demolition Landfill NCDEQ Permit No. 34-12 Forsyth County, North Carolina Date ID # H2S PPm CH4 (%) CO2 (%) 02 M) 12-Nov-19 MM-1 0.0% 12-Nov-19 MW-13 0.0% 0.0% 21.1% 12-Nov-19 MW-15 0.0% 0.2% 20.7% 12-Nov-19 MW-1R 0.0% 0.0% 21.1% 12-Nov-19 MW-2R 0.0% 0.0% 21.0% 4-May-20 MM-1 1 0.0% 4-May-20 MW-13 0 0.1% 0.1% 20.9% 4-May-20 MW-15 0 0.0% 0.2% 21.2% 4-May-20 MW-1R 0 0.0% 0.1% 20.9% 4-May-20 MW-2R 0 0.0% 0.1% 20.7% 3-Nov-20 3-Nov-20 MM-1 MW-1R 0.0% 0.0% 0.1% 20.7% 3-Nov-20 MW-2R 0.0% 0.1% 20.4% 3-Nov-20 MW-13 0.0% 0.2% 21.0% 3-Nov-20 MW-15 0.0% 0.5% 20.3% 11-May-21 11-May-21 MM-1 MW-1R 0.0% 0.0% 1.3% 0.2% 21.1% 11-May-21 MW-2R 0.0% 0.1% 20.8% 11-May-21 MW-13 0.0% 0.1% 21.0% 11-May-21 MW-15 0.0% 0.2% 21.1% 8-Nov-21 8-Nov-21 MM-1 MW-1R 0.0% 0.0% 0.2% 21.2% 8-Nov-21 MW-2R 0.0% 0.5% 20.8% 8-Nov-21 MW-13 0.0% 1.3% 20.8% 8-Nov-21 MW-15 0.0% 0.4% 20.8% 9-May-22 MM-1 0.0% 9-May-22 MW-1R 0.0% 0.1% 20.3% 9-May-22 MW-2R 0.0% 0.1% 20.3% 9-May-22 MW-13 0.0% 0.1% 21.0% 9-May-22 MW-15 0.0% 0.2% 20.7% 7-Nov-22 MM-1 0.0% 7-Nov-22 MW-1 R 0.2% 0.1% 20.9% 7-Nov-22 MW-2R 0.2% 0.2% 20.4% 7-Nov-22 7-Nov-22 MW-13 MW-15 0.0% 0.2% A 1.1% 19.79%. Notes: Prepared by CWG, QC'd by: ZDH Normal atmospheric range for CO2 is 0.0% to 1.3%; measurements outside of this range are shaded red. Normal atmospheric range for 02 is greater than 19.5%; measurements less than this range are shaded blue. Highlighted cells are outside normal atmospheric ranges Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Tables This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report Appendix A — Summary of Monitoring Results 6 1#1,---,*r Appendix A —Summary of Monitoring Results Al — Detections of Concern A2 — Groundwater Detections by Well Location A3 — Surface Water Detections A4 — Historical Detections by Date Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results Al — Detections of Concern Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Al 50 pg/L 50 pg/L 70 pg/L 70 pg/L 70 pg/L NE pg/L NE pg/L NE pg/L NE pg/L NE pg/L 40 pg/L 40 pg/L 0.008 pg/L 0.008 pg/L 0.004 pg/L 0.004 pg/L 1000 pg/L 1000 pg/L 0.005 pg/L 0.005 pg/L 0.05 pg/L 0.05 pg/L 6 pg/L 6 pg/L 6 pg/L 0.4 pg/L 0.4 pg/L 6 pg/L 6 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 40 pg/L 40 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column N Labels N CD M O 00 CO � n r O CO Row Labels j z N T 2 N j z N T 2 N j z N T 2 j z T 2 j z T 2 U o > z T 2 > z T 2 Herbicides ■■■■■■■■■■CPP Pesticides Heptachlor epoxide SeButylbenzylphthalate miVOCs ■■............■EN SW-2 2 Indeno(1,2,3-cd)pyrene-.■■■_ ■■■■■■■■■■ vocs MI 0000001 =31 1,1-Dichloroethane 3.7 3.3 4.1 3.4 4.2 3.9 3.7 M 4.9 5.2 6.7 5.9 6.3 4.7 4 5.1 7.8 7.3 =®®®=© 5.7 5.4 4.3 4.4 3.6 6.6 7.9 6.4 8.5 6.1 7.9 5.7 5.8 10.3 5.3 4.4 3.3 0 ��=� 4.5 16.5 5.6 7.4 3.2 6.6 6.5_ _____ _M_ W-S GW Revised.xlsb 1 of 4 Al NE pg/L NE pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 700 pg/L 700 pg/L 3000 pg/L 3000 pg/L 3000 pg/L 70 pg/L 70 pg/L 3 pg/L 3 pg/L 3 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels 1 '• 4-Meth I-2- entanone MIBK MW-10 0.65 1.7 1.1 2.8 2.5 Acetone MW-2R 10.3 M W-3R 21.4 MW-4R 11 MW-5R 18.4 M W-7 15.7 M W-8 15.8 MW-10 16.4 13.7 12.1 22.5 14.1 MW-11 21.1 MW-12 12.1 MW-13 17.3 MW-14 14.7 MW-15 13.2 SW-1 11.2 SW-2 12.9 SW-3 132 16.2 SW-4 16 Benzene MW-2R MW-4R 0.38 MW-5R 0.28 MW-7 0.95 0.69 0.6 0.64 0.48 0.6 0.68 0.37 0.41 0.39 0.38 0.43 0.42 0.3 MW-10 0.63 0.62 0.47 0.48 0.56 0.78 0.33 0.55 0.55 0.57 0.52 0.83 MW-12 0.36 0.49 0.41 0.37 0.29 0.25 0.33 SW-3 0.73 0.42 SW-4 0.99 0.25 Carbon Disulfide MW-10 2.1 2 5.2 Chloroethane MW-2R 4.3 M W-7 0.85 Chloroform MW-15 0.45 0.45 0.44 0.44 0.4 0.44 0.7 Chloromethane MW-11 0.23 SW-2 0.12 cis- 1,2-Dichloroethene 0.82 0.8 1.3 1.2 1.1 0.9 0.85 0.71 0.76 0.62 0.38 0.2 MW-1R 0.64 1.2 MW-2R 1.1 1.2 1.3 1.2 0.58 0.84 0.95 0.67 0.38 0.55 0.66 0.6 0.51 0.47 MW-7 1 0.82 0.83 0.74 1.7 0.91 1.4 1.5 0.86 0.85 1.1 1.1 1.1 1.1 0.8 MW-10 0.23 0.27 0.23 0.2 0.33 MW-12 0.5 0.4 0.23 SW-2 0.33 SW-3 0.26 SW-4 1.1 0.32 Dichlorodifluoromethane MW-2R 0.74 MW-7 0.52 0.62 MW-9 0.35 1.1 0.57 1.1 0.9 1.4 0.99 1.2 1.7 1.2 1.5 0.88 MW-14 3-71 3.31 3.7 4.1 2.4 2.4 4.51 3 2.4 3 3.61 3.91 3.61 2.31 3.6 W-S GW Revised.xlsb 2 of 4 Al 600 pg/L 600 pg/L 600 pg/L NE pg/L NE pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels 1 R Eth (benzene MW-1R 0.67 0.32 0.37 0.34 0.38 MW-10 0.41 0.53 0.55 lodomethane MW-2R 9.9 _ m&p-Xylene 0.73 MW-5R MW-7 0.74 0.95 0.72 0.93 1 1.1 1.7 1.6 1.4 1.2 2.2 1.8 MW-10 0.68 1.3 1.1 1.2 2.1 Methylene Chloride MW-1 R 2.3 MW-2R 22 1.1 MW-3R MW-4R 2.9 MW-5R M W-7 MMilEREM 1.7 MW-8 1.1 MW-10 2.8 MW-11 1.4 MW-12 2 MW-14 1.6 MW-15 2.4 SW-1 2 SW-2 SW-3 1 SW-4 1.2 o-Xylene 0.45 MW-5R _ MW-7 0.44 0.38 0.48 0.46 0.66 0.46 0.54 0.68 0.59 0.65 0.62 0.68 0.46 0.63 0.5 MW-10 0.34 0.84 0.28 0.53 0.78 1.1 0.97 1 2.1 MW-11 0.27 Tetrachloroethene MW-2R 0.48 M W-7 MW-14 0.5 0.55 0.68 0.65 0.53 0.48 0.52 0.61 Tetrahydrofuran MW-2R 12.8 15 19.5 25.2 12.9 38.6 83 51.3 45.4 46 59.1 28 36.3 39.1 50 MW-4R 10 10.4 14.7 16.8 13.4 11.4 8.6 11.4 9.3 13.6 3.5 MW-7 48 50.4 68.8 77.5 90.9 70.5 77.9 80.4 50.5 24.9 20.1 32 21.7 14 MW-10 74.3 74.8 65.1 89.1 69.6 130 141 113 169 192 135 131 182 237 6.1 MW-11 4.5 MW-12 5.9 11.4 26.8 12 MW-13 10.1 13.9 12.7 11.4 MW-15 4.8 6.5 8.9 8.2 9.2 14.8 12 16.8 27 SW-2 61.3 SW-3 6.1 3.4 6.3 SW-4 5.2 7.4 9.6 5.5 3.5 9.1 6.7 13.7 5.7 3.5 3.6 W-S GW Revised.xlsb 3 of 4 Al 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 88 pg/L 88 pg/L 0.03 pg/L 0.03 pg/L 500 pg/L 500 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels 1 R Toluene MW-1 R 0.28 MW-5R 1.7 MW-10 0.26 0.35 0.27 MW-11 1 MW-12 0.74 MW-13 0.58 SW-2 0.3 0.52 SW-3 0.26 Trichloroethene MW-1 R 0.65 MW-2R 0.61 0.82 1 1.4 1 1.1 1.1 0.97 0.9 0.93 1.3 0.93 1 1.2 0.7 M W-7 0.58 Trich lorofluoromethane MW-2R 0.61 0.61 1.5 0.7 MW-7 0.96 0.78 4.4 10.2 5.4 5.6 4 2 1.2 1.2 1.6 1.6 0.91 1.5 0.9 MW-9 0.37 0.38 1.2 0.66 1.3 0.86 1.7 1.3 1.3 1.4 1.2 1.4 1 1.3 MW-12 0.81 1 0.89 1.4 0.52 1 2.8 1.4 MW-13 0.45 MW-14 1.7 1.9 1.7 2.5 1.6 1 1.5 0.92 0.86 0.79 0.8 0.87 0.75 0.58 1.1 MW-15 0.21 0.42 0.22 0.71 2.1 4.4 5.1 SW-4 0.32 Vinyl acetate MW-2R 2 Vinyl chloride MW-2R 1 1 • • 1 Xylenes (Total) MW-10 1.1 W-S GW Revised.xlsb 4 of 4 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results A2 — Groundwater Detections by Well Location r -I Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. F,NPe�, .,, Old Salisbury Road Landfill (C&D) .,, Old Salisbury Road Landfill (C&D) F,„Pe�.,, Old Salisbury Road Landfill (C&D) F,„Pe�n .,, Old Salisbury Road Landfill (C&D) F,,Pe�n —, Old Salisbury Road Landfill (C&D) F,NPe�, .,, Old Salisbury Road Landfill (C&D) F,„Pe�n .,, Old Salisbury Road Landfill (C&D) This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results or A3 -Surface Water Detections Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Old Salisbury Road Landfill A3 Surface Water Detections within the last 6 years 2B units Max of Result ColumnLabels 2000 pg/L ad- Acetone 11.2 20000 pg/L Alkalinity, Total as CaCO3 41700 22000 71400 36800 39400 40100 15900 22300 27400 49200 43600 33200 57400 150 pg/L Arsenic 0.71 8.5 8.5 3.6 21000 pg/L Barium 45.9 27.9 535 70.7 30.5 25.6 120 109 47 68.2 47.5 86.8 65.9 6.5 pg/L Beryllium 0.11 2 0.54 NE pg/L Cadmium 0.48 230000 pg/L Chloride 19500 972 24400 29600 14500 12100 35100 55400 18300 29700 35700 49200 26800 11 pg/L Chromium 2.5 1.8 24.8 3.8 1.6 pg/L Cobalt 1.9 1.2 13 NE pg/L Copper 4 5 13.8 5.5 5 pg/L Cyanide 4.4 1000 pg/L Iron 6950 2300 69000 794 12600 1550 6980 889 1840 6560 4900 5040 5660 NE pg/L Lead 2.4 18.3 3.4 NE pg/L Manganese 721 258 1250 63.9 488 255 149 48.5 135 926 461 804 1050 11000 pg/L Methylene Chloride 25 pg/L Nickel 1.7 12.2 2.5 5 pg/L Selenium 0.37 NE pg/L Sodium 13100 3040 17900 15000 9360 10400 17000 19400 11800 15600 17000 23000 14200 250000 pg/L Sulfate 2840 612 7440 7570 979 533 7890 7970 4140 2060 2730 2530 3410 NE pg/L Sulfide 52.1 NE pg/L Total Dissolved Solids 88000 50000 199000 144000 85000 76000 143000 174000 106000 131000 123000 143000 116000 NE pg/L Vanadium 4.7 3.6 65.8 9.2 NE pg/L Zinc 22.9 70.2 16.1 5.2 10.1 NE pg/L 1,4-Dioxane (p-Dioxane) 4.4 3.3 2.5 2.2 2.7 1.3 FM 2000 pg/L Acetone 12.9 20000 pg/L Alkalinity, Total as CaCO3 140000 89000 111000 309000 87000 78800 74900 54900 62600 56000 57600 46200 58800 150 pg/L Arsenic 0.55 8.3 3.7 21000 pg/L Barium 143 179 92.5 96.9 99.3 100 110 85.6 78.8 74.2 65.4 77.5 108 6.5 pg/L Beryllium 0.034 230000 pg/L Chloride 27200 11800 21900 9880 19700 19300 20200 19400 12800 13500 15200 13800 6190 NE pg/L Chloromethane 0.12 11 pg/L Chromium 0.68 2.8 3.8 NE pg/L cis- 1,2-Dichloroethene 0.33 1.6 pg/L Cobalt 1.4 NE pg/L Copper 0.55 2.2 4.1 5 pg/L Cyanide 4.2 5 pg/L Dibenz(a,h)anthracene 2 NE pg/L Indeno(1,2,3-cd)pyrene 2.2 1000 pg/L Iron 4170 27800 1500 464 2870 4030 8890 4370 4140 2540 1740 1790 29900 NE pg/L Lead 2.7 NE pg/L Manganese 2990 1050 549 3180 755 1040 825 680 615 397 196 304 1160 11000 pg/L Methylene Chloride 25 pg/L Nickel 2.2 3.5 1.6 5 pg/L Selenium 4.7 NE pg/L Sodium 18800 11100 15300 9850 14400 14200 14500 12300 11900 11300 11600 11600 10200 250000 pg/L Sulfate 11700 14800 13900 79400 21200 19300 16600 13500 20000 11100 9920 10900 6270 110000 pg/L Tetrahydrofuran 61.3 11 pg/L Toluene 0.3 _ 0.52 NE pg/L Total Dissolved Solids 245000 150000 202000 420000 174000 171060 166000 182000 144000 135000 125000 129000 106000 NE pg/L Vanadium 0.99 1.3 4.5 2.4 3.2 NE pg/L Zinc 250 _ 5 12/20/2022 1 of 2 Old Salisbury Road Landfill A3 Surface Water Detections within the last 6 years 2B units Max of Result ColumnLabels NE pg/L �,.N 1.3 1,4-Dioxane (p-Dioxane) 2000 pg/L Acetone 13.2 16.2 20000 pg/L Alkalinity, Total as CaCO3 234000 350000 379000 361000 324000 330000 360000 473000 181000 356000 477000 251000 520000 150 pg/L Arsenic 2 21000 pg/L Barium 367 243 278 246 191 169 189 273 122 223 217 173 270 NE pg/L Benzene 0.73 0.42 6.5 pg/L Beryllium 0.4 230000 pg/L Chloride 20600 28300 25100 22400 21600 19600 26100 28000 12000 22300 33800 18400 34000 11 pg/L Chromium 9.4 NE pg/L cis- 1,2-Dichloroethene 0.26 1.6 pg/L Cobalt 4.5 3 4.5 4.2 12.6 5.3 7.2 3 6.8 NE pg/L Copper 16.5 5 pg/L Cyanide 4.6 1000 pg/L Iron 37400 13600 26700 29900 8300 7910 5650 13000 2500 13100 1720 8240 10500 NE pg/L Lead 6.7 5 7.3 NE pg/L Manganese 2690 7550 5640 3870 3400 3280 5130 7890 2130 6310 7340 4750 8350 0.012 pg/L Mercury 0.18 11000 pg/L Methylene Chloride 25 pg/L Nickel 5.8 5.7 7.4 4 6.9 3.9 5.5 3.6 6.8 5 pg/L Selenium 1.2 NE pg/L Sodium 16800 27200 26100 21000 23800 22500 27200 34000 16900 27000 35500 24600 38400 250000 pg/L Sulfate 34000 16600 21800 14000 18800 28600 29600 43600 16000 18500 33800 15200 18500 NE pg/L Sulfide 54 110000 pg/L Tetrahydrofuran 6.1 3.4 6.3 NE pg/L Tin 11 pg/L Toluene 0.26 NE pg/L Total Dissolved Solids 312000 470000 477000 402000 406000 421000 415000 668000 241000 413000 600000 321000 623000 NE pg/L Vanadium 21.4 3.1 35.3 7.9 2 2.5 NE pg/L Zinc _ 51.8 7.1 NE pg/L 1,4-Dioxane (p-Dioxane) 5.6 4.5 7.4 16.5 3.2 6.6 6.5 2000 pg/L Acetone 16 20000 pg/L Alkalinity, Total as CaCO3 351000 330000 453000 411000 299000 281000 207000 265000 145000 211000 192000 187000 240000 150 pg/L Arsenic 0.97 21000 pg/L Barium 263 180 202 310 153 170 215 382 124 138 110 121 128 NE pg/L Benzene 0.99 0.25 6.5 pg/L Beryllium 0.22 230000 pg/L Chloride 43500 28900 50000 57000 33600 42200 44300 18700 24800 29800 36800 27400 27900 11 pg/L Chromium 5.3 4.7 NE pg/L cis- 1,2-Dichloroethene 1.1 0.32 1.6 pg/L Cobalt 5.9 5.5 5.3 6.4 2.6 11.6 NE pg/L Copper 5.5 5.8 5 pg/L Cyanide 4.1 1000 pg/L Iron 10800 7800 3110 26000 5080 5580 17400 38700 3890 3020 802 1480 1520 NE pg/L Lead 2.4 3.6 NE pg/L Manganese 6200 6570 6400 3600 4840 4510 2960 7710 1470 3580 1020 2900 2930 11000 pg/L Methylene Chloride 25 pg/L Nickel 6.4 6.3 8.8 4.9 4.8 4.4 2.6 5 pg/L Selenium 0.65 NE pg/L Sodium 35500 29000 42400 37800 31400 31400 29100 22000 20000 23400 25600 23400 26000 250000 pg/L Sulfate 46500 28200 66700 75000 53700 68200 52500 17400 27500 24400 26700 18200 28600 110000 pg/L Tetrahydrofuran 5.2 7.4 9.6 5.5 3.5 9.1 6.7 13.7 5.7 3.5 3.6 NE pg/L Total Dissolved Solids 511000 426000 644000 606000 452000 471000 392000 444000 236000 327000 317000 289000 325000 NE pg/L Trichlorofluoromethane 0.32 NE pg/L Vanadium 12.7 1.8 38.4 4.6 7.6 4.5 NE pg/L Zinc 17.8 14.4 90.1 6.9 8.3 12/20/2022 2 of 2 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results /m\4 A4 — Historical Detections by Date Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 250000 pg/L NE pg/L 1 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L 20 pg/L 7 pg/L 1000 pg/L 1 pg/L 0.1 pg/L 0.006 pg/L 40 pg/L 6 pg/L 6 pg/L 1 pg/L 10 pg/L 3000 pg/L 70 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 2000 pg/L November-22 pg/L EPA 300.0 Rev 2.1 1993 Sulfate EPA 6010 Sodium EPA 6020 Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Vanadium Zinc EPA 7470A Mercury EPA 8081 B 4,4'-DDT alpha-BHC Methoxychlor EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Bromomethane Chloroethane Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrahydrofuran 790 66300 1760 133000 8420 98400 8290 807 146000 9830 94600 27300 22800 16200 60500 2480 74000 13300 43900 11200 14600 112000 11900 23700 17800 18000 16800 0.56 1 5.3 1.6 0.62 0.9 0.57 304 467 231 157 59.1 283 60.1 191 93 69.6 161 515 249 18.1 0.46 0.082 0.063 0.055 0.49 0.47 0.26 0.17 0.067 0.063 1.8 0.69 0.049 0.09 0.16 0.072 7.9 0.75 0.69 0.55 6.6 0.8 3.8 0.61 2.1 0.77 0.97 1.7 0.74 5.3 1.5 0.39 .0 0.64 0.25 3.5 0.37 0.69 0.27 0.86 0.56 0.62 0.27 1.1 0.36 3.8 0.46 5.8 is : • 13.8 :1 1 • 1 0.81 1611 8.9 42.5 1 1.2 5.2 74.3 5.3 0.31 142 6.2 0.58 .1 0.51 1 $ 10.5 0.67 • 9 183 2.2 50.9 48.6 4.6 1 0.33 2.4 0.37 0.39 0.23 0.23 0.25 1.2 1.4 0.053 0.047 0.079 3 1.3 5.5 1.1 1.5 2.1 15.2 6 18.6 16.9 8.9 9.5 11.5 0.17 0.15 0.022 0.022 0.023 0.023 0.035 0.035 0.038 0.038 0.87 0.59 1.7 1.7 0.95 1.7 1.7 1.7 0.63 0.36 1.7 0.65 0.65 0.65 0.65 0.65 0.65 0.65 0.65 0.65 0.45 0.64 1.1 1 0.35 0.35 0.35 0.35 0.35 3.7 0.67 2 2 2 2 2 2 2 21 21 2 1 0.44 3.51 12.81 48 74.3 3.5 3.5 10.1 3.51 3.5 3.5 12/20/2022 1 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 600 pg/L 3 pg/L 2000 pg/L 88 pg/L 0.03 pg/L 3 pg/L NE pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 7 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 10 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 0.28 i e Toluene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride EPA 8260D Mod. 1,4-Dioxane(p-Dioxane) EPA 8321 MCPP SM 2320B-2011 Alkalinity, Total as CaCO3 SM 2640C-2015 Total Dissolved Solids SM 4500-CI-E-2011 Chloride SM 4500-S2D-2011 Sulfide May-22 pg/L EPA 300.0 Rev 2.1 1993 Sulfate EPA 6010D Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Sodium Vanadium Zinc EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Bromomethane Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene 0.61 0.96 0.37 0.45 1.7 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 5.67 8.02 90400 879000 130000 552000 33900 2 55000 29300 29200 9 99000 106000 294000 84400 63100 83100 163000 o11 121000 : 011 169000 else 86000 139000 1111 173000 496000 272000 158000 255000 11700 39800 2860 46200 14700 32500 3710 3690 51400 8540 28200 47300 3910 54700 27.6 22 719 58200 139000 9030 128000 9090 1170 166000 11500 96700 29300 26000 308 367 185 61.2 311 61.2 204 155 79.5 191 573 304 18.5 1.5 0.31 0.78 0.33 0.37 1.5 0.48 6.2 3.5 3.7 1.7 3 • 3 8.9 3.1 44.9 •8 1 1 60.8 75.3 13.3 231 32 44.1 2.2 17.9 13.1 3.6 7 5.3 11. 29100 15.3T 1190 5560 15.6 121 4 569 6.8 74 2.8 7 6.9 15500 57200 75200 12700 35700 10800 15500 125000 11600 27600 18300 18000 17100 1.6 1.8 1.7 5 1.8 1.6 2.4 1.1 2.1 1.3 13.3 11.8 0.52 0.72 0.62 0.49 1.7 0.54 0.82 1.2 0.82 0.5 3.3 0.32 2 0.38 0.5 151 10.41 50.4 74.8 13.9 0.82 12/20/2022 2 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date w 2L Units NE • 00■■■ •TotalDissolved 0000 . r ./L NE pg/L r . 0 r ./L . 0 0--------------__- Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 EPA 8260D Mod. ■ . ■ • EPA 9r SM r 0 SM 0 Solids SM r EPA 300.0---------------__- - Copper------®--®--__- Sodium EPA 7470A ` 8081 EPA 8151 EPA 8260D Chloroethane-®-------------__- ---------------__- 3.3- 5.2-- 7.3-- 5.4- 7.9 6.4--__- ---------------__- 111 111111111111111111111111, '���� 11111111111111111111111, ���� ��� :��� •'���� ..��� •���� :•��� ��� ����111111111111111,11111111111111111- ---------------__- 868000 - 910000 •rrr - 512000 . 166 rrr 1350000 566000 :•��� rrr ��� __- •11 : .11 1111111111111111111111, ��111111111111111,11111111111111111- --------- 6.2 -----__- - 26.2 10.1 96.3 ----- 4.6 -----__- 7700 72900 2100 3950 24600 1020 1780 20100 4140 1220 -- 207 26400 1190 3440 155 134 314 - ----------®®®__- 96.9 25.8 9.3 ®---- 125 13.2 22.4 -®-__- 3.1 -------------__- ---------------__- ---------------__ 0.0305 3.7 ---------__- 12/20/2022 3 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date NE pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 7 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 9.9 e lodomethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2640C Total Dissolved Solids SM 4600-CI-E Chloride SM 4500-CN-E Cyanide ft Field Static Water Level May-21 pg/L EPA 300.0 Sulfate EPA 601OD Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Sodium Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene 0.74 2.2 0.48 0.55 19.5 14.7 68.8 65.1 12.7 4.8 1 0.61 4.4 0.38 1.7 2.4 88700 782000 63100 585000 32000 85000 30000 33800;43900 81300 296000 93800 63000 104000 152000 fill 129000 .sit 165000 207000 84000 145000 176000 489000 276000 160000 247000 9750 46800 2360 61500 14100 10000 3800 3640 8460 22400 49800 3650 37700 7.8 31.83 7.82 16.8 5.55 10.13 31.54 16.31 48.6 11.31 4.03 5.4 8.31 49.68 38.82 1130 53800 1910 180000 12000 9840 8580 202000 16800 92500 14100 27400 6.2 271 299 246 168 57.7 121 54 238 106 78.1 141 397 241 6.4 1.4 6 1 •• •: 81.8 5.1 5.8 49.7 107 31.4 so 14 0.1 8.8 4.6 47.6 19.5 28600 9.3 1200 3840 9 3.7 15000 52400 1850 79400 13200 14900 10900 15100 108000 11700 25000 15900 18200 14900 5.2 5.9 3.9 4.3 0.3 0.39 0.96 0.52 1.3 1.2 0.6 0.74 0.48 0.37 1.1 4.1 0.46 0.68 25.21 77.5 89.1 11.4 6.5 1.4 12/20/2022 4 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 2000 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 7 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 10.2 1.2 2.5 e: Trichlorofluoromethane EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2640C Total Dissolved Solids SM 4500-CI-E Chloride ft Field Static Water Level November-20 pg/L EPA 300.0 Sulfate EPA 601OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Sodium Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane 1.5 91100 692000 78900t627OOO 597000 69100 29500 31000 682000 91700 299000 90900 69100 95200 160000 :�:�11 122000 153000 145000 93000 155000 �:I114 183000 too 230000 158000 237000 9990 50400 2120 53600 53100 7910 4370 8040 45400 10100 28000 39000 3830 43500 32.49 6.08 12.51 3.02 8.58 30.5 9.92 49.14 9.89 2.54 3.83 7.07 49.23 37.27 70300 589 189000 8100 8080 8940 2480 156000 23200 90400 7030 36600 4.8 8.5 5.8 5 291 317 273 201 57.3 139 55.8 193 60.2 87 95.9 292 256 41.1 0.78 0.45 0.48 5.8 4.2 6.5 6.1 32.3 .0 19.4 9.7 5.4 48 14600 8.41 1530 23803.5 5.1 4.5 7.8 5.5 15900 59400 2120 84800 13700 16500 11100 20600 77400 12700 18300 15000 19600 18900 4.6 1.8 0.51 3 0.64 1.2 0.58 1.7 0.57 2.4 0.34 0.95 0.66 0.65 12.9 13.4 90.9 69.6 1 0.611 1 5.4 0.66 1.6 12/20/2022 5 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 2000 pg/L 7 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L e: EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide ft Field Static Water Level May-20 feet Field Static Water Level pg/L EPA 300.0 Sulfate EPA 601OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Iron Manganese Nickel Sodium Tin Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Chloroethane cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane 1.5 1.9 90800 765000 81100 577000 35000 78900 25200 38900 535000 94700 174000 83400 66900 83500 153000 ��1� 146000 ��1� 154000 139000 76000 134000 :1�110 194000 337000 158000 146000 262000 9610 49300 1920 52700 15400 6510 4410 4770 30800 11100 14100 20700 3860 61400 6.3 82.2 32.15 6.97 14.24 4.91 9.51 31.8 11.96 49.5 10.88 3.22 4.61 7.76 49.85 38.23 32.82 6.69 13.01 4.85 9.3 32.51 9.37 50.28 10.43 3.37 4.55 7.87 50.1 37.81 76400 801 162000 7770 10400 9360 $II 22800 227000 6520 38300 5.8 290 309 257 176 56.5 136 52.9 238 66 98.1 224 196 241 23.8 0.72 0.62 6.8 5.6 4 8 31.4 3650 11300 21.1 74900 5640 1 0: 10805.1 8 211 125 4) 27410P 25700 7.9 1650 60 6410 10.61 80.8 27.4 3.9 16800 65600 2150 73800 17100 16200 12900 16200 148000 12400 28600 12600 17900 19700 4.8 7.1 5.5 0.65 0.69 0.52 0.66 0.46 0.9 0.56 0.48 0.56 0.29 0.85 1.2 0.84 0.91 0.52 1.1 2.4 0.72 0.46 0.34 0.53 38.6 11.4 70.5 130 8.9 1.1 5.6 1.3 1 12/20/2022 6 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 7 pg/L 1000 pg/L 1 pg/L 6 pg/L e: Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2640C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-S2D Sulfide November-19 feet Field Static Water Level mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 601OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Sodium Vanadium Zinc EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 2.2 1 86600 688000 70900 517000 35700 71600 25000 33900 635000 127000 333000 66400 65500 96500 172000 4011 146000 set 163000 165000 93000 130000 '1114 230000 too 126000 150000 269000 905 664300 3320 42100 14500 5910 4090 6370 63100 11000 29500 8400 3730 55500 80.1 242 66.72 15.74 33.96 13.87 20.93 67.7 31.66 101.3 23.17 7.2 9.75 16.76 101.22 77.94 2.77 0.66 0.49 0.44 8.53 1.54 6.83 9.03 3.07 0.34 4.3 4.35 2.1 2 0.22 5.4 4.45 5.56 1.48 0.24 0.85 3.81 9.63 6.35 2.3 1.32 1.32 2.57 5.35 6.15 6.23 6.03 5.88 5.35 5.17 5.48 6.14 5.84 5.97 5.39 5.27 6.08 137.5 -31.1 -80.6 51.7 127.7 126.9 115.7 143.5 -116.4 -91.2 58.2 164.7 109.51 57.9 111000 771 122000 8380 13000 7860 3610 M $$ 23900 99500 5450 40600 6.4 5.1 290 359 286 166 58.3 163 50.9 203 111 91.6 146 156 238 13.5 0.5 0.35 0.2 0.78 0.41 0.28 0.23 0.78 0.81 0.22 0.66 5.6 4 18.6 2.7 3.1 2.5 3.2 3.4 218 21.5 27 91.4 3.7 87.9 40.3 24.7 1.5 Be 21.1 . :1 1.2 • $ 7.4 3 1.6 1.3 4.2 5.3 of 11 1 4.3 6.9 1.5 • 6 1.6 1.4 2.8 6.1 6.3 12 16300 71900 2520 62300 14100 18400 10800 23400 138000 13500 17400 11500 18600 19900 3 1.6 1.8 5.1 4 1.3 1.6 1.5 4.3 24.5 5.4 5 4.2 5.1 0.6 1.3 12/20/2022 7 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 6 pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L Concentration 0.45 i Trip e 1,4-Dichlorobenzene Benzene cis- 1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance deg C Field Field Temperature May-19 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate 1.1 0.95 0.28 0.6 1.4 0.78 0.25 7 0.9 4.5 0.73 0.93 0.45 0.54 0.84 0.27 0.48 83 8.6 77.9 141 8.2 1.7 1 0.74 0.58 1.1 4 0.86 1.5 1.8 2.6 84000 736000 69800 384000 34300 82700 25300 39000 726000 102000 150000 58500 66600 91300 180000 St. :111 179000 set 169000 168000 78000 157000 : see 240000 369000 115000 152000 311000 9150 52500 2000 34000 14800 7500 3860 4190 71800 11400 17600 6310 3710 72100 6.4 192 221.9 1450 375.6 967 175.7 221.5 83 198.2 184.8 354.6 531.8 144.9 192.4 507.6 13 13.7 14.5 16.1 15.7 13.1 14.5 13.7 16.2 14.8 15.2 14.2 14.2 16.3 100.3 20.5 43.18 16.43 28.22 102.35 32.3 154.41 31.02 11.22 15.15 24.42 151.2 113.25 120 42 54 40 60 96 54 120 42 40 31.28 40 120 96 2.31 1.78 3.85 1.58 11.68 0.94 12.52 11.94 4.17 6.8 4.97 8.11 3.07 3.65 3.37 11.71 59.87 19.46 7.55 0.94 3.05 9.06 23.79 12.98 2.42 4.17 3 24.7 10.46 12.09 12.43 12 11.42 10.47 10.24 10.26 12.49 11.57 11.53 10.45 10.25 12.15 -193 -333.4 -293.4 -297.8 -81.6 -165.9 -65.1 -47.7 -603.7 -608.2 -469.8 -402.2 -219.3 111.2 85100 1210 163000 8620 12800 6560 235000 22300 149000 5910 45900 12/20/2022 8 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date W 21 Units 1000 •/L 11 • 1 • 11 •Nickel NE •/L 111 • • .111 • 11 • • 1 •/L 111 •/L NE pg/L 11111 . 1111 . 1 . pg/L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Copper-----------__- • Manganese - - Sodium:11 EPA 1 8260B Mod. ■ . . ■ . 8260D Acetone - - Chloride Tetrachloroethene Tetrahydrofuran-®-®----®----®__- 1• • romethane SM . Alkalinity,SM • 1 Dissolved Solids •- SM ' 11 - SM ` 11 ■NE Sulfide Field Field Specific Conductance deg C Field Field Temperature 1 feet Field Static Water Level Total Well Depth - 19.81 16.11 103 ----- 15.1 4.8 5.5 4690 8240 91800 6850 476---� 1130 -- -----®--®-__- 57.7 ®® 2320 20500 27500 1740 1990 2260 �� 374 110 __- 11� 11 111 - 11� 11 .111 :11 1 11� 'll 111 __- --llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ®®-®----------®__- ---------------__- 1.2EPA --------------__- -®- 5.1 --©-- 6.4 - 5.3EPA ---__- ---------------_�- --------------__- ------ 4.3 --------__- 1.4 -----------�-__- ---------------__- :11 111 �::111 •111 • 11 - 11 ..11 • 11 1.111 111 .111 :11 .=•11 ---------------__- 1150000 1040000 111 111 - • 111 1111 •1111 1110000 .111 1710000 111 111 `:111 _ 1111 - 11 . 11 lllllllllll-,,... . 11 llllllllllllllllllll,lllllllllll.�a...11lllllllli:��a..11lllllllll...r... 11 11 111 lllllllllll..�...11lllllllll.,..a.. 111 111111111111111,11111111111111111- ---------------__- ----®----------__- ---------------__- --------------__- 12/20/2022 9 of 47 A4 Facility Permit 34-12 ]Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mV Field REDOX Nmhos/cm Field Field Specific Conductance deg C Field Field Temperature November-18 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved 1.3 4.1 6.5 -91.7 386.3 15.1 70.39 14.9 33.24 16.3 21.77 60 21 27 20 30 0.4 1.6 1.5 0.8 5.5 23.01 1 6.6� 8.951 15.79� 103.891 77.51 21 20 15.7 20 60 48 12/20/2022 10 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 •/L 1 •/L 1000 •/L 11 • 1 . NE pg/L 3 pg/L 11 • 1.7 pg/L .11 . 88 pg/L NE • 11111 •/L Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 Sulfate Chromium-®--®---®®-----_�- Copper-----------__- Manganese Sodium EPA 1 . EPA 8151 EPA 8260B Methylene Chloride------ o-Xylene------®--®-----__- Tetrachloroethene Toluene Vinyl acetate EPA 8260B Mod. SM 1 : • • SM • 1 Total Dissolved . .s SM 1 1 ---------------__- 357000 1 11 11 ®. 1 - ••11 __- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllll®1 "" llllllllllll..w..11llllllllll�llllllllllllllllllll,lllllllllllllll,llllllllllllllll1- - 15.91 11.31 35 ----- 22 2090 00800 475 ---�®i 5030 28200 371 653 -_�- 8920 7940 584 24700 1620 336 170 115 11 111 .11 .11 off 1.11 ON:.11 11111111111111111,11111111111111111- ---------------__- 1.7 -----------__- 5.7 --------__- 0.88 -------------__- --------------__- ---------------__- . 11 111 111 111 .11 - 11 11 11 • 111 . 111 111 :11 . 11 :'•11 __- ---------------__- 726000 111•.111 .111 - 111 .:111 •111 1370000 111 1 111 111111 111 __- ---------------__- 12/20/2022 11 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date W 21 Units 1111 . NE pg/L 1111 . 1 ./L 111 ./L 11 • 1 . • 1 •Thallium Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 •- SM ` 11 SM ` 11 Sulfide Field Field Specific Conductance deg C Field Field Temperature May-1 8 feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 - EPA 6010 Arsenic--®------------__- Copper©----------©__- - - • , • .. . 1 1 : EPA 1 ` 8260 • - - ---------------__- ---------------__- --------�,�,.},�-------__- 1 111 1111111111111� 1 11 �- 11 ®':1 - 307000 11 . ` 11 �- ' . 11 ---------------__- - 20.5 11 10.4 ----- 18 -----__- ®lm 4260 84300 3980-®�® 3300 27300 ®®1. 453 10300 8100 •11 357 --��� 17500 1580 95.5 �� 507 11 lllllllllll" 11 : 11 : 1 1 llllllllllllllllllll, .. 1 1 llllllllll®" 1 1 1 11 1 1 1 1 ` 1 1 lllllllllll� .• 11 1 1 1 111111111111111,11111111111111111- --- 10.3----------__- ---------------__- --llllllllllllllllllll, 1 1 llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- ---------------__- ---------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- 12/20/2022 12 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 6 pg/L 0.41 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance oC Field Field Temperature December-17 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 8260 1,1-Dichloroethane 7 0.72 1.7 16.4 0 441 0.55 0.45 0.71 0.55 0.85 0.23 1.2 3 1.7 0.68 1.7 2.4 0.65 0.78 46 24.9 192 5.9 14.8 0.93 1.2 1.3 0.89 0.79 0.42 76100 663000 115000 101000 33600 75900 27000 31800 506000 130000 65800 47200 61800 112000 166000 :::III 177000 250000 164000 181000 75000 133000 9111 232000 218000 107000 152000 369000 9040 42200 2180 12500 15200 6490 3660 4830 158000 12500 11100 4790 3930 89700 5 4.8 4.4 4.8 4.2 105 240 221.7 1391 423.5 343.9 176.7 234.9 70.7 155.8 1840 349.9 304.2 121.8 183.9 641 22 17.2 18.7 18.2 17.3 17.8 16.5 18.9 17.4 17.9 17 16.2 19.1 16.9 35.1 8.3 21.15 9.44 11.5 37 18.55 52.94 12.18 4.14 5.46 9.09 5209. 39.58 60 21 27 20 50 48 27 60 21 20 15.7 20 60 48 3.3 0.4 0.5 0.6 5.1 1 4.5 6.2 0.1 0.1 0.3 1.3 2.9 2.3 2.8 2.4 9.4 9.6 4.2 3.5 9.7 9.6 7.8 9.8 9.7 9.7 7.4 2.7 5.6 6.4 6.4 6.1 6.1 5.6 5.7 5.7 6.4 6.1 6 5.8 5.6 6.1 112.4 -38.8 -37.4 100.2 106.5 78.2 169.8 132.7 -50.6 43.9 163.2 216.5 150.5 105.1 0.54 1.6 12/20/2022 13 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units pg/L 1 • 111 •/L 11 • 11 • 1 •/L 111 •Tetrahydrofuran • 11 •/L 111 • 0.03 . 1111 • 1 • 1pg/L •/L 11 • Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Carbon Disulfide Dichlorodifluoromethane--------®----®-__- - - Tetrachloroethene Tolu_ ' _ • • • • - - - Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved INITU Field Turbidity Std. Units Field Field pH Mv Field REDOX ` 300.0 ` 6010 Chromium®-® Cobalt 2.5700 -----------__- --------------�__- ------®--®-----__- --------®-----__- 1.5 -------------__- -®-------®-----__- --------------__- ®®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- 1.4 -------------__- EMT, M., --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,---__- 111 - 'lll�- ll�- .� 11 . 11 •11 �- '.11 __- ---------------__- --------------__- 10.2 --®�----_®- 23.5 3010 9.4 78700 93 365 ----- 22.5 3270 -----__- 29300 1050 __- 12/20/2022 14 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date w 2L Units 15 pg/L 50 pg/L 100 pg/L NE pg/L 7 pg/L 1000 pg/L 1 pg/L 50 pg/L 70 pg/L 0.3 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L Concentration 3.4 iEQBL Trip FBA Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8151 2,4,5-TP (Silvex) 2,4-D Pentachlorophenol EPA 8260 1,1-Dichloroethane IA-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 Butylbenzylphthalate SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance 11.8 � 20.3 1 7.5 4.2 43 3.6 10.6 7.6 17.9 18.4 15200 77600 2380 65500 13500 15300 9860 14900 138000 12300 13200 9740 17100 19800 539 4.9 3.6 5.8 5 5.3 7.1 0.23 0.072 0.27 0.018 0.48 1.4 0.46 1.1 12.1 0.38 0.52 0.44 0.62 0.6 1.1 0.23 1.2 3.9 1.4 1.1 0.68 0.97 28 20.1 131 0.93 1.5 1.6 1.2 0.52 0.87 0.71 1.7 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 153000 :III 164000 :. 1Ol 144000 175000 82000 136000 ���� 218000 219000 90000 142000 370000 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 127 208.3 1393 394.2 1209 176.8 288.4 77.4 160 1989 348.3 299.8 111.4 172.7 624 12/20/2022 15 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 . 11 . 1 .Chromium---------® 11 • 1 .Manganese, 11 • NE •/L 1 • 111 • 1 • • pg/L 1 . • 11 •/L 11 • • 11 • Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 oc Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 - EPA 6010 .• - Sodium ' 8260 • - • • - - Carbon Disulfide Chloromethane . . - - Ethylbenzene - - Toluene SM 1 : ---------------__- 1111 - 111 ----- 333000 11 ---------------__- -®-®-----® 1 ----__- ----__- - 20.6 3870 - - 59.9 302 ----- ----- 21.8 2400 26700 ----__- ----__- 9200 - 801 ----- ----- 8390 1720 -----__- ----__- 1 ----__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll, 1 1 11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --------®-----__- ---------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- -®-------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- 2.1700 -------------__- ------------__- --------------__- --------------__- ---------®-----__- ---------------__- 12/20/2022 16 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units NE pg/L 00rirTotalDissolved 0rir pg/L r . NE pg/L r r Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Alkalinity, Total as CaCO3 SM r Solids SM r Chloride Field Field Specific Conductance oc Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX - • 300.0---------------__- - • 6010 Copper Sodium EPA 8260 ---------------__- ---------------__- 796000 - 552000 ----- 1150000 •��� ----__- 318000Field �� ----__- ---------------__- --------------__- 89300 --®---- 714 1740 ®- 6460 --- 51.9 134 359 llllllllll1MI '� I lllllllllllllllllllll,llllllllllllllllllll, off I11� off .•�I .��111111111111111,11111111111111111- ----------- r r' • __- ---------------_�- ®------®---®-�_®- 12/20/2022 17 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 10 pg/L 700 pg/L 21.4 18.4 15.7 15.8 12.1 17.3 14.7 13.2 18.7 e: 18.3 Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2640C Total Dissolved Solids SM 4600-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance oC Field Field Temperature November-16 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mV Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium 0.43 0.4 0.38 1.1 1.5 3.6 1.2 0.46 0.61 32 11.4 12 0.91 1.4 1 2.1 68600 114000 32300 85000 20800 25400 64500 42400 F55300 98100 165000 133000 156000 175000 67000 141000 288000 89000 410000 8860 2520 15100 5290 3060 4610 19700 4310 3260 104000 4.4 4.4 9.9 4.3 209.7 392.9 175.5 220.7 68.1 159 367.4 116.5 173.7 690 20.3 20.4 21.2 19.7 17 19.8 17.4 16.9 18.4 17.6 68.82 16.64 20.47 17.87 22.26 36.41 34.35 104.13 24.2 8.77 10.74 18.41 103.03 39.3 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.52 1.18 2.9 3.5 5.73 1.2 7.7 8.26 1.16 4.39 1.34 4.6 4 3.19 0.72 1.51 5.3 7.03 0.31 0.25 0.31 4.61 6.38 5.81 2.97 7.23 1.95 44.5 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6 5.9 5.7 5.6 6.4 137.2 24.1 -61.4 176.7 242.9 152 217.5 272 62.3 16.7 175.1 241.4 270.5 177.6 1380 121000 1530 193000 8450 3800 4090 3440 M 17100 129000 5390 1400 58700 3.9 2.6 241 2721 297 255 55.9 140 44 195 148 93.1 144 91.6 188 14 12/20/2022 18 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 7 pg/L 1000 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 10.58 TV 0.57 e: Beryllium Chromium Cobalt Iron Lead Manganese Nickel Selenium Sodium Vanadium Zinc EPA 8081 Heptachlor Heptachlor epoxide EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Carbon Disulfide Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance .0 2.8 5.8 4.1 6.4 96.2 •: 86400 3.5 , 149 1 2.6 11 274 123 7.3 1 •18.5 1 1 8 35.6 2.7 8.5 11 10.7 1 6.2 26.7 13.7 5 14600 70200 2450 71000 14200 16200 9700 15700 184000 12000 19200 9380 16200 20200 5 5.7 8.4 7.3 5.7 5.1 12.8 6.3 1 1 0.53 1.5 0.39 2.5 14.1 25.4 0.38 0.42 0.83 5.2 0.44 0.4 0.2 0.47 1.1 0.33 0.62 0.88 2.3 0.38 0.55 2.2 2.1 0.63 2.1 0.48 39.1 13.6 21.7 237 26.8 16.8 1.2 1.5 1 2.8 0.58 4.4 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 154000 111 168000 R.X, g11 145000 153000 67000 135000 1 1111 189000 286000 79000 118000 371000 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 3410 98000 5.4 202.81 12621 380A 1204 176 203.1 73.7 167.8 2535 355 463.1 106.2 158.E 609.9 12/20/2022 19 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 1111 • 1 . 1 ./L 11 ./L 1 ./L 11 • 1 . NE pg/L 2000 . Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX • 8260 Chloride Field Field Specific Conductance Field Field Temperature feet Field Water Level .. 300.0 .. 6010 Antimony Chromium Cobalt Iron Manganese Sodium ------ 3.7Static --------__- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ---------------__- 1 : 1 111 : 11 • : 11 ®llllllllllllllllllll,®®llllllllllllllllllll, : 11 11 . • 111 ®llllllllllllllllllll, 11 111111111111111,11111111111111111- ---------------__- 4.7 -------------__- --®------®-----__- 18 10.2 10.5 ----- 3.1 -----__- 13.6 --__- 4360 77200 1550 ------ 11800 19.1 29400 ----__- 312 11000 312 ® 10900 6800 515 ®------®�®-__- 530 1820 90.8 284 116 __- ------------__- 009976M 61500 231 1 Iff 11 1111111111111111111111, .'11® 11ME 1 11 11 • 11® '11 1 ---------®--®--_®- ---®®---- 20 -- 22.6 --__- 12/20/2022 20 of 47 A4 Facility Permit Qualifier 1000 pg/L Zinc EPA 7470 1 pg/L Mercury EPA 8081 40 pg/L EndosulfanI EPA 8260 6 pg/L 1,1-Dichloroethane 1 pg/L Benzene 70 pg/L Chloroform 70 pg/L cis- 1,2-Dichloroethene 1000 pg/L Dichlorodifluoromethane 500 pg/L m&p-Xylene 3 pg/L Methylene Chloride 500 pg/L o-Xylene 0.7 pg/L Tetrachloroethene 2000 pg/L Tetrahydrofuran 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.03 pg/L Vinyl chloride SM 2320B NE pg/L Alkalinity, Total as CaCO3 SM 2540C 500000 pg/L Total Dissolved Solids SM 4500-CI-E 250000 pg/L Chloride SM 4500-CN-E 70 pg/L Cyanide December-15 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field 34-12 Old Salisbury Road Landfill (C&D) (Multiplelte Historical detections by date 5.9 ® 4.4 3.4 3.2 - 9.5 6 - 1.3 -------------__- 0.72 :161 769000 ::111 , 111 ,111 - 111 W. 111 E 1 111 111 .111 : 111 111 W. 111 W, :111 --- 5.11 4.71 4.2 4.11 4.1 12/20/2022 21 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 . /L ' 1 . 11 . 1 .Manganese' 11 . 1 . NE pg/L 1 . 2000 . Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Field pH mv Field REDOX Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units FieldField. mv Field ..®wwwwwww®w®®ww��� - • 300.0 - - • 6010700 Barium Cobalt . " - Sodium EPA 1 .. 8081 ��wwwwwww■�wwwww��� ®�ww®wwww�®wwww��� ��©wwwwww�wwwww��� --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,---__- ---------------__- ��wwwwwww�wwwww��� ---------®----�__- 17.4 9.1 3080 68200 28.3 2.5 312 32600 ---- -- 3.1 2.9 3690 34600 ----__- 523 790 466 8180 -�-® 9010 7100 407 1890 -�®� ----®-®-�®__- 587 2020 62.1 69.3 297 __- ---- ---------__- 11 . � 11 111111111111101 :11MR11 llllllllllllllllllll, 11 � 11 •:11 111NKRF11 1109.11 :11111111111111111,11111111111111111- ---------- 8.8 --------------__- 11.9 9.9 18.9 ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ---------------__- 12/20/2022 22 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 40 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L NE pg/L 200 pg/L 0.005 pg/L 100 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L e: Endosulfan 1 Heptachlor Heptachlor epoxide EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 2,4-Dinitrotoluene 2,6-Dinitrotoluene Benzo(g,h,i)perylene Dibenz(a,h)anthracene Di-n-octylphthalate Indeno(1,2,3-cd)pyrene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance •C Field Field Temperature May-15 7n.,, 09916 0.38 2.6 11.8 0.44 0.25 0.26 0.8 0.26 1 0.76 0.23 2.1 0.4 1 0.841 0.68 1.31 2.3 1.2 2 1.1 0.27 0.43 35.8 7 17.7 120 19.8 0.27 0.66 1 1.4 1.1 0.82 0.54 4.8 1 5.9 8.1 1 5.6 5.6 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 78000 :=IjI§ 137000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 7.5 5.1 4.7 9.8d4.2 5.3 5 5.3 163.2 1044 211.4 395.9 164.5 1966 58.4 151.5 365.1 281.5 1089 1521 596.2 16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 16.2 16.2 16.3 15.6 12/20/2022 23 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 . 11 • 1 .... 11 •/L NE •Sodium 1 . 111 • 1 • 1 • 1 • 1 ./L 1 . .11 •/L 11 • 1 ./L Concentration MW-1R MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 - 6010 Cobalt20.3 .•• er ' - Nickel-----®---�®__- EPA 1EPA 8151 - ` 8260 Chloroform--------------�__- Chloromethane . . - - Ethylbenzene Methylene _ o-Xylene------®--®-----__- Tetrachloroethene 1EPA lllllllllll•nn.•'lllllllllll..�... ' 11111111111111111,11111111111111111- 10.1 15.2 ----- 4.8 2.5 9560 56000�®_-_-_�_-_ 3650 31400 524 1400 695 10600 11900 7980 315 736 1990 271 1 11 11 1 11 __- 5.1 -------------__- 11.4 8.8 -®----®®-®- 24.7 __- -®----®--®-�__- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- -®-------------__- -------------__- ---------------__- --------------__- 1.7 -----------__- --------------__- --------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®®- 1.2 -------------__- 12/20/2022 24 of 47 A4 Facility Permit 34-12 ]Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 10 pg/L 700 pg/L Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride pmhos/cm Field Field Specific Conductance 'C Field Field Temperature November-14 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mV Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium 1 34.6 1 5.8 11 14.11 1 1451 1 1 16.9 0.63 0.79 1.5 0.79 0.98 0.22 0.59 4.4 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000 19200 36900 45200 9150C 133000 . IjI1 182000 304000 166000 145000 61000 134000 279000 239000 163000 107000 131000 36000C 7640 44200 2990 22200 15700 4340 1960 4290 51800 14400 8070 3760 3510 9820C 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8 234.3 115 150.1 611 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4 14.9 18.7 17.1 17.3 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.8E 1 0.51 6.3 0.5 5 0.5 2.3 8.3 0.51 0.5 0.5 3.8 1.2E 1.7 3.53 5.2 10 3.6 1.2 9.1 2 98 9.9 5.2 152 7.8 20.1 5.6 6.1 6 5.9 6 5.6 5.7 5.5 5.1 5.9 5.9 5.6 5.6 6.2 194 38 13 158 198 184 224 252 198 -61 101 232 242 182 1720 117000 3740 143000 8180 1360 2100 12800 32800 8660 4380C 2.6 3.5 142 339 221 305 58.2 111 38 193 262 96.8 59.2 130 193 41.5 12/20/2022 25 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 7 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L NE pg/L 1 pg/L 3000 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 1.4 1.2 0.6 e Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Benzene Chloroethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance •C Field Field Temperature May-14 feet Field Static Water Level Total Well Depth mg/I 3.4 4.8 3 4.5 9.6 3.8 4.8 85.8 11 2.7 126 221 76.5 55.9 1 4.1 3.6 1 5.4 1 233 2.9 •:: : • I I 2.6 22.9 19.9 1.6 1 33 25.9 7.2 4.1 5.3 10600 58300 2770 55400 13700 16600 7810 14600 6860 10000 12800 10700 14400 24000 2.8 2.7 5.6 3.6 5.5 16.8 7.2 5.3 6.2 13.7 13.3 5.3 0.33 1.1 1.3 0.4 2.2 0.42 0.44 2.1 0.5 0.73 0.35 0.73 1.1 1.1 0.33 2.9 0.36 0.65 79.2 15.9 8.8 106 15.5 0.85 2.4 1.2 0.96 0.57 3.9 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 40500 36200 42300 54700 120000 fit 191000 .• sit 163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 4.4 4.2 10.4 4.3 5.1 260 1301 151 138 1150 363 971 184 186 59 161 106 440 203 120 159 647 14.8 13.2 13.2 13.7 12.9 13.7 13 12.4 15.3 15.4 15.4 13.8 11.9 16.7 70.78 14.24 37.86 14.47 2022. 74.12 26.82 52.72 11.34 8.55 9.77 17.91 103.61 76.95 60 21 27 20 30 37.051 271 60 21 20 15.58 201 60 50.85 12/20/2022 26 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date W 2L Units 250000 pg/L 1 pg/L 10 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 1000 pg/L 1 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L Concentration i Trip e Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Antimony Arsenic Barium Chromium Cobalt Iron Manganese Nickel Selenium Sodium Zinc EPA 7470 Mercury EPA 8260 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4600-CI-E Chloride pmhos/cm Field Field Specific Conductance .0 5.3 4.8 6.3 6.2 8.6 3.8 8.4 8.7 8.3 7.5 8.4 6.8 8.1 5.4 3 11 6 17 10 6 8 5 4 22 15 147 118 50 5.6 5.8 6 5.7 5.7 5.3 5 5.2 5 6 5.9 5.6 5.5 6.3 411 243 146 374 389 363 389 436 436 27 315 367 437 406 136000 4230 85200 8060 10700 48000 8680 59500 8.9 124 324 205 264 54.4 90.8 30.7 168 132 94.3 61.1 77.1 163 8.6 5.6 52.9 i 123 2321 142 292 20.6 6.1 15.5 10.9 14.6 34.1 40.2 34.7 16.5 11.5 10800 59700 39700 13600 14200 6160 12400 8490 11000 11200 12800 24200 11.4 17.2 11.7 0.51 0.83 0.81 0.28 0.49 0.38 0.37 0.31 1.1 72.6 11.8 5.2 18.6 21.4 0.71 3.7 0.62 0.47 0.2 0.32 0.34 5.3 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 91000 11� 187000 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 5600 50500 3260 29700 13900 3600 1800 3610 1820 12400 6180 3880 3630 83400 1371 10401 171 64 155 86 430 243 149 156 623 12/20/2022 27 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date W 21 Units 1111 . 11 . 1 • 11 . NE pg/L 1000 . 1 . 1 ./L 1 . 111 . 3 pg/L 11 . 1 ./L 111 • 0.03 . NE • Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 EPA 6010 Cobalt . Manganese Sodium EPA 8151 - EPA .1 Chloroform--------------�__- • . - - - Dichlorodifluoromethane Methylene Chloride - - Tetrachloroethene • - - •chloride• SM 1 : Alkalinity, Total• SM 1 ---------------__- :11111 111----- 1�1111 �- 11 __- ---------------__- - 19.2 766 53.5 31300 49.4 ------ 47.5 32100 ----__- ® 1330 915 -® 8710 9990 688 ®-----------__- 1920 86.1 110 1 1 1 1 1 1 1 1 1 111111111111111,11111111111111111- -®------------®__- -------------__- ---------------__- 1.9 ------------__- ------------__- --------------__- 3 -------------__- -------------__- 2.2 -------------__- -®-----��----�__- ---------------__- 0.95 -------------__- 11 �•111 111 �111 11 - .11 11 :�11 . 11 . 111 11 11 :11 . 11 __- ---------------__- 12/20/2022 28 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 11111 • 1111 • 1 • 250000 • •/L 111 • 11 • 1Manganese, • NE •/L 111 • •/L 111 • Concentration MW-1R 1 111 MW-2R 654000 MW-3R • 111 MW-4R '•.111 MW-5R 'lll MW-611 - MW-7 .111 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 11 ■ - SM • • •- SM ' 11 Field Field Specific Conductance oc Field Field Temperature May-1 3 feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX .. 300.0 - .. 6010 Cobalt •••- . Sodium•1:1 Vanadium ' 8260 ■ • - - . 111 'lll ..111 .111 .111 ' 111 111 1111 _-- --------!�-------__- 11 11 11 llllllllllllllllllll,llllllllll�lllllllllll�n....11lllllllll.�n...11llllllllll�.�... ' 111 lllllllllll..�... 11 11 ' 111 111111111111111,11111111111111111- ---------------__- --®®---------�®__- 1 1 1 1 1 •. 1 1 1 1 llllllllllllllllllll,llllllllllllllllllll, 1 1 1 1 lllllllllllllllllllll, 1 1 1 : 1 1 ®llllllllllllllllllll, 1 1 111111111111111,11111111111111111- ---------------__- 18.2 64.1 35.3 ---------®-__- ------ 65.1 - 6.6 --__- 877 34100 867 30700 324 8610 5820 4140 7880 96301 496 1890 ® 158 240 160 __- 11 .11 111 - 11� •11 -� 11 11 11 . 11 __- --®------------__- -®��--------®�®__- 14.6 9.9 8.6 __- ---------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- 12/20/2022 29 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 40 pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 500 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 500 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Concentration 0.48 Trip e 2-Hexanone Acetone Benzene Chloroform cis- 1,2-Dichloroethene m&p-Xylene Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance oC Field Field Temperature November-12 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH 20.3 0.63 0.26 0.72 0.96 1.3 0.54 0.27 111 8.5 24.2 7.4 0.68 12.1 0.25 0.36 0.38 4.3 1.2 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000 29600 58700 35600 78900 84000 ,-111 175000 413000 131000 108000 51000 100000 46000 228000 138000 87000 102000 442000 5910 50000 3860 33700 16200 5340 2070 4300 2040 14200 5820 3820 4290 124000 8.1 5 68 802 217 382 116 106 31 88 43 400 197 136 81 403 20.9 19.7 15.7 15.6 15.2 16.3 17.5 18.1 16.3 14.7 14.7 16.5 18.2 17.9 72.24 17.78 45.36 19.26 22.81 77.49 37.56 105.53 25.13 8.94 10.71 18.71 104.68 79.91 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5.5 1.5 1.2 2.3 6.4 1.8 9.8 7.3 4.4 0.9 3 2.3 6.4 2.3 1 1 25 14 14 7 1 1 1 25 1 605 329 456 5.71 5.81 5.6 5.7 5.8 5.4 5.7 5.5 5 6.1 5.9 5.5 5.5 6.5 12/20/2022 30 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 . 1 . 11pg/L 1 . 1000 . 11 . 1Manganese, . 11 ./L pg/L 1000 . 1 . 0.002 1 1 1 •/L • . 111 • 1 •/L 3 pg/L 11 • 1 ./L 111 • 11 • 0.05 . NE pg/L 11111 ./L Concentration MWAR MW-2R MW-3R MW-411 MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 mv Field REDOX EPA 300.0 EPA 6010 Barium Cobalt ••- . NickelNE Sodium•11 EPA 8081 ■ ■ ■ Dieldrin Heptachloepoxide ' 8260 ■ • - - - Chloroform------------�__- Methylene Chloride - - Tetrachloroethene • • . •)80EPA : - . SM 1 : Alkalinity, Total as CaCO3. SM 1 Total Dissolved . . SM 1 1 --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,---__- __- ---------------__- --------------®__- ------------ 11.8 15.2 - 35.5 --------���__- 1730 25300 344 .1 29000 1430 11300 4520 12300 __- 8400 11600 541 1740 301 251 317 __- - .11 11 - '11 ®' '1 11 �� 111.11 111 11 __- ------------ -®-----®--��®®�__- 18.7 8 28.6 ---------------__- -------------- 1 1 . 0.11 --------__- ------ 0.12 --------__- ---------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- 1.3 -------------__- ------®--------__- 4.5 -------------__- -------------__- 1.8 -------------__- -----��----�__- 1.4 --------------__- 13 ---- 9.8 -__- ---------------__- 11 111 111 �111 11 - •11 11 11 11 111 �1 11 •11 :•11 .11 __- ---------------__- 111 564000 111 111 111 - 111 :111 :111 . 111 1111 111�111 111 •:111 __- ---------------__- 12/20/2022 31 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 1111 . 1 . NE pg/L 1111 . 1 ./L 1 ./L 11 • 1 • 11 • 1 • NE pg/L Concentration MW-1R MW-2R .�111� MW-3R MW-4R 11 MW-5R 11 MW-611 -�� MW-7 MW-8 MW-9 MW-10 :11 MW-11 •11 MW-12 �•11 MW-13 �� MW-14 MW-15 111 Trip Blank _-- EQBL FB-1 •- SM 11 - SM 11 Sulfide Field Field Specific Conductance oc Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 - EPA 6010 Arsenic--------------®__- Chromium----®---------®__- .• ,.. - - Sodium® ---------------__- --®------------__- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllll•.....11llllllllllllllllll, 11111111111111111,11111111111111111- ---------------__- ' 111 lllllllllll�"' 11 ' : 11 lllllllllll�llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll, ' 11 1 11 lllllllllll�llllllllllllllllllll, : 11 111111111111111,11111111111111111- ---------------__- - 14.8 16.4 21.5 ---------- _- 3190 41500�®i' -_-_�_-_ 26300 1580 539 3760 91.5 1140 1701327 10000 -® 8280 9310 370 ----------® 1 _- -®�----------- _- :�1111111111111111111111, �1�11 11- 11® .11111111111111111111111,® .11 11 11 11111111111111111,11111111111111111- 12/20/2022 32 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 21 Units 111 • 1 • 1.1 pg/L 1 1 1 • 0.006 . 0.019 0.004 ./L • 1 • 3 pg/L 11 . 1 •/L 111 •/L 111 • 0.05 • 0.05 . NE pg/L 11111 • 250000 • 1 •Cyanide NE pg/L Concentration MWAR ------------ MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 7.2 MW-14 - MW-15 23.4 Trip Blank EQBL -- FBA EPA 8081 ■ • ■ 4,4'-DDT Aldrin - Heptachlor epoxide EPA .1 Methylene Chloride - - Tetrachloroethene Tetrahydrofuran-®------®----__- EPA • 1 - - - - - - SIM 1 Alkalinity,SIM • 1 11 ■ - SIM • • •- SIM 11 SIM 1 1 ■ Sulfide Field Specific Conductance oc -®----------�- _- -------------- _- ----- 0.13 ------- _- 0.54----__- 0.12 0.12 -------------__- 0.18 - 0.069 -----------__- ------ 0.066 --------__- ---------------__- 1.5 -------------__- --------------®__- 3.2 -------------__- -------------__- 1.7 -------------__- ------------®__- ---------------__- ------------ 1 --__- -- 5.5 ------------__- ----------- 1.2 1.5 --__- ---------------__- 11 •.111 1111 11 �111 - 1 11 1 11 1 11 111 1111 11 11 1 11 ---------------__- • 111 531000 .:111 �111 �•111 - 1.111 111 111 �•111 111 1111 1111 111 .1111 __- . 1 1 llllllllllllllllllll, 1 1 1 1 llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll, 1: 1 1 1 1 lllllllllll•�.•.•'llllllllllllllllllll, . 1. 1 1 111111111111111,11111111111111111- ---------------__- --®------------__- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111-Field --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111Field - 12/20/2022 33 of 47 A4 250000 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L NE pg/L 7 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L Facility Permit Qualifier Field Temperature December-11 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Chromium Cobalt Iron Manganese Sodium Vanadium Zinc SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride pmhos/cm Field Field Specific Conductance oC 34-12 Old Salisbury Road Landfill (C&D) (Multiplelte Historical detections by date 3.81 131 13.9 9.33 11.2 20 30 401 90 5.91 5.7 1 2181 1 1 1751 2001 1 1 1 1 1 1 1 1 1 1 1 1 618001 7020 3281 85.2 43.5 35300 13300 15.3 143000 32800 345000 139000 29200 16400 4901 177 12/20/2022 34 of 47 A4 Facility Permit 34-12 ]Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 7 pg/L 1000 pg/L 6 pg/L Field Temperature November-11 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Silver Sodium Vanadium Zinc EPA 8260 1,1-Dichloroethane 15.4 12.5 15.2 36.52 16.58 44.06 9.04 11.1 21 27 1.7 3.1 1 4 5.9 6 95 71 96300 351 237 20.9 5 31800 33.3 1.2 97.1 151 21 0 1411 91 3000 3030 6140 2050 9980600 12700 1 . 31.61 12 12/20/2022 35 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 6000 0 ./L NE pg/L 00000 .Total. Concentration MWAR MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Acetone-®-------------�®- Chloride Tetrachloroethene Alkalinity, Total • . Solids.:r�� Field Field Specific Conductance Field June-11 Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH MV Field REDOX EPA 350.1 2 3.5 -------------_ 3.2 - 1.8 -------------__- '��� rrr --- rr •.r� �r �r rrr � �� rr �-�� -__- :rrr --- rrr rrr :err :•��� rrr ��r •rrr :��� -__- 12/20/2022 36 of 47 A4 NS pg/L NE pg/L 1 pg/L 0.7 pg/L 2000 pg/L NS pg/L NE pg/L 250000 pg/L Facility Permit 34-12 ]Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date EPA 6010 Sodium EPA 8260 Benzene Tetrachloroethene Tetrahydrofuran RSK 175 Methane SM 2320B Alkalinity, Total as CaCO3 SM 4500-CI-E Chloride pmhos/cm Field Field Specific Conductance oC Field Field Temperature May-11 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field 27200 274 1280 165000 39900 698 19.1 35.93 8.17 20.56 8.34 10.44 37.99 15.08 51.11 11.72 4 4.91 8.85 51.45 60 21 27 20 19.56 48 27 60 21 20 15.58 20 60 6.3 3.9 6.3 5.3 9 3.2 8.7 7.3 7.1 4.3 7.4 5.2 7.8 55 57 70 96 85 40 18 1 4 23 25 177 39 12/20/2022 37 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date w 21 Units 11 . .111 . • 1 • 1 • 11 • 3 pg/L 11 • 1 ./L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FBA Field pH MV Field REDOX EPA 6010 ` 8260 - - Acetone • - - - • Methylene Chloride o-Xylene------------__- Tetrachloroethene Field Field Specific Conductance Field Temperature '' 'feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field TurbidityStd. Units Field Field pH MV Field REDOX ` 6010 ---------------__- ---------------__- --------------__- --------------__- 1.3 -------------__- -------------__- ------------__- ----®--------__- 4.1 -------------__- 1.4Field -------------__- ©�' IIIIIIIIIIIIIIIImlllllllllllllllliiL©llllllllllllllllllll,®llllllllllllllllllll�llllllllllllllllllll�llllllllllllllll�llllllllllllllllmllllllllllllllllllll� 11 llllllllllllllllli711111111111111111111,111111111111111,11111111111111111- ---------------__- 12/20/2022 38 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 1 . Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 8260EPA Chloride Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX ' 8260Field Field Specific FieldField Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field 4.2 -------------__- ---------------__- --llllllllllllllllllll,111111111111111111111111111111111111111111,111111111111111111111111111111111111111111,111111111111111111111111111111111111111111,111111111111111111111,111111111111111111111111111111111111111111,111111111111111111111111111111111111111111,1111111111111111111111111111111111111,11111111111111111- �■��w��������■�w���� 12/20/2022 39 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units Concentration MWAR MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Turbidity I Std. Units Field Field pH MV Field REDOX EPA 6010 EPA 8260 Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH MV Field REDOX Field Field Specific Conductance Field Field Temperature feet Field Static Water Level 12/20/2022 40 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date W 21 Units 700 pg/L r Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FBA Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH MV Field REDOX EPA 6010 ChlorideEPA 8260 Carbon Disulfide . Trichlorofluoromethane Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH MV Field REDOX EPA 6010 EPA 8260 ---------------__- ---------------__- 12/20/2022 41 of 47 A4 700 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 20 pg/L 20 pg/L 70 pg/L Facility Permit Qualifier pmhos/cm Field Field Specific Conductance oC Field Field Temperature December-08 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved Std. Units Field Field pH mV Field REDOX pg/L EPA 6010 Arsenic Barium Chromium Lead Selenium Silver EPA 8260 Chloroform pmhos/cm Field 34-12 Old Salisbury Road Landfill (C&D) (Multiplelte Historical detections by date ------------- 40.2 26.2 -__- -__- 12/20/2022 42 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple ltel Historical detections by date 2L Units 4000 . 6000 Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FB-1 Field Specific Conductance Field Field Temperature Static Water Level Total Well Depth FieldField Field Oxygen, Dissolved Std. Units Field ' mv Field REDOX EPA 6010 EPA 7470 EPA 8260 . . Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field m��w mow ■ Vfeet ---------------®_- 12/20/2022 43 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date w 21 Units 4000 1 • Concentration MW-1R MW-2R MW-3R MW-411 MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FBA REDOX Field Field Specific Conductance Field Field Temperature April-07feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX Selenium Field Field Specific Conductance oc Field Field Temperature feet Field Static Water Level Total Well Depth Field ---------------_�- -- 24 ------------__- 12/20/2022 44 of 47 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiplelte Historical detections by date w 2L Units Concentration Std. Units Field Field pH mv BariumOxygen, Dissolved Field REDOX Cadmium-- Field Field Specific Conductance Field Field Temperature Barium 10 Chromium Lead EPA 6010 700 Barium 10 Chromium 15 Lead EPA 7470 1 Mercury EPA 8260 Chloromethane 700 Barium 10 Chromium 20 Selenium 10 Arsenic 700 Barium • MW-1R MW-2R MW-3R MW-411 MW-5R MW-611 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL FBA 2 ------------__- ------------ 35 -__- ------------- 23700 -__- 1515 -__- 5.4 ----------__- �a- _�---------__- 12/20/2022 45 of 47 2L Units Concentration Trip MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank EQBL FBA -------- 14 13 ®-®---� 22 14 26 28 18®-- 41 2.7 820 150 24 lirl 100 140 13 86 65 41 210 1.9 2.3 2.1 5 7.4 3.2 32 6 6 7.4 130 100 370 61 150 180 84 1 5 15 23 26 6.8 21. 7.6 5.8 8.4 12 7 16 1 280 160 400 900 610 530 130 22 16 19 95 140. 95 27 A4 12/20/2022 47 of 47 This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports Appendix Laboratory Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports This page intentionally left blank. leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 12, 2022 Mark Filardi HDR 440 S. Church St Suite 900 Charlotte, NC 28202 RE: Project: OSR LANDFILL Pace Project No.: 92636049 Dear Mark Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Ormond Beach If you have any questions concerning this report, please feel free to contact me. Sincerely, Sara Poulson sara.poulson@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Joelle Giesler, HDR Charles Gruenberg Zach Hector, HDR Mike Plummer, HDR Brian Spillane, HDR Ben Weiserbs, HDR �pQ ACcr?FO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, 9e0 without the written consent of Pace Analytical Services, LLC. Page 1 of 165 lacieAnalyfical'f' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Pace Analytical Services Ormond Beach 8 East Tower Circle, Ormond Beach, FL 32174 Alaska DEC- CS/UST/LUST Alabama Certification #: 41320 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maine Certification #: FL01264 Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification M PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 CERTIFICATIONS Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 New Hampshire Certification #: 2958 New Jersey Certification #: FL022 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 North Dakota Certification #: R-216 Ohio DEP 87780 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FLO1264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification #: CERT0086 Nebraska Certification #: NE-OS-15-05 Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate M 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification M TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Pace Analytical Services National Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21-A 2926.01 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS A2LA-IS0 17025 Certification #: 1461.01 A2LA-IS0 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID Matrix Date Collected Date Received 92636049001 MW-1R Water 11/10/2212:15 11/10/22 16:10 92636049002 MW-2R Water 11/08/22 09:00 11/10/22 16:10 92636049003 MW-4R Water 11/09/2214:30 11/10/22 16:10 92636049004 MW-15 Water 11/07/2215:05 11/10/22 16:10 92636049005 EQBL Water 11/07/2216:05 11/10/22 16:10 92636049006 FB Water 11/09/2213:25 11/10/22 16:10 92636049007 DUP-1 Water 11/09/22 00:00 11/10/22 16:10 92636049008 MW-3R Water 11/10/22 09:15 11/10/22 16:10 92636049009 SW-2 Water 11/07/2213:35 11/10/22 16:10 92636049010 MW-5R Water 11/09/2215:35 11/10/22 16:10 92636049011 MW-8 Water 11/09/2210:10 11/10/22 16:10 92636049012 MW-9 Water 11/09/22 09:05 11/10/22 16:10 92636049013 MW-11 Water 11/08/2213:05 11/10/22 16:10 92636049014 MW-12 Water 11/08/2211:10 11/10/22 16:10 92636049015 MW-13 Water 11/08/2210:35 11/10/22 16:10 92636049016 MW-14 Water 11/08/2215:35 11/10/22 16:10 92636049017 SW-1 Water 11/06/2214:00 11/10/22 16:10 92636049018 SW-3 Water 11/07/2212:20 11/10/22 16:10 92636049019 SW-4 Water 11/07/2212:50 11/10/22 16:10 92636049020 MW-7 Water 11/09/2212:55 11/10/22 16:10 92636049021 MW-10 Water 11/08/2214:15 11/10/22 16:10 92636049022 T13-1 Water 11/10/22 00:00 11/10/22 16:10 92636049023 T13-2 Water 11/10/22 00:00 11/10/22 16:10 92636049024 T13-3 Water 11/10/22 00:00 11/10/22 16:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL 92636049 Analytes Lab lD Sample ID Method Analysts Reported Laboratory 92636049001 MW-1 R EPA 8081 B BAJ 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 CS1 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049002 MW-2R EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049003 MW-4R EPA 8081B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2540C-2015 CS1 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049004 MW-115 EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049005 EQBL EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049006 FB EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL 92636049 Analytes Lab lD Sample ID Method Analysts Reported Laboratory EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 CS1 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049007 DUP-1 EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8321 JNJ 11 PAN EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 CS1 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049008 MW-3R EPA 6010 AME 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 CS1 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049009 SW-2 EPA 6010 KPP 2 PASI-O REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049010 MW-5R EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049011 MW-8 EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049012 MW-9 EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049013 MW-11 EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049014 MW-12 EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049015 MW-13 EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL 92636049 Analytes Lab lD Sample ID Method Analysts Reported Laboratory EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049016 MW-14 EPA 6010 KPP 2 PASI-O EPA 6020 BSL 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049017 SW-1 EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049018 SW-3 EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049019 SW-4 EPA 6010 KPP 2 PASI-O REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL 92636049 Analytes Lab lD Sample ID Method Analysts Reported Laboratory EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049020 MW-7 EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049021 MW-10 EPA 8081 B SEM 14 PASI-C EPA 6010 KPP 2 PASI-O EPA 6020 BSL, LEC 16 PASI-O EPA 7470A NMP 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 MA62 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 JCM 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92636049022 T13-1 EPA 8260D CL 53 PASI-C 92636049023 T13-2 EPA 8260D CL 53 PASI-C 92636049024 T13-3 EPA 8260D CL 53 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92636049 Analytes Lab ID Sample ID Method Analysts Reported Laboratory PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-O = Pace Analytical Services - Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SUMMARY OF DETECTION Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed 92636049001 MWA R EPA 6010 Sodium 16200 ug/L 2000 12/08/22 14:12 EPA 6020 Antimony 0.56J ug/L 1.0 12/08/22 14:31 EPA 6020 Barium 304 ug/L 1.0 12/08/22 14:31 EPA 6020 Beryllium 0.46 ug/L 0.10 12/08/22 14:31 EPA 6020 Cadmium 0.0901 ug/L 0.10 12/08/22 14:31 EPA 6020 Chromium 7.9 ug/L 1.0 12/08/22 14:31 EPA 6020 Cobalt 0.74J ug/L 1.0 12/08/22 14:31 EPA 6020 Copper 5.3 ug/L 1.0 12/08/22 14:31 EPA 6020 Iron 719 ug/L 10.0 12/08/22 14:31 EPA 6020 Lead 0.46J ug/L 1.0 12/08/22 14:31 EPA 6020 Manganese 63.4 ug/L 1.0 12/08/22 14:31 EPA 6020 Nickel 5.8 ug/L 1.0 12/08/22 14:31 EPA 6020 Selenium 0.39J ug/L 2.0 12/08/22 14:31 EPA 6020 Silver 0.053J ug/L 0.50 12/08/22 14:31 EPA 6020 Vanadium 3.0 ug/L 1.0 12/08/22 14:31 EPA 6020 Zinc 15.2 ug/L 5.0 12/08/22 14:31 EPA 7470A Mercury 36.2 ug/L 2.0 11/29/22 09:41 EPA 8260D cis-1,2-Dichloroethene 0.64J ug/L 1.0 11/15/22 06:07 EPA 8260D Ethylbenzene 0.67J ug/L 1.0 11/15/22 06:07 EPA 8260D Toluene 0.28J ug/L 1.0 11/15/22 06:07 SM 2320B-2011 Alkalinity, Total as CaCO3 90400 ug/L 5000 11/11/22 21:28 SM 2540C-2015 Total Dissolved Solids 163000 ug/L 25000 11/15/22 17:49 EPA 300.0 Rev 2.1 1993 Sulfate 790J ug/L 1000 11/12/22 22:42 SM 4500-CI-E-2011 Chloride 11700 ug/L 1000 11/15/22 19:08 92636049002 MW-2R EPA 6010 Sodium 60500 ug/L 2000 12/08/22 14:16 EPA 6020 Arsenic 1.0 ug/L 1.0 12/08/22 14:51 EPA 6020 Barium 467 ug/L 1.0 12/08/22 14:51 EPA 6020 Beryllium 0.082J ug/L 0.10 12/08/22 14:51 EPA 6020 Chromium 0.75J ug/L 1.0 12/08/22 14:51 EPA 6020 Cobalt 26.3 ug/L 1.0 12/08/22 14:51 EPA 6020 Copper 1.5 ug/L 1.0 12/08/22 14:51 EPA 6020 Iron 10100 ug/L 50.0 12/09/22 15:23 EPA 6020 Manganese 18900 ug/L 50.0 12/09/22 15:26 EPA 6020 Nickel 13.8 ug/L 1.0 12/08/22 14:51 EPA 6020 Vanadium 1.3 ug/L 1.0 12/08/22 14:51 EPA 6020 Zinc 6.0 ug/L 5.0 12/08/22 14:51 EPA8321 MCPP 5.67 ug/L 2.00 11/30/2218:25 EPA 8260D Benzene 2.7 ug/L 1.0 11/15/22 07:21 EPA 8260D 1,4-Dichlorobenzene 0.591 ug/L 1.0 11/15/22 07:21 EPA 8260D cis-1,2-Dichloroethene 1.1 ug/L 1.0 11/15/22 07:21 EPA 8260D Tetrahydrofuran 12.8 ug/L 10.0 11/15/22 07:21 EPA 8260D Trichloroethene 0.61 J ug/L 1.0 11/15/22 07:21 EPA 8260D Vinyl chloride 0.73J ug/L 1.0 11/15/22 07:21 EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) 3.7 ug/L 2.0 11/10/22 21:27 SM 2320B-2011 Alkalinity, Total as CaCO3 879000 ug/L 5000 11/12/22 10:56 SM 2540C-2015 Total Dissolved Solids 972000 ug/L 50000 11/13/22 13:57 REPORT OF LABORATORY ANALYSIS H3 v3 Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters 92636049002 SM 4500-S2D-2011 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049003 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8321 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049004 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049005 EPA 6020 EPA 6020 MW-2R Sulfide Sulfate Chloride MW-4R Sodium Arsenic Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Zinc MCPP Tetrahydrofuran 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-15 Sodium Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Silver Vanadium Zinc Chloroform Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride EQBL Manganese Zinc SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 27.6J 66300 39800 74000 1.6 157 0.055J 0.55J 80.1 0.64J 2150 1110 8.9 18.6 8.02 10J 4.9 552000 832000 133000 46200 16800 18.1 0.049J 1.7 0.36J 3.8 440 0.33J 475 2.4 0.079J 2.1 9.5 0.45J 83100 255000 22800 54700 0.37J 11.5 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 100 11/11/22 03:48 1000 11/12/22 22:57 1000 11/15/22 19:09 2000 12/08/22 14:20 1.0 12/08/22 14:53 1.0 12/08/22 14:53 0.10 12/08/22 14:53 1.0 12/08/22 14:53 1.0 12/08/22 14:53 1.0 12/08/22 14:53 10.0 12/08/22 14:53 5.0 12/09/22 15:28 1.0 12/08/22 14:53 5.0 12/08/22 14:53 2.00 11/30/2218:43 H3 10.0 11/15/22 06:26 v2 2.0 11/10/22 21:46 5000 11/12/22 11:26 50000 11 /14/22 15:17 3000 11/13/22 05:50 2000 11/15/22 20:04 2000 12/08/22 14:23 1.0 12/08/22 14:56 0.10 12/08/22 14:56 1.0 12/08/22 14:56 1.0 12/08/22 14:56 1.0 12/08/22 14:56 10.0 12/08/22 14:56 1.0 12/08/22 14:56 2.0 12/09/22 15:41 1.0 12/08/22 14:56 0.50 12/08/22 14:56 1.0 12/08/22 14:56 5.0 12/08/22 14:56 1.0 11/15/22 06:44 5000 11 /11 /22 17:47 25000 11 /11 /22 12:02 1000 11/12/22 23:27 4000 11/15/22 19:11 1.0 12/08/22 14:58 5.0 12/08/22 14:58 Page 14 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters 92636049006 EPA 6020 EPA 6020 EPA 8260D 92636049007 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8321 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049008 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049009 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 FB Copper Iron m&p-Xylene DUP-1 Sodium Arsenic Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Zinc MCPP Tetrahydrofuran 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-3R Sodium Arsenic Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Selenium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SW-2 Sodium Arsenic Barium Beryllium Chromium Cobalt Copper SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 0.74J ug/L 1.0 12/08/2215:06 6.7J ug/L 10.0 12/08/2215:06 0.75J ug/L 2.0 11/15/22 02:46 CO 72000 ug/L 2000 12/08/2214:40 1.6 ug/L 1.0 12/08/2215:09 154 ug/L 1.0 12/08/2215:09 0.056J ug/L 0.10 12/08/2215:09 0.62J ug/L 1.0 12/08/2215:09 79.0 ug/L 1.0 12/08/2215:09 0.68J ug/L 1.0 12/08/2215:09 2160 ug/L 10.0 12/08/2215:09 1170 ug/L 5.0 12/09/2215:44 8.6 ug/L 1.0 12/08/2215:09 5.1 ug/L 5.0 12/08/2215:09 8.96 ug/L 2.00 11/30/2219:55 H3 9.91 ug/L 10.0 11/15/22 08:16 v2 4.3 ug/L 2.0 11/11/22 05:25 544000 ug/L 5000 11/12/22 11:35 812000 ug/L 50000 11/14/2215:17 139000 ug/L 3000 11/13/22 06:05 45300 ug/L 2000 11/15/22 20:05 2480 ug/L 2000 12/09/22 01:17 5.3 ug/L 1.0 12/08/2216:13 231 ug/L 1.0 12/08/2216:13 0.063J ug/L 0.10 12/08/2216:13 0.69J ug/L 1.0 12/08/2216:13 12.0 ug/L 1.0 12/08/2216:13 0.39J ug/L 1.0 12/08/2216:13 80000 ug/L 200 12/09/2216:29 5490 ug/L 20.0 12/09/2216:29 0.81 J ug/L 1.0 12/08/22 16:13 0.23J ug/L 2.0 12/08/2216:13 130000 ug/L 5000 11/11/22 21:58 121000 ug/L 25000 11/15/2217:49 1760 ug/L 1000 11/13/22 00:56 2860 ug/L 1000 11/15/2219:17 18800 ug/L 2000 12/08/2214:43 0.55J ug/L 1.0 12/08/2215:11 143 ug/L 1.0 12/08/2215:11 0.034J ug/L 0.10 12/08/2215:11 0.68J ug/L 1.0 12/08/2215:11 1.4 ug/L 1.0 12/08/2215:11 0.55J ug/L 1.0 12/08/2215:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters 92636049009 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049010 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049011 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049012 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SW-2 Iron Manganese Nickel Vanadium Toluene 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-5R Sodium Barium Chromium Copper Iron Manganese Nickel Selenium Vanadium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-8 Sodium Barium Beryllium Chromium Iron Manganese Nickel Selenium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-9 Sodium Barium Beryllium Chromium Copper Iron Manganese Nickel SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 4170 ug/L 10.0 12/08/2215:11 2990 ug/L 10.0 12/09/2215:46 2.2 ug/L 1.0 12/08/2215:11 0.991 ug/L 1.0 12/08/2215:11 0.30J ug/L 1.0 11/15/22 04:36 4.4 ug/L 2.0 11/10/22 22:43 140000 ug/L 5000 11/11/2218:00 245000 ug/L 25000 11/11/2212:02 11700 ug/L 1000 11/13/22 01:40 27200 ug/L 1000 11/15/2219:18 13300 ug/L 2000 12/08/2214:47 59.1 ug/L 1.0 12/08/2215:14 6.6 ug/L 1.0 12/08/2215:14 0.25J ug/L 1.0 12/08/2215:14 42.5 ug/L 10.0 12/08/2215:14 1.0 ug/L 1.0 12/08/2215:14 1.2 ug/L 1.0 12/08/2215:14 0.23J ug/L 2.0 12/08/2215:14 5.5 ug/L 1.0 12/08/2215:14 33900 ug/L 5000 11/11/22 22:09 159000 ug/L 25000 11/15/2213:05 8420 ug/L 1000 11/13/22 01:55 14700 ug/L 1000 11/15/2219:19 11200 ug/L 2000 12/08/2214:50 60.1 ug/L 1.0 12/08/2215:16 0.47 ug/L 0.10 12/08/2215:16 3.8 ug/L 1.0 12/08/2215:16 74.3 ug/L 10.0 12/08/2215:16 5.3 ug/L 1.0 12/08/2215:16 0.31 J ug/L 1.0 12/08/22 15:16 1.2J ug/L 2.0 12/08/2215:16 29300 ug/L 5000 11/11/22 22:16 86000 ug/L 25000 11/15/2213:05 8290 ug/L 1000 11/13/22 02:10 3710 ug/L 1000 11/15/2219:20 14600 ug/L 2000 12/08/2214:54 191 ug/L 1.0 12/08/2215:19 0.26 ug/L 0.10 12/08/2215:19 0.61 J ug/L 1.0 12/08/22 15:19 0.37J ug/L 1.0 12/08/2215:19 142 ug/L 10.0 12/08/2215:19 6.2 ug/L 1.0 12/08/2215:19 0.58J ug/L 1.0 12/08/2215:19 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters 92636049012 EPA 8260D EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049013 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049014 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049015 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 MW-9 Dichlorodifluoromethane Trichlorofluoromethane Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-11 Sodium Barium Beryllium Cobalt Copper Iron Manganese Nickel Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-12 Sodium Arsenic Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Benzene 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-13 Sodium Barium Beryllium Cadmium Cobalt Copper Iron Manganese Nickel SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 0.35J ug/L 1.0 11/14/22 20:25 v3 0.37J ug/L 1.0 11/14/22 20:25 29200 ug/L 5000 11/11/22 22:22 139000 ug/L 25000 11/15/2213:05 807J ug/L 1000 11/13/22 02:25 3690 ug/L 1000 11/15/2219:21 11900 ug/L 2000 12/08/2214:57 69.6 ug/L 1.0 12/08/2215:21 0.067J ug/L 0.10 12/08/2215:21 2.2 ug/L 1.0 12/08/2215:21 0.27J ug/L 1.0 12/08/2215:21 21200 ug/L 50.0 12/09/2215:49 1380 ug/L 5.0 12/09/2215:49 0.67J ug/L 1.0 12/08/2215:21 106000 ug/L 5000 11/11/22 20:29 173000 ug/L 25000 11/13/2213:57 9830 ug/L 1000 11/13/22 02:39 8540 ug/L 1000 11/15/2219:22 23700 ug/L 2000 12/08/2215:19 0.57J ug/L 1.0 12/08/2215:24 161 ug/L 1.0 12/08/2215:24 0.063J ug/L 0.10 12/08/2215:24 0.77J ug/L 1.0 12/08/2215:24 5.5 ug/L 1.0 12/08/2215:24 0.86J ug/L 1.0 12/08/2215:24 1290 ug/L 10.0 12/08/2215:24 5160 ug/L 10.0 12/09/2215:52 9.0 ug/L 1.0 12/08/2215:24 0.36J ug/L 1.0 11/15/22 05:31 6.1 ug/L 2.0 11/11/22 00:19 294000 ug/L 5000 11/12/22 11:06 496000 ug/L 25000 11/13/2213:57 94600 ug/L 1000 11/13/22 02:54 28200 ug/L 1000 11/15/2219:23 17800 ug/L 2000 12/08/2215:22 515 ug/L 2.0 12/09/2215:54 1.8 ug/L 0.10 12/08/2215:26 0.072J ug/L 0.10 12/08/2215:26 0.56J ug/L 1.0 12/08/2215:26 0.62J ug/L 1.0 12/08/2215:26 183 ug/L 10.0 12/08/2215:26 119 ug/L 1.0 12/08/2215:26 2.2 ug/L 1.0 12/08/2215:26 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Client Sample ID Method Parameters 92636049015 EPA 6020 EPA 7470A EPA 8260D EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049016 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D SM 2320B-2011 SM 2540C-2015 SM 4500-CI-E-2011 92636049017 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049018 EPA 6010 EPA 6020 MW-13 Zinc Mercury Tetrahydrofuran Trichlorofluoromethane 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-14 Sodium Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Dichlorodifluoromethane Trichlorofluoromethane Alkalinity, Total as CaCO3 Total Dissolved Solids Chloride SW-1 Sodium Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Vanadium Zinc Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SW-3 Sodium Arsenic SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 8.9 ug/L 5.0 12/08/2215:26 0.151 ug/L 0.20 11/28/2213:52 10.1 ug/L 10.0 11/15/22 05:49 v3 0.45J ug/L 1.0 11/15/22 05:49 7.7 ug/L 2.0 11/11/22 00:38 84400 ug/L 5000 11/11/22 20:49 272000 ug/L 25000 11/13/2213:58 27300 ug/L 1000 11/13/22 03:09 47300 ug/L 2000 11/15/22 20:06 18000 ug/L 2000 12/08/2215:25 249 ug/L 1.0 12/08/2215:29 0.69 ug/L 0.10 12/08/2215:29 0.97J ug/L 1.0 12/08/2215:29 0.27J ug/L 1.0 12/08/2215:29 1.1 ug/L 1.0 12/08/2215:29 50.9 ug/L 10.0 12/08/2215:29 48.6 ug/L 1.0 12/08/2215:29 4.6 ug/L 1.0 12/08/2215:29 3.7 ug/L 1.0 11/15/22 07:39 1.7 ug/L 1.0 11/15/22 07:39 63100 ug/L 5000 11/11/22 21:03 158000 ug/L 25000 11/13/2213:58 3910 ug/L 1000 11/15/2219:27 13100 ug/L 2000 12/08/2215:29 0.71 J ug/L 1.0 12/08/22 15:37 45.9 ug/L 1.0 12/08/2215:37 0.11 ug/L 0.10 12/08/2215:37 2.5 ug/L 1.0 12/08/2215:37 1.9 ug/L 1.0 12/08/2215:37 4.0 ug/L 1.0 12/08/2215:37 6950 ug/L 20.0 12/09/2215:57 2.4 ug/L 1.0 12/08/2215:37 721 ug/L 2.0 12/09/2215:57 1.7 ug/L 1.0 12/08/2215:37 0.37J ug/L 2.0 12/08/2215:37 4.7 ug/L 1.0 12/08/2215:37 22.9 ug/L 5.0 12/08/2215:37 41700 ug/L 5000 11/11/2216:57 88000 ug/L 25000 11/11/2211:55 2840 ug/L 1000 11/13/22 04:08 19500 ug/L 1000 11/15/2219:30 16800 ug/L 2000 12/08/2215:32 2.0 ug/L 1.0 12/08/2215:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Method 92636049018 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049019 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SUMMARY OF DETECTION Client Sample ID Parameters Result Units Report Limit Analyzed SW-3 Barium 367 ug/L 1.0 12/08/2215:39 Beryllium 0.40 ug/L 0.10 12/08/2215:39 Chromium 9.4 ug/L 1.0 12/08/2215:39 Cobalt 4.5 ug/L 1.0 12/08/2215:39 Copper 16.5 ug/L 1.0 12/08/2215:39 Iron 37400 ug/L 100 12/09/2215:59 Lead 6.7 ug/L 1.0 12/08/2215:39 Manganese 2690 ug/L 10.0 12/09/2215:59 Nickel 5.8 ug/L 1.0 12/08/2215:39 Selenium 1.2J ug/L 2.0 12/08/2215:39 Vanadium 21.4 ug/L 1.0 12/08/2215:39 Zinc 51.8 ug/L 5.0 12/08/2215:39 Acetone 13.2J ug/L 25.0 11/15/22 04:54 Toluene 0.26J ug/L 1.0 11/15/22 04:54 Alkalinity, Total as CaCO3 234000 ug/L 5000 11/12/22 10:37 Total Dissolved Solids 312000 ug/L 25000 11/11/22 12:02 Sulfate 34000 ug/L 1000 11/13/22 20:39 Chloride 20600 ug/L 1000 11/15/2219:33 SW-4 Sodium 35500 ug/L 2000 12/08/2215:35 Arsenic 0.97J ug/L 1.0 12/08/2215:42 Barium 263 ug/L 1.0 12/08/2215:42 Beryllium 0.22 ug/L 0.10 12/08/2215:42 Chromium 5.3 ug/L 1.0 12/08/2215:42 Cobalt 5.9 ug/L 1.0 12/08/2215:42 Copper 5.5 ug/L 1.0 12/08/2215:42 Iron 10800 ug/L 200 12/09/2216:07 Lead 2.4 ug/L 1.0 12/08/2215:42 Manganese 6200 ug/L 20.0 12/09/2216:07 Nickel 6.4 ug/L 1.0 12/08/2215:42 Selenium 0.65J ug/L 2.0 12/08/2215:42 Vanadium 12.7 ug/L 1.0 12/08/2215:42 Zinc 17.8 ug/L 5.0 12/08/2215:42 Tetrahydrofuran 5.2J ug/L 10.0 11/15/22 07:02 v2 1,4-Dioxane (p-Dioxane) 5.6 ug/L 2.0 11/11/22 04:27 Alkalinity, Total as CaCO3 351000 ug/L 5000 11/12/22 10:47 Total Dissolved Solids 511000 ug/L 25000 11/11/22 12:02 Sulfate 46500 ug/L 1000 11/13/22 21:25 Chloride 43500 ug/L 2000 11/15/22 20:06 92636049020 MW-7 EPA 6010 Sodium 43900 ug/L 2000 12/08/22 15:39 EPA 6020 Arsenic 0.62J ug/L 1.0 12/08/22 15:44 EPA 6020 Barium 283 ug/L 1.0 12/08/22 15:44 EPA 6020 Beryllium 0.49 ug/L 0.10 12/08/22 15:44 EPA 6020 Cadmium 0.16 ug/L 0.10 12/08/22 15:44 EPA 6020 Chromium 0.80J ug/L 1.0 12/08/22 15:44 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 Lab Sample ID Method 92636049020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 7470A EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92636049021 EPA 6010 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 6020 EPA 8260D EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SUMMARY OF DETECTION Client Sample ID Parameters Result Units Report Limit Analyzed MW-7 Cobalt 3.8 ug/L 1.0 12/08/2215:44 Copper 3.5 ug/L 1.0 12/08/2215:44 Iron 413 ug/L 10.0 12/08/2215:44 Manganese 657 ug/L 2.0 12/09/2216:10 Nickel 5.2 ug/L 1.0 12/08/2215:44 Selenium 0.25J ug/L 2.0 12/08/2215:44 Silver 0.047J ug/L 0.50 12/08/2215:44 Vanadium 1.1 ug/L 1.0 12/08/2215:44 Zinc 16.9 ug/L 5.0 12/08/2215:44 Mercury 0.17J ug/L 0.20 11/28/2214:03 Benzene 0.95J ug/L 1.0 11/14/22 20:43 1,1-Dichloroethane 0.87J ug/L 1.0 11/14/22 20:43 cis-1,2-Dichloroethene 1.0J ug/L 1.0 11/14/22 20:43 Tetrahydrofuran 48.0 ug/L 10.0 11/14/22 20:43 Trichlorofluoromethane 0.96J ug/L 1.0 11/14/22 20:43 o-Xylene 0.44J ug/L 1.0 11/14/22 20:43 1,4-Dioxane (p-Dioxane) 7.8 ug/L 2.0 11/11/22 04:47 Alkalinity, Total as CaCO3 265000 ug/L 5000 11/12/22 11:44 Total Dissolved Solids 510000 ug/L 25000 11/15/22 13:05 Sulfate 98400 ug/L 2000 11/14/2212:07 Chloride 32500 ug/L 1000 11/15/2219:39 MW-10 Sodium 112000 ug/L 2000 12/08/2215:42 Arsenic 0.901 ug/L 1.0 12/08/22 15:47 Barium 93.0 ug/L 1.0 12/08/22 15:47 Beryllium 0.17 ug/L 0.10 12/08/22 15:47 Chromium 2.1 ug/L 1.0 12/08/22 15:47 Cobalt 5.8 ug/L 1.0 12/08/22 15:47 Copper 0.69J ug/L 1.0 12/08/22 15:47 Iron 2460 ug/L 10.0 12/08/22 15:47 Lead 0.511 ug/L 1.0 12/08/22 15:47 Manganese 21100 ug/L 50.0 12/09/2216:12 Nickel 10.5 ug/L 1.0 12/08/22 15:47 Selenium 1 AJ ug/L 2.0 12/08/22 15:47 Vanadium 1.5 ug/L 1.0 12/08/22 15:47 Benzene 0.63J ug/L 1.0 11/15/22 07:57 Tetrahydrofuran 74.3 ug/L 10.0 11/15/22 07:57 v3 1,4-Dioxane (p-Dioxane) 5.7 ug/L 2.0 11/11/22 05:06 Alkalinity, Total as CaCO3 919000 ug/L 5000 11/12/22 11:15 Total Dissolved Solids 1220000 ug/L 50000 11/13/22 13:58 Sulfate 146000 ug/L 3000 11/14/2212:22 Chloride 51400 ug/L 2000 11/15/22 20:07 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MWAR Lab ID: 92636049001 Collected: 11/10/22 12:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Sodium Tin Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.050 0.014 1 11/15/2211:28 11/16/2214:05 309-00-2 ND ug/L 0.050 0.012 1 11/15/2211:28 11/16/2214:05 319-84-6 ND ug/L 0.050 0.014 1 11/15/2211:28 11/16/2214:05 319-86-8 ND ug/L 0.050 0.017 1 11/15/2211:28 11/16/2214:05 72-54-8 ND ug/L 0.050 0.026 1 11/15/2211:28 11/16/2214:05 50-29-3 ND ug/L 0.050 0.017 1 11/15/2211:28 11/16/2214:05 959-98-8 ND ug/L 0.050 0.016 1 11/15/2211:28 11/16/2214:05 33213-65-9 ND ug/L 0.050 0.018 1 11/15/2211:28 11/16/2214:05 72-20-8 ND ug/L 0.050 0.016 1 11/15/2211:28 11/16/2214:05 7421-93-4 ND ug/L 0.050 0.020 1 11/15/2211:28 11/16/2214:05 76-44-8 ND ug/L 0.050 0.028 1 11/15/2211:28 11/16/2214:05 1024-57-3 ND ug/L 0.15 0.042 1 11/15/2211:28 11/16/2214:05 72-43-5 98 % 10-182 1 11/15/2211:28 11/16/2214:05 877-09-8 151 % 10-200 1 11 /15/22 11:28 11 /16/22 14:05 2051-24-3 Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach 16200 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:12 7440-23-5 ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:12 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony 0.56.11 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:31 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:31 7440-38-2 Barium 304 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:31 7440-39-3 Beryllium 0.46 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 14:31 7440-41-7 Cadmium 0.090.1 ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 14:31 7440-43-9 Chromium 7.9 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:31 7440-47-3 Cobalt 0.74.11 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 14:31 7440-48-4 Copper 5.3 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 14:31 7440-50-8 Iron 719 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 14:31 7439-89-6 Lead 0.46.11 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 14:31 7439-92-1 Manganese 63.4 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 14:31 7439-96-5 Nickel 5.8 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 14:31 7440-02-0 Selenium 0.39.11 ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 14:31 7782-49-2 Silver 0.053.11 ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 14:31 7440-22-4 Vanadium 3.0 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 14:31 7440-62-2 Zinc 15.2 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 14:31 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 36.2 ug/L 2.0 1.2 10 11/21/22 08:11 11/29/22 09:41 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MWAR Lab ID: 92636049001 Collected: 11/10/22 12:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 17:32 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 17:32 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 17:32 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 17:32 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 17:32 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 17:32 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 17:32 94-74-6 H3 ND ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 17:32 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 17:32 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 17:32 93-72-1 H3 98.0 % 70.0-130 1 11/25/22 06:08 11/30/22 17:32 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/15/2215:01 11/16/2215:09 56-55-3 ND ug/L 8.3 2.3 1 11/15/2215:01 11/16/2215:09 218-01-9 ND ug/L 8.3 2.5 1 11/15/2215:01 11/16/2215:09 53-70-3 ND ug/L 5.0 3.1 1 11/15/2215:01 11/16/2215:09 117-81-7 ND ug/L 8.3 2.4 1 11/15/2215:01 11/16/2215:09 193-39-5 75 % 10-144 1 11/15/2215:01 11/16/2215:09 4165-60-0 62 % 10-130 1 11/15/2215:01 11/16/2215:09 321-60-8 94 % 34-163 1 11/15/2215:01 11/16/2215:09 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 06:07 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 06:07 107-13-1 ND ug/L 1.0 0.34 1 11/15/22 06:07 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 06:07 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 06:07 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 06:07 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 06:07 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 06:07 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 06:07 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 06:07 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 06:07 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 06:07 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 06:07 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 06:07 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 06:07 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 06:07 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 06:07 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 06:07 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MWAR Lab ID: 92636049001 Collected: 11/10/22 12:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 06:07 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 06:07 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 06:07 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 06:07 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 06:07 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 06:07 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 06:07 75-35-4 0.64J ug/L 1.0 0.38 1 11/15/22 06:07 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 06:07 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 06:07 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 06:07 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 06:07 10061-02-6 0.67J ug/L 1.0 0.30 1 11/15/22 06:07 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 06:07 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 06:07 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 06:07 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 06:07 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 06:07 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 06:07 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 06:07 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 06:07 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 06:07 109-99-9 v2 0.28J ug/L 1.0 0.24 1 11/15/22 06:07 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 06:07 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 06:07 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 06:07 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 06:07 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 06:07 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 06:07 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 06:07 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 06:07 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 06:07 95-47-6 103 % 70-130 1 11/15/22 06:07 460-00-4 104 % 70-130 1 11/15/22 06:07 17060-07-0 103 % 70-130 1 11/15/22 06:07 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 21:07 123-91-1 92 % 70-130 1 11/10/22 21:07 17060-07-0 97 % 70-130 1 11/10/22 21:07 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MWAR Lab ID: 92636049001 Collected: 11/10/22 12:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 90400 ug/L 5000 5000 1 11/11/22 21:28 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 163000 ug/L 25000 25000 1 11/15/22 17:49 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:21 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 790J ug/L 1000 500 1 11/12/22 22:42 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 11700 ug/L 1000 500 1 11/15/2219:08 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 18:02 11/22/22 22:16 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-2R Lab ID: 92636049002 Collected: 11/08/22 09:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 0.012 1 11/14/22 17:33 11/15/22 13:40 309-00-2 alpha-BHC ND ug/L 0.042 0.010 1 11/14/22 17:33 11/15/22 13:40 319-84-6 delta-BHC ND ug/L 0.042 0.012 1 11/14/22 17:33 11/15/22 13:40 319-86-8 4,4'-DDD ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 13:40 72-54-8 4,4'-DDT ND ug/L 0.042 0.022 1 11/14/22 17:33 11/15/22 13:40 50-29-3 L1 Endosulfan I ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 13:40 959-98-8 Endosulfan 11 ND ug/L 0.042 0.013 1 11/14/22 17:33 11/15/22 13:40 33213-65-9 Endrin ND ug/L 0.042 0.015 1 11/14/22 17:33 11/15/22 13:40 72-20-8 Endrin aldehyde ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 13:40 7421-93-4 Heptachlor ND ug/L 0.042 0.016 1 11/14/22 17:33 11/15/22 13:40 76-44-8 Heptachlor epoxide ND ug/L 0.042 0.024 1 11/14/22 17:33 11/15/22 13:40 1024-57-3 Methoxychlor ND ug/L 0.12 0.035 1 11/14/22 17:33 11/15/22 13:40 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 99 % 10-182 1 11/14/22 17:33 11/15/22 13:40 877-09-8 Decachlorobiphenyl (S) 130 % 10-200 1 11/14/22 17:33 11/15/22 13:40 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 60500 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:16 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:16 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:51 7440-36-0 Arsenic 1.0 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:51 7440-38-2 Barium 467 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:51 7440-39-3 Beryllium 0.082.11 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 14:51 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 14:51 7440-43-9 Chromium 0.75.11 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:51 7440-47-3 Cobalt 26.3 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 14:51 7440-48-4 Copper 1.5 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 14:51 7440-50-8 Iron 10100 ug/L 50.0 31.8 5 12/07/22 23:33 12/09/22 15:23 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 14:51 7439-92-1 Manganese 18900 ug/L 50.0 14.6 50 12/07/22 23:33 12/09/22 15:26 7439-96-5 Nickel 13.8 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 14:51 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 14:51 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 14:51 7440-22-4 Vanadium 1.3 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 14:51 7440-62-2 Zinc 6.0 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 14:51 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 14:51 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-2R Lab ID: 92636049002 Collected: 11/08/22 09:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 18:25 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 18:25 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 18:25 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 18:25 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 18:25 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 18:25 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 18:25 94-74-6 H3 5.67 ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 18:25 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 18:25 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 18:25 93-72-1 H3 101 % 70.0-130 1 11/25/22 06:08 11/30/22 18:25 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/14/22 12:34 11/16/22 09:38 56-55-3 ND ug/L 8.3 2.3 1 11/14/22 12:34 11/16/22 09:38 218-01-9 ND ug/L 8.3 2.5 1 11/14/22 12:34 11/16/22 09:38 53-70-3 ND ug/L 5.0 3.1 1 11/14/22 12:34 11/16/22 09:38 117-81-7 ND ug/L 8.3 2.4 1 11/14/22 12:34 11/16/22 09:38 193-39-5 26 % 10-144 1 11/14/22 12:34 11/16/22 09:38 4165-60-0 42 % 10-130 1 11/14/22 12:34 11/16/22 09:38 321-60-8 115 % 34-163 1 11/14/22 12:34 11/16/22 09:38 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 07:21 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 07:21 107-13-1 2.7 ug/L 1.0 0.34 1 11/15/22 07:21 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 07:21 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 07:21 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 07:21 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 07:21 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 07:21 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 07:21 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 07:21 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 07:21 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 07:21 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 07:21 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 07:21 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 07:21 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 07:21 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 07:21 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 07:21 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-2R Lab ID: 92636049002 Collected: 11/08/22 09:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 07:21 95-50-1 0.591 ug/L 1.0 0.33 1 11/15/22 07:21 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 07:21 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 07:21 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 07:21 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 07:21 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 07:21 75-35-4 1.1 ug/L 1.0 0.38 1 11/15/22 07:21 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 07:21 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 07:21 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 07:21 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 07:21 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 07:21 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 07:21 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 07:21 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 07:21 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 07:21 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 07:21 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 07:21 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 07:21 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 07:21 127-18-4 12.8 ug/L 10.0 3.5 1 11/15/22 07:21 109-99-9 v3 ND ug/L 1.0 0.24 1 11/15/22 07:21 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 07:21 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 07:21 79-00-5 0.61J ug/L 1.0 0.38 1 11/15/22 07:21 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 07:21 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 07:21 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 07:21 108-05-4 v2 0.73J ug/L 1.0 0.39 1 11/15/22 07:21 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 07:21 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 07:21 95-47-6 104 % 70-130 1 11/15/22 07:21 460-00-4 106 % 70-130 1 11/15/22 07:21 17060-07-0 105 % 70-130 1 11/15/22 07:21 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 3.7 ug/L 2.0 0.86 1 11/10/22 21:27 123-91-1 101 % 70-130 1 11/10/22 21:27 17060-07-0 99 % 70-130 1 11/10/22 21:27 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-2R Lab ID: 92636049002 Collected: 11/08/22 09:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 879000 ug/L 5000 5000 1 11/12/22 10:56 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 972000 ug/L 50000 50000 1 11/13/22 13:57 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide 27.6J ug/L 100 22.0 1 11/11/22 03:48 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 66300 ug/L 1000 500 1 11/12/22 22:57 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 39800 ug/L 1000 500 1 11/15/2219:09 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:15 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-4R Lab ID: 92636049003 Collected: 11/09/22 14:30 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 0.012 1 11/14/22 17:33 11/15/22 14:05 309-00-2 alpha-BHC ND ug/L 0.042 0.010 1 11/14/22 17:33 11/15/22 14:05 319-84-6 delta-BHC ND ug/L 0.042 0.012 1 11/14/22 17:33 11/15/22 14:05 319-86-8 4,4'-DDD ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 14:05 72-54-8 4,4'-DDT ND ug/L 0.042 0.022 1 11/14/22 17:33 11/15/22 14:05 50-29-3 L1 Endosulfan I ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 14:05 959-98-8 Endosulfan 11 ND ug/L 0.042 0.013 1 11/14/22 17:33 11/15/22 14:05 33213-65-9 Endrin ND ug/L 0.042 0.015 1 11/14/22 17:33 11/15/22 14:05 72-20-8 Endrin aldehyde ND ug/L 0.042 0.014 1 11/14/22 17:33 11/15/22 14:05 7421-93-4 Heptachlor ND ug/L 0.042 0.016 1 11/14/22 17:33 11/15/22 14:05 76-44-8 Heptachlor epoxide ND ug/L 0.042 0.024 1 11/14/22 17:33 11/15/22 14:05 1024-57-3 Methoxychlor ND ug/L 0.12 0.035 1 11/14/22 17:33 11/15/22 14:05 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 103 % 10-182 1 11/14/22 17:33 11/15/22 14:05 877-09-8 Decachlorobiphenyl (S) 201 % 10-200 1 11/14/22 17:33 11/15/22 14:05 2051-24-3 S3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 74000 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:20 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:20 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:53 7440-36-0 Arsenic 1.6 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:53 7440-38-2 Barium 157 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:53 7440-39-3 Beryllium 0.055.11 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 14:53 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 14:53 7440-43-9 Chromium 0.55J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:53 7440-47-3 Cobalt 80.1 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 14:53 7440-48-4 Copper 0.64J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 14:53 7440-50-8 Iron 2150 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 14:53 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 14:53 7439-92-1 Manganese 1110 ug/L 5.0 1.5 5 12/07/22 23:33 12/09/22 15:28 7439-96-5 Nickel 8.9 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 14:53 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 14:53 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 14:53 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 14:53 7440-62-2 Zinc 18.6 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 14:53 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 14:53 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-4R Lab ID: 92636049003 Collected: 11/09/22 14:30 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 18:43 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 18:43 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 18:43 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 18:43 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 18:43 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 18:43 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 18:43 94-74-6 H3 8.02 ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 18:43 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 18:43 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 18:43 93-72-1 H3 100 % 70.0-130 1 11/25/22 06:08 11/30/22 18:43 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 10.0 2.7 1 11/15/2215:01 11/16/2213:53 56-55-3 ND ug/L 10.0 2.8 1 11/15/2215:01 11/16/2213:53 218-01-9 ND ug/L 10.0 3.0 1 11/15/2215:01 11/16/2213:53 53-70-3 ND ug/L 6.0 3.7 1 11/15/2215:01 11/16/2213:53 117-81-7 ND ug/L 10.0 2.9 1 11/15/2215:01 11/16/2213:53 193-39-5 58 % 10-144 1 11/15/2215:01 11/16/2213:53 4165-60-0 51 % 10-130 1 11/15/2215:01 11/16/2213:53 321-60-8 110 % 34-163 1 11/15/2215:01 11/16/2213:53 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 06:26 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 06:26 107-13-1 ND ug/L 1.0 0.34 1 11/15/22 06:26 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 06:26 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 06:26 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 06:26 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 06:26 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 06:26 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 06:26 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 06:26 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 06:26 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 06:26 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 06:26 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 06:26 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 06:26 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 06:26 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 06:26 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 06:26 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-4R Lab ID: 92636049003 Collected: 11/09/22 14:30 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 06:26 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 06:26 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 06:26 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 06:26 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 06:26 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 06:26 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 06:26 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 06:26 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 06:26 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 06:26 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 06:26 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 06:26 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 06:26 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 06:26 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 06:26 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 06:26 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 06:26 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 06:26 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 06:26 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 06:26 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 06:26 127-18-4 10J ug/L 10.0 3.5 1 11/15/22 06:26 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 06:26 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 06:26 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 06:26 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 06:26 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 06:26 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 06:26 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 06:26 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 06:26 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 06:26 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 06:26 95-47-6 101 % 70-130 1 11/15/22 06:26 460-00-4 102 % 70-130 1 11/15/22 06:26 17060-07-0 106 % 70-130 1 11/15/22 06:26 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 4.9 ug/L 2.0 0.86 1 11/10/22 21:46 123-91-1 96 % 70-130 1 11/10/22 21:46 17060-07-0 97 % 70-130 1 11/10/22 21:46 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-4R Lab ID: 92636049003 Collected: 11/09/22 14:30 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 552000 ug/L 5000 5000 1 11/12/22 11:26 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 832000 ug/L 50000 50000 1 11/14/22 15:17 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:14 18496-25-8 M1 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 133000 ug/L 3000 1500 3 11/13/22 05:50 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 46200 ug/L 2000 1000 2 11/15/22 20:04 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:18 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-15 Lab ID: 92636049004 Collected: 11/07/22 15:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Sodium Tin Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.042 0.012 1 11/11/2213:04 11/14/2212:29 309-00-2 ND ug/L 0.042 0.010 1 11/11/2213:04 11/14/2212:29 319-84-6 R1 ND ug/L 0.042 0.012 1 11/11/2213:04 11/14/2212:29 319-86-8 ND ug/L 0.042 0.014 1 11/11/2213:04 11/14/2212:29 72-54-8 ND ug/L 0.042 0.022 1 11/11/2213:04 11/14/2212:29 50-29-3 ND ug/L 0.042 0.014 1 11/11/2213:04 11/14/2212:29 959-98-8 ND ug/L 0.042 0.013 1 11/11/2213:04 11/14/2212:29 33213-65-9 ND ug/L 0.042 0.015 1 11/11/2213:04 11/14/2212:29 72-20-8 ND ug/L 0.042 0.014 1 11 /11 /22 13:04 11 /14/22 12:29 7421-93-4 ND ug/L 0.042 0.016 1 11/11/2213:04 11/14/2212:29 76-44-8 ND ug/L 0.042 0.024 1 11/11/2213:04 11/14/2212:29 1024-57-3 ND ug/L 0.12 0.035 1 11/11/2213:04 11/14/2212:29 72-43-5 89 % 10-182 1 11/11/2213:04 11/14/2212:29 877-09-8 145 % 10-200 1 11 /11 /22 13:04 11 /14/22 12:29 2051-24-3 Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach 16800 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:23 7440-23-5 ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:23 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:56 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:56 7440-38-2 Barium 18.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:56 7440-39-3 Beryllium 0.049.11 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 14:56 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 14:56 7440-43-9 Chromium 1.7 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:56 7440-47-3 Cobalt 0.36.11 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 14:56 7440-48-4 Copper 3.8 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 14:56 7440-50-8 Iron 440 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 14:56 7439-89-6 Lead 0.33.11 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 14:56 7439-92-1 Manganese 475 ug/L 2.0 0.58 2 12/07/22 23:33 12/09/22 15:41 7439-96-5 Nickel 2.4 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 14:56 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 14:56 7782-49-2 Silver 0.079.11 ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 14:56 7440-22-4 Vanadium 2.1 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 14:56 7440-62-2 Zinc 9.5 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 14:56 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 14:55 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-15 Lab ID: 92636049004 Collected: 11/07/22 15:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:01 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 19:01 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:01 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 19:01 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 19:01 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 19:01 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 19:01 94-74-6 H3 ND ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 19:01 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 19:01 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 19:01 93-72-1 H3 102 % 70.0-130 1 11/25/22 06:08 11/30/22 19:01 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/14/2212:34 11/15/2215:29 56-55-3 ND ug/L 8.3 2.3 1 11/14/2212:34 11/15/2215:29 218-01-9 ND ug/L 8.3 2.5 1 11/14/2212:34 11/15/2215:29 53-70-3 ND ug/L 5.0 3.1 1 11/14/2212:34 11/15/2215:29 117-81-7 ND ug/L 8.3 2.4 1 11/14/2212:34 11/15/2215:29 193-39-5 39 % 10-144 1 11/14/2212:34 11/15/2215:29 4165-60-0 34 % 10-130 1 11/14/2212:34 11/15/2215:29 321-60-8 105 % 34-163 1 11/14/2212:34 11/15/2215:29 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.45J ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 06:44 67-64-1 1.8 1 11/15/22 06:44 107-13-1 0.34 1 11/15/22 06:44 71-43-2 0.47 1 11/15/22 06:44 74-97-5 0.31 1 11/15/22 06:44 75-27-4 0.34 1 11/15/22 06:44 75-25-2 1.7 1 11/15/22 06:44 74-83-9 4.0 1 11/15/22 06:44 78-93-3 0.36 1 11/15/22 06:44 75-15-0 0.33 1 11/15/22 06:44 56-23-5 0.28 1 11/15/22 06:44 108-90-7 0.65 1 11/15/22 06:44 75-00-3 0.43 1 11/15/22 06:44 67-66-3 0.54 1 11/15/22 06:44 74-87-3 0.34 1 11/15/22 06:44 96-12-8 0.36 1 11/15/22 06:44 124-48-1 0.27 1 11/15/22 06:44 106-93-4 0.39 1 11/15/22 06:44 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 34 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-15 Lab ID: 92636049004 Collected: 11/07/22 15:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 06:44 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 06:44 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 06:44 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 06:44 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 06:44 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 06:44 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 06:44 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 06:44 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 06:44 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 06:44 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 06:44 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 06:44 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 06:44 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 06:44 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 06:44 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 06:44 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 06:44 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 06:44 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 06:44 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 06:44 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 06:44 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 06:44 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 06:44 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 06:44 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 06:44 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 06:44 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 06:44 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 06:44 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 06:44 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 06:44 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 06:44 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 06:44 95-47-6 102 % 70-130 1 11/15/22 06:44 460-00-4 102 % 70-130 1 11/15/22 06:44 17060-07-0 104 % 70-130 1 11/15/22 06:44 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 22:05 123-91-1 94 % 70-130 1 11/10/22 22:05 17060-07-0 100 % 70-130 1 11/10/22 22:05 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-15 Lab ID: 92636049004 Collected: 11/07/22 15:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 83100 ug/L 5000 5000 1 11/11/22 17:47 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 255000 ug/L 25000 25000 1 11/11/22 12:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:37 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 22800 ug/L 1000 500 1 11/12/22 23:27 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 54700 ug/L 4000 2000 4 11/15/2219:11 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:03 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: EQBL Lab ID: 92636049005 Collected: 11/07/22 16:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Sodium Tin Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.042 0.012 1 11/11/2213:04 11/14/2213:07 309-00-2 ND ug/L 0.042 0.010 1 11/11/2213:04 11/14/2213:07 319-84-6 ND ug/L 0.042 0.012 1 11/11/2213:04 11/14/2213:07 319-86-8 ND ug/L 0.042 0.014 1 11/11/2213:04 11/14/2213:07 72-54-8 ND ug/L 0.042 0.022 1 11/11/2213:04 11/14/2213:07 50-29-3 ND ug/L 0.042 0.014 1 11/11/2213:04 11/14/2213:07 959-98-8 ND ug/L 0.042 0.013 1 11/11/2213:04 11/14/2213:07 33213-65-9 ND ug/L 0.042 0.015 1 11/11/2213:04 11/14/2213:07 72-20-8 ND ug/L 0.042 0.014 1 11 /11 /22 13:04 11 /14/22 13:07 7421-93-4 ND ug/L 0.042 0.016 1 11/11/2213:04 11/14/2213:07 76-44-8 ND ug/L 0.042 0.024 1 11/11/2213:04 11/14/2213:07 1024-57-3 ND ug/L 0.12 0.035 1 11/11/2213:04 11/14/2213:07 72-43-5 52 % 10-182 1 11/11/2213:04 11/14/2213:07 877-09-8 138 % 10-200 1 11 /11 /22 13:04 11 /14/22 13:07 2051-24-3 Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach ND ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:26 7440-23-5 ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:26 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:58 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:58 7440-38-2 Barium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:58 7440-39-3 Beryllium ND ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 14:58 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 14:58 7440-43-9 Chromium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 14:58 7440-47-3 Cobalt ND ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 14:58 7440-48-4 Copper ND ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 14:58 7440-50-8 Iron ND ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 14:58 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 14:58 7439-92-1 Manganese 0.37.11 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 14:58 7439-96-5 Nickel ND ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 14:58 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 14:58 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 14:58 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 14:58 7440-62-2 Zinc 11.5 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 14:58 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 14:58 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: EQBL Lab ID: 92636049005 Collected: 11/07/22 16:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:19 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 19:19 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:19 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 19:19 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 19:19 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 19:19 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 19:19 94-74-6 H3 ND ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 19:19 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 19:19 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 19:19 93-72-1 H3 105 % 70.0-130 1 11/25/22 06:08 11/30/22 19:19 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 9.1 2.4 1 11/14/2212:34 11/15/2215:54 56-55-3 ND ug/L 9.1 2.5 1 11/14/2212:34 11/15/2215:54 218-01-9 ND ug/L 9.1 2.7 1 11/14/2212:34 11/15/2215:54 53-70-3 ND ug/L 5.5 3.4 1 11/14/2212:34 11/15/2215:54 117-81-7 ND ug/L 9.1 2.6 1 11/14/2212:34 11/15/2215:54 193-39-5 35 % 10-144 1 11/14/2212:34 11/15/2215:54 4165-60-0 45 % 10-130 1 11/14/2212:34 11/15/2215:54 321-60-8 105 % 34-163 1 11/14/2212:34 11/15/2215:54 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 04:17 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 04:17 107-13-1 ND ug/L 1.0 0.34 1 11/15/22 04:17 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 04:17 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 04:17 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 04:17 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 04:17 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 04:17 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 04:17 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 04:17 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 04:17 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 04:17 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 04:17 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 04:17 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 04:17 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 04:17 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 04:17 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 04:17 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: EQBL Lab ID: 92636049005 Collected: 11/07/22 16:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 04:17 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 04:17 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 04:17 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 04:17 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 04:17 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 04:17 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 04:17 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 04:17 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 04:17 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 04:17 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 04:17 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 04:17 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 04:17 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 04:17 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 04:17 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 04:17 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 04:17 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 04:17 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 04:17 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 04:17 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 04:17 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 04:17 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 04:17 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 04:17 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 04:17 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 04:17 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 04:17 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 04:17 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 04:17 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 04:17 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 04:17 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 04:17 95-47-6 102 % 70-130 1 11/15/22 04:17 460-00-4 98 % 70-130 1 11/15/22 04:17 17060-07-0 103 % 70-130 1 11/15/22 04:17 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/2219:32 123-91-1 88 % 70-130 1 11/10/2219:32 17060-07-0 98 % 70-130 1 11/10/2219:32 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: EQBL Lab ID: 92636049005 Collected: 11/07/22 16:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 ND ug/L 5000 5000 1 11/11/22 17:56 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND ug/L 25000 25000 1 11/11/22 12:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:38 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/12/22 23:42 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 11/15/2219:14 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:04 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: F13 Lab ID: 92636049006 Collected: 11/09/22 13:25 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.014 1 11/14/22 17:33 11/15/22 14:18 309-00-2 alpha-BHC ND ug/L 0.050 0.012 1 11/14/22 17:33 11/15/22 14:18 319-84-6 delta-BHC ND ug/L 0.050 0.014 1 11/14/22 17:33 11/15/22 14:18 319-86-8 4,4'-DDD ND ug/L 0.050 0.017 1 11/14/22 17:33 11/15/22 14:18 72-54-8 4,4'-DDT ND ug/L 0.050 0.026 1 11/14/22 17:33 11/15/22 14:18 50-29-3 L1 Endosulfan I ND ug/L 0.050 0.017 1 11/14/22 17:33 11/15/22 14:18 959-98-8 Endosulfan 11 ND ug/L 0.050 0.016 1 11/14/22 17:33 11/15/22 14:18 33213-65-9 Endrin ND ug/L 0.050 0.018 1 11/14/22 17:33 11/15/22 14:18 72-20-8 Endrin aldehyde ND ug/L 0.050 0.016 1 11/14/22 17:33 11/15/22 14:18 7421-93-4 Heptachlor ND ug/L 0.050 0.020 1 11/14/22 17:33 11/15/22 14:18 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.028 1 11/14/22 17:33 11/15/22 14:18 1024-57-3 Methoxychlor ND ug/L 0.15 0.042 1 11/14/22 17:33 11/15/22 14:18 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 76 % 10-182 1 11/14/22 17:33 11/15/22 14:18 877-09-8 Decachlorobiphenyl (S) 144 % 10-200 1 11/14/22 17:33 11/15/22 14:18 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium ND ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:36 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:36 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:06 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:06 7440-38-2 Barium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:06 7440-39-3 Beryllium ND ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:06 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:06 7440-43-9 Chromium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:06 7440-47-3 Cobalt ND ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:06 7440-48-4 Copper 0.74.11 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:06 7440-50-8 Iron 6.7J ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:06 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:06 7439-92-1 Manganese ND ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:06 7439-96-5 Nickel ND ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:06 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:06 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:06 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:06 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:06 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 13:22 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: FB Lab ID: 92636049006 Collected: 11/09/22 13:25 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:37 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 19:37 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:37 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 19:37 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 19:37 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 19:37 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 19:37 94-74-6 H3 ND ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 19:37 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 19:37 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 19:37 93-72-1 H3 106 % 70.0-130 1 11/25/22 06:08 11/30/22 19:37 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 9.1 2.4 1 11/15/2215:01 11/16/2214:18 56-55-3 ND ug/L 9.1 2.5 1 11/15/2215:01 11/16/2214:18 218-01-9 ND ug/L 9.1 2.7 1 11/15/2215:01 11/16/2214:18 53-70-3 ND ug/L 5.5 3.4 1 11/15/2215:01 11/16/2214:18 117-81-7 ND ug/L 9.1 2.6 1 11/15/2215:01 11/16/2214:18 193-39-5 74 % 10-144 1 11/15/2215:01 11/16/2214:18 4165-60-0 72 % 10-130 1 11/15/2215:01 11/16/2214:18 321-60-8 97 % 34-163 1 11/15/2215:01 11/16/2214:18 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 02:46 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 02:46 107-13-1 ND ug/L 1.0 0.34 1 11/15/22 02:46 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 02:46 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 02:46 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 02:46 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 02:46 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 02:46 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 02:46 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 02:46 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 02:46 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 02:46 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 02:46 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 02:46 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 02:46 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 02:46 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 02:46 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 02:46 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: FB Lab ID: 92636049006 Collected: 11/09/22 13:25 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 02:46 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 02:46 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 02:46 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 02:46 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 02:46 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 02:46 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 02:46 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 02:46 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 02:46 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 02:46 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 02:46 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 02:46 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 02:46 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 02:46 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 02:46 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 02:46 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 02:46 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 02:46 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 02:46 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 02:46 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 02:46 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 02:46 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 02:46 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 02:46 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 02:46 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 02:46 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 02:46 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 02:46 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 02:46 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 02:46 75-01-4 0.75J ug/L 2.0 0.71 1 11/15/22 02:46 179601-23-1 CO ND ug/L 1.0 0.34 1 11/15/22 02:46 95-47-6 101 % 70-130 1 11/15/22 02:46 460-00-4 95 % 70-130 1 11/15/22 02:46 17060-07-0 102 % 70-130 1 11/15/22 02:46 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/2219:51 123-91-1 90 % 70-130 1 11/10/2219:51 17060-07-0 101 % 70-130 1 11/10/2219:51 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: FB Lab ID: 92636049006 Collected: 11/09/22 13:25 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 ND ug/L 5000 5000 1 11/11/22 21:46 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND ug/L 25000 25000 1 11/14/22 15:17 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:15 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/12/22 23:56 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 11/15/2219:15 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:19 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: DUP-1 Lab ID: 92636049007 Collected: 11/09/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.014 1 11/14/22 17:33 11/15/22 14:31 309-00-2 alpha-BHC ND ug/L 0.050 0.012 1 11/14/22 17:33 11/15/22 14:31 319-84-6 delta-BHC ND ug/L 0.050 0.014 1 11/14/22 17:33 11/15/22 14:31 319-86-8 4,4'-DDD ND ug/L 0.050 0.017 1 11/14/22 17:33 11/15/22 14:31 72-54-8 4,4'-DDT ND ug/L 0.050 0.026 1 11/14/22 17:33 11/15/22 14:31 50-29-3 L1 Endosulfan I ND ug/L 0.050 0.017 1 11/14/22 17:33 11/15/22 14:31 959-98-8 Endosulfan 11 ND ug/L 0.050 0.016 1 11/14/22 17:33 11/15/22 14:31 33213-65-9 Endrin ND ug/L 0.050 0.018 1 11/14/22 17:33 11/15/22 14:31 72-20-8 Endrin aldehyde ND ug/L 0.050 0.016 1 11/14/22 17:33 11/15/22 14:31 7421-93-4 Heptachlor ND ug/L 0.050 0.020 1 11/14/22 17:33 11/15/22 14:31 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.028 1 11/14/22 17:33 11/15/22 14:31 1024-57-3 Methoxychlor ND ug/L 0.15 0.042 1 11/14/22 17:33 11/15/22 14:31 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 107 % 10-182 1 11/14/22 17:33 11/15/22 14:31 877-09-8 Decachlorobiphenyl (S) 176 % 10-200 1 11/14/22 17:33 11/15/22 14:31 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 72000 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:40 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:40 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:09 7440-36-0 Arsenic 1.6 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:09 7440-38-2 Barium 154 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:09 7440-39-3 Beryllium 0.056.11 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:09 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:09 7440-43-9 Chromium 0.62J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:09 7440-47-3 Cobalt 79.0 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:09 7440-48-4 Copper 0.68J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:09 7440-50-8 Iron 2160 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:09 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:09 7439-92-1 Manganese 1170 ug/L 5.0 1.5 5 12/07/22 23:33 12/09/22 15:44 7439-96-5 Nickel 8.6 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:09 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:09 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:09 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:09 7440-62-2 Zinc 5.1 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:09 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 13:29 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 45 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: DUP-1 Lab ID: 92636049007 Collected: 11/09/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual SVOA (LCMS) SW-846 8321 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DB-d3 (S) 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8321 Preparation Method: 8321 Pace National - Mt. Juliet ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:55 94-75-7 H3 ND ug/L 2.00 0.621 1 11/25/22 06:08 11/30/22 19:55 127-20-8 H3 ND ug/L 2.00 1.00 1 11/25/22 06:08 11/30/22 19:55 94-82-6 H3 ND ug/L 2.00 0.548 1 11/25/22 06:08 11/30/22 19:55 1918-00-9 H3 ND ug/L 2.00 0.367 1 11/25/22 06:08 11/30/22 19:55 15165-67-0 H3 ND ug/L 2.00 0.639 1 11/25/22 06:08 11/30/22 19:55 88-85-7 H3 ND ug/L 2.00 0.363 1 11/25/22 06:08 11/30/22 19:55 94-74-6 H3 8.96 ug/L 2.00 0.323 1 11/25/22 06:08 11/30/22 19:55 7085-19-0 H3 ND ug/L 2.00 0.573 1 11/25/22 06:08 11/30/22 19:55 93-76-5 H3 ND ug/L 2.00 0.807 1 11/25/22 06:08 11/30/22 19:55 93-72-1 H3 110 % 70.0-130 1 11/25/22 06:08 11/30/22 19:55 1219802-46- Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/15/2215:01 11/16/2214:44 56-55-3 ND ug/L 8.3 2.3 1 11/15/2215:01 11/16/2214:44 218-01-9 ND ug/L 8.3 2.5 1 11/15/2215:01 11/16/2214:44 53-70-3 ND ug/L 5.0 3.1 1 11/15/2215:01 11/16/2214:44 117-81-7 ND ug/L 8.3 2.4 1 11/15/2215:01 11/16/2214:44 193-39-5 88 % 10-144 1 11/15/2215:01 11/16/2214:44 4165-60-0 82 % 10-130 1 11/15/2215:01 11/16/2214:44 321-60-8 112 % 34-163 1 11/15/2215:01 11/16/2214:44 1718-51-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 08:16 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 08:16 107-13-1 ND ug/L 1.0 0.34 1 11/15/22 08:16 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 08:16 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 08:16 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 08:16 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 08:16 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 08:16 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 08:16 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 08:16 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 08:16 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 08:16 75-00-3 v2 ND ug/L 1.0 0.43 1 11/15/22 08:16 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 08:16 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 08:16 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 08:16 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 08:16 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 08:16 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: DUP-1 Lab ID: 92636049007 Collected: 11/09/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 08:16 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 08:16 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 08:16 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 08:16 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 08:16 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 08:16 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 08:16 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 08:16 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 08:16 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 08:16 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 08:16 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 08:16 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 08:16 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 08:16 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 08:16 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 08:16 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 08:16 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 08:16 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 08:16 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 08:16 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 08:16 127-18-4 9.91 ug/L 10.0 3.5 1 11/15/22 08:16 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 08:16 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 08:16 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 08:16 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 08:16 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 08:16 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 08:16 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 08:16 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 08:16 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 08:16 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 08:16 95-47-6 104 % 70-130 1 11/15/22 08:16 460-00-4 103 % 70-130 1 11/15/22 08:16 17060-07-0 104 % 70-130 1 11/15/22 08:16 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 4.3 ug/L 2.0 0.86 1 11/11/22 05:25 123-91-1 96 % 70-130 1 11/11/22 05:25 17060-07-0 101 % 70-130 1 11/11/22 05:25 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: DUP-1 Lab ID: 92636049007 Collected: 11/09/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 544000 ug/L 5000 5000 1 11/12/22 11:35 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 812000 ug/L 50000 50000 1 11/14/22 15:17 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:16 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 139000 ug/L 3000 1500 3 11/13/22 06:05 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 45300 ug/L 2000 1000 2 11/15/22 20:05 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:20 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 48 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-3R Lab ID: 92636049008 Collected: 11/10/22 09:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 2480 ug/L 2000 540 1 12/08/22 05:42 12/09/22 01:17 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/08/22 05:42 12/09/22 01:17 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/08/22 05:42 12/08/22 16:13 7440-36-0 Arsenic 5.3 ug/L 1.0 0.50 1 12/08/22 05:42 12/08/22 16:13 7440-38-2 Barium 231 ug/L 1.0 0.50 1 12/08/22 05:42 12/08/22 16:13 7440-39-3 Beryllium 0.063J ug/L 0.10 0.033 1 12/08/22 05:42 12/08/22 16:13 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/08/22 05:42 12/08/22 16:13 7440-43-9 Chromium 0.69J ug/L 1.0 0.50 1 12/08/22 05:42 12/08/22 16:13 7440-47-3 Cobalt 12.0 ug/L 1.0 0.24 1 12/08/22 05:42 12/08/22 16:13 7440-48-4 Copper 0.39J ug/L 1.0 0.16 1 12/08/22 05:42 12/08/22 16:13 7440-50-8 Iron 80000 ug/L 200 127 20 12/08/22 05:42 12/09/22 16:29 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/08/22 05:42 12/08/22 16:13 7439-92-1 Manganese 5490 ug/L 20.0 5.8 20 12/08/22 05:42 12/09/22 16:29 7439-96-5 Nickel 0.81J ug/L 1.0 0.26 1 12/08/22 05:42 12/08/22 16:13 7440-02-0 Selenium 0.23J ug/L 2.0 0.20 1 12/08/22 05:42 12/08/22 16:13 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/08/22 05:42 12/08/22 16:13 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/08/22 05:42 12/08/22 16:13 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/08/22 05:42 12/08/22 16:13 7440-66-6 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:31 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 9.1 2.4 1 11/15/2215:01 11/16/2215:35 56-55-3 ND ug/L 9.1 2.5 1 11/15/2215:01 11 /16/22 15:35 218-01-9 ND ug/L 9.1 2.7 1 11/15/2215:01 11/16/2215:35 53-70-3 ND ug/L 5.5 3.4 1 11/15/2215:01 11/16/2215:35 117-81-7 ND ug/L 9.1 2.6 1 11/15/2215:01 11/16/2215:35 193-39-5 67 % 10-144 74 % 10-130 103 % 34-163 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 1 11/15/2215:01 11/16/2215:35 4165-60-0 1 11 /15/22 15:01 11 /16/22 15:35 321-60-8 1 11 /15/22 15:01 11 /16/22 15:35 1718-51-0 5.1 1 11/14/2219:34 67-64-1 1.8 1 11 /14/22 19:34 107-13-1 0.34 1 11 /14/22 19:34 71-43-2 0.47 1 11/14/2219:34 74-97-5 0.31 1 11/14/2219:34 75-27-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 49 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-3R Lab ID: 92636049008 Collected: 11/10/22 09:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/14/2219:34 75-25-2 ND ug/L 2.0 1.7 1 11/14/2219:34 74-83-9 ND ug/L 5.0 4.0 1 11/14/2219:34 78-93-3 ND ug/L 2.0 0.36 1 11/14/2219:34 75-15-0 ND ug/L 1.0 0.33 1 11/14/2219:34 56-23-5 ND ug/L 1.0 0.28 1 11/14/2219:34 108-90-7 ND ug/L 1.0 0.65 1 11/14/2219:34 75-00-3 ND ug/L 1.0 0.43 1 11/14/2219:34 67-66-3 ND ug/L 1.0 0.54 1 11/14/2219:34 74-87-3 ND ug/L 2.0 0.34 1 11/14/2219:34 96-12-8 ND ug/L 1.0 0.36 1 11/14/2219:34 124-48-1 ND ug/L 1.0 0.27 1 11/14/2219:34 106-93-4 ND ug/L 1.0 0.39 1 11/14/2219:34 74-95-3 ND ug/L 1.0 0.34 1 11/14/2219:34 95-50-1 ND ug/L 1.0 0.33 1 11/14/2219:34 106-46-7 ND ug/L 1.0 0.56 1 11/14/2219:34 110-57-6 ND ug/L 1.0 0.35 1 11/14/2219:34 75-71-8 ND ug/L 1.0 0.37 1 11/14/2219:34 75-34-3 ND ug/L 1.0 0.32 1 11/14/2219:34 107-06-2 ND ug/L 1.0 0.35 1 11/14/2219:34 75-35-4 ND ug/L 1.0 0.38 1 11/14/2219:34 156-59-2 ND ug/L 1.0 0.40 1 11/14/2219:34 156-60-5 ND ug/L 1.0 0.36 1 11/14/2219:34 78-87-5 ND ug/L 1.0 0.36 1 11 /14/22 19:34 10061-01-5 ND ug/L 1.0 0.36 1 11/14/2219:34 10061-02-6 ND ug/L 1.0 0.30 1 11/14/2219:34 100-41-4 ND ug/L 5.0 0.48 1 11/14/2219:34 591-78-6 ND ug/L 20.0 9.7 1 11/14/2219:34 74-88-4 ND ug/L 5.0 2.0 1 11/14/2219:34 75-09-2 ND ug/L 5.0 2.7 1 11/14/2219:34 108-10-1 ND ug/L 1.0 0.29 1 11/14/2219:34 100-42-5 ND ug/L 1.0 0.31 1 11/14/2219:34 630-20-6 ND ug/L 1.0 0.22 1 11/14/2219:34 79-34-5 ND ug/L 1.0 0.29 1 11/14/2219:34 127-18-4 ND ug/L 10.0 3.5 1 11/14/2219:34 109-99-9 ND ug/L 1.0 0.24 1 11/14/2219:34 108-88-3 ND ug/L 1.0 0.33 1 11/14/2219:34 71-55-6 ND ug/L 1.0 0.32 1 11/14/2219:34 79-00-5 ND ug/L 1.0 0.38 1 11/14/2219:34 79-01-6 ND ug/L 1.0 0.30 1 11/14/2219:34 75-69-4 ND ug/L 1.0 0.26 1 11/14/2219:34 96-18-4 ND ug/L 2.0 1.3 1 11/14/2219:34 108-05-4 ND ug/L 1.0 0.39 1 11/14/2219:34 75-01-4 ND ug/L 2.0 0.71 1 11/14/2219:34 179601-23-1 ND ug/L 1.0 0.34 1 11/14/2219:34 95-47-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 50 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-3R Lab ID: 92636049008 Collected: 11/10/22 09:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 100 % 70-130 1 11/14/2219:34 460-00-4 96 % 70-130 1 11/14/2219:34 17060-07-0 104 % 70-130 1 11/14/2219:34 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 22:24 123-91-1 90 % 70-130 1 11/10/22 22:24 17060-07-0 99 % 70-130 1 11/10/22 22:24 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 130000 ug/L 5000 5000 1 11/11/22 21:58 Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville 121000 ug/L 25000 25000 1 11/15/2217:49 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 22.0 1 11/15/22 04:23 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 1760 ug/L 1000 500 1 11/13/22 00:56 14808-79-8 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville 2860 ug/L 1000 500 1 11/15/2219:17 16887-00-6 Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville ND ug/L 8.0 6.0 1 11/22/22 18:02 11/22/22 22:17 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-2 Lab ID: 92636049009 Collected: 11/07/22 13:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 18800 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:43 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:43 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:11 7440-36-0 Arsenic 0.55J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:11 7440-38-2 Barium 143 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:11 7440-39-3 Beryllium 0.034J ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:11 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:11 7440-43-9 Chromium 0.68J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:11 7440-47-3 Cobalt 1.4 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:11 7440-48-4 Copper 0.55J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:11 7440-50-8 Iron 4170 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:11 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:11 7439-92-1 Manganese 2990 ug/L 10.0 2.9 10 12/07/22 23:33 12/09/22 15:46 7439-96-5 Nickel 2.2 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:11 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:11 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:11 7440-22-4 Vanadium 0.991 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:11 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:11 7440-66-6 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:33 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/14/2212:34 11/15/22 16:20 56-55-3 ND ug/L 8.3 2.3 1 11/14/2212:34 11 /15/22 16:20 218-01-9 ND ug/L 8.3 2.5 1 11/14/2212:34 11/15/22 16:20 53-70-3 ND ug/L 5.0 3.1 1 11/14/2212:34 11 /15/22 16:20 117-81-7 ND ug/L 8.3 2.4 1 11/14/2212:34 11 /15/22 16:20 193-39-5 17 % 10-144 32 % 10-130 78 % 34-163 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 1 11/14/2212:34 11/15/22 16:20 4165-60-0 1 11 /14/22 12:34 11/15/22 16:20 321-60-8 1 11 /14/22 12:34 11/15/22 16:20 1718-51-0 5.1 1 11/15/22 04:36 67-64-1 1.8 1 11/15/22 04:36 107-13-1 0.34 1 11/15/22 04:36 71-43-2 0.47 1 11/15/22 04:36 74-97-5 0.31 1 11/15/22 04:36 75-27-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 52 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-2 Lab ID: 92636049009 Collected: 11/07/22 13:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 11/15/22 04:36 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 04:36 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 04:36 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 04:36 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 04:36 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 04:36 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 04:36 75-00-3 ND ug/L 1.0 0.43 1 11/15/22 04:36 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 04:36 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 04:36 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 04:36 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 04:36 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 04:36 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 04:36 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 04:36 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 04:36 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 04:36 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 04:36 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 04:36 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 04:36 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 04:36 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 04:36 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 04:36 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 04:36 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 04:36 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 04:36 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 04:36 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 04:36 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 04:36 75-09-2 ND ug/L 5.0 2.7 1 11/15/22 04:36 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 04:36 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 04:36 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 04:36 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 04:36 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 04:36 109-99-9 0.30J ug/L 1.0 0.24 1 11/15/22 04:36 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 04:36 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 04:36 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 04:36 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 04:36 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 04:36 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 04:36 108-05-4 ND ug/L 1.0 0.39 1 11/15/22 04:36 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 04:36 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 04:36 95-47-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 v2 v2 Page 53 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-2 Lab ID: 92636049009 Collected: 11/07/22 13:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 102 % 70-130 1 11/15/22 04:36 460-00-4 99 % 70-130 1 11/15/22 04:36 17060-07-0 104 % 70-130 1 11/15/22 04:36 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 4.4 ug/L 2.0 0.86 1 11/10/22 22:43 123-91-1 88 % 70-130 1 11/10/22 22:43 17060-07-0 97 % 70-130 1 11/10/22 22:43 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 140000 ug/L 5000 5000 1 11/11/2218:00 Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville 245000 ug/L 25000 25000 1 11/11/2212:02 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 22.0 1 11/11/22 03:38 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 11700 ug/L 1000 500 1 11/13/22 01:40 14808-79-8 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville 27200 ug/L 1000 500 1 11/15/2219:18 16887-00-6 Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville ND ug/L 8.0 6.0 1 11 /21 /22 17:50 11 /21 /22 22:04 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 54 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-5R Lab ID: 92636049010 Collected: 11/09/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 13300 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:47 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:47 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:14 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:14 7440-38-2 Barium 59.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:14 7440-39-3 Beryllium ND ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:14 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:14 7440-43-9 Chromium 6.6 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:14 7440-47-3 Cobalt ND ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:14 7440-48-4 Copper 0.25J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:14 7440-50-8 Iron 42.5 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:14 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:14 7439-92-1 Manganese 1.0 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:14 7439-96-5 Nickel 1.2 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:14 7440-02-0 Selenium 0.23J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:14 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:14 7440-22-4 Vanadium 5.5 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:14 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:14 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:36 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11 /14/22 19:51 67-64-1 1.8 1 11 /14/22 19:51 107-13-1 0.34 1 11 /14/22 19:51 71-43-2 0.47 1 11 /14/22 19:51 74-97-5 0.31 1 11 /14/22 19:51 75-27-4 0.34 1 11 /14/22 19:51 75-25-2 1.7 1 11 /14/22 19:51 74-83-9 4.0 1 11 /14/22 19:51 78-93-3 0.36 1 11 /14/22 19:51 75-15-0 0.33 1 11 /14/22 19:51 56-23-5 0.28 1 11 /14/22 19:51 108-90-7 0.65 1 11 /14/22 19:51 75-00-3 0.43 1 11 /14/22 19:51 67-66-3 0.54 1 11 /14/22 19:51 74-87-3 0.34 1 11 /14/22 19:51 96-12-8 0.36 1 11 /14/22 19:51 124-48-1 0.27 1 11 /14/22 19:51 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 55 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-5R Lab ID: 92636049010 Collected: 11/09/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) [**- 1]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/14/2219:51 74-95-3 ND ug/L 1.0 0.34 1 11/14/2219:51 95-50-1 ND ug/L 1.0 0.33 1 11/14/2219:51 106-46-7 ND ug/L 1.0 0.56 1 11/14/2219:51 110-57-6 ND ug/L 1.0 0.35 1 11/14/2219:51 75-71-8 v2 ND ug/L 1.0 0.37 1 11/14/2219:51 75-34-3 ND ug/L 1.0 0.32 1 11/14/2219:51 107-06-2 ND ug/L 1.0 0.35 1 11/14/2219:51 75-35-4 ND ug/L 1.0 0.38 1 11/14/2219:51 156-59-2 ND ug/L 1.0 0.40 1 11/14/2219:51 156-60-5 ND ug/L 1.0 0.36 1 11/14/2219:51 78-87-5 ND ug/L 1.0 0.36 1 11 /14/22 19:51 10061-01-5 ND ug/L 1.0 0.36 1 11/14/2219:51 10061-02-6 ND ug/L 1.0 0.30 1 11/14/2219:51 100-41-4 ND ug/L 5.0 0.48 1 11/14/2219:51 591-78-6 ND ug/L 20.0 9.7 1 11/14/2219:51 74-88-4 ND ug/L 5.0 2.0 1 11/14/2219:51 75-09-2 ND ug/L 5.0 2.7 1 11/14/2219:51 108-10-1 ND ug/L 1.0 0.29 1 11/14/2219:51 100-42-5 ND ug/L 1.0 0.31 1 11/14/2219:51 630-20-6 ND ug/L 1.0 0.22 1 11/14/2219:51 79-34-5 ND ug/L 1.0 0.29 1 11/14/2219:51 127-18-4 ND ug/L 10.0 3.5 1 11/14/2219:51 109-99-9 ND ug/L 1.0 0.24 1 11/14/2219:51 108-88-3 ND ug/L 1.0 0.33 1 11/14/2219:51 71-55-6 ND ug/L 1.0 0.32 1 11/14/2219:51 79-00-5 ND ug/L 1.0 0.38 1 11/14/2219:51 79-01-6 ND ug/L 1.0 0.30 1 11/14/2219:51 75-69-4 ND ug/L 1.0 0.26 1 11/14/2219:51 96-18-4 ND ug/L 2.0 1.3 1 11/14/2219:51 108-05-4 ND ug/L 1.0 0.39 1 11/14/2219:51 75-01-4 ND ug/L 2.0 0.71 1 11/14/2219:51 179601-23-1 ND ug/L 1.0 0.34 1 11/14/2219:51 95-47-6 98 % 70-130 1 11/14/2219:51 460-00-4 92 % 70-130 1 11/14/2219:51 17060-07-0 105 % 70-130 1 11/14/2219:51 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 23:02 123-91-1 90 % 70-130 1 11/10/22 23:02 17060-07-0 97 % 70-130 1 11/10/22 23:02 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 56 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-5R Lab ID: 92636049010 Collected: 11/09/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 33900 ug/L 5000 5000 1 11/11/22 22:09 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 159000 ug/L 25000 25000 1 11/15/22 13:05 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:16 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 8420 ug/L 1000 500 1 11/13/22 01:55 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 14700 ug/L 1000 500 1 11/15/2219:19 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:21 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 57 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-8 Lab ID: 92636049011 Collected: 11/09/22 10:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 11200 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:50 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:50 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:16 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:16 7440-38-2 Barium 60.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:16 7440-39-3 Beryllium 0.47 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:16 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:16 7440-43-9 Chromium 3.8 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:16 7440-47-3 Cobalt ND ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:16 7440-48-4 Copper ND ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:16 7440-50-8 Iron 74.3 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:16 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:16 7439-92-1 Manganese 5.3 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:16 7439-96-5 Nickel 0.31J ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:16 7440-02-0 Selenium 1.2J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:16 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:16 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:16 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:16 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:38 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/14/22 20:08 67-64-1 1.8 1 11/14/22 20:08 107-13-1 0.34 1 11/14/22 20:08 71-43-2 0.47 1 11/14/22 20:08 74-97-5 0.31 1 11/14/22 20:08 75-27-4 0.34 1 11/14/22 20:08 75-25-2 1.7 1 11/14/22 20:08 74-83-9 4.0 1 11/14/22 20:08 78-93-3 0.36 1 11/14/22 20:08 75-15-0 0.33 1 11/14/22 20:08 56-23-5 0.28 1 11/14/22 20:08 108-90-7 0.65 1 11/14/22 20:08 75-00-3 0.43 1 11/14/22 20:08 67-66-3 0.54 1 11/14/22 20:08 74-87-3 0.34 1 11/14/22 20:08 96-12-8 0.36 1 11/14/22 20:08 124-48-1 0.27 1 11/14/22 20:08 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 58 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-8 Lab ID: 92636049011 Collected: 11/09/22 10:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y*-:11]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/14/22 20:08 74-95-3 ND ug/L 1.0 0.34 1 11/14/22 20:08 95-50-1 ND ug/L 1.0 0.33 1 11/14/22 20:08 106-46-7 ND ug/L 1.0 0.56 1 11/14/22 20:08 110-57-6 ND ug/L 1.0 0.35 1 11/14/22 20:08 75-71-8 v2 ND ug/L 1.0 0.37 1 11/14/22 20:08 75-34-3 ND ug/L 1.0 0.32 1 11/14/22 20:08 107-06-2 ND ug/L 1.0 0.35 1 11/14/22 20:08 75-35-4 ND ug/L 1.0 0.38 1 11/14/22 20:08 156-59-2 ND ug/L 1.0 0.40 1 11/14/22 20:08 156-60-5 ND ug/L 1.0 0.36 1 11/14/22 20:08 78-87-5 ND ug/L 1.0 0.36 1 11/14/22 20:08 10061-01-5 ND ug/L 1.0 0.36 1 11/14/22 20:08 10061-02-6 ND ug/L 1.0 0.30 1 11/14/22 20:08 100-41-4 ND ug/L 5.0 0.48 1 11/14/22 20:08 591-78-6 ND ug/L 20.0 9.7 1 11/14/22 20:08 74-88-4 ND ug/L 5.0 2.0 1 11/14/22 20:08 75-09-2 ND ug/L 5.0 2.7 1 11/14/22 20:08 108-10-1 ND ug/L 1.0 0.29 1 11/14/22 20:08 100-42-5 ND ug/L 1.0 0.31 1 11/14/22 20:08 630-20-6 ND ug/L 1.0 0.22 1 11/14/22 20:08 79-34-5 ND ug/L 1.0 0.29 1 11/14/22 20:08 127-18-4 ND ug/L 10.0 3.5 1 11/14/22 20:08 109-99-9 ND ug/L 1.0 0.24 1 11/14/22 20:08 108-88-3 ND ug/L 1.0 0.33 1 11/14/22 20:08 71-55-6 ND ug/L 1.0 0.32 1 11/14/22 20:08 79-00-5 ND ug/L 1.0 0.38 1 11/14/22 20:08 79-01-6 ND ug/L 1.0 0.30 1 11/14/22 20:08 75-69-4 ND ug/L 1.0 0.26 1 11/14/22 20:08 96-18-4 ND ug/L 2.0 1.3 1 11/14/22 20:08 108-05-4 ND ug/L 1.0 0.39 1 11/14/22 20:08 75-01-4 ND ug/L 2.0 0.71 1 11/14/22 20:08 179601-23-1 ND ug/L 1.0 0.34 1 11/14/22 20:08 95-47-6 95 % 70-130 1 11/14/22 20:08 460-00-4 93 % 70-130 1 11/14/22 20:08 17060-07-0 104 % 70-130 1 11/14/22 20:08 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 23:21 123-91-1 93 % 70-130 1 11/10/22 23:21 17060-07-0 99 % 70-130 1 11/10/22 23:21 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-8 Lab ID: 92636049011 Collected: 11/09/22 10:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 29300 ug/L 5000 5000 1 11/11/22 22:16 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 86000 ug/L 25000 25000 1 11/15/22 13:05 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:17 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 8290 ug/L 1000 500 1 11/13/22 02:10 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3710 ug/L 1000 500 1 11/15/2219:20 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:25 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 60 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-9 Lab ID: 92636049012 Collected: 11/09/22 09:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 14600 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:54 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:54 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:19 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:19 7440-38-2 Barium 191 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:19 7440-39-3 Beryllium 0.26 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:19 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:19 7440-43-9 Chromium 0.61J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:19 7440-47-3 Cobalt ND ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:19 7440-48-4 Copper 0.37J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:19 7440-50-8 Iron 142 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:19 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:19 7439-92-1 Manganese 6.2 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:19 7439-96-5 Nickel 0.58J ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:19 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:19 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:19 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:19 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:19 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:45 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/14/22 20:25 67-64-1 1.8 1 11/14/22 20:25 107-13-1 0.34 1 11/14/22 20:25 71-43-2 0.47 1 11/14/22 20:25 74-97-5 0.31 1 11/14/22 20:25 75-27-4 0.34 1 11/14/22 20:25 75-25-2 1.7 1 11/14/22 20:25 74-83-9 4.0 1 11/14/22 20:25 78-93-3 0.36 1 11/14/22 20:25 75-15-0 0.33 1 11/14/22 20:25 56-23-5 0.28 1 11/14/22 20:25 108-90-7 0.65 1 11/14/22 20:25 75-00-3 0.43 1 11/14/22 20:25 67-66-3 0.54 1 11/14/22 20:25 74-87-3 0.34 1 11/14/22 20:25 96-12-8 0.36 1 11/14/22 20:25 124-48-1 0.27 1 11/14/22 20:25 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 61 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-9 Lab ID: 92636049012 Collected: 11/09/22 09:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) [**- 1]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/14/22 20:25 74-95-3 ND ug/L 1.0 0.34 1 11/14/22 20:25 95-50-1 ND ug/L 1.0 0.33 1 11/14/22 20:25 106-46-7 ND ug/L 1.0 0.56 1 11/14/22 20:25 110-57-6 0.35.1 ug/L 1.0 0.35 1 11/14/22 20:25 75-71-8 v3 ND ug/L 1.0 0.37 1 11/14/22 20:25 75-34-3 ND ug/L 1.0 0.32 1 11/14/22 20:25 107-06-2 ND ug/L 1.0 0.35 1 11/14/22 20:25 75-35-4 ND ug/L 1.0 0.38 1 11/14/22 20:25 156-59-2 ND ug/L 1.0 0.40 1 11/14/22 20:25 156-60-5 ND ug/L 1.0 0.36 1 11/14/22 20:25 78-87-5 ND ug/L 1.0 0.36 1 11/14/22 20:25 10061-01-5 ND ug/L 1.0 0.36 1 11/14/22 20:25 10061-02-6 ND ug/L 1.0 0.30 1 11/14/22 20:25 100-41-4 ND ug/L 5.0 0.48 1 11/14/22 20:25 591-78-6 ND ug/L 20.0 9.7 1 11/14/22 20:25 74-88-4 ND ug/L 5.0 2.0 1 11/14/22 20:25 75-09-2 ND ug/L 5.0 2.7 1 11/14/22 20:25 108-10-1 ND ug/L 1.0 0.29 1 11/14/22 20:25 100-42-5 ND ug/L 1.0 0.31 1 11/14/22 20:25 630-20-6 ND ug/L 1.0 0.22 1 11/14/22 20:25 79-34-5 ND ug/L 1.0 0.29 1 11/14/22 20:25 127-18-4 ND ug/L 10.0 3.5 1 11/14/22 20:25 109-99-9 ND ug/L 1.0 0.24 1 11/14/22 20:25 108-88-3 ND ug/L 1.0 0.33 1 11/14/22 20:25 71-55-6 ND ug/L 1.0 0.32 1 11/14/22 20:25 79-00-5 ND ug/L 1.0 0.38 1 11/14/22 20:25 79-01-6 0.37J ug/L 1.0 0.30 1 11/14/22 20:25 75-69-4 ND ug/L 1.0 0.26 1 11/14/22 20:25 96-18-4 ND ug/L 2.0 1.3 1 11/14/22 20:25 108-05-4 ND ug/L 1.0 0.39 1 11/14/22 20:25 75-01-4 ND ug/L 2.0 0.71 1 11/14/22 20:25 179601-23-1 ND ug/L 1.0 0.34 1 11/14/22 20:25 95-47-6 96 % 70-130 1 11/14/22 20:25 460-00-4 92 % 70-130 1 11/14/22 20:25 17060-07-0 105 % 70-130 1 11/14/22 20:25 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/10/22 23:40 123-91-1 91 % 70-130 1 11/10/22 23:40 17060-07-0 99 % 70-130 1 11/10/22 23:40 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 62 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-9 Lab ID: 92636049012 Collected: 11/09/22 09:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 29200 ug/L 5000 5000 1 11/11/22 22:22 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 139000 ug/L 25000 25000 1 11/15/22 13:05 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:17 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 807J ug/L 1000 500 1 11/13/22 02:25 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3690 ug/L 1000 500 1 11/15/2219:21 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:26 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 63 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-11 Lab ID: 92636049013 Collected: 11/08/22 13:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 11900 ug/L 2000 540 1 12/07/22 23:33 12/08/22 14:57 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 14:57 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:21 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:21 7440-38-2 Barium 69.6 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:21 7440-39-3 Beryllium 0.067J ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:21 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:21 7440-43-9 Chromium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:21 7440-47-3 Cobalt 2.2 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:21 7440-48-4 Copper 0.27J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:21 7440-50-8 Iron 21200 ug/L 50.0 31.8 5 12/07/22 23:33 12/09/22 15:49 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:21 7439-92-1 Manganese 1380 ug/L 5.0 1.5 5 12/07/22 23:33 12/09/22 15:49 7439-96-5 Nickel 0.67J ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:21 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:21 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:21 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:21 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:21 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:47 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 05:12 67-64-1 1.8 1 11/15/22 05:12 107-13-1 0.34 1 11/15/22 05:12 71-43-2 0.47 1 11/15/22 05:12 74-97-5 0.31 1 11/15/22 05:12 75-27-4 0.34 1 11/15/22 05:12 75-25-2 1.7 1 11/15/22 05:12 74-83-9 4.0 1 11/15/22 05:12 78-93-3 0.36 1 11/15/22 05:12 75-15-0 0.33 1 11/15/22 05:12 56-23-5 0.28 1 11/15/22 05:12 108-90-7 0.65 1 11/15/22 05:12 75-00-3 0.43 1 11/15/22 05:12 67-66-3 0.54 1 11/15/22 05:12 74-87-3 0.34 1 11/15/22 05:12 96-12-8 0.36 1 11/15/22 05:12 124-48-1 0.27 1 11/15/22 05:12 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 64 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-11 Lab ID: 92636049013 Collected: 11/08/22 13:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y*-:11]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 05:12 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 05:12 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 05:12 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 05:12 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 05:12 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 05:12 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 05:12 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 05:12 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 05:12 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 05:12 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 05:12 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 05:12 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 05:12 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 05:12 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 05:12 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 05:12 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 05:12 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 05:12 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 05:12 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 05:12 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 05:12 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 05:12 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 05:12 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 05:12 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 05:12 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 05:12 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 05:12 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 05:12 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 05:12 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 05:12 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 05:12 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 05:12 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 05:12 95-47-6 103 % 70-130 1 11/15/22 05:12 460-00-4 104 % 70-130 1 11/15/22 05:12 17060-07-0 103 % 70-130 1 11/15/22 05:12 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/11/22 00:00 123-91-1 87 % 70-130 1 11/11/22 00:00 17060-07-0 96 % 70-130 1 11/11/22 00:00 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 65 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-11 Lab ID: 92636049013 Collected: 11/08/22 13:05 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 106000 ug/L 5000 5000 1 11/11/22 20:29 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 173000 ug/L 25000 25000 1 11/13/22 13:57 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:48 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 9830 ug/L 1000 500 1 11/13/22 02:39 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 8540 ug/L 1000 500 1 11/15/2219:22 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:16 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 66 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-12 Lab ID: 92636049014 Collected: 11/08/22 11:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 23700 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:19 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:19 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:24 7440-36-0 Arsenic 0.57J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:24 7440-38-2 Barium 161 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:24 7440-39-3 Beryllium 0.063J ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:24 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:24 7440-43-9 Chromium 0.77J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:24 7440-47-3 Cobalt 5.5 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:24 7440-48-4 Copper 0.86J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:24 7440-50-8 Iron 1290 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:24 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:24 7439-92-1 Manganese 5160 ug/L 10.0 2.9 10 12/07/22 23:33 12/09/22 15:52 7439-96-5 Nickel 9.0 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:24 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:24 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:24 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:24 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:24 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:49 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 0.36J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 05:31 67-64-1 1.8 1 11/15/22 05:31 107-13-1 0.34 1 11/15/22 05:31 71-43-2 0.47 1 11/15/22 05:31 74-97-5 0.31 1 11/15/22 05:31 75-27-4 0.34 1 11/15/22 05:31 75-25-2 1.7 1 11/15/22 05:31 74-83-9 4.0 1 11/15/22 05:31 78-93-3 0.36 1 11/15/22 05:31 75-15-0 0.33 1 11/15/22 05:31 56-23-5 0.28 1 11/15/22 05:31 108-90-7 0.65 1 11/15/22 05:31 75-00-3 0.43 1 11/15/22 05:31 67-66-3 0.54 1 11/15/22 05:31 74-87-3 0.34 1 11/15/22 05:31 96-12-8 0.36 1 11/15/22 05:31 124-48-1 0.27 1 11/15/22 05:31 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 67 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-12 Lab ID: 92636049014 Collected: 11/08/22 11:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y*-:11]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 05:31 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 05:31 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 05:31 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 05:31 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 05:31 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 05:31 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 05:31 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 05:31 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 05:31 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 05:31 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 05:31 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 05:31 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 05:31 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 05:31 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 05:31 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 05:31 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 05:31 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 05:31 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 05:31 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 05:31 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 05:31 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 05:31 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 05:31 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 05:31 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 05:31 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 05:31 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 05:31 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 05:31 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 05:31 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 05:31 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 05:31 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 05:31 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 05:31 95-47-6 102 % 70-130 1 11/15/22 05:31 460-00-4 104 % 70-130 1 11/15/22 05:31 17060-07-0 104 % 70-130 1 11/15/22 05:31 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 6.1 ug/L 2.0 0.86 1 11/11/22 00:19 123-91-1 95 % 70-130 1 11/11/22 00:19 17060-07-0 98 % 70-130 1 11/11/22 00:19 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 68 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-12 Lab ID: 92636049014 Collected: 11/08/22 11:10 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 294000 ug/L 5000 5000 1 11/12/22 11:06 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 496000 ug/L 25000 25000 1 11/13/22 13:57 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:49 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 94600 ug/L 1000 500 1 11/13/22 02:54 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 28200 ug/L 1000 500 1 11/15/2219:23 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:17 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-13 Lab ID: 92636049015 Collected: 11/08/22 10:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 17800 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:22 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:22 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:26 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:26 7440-38-2 Barium 515 ug/L 2.0 1.0 2 12/07/22 23:33 12/09/22 15:54 7440-39-3 Beryllium 1.8 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:26 7440-41-7 Cadmium 0.072J ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:26 7440-43-9 Chromium ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:26 7440-47-3 Cobalt 0.56J ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:26 7440-48-4 Copper 0.62J ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:26 7440-50-8 Iron 183 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:26 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:26 7439-92-1 Manganese 119 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:26 7439-96-5 Nickel 2.2 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:26 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:26 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:26 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:26 7440-62-2 Zinc 8.9 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:26 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 0.151 ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:52 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 05:49 67-64-1 1.8 1 11/15/22 05:49 107-13-1 0.34 1 11/15/22 05:49 71-43-2 0.47 1 11/15/22 05:49 74-97-5 0.31 1 11/15/22 05:49 75-27-4 0.34 1 11/15/22 05:49 75-25-2 1.7 1 11/15/22 05:49 74-83-9 4.0 1 11/15/22 05:49 78-93-3 0.36 1 11/15/22 05:49 75-15-0 0.33 1 11/15/22 05:49 56-23-5 0.28 1 11/15/22 05:49 108-90-7 0.65 1 11/15/22 05:49 75-00-3 0.43 1 11/15/22 05:49 67-66-3 0.54 1 11/15/22 05:49 74-87-3 0.34 1 11/15/22 05:49 96-12-8 0.36 1 11/15/22 05:49 124-48-1 0.27 1 11/15/22 05:49 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 70 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-13 Lab ID: 92636049015 Collected: 11/08/22 10:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y*-:11]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 05:49 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 05:49 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 05:49 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 05:49 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 05:49 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 05:49 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 05:49 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 05:49 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 05:49 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 05:49 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 05:49 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 05:49 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 05:49 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 05:49 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 05:49 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 05:49 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 05:49 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 05:49 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 05:49 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 05:49 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 05:49 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 05:49 127-18-4 10.1 ug/L 10.0 3.5 1 11/15/22 05:49 109-99-9 v3 ND ug/L 1.0 0.24 1 11/15/22 05:49 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 05:49 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 05:49 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 05:49 79-01-6 0.45J ug/L 1.0 0.30 1 11/15/22 05:49 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 05:49 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 05:49 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 05:49 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 05:49 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 05:49 95-47-6 101 % 70-130 1 11/15/22 05:49 460-00-4 104 % 70-130 1 11/15/22 05:49 17060-07-0 102 % 70-130 1 11/15/22 05:49 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 7.7 ug/L 2.0 0.86 1 11/11/22 00:38 123-91-1 85 % 70-130 1 11/11/22 00:38 17060-07-0 97 % 70-130 1 11/11/22 00:38 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 71 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-13 Lab ID: 92636049015 Collected: 11/08/22 10:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 84400 ug/L 5000 5000 1 11/11/22 20:49 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 272000 ug/L 25000 25000 1 11/13/22 13:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:49 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 27300 ug/L 1000 500 1 11/13/22 03:09 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 47300 ug/L 2000 1000 2 11/15/22 20:06 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:15 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 72 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-14 Lab ID: 92636049016 Collected: 11/08/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 18000 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:25 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:25 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:29 7440-36-0 Arsenic ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:29 7440-38-2 Barium 249 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:29 7440-39-3 Beryllium 0.69 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:29 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:29 7440-43-9 Chromium 0.97J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:29 7440-47-3 Cobalt 0.27J ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:29 7440-48-4 Copper 1.1 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:29 7440-50-8 Iron 50.9 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:29 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:29 7439-92-1 Manganese 48.6 ug/L 1.0 0.29 1 12/07/22 23:33 12/08/22 15:29 7439-96-5 Nickel 4.6 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:29 7440-02-0 Selenium ND ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:29 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:29 7440-22-4 Vanadium ND ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:29 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:29 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:54 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 07:39 67-64-1 1.8 1 11/15/22 07:39 107-13-1 0.34 1 11/15/22 07:39 71-43-2 0.47 1 11/15/22 07:39 74-97-5 0.31 1 11/15/22 07:39 75-27-4 0.34 1 11/15/22 07:39 75-25-2 1.7 1 11/15/22 07:39 74-83-9 4.0 1 11/15/22 07:39 78-93-3 0.36 1 11/15/22 07:39 75-15-0 0.33 1 11/15/22 07:39 56-23-5 0.28 1 11/15/22 07:39 108-90-7 0.65 1 11/15/22 07:39 75-00-3 0.43 1 11/15/22 07:39 67-66-3 0.54 1 11/15/22 07:39 74-87-3 0.34 1 11/15/22 07:39 96-12-8 0.36 1 11/15/22 07:39 124-48-1 0.27 1 11/15/22 07:39 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 73 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-14 Lab ID: 92636049016 Collected: 11/08/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y*-:11]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 07:39 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 07:39 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 07:39 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 07:39 110-57-6 3.7 ug/L 1.0 0.35 1 11/15/22 07:39 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 07:39 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 07:39 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 07:39 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 07:39 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 07:39 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 07:39 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 07:39 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 07:39 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 07:39 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 07:39 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 07:39 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 07:39 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 07:39 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 07:39 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 07:39 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 07:39 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 07:39 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 07:39 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 07:39 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 07:39 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 07:39 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 07:39 79-01-6 1.7 ug/L 1.0 0.30 1 11/15/22 07:39 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 07:39 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 07:39 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 07:39 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 07:39 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 07:39 95-47-6 101 % 70-130 1 11/15/22 07:39 460-00-4 107 % 70-130 1 11/15/22 07:39 17060-07-0 104 % 70-130 1 11/15/22 07:39 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/11/22 03:30 123-91-1 91 % 70-130 1 11/11/22 03:30 17060-07-0 103 % 70-130 1 11/11/22 03:30 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 74 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-14 Lab ID: 92636049016 Collected: 11/08/22 15:35 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 63100 ug/L 5000 5000 1 11/11/22 21:03 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 158000 ug/L 25000 25000 1 11/13/22 13:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:49 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/13/22 03:53 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3910 ug/L 1000 500 1 11/15/2219:27 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:16 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 75 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-1 Lab ID: 92636049017 Collected: 11/06/22 14:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 13100 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:29 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:29 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:37 7440-36-0 Arsenic 0.71J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:37 7440-38-2 Barium 45.9 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:37 7440-39-3 Beryllium 0.11 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:37 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:37 7440-43-9 Chromium 2.5 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:37 7440-47-3 Cobalt 1.9 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:37 7440-48-4 Copper 4.0 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:37 7440-50-8 Iron 6950 ug/L 20.0 12.7 2 12/07/22 23:33 12/09/22 15:57 7439-89-6 Lead 2.4 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:37 7439-92-1 Manganese 721 ug/L 2.0 0.58 2 12/07/22 23:33 12/09/22 15:57 7439-96-5 Nickel 1.7 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:37 7440-02-0 Selenium 0.37J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:37 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:37 7440-22-4 Vanadium 4.7 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:37 7440-62-2 Zinc 22.9 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:37 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:56 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 03:59 67-64-1 1.8 1 11/15/22 03:59 107-13-1 0.34 1 11/15/22 03:59 71-43-2 0.47 1 11/15/22 03:59 74-97-5 0.31 1 11/15/22 03:59 75-27-4 0.34 1 11/15/22 03:59 75-25-2 1.7 1 11/15/22 03:59 74-83-9 4.0 1 11/15/22 03:59 78-93-3 0.36 1 11/15/22 03:59 75-15-0 0.33 1 11/15/22 03:59 56-23-5 0.28 1 11/15/22 03:59 108-90-7 0.65 1 11/15/22 03:59 75-00-3 0.43 1 11/15/22 03:59 67-66-3 0.54 1 11/15/22 03:59 74-87-3 0.34 1 11/15/22 03:59 96-12-8 0.36 1 11/15/22 03:59 124-48-1 0.27 1 11/15/22 03:59 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 76 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-1 Lab ID: 92636049017 Collected: 11/06/22 14:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) [**- 1]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 03:59 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 03:59 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 03:59 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 03:59 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 03:59 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 03:59 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 03:59 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 03:59 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 03:59 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 03:59 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 03:59 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 03:59 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 03:59 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 03:59 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 03:59 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 03:59 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 03:59 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 03:59 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 03:59 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 03:59 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 03:59 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 03:59 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 03:59 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 03:59 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 03:59 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 03:59 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 03:59 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 03:59 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 03:59 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 03:59 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 03:59 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 03:59 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 03:59 95-47-6 101 % 70-130 1 11/15/22 03:59 460-00-4 104 % 70-130 1 11/15/22 03:59 17060-07-0 103 % 70-130 1 11/15/22 03:59 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/11/22 03:49 123-91-1 91 % 70-130 1 11/11/22 03:49 17060-07-0 100 % 70-130 1 11/11/22 03:49 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 77 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-1 Lab ID: 92636049017 Collected: 11/06/22 14:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 41700 ug/L 5000 5000 1 11/11/22 16:57 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 88000 ug/L 25000 25000 1 11/11/22 11:55 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:35 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 2840 ug/L 1000 500 1 11/13/22 04:08 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 19500 ug/L 1000 500 1 11/15/2219:30 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/22 17:27 11/17/22 21:19 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 78 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-3 Lab ID: 92636049018 Collected: 11/07/22 12:20 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 16800 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:32 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:32 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:39 7440-36-0 Arsenic 2.0 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:39 7440-38-2 Barium 367 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:39 7440-39-3 Beryllium 0.40 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:39 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:39 7440-43-9 Chromium 9.4 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:39 7440-47-3 Cobalt 4.5 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:39 7440-48-4 Copper 16.5 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:39 7440-50-8 Iron 37400 ug/L 100 63.7 10 12/07/22 23:33 12/09/22 15:59 7439-89-6 Lead 6.7 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:39 7439-92-1 Manganese 2690 ug/L 10.0 2.9 10 12/07/22 23:33 12/09/22 15:59 7439-96-5 Nickel 5.8 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:39 7440-02-0 Selenium 1.2J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:39 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:39 7440-22-4 Vanadium 21.4 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:39 7440-62-2 Zinc 51.8 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:39 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 13:58 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 13.2J ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 04:54 67-64-1 1.8 1 11/15/22 04:54 107-13-1 0.34 1 11/15/22 04:54 71-43-2 0.47 1 11/15/22 04:54 74-97-5 0.31 1 11/15/22 04:54 75-27-4 0.34 1 11/15/22 04:54 75-25-2 1.7 1 11/15/22 04:54 74-83-9 4.0 1 11/15/22 04:54 78-93-3 0.36 1 11/15/22 04:54 75-15-0 0.33 1 11/15/22 04:54 56-23-5 0.28 1 11/15/22 04:54 108-90-7 0.65 1 11/15/22 04:54 75-00-3 0.43 1 11/15/22 04:54 67-66-3 0.54 1 11/15/22 04:54 74-87-3 0.34 1 11/15/22 04:54 96-12-8 0.36 1 11/15/22 04:54 124-48-1 0.27 1 11/15/22 04:54 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 79 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-3 Lab ID: 92636049018 Collected: 11/07/22 12:20 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) [**- 1]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 04:54 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 04:54 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 04:54 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 04:54 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 04:54 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 04:54 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 04:54 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 04:54 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 04:54 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 04:54 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 04:54 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 04:54 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 04:54 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 04:54 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 04:54 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 04:54 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 04:54 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 04:54 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 04:54 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 04:54 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 04:54 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 04:54 127-18-4 ND ug/L 10.0 3.5 1 11/15/22 04:54 109-99-9 v2 0.26J ug/L 1.0 0.24 1 11/15/22 04:54 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 04:54 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 04:54 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 04:54 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 04:54 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 04:54 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 04:54 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 04:54 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 04:54 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 04:54 95-47-6 103 % 70-130 1 11/15/22 04:54 460-00-4 105 % 70-130 1 11/15/22 04:54 17060-07-0 104 % 70-130 1 11/15/22 04:54 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/11/22 04:08 123-91-1 94 % 70-130 1 11/11/22 04:08 17060-07-0 97 % 70-130 1 11/11/22 04:08 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 80 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-3 Lab ID: 92636049018 Collected: 11/07/22 12:20 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 234000 ug/L 5000 5000 1 11/12/22 10:37 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 312000 ug/L 25000 25000 1 11/11/22 12:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:38 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 34000 ug/L 1000 500 1 11/13/22 20:39 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 20600 ug/L 1000 500 1 11/15/2219:33 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:05 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 81 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-4 Lab ID: 92636049019 Collected: 11/07/22 12:50 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 35500 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:35 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:35 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:42 7440-36-0 Arsenic 0.97J ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:42 7440-38-2 Barium 263 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:42 7440-39-3 Beryllium 0.22 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:42 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:42 7440-43-9 Chromium 5.3 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:42 7440-47-3 Cobalt 5.9 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:42 7440-48-4 Copper 5.5 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:42 7440-50-8 Iron 10800 ug/L 200 127 20 12/07/22 23:33 12/09/22 16:07 7439-89-6 Lead 2.4 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:42 7439-92-1 Manganese 6200 ug/L 20.0 5.8 20 12/07/22 23:33 12/09/22 16:07 7439-96-5 Nickel 6.4 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:42 7440-02-0 Selenium 0.65J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:42 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:42 7440-22-4 Vanadium 12.7 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:42 7440-62-2 Zinc 17.8 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:42 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Date: 12/12/2022 05:09 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11 /21 /22 08:11 11 /28/22 14:01 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/15/22 07:02 67-64-1 1.8 1 11/15/22 07:02 107-13-1 0.34 1 11/15/22 07:02 71-43-2 0.47 1 11/15/22 07:02 74-97-5 0.31 1 11/15/22 07:02 75-27-4 0.34 1 11/15/22 07:02 75-25-2 1.7 1 11/15/22 07:02 74-83-9 4.0 1 11/15/22 07:02 78-93-3 0.36 1 11/15/22 07:02 75-15-0 0.33 1 11/15/22 07:02 56-23-5 0.28 1 11/15/22 07:02 108-90-7 0.65 1 11/15/22 07:02 75-00-3 0.43 1 11/15/22 07:02 67-66-3 0.54 1 11/15/22 07:02 74-87-3 0.34 1 11/15/22 07:02 96-12-8 0.36 1 11/15/22 07:02 124-48-1 0.27 1 11/15/22 07:02 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 82 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-4 Lab ID: 92636049019 Collected: 11/07/22 12:50 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) [**- 1]H�46yTAyI�4 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.39 1 11/15/22 07:02 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 07:02 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 07:02 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 07:02 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 07:02 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 07:02 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 07:02 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 07:02 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 07:02 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 07:02 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 07:02 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 07:02 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 07:02 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 07:02 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 07:02 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 07:02 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 07:02 75-09-2 v2 ND ug/L 5.0 2.7 1 11/15/22 07:02 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 07:02 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 07:02 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 07:02 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 07:02 127-18-4 5.2J ug/L 10.0 3.5 1 11/15/22 07:02 109-99-9 v2 ND ug/L 1.0 0.24 1 11/15/22 07:02 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 07:02 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 07:02 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 07:02 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 07:02 75-69-4 ND ug/L 1.0 0.26 1 11/15/22 07:02 96-18-4 ND ug/L 2.0 1.3 1 11/15/22 07:02 108-05-4 v2 ND ug/L 1.0 0.39 1 11/15/22 07:02 75-01-4 ND ug/L 2.0 0.71 1 11/15/22 07:02 179601-23-1 ND ug/L 1.0 0.34 1 11/15/22 07:02 95-47-6 103 % 70-130 1 11/15/22 07:02 460-00-4 104 % 70-130 1 11/15/22 07:02 17060-07-0 105 % 70-130 1 11/15/22 07:02 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 5.6 ug/L 2.0 0.86 1 11/11/22 04:27 123-91-1 96 % 70-130 1 11/11/22 04:27 17060-07-0 98 % 70-130 1 11/11/22 04:27 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 83 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: SW-4 Lab ID: 92636049019 Collected: 11/07/22 12:50 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 351000 ug/L 5000 5000 1 11/12/22 10:47 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 511000 ug/L 25000 25000 1 11/11/22 12:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:39 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 46500 ug/L 1000 500 1 11/13/22 21:25 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 43500 ug/L 2000 1000 2 11/15/22 20:06 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/21/22 17:50 11/21/22 22:06 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 84 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-7 Lab ID: 92636049020 Collected: 11/09/22 12:55 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.045 0.013 1 11/14/22 17:33 11/15/22 14:43 309-00-2 alpha-BHC ND ug/L 0.045 0.011 1 11/14/22 17:33 11/15/22 14:43 319-84-6 delta-BHC ND ug/L 0.045 0.013 1 11/14/22 17:33 11/15/22 14:43 319-86-8 4,4'-DDD ND ug/L 0.045 0.015 1 11/14/22 17:33 11/15/22 14:43 72-54-8 4,4'-DDT ND ug/L 0.045 0.023 1 11/14/22 17:33 11/15/22 14:43 50-29-3 L1 Endosulfan I ND ug/L 0.045 0.016 1 11/14/22 17:33 11/15/22 14:43 959-98-8 Endosulfan 11 ND ug/L 0.045 0.014 1 11/14/22 17:33 11/15/22 14:43 33213-65-9 Endrin ND ug/L 0.045 0.016 1 11/14/22 17:33 11/15/22 14:43 72-20-8 Endrin aldehyde ND ug/L 0.045 0.015 1 11/14/22 17:33 11/15/22 14:43 7421-93-4 Heptachlor ND ug/L 0.045 0.018 1 11/14/22 17:33 11/15/22 14:43 76-44-8 Heptachlor epoxide ND ug/L 0.045 0.026 1 11/14/22 17:33 11/15/22 14:43 1024-57-3 Methoxychlor ND ug/L 0.14 0.038 1 11/14/22 17:33 11/15/22 14:43 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 180 % 10-182 1 11/14/22 17:33 11/15/22 14:43 877-09-8 Decachlorobiphenyl (S) 133 % 10-200 1 11/14/22 17:33 11/15/22 14:43 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 43900 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:39 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:39 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:44 7440-36-0 Arsenic 0.62.11 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:44 7440-38-2 Barium 283 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:44 7440-39-3 Beryllium 0.49 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:44 7440-41-7 Cadmium 0.16 ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:44 7440-43-9 Chromium 0.80.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:44 7440-47-3 Cobalt 3.8 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:44 7440-48-4 Copper 3.5 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:44 7440-50-8 Iron 413 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:44 7439-89-6 Lead ND ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:44 7439-92-1 Manganese 657 ug/L 2.0 0.58 2 12/07/22 23:33 12/09/22 16:10 7439-96-5 Nickel 5.2 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:44 7440-02-0 Selenium 0.25.11 ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:44 7782-49-2 Silver 0.047.11 ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:44 7440-22-4 Vanadium 1.1 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:44 7440-62-2 Zinc 16.9 ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:44 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 0.17J ug/L 0.20 0.12 1 11/21/22 08:11 11/28/22 14:03 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 85 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-7 Lab ID: 92636049020 Collected: 11/09/22 12:55 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/14/22 20:43 67-64-1 ND ug/L 10.0 1.8 1 11/14/22 20:43 107-13-1 0.95J ug/L 1.0 0.34 1 11/14/22 20:43 71-43-2 ND ug/L 1.0 0.47 1 11/14/22 20:43 74-97-5 ND ug/L 1.0 0.31 1 11/14/22 20:43 75-27-4 ND ug/L 1.0 0.34 1 11/14/22 20:43 75-25-2 ND ug/L 2.0 1.7 1 11/14/22 20:43 74-83-9 ND ug/L 5.0 4.0 1 11/14/22 20:43 78-93-3 ND ug/L 2.0 0.36 1 11/14/22 20:43 75-15-0 ND ug/L 1.0 0.33 1 11/14/22 20:43 56-23-5 ND ug/L 1.0 0.28 1 11/14/22 20:43 108-90-7 ND ug/L 1.0 0.65 1 11/14/22 20:43 75-00-3 ND ug/L 1.0 0.43 1 11/14/22 20:43 67-66-3 ND ug/L 1.0 0.54 1 11/14/22 20:43 74-87-3 ND ug/L 2.0 0.34 1 11/14/22 20:43 96-12-8 ND ug/L 1.0 0.36 1 11/14/22 20:43 124-48-1 ND ug/L 1.0 0.27 1 11/14/22 20:43 106-93-4 ND ug/L 1.0 0.39 1 11/14/22 20:43 74-95-3 ND ug/L 1.0 0.34 1 11/14/22 20:43 95-50-1 ND ug/L 1.0 0.33 1 11/14/22 20:43 106-46-7 ND ug/L 1.0 0.56 1 11/14/22 20:43 110-57-6 ND ug/L 1.0 0.35 1 11/14/22 20:43 75-71-8 0.87J ug/L 1.0 0.37 1 11/14/22 20:43 75-34-3 ND ug/L 1.0 0.32 1 11/14/22 20:43 107-06-2 ND ug/L 1.0 0.35 1 11/14/22 20:43 75-35-4 1.0.1 ug/L 1.0 0.38 1 11/14/22 20:43 156-59-2 ND ug/L 1.0 0.40 1 11/14/22 20:43 156-60-5 ND ug/L 1.0 0.36 1 11/14/22 20:43 78-87-5 ND ug/L 1.0 0.36 1 11/14/22 20:43 10061-01-5 ND ug/L 1.0 0.36 1 11/14/22 20:43 10061-02-6 ND ug/L 1.0 0.30 1 11/14/22 20:43 100-41-4 ND ug/L 5.0 0.48 1 11/14/22 20:43 591-78-6 ND ug/L 20.0 9.7 1 11/14/22 20:43 74-88-4 ND ug/L 5.0 2.0 1 11/14/22 20:43 75-09-2 ND ug/L 5.0 2.7 1 11/14/22 20:43 108-10-1 ND ug/L 1.0 0.29 1 11/14/22 20:43 100-42-5 ND ug/L 1.0 0.31 1 11/14/22 20:43 630-20-6 ND ug/L 1.0 0.22 1 11/14/22 20:43 79-34-5 ND ug/L 1.0 0.29 1 11/14/22 20:43 127-18-4 48.0 ug/L 10.0 3.5 1 11/14/22 20:43 109-99-9 ND ug/L 1.0 0.24 1 11/14/22 20:43 108-88-3 ND ug/L 1.0 0.33 1 11/14/22 20:43 71-55-6 ND ug/L 1.0 0.32 1 11/14/22 20:43 79-00-5 ND ug/L 1.0 0.38 1 11/14/22 20:43 79-01-6 0.96J ug/L 1.0 0.30 1 11/14/22 20:43 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 86 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-7 Lab ID: 92636049020 Collected: 11/09/22 12:55 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/14/22 20:43 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/14/22 20:43 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/14/22 20:43 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/14/22 20:43 179601-23-1 o-Xylene 0.44.1 ug/L 1.0 0.34 1 11/14/22 20:43 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 11/14/22 20:43 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 11/14/22 20:43 17060-07-0 Toluene-d8 (S) 107 % 70-130 1 11/14/22 20:43 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 7.8 ug/L 2.0 0.86 1 11/11/22 04:47 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 11/11/22 04:47 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 11/11/22 04:47 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 265000 ug/L 5000 5000 1 11/12/22 11:44 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 510000 ug/L 25000 25000 1 11/15/22 13:05 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/15/22 04:18 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 98400 ug/L 2000 1000 2 11/14/2212:07 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 32500 ug/L 1000 500 1 11/15/2219:39 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:27 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 87 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-10 Lab ID: 92636049021 Collected: 11/08/22 14:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.045 0.013 1 11/14/22 17:33 11/15/22 13:53 309-00-2 alpha-BHC ND ug/L 0.045 0.011 1 11/14/22 17:33 11/15/22 13:53 319-84-6 delta-BHC ND ug/L 0.045 0.013 1 11/14/22 17:33 11/15/22 13:53 319-86-8 4,4'-DDD ND ug/L 0.045 0.015 1 11/14/22 17:33 11/15/22 13:53 72-54-8 4,4'-DDT ND ug/L 0.045 0.023 1 11/14/22 17:33 11/15/22 13:53 50-29-3 L1 Endosulfan I ND ug/L 0.045 0.016 1 11/14/22 17:33 11/15/22 13:53 959-98-8 Endosulfan 11 ND ug/L 0.045 0.014 1 11/14/22 17:33 11/15/22 13:53 33213-65-9 Endrin ND ug/L 0.045 0.016 1 11/14/22 17:33 11/15/22 13:53 72-20-8 Endrin aldehyde ND ug/L 0.045 0.015 1 11/14/22 17:33 11/15/22 13:53 7421-93-4 Heptachlor ND ug/L 0.045 0.018 1 11/14/22 17:33 11/15/22 13:53 76-44-8 Heptachlor epoxide ND ug/L 0.045 0.026 1 11/14/22 17:33 11/15/22 13:53 1024-57-3 Methoxychlor ND ug/L 0.14 0.038 1 11/14/22 17:33 11/15/22 13:53 72-43-5 L1 Surrogates Tetrachloro-m-xylene (S) 73 % 10-182 1 11/14/22 17:33 11/15/22 13:53 877-09-8 Decachlorobiphenyl (S) 180 % 10-200 1 11/14/22 17:33 11/15/22 13:53 2051-24-3 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Sodium 112000 ug/L 2000 540 1 12/07/22 23:33 12/08/22 15:42 7440-23-5 Tin ND ug/L 50.0 16.0 1 12/07/22 23:33 12/08/22 15:42 7440-31-5 6020 MET ICPMS Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach Antimony ND ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:47 7440-36-0 Arsenic 0.90.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:47 7440-38-2 Barium 93.0 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:47 7440-39-3 Beryllium 0.17 ug/L 0.10 0.033 1 12/07/22 23:33 12/08/22 15:47 7440-41-7 Cadmium ND ug/L 0.10 0.067 1 12/07/22 23:33 12/08/22 15:47 7440-43-9 Chromium 2.1 ug/L 1.0 0.50 1 12/07/22 23:33 12/08/22 15:47 7440-47-3 Cobalt 5.8 ug/L 1.0 0.24 1 12/07/22 23:33 12/08/22 15:47 7440-48-4 Copper 0.69.11 ug/L 1.0 0.16 1 12/07/22 23:33 12/08/22 15:47 7440-50-8 Iron 2460 ug/L 10.0 6.4 1 12/07/22 23:33 12/08/22 15:47 7439-89-6 Lead 0.51.1 ug/L 1.0 0.22 1 12/07/22 23:33 12/08/22 15:47 7439-92-1 Manganese 21100 ug/L 50.0 14.6 50 12/07/22 23:33 12/09/22 16:12 7439-96-5 Nickel 10.5 ug/L 1.0 0.26 1 12/07/22 23:33 12/08/22 15:47 7440-02-0 Selenium 1.4J ug/L 2.0 0.20 1 12/07/22 23:33 12/08/22 15:47 7782-49-2 Silver ND ug/L 0.50 0.028 1 12/07/22 23:33 12/08/22 15:47 7440-22-4 Vanadium 1.5 ug/L 1.0 0.91 1 12/07/22 23:33 12/08/22 15:47 7440-62-2 Zinc ND ug/L 5.0 4.3 1 12/07/22 23:33 12/08/22 15:47 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/26/2211:43 11/28/2215:09 7439-97-6 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 88 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-10 Lab ID: 92636049021 Collected: 11/08/22 14:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/15/22 07:57 67-64-1 ND ug/L 10.0 1.8 1 11/15/22 07:57 107-13-1 0.63J ug/L 1.0 0.34 1 11/15/22 07:57 71-43-2 ND ug/L 1.0 0.47 1 11/15/22 07:57 74-97-5 ND ug/L 1.0 0.31 1 11/15/22 07:57 75-27-4 ND ug/L 1.0 0.34 1 11/15/22 07:57 75-25-2 ND ug/L 2.0 1.7 1 11/15/22 07:57 74-83-9 ND ug/L 5.0 4.0 1 11/15/22 07:57 78-93-3 ND ug/L 2.0 0.36 1 11/15/22 07:57 75-15-0 ND ug/L 1.0 0.33 1 11/15/22 07:57 56-23-5 ND ug/L 1.0 0.28 1 11/15/22 07:57 108-90-7 ND ug/L 1.0 0.65 1 11/15/22 07:57 75-00-3 ND ug/L 1.0 0.43 1 11/15/22 07:57 67-66-3 ND ug/L 1.0 0.54 1 11/15/22 07:57 74-87-3 ND ug/L 2.0 0.34 1 11/15/22 07:57 96-12-8 ND ug/L 1.0 0.36 1 11/15/22 07:57 124-48-1 ND ug/L 1.0 0.27 1 11/15/22 07:57 106-93-4 ND ug/L 1.0 0.39 1 11/15/22 07:57 74-95-3 ND ug/L 1.0 0.34 1 11/15/22 07:57 95-50-1 ND ug/L 1.0 0.33 1 11/15/22 07:57 106-46-7 ND ug/L 1.0 0.56 1 11/15/22 07:57 110-57-6 ND ug/L 1.0 0.35 1 11/15/22 07:57 75-71-8 ND ug/L 1.0 0.37 1 11/15/22 07:57 75-34-3 ND ug/L 1.0 0.32 1 11/15/22 07:57 107-06-2 ND ug/L 1.0 0.35 1 11/15/22 07:57 75-35-4 ND ug/L 1.0 0.38 1 11/15/22 07:57 156-59-2 ND ug/L 1.0 0.40 1 11/15/22 07:57 156-60-5 ND ug/L 1.0 0.36 1 11/15/22 07:57 78-87-5 ND ug/L 1.0 0.36 1 11/15/22 07:57 10061-01-5 ND ug/L 1.0 0.36 1 11/15/22 07:57 10061-02-6 ND ug/L 1.0 0.30 1 11/15/22 07:57 100-41-4 ND ug/L 5.0 0.48 1 11/15/22 07:57 591-78-6 ND ug/L 20.0 9.7 1 11/15/22 07:57 74-88-4 ND ug/L 5.0 2.0 1 11/15/22 07:57 75-09-2 ND ug/L 5.0 2.7 1 11/15/22 07:57 108-10-1 ND ug/L 1.0 0.29 1 11/15/22 07:57 100-42-5 ND ug/L 1.0 0.31 1 11/15/22 07:57 630-20-6 ND ug/L 1.0 0.22 1 11/15/22 07:57 79-34-5 ND ug/L 1.0 0.29 1 11/15/22 07:57 127-18-4 74.3 ug/L 10.0 3.5 1 11/15/22 07:57 109-99-9 ND ug/L 1.0 0.24 1 11/15/22 07:57 108-88-3 ND ug/L 1.0 0.33 1 11/15/22 07:57 71-55-6 ND ug/L 1.0 0.32 1 11/15/22 07:57 79-00-5 ND ug/L 1.0 0.38 1 11/15/22 07:57 79-01-6 ND ug/L 1.0 0.30 1 11/15/22 07:57 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 v3 Page 89 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: MW-10 Lab ID: 92636049021 Collected: 11/08/22 14:15 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/15/22 07:57 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/15/22 07:57 108-05-4 v2 Vinyl chloride ND ug/L 1.0 0.39 1 11/15/22 07:57 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/15/22 07:57 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/15/22 07:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 104 % 70-130 1 11/15/22 07:57 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 11/15/22 07:57 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 11/15/22 07:57 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 5.7 ug/L 2.0 0.86 1 11/11/22 05:06 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 11/11/22 05:06 17060-07-0 Toluene-d8 (S) 95 % 70-130 1 11/11/22 05:06 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 919000 ug/L 5000 5000 1 11/12/22 11:15 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 1220000 ug/L 50000 50000 1 11/13/22 13:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 11/11/22 03:50 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 146000 ug/L 3000 1500 3 11/14/2212:22 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 51400 ug/L 2000 1000 2 11/15/22 20:07 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/22/22 17:27 11/22/22 21:17 57-12-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 90 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: TB-1 Lab ID: 92636049022 Collected: 11/10/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/14/2218:42 67-64-1 ND ug/L 10.0 1.8 1 11/14/2218:42 107-13-1 ND ug/L 1.0 0.34 1 11/14/2218:42 71-43-2 ND ug/L 1.0 0.47 1 11/14/2218:42 74-97-5 ND ug/L 1.0 0.31 1 11/14/2218:42 75-27-4 ND ug/L 1.0 0.34 1 11/14/2218:42 75-25-2 ND ug/L 2.0 1.7 1 11/14/2218:42 74-83-9 ND ug/L 5.0 4.0 1 11/14/2218:42 78-93-3 ND ug/L 2.0 0.36 1 11/14/2218:42 75-15-0 ND ug/L 1.0 0.33 1 11/14/2218:42 56-23-5 ND ug/L 1.0 0.28 1 11/14/2218:42 108-90-7 ND ug/L 1.0 0.65 1 11/14/2218:42 75-00-3 ND ug/L 1.0 0.43 1 11/14/2218:42 67-66-3 ND ug/L 1.0 0.54 1 11/14/2218:42 74-87-3 ND ug/L 2.0 0.34 1 11/14/2218:42 96-12-8 ND ug/L 1.0 0.36 1 11/14/2218:42 124-48-1 ND ug/L 1.0 0.27 1 11/14/2218:42 106-93-4 ND ug/L 1.0 0.39 1 11/14/2218:42 74-95-3 ND ug/L 1.0 0.34 1 11/14/2218:42 95-50-1 ND ug/L 1.0 0.33 1 11/14/2218:42 106-46-7 ND ug/L 1.0 0.56 1 11/14/2218:42 110-57-6 ND ug/L 1.0 0.35 1 11/14/2218:42 75-71-8 ND ug/L 1.0 0.37 1 11/14/2218:42 75-34-3 ND ug/L 1.0 0.32 1 11/14/2218:42 107-06-2 ND ug/L 1.0 0.35 1 11/14/2218:42 75-35-4 ND ug/L 1.0 0.38 1 11/14/2218:42 156-59-2 ND ug/L 1.0 0.40 1 11/14/2218:42 156-60-5 ND ug/L 1.0 0.36 1 11/14/2218:42 78-87-5 ND ug/L 1.0 0.36 1 11 /14/22 18:42 10061-01-5 ND ug/L 1.0 0.36 1 11/14/2218:42 10061-02-6 ND ug/L 1.0 0.30 1 11/14/2218:42 100-41-4 ND ug/L 5.0 0.48 1 11/14/2218:42 591-78-6 ND ug/L 20.0 9.7 1 11/14/2218:42 74-88-4 ND ug/L 5.0 2.0 1 11/14/2218:42 75-09-2 ND ug/L 5.0 2.7 1 11/14/2218:42 108-10-1 ND ug/L 1.0 0.29 1 11/14/2218:42 100-42-5 ND ug/L 1.0 0.31 1 11/14/2218:42 630-20-6 ND ug/L 1.0 0.22 1 11/14/2218:42 79-34-5 ND ug/L 1.0 0.29 1 11/14/2218:42 127-18-4 ND ug/L 10.0 3.5 1 11/14/2218:42 109-99-9 ND ug/L 1.0 0.24 1 11/14/2218:42 108-88-3 ND ug/L 1.0 0.33 1 11/14/2218:42 71-55-6 ND ug/L 1.0 0.32 1 11/14/2218:42 79-00-5 ND ug/L 1.0 0.38 1 11/14/2218:42 79-01-6 ND ug/L 1.0 0.30 1 11/14/2218:42 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 91 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: T13-1 Parameters Lab ID: Results 92636049022 Units Collected: Report Limit 11/10/22 00:00 MDL DF Received: 11/10/22 16:10 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/14/22 18:42 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/14/22 18:42 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/14/22 18:42 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/14/22 18:42 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/14/22 18:42 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/14/22 18:42 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/14/22 18:42 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 11/14/22 18:42 2037-26-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 92 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: TB-2 Lab ID: 92636049023 Collected: 11/10/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/14/2219:00 67-64-1 ND ug/L 10.0 1.8 1 11/14/2219:00 107-13-1 ND ug/L 1.0 0.34 1 11/14/2219:00 71-43-2 ND ug/L 1.0 0.47 1 11/14/2219:00 74-97-5 ND ug/L 1.0 0.31 1 11/14/2219:00 75-27-4 ND ug/L 1.0 0.34 1 11/14/2219:00 75-25-2 ND ug/L 2.0 1.7 1 11/14/2219:00 74-83-9 ND ug/L 5.0 4.0 1 11/14/2219:00 78-93-3 ND ug/L 2.0 0.36 1 11/14/2219:00 75-15-0 ND ug/L 1.0 0.33 1 11/14/2219:00 56-23-5 ND ug/L 1.0 0.28 1 11/14/2219:00 108-90-7 ND ug/L 1.0 0.65 1 11/14/2219:00 75-00-3 ND ug/L 1.0 0.43 1 11/14/2219:00 67-66-3 ND ug/L 1.0 0.54 1 11/14/2219:00 74-87-3 ND ug/L 2.0 0.34 1 11/14/2219:00 96-12-8 ND ug/L 1.0 0.36 1 11/14/2219:00 124-48-1 ND ug/L 1.0 0.27 1 11/14/2219:00 106-93-4 ND ug/L 1.0 0.39 1 11/14/2219:00 74-95-3 ND ug/L 1.0 0.34 1 11/14/2219:00 95-50-1 ND ug/L 1.0 0.33 1 11/14/2219:00 106-46-7 ND ug/L 1.0 0.56 1 11/14/2219:00 110-57-6 ND ug/L 1.0 0.35 1 11/14/2219:00 75-71-8 ND ug/L 1.0 0.37 1 11/14/2219:00 75-34-3 ND ug/L 1.0 0.32 1 11/14/2219:00 107-06-2 ND ug/L 1.0 0.35 1 11/14/2219:00 75-35-4 ND ug/L 1.0 0.38 1 11/14/2219:00 156-59-2 ND ug/L 1.0 0.40 1 11/14/2219:00 156-60-5 ND ug/L 1.0 0.36 1 11/14/2219:00 78-87-5 ND ug/L 1.0 0.36 1 11 /14/22 19:00 10061-01-5 ND ug/L 1.0 0.36 1 11/14/2219:00 10061-02-6 ND ug/L 1.0 0.30 1 11/14/2219:00 100-41-4 ND ug/L 5.0 0.48 1 11/14/2219:00 591-78-6 ND ug/L 20.0 9.7 1 11/14/2219:00 74-88-4 ND ug/L 5.0 2.0 1 11/14/2219:00 75-09-2 ND ug/L 5.0 2.7 1 11/14/2219:00 108-10-1 ND ug/L 1.0 0.29 1 11/14/2219:00 100-42-5 ND ug/L 1.0 0.31 1 11/14/2219:00 630-20-6 ND ug/L 1.0 0.22 1 11/14/2219:00 79-34-5 ND ug/L 1.0 0.29 1 11/14/2219:00 127-18-4 ND ug/L 10.0 3.5 1 11/14/2219:00 109-99-9 ND ug/L 1.0 0.24 1 11/14/2219:00 108-88-3 ND ug/L 1.0 0.33 1 11/14/2219:00 71-55-6 ND ug/L 1.0 0.32 1 11/14/2219:00 79-00-5 ND ug/L 1.0 0.38 1 11/14/2219:00 79-01-6 ND ug/L 1.0 0.30 1 11/14/2219:00 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 93 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: T13-2 Parameters Lab ID: Results 92636049023 Units Collected: Report Limit 11/10/22 00:00 MDL DF Received: 11/10/22 16:10 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/14/22 19:00 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/14/22 19:00 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/14/22 19:00 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/14/22 19:00 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/14/22 19:00 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 11/14/22 19:00 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 11/14/22 19:00 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 11/14/22 19:00 2037-26-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 94 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: TB-3 Lab ID: 92636049024 Collected: 11/10/22 00:00 Received: 11/10/22 16:10 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/12/2022 05:09 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/14/2219:17 67-64-1 ND ug/L 10.0 1.8 1 11/14/2219:17 107-13-1 ND ug/L 1.0 0.34 1 11/14/2219:17 71-43-2 ND ug/L 1.0 0.47 1 11/14/2219:17 74-97-5 ND ug/L 1.0 0.31 1 11/14/2219:17 75-27-4 ND ug/L 1.0 0.34 1 11/14/2219:17 75-25-2 ND ug/L 2.0 1.7 1 11/14/2219:17 74-83-9 ND ug/L 5.0 4.0 1 11/14/2219:17 78-93-3 ND ug/L 2.0 0.36 1 11/14/2219:17 75-15-0 ND ug/L 1.0 0.33 1 11/14/2219:17 56-23-5 ND ug/L 1.0 0.28 1 11/14/2219:17 108-90-7 ND ug/L 1.0 0.65 1 11/14/2219:17 75-00-3 ND ug/L 1.0 0.43 1 11/14/2219:17 67-66-3 ND ug/L 1.0 0.54 1 11/14/2219:17 74-87-3 ND ug/L 2.0 0.34 1 11/14/2219:17 96-12-8 ND ug/L 1.0 0.36 1 11/14/2219:17 124-48-1 ND ug/L 1.0 0.27 1 11/14/2219:17 106-93-4 ND ug/L 1.0 0.39 1 11/14/2219:17 74-95-3 ND ug/L 1.0 0.34 1 11/14/2219:17 95-50-1 ND ug/L 1.0 0.33 1 11/14/2219:17 106-46-7 ND ug/L 1.0 0.56 1 11/14/2219:17 110-57-6 ND ug/L 1.0 0.35 1 11/14/2219:17 75-71-8 ND ug/L 1.0 0.37 1 11/14/2219:17 75-34-3 ND ug/L 1.0 0.32 1 11/14/2219:17 107-06-2 ND ug/L 1.0 0.35 1 11/14/2219:17 75-35-4 ND ug/L 1.0 0.38 1 11/14/2219:17 156-59-2 ND ug/L 1.0 0.40 1 11/14/2219:17 156-60-5 ND ug/L 1.0 0.36 1 11/14/2219:17 78-87-5 ND ug/L 1.0 0.36 1 11 /14/22 19:17 10061-01-5 ND ug/L 1.0 0.36 1 11/14/2219:17 10061-02-6 ND ug/L 1.0 0.30 1 11/14/2219:17 100-41-4 ND ug/L 5.0 0.48 1 11/14/2219:17 591-78-6 ND ug/L 20.0 9.7 1 11/14/2219:17 74-88-4 ND ug/L 5.0 2.0 1 11/14/2219:17 75-09-2 ND ug/L 5.0 2.7 1 11/14/2219:17 108-10-1 ND ug/L 1.0 0.29 1 11/14/2219:17 100-42-5 ND ug/L 1.0 0.31 1 11/14/2219:17 630-20-6 ND ug/L 1.0 0.22 1 11/14/2219:17 79-34-5 ND ug/L 1.0 0.29 1 11/14/2219:17 127-18-4 ND ug/L 10.0 3.5 1 11/14/2219:17 109-99-9 ND ug/L 1.0 0.24 1 11/14/2219:17 108-88-3 ND ug/L 1.0 0.33 1 11/14/2219:17 71-55-6 ND ug/L 1.0 0.32 1 11/14/2219:17 79-00-5 ND ug/L 1.0 0.38 1 11/14/2219:17 79-01-6 ND ug/L 1.0 0.30 1 11/14/2219:17 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 95 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92636049 Sample: T13-3 Parameters Lab ID: Results 92636049024 Units Collected: Report Limit 11/10/22 00:00 MDL DF Received: 11/10/22 16:10 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/14/22 19:17 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/14/22 19:17 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/14/22 19:17 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/14/22 19:17 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/14/22 19:17 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/14/22 19:17 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/14/22 19:17 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 11/14/22 19:17 2037-26-5 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 96 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 738303 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005 METHOD BLANK: 3842370 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 11/28/2214:05 LABORATORY CONTROL SAMPLE: 3842371 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.8 114 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3842372 3842373 MS MSD 92635805001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.8 2.9 112 115 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 738304 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049006,92636049007,92636049008,92636049009,92636049010,92636049011,92636049012, 92636049013, 92636049014, 92636049015, 92636049016, 92636049017, 92636049018, 92636049019, 92636049020 METHOD BLANK: 3842374 Matrix: Water Associated Lab Samples: 92636049006,92636049007,92636049008,92636049009,92636049010,92636049011,92636049012, 92636049013, 92636049014, 92636049015, 92636049016, 92636049017, 92636049018, 92636049019, 92636049020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 11/28/2213:17 LABORATORY CONTROL SAMPLE: 3842375 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.8 113 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3842376 3842377 MS MSD 92636049006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.8 2.7 110 109 75-125 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 739333 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049021 METHOD BLANK: 3847302 Matrix: Water Associated Lab Samples: 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 11/28/2215:05 LABORATORY CONTROL SAMPLE: 3847303 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.9 115 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3847310 3847311 MS MSD 92637103010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.6 101 104 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 877576 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Laboratory: Pace Analytical Services - Ormond Beach Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015, 92636049016,92636049017,92636049018,92636049019,92636049020,92636049021 METHOD BLANK: 4828491 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015, 92636049016,92636049017,92636049018,92636049019,92636049020,92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sodium ug/L ND 2000 540 12/08/2214:01 Tin ug/L ND 50.0 16.0 12/08/2214:01 LABORATORY CONTROL SAMPLE: 4828492 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sodium ug/L 12500 12000 96 80-120 Tin ug/L 1250 1170 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4828493 4828494 MS MSD 92636049013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sodium ug/L 11900 12500 12500 24200 24300 98 99 75-125 0 20 Tin ug/L ND 1250 1250 1160 1160 92 93 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 100 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 877609 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Laboratory: Pace Analytical Services - Ormond Beach Associated Lab Samples: 92636049008 METHOD BLANK: 4828688 Matrix: Water Associated Lab Samples: 92636049008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sodium ug/L ND 2000 540 12/09/22 00:47 Tin ug/L ND 50.0 16.0 12/09/22 00:47 LABORATORY CONTROL SAMPLE: 4828689 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sodium ug/L 12500 12100 97 80-120 Tin ug/L 1250 1250 100 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4828690 4828691 MS MSD 35764153001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sodium ug/L 35.7 mg/L 12500 12500 49300 48000 109 99 75-125 3 20 Tin ug/L 16.01-1 1250 1250 1260 1240 100 99 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 101 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 877575 Analysis Method: EPA 6020 QC Batch Method: EPA 3010 Analysis Description: 6020 MET Laboratory: Pace Analytical Services - Ormond Beach Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015, 92636049016,92636049017,92636049018,92636049019,92636049020,92636049021 METHOD BLANK: 4828487 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015, 92636049016,92636049017,92636049018,92636049019,92636049020,92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 1.0 0.50 12/08/2214:26 Arsenic ug/L ND 1.0 0.50 12/08/2214:26 Barium ug/L ND 1.0 0.50 12/08/2214:26 Beryllium ug/L ND 0.10 0.033 12/08/2214:26 Cadmium ug/L ND 0.10 0.067 12/08/2214:26 Chromium ug/L ND 1.0 0.50 12/08/2214:26 Cobalt ug/L ND 1.0 0.24 12/08/2214:26 Copper ug/L ND 1.0 0.16 12/08/2214:26 Iron ug/L ND 10.0 6.4 12/08/2214:26 Lead ug/L ND 1.0 0.22 12/08/2214:26 Manganese ug/L ND 1.0 0.29 12/08/2214:26 Nickel ug/L ND 1.0 0.26 12/08/2214:26 Selenium ug/L ND 2.0 0.20 12/08/2214:26 Silver ug/L ND 0.50 0.028 12/08/2214:26 Vanadium ug/L ND 1.0 0.91 12/08/2214:26 Zinc ug/L ND 5.0 4.3 12/08/2214:26 LABORATORY CONTROL SAMPLE: Parameter 4828488 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 50 50.0 100 80-120 Arsenic ug/L 50 53.6 107 80-120 Barium ug/L 50 50.5 101 80-120 Beryllium ug/L 5 5.5 110 80-120 Cadmium ug/L 5 5.5 111 80-120 Chromium ug/L 50 54.3 109 80-120 Cobalt ug/L 50 54.2 108 80-120 Copper ug/L 50 55.1 110 80-120 Iron ug/L 500 540 108 80-120 Lead ug/L 50 53.1 106 80-120 Manganese ug/L 50 53.6 107 80-120 Nickel ug/L 50 55.6 111 80-120 Selenium ug/L 50 49.6 99 80-120 Silver ug/L 5 5.7 113 80-120 Vanadium ug/L 50 52.5 105 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 102 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 LABORATORY CONTROL SAMPLE: 4828488 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Zinc ug/L 250 257 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4828489 4828490 MS MSD 92636049001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L 0.56J 50 50 50.4 50.7 100 100 75-125 1 20 Arsenic ug/L ND 50 50 52.7 52.5 105 104 75-125 0 20 Barium ug/L 304 50 50 362 355 116 103 75-125 2 20 Beryllium ug/L 0.46 5 5 5.7 5.8 105 108 75-125 2 20 Cadmium ug/L 0.0901 5 5 5.4 5.4 106 107 75-125 1 20 Chromium ug/L 7.9 50 50 60.9 60.7 106 106 75-125 0 20 Cobalt ug/L 0.74J 50 50 53.4 53.3 105 105 75-125 0 20 Copper ug/L 5.3 50 50 58.2 58.3 106 106 75-125 0 20 Iron ug/L 719 500 500 1250 1210 106 98 75-125 3 20 Lead ug/L 0.46J 50 50 52.3 52.5 104 104 75-125 0 20 Manganese ug/L 63.4 50 50 116 114 105 102 75-125 1 20 Nickel ug/L 5.8 50 50 58.8 58.7 106 106 75-125 0 20 Selenium ug/L 0.39J 50 50 49.2 48.9 98 97 75-125 1 20 Silver ug/L 0.053J 5 5 5.4 5.4 106 107 75-125 1 20 Vanadium ug/L 3.0 50 50 54.9 54.8 104 104 75-125 0 20 Zinc ug/L 15.2 250 250 261 259 98 98 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 877608 Analysis Method: EPA 6020 QC Batch Method: EPA 3010 Analysis Description: 6020 MET Laboratory: Pace Analytical Services - Ormond Beach Associated Lab Samples: 92636049008 METHOD BLANK: 4828684 Associated Lab Samples: 92636049008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 1.0 0.50 12/09/2216:27 Arsenic ug/L ND 1.0 0.50 12/09/2216:27 Barium ug/L ND 1.0 0.50 12/09/2216:27 Beryllium ug/L ND 0.10 0.033 12/09/2216:27 Cadmium ug/L ND 0.10 0.067 12/09/2216:27 Chromium ug/L ND 1.0 0.50 12/09/2216:27 Cobalt ug/L ND 1.0 0.24 12/09/2216:27 Copper ug/L ND 1.0 0.16 12/09/2216:27 Iron ug/L ND 10.0 6.4 12/09/2216:27 Lead ug/L ND 1.0 0.22 12/09/2216:27 Manganese ug/L ND 1.0 0.29 12/09/2216:27 Nickel ug/L ND 1.0 0.26 12/09/2216:27 Selenium ug/L ND 2.0 0.20 12/09/2216:27 Silver ug/L ND 0.50 0.028 12/09/2216:27 Vanadium ug/L ND 1.0 0.91 12/09/2216:27 Zinc ug/L ND 5.0 4.3 12/09/2216:27 LABORATORY CONTROL SAMPLE: Parameter 4828685 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 50 50.6 101 80-120 Arsenic ug/L 50 54.7 109 80-120 Barium ug/L 50 51.7 103 80-120 Beryllium ug/L 5 5.5 109 80-120 Cadmium ug/L 5 5.5 110 80-120 Chromium ug/L 50 54.7 109 80-120 Cobalt ug/L 50 54.2 108 80-120 Copper ug/L 50 53.9 108 80-120 Iron ug/L 500 545 109 80-120 Lead ug/L 50 53.8 108 80-120 Manganese ug/L 50 54.1 108 80-120 Nickel ug/L 50 56.0 112 80-120 Selenium ug/L 50 49.2 98 80-120 Silver ug/L 5 5.6 111 80-120 Vanadium ug/L 50 52.7 105 80-120 Zinc ug/L 250 250 100 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 104 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: OSR LANDFILL 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4828686 4828687 MS MSD 35764153002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L 0.50U 50 50 48.6 49.8 97 99 75-125 2 20 Arsenic ug/L 1.1 50 50 53.7 53.6 105 105 75-125 0 20 Barium ug/L 230 50 50 272 282 84 104 75-125 4 20 Beryllium ug/L 0.033U 5 5 5.3 5.2 105 104 75-125 1 20 Cadmium ug/L 0.71 5 5 5.9 6.0 104 107 75-125 3 20 Chromium ug/L 1.0 50 50 54.2 54.3 106 106 75-125 0 20 Cobalt ug/L 0.84J 50 50 52.4 52.4 103 103 75-125 0 20 Copper ug/L 0.38J 50 50 51.0 51.1 101 101 75-125 0 20 Iron ug/L 712 500 500 1220 1220 102 102 75-125 0 20 Lead ug/L 0.22U 50 50 49.9 50.9 100 102 75-125 2 20 Manganese ug/L 1210 50 50 1240 1250 47 79 75-125 1 20 E Nickel ug/L 8.9 50 50 60.7 61.0 104 104 75-125 1 20 Selenium ug/L 0.20U 50 50 45.9 46.9 92 94 75-125 2 20 Silver ug/L 0.056J 5 5 5.3 5.3 104 105 75-125 1 20 Vanadium ug/L 1.3 50 50 53.8 54.1 105 106 75-125 1 20 Zinc ug/L 4.3U 250 250 230 233 91 92 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 105 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 1964182 Analysis Method: EPA 8321 QC Batch Method: 8321 Analysis Description: SVOA (LCMS) SW-846 8321 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007 METHOD BLANK: R3865905-2 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 1.00 11/29/22 01:41 Dalapon ug/L ND 2.00 0.621 11/29/22 01:41 2,4-DB ug/L ND 2.00 1.00 11/29/22 01:41 Dicamba ug/L ND 2.00 0.548 11/29/22 01:41 Dichloroprop ug/L ND 2.00 0.367 11/29/22 01:41 Dinoseb ug/L ND 2.00 0.639 11/29/22 01:41 MCPA ug/L ND 2.00 0.363 11/29/22 01:41 MCPP ug/L ND 2.00 0.323 11/29/22 01:41 2,4,5-T ug/L ND 2.00 0.573 11/29/22 01:41 2,4,5-TP (Silvex) ug/L ND 2.00 0.807 11/29/22 01:41 2,4-DB-d3 (S) % 109 70.0-130 11/29/22 01:41 LABORATORY CONTROL SAMPLE: R3865905-1 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4-D ug/L 20.0 22.6 113 70.0-130 Dalapon ug/L 20.0 25.0 125 70.0-130 2,4-DB ug/L 20.0 19.3 96.5 70.0-130 Dicamba ug/L 20.0 24.5 123 70.0-130 Dichloroprop ug/L 20.0 21.7 109 70.0-130 Dinoseb ug/L 20.0 23.1 116 70.0-130 MCPA ug/L 20.0 22.4 112 70.0-130 MCPP ug/L 20.0 22.6 113 70.0-130 2,4,5-T ug/L 20.0 19.8 99.0 70.0-130 2,4,5-TP (Silvex) ug/L 20.0 19.6 98.0 70.0-130 2,4-DB-d3 (S) % 100 70.0-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3866878-1 R3866878-2 MS MSD 92636049001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4-D ug/L ND 20.0 20.0 19.4 19.0 97.0 95.0 70.0-130 2.08 30 Dalapon ug/L ND 20.0 20.0 20.8 20.5 104 103 70.0-130 1.45 30 2,4-DB ug/L ND 20.0 20.0 20.1 18.8 101 94.0 70.0-130 6.68 30 Dicamba ug/L ND 20.0 20.0 20.9 20.3 105 102 70.0-130 2.91 30 Dichloroprop ug/L ND 20.0 20.0 20.6 19.9 103 99.5 70.0-130 3.46 30 Dinoseb ug/L ND 20.0 20.0 18.3 17.8 91.5 89.0 70.0-130 2.77 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 106 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: OSR LANDFILL 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3866878-1 R3866878-2 MS MSD 92636049001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual MCPA ug/L ND 20.0 20.0 20.6 20.2 103 101 70.0-130 1.96 30 MCPP ug/L ND 20.0 20.0 19.9 19.9 99.5 99.5 70.0-130 0.00 30 2,4,5-T ug/L ND 20.0 20.0 20.3 19.8 102 99.0 70.0-130 2.49 30 2,4,5-TP (Silvex) ug/L ND 20.0 20.0 19.8 19.4 99.0 97.0 70.0-130 2.04 30 2,4-DB-d3 (S) % 99.5 95.0 70.0-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 107 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736974 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049013,92636049014,92636049015,92636049016,92636049017,92636049018, 92636049019,92636049021 METHOD BLANK: 3835400 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049013,92636049014,92636049015,92636049016,92636049017,92636049018, 92636049019,92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 11/15/22 02:09 1,1,1-Trichloroethane ug/L ND 1.0 0.33 11/15/22 02:09 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 11/15/22 02:09 1,1,2-Trichloroethane ug/L ND 1.0 0.32 11/15/22 02:09 1,1-Dichloroethane ug/L ND 1.0 0.37 11/15/22 02:09 1,1-Dichloroethene ug/L ND 1.0 0.35 11/15/22 02:09 1,2,3-Trichloropropane ug/L ND 1.0 0.26 11/15/22 02:09 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 11/15/22 02:09 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 11/15/22 02:09 1,2-Dichlorobenzene ug/L ND 1.0 0.34 11/15/22 02:09 1,2-Dichloroethane ug/L ND 1.0 0.32 11/15/22 02:09 1,2-Dichloropropane ug/L ND 1.0 0.36 11/15/22 02:09 1,4-Dichlorobenzene ug/L ND 1.0 0.33 11/15/22 02:09 2-Butanone (MEK) ug/L ND 5.0 4.0 11/15/22 02:09 2-Hexanone ug/L ND 5.0 0.48 11/15/22 02:09 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 11/15/22 02:09 Acetone ug/L ND 25.0 5.1 11/15/22 02:09 Acrylonitrile ug/L ND 10.0 1.8 11/15/22 02:09 Benzene ug/L ND 1.0 0.34 11/15/22 02:09 Bromochloromethane ug/L ND 1.0 0.47 11/15/22 02:09 Bromodichloromethane ug/L ND 1.0 0.31 11/15/22 02:09 Bromoform ug/L ND 1.0 0.34 11/15/22 02:09 Bromomethane ug/L ND 2.0 1.7 11/15/22 02:09 Carbon disulfide ug/L ND 2.0 0.36 11/15/22 02:09 Carbon tetrachloride ug/L ND 1.0 0.33 11/15/22 02:09 Chlorobenzene ug/L ND 1.0 0.28 11/15/22 02:09 Chloroethane ug/L ND 1.0 0.65 11/15/22 02:09 v2 Chloroform ug/L ND 1.0 0.43 11/15/22 02:09 Chloromethane ug/L ND 1.0 0.54 11/15/22 02:09 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 11/15/22 02:09 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 11/15/22 02:09 Dibromochloromethane ug/L ND 1.0 0.36 11/15/22 02:09 Dibromomethane ug/L ND 1.0 0.39 11/15/22 02:09 Dichlorodifluoromethane ug/L ND 1.0 0.35 11/15/22 02:09 Ethylbenzene ug/L ND 1.0 0.30 11/15/22 02:09 lodomethane ug/L ND 20.0 9.7 11/15/22 02:09 m&p-Xylene ug/L ND 2.0 0.71 11/15/22 02:09 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 108 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 METHOD BLANK: 3835400 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049009,92636049013,92636049014,92636049015,92636049016,92636049017,92636049018, 92636049019,92636049021 Parameter Units Blank Result Reporting Limit MDL Analyzed Methylene Chloride ug/L ND 5.0 2.0 11/15/22 02:09 o-Xylene ug/L ND 1.0 0.34 11/15/22 02:09 Styrene ug/L ND 1.0 0.29 11/15/22 02:09 Tetrachloroethene ug/L ND 1.0 0.29 11/15/22 02:09 Tetrahydrofuran ug/L ND 10.0 3.5 11/15/22 02:09 Toluene ug/L ND 1.0 0.24 11/15/22 02:09 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 11/15/22 02:09 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 11/15/22 02:09 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 11/15/22 02:09 Trichloroethene ug/L ND 1.0 0.38 11/15/22 02:09 Trichlorofluoromethane ug/L ND 1.0 0.30 11/15/22 02:09 Vinyl acetate ug/L ND 2.0 1.3 11/15/22 02:09 Vinyl chloride ug/L ND 1.0 0.39 11/15/22 02:09 1,2-Dichloroethane-d4 (S) % 93 70-130 11/15/22 02:09 4-Bromofluorobenzene (S) % 101 70-130 11/15/22 02:09 Toluene-d8 (S) % 101 70-130 11/15/22 02:09 LABORATORY CONTROL SAMPLE: Parameter 3835401 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 52.3 105 70-130 1,1,1-Trichloroethane ug/L 50 48.5 97 70-130 1,1,2,2-Tetrachloroethane ug/L 50 50.2 100 70-130 1,1,2-Trichloroethane ug/L 50 52.4 105 70-130 1,1-Dichloroethane ug/L 50 42.8 86 70-130 1,1-Dichloroethene ug/L 50 45.5 91 70-130 1,2,3-Trichloropropane ug/L 50 47.2 94 70-130 1,2-Dibromo-3-chloropropane ug/L 50 54.7 109 70-131 1,2-Dibromoethane (EDB) ug/L 50 52.6 105 70-130 1,2-Dichlorobenzene ug/L 50 51.7 103 70-130 1,2-Dichloroethane ug/L 50 45.8 92 70-130 1,2-Dichloropropane ug/L 50 44.2 88 70-130 1,4-Dichlorobenzene ug/L 50 50.2 100 70-130 2-Butanone (MEK) ug/L 100 81.8 82 70-134 2-Hexanone ug/L 100 87.8 88 70-131 4-Methyl-2-pentanone (MIBK) ug/L 100 88.6 89 70-130 Acetone ug/L 100 80.5 80 70-133 Acrylonitrile ug/L 250 226 90 70-130 Benzene ug/L 50 43.3 87 70-130 Bromochloromethane ug/L 50 52.4 105 70-130 Bromodichloromethane ug/L 50 48.3 97 70-130 Bromoform ug/L 50 53.5 107 70-130 Qualifiers v2 v2 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 109 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 LABORATORY CONTROL SAMPLE: 3835401 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Bromomethane ug/L 50 50.9 102 45-151 Carbon disulfide ug/L 50 46.5 93 70-130 Carbon tetrachloride ug/L 50 48.9 98 70-130 Chlorobenzene ug/L 50 50.7 101 70-130 Chloroethane ug/L 50 34.0 68 39-152 v3 Chloroform ug/L 50 47.0 94 70-130 Chloromethane ug/L 50 41.2 82 58-130 cis-1,2-Dichloroethene ug/L 50 43.0 86 70-130 cis-1,3-Dichloropropene ug/L 50 48.6 97 70-130 Dibromochloromethane ug/L 50 52.7 105 70-130 Dibromomethane ug/L 50 49.2 98 70-130 Dichlorodifluoromethane ug/L 50 51.3 103 54-133 Ethylbenzene ug/L 50 48.2 96 70-130 lodomethane ug/L 100 103 103 53-141 m&p-Xylene ug/L 100 96.4 96 70-130 Methylene Chloride ug/L 50 38.5 77 66-130 v3 o-Xylene ug/L 50 51.0 102 70-130 Styrene ug/L 50 52.1 104 70-130 Tetrachloroethene ug/L 50 47.3 95 70-130 Tetrahydrofuran ug/L 500 408 82 70-130 v3 Toluene ug/L 50 47.1 94 70-130 trans-1,2-Dichloroethene ug/L 50 45.6 91 70-130 trans- 1,3-Dichloropropene ug/L 50 49.3 99 70-130 trans-1,4-Dichloro-2-butene ug/L 50 47.8 96 57-185 Trichloroethene ug/L 50 51.5 103 70-130 Trichlorofluoromethane ug/L 50 44.7 89 62-130 Vinyl acetate ug/L 100 76.3 76 70-144 v3 Vinyl chloride ug/L 50 42.0 84 62-130 1,2-Dichloroethane-d4 (S) % 86 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 97 70-130 MATRIX SPIKE SAMPLE: 3835403 92636049009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 20.7 104 70-141 1,1,1-Trichloroethane ug/L ND 20 20.2 101 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 21.3 106 69-142 1,1,2-Trichloroethane ug/L ND 20 21.5 107 70-138 1,1-Dichloroethane ug/L ND 20 19.2 96 70-150 1,1-Dichloroethene ug/L ND 20 20.9 105 70-156 1,2,3-Trichloropropane ug/L ND 20 21.7 108 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 22.3 111 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 21.3 107 70-138 1,2-Dichlorobenzene ug/L ND 20 21.8 109 70-141 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 110 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE SAMPLE: 3835403 92636049009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2-Dichloroethane ug/L ND 20 20.5 102 69-143 1,2-Dichloropropane ug/L ND 20 20.4 102 68-156 1,4-Dichlorobenzene ug/L ND 20 21.1 106 70-142 2-Butanone (MEK) ug/L ND 40 42.2 105 60-157 2-Hexanone ug/L ND 40 43.8 110 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 42.9 107 70-141 Acetone ug/L ND 40 44.6 112 58-157 Acrylonitrile ug/L ND 100 101 101 69-147 Benzene ug/L ND 20 19.1 95 70-142 Bromochloromethane ug/L ND 20 20.1 101 70-146 Bromodichloromethane ug/L ND 20 20.6 103 70-139 Bromoform ug/L ND 20 21.1 105 64-140 Bromomethane ug/L ND 20 20.6 103 28-192 Carbon disulfide ug/L ND 20 19.0 95 70-151 Carbon tetrachloride ug/L ND 20 20.1 100 70-148 Chlorobenzene ug/L ND 20 21.2 106 70-141 Chloroethane ug/L ND 20 22.0 110 58-191 Chloroform ug/L ND 20 20.2 101 70-148 Chloromethane ug/L ND 20 17.9 90 43-162 cis-1,2-Dichloroethene ug/L ND 20 20.1 101 68-151 cis-1,3-Dichloropropene ug/L ND 20 20.9 105 70-139 Dibromochloromethane ug/L ND 20 21.1 105 70-144 Dibromomethane ug/L ND 20 20.1 100 70-139 Dichlorodifluoromethane ug/L ND 20 18.1 90 39-171 v3 Ethylbenzene ug/L ND 20 21.4 107 70-143 lodomethane ug/L ND 40 40.0 100 35-171 m&p-Xylene ug/L ND 40 43.8 110 70-144 Methylene Chloride ug/L ND 20 19.4 97 62-149 o-Xylene ug/L ND 20 21.6 108 70-145 Styrene ug/L ND 20 21.8 109 70-143 Tetrachloroethene ug/L ND 20 19.7 99 70-145 Tetrahydrofuran ug/L ND 200 200 100 69-144 Toluene ug/L 0.30J 20 20.8 102 70-142 trans-1,2-Dichloroethene ug/L ND 20 19.5 98 70-151 trans- 1,3-Dichloropropene ug/L ND 20 21.5 108 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 18.2 91 51-159 Trichloroethene ug/L ND 20 20.3 102 62-146 Trichlorofluoromethane ug/L ND 20 19.0 95 63-153 Vinyl acetate ug/L ND 40 40.6 102 61-162 Vinyl chloride ug/L ND 20 21.0 105 61-163 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 111 of 165 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 SAMPLE DUPLICATE: 3835402 Parameter Units 92636049005 Result Dup Result RPD Max RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 v2 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 m&p-Xylene ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 o-Xylene ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Tetrahydrofuran ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92636049 SAMPLE DUPLICATE: 3835402 Parameter Trichlorofluoromethane Vinyl acetate Vinyl chloride 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92636049005 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND % 98 105 102 98 103 99 Max RPD RPD Qualifiers 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 113 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736984 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049008,92636049010,92636049011,92636049012,92636049020,92636049022,92636049023, 92636049024 METHOD BLANK: 3835461 Matrix: Water Associated Lab Samples: 92636049008,92636049010,92636049011,92636049012,92636049020,92636049022,92636049023, 92636049024 Parameter Units Blank Result Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 11/14/22 12:59 1,1,1-Trichloroethane ug/L ND 1.0 0.33 11/14/22 12:59 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 11/14/22 12:59 1,1,2-Trichloroethane ug/L ND 1.0 0.32 11/14/22 12:59 1,1-Dichloroethane ug/L ND 1.0 0.37 11/14/22 12:59 1,1-Dichloroethene ug/L ND 1.0 0.35 11/14/22 12:59 1,2,3-Trichloropropane ug/L ND 1.0 0.26 11/14/22 12:59 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 11/14/22 12:59 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 11/14/22 12:59 1,2-Dichlorobenzene ug/L ND 1.0 0.34 11/14/22 12:59 1,2-Dichloroethane ug/L ND 1.0 0.32 11/14/22 12:59 1,2-Dichloropropane ug/L ND 1.0 0.36 11/14/22 12:59 1,4-Dichlorobenzene ug/L ND 1.0 0.33 11/14/22 12:59 2-Butanone (MEK) ug/L ND 5.0 4.0 11/14/22 12:59 2-Hexanone ug/L ND 5.0 0.48 11/14/22 12:59 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 11/14/22 12:59 Acetone ug/L ND 25.0 5.1 11/14/22 12:59 Acrylonitrile ug/L ND 10.0 1.8 11/14/22 12:59 Benzene ug/L ND 1.0 0.34 11/14/22 12:59 Bromochloromethane ug/L ND 1.0 0.47 11/14/22 12:59 Bromodichloromethane ug/L ND 1.0 0.31 11/14/22 12:59 Bromoform ug/L ND 1.0 0.34 11/14/22 12:59 Bromomethane ug/L ND 2.0 1.7 11/14/22 12:59 Carbon disulfide ug/L ND 2.0 0.36 11/14/22 12:59 Carbon tetrachloride ug/L ND 1.0 0.33 11/14/22 12:59 Chlorobenzene ug/L ND 1.0 0.28 11/14/22 12:59 Chloroethane ug/L ND 1.0 0.65 11/14/22 12:59 Chloroform ug/L ND 1.0 0.43 11/14/22 12:59 Chloromethane ug/L ND 1.0 0.54 11/14/22 12:59 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 11/14/22 12:59 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 11/14/22 12:59 Dibromochloromethane ug/L ND 1.0 0.36 11/14/22 12:59 Dibromomethane ug/L ND 1.0 0.39 11/14/22 12:59 Dichlorodifluoromethane ug/L ND 1.0 0.35 11/14/22 12:59 Ethylbenzene ug/L ND 1.0 0.30 11/14/22 12:59 lodomethane ug/L ND 20.0 9.7 11/14/22 12:59 m&p-Xylene ug/L ND 2.0 0.71 11/14/22 12:59 Methylene Chloride ug/L ND 5.0 2.0 11/14/22 12:59 o-Xylene ug/L ND 1.0 0.34 11/14/22 12:59 v2 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 114 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 METHOD BLANK: 3835461 Matrix: Water Associated Lab Samples: 92636049008,92636049010,92636049011,92636049012,92636049020,92636049022,92636049023, 92636049024 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Styrene ug/L ND 1.0 0.29 11/14/22 12:59 Tetrachloroethene ug/L ND 1.0 0.29 11/14/22 12:59 Tetrahydrofuran ug/L ND 10.0 3.5 11/14/22 12:59 Toluene ug/L ND 1.0 0.24 11/14/22 12:59 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 11/14/22 12:59 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 11/14/22 12:59 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 11/14/22 12:59 Trichloroethene ug/L ND 1.0 0.38 11/14/22 12:59 Trichlorofluoromethane ug/L ND 1.0 0.30 11/14/22 12:59 Vinyl acetate ug/L ND 2.0 1.3 11/14/22 12:59 Vinyl chloride ug/L ND 1.0 0.39 11/14/22 12:59 1,2-Dichloroethane-d4 (S) % 90 70-130 11/14/22 12:59 4-Bromofluorobenzene (S) % 98 70-130 11/14/22 12:59 Toluene-d8 (S) % 106 70-130 11/14/22 12:59 LABORATORY CONTROL SAMPLE: Parameter 3835462 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.7 111 70-130 1,1,1-Trichloroethane ug/L 50 45.5 91 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.0 106 70-130 1,1,2-Trichloroethane ug/L 50 51.7 103 70-130 1,1-Dichloroethane ug/L 50 45.4 91 70-130 1,1-Dichloroethene ug/L 50 47.9 96 70-130 1,2,3-Trichloropropane ug/L 50 52.8 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 53.9 108 70-131 1,2-Dibromoethane (EDB) ug/L 50 55.0 110 70-130 1,2-Dichlorobenzene ug/L 50 54.6 109 70-130 1,2-Dichloroethane ug/L 50 44.6 89 70-130 1,2-Dichloropropane ug/L 50 52.6 105 70-130 1,4-Dichlorobenzene ug/L 50 53.5 107 70-130 2-Butanone (MEK) ug/L 100 94.8 95 70-134 2-Hexanone ug/L 100 106 106 70-131 4-Methyl-2-pentanone (MIBK) ug/L 100 102 102 70-130 Acetone ug/L 100 91.1 91 70-133 Acrylonitrile ug/L 250 252 101 70-130 Benzene ug/L 50 48.8 98 70-130 Bromochloromethane ug/L 50 51.9 104 70-130 Bromodichloromethane ug/L 50 50.2 100 70-130 Bromoform ug/L 50 54.6 109 70-130 Bromomethane ug/L 50 30.5 61 45-151 v2 Carbon disulfide ug/L 50 46.6 93 70-130 Carbon tetrachloride ug/L 50 49.4 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 115 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 LABORATORY CONTROL SAMPLE: Parameter 3835462 Units Spike LCS Conc. Result Chlorobenzene ug/L 50 Chloroethane ug/L 50 Chloroform ug/L 50 Chloromethane ug/L 50 cis-1,2-Dichloroethene ug/L 50 cis-1,3-Dichloropropene ug/L 50 Dibromochloromethane ug/L 50 Dibromomethane ug/L 50 Dichlorodifluoromethane ug/L 50 Ethylbenzene ug/L 50 lodomethane ug/L 100 m&p-Xylene ug/L 100 Methylene Chloride ug/L 50 o-Xylene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Tetrahydrofuran ug/L 500 Toluene ug/L 50 trans-1,2-Dichloroethene ug/L 50 trans- 1,3-Dichloropropene ug/L 50 trans-1,4-Dichloro-2-butene ug/L 50 Trichloroethene ug/L 50 Trichlorofluoromethane ug/L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % LCS % Rec % Rec Limits Qualifiers 52.6 105 70-130 45.6 91 39-152 46.4 93 70-130 42.0 84 58-130 46.1 92 70-130 52.4 105 70-130 55.5 111 70-130 49.4 99 70-130 38.3 77 54-133 v2 51.9 104 70-130 77.6 78 53-141 104 104 70-130 43.7 87 66-130 52.8 106 70-130 53.8 108 70-130 51.1 102 70-130 489 98 70-130 48.0 96 70-130 47.3 95 70-130 53.5 107 70-130 51.3 103 57-185 52.3 105 70-130 41.8 84 62-130 102 102 70-144 47.0 94 62-130 85 70-130 94 70-130 97 70-130 MATRIX SPIKE SAMPLE: Parameter 3835464 Units 92636049011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 70-141 1,1,1-Trichloroethane ug/L ND 20 23.9 120 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 21.0 105 69-142 1,1,2-Trichloroethane ug/L ND 20 21.8 109 70-138 1,1-Dichloroethane ug/L ND 20 23.7 118 70-150 1,1-Dichloroethene ug/L ND 20 23.3 116 70-156 1,2,3-Trichloropropane ug/L ND 20 20.5 102 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 20.4 102 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 22.0 110 70-138 1,2-Dichlorobenzene ug/L ND 20 19.0 95 70-141 1,2-Dichloroethane ug/L ND 20 24.1 121 69-143 1,2-Dichloropropane ug/L ND 20 22.0 110 68-156 1,4-Dichlorobenzene ug/L ND 20 18.2 91 70-142 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 116 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE SAMPLE: Parameter 3835464 Units 92636049011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 2-Butanone (MEK) ug/L ND 40 48.8 122 60-157 2-Hexanone ug/L ND 40 43.1 108 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 41.8 105 70-141 Acetone ug/L ND 40 47.5 119 58-157 Acrylonitrile ug/L ND 100 118 118 69-147 Benzene ug/L ND 20 20.8 104 70-142 Bromochloromethane ug/L ND 20 23.3 116 70-146 Bromodichloromethane ug/L ND 20 22.2 111 70-139 Bromoform ug/L ND 20 21.2 106 64-140 Bromomethane ug/L ND 20 13.6 68 28-192 Carbon disulfide ug/L ND 20 23.9 120 70-151 Carbon tetrachloride ug/L ND 20 22.1 110 70-148 Chlorobenzene ug/L ND 20 21.2 106 70-141 Chloroethane ug/L ND 20 26.4 132 58-191 Chloroform ug/L ND 20 23.4 117 70-148 Chloromethane ug/L ND 20 20.0 100 43-162 cis-1,2-Dichloroethene ug/L ND 20 23.8 119 68-151 cis-1,3-Dichloropropene ug/L ND 20 22.2 111 70-139 Dibromochloromethane ug/L ND 20 21.0 105 70-144 Dibromomethane ug/L ND 20 22.0 110 70-139 Dichlorodifluoromethane ug/L ND 20 19.4 97 39-171 Ethylbenzene ug/L ND 20 20.4 102 70-143 lodomethane ug/L ND 40 36.0 90 35-171 m&p-Xylene ug/L ND 40 40.8 102 70-144 Methylene Chloride ug/L ND 20 23.1 114 62-149 o-Xylene ug/L ND 20 20.5 103 70-145 Styrene ug/L ND 20 20.8 104 70-143 Tetrachloroethene ug/L ND 20 19.4 97 70-145 Tetrahydrofuran ug/L ND 200 232 116 69-144 Toluene ug/L ND 20 20.8 104 70-142 trans-1,2-Dichloroethene ug/L ND 20 24.4 122 70-151 trans- 1,3-Dichloropropene ug/L ND 20 22.6 113 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 18.3 91 51-159 Trichloroethene ug/L ND 20 21.6 108 62-146 Trichlorofluoromethane ug/L ND 20 21.4 107 63-153 Vinyl acetate ug/L ND 40 46.2 115 61-162 Vinyl chloride ug/L ND 20 22.4 112 61-163 1,2-Dichloroethane-d4 (S) % 108 70-130 4-Bromofluorobenzene (S) % 103 70-130 Toluene-d8 (S) % 102 70-130 SAMPLE DUPLICATE: 3835463 92636049010 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 117 of 165 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 SAMPLE DUPLICATE: 3835463 Parameter Units 92636049010 Result Dup Result RPD Max RPD Qualifiers 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 m&p-Xylene ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 o-Xylene ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Tetrahydrofuran ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 118 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 SAMPLE DUPLICATE: 3835463 92636049010 Dup Max Parameter Units Result Result RPD RPD Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 92 108 4-Bromofluorobenzene (S) % 98 100 Toluene-d8(S) % 105 104 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 119 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736360 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049008, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015 METHOD BLANK: 3832569 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049008, 92636049009,92636049010,92636049011,92636049012,92636049013,92636049014,92636049015 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 11/10/22 16:59 1,2-Dichloroethane-d4 (S) % 90 70-130 11/10/22 16:59 Toluene-d8 (S) % 102 70-130 11/10/22 16:59 LABORATORY CONTROL SAMPLE: 3832570 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 16.5 83 70-130 1,2-Dichloroethane-d4 (S) % 98 70-130 Toluene-d8 (S) % 103 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832571 3832572 Parameter 1,4-Dioxane (p-Dioxane) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) MS 92636049015 Spike Units Result Conc. ug/L 7.7 20 MSD Spike MS MSD Conc. Result Result 20 27.0 26.1 MS MSD % Rec Max % Rec % Rec Limits RPD RPD Qual 97 92 63-136 4 30 104 98 70-130 30 101 98 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 120 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736361 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049007, 92636049016, 92636049017, 92636049018, 92636049019, 92636049020, 92636049021 METHOD BLANK: 3832573 Matrix: Water Associated Lab Samples: 92636049007, 92636049016, 92636049017, 92636049018, 92636049019, 92636049020, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 11/11/22 02:52 1,2-Dichloroethane-d4 (S) % 89 70-130 11/11/22 02:52 Toluene-d8 (S) % 104 70-130 11/11/22 02:52 LABORATORY CONTROL SAMPLE: 3832574 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 17.6 88 70-130 1,2-Dichloroethane-d4 (S) % 92 70-130 Toluene-d8(S) % 101 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832575 3832576 MS MSD 92635751006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.9 20.6 99 103 63-136 4 30 1,2-Dichloroethane-d4 (S) % 99 91 70-130 30 Toluene-d8 (S) % 94 94 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 121 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736519 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049004, 92636049005 METHOD BLANK: 3833196 Associated Lab Samples: 92636049004, 92636049005 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 4,4'-DDD ug/L ND 0.050 0.017 11/14/22 13:32 4,4'-DDT ug/L ND 0.050 0.026 11/14/22 13:32 Aldrin ug/L ND 0.050 0.014 11/14/22 13:32 alpha-BHC ug/L ND 0.050 0.012 11/14/22 13:32 delta-BHC ug/L ND 0.050 0.014 11/14/22 13:32 Endosulfan I ug/L ND 0.050 0.017 11/14/22 13:32 Endosulfan 11 ug/L ND 0.050 0.016 11/14/22 13:32 Endrin ug/L ND 0.050 0.018 11/14/22 13:32 Endrin aldehyde ug/L ND 0.050 0.016 11/14/22 13:32 Heptachlor ug/L ND 0.050 0.020 11/14/22 13:32 Heptachlor epoxide ug/L ND 0.050 0.028 11/14/22 13:32 Methoxychlor ug/L ND 0.15 0.042 11/14/22 13:32 Decachlorobiphenyl (S) % 133 10-200 11/14/22 13:32 Tetrachloro-m-xylene (S) % 82 10-182 11/14/22 13:32 LABORATORY CONTROL SAMPLE: 3833197 Parameter 4,4'-DDD 4,4'-DDT Aldrin alpha-BHC delta-BHC Endosulfan I Endosulfan II Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Units Spike Conc. LCS Result LCS % Rec % Rec Limits ug/L 0.25 0.31 123 50-178 ug/L 0.25 0.35 142 23-198 ug/L 0.25 0.22 87 13-137 ug/L 0.25 0.24 98 32-161 ug/L 0.25 0.24 96 42-169 ug/L 0.25 0.27 109 44-168 ug/L 0.25 0.26 106 45-176 ug/L 0.25 0.34 135 46-178 ug/L 0.25 0.25 102 35-168 ug/L 0.25 0.25 102 25-153 ug/L 0.25 0.26 105 43-170 ug/L 0.75 0.92 123 37-187 % 126 10-200 % 68 10-182 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 122 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3833198 3833199 MS MSD 92636049004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.42 0.42 0.59 0.52 142 125 13-200 13 30 4,4'-DDT ug/L ND 0.42 0.42 0.59 0.60 143 144 10-200 1 30 Aldrin ug/L ND 0.42 0.42 0.21 0.24 51 58 10-161 12 30 alpha-BHC ug/L ND 0.42 0.42 0.38 0.24 92 59 10-186 44 30 R1 delta-BHC ug/L ND 0.42 0.42 0.41 0.33 97 80 11-199 20 30 Endosulfan I ug/L ND 0.42 0.42 0.44 0.41 105 99 10-191 5 30 Endosulfan II ug/L ND 0.42 0.42 0.45 0.42 109 100 10-200 8 30 Endrin ug/L ND 0.42 0.42 0.55 0.53 133 128 11-193 4 30 Endrin aldehyde ug/L ND 0.42 0.42 0.44 0.41 105 98 10-198 6 30 Heptachlor ug/L ND 0.42 0.42 0.36 0.29 87 70 13-166 23 30 Heptachlor epoxide ug/L ND 0.42 0.42 0.41 0.38 98 91 10-200 7 30 Methoxychlor ug/L ND 1.2 1.2 1.6 1.6 130 125 10-200 4 30 Decachlorobiphenyl (S) % 149 144 10-200 Tetrachloro-m-xylene (S) % 38 28 10-182 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 123 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736921 Analysis Method: EPA 8081 B QC Batch Method: EPA 351 OC Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049002, 92636049003, 92636049006, 92636049007, 92636049020, 92636049021 METHOD BLANK: 3835083 Matrix: Water Associated Lab Samples: 92636049002, 92636049003, 92636049006, 92636049007, 92636049020, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 0.017 11/15/22 15:46 4,4'-DDT ug/L ND 0.050 0.026 11/15/22 15:46 Aldrin ug/L ND 0.050 0.014 11/15/22 15:46 alpha-BHC ug/L ND 0.050 0.012 11/15/22 15:46 delta-BHC ug/L ND 0.050 0.014 11/15/22 15:46 Endosulfan I ug/L ND 0.050 0.017 11/15/22 15:46 Endosulfan 11 ug/L ND 0.050 0.016 11/15/22 15:46 Endrin ug/L ND 0.050 0.018 11/15/22 15:46 Endrin aldehyde ug/L ND 0.050 0.016 11/15/22 15:46 Heptachlor ug/L ND 0.050 0.020 11/15/22 15:46 Heptachlor epoxide ug/L ND 0.050 0.028 11/15/22 15:46 Methoxychlor ug/L ND 0.15 0.042 11/15/22 15:46 Decachlorobiphenyl (S) % 169 10-200 11/15/22 15:46 Tetrachloro-m-xylene (S) % 96 10-182 11/15/22 15:46 LABORATORY CONTROL SAMPLE: Parameter 3835084 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.43 173 50-178 4,4'-DDT ug/L 0.25 0.53 211 23-198 L1 Aldrin ug/L 0.25 0.25 102 13-137 alpha-BHC ug/L 0.25 0.27 108 32-161 delta-BHC ug/L 0.25 0.28 112 42-169 Endosulfan I ug/L 0.25 0.29 118 44-168 Endosulfan II ug/L 0.25 0.34 135 45-176 Endrin ug/L 0.25 0.40 161 46-178 Endrin aldehyde ug/L 0.25 0.41 163 35-168 Heptachlor ug/L 0.25 0.31 122 25-153 Heptachlor epoxide ug/L 0.25 0.28 113 43-170 Methoxychlor ug/L 0.75 1.5 202 37-187 L1 Decachlorobiphenyl (S) % 274 10-200 SO Tetrachloro-m-xylene (S) % 96 10-182 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 124 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3835134 3835135 MS MSD 92623805009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.42 0.42 0.60 0.59 144 143 13-200 1 30 4,4'-DDT ug/L ND 0.42 0.42 0.73 0.76 176 182 10-200 4 30 Aldrin ug/L ND 0.42 0.42 0.41 0.44 99 105 10-161 6 30 alpha-BHC ug/L ND 0.42 0.42 0.44 0.49 106 117 10-186 10 30 delta-BHC ug/L ND 0.42 0.42 0.48 0.55 114 133 11-199 15 30 Endosulfan I ug/L ND 0.42 0.42 0.50 0.51 121 122 10-191 1 30 Endosulfan II ug/L ND 0.42 0.42 0.47 0.48 112 116 10-200 4 30 Endrin ug/L ND 0.42 0.42 0.57 0.59 136 142 11-193 4 30 Endrin aldehyde ug/L ND 0.42 0.42 0.49 0.48 118 115 10-198 3 30 Heptachlor ug/L ND 0.42 0.42 0.51 0.57 122 136 13-166 11 30 Heptachlor epoxide ug/L ND 0.42 0.42 0.47 0.47 114 112 10-200 1 30 Methoxychlor ug/L ND 1.2 1.2 2.2 2.0 174 162 10-200 7 30 Decachlorobiphenyl (S) % 272 390 10-200 SO Tetrachloro-m-xylene (S) % 90 110 10-182 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 125 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737101 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049001 METHOD BLANK: 3836055 Associated Lab Samples: 92636049001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 4,4'-DDD ug/L ND 0.050 0.017 11/16/22 15:08 4,4'-DDT ug/L ND 0.050 0.026 11/16/22 15:08 Aldrin ug/L ND 0.050 0.014 11/16/22 15:08 alpha-BHC ug/L ND 0.050 0.012 11/16/22 15:08 delta-BHC ug/L ND 0.050 0.014 11/16/22 15:08 Endosulfan I ug/L ND 0.050 0.017 11/16/22 15:08 Endosulfan 11 ug/L ND 0.050 0.016 11/16/22 15:08 Endrin ug/L ND 0.050 0.018 11/16/22 15:08 Endrin aldehyde ug/L ND 0.050 0.016 11/16/22 15:08 Heptachlor ug/L ND 0.050 0.020 11/16/22 15:08 Heptachlor epoxide ug/L ND 0.050 0.028 11/16/22 15:08 Methoxychlor ug/L ND 0.15 0.042 11/16/22 15:08 Decachlorobiphenyl (S) % 142 10-200 11/16/22 15:08 Tetrachloro-m-xylene (S) % 92 10-182 11/16/22 15:08 LABORATORY CONTROL SAMPLE: 3836056 Parameter 4,4'-DDD 4,4'-DDT Aldrin alpha-BHC delta-BHC Endosulfan I Endosulfan II Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Units Spike Conc. LCS Result LCS % Rec % Rec Limits ug/L 0.25 0.30 120 50-178 ug/L 0.25 0.35 139 23-198 ug/L 0.25 0.21 85 13-137 ug/L 0.25 0.23 91 32-161 ug/L 0.25 0.24 94 42-169 ug/L 0.25 0.25 101 44-168 ug/L 0.25 0.25 100 45-176 ug/L 0.25 0.31 125 46-178 ug/L 0.25 0.24 96 35-168 ug/L 0.25 0.24 98 25-153 ug/L 0.25 0.25 100 43-170 ug/L 0.75 0.91 121 37-187 % 131 10-200 % 76 10-182 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 126 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836057 3836058 MS MSD 92623805010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 2.5 2.5 1.5 6.7 62 269 13-200 125 30 M1,R1 4,4'-DDT ug/L ND 2.5 2.5 1.4 5.1 55 205 10-200 115 30 M1,R1 Aldrin ug/L ND 2.5 2.5 1.1 6.4 44 258 10-161 142 30 M1,R1 alpha-BHC ug/L ND 2.5 2.5 1.1 2.7 43 106 10-186 84 30 R1 delta-BHC ug/L ND 2.5 2.5 0.81 4.2 32 168 11-199 135 30 R1 Endosulfan I ug/L ND 2.5 2.5 2.1 8.4 84 335 10-191 120 30 M1,R1 Endosulfan II ug/L ND 2.5 2.5 1.0 4.3 41 172 10-200 123 30 R1 Endrin ug/L ND 2.5 2.5 1.5 5.5 59 220 11-193 115 30 M1,R1 Endrin aldehyde ug/L ND 2.5 2.5 0.74 3.3 30 130 10-198 126 30 R1 Heptachlor ug/L ND 2.5 2.5 1.2 3.4 47 138 13-166 98 30 R1 Heptachlor epoxide ug/L ND 2.5 2.5 1.4 9.7 55 388 10-200 150 30 M1,R1 Methoxychlor ug/L ND 7.5 7.5 4.5 9.6 60 128 10-200 73 30 R1 Decachlorobiphenyl (S) % 56 101 10-200 Tetrachloro-m-xylene (S) % 34 88 10-182 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 127 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736854 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049002, 92636049004, 92636049005, 92636049009 METHOD BLANK: 3834664 Matrix: Water Associated Lab Samples: 92636049002, 92636049004, 92636049005, 92636049009 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 2.7 11/15/22 08:45 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 3.7 11/15/22 08:45 Chrysene ug/L ND 10.0 2.8 11/15/22 08:45 Dibenz(a,h)anthracene ug/L ND 10.0 3.0 11/15/22 08:45 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.9 11/15/22 08:45 2,4,6-Tribromophenol (S) % 92 10-144 11/15/22 08:45 2-Fluorobiphenyl (S) % 50 10-130 11/15/22 08:45 2-Fluorophenol (S) % 47 10-130 11/15/22 08:45 Nitrobenzene-d5 (S) % 64 10-144 11/15/22 08:45 Phenol-d6 (S) % 38 10-130 11/15/22 08:45 Terphenyl-d14 (S) % 126 34-163 11/15/22 08:45 LABORATORY CONTROL SAMPLE: 3834665 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 47.7 95 48-137 bis(2-Ethylhexyl)phthalate ug/L 50 52.2 104 32-165 Chrysene ug/L 50 48.3 97 47-131 Dibenz(a,h)anthracene ug/L 50 49.3 99 49-138 Indeno(1,2,3-cd)pyrene ug/L 50 51.0 102 41-130 2,4,6-Tribromophenol (S) % 100 10-144 2-Fluorobiphenyl (S) % 84 10-130 2-Fluorophenol(S) % 64 10-130 Nitrobenzene-d5 (S) % 80 10-144 Phenol-d6 (S) % 58 10-130 Terphenyl-d14 (S) % 110 34-163 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834666 3834667 MS MSD 92635663001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzo(a)anthracene ug/L ND 83.3 83.3 75.2 75.0 90 90 40-145 0 30 bis(2- Ethyl hexyl)phthalate ug/L ND 83.3 83.3 80.4 78.8 96 95 28-166 2 30 Chrysene ug/L ND 83.3 83.3 75.7 74.7 91 90 38-141 1 30 Dibenz(a,h)anthracene ug/L ND 83.3 83.3 79.4 75.8 95 91 39-148 5 30 Indeno(1,2,3-cd)pyrene ug/L ND 83.3 83.3 83.3 78.9 100 95 39-148 5 30 2,4,6-Tribromophenol (S) % 89 13 10-144 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 128 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834666 3834667 MS MSD 92635663001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Fluorobiphenyl (S) % 41 37 10-130 2-Fluorophenol (S) % 27 5 10-130 SO Nitrobenzene-d5(S) % 40 34 10-144 Phenol-d6 (S) % 27 17 10-130 Terphenyl-d14(S) % 100 98 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 129 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737152 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92636049001, 92636049003, 92636049006, 92636049007, 92636049008 METHOD BLANK: 3836343 Matrix: Water Associated Lab Samples: 92636049001, 92636049003, 92636049006, 92636049007, 92636049008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 2.7 11/16/22 08:47 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 3.7 11/16/22 08:47 Chrysene ug/L ND 10.0 2.8 11/16/22 08:47 Dibenz(a,h)anthracene ug/L ND 10.0 3.0 11/16/22 08:47 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.9 11/16/22 08:47 2,4,6-Tribromophenol (S) % 106 10-144 11/16/22 08:47 2-Fluorobiphenyl (S) % 61 10-130 11/16/22 08:47 2-Fluorophenol (S) % 69 10-130 11/16/22 08:47 Nitrobenzene-d5 (S) % 84 10-144 11/16/22 08:47 Phenol-d6 (S) % 56 10-130 11/16/22 08:47 Terphenyl-d14 (S) % 132 34-163 11/16/22 08:47 LABORATORY CONTROL SAMPLE: 3836344 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 50.3 101 48-137 bis(2-Ethylhexyl)phthalate ug/L 50 53.6 107 32-165 Chrysene ug/L 50 49.9 100 47-131 Dibenz(a,h)anthracene ug/L 50 52.5 105 49-138 Indeno(1,2,3-cd)pyrene ug/L 50 53.5 107 41-130 2,4,6-Tribromophenol (S) % 99 10-144 2-Fluorobiphenyl (S) % 74 10-130 2-Fluorophenol(S) % 66 10-130 Nitrobenzene-d5 (S) % 86 10-144 Phenol-d6 (S) % 57 10-130 Terphenyl-d14 (S) % 107 34-163 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836345 3836346 MS MSD 92636386002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzo(a)anthracene ug/L ND 90.9 90.9 86.5 92.4 95 102 40-145 7 30 bis(2- Ethyl hexyl)phthalate ug/L ND 90.9 90.9 99.7 101 110 111 28-166 1 30 Chrysene ug/L ND 90.9 90.9 86.0 92.4 95 102 38-141 7 30 Dibenz(a,h)anthracene ug/L ND 90.9 90.9 90.4 93.4 99 103 39-148 3 30 Indeno(1,2,3-cd)pyrene ug/L ND 90.9 90.9 94.2 95.8 104 105 39-148 2 30 2,4,6-Tribromophenol (S) % 50 97 10-144 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 130 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836345 3836346 MS MSD 92636386002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Fluorobiphenyl (S) % 75 76 10-130 2-Fluorophenol(S) % 30 62 10-130 Nitrobenzene-d5(S) % 94 83 10-144 Phenol-d6 (S) % 46 56 10-130 Terphenyl-d14(S) % 103 108 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 131 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736550 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049017, 92636049018, 92636049019 METHOD BLANK: 3833343 Matrix: Water Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049017, 92636049018, 92636049019 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/11/22 16:15 LABORATORY CONTROL SAMPLE: 3833344 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50500 101 80-120 LABORATORY CONTROL SAMPLE: 3833345 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50600 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3833346 3833347 MS MSD 92635481026 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 76.7 mg/L 50000 50000 125000 121000 96 89 80-120 3 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3833348 3833349 MS MSD 92635481027 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 29.6 mg/L 50000 50000 76900 77800 95 96 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 132 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736558 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049006, 92636049007, 92636049008, 92636049010, 92636049011,92636049012,92636049013,92636049014,92636049015,92636049016,92636049020, 92636049021 METHOD BLANK: 3833370 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049006, 92636049007, 92636049008, 92636049010, 92636049011,92636049012,92636049013,92636049014,92636049015,92636049016,92636049020, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/11/22 19:56 LABORATORY CONTROL SAMPLE: 3833371 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50300 101 80-120 LABORATORY CONTROL SAMPLE: 3833372 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50300 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3833373 3833374 MS MSD 92635847002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 93.3 mg/L 50000 50000 143000 144000 99 102 80-120 1 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3833375 3833376 MS MSD 92635847003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 191 mg/L 50000 50000 258000 252000 133 122 80-120 2 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 133 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736482 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049017 METHOD BLANK: 3832914 Associated Lab Samples: 92636049017 Parameter Units Total Dissolved Solids ug/L LABORATORY CONTROL SAMPLE: 3832915 Parameter Units Total Dissolved Solids ug/L SAMPLE DUPLICATE: 3832916 Parameter Units Total Dissolved Solids ug/L SAMPLE DUPLICATE: 3832917 Parameter Total Dissolved Solids Matrix: Water Blank Reporting Result Limit MDL Analyzed Qualifiers ND 25000 25000 11 /11 /22 11:55 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250000 234000 94 90-110 92636049017 Dup Max Result Result RPD RPD Qualifiers 88000 87000 1 25 92635452004 Dup Units Result Result ug/L 297 mg/L 294000 Max RPD RPD Qualifiers 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 134 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736483 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049018, 92636049019 METHOD BLANK: 3832919 Matrix: Water Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049018, 92636049019 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/11/22 12:01 LABORATORY CONTROL SAMPLE: 3832920 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 248000 99 90-110 SAMPLE DUPLICATE: 3832921 92635453003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 3560 mg/L 3580000 0 25 SAMPLE DUPLICATE: 3832922 92636049005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L ND ND 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 135 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736763 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049002, 92636049013, 92636049014, 92636049015, 92636049016, 92636049021 METHOD BLANK: 3834399 Matrix: Water Associated Lab Samples: 92636049002, 92636049013, 92636049014, 92636049015, 92636049016, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/13/22 13:57 LABORATORY CONTROL SAMPLE: 3834400 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 244000 98 90-110 SAMPLE DUPLICATE: 3834401 92635763012 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 60.0 mg/L 59000 2 25 SAMPLE DUPLICATE: 3834402 92635736001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 163 mg/L 167000 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 136 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736791 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049003, 92636049006, 92636049007 METHOD BLANK: 3834463 Matrix: Water Associated Lab Samples: 92636049003, 92636049006, 92636049007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/14/22 15:15 LABORATORY CONTROL SAMPLE: 3834464 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 250000 100 90-110 SAMPLE DUPLICATE: 3834465 92635847028 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 219 mg/L 221000 1 25 SAMPLE DUPLICATE: 3834466 92635853002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 552 mg/L 544000 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 137 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737095 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049010, 92636049011, 92636049012, 92636049020 METHOD BLANK: 3836030 Matrix: Water Associated Lab Samples: 92636049010, 92636049011, 92636049012, 92636049020 Blank Reporting Parameter Units Result Limit Total Dissolved Solids ug/L ND 25000 LABORATORY CONTROL SAMPLE: 3836031 Spike LCS Parameter Units Conc. Result Total Dissolved Solids ug/L 250000 246000 SAMPLE DUPLICATE: 3836032 92636049010 Dup Parameter Units Result Result Total Dissolved Solids ug/L 159000 160000 SAMPLE DUPLICATE: 3836033 92636065007 Dup Parameter Units Result Result Total Dissolved Solids ug/L 208 mg/L 211000 MDL Analyzed Qualifiers 25000 11 /15/22 13:05 LCS % Rec % Rec Limits Qualifiers 98 90-110 Max RPD RPD Qualifiers 1 25 Max RPD RPD Qualifiers 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 138 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737250 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049008 METHOD BLANK: 3836961 Matrix: Water Associated Lab Samples: 92636049001, 92636049008 Blank Reporting Parameter Units Result Limit Total Dissolved Solids ug/L ND 25000 LABORATORY CONTROL SAMPLE: 3836962 Spike LCS Parameter Units Conc. Result Total Dissolved Solids ug/L 250000 242000 SAMPLE DUPLICATE: 3836963 92636075022 Dup Parameter Units Result Result Total Dissolved Solids ug/L 19300 mg/L 18800000 SAMPLE DUPLICATE: 3836964 92636049001 Dup Parameter Units Result Result Total Dissolved Solids ug/L 163000 162000 MDL Analyzed Qualifiers 25000 11 /15/22 17:46 LCS % Rec % Rec Limits Qualifiers 97 90-110 Max RPD RPD Qualifiers 3 25 1 g Max RPD RPD Qualifiers 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 139 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736396 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049017, 92636049018, 92636049019 METHOD BLANK: 3832657 Matrix: Water Associated Lab Samples: 92636049004, 92636049005, 92636049009, 92636049017, 92636049018, 92636049019 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 22.0 11/11/22 03:33 LABORATORY CONTROL SAMPLE: 3832658 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 505 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832659 3832660 MS MSD 92635806001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 504 516 101 103 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832661 3832662 MS MSD 92635806002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 496 509 99 102 80-120 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 140 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736397 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049002, 92636049013, 92636049014, 92636049015, 92636049016, 92636049021 METHOD BLANK: 3832663 Matrix: Water Associated Lab Samples: 92636049002, 92636049013, 92636049014, 92636049015, 92636049016, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 22.0 11/11/22 03:47 LABORATORY CONTROL SAMPLE: 3832664 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 496 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832665 3832666 MS MSD 92635806003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 497 513 99 103 80-120 3 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832667 3832668 MS MSD 92635853004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 491 494 98 99 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 141 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737023 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049003, 92636049006, 92636049007, 92636049008, 92636049010, 92636049011, 92636049012,92636049020 METHOD BLANK: 3835807 Matrix: Water Associated Lab Samples: 92636049001, 92636049003, 92636049006, 92636049007, 92636049008, 92636049010, 92636049011, 92636049012,92636049020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 22.0 11/15/22 04:13 LABORATORY CONTROL SAMPLE: 3835808 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 489 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3835809 3835810 MS MSD 92636049003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 358 369 71 74 80-120 3 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3835811 3835812 MS MSD 92636251004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 482 507 96 101 80-120 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 142 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736436 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049008,92636049009,92636049010,92636049011,92636049012,92636049013,92636049014, 92636049015,92636049016,92636049017 METHOD BLANK: 3832744 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049008,92636049009,92636049010,92636049011,92636049012,92636049013,92636049014, 92636049015,92636049016,92636049017 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 11/13/2219:20 LABORATORY CONTROL SAMPLE: 3832745 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 49000 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832746 3832747 MS MSD 92635778001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 5.5 mg/L 50000 50000 56100 56000 101 101 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832748 3832749 MS MSD 92636049008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 1760 50000 50000 52300 52600 101 102 90-110 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 143 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 736439 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049018, 92636049019, 92636049020, 92636049021 METHOD BLANK: 3832750 Matrix: Water Associated Lab Samples: 92636049018, 92636049019, 92636049020, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 11/13/22 20:08 LABORATORY CONTROL SAMPLE: 3832751 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 51300 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832752 3832753 MS MSD 92636049018 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 34000 50000 50000 82600 82800 97 98 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832754 3832755 MS MSD 92635847007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 0.58J 50000 50000 49900 49700 99 98 90-110 0 10 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 144 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737204 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049008,92636049009,92636049010,92636049011,92636049012,92636049013,92636049014, 92636049015,92636049016 METHOD BLANK: 3836647 Matrix: Water Associated Lab Samples: 92636049001, 92636049002, 92636049003, 92636049004, 92636049005, 92636049006, 92636049007, 92636049008,92636049009,92636049010,92636049011,92636049012,92636049013,92636049014, 92636049015,92636049016 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 11/15/2218:50 LABORATORY CONTROL SAMPLE: 3836648 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20600 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836649 3836650 MS MSD 92635401002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 9.5 mg/L 10000 10000 19900 19800 103 103 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836651 3836652 MS MSD 92635401003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 44.7 mg/L 10000 10000 54400 54300 97 96 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 145 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737205 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049017, 92636049018, 92636049019, 92636049020, 92636049021 METHOD BLANK: 3836653 Matrix: Water Associated Lab Samples: 92636049017, 92636049018, 92636049019, 92636049020, 92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 11/15/2219:29 LABORATORY CONTROL SAMPLE: 3836654 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20700 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836655 3836656 MS MSD 92636049017 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 19500 10000 10000 29700 29700 102 102 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3836657 3836658 MS MSD 92636049018 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 20600 10000 10000 30800 30500 102 99 90-110 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 146 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 737838 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049017 METHOD BLANK: 3839919 Matrix: Water Associated Lab Samples: 92636049017 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/17/22 21:11 LABORATORY CONTROL SAMPLE: 3839920 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 93.9 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3839921 3839922 MS MSD 92635717002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 ND ND 1 1 80-120 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 147 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 738503 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049002,92636049004,92636049005,92636049009,92636049013,92636049014,92636049018, 92636049019 METHOD BLANK: 3843123 Matrix: Water Associated Lab Samples: 92636049002,92636049004,92636049005,92636049009,92636049013,92636049014,92636049018, 92636049019 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/21/22 21:49 LABORATORY CONTROL SAMPLE: 3843124 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 95.9 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3843125 3843126 MS MSD 92635359002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 97.2 91.6 91 86 80-120 6 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3843127 3843128 MS MSD 92635405002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.0080 100 100 ND ND -8 -8 80-120 10 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 148 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 738796 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049003,92636049006,92636049007,92636049010,92636049011,92636049012,92636049015, 92636049016,92636049020,92636049021 METHOD BLANK: 3844827 Matrix: Water Associated Lab Samples: 92636049003,92636049006,92636049007,92636049010,92636049011,92636049012,92636049015, 92636049016,92636049020,92636049021 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/22/22 21:01 LABORATORY CONTROL SAMPLE: 3844828 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 94.8 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3844829 3844830 MS MSD 92635511001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 95.5 94.4 94 93 80-120 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3844831 3844832 MS MSD 92635549001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 76.9 40.5 76 40 80-120 62 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 149 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92636049 QC Batch: 738815 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92636049001, 92636049008 METHOD BLANK: 3844904 Matrix: Water Associated Lab Samples: 92636049001, 92636049008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/22/22 22:02 LABORATORY CONTROL SAMPLE: 3844905 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 94.1 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3844906 3844907 MS MSD 92635870001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 92.8 92.0 92 92 80-120 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3844908 3844909 MS MSD 92635870002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 91.9 90.7 92 90 80-120 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 150 of 165 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: OSR LANDFILL Pace Project No.: 92636049 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. SAMPLE QUALIFIERS Sample: 92636049001 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. Sample: 92636049002 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. Sample: 92636049003 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. Sample: 92636049004 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. Sample: 92636049005 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. Sample: 92636049006 [1j Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 151 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: OSR LANDFILL Pace Project No.: 92636049 SAMPLE QUALIFIERS Sample: 92636049007 I11 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 - Duplicate Analysis performed due to IS failure. No reportable in -hold data. ANALYTE QUALIFIERS 1 g Constant weight could not be achieved for this sample after 4 drying cycles. The final weight change was 0.0065 grams. CO Result confirmed by second analysis. E Analyte concentration exceeded the calibration range. The reported result is estimated. H3 Sample was received or analysis requested beyond the recognized method holding time. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 152 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL 92636049 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92636049001 MWA R EPA 3510C 737101 EPA 8081 B 737386 92636049002 MW-2R EPA 3510C 736921 EPA 8081 B 737145 92636049003 MW-4R EPA 3510C 736921 EPA 8081 B 737145 92636049004 MW-15 EPA 3510C 736519 EPA 8081 B 736795 92636049005 EQBL EPA 3510C 736519 EPA 8081 B 736795 92636049006 FB EPA 3510C 736921 EPA 8081 B 737145 92636049007 DUP-1 EPA 3510C 736921 EPA 8081 B 737145 92636049020 MW-7 EPA 3510C 736921 EPA 8081 B 737145 92636049021 MW-10 EPA 3510C 736921 EPA 8081 B 737145 92636049001 MWA R EPA 3010 877576 EPA 6010 877600 92636049002 MW-2R EPA 3010 877576 EPA 6010 877600 92636049003 MW-4R EPA 3010 877576 EPA 6010 877600 92636049004 MW-15 EPA 3010 877576 EPA 6010 877600 92636049005 EQBL EPA 3010 877576 EPA 6010 877600 92636049006 FB EPA 3010 877576 EPA 6010 877600 92636049007 DUP-1 EPA 3010 877576 EPA6010 877600 92636049008 MW-3R EPA 3010 877609 EPA 6010 877668 92636049009 SW-2 EPA 3010 877576 EPA 6010 877600 92636049010 MW-5R EPA 3010 877576 EPA 6010 877600 92636049011 MW-8 EPA 3010 877576 EPA 6010 877600 92636049012 MW-9 EPA 3010 877576 EPA 6010 877600 92636049013 MW-11 EPA 3010 877576 EPA 6010 877600 92636049014 MW-12 EPA 3010 877576 EPA 6010 877600 92636049015 MW-13 EPA 3010 877576 EPA 6010 877600 92636049016 MW-14 EPA 3010 877576 EPA 6010 877600 92636049017 SW-1 EPA 3010 877576 EPA 6010 877600 92636049018 SW-3 EPA 3010 877576 EPA 6010 877600 92636049019 SW-4 EPA 3010 877576 EPA 6010 877600 92636049020 MW-7 EPA 3010 877576 EPA 6010 877600 92636049021 MW-10 EPA 3010 877576 EPA 6010 877600 92636049001 MWA R EPA 3010 877575 EPA 6020 877599 92636049002 MW-2R EPA 3010 877575 EPA 6020 877599 92636049003 MW-411 EPA 3010 877575 EPA 6020 877599 92636049004 MW-15 EPA 3010 877575 EPA 6020 877599 92636049005 EQBL EPA 3010 877575 EPA 6020 877599 92636049006 FB EPA 3010 877575 EPA 6020 877599 92636049007 DUP-1 EPA 3010 877575 EPA 6020 877599 92636049008 MW-3R EPA 3010 877608 EPA 6020 877666 92636049009 SW-2 EPA 3010 877575 EPA 6020 877599 92636049010 MW-5R EPA 3010 877575 EPA 6020 877599 92636049011 MW-8 EPA 3010 877575 EPA 6020 877599 92636049012 MW-9 EPA 3010 877575 EPA 6020 877599 92636049013 MW-11 EPA 3010 877575 EPA 6020 877599 92636049014 MW-12 EPA 3010 877575 EPA 6020 877599 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 153 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL 92636049 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92636049015 MW-13 EPA 3010 877575 EPA 6020 877599 92636049016 MW-14 EPA 3010 877575 EPA 6020 877599 92636049017 SW-1 EPA 3010 877575 EPA 6020 877599 92636049018 SW-3 EPA 3010 877575 EPA 6020 877599 92636049019 SW-4 EPA 3010 877575 EPA 6020 877599 92636049020 MW-7 EPA 3010 877575 EPA 6020 877599 92636049021 MW-10 EPA 3010 877575 EPA 6020 877599 92636049001 MW-1 R EPA 7470A 738303 EPA 7470A 738477 92636049002 MW-2R EPA 7470A 738303 EPA 7470A 738477 92636049003 MW-4R EPA 7470A 738303 EPA 7470A 738477 92636049004 MW-15 EPA 7470A 738303 EPA 7470A 738477 92636049005 EQBL EPA 7470A 738303 EPA 7470A 738477 92636049006 FB EPA 7470A 738304 EPA 7470A 738461 92636049007 DUP-1 EPA 7470A 738304 EPA 7470A 738461 92636049008 MW-3R EPA 7470A 738304 EPA 7470A 738461 92636049009 SW-2 EPA 7470A 738304 EPA 7470A 738461 92636049010 MW-5R EPA 7470A 738304 EPA 7470A 738461 92636049011 MW-8 EPA 7470A 738304 EPA 7470A 738461 92636049012 MW-9 EPA 7470A 738304 EPA 7470A 738461 92636049013 MW-11 EPA 7470A 738304 EPA 7470A 738461 92636049014 MW-12 EPA 7470A 738304 EPA 7470A 738461 92636049015 MW-13 EPA 7470A 738304 EPA 7470A 738461 92636049016 MW-14 EPA 7470A 738304 EPA 7470A 738461 92636049017 SW-1 EPA 7470A 738304 EPA 7470A 738461 92636049018 SW-3 EPA 7470A 738304 EPA 7470A 738461 92636049019 SW-4 EPA 7470A 738304 EPA 7470A 738461 92636049020 MW-7 EPA 7470A 738304 EPA 7470A 738461 92636049021 MW-10 EPA 7470A 739333 EPA 7470A 739364 92636049001 MWA R 8321 1964182 EPA 8321 1964182 92636049002 MW-2R 8321 1964182 EPA 8321 1964182 92636049003 MW-4R 8321 1964182 EPA 8321 1964182 92636049004 MW-15 8321 1964182 EPA 8321 1964182 92636049005 EQBL 8321 1964182 EPA 8321 1964182 92636049006 FB 8321 1964182 EPA 8321 1964182 92636049007 DUP-1 8321 1964182 EPA 8321 1964182 92636049001 MWA R EPA 3510C 737152 EPA 8270E 737366 92636049002 MW-2R EPA 3510C 736854 EPA 8270E 737054 92636049003 MW-4R EPA 3510C 737152 EPA 8270E 737366 92636049004 MW-15 EPA 3510C 736854 EPA 8270E 737054 92636049005 EQBL EPA 3510C 736854 EPA 8270E 737054 92636049006 FB EPA 3510C 737152 EPA 8270E 737366 92636049007 DUP-1 EPA 3510C 737152 EPA 8270E 737366 92636049008 MW-3R EPA 3510C 737152 EPA 8270E 737366 92636049009 SW-2 EPA 3510C 736854 EPA 8270E 737054 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 154 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92636049 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92636049001 MWA R EPA 8260D 736974 92636049002 MW-2R EPA 8260D 736974 92636049003 MW-4R EPA 8260D 736974 92636049004 MW-15 EPA 8260D 736974 92636049005 EQBL EPA 8260D 736974 92636049006 FB EPA 8260D 736974 92636049007 DUP-1 EPA 8260D 736974 92636049008 MW-3R EPA 8260D 736984 92636049009 SW-2 EPA 8260D 736974 92636049010 MW-5R EPA 8260D 736984 92636049011 MW-8 EPA 8260D 736984 92636049012 MW-9 EPA 8260D 736984 92636049013 MW-11 EPA 8260D 736974 92636049014 MW-12 EPA 8260D 736974 92636049015 MW-13 EPA 8260D 736974 92636049016 MW-14 EPA 8260D 736974 92636049017 SW-1 EPA 8260D 736974 92636049018 SW-3 EPA 8260D 736974 92636049019 SW-4 EPA 8260D 736974 92636049020 MW-7 EPA 8260D 736984 92636049021 MW-10 EPA 8260D 736974 92636049022 TB-1 EPA 8260D 736984 92636049023 TB-2 EPA 8260D 736984 92636049024 TB-3 EPA 8260D 736984 92636049001 MWA R EPA 8260D Mod. 736360 92636049002 MW-2R EPA 8260D Mod. 736360 92636049003 MW-4R EPA 8260D Mod. 736360 92636049004 MW-15 EPA 8260D Mod. 736360 92636049005 EQBL EPA 8260D Mod. 736360 92636049006 FB EPA 8260D Mod. 736360 92636049007 DUP-1 EPA 8260D Mod. 736361 92636049008 MW-3R EPA 8260D Mod. 736360 92636049009 SW-2 EPA 8260D Mod. 736360 92636049010 MW-5R EPA 8260D Mod. 736360 92636049011 MW-8 EPA 8260D Mod. 736360 92636049012 MW-9 EPA 8260D Mod. 736360 92636049013 MW-11 EPA 8260D Mod. 736360 92636049014 MW-12 EPA 8260D Mod. 736360 92636049015 MW-13 EPA 8260D Mod. 736360 92636049016 MW-14 EPA 8260D Mod. 736361 92636049017 SW-1 EPA 8260D Mod. 736361 92636049018 SW-3 EPA 8260D Mod. 736361 92636049019 SW-4 EPA 8260D Mod. 736361 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 155 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID QC Batch Method QC Batch 92636049020 MW-7 EPA 8260D Mod. 736361 92636049021 MW-10 EPA 8260D Mod. 736361 92636049001 MWA R SM 2320E-2011 736558 92636049002 MW-2R SM 2320B-2011 736558 92636049003 MW-4R SM 2320B-2011 736558 92636049004 MW-15 SM 2320B-2011 736550 92636049005 EQBL SM 2320B-2011 736550 92636049006 FB SM 2320E-2011 736558 92636049007 DU P-1 SM 2320B-2011 736558 92636049008 MW-3R SM 2320B-2011 736558 92636049009 SW-2 SM 2320E-2011 736550 92636049010 MW-5R SM 2320B-2011 736558 92636049011 MW-8 SM 2320B-2011 736558 92636049012 MW-9 SM 2320B-2011 736558 92636049013 MW-11 SM 2320B-2011 736558 92636049014 MW-12 SM 2320B-2011 736558 92636049015 MW-13 SM 2320B-2011 736558 92636049016 MW-14 SM 2320B-2011 736558 92636049017 SW-1 SM 2320E-2011 736550 92636049018 SW-3 SM 2320E-2011 736550 92636049019 SW-4 SM 2320E-2011 736550 92636049020 MW-7 SM 2320B-2011 736558 92636049021 MW-10 SM 2320B-2011 736558 92636049001 MWA R SM 2540C-2015 737250 92636049002 MW-2R SM 254OC-2015 736763 92636049003 MW-4R SM 2540C-2015 736791 92636049004 MW-15 SM 254OC-2015 736483 92636049005 EQBL SM 254OC-2015 736483 92636049006 FB SM 2540C-2015 736791 92636049007 DUP-1 SM 2540C-2015 736791 92636049008 MW-3R SM 254OC-2015 737250 92636049009 SW-2 SM 2540C-2015 736483 92636049010 MW-5R SM 254OC-2015 737095 92636049011 MW-8 SM 254OC-2015 737095 92636049012 MW-9 SM 254OC-2015 737095 92636049013 MW-11 SM 2540C-2015 736763 92636049014 MW-12 SM 2540C-2015 736763 92636049015 MW-13 SM 2540C-2015 736763 92636049016 MW-14 SM 2540C-2015 736763 92636049017 SW-1 SM 254OC-2015 736482 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 156 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92636049 Lab ID Sample ID QC Batch Method QC Batch 92636049018 SW-3 SM 2540C-2015 736483 92636049019 SW-4 SM 2540C-2015 736483 92636049020 MW-7 SM 254OC-2015 737095 92636049021 MW-10 SM 2540C-2015 736763 92636049001 MW-1R SM 4500-S2D-2011 737023 92636049002 MW-2R SM 4500-S2D-2011 736397 92636049003 MW-4R SM 4500-S2D-2011 737023 92636049004 MW-15 SM 4500-S2D-2011 736396 92636049005 EQBL SM 4500-S2D-2011 736396 92636049006 FB SM 4500-S2D-2011 737023 92636049007 DUP-1 SM 4500-S2D-2011 737023 92636049008 MW-3R SM 4500-S2D-2011 737023 92636049009 SW-2 SM 4500-S2D-2011 736396 92636049010 MW-5R SM 4500-S2D-2011 737023 92636049011 MW-8 SM 4500-S2D-2011 737023 92636049012 MW-9 SM 4500-S2D-2011 737023 92636049013 MW-11 SM 4500-S2D-2011 736397 92636049014 MW-12 SM 4500-S2D-2011 736397 92636049015 MW-13 SM 4500-S2D-2011 736397 92636049016 MW-14 SM 4500-S2D-2011 736397 92636049017 SW-1 SM 4500-S2D-2011 736396 92636049018 SW-3 SM 4500-S2D-2011 736396 92636049019 SW-4 SM 4500-S2D-2011 736396 92636049020 MW-7 SM 4500-S2D-2011 737023 92636049021 MW-10 SM 4500-S2D-2011 736397 92636049001 MWA R EPA 300.0 Rev 2.1 1993 736436 92636049002 MW-2R EPA 300.0 Rev 2.1 1993 736436 92636049003 MW-4R EPA 300.0 Rev 2.1 1993 736436 92636049004 MW-15 EPA 300.0 Rev 2.1 1993 736436 92636049005 EQBL EPA 300.0 Rev 2.1 1993 736436 92636049006 FB EPA 300.0 Rev 2.1 1993 736436 92636049007 DUP-1 EPA 300.0 Rev 2.1 1993 736436 92636049008 MW-3R EPA 300.0 Rev 2.1 1993 736436 92636049009 SW-2 EPA 300.0 Rev 2.1 1993 736436 92636049010 MW-5R EPA 300.0 Rev 2.1 1993 736436 92636049011 MW-8 EPA 300.0 Rev 2.1 1993 736436 92636049012 MW-9 EPA 300.0 Rev 2.1 1993 736436 92636049013 MWA1 EPA 300.0 Rev 2.1 1993 736436 92636049014 MW-12 EPA 300.0 Rev 2.1 1993 736436 92636049015 MW-13 EPA 300.0 Rev 2.1 1993 736436 92636049016 MW-14 EPA 300.0 Rev 2.1 1993 736436 92636049017 SW-1 EPA 300.0 Rev 2.1 1993 736436 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 157 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92636049 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92636049018 SW-3 EPA 300.0 Rev 2.1 1993 736439 92636049019 SW-4 EPA 300.0 Rev 2.1 1993 736439 92636049020 MW-7 EPA 300.0 Rev 2.1 1993 736439 92636049021 MW-10 EPA 300.0 Rev 2.1 1993 736439 92636049001 MWA R SM 4500-CI-E-2011 737204 92636049002 MW-2R SM 4500-CI-E-2011 737204 92636049003 MW-4R SM 4500-CI-E-2011 737204 92636049004 MW-15 SM 4500-CI-E-2011 737204 92636049005 EQBL SM 4500-CI-E-2011 737204 92636049006 FB SM 4500-CI-E-2011 737204 92636049007 DUP-1 SM 4500-CI-E-2011 737204 92636049008 MW-3R SM 4500-CI-E-2011 737204 92636049009 SW-2 SM 4500-CI-E-2011 737204 92636049010 MW-5R SM 4500-CI-E-2011 737204 92636049011 MW-8 SM 4500-CI-E-2011 737204 92636049012 MW-9 SM 4500-CI-E-2011 737204 92636049013 MW-11 SM 4500-CI-E-2011 737204 92636049014 MW-12 SM 4500-CI-E-2011 737204 92636049015 MW-13 SM 4500-CI-E-2011 737204 92636049016 MW-14 SM 4500-CI-E-2011 737204 92636049017 SW-1 SM 4500-CI-E-2011 737205 92636049018 SW-3 SM 4500-CI-E-2011 737205 92636049019 SW-4 SM 4500-CI-E-2011 737205 92636049020 MW-7 SM 4500-CI-E-2011 737205 92636049021 MW-10 SM 4500-CI-E-2011 737205 92636049001 MWA R SM 4500-CN-E-2016 738815 SM 4500-CN-E-2016 738959 92636049002 MW-2R SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049003 MW-4R SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049004 MW-15 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049005 EQBL SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049006 FB SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049007 DUP-1 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049008 MW-3R SM 4500-CN-E-2016 738815 SM 4500-CN-E-2016 738959 92636049009 SW-2 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049010 MW-5R SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049011 MW-8 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049012 MW-9 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049013 MW-11 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049014 MW-12 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049015 MW-13 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049016 MW-14 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049017 SW-1 SM 4500-CN-E-2016 737838 SM 4500-CN-E-2016 737933 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2022 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 158 of 165 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92636049 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92636049018 SW-3 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049019 SW-4 SM 4500-CN-E-2016 738503 SM 4500-CN-E-2016 738646 92636049020 MW-7 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 92636049021 MW-10 SM 4500-CN-E-2016 738796 SM 4500-CN-E-2016 738957 Date: 12/12/2022 05:09 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 159 of 165 -ace _Title: ENV-FRM-HUN1-0083 v0'1 Sample Condition Upon Receipt Effective Date: 05/12/202205/12/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville V Raleigh[] Mefc-hanicsville❑ Atlanta[—] Kernersville❑ ,Sample Client Marne: wo# • 9��6360149 on Receipt(} /� Project #1111111111111111111111 Courier: ❑Fed Ex ❑UPS ❑LISPS ]Client ❑ Commercial ❑Pace ❑Other: 926361349 Custody Seal Present? ❑Yes QNo Seals Intact? ❑Yes QNO Packing Material: []Bubble Wrap Bubble Bags ❑None ❑ Other Thermometer: IR Gun ID: Type of Ice: J Wet ❑Blue Correction factor: Cooler Temp: Add/Subtract (°C) ~U l Cooler Temp Corrected (*Q. USDA Regulated Soil (Q N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? []yes ❑No Chain of Custody Present? 'Elyes ❑No ❑N/A 1. Samples Arrived within Hotcl 7 es ❑No ©N/A 2. Short Mold Time Analysis (<72 hr.)? ❑Yes Nn ❑N/A 3. Rush Turn Around Time Requested? ❑Yes ONO ❑N/A 4. Sufficient Volume? Yes ©No ❑N/A 5, Correct Containers Used? WYes ❑No ❑N/A 6. -Pace Containers Used? ®Yes ONO []N/A Containers Intact? ®Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No KIN/A 8. Sample Labels Match COC? Yes ❑No ❑N/A 9. -Includes r U`' Date/Time/ID/Analysis Matrix: ! Headspace in VOA Vials (>5-6mm)? ❑Yes No ❑N/A 10. Trip Blank Present? ®Yes 0 No ❑N/A 11. Trip Blank Custody Seals Present? QYes ONO ❑N/A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTfFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: _t` O!i2ct Manager SRF Review: __ Biological Tissue Frozen? ❑Yes ❑No EN/A ❑None Temp should be above freezing to 6°C ❑Samples out oftemp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? ❑Yes ❑Nn Field Data Required? ❑Yes ❑No Lot ID of split containers: Date/Time: Date: Date: - Qualtrax ID: 69614 Page 1 of 2 Page 160 of 165 P — •-•-• �•-• - vV YVF VPIi1t.11G VVI]iAlIIVII\/tfvlFi1Ci4411J� fl- ace Effectivo Date: 051121202205/12/2022 - ■O W #9M636049 *Check mark top half of box if pH and/or dechlorination is verified and Proact PM: Sl- ��_� within the acceptance range for preservation samples, f CLIEN'r: 92-HOR Due Date, 11/28/ 22 Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLitg **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine U TTV U 1 Iz x m i tt E u z G1 RF Yl dO e G u Q E H V 6 d Q N a c a E N > M d m ? d W1 a c E V01 > N 4 M z -p y w CL c � ro ri M N 4 In N V a O y u a E eq th O O. to N v a MO z r Y u E N�! f z M 6 m z A N .. u Q N '� a a a E rq IV a W t n S x M z u a E N-i , m 4 a a a 7� '„1 y r 'a ti Lry z Z 2 ci a a c n E ¢ `m N [7 X _ N v Q 2 E ¢ a S ri C7 Q z a 6i N W a c 'u E Q 7 M l7 Q V Z a K 0 N x E Q a v1 N E,7 ¢ v a Q r�i 2 ai E ¢ E rj t/7 K1 l7 a u Q 2 2 m E Q E N V dl L4 Q ¢ z u ¢ 0 > E 4 =1 Mr ' O z z m O v{ N ¢ 0 > F•• OF L7 > Q z a, m ❑ rIf d O > E q 7 01 0 > Q ` ? `r d 0 a E d i OI Q O Q ? o 0 ¢ o j VI 01 0 0 \ z .' n ro a > d a X �7 \ 7 ro I Q z u ro v v, E N Vf 4 vi I z z v ' b n`+ , n _ E Uhl F N 6. VI a, :n Q1 0 0 z _ro 4 E 6' M a, m z ? W Z h u c 7 E `r E C 4 � z ,n c o c �, L N 7 > 97 2 d n c E a p V7 I 1 l f L) 4 4 1 I_ 6 L — 8 2 � ll IJ \J U 10 L f J { J X — 12 pH Adjustment Log for Preserved Samples Sample 1p Type of Preservative pH upon recelpt Date preservation adjusted Time preseativervation Amount of PreseryLot ii adjusted added Note:-WherFVV'0TttMre 13' a discrepancy ai ecunt - g A1oFt}i Ca�ol'ina conit Out of hold, incorrect preservative, out of temp, incorrect containers. a copy of this form will he sent to the North Carolina OENR Certification office {i.e. Qualtrax ID: 69614 Page 2 of 2 Page 161 of 165 /-Pace --- ..... ..v,r E-v VM'J Yv k_w7p1I IiPIV LVI Ii11LI VI I LJtjw E k E1c�. v-ktr� Effective Data: 05/12/2022OS/12/2022 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples, Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, Wig *"Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine 011 : 92'6360149 Project N PM: SC CLIENT: 92-HOR Due Date: 11/28/22 z z d z v z v z v 'D at � ry V 2 y Cr z co w „� n o `. 7 z a a ry^ Z _ N y N V = U V Q z a Z v ¢ z Y m ro 1 Q z r d z M 7 ? ar w Q 2 d C 3 G G 7 2 G ry 2 z = M Z _ro 0 `L U G V, N O ry = `� z z q z m r1f `, R z C Q V1 a d 2 Z G G Q R ,n ro m ro m v E Q Q 7 EE [ O J> xq z O 7 d J a:o 0 O % QF rQEE J =cuC 0J QE6E Ln N o o o Ln .y E o In o n to a EE ❑ O Q Ln ❑ry E o ru a v cu a m 7 a m a m 7 Q m en a m Z a to N a m m a m LL L7 d S l~9 a cm7 a l7 a C7 a 4 t�7 o S f7 O F�- l�7 n 7 lm7 a o V1 y 7 a. ti n. LA IL to C�7 a V1 l�3 0 7 3 4 , 1t/ IJ _ ` — 6 , 7 I ,r - 10 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot p tvote-vvrrcrrrvertiterets a d scre Cp ncy attecung Nortn iarouna compliance samples, a copyor tnis roan win oe sent to the Narth Carolina DENR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID: 69614 Page 2 of 2 Page 162 of 165 f - - - •- • . I—. . 1— .-VVMJ vU I_�JczgIIFIC \.VrILlILIVII t-AVVII nu;,VIHL Effective Date: 05/121202205/12/2022 'Check mark top half of box if pH and/or dechiorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, oil and Grease, 0RO/8015 (water) DOC, Wig *"Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine W0# : 92:636049 project (l PM: SC Due Date: 11/7$i22 CLIENT: 92-HOR -F r- -,,,T_T_ -JIT- � a z z i ;I z N a ? N u Q . z m m T m ? i2 ro v v u a v v °d n v>> _ m v i I I °.' 0 IVv N a °� V 4! _ Q n Z 1 Z O 4 v H !' v a v a v a al a O M O a d O ro O 0 `f O z ? 0 i -' ` `-' I r � v n .o > a 7 c n = Z = z N .o Z v r _ G D N T Z z = M nl 4 a 0 > <° !a z 0 0 a c x u m c M n^, a a. 7 N ro Jf ro V. o , •" n vl N m y es o y A Gl E a -0 A E - E Q Z Q 7 4 2 Q Y' Q y v - a - Li w 9 a 4 1 E a a E ¢ `� o b o a `^ ' a ¢ Ln Q E u1 E 0 E o °= 0 .n u w o °% E C .J E E J J E E N !3 �1 € J E J E [: E J E N v1 O — ,n rV Ln N Ln N �y N M S = N ._ •-i = ri 0 Ln f•1 0 Ln nl G v O c� O •� p V p V M Ln W O N O Ln O .-E 0 ry O c! tt E 7 M j N 7 e-1 V1 Z M N d 00 iy 7 ri 2 ri M N ri Y r H SY 7 ' 7 m ra m m G. 0. 4 0. �, 3 L7 lj' L7 L7 f+1 L7 (9 to 1 Obi l7 T 0 O>i 0 CNi 0 0 'A N °�, m O Lyr Gt co ro to m ¢ ¢ ¢ a ¢ Q o > 0 0 7 m a � o 3LN — — 5 6 7 8 9 10 — i2 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative tot 4 adjusted added _ �Infn.-��rk nrrr,n,rrlNvrrx»�; �.• :-�,.w ��rr—�xr-_��r �-1:--.. �l �': �-.. ti. �...: � _r .�_:. r___- ..._.. � - ��....... ...........o....,................ ._..-,..._..__ ._...�....., .....,., ......., .....�....�� .,. ,cn� .o u.e "UFr 15 taro€Ina utwt L.ertliicdtlon Office (i.e. Out of hold, incorrect preservative, out of ternp, incorrect containers. Qualtrax ID: 69614 Page 2 of 2 Page 163 of 165 ry v` ck ui a °1 N I?mue1E a y W w C (0 (NIM euuol4O Esnpisea du109Z8 s(?plDl4WaH 4M L80B ij U _ � � � . � 4 N x -1 x x x I x 4 ! ` ,' � � � t {� s! 9. [� ? z(NIA) iy i 41 z 0 - X x (Nu) l�alul saldweg paleaS R o sn uO Pan10308 w dwAl TI [ m E OLZB Xi x x x n � 9 apyInS x x x x x x X x x x X x rCL r � e eplueFO X x x x x X x x x x x x 4 � f_vS 'N o � sal x x x x x x x x x x x x 1 U � m m G 4 NIS 09Ze X X x X x Xi x x x X X X U �J m [Oc #+ 09Z8 X x x x x x X X X x x X c No OL17LIO(Og x x x X x x x x x x a)a ✓1!u!le fIV x x X X x x x x x ±XX XamIO 00130&08 0 00EX x X x x X x v NIA 38a1 WSAIBUV ? 3 40 T o a Iaue4laW � Ai W EOZSZBN !11 u -7 U HoeN f Y K jC - Cc w a EONH Y S k Y k X ! !C k O LU ID z m t^OSZH (li a o u a n 6 a a` Pamasaidu0 1 a C k �v k !1r jp ♦/M V O O N C Q U Q K w N01103TI00 iV dW313ldWV3 n �1V 0: W U 'g OLLI w c7 a C V F a o uaj o z uj `o G U m = m o w rc E J t� z rc CL r- cc O V) ^ o (d400=0 6V2l9=g} 3aA13'lari7s U iL m Wal of ODPW REA aril 3000 X181VW r $ rr $ a Q v m 1L O E rc 1 m v o � C m ci 0 p m U0Sa. m03 aOk u 6 u x m g �a`33am°03a�w o 'S m 4 m On x g ck 2 w 1 u E Lu $ 2 o 0 Id 2 V a u o g }� U Z m Q U o RF to N Y [mri r m 0 4 c � u m F t # W311 �' �+ M v m m Y Page 164 of 165 V1 d' 0 a to w a e (N)A) N ' •�+ { saldwgSweg w NIA 3 f 0 Jal000 ni ;" " N ,s IV _r1 fV o PaleeS u� {NIA) ail c m c - � � � � N ¢ q 21 z uo Pansa�a v $ (NIA) auuolul0 lenplsab 3 drn r uela dpl O9Z9 x L e9 a a seplolcpaH 1919 x X x X 5 4909 X K x x U h OLZ9 X x X X x m apUpS x x x X x x x x X ++ C ' LL aplue,(O X x x x X X x x X d¢ c (" Em o '� E SOU x X x x x x X x X WISO9Z9 x X X x X X x X x ci U P m 09Z9 x x x x x x x x X QQ y� 9 com N OLI LIMN x X X X X X x x x m N n E a w kUilemly X x x x x X X lO h16 OOSO5 O OOE x X X x x x X X x QD c �c a m m U LLqu N/A ;sa; sastjeud y Q w n.. o o n I4ueylaW SJ £OZSZeN W a - m — — ¢ U Q U q m HOeN lh a W AEI m m bOSZH O W m " z m m° .� U 0 L v c c ri Q 0, it f pamesaidun U-p ul 6 U 4 a a d 5?J3 NItl1NO3dO i1LL N0110311001V dW313ldViVS y m U w \ '. W �, ) O N F x N N '5 '� Z c ,c3 ❑ ¢ Q v c w a i o V f— z fir, z cn w0 w ` d- y `)p w C a'Y h A h o `n o M1n Ctt Q .= u f ~ a1 1 (dFY00=0 9Va'�=0) 3dA13ldWtlS � U � O N m E m di r $ rr 5 LU w (�lal as sapoo Allen sas) 3000 XIki1VW c4 LL m a a m~ H O E g 2 ik p rr aOr v 0 O U C o >. n 0. 2m m u0i acn0 c rn 12 K U d d d o u K H , e IE6 m m Q p W f (�}y E Lu a am �I N R C DL U N C m W' T O \ _ f lFC R � N o c�� O O rn w w ❑ w eo N 0 V 1 E (� l's Q alNq o f y U) 0 u - a h - P v z m * W31� r r N N N cmN Page 165 of 165 This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C - Field Data t r- Appendix C — Field Data Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C — Field Data This page intentionally left blank. F37Z DEPTH TO WATER AND GAS READINGS Project Name: OSR Landfill Date: _1 V17/'ZZ Locaiton: Winston-Salem, NC Protect Number: 10243102 Time Started: Time Finished: 1 2 Personnel: Signature: - - Well ID Depth to water (ft btoc) Total Depth (ft btoc) Notes/Comments MW-111 3LI, ( 7 ay. MW-211 �, z �'V MW-311 AM r� 7 MW-4R AIA MW-5R _ r MW-7 2I,dMA MW-8 AIA d MW-9 . i ,' c MW-10 A) MW-11 MW-12 rj . �l Ili M W-13 M W-14 NA MW-15 j Well ID CH4 % CO2 % 02 % Balance MM-1 0-0 157, S MW-111 0 i (C> v 1 % MW-211 ©. `Z 20 `l cn7 MW-13 MW-15 i 7,0i a Notes/Comments: J, 2C) M) Version: 10/31/2022 Sheet of _ KR Groundwater Sampling Form Sample ID: MW-iR Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: T-77 Weather: S -5 0( [ Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 45' - 60' Pump Type: Dedicated Bladder Pump Well Depth (ft): 60' (' 1, 7 S Pump Depth (ft-bTOC): _60' Depth -to -Water (ft-bT0Q 34-70" 737 , - Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): 2:3 -27 Well Volume (ft^3): 4:SP&► `�-1 - 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) � TEMP (CI) COND. (µ5/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) r _S 3.. S , t 6 d5� 23 OA-t. <:2)0 102_a - - a AQt 2- z 7 I� ,7 5rG A -17 S92 ICE 5.2 S 3Sc) L �; Gy�S 2, 3`jv 3r5� )7.�1 23+�. d. * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative M W-1 R VV �j 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly 44A 8270 SVOC 2 100ml Amber glass NA 8081 Pesticides 2 100ml Amber glass NA 8151 Herbicides 2 1L Amber glass NA Sampled By: - ,}g:7 Sample Time: Date Sampled: �l rd� Sampler Signature:�-- 11).O h} i �K5 r i - eel, C'J. 104 Version: 10/31/2022 Sheet Of _ IIIIIIIIIINN Groundwater Sampling Form Sample ID: MWAR Purging Information (Page 2) VOLUME VOLUME PURGE DEPTH TO .. pH COND. DISSOLVED OXYGEN = ORP TURBIDITY 0% COLOR/ ...• (describe)77 00-belaw 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable L/ Version: 10/31/2022 Sheet _ of KR Groundwater Sampling Form Sample ID: MW-211 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: <' Date: 11 Weather: el �w s Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 6' - 21' Pump Type: Dedicated Bladder Pump Well Depth (ft): 21' Pump Depth (ft-bTOC): •,� -� Depth -to -Water (ft-bToQ _ '2 Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): i 2, , Well Volume (ft^3): 2, 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP. (C�) COND. (µS/cm) (5%) DISSOLVED OXYGEN (10%)* (0%) ORP (mV) (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) l-�y ? o ( `J (ter V ` . l iC, i ., J 8 71/ +'l 0,173 �� r• ic`? io_3 `�l < 2 o ice_.&II I�.:�� r '.37., i r.z9 r/ * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative Orl 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 2SOml Poly NA 6010/7470 250ml Poly HNO3 VY M W-2 R 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500mi Poly NA Cyanide 125ml Poly 4A ii 8270 SVOC 2 100ml Amber glass I NA 8081 Pesticides 2 100ml Amber glass NA 8151 Herbicides 2 1L Amber glass NA Sampled By: ) L . ( Sample Time: Date Sampled: 1f 2 2 Sampler Signature: D11 +25 i4�>r. Version: 10/31/2022 Sheet I off <J. v' Fez Groundwater Sampling Form Sample ID: MW-3R Site Information .Site Name: OSR Landfill Project Number: 10347433 Site Locati n: Winston-Salem, NC Sampling Personnel: L& Date: 2 `2 Weather: Well Information Well Diameter (in): 2" Purge Equipment: GeeWch Screened Interval (ft): 12' - 27' Pump Type: D di • r Pum Well Depth (ft): ZT `--� fr l Pump Depth (ft-bTOC):` Depth -to -Water (ft-bTOC): lam, Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): j • �, '' Well Volume (ft^3): 1.j s '�• " 1 Well Volume = (Total Depth - Static Water Level) * Wel Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) P / TEMP, (C°) COND. (µ5/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) /13 �7-5 -3 �00.cX3 20. j 2 C_S / 2 16.0 326.1 . 3 ?� 3-.112 � .-`2 7 -75 �� S 23Et_ -2 -2 151 .�� se' � C. -1,Q /, , 22-50 2011 1g tr, I le. 2 ,i 2-2.9 0-' 9 S WR2,0 SS3.'26 :3 8QC 1,7,5 ►tl_26 3-ecs ?o.17 L, _L/ci 16, 2.32q- I !. 5 a Il, 5 / , -76 13, oe� 3 20,i 7 µZ'/7 16, - ;,29., 2, 471-1 --4'3. 3 50 v . 7 15 1 Lf. i `7 -Cv -ec) Z, 4 327,Z 2 .e' 0 -S f 21�75.5 0 35<7z:, i 6 I V 16. 5 327-6 2 -(os' 1 60,o " DO below 2.0 mg/L is stable at ±0-2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative M1A1_3p YY R 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly NL 8270 SVOC 2 100ml Amber glass NA 1 P es --PiA NA 815 - — Sample Time: r lass Sampled By: Date Sampled: f I`7I Sampler Signature: • �- Version: 10/31/2027 Sheet a of 2 F)l Groundwater Sampling Form Sample ID: MW-311 Purging Information (Page 2) VOLUME PURGE DEPTH TO pH COND. DISSOLVED OXYGEN .•• :.COLOR/ 0 ...• ' DO below 2.0 mg/l. is stable at t0.2 mglL; DO below 0.5 mglt is stable Version: 10/31/2022 Sheet" of FP Groundwater Sampling Form Sample ID: MW-411 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: tr W -T-T Weather: c .-- cr - 11( p Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 5' - 20' Pump Type: Dedicated Bladder Pump Well Depth (ft): 20' Pump Depth (ft-bTOC): — Depth -to -Water (ft-bTOC): _ �,i Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): 12 - 13 Well Volume (ft^3): a ,' i / 7 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP, (C') COND. ([IS/cm)(mV) (5%) DISSOLVED OXYGEN (mg/1-)(Liters) (10%)* ORP (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) 13u d, ZS 7Gc� 7,'r- , o7,75 0 3 1. cl 2 l 2, 5L173 : rya-/A,,,a l3Z 1 zS - 2-S - 7,'IZ4 16 9 l 5 vim ':35 i . ZS ,7 S 2,3�_`7 7Z � 3� 12 7 0 : '� r I L-! , s ) , E iq00 . ZS `]' ,� 1 �� 3'9 1123 - 3 1It,C-) 6c .""'ItN'4 Ir J44''S IL (O, 1 f6 6 1 r Z -7--1 ,3 —IAA 11415 125 lU.--s 35C> 6r,/ sT Q-ems 1 7- 3 .IS 4 t&i 1, 7 s I .coca 3SC5 16 6, 3� d. 3 1202 Z5—F7s 75- ,-spa o,i-7 <f_3e T 1213 <5 777 " DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative Li 13c) 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 M`A'_�-if� n o VV 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly —kA 8270 SVOC 2 100ml Amber glass NA 8081 Pesticides 2 100ml Amber glass NA 8151 Herbicides 2 1L Amber glass NA Sampled By: Sample Time: pate Sampled: Sampler Signature: N=O /-/ S . /" � �"C44 Version: 10/31/2022 Sheet. _ of IIIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: MW-5R Site Information .Site Name: OSR Landfill Project Number: 10347433 .Site Location: Winston-Salem, NC Sampling Personnel: , 7 C Date: 11 ct 2 Weather: 77775 Well Information 'Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 15' - 30' Pump Type: Dedicated Bladder Pump Well Depth (ft): 30' Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): `(. L/ Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) ' TEMP. (C°) COND. (µ5/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (s10 or 10%) COLOR/ ODOR (describe) �cG i.Zs .2-.s0 I _9cD G IS [r,_.2 C73: e6 2 R3.� r S, 1,2 -5 IG 2-5c--, [_ 1 '3 .2 V7L. ? 5, 5-7 log 3 0,�2L-r �r 526 i,2 S 5.0 a 2-. fl,` z-1 j L'i 16 172 J,Ca r I I 152-5 l>2S 61,11S /j t(&,3 172.7 5. -7 1 122.1 ©.;;_5 c �AM �53o iI. 7• o G I I,I co ,1 C( 3 t? 2-2 123 i O -.1 c tv * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA A'C o 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL M, VV_ 7R TDS 500ml Poly NA Cyanide 125ml Poly INA- -C— m er g 'assNA esticides 210 �erg+as — Icides 2 1L Sampled By: Isample Time: 16 2,,,S Date Sampled: // �i -77z- Isampler Signature: rE� s�lRd A�df- Z Version: 10/31/2022 Sheet of IIIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: MW-7 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: �J Date: [ l i Z.Z Weather: SD a = /22C:> - 77 S6 Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 33' - 48' Pump Type: Dedicated Bladder Pump Well Depth (ft): 48' Pump Depth (ft-bT0Q r— Depth-to-Water (ft-bTOC): 1-/.0 S Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): j$,-q_S iWell Volume (ft"3): 2,.?- 7.. osr ,. Q C--� 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP (C") COND. (Ps/cm) (S%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) 1.75 260 3 Y.91 4 Q 4 �� , p 3 0.2 1 r.Zs 2.50 2.s� V.35 5.413 16.0 25 0.2-10 1/ .1 41.f, 9 1 -� / 3s 1.25 3.75 2.3d N.1-12 5.92 6.b etc 0.1,9 OQ.9 0,2d -x• e,l I.2s S . 34f 3S' , 7 7 © f at 10 Z. O. 0 / C , 1795 1,25 ra 2.5 2sa 39-I.Ho S.99 15.01 ?cr O 45.'-I O. 15 CIO, 1 .2 s cr� 'Z_�o a Ll.1-I 1 S• Cl U 15. 5 Iry 3 0, 13 `F 3. -©. 2 V c fe,-hj * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative C 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 VY MW_7 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly NA 8270 SVOC 2 100ml Amber glass NA --Pd �r glass ---UA --- SampledBy: /-��` Sample Time: / Date Sampled: / J -32 -L Isampler Signature: pj�'c cf' N-,014 e & , 441 5v (FIJ -e Version: 10/31/2022 Sheet of FYZGroundwater Sampling Form Sample ID: MW-8 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: J5� Date: 1 1 4 -Z Weather: s C 4� Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 12' - 27' Pump Type: Dedicated Bladder Pump Well Depth (ft): 27' Pump Depth (ft-bTOC): (Depth -to -Water (ft-bT0Q I 16 Tubing Diameter (in): 3/8" X 1/2" 'Water Column Thickness (ft): Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) 4 ! 4 / TEMP. (CI) COND. (VS/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (<10 or 10%) COLOR/ ODOR (describe) Oq 35 1. . 25 2 6c3 11. 58 16.5 81. 5. a -7 JQ 7, c3 3.07 CKA (. 25 26 o 11;.70 5.G5 15.5 Qg. Cj.�6 I63. 1 ?. 7 3 aS�iS .25 got.0 e-q 5 .cam 15.5 go(.'-( G.al 1 0Y o r ©gss r. as 6. 25 ZJ (at.13 5.6 f-i 1s.5 �?'q t 5.4/0 17zi. 3 2 .zl,q I low 1,2-5 9.6c� 5d /g.9 7 194,0 5.52 1/76.3 1 !. 6 0 C ro,� 10>5 ). Z5 SY.75 I 2-sc-, 20.02 I91o.'1 6 .58 1 177�7 10.6 A I* DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable I Sample Information Sample Number Collection Time Parameter Container Preservative M,� A,_� V V 0-7i 300.0 SO4/ 4500 CL 250ml Poly NA t.ro Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS SOOmI Poly NA Cvanide 125ml Polv 44A Sampled By: Sample Time: Date Sampled: 15ampler Signature: �� Version: 10/31/2022 Sheet of FN Groundwater Sampling Form Sample ID: MW-9 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: j(Tei � Weather: (�CD Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 45' - 60' Pump Type: Dedicated Bladder Pump Well Depth (ft): 60' Pump Depth (ft-bTOC):'- Depth-to-Water (ft-bTOC): , 1 Z I iTubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): Well Volume (ft^3): ,_ 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP, (Co) COND. (PS/cm) (5%) DISSOLVED OXYGEN (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (<_SO or 10%) COLOR/ ODOR (describe) d `�S ).25 /: 2 23 5, 6 Z 15, 1 16( . 6.41 13-7_ z 7,06 �. oQ�s 1 2 © 2-So j J..1/o 9 6 15. 3 '-1. '-1 _6 1Sf . l �/, zS -S 2 s 0 .6 1, 3 /S.'Z 15`/,S S. fffi :5 A ogs /, 2S 5 (D 2- Sc /y 3�/ �. °�� t/L5_` I�ji LI _� �7F 2IA J j 2-5'C� 51.3x-1 5,6 G I.J,3 155,1 5.l66,1. //1l!61 42- 2'9 -2® S© 2SC 5(-`3E-1 _ © 15�3 155, N� ' DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative dq0 300.0 504/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL MW-9 TDS 500ml Poly NA Cyanide 125ml Poly .NA -. 1-00mt A n-beFgla -NA- -S-1�r3-I�Erbrcid-es �"�_ �'�L ATrrb Sampled By: A Sample Time: mac' Date Sampled: ( Z-Z Sampler Signature:_ Version: 10/31/2022 Sheet of Groundwater Sampling Form Sample ID: MW-10 Site Information :Site Name: OSR Landfill Project Number: 10347433 :Site Location: Winston-Salem, NC Sampling Personnel: Date: Weather:66 e.a Well Information 'Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 6' - 21' Pump Type: Dedicated Bladder Pump 'Well Depth (ft): 21.0' Pump Depth (ft-bT0Q —� Depth -to -Water (ft-bTOC): /! . 7 3 'Tubing Diameter (in): 3/8" X 1/2" 'Water Column Thickness (ft): % lWell Volume (ft^3): ! . 5 ! ^ oI 0. 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) j ( TEMP. (C`) COND. (µ5/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (510 or 10%) COLOR/ ODOR (describe) 13 vo t . 2 S : 5CD 12.20 6.2 t om! ho8 I- - �, 3 V�.�ti ,v a- /34rs /. Z _Sa '1S o 12.22 6.?g I�;�1 1fr" I.41'k (3-5r,) I.2 5 2ss 2.2 z( ro,7 7 17.3 18 2r, /155 12 5 .00 2 sn 12, 23 C.75 D 1 et 2,65 - K 1,6 8 ` &2-70 (, 2S 2- 2a 5 (2, 2 4,77 17 S 198 50 3 S (2 -1 � �� � 44, /`(05 (-2-5 ? 2-5C> 12. 2 7 i'I . 2 17 7 3 9_ 4 -ik. zt q c1 -10 t , 2-S 2-5 2-S< l 2 . Z3 r 1 -7 ? 17. 2 17 ti a * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 M W-1� 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly .W �Z2�S 2 100ml Amber glass NA estiEici�s—� __NA A�xrber- giassr— Sampled By: Sample Time: Date Sampled: Isampler Signature: U -,o 0 Version: 10/31/2022 Sheet of ER Groundwater Sampling Form Sample ID: MW-11 Site Information Site Name: OSR Landfill Project Number: 10347433 F. Site Location: Winston-Salem, NC Sampling Personnel: Date: 11 9 z-Z Weather: 3 Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 5' - 20' Pump Type: Dedicated Bladder Pump Well Depth (ft): 20.0' Pump Depth (ft-bT0Q -7---' Depth -to -Water (ft-bTOC): 3, Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): 1 �, I �7 Well Volume (ftA3): ( oV 0 ' - 1 Well Volume = (Total Depth - Static Water Level) * We Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) r ^v I 1 TEMP. (C") COND. (PS/cm) (S%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (<10 or 10%) COLOR/ ODOR (describe) h 2-1 -5 3 `=r2 G,ai1 1�.6, qo..';l 21,4i1 9-2 9 All �. S �.. 50 250 -(ZO 6,66 2`0,. , 2 1 13. ,) R -2-5-01 0. 2 5,3.. 0..I -2,"7 11.6(S' 1!2 ,. 2 5 2fn k,02 Q;� 16,3 . � Q,Z-( e i MO I' ,!5, 5c3 <3'q c� G. n 1 sq� " q o &,oz I 7-5 z .,)-2 --lo �.3Li N 0-50 - 00 0-) q. U'2 6,Q-"-q 16 . 253.`' r i 1 V-11. 9 1,9. 7 7 A ti 125 1,2- 111 ,15 2 SC) 4,0 G,bc1 l�*`J 3- ©, i .-7 r )3- 1,9, -/tA 12_Sc� 45� '02 .i I ---INA * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL MW-11 TDS 500ml Poly NA Cyanide 125ml Poly r ttrG fS 2 e2 10131 n -AM155Ffr-gTa55 NSA _-&LS1-H r-bi64e-,— — 4L--Aiyfber--g6i5-N Imo_ Sampled By: Sample Time: 1,2,fx!5 Date Sampled: I Sampler Signature: -. J' I k, c) 77 f %ti '� -'�� rk.,( furl Version: 10/31/2022 Sheet of IMN Groundwater Sampling Form Sample ID: MW-12 Site Information .Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: } s Date: 72 Weather: , r 7" Well Information 'Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 5.58' - 15.58' Pump Type: Dedicated Bladder Pump 'Well Depth (ft): 15.58' Pump Depth (ft-bTOC):K--� Depth -to -Water (ft-bTOC): �,• Tubing Diameter (in): 3/8" X 1/2" 'Water Column Thickness (ft): lWell Volume (ft^3): >,- 0, 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP. (C") COND. (PS/Cm (5%) DISSOLVED OXYGEN) (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (!510 or 10%) COLOR/ ODOR (describe) trt 1, -3 Z Q, 37 16.6 1. Z7 - lc,, 7 -2 9 _ l Z C36 1, 17,• 7 , Cq C. 3`7 Ib.7 -72�2 31/.0 * DO below 2,0 mg/L is stable at±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative L/ 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL MW-12 8260 S/M 3 40ml Amber glass HCL VY TDS SOOmI Poly NA Cyanide 125ml Poly —4A —AIA� Sampled By: , z Sample Time: L. f Date Sampled: A ,Z zz- Sampler Signature:_,,,,--- Imo.. i7 .1 V,xo ,-/ 5 c/1 f'Yc", E Version: 10/31/2022 Sheet of FN Groundwater Sampling Form Sample ID: MW-13 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: [ - Weather: c-� �-- c; r o , Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 5' - 20' Pump Type: Dedicated Bladder Pump Well Depth (ft): 20' Pump Depth (ft-bTOC):-- Depth -to -Water (ft-bTOC): K, ? Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): ,11,7 Well Volume (ft^3): j 9 1 q-1 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO ' WATER (ft-bTOC) P TEMP. (C`) COND. (PS/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (<10 or 10% ) COLOR/ ODOR (describe) -2_ 6 c?,10 Kod'� 333-6 1,69 163.. S 'i? . S- I � 1 .3 L 2 3 122. Zr . I 7 << � 1020 _ 26'0 ` L-5 5.yrC-) 1 1'z17,9 cj:6'-1 5,.Li 2 i -7 �G,q_3 0 '99 192 N '23 �u C53O I 7H 2 -?2 - '30-1 0_q I rq3-5 ` " DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative MW-13 r!j 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly —4Pr 8270 SVOC 2 100ml Amber glass NA �— Q;-; -L-ember-g NA Sampled By: �'. !._, t �. Sample Time: Date Sampled: Sampler Signature: -- U zip' /-j 1d-�S 501N"y—e / 25 1 l�j 1-1 Version: 10/31/2022 Sheet of IIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: MW-14 Site Information Site Name: OSR Landfill Project Number: 10347433 .Site Location: Winston-Salem, NC Sampling Personnel: - �f c Date: 114V4z Weather: 7) 7! 3 Well Information Well Diameter (in): 2" Purge Equipment: Geotech Screened Interval (ft): 4S' - 60' Pump Type: Dedicated Bladder Pump Well Depth (ft): 60' Pump Depth (ft-bT0Q �- Depth-to-Water (ft-bTOC): i Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): Well Volume (ft,' 3): 1 o4-1 7 y 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) D / TEMP. (C°) COND. (µS/cm) (5%) DISSOLVED OXYGEN (10%)* ORP (mV) +20mV (- ) TURBIDITY (NTUs) (<10 or 10% ) COLOR/ ODOR (describe) h/ /7 -J�,1- 7 /�'7 Z 1 /., _) � /� �,) 10.'1 '''()10%)*/ ` /- �i % (OC%: `7 9 N-�- 1t�re� 1-5 !S 1,'2S 2, Rio Sc� l.[Gt _ ! ?. 203.o y.,9) 5171 3.5 3�N4 -�,75 A .L1 - 2 Ll� 1W, C'-.;,A (5 1125 5-1 /65 1-17,9 1-1 l7.1 y.ti S. !, s 20 6 Q 25Ce 5 5-60 L6 . tj 9. 1171, , r * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative M� � VY_f1 A 'F 57 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Cyanide 125ml Poly -UA 92;19 SVQ(; _ 2-t00m4Am 80 0M m er g ._$1S,LLIe.rbicides —�-- Sampled By: �. r f Sample Time: Date Sampled: ( Sampler Signature: iH rGy Version: 10/31/2022 Sheet of FN Groundwater Sampling Form Sample ID: MW-15 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: Weather: Well Information Well Diameter (in): 2" Purge Equipment: Mega Monsoon Pro Screened Interval (ft): 33' - 48' Pump Type: ESP Well Depth (ft):<I<8* .-SCO, Q r, c Pump Depth (ft-bTOC): Lj Depth -to -Water (ft-bTOC): �p Tubing Diameter (in): 3/8" X 1/2" Water Column Thickness (ft): 6(. Well Volume (ft^3): .act or 0. 26 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) � P r TEMP, (C°) COND. (Ps/cm) (5/) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±ZOmV) TURBIDITY (NTUs) (<_10 or 10%) COLOR/ ODOR (describe) �3 '4?5 Z 2�.1� _ 1 3 .9a 1 v fl Wn C. :Z®. 3't-3.3 7.9 67. y �s Z Sc 3, CDO ! 'Yak. I S '-Z 5�, 7,'Ll 52 1 e--" tJA 1,J 5 s75 jy�� ,1 C) {d 05 //� 6G 2. ��2jj1��,.5 W• 3-7jw7 `! 3 { d -7V.'O Q l� C 1 w �i Ko.07 C. Z) 21.0 30-C 7.2.1 77v C5 2 � * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative YY J MW_1 C 300.0 SO4/ 4500 CL 250m6 Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500MI Poly NA Cyanide 125ml Poly ftA-� . 8270 SVOC 2 100ml Amber glass NA 8081 Pesticides 2 100ml Amber glass NA 8151 Herbicides 2 1L'Amber glass NA Sampled By: 6,e- Sample Time: %50 cj Date Sampled: Z2 Sampler Signature:. .C,14 Version: 10/31/2022 Sheet of 1111111111111N Groundwater Sampling Form Sample ID: SW-1 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: =fib Date: Z `Z Weather: Well Information Well Diameter (in): N/A Purge Equipment: N/A Screened Interval (ft): N/A Pump Type: N/A Well Depth (ft): N/A Pump Depth (ft-bTOC): N/A Depth -to -Water (ft-bTOC): N/A Tubing Diameter (in): N/A Water Column Thickness (ft): N/A Well Volume (ft^3): N/A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) Q r TEMP. (C°) COND. (µ5/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (_<10 or 10%) COLOR/ ODOR (describe) 65 ,i-2 * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative S� `._� {j�/ Gl 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA Sampled By: j �� Sample Time: �= Date Sampled: �C �Z"r Isampler Signature• _----[— Version: 10/31/2022 Sheet Of IIIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: SW-2 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel:' �. Date: f 7 Z 2 Weather: Well Information Well Diameter (in): N/A Purge Equipment: N/A Screened Interval (ft): N/A Pump Type: N/A Well Depth (ft): N/A Pump Depth (ft-bT0Q N/A Depth -to -Water (ft-bT0Q N/A Tubing Diameter (in): N/A Water Column Thickness (ft): N/A Well Volume (ft^3): N/A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) TEMP. (C.) COND. (µS/cm) S/c DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±20mV) TURBIDITY (NTUs) (<_10 or 10%) COLOR/ ODOR (describe) �Z2_ R5).-/ * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative SW-2 9j 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA 8270 SVOC 2 100ml Amber glass NA c=- �x f 1 •--zp A/ Sampled By: �7 - Sample Time: Date Sampled: v—, —Z Sampler Signature Version: 1013112022 Sheet of IIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: SW-3 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: j 7 2 Weather: Well Information Well Diameter (in): N/A Purge Equipment: N/A Screened Interval (ft): N/A Pump Type: N/A Well Depth (ft): N/A Pump Depth (ft-bTOC): N/A Depth -to -Water (ft-bT0Q N/A Tubing Diameter (in): N/A Water Column Thickness (ft): N/A lWell Volume ("3): N/A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI VOLUME CUMULATIVE VOLUME PURGE DEPTH TO /� TEMP COND. DISSOLVED OXYGEN ORP TURBIDITY COLOR/ TIME PURGED (Liters) PURGED RATE (mL/min) WATER % � . (C°) (PS/cm) (mg/L) (mV) (NTUs) (<10 ODOR (Liters) (ft-bTOC) (5%) (10/)* (±20mV) or 10%) (describe) ) * DO below 2.0 mg/L is sable at ±0.2 mg/L; DO below 0.5 MAJI. is stable Sample Information Sample Number Collection Parameter Time 300.0 SO4/ 4500 CL Alkalinity 6010/7470 8260 VOC SUV_3 8260 S/M VY �I TDS Sampled By: Sample Time: Date Sampled: Isampler 5ignE Container I Preservative 250ml •Poly NA 250mrPoly NA 250ml Poly HNO3 3 40ml Amber glass HCL 3 40ml Amber glass HCL 500ml Poly NA [' /2-611'{ ,ems I., 11CM ( --12,ri ,f ,rr�� �91" Version: 10/31/2022 Sheet Of FN Groundwater Sampling Form Sample ID: SW-4 Site Information Site Name: OSR Landfill Project Number: 10347433 Site Location: Winston-Salem, NC Sampling Personnel: Date: 2 'Z Weather: '7(n) Well Information Well Diameter (in): N/A Purge Equipment: N/A Screened Interval (ft): N/A Pump Type: N/A Well Depth (ft): N/A Pump Depth (ft-bTOC): N/A Depth -to -Water (ft-bTOC): N/A Tubing Diameter (in): N/A Water Column Thickness (ft): N/A lWell Volume (ft^3): N/A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hanna, YSI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) n TEMP. (CI) COND. (PS/cm) (5%) DISSOLVED OXYGEN (mg/L) (10%)* ORP (mV) (±20mV) TURBIDITY (NTUs) (<_10 or 10%) COLOR/ ODOR (describe) * DO below 2.0 mg/L is stable at ±0.2 mg/L; DO below 0.5 mg/L is stable Sample Information Sample Number Collection Time Parameter Container Preservative SIN-4 VV ?� 300.0 SO4/ 4500 CL 250ml Poly NA Alkalinity 250ml Poly NA 6010/7470 250ml Poly HNO3 8260 VOC 3 40ml Amber glass HCL 8260 S/M 3 40ml Amber glass HCL TDS 500ml Poly NA mpled By: �1� Sample Time: Date Sampled: 1 i -72`2 Sampler signature: l ra This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files (Paper Copies Only) f 1 Appendix D —Electronic Files (Paper Copies Only) Portable document format (PDF) of this report Electronic data deliverable (EDD) of Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files (Paper Copies Only) This page intentionally left blank. FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-1R 72-54-8 60 4,4'-DDD 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 50-29-3 62 4,4'-DDT 0.026 ug/L U EPA 8081E 0.026 0.05 0.1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 309-00-2 9 Aldrin 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 959-98-8 105 Endosulfanl 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 33213-65-9 106 Endosulfan1) 0.016 ug/L U EPA 8081E 0.016 0.05 0.1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 72-20-8 108 Endrin 0.018 ug/L U EPA 8081E 0.018 0.05 0.11 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 7421-93-4 109 Endrin aldehyde 0.016 ug/L U EPA 8081E 0.0161 0.05 0.1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 76-44-8 117 Heptachlor 0.02 ug/L U EPA 8081E 0.02 0.05 0.05 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 1024-57-3 118 Heptachlor epoxide 0.028 ug/L U EPA 8081E 0.028 0.05 0.075 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 72-43-5 135 Methoxychlor 0.042 ug/L U EPA 8081E 0.042 0.15 1 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 319-84-6 24 alpha-BHC 0.012 ug/L U EPA 8081E 0.012 0.05 0.05 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 319-86-8 26 delta-BHC 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/10/2022 11/15/2022 11/16/2022 12 MW-2R 72-54-8 60 4,4'-DDD 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 50-29-3 62 4,4'-DDT 0.022 ug/L U,L1 EPA 8081E 0.222 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 309-00-2 9 Aldrin 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 959-98-8 105 Endosulfanl 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 33213-65-9 106 Endosulfan1) 0.013 ug/L U EPA 8081E 0.013 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 72-20-8 108 Endrin 0.015 ug/L U EPA 8081E 0.015 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 7421-93-4 109 Endrin aldehyde 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 76-44-8 117 Heptachlor 0.016 ug/L U EPA 8081E 0.016 0.042 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 1024-57-3 118 Heptachlor epoxide 0.024 ug/L U EPA 8081E 0.024 0.042 0.075 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 72-43-5 135 Methoxychlor 0.035 ug/L U,L1 EPA 8081E 0.035 0.12 1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 319-84-6 24 alpha-BHC 0.01 ug/L U EPA 8081E 0.01 0.042 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-2R 319-86-8 26 delta-BHC 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-4R 72-54-8 60 4,4'-DDD 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 50-29-3 62 4,4'-DDT 0.022 ug/L U,L1 EPA 8081E 0.022 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 309-00-2 9 Aldrin 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 959-98-8 105 Endosulfanl 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 33213-65-9 106 Endosulfan1) 0.013 ug/L U EPA 8081E 0.013 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 72-20-8 108 Endrin 0.015 ug/L U EPA 8081E 0.015 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 7421-93-4 109 Endrin aldehyde 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 76-44-8 117 Heptachlor 0.016 ug/L U EPA 8081E 0.016 0.042 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 1024-57-3 118 Heptachlor epoxide 0.024 ug/L U EPA 8081E 0.024 0.042 0.075 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 72-43-5 135 Methoxychlor 0.035 ug/L U,L1 EPA 8081E 0.035 0.12 1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 319-84-6 24 alpha-BHC 0.01 ug/L U EPA 8081E 0.01 0.0421 0.051 1 11/9/2022 11/14/2022 11/15/2022 12 MW-4R 319-86-8 26 delta-BHC 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-15 72-54-8 60 4,4'-DDD 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 50-29-3 62 4,4'-DDT 0.022 ug/L U EPA 8081E 0.022 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 309-00-2 9 Aldrin 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 959-98-8 105 Endosulfanl 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 33213-65-9 106 Endosulfan1) 0.013 ug/L U EPA 8081E 0.013 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 72-20-8 108 Endrin 0.015 ug/L U EPA 8081E 0.015 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 7421-93-4 109 Endrin aldehyde 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 76-44-8 117 Heptachlor 0.016 ug/L U EPA 8081E 0.016 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 1024-57-3 118 Heptachlor epoxide 0.024 ug/L U EPA 8081E 0.024 0.042 0.075 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 72-43-5 135 Methoxychlor 0.035 ug/L U EPA 8081E 0.035 0.12 1 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 319-84-6 24 alpha-BHC 0.01 ug/L U,R1 EPA 8081E 0.01 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 MW-15 319-86-8 26 delta-BHC 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 72-54-8 60 4,4'-DDD 0.014 ug/L U EPA 8081E 0.0141 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 50-29-3 62 4,4'-DDT 0.022 ug/L U EPA 8081E 0.022 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 309-00-2 9 Aldrin 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 959-98-8 105 Endosulfanl 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 33213-65-9 106 Endosulfan1) 0.013 ug/L U EPA 8081E 0.013 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 72-20-8 108 Endrin 0.015 ug/L U EPA 8081E 0.015 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 7421-93-4 109 Endrin aldehyde 0.014 ug/L U EPA 8081E 0.014 0.042 0.1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 76-44-8 117 Heptachlor 0.016 ug/L U EPA 8081E 0.016 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 1024-57-3 118 Heptachlor epoxide 0.024 ug/L U EPA 8081E 0.024 0.042 0.075 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 72-43-5 135 Methoxychlor 0.035 ug/L U EPA 8081E 0.035 0.12 1 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 319-84-6 24 alpha-BHC 0.01 ug/L U EPA 8081E 0.01 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 EQBL 319-86-8 26 delta-BHC 0.012 ug/L U EPA 8081E 0.012 0.042 0.05 1 11/7/2022 11/11/2022 11/14/2022 12 FB 72-54-8 60 4,4'-DDD 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 50-29-3 62 4,4'-DDT 0.026 ug/L U,L1 EPA 8081E 0.026 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 309-00-2 9 Aldrin 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 FB 959-98-8 105 Endosulfanl 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 33213-65-9 106 Endosulfan1) 0.016 ug/L U EPA 8081E 0.016 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 72-20-8 108 Endrin 0.018 ug/L U EPA 8081E 0.018 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 7421-93-4 109 Endrin aldehyde 0.016 ug/L U EPA 8081E 0.016 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 76-44-8 117 Heptachlor 0.02 ug/L U EPA 8081E 0.02 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 FB 1024-57-3 118 Heptachlor epoxide 0.028 ug/L U EPA 8081E 0.028 0.05 0.075 1 11/9/2022 11/14/2022 11/15/2022 12 FB 72-43-5 135 Methoxychlor 0.042 ug/L U,L1 EPA 8081E 0.042 0.15 1 1 11/9/2022 11/14/2022 11/15/2022 12 FB 319-84-6 24 alpha-BHC 0.012 ug/L U EPA 8081E 0.0121 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 FB 319-86-8 26 delta-BHC 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 72-54-8 60 4,4'-DDD 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 50-29-3 62 4,4'-DDT 0.026 ug/L U,L1 EPA 8081E 0.026 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 309-00-2 9 Aldrin 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 959-98-8 105 Endosulfanl 0.017 ug/L U EPA 8081E 0.017 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 33213-65-9 106 Endosulfan1) 0.016 ug/L U EPA 8081E 0.016 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 72-20-8 108 Endrin 0.018 ug/L U EPA 8081E 0.018 0.05 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 7421-93-4 109 Endrin aldehyde 0.016 ug/L U EPA 8081E 0.0161 0.051 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 76-44-8 117 Heptachlor 0.02 ug/L U EPA 8081E 0.02 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 1024-57-3 118 Heptachlor epoxide 0.028 ug/L U EPA 8081E 0.028 0.05 0.075 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 72-43-5 135 Methoxychlor 0.042 ug/L U,L1 EPA 8081E 0.042 0.15 1 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 319-84-6 24 alpha-BHC 0.012 ug/L U EPA 8081E 0.012 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 DUP-1 319-86-8 26 delta-BHC 0.014 ug/L U EPA 8081E 0.014 0.05 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 72-54-8 60 4,4'-DDD 0.015 ug/L U EPA 8081E 0.015 0.045 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 50-29-3 62 4,4'-DDT 0.023 ug/L U,L1 EPA 8081E 0.023 0.045 0.11 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 309-00-2 9 Aldrin 0.013 ug/L U EPA 8081E 0.013 0.045 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 959-98-8 105 Endosulfanl 0.016 ug/L U EPA 8081E 0.016 0.045 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 33213-65-9 106 Endosulfan1) 0.014 ug/L U EPA 8081E 0.014 0.045 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 72-20-8 108 Endrin 0.016 ug/L U EPA 8081E 0.016 0.045 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 7421-93-4 109 Endrin aldehyde 0.015 ug/L U EPA 8081E 0.015 0.045 0.1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 76-44-8 117 Heptachlor 0.018 ug/L U EPA 8081E 0.018 0.045 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 1024-57-3 118 Heptachlor epoxide 0.026 ug/L U EPA 8081E 0.026 0.045 0.075 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 72-43-5 135 Methoxychlor 0.038 ug/L U,L1 EPA 8081E 0.0381 0.141 1 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 319-84-6 24 alpha-BHC 0.011 ug/L U EPA 8081E 0.011 0.045 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-7 319-86-8 26 delta-BHC 0.013 ug/L U EPA 8081E 0.013 0.045 0.05 1 11/9/2022 11/14/2022 11/15/2022 12 MW-10 72-54-8 60 4,4'-DDD 0.015 ug/L U EPA 8081E 0.015 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 50-29-3 62 4,4'-DDT 0.023 ug/L U,L1 EPA 8081E 0.023 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 309-00-2 9 Aldrin 0.013 ug/L U EPA 8081E 0.013 0.045 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 959-98-8 105 Endosulfanl 0.016 ug/L U EPA 8081E 0.016 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 33213-65-9 106 Endosulfan1) 0.014 ug/L U EPA 8081E 0.014 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 72-20-8 108 Endrin 0.016 ug/L U EPA 8081E 0.0161 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 7421-93-4 109 Endrin aldehyde 0.015 ug/L U EPA 8081E 0.015 0.045 0.1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 76-44-8 117 Heptachlor 0.018 ug/L U EPA 8081E 0.018 0.045 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 1024-57-3 118 Heptachlor epoxide 0.026 ug/L U EPA 8081E 0.026 0.045 0.075 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 72-43-5 135 Methoxychlor 0.038 ug/L U,L1 EPA 8081E 0.038 0.14 1 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 319-84-6 24 alpha-BHC 0.011 ug/L U EPA 8081E 0.011 0.045 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-10 319-86-8 26 delta-BHC 0.013 ug/L U EPA 8081E 0.013 0.045 0.05 1 11/8/2022 11/14/2022 11/15/2022 12 MW-1R 7440-23-5 322 Sodium 16200 ug/L EPA 6010 540 2000 NE 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-31-5 195 Tin 16 ug/L U EPA 6010 161 50 100 1 11/10/2022 12/7/2022 12/8/2022 667 MW-2R 7440-23-5 322 Sodium 60500 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-4R 7440-23-5 322 Sodium 74000 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-15 7440-23-5 322 Sodium 16800 ug/L EPA 6010 540 2000 NE 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-23-5 322 Sodium 540 ug/L U EPA 6010 540 2000 NE 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/7/2022 12/7/2022 12/8/2022 667 FB 7440-23-5 322 Sodium 540 ug/L U EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-23-5 322 Sodium 72000 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-3R 7440-23-5 322 Sodium 2480 ug/L EPA 6010 540 2000 NE 1 11/10/2022 12/8/2022 12/9/2022 667 MW-3R 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/10/2022 12/8/2022 12/9/2022 667 SW-2 7440-23-5 322 Sodium 18800 ug/L EPA 6010 540 2000 NE 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/7/2022 12/7/2022 12/8/2022 667 MW-5R 7440-23-5 322 Sodium 13300 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-23-5 322 Sodium 11200 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-23-5 322 Sodium 14600 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-31-5 195 Tin 16 ug/L U EPA 6010 161 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-11 7440-23-5 322 Sodium 11900 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-23-5 322 Sodium 23700 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-31-5 195 Tin 16 ug/L U EPA 6010 161 501 1001 11 11/8/2022 12/7/2022 12/8/2022 667 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-13 7440-23-5 322 Sodium 17800 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-23-5 322 Sodium 18000 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/8/2022 12/7/2022 12/8/2022 667 SW-1 7440-23-5 322 Sodium 13100 ug/L EPA 6010 540 2000 NE 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 1001 1 11/6/2022 12/7/2022 12/8/2022 667 SW-3 7440-23-5 322 Sodium 16800 ug/L EPA 6010 540 2000 NE 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-23-5 322 Sodium 35500 ug/L EPA 6010 540 2000 NE 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/7/2022 12/7/2022 12/8/2022 667 MW-7 7440-23-5 322 Sodium 43900 ug/L EPA 6010 540 2000 NE 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-10 7440-23-5 322 Sodium 112000 ug/L EPA 6010 540 2000 NE 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-31-5 195 Tin 16 ug/L U EPA 6010 16 50 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-1R 7440-36-0 13 Antimony 0.56 ug/L 1 EPA 6020 0.5 1 6 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-39-3 15 Barium 304 ug/L EPA 6020 0.5 1 100 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-41-7 23 Beryllium 0.46 ug/L EPA 6020 0.033 0.1 1 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-43-9 34 Cadmium 0.09 ug/L 1 EPA 6020 0.067 0.1 1 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-47-3 51 Chromium 7.9 ug/L EPA 6020 0.5 1 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-48-4 53 Cobalt 0.74 ug/L 1 EPA 6020 0.24 11 101 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-50-8 54 Copper 5.3 ug/L EPA 6020 0.16 1 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7439-89-6 340 Iron 719 ug/L EPA 6020 6.4 10 300 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7439-92-1 131 Lead 0.46 ug/L 1 EPA 6020 0.22 1 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7439-96-5 342 Manganese 63.4 ug/L EPA 6020 0.29 1 50 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-02-0 152 Nickel 5.8 ug/L EPA 6020 0.26 1 50 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7782-49-2 183 Selenium 0.39 ug/L 1 EPA 6020 0.2 2 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-22-4 184 Silver 0.053 ug/L 1 EPA 6020 0.028 0.5 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-62-2 209 Vanadium 3 ug/L EPA 6020 0.91 11 25 1 11/10/2022 12/7/2022 12/8/2022 667 MW-1R 7440-66-6 213 Zinc 15.2 ug/L EPA 6020 4.3 5 10 1 11/10/2022 12/7/2022 12/8/2022 667 MW-2R 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-38-2 14 Arsenic 1 ug/L EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-39-3 15 Barium 467 ug/L EPA 6020 0.5 1 1001 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-41-7 23 Beryllium 0.082 ug/L 1 EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-47-3 51 Chromium 0.75 ug/L 1 EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-48-4 53 Cobalt 26.3 ug/L EPA 6020 0.24 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-50-8 54 Copper 1.5 ug/L EPA 6020 0.16 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7439-89-6 340 Iron 10100 ug/L EPA 6020 31.8 50 300 5 11/8/2022 12/7/2022 12/9/2022 667 MW-2R 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7439-96-5 342 Manganese 18900 ug/L EPA 6020 14.6 50 50 50 11/8/2022 12/7/2022 12/9/2022 667 MW-2R 7440-02-0 152 Nickel 13.8 ug/L EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-62-2 209 Vanadium 1.3 ug/L EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-2R 7440-66-6 213 Zinc 6 ug/L EPA 6020 4.31 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-4R 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-38-2 14 Arsenic 1.6 ug/L EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-39-3 15 Barium 157 ug/L EPA 6020 0.5 1 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-41-7 23 Beryllium 0.055 ug/L 1 EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-47-3 51 Chromium 0.55 ug/L 1 EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-48-4 53 Cobalt 80.1 ug/L EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-50-8 54 Copper 0.64 ug/L 1 EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7439-89-6 340 Iron 2150 ug/L EPA 6020 6.4 10 300 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7439-96-5 342 Manganese 1110 ug/L EPA 6020 1.5 5 50 5 11/9/2022 12/7/2022 12/9/2022 667 MW-4R 7440-02-0 152 Nickel 8.9 ug/L EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 MW-4R 7440-66-6 213 Zinc 18.6 ug/L EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-15 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-39-3 15 Barium 18.1 ug/L EPA 6020 0.5 1 100 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-41-7 23 Beryllium 0.049 ug/L 1 EPA 6020 0.033 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-47-3 51 Chromium 1.7 ug/L EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-48-4 53 Cobalt 0.36 ug/L 1 EPA 6020 0.241 11 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-50-8 54 Copper 3.8 ug/L EPA 6020 0.16 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7439-89-6 340 Iron 440 ug/L EPA 6020 6.4 10 300 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7439-92-1 131 Lead 0.33 ug/L 1 EPA 6020 0.22 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7439-96-5 342 Manganese 475 ug/L EPA 6020 0.58 2 50 2 11/7/2022 12/7/2022 12/9/2022 667 MW-15 7440-02-0 152 Nickel 2.4 ug/L EPA 6020 0.26 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-22-4 184 Silver 0.079 ug/L 1 EPA 6020 0.028 0.5 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-62-2 209 Vanadium 2.1 ug/L EPA 6020 0.91 1 25 1 11/7/2022 12/7/2022 12/8/2022 667 MW-15 7440-66-6 213 Zinc 9.5 ug/L EPA 6020 4.3 5 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-39-3 15 Barium 0.5 ug/L U EPA 6020 0.5 1 100 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-41-7 23 Beryllium 0.033 ug/L U EPA 6020 0.033 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-47-3 51 Chromium 0.5 ug/L U EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-48-4 53 Cobalt 0.24 ug/L U EPA 6020 0.24 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-50-8 54 Copper 0.16 ug/L U EPA 6020 0.16 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7439-89-6 340 Iron 6.4 ug/L U EPA 6020 6.4 10 300 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7439-96-5 342 Manganese 0.37 ug/L 1 EPA 6020 0.29 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-02-0 152 Nickel 0.26 ug/L U EPA 6020 0.26 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/7/2022 12/7/2022 12/8/2022 667 EQBL 7440-66-6 213 Zinc 11.5 ug/L EPA 6020 4.3 5 10 1 11/7/2022 12/7/2022 12/8/2022 667 FB 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-39-3 15 Barium 0.5 ug/L U EPA 6020 0.5 1 1001 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-41-7 23 Beryllium 0.033 ug/L U EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-47-3 51 Chromium 0.5 ug/L U EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-48-4 53 Cobalt 0.24 ug/L U EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-50-8 54 Copper 0.74 ug/L 1 EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7439-89-6 340 Iron 6.7 ug/L 1 EPA 6020 6.4 10 300 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7439-96-5 342 Manganese 0.29 ug/L U EPA 6020 0.29 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-02-0 152 Nickel 0.26 ug/L U EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 FB 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-38-2 14 Arsenic 1.6 ug/L EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-39-3 15 Barium 154 ug/L EPA 6020 0.5 1 100 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-41-7 23 Beryllium 0.056 ug/L 1 EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-47-3 51 Chromium 0.62 ug/L 1 EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-48-4 53 Cobalt 79 ug/L EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-50-8 54 Copper 0.68 ug/L 1 EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7439-89-6 340 Iron 2160 ug/L EPA 6020 6.4 101 3001 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7439-96-5 342 Manganese 1170 ug/L EPA 6020 1.5 5 50 5 11/9/2022 12/7/2022 12/9/2022 667 DUP-1 7440-02-0 152 Nickel 8.6 ug/L EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 DUP-1 7440-66-6 213 Zinc 5.1 ug/L EPA 6020 4.31 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-3R 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-38-2 14 Arsenic 5.3 ug/L EPA 6020 0.5 1 10 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-39-3 15 Barium 231 ug/L EPA 6020 0.5 1 100 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-41-7 23 Beryllium 0.063 ug/L 1 EPA 6020 0.033 0.1 1 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-47-3 51 Chromium 0.69 ug/L 1 EPA 6020 0.5 1 10 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-48-4 53 Cobalt 12 ug/L EPA 6020 0.24 1 10 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-50-8 54 Copper 0.39 ug/L 1 EPA 6020 0.16 11 101 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7439-89-6 340 Iron 80000 ug/L EPA 6020 127 2001 3001 20 11/10/2022 12/8/2022 12/9/2022 667 MW-3R 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.221 11 10 1 11/10/2022 12/8/2022 12/8/2022 667 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-3R 7439-96-5 342 Manganese 5490 ug/L EPA 6020 5.8 20 50 20 11/10/2022 12/8/2022 12/9/2022 667 MW-3R 7440-02-0 152 Nickel 0.81 ug/L 1 EPA 6020 0.26 1 50 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7782-49-2 183 Selenium 0.23 ug/L 1 EPA 6020 0.2 2 10 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/10/2022 12/8/2022 12/8/2022 667 MW-3R 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 101 1 11/10/2022 12/8/2022 12/8/2022 667 SW-2 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.51 1 6 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-38-2 14 Arsenic 0.55 ug/L 1 EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-39-3 15 Barium 143 ug/L EPA 6020 0.5 1 100 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-41-7 23 Beryllium 0.034 ug/L 1 EPA 6020 0.033 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-47-3 51 Chromium 0.68 ug/L 1 EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-48-4 53 Cobalt 1.4 ug/L EPA 6020 0.24 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-50-8 54 Copper 0.55 ug/L 1 EPA 6020 0.16 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7439-89-6 340 Iron 4170 ug/L EPA 6020 6.4 10 300 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7439-96-5 342 Manganese 2990 ug/L EPA 6020 2.9 10 50 10 11/7/2022 12/7/2022 12/9/2022 667 SW-2 7440-02-0 152 Nickel 2.2 ug/L EPA 6020 0.26 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-62-2 209 Vanadium 0.99 ug/L 1 EPA 6020 0.91 1 25 1 11/7/2022 12/7/2022 12/8/2022 667 SW-2 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-5R 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-39-3 15 Barium 59.1 ug/L EPA 6020 0.5 1 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-41-7 23 Beryllium 0.033 ug/L U EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-47-3 51 Chromium 6.6 ug/L EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-48-4 53 Cobalt 0.24 ug/L U EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-50-8 54 Copper 0.25 ug/L 1 EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7439-89-6 340 Iron 42.5 ug/L EPA 6020 6.4 10 300 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7439-96-5 342 Manganese 1 ug/L EPA 6020 0.29 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-02-0 152 Nickel 1.2 ug/L EPA 6020 0.26 11 501 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7782-49-2 183 Selenium 0.23 ug/L 1 EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-62-2 209 Vanadium 5.5 ug/L EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 MW-5R 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-39-3 15 Barium 60.1 ug/L EPA 6020 0.5 1 100 11 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-41-7 23 Beryllium 0.47 ug/L EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-47-3 51 Chromium 3.8 ug/L EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-48-4 53 Cobalt 0.24 ug/L U EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-50-8 54 Copper 0.16 ug/L U EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7439-89-6 340 Iron 74.3 ug/L EPA 6020 6.4 10 300 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7439-96-5 342 Manganese 5.3 ug/L EPA 6020 0.29 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-02-0 152 Nickel 0.31 ug/L 1 EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7782-49-2 183 Selenium 1.2 ug/L 1 EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 MW-8 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-39-3 15 Barium 191 ug/L EPA 6020 0.5 1 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-41-7 23 Beryllium 0.26 ug/L EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-47-3 51 Chromium 0.61 ug/L 1 EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-48-4 53 Cobalt 0.24 ug/L U EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-50-8 54 Copper 0.37 ug/L 1 EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7439-89-6 340 Iron 142 ug/L EPA 6020 6.4 101 3001 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7439-96-5 342 Manganese 6.2 ug/L EPA 6020 0.29 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-02-0 152 Nickel 0.58 ug/L 1 EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 MW-9 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-11 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-39-3 15 Barium 69.6 ug/L EPA 6020 0.5 1 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-41-7 23 Beryllium 0.067 ug/L 1 EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-47-3 51 Chromium 0.5 ug/L U EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-48-4 53 Cobalt 2.2 ug/L EPA 6020 0.24 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-50-8 54 Copper 0.27 ug/L 1 EPA 6020 0.161 11 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7439-89-6 340 Iron 21200 ug/L EPA 6020 31.8 50 300 5 11/8/2022 12/7/2022 12/9/2022 667 MW-11 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7439-96-5 342 Manganese 1380 ug/L EPA 6020 1.5 5 50 5 11/8/2022 12/7/2022 12/9/2022 667 MW-11 7440-02-0 152 Nickel 0.67 ug/L 1 EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-11 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-38-2 14 Arsenic 0.57 ug/L 1 EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-39-3 15 Barium 161 ug/L EPA 6020 0.5 1 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-41-7 23 Beryllium 0.063 ug/L 1 EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-47-3 51 Chromium 0.77 ug/L 1 EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-48-4 53 Cobalt 5.5 ug/L EPA 6020 0.24 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-50-8 54 Copper 0.86 ug/L 1 EPA 6020 0.16 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7439-89-6 340 Iron 1290 ug/L EPA 6020 6.4 10 300 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7439-96-5 342 Manganese 5160 ug/L EPA 6020 2.9 10 50 10 11/8/2022 12/7/2022 12/9/2022 667 MW-12 7440-02-0 152 Nickel 9 ug/L EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-12 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-39-3 15 Barium 515 ug/L EPA 6020 1 2 100 2 11/8/2022 12/7/2022 12/9/2022 667 MW-13 7440-41-7 23 Beryllium 1.8 ug/L EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-43-9 34 Cadmium 0.072 ug/L 1 EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-47-3 51 Chromium 0.5 ug/L U EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-48-4 53 Cobalt 0.56 ug/L 1 EPA 6020 0.24 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-50-8 54 Copper 0.62 ug/L 1 EPA 6020 0.161 11 10 11 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7439-89-6 340 Iron 183 ug/L EPA 6020 6.4 10 300 11 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7439-96-5 342 Manganese 119 ug/L EPA 6020 0.29 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-02-0 152 Nickel 2.2 ug/L EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-13 7440-66-6 213 Zinc 8.9 ug/L EPA 6020 4.3 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-38-2 14 Arsenic 0.5 ug/L U EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-39-3 15 Barium 249 ug/L EPA 6020 0.5 1 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-41-7 23 Beryllium 0.69 ug/L EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-47-3 51 Chromium 0.97 ug/L 1 EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-48-4 53 Cobalt 0.27 ug/L 1 EPA 6020 0.24 11 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-50-8 54 Copper 1.1 ug/L EPA 6020 0.16 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7439-89-6 340 Iron 50.9 ug/L EPA 6020 6.4 10 300 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7439-96-5 342 Manganese 48.6 ug/L EPA 6020 0.29 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-02-0 152 Nickel 4.6 ug/L EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7782-49-2 183 Selenium 0.2 ug/L U EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-62-2 209 Vanadium 0.91 ug/L U EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-14 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 SW-1 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-38-2 14 Arsenic 0.71 ug/L 1 EPA 6020 0.5 1 10 1 11/6/2022 12/7/2022 12/8/2022 667 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY SW-1 7440-39-3 15 Barium 45.9 ug/L EPA 6020 0.5 1 100 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-41-7 23 Beryllium 0.11 ug/L EPA 6020 0.033 0.1 1 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-47-3 51 Chromium 2.5 ug/L EPA 6020 0.5 1 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-48-4 53 Cobalt 1.9 ug/L EPA 6020 0.24 1 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-50-8 54 Copper 4 ug/L EPA 6020 0.16 1 101 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7439-89-6 340 Iron 6950 ug/L EPA 6020 12.7 20 300 2 11/6/2022 12/7/2022 12/9/2022 667 SW-1 7439-92-1 131 Lead 2.4 ug/L EPA 6020 0.22 1 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7439-96-5 342 Manganese 721 ug/L EPA 6020 0.58 2 50 2 11/6/2022 12/7/2022 12/9/2022 667 SW-1 7440-02-0 152 Nickel 1.7 ug/L EPA 6020 0.26 1 50 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7782-49-2 183 Selenium 0.37 ug/L 1 EPA 6020 0.2 2 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-62-2 209 Vanadium 4.7 ug/L EPA 6020 0.91 1 25 1 11/6/2022 12/7/2022 12/8/2022 667 SW-1 7440-66-6 213 Zinc 22.9 ug/L EPA 6020 4.3 5 10 1 11/6/2022 12/7/2022 12/8/2022 667 SW-3 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-38-2 14 Arsenic 2 ug/L EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-39-3 15 Barium 367 ug/L EPA 6020 0.5 1 100 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-41-7 23 Beryllium 0.4 ug/L EPA 6020 0.033 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-47-3 51 Chromium 9.4 ug/L EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-48-4 53 Cobalt 4.5 ug/L EPA 6020 0.24 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-50-8 54 Copper 16.5 ug/L EPA 6020 0.16 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7439-89-6 340 Iron 37400 ug/L EPA 6020 63.7 100 300 10 11/7/2022 12/7/2022 12/9/2022 667 SW-3 7439-92-1 131 Lead 6.7 ug/L EPA 6020 0.22 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7439-96-5 342 Manganese 2690 ug/L EPA 6020 2.9 10 50 10 11/7/2022 12/7/2022 12/9/2022 667 SW-3 7440-02-0 152 Nickel 5.8 ug/L EPA 6020 0.26 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7782-49-2 183 Selenium 1.2 ug/L 1 EPA 6020 0.2 2 10 11 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-62-2 209 Vanadium 21.4 ug/L EPA 6020 0.91 1 25 1 11/7/2022 12/7/2022 12/8/2022 667 SW-3 7440-66-6 213 Zinc 51.8 ug/L EPA 6020 4.3 5 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-38-2 14 Arsenic 0.97 ug/L 1 EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-39-3 15 Barium 263 ug/L EPA 6020 0.5 1 100 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-41-7 23 Beryllium 0.22 ug/L EPA 6020 0.033 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-47-3 51 Chromium 5.3 ug/L EPA 6020 0.5 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-48-4 53 Cobalt 5.9 ug/L EPA 6020 0.24 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-50-8 54 Copper 5.5 ug/L EPA 6020 0.16 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7439-89-6 340 Iron 10800 ug/L EPA 6020 127 200 300 20 11/7/2022 12/7/2022 12/9/2022 667 SW-4 7439-92-1 131 Lead 2.4 ug/L EPA 6020 0.22 1 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7439-96-5 342 Manganese 6200 ug/L EPA 6020 5.8 20 50 20 11/7/2022 12/7/2022 12/9/2022 667 SW-4 7440-02-0 152 Nickel 6.4 ug/L EPA 6020 0.26 1 50 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7782-49-2 183 Selenium 0.65 ug/L 1 EPA 6020 0.21 2 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-62-2 209 Vanadium 12.7 ug/L EPA 6020 0.91 1 25 1 11/7/2022 12/7/2022 12/8/2022 667 SW-4 7440-66-6 213 Zinc 17.8 ug/L EPA 6020 4.3 5 10 1 11/7/2022 12/7/2022 12/8/2022 667 MW-7 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-38-2 14 Arsenic 0.62 ug/L 1 EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-39-3 15 Barium 283 ug/L EPA 6020 0.5 1 100 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-41-7 23 Beryllium 0.49 ug/L EPA 6020 0.033 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-43-9 34 Cadmium 0.16 ug/L EPA 6020 0.067 0.1 1 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-47-3 51 Chromium 0.8 ug/L 1 EPA 6020 0.5 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-48-4 53 Cobalt 3.8 ug/L EPA 6020 0.24 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-50-8 54 Copper 3.5 ug/L EPA 6020 0.16 1 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7439-89-6 340 Iron 413 ug/L EPA 6020 6.4 10 300 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7439-92-1 131 Lead 0.22 ug/L U EPA 6020 0.22 1 10 11 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7439-96-5 342 Manganese 657 ug/L EPA 6020 0.58 2 50 2 11/9/2022 12/7/2022 12/9/2022 667 MW-7 7440-02-0 152 Nickel 5.2 ug/L EPA 6020 0.26 1 50 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7782-49-2 183 Selenium 0.25 ug/L 1 EPA 6020 0.2 2 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-22-4 184 Silver 0.047 ug/L 1 EPA 6020 0.028 0.5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-62-2 209 Vanadium 1.1 ug/L EPA 6020 0.91 1 25 1 11/9/2022 12/7/2022 12/8/2022 667 MW-7 7440-66-6 213 Zinc 16.9 ug/L EPA 6020 4.3 5 10 1 11/9/2022 12/7/2022 12/8/2022 667 MW-10 7440-36-0 13 Antimony 0.5 ug/L U EPA 6020 0.5 1 6 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-38-2 14 Arsenic 0.9 ug/L 1 EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-39-3 15 Barium 93 ug/L EPA 6020 0.5 1 100 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-41-7 23 Beryllium 0.17 ug/L EPA 6020 0.033 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-43-9 34 Cadmium 0.067 ug/L U EPA 6020 0.067 0.1 1 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-47-3 51 Chromium 2.1 ug/L EPA 6020 0.5 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-48-4 53 Cobalt 5.8 ug/L EPA 6020 0.241 11 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-50-8 54 Copper 0.69 ug/L 1 EPA 6020 0.16 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7439-89-6 340 Iron 2460 ug/L EPA 6020 6.4 10 300 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7439-92-1 131 Lead 0.51 ug/L 1 EPA 6020 0.22 1 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7439-96-5 342 Manganese 21100 ug/L EPA 6020 14.6 50 50 50 11/8/2022 12/7/2022 12/9/2022 667 MW-10 7440-02-0 152 Nickel 10.5 ug/L EPA 6020 0.26 1 50 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7782-49-2 183 Selenium 1.4 ug/L 1 EPA 6020 0.2 2 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-22-4 184 Silver 0.028 ug/L U EPA 6020 0.028 0.5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-62-2 209 Vanadium 1.5 ug/L EPA 6020 0.91 1 25 1 11/8/2022 12/7/2022 12/8/2022 667 MW-10 7440-66-6 213 Zinc 4.3 ug/L U EPA 6020 4.3 5 10 1 11/8/2022 12/7/2022 12/8/2022 667 MW-1R 7439-97-6 132 Mercury 36.2 ug/L EPA 7470A 1.2 2 0.2 10 11/10/2022 11/21/2022 11/29/2022 40 MW-2R 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/8/2022 11/21/2022 11/28/2022 40 MW-4R 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 MW-15 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/7/2022 11/21/2022 11/28/2022 40 EQBL 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/7/2022 11/21/2022 11/28/2022 40 FB 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.21 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 DUP-1 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 MW-3R 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/10/2022 11/21/2022 11/28/2022 40 SW-2 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/7/2022 11/21/2022 11/28/2022 40 MW-5R 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 MW-8 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 MW-9 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.21 1 11/9/2022 11/21/2022 11/28/2022 40 MW-11 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.21 1 11/8/2022 11/21/2022 11/28/2022 40 MW-12 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/8/2022 11/21/2022 11/28/2022 40 MW-13 7439-97-6 132 Mercury 0.15 ug/L 1 EPA 7470A 0.12 0.2 0.2 1 11/8/2022 11/21/2022 11/28/2022 40 MW-14 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/8/2022 11/21/2022 11/28/2022 40 SW-1 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/6/2022 11/21/2022 11/28/2022 40 SW-3 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/7/2022 11/21/2022 11/28/2022 40 SW-4 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.2 0.2 1 11/7/2022 11/21/2022 11/28/2022 40 MW-7 7439-97-6 132 Mercury 0.17 ug/L 1 EPA 7470A 0.12 0.2 0.2 1 11/9/2022 11/21/2022 11/28/2022 40 MW-10 7439-97-6 132 Mercury 0.12 ug/L U EPA 7470A 0.12 0.21 0.21 1 11/8/2022 11/26/2022 11/28/2022 40 MW-1R 56-55-3 17 Benzo(a)anthracene 2.2 ug/L U EPA 8270E 2.2 8.3 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 218-01-9 52 Chrysene 2.3 ug/L U EPA 8270E 2.3 8.3 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 53-70-3 64 Dibenz(a,h)anthracene 2.5 ug/L U EPA 8270E 2.5 8.3 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.4 ug/L U EPA 8270E 2.4 8.3 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-1R 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.1 ug/L U EPA 8270E 3.1 5 15 1 11/10/2022 11/15/2022 11/16/2022 12 MW-2R 56-55-3 17 Benzo(a)anthracene 2.2 ug/L U EPA 8270E 2.2 8.3 10 1 11/8/2022 11/14/2022 11/16/2022 12 MW-2R 218-01-9 52 Chrysene 2.3 ug/L U EPA 8270E 2.3 8.3 10 1 11/8/2022 11/14/2022 11/16/2022 12 MW-2R 53-70-3 64 Dibenz(a,h)anthracene 2.5 ug/L U EPA 8270E 2.5 8.3 10 1 11/8/2022 11/14/2022 11/16/2022 12 MW-2R 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.4 ug/L U EPA 8270E 2.4 8.3 10 1 11/8/2022 11/14/2022 11/16/2022 12 MW-2R 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.1 ug/L U EPA 8270E 3.1 5 15 1 11/8/2022 11/14/2022 11/16/2022 12 MW-4R 56-55-3 17 Benzo(a)anthracene 2.7 ug/L U EPA 8270E 2.7 10 10 1 11/9/2022 11/15/2022 11/16/2022 12 MW-4R 218-01-9 52 Chrysene 2.8 ug/L U EPA 8270E 2.8 10 10 1 11/9/2022 11/15/2022 11/16/2022 12 MW-4R 53-70-3 64 Dibenz(a,h)anthracene 3 ug/L U EPA 8270E 3 10 10 1 11/9/2022 11/15/2022 11/16/2022 12 MW-4R 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.9 ug/L U EPA 8270E 2.9 10 10 1 11/9/2022 11/15/2022 11/16/2022 12 MW-4R 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.7 ug/L U EPA 8270E 3.7 6 15 1 11/9/2022 11/15/2022 11/16/2022 12 MW-15 56-55-3 171 Benzo(a)anthracene 2.2 ug/L U EPA 8270E 2.2 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 MW-15 218-01-9 52 Chrysene 2.3 ug/L U EPA 8270E 2.3 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 MW-15 53-70-3 64 Dibenz(a,h)anthracene 2.5 ug/L U EPA 8270E 2.5 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 MW-15 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.4 ug/L U EPA 8270E 2.4 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 MW-15 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.1 ug/L U EPA 8270E 3.1 5 15 1 11/7/2022 11/14/2022 11/15/2022 12 EQBL 56-55-3 17 Benzo(a)anthracene 2.4 ug/L U EPA 8270E 2.4 9.1 10 1 11/7/2022 11/14/2022 11/15/2022 12 EQBL 218-01-9 52 Chrysene 2.5 ug/L U EPA 8270E 2.5 9.1 101 1 11/7/2022 11/14/2022 11/15/2022 12 EQBL 53-70-3 64 Dibenz(a,h)anthracene 2.7 ug/L U EPA 8270E 2.7 9.1 10 1 11/7/2022 11/14/2022 11/15/20221 12 EQBL 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.6 ug/L U EPA 8270E 2.6 9.1 10 1 11/7/2022 11/14/2022 11/15/2022 12 EQBL 117-81-7 1111 bis(2-Ethylhexyl)phthalate 3.4 ug/L U EPA 8270E 3.4 5.5 15 1 11/7/2022 11/14/2022 11/15/2022 12 FB 56-55-3 171 Benzo(a)anthracene 2.4 ug/L U EPA 8270E 2.4 9.1 10 1 11/9/2022 11/15/2022 11/16/2022 12 FB 218-01-9 52 Chrysene 2.5 ug/L U EPA 8270E 2.5 9.1 10 1 11/9/2022 11/15/2022 11/16/2022 12 FB 53-70-3 64 Dibenz(a,h)anthracene 2.7 ug/L U EPA 8270E 2.7 9.1 10 1 11/9/2022 11/15/2022 11/16/2022 12 FB 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.6 ug/L U EPA 8270E 2.61 9.1 10 1 11/9/2022 11/15/2022 11/16/2022 12 FB 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.4 ug/L U EPA 8270E 3.4 5.5 15 1 11/9/2022 11/15/2022 11/16/2022 12 DUP-1 56-55-3 17 Benzo(a)anthracene 2.2 ug/L U EPA 8270E 2.2 8.3 10 1 11/9/2022 11/15/2022 11/16/2022 12 DUP-1 218-01-9 52 Chrysene 2.3 ug/L U EPA 8270E 2.3 8.3 10 1 11/9/2022 11/15/2022 11/16/2022 12 DUP-1 53-70-3 64 Dibenz(a,h)anthracene 2.5 ug/L U EPA 8270E 2.5 8.3 10 1 11/9/2022 11/15/2022 11/16/2022 12 DUP-1 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.4Lug/LL U EPA 8270E 2.4 8.3 10 1 11/9/2022 11/15/2022 11/16/2022 12 DUP-1 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.0 EPA 8270E 3.1 5 15 1 11/9/2022 11/15/2022 11/16/2022 12 MW-3R 56-55-3 17 Benzo(a)anthracene 2.4U EPA 8270E 2.4 9.1 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-3R 218-01-9 52 Chrysene 2.5U EPA 8270E 2.51 911 10 1 11/10/2022 11/15/2022 11/16/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-3R 53-70-3 64 Dibenz(a,h)anthracene 2.7 ug/L U EPA 8270E 2.7 9.1 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-3R 193-39-5 125 Indeno(1,2,3-cd)pyrene 2.6 ug/L U EPA 8270E 2.6 9.1 10 1 11/10/2022 11/15/2022 11/16/2022 12 MW-3R 117-81-7 111 bis(2-Ethylhexyl)phthalate 3.4 ug/L U EPA 8270E 3.4 5.5 15 1 11/10/2022 11/15/2022 11/16/2022 12 SW-2 56-55-3 17 Benzo(a)anthracene 2.2 ug/L U EPA 8270E 2.2 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 SW-2 218-01-9 52 Chrysene 2.3 ug/L U EPA 8270E 2.3 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 SW-2 53-70-3 641 Dibenz(a,h)anthracene 2.5 ug/L U EPA 8270E 2.5 8.3 101 1 11/7/2022 11/14/2022 11/15/2022 12 SW-2 193-39-5 1251 Indeno(1,2,3-cd)pyrene 2.4 ug/L U EPA 8270E 2.41 8.3 10 1 11/7/2022 11/14/2022 11/15/2022 12 SW-2 117-81-7 1111 bis(2-Ethylhexyl)phthalate 3.1 ug/L U EPA 8270E 3.1 5 15 1 11/7/2022 11/14/2022 11/15/2022 12 MW-1R 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-1R 7085-19-0 354 MCPP 0.323 ug/L U EPA 8321 0.323 2 NE 1 11/10/2022 11/25/2022 11/30/2022 MW-2R 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 11 11/8/2022 11/25/2022 11/30/2022 MW-2R 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-2R 7085-19-0 354 MCPP 5.67 ug/L EPA 8321 0.323 2 NE 1 11/8/2022 11/25/2022 11/30/2022 MW-4R 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-4R 7085-19-0 354 MCPP 8.02 ug/L EPA 8321 0.323 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-15 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/7/2022 11/25/2022 11/30/2022 MW-15 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/7/2022 11/25/2022 11/30/2022 MW-15 94-75-7 59 2,4-D 1 ug/L U EPA 8321 11 21 2 1 11/7/2022 11/25/2022 11/30/2022 MW-15 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/7/2022 11/25/2022 11/30/2022 MW-15 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/7/2022 11/25/2022 11/30/2022 MW-15 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/7/2022 11/25/2022 11/30/2022 MW-15 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/7/2022 11/25/2022 11/30/2022 MW-15 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/7/2022 11/25/2022 11/30/2022 MW-15 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/7/2022 11/25/2022 11/30/2022 MW-15 7085-19-0 354 MCPP 0.323 ug/L U EPA 8321 0.323 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/7/2022 11/25/2022 11/30/2022 EQBL 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/7/2022 11/25/2022 11/30/2022 EQBL 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/7/2022 11/25/2022 11/30/2022 EQBL 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 21 1 1 11/7/2022 11/25/2022 11/30/2022 EQBL 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/7/2022 11/25/2022 11/30/2022 EQBL 7085-19-0 354 MCPP 0.323 ug/L U EPA 8321 0.323 2 NE 1 11/7/2022 11/25/2022 11/30/2022 FB 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/9/2022 11/25/2022 11/30/2022 FB 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/9/2022 11/25/2022 11/30/2022 FB 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/9/2022 11/25/2022 11/30/2022 FB 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/9/2022 11/25/2022 11/30/2022 FB 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/9/2022 11/25/2022 11/30/2022 FB 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/9/2022 11/25/2022 11/30/2022 FB 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/9/2022 11/25/2022 11/30/2022 FB 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/9/2022 11/25/2022 11/30/2022 FB 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/9/2022 11/25/2022 11/30/2022 FB 7085-19-0 354 MCPP 0.323 ug/L U EPA 8321 0.323 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 93-76-5 188 2,4,5-T 0.573 ug/L U EPA 8321 0.573 2 2 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 93-72-1 185 2,4,5-TP(Silvex) 0.807 ug/L U EPA 8321 0.807 2 2 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 94-75-7 59 2,4-D 1 ug/L U EPA 8321 1 2 2 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 94-82-6 350 2,4-DB 1 ug/L U EPA 8321 1 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 127-20-8 355 Dalapon 0.621 ug/L U EPA 8321 0.621 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 1918-00-9 353 Dicamba 0.548 ug/L U EPA 8321 0.548 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 15165-67-0 352 Dichloroprop 0.367 ug/L U EPA 8321 0.367 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 88-85-7 102 Dinoseb 0.639 ug/L U EPA 8321 0.639 2 1 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 94-74-6 351 MCPA 0.363 ug/L U EPA 8321 0.363 2 NE 1 11/9/2022 11/25/2022 11/30/2022 DUP-1 7085-19-0 354 MCPP 8.96 ug/L EPA 8321 0.323 2 NE 1 11/9/2022 11/25/2022 11/30/2022 MW-1R 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/10/2022 11/15/2022 12 MW-1R 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/15/2022 12 MW-1R 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/10/2022 11/15/2022 12 MW-1R 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/15/2022 12 MW-1R 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/10/2022 11/15/2022 12 MW-1R 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/15/2022 12 MW-1R 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/10/2022 11/15/2022 12 MW-1R 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/10/2022 1 11/15/2022 12 MW-1R 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/10/2022 11/15/2022 12 MW-1R 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/10/2022 11/15/2022 12 MW-1R 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/15/2022 12 MW-1R 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/15/2022 12 MW-1R 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/15/2022 12 MW-1R 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/10/2022 11/15/2022 12 MW-1R 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/10/2022 11/15/2022 12 MW-1R 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/10/2022 11/15/2022 12 MW-1R 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/10/2022 11/15/2022 12 MW-1R 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/10/2022 11/15/2022 12 MW-1R 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/10/2022 11/15/2022 12 MW-1R 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/10/2022 11/15/2022 12 MW-1R 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/15/2022 12 MW-1R 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/10/2022 11/15/2022 12 MW-1R 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/10/2022 11/15/2022 12 MW-1R 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/10/2022 11/15/2022 12 MW-1R 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/15/2022 12 MW-1R 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/10/2022 11/15/2022 12 MW-1R 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/10/2022 11/15/2022 12 MW-1R 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/10/2022 11/15/2022 12 MW-1R 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/10/2022 11/15/2022 12 MW-1R 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/10/2022 11/15/2022 12 MW-1R 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/10/2022 11/15/2022 12 MW-1R 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/15/2022 12 MW-1R 100-41-4 110 Ethylbenzene 0.67 ug/L 1 EPA 8260D 0.3 1 1 1 11/10/2022 11/15/2022 12 MW-1R 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/10/2022 11/15/2022 12 MW-1R 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/10/2022 11/15/2022 12 MW-1R 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/15/2022 12 MW-1R 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/15/2022 12 MW-1R 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/10/2022 11/15/2022 12 MW-1R 108-88-3 196 Toluene 0.28 ug/L 1 EPA 8260D 0.24 1 1 1 11/10/2022 11/15/2022 12 MW-1R 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/10/2022 11/15/2022 12 MW-1R 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/15/2022 12 MW-1R 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.31 21 50 1 11/10/2022 11/15/2022 12 MW-1R 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/10/2022 11/15/2022 12 MW-1R 156-59-2 78 cis-1,2-Dichloroethene 0.64 ug/L 1 EPA 8260D 0.38 1 5 1 11/10/2022 11/15/2022 12 MW-1R 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/15/2022 12 MW-1R 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/10/2022 11/15/2022 12 MW-1R 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/10/2022 11/15/2022 12 MW-1R 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/10/2022 11/15/2022 12 MW-1R 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/15/2022 12 MW-1R 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.561 11 100 1 11/10/2022 11/15/2022 12 MW-2R 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/8/2022 11/15/2022 12 MW-2R 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-2R 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-2R 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-2R 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-2R 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-2R 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 11 11/8/2022 11/15/2022 12 MW-2R 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.341 21 13 11 11/8/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-2R 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/8/2022 11/15/2022 12 MW-2R 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/8/2022 11/15/2022 12 MW-2R 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-2R 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-2R 106-46-7 71 1,4-Dichlorobenzene 0.59 ug/L 1 EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-2R 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/8/2022 11/15/2022 12 MW-2R 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.481 5 50 1 11/8/2022 11/15/2022 12 MW-2R 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/8/2022 11/15/2022 12 MW-2R 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/8/2022 11/15/2022 12 MW-2R 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/8/2022 11/15/2022 12 MW-2R 71-43-2 16 Benzene 2.7 ug/L EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-2R 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-2R 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 11 1 11/8/2022 11/15/2022 12 MW-2R 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-2R 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.71 2 10 1 11/8/2022 11/15/2022 12 MW-2R 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-2R 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-2R 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/8/2022 11/15/2022 12 MW-2R 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-2R 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-2R 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-2R 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/8/2022 11/15/2022 12 MW-2R 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-2R 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-2R 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-2R 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-2R 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-2R 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-2R 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-2R 109-99-9 458 Tetrahydrofuran 12.8 ug/L v3 EPA 8260D 3.5 10 NE 1 11/8/2022 11/15/2022 12 MW-2R 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-2R 79-01-6 201 Trichloroethene 0.61 ug/L 1 EPA 8260D 0.38 1 1 1 11/8/2022 11/15/2022 12 MW-2R 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-2R 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-2R 75-01-4 211 Vinyl chloride 0.73 ug/L 1 EPA 8260D 0.39 1 1 1 11/8/2022 11/15/2022 12 MW-2R 156-59-2 78 cis-1,2-Dichloroethene 1.1 ug/L EPA 8260D 0.381 11 5 1 11/8/2022 11/15/2022 12 MW-2R 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-2R 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/8/2022 11/15/2022 12 MW-2R 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-2R 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-2R 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-2R 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/8/2022 11/15/2022 12 MW-4R 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 51 1 11/9/2022 11/15/2022 12 MW-4R 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.331 1 1 1 11/9/2022 11/15/2022 12 MW-4R 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/15/2022 12 MW-4R 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/15/2022 12 MW-4R 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/15/2022 12 MW-4R 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 MW-4R 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/15/2022 12 MW-4R 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/15/2022 12 MW-4R 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 11 1 11/9/2022 11/15/2022 12 MW-4R 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/15/2022 12 MW-4R 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/15/2022 12 MW-4R 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 MW-4R 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 MW-4R 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/15/2022 12 MW-4R 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/15/2022 12 MW-4R 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/15/2022 12 MW-4R 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 1001 1 11/9/2022 11/15/2022 12 MW-4R 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/15/2022 12 MW-4R 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/15/2022 12 MW-4R 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/15/2022 12 MW-4R 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/15/2022 12 MW-4R 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/15/2022 12 MW-4R 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/9/2022 11/15/2022 12 MW-4R 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.361 2 100 1 11/9/2022 11/15/2022 12 MW-4R 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 MW-4R 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/15/2022 12 MW-4R 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/9/2022 11/15/2022 12 MW-4R 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/9/2022 11/15/2022 12 MW-4R 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/15/2022 12 MW-4R 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/15/2022 12 MW-4R 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/9/2022 11/15/2022 12 MW-4R 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 MW-4R 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 MW-4R 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/15/2022 12 MW-4R 75-09-2 1401 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/9/2022 11/15/2022 12 MW-4R 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/15/2022 12 MW-4R 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/15/2022 12 MW-4R 109-99-9 458 Tetrahydrofuran 10 ug/L J,v2 EPA 8260D 3.5 10 NE 1 11/9/2022 11/15/2022 12 MW-4R 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/15/2022 12 MW-4R 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/15/2022 12 MW-4R 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 MW-4R 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/9/2022 11/15/2022 12 MW-4R 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/15/2022 12 MW-4R 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/9/2022 11/15/2022 12 MW-4R 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 MW-4R 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.711 2 NE 1 11/9/2022 11/15/2022 12 MW-4R 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/15/2022 12 MW-4R 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/15/2022 12 MW-4R 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 MW-4R 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/15/2022 12 MW-15 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/7/2022 11/15/2022 12 MW-15 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 MW-15 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/7/2022 11/15/2022 12 MW-15 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.321 1 1 1 11/7/2022 11/15/2022 12 MW-15 75-34-3 751 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/7/2022 11/15/2022 12 MW-15 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 MW-15 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/7/2022 11/15/2022 12 MW-15 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/7/2022 11/15/2022 12 MW-15 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/7/2022 11/15/2022 12 MW-15 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/7/2022 11/15/2022 12 MW-15 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 MW-15 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.361 1 1 1 11/7/2022 11/15/2022 12 MW-15 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 MW-15 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/7/2022 11/15/2022 12 MW-15 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/7/2022 11/15/2022 12 MW-15 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/7/2022 11/15/2022 12 MW-15 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 251 1001 1 11/7/2022 11/15/2022 12 MW-15 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/7/2022 11/15/2022 12 MW-15 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/7/2022 11/15/2022 12 MW-15 74-97-5 281 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/7/2022 11/15/2022 12 MW-15 75-27-4 291 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/7/2022 11/15/2022 12 MW-15 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/7/2022 11/15/2022 12 MW-15 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/7/2022 11/15/2022 12 MW-15 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.361 2 100 1 11/7/2022 11/15/2022 12 MW-15 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 MW-15 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/7/2022 11/15/2022 12 MW-15 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/7/2022 11/15/2022 12 MW-15 67-66-3 44 Chloroform 0.45 ug/L 1 EPA 8260D 0.43 1 5 1 11/7/2022 11/15/2022 12 MW-15 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/7/2022 11/15/2022 12 MW-15 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/7/2022 11/15/2022 12 MW-15 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/7/2022 11/15/2022 12 MW-15 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 MW-15 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 MW-15 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/7/2022 11/15/2022 12 MW-15 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/7/2022 11/15/2022 12 MW-15 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 MW-15 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 MW-15 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/7/2022 11/15/2022 12 MW-15 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 11 11 1 11/7/2022 11/15/2022 12 MW-15 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 11 1 11/7/2022 11/15/2022 12 MW-15 75-69-4 203 Trichlorofluoromethane 0.tg_/ U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 MW-15 108-05-4 210 Vinyl acetate 1.U,v2 EPA 8260D 1.3 2 50 1 11/7/2022 11/15/2022 12 MW-15 75-01-4 211 Vinyl chloride 0.3U EPA 8260D 0.39 1 1 1 11/7MW-15 156-59-2 78 cis-1,2-Dichloroethene 0.3U EPA 8260D 0.38 1 5 1 11/7/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-15 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 MW-15 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/7/2022 11/15/2022 12 MW-15 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/7/2022 11/15/2022 12 MW-15 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/7/2022 11/15/2022 12 MW-15 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 MW-15 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/7/2022 11/15/2022 12 EQBL 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/7/2022 11/15/2022 12 EQBL 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 EQBL 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/7/2022 11/15/2022 12 EQBL 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 EQBL 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/7/2022 11/15/2022 12 EQBL 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 EQBL 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/7/2022 11/15/2022 12 EQBL 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/7/2022 11/15/2022 12 EQBL 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/7/2022 11/15/2022 12 EQBL 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/7/2022 11/15/2022 12 EQBL 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 EQBL 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 EQBL 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 EQBL 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 11 11/7/2022 11/15/2022 12 EQBL 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.481 51 50 11 11/7/2022 11/15/2022 12 EQBL 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/7/2022 11/15/2022 12 EQBL 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/7/2022 11/15/2022 12 EQBL 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/7/2022 11/15/2022 12 EQBL 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/7/2022 11/15/2022 12 EQBL 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/7/2022 11/15/2022 12 EQBL 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/7/2022 11/15/2022 12 EQBL 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/7/2022 11/15/20221 12 EQBL 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.71 21 10 11 11/7/2022 11/15/2022 12 EQBL 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/7/2022 11/15/2022 12 EQBL 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 EQBL 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/7/2022 11/15/2022 12 EQBL 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/7/2022 11/15/2022 12 EQBL 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/7/2022 11/15/2022 12 EQBL 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/7/2022 11/15/2022 12 EQBL 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/7/2022 11/15/2022 12 EQBL 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.391 11 10 11 11/7/2022 11/15/2022 12 EQBL 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 EQBL 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 EQBL 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/7/2022 11/15/2022 12 EQBL 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/7/2022 11/15/2022 12 EQBL 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 EQBL 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 EQBL 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 1 11/7/2022 11/15/2022 12 EQBL 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/7/2022 11/15/2022 12 EQBL 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/7/2022 11/15/2022 12 EQBL 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 EQBL 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/7/2022 11/15/2022 12 EQBL 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/7/2022 11/15/2022 12 EQBL 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/7/2022 11/15/2022 12 EQBL 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 EQBL 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/7/2022 11/15/2022 12 EQBL 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/7/2022 11/15/2022 12 EQBL 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/7/2022 11/15/2022 12 EQBL 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 EQBL 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/7/2022 11/15/2022 12 FB 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/9/2022 11/15/2022 12 FB 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 FB 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/15/2022 12 FB 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/15/2022 12 FB 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/15/2022 12 FB 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 FB 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/15/2022 12 FB 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/15/2022 12 FB 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/15/2022 12 FB 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/15/2022 12 FB 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/15/2022 12 FB 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 FB 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 FB 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/15/2022 12 FB 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/15/20221 12 FB 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/15/2022 12 FB 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/15/2022 12 FB 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/15/2022 12 FB 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/15/2022 12 FB 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/15/2022 12 FB 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/15/2022 12 FB 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/15/2022 12 FB 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/9/2022 11/15/2022 12 FB 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/15/2022 12 FB 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 FB 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/15/2022 12 FB 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/9/2022 11/15/2022 12 FB 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/9/2022 11/15/2022 12 FB 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/15/2022 12 FB 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/15/2022 12 FB 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 101 1 11/9/2022 11/15/2022 12 FB 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 FB 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 FB 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/15/2022 12 FB 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/9/2022 11/15/2022 12 FB 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/15/2022 12 FB 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/15/2022 12 FB 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/9/2022 11/15/2022 12 FB 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 11 1 11/9/2022 11/15/2022 12 FB 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/15/2022 12 FB 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 FB 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/9/2022 11/15/2022 12 FB 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/15/2022 12 FB 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/9/2022 11/15/2022 12 FB 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 FB 179601-23-1 359 m&p-Xylene 0.75 ug/L 1,C0 EPA 8260D 0.71 2 NE 1 11/9/2022 11/15/2022 12 FB 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/15/2022 12 FB 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/15/2022 12 FB 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 FB 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/15/2022 12 DUP-1 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/9/2022 11/15/2022 12 DUP-1 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 DUP-1 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/15/2022 12 DUP-1 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.321 11 1 1 11/9/2022 11/15/2022 12 DUP-1 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/15/2022 12 DUP-1 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 DUP-1 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/15/2022 12 DUP-1 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/15/2022 12 DUP-1 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/15/2022 12 DUP-1 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/15/2022 12 DUP-1 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 11 1 11/9/2022 11/15/2022 12 DUP-1 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.361 1 1 1 11/9/2022 11/15/2022 12 DUP-1 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 DUP-1 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/15/2022 12 DUP-1 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/15/2022 12 DUP-1 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/15/2022 12 DUP-1 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/15/2022 12 DUP-1 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/15/2022 12 DUP-1 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/15/2022 12 DUP-1 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/15/2022 12 DUP-1 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/15/2022 12 DUP-1 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/15/2022 12 DUP-1 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/9/2022 11/15/2022 12 DUP-1 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/15/2022 12 DUP-1 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/15/2022 12 DUP-1 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28W13 1 11/9/2022 11/15/2022 12 DUP-1 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 11/9/2022 11/15/2022 12 DUP-1 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D ..43 1 11/9/2022 11/15/2022 12 DUP-1 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 11/9/2022 11/15/2022 12 DUP-1 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 11/9/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY DUP-1 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/9/2022 11/15/2022 12 DUP-1 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/15/2022 12 DUP-1 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 DUP-1 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/15/2022 12 DUP-1 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/9/2022 11/15/2022 12 DUP-1 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 11 1 11/9/2022 11/15/2022 12 DUP-1 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.291 1 1 1 11/9/2022 11/15/2022 12 DUP-1 109-99-9 458 Tetrahydrofuran 9.9 ug/L J,v2 EPA 8260D 3.5 10 NE 1 11/9/2022 11/15/2022 12 DUP-1 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/15/2022 12 DUP-1 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/15/2022 12 DUP-1 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/15/2022 12 DUP-1 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/9/2022 11/15/2022 12 DUP-1 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/15/2022 12 DUP-1 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/9/2022 11/15/2022 12 DUP-1 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 DUP-1 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/9/2022 11/15/2022 12 DUP-1 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/15/2022 12 DUP-1 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/15/2022 12 DUP-1 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/15/2022 12 DUP-1 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/15/2022 12 MW-3R 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/10/2022 11/14/2022 12 MW-3R 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 MW-3R 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/10/2022 11/14/2022 12 MW-3R 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 MW-3R 75-34-3 751 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/10/2022 11/14/2022 12 MW-3R 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 MW-3R 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 11 1 11/10/2022 11/14/2022 12 MW-3R 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/10/2022 11/14/2022 12 MW-3R 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/10/2022 11/14/2022 12 MW-3R 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/10/2022 11/14/2022 12 MW-3R 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 MW-3R 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 MW-3R 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 MW-3R 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/10/2022 11/14/2022 12 MW-3R 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/10/2022 11/14/2022 12 MW-3R 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/10/2022 11/14/2022 12 MW-3R 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/10/2022 11/14/2022 12 MW-3R 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/10/2022 11/14/2022 12 MW-3R 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/10/2022 11/14/2022 12 MW-3R 74-97-5 281 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/10/2022 11/14/2022 12 MW-3R 75-27-4 291 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/14/2022 12 MW-3R 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 11 31 1 11/10/2022 11/14/2022 12 MW-3R 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/10/2022 11/14/2022 12 MW-3R 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/10/2022 11/14/2022 12 MW-3R 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 MW-3R 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/10/2022 11/14/2022 12 MW-3R 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/10/2022 11/14/2022 12 MW-3R 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/10/2022 11/14/2022 12 MW-3R 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/10/2022 11/14/2022 12 MW-3R 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.361 11 3 1 11/10/2022 11/14/2022 12 MW-3R 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/10/2022 11/14/2022 12 MW-3R 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 MW-3R 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 MW-3R 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/10/2022 11/14/2022 12 MW-3R 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/10/2022 11/14/2022 12 MW-3R 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 MW-3R 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 MW-3R 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/10/2022 11/14/2022 12 MW-3R 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/10/2022 11/14/2022 12 MW-3R 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/10/2022 11/14/2022 12 MW-3R 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 MW-3R 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/10/2022 11/14/2022 12 MW-3R 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/10/2022 11/14/2022 12 MW-3R 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/10/2022 11/14/2022 12 MW-3R 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 MW-3R 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/10/2022 11/14/2022 12 MW-3R 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/10/2022 11/14/2022 12 MW-3R 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/10/2022 11/14/2022 12 MW-3R 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 MW-3R 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/10/2022 11/14/2022 12 SW-2 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/7/2022 11/15/2022 12 SW-2 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-2 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/7/2022 11/15/2022 12 SW-2 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-2 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/7/2022 11/15/2022 12 SW-2 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 SW-2 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/7/2022 11/15/2022 12 SW-2 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/7/2022 11/15/2022 12 SW-2 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/7/2022 11/15/2022 12 SW-2 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/7/2022 11/15/2022 12 SW-2 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-2 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-2 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-2 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/7/2022 11/15/2022 12 SW-2 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/7/2022 11/15/2022 12 SW-2 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/7/2022 11/15/2022 12 SW-2 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/7/2022 11/15/2022 12 SW-2 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/7/2022 11/15/2022 12 SW-2 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/7/2022 11/15/2022 12 SW-2 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/7/2022 11/15/2022 12 SW-2 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/7/2022 11/15/2022 12 SW-2 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/7/2022 11/15/2022 12 SW-2 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/7/2022 11/15/2022 12 SW-2 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/7/2022 11/15/2022 12 SW-2 56-23-5 361 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-2 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.281 1 3 1 11/7/2022 11/15/2022 12 SW-2 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/7/2022 11/15/2022 12 SW-2 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/7/2022 11/15/2022 12 SW-2 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/7/2022 11/15/2022 12 SW-2 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/7/2022 11/15/2022 12 SW-2 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/7/2022 11/15/2022 12 SW-2 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 SW-2 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 SW-2 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/7/2022 11/15/2022 12 SW-2 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/7/2022 11/15/2022 12 SW-2 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.291 1 1 1 11/7/2022 11/15/2022 12 SW-2 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 SW-2 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/7/2022 11/15/2022 12 SW-2 108-88-3 196 Toluene 0.3 ug/L 1 EPA 8260D 0.24 1 1 1 11/7/2022 11/15/2022 12 SW-2 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/7/2022 11/15/2022 12 SW-2 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 11 1 11/7/2022 11/15/2022 12 SW-2 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/7/2022 11/15/2022 12 SW-2 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/7/2022 11/15/2022 12 SW-2 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/7/2022 11/15/2022 12 SW-2 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-2 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/7/2022 11/15/2022 12 SW-2 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/7/2022 11/15/2022 12 SW-2 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/7/2022 11/15/2022 12 SW-2 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-2 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/7/2022 11/15/2022 12 MW-5R 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.311 1 5 1 11/9/2022 11/14/2022 12 MW-5R 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-5R 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/14/2022 12 MW-5R 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-5R 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/14/2022 12 MW-5R 75-35-4 771 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 51 1 11/9/2022 11/14/2022 12 MW-5R 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/14/2022 12 MW-5R 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/14/2022 12 MW-5R 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/14/2022 12 MW-5R 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/14/2022 12 MW-5R 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-5R 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-5R 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-5R 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 51 1001 1 11/9/2022 11/14/2022 12 MW-5R 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 51 501 1 11/9/2022 11/14/2022 12 MW-5R 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 51 1001 1 11/9/2022 11/14/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-5R 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/14/2022 12 MW-5R 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/14/2022 12 MW-5R 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/14/2022 12 MW-5R 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/14/2022 12 MW-5R 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/14/2022 12 MW-5R 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 31 1 11/9/2022 11/14/2022 12 MW-5R 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/9/2022 11/14/2022 12 MW-5R 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/14/2022 12 MW-5R 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-5R 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/14/2022 12 MW-5R 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/9/2022 11/14/2022 12 MW-5R 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/9/2022 11/14/2022 12 MW-5R 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/14/2022 12 MW-5R 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/14/2022 12 MW-5R 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/9/2022 11/14/2022 12 MW-5R 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-5R 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-5R 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/14/2022 12 MW-5R 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/9/2022 11/14/2022 12 MW-5R 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-5R 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-5R 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/9/2022 11/14/2022 12 MW-5R 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/14/2022 12 MW-5R 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/14/2022 12 MW-5R 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-5R 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/9/2022 11/14/2022 12 MW-5R 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/14/2022 12 MW-5R 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 51 1 11/9/2022 11/14/2022 12 MW-5R 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-5R 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.711 2 NE 1 11/9/2022 11/14/2022 12 MW-5R 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/14/2022 12 MW-5R 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/14/2022 12 MW-5R 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-5R 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/14/2022 12 MW-8 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/9/2022 11/14/2022 12 MW-8 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-8 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/14/2022 12 MW-8 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-8 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/14/2022 12 MW-8 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-8 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/14/2022 12 MW-8 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/14/2022 12 MW-8 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/14/2022 12 MW-8 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/14/2022 12 MW-8 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-8 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-8 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-8 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/14/2022 12 MW-8 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/14/2022 12 MW-8 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/14/2022 12 MW-8 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/14/2022 12 MW-8 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/14/2022 12 MW-8 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/14/2022 12 MW-8 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/14/2022 12 MW-8 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/14/2022 12 MW-8 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/14/2022 12 MW-8 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/9/2022 11/14/2022 12 MW-8 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/14/2022 12 MW-8 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-8 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/14/2022 12 MW-8 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/9/2022 11/14/2022 12 MW-8 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/9/2022 11/14/2022 12 MW-8 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/14/2022 12 MW-8 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/14/2022 12 MW-8 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.391 1 10 1 11/9/2022 11/14/2022 12 MW-8 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-8 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-8 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/14/2022 12 MW-8 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/9/2022 11/14/2022 12 MW-8 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-8 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-8 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/9/2022 11/14/2022 12 MW-8 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/14/2022 12 MW-8 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/14/2022 12 MW-8 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-8 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/9/2022 11/14/2022 12 MW-8 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/14/2022 12 MW-8 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/9/2022 11/14/2022 12 MW-8 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-8 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.711 2 NE 1 11/9/2022 11/14/2022 12 MW-8 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/14/2022 12 MW-8 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/14/2022 12 MW-8 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-8 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/14/2022 12 MW-9 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/9/2022 11/14/2022 12 MW-9 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-9 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/14/2022 12 MW-9 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.321 1 1 1 11/9/2022 11/14/2022 12 MW-9 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/9/2022 11/14/2022 12 MW-9 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-9 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/14/2022 12 MW-9 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/14/2022 12 MW-9 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/14/2022 12 MW-9 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/14/2022 12 MW-9 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-9 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-9 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-9 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/14/2022 12 MW-9 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/14/2022 12 MW-9 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/14/2022 12 MW-9 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/14/2022 12 MW-9 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/14/2022 12 MW-9 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/9/2022 11/14/2022 12 MW-9 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/14/2022 12 MW-9 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/14/2022 12 MW-9 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/14/2022 12 MW-9 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/9/2022 11/14/2022 12 MW-9 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/14/2022 12 MW-9 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-9 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/14/2022 12 MW-9 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/9/2022 11/14/2022 12 MW-9 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/9/2022 11/14/2022 12 MW-9 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/14/2022 12 MW-9 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/14/2022 12 MW-9 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/9/2022 11/14/2022 12 MW-9 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L J,v3 EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-9 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-9 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/14/2022 12 MW-9 75-09-2 140 Methylene Chloride 21 ug/L U EPA 8260D 2 5 1 1 11/9/2022 11/14/2022 12 MW-9 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-9 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-9 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/9/2022 11/14/2022 12 MW-9 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/14/2022 12 MW-9 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/14/2022 12 MW-9 75-69-4 203 Trichlorofluoromethane 0.37 ug/L 1 EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-9 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/9/2022 11/14/2022 12 MW-9 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/14/2022 12 MW-9 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/9/2022 11/14/2022 12 MW-9 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-9 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/9/2022 11/14/2022 12 MW-9 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/9/2022 11/14/2022 12 MW-9 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/14/2022 12 MW-9 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-9 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/14/2022 12 MW-11 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/8/2022 11/15/2022 12 MW-11 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-11 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-11 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-11 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-11 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-11 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/8/2022 11/15/2022 12 MW-11 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 131 1 11/8/2022 11/15/2022 12 MW-11 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.271 1 1 1 11/8/2022 11/15/2022 12 MW-11 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/8/2022 11/15/2022 12 MW-11 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-11 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-11 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-11 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/8/2022 11/15/2022 12 MW-11 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/8/2022 11/15/2022 12 MW-11 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/8/2022 11/15/2022 12 MW-11 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/8/2022 11/15/2022 12 MW-11 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/8/2022 11/15/2022 12 MW-11 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-11 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-11 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/8/2022 11/15/2022 12 MW-11 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-11 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/8/2022 11/15/2022 12 MW-11 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-11 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-11 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/8/2022 11/15/2022 12 MW-11 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-11 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-11 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-11 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/8/2022 11/15/2022 12 MW-11 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-11 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-11 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-11 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-11 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-11 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-11 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-11 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/8/2022 11/15/2022 12 MW-11 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-11 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/8/2022 11/15/2022 12 MW-11 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-11 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-11 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/8/2022 11/15/2022 12 MW-11 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 51 1 11/8/2022 11/15/2022 12 MW-11 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-11 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/8/2022 11/15/2022 12 MW-11 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-11 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-11 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-11 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/8/2022 11/15/2022 12 MW-12 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/8/2022 11/15/2022 12 MW-12 71-55-6 2001 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-12 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-12 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-12 75-34-3 751 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-12 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-12 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/8/2022 11/15/2022 12 MW-12 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/8/2022 11/15/2022 12 MW-12 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.271 11 1 1 11/8/2022 11/15/2022 12 MW-12 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/8/2022 11/15/2022 12 MW-12 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-12 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-12 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-12 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 11 11/8/2022 11/15/2022 12 MW-12 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/8/2022 11/15/2022 12 MW-12 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/8/2022 11/15/2022 12 MW-12 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.11 251 100 1 11/8/2022 11/15/2022 12 MW-12 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/8/2022 11/15/2022 12 MW-12 71-43-2 16 Benzene 0.36 ug/L 1 EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-12 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-12 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 11 1 11/8/2022 11/15/2022 12 MW-12 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-12 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/8/2022 11/15/2022 12 MW-12 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-12 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.331 1 1 1 11/8/2022 11/15/2022 12 MW-12 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/8/2022 11/15/2022 12 MW-12 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-12 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-12 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-12 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/8/2022 11/15/2022 12 MW-12 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-12 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-12 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.31 1 1 1 11/8/2022 11/15/2022 12 MW-12 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-12 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-12 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 11 11 1 11/8/2022 11/15/2022 12 MW-12 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-12 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/8/2022 11/15/2022 12 MW-12 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-12 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/8/2022 11/15/2022 12 MW-12 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-12 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-12 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 11 11/8/2022 11/15/2022 12 MW-12 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/8/2022 11/15/2022 12 MW-12 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-12 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/8/2022 11/15/2022 12 MW-12 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-12 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-12 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-12 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 1001 1 11/8/2022 11/15/2022 12 MW-13 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.311 1 5 1 11/8/2022 11/15/2022 12 MW-13 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-13 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-13 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-13 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-13 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-13 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/8/2022 11/15/2022 12 MW-13 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/8/2022 11/15/2022 12 MW-13 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.271 1 1 1 11/8/2022 11/15/2022 12 MW-13 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.341 1 5 1 11/8/2022 11/15/2022 12 MW-13 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-13 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-13 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-13 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/8/2022 11/15/2022 12 MW-13 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/8/2022 11/15/2022 12 MW-13 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/8/2022 11/15/2022 12 MW-13 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/8/2022 11/15/2022 12 MW-13 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.81 10 200 1 11/8/2022 11/15/2022 12 MW-13 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-13 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-13 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/8/2022 11/15/2022 12 MW-13 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-13 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/8/2022 11/15/2022 12 MW-13 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-13 56-23-5 361 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-13 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.281 1 3 1 11/8/2022 11/15/2022 12 MW-13 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-13 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-13 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-13 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/8/2022 11/15/2022 12 MW-13 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-13 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-13 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-13 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-13 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-13 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 11 11 11/8/2022 11/15/2022 12 MW-13 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 11 11 11/8/2022 11/15/2022 12 MW-13 109-99-9 458 Tetrahydrofuran 10.1 ug/L v3 EPA 8260D 3.5 10 NE 1 11 11/8/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-13 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-13 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/8/2022 11/15/2022 12 MW-13 75-69-4 203 Trichlorofluoromethane 0.45 ug/L 1 EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-13 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-13 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/8/2022 11/15/2022 12 MW-13 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 51 1 11/8/2022 11/15/2022 12 MW-13 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-13 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/8/2022 11/15/2022 12 MW-13 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-13 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-13 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-13 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/8/2022 11/15/2022 12 MW-14 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/8/2022 11/15/2022 12 MW-14 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-14 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-14 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-14 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-14 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-14 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/8/2022 11/15/2022 12 MW-14 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/8/2022 11/15/2022 12 MW-14 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/8/2022 11/15/2022 12 MW-14 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/8/2022 11/15/2022 12 MW-14 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-14 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-14 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-14 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/8/2022 11/15/2022 12 MW-14 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/8/2022 11/15/2022 12 MW-14 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/8/2022 11/15/2022 12 MW-14 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/8/2022 11/15/2022 12 MW-14 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/8/2022 11/15/2022 12 MW-14 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-14 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-14 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/8/2022 11/15/2022 12 MW-14 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-14 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/8/2022 11/15/2022 12 MW-14 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-14 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-14 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/8/2022 11/15/2022 12 MW-14 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-14 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-14 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-14 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 11 31 1 11/8/2022 11/15/2022 12 MW-14 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-14 75-71-8 74 Dichlorodifluoromethane 3.7 ug/L EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-14 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-14 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-14 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-14 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-14 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-14 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.51 10 NE 1 11/8/2022 11/15/2022 12 MW-14 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-14 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/8/2022 11/15/2022 12 MW-14 75-69-4 203 Trichlorofluoromethane 1.7 ug/L EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-14 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-14 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/8/2022 11/15/2022 12 MW-14 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/8/2022 11/15/2022 12 MW-14 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-14 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.711 2 NE 1 11/8/2022 11/15/2022 12 MW-14 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-14 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-14 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-14 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/8/2022 11/15/2022 12 SW-1 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/6/2022 11/15/2022 12 SW-1 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/6/2022 11/15/2022 12 SW-1 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/6/2022 11/15/2022 12 SW-1 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/6/2022 11/15/2022 12 SW-1 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/6/2022 11/15/2022 12 SW-1 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/6/2022 11/15/2022 12 SW-1 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/6/2022 11/15/2022 12 SW-1 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/6/2022 11/15/2022 12 SW-1 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 11 1 11/6/2022 11/15/2022 12 SW-1 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/6/2022 11/15/2022 12 SW-1 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.321 1 1 1 11/6/2022 11/15/2022 12 SW-1 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/6/2022 11/15/2022 12 SW-1 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/6/2022 11/15/2022 12 SW-1 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/6/2022 11/15/2022 12 SW-1 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/6/2022 11/15/2022 12 SW-1 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/6/2022 11/15/2022 12 SW-1 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/6/2022 11/15/2022 12 SW-1 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/6/2022 11/15/2022 12 SW-1 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/6/2022 11/15/2022 12 SW-1 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/6/2022 11/15/2022 12 SW-1 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/6/2022 11/15/2022 12 SW-1 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/6/2022 11/15/2022 12 SW-1 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/6/2022 11/15/2022 12 SW-1 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 1001 1 11/6/2022 11/15/2022 12 SW-1 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/6/2022 11/15/2022 12 SW-1 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.281 1 3 1 11/6/2022 11/15/2022 12 SW-1 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/6/2022 11/15/2022 12 SW-1 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/6/2022 11/15/2022 12 SW-1 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/6/2022 11/15/2022 12 SW-1 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/6/2022 11/15/2022 12 SW-1 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/6/2022 11/15/2022 12 SW-1 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/6/2022 11/15/2022 12 SW-1 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/6/2022 11/15/2022 12 SW-1 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/6/2022 11/15/2022 12 SW-1 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/6/2022 11/15/2022 12 SW-1 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/6/2022 11/15/2022 12 SW-1 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/6/2022 11/15/2022 12 SW-1 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/6/2022 11/15/2022 12 SW-1 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/6/2022 11/15/2022 12 SW-1 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/6/2022 11/15/2022 12 SW-1 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/6/2022 11/15/2022 12 SW-1 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.31 2 50 11 11/6/2022 11/15/2022 12 SW-1 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/6/2022 11/15/2022 12 SW-1 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/6/2022 11/15/2022 12 SW-1 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/6/2022 11/15/2022 12 SW-1 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/6/2022 11/15/2022 12 SW-1 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/6/2022 11/15/2022 12 SW-1 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/6/2022 11/15/2022 12 SW-1 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/6/2022 11/15/2022 12 SW-1 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 11 11/6/2022 11/15/2022 12 SW-3 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/7/2022 11/15/2022 12 SW-3 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-3 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/7/2022 11/15/2022 12 SW-3 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-3 75-34-3 751 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/7/2022 11/15/2022 12 SW-3 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 SW-3 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/7/2022 11/15/2022 12 SW-3 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/7/2022 11/15/2022 12 SW-3 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/7/2022 11/15/2022 12 SW-3 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/7/2022 11/15/2022 12 SW-3 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-3 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-3 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-3 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/7/2022 11/15/2022 12 SW-3 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 11 11/7/2022 11/15/2022 12 SW-3 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/7/2022 11/15/2022 12 SW-3 67-64-1 3 Acetone 13.2 ug/L 1 EPA 8260D 5.1 25 100 1 11/7/2022 11/15/2022 12 SW-3 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/7/2022 11/15/2022 12 SW-3 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/7/2022 11/15/2022 12 SW-3 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/7/2022 11/15/2022 12 SW-3 75-27-4 29 Bromodichloromethane EPA 8260D 0.31 1 1 1 11/7/2022 1SW-3 75-25-2 30 Bromoform U EPA 8260D 0.34 1 3 1 11/7/2022 SW-3 74-83-9 136 Bromomethane 40.31ug/LU U EPA 8260D 1.7 2 10 1 11/SW-3 75-15-0 35 Carbon disulfide U EPA 8260D 0.36 21 100 1 11/7/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY SW-3 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-3 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/7/2022 11/15/2022 12 SW-3 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/7/2022 11/15/2022 12 SW-3 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/7/2022 11/15/2022 12 SW-3 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/7/2022 11/15/2022 12 SW-3 124-48-1 661 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 31 1 11/7/2022 11/15/2022 12 SW-3 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.391 1 10 1 11/7/2022 11/15/2022 12 SW-3 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 SW-3 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 SW-3 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/7/2022 11/15/2022 12 SW-3 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/7/2022 11/15/2022 12 SW-3 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 SW-3 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 11 11/7/2022 11/15/2022 12 SW-3 109-99-9 458 Tetrahydrofuran 3.5 ug/L U,v2 EPA 8260D 3.5 10 NE 1 11/7/2022 11/15/2022 12 SW-3 108-88-3 196 Toluene 0.26 ug/L 1 EPA 8260D 0.241 1 1 1 11/7/2022 11/15/2022 12 SW-3 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/7/2022 11/15/2022 12 SW-3 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 SW-3 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/7/2022 11/15/2022 12 SW-3 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/7/2022 11/15/2022 12 SW-3 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/7/2022 11/15/2022 12 SW-3 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-3 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/7/2022 11/15/2022 12 SW-3 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/7/2022 11/15/2022 12 SW-3 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/7/2022 11/15/2022 12 SW-3 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-3 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/7/2022 11/15/2022 12 SW-4 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.311 11 5 1 11/7/2022 11/15/2022 12 SW-4 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-4 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/7/2022 11/15/2022 12 SW-4 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-4 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/7/2022 11/15/2022 12 SW-4 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/7/2022 11/15/2022 12 SW-4 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/7/2022 11/15/2022 12 SW-4 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/7/2022 11/15/2022 12 SW-4 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.271 11 1 1 11/7/2022 11/15/2022 12 SW-4 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/7/2022 11/15/2022 12 SW-4 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/7/2022 11/15/2022 12 SW-4 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-4 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-4 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/7/2022 11/15/2022 12 SW-4 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/7/2022 11/15/2022 12 SW-4 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/7/2022 11/15/2022 12 SW-4 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/7/2022 11/15/2022 12 SW-4 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/7/2022 11/15/2022 12 SW-4 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/7/2022 11/15/2022 12 SW-4 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/7/2022 11/15/2022 12 SW-4 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/7/2022 11/15/2022 12 SW-4 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/7/2022 11/15/2022 12 SW-4 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/7/2022 11/15/2022 12 SW-4 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.361 21 100 1 11/7/2022 11/15/2022 12 SW-4 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/7/2022 11/15/2022 12 SW-4 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/7/2022 11/15/2022 12 SW-4 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/7/2022 11/15/2022 12 SW-4 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/7/2022 11/15/2022 12 SW-4 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/7/2022 11/15/2022 12 SW-4 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/7/2022 11/15/2022 12 SW-4 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/7/2022 11/15/2022 12 SW-4 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.351 11 5 1 11/7/2022 11/15/2022 12 SW-4 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 SW-4 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/7/2022 11/15/2022 12 SW-4 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/7/2022 11/15/2022 12 SW-4 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 SW-4 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/7/2022 11/15/2022 12 SW-4 109-99-9 458 Tetrahydrofuran 5.2 ug/L J,v2 EPA 8260D 3.5 10 NE 1 11/7/2022 11/15/2022 12 SW-4 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/7/2022 11/15/2022 12 SW-4 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.381 11 1 1 11/7/2022 11/15/2022 12 SW-4 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/7/2022 11/15/2022 12 SW-4 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/7/2022 11/15/2022 12 SW-4 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/7/2022 11/15/2022 12 SW-4 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/7/2022 11/15/2022 12 SW-4 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-4 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/7/2022 11/15/2022 12 SW-4 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/7/2022 11/15/2022 12 SW-4 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/7/2022 11/15/2022 12 SW-4 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/7/2022 11/15/2022 12 SW-4 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/7/2022 11/15/2022 12 MW-7 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/9/2022 11/14/2022 12 MW-7 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-7 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/9/2022 11/14/2022 12 MW-7 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-7 75-34-3 751 1,1-Dichloroethane 0.87 ug/L 1 EPA 8260D 0.371 11 5 1 11/9/2022 11/14/2022 12 MW-7 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-7 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/9/2022 11/14/2022 12 MW-7 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/9/2022 11/14/2022 12 MW-7 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/9/2022 11/14/2022 12 MW-7 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/9/2022 11/14/2022 12 MW-7 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/9/2022 11/14/2022 12 MW-7 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-7 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.331 11 1 1 11/9/2022 11/14/2022 12 MW-7 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/9/2022 11/14/2022 12 MW-7 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/9/2022 11/14/2022 12 MW-7 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/9/2022 11/14/2022 12 MW-7 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/9/2022 11/14/2022 12 MW-7 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/9/2022 11/14/2022 12 MW-7 71-43-2 16 Benzene 0.95 ug/L 1 EPA 8260D 0.34 1 1 1 11/9/2022 11/14/2022 12 MW-7 74-97-5 281 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/9/2022 11/14/2022 12 MW-7 75-27-4 291 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/9/2022 11/14/2022 12 MW-7 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/9/2022 11/14/2022 12 MW-7 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/9/2022 11/14/2022 12 MW-7 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/9/2022 11/14/2022 12 MW-7 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/9/2022 11/14/2022 12 MW-7 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/9/2022 11/14/2022 12 MW-7 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/9/2022 11/14/2022 12 MW-7 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.431 11 5 1 11/9/2022 11/14/2022 12 MW-7 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/9/2022 11/14/2022 12 MW-7 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/9/2022 11/14/2022 12 MW-7 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/9/2022 11/14/2022 12 MW-7 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/9/2022 11/14/2022 12 MW-7 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-7 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/9/2022 11/14/2022 12 MW-7 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/9/2022 11/14/2022 12 MW-7 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.291 11 1 11 11/9/2022 11/14/2022 12 MW-7 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/9/2022 11/14/2022 12 MW-7 109-99-9 458 Tetrahydrofuran 48 ug/L EPA 8260D 3.5 10 NE 1 11/9/2022 11/14/2022 12 MW-7 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/9/2022 11/14/2022 12 MW-7 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/9/2022 11/14/2022 12 MW-7 75-69-4 203 Trichlorofluoromethane 0.96 ug/L 1 EPA 8260D 0.3 1 1 1 11/9/2022 11/14/2022 12 MW-7 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/9/2022 11/14/2022 12 MW-7 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/9/2022 11/14/2022 12 MW-7 156-59-2 78 cis-1,2-Dichloroethene 1 ug/L 1 EPA 8260D 0.381 11 5 1 11/9/2022 11/14/2022 12 MW-7 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-7 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/9/2022 11/14/2022 12 MW-7 95-47-6 408 o-Xylene 0.44 ug/L 1 EPA 8260D 0.34 1 NE 1 11/9/2022 11/14/2022 12 MW-7 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/9/2022 11/14/2022 12 MW-7 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/9/2022 11/14/2022 12 MW-7 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/9/2022 11/14/2022 12 MW-10 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/8/2022 11/15/2022 12 MW-10 71-55-6 2001 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.331 11 1 1 11/8/2022 11/15/2022 12 MW-10 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/8/2022 11/15/2022 12 MW-10 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-10 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/8/2022 11/15/2022 12 MW-10 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/8/2022 11/15/2022 12 MW-10 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/8/2022 11/15/2022 12 MW-10 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/8/2022 11/15/2022 12 MW-10 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/8/2022 11/15/2022 12 MW-10 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.341 11 5 11 11/8/2022 11/15/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-10 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/8/2022 11/15/2022 12 MW-10 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-10 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-10 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/8/2022 11/15/2022 12 MW-10 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/8/2022 11/15/2022 12 MW-10 108-10-1 147 4-Methyl-2-pentanone(MIBK) 2.7 ug/L U EPA 8260D 2.7 5 1001 1 11/8/2022 11/15/2022 12 MW-10 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.11 25 100 1 11/8/2022 11/15/2022 12 MW-10 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/8/2022 11/15/2022 12 MW-10 71-43-2 16 Benzene 0.63 ug/L 1 EPA 8260D 0.34 1 1 1 11/8/2022 11/15/2022 12 MW-10 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/8/2022 11/15/2022 12 MW-10 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/8/2022 11/15/2022 12 MW-10 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/8/2022 11/15/2022 12 MW-10 74-83-9 136 Bromomethane 1.7 ug/L U EPA 8260D 1.7 2 10 1 11/8/2022 11/15/2022 12 MW-10 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/8/2022 11/15/2022 12 MW-10 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/8/2022 11/15/2022 12 MW-10 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/8/2022 11/15/2022 12 MW-10 75-00-3 41 Chloroethane 0.65 ug/L U,v2 EPA 8260D 0.65 1 10 1 11/8/2022 11/15/2022 12 MW-10 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/8/2022 11/15/2022 12 MW-10 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/8/2022 11/15/2022 12 MW-10 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 31 1 11/8/2022 11/15/2022 12 MW-10 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/8/2022 11/15/2022 12 MW-10 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U EPA 8260D 0.351 1 5 1 11/8/2022 11/15/2022 12 MW-10 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-10 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/8/2022 11/15/2022 12 MW-10 75-09-2 140 Methylene Chloride 2 ug/L U,v2 EPA 8260D 2 5 1 1 11/8/2022 11/15/2022 12 MW-10 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-10 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/8/2022 11/15/2022 12 MW-10 109-99-9 458 Tetrahydrofuran 74.3 ug/L v3 EPA 8260D 3.5 10 NE 1 11/8/2022 11/15/2022 12 MW-10 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/8/2022 11/15/2022 12 MW-10 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.381 1 1 1 11/8/2022 11/15/2022 12 MW-10 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/8/2022 11/15/2022 12 MW-10 108-05-4 210 Vinyl acetate 1.3 ug/L U,v2 EPA 8260D 1.3 2 50 1 11/8/2022 11/15/2022 12 MW-10 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/8/2022 11/15/2022 12 MW-10 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/8/2022 11/15/2022 12 MW-10 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-10 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/8/2022 11/15/2022 12 MW-10 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/8/2022 11/15/2022 12 MW-10 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/8/2022 11/15/2022 12 MW-10 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/8/2022 11/15/2022 12 MW-10 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/8/2022 11/15/2022 12 TB-1 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/10/2022 11/14/2022 12 TB-1 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-1 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/10/2022 11/14/2022 12 TB-1 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-1 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.371 1 5 1 11/10/2022 11/14/2022 12 TB-1 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 TB-1 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/10/2022 11/14/2022 12 TB-1 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/10/2022 11/14/2022 12 TB-1 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/10/2022 11/14/2022 12 TB-1 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/10/2022 11/14/2022 12 TB-1 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-1 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-1 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-1 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/10/2022 11/14/2022 12 TB-1 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/10/2022 11/14/2022 12 TB-1 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/10/2022 11/14/2022 12 TB-1 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 25 100 1 11/10/2022 11/14/2022 12 TB-1 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/10/2022 11/14/2022 12 TB-1 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/10/2022 11/14/2022 12 TB-1 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/10/2022 11/14/2022 12 TB-1 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/14/2022 12 TB-1 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/10/2022 11/14/2022 12 TB-1 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/10/2022 11/14/2022 12 TB-1 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/10/2022 11/14/2022 12 TB-1 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-1 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/10/2022 11/14/2022 12 TB-1 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/10/2022 11/14/2022 12 TB-1 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/10/2022 11/14/2022 12 TB-1 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/10/2022 11/14/2022 12 TB-1 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/10/2022 11/14/2022 12 TB-1 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/10/2022 11/14/2022 12 TB-1 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 TB-1 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 TB-1 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/10/2022 11/14/2022 12 TB-1 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/10/2022 11/14/2022 12 TB-1 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 TB-1 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.291 11 1 1 11/10/2022 11/14/2022 12 TB-1 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/10/2022 11/14/2022 12 TB-1 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/10/2022 11/14/2022 12 TB-1 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/10/2022 11/14/2022 12 TB-1 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 TB-1 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/10/2022 11/14/2022 12 TB-1 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/10/2022 11/14/2022 12 TB-1 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/10/2022 11/14/2022 12 TB-1 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-1 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/10/2022 11/14/2022 12 TB-1 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/10/2022 11/14/2022 12 TB-1 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/10/2022 11/14/2022 12 TB-1 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-1 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/10/2022 11/14/2022 12 TB-2 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/10/2022 11/14/2022 12 TB-2 71-55-6 200 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.331 11 1 1 11/10/2022 11/14/2022 12 TB-2 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.22 1 3 1 11/10/2022 11/14/2022 12 TB-2 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-2 75-34-3 75 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/10/2022 11/14/2022 12 TB-2 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 TB-2 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/10/2022 11/14/2022 12 TB-2 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/10/2022 11/14/2022 12 TB-2 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/10/2022 11/14/2022 12 TB-2 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/10/2022 11/14/2022 12 TB-2 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-2 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-2 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-2 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/10/2022 11/14/2022 12 TB-2 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/10/2022 11/14/2022 12 TB-2 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/10/2022 11/14/2022 12 TB-2 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.11 251 100 1 11/10/2022 11/14/2022 12 TB-2 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/10/2022 11/14/2022 12 TB-2 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/10/2022 11/14/2022 12 TB-2 74-97-5 28 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/10/2022 11/14/2022 12 TB-2 75-27-4 29 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/14/2022 12 TB-2 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/10/2022 11/14/2022 12 TB-2 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/10/2022 11/14/2022 12 TB-2 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.36 2 100 1 11/10/2022 11/14/2022 12 TB-2 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.331 1 1 1 11/10/2022 11/14/2022 12 TB-2 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/10/2022 11/14/2022 12 TB-2 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/10/2022 11/14/2022 12 TB-2 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/10/2022 11/14/2022 12 TB-2 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/10/2022 11/14/2022 12 TB-2 124-48-1 66 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/10/2022 11/14/2022 12 TB-2 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/10/2022 11/14/2022 12 TB-2 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 TB-2 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/14/2022 12 TB-2 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/10/2022 11/14/2022 12 TB-2 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/10/2022 11/14/2022 12 TB-2 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 TB-2 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 TB-2 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/10/2022 11/14/2022 12 TB-2 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 1 1 11/10/2022 11/14/2022 12 TB-2 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 1 1 1 11/10/2022 11/14/2022 12 TB-2 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 TB-2 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/10/2022 11/14/2022 12 TB-2 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/10/2022 11/14/2022 12 TB-2 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/10/2022 11/14/2022 12 TB-2 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-2 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/10/2022 11/14/2022 12 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY TB-2 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 11/10/2022 11/14/2022 12 TB-2 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 S 1 11/10/2022 11/14/2022 12 TB-2 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-2 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/10/2022 11/14/2022 12 TB-3 630-20-6 190 1,1,1,2-Tetrachloroethane 0.31 ug/L U EPA 8260D 0.31 1 5 1 11/10/2022 11/14/2022 12 TB-3 71-55-6 2001 1,1,1-Trichloroethane 0.33 ug/L U EPA 8260D 0.33 1 11 1 11/10/2022 11/14/2022 12 TB-3 79-34-5 191 1,1,2,2-Tetrachloroethane 0.22 ug/L U EPA 8260D 0.221 1 3 1 11/10/2022 11/14/2022 12 TB-3 79-00-5 202 1,1,2-Trichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-3 75-34-3 751 1,1-Dichloroethane 0.37 ug/L U EPA 8260D 0.37 1 5 1 11/10/2022 11/14/2022 12 TB-3 75-35-4 77 1,1-Dichloroethene 0.35 ug/L U EPA 8260D 0.35 1 5 1 11/10/2022 11/14/2022 12 TB-3 96-18-4 206 1,2,3-Trichloropropane 0.26 ug/L U EPA 8260D 0.26 1 1 1 11/10/2022 11/14/2022 12 TB-3 96-12-8 67 1,2-Dibromo-3-chloropropane 0.34 ug/L U EPA 8260D 0.34 2 13 1 11/10/2022 11/14/2022 12 TB-3 106-93-4 68 1,2-Dibromoethane(EDB) 0.27 ug/L U EPA 8260D 0.27 1 1 1 11/10/2022 11/14/2022 12 TB-3 95-50-1 69 1,2-Dichlorobenzene 0.34 ug/L U EPA 8260D 0.34 1 5 1 11/10/2022 11/14/2022 12 TB-3 107-06-2 76 1,2-Dichloroethane 0.32 ug/L U EPA 8260D 0.32 1 1 1 11/10/2022 11/14/2022 12 TB-3 78-87-5 82 1,2-Dichloropropane 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-3 106-46-7 71 1,4-Dichlorobenzene 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-3 78-93-3 141 2-Butanone(MEK) 4 ug/L U EPA 8260D 4 5 100 1 11/10/2022 11/14/2022 12 TB-3 591-78-6 124 2-Hexanone 0.48 ug/L U EPA 8260D 0.48 5 50 1 11/10/2022 11/14/2022 12 TB-3 108-10-1 147 4-Methyl-2-penta none (MIBK) 2.7 ug/L U EPA 8260D 2.7 5 100 1 11/10/2022 11/14/2022 12 TB-3 67-64-1 3 Acetone 5.1 ug/L U EPA 8260D 5.1 251 1001 1 11/10/2022 11/14/2022 12 TB-3 107-13-1 8 Acrylonitrile 1.8 ug/L U EPA 8260D 1.8 10 200 1 11/10/2022 11/14/2022 12 TB-3 71-43-2 16 Benzene 0.34 ug/L U EPA 8260D 0.34 1 1 1 11/10/2022 11/14/2022 12 TB-3 74-97-5 281 Bromochloromethane 0.47 ug/L U EPA 8260D 0.47 1 3 1 11/10/2022 11/14/2022 12 TB-3 75-27-4 291 Bromodichloromethane 0.31 ug/L U EPA 8260D 0.31 1 1 1 11/10/2022 11/14/2022 12 TB-3 75-25-2 30 Bromoform 0.34 ug/L U EPA 8260D 0.34 1 3 1 11/10/2022 11/14/2022 12 TB-3 74-83-9 136 Bromomethane 1.7 ug/L U,v2 EPA 8260D 1.7 2 10 1 11/10/2022 11/14/2022 12 TB-3 75-15-0 35 Carbon disulfide 0.36 ug/L U EPA 8260D 0.361 2 100 1 11/10/2022 11/14/2022 12 TB-3 56-23-5 36 Carbon tetrachloride 0.33 ug/L U EPA 8260D 0.33 1 1 1 11/10/2022 11/14/2022 12 TB-3 108-90-7 39 Chlorobenzene 0.28 ug/L U EPA 8260D 0.28 1 3 1 11/10/2022 11/14/2022 12 TB-3 75-00-3 41 Chloroethane 0.65 ug/L U EPA 8260D 0.65 1 10 1 11/10/2022 11/14/2022 12 TB-3 67-66-3 44 Chloroform 0.43 ug/L U EPA 8260D 0.43 1 5 1 11/10/2022 11/14/2022 12 TB-3 74-87-3 137 Chloromethane 0.54 ug/L U EPA 8260D 0.54 1 1 1 11/10/2022 11/14/2022 12 TB-3 124-48-1 661 Dibromochloromethane 0.36 ug/L U EPA 8260D 0.36 1 3 1 11/10/2022 11/14/2022 12 TB-3 74-95-3 139 Dibromomethane 0.39 ug/L U EPA 8260D 0.39 1 10 1 11/10/2022 11/14/2022 12 TB-3 75-71-8 74 Dichlorodifluoromethane 0.35 ug/L U,v2 EPA 8260D 0.351 11 5 1 11/10/2022 11/14/2022 12 TB-3 100-41-4 110 Ethylbenzene 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 TB-3 74-88-4 142 lodomethane 9.7 ug/L U EPA 8260D 9.7 20 10 1 11/10/2022 11/14/2022 12 TB-3 75-09-2 140 Methylene Chloride 2 ug/L U EPA 8260D 2 5 1 1 11/10/2022 11/14/2022 12 TB-3 100-42-5 186 Styrene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 TB-3 127-18-4 192 Tetrachloroethene 0.29 ug/L U EPA 8260D 0.29 1 1 1 11/10/2022 11/14/2022 12 TB-3 109-99-9 458 Tetrahydrofuran 3.5 ug/L U EPA 8260D 3.5 10 NE 1 11/10/2022 11/14/2022 12 TB-3 108-88-3 196 Toluene 0.24 ug/L U EPA 8260D 0.24 1 11 1 11/10/2022 11/14/2022 12 TB-3 79-01-6 201 Trichloroethene 0.38 ug/L U EPA 8260D 0.38 11 1 1 11/10/2022 11/14/2022 12 TB-3 75-69-4 203 Trichlorofluoromethane 0.3 ug/L U EPA 8260D 0.3 1 1 1 11/10/2022 11/14/2022 12 TB-3 108-05-4 210 Vinyl acetate 1.3 ug/L U EPA 8260D 1.3 2 50 1 11/10/2022 11/14/2022 12 TB-3 75-01-4 211 Vinyl chloride 0.39 ug/L U EPA 8260D 0.39 1 1 1 11/10/2022 11/14/2022 12 TB-3 156-59-2 78 cis-1,2-Dichloroethene 0.38 ug/L U EPA 8260D 0.38 1 5 1 11/10/2022 11/14/2022 12 TB-3 10061-01-5 86 cis-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-3 179601-23-1 359 m&p-Xylene 0.71 ug/L U EPA 8260D 0.71 2 NE 1 11/10/2022 11/14/2022 12 TB-3 95-47-6 408 o-Xylene 0.34 ug/L U EPA 8260D 0.34 1 NE 1 1 11/10/2022 11/14/2022 12 TB-3 156-60-5 79 trans-1,2-Dichloroethene 0.4 ug/L U EPA 8260D 0.4 1 5 1 11/10/2022 11/14/2022 12 TB-3 10061-02-6 87 trans-1,3-Dichloropropene 0.36 ug/L U EPA 8260D 0.36 1 1 1 11/10/2022 11/14/2022 12 TB-3 110-57-6 73 trans-1,4-Dichloro-2-butene 0.56 ug/L U EPA 8260D 0.56 1 100 1 11/10/2022 11/14/2022 12 MW-1R 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/10/2022 11/10/2022 12 MW-2R 123-91-1 422 1,4-Dioxane(p-Dioxane) 3.7 ug/L EPA 8260D Mod. 0.86 2 10 1 11/8/2022 11/10/2022 12 MW-4R 123-91-1 422 1,4-Dioxane(p-Dioxane) 4.9 ug/L EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/10/2022 12 MW-15 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/7/2022 11/10/2022 12 EQBL 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.861 2 10 1 11/7/2022 11/10/2022 12 FIB 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/10/2022 12 DUP-1 123-91-1 422 1,4-Dioxane(p-Dioxane) 4.3 ug/L EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/11/2022 12 MW-3R 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/10/2022 11/10/2022 12 SW-2 123-91-1 422 1,4-Dioxane(p-Dioxane) 4.4 ug/L EPA 8260D Mod. 0.86 2 10 1 11/7/2022 11/10/2022 12 MW-5R 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/10/2022 12 MW-8 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/10/2022 12 MW-9 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/10/2022 12 MW-11 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.861 2 10 1 11/8/2022 11/11/2022 12 MW-12 123-91-1 422 1,4-Dioxane(p-Dioxane) 6.1 ug/L EPA 8260D Mod. 0.86 2 10 1 11/8/2022 11/11/2022 12 MW-13 123-91-1 422 1,4-Dioxane(p-Dioxane) 7.7 ug/L EPA 8260D Mod. 0.86 2 10 1 11/8/2022 11/11/2022 12 MW-14 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/8/2022 11/11/2022 12 SW-1 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/6/2022 11/11/2022 12 SW-3 123-91-1 422 1,4-Dioxane(p-Dioxane) 0.86 ug/L U EPA 8260D Mod. 0.86 2 10 1 11/7/2022 11/11/2022 12 SW-4 123-91-1 422 1,4-Dioxane(p-Dioxane) 5.6 ug/L EPA 8260D Mod. 0.86 2 10 1 11/7/2022 11/11/2022 12 MW-7 123-91-1 422 1,4-Dioxane(p-Dioxane) 7.8 ug/L EPA 8260D Mod. 0.86 2 10 1 11/9/2022 11/11/2022 12 MW-10 123-91-1 422 1,4-Dioxane(p-Dioxane) 5.7 ug/L EPA 8260D Mod. 0.861 2 10 1 11/8/2022 11/11/2022 12 MW-1R SW337 337 Alkalinity, Total as CaCO3 90400 ug/L SM 2320B-2011 5000 5000 NE 1 11/10/2022 11/11/2022 40 MW-2R SW337 337 Alkalinity, Total as CaCO3 879000 ug/L SM 2320B-2011 5000 5000 NE 1 11/8/2022 11/12/2022 40 MW-4R SW337 337 Alkalinity, Total as CaCO3 552000 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/12/2022 40 MW-15 SW337 337 Alkalinity, Total as CaCO3 83100 ug/L SM 2320B-2011 5000 5000 NE 1 11/7/2022 11/11/2022 40 EQBL SW337 337 Alkalinity, Total as CaCO3 5000 ug/L U SM 2320E-2011 5000 5000 NE 1 11/7/2022 11/11/2022 40 FIB SW337 337 Alkalinity, Total as CaCO3 5000 ug/L U SM 2320E-2011 5000 5000 NE 1 11/9/2022 11/11/2022 40 DUP-1 SW337 337 Alkalinity, Total as CaCO3 544000 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/12/2022 40 MW-3R SW337 337 Alkalinity, Total as CaCO3 130000 ug/L SM 2320B-2011 5000 5000 NE 1 11/10/2022 11/11/2022 40 SW-2 SW337 337 Alkalinity, Total as CaCO3 140000 ug/L SM 2320B-2011 5000 5000 NE 1 11/7/2022 11/11/2022 40 MW-5R SW337 337 Alkalinity, Total as CaCO3 33900 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/11/2022 40 MW-8 SW337 337 Alkalinity, Total as CaCO3 29300 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/11/2022 40 MW-9 SW337 337 Alkalinity, Total as CaCO3 29200 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/11/2022 40 MW-11 SW337 337 Alkalinity, Total as CaCO3 106000 ug/L SM 2320B-2011 5000 5000 NE 1 11/8/2022 11/11/2022 40 MW-12 SW337 337 Alkalinity, Total as CaCO3 294000 ug/L SM 2320B-2011 5000 5000 NE 1 11/8/2022 11/12/2022 40 MW-13 SW337 337 Alkalinity, Total as CaCO3 84400 ug/L SM 2320B-2011 50001 5000 NE 11 11/8/2022 11/11/2022 40 MW-14 SW337 337 Alkalinity, Total as CaCO3 63100 ug/L SM 2320B-2011 5000 5000 NE 1 11/8/2022 11/11/2022 40 SW-1 SW337 337 Alkalinity, Total as CaCO3 41700 ug/L SM 2320B-2011 5000 5000 NE 1 11/6/2022 11/11/2022 40 SW-3 SW337 337 Alkalinity, Total as CaCO3 234000 ug/L SM 2320B-2011 5000 5000 NE 1 11/7/2022 11/12/2022 40 SW-4 SW337 337 Alkalinity, Total as CaCO3 351000 ug/L SM 2320B-2011 5000 5000 NE 1 11/7/2022 11/12/2022 40 MW-7 SW337 337 Alkalinity, Total as CaCO3 265000 ug/L SM 2320B-2011 5000 5000 NE 1 11/9/2022 11/12/2022 40 MW-10 SW337 337 Alkalinity, Total as CaCO3 919000 ug/L SM 2320B-2011 5000 5000 NE 1 11/8/2022 11/12/2022 40 MW-1R SW311 311 Total Dissolved Solids, Dissolved 163000 ug/L SM 2540C-2015 25000 25000 NE 1 11/10/2022 11/15/2022 40 MW-2R SW311 311 Total Dissolved Solids, Dissolved 972000 ug/L SM 2540C-2015 50000 50000 NE 11 11/8/2022 11/13/2022 40 MW-4R SW311 311 Total Dissolved Solids, Dissolved 832000 ug/L SM 2540C-2015 50000 50000 NE 1 11/9/2022 11/14/2022 40 MW-15 SW311 311 Total Dissolved Solids, Dissolved 255000 ug/L SM 2540C-2015 25000 25000 NE 1 11/7/2022 11/11/2022 40 EQBL SW311 311 Total Dissolved Solids, Dissolved 25000 ug/L U SM 2540C-2015 25000 25000 NE 1 11/7/2022 11/11/2022 40 FIB SW311 311 Total Dissolved Solids, Dissolved 25000 ug/L U SM 2540C-2015 25000 25000 NE 1 11/9/2022 11/14/2022 40 DUP-1 SW311 311 Total Dissolved Solids, Dissolved 812000 ug/L SM 2540C-2015 50000 50000 NE 1 11/9/2022 11/14/2022 40 MW-3R SW311 311 Total Dissolved Solids, Dissolved 121000 ug/L SM 2540C-2015 25000 25000 NE 1 11/10/2022 11/15/2022 40 SW-2 SW311 311 Total Dissolved Solids, Dissolved 245000 ug/L SM 2540C-2015 25000 25000 NE 1 11/7/2022 11/11/2022 40 MW-5R SW311 311 Total Dissolved Solids, Dissolved 159000 ug/L SM 2540C-2015 25000 25000 NE 1 1 11/9/2022 11/15/2022 40 MW-8 SW311 311 Total Dissolved Solids, Dissolved 86000 ug/L SM 2540C-2015 25000 25000 NE 1 11/9/2022 11/15/2022 40 MW-9 SW311 311 Total Dissolved Solids, Dissolved 139000 ug/L SM 2540C-2015 25000 25000 NE 1 11/9/2022 11/15/2022 40 MW-11 SW311 311 Total Dissolved Solids, Dissolved 173000 ug/L SM 2540C-2015 25000 25000 NE 1 11/8/2022 11/13/2022 40 MW-12 SW311 311 Total Dissolved Solids, Dissolved 496000 ug/L SM 2540C-2015 25000 25000 NE 1 11/8/2022 11/13/2022 40 MW-13 SW311 311 Total Dissolved Solids, Dissolved 272000 ug/L SM 2540C-2015 25000 25000 NE 1 11/8/2022 11/13/2022 40 MW-14 SW311 311 Total Dissolved Solids, Dissolved 158000 ug/L SM 2540C-2015 25000 25000 NE 1 11/8/2022 11/13/2022 40 SW-1 SW311 311 Total Dissolved Solids, Dissolved 88000 ug/L SM 2540C-2015 25000 25000 NE 1 11/6/2022 11/11/2022 40 SW-3 SW311 311 Total Dissolved Solids, Dissolved 312000 ug/L SM 2540C-2015 25000 25000 NE 1 11/7/2022 11/11/2022 40 SW-4 SW311 311 Total Dissolved Solids, Dissolved 511000 ug/L SM 2540C-2015 25000 25000 NE 1 11/7/2022 11/11/2022 40 MW-7 SW311 311 Total Dissolved Solids, Dissolved 510000 ug/L SM 2540C-2015 25000 25000 NE 1 11/9/2022 11/15/2022 40 MW-10 SW311 311 Total Dissolved Solids, Dissolved 1220000 ug/L SM 2540C-2015 50000 50000 NE 1 11/8/2022 11/13/2022 40 MW-1R 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/10/2022 11/15/2022 40 MW-2R 18496-25-8 187 Sulfide 27.6 ug/L 1 SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 MW-4R 18496-25-8 187 Sulfide 22 ug/L U,M1 SM 4500-S2D-2011 22 1001 10001 1 11/9/2022 11/15/2022 40 MW-15 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/7/2022 11/11/2022 40 EQBL 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/7/2022 11/11/2022 40 FIB 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/9/2022 11/15/2022 40 DUP-1 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/9/2022 11/15/2022 40 MW-3R 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/10/2022 11/15/2022 40 SW-2 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/7/2022 11/11/2022 40 MW-5R 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 11 11/9/2022 11/15/2022 40 MW-8 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 221 100 1000 11 11/9/2022 11/15/2022 40 MW-9 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/9/2022 11/15/2022 40 MW-11 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 MW-12 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 MW-13 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 MW-14 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 SW-1 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/6/2022 11/11/2022 40 SW-3 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/7/2022 11/11/2022 40 SW-4 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 221 inol 1000 11 11/7/2022 11/11/2022 40 FACILITY PERMIT WELL ID CAS Number SWS ID PARAMETER RESULT UNITS QUALIFIER METHOD MOIL MRL SWSL DILUTION FACTOR COLLECT DATE EXTRACTION DATE ANALYSIS DATE NC LABORATORY MW-7 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/9/2022 11/15/2022 40 MW-10 18496-25-8 187 Sulfide 22 ug/L U SM 4500-S2D-2011 22 100 1000 1 11/8/2022 11/11/2022 40 MW-1R 14808-79-8 315 Sulfate 790 ug/L 1 EPA 300.0 Rev 2.11993 500 1000 250000 1 11/10/2022 11/12/2022 40 MW-2R 14808-79-8 315 Sulfate 66300 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/8/2022 11/12/2022 40 MW-4R 14808-79-8 315 Sulfate 133000 ug/L EPA 300.0 Rev 2.11993 1500 3000 250000 3 11/9/2022 11/13/2022 40 MW-15 14808-79-8 315 Sulfate 22800 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/7/2022 11/12/2022 40 EQBL 14808-79-8 315 Sulfate 500 ug/L U EPA 300.0 Rev 2.11993 500 1000 250000 1 11/7/2022 11/12/2022 40 FIB 14808-79-8 315 Sulfate 500 ug/L U EPA 300.0 Rev 2.11993 500 1000 250000 1 11/9/2022 11/12/2022 40 DUP-1 14808-79-8 315 Sulfate 139000 ug/L EPA 300.0 Rev 2.11993 1500 3000 250000 3 11/9/2022 11/13/2022 40 MW-3R 14808-79-8 315 Sulfate 1760 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/10/2022 11/13/2022 40 SW-2 14808-79-8 315 Sulfate 11700 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/7/2022 11/13/2022 40 MW-5R 14808-79-8 315 Sulfate 8420 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/9/2022 11/13/2022 40 MW-8 14808-79-8 315 Sulfate 8290 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 11 11/9/2022 11/13/2022 40 MW-9 14808-79-8 315 Sulfate 807 ug/L 1 EPA 300.0 Rev 2.11993 500 1000 250000 1 11/9/2022 11/13/2022 40 MW-11 14808-79-8 315 Sulfate 9830 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/8/2022 11/13/2022 40 MW-12 14808-79-8 315 Sulfate 94600 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/8/2022 11/13/2022 40 MW-13 14808-79-8 315 Sulfate 27300 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/8/2022 11/13/2022 40 MW-14 14808-79-8 315 Sulfate 500 ug/L U EPA 300.0 Rev 2.11993 500 1000 250000 1 11/8/2022 11/13/2022 40 SW-1 14808-79-8 315 Sulfate 2840 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/6/2022 11/13/2022 40 SW-3 14808-79-8 315 Sulfate 34000 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/7/2022 11/13/2022 40 SW-4 14808-79-8 315 Sulfate 46500 ug/L EPA 300.0 Rev 2.11993 500 1000 250000 1 11/7/2022 11/13/2022 40 MW-7 14808-79-8 315 Sulfate 98400 ug/L EPA 300.0 Rev 2.11993 10001 2000 250000 2 11/9/2022 11/14/2022 40 MW-10 14808-79-8 315 Sulfate 146000 ug/L EPA 300.0 Rev 2.11993 1500 3000 250000 3 11/8/2022 11/14/2022 40 MW-1R 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/10/2022 11/22/2022 11/22/2022 40 MW-2R 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/21/2022 11/21/2022 40 MW-4R 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-15 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/7/2022 11/21/2022 11/21/2022 40 EQBL 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/7/2022 11/21/2022 11/21/2022 40 FIB 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 DUP-1 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 61 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-3R 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/10/2022 11/22/2022 11/22/2022 40 SW-2 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/7/2022 11/21/2022 11/21/2022 40 MW-5R 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-8 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-9 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-11 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/21/2022 11/21/2022 40 MW-12 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/21/2022 11/21/2022 40 MW-13 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/22/2022 11/22/2022 40 MW-14 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/22/2022 11/22/2022 40 SW-1 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/6/2022 11/17/2022 11/17/2022 40 SW-3 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/7/2022 11/21/2022 11/21/2022 40 SW-4 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/7/2022 11/21/2022 11/21/2022 40 MW-7 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/9/2022 11/22/2022 11/22/2022 40 MW-10 57-12-5 58 Cyanide 6 ug/L U SM 4500-CN-E-2016 6 8 10 1 11/8/2022 11/22/2022 11/22/2022 40 MW-1R 16887-00-6 455 Chloride 11700 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/10/2022 11/15/2022 40 MW-2R 16887-00-6 455 Chloride 39800 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/8/2022 11/15/2022 40 MW-4R 16887-00-6 455 Chloride 46200 ug/L SM 4500-CI-E-2011 1000 2000 NE 2 11/9/2022 11/15/2022 40 MW-15 16887-00-6 455 Chloride 54700 ug/L SM 4500-CI-E-2011 2000 4000 NE 4 11/7/2022 11/15/2022 40 EQBL 16887-00-6 455 Chloride 500 ug/L U SM 4500-CI-E-2011 500 1000 NE 1 11/7/2022 11/15/2022 40 FIB 16887-00-6 455 Chloride 500 ug/L U SM 4500-CI-E-2011 500 1000 NE 1 11/9/2022 11/15/2022 40 DUP-1 16887-00-6 455 Chloride 45300 ug/L SM 4500-CI-E-2011 1000 2000 NE 2 11/9/2022 11/15/2022 40 MW-3R 16887-00-6 455 Chloride 2860 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/10/2022 11/15/2022 40 SW-2 16887-00-6 455 Chloride 27200 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/7/2022 11/15/2022 40 MW-5R 16887-00-6 455 Chloride 14700 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/9/2022 11/15/2022 40 MW-8 16887-00-6 455 Chloride 3710 ug/L SM 4500-CI-E-2011 5001 1000 NE 1 11/9/2022 11/15/2022 40 MW-9 16887-00-6 455 Chloride 3690 ug/L SM 4500-CI-E-2011 500 1000 NE 11 11/9/2022 11/15/2022 40 MW-11 16887-00-6 455 Chloride 8540 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/8/2022 11/15/2022 40 MW-12 16887-00-6 455 Chloride 28200 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/8/2022 11/15/2022 40 MW-13 16887-00-6 455 Chloride 47300 ug/L SM 4500-CI-E-2011 1000 2000 NE 2 11/8/2022 11/15/2022 40 MW-14 16887-00-6 455 Chloride 3910 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/8/2022 11/15/2022 40 SW-1 16887-00-6 455 Chloride 19500 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/6/2022 11/15/2022 40 SW-3 16887-00-6 455 Chloride 20600 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/7/2022 11/15/2022 40 SW-4 16887-00-6 455 Chloride 43500 ug/L SM 4500-CI-E-2011 1000 2000 NE 2 11/7/2022 11/15/2022 40 MW-7 16887-00-6 455 Chloride 32500 ug/L SM 4500-CI-E-2011 500 1000 NE 1 11/9/2022 11/15/2022 40 MW-10 16887-00-6 455 Chloride 51400 ug/L I ISM 4500-CI-E-2011 10001 2000 NE 1 2 11/8/2022 11/15/2022 40 This page intentionally left blank. 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