22031_K-Town Furniture_Redevelopment Summary Rpt 20230203

https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Redevelopment Report/22031_K-Town Furniture_Redevelopment Summary Rpt.doc
Via Email
February 3, 2023
NCDEQ – Division of Waste Management Brownfields Program Mail Service Center 1646 Raleigh, North Carolina 27699-1646
Attn: Mr. Bill Schmithorst
Re: Annual Redevelopment Summary Report K-Town Furniture
Stadium Lofts and Block 4 North
Kannapolis, North CarolinaBrownfields Project No. 22031-18-013H&H Job No. LSG-001
Dear Bill:
1.0 Introduction
On behalf of Right Field Development, LLC and KB4, LLC, Hart & Hickman, PC (H&H) has
prepared this brief summary to document annual environment-related redevelopment activities at
the Block 4 North and Stadium Lofts (Block 4 South) developments at the K-Town Furniture
Brownfields property (Brownfields Project No. 22031-18-013) located at 110 and 120 West
Avenue, respectively in Kannapolis, Cabarrus County, North Carolina (Site). The K-Town
Furniture Brownfields property totals approximately 9.2 acres of land. This report only reflects
redevelopment activities for Parcel Identification Numbers (PINs) 5614601290000 and
56146001440000 in which the Block 4 North and Stadium Loft developments are located. A Site
location map is provided as Figure 1.
A Brownfields Agreement between the City of Kannapolis and the North Carolina Department
of Environmental Quality (DEQ) was recorded for the Site on January 17, 2020. Land Use
Restriction (LUR) No. 9 of the Brownfields Agreement generally states that a report of
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Mr. Bill Schmithorst February 3, 2023
Page 2
environment-related activities will be prepared for submittal to the DEQ Brownfields Program
each year for as long as physical redevelopment of the Brownfields property continues. This
report has been prepared in accordance with LUR No. 9 of the recorded Brownfields Agreement
for the Site.
Redevelopment plans for the eastern portion of the Brownfields property included minor grading
and leveling of the Site for the construction of two mixed-use commercial/retail buildings. One
level of partial subgrade parking is anticipated to be constructed below the mixed-use building
on Block 4 North and high-density residential use is planned on the upper stories of both the
Block 4 North and Stadium Lofts developments. Redevelopment plans also include the
installation of utilities and infrastructure and the construction of paved walkways and parking
areas and landscaped areas.
Redevelopment activities at the Site are ongoing and have included grading activities, utility
installations, and initial construction of the Stadium Loft building. A summary of environment-
related activities associated with redevelopment of this development is provided in the following
sections.
2.0 Redevelopment Activities
Redevelopment of the Site is being conducted in accordance with the DEQ Brownfields
approved Environmental Management Plan (EMP) dated August 8, 2018. Redevelopment at the
Site has included grading and excavations for utilities and foundations on the Stadium Lofts
portion of the Site which resulted in the export of soil. A Site map is included as Figure 2. A
brief summary of soil management activities is provided below.
2.1 Soil Management
Redevelopment activities completed at the Site have included grading activities, installation of
subsurface utilities, and foundation and vertical construction of the proposed Stadium Lofts
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Mr. Bill Schmithorst February 3, 2023
Page 3
building. The grading and excavation activities resulted in excess soil that could not be re-used
on-Site during redevelopment activities.
Soil Export
Excess soil generated during grading activities conducted at the Site was collected in stockpiles.
In March and June 2022, H&H conducted soil characterization sampling from stockpiles on Site
at the time in accordance with the DEQ-approved EMP.
In March 2022, soil from initial grubbing and grading activities on the Stadium Lofts
development was stockpiled into one stockpile located on the Site. The stockpile (labeled
Stockpile 1) was approximately 30 cubic yards and was located on the western portion of the
development Site. One sample and one duplicate sample were collected from the stockpile, and a
summary of the analytical data is included in Table 1. Based on the results of the soil
characterization sampling and in accordance with the DEQ-approved EMP, the soil in
Stockpile 1 was profiled to be transported and received at the Republic Services Charlotte Motor
Speedway (CMS) Subtitle D landfill in Concord, North Carolina. The General Contractor (GC)
is in the process of obtaining copies of the waste manifests documenting the disposal of the
export of this soil. Copies of the waste manifests documenting disposal of this export soil will be
provided under separate cover upon receipt of the manifests. Copies of the laboratory analytical
data sheets for the March 2022 stockpile characterization activities is included in Appendix A.
In June 2022, soil from additional grading activities on the Stadium Lofts development was
stockpiled into one stockpile located on the Site. The stockpile (labeled Stockpile 1) was
estimated to be approximately 1,000 cubic yards and was located on the western portion of the
development Site. One sample and one duplicate sample were collected from the stockpile, and a
summary of the analytical data is included in Table 2. The soil characterization assessment
activities are documented in a soil export request email dated June 16, 2022. Based on the results
of the soil characterization sampling activities, the DEQ Brownfields Program provided a
Brownfields Soil Management Options letter dated June 16, 2022. Copies of the June 16, 2022
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Mr. Bill Schmithorst February 3, 2023
Page 4
email correspondence and the June 16, 2022 Brownfields Soil Management Options letter are
provided in Appendix A.
Following receipt of the June 16, 2022 Brownfields Soil Management Options letter,
approximately 1,202 cubic yards from Stockpile 1 were loaded onto trucks and transported to
Reeve’s Landfill (Permit No. 60S-LCID) located at 2323 Salome Church Road in Charlotte,
North Carolina on June 23, 2022. During the truck loading activities, excavated soils were field
screened by H&H personnel for the presence of visual and olfactory indication of potential
impacts, and screened for the presence of volatile organic vapors with a calibrated
photoionization detector (PID). No obvious evidence of soil impacts were identified by H&H
personnel during the excavation or truck-loading activities. The waste manifests documenting
disposal of the export soil are provided in Appendix B.
In June 2022, soil stockpiled beside the original Stockpile 1 was stockpiled into another stockpile
in the western portion of the development. This stockpile (labeled Stockpile 2) was estimated to
contain approximately 300 cubic yards. One sample and one duplicate sample were collected
from the stockpile, and a summary of the analytical data is included in Table 3. Based on the
results of the soil characterization sampling and in accordance with the DEQ-approved EMP, the
soil will either be used on-Site beneath impervious surfaces or transported off-Site to the
Republic Services CMS Subtitle D landfill in Concord, North Carolina. Copies of the laboratory
analytical data sheets for the June 23, 2022 stockpile characterization activities are included in
Appendix A.
3.0 Summary
In summary, redevelopment activities at the Block 4 North and Stadium Lofts developments at
the K-Town Furniture Brownfields property (PINs 5614601290000 and 56146001440000) were
conducted in accordance with the DEQ-approved EMP.
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Redevelopment Report/22031_K-Town Furniture_Redevelopment Summary Rpt.doc
Mr. Bill Schmithorst February 3, 2023
Page 5
Should you have any questions or need additional information, please do not hesitate to call me
at [phone].
Very truly yours,
Hart & Hickman, PC
Shannon Cottrill Senior Project Manager
Attachments:
cc: Mr. Peter Flotz, RFD, LLC and KB4, LLC (Via Email) Ms. Amy Myers, LMG (Via Email)
Table 1 (Page 1 of 1)
Summary of Soil Stockpile Analytical Results (March 2022)
K-Town Furniture (22031-18-013)
Kannapolis, North CarolinaH&H Job No. LSG-001
Export Area
Composite Grab Composite Grab
Date Range Mean
Units
VOCs (8260D)
Toluene --0.0074 --<0.0019 8.3 990 9,700 ----
SVOCs (8270E)
Anthracene 0.181 J --<0.123 --1,300 3,600 45,000 ----
Benzo(a)anthracene 0.469 --0.257J --0.35 1.1 21 ----
Benzo(a)pyrene 0.456 --0.244J --0.12 0.11 2.1 ----
Benzo(b)fluoranthene 0.540 --0.333J --1.2 1.1 21 ----
Benzo(g,h,i)perylene 0.297J --0.181J --NE NE NE ----
Benzo(k)fluoranthene 0.257J --0.133J --12 11 210 ----
Chrysene 0.459 --0.236J --36 110 2,100 ----
Fluoranthene 0.911 --0.456 --670 480 6,000 ----
Indeno(1,2,3-cd)pyrene 0.262J --<0.148 --3.9 1.1 21 ----
Phenanthrene 0.652 --0.168J --NE NE NE ----
Pyrene 0.814 --0.423 --440 360 4,500 ----
Metals (6020B/7471B/7199)
Arsenic 2.1 --1.9 --5.8 0.68 3.0 1.0 - 18 4.8
Barium 125 M1 --113 --580 3,100 47,000 50 - 1,000 356
Cadmium 0.056J --0.047J --3.0 1.4 20 1.0 - 10 4.3
Chromium (total)9.6 --7.6 --NE NE NE 7.0 - 300 65
Trivalent Chromium 9.24 --7.6 --360,000 23,000 350,000 NS NS
Hexavalent Chromium 0.360J --<0.306 --3.8 0.31 6.5 NS NS
Lead 22.2 --18.6 --270 400 800 ND - 50 16
Mercury 0.027 --0.031 --1.0 2.3 9.7 0.03 - 0.52 0.121
Selenium 0.30J --0.25J --2.1 78 1,200 <0.1 - 0.8 0.42
Silver <0.16 --<0.16 --3.4 78 1,200 ND - 5.0 NS
Notes:
1) NorthCarolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated January 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.
Compound concentrations are reported in milligrams per kilograms (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Yellow highlighting indicates concentration exceeds Protection of Groundwater PSRG.
Bold indicates concentration exceeds Residential PSRG.
With the exception of metals, only compounds detected in at least one sample are shown.Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds.
J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration.
-- = not applicable; NE = not established; NS = not specified; ND = not detected
M1 = Matrix spike recovery exceeded QC limits, therefore result is an estimate.
milligrams per kilogram (mg/kg)
Sample ID SP-1 SP-DUP Protection of
Groundwater
PSRGs(1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Regional Background Metals in
Soil (2)
3/15/2022
STOCKPILE 1
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Stockpile Sampling/March 2022/K-Town Furniture TablesDate:3/24/2022
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2 (Page 1 of 1)
Summary of Soil Stockpile Analytical Results (June 2022)
K-Town Furniture (22031-18-013)
Kannapolis, North CarolinaH&H Job No. LSG-001
Export Area
Composite Grab Composite Grab
Date Range Mean
Units
VOCs (8260D)
Naphthalene --0.0101 --0.0114 0.39 2.1 8.8
Toluene --0.0053 J --<0.0017 8.3 990 9,700 ----
SVOCs (8270E)
Benzo(a)anthracene <0.118 --0.145 J --0.35 1.1 21 ----
Benzo(b)fluoranthene 0.141 J --0.161 J --1.2 1.1 21 ----
Chrysene <0.129 --0.137 J --36 110 2,100 ----
Fluoranthene 0.178 J --0.274 J --670 480 6,000 ----
Phenanthrene 0.136 J --0.214 J --NE NE NE ----
Pyrene 0.184 J --0.251 J --440 360 4,500 ----
Metals (6020B/7471B/7199)
Arsenic 1.7 --1.6 --5.8 0.68 3.0 1.0 - 18 4.8
Barium 114 --113 --580 3,100 47,000 50 - 1,000 356
Cadmium 0.055 J --0.055 J --3.0 1.4 20 1.0 - 10 4.3
Chromium (total)9.0 --9.8 --NE NE NE 7.0 - 300 65
Trivalent Chromium 8.16 --9.06 --360,000 23,000 350,000 NS NS
Hexavalent Chromium 0.84 --0.74 --3.8 0.31 6.5 NS NS
Lead 22.4 --27.2 --270 400 800 ND - 50 16
Mercury 0.035 --0.042 --1.0 2.3 9.7 0.03 - 0.52 0.121
Selenium 0.30 J --0.29 J --2.1 78 1,200 <0.1 - 0.8 0.42
Silver <0.15 --<0.15 --3.4 78 1,200 ND - 5.0 NS
Notes:
1) NorthCarolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated January 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.Compound concentrations are reported in milligrams per kilograms (mg/kg).Compound concentrations are reported to the laboratory method detection limits.
Bold indicates concentration exceeds Residential PSRG.
With the exception of metals, only compounds detected in at least one sample are shown.
Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds.J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration.
-- = not applicable; NE = not established; NS = not specified; ND = not detected
milligrams per kilogram (mg/kg)
Sample ID SP-1 DUP-1 Protection of
Groundwater
PSRGs(1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Regional Background Metals in
Soil (2)
6/1/2022
STOCKPILE 1
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Stockpile Sampling/June 2022/K-Town Furniture TablesDate:6/16/2022
Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3 (Page 1 of 1)
Summary of Soil Stockpile Analytical Results (June 2022)
K-Town Furniture (22031-18-013)
Kannapolis, North CarolinaH&H Job No. LSG-001
Export Area
Composite Grab Composite Grab
Date Range Mean
Units
VOCs (8260D)
2-Butanone (MEK)--0.0872 J --0.104 J 17 5,500 40,000 ----
Toluene --0.0093 IK --0.0078 J IK 8.3 990 9,700 ----
SVOCs (8270E)
Benzo(a)anthracene 0.125 J --0.219 J --0.35 1.1 21 ----
Benzo(a)pyrene <0.126 --0.212 J --0.12 0.11 2.1 ----
Benzo(b)fluoranthene 0.145 J --0.272 J --1.2 1.1 21 ----
Chrysene <0.133 --0.225 J --36 110 2,100 ----
Fluoranthene 0.264 J --0.449 --670 480 6,000 ----
Phenanthrene 0.175 J --0.319 J --NE NE NE ----
Pyrene 0.211 J --0.407 --440 360 4,500 ----
Metals (6020B/7471B/7199)
Arsenic 1.4 --1.1 --5.8 0.68 3.0 1.0 - 18 4.8
Barium 113 M1 --93.3 --580 3,100 47,000 50 - 1,000 356
Cadmium 1.0 --1.1 --3.0 1.4 20 1.0 - 10 4.3
Chromium (total)8.4 --7.3 --NE NE NE 7.0 - 300 65
Trivalent Chromium 7.60 --6.0 --360,000 23,000 350,000 NS NS
Hexavalent Chromium 0.80 --1.3 --3.8 0.31 6.5 NS NS
Lead 21.4 --19.0 --270 400 800 ND - 50 16
Mercury 0.037 --0.32 J --1.0 2.3 9.7 0.03 - 0.52 0.121
Selenium 0.37 J --0.029 --2.1 78 1,200 <0.1 - 0.8 0.42
Silver <0.16 --<0.16 --3.4 78 1,200 ND - 5.0 NS
Notes:
1) NorthCarolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated January 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.Compound concentrations are reported in milligrams per kilograms (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Yellow highlighting indicates concentration exceeds Protection of Groundwater PSRG.
Bold indicates concentration exceeds Residential PSRG.With the exception of metals, only compounds detected in at least one sample are shown.Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds.
J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration.-- = not applicable; NE = not established; NS = not specified; ND = not detectedIK = The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value.
M1 = Matrix spike recovery exceeded quality control (QC) limits. Batch accepted based on laboratory control sample (LCS) recovery.
milligrams per kilogram (mg/kg)
Sample ID SP-2 DUP-2 Protection of
Groundwater
PSRGs(1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Regional Background Metals in
Soil (2)
6/23/2022
STOCKPILE 1
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Stockpile Sampling/Late June 2022/Tables/K-Town Furniture TablesDate:7/12/2022
Table 3 (Page 1 of 1)
Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.
Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed August, 2021.
SITE LOCATION MAP
K-TOWN FURNITUREBROWNFIELDS PROPERTY
KANNAPOLIS, NORTH CAROLINA
DATE: 2-9-22
JOB NO: LSG-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\LSG-001\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHINA GROVE, CONCORD, ENOCHVILLE AND KANNAPOLIS, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
FORMER GAS STATION
(400 W. A STREET)
FORMER AUTO REPAIR SHOPS (DEMOLISHED)
(136-138 OAK AVENUE)
FORMER WATER VAULT
FORMER PURITAN/ BOB'S LAUNDRY &
DRY CLEANERS (DEMOLISHED)
(311 WEST A STREET)
W.
A

S
T
R
E
E
T
W.
B

S
T
R
E
E
T
OAK AVENUEWELLNESS WAY
CHES
T
N
U
T
A
V
E
N
U
E
LA
U
R
E
A
T
E

W
A
Y
BURIED TIMBER PILINGS
FORMER WRENN'S CLEANERS (DEMOLISHED)
(136 WEST AVENUE)
REVISION NO. 0
JOB NO. LSG-001
DATE: 2-1-23
FIGURE NO. 2
K-TOWN FURNITURE
BROWNFIELDS PROPERTY
KANNAPOLIS, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS SITE PROPERTY
BOUNDARY
PARCEL BOUNDARY
FORMER BUILDING OUTLINE
APPROXIMATE AREA SUBJECT TO
PREVIOUS BROWNFIELDS
AGREEMENT FOR NC RESEARCH
CAMPUS (INCLUDING WATER VAULT)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTE:
1.PARCEL BOUNDARY DATA OBTAINED FROM CABARRUS
COUNTY GIS, 2022.
PROPOSED BLOCK 4
NORTH REDEVELOPMENT
FORMER STAR CLEANERS
(DEMOLISHED)
(108 WEST AVENUE)
FORMER GOODYEAR SERVICE
GARAGE (DEMOLISHED)
(100 WEST AVENUE)
(UNDER CONSTRUCTION)S:\AAA-Master Projects\Lansing Melbourne Group (LSG)\LSG-001 Kannapolis NC\In Situ Soil Assessment\Figures\LSG-001 SITE MAP 20220816.dwg, FIG 2 - SITE MAP, 2/1/2023 1:53:34 PM, sperry

Appendix A

Laboratory Analytical Data Sheets, Soil Transfer Request, and Brownfields Soil Management
Options Letters

#=CL#
March 23, 2022
LIMS USE: FR - SHANNON COTTRILL
LIMS OBJECT ID: 92593450
92593450
Project:
Pace Project No.:
RE:
Mr. Shannon Cottrill
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
LSG-001
Dear Mr. Cottrill:
Enclosed are the analytical results for sample(s) received by the laboratory on March 15, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
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EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92593450
LSG-001
Pace Analytical Services National
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92593450
LSG-001
Lab ID Sample ID Matrix Date Collected Date Received
92593450001 SP-1 Solid 03/15/22 11:00 03/15/22 12:30
92593450002 SP-DUP Solid 03/15/22 00:00 03/15/22 12:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92593450
LSG-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92593450001 SP-1 EPA 6020B 7 PASI-MJFB, NN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANJER
92593450002 SP-DUP EPA 6020B 7 PASI-MJFB, NN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANJER
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-1 Lab ID:92593450001 Collected:03/15/22 11:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.1 mg/kg 03/21/22 17:21 7440-38-203/21/22 10:270.57 0.12 1
Barium 125 mg/kg 03/21/22 17:21 7440-39-3 M103/21/22 10:270.34 0.061 1
Cadmium 0.056J mg/kg 03/21/22 17:21 7440-43-903/21/22 10:270.091 0.036 1
Chromium 9.6 mg/kg 03/21/22 17:21 7440-47-303/21/22 10:270.57 0.16 1
Lead 22.2 mg/kg 03/21/22 17:21 7439-92-103/21/22 10:270.23 0.033 1
Selenium 0.30J mg/kg 03/21/22 17:21 7782-49-203/21/22 10:270.57 0.097 1
Silver ND mg/kg 03/22/22 16:02 7440-22-403/21/22 10:270.57 0.16 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.027 mg/kg 03/21/22 13:42 7439-97-603/21/22 11:100.022 0.0095 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/16/22 17:14 83-32-903/15/22 22:463871361
Acenaphthylene ND ug/kg 03/16/22 17:14 208-96-803/15/22 22:463871361
Aniline ND ug/kg 03/16/22 17:14 62-53-303/15/22 22:463871511
Anthracene 181J ug/kg 03/16/22 17:14 120-12-703/15/22 22:463871271
Benzo(a)anthracene 469 ug/kg 03/16/22 17:14 56-55-303/15/22 22:463871291
Benzo(a)pyrene 456 ug/kg 03/16/22 17:14 50-32-803/15/22 22:463871341
Benzo(b)fluoranthene 540 ug/kg 03/16/22 17:14 205-99-203/15/22 22:463871291
Benzo(g,h,i)perylene 297J ug/kg 03/16/22 17:14 191-24-203/15/22 22:463871501
Benzo(k)fluoranthene 257J ug/kg 03/16/22 17:14 207-08-903/15/22 22:463871361
Benzoic Acid ND ug/kg 03/16/22 17:14 65-85-003/15/22 22:4619308311
Benzyl alcohol ND ug/kg 03/16/22 17:14 100-51-603/15/22 22:467732931
4-Bromophenylphenyl ether ND ug/kg 03/16/22 17:14 101-55-303/15/22 22:463871491
Butylbenzylphthalate ND ug/kg 03/16/22 17:14 85-68-703/15/22 22:463871631
4-Chloro-3-methylphenol ND ug/kg 03/16/22 17:14 59-50-703/15/22 22:467732721
4-Chloroaniline ND ug/kg 03/16/22 17:14 106-47-803/15/22 22:467733031
bis(2-Chloroethoxy)methane ND ug/kg 03/16/22 17:14 111-91-103/15/22 22:463871611
bis(2-Chloroethyl) ether ND ug/kg 03/16/22 17:14 111-44-403/15/22 22:463871451
2-Chloronaphthalene ND ug/kg 03/16/22 17:14 91-58-703/15/22 22:463871531
2-Chlorophenol ND ug/kg 03/16/22 17:14 95-57-803/15/22 22:463871451
4-Chlorophenylphenyl ether ND ug/kg 03/16/22 17:14 7005-72-303/15/22 22:463871441
Chrysene 459 ug/kg 03/16/22 17:14 218-01-903/15/22 22:463871411
Dibenz(a,h)anthracene ND ug/kg 03/16/22 17:14 53-70-303/15/22 22:463871491
Dibenzofuran ND ug/kg 03/16/22 17:14 132-64-903/15/22 22:463871391
1,2-Dichlorobenzene ND ug/kg 03/16/22 17:14 95-50-103/15/22 22:463871391
1,3-Dichlorobenzene ND ug/kg 03/16/22 17:14 541-73-103/15/22 22:463871371
1,4-Dichlorobenzene ND ug/kg 03/16/22 17:14 106-46-703/15/22 22:463871481
3,3'-Dichlorobenzidine ND ug/kg 03/16/22 17:14 91-94-1 IL03/15/22 22:467732611
2,4-Dichlorophenol ND ug/kg 03/16/22 17:14 120-83-203/15/22 22:463871511
Diethylphthalate ND ug/kg 03/16/22 17:14 84-66-203/15/22 22:463871421
2,4-Dimethylphenol ND ug/kg 03/16/22 17:14 105-67-903/15/22 22:463871611
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-1 Lab ID:92593450001 Collected:03/15/22 11:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/16/22 17:14 131-11-303/15/22 22:463871411
Di-n-butylphthalate ND ug/kg 03/16/22 17:14 84-74-203/15/22 22:463871301
4,6-Dinitro-2-methylphenol ND ug/kg 03/16/22 17:14 534-52-103/15/22 22:467733611
2,4-Dinitrophenol ND ug/kg 03/16/22 17:14 51-28-503/15/22 22:46193011901
2,4-Dinitrotoluene ND ug/kg 03/16/22 17:14 121-14-203/15/22 22:463871491
2,6-Dinitrotoluene ND ug/kg 03/16/22 17:14 606-20-203/15/22 22:463871421
Di-n-octylphthalate ND ug/kg 03/16/22 17:14 117-84-0 v103/15/22 22:463871521
bis(2-Ethylhexyl)phthalate ND ug/kg 03/16/22 17:14 117-81-703/15/22 22:463871501
Fluoranthene 911 ug/kg 03/16/22 17:14 206-44-003/15/22 22:463871321
Fluorene ND ug/kg 03/16/22 17:14 86-73-703/15/22 22:463871361
Hexachloro-1,3-butadiene ND ug/kg 03/16/22 17:14 87-68-303/15/22 22:463871681
Hexachlorobenzene ND ug/kg 03/16/22 17:14 118-74-103/15/22 22:463871511
Hexachlorocyclopentadiene ND ug/kg 03/16/22 17:14 77-47-403/15/22 22:463872211
Hexachloroethane ND ug/kg 03/16/22 17:14 67-72-103/15/22 22:463871481
Indeno(1,2,3-cd)pyrene 262J ug/kg 03/16/22 17:14 193-39-503/15/22 22:463871521
Isophorone ND ug/kg 03/16/22 17:14 78-59-103/15/22 22:463871721
1-Methylnaphthalene ND ug/kg 03/16/22 17:14 90-12-003/15/22 22:463871361
2-Methylnaphthalene ND ug/kg 03/16/22 17:14 91-57-603/15/22 22:463871551
2-Methylphenol(o-Cresol)ND ug/kg 03/16/22 17:14 95-48-703/15/22 22:463871581
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/16/22 17:14 15831-10-403/15/22 22:463871561
Naphthalene ND ug/kg 03/16/22 17:14 91-20-303/15/22 22:463871311
2-Nitroaniline ND ug/kg 03/16/22 17:14 88-74-403/15/22 22:4619303161
3-Nitroaniline ND ug/kg 03/16/22 17:14 99-09-203/15/22 22:4619303031
4-Nitroaniline ND ug/kg 03/16/22 17:14 100-01-603/15/22 22:467732941
Nitrobenzene ND ug/kg 03/16/22 17:14 98-95-303/15/22 22:463871791
2-Nitrophenol ND ug/kg 03/16/22 17:14 88-75-503/15/22 22:463871681
4-Nitrophenol ND ug/kg 03/16/22 17:14 100-02-703/15/22 22:4619307471
N-Nitrosodimethylamine ND ug/kg 03/16/22 17:14 62-75-903/15/22 22:463871301
N-Nitroso-di-n-propylamine ND ug/kg 03/16/22 17:14 621-64-703/15/22 22:463871451
N-Nitrosodiphenylamine ND ug/kg 03/16/22 17:14 86-30-603/15/22 22:463871371
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/16/22 17:14 108-60-1 v103/15/22 22:463871841
Pentachlorophenol ND ug/kg 03/16/22 17:14 87-86-503/15/22 22:467733781
Phenanthrene 652 ug/kg 03/16/22 17:14 85-01-803/15/22 22:463871271
Phenol ND ug/kg 03/16/22 17:14 108-95-203/15/22 22:463871721
Pyrene 814 ug/kg 03/16/22 17:14 129-00-003/15/22 22:463871571
Pyridine ND ug/kg 03/16/22 17:14 110-86-103/15/22 22:463871221
1,2,4-Trichlorobenzene ND ug/kg 03/16/22 17:14 120-82-103/15/22 22:463871521
2,4,5-Trichlorophenol ND ug/kg 03/16/22 17:14 95-95-403/15/22 22:463871771
2,4,6-Trichlorophenol ND ug/kg 03/16/22 17:14 88-06-203/15/22 22:463871591
Surrogates
Nitrobenzene-d5 (S)74 %03/16/22 17:14 4165-60-003/15/22 22:4621-130 1
2-Fluorobiphenyl (S)73 %03/16/22 17:14 321-60-803/15/22 22:4619-130 1
Terphenyl-d14 (S)88 %03/16/22 17:14 1718-51-003/15/22 22:4615-130 1
Phenol-d6 (S)71 %03/16/22 17:14 13127-88-303/15/22 22:4618-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-1 Lab ID:92593450001 Collected:03/15/22 11:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)65 %03/16/22 17:14 367-12-403/15/22 22:4618-130 1
2,4,6-Tribromophenol (S)99 %03/16/22 17:14 118-79-603/15/22 22:4618-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/16/22 04:24 67-64-103/15/22 18:3514145.2 1
Benzene ND ug/kg 03/16/22 04:24 71-43-203/15/22 18:357.0 2.8 1
Bromobenzene ND ug/kg 03/16/22 04:24 108-86-103/15/22 18:357.0 2.3 1
Bromochloromethane ND ug/kg 03/16/22 04:24 74-97-503/15/22 18:357.0 2.1 1
Bromodichloromethane ND ug/kg 03/16/22 04:24 75-27-403/15/22 18:357.0 2.7 1
Bromoform ND ug/kg 03/16/22 04:24 75-25-203/15/22 18:357.0 2.5 1
Bromomethane ND ug/kg 03/16/22 04:24 74-83-903/15/22 18:3514.1 11.1 1
2-Butanone (MEK)ND ug/kg 03/16/22 04:24 78-93-303/15/22 18:3514133.8 1
n-Butylbenzene ND ug/kg 03/16/22 04:24 104-51-803/15/22 18:357.0 3.3 1
sec-Butylbenzene ND ug/kg 03/16/22 04:24 135-98-803/15/22 18:357.0 3.1 1
tert-Butylbenzene ND ug/kg 03/16/22 04:24 98-06-603/15/22 18:357.0 2.5 1
Carbon tetrachloride ND ug/kg 03/16/22 04:24 56-23-503/15/22 18:357.0 2.6 1
Chlorobenzene ND ug/kg 03/16/22 04:24 108-90-703/15/22 18:357.0 1.4 1
Chloroethane ND ug/kg 03/16/22 04:24 75-00-303/15/22 18:3514.1 5.4 1
Chloroform ND ug/kg 03/16/22 04:24 67-66-303/15/22 18:357.0 4.3 1
Chloromethane ND ug/kg 03/16/22 04:24 74-87-303/15/22 18:3514.1 5.9 1
2-Chlorotoluene ND ug/kg 03/16/22 04:24 95-49-803/15/22 18:357.0 2.5 1
4-Chlorotoluene ND ug/kg 03/16/22 04:24 106-43-403/15/22 18:357.0 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/16/22 04:24 96-12-803/15/22 18:357.0 2.7 1
Dibromochloromethane ND ug/kg 03/16/22 04:24 124-48-103/15/22 18:357.0 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 03/16/22 04:24 106-93-403/15/22 18:357.0 3.1 1
Dibromomethane ND ug/kg 03/16/22 04:24 74-95-303/15/22 18:357.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 03/16/22 04:24 95-50-103/15/22 18:357.0 2.5 1
1,3-Dichlorobenzene ND ug/kg 03/16/22 04:24 541-73-103/15/22 18:357.0 2.2 1
1,4-Dichlorobenzene ND ug/kg 03/16/22 04:24 106-46-703/15/22 18:357.0 1.8 1
Dichlorodifluoromethane ND ug/kg 03/16/22 04:24 75-71-803/15/22 18:3514.1 3.1 1
1,1-Dichloroethane ND ug/kg 03/16/22 04:24 75-34-303/15/22 18:357.0 2.9 1
1,2-Dichloroethane ND ug/kg 03/16/22 04:24 107-06-203/15/22 18:357.0 4.7 1
1,1-Dichloroethene ND ug/kg 03/16/22 04:24 75-35-403/15/22 18:357.0 2.9 1
cis-1,2-Dichloroethene ND ug/kg 03/16/22 04:24 156-59-203/15/22 18:357.0 2.4 1
trans-1,2-Dichloroethene ND ug/kg 03/16/22 04:24 156-60-503/15/22 18:357.0 2.5 1
1,2-Dichloropropane ND ug/kg 03/16/22 04:24 78-87-503/15/22 18:357.0 2.1 1
1,3-Dichloropropane ND ug/kg 03/16/22 04:24 142-28-903/15/22 18:357.0 2.2 1
2,2-Dichloropropane ND ug/kg 03/16/22 04:24 594-20-703/15/22 18:357.0 2.3 1
1,1-Dichloropropene ND ug/kg 03/16/22 04:24 563-58-603/15/22 18:357.0 3.4 1
cis-1,3-Dichloropropene ND ug/kg 03/16/22 04:24 10061-01-503/15/22 18:357.0 1.9 1
trans-1,3-Dichloropropene ND ug/kg 03/16/22 04:24 10061-02-603/15/22 18:357.0 2.4 1
Diisopropyl ether ND ug/kg 03/16/22 04:24 108-20-303/15/22 18:357.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-1 Lab ID:92593450001 Collected:03/15/22 11:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/16/22 04:24 100-41-403/15/22 18:357.0 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 03/16/22 04:24 87-68-303/15/22 18:3514.1 11.5 1
2-Hexanone ND ug/kg 03/16/22 04:24 591-78-603/15/22 18:3570.4 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 03/16/22 04:24 98-82-803/15/22 18:357.0 2.4 1
p-Isopropyltoluene ND ug/kg 03/16/22 04:24 99-87-603/15/22 18:357.0 3.5 1
Methylene Chloride ND ug/kg 03/16/22 04:24 75-09-203/15/22 18:3528.2 19.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/16/22 04:24 108-10-103/15/22 18:3570.4 6.8 1
Methyl-tert-butyl ether ND ug/kg 03/16/22 04:24 1634-04-403/15/22 18:357.0 2.6 1
Naphthalene ND ug/kg 03/16/22 04:24 91-20-303/15/22 18:357.0 3.7 1
n-Propylbenzene ND ug/kg 03/16/22 04:24 103-65-103/15/22 18:357.0 2.5 1
Styrene ND ug/kg 03/16/22 04:24 100-42-503/15/22 18:357.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/16/22 04:24 630-20-603/15/22 18:357.0 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/16/22 04:24 79-34-503/15/22 18:357.0 1.9 1
Tetrachloroethene ND ug/kg 03/16/22 04:24 127-18-403/15/22 18:357.0 2.2 1
Toluene 7.4 ug/kg 03/16/22 04:24 108-88-303/15/22 18:357.0 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 03/16/22 04:24 87-61-603/15/22 18:357.0 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/16/22 04:24 120-82-103/15/22 18:357.0 5.9 1
1,1,1-Trichloroethane ND ug/kg 03/16/22 04:24 71-55-603/15/22 18:357.0 3.7 1
1,1,2-Trichloroethane ND ug/kg 03/16/22 04:24 79-00-503/15/22 18:357.0 2.3 1
Trichloroethene ND ug/kg 03/16/22 04:24 79-01-603/15/22 18:357.0 1.8 1
Trichlorofluoromethane ND ug/kg 03/16/22 04:24 75-69-403/15/22 18:357.0 3.9 1
1,2,3-Trichloropropane ND ug/kg 03/16/22 04:24 96-18-403/15/22 18:357.0 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 03/16/22 04:24 95-63-603/15/22 18:357.0 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 03/16/22 04:24 108-67-803/15/22 18:357.0 2.4 1
Vinyl acetate ND ug/kg 03/16/22 04:24 108-05-403/15/22 18:3570.4 5.1 1
Vinyl chloride ND ug/kg 03/16/22 04:24 75-01-403/15/22 18:3514.1 3.6 1
Xylene (Total)ND ug/kg 03/16/22 04:24 1330-20-703/15/22 18:3514.1 4.0 1
m&p-Xylene ND ug/kg 03/16/22 04:24 179601-23-103/15/22 18:3514.1 4.8 1
o-Xylene ND ug/kg 03/16/22 04:24 95-47-603/15/22 18:357.0 3.1 1
Surrogates
Toluene-d8 (S)99 %03/16/22 04:24 2037-26-503/15/22 18:3570-130 1
4-Bromofluorobenzene (S)100 %03/16/22 04:24 460-00-403/15/22 18:3569-134 1
1,2-Dichloroethane-d4 (S)87 %03/16/22 04:24 17060-07-003/15/22 18:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.1 %03/15/22 17:48 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 84.3 %03/18/22 09:1803/18/22 09:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-1 Lab ID:92593450001 Collected:03/15/22 11:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.360J mg/kg 03/22/22 17:15 18540-29-9 J03/22/22 00:301.19 0.302 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-DUP Lab ID:92593450002 Collected:03/15/22 00:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.9 mg/kg 03/21/22 17:50 7440-38-203/21/22 10:270.56 0.12 1
Barium 113 mg/kg 03/21/22 17:50 7440-39-303/21/22 10:270.34 0.060 1
Cadmium 0.047J mg/kg 03/21/22 17:50 7440-43-903/21/22 10:270.089 0.035 1
Chromium 7.6 mg/kg 03/21/22 17:50 7440-47-303/21/22 10:270.56 0.16 1
Lead 18.6 mg/kg 03/21/22 17:50 7439-92-103/21/22 10:270.22 0.033 1
Selenium 0.25J mg/kg 03/21/22 17:50 7782-49-203/21/22 10:270.56 0.096 1
Silver ND mg/kg 03/22/22 16:19 7440-22-403/21/22 10:270.56 0.16 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.031 mg/kg 03/21/22 13:47 7439-97-603/21/22 11:100.020 0.0088 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 03/16/22 17:40 83-32-903/15/22 22:463761321
Acenaphthylene ND ug/kg 03/16/22 17:40 208-96-803/15/22 22:463761321
Aniline ND ug/kg 03/16/22 17:40 62-53-303/15/22 22:463761471
Anthracene ND ug/kg 03/16/22 17:40 120-12-703/15/22 22:463761231
Benzo(a)anthracene 257J ug/kg 03/16/22 17:40 56-55-303/15/22 22:463761251
Benzo(a)pyrene 244J ug/kg 03/16/22 17:40 50-32-803/15/22 22:463761301
Benzo(b)fluoranthene 333J ug/kg 03/16/22 17:40 205-99-203/15/22 22:463761251
Benzo(g,h,i)perylene 181J ug/kg 03/16/22 17:40 191-24-203/15/22 22:463761461
Benzo(k)fluoranthene 133J ug/kg 03/16/22 17:40 207-08-903/15/22 22:463761321
Benzoic Acid ND ug/kg 03/16/22 17:40 65-85-003/15/22 22:4618808081
Benzyl alcohol ND ug/kg 03/16/22 17:40 100-51-603/15/22 22:467522851
4-Bromophenylphenyl ether ND ug/kg 03/16/22 17:40 101-55-303/15/22 22:463761451
Butylbenzylphthalate ND ug/kg 03/16/22 17:40 85-68-703/15/22 22:463761581
4-Chloro-3-methylphenol ND ug/kg 03/16/22 17:40 59-50-703/15/22 22:467522641
4-Chloroaniline ND ug/kg 03/16/22 17:40 106-47-803/15/22 22:467522951
bis(2-Chloroethoxy)methane ND ug/kg 03/16/22 17:40 111-91-103/15/22 22:463761561
bis(2-Chloroethyl) ether ND ug/kg 03/16/22 17:40 111-44-403/15/22 22:463761411
2-Chloronaphthalene ND ug/kg 03/16/22 17:40 91-58-703/15/22 22:463761491
2-Chlorophenol ND ug/kg 03/16/22 17:40 95-57-803/15/22 22:463761411
4-Chlorophenylphenyl ether ND ug/kg 03/16/22 17:40 7005-72-303/15/22 22:463761401
Chrysene 236J ug/kg 03/16/22 17:40 218-01-903/15/22 22:463761371
Dibenz(a,h)anthracene ND ug/kg 03/16/22 17:40 53-70-303/15/22 22:463761451
Dibenzofuran ND ug/kg 03/16/22 17:40 132-64-903/15/22 22:463761361
1,2-Dichlorobenzene ND ug/kg 03/16/22 17:40 95-50-103/15/22 22:463761361
1,3-Dichlorobenzene ND ug/kg 03/16/22 17:40 541-73-103/15/22 22:463761331
1,4-Dichlorobenzene ND ug/kg 03/16/22 17:40 106-46-703/15/22 22:463761441
3,3'-Dichlorobenzidine ND ug/kg 03/16/22 17:40 91-94-1 IL03/15/22 22:467522541
2,4-Dichlorophenol ND ug/kg 03/16/22 17:40 120-83-203/15/22 22:463761471
Diethylphthalate ND ug/kg 03/16/22 17:40 84-66-203/15/22 22:463761381
2,4-Dimethylphenol ND ug/kg 03/16/22 17:40 105-67-903/15/22 22:463761561
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-DUP Lab ID:92593450002 Collected:03/15/22 00:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 03/16/22 17:40 131-11-303/15/22 22:463761371
Di-n-butylphthalate ND ug/kg 03/16/22 17:40 84-74-203/15/22 22:463761271
4,6-Dinitro-2-methylphenol ND ug/kg 03/16/22 17:40 534-52-103/15/22 22:467523511
2,4-Dinitrophenol ND ug/kg 03/16/22 17:40 51-28-503/15/22 22:46188011601
2,4-Dinitrotoluene ND ug/kg 03/16/22 17:40 121-14-203/15/22 22:463761451
2,6-Dinitrotoluene ND ug/kg 03/16/22 17:40 606-20-203/15/22 22:463761381
Di-n-octylphthalate ND ug/kg 03/16/22 17:40 117-84-0 v103/15/22 22:463761481
bis(2-Ethylhexyl)phthalate ND ug/kg 03/16/22 17:40 117-81-703/15/22 22:463761461
Fluoranthene 456 ug/kg 03/16/22 17:40 206-44-003/15/22 22:463761291
Fluorene ND ug/kg 03/16/22 17:40 86-73-703/15/22 22:463761321
Hexachloro-1,3-butadiene ND ug/kg 03/16/22 17:40 87-68-303/15/22 22:463761631
Hexachlorobenzene ND ug/kg 03/16/22 17:40 118-74-103/15/22 22:463761471
Hexachlorocyclopentadiene ND ug/kg 03/16/22 17:40 77-47-403/15/22 22:463762151
Hexachloroethane ND ug/kg 03/16/22 17:40 67-72-103/15/22 22:463761441
Indeno(1,2,3-cd)pyrene ND ug/kg 03/16/22 17:40 193-39-503/15/22 22:463761481
Isophorone ND ug/kg 03/16/22 17:40 78-59-103/15/22 22:463761681
1-Methylnaphthalene ND ug/kg 03/16/22 17:40 90-12-003/15/22 22:463761321
2-Methylnaphthalene ND ug/kg 03/16/22 17:40 91-57-603/15/22 22:463761501
2-Methylphenol(o-Cresol)ND ug/kg 03/16/22 17:40 95-48-703/15/22 22:463761541
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/16/22 17:40 15831-10-403/15/22 22:463761521
Naphthalene ND ug/kg 03/16/22 17:40 91-20-303/15/22 22:463761281
2-Nitroaniline ND ug/kg 03/16/22 17:40 88-74-403/15/22 22:4618803081
3-Nitroaniline ND ug/kg 03/16/22 17:40 99-09-203/15/22 22:4618802951
4-Nitroaniline ND ug/kg 03/16/22 17:40 100-01-603/15/22 22:467522861
Nitrobenzene ND ug/kg 03/16/22 17:40 98-95-303/15/22 22:463761741
2-Nitrophenol ND ug/kg 03/16/22 17:40 88-75-503/15/22 22:463761631
4-Nitrophenol ND ug/kg 03/16/22 17:40 100-02-703/15/22 22:4618807271
N-Nitrosodimethylamine ND ug/kg 03/16/22 17:40 62-75-903/15/22 22:463761271
N-Nitroso-di-n-propylamine ND ug/kg 03/16/22 17:40 621-64-703/15/22 22:463761411
N-Nitrosodiphenylamine ND ug/kg 03/16/22 17:40 86-30-603/15/22 22:463761331
2,2'-Oxybis(1-chloropropane)ND ug/kg 03/16/22 17:40 108-60-1 v103/15/22 22:463761791
Pentachlorophenol ND ug/kg 03/16/22 17:40 87-86-503/15/22 22:467523681
Phenanthrene 168J ug/kg 03/16/22 17:40 85-01-803/15/22 22:463761231
Phenol ND ug/kg 03/16/22 17:40 108-95-203/15/22 22:463761681
Pyrene 423 ug/kg 03/16/22 17:40 129-00-003/15/22 22:463761531
Pyridine ND ug/kg 03/16/22 17:40 110-86-103/15/22 22:463761191
1,2,4-Trichlorobenzene ND ug/kg 03/16/22 17:40 120-82-103/15/22 22:463761481
2,4,5-Trichlorophenol ND ug/kg 03/16/22 17:40 95-95-403/15/22 22:463761721
2,4,6-Trichlorophenol ND ug/kg 03/16/22 17:40 88-06-203/15/22 22:463761551
Surrogates
Nitrobenzene-d5 (S)79 %03/16/22 17:40 4165-60-003/15/22 22:4621-130 1
2-Fluorobiphenyl (S)76 %03/16/22 17:40 321-60-803/15/22 22:4619-130 1
Terphenyl-d14 (S)92 %03/16/22 17:40 1718-51-003/15/22 22:4615-130 1
Phenol-d6 (S)81 %03/16/22 17:40 13127-88-303/15/22 22:4618-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-DUP Lab ID:92593450002 Collected:03/15/22 00:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)75 %03/16/22 17:40 367-12-403/15/22 22:4618-130 1
2,4,6-Tribromophenol (S)108 %03/16/22 17:40 118-79-603/15/22 22:4618-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/16/22 04:41 67-64-103/15/22 18:3513142.0 1
Benzene ND ug/kg 03/16/22 04:41 71-43-203/15/22 18:356.5 2.6 1
Bromobenzene ND ug/kg 03/16/22 04:41 108-86-103/15/22 18:356.5 2.1 1
Bromochloromethane ND ug/kg 03/16/22 04:41 74-97-503/15/22 18:356.5 1.9 1
Bromodichloromethane ND ug/kg 03/16/22 04:41 75-27-403/15/22 18:356.5 2.5 1
Bromoform ND ug/kg 03/16/22 04:41 75-25-203/15/22 18:356.5 2.3 1
Bromomethane ND ug/kg 03/16/22 04:41 74-83-903/15/22 18:3513.1 10.3 1
2-Butanone (MEK)ND ug/kg 03/16/22 04:41 78-93-303/15/22 18:3513131.4 1
n-Butylbenzene ND ug/kg 03/16/22 04:41 104-51-803/15/22 18:356.5 3.1 1
sec-Butylbenzene ND ug/kg 03/16/22 04:41 135-98-803/15/22 18:356.5 2.9 1
tert-Butylbenzene ND ug/kg 03/16/22 04:41 98-06-603/15/22 18:356.5 2.3 1
Carbon tetrachloride ND ug/kg 03/16/22 04:41 56-23-503/15/22 18:356.5 2.4 1
Chlorobenzene ND ug/kg 03/16/22 04:41 108-90-703/15/22 18:356.5 1.3 1
Chloroethane ND ug/kg 03/16/22 04:41 75-00-303/15/22 18:3513.1 5.0 1
Chloroform ND ug/kg 03/16/22 04:41 67-66-303/15/22 18:356.5 4.0 1
Chloromethane ND ug/kg 03/16/22 04:41 74-87-303/15/22 18:3513.1 5.5 1
2-Chlorotoluene ND ug/kg 03/16/22 04:41 95-49-803/15/22 18:356.5 2.3 1
4-Chlorotoluene ND ug/kg 03/16/22 04:41 106-43-403/15/22 18:356.5 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/16/22 04:41 96-12-803/15/22 18:356.5 2.5 1
Dibromochloromethane ND ug/kg 03/16/22 04:41 124-48-103/15/22 18:356.5 3.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/16/22 04:41 106-93-403/15/22 18:356.5 2.9 1
Dibromomethane ND ug/kg 03/16/22 04:41 74-95-303/15/22 18:356.5 1.4 1
1,2-Dichlorobenzene ND ug/kg 03/16/22 04:41 95-50-103/15/22 18:356.5 2.4 1
1,3-Dichlorobenzene ND ug/kg 03/16/22 04:41 541-73-103/15/22 18:356.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 03/16/22 04:41 106-46-703/15/22 18:356.5 1.7 1
Dichlorodifluoromethane ND ug/kg 03/16/22 04:41 75-71-803/15/22 18:3513.1 2.8 1
1,1-Dichloroethane ND ug/kg 03/16/22 04:41 75-34-303/15/22 18:356.5 2.7 1
1,2-Dichloroethane ND ug/kg 03/16/22 04:41 107-06-203/15/22 18:356.5 4.3 1
1,1-Dichloroethene ND ug/kg 03/16/22 04:41 75-35-403/15/22 18:356.5 2.7 1
cis-1,2-Dichloroethene ND ug/kg 03/16/22 04:41 156-59-203/15/22 18:356.5 2.2 1
trans-1,2-Dichloroethene ND ug/kg 03/16/22 04:41 156-60-503/15/22 18:356.5 2.3 1
1,2-Dichloropropane ND ug/kg 03/16/22 04:41 78-87-503/15/22 18:356.5 2.0 1
1,3-Dichloropropane ND ug/kg 03/16/22 04:41 142-28-903/15/22 18:356.5 2.0 1
2,2-Dichloropropane ND ug/kg 03/16/22 04:41 594-20-703/15/22 18:356.5 2.1 1
1,1-Dichloropropene ND ug/kg 03/16/22 04:41 563-58-603/15/22 18:356.5 3.1 1
cis-1,3-Dichloropropene ND ug/kg 03/16/22 04:41 10061-01-503/15/22 18:356.5 1.8 1
trans-1,3-Dichloropropene ND ug/kg 03/16/22 04:41 10061-02-603/15/22 18:356.5 2.2 1
Diisopropyl ether ND ug/kg 03/16/22 04:41 108-20-303/15/22 18:356.5 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-DUP Lab ID:92593450002 Collected:03/15/22 00:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 03/16/22 04:41 100-41-403/15/22 18:356.5 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 03/16/22 04:41 87-68-303/15/22 18:3513.1 10.7 1
2-Hexanone ND ug/kg 03/16/22 04:41 591-78-603/15/22 18:3565.4 6.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/16/22 04:41 98-82-803/15/22 18:356.5 2.2 1
p-Isopropyltoluene ND ug/kg 03/16/22 04:41 99-87-603/15/22 18:356.5 3.2 1
Methylene Chloride ND ug/kg 03/16/22 04:41 75-09-203/15/22 18:3526.2 17.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/16/22 04:41 108-10-103/15/22 18:3565.4 6.3 1
Methyl-tert-butyl ether ND ug/kg 03/16/22 04:41 1634-04-403/15/22 18:356.5 2.4 1
Naphthalene ND ug/kg 03/16/22 04:41 91-20-303/15/22 18:356.5 3.4 1
n-Propylbenzene ND ug/kg 03/16/22 04:41 103-65-103/15/22 18:356.5 2.3 1
Styrene ND ug/kg 03/16/22 04:41 100-42-503/15/22 18:356.5 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/16/22 04:41 630-20-603/15/22 18:356.5 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/16/22 04:41 79-34-503/15/22 18:356.5 1.7 1
Tetrachloroethene ND ug/kg 03/16/22 04:41 127-18-403/15/22 18:356.5 2.1 1
Toluene ND ug/kg 03/16/22 04:41 108-88-303/15/22 18:356.5 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 03/16/22 04:41 87-61-603/15/22 18:356.5 5.3 1
1,2,4-Trichlorobenzene ND ug/kg 03/16/22 04:41 120-82-103/15/22 18:356.5 5.5 1
1,1,1-Trichloroethane ND ug/kg 03/16/22 04:41 71-55-603/15/22 18:356.5 3.4 1
1,1,2-Trichloroethane ND ug/kg 03/16/22 04:41 79-00-503/15/22 18:356.5 2.2 1
Trichloroethene ND ug/kg 03/16/22 04:41 79-01-603/15/22 18:356.5 1.7 1
Trichlorofluoromethane ND ug/kg 03/16/22 04:41 75-69-403/15/22 18:356.5 3.6 1
1,2,3-Trichloropropane ND ug/kg 03/16/22 04:41 96-18-403/15/22 18:356.5 3.3 1
1,2,4-Trimethylbenzene ND ug/kg 03/16/22 04:41 95-63-603/15/22 18:356.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/16/22 04:41 108-67-803/15/22 18:356.5 2.2 1
Vinyl acetate ND ug/kg 03/16/22 04:41 108-05-403/15/22 18:3565.4 4.8 1
Vinyl chloride ND ug/kg 03/16/22 04:41 75-01-403/15/22 18:3513.1 3.3 1
Xylene (Total)ND ug/kg 03/16/22 04:41 1330-20-703/15/22 18:3513.1 3.7 1
m&p-Xylene ND ug/kg 03/16/22 04:41 179601-23-103/15/22 18:3513.1 4.5 1
o-Xylene ND ug/kg 03/16/22 04:41 95-47-603/15/22 18:356.5 2.9 1
Surrogates
Toluene-d8 (S)100 %03/16/22 04:41 2037-26-503/15/22 18:3570-130 1
4-Bromofluorobenzene (S)99 %03/16/22 04:41 460-00-403/15/22 18:3569-134 1
1,2-Dichloroethane-d4 (S)86 %03/16/22 04:41 17060-07-003/15/22 18:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.6 %03/15/22 17:48 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.2 %03/18/22 09:1803/18/22 09:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92593450
LSG-001
Sample:SP-DUP Lab ID:92593450002 Collected:03/15/22 00:00 Received:03/15/22 12:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 03/22/22 17:20 18540-29-903/22/22 00:301.20 0.306 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804369
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4269983
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.017 03/21/22 13:380.0076
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4269984LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.450.45 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4269985MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92593450001
4269986
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.524 99 80-12099 2 200.5240.027 0.55 0.54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
804362
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4269954
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.48 03/21/22 17:150.11
Barium mg/kg ND 0.29 03/21/22 17:150.051
Cadmium mg/kg ND 0.077 03/21/22 17:150.030
Chromium mg/kg ND 0.48 03/21/22 17:150.14
Lead mg/kg ND 0.19 03/21/22 17:150.028
Selenium mg/kg ND 0.48 03/21/22 17:150.083
Silver mg/kg ND 0.48 03/22/22 15:560.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4269955LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 45.448.9 93 80-120
Barium mg/kg 44.748.9 91 80-120
Cadmium mg/kg 44.848.9 92 80-120
Chromium mg/kg 45.948.9 94 80-120
Lead mg/kg 46.248.9 95 80-120
Selenium mg/kg 49.248.9 101 80-120
Silver mg/kg 24.024.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4269956MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92593450001
4269957
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 57.3 97 75-12590 11 2055.32.1 57.9 51.9
Barium mg/kg M157.3 165 75-125109 17 2055.3125 219 185
Cadmium mg/kg 57.3 99 75-12594 9 2055.30.056J 56.7 51.9
Chromium mg/kg 57.3 102 75-12593 10 2055.39.6 67.8 61.1
Lead mg/kg 57.3 108 75-12594 13 2055.322.2 84.0 74.0
Selenium mg/kg 57.3 110 75-125101 12 2055.30.30J 63.4 56.0
Silver mg/kg 28.6 99 75-12596 7 2027.7ND 28.4 26.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
684952
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3581868
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/16/22 01:441.9
1,1,1-Trichloroethane ug/kg ND 5.0 03/16/22 01:442.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/16/22 01:441.3
1,1,2-Trichloroethane ug/kg ND 5.0 03/16/22 01:441.7
1,1-Dichloroethane ug/kg ND 5.0 03/16/22 01:442.1
1,1-Dichloroethene ug/kg ND 5.0 03/16/22 01:442.1
1,1-Dichloropropene ug/kg ND 5.0 03/16/22 01:442.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/16/22 01:444.0
1,2,3-Trichloropropane ug/kg ND 5.0 03/16/22 01:442.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/16/22 01:444.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/16/22 01:441.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/16/22 01:441.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/16/22 01:442.2
1,2-Dichlorobenzene ug/kg ND 5.0 03/16/22 01:441.8
1,2-Dichloroethane ug/kg ND 5.0 03/16/22 01:443.3
1,2-Dichloropropane ug/kg ND 5.0 03/16/22 01:441.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/16/22 01:441.7
1,3-Dichlorobenzene ug/kg ND 5.0 03/16/22 01:441.6
1,3-Dichloropropane ug/kg ND 5.0 03/16/22 01:441.6
1,4-Dichlorobenzene ug/kg ND 5.0 03/16/22 01:441.3
2,2-Dichloropropane ug/kg ND 5.0 03/16/22 01:441.6
2-Butanone (MEK)ug/kg ND 100 03/16/22 01:4424.0
2-Chlorotoluene ug/kg ND 5.0 03/16/22 01:441.8
2-Hexanone ug/kg ND 50.0 03/16/22 01:444.8
4-Chlorotoluene ug/kg ND 5.0 03/16/22 01:440.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/16/22 01:444.8
Acetone ug/kg ND 100 03/16/22 01:4432.1
Benzene ug/kg ND 5.0 03/16/22 01:442.0
Bromobenzene ug/kg ND 5.0 03/16/22 01:441.6
Bromochloromethane ug/kg ND 5.0 03/16/22 01:441.5
Bromodichloromethane ug/kg ND 5.0 03/16/22 01:441.9
Bromoform ug/kg ND 5.0 03/16/22 01:441.8
Bromomethane ug/kg ND 10.0 03/16/22 01:447.9
Carbon tetrachloride ug/kg ND 5.0 03/16/22 01:441.9
Chlorobenzene ug/kg ND 5.0 03/16/22 01:440.96
Chloroethane ug/kg ND 10.0 03/16/22 01:443.9
Chloroform ug/kg ND 5.0 03/16/22 01:443.0
Chloromethane ug/kg ND 10.0 03/16/22 01:444.2
cis-1,2-Dichloroethene ug/kg ND 5.0 03/16/22 01:441.7
cis-1,3-Dichloropropene ug/kg ND 5.0 03/16/22 01:441.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3581868
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 03/16/22 01:442.8
Dibromomethane ug/kg ND 5.0 03/16/22 01:441.1
Dichlorodifluoromethane ug/kg ND 10.0 03/16/22 01:442.2
Diisopropyl ether ug/kg ND 5.0 03/16/22 01:441.4
Ethylbenzene ug/kg ND 5.0 03/16/22 01:442.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 03/16/22 01:448.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/16/22 01:441.7
m&p-Xylene ug/kg ND 10.0 03/16/22 01:443.4
Methyl-tert-butyl ether ug/kg ND 5.0 03/16/22 01:441.9
Methylene Chloride ug/kg ND 20.0 03/16/22 01:4413.7
n-Butylbenzene ug/kg ND 5.0 03/16/22 01:442.4
n-Propylbenzene ug/kg ND 5.0 03/16/22 01:441.8
Naphthalene ug/kg ND 5.0 03/16/22 01:442.6
o-Xylene ug/kg ND 5.0 03/16/22 01:442.2
p-Isopropyltoluene ug/kg ND 5.0 03/16/22 01:442.5
sec-Butylbenzene ug/kg ND 5.0 03/16/22 01:442.2
Styrene ug/kg ND 5.0 03/16/22 01:441.3
tert-Butylbenzene ug/kg ND 5.0 03/16/22 01:441.8
Tetrachloroethene ug/kg ND 5.0 03/16/22 01:441.6
Toluene ug/kg ND 5.0 03/16/22 01:441.4
trans-1,2-Dichloroethene ug/kg ND 5.0 03/16/22 01:441.8
trans-1,3-Dichloropropene ug/kg ND 5.0 03/16/22 01:441.7
Trichloroethene ug/kg ND 5.0 03/16/22 01:441.3
Trichlorofluoromethane ug/kg ND 5.0 03/16/22 01:442.8
Vinyl acetate ug/kg ND 50.0 03/16/22 01:443.6
Vinyl chloride ug/kg ND 10.0 03/16/22 01:442.5
Xylene (Total)ug/kg ND 10.0 03/16/22 01:442.8
1,2-Dichloroethane-d4 (S)%94 70-130 03/16/22 01:44
4-Bromofluorobenzene (S)%100 69-134 03/16/22 01:44
Toluene-d8 (S)%99 70-130 03/16/22 01:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581869LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12801250 102 70-130
1,1,1-Trichloroethane ug/kg 13001250 104 70-130
1,1,2,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,2-Trichloroethane ug/kg 12901250 103 70-130
1,1-Dichloroethane ug/kg 13201250 106 70-130
1,1-Dichloroethene ug/kg 13201250 105 70-130
1,1-Dichloropropene ug/kg 13701250 109 70-130
1,2,3-Trichlorobenzene ug/kg 13801250 110 65-130
1,2,3-Trichloropropane ug/kg 12101250 96 70-130
1,2,4-Trichlorobenzene ug/kg 13401250 107 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581869LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13001250 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 11501250 92 70-130
1,2-Dibromoethane (EDB)ug/kg 12301250 98 70-130
1,2-Dichlorobenzene ug/kg 12901250 103 70-130
1,2-Dichloroethane ug/kg 12601250 101 63-130
1,2-Dichloropropane ug/kg 13301250 106 70-130
1,3,5-Trimethylbenzene ug/kg 13101250 105 70-130
1,3-Dichlorobenzene ug/kg 12801250 103 70-130
1,3-Dichloropropane ug/kg 12301250 99 70-130
1,4-Dichlorobenzene ug/kg 12501250 100 70-130
2,2-Dichloropropane ug/kg 13401250 107 66-130
2-Butanone (MEK)ug/kg 23302500 93 70-130
2-Chlorotoluene ug/kg 13301250 106 70-130
2-Hexanone ug/kg 23402500 94 70-130
4-Chlorotoluene ug/kg 12701250 101 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24402500 98 70-130
Acetone ug/kg 21602500 86 69-130
Benzene ug/kg 12601250 101 70-130
Bromobenzene ug/kg 12901250 104 70-130
Bromochloromethane ug/kg 13101250 105 70-130
Bromodichloromethane ug/kg 13101250 105 69-130
Bromoform ug/kg 13001250 104 70-130
Bromomethane ug/kg 14901250 119 52-130
Carbon tetrachloride ug/kg 13401250 108 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 15001250 120 65-130
Chloroform ug/kg 13201250 106 70-130
Chloromethane ug/kg 13301250 106 55-130
cis-1,2-Dichloroethene ug/kg 13401250 107 70-130
cis-1,3-Dichloropropene ug/kg 12901250 103 70-130
Dibromochloromethane ug/kg 11801250 95 70-130
Dibromomethane ug/kg 12601250 101 70-130
Dichlorodifluoromethane ug/kg 13301250 106 45-156
Diisopropyl ether ug/kg 12301250 98 70-130
Ethylbenzene ug/kg 12301250 98 70-130
Hexachloro-1,3-butadiene ug/kg 13201250 105 66-130
Isopropylbenzene (Cumene)ug/kg 13401250 107 70-130
m&p-Xylene ug/kg 25502500 102 70-130
Methyl-tert-butyl ether ug/kg 12401250 100 70-130
Methylene Chloride ug/kg 11801250 95 65-130
n-Butylbenzene ug/kg 13301250 106 67-130
n-Propylbenzene ug/kg 12901250 103 70-130
Naphthalene ug/kg 13001250 104 70-130
o-Xylene ug/kg 12901250 103 70-130
p-Isopropyltoluene ug/kg 13201250 105 67-130
sec-Butylbenzene ug/kg 13001250 104 69-130
Styrene ug/kg 13301250 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581869LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12901250 103 67-130
Tetrachloroethene ug/kg 12401250 99 70-130
Toluene ug/kg 12901250 103 70-130
trans-1,2-Dichloroethene ug/kg 13601250 109 70-130
trans-1,3-Dichloropropene ug/kg 13101250 105 68-130
Trichloroethene ug/kg 12901250 103 70-130
Trichlorofluoromethane ug/kg 12701250 101 70-130
Vinyl acetate ug/kg 25502500 102 70-130
Vinyl chloride ug/kg 14101250 113 61-130
Xylene (Total)ug/kg 38403750 102 70-130
1,2-Dichloroethane-d4 (S)%85 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3581870MATRIX SPIKE SAMPLE:
MSSpike
Result
92593330003
1,1,1,2-Tetrachloroethane ug/kg 502628 80 70-131ND
1,1,1-Trichloroethane ug/kg 526628 84 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 501628 80 66-130ND
1,1,2-Trichloroethane ug/kg 528628 84 66-133ND
1,1-Dichloroethane ug/kg 524628 83 65-130ND
1,1-Dichloroethene ug/kg 528628 84 10-158ND
1,1-Dichloropropene ug/kg 523628 83 68-133ND
1,2,3-Trichlorobenzene ug/kg 487628 77 27-138ND
1,2,3-Trichloropropane ug/kg 475628 76 67-130ND
1,2,4-Trichlorobenzene ug/kg 466628 74 51-134ND
1,2,4-Trimethylbenzene ug/kg 489628 78 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 438628 70 32-130ND
1,2-Dibromoethane (EDB)ug/kg 504628 80 70-130ND
1,2-Dichlorobenzene ug/kg 508628 81 69-130ND
1,2-Dichloroethane ug/kg 498628 79 59-130ND
1,2-Dichloropropane ug/kg 547628 87 70-130ND
1,3,5-Trimethylbenzene ug/kg 496628 79 65-137ND
1,3-Dichlorobenzene ug/kg 487628 77 70-130ND
1,3-Dichloropropane ug/kg 505628 80 70-130ND
1,4-Dichlorobenzene ug/kg 473628 75 68-130ND
2,2-Dichloropropane ug/kg 473628 75 32-130ND
2-Butanone (MEK)ug/kg 8961250 70 10-136ND
2-Chlorotoluene ug/kg 506628 80 69-141ND
2-Hexanone ug/kg 8821250 70 10-144ND
4-Chlorotoluene ug/kg 460628 73 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 9391250 75 25-143ND
Acetone ug/kg 8021250 64 10-130ND
Benzene ug/kg 536628 85 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3581870MATRIX SPIKE SAMPLE:
MSSpike
Result
92593330003
Bromobenzene ug/kg 511628 81 70-130ND
Bromochloromethane ug/kg 515628 82 69-134ND
Bromodichloromethane ug/kg 508628 81 64-130ND
Bromoform ug/kg 456628 73 62-130ND
Bromomethane ug/kg 258628 41 20-176ND
Carbon tetrachloride ug/kg 544628 86 65-140ND
Chlorobenzene ug/kg 509628 81 70-130ND
Chloroethane ug/kg 201628 32 10-130ND
Chloroform ug/kg 531628 84 63-130ND
Chloromethane ug/kg 532628 85 58-130ND
cis-1,2-Dichloroethene ug/kg 535628 85 66-130ND
cis-1,3-Dichloropropene ug/kg 500628 80 67-130ND
Dibromochloromethane ug/kg 437628 69 67-130ND
Dibromomethane ug/kg 526628 84 63-131ND
Dichlorodifluoromethane ug/kg 546628 87 44-180ND
Diisopropyl ether ug/kg 475628 76 63-130ND
Ethylbenzene ug/kg 487628 77 66-130ND
Hexachloro-1,3-butadiene ug/kg 447628 71 64-150ND
Isopropylbenzene (Cumene)ug/kg 542628 86 69-135ND
m&p-Xylene ug/kg 9941250 79 60-133ND
Methyl-tert-butyl ether ug/kg 493628 78 65-130ND
Methylene Chloride ug/kg 447628 71 61-130ND
n-Butylbenzene ug/kg 446628 71 65-140ND
n-Propylbenzene ug/kg 482628 77 67-140ND
Naphthalene ug/kg 469628 75 15-145ND
o-Xylene ug/kg 508628 81 66-133ND
p-Isopropyltoluene ug/kg 485628 77 56-147ND
sec-Butylbenzene ug/kg 505628 80 65-139ND
Styrene ug/kg 506628 80 70-132ND
tert-Butylbenzene ug/kg 506628 80 62-135ND
Tetrachloroethene ug/kg 466628 74 70-135ND
Toluene ug/kg 532628 85 67-130ND
trans-1,2-Dichloroethene ug/kg 521628 83 69-130ND
trans-1,3-Dichloropropene ug/kg 497628 79 62-130ND
Trichloroethene ug/kg 530628 84 70-135ND
Trichlorofluoromethane ug/kg 190628 30 10-130ND
Vinyl acetate ug/kg 9021250 72 53-130ND
Vinyl chloride ug/kg 545628 87 61-148ND
Xylene (Total)ug/kg 15001890 80 63-132ND
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593330004
3581871SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593330004
3581871SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9188
4-Bromofluorobenzene (S)%100101
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
684971
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3581980
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 336 03/16/22 13:11132
1,2-Dichlorobenzene ug/kg ND 336 03/16/22 13:11121
1,3-Dichlorobenzene ug/kg ND 336 03/16/22 13:11119
1,4-Dichlorobenzene ug/kg ND 336 03/16/22 13:11128
1-Methylnaphthalene ug/kg ND 336 03/16/22 13:11118
2,2'-Oxybis(1-chloropropane)ug/kg ND 336 03/16/22 13:11160
2,4,5-Trichlorophenol ug/kg ND 336 03/16/22 13:11154
2,4,6-Trichlorophenol ug/kg ND 336 03/16/22 13:11138
2,4-Dichlorophenol ug/kg ND 336 03/16/22 13:11131
2,4-Dimethylphenol ug/kg ND 336 03/16/22 13:11139
2,4-Dinitrophenol ug/kg ND 1680 03/16/22 13:111040
2,4-Dinitrotoluene ug/kg ND 336 03/16/22 13:11129
2,6-Dinitrotoluene ug/kg ND 336 03/16/22 13:11123
2-Chloronaphthalene ug/kg ND 336 03/16/22 13:11133
2-Chlorophenol ug/kg ND 336 03/16/22 13:11126
2-Methylnaphthalene ug/kg ND 336 03/16/22 13:11134
2-Methylphenol(o-Cresol)ug/kg ND 336 03/16/22 13:11137
2-Nitroaniline ug/kg ND 1680 03/16/22 13:11275
2-Nitrophenol ug/kg ND 336 03/16/22 13:11145
3&4-Methylphenol(m&p Cresol)ug/kg ND 336 03/16/22 13:11135
3,3'-Dichlorobenzidine ug/kg ND 671 IL03/16/22 13:11227
3-Nitroaniline ug/kg ND 1680 IL03/16/22 13:11263
4,6-Dinitro-2-methylphenol ug/kg ND 671 03/16/22 13:11313
4-Bromophenylphenyl ether ug/kg ND 336 03/16/22 13:11129
4-Chloro-3-methylphenol ug/kg ND 671 03/16/22 13:11236
4-Chloroaniline ug/kg ND 671 03/16/22 13:11263
4-Chlorophenylphenyl ether ug/kg ND 336 03/16/22 13:11125
4-Nitroaniline ug/kg ND 671 IL03/16/22 13:11255
4-Nitrophenol ug/kg ND 1680 03/16/22 13:11649
Acenaphthene ug/kg ND 336 03/16/22 13:11118
Acenaphthylene ug/kg ND 336 03/16/22 13:11118
Aniline ug/kg ND 336 03/16/22 13:11131
Anthracene ug/kg ND 336 03/16/22 13:11110
Benzo(a)anthracene ug/kg ND 336 03/16/22 13:11112
Benzo(a)pyrene ug/kg ND 336 03/16/22 13:11116
Benzo(b)fluoranthene ug/kg ND 336 03/16/22 13:11112
Benzo(g,h,i)perylene ug/kg ND 336 03/16/22 13:11130
Benzo(k)fluoranthene ug/kg ND 336 03/16/22 13:11118
Benzoic Acid ug/kg ND 1680 03/16/22 13:11721
Benzyl alcohol ug/kg ND 671 03/16/22 13:11254
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3581980
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 336 03/16/22 13:11139
bis(2-Chloroethyl) ether ug/kg ND 336 03/16/22 13:11126
bis(2-Ethylhexyl)phthalate ug/kg ND 336 03/16/22 13:11130
Butylbenzylphthalate ug/kg ND 336 03/16/22 13:11141
Chrysene ug/kg ND 336 03/16/22 13:11122
Di-n-butylphthalate ug/kg ND 336 03/16/22 13:11113
Di-n-octylphthalate ug/kg ND 336 03/16/22 13:11132
Dibenz(a,h)anthracene ug/kg ND 336 03/16/22 13:11129
Dibenzofuran ug/kg ND 336 03/16/22 13:11121
Diethylphthalate ug/kg ND 336 03/16/22 13:11123
Dimethylphthalate ug/kg ND 336 03/16/22 13:11122
Fluoranthene ug/kg ND 336 03/16/22 13:11115
Fluorene ug/kg ND 336 03/16/22 13:11118
Hexachloro-1,3-butadiene ug/kg ND 336 03/16/22 13:11145
Hexachlorobenzene ug/kg ND 336 03/16/22 13:11131
Hexachlorocyclopentadiene ug/kg ND 336 03/16/22 13:11192
Hexachloroethane ug/kg ND 336 03/16/22 13:11128
Indeno(1,2,3-cd)pyrene ug/kg ND 336 03/16/22 13:11132
Isophorone ug/kg ND 336 03/16/22 13:11149
N-Nitroso-di-n-propylamine ug/kg ND 336 03/16/22 13:11126
N-Nitrosodimethylamine ug/kg ND 336 03/16/22 13:11113
N-Nitrosodiphenylamine ug/kg ND 336 03/16/22 13:11119
Naphthalene ug/kg ND 336 03/16/22 13:11114
Nitrobenzene ug/kg ND 336 03/16/22 13:11156
Pentachlorophenol ug/kg ND 671 03/16/22 13:11328
Phenanthrene ug/kg ND 336 03/16/22 13:11110
Phenol ug/kg ND 336 03/16/22 13:11149
Pyrene ug/kg ND 336 03/16/22 13:11136
Pyridine ug/kg ND 336 03/16/22 13:11106
2,4,6-Tribromophenol (S)%69 18-130 03/16/22 13:11
2-Fluorobiphenyl (S)%62 19-130 03/16/22 13:11
2-Fluorophenol (S)%63 18-130 03/16/22 13:11
Nitrobenzene-d5 (S)%61 21-130 03/16/22 13:11
Phenol-d6 (S)%63 18-130 03/16/22 13:11
Terphenyl-d14 (S)%73 15-130 03/16/22 13:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581981LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12501660 75 47-130
1,2-Dichlorobenzene ug/kg 12301660 74 49-130
1,3-Dichlorobenzene ug/kg 12301660 74 48-130
1,4-Dichlorobenzene ug/kg 12201660 74 49-130
1-Methylnaphthalene ug/kg 13101660 79 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581981LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 11401660 69 38-130
2,4,5-Trichlorophenol ug/kg 13801660 83 49-130
2,4,6-Trichlorophenol ug/kg 14001660 84 50-130
2,4-Dichlorophenol ug/kg 13801660 83 51-130
2,4-Dimethylphenol ug/kg 13301660 80 53-130
2,4-Dinitrophenol ug/kg 66808310 80 39-130
2,4-Dinitrotoluene ug/kg 14001660 84 53-130
2,6-Dinitrotoluene ug/kg 14601660 88 55-130
2-Chloronaphthalene ug/kg 12801660 77 48-130
2-Chlorophenol ug/kg 13101660 79 54-130
2-Methylnaphthalene ug/kg 13101660 79 57-130
2-Methylphenol(o-Cresol)ug/kg 12901660 78 50-130
2-Nitroaniline ug/kg 24003320 72 49-130
2-Nitrophenol ug/kg 14701660 89 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 12901660 78 50-130
3,3'-Dichlorobenzidine ug/kg 2270 IL33206847-130
3-Nitroaniline ug/kg 2380 IL33207245-130
4,6-Dinitro-2-methylphenol ug/kg 26603320 80 50-142
4-Bromophenylphenyl ether ug/kg 14001660 84 55-130
4-Chloro-3-methylphenol ug/kg 26003320 78 52-130
4-Chloroaniline ug/kg 23603320 71 49-130
4-Chlorophenylphenyl ether ug/kg 13301660 80 53-130
4-Nitroaniline ug/kg 2450 IL33207451-130
4-Nitrophenol ug/kg 64708310 78 40-130
Acenaphthene ug/kg 13301660 80 56-130
Acenaphthylene ug/kg 13301660 80 58-130
Aniline ug/kg 11401660 68 44-130
Anthracene ug/kg 12901660 78 60-130
Benzo(a)anthracene ug/kg 13401660 81 59-130
Benzo(a)pyrene ug/kg 14101660 85 57-130
Benzo(b)fluoranthene ug/kg 14301660 86 54-130
Benzo(g,h,i)perylene ug/kg 12401660 75 59-130
Benzo(k)fluoranthene ug/kg 14801660 89 54-130
Benzoic Acid ug/kg 55708310 67 19-130
Benzyl alcohol ug/kg 24703320 74 50-130
bis(2-Chloroethoxy)methane ug/kg 12601660 76 55-130
bis(2-Chloroethyl) ether ug/kg 12201660 73 53-130
bis(2-Ethylhexyl)phthalate ug/kg 13401660 81 58-130
Butylbenzylphthalate ug/kg 14501660 87 46-138
Chrysene ug/kg 13301660 80 57-130
Di-n-butylphthalate ug/kg 13101660 79 57-130
Di-n-octylphthalate ug/kg 14401660 87 57-130
Dibenz(a,h)anthracene ug/kg 12401660 75 60-130
Dibenzofuran ug/kg 13301660 80 54-130
Diethylphthalate ug/kg 13101660 79 55-130
Dimethylphthalate ug/kg 13201660 79 57-130
Fluoranthene ug/kg 13101660 79 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3581981LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13601660 82 56-130
Hexachloro-1,3-butadiene ug/kg 12601660 76 41-130
Hexachlorobenzene ug/kg 13401660 81 53-130
Hexachlorocyclopentadiene ug/kg 12101660 73 23-130
Hexachloroethane ug/kg 12501660 75 48-130
Indeno(1,2,3-cd)pyrene ug/kg 12201660 74 61-130
Isophorone ug/kg 12101660 73 49-130
N-Nitroso-di-n-propylamine ug/kg 11901660 72 52-130
N-Nitrosodimethylamine ug/kg 11001660 66 45-130
N-Nitrosodiphenylamine ug/kg 13101660 79 56-130
Naphthalene ug/kg 12801660 77 56-130
Nitrobenzene ug/kg 12201660 73 50-130
Pentachlorophenol ug/kg 28503320 86 33-130
Phenanthrene ug/kg 13601660 82 60-130
Phenol ug/kg 13801660 83 54-130
Pyrene ug/kg 14501660 88 61-130
Pyridine ug/kg 9221660 56 35-130
2,4,6-Tribromophenol (S)%88 18-130
2-Fluorobiphenyl (S)%74 19-130
2-Fluorophenol (S)%76 18-130
Nitrobenzene-d5 (S)%72 21-130
Phenol-d6 (S)%75 18-130
Terphenyl-d14 (S)%77 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3581982MATRIX SPIKE SAMPLE:
MSSpike
Result
92593209019
1,2,4-Trichlorobenzene ug/kg 16002130 75 22-130ND
1,2-Dichlorobenzene ug/kg 16302130 76 23-130ND
1,3-Dichlorobenzene ug/kg 16302130 76 26-130ND
1,4-Dichlorobenzene ug/kg 16202130 76 27-130ND
1-Methylnaphthalene ug/kg 16302130 77 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 14802130 70 30-130ND
2,4,5-Trichlorophenol ug/kg 16202130 76 26-130ND
2,4,6-Trichlorophenol ug/kg 14002130 66 23-130ND
2,4-Dichlorophenol ug/kg 16502130 77 29-130ND
2,4-Dimethylphenol ug/kg 15902130 75 13-130ND
2,4-Dinitrophenol ug/kg ND M110700010-131ND
2,4-Dinitrotoluene ug/kg 17802130 84 28-130ND
2,6-Dinitrotoluene ug/kg 19002130 89 36-130ND
2-Chloronaphthalene ug/kg 16102130 76 27-130ND
2-Chlorophenol ug/kg 16302130 76 29-130ND
2-Methylnaphthalene ug/kg 16302130 77 29-130ND
2-Methylphenol(o-Cresol)ug/kg 15702130 74 20-130ND
2-Nitroaniline ug/kg 31004260 73 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3581982MATRIX SPIKE SAMPLE:
MSSpike
Result
92593209019
2-Nitrophenol ug/kg 18302130 86 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 16002130 75 10-176ND
3,3'-Dichlorobenzidine ug/kg 2980 IL42607015-130ND
3-Nitroaniline ug/kg 3290 IL42607728-130ND
4,6-Dinitro-2-methylphenol ug/kg 14004260 33 15-132ND
4-Bromophenylphenyl ether ug/kg 16902130 79 35-130ND
4-Chloro-3-methylphenol ug/kg 33104260 78 30-130ND
4-Chloroaniline ug/kg 30704260 72 28-130ND
4-Chlorophenylphenyl ether ug/kg 16002130 75 32-130ND
4-Nitroaniline ug/kg 3190 IL42607530-130ND
4-Nitrophenol ug/kg 356010700 33 17-130ND
Acenaphthene ug/kg 16302130 77 29-130ND
Acenaphthylene ug/kg 16602130 78 31-130ND
Aniline ug/kg 14002130 66 10-130ND
Anthracene ug/kg 15402130 72 33-130ND
Benzo(a)anthracene ug/kg 15602130 73 32-130ND
Benzo(a)pyrene ug/kg 16702130 78 32-130ND
Benzo(b)fluoranthene ug/kg 16902130 79 33-130ND
Benzo(g,h,i)perylene ug/kg 15402130 72 28-130ND
Benzo(k)fluoranthene ug/kg 17502130 82 31-130ND
Benzoic Acid ug/kg ND M110700110-130ND
Benzyl alcohol ug/kg 31504260 74 31-130ND
bis(2-Chloroethoxy)methane ug/kg 16102130 76 30-130ND
bis(2-Chloroethyl) ether ug/kg 15702130 74 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 16302130 76 40-130ND
Butylbenzylphthalate ug/kg 17502130 82 40-130ND
Chrysene ug/kg 15602130 73 30-130ND
Di-n-butylphthalate ug/kg 15402130 72 41-130ND
Di-n-octylphthalate ug/kg 17202130 81 42-130ND
Dibenz(a,h)anthracene ug/kg 15202130 72 27-130ND
Dibenzofuran ug/kg 16202130 76 32-130ND
Diethylphthalate ug/kg 17002130 80 40-130ND
Dimethylphthalate ug/kg 17002130 80 37-130ND
Fluoranthene ug/kg 15302130 72 26-130ND
Fluorene ug/kg 16502130 77 31-130ND
Hexachloro-1,3-butadiene ug/kg 15702130 74 20-130ND
Hexachlorobenzene ug/kg 16302130 77 29-130ND
Hexachlorocyclopentadiene ug/kg 14402130 68 10-130ND
Hexachloroethane ug/kg 15802130 74 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15002130 70 28-130ND
Isophorone ug/kg 15502130 73 32-130ND
N-Nitroso-di-n-propylamine ug/kg 15302130 72 31-130ND
N-Nitrosodimethylamine ug/kg 14202130 66 20-130ND
N-Nitrosodiphenylamine ug/kg 16702130 78 32-130ND
Naphthalene ug/kg 16802130 79 30-130ND
Nitrobenzene ug/kg 16002130 75 25-130ND
Pentachlorophenol ug/kg 20304260 48 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3581982MATRIX SPIKE SAMPLE:
MSSpike
Result
92593209019
Phenanthrene ug/kg 16202130 76 34-130ND
Phenol ug/kg 17002130 80 14-130ND
Pyrene ug/kg 17902130 84 31-130ND
Pyridine ug/kg 12502130 59 10-130ND
2,4,6-Tribromophenol (S)%77 18-130
2-Fluorobiphenyl (S)%63 19-130
2-Fluorophenol (S)%67 18-130
Nitrobenzene-d5 (S)%72 21-130
Phenol-d6 (S)%70 18-130
Terphenyl-d14 (S)%71 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593202001
3581983SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND IL30ND
3-Nitroaniline ug/kg ND IL30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND IL30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593202001
3581983SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%7280
2-Fluorobiphenyl (S)%6068
2-Fluorophenol (S)%6169
Nitrobenzene-d5 (S)%6169
Phenol-d6 (S)%6266
Terphenyl-d14 (S)%5661
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
684935
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593330003
3581699SAMPLE DUPLICATE:
Percent Moisture %16.3 N202516.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92593541001
3581854SAMPLE DUPLICATE:
Percent Moisture %20.4 N212520.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1833856
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3771641-1
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 03/18/22 09:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3771641-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1471647-01
R3771641-3SAMPLE DUPLICATE:
Total Solids %88.1 7.23 1082.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92593450
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1835990
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92593450001, 92593450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3772989-1
Associated Lab Samples:92593450001, 92593450002
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 03/22/22 16:520.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3772989-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.8910.0 98.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3772989-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1472337-01
R3772989-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML,R120.0 3.52 75.0-1254.50 24.4 2020.0ND 0.704 0.899
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3772989-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1472337-01
Chromium, Hexavalent mg/kg 173 ML66126.1 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1472457-02
R3772989-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1472464-04
R3772989-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92593450
LSG-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: L1472337-01
Wet Chemistry by Method 7199 - Sample is a reducer.[1]
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92593450
LSG-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92593450001 804362 804835SP-1 EPA 3050B EPA 6020B
92593450002 804362 804835SP-DUP EPA 3050B EPA 6020B
92593450001 804369 804800SP-1 EPA 7471B EPA 7471B
92593450002 804369 804800SP-DUP EPA 7471B EPA 7471B
92593450001 684971 685143SP-1 EPA 3546 EPA 8270E
92593450002 684971 685143SP-DUP EPA 3546 EPA 8270E
92593450001 684952 685091SP-1 EPA 5035A/5030B EPA 8260D
92593450002 684952 685091SP-DUP EPA 5035A/5030B EPA 8260D
92593450001 684935SP-1 SW-846
92593450002 684935SP-DUP SW-846
92593450001 1833856 1833856SP-1 SM 2540 G SM 2540G
92593450002 1833856 1833856SP-DUP SM 2540 G SM 2540G
92593450001 1835990 1835990SP-1 3060A EPA 7199
92593450002 1835990 1835990SP-DUP 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/23/2022 04:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 39
Page 37 of 39
Page 38 of 39
Page 39 of 39
1
Shannon Cottrill
From:Shannon Cottrill
Sent:Thursday, June 16, 2022 12:04 PM
To:[e-mail]
Subject:Soil Transfer Request - K-Town Furniture - Stadium Lofts Site (22031-18-013) to Reeve's LCID Landfill
(60S-LCID) or Old 27 LCID Landfill (36A-LCID)
Attachments:Data Summary Package (22031-18-013).pdf; Old 27 - Background Soil Samples.pdf; Reeves
Background Soil Sample Data Summary Package (Includes Manganese).pdf
Hi Bill, 

On behalf of Right Field Development, LLC (the PD), Hart & Hickman, PC (H&H) is requesting approval to transfer 
approximately 900 to 1,000 cubic yards (CY) (estimated) of soil from the Stadium Lofts construction site at the K‐Town 
Brownfields Property (22031‐18‐013) to either the Reeve’s Land Clearing Inert Debris (LCID) landfill (60S‐LCID) or the Old 
27 LCID landfill (36A‐LCID).  Soil stockpile sampling activities to characterize the soil were recently completed on June 1, 
2022, in accordance with our DEQ‐approved Environmental Management Plan (EMP).   

The soil proposed to be transported to the LCIDs consists of approximately 900 to 1,000 CYs located in a stockpile 
labeled “Stockpile 1” situated in the northeastern portion of the K‐Town Furniture Brownfields Property (see Figure 2).  

During the soil stockpile sampling event, soils from Stockpile 1 were characterized at a frequency of 1 representative 
sample per 1,000 CY of material.  H&H collected one soil sample (labeled SP‐1) and a duplicate soil sample (labeled DUP‐
1) from Stockpile 1.  Each sample submitted for laboratory analysis included 1 composite sample comprised of 9 to 11 
grab (aliquot) samples which were homogenized to form composite samples and 1 grab sample each representing 1,000 
CY of soil.  Soil sample aliquots were observed for visual and olfactory evidence of impacts and screened for the 
presence of volatile organic vapors with a calibrated photoionization detector.  Soil stockpile samples were placed in 
dedicated laboratory‐supplied sample containers, labeled with the sample identification, date/time, and requested 
analyses, and placed in a laboratory‐supplied cooler with ice.  The collected soil samples were delivered to Pace 
Analytical under standard chain of custody protocols for analysis of volatile organic compounds (VOCs) by EPA Method 
8260, semi‐VOCs (SVOCs) by EPA Method 8270, and RCRA Metals by EPA Method 6020 and 7471 (mercury only), and 
hexavalent chromium (Cr VI) by EPA Method 7199.  Please note that the sample portions for hexavalent chromium were 
shipped from Pace Analytical to SGS’s laboratory in Dayton, NJ for analysis of hexavalent chromium due to a long sample 
analysis turnaround time.  Soil stockpile samples for VOC analysis were collected as grab samples from undisturbed 
portions of the aliquot exhibiting the highest potential for impact based on field screening results.     

The attached data summary package includes a tabular summary of the soil stockpile sample laboratory analytical 
results in comparison to DEQ’s Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated 
January 2022, a Figure 1 showing the site location, a Figure 2 showing the June 2022 sample locations, and copies of the 
laboratory analytical reports.  The data summary package also includes a comparison of the detected compounds in the 
proposed soil to be transferred to the potential LCID receiving sites.  A summary of the soil stockpile sampling results for 
the June 2022 sampling event is provided below.   

As shown in the attached Table 1, the laboratory analytical results for Stockpile 1 indicate that low levels of the VOC 
naphthalene were detected in soil sample SP‐1 and the duplicate sample (DUP‐1) above the laboratory method 
detection limits. In addition, a trace estimated concentration of toluene was detected in soil SP‐1 above the laboratory 
method detection limit.  The low‐level concentrations of naphthalene and trace estimated concentration of toluene are 
below the most stringent Protection of Groundwater PSRGs for each of these compounds. No other VOCs were detected 
above the laboratory method detection limits in the soil stockpile samples.   

2
Several trace estimated concentrations of SVOCs, including benzo(a)anthracene, benzo(b)fluoranthene, chrysene, 
fluoranthene, phenanthrene, and pyrene, were detected above the laboratory method detection limits in the soil 
stockpile samples.  The trace estimated levels of SVOCs are below the most stringent Protection of Groundwater PSRGs 
for each of these compounds. No other SVOCs were detected above the laboratory method detection limits in the soil 
stockpile samples.      

Low levels of arsenic (up to 1.7 mg/kg) and hexavalent chromium (up to 0.84 mg/kg) were detected in the soil stockpile 
samples above the Residential PSRGs of 0.68 mg/kg for arsenic and 0.31 mg/kg for hexavalent chromium.  The detected 
concentrations of arsenic and hexavalent chromium in the soil stockpile samples appear to be consistent with 
background levels and are considered to be naturally occurring.  Several other metals were detected at low 
concentrations above laboratory method detection limits, but these detections appear to be consistent with background 
levels and are likely naturally occurring.      

Comparison of Soil Data 
Of the samples collected from Stockpile 1 on the K‐Town Furniture Brownfields property, no VOCs or SVOCs were 
detected above the Protection of Groundwater, Residential, or Industrial/Commercial PSRGs.  Only arsenic and 
hexavalent chromium were detected above their respective Residential PSRGs in the soil stockpile samples.  The highest 
reported concentrations of arsenic were 1.7 mg/kg and 0.84 mg/kg for hexavalent chromium. These concentrations are 
comparable to the detections of these compounds at the Reeve’s LCID (60S‐LCID) and the Old 27 LCID (36A‐LCID‐2010) 
landfills.  The attached soil comparison table presents the highest concentration for each constituent detected at the K‐
Town Furniture Brownfields Property compared to those detected at the Reeve’s LCID and Old 27 LCID landfills.  

Based on a review of stockpile soil sample analytical results, Right Field Development, LLC is requesting approval to 
transport soils from the above‐referenced stockpiled area to either the Reeve’s or Old 27 LCID landfills.  The PD’s group 
at the K‐Town Furniture property is ready to export the material pending DEQ approval and would like to begin 
exporting as soon as possible.  As such, we would appreciate any consideration you can afford to expedite this review.    

If you have any questions or need additional information, please do not hesitate to contact me. 

Thank you, 
Shannon 

Shannon Cottrill, Senior Project Manager
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 ꞏ Charlotte, NC 28203
Direct: 704- 887-4605 ꞏ Mobile: [phone]
www.harthickman.com   

Table 1 (Page 1 of 1)
Summary of Soil Stockpile Analytical Results (June 2022)
K-Town Furniture (22031-18-013)
Kannapolis, North CarolinaH&H Job No. LSG-001
Export Area
Composite Grab Composite Grab
Date Range Mean
Units
VOCs (8260D)
Naphthalene --0.0101 --0.0114 0.39 2.1 8.8
Toluene --0.0053 J --<0.0017 8.3 990 9,700 ----
SVOCs (8270E)
Benzo(a)anthracene <0.118 --0.145 J --0.35 1.1 21 ----
Benzo(b)fluoranthene 0.141 J --0.161 J --1.2 1.1 21 ----
Chrysene <0.129 --0.137 J --36 110 2,100 ----
Fluoranthene 0.178 J --0.274 J --670 480 6,000 ----
Phenanthrene 0.136 J --0.214 J --NE NE NE ----
Pyrene 0.184 J --0.251 J --440 360 4,500 ----
Metals (6020B/7471B/7199)
Arsenic 1.7 --1.6 --5.8 0.68 3.0 1.0 - 18 4.8
Barium 114 --113 --580 3,100 47,000 50 - 1,000 356
Cadmium 0.055 J --0.055 J --3.0 1.4 20 1.0 - 10 4.3
Chromium (total)9.0 --9.8 --NE NE NE 7.0 - 300 65
Trivalent Chromium 8.16 --9.06 --360,000 23,000 350,000 NS NS
Hexavalent Chromium 0.84 --0.74 --3.8 0.31 6.5 NS NS
Lead 22.4 --27.2 --270 400 800 ND - 50 16
Mercury 0.035 --0.042 --1.0 2.3 9.7 0.03 - 0.52 0.121
Selenium 0.30 J --0.29 J --2.1 78 1,200 <0.1 - 0.8 0.42
Silver <0.15 --<0.15 --3.4 78 1,200 ND - 5.0 NS
Notes:
1) NorthCarolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated January 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.Compound concentrations are reported in milligrams per kilograms (mg/kg).Compound concentrations are reported to the laboratory method detection limits.
Bold indicates concentration exceeds Residential PSRG.
With the exception of metals, only compounds detected in at least one sample are shown.
Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds.J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration.
-- = not applicable; NE = not established; NS = not specified; ND = not detected
milligrams per kilogram (mg/kg)
Sample ID SP-1 DUP-1 Protection of
Groundwater
PSRGs(1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Regional Background Metals in
Soil (2)
6/1/2022
STOCKPILE 1
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Stockpile Sampling/June 2022/K-Town Furniture TablesDate:6/16/2022
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2 (Page 1 of 1)
Comparison of Detected Compounds to Export Sites (June 2022)
K-Town Furniture (22023-18-013)
Kannapolis, North Carolina
H&H Job No. LSG-001
Highest Concentration in
Proposed Export (mg/kg)Export Sample ID
Highest Concentration at
Receiving Site (mg/kg)Receiving Site Sample ID
Highest Concentration at
Receiving Site (mg/kg)Receiving Site Sample ID
Arsenic 5.8 0.68 3.0 1.7 SP-1 3.0 BKG-R-01 2.7 BG-OL27-2
Barium 580 3,100 47,000 114 SP-1 150 BKG-R-05 220 BG-OL27-3
Chromium (Total)NE NE NE 9.8 DUP-1 58 BKG-R-01/BKG-R-05 90 BG-OL27-4
Chromium (III)360,000 23,000 350,000 9.1 DUP-1 57.76 BKG-R-01 90 BG-OL27-4
Chromium (VI)3.8 0.31 6.5 0.84 SP-1 0.43 J BKG-R-04 2.0 BG-OL27-4
Cadmium 3.0 1.4 20 0.055 J SP-1/DUP-1 0.13 J BKG-R-01 <0.051 BG-OL27-4
Lead 270 400 800 27.2 DUP-1 29 BKG-R-04 18 BG-OL27-2
Mercury 1.0 2.3 9.7 0.042 DUP-1 0.097 BKG-R-01 0.074 BG-OL27-4
Selenium 2.1 78 1,200 0.30 J SP-1 6.4 BKG-R-01 4.1 BG-OL27-2
Naphthalene 0.39 2.1 8.8 0.0114 DUP-1 N/A N/A N/A N/A
Toluene 8.3 990 9,700 0.0053 J SP-1 N/A N/A N/A N/A
Benzo(a)anthracene 0.35 1.1 21 0.145 J DUP-1 NA NA NA NA
Benzo(b)fluoranthene 1.2 1.1 21 0.161 J DUP-1 NA N/A NA N/A
Chrysene 36 110 2,100 0.137 J DUP-1 NA N/A NA N/A
Fluoranthene 670 480 6,000 0.274 J DUP-1 NA N/A NA N/A
Phenanthrene NE NE NE 0.214 J DUP-1 N/A N/A N/A N/A
Pyrene 440 360 4,500 0.251 J DUP-1 NA N/A NA N/A
Notes:
1) NC Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Residential Health Based Soil Remediation Goals (PSRGs) dated January 2022. Compound concentrations are reported in milligrams per kilograms (mg/kg).
Bold indicates concentration exceeds Residential PSRGs.Underlined bold indicates concentration exceeds Industrial/Commercial PSRGs.J = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration. ND = non-detect; NA = not analyzed; N/A = not applicable.
2) K-Town Furniture data collected on June 1, 20223) Reeve's LCID data were obtained from Table 2 of the Soil Management Options Letter prepared for NCDEQ by Hart & Hickman, PC on August 7, 2020
4) Old 27 LCID data were obtained from Table 2 of the Background Soil Asssessament Report prepared for NCDEQ by Hart & Hickman, PC on May 11, 2021
Chemical Constituent
NCDEQ Protection of
Groundwater PSRG(1)
(mg/kg)
NCDEQ
Residential PSRG(1)
(mg/kg)
NCDEQIndustrial/Commercial
PSRG(1)
(mg/kg)
K-Town Furniture (22031-18-013)2 Reeve’s LCID (60S-LCID)3 Old 27 LCID (36A-LCID)4
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lansing Melbourne Group (LSG)/LSG-001 Kannapolis NC/Stockpile Sampling/June 2022/K-Town Furniture Tables K-Town Furniture TablesDate: 6/16/2022
Table 2 (Page 1 of 1)
Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.
Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed August, 2021.
SITE LOCATION MAP
K-TOWN FURNITUREBROWNFIELDS PROPERTY
KANNAPOLIS, NORTH CAROLINA
DATE: 2-9-22
JOB NO: LSG-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\LSG-001\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHINA GROVE, CONCORD, ENOCHVILLE AND KANNAPOLIS, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
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VMP-4
SB-15
SB-13
SB-17
SB-16
SB-14
SB-18
SB-18A
SB-18R
SB-13RSB-14R
SB-15R
SB-16R
SB-17R
FORMER GAS STATION
(400 W. A STREET)
FORMER AUTO REPAIR SHOPS (DEMOLISHED)
(136-138 OAK AVENUE)
FORMER WATER VAULT
FORMER STAR CLEANERS (DEMOLISHED)
(108 WEST AVENUE)
FORMER PURITAN/ BOB'S LAUNDRY &
DRY CLEANERS (DEMOLISHED)
(311 WEST A STREET)
W.
A

S
T
R
E
E
T
W.
B

S
T
R
E
E
T
OAK AVENUEWELLNESS WAY
CHES
T
N
U
T

A
V
E
N
U
E
LA
U
R
E
A
T
E

W
A
Y
BURIED TIMBER PILINGS
FORMER WRENN'S CLEANERS (DEMOLISHED)
(136 WEST AVENUE)
REVISION NO. 0
JOB NO. LSG-001
DATE: 6-16-22
FIGURE NO. 2
K-TOWN FURNITURE
BROWNFIELDS PROPERTY
KANNAPOLIS, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS SITE PROPERTY
BOUNDARY
PARCEL BOUNDARY
FORMER BUILDING OUTLINE
TEMPORARY MONITORING WELL
LOCATION (JANUARY 2018)
TEMPORARY MONITORING WELL/ SOIL
BORING LOCATION (JANUARY 2018)
SOIL BORING LOCATION
(JANUARY-MARCH 2018)
SOIL BORING LOCATION
(AUGUST 2018)
SOIL VAPOR SAMPLE LOCATION
(AUGUST 2018)
SOIL VAPOR SAMPLE LOCATION
(FEBRUARY 2022)
STOCKPILE SOIL ALIQUOT SAMPLE
LOCATION (JUNE 2022)
APPROXIMATE AREA SUBJECT TO
PREVIOUS BROWNFIELDS
AGREEMENT FOR NC RESEARCH
CAMPUS (INCLUDING WATER VAULT)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1. PARCEL BOUNDARY DATA OBTAINED FROM
CABARRUS COUNTY GIS, 2022. AERIAL IMAGERY
OBTAINED FROM GOOGLE EARTH PRO, 2021.
2. PREVIOUS SAMPLE LOCATIONS FROM H&H FIGURE
NOS. 5 AND 6.
VMP-5
VMP-14
VMP-13
VMP-12
VMP-11
VMP-9
VMP-8
VMP-7
VMP-10
VMP-6
STADIUM LOFTS
(UNDER CONSTRUCTION)
STOCKPILE 1
(APPROX. 900 - 1,000 CUBIC YARDS)S:\AAA-Master Projects\Lansing Melbourne Group (LSG)\LSG-001 Kannapolis NC\Figures\Site Map.dwg, FIG 2 Sample Location, 6/16/2022 8:19:13 AM, shaynes
#=CL#
June 09, 2022
LIMS USE: FR - SHANNON COTTRILL
LIMS OBJECT ID: 92607324
92607324
Project:
Pace Project No.:
RE:
Mr. Shannon Cottrill
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
LSG-001
Dear Mr. Cottrill:
Enclosed are the analytical results for sample(s) received by the laboratory on June 01, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92607324
LSG-001
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A2LA Certification #: 2926.01*
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563*
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 34
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92607324
LSG-001
Lab ID Sample ID Matrix Date Collected Date Received
92607324001 SP-1 Solid 06/01/22 09:45 06/01/22 11:40
92607324002 DUP-1 Solid 06/01/22 00:00 06/01/22 11:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92607324
LSG-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92607324001 SP-1 EPA 6020B 7 PASI-MWBS
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607324002 DUP-1 EPA 6020B 7 PASI-MWBS
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:SP-1 Lab ID:92607324001 Collected:06/01/22 09:45 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.7 mg/kg 06/08/22 20:12 7440-38-206/06/22 11:560.53 0.12 1
Barium 114 mg/kg 06/08/22 20:12 7440-39-306/06/22 11:560.32 0.057 1
Cadmium 0.055J mg/kg 06/08/22 20:12 7440-43-906/06/22 11:560.085 0.033 1
Chromium 9.0 mg/kg 06/08/22 20:12 7440-47-306/06/22 11:562.1 0.15 1
Lead 22.4 mg/kg 06/08/22 20:12 7439-92-106/06/22 11:560.53 0.031 1
Selenium 0.30J mg/kg 06/08/22 20:12 7782-49-206/06/22 11:560.53 0.091 1
Silver ND mg/kg 06/08/22 20:12 7440-22-406/06/22 11:560.53 0.15 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.035 mg/kg 06/08/22 13:41 7439-97-606/06/22 12:000.020 0.0086 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/07/22 12:57 83-32-906/03/22 16:103551251
Acenaphthylene ND ug/kg 06/07/22 12:57 208-96-806/03/22 16:103551251
Aniline ND ug/kg 06/07/22 12:57 62-53-306/03/22 16:103551391
Anthracene ND ug/kg 06/07/22 12:57 120-12-706/03/22 16:103551161
Benzo(a)anthracene ND ug/kg 06/07/22 12:57 56-55-306/03/22 16:103551181
Benzo(a)pyrene ND ug/kg 06/07/22 12:57 50-32-806/03/22 16:103551231
Benzo(b)fluoranthene 141J ug/kg 06/07/22 12:57 205-99-206/03/22 16:103551181
Benzo(g,h,i)perylene ND ug/kg 06/07/22 12:57 191-24-206/03/22 16:103551381
Benzo(k)fluoranthene ND ug/kg 06/07/22 12:57 207-08-906/03/22 16:103551251
Benzoic Acid ND ug/kg 06/07/22 12:57 65-85-006/03/22 16:1017807641
Benzyl alcohol ND ug/kg 06/07/22 12:57 100-51-6 v206/03/22 16:107112691
4-Bromophenylphenyl ether ND ug/kg 06/07/22 12:57 101-55-306/03/22 16:103551371
Butylbenzylphthalate ND ug/kg 06/07/22 12:57 85-68-706/03/22 16:103551501
4-Chloro-3-methylphenol ND ug/kg 06/07/22 12:57 59-50-706/03/22 16:107112501
4-Chloroaniline ND ug/kg 06/07/22 12:57 106-47-806/03/22 16:107112791
bis(2-Chloroethoxy)methane ND ug/kg 06/07/22 12:57 111-91-106/03/22 16:103551481
bis(2-Chloroethyl) ether ND ug/kg 06/07/22 12:57 111-44-406/03/22 16:103551341
2-Chloronaphthalene ND ug/kg 06/07/22 12:57 91-58-706/03/22 16:103551411
2-Chlorophenol ND ug/kg 06/07/22 12:57 95-57-806/03/22 16:103551341
4-Chlorophenylphenyl ether ND ug/kg 06/07/22 12:57 7005-72-306/03/22 16:103551321
Chrysene ND ug/kg 06/07/22 12:57 218-01-906/03/22 16:103551291
Dibenz(a,h)anthracene ND ug/kg 06/07/22 12:57 53-70-306/03/22 16:103551371
Dibenzofuran ND ug/kg 06/07/22 12:57 132-64-906/03/22 16:103551281
1,2-Dichlorobenzene ND ug/kg 06/07/22 12:57 95-50-106/03/22 16:103551281
1,3-Dichlorobenzene ND ug/kg 06/07/22 12:57 541-73-106/03/22 16:103551261
1,4-Dichlorobenzene ND ug/kg 06/07/22 12:57 106-46-706/03/22 16:103551361
3,3'-Dichlorobenzidine ND ug/kg 06/07/22 12:57 91-94-1 IL06/03/22 16:107112401
2,4-Dichlorophenol ND ug/kg 06/07/22 12:57 120-83-206/03/22 16:103551391
Diethylphthalate ND ug/kg 06/07/22 12:57 84-66-206/03/22 16:103551301
2,4-Dimethylphenol ND ug/kg 06/07/22 12:57 105-67-906/03/22 16:103551481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:SP-1 Lab ID:92607324001 Collected:06/01/22 09:45 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/07/22 12:57 131-11-306/03/22 16:103551291
Di-n-butylphthalate ND ug/kg 06/07/22 12:57 84-74-206/03/22 16:103551201
4,6-Dinitro-2-methylphenol ND ug/kg 06/07/22 12:57 534-52-106/03/22 16:107113321
2,4-Dinitrophenol ND ug/kg 06/07/22 12:57 51-28-506/03/22 16:10178011001
2,4-Dinitrotoluene ND ug/kg 06/07/22 12:57 121-14-206/03/22 16:103551371
2,6-Dinitrotoluene ND ug/kg 06/07/22 12:57 606-20-206/03/22 16:103551301
Di-n-octylphthalate ND ug/kg 06/07/22 12:57 117-84-006/03/22 16:103551401
bis(2-Ethylhexyl)phthalate ND ug/kg 06/07/22 12:57 117-81-706/03/22 16:103551381
Fluoranthene 178J ug/kg 06/07/22 12:57 206-44-006/03/22 16:103551221
Fluorene ND ug/kg 06/07/22 12:57 86-73-706/03/22 16:103551251
Hexachloro-1,3-butadiene ND ug/kg 06/07/22 12:57 87-68-306/03/22 16:103551541
Hexachlorobenzene ND ug/kg 06/07/22 12:57 118-74-106/03/22 16:103551391
Hexachlorocyclopentadiene ND ug/kg 06/07/22 12:57 77-47-406/03/22 16:103552041
Hexachloroethane ND ug/kg 06/07/22 12:57 67-72-106/03/22 16:103551361
Indeno(1,2,3-cd)pyrene ND ug/kg 06/07/22 12:57 193-39-506/03/22 16:103551401
Isophorone ND ug/kg 06/07/22 12:57 78-59-106/03/22 16:103551581
1-Methylnaphthalene ND ug/kg 06/07/22 12:57 90-12-006/03/22 16:103551251
2-Methylnaphthalene ND ug/kg 06/07/22 12:57 91-57-606/03/22 16:103551421
2-Methylphenol(o-Cresol)ND ug/kg 06/07/22 12:57 95-48-706/03/22 16:103551451
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/07/22 12:57 15831-10-4 v206/03/22 16:103551431
Naphthalene ND ug/kg 06/07/22 12:57 91-20-306/03/22 16:103551211
2-Nitroaniline ND ug/kg 06/07/22 12:57 88-74-406/03/22 16:1017802911
3-Nitroaniline ND ug/kg 06/07/22 12:57 99-09-2 IL06/03/22 16:1017802791
4-Nitroaniline ND ug/kg 06/07/22 12:57 100-01-6 IL06/03/22 16:107112701
Nitrobenzene ND ug/kg 06/07/22 12:57 98-95-306/03/22 16:103551651
2-Nitrophenol ND ug/kg 06/07/22 12:57 88-75-506/03/22 16:103551541
4-Nitrophenol ND ug/kg 06/07/22 12:57 100-02-7 v206/03/22 16:1017806871
N-Nitrosodimethylamine ND ug/kg 06/07/22 12:57 62-75-9 L206/03/22 16:103551201
N-Nitroso-di-n-propylamine ND ug/kg 06/07/22 12:57 621-64-7 v206/03/22 16:103551341
N-Nitrosodiphenylamine ND ug/kg 06/07/22 12:57 86-30-606/03/22 16:103551261
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/07/22 12:57 108-60-1 v106/03/22 16:103551691
Pentachlorophenol ND ug/kg 06/07/22 12:57 87-86-506/03/22 16:107113481
Phenanthrene 136J ug/kg 06/07/22 12:57 85-01-806/03/22 16:103551161
Phenol ND ug/kg 06/07/22 12:57 108-95-206/03/22 16:103551581
Pyrene 184J ug/kg 06/07/22 12:57 129-00-006/03/22 16:103551441
Pyridine ND ug/kg 06/07/22 12:57 110-86-106/03/22 16:103551121
1,2,4-Trichlorobenzene ND ug/kg 06/07/22 12:57 120-82-106/03/22 16:103551401
2,4,5-Trichlorophenol ND ug/kg 06/07/22 12:57 95-95-406/03/22 16:103551631
2,4,6-Trichlorophenol ND ug/kg 06/07/22 12:57 88-06-206/03/22 16:103551461
Surrogates
Nitrobenzene-d5 (S)47 %06/07/22 12:57 4165-60-006/03/22 16:1021-130 1
2-Fluorobiphenyl (S)49 %06/07/22 12:57 321-60-806/03/22 16:1019-130 1
Terphenyl-d14 (S)58 %06/07/22 12:57 1718-51-006/03/22 16:1015-130 1
Phenol-d6 (S)46 %06/07/22 12:57 13127-88-306/03/22 16:1018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:SP-1 Lab ID:92607324001 Collected:06/01/22 09:45 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)45 %06/07/22 12:57 367-12-406/03/22 16:1018-130 1
2,4,6-Tribromophenol (S)59 %06/07/22 12:57 118-79-606/03/22 16:1018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 12:32 67-64-106/02/22 18:5010834.7 1
Benzene ND ug/kg 06/03/22 12:32 71-43-206/02/22 18:505.4 2.2 1
Bromobenzene ND ug/kg 06/03/22 12:32 108-86-106/02/22 18:505.4 1.8 1
Bromochloromethane ND ug/kg 06/03/22 12:32 74-97-506/02/22 18:505.4 1.6 1
Bromodichloromethane ND ug/kg 06/03/22 12:32 75-27-406/02/22 18:505.4 2.1 1
Bromoform ND ug/kg 06/03/22 12:32 75-25-206/02/22 18:505.4 1.9 1
Bromomethane ND ug/kg 06/03/22 12:32 74-83-9 IK06/02/22 18:5010.8 8.5 1
2-Butanone (MEK)ND ug/kg 06/03/22 12:32 78-93-306/02/22 18:5010825.9 1
n-Butylbenzene ND ug/kg 06/03/22 12:32 104-51-806/02/22 18:505.4 2.6 1
sec-Butylbenzene ND ug/kg 06/03/22 12:32 135-98-806/02/22 18:505.4 2.4 1
tert-Butylbenzene ND ug/kg 06/03/22 12:32 98-06-606/02/22 18:505.4 1.9 1
Carbon tetrachloride ND ug/kg 06/03/22 12:32 56-23-506/02/22 18:505.4 2.0 1
Chlorobenzene ND ug/kg 06/03/22 12:32 108-90-706/02/22 18:505.4 1.0 1
Chloroethane ND ug/kg 06/03/22 12:32 75-00-306/02/22 18:5010.8 4.2 1
Chloroform ND ug/kg 06/03/22 12:32 67-66-306/02/22 18:505.4 3.3 1
Chloromethane ND ug/kg 06/03/22 12:32 74-87-306/02/22 18:5010.8 4.5 1
2-Chlorotoluene ND ug/kg 06/03/22 12:32 95-49-806/02/22 18:505.4 1.9 1
4-Chlorotoluene ND ug/kg 06/03/22 12:32 106-43-406/02/22 18:505.4 0.96 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 12:32 96-12-806/02/22 18:505.4 2.1 1
Dibromochloromethane ND ug/kg 06/03/22 12:32 124-48-106/02/22 18:505.4 3.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 12:32 106-93-406/02/22 18:505.4 2.4 1
Dibromomethane ND ug/kg 06/03/22 12:32 74-95-306/02/22 18:505.4 1.2 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 12:32 95-50-106/02/22 18:505.4 1.9 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 12:32 541-73-106/02/22 18:505.4 1.7 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 12:32 106-46-706/02/22 18:505.4 1.4 1
Dichlorodifluoromethane ND ug/kg 06/03/22 12:32 75-71-8 v106/02/22 18:5010.8 2.3 1
1,1-Dichloroethane ND ug/kg 06/03/22 12:32 75-34-306/02/22 18:505.4 2.2 1
1,2-Dichloroethane ND ug/kg 06/03/22 12:32 107-06-206/02/22 18:505.4 3.6 1
1,1-Dichloroethene ND ug/kg 06/03/22 12:32 75-35-406/02/22 18:505.4 2.2 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 12:32 156-59-206/02/22 18:505.4 1.8 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 12:32 156-60-506/02/22 18:505.4 1.9 1
1,2-Dichloropropane ND ug/kg 06/03/22 12:32 78-87-506/02/22 18:505.4 1.6 1
1,3-Dichloropropane ND ug/kg 06/03/22 12:32 142-28-906/02/22 18:505.4 1.7 1
2,2-Dichloropropane ND ug/kg 06/03/22 12:32 594-20-706/02/22 18:505.4 1.8 1
1,1-Dichloropropene ND ug/kg 06/03/22 12:32 563-58-606/02/22 18:505.4 2.6 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 12:32 10061-01-506/02/22 18:505.4 1.5 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 12:32 10061-02-606/02/22 18:505.4 1.9 1
Diisopropyl ether ND ug/kg 06/03/22 12:32 108-20-306/02/22 18:505.4 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:SP-1 Lab ID:92607324001 Collected:06/01/22 09:45 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/03/22 12:32 100-41-406/02/22 18:505.4 2.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 12:32 87-68-306/02/22 18:5010.8 8.8 1
2-Hexanone ND ug/kg 06/03/22 12:32 591-78-606/02/22 18:5054.0 5.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 12:32 98-82-806/02/22 18:505.4 1.8 1
p-Isopropyltoluene ND ug/kg 06/03/22 12:32 99-87-606/02/22 18:505.4 2.7 1
Methylene Chloride ND ug/kg 06/03/22 12:32 75-09-206/02/22 18:5021.6 14.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 12:32 108-10-106/02/22 18:5054.0 5.2 1
Methyl-tert-butyl ether ND ug/kg 06/03/22 12:32 1634-04-406/02/22 18:505.4 2.0 1
Naphthalene 10.1 ug/kg 06/03/22 12:32 91-20-306/02/22 18:505.4 2.8 1
n-Propylbenzene ND ug/kg 06/03/22 12:32 103-65-106/02/22 18:505.4 1.9 1
Styrene ND ug/kg 06/03/22 12:32 100-42-506/02/22 18:505.4 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 12:32 630-20-606/02/22 18:505.4 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 12:32 79-34-506/02/22 18:505.4 1.4 1
Tetrachloroethene ND ug/kg 06/03/22 12:32 127-18-406/02/22 18:505.4 1.7 1
Toluene 5.3J ug/kg 06/03/22 12:32 108-88-306/02/22 18:505.4 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 12:32 87-61-606/02/22 18:505.4 4.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 12:32 120-82-106/02/22 18:505.4 4.5 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 12:32 71-55-606/02/22 18:505.4 2.8 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 12:32 79-00-506/02/22 18:505.4 1.8 1
Trichloroethene ND ug/kg 06/03/22 12:32 79-01-606/02/22 18:505.4 1.4 1
Trichlorofluoromethane ND ug/kg 06/03/22 12:32 75-69-406/02/22 18:505.4 3.0 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 12:32 96-18-406/02/22 18:505.4 2.7 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 12:32 95-63-606/02/22 18:505.4 1.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 12:32 108-67-806/02/22 18:505.4 1.8 1
Vinyl acetate ND ug/kg 06/03/22 12:32 108-05-406/02/22 18:5054.0 3.9 1
Vinyl chloride ND ug/kg 06/03/22 12:32 75-01-4 v106/02/22 18:5010.8 2.7 1
Xylene (Total)ND ug/kg 06/03/22 12:32 1330-20-706/02/22 18:5010.8 3.1 1
m&p-Xylene ND ug/kg 06/03/22 12:32 179601-23-106/02/22 18:5010.8 3.7 1
o-Xylene ND ug/kg 06/03/22 12:32 95-47-606/02/22 18:505.4 2.4 1
Surrogates
Toluene-d8 (S)100 %06/03/22 12:32 2037-26-506/02/22 18:5070-130 1
4-Bromofluorobenzene (S)98 %06/03/22 12:32 460-00-406/02/22 18:5069-134 1
1,2-Dichloroethane-d4 (S)97 %06/03/22 12:32 17060-07-006/02/22 18:5070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.2 %06/03/22 16:08 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:DUP-1 Lab ID:92607324002 Collected:06/01/22 00:00 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.6 mg/kg 06/08/22 20:15 7440-38-206/06/22 11:560.52 0.11 1
Barium 113 mg/kg 06/08/22 20:15 7440-39-306/06/22 11:560.31 0.056 1
Cadmium 0.055J mg/kg 06/08/22 20:15 7440-43-906/06/22 11:560.084 0.033 1
Chromium 9.8 mg/kg 06/08/22 20:15 7440-47-306/06/22 11:562.1 0.15 1
Lead 27.2 mg/kg 06/08/22 20:15 7439-92-106/06/22 11:560.52 0.031 1
Selenium 0.29J mg/kg 06/08/22 20:15 7782-49-206/06/22 11:560.52 0.090 1
Silver ND mg/kg 06/08/22 20:15 7440-22-406/06/22 11:560.52 0.15 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.042 mg/kg 06/08/22 13:43 7439-97-606/06/22 12:000.020 0.0085 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/07/22 15:13 83-32-906/03/22 16:103581261
Acenaphthylene ND ug/kg 06/07/22 15:13 208-96-806/03/22 16:103581261
Aniline ND ug/kg 06/07/22 15:13 62-53-306/03/22 16:103581401
Anthracene ND ug/kg 06/07/22 15:13 120-12-706/03/22 16:103581171
Benzo(a)anthracene 145J ug/kg 06/07/22 15:13 56-55-306/03/22 16:103581191
Benzo(a)pyrene ND ug/kg 06/07/22 15:13 50-32-806/03/22 16:103581241
Benzo(b)fluoranthene 161J ug/kg 06/07/22 15:13 205-99-206/03/22 16:103581191
Benzo(g,h,i)perylene ND ug/kg 06/07/22 15:13 191-24-206/03/22 16:103581391
Benzo(k)fluoranthene ND ug/kg 06/07/22 15:13 207-08-906/03/22 16:103581261
Benzoic Acid ND ug/kg 06/07/22 15:13 65-85-006/03/22 16:1017907681
Benzyl alcohol ND ug/kg 06/07/22 15:13 100-51-606/03/22 16:107152711
4-Bromophenylphenyl ether ND ug/kg 06/07/22 15:13 101-55-306/03/22 16:103581381
Butylbenzylphthalate ND ug/kg 06/07/22 15:13 85-68-706/03/22 16:103581511
4-Chloro-3-methylphenol ND ug/kg 06/07/22 15:13 59-50-706/03/22 16:107152511
4-Chloroaniline ND ug/kg 06/07/22 15:13 106-47-8 IL06/03/22 16:107152811
bis(2-Chloroethoxy)methane ND ug/kg 06/07/22 15:13 111-91-106/03/22 16:103581481
bis(2-Chloroethyl) ether ND ug/kg 06/07/22 15:13 111-44-406/03/22 16:103581341
2-Chloronaphthalene ND ug/kg 06/07/22 15:13 91-58-706/03/22 16:103581421
2-Chlorophenol ND ug/kg 06/07/22 15:13 95-57-806/03/22 16:103581341
4-Chlorophenylphenyl ether ND ug/kg 06/07/22 15:13 7005-72-306/03/22 16:103581331
Chrysene 137J ug/kg 06/07/22 15:13 218-01-906/03/22 16:103581301
Dibenz(a,h)anthracene ND ug/kg 06/07/22 15:13 53-70-306/03/22 16:103581381
Dibenzofuran ND ug/kg 06/07/22 15:13 132-64-906/03/22 16:103581291
1,2-Dichlorobenzene ND ug/kg 06/07/22 15:13 95-50-106/03/22 16:103581291
1,3-Dichlorobenzene ND ug/kg 06/07/22 15:13 541-73-106/03/22 16:103581271
1,4-Dichlorobenzene ND ug/kg 06/07/22 15:13 106-46-706/03/22 16:103581371
3,3'-Dichlorobenzidine ND ug/kg 06/07/22 15:13 91-94-1 IL06/03/22 16:107152421
2,4-Dichlorophenol ND ug/kg 06/07/22 15:13 120-83-206/03/22 16:103581401
Diethylphthalate ND ug/kg 06/07/22 15:13 84-66-206/03/22 16:103581311
2,4-Dimethylphenol ND ug/kg 06/07/22 15:13 105-67-906/03/22 16:103581481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:DUP-1 Lab ID:92607324002 Collected:06/01/22 00:00 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/07/22 15:13 131-11-306/03/22 16:103581301
Di-n-butylphthalate ND ug/kg 06/07/22 15:13 84-74-206/03/22 16:103581201
4,6-Dinitro-2-methylphenol ND ug/kg 06/07/22 15:13 534-52-106/03/22 16:107153341
2,4-Dinitrophenol ND ug/kg 06/07/22 15:13 51-28-506/03/22 16:10179011101
2,4-Dinitrotoluene ND ug/kg 06/07/22 15:13 121-14-206/03/22 16:103581381
2,6-Dinitrotoluene ND ug/kg 06/07/22 15:13 606-20-206/03/22 16:103581311
Di-n-octylphthalate ND ug/kg 06/07/22 15:13 117-84-0 v106/03/22 16:103581411
bis(2-Ethylhexyl)phthalate ND ug/kg 06/07/22 15:13 117-81-706/03/22 16:103581391
Fluoranthene 274J ug/kg 06/07/22 15:13 206-44-006/03/22 16:103581221
Fluorene ND ug/kg 06/07/22 15:13 86-73-706/03/22 16:103581261
Hexachloro-1,3-butadiene ND ug/kg 06/07/22 15:13 87-68-306/03/22 16:103581551
Hexachlorobenzene ND ug/kg 06/07/22 15:13 118-74-106/03/22 16:103581401
Hexachlorocyclopentadiene ND ug/kg 06/07/22 15:13 77-47-4 v206/03/22 16:103582051
Hexachloroethane ND ug/kg 06/07/22 15:13 67-72-106/03/22 16:103581371
Indeno(1,2,3-cd)pyrene ND ug/kg 06/07/22 15:13 193-39-506/03/22 16:103581411
Isophorone ND ug/kg 06/07/22 15:13 78-59-106/03/22 16:103581591
1-Methylnaphthalene ND ug/kg 06/07/22 15:13 90-12-006/03/22 16:103581261
2-Methylnaphthalene ND ug/kg 06/07/22 15:13 91-57-606/03/22 16:103581431
2-Methylphenol(o-Cresol)ND ug/kg 06/07/22 15:13 95-48-706/03/22 16:103581461
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/07/22 15:13 15831-10-406/03/22 16:103581441
Naphthalene ND ug/kg 06/07/22 15:13 91-20-306/03/22 16:103581211
2-Nitroaniline ND ug/kg 06/07/22 15:13 88-74-406/03/22 16:1017902931
3-Nitroaniline ND ug/kg 06/07/22 15:13 99-09-2 IL06/03/22 16:1017902811
4-Nitroaniline ND ug/kg 06/07/22 15:13 100-01-606/03/22 16:107152721
Nitrobenzene ND ug/kg 06/07/22 15:13 98-95-306/03/22 16:103581661
2-Nitrophenol ND ug/kg 06/07/22 15:13 88-75-5 v106/03/22 16:103581551
4-Nitrophenol ND ug/kg 06/07/22 15:13 100-02-706/03/22 16:1017906911
N-Nitrosodimethylamine ND ug/kg 06/07/22 15:13 62-75-9 L206/03/22 16:103581201
N-Nitroso-di-n-propylamine ND ug/kg 06/07/22 15:13 621-64-706/03/22 16:103581341
N-Nitrosodiphenylamine ND ug/kg 06/07/22 15:13 86-30-606/03/22 16:103581271
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/07/22 15:13 108-60-106/03/22 16:103581701
Pentachlorophenol ND ug/kg 06/07/22 15:13 87-86-506/03/22 16:107153501
Phenanthrene 214J ug/kg 06/07/22 15:13 85-01-806/03/22 16:103581171
Phenol ND ug/kg 06/07/22 15:13 108-95-206/03/22 16:103581591
Pyrene 251J ug/kg 06/07/22 15:13 129-00-006/03/22 16:103581451
Pyridine ND ug/kg 06/07/22 15:13 110-86-106/03/22 16:103581131
1,2,4-Trichlorobenzene ND ug/kg 06/07/22 15:13 120-82-106/03/22 16:103581411
2,4,5-Trichlorophenol ND ug/kg 06/07/22 15:13 95-95-406/03/22 16:103581641
2,4,6-Trichlorophenol ND ug/kg 06/07/22 15:13 88-06-206/03/22 16:103581471
Surrogates
Nitrobenzene-d5 (S)44 %06/07/22 15:13 4165-60-006/03/22 16:1021-130 1
2-Fluorobiphenyl (S)45 %06/07/22 15:13 321-60-806/03/22 16:1019-130 1
Terphenyl-d14 (S)66 %06/07/22 15:13 1718-51-006/03/22 16:1015-130 1
Phenol-d6 (S)52 %06/07/22 15:13 13127-88-306/03/22 16:1018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:DUP-1 Lab ID:92607324002 Collected:06/01/22 00:00 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)47 %06/07/22 15:13 367-12-406/03/22 16:1018-130 1
2,4,6-Tribromophenol (S)56 %06/07/22 15:13 118-79-606/03/22 16:1018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 12:51 67-64-106/02/22 18:5012138.8 1
Benzene ND ug/kg 06/03/22 12:51 71-43-206/02/22 18:506.0 2.4 1
Bromobenzene ND ug/kg 06/03/22 12:51 108-86-106/02/22 18:506.0 2.0 1
Bromochloromethane ND ug/kg 06/03/22 12:51 74-97-506/02/22 18:506.0 1.8 1
Bromodichloromethane ND ug/kg 06/03/22 12:51 75-27-406/02/22 18:506.0 2.3 1
Bromoform ND ug/kg 06/03/22 12:51 75-25-206/02/22 18:506.0 2.1 1
Bromomethane ND ug/kg 06/03/22 12:51 74-83-9 IK06/02/22 18:5012.1 9.5 1
2-Butanone (MEK)ND ug/kg 06/03/22 12:51 78-93-306/02/22 18:5012129.0 1
n-Butylbenzene ND ug/kg 06/03/22 12:51 104-51-806/02/22 18:506.0 2.8 1
sec-Butylbenzene ND ug/kg 06/03/22 12:51 135-98-806/02/22 18:506.0 2.7 1
tert-Butylbenzene ND ug/kg 06/03/22 12:51 98-06-606/02/22 18:506.0 2.1 1
Carbon tetrachloride ND ug/kg 06/03/22 12:51 56-23-506/02/22 18:506.0 2.3 1
Chlorobenzene ND ug/kg 06/03/22 12:51 108-90-706/02/22 18:506.0 1.2 1
Chloroethane ND ug/kg 06/03/22 12:51 75-00-306/02/22 18:5012.1 4.7 1
Chloroform ND ug/kg 06/03/22 12:51 67-66-306/02/22 18:506.0 3.7 1
Chloromethane ND ug/kg 06/03/22 12:51 74-87-306/02/22 18:5012.1 5.1 1
2-Chlorotoluene ND ug/kg 06/03/22 12:51 95-49-806/02/22 18:506.0 2.1 1
4-Chlorotoluene ND ug/kg 06/03/22 12:51 106-43-406/02/22 18:506.0 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 12:51 96-12-806/02/22 18:506.0 2.3 1
Dibromochloromethane ND ug/kg 06/03/22 12:51 124-48-106/02/22 18:506.0 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 12:51 106-93-406/02/22 18:506.0 2.7 1
Dibromomethane ND ug/kg 06/03/22 12:51 74-95-306/02/22 18:506.0 1.3 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 12:51 95-50-106/02/22 18:506.0 2.2 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 12:51 541-73-106/02/22 18:506.0 1.9 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 12:51 106-46-706/02/22 18:506.0 1.6 1
Dichlorodifluoromethane ND ug/kg 06/03/22 12:51 75-71-8 v106/02/22 18:5012.1 2.6 1
1,1-Dichloroethane ND ug/kg 06/03/22 12:51 75-34-306/02/22 18:506.0 2.5 1
1,2-Dichloroethane ND ug/kg 06/03/22 12:51 107-06-206/02/22 18:506.0 4.0 1
1,1-Dichloroethene ND ug/kg 06/03/22 12:51 75-35-406/02/22 18:506.0 2.5 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 12:51 156-59-206/02/22 18:506.0 2.1 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 12:51 156-60-506/02/22 18:506.0 2.1 1
1,2-Dichloropropane ND ug/kg 06/03/22 12:51 78-87-506/02/22 18:506.0 1.8 1
1,3-Dichloropropane ND ug/kg 06/03/22 12:51 142-28-906/02/22 18:506.0 1.9 1
2,2-Dichloropropane ND ug/kg 06/03/22 12:51 594-20-706/02/22 18:506.0 2.0 1
1,1-Dichloropropene ND ug/kg 06/03/22 12:51 563-58-606/02/22 18:506.0 2.9 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 12:51 10061-01-506/02/22 18:506.0 1.6 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 12:51 10061-02-606/02/22 18:506.0 2.1 1
Diisopropyl ether ND ug/kg 06/03/22 12:51 108-20-306/02/22 18:506.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607324
LSG-001
Sample:DUP-1 Lab ID:92607324002 Collected:06/01/22 00:00 Received:06/01/22 11:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/03/22 12:51 100-41-406/02/22 18:506.0 2.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 12:51 87-68-306/02/22 18:5012.1 9.9 1
2-Hexanone ND ug/kg 06/03/22 12:51 591-78-606/02/22 18:5060.4 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 12:51 98-82-806/02/22 18:506.0 2.1 1
p-Isopropyltoluene ND ug/kg 06/03/22 12:51 99-87-606/02/22 18:506.0 3.0 1
Methylene Chloride ND ug/kg 06/03/22 12:51 75-09-206/02/22 18:5024.2 16.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 12:51 108-10-106/02/22 18:5060.4 5.8 1
Methyl-tert-butyl ether ND ug/kg 06/03/22 12:51 1634-04-406/02/22 18:506.0 2.3 1
Naphthalene 11.4 ug/kg 06/03/22 12:51 91-20-306/02/22 18:506.0 3.2 1
n-Propylbenzene ND ug/kg 06/03/22 12:51 103-65-106/02/22 18:506.0 2.1 1
Styrene ND ug/kg 06/03/22 12:51 100-42-506/02/22 18:506.0 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 12:51 630-20-606/02/22 18:506.0 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 12:51 79-34-506/02/22 18:506.0 1.6 1
Tetrachloroethene ND ug/kg 06/03/22 12:51 127-18-406/02/22 18:506.0 1.9 1
Toluene ND ug/kg 06/03/22 12:51 108-88-306/02/22 18:506.0 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 12:51 87-61-606/02/22 18:506.0 4.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 12:51 120-82-106/02/22 18:506.0 5.1 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 12:51 71-55-606/02/22 18:506.0 3.1 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 12:51 79-00-506/02/22 18:506.0 2.0 1
Trichloroethene ND ug/kg 06/03/22 12:51 79-01-606/02/22 18:506.0 1.6 1
Trichlorofluoromethane ND ug/kg 06/03/22 12:51 75-69-406/02/22 18:506.0 3.3 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 12:51 96-18-406/02/22 18:506.0 3.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 12:51 95-63-606/02/22 18:506.0 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 12:51 108-67-806/02/22 18:506.0 2.0 1
Vinyl acetate ND ug/kg 06/03/22 12:51 108-05-406/02/22 18:5060.4 4.4 1
Vinyl chloride ND ug/kg 06/03/22 12:51 75-01-4 v106/02/22 18:5012.1 3.1 1
Xylene (Total)ND ug/kg 06/03/22 12:51 1330-20-706/02/22 18:5012.1 3.4 1
m&p-Xylene ND ug/kg 06/03/22 12:51 179601-23-106/02/22 18:5012.1 4.1 1
o-Xylene ND ug/kg 06/03/22 12:51 95-47-606/02/22 18:506.0 2.7 1
Surrogates
Toluene-d8 (S)101 %06/03/22 12:51 2037-26-506/02/22 18:5070-130 1
4-Bromofluorobenzene (S)97 %06/03/22 12:51 460-00-406/02/22 18:5069-134 1
1,2-Dichloroethane-d4 (S)96 %06/03/22 12:51 17060-07-006/02/22 18:5070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.7 %06/03/22 16:08 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
819665
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92607324001, 92607324002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4343807
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.018 06/08/22 13:310.0077
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4343808LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.440.45 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4343809MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605869016
4343810
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.563 94 80-12095 8 200.515ND 0.53 0.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
819660
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92607324001, 92607324002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4343785
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.48 06/08/22 19:450.10
Barium mg/kg ND 0.29 06/08/22 19:450.051
Cadmium mg/kg ND 0.077 06/08/22 19:450.030
Chromium mg/kg ND 1.9 06/08/22 19:450.13
Lead mg/kg ND 0.48 06/08/22 19:450.028
Selenium mg/kg ND 0.48 06/08/22 19:450.082
Silver mg/kg ND 0.48 06/08/22 19:450.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4343786LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 58.149.6 117 80-120
Barium mg/kg 55.549.6 112 80-120
Cadmium mg/kg 55.849.6 112 80-120
Chromium mg/kg 58.849.6 118 80-120
Lead mg/kg 56.149.6 113 80-120
Selenium mg/kg 46.649.6 94 80-120
Silver mg/kg 28.424.8 114 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4343787MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605869016
4343788
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 56.1 104 75-125100 1 2058.70.93 58.9 59.4
Barium mg/kg M156.1 142 75-125140 1 2058.7116 196 199
Cadmium mg/kg 56.1 111 75-125108 2 2058.70.063J 62.5 63.6
Chromium mg/kg M156.1 127 75-125108 8 2058.726.0 96.9 89.6
Lead mg/kg 56.1 112 75-125109 2 2058.77.3 69.9 71.5
Selenium mg/kg 56.1 90 75-12586 0 2058.70.25J 50.9 50.8
Silver mg/kg 28 110 75-125107 2 2029.40.23J 31.1 31.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702033
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607324001, 92607324002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664117
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/03/22 05:591.9
1,1,1-Trichloroethane ug/kg ND 5.0 06/03/22 05:592.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/03/22 05:591.3
1,1,2-Trichloroethane ug/kg ND 5.0 06/03/22 05:591.7
1,1-Dichloroethane ug/kg ND 5.0 06/03/22 05:592.1
1,1-Dichloroethene ug/kg ND 5.0 06/03/22 05:592.1
1,1-Dichloropropene ug/kg ND 5.0 06/03/22 05:592.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/03/22 05:594.0
1,2,3-Trichloropropane ug/kg ND 5.0 06/03/22 05:592.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/03/22 05:594.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/03/22 05:591.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/03/22 05:591.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/03/22 05:592.2
1,2-Dichlorobenzene ug/kg ND 5.0 06/03/22 05:591.8
1,2-Dichloroethane ug/kg ND 5.0 06/03/22 05:593.3
1,2-Dichloropropane ug/kg ND 5.0 06/03/22 05:591.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/03/22 05:591.7
1,3-Dichlorobenzene ug/kg ND 5.0 06/03/22 05:591.6
1,3-Dichloropropane ug/kg ND 5.0 06/03/22 05:591.6
1,4-Dichlorobenzene ug/kg ND 5.0 06/03/22 05:591.3
2,2-Dichloropropane ug/kg ND 5.0 06/03/22 05:591.6
2-Butanone (MEK)ug/kg ND 100 06/03/22 05:5924.0
2-Chlorotoluene ug/kg ND 5.0 06/03/22 05:591.8
2-Hexanone ug/kg ND 50.0 06/03/22 05:594.8
4-Chlorotoluene ug/kg ND 5.0 06/03/22 05:590.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/03/22 05:594.8
Acetone ug/kg ND 100 06/03/22 05:5932.1
Benzene ug/kg ND 5.0 06/03/22 05:592.0
Bromobenzene ug/kg ND 5.0 06/03/22 05:591.6
Bromochloromethane ug/kg ND 5.0 06/03/22 05:591.5
Bromodichloromethane ug/kg ND 5.0 06/03/22 05:591.9
Bromoform ug/kg ND 5.0 06/03/22 05:591.8
Bromomethane ug/kg ND 10.0 IK06/03/22 05:597.9
Carbon tetrachloride ug/kg ND 5.0 06/03/22 05:591.9
Chlorobenzene ug/kg ND 5.0 06/03/22 05:590.96
Chloroethane ug/kg ND 10.0 06/03/22 05:593.9
Chloroform ug/kg ND 5.0 06/03/22 05:593.0
Chloromethane ug/kg ND 10.0 06/03/22 05:594.2
cis-1,2-Dichloroethene ug/kg ND 5.0 06/03/22 05:591.7
cis-1,3-Dichloropropene ug/kg ND 5.0 06/03/22 05:591.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664117
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 06/03/22 05:592.8
Dibromomethane ug/kg ND 5.0 06/03/22 05:591.1
Dichlorodifluoromethane ug/kg ND 10.0 v106/03/22 05:592.2
Diisopropyl ether ug/kg ND 5.0 06/03/22 05:591.4
Ethylbenzene ug/kg ND 5.0 06/03/22 05:592.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/03/22 05:598.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/03/22 05:591.7
m&p-Xylene ug/kg ND 10.0 06/03/22 05:593.4
Methyl-tert-butyl ether ug/kg ND 5.0 06/03/22 05:591.9
Methylene Chloride ug/kg ND 20.0 06/03/22 05:5913.7
n-Butylbenzene ug/kg ND 5.0 06/03/22 05:592.4
n-Propylbenzene ug/kg ND 5.0 06/03/22 05:591.8
Naphthalene ug/kg ND 5.0 06/03/22 05:592.6
o-Xylene ug/kg ND 5.0 06/03/22 05:592.2
p-Isopropyltoluene ug/kg ND 5.0 06/03/22 05:592.5
sec-Butylbenzene ug/kg ND 5.0 06/03/22 05:592.2
Styrene ug/kg ND 5.0 06/03/22 05:591.3
tert-Butylbenzene ug/kg ND 5.0 06/03/22 05:591.8
Tetrachloroethene ug/kg ND 5.0 06/03/22 05:591.6
Toluene ug/kg ND 5.0 06/03/22 05:591.4
trans-1,2-Dichloroethene ug/kg ND 5.0 06/03/22 05:591.8
trans-1,3-Dichloropropene ug/kg ND 5.0 06/03/22 05:591.7
Trichloroethene ug/kg ND 5.0 06/03/22 05:591.3
Trichlorofluoromethane ug/kg ND 5.0 06/03/22 05:592.8
Vinyl acetate ug/kg ND 50.0 06/03/22 05:593.6
Vinyl chloride ug/kg ND 10.0 v106/03/22 05:592.5
Xylene (Total)ug/kg ND 10.0 06/03/22 05:592.8
1,2-Dichloroethane-d4 (S)%104 70-130 06/03/22 05:59
4-Bromofluorobenzene (S)%97 69-134 06/03/22 05:59
Toluene-d8 (S)%99 70-130 06/03/22 05:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664118LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13501250 108 70-130
1,1,1-Trichloroethane ug/kg 12701250 101 70-130
1,1,2,2-Tetrachloroethane ug/kg 12301250 99 70-130
1,1,2-Trichloroethane ug/kg 13201250 106 70-130
1,1-Dichloroethane ug/kg 12201250 97 70-130
1,1-Dichloroethene ug/kg 13301250 106 70-130
1,1-Dichloropropene ug/kg 13401250 107 70-130
1,2,3-Trichlorobenzene ug/kg 13901250 111 65-130
1,2,3-Trichloropropane ug/kg 11601250 93 70-130
1,2,4-Trichlorobenzene ug/kg 13401250 107 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664118LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 14301250 114 70-130
1,2-Dibromo-3-chloropropane ug/kg 12401250 99 70-130
1,2-Dibromoethane (EDB)ug/kg 13001250 104 70-130
1,2-Dichlorobenzene ug/kg 13201250 106 70-130
1,2-Dichloroethane ug/kg 11501250 92 63-130
1,2-Dichloropropane ug/kg 13201250 106 70-130
1,3,5-Trimethylbenzene ug/kg 14201250 113 70-130
1,3-Dichlorobenzene ug/kg 13401250 107 70-130
1,3-Dichloropropane ug/kg 12801250 102 70-130
1,4-Dichlorobenzene ug/kg 12601250 101 70-130
2,2-Dichloropropane ug/kg 11501250 92 66-130
2-Butanone (MEK)ug/kg 22502500 90 70-130
2-Chlorotoluene ug/kg 13701250 110 70-130
2-Hexanone ug/kg 25002500 100 70-130
4-Chlorotoluene ug/kg 13301250 107 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25702500 103 70-130
Acetone ug/kg 21802500 87 69-130
Benzene ug/kg 12601250 101 70-130
Bromobenzene ug/kg 14101250 112 70-130
Bromochloromethane ug/kg 12201250 98 70-130
Bromodichloromethane ug/kg 11601250 93 69-130
Bromoform ug/kg 14201250 114 70-130
Bromomethane ug/kg 1290 IK125010352-130
Carbon tetrachloride ug/kg 14101250 113 70-130
Chlorobenzene ug/kg 13101250 105 70-130
Chloroethane ug/kg 14101250 112 65-130
Chloroform ug/kg 12001250 96 70-130
Chloromethane ug/kg 14601250 116 55-130
cis-1,2-Dichloroethene ug/kg 12801250 102 70-130
cis-1,3-Dichloropropene ug/kg 13301250 106 70-130
Dibromochloromethane ug/kg 13301250 106 70-130
Dibromomethane ug/kg 13601250 109 70-130
Dichlorodifluoromethane ug/kg 1930 v1125015445-156
Diisopropyl ether ug/kg 12801250 102 70-130
Ethylbenzene ug/kg 12401250 99 70-130
Hexachloro-1,3-butadiene ug/kg 13601250 109 66-130
Isopropylbenzene (Cumene)ug/kg 13501250 108 70-130
m&p-Xylene ug/kg 26702500 107 70-130
Methyl-tert-butyl ether ug/kg 11701250 93 70-130
Methylene Chloride ug/kg 11801250 94 65-130
n-Butylbenzene ug/kg 13901250 112 67-130
n-Propylbenzene ug/kg 13801250 110 70-130
Naphthalene ug/kg 13101250 105 70-130
o-Xylene ug/kg 14201250 113 70-130
p-Isopropyltoluene ug/kg 14301250 114 67-130
sec-Butylbenzene ug/kg 14001250 112 69-130
Styrene ug/kg 14801250 118 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664118LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13301250 107 67-130
Tetrachloroethene ug/kg 13801250 110 70-130
Toluene ug/kg 12501250 100 70-130
trans-1,2-Dichloroethene ug/kg 13101250 105 70-130
trans-1,3-Dichloropropene ug/kg 13301250 106 68-130
Trichloroethene ug/kg 14001250 112 70-130
Trichlorofluoromethane ug/kg 13901250 112 70-130
Vinyl acetate ug/kg 25302500 101 70-130
Vinyl chloride ug/kg 1520 v1125012161-130
Xylene (Total)ug/kg 40803750 109 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664120MATRIX SPIKE SAMPLE:
MSSpike
Result
92606920005
1,1,1,2-Tetrachloroethane ug/kg 596698 85 70-131ND
1,1,1-Trichloroethane ug/kg 615698 88 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 546698 78 66-130ND
1,1,2-Trichloroethane ug/kg 567698 81 66-133ND
1,1-Dichloroethane ug/kg 561698 80 65-130ND
1,1-Dichloroethene ug/kg 601698 86 10-158ND
1,1-Dichloropropene ug/kg 643698 92 68-133ND
1,2,3-Trichlorobenzene ug/kg 583698 84 27-138ND
1,2,3-Trichloropropane ug/kg 513698 73 67-130ND
1,2,4-Trichlorobenzene ug/kg 569698 81 51-134ND
1,2,4-Trimethylbenzene ug/kg 585698 83 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 473698 68 32-130ND
1,2-Dibromoethane (EDB)ug/kg 556698 80 70-130ND
1,2-Dichlorobenzene ug/kg 581698 83 69-130ND
1,2-Dichloroethane ug/kg 553698 79 59-130ND
1,2-Dichloropropane ug/kg 615698 88 70-130ND
1,3,5-Trimethylbenzene ug/kg 579698 83 65-137ND
1,3-Dichlorobenzene ug/kg 564698 81 70-130ND
1,3-Dichloropropane ug/kg 575698 82 70-130ND
1,4-Dichlorobenzene ug/kg 538698 77 68-130ND
2,2-Dichloropropane ug/kg 487698 70 32-130ND
2-Butanone (MEK)ug/kg 8781400 63 10-136ND
2-Chlorotoluene ug/kg 554698 79 69-141ND
2-Hexanone ug/kg 10101400 72 10-144ND
4-Chlorotoluene ug/kg 552698 79 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 10501400 75 25-143ND
Acetone ug/kg 7001400 50 10-130ND
Benzene ug/kg 603698 86 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664120MATRIX SPIKE SAMPLE:
MSSpike
Result
92606920005
Bromobenzene ug/kg 553698 79 70-130ND
Bromochloromethane ug/kg 538698 77 69-134ND
Bromodichloromethane ug/kg 498698 71 64-130ND
Bromoform ug/kg 580698 83 62-130ND
Bromomethane ug/kg 357 IK6985120-176ND
Carbon tetrachloride ug/kg 674698 97 65-140ND
Chlorobenzene ug/kg 592698 85 70-130ND
Chloroethane ug/kg 203698 29 10-130ND
Chloroform ug/kg 471698 68 63-130ND
Chloromethane ug/kg 761698 109 58-130ND
cis-1,2-Dichloroethene ug/kg 601698 86 66-130ND
cis-1,3-Dichloropropene ug/kg 570698 82 67-130ND
Dibromochloromethane ug/kg 548698 78 67-130ND
Dibromomethane ug/kg 576698 82 63-131ND
Dichlorodifluoromethane ug/kg 865 v169812444-180ND
Diisopropyl ether ug/kg 595698 85 63-130ND
Ethylbenzene ug/kg 558698 80 66-130ND
Hexachloro-1,3-butadiene ug/kg 669698 96 64-150ND
Isopropylbenzene (Cumene)ug/kg 599698 86 69-135ND
m&p-Xylene ug/kg 11901400 85 60-133ND
Methyl-tert-butyl ether ug/kg 496698 71 65-130ND
Methylene Chloride ug/kg 534698 77 61-130ND
n-Butylbenzene ug/kg 590698 85 65-140ND
n-Propylbenzene ug/kg 560698 80 67-140ND
Naphthalene ug/kg 508698 73 15-145ND
o-Xylene ug/kg 620698 89 66-133ND
p-Isopropyltoluene ug/kg 591698 85 56-147ND
sec-Butylbenzene ug/kg 617698 88 65-139ND
Styrene ug/kg 602698 86 70-132ND
tert-Butylbenzene ug/kg 562698 80 62-135ND
Tetrachloroethene ug/kg 599698 86 70-135ND
Toluene ug/kg 572698 81 67-130ND
trans-1,2-Dichloroethene ug/kg 610698 87 69-130ND
trans-1,3-Dichloropropene ug/kg 552698 79 62-130ND
Trichloroethene ug/kg 657698 94 70-135ND
Trichlorofluoromethane ug/kg 234698 34 10-130ND
Vinyl acetate ug/kg 7671400 55 53-130ND
Vinyl chloride ug/kg 673 v16989661-148ND
Xylene (Total)ug/kg 18102090 86 63-132ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606920004
3664119SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 9.6 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 5.8J 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606920004
3664119SAMPLE DUPLICATE:
m&p-Xylene ug/kg 14.8 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 5.3J 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 11.1 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND v130ND
Xylene (Total)ug/kg 14.8 30ND
1,2-Dichloroethane-d4 (S)%9695
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%10098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702172
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607324001, 92607324002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664496
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 329 06/06/22 11:42130
1,2-Dichlorobenzene ug/kg ND 329 06/06/22 11:42119
1,3-Dichlorobenzene ug/kg ND 329 06/06/22 11:42117
1,4-Dichlorobenzene ug/kg ND 329 06/06/22 11:42126
1-Methylnaphthalene ug/kg ND 329 06/06/22 11:42116
2,2'-Oxybis(1-chloropropane)ug/kg ND 329 06/06/22 11:42156
2,4,5-Trichlorophenol ug/kg ND 329 06/06/22 11:42150
2,4,6-Trichlorophenol ug/kg ND 329 06/06/22 11:42136
2,4-Dichlorophenol ug/kg ND 329 06/06/22 11:42129
2,4-Dimethylphenol ug/kg ND 329 06/06/22 11:42137
2,4-Dinitrophenol ug/kg ND 1640 06/06/22 11:421020
2,4-Dinitrotoluene ug/kg ND 329 06/06/22 11:42127
2,6-Dinitrotoluene ug/kg ND 329 06/06/22 11:42121
2-Chloronaphthalene ug/kg ND 329 06/06/22 11:42131
2-Chlorophenol ug/kg ND 329 06/06/22 11:42124
2-Methylnaphthalene ug/kg ND 329 06/06/22 11:42132
2-Methylphenol(o-Cresol)ug/kg ND 329 06/06/22 11:42135
2-Nitroaniline ug/kg ND 1640 06/06/22 11:42269
2-Nitrophenol ug/kg ND 329 06/06/22 11:42143
3&4-Methylphenol(m&p Cresol)ug/kg ND 329 06/06/22 11:42133
3,3'-Dichlorobenzidine ug/kg ND 658 IL06/06/22 11:42222
3-Nitroaniline ug/kg ND 1640 06/06/22 11:42258
4,6-Dinitro-2-methylphenol ug/kg ND 658 06/06/22 11:42307
4-Bromophenylphenyl ether ug/kg ND 329 06/06/22 11:42127
4-Chloro-3-methylphenol ug/kg ND 658 06/06/22 11:42231
4-Chloroaniline ug/kg ND 658 06/06/22 11:42258
4-Chlorophenylphenyl ether ug/kg ND 329 06/06/22 11:42123
4-Nitroaniline ug/kg ND 658 06/06/22 11:42250
4-Nitrophenol ug/kg ND 1640 06/06/22 11:42636
Acenaphthene ug/kg ND 329 06/06/22 11:42116
Acenaphthylene ug/kg ND 329 06/06/22 11:42116
Aniline ug/kg ND 329 06/06/22 11:42129
Anthracene ug/kg ND 329 06/06/22 11:42108
Benzo(a)anthracene ug/kg ND 329 06/06/22 11:42110
Benzo(a)pyrene ug/kg ND 329 06/06/22 11:42114
Benzo(b)fluoranthene ug/kg ND 329 06/06/22 11:42110
Benzo(g,h,i)perylene ug/kg ND 329 06/06/22 11:42128
Benzo(k)fluoranthene ug/kg ND 329 06/06/22 11:42116
Benzoic Acid ug/kg ND 1640 06/06/22 11:42707
Benzyl alcohol ug/kg ND 658 06/06/22 11:42249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664496
Associated Lab Samples:92607324001, 92607324002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 329 06/06/22 11:42137
bis(2-Chloroethyl) ether ug/kg ND 329 06/06/22 11:42124
bis(2-Ethylhexyl)phthalate ug/kg ND 329 06/06/22 11:42128
Butylbenzylphthalate ug/kg ND 329 06/06/22 11:42139
Chrysene ug/kg ND 329 06/06/22 11:42120
Di-n-butylphthalate ug/kg ND 329 06/06/22 11:42111
Di-n-octylphthalate ug/kg ND 329 06/06/22 11:42130
Dibenz(a,h)anthracene ug/kg ND 329 06/06/22 11:42127
Dibenzofuran ug/kg ND 329 06/06/22 11:42119
Diethylphthalate ug/kg ND 329 06/06/22 11:42121
Dimethylphthalate ug/kg ND 329 06/06/22 11:42120
Fluoranthene ug/kg ND 329 06/06/22 11:42113
Fluorene ug/kg ND 329 06/06/22 11:42116
Hexachloro-1,3-butadiene ug/kg ND 329 06/06/22 11:42143
Hexachlorobenzene ug/kg ND 329 06/06/22 11:42129
Hexachlorocyclopentadiene ug/kg ND 329 v206/06/22 11:42188
Hexachloroethane ug/kg ND 329 06/06/22 11:42126
Indeno(1,2,3-cd)pyrene ug/kg ND 329 06/06/22 11:42130
Isophorone ug/kg ND 329 06/06/22 11:42147
N-Nitroso-di-n-propylamine ug/kg ND 329 06/06/22 11:42124
N-Nitrosodimethylamine ug/kg ND 329 v206/06/22 11:42111
N-Nitrosodiphenylamine ug/kg ND 329 06/06/22 11:42117
Naphthalene ug/kg ND 329 06/06/22 11:42112
Nitrobenzene ug/kg ND 329 06/06/22 11:42152
Pentachlorophenol ug/kg ND 658 06/06/22 11:42322
Phenanthrene ug/kg ND 329 06/06/22 11:42108
Phenol ug/kg ND 329 06/06/22 11:42147
Pyrene ug/kg ND 329 06/06/22 11:42134
Pyridine ug/kg ND 329 06/06/22 11:42104
2,4,6-Tribromophenol (S)%66 18-130 06/06/22 11:42
2-Fluorobiphenyl (S)%65 19-130 06/06/22 11:42
2-Fluorophenol (S)%55 18-130 06/06/22 11:42
Nitrobenzene-d5 (S)%58 21-130 06/06/22 11:42
Phenol-d6 (S)%56 18-130 06/06/22 11:42
Terphenyl-d14 (S)%69 15-130 06/06/22 11:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664497LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10601660 64 47-130
1,2-Dichlorobenzene ug/kg 10001660 60 49-130
1,3-Dichlorobenzene ug/kg 9901660 60 48-130
1,4-Dichlorobenzene ug/kg 10101660 61 49-130
1-Methylnaphthalene ug/kg 10701660 65 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664497LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 8231660 50 38-130
2,4,5-Trichlorophenol ug/kg 10701660 64 49-130
2,4,6-Trichlorophenol ug/kg 9981660 60 50-130
2,4-Dichlorophenol ug/kg 10601660 64 51-130
2,4-Dimethylphenol ug/kg 10001660 60 53-130
2,4-Dinitrophenol ug/kg 43208310 52 39-130
2,4-Dinitrotoluene ug/kg 9961660 60 53-130
2,6-Dinitrotoluene ug/kg 10601660 64 55-130
2-Chloronaphthalene ug/kg 10401660 63 48-130
2-Chlorophenol ug/kg 9531660 57 54-130
2-Methylnaphthalene ug/kg 10501660 63 57-130
2-Methylphenol(o-Cresol)ug/kg 9721660 59 50-130
2-Nitroaniline ug/kg 17603320 53 49-130
2-Nitrophenol ug/kg 9941660 60 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 8621660 52 50-130
3,3'-Dichlorobenzidine ug/kg 2150 IL33206547-130
3-Nitroaniline ug/kg 20303320 61 45-130
4,6-Dinitro-2-methylphenol ug/kg 19003320 57 50-142
4-Bromophenylphenyl ether ug/kg 11201660 67 55-130
4-Chloro-3-methylphenol ug/kg 20103320 61 52-130
4-Chloroaniline ug/kg 19303320 58 49-130
4-Chlorophenylphenyl ether ug/kg 10601660 64 53-130
4-Nitroaniline ug/kg 17103320 52 51-130
4-Nitrophenol ug/kg 42308310 51 40-130
Acenaphthene ug/kg 10601660 64 56-130
Acenaphthylene ug/kg 10601660 64 58-130
Aniline ug/kg 7881660 47 44-130
Anthracene ug/kg 10301660 62 60-130
Benzo(a)anthracene ug/kg 10201660 61 59-130
Benzo(a)pyrene ug/kg 9991660 60 57-130
Benzo(b)fluoranthene ug/kg 9001660 54 54-130
Benzo(g,h,i)perylene ug/kg 11001660 66 59-130
Benzo(k)fluoranthene ug/kg 10101660 61 54-130
Benzoic Acid ug/kg 33708310 41 19-130
Benzyl alcohol ug/kg 18303320 55 50-130
bis(2-Chloroethoxy)methane ug/kg 9621660 58 55-130
bis(2-Chloroethyl) ether ug/kg 9821660 59 53-130
bis(2-Ethylhexyl)phthalate ug/kg 10901660 65 58-130
Butylbenzylphthalate ug/kg 10601660 64 46-138
Chrysene ug/kg 11001660 66 57-130
Di-n-butylphthalate ug/kg 10801660 65 57-130
Di-n-octylphthalate ug/kg 11801660 71 57-130
Dibenz(a,h)anthracene ug/kg 11201660 67 60-130
Dibenzofuran ug/kg 10701660 64 54-130
Diethylphthalate ug/kg 10101660 61 55-130
Dimethylphthalate ug/kg 10201660 61 57-130
Fluoranthene ug/kg 11101660 67 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664497LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 10601660 64 56-130
Hexachloro-1,3-butadiene ug/kg 11001660 66 41-130
Hexachlorobenzene ug/kg 10501660 63 53-130
Hexachlorocyclopentadiene ug/kg 800 v316604823-130
Hexachloroethane ug/kg 10001660 60 48-130
Indeno(1,2,3-cd)pyrene ug/kg 11001660 66 61-130
Isophorone ug/kg 8741660 53 49-130
N-Nitroso-di-n-propylamine ug/kg 9181660 55 52-130
N-Nitrosodimethylamine ug/kg 694 L2,v316604245-130
N-Nitrosodiphenylamine ug/kg 10701660 64 56-130
Naphthalene ug/kg 10301660 62 56-130
Nitrobenzene ug/kg 9091660 55 50-130
Pentachlorophenol ug/kg 18303320 55 33-130
Phenanthrene ug/kg 10801660 65 60-130
Phenol ug/kg 9481660 57 54-130
Pyrene ug/kg 10201660 62 61-130
Pyridine ug/kg 7371660 44 35-130
2,4,6-Tribromophenol (S)%63 18-130
2-Fluorobiphenyl (S)%60 19-130
2-Fluorophenol (S)%52 18-130
Nitrobenzene-d5 (S)%51 21-130
Phenol-d6 (S)%51 18-130
Terphenyl-d14 (S)%59 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664498MATRIX SPIKE SAMPLE:
MSSpike
Result
92607565003
1,2,4-Trichlorobenzene ug/kg 9761650 59 22-130ND
1,2-Dichlorobenzene ug/kg 9361650 57 23-130ND
1,3-Dichlorobenzene ug/kg 9171650 56 26-130ND
1,4-Dichlorobenzene ug/kg 9341650 57 27-130ND
1-Methylnaphthalene ug/kg 9971650 60 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 7971650 48 30-130ND
2,4,5-Trichlorophenol ug/kg 10101650 61 26-130ND
2,4,6-Trichlorophenol ug/kg 9321650 56 23-130ND
2,4-Dichlorophenol ug/kg 9901650 60 29-130ND
2,4-Dimethylphenol ug/kg 9521650 58 13-130ND
2,4-Dinitrophenol ug/kg 23708250 29 10-131ND
2,4-Dinitrotoluene ug/kg 10201650 62 28-130ND
2,6-Dinitrotoluene ug/kg 10501650 63 36-130ND
2-Chloronaphthalene ug/kg 9791650 59 27-130ND
2-Chlorophenol ug/kg 8951650 54 29-130ND
2-Methylnaphthalene ug/kg 9691650 59 29-130ND
2-Methylphenol(o-Cresol)ug/kg 9121650 55 20-130ND
2-Nitroaniline ug/kg 17903300 54 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664498MATRIX SPIKE SAMPLE:
MSSpike
Result
92607565003
2-Nitrophenol ug/kg 9011650 55 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 7791650 47 10-176ND
3,3'-Dichlorobenzidine ug/kg 2110 v333006415-130ND
3-Nitroaniline ug/kg 20103300 61 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 14003300 42 15-132ND
4-Bromophenylphenyl ether ug/kg 10001650 61 35-130ND
4-Chloro-3-methylphenol ug/kg 18703300 57 30-130ND
4-Chloroaniline ug/kg 17803300 54 28-130ND
4-Chlorophenylphenyl ether ug/kg 9871650 60 32-130ND
4-Nitroaniline ug/kg 17603300 53 30-130ND
4-Nitrophenol ug/kg 45208250 55 17-130ND
Acenaphthene ug/kg 9901650 60 29-130ND
Acenaphthylene ug/kg 10101650 61 31-130ND
Aniline ug/kg 7421650 45 10-130ND
Anthracene ug/kg 9941650 60 33-130ND
Benzo(a)anthracene ug/kg 10001650 61 32-130ND
Benzo(a)pyrene ug/kg 9951650 60 32-130ND
Benzo(b)fluoranthene ug/kg 9291650 56 33-130ND
Benzo(g,h,i)perylene ug/kg 10201650 62 28-130ND
Benzo(k)fluoranthene ug/kg 9861650 60 31-130ND
Benzoic Acid ug/kg 17108250 21 10-130ND
Benzyl alcohol ug/kg 16903300 51 31-130ND
bis(2-Chloroethoxy)methane ug/kg 8861650 54 30-130ND
bis(2-Chloroethyl) ether ug/kg 883 M116505468-130ND
bis(2-Ethylhexyl)phthalate ug/kg 10401650 63 40-130ND
Butylbenzylphthalate ug/kg 10101650 61 40-130ND
Chrysene ug/kg 10901650 66 30-130ND
Di-n-butylphthalate ug/kg 10401650 63 41-130ND
Di-n-octylphthalate ug/kg 11801650 72 42-130ND
Dibenz(a,h)anthracene ug/kg 10301650 62 27-130ND
Dibenzofuran ug/kg 10301650 62 32-130ND
Diethylphthalate ug/kg 10101650 62 40-130ND
Dimethylphthalate ug/kg 10001650 61 37-130ND
Fluoranthene ug/kg 11601650 70 26-130ND
Fluorene ug/kg 10301650 63 31-130ND
Hexachloro-1,3-butadiene ug/kg 9661650 59 20-130ND
Hexachlorobenzene ug/kg 9551650 58 29-130ND
Hexachlorocyclopentadiene ug/kg 529 v216503210-130ND
Hexachloroethane ug/kg 9371650 57 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 10201650 62 28-130ND
Isophorone ug/kg 8291650 50 32-130ND
N-Nitroso-di-n-propylamine ug/kg 8901650 54 31-130ND
N-Nitrosodimethylamine ug/kg 671 v216504120-130ND
N-Nitrosodiphenylamine ug/kg 9821650 59 32-130ND
Naphthalene ug/kg 9471650 57 30-130ND
Nitrobenzene ug/kg 8501650 52 25-130ND
Pentachlorophenol ug/kg 17903300 54 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664498MATRIX SPIKE SAMPLE:
MSSpike
Result
92607565003
Phenanthrene ug/kg 10401650 63 34-130ND
Phenol ug/kg 8711650 53 14-130ND
Pyrene ug/kg 9461650 57 31-130ND
Pyridine ug/kg 6931650 42 10-130ND
2,4,6-Tribromophenol (S)%54 18-130
2-Fluorobiphenyl (S)%54 19-130
2-Fluorophenol (S)%46 18-130
Nitrobenzene-d5 (S)%48 21-130
Phenol-d6 (S)%47 18-130
Terphenyl-d14 (S)%52 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92607565004
3664499SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND IL30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92607565004
3664499SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND v230ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND v230ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%5852
2-Fluorobiphenyl (S)%4438
2-Fluorophenol (S)%4534
Nitrobenzene-d5 (S)%4841
Phenol-d6 (S)%4635
Terphenyl-d14 (S)%4039
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607324
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702253
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607324001, 92607324002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606895022
3665105SAMPLE DUPLICATE:
Percent Moisture %17.2 N292518.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92605449007
3665106SAMPLE DUPLICATE:
Percent Moisture %21.9 N232522.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92607324
LSG-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92607324
Regulated Soil - Special Handling Required[1]
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92607324
LSG-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92607324001 819660 819983SP-1 EPA 3050B EPA 6020B
92607324002 819660 819983DUP-1 EPA 3050B EPA 6020B
92607324001 819665 820184SP-1 EPA 7471B EPA 7471B
92607324002 819665 820184DUP-1 EPA 7471B EPA 7471B
92607324001 702172 702421SP-1 EPA 3546 EPA 8270E
92607324002 702172 702421DUP-1 EPA 3546 EPA 8270E
92607324001 702033 702050SP-1 EPA 5035A/5030B EPA 8260D
92607324002 702033 702050DUP-1 EPA 5035A/5030B EPA 8260D
92607324001 702253SP-1 SW-846
92607324002 702253DUP-1 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/09/2022 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 34
Page 32 of 34
Page 33 of 34
Page 34 of 34
06/10/22
Technical Report for
Hart & Hickman
LSG-001
LSG-001
SGS Job Number: JD46091
Sampling Date: 06/01/22
Report to:
Hart & Hickman
2923 South Tyron Street Suite 101
Charlotte, NC 28217
[e-mail]
ATTN: Shannon Cottrill
Total number of pages in report:
Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC,
OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Ramos 732-329-0200
David Chastain
General Manager
Dayton, NJ 06/10/22
e-Hardcopy 2.0
Automated Report
15
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 15
JD46091
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................4
Section 3: Summary of Hits ....................................................................................................5
Section 4: Sample Results ........................................................................................................6
4.1: JD46091-1: SP-1 ...........................................................................................................7
4.2: JD46091-2: DUP-1 .......................................................................................................8
Section 5: Misc. Forms ............................................................................................................9
5.1: Chain of Custody ...........................................................................................................10
Section 6: General Chemistry - QC Data Summaries ..........................................................12
6.1: Method Blank and Spike Results Summary ..................................................................13
6.2: Duplicate Results Summary ..........................................................................................14
6.3: Matrix Spike Results Summary .....................................................................................15 1234562 of 15
JD46091
SGS North America Inc.
Sample Summary
Hart & Hickman
Job No:JD46091
LSG-001
Project No: LSG-001
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
JD46091-1 06/01/22 09:45 JB 06/04/22 SO Soil SP-1
JD46091-2 06/01/22 00:00 JB 06/04/22 SO Soil DUP-1
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 15
JD460911
On 06/04/2022, 2 Sample(s), 0 Trip Blank(s) and 0 Field Blank(s) were received at SGS North America Inc. at a maximum
corrected temperature of 3.5 C. Samples were intact and chemically preserved, unless noted below. A SGS North America Inc. Job
Number of JD46091 was assigned to the project. Laboratory sample ID, client sample ID and dates of sample collection are
detailed in the report’s Results Summary Section.
Specified quality control criteria were achieved for this job except as noted below. For more information, please refer to the
analytical results and QC summary pages.
Client:Hart & Hickman
Site:LSG-001
Job No:JD46091
Report Date 6/10/2022 10:58:20 A
CASE NARRATIVE / CONFORMANCE SUMMARY
Compounds qualified as out of range in the continuing calibration summary report are acceptable as per method requirements when
there is a high bias but the sample result is non-detect.
General Chemistry By Method SM2540 G 18TH ED MOD
Matrix:SO Batch ID:GN29979
Sample(s) JD46058-1DUP were used as the QC samples for Solids, Percent.
General Chemistry By Method SW846 3060A/7199
Matrix:SO Batch ID:GP40511
All samples were prepared within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) JD46091-2PS, JD46091-2MS, JD46091-2DUP were used as the QC samples for Chromium, Hexavalent.
RPD(s) for Duplicate for Chromium, Hexavalent are outside control limits for sample GP40511-D1. RPD acceptable due to
low duplicate and sample concentrations.
GP40511-S1 for Chromium, Hexavalent: Good recovery on soluble XCR matrix spike. Good recovery (104 %) on the post-
spike.
SGS North America Inc. certifies that data reported for samples received, listed on the associated custody chain or analytical task
order, were produced to specifications meeting the Quality System precision, accuracy and completeness objectives except as noted.
Estimated non-standard method measurement uncertainty data is available on request, based on quality control bias and implicit for
standard methods. Acceptable uncertainty requires tested parameter quality control data to meet method criteria.
SGS North America Inc. is not responsible for data quality assumptions if partial reports are used and recommends that this report
be used in its entirety. Data release is authorized by SGS North America Inc indicated via signature on the report cover
Friday, June 10, 2022 Page 1 of 1
4 of 15
JD460912
Summary of Hits Page 1 of 1
Job Number:JD46091
Account:Hart & Hickman
Project:LSG-001
Collected:06/01/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD46091-1 SP-1
Chromium, Hexavalent 0.84 0.44 0.25 mg/kg SW846 3060A/7199
JD46091-2 DUP-1
Chromium, Hexavalent 0.74 0.43 0.25 mg/kg SW846 3060A/7199
5 of 15
JD460913
SGS North America Inc.
Sample Results
Report of Analysis
Dayton, NJ
Section 4
6 of 15
JD460914
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SP-1
Lab Sample ID:JD46091-1 Date Sampled:06/01/22
Matrix:SO - Soil Date Received:06/04/22
Percent Solids:92.0
Project:LSG-001
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent 0.84 0.44 0.25 mg/kg 1 06/07/22 15:36 RI SW846 3060A/7199
Solids, Percent 92 %1 06/06/22 16:37 BG SM2540 G 18TH ED MOD
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
7 of 15
JD4609144.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:DUP-1
Lab Sample ID:JD46091-2 Date Sampled:06/01/22
Matrix:SO - Soil Date Received:06/04/22
Percent Solids:92.0
Project:LSG-001
General Chemistry
Analyte Result RL MDL Units DF Analyzed By Method
Chromium, Hexavalent 0.74 0.43 0.25 mg/kg 1 06/07/22 14:01 RI SW846 3060A/7199
Solids, Percent 92 %1 06/06/22 16:37 BG SM2540 G 18TH ED MOD
RL = Reporting Limit U = Indicates a result < MDL
MDL = Method Detection Limit J = Indicates a result >= MDL but < RL
8 of 15
JD4609144.2
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Dayton, NJ
Section 5
9 of 15
JD460915
5o trT yrfl trrq
CHAIN-OF-CUSTODY / Analytical Request DocumentThe Che'n-of-Custody is a LEGAL DOCUMENT. A reteva;t fietds musl be comptete{, accuralety.
cD't 6 o1 \
SAMPLE lD :t*" :iOn. Ch.Ecid F.r bor,
{A+,0.9 ', -1 : IS:mrl. rdr must b. uniqu! ;l: ;l
1zGD13z4
x E ro $cx^ruFEl
ooi
t-\,' ' t L
3 tr'.t"**" *n.*lU:nk,t *
Lrbd| Vrrffiea{cn._-.
q1,-q0
,$u*
Soerio, B
JD46091: Chain of Custody
Page 1 of 2
10 of 15
JD4609155.1
Job Number:JD46091 Client:
Date / Time Received:6/4/2022 9:45:00 AM Delivery Method:
Project:
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (Bag)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.8);
Cooler 1: (3.5);
SM089-03Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
JD46091: Chain of Custody
Page 2 of 2
11 of 15
JD4609155.1
SGS North America Inc.
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
Dayton, NJ
Section 6
12 of 15
JD460916
METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD46091
Account: HAHNCC - Hart & Hickman
Project: LSG-001
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chromium, Hexavalent GP40511/GN30030 0.40 0.0 mg/kg 40 37.5 93.8 80-120%
Chromium, Hexavalent GP40511/GN30030 mg/kg 824 801 97.2 80-120%
Chromium, Hexavalent GP40511/GN30030 mg/kg 135 91.1 67.5 28-78%
Associated Samples:
Batch GP40511: JD46091-1, JD46091-2
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
13 of 15
JD4609166.1
DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD46091
Account: HAHNCC - Hart & Hickman
Project: LSG-001
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Chromium, Hexavalent GP40511/GN30030 JD46091-2 mg/kg 0.74 0.60 20.9(a) 0-20%
Solids, Percent GN29979 JD46058-1 % 82 82.8 1.0 0-5%
Associated Samples:
Batch GN29979: JD46091-1, JD46091-2
Batch GP40511: JD46091-1, JD46091-2
(*) Outside of QC limits
(a) RPD acceptable due to low duplicate and sample concentrations.
__________________________________________________________________________________________________________________________
Page 1
14 of 15
JD4609166.2
MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: JD46091
Account: HAHNCC - Hart & Hickman
Project: LSG-001
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chromium, Hexavalent GP40511/GN30030 JD46091-2 mg/kg 0.74 1290 1350 104.2(a) 75-125%
Chromium, Hexavalent GP40511/GN30030 JD46091-2 mg/kg 0.74 44.7 45.1 99.2(b) 75-125%
Associated Samples:
Batch GP40511: JD46091-1, JD46091-2
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(a) Good recovery on insoluble XCR matrix spike. See additional comments on soluble matrix spike recovery.
(b) Good recovery on soluble XCR matrix spike. Good recovery (104 %) on the post-spike.
__________________________________________________________________________________________________________________________
Page 1
15 of 15
JD4609166.3
#=CL#
July 11, 2022
LIMS USE: FR - SHANNON COTTRILL
LIMS OBJECT ID: 92611578
92611578
Project:
Pace Project No.:
RE:
Mr. Shannon Cottrill
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
LSG-001
Dear Mr. Cottrill:
Enclosed are the analytical results for sample(s) received by the laboratory on June 23, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92611578
LSG-001
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A2LA Certification #: 2926.01*
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563*
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92611578
LSG-001
Lab ID Sample ID Matrix Date Collected Date Received
92611578001 SP-2 Solid 06/23/22 15:25 06/23/22 16:38
92611578002 DUP-2 Solid 06/23/22 00:00 06/23/22 16:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92611578
LSG-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92611578001 SP-2 EPA 6020B 7 PASI-MRJS
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92611578002 DUP-2 EPA 6020B 7 PASI-MRJS
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:SP-2 Lab ID:92611578001 Collected:06/23/22 15:25 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.4 mg/kg 07/07/22 13:01 7440-38-206/29/22 15:260.54 0.12 1
Barium 113 mg/kg 07/07/22 13:01 7440-39-3 M106/29/22 15:260.32 0.057 1
Cadmium 1.0 mg/kg 07/07/22 13:01 7440-43-906/29/22 15:260.086 0.034 1
Chromium 8.4 mg/kg 07/07/22 13:01 7440-47-306/29/22 15:262.1 0.15 1
Lead 21.4 mg/kg 07/07/22 13:01 7439-92-106/29/22 15:260.54 0.031 1
Selenium 0.37J mg/kg 07/07/22 13:01 7782-49-206/29/22 15:260.54 0.092 1
Silver ND mg/kg 07/07/22 13:01 7440-22-406/29/22 15:260.54 0.16 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.037 mg/kg 06/30/22 09:16 7439-97-606/29/22 10:390.019 0.0084 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/28/22 17:25 83-32-906/24/22 16:113651281
Acenaphthylene ND ug/kg 06/28/22 17:25 208-96-806/24/22 16:113651281
Aniline ND ug/kg 06/28/22 17:25 62-53-306/24/22 16:113651431
Anthracene ND ug/kg 06/28/22 17:25 120-12-706/24/22 16:113651201
Benzo(a)anthracene 125J ug/kg 06/28/22 17:25 56-55-306/24/22 16:113651221
Benzo(a)pyrene ND ug/kg 06/28/22 17:25 50-32-806/24/22 16:113651261
Benzo(b)fluoranthene 145J ug/kg 06/28/22 17:25 205-99-206/24/22 16:113651221
Benzo(g,h,i)perylene ND ug/kg 06/28/22 17:25 191-24-206/24/22 16:113651421
Benzo(k)fluoranthene ND ug/kg 06/28/22 17:25 207-08-906/24/22 16:113651281
Benzoic Acid ND ug/kg 06/28/22 17:25 65-85-0 M106/24/22 16:1118307851
Benzyl alcohol ND ug/kg 06/28/22 17:25 100-51-606/24/22 16:117302771
4-Bromophenylphenyl ether ND ug/kg 06/28/22 17:25 101-55-306/24/22 16:113651411
Butylbenzylphthalate ND ug/kg 06/28/22 17:25 85-68-706/24/22 16:113651541
4-Chloro-3-methylphenol ND ug/kg 06/28/22 17:25 59-50-706/24/22 16:117302571
4-Chloroaniline ND ug/kg 06/28/22 17:25 106-47-806/24/22 16:117302871
bis(2-Chloroethoxy)methane ND ug/kg 06/28/22 17:25 111-91-106/24/22 16:113651521
bis(2-Chloroethyl) ether ND ug/kg 06/28/22 17:25 111-44-4 M106/24/22 16:113651371
2-Chloronaphthalene ND ug/kg 06/28/22 17:25 91-58-706/24/22 16:113651451
2-Chlorophenol ND ug/kg 06/28/22 17:25 95-57-806/24/22 16:113651371
4-Chlorophenylphenyl ether ND ug/kg 06/28/22 17:25 7005-72-306/24/22 16:113651361
Chrysene ND ug/kg 06/28/22 17:25 218-01-906/24/22 16:113651331
Dibenz(a,h)anthracene ND ug/kg 06/28/22 17:25 53-70-306/24/22 16:113651411
Dibenzofuran ND ug/kg 06/28/22 17:25 132-64-906/24/22 16:113651321
1,2-Dichlorobenzene ND ug/kg 06/28/22 17:25 95-50-106/24/22 16:113651321
1,3-Dichlorobenzene ND ug/kg 06/28/22 17:25 541-73-106/24/22 16:113651291
1,4-Dichlorobenzene ND ug/kg 06/28/22 17:25 106-46-706/24/22 16:113651391
3,3'-Dichlorobenzidine ND ug/kg 06/28/22 17:25 91-94-1 IL06/24/22 16:117302471
2,4-Dichlorophenol ND ug/kg 06/28/22 17:25 120-83-206/24/22 16:113651431
Diethylphthalate ND ug/kg 06/28/22 17:25 84-66-206/24/22 16:113651341
2,4-Dimethylphenol ND ug/kg 06/28/22 17:25 105-67-906/24/22 16:113651521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:SP-2 Lab ID:92611578001 Collected:06/23/22 15:25 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/28/22 17:25 131-11-306/24/22 16:113651331
Di-n-butylphthalate ND ug/kg 06/28/22 17:25 84-74-206/24/22 16:113651231
4,6-Dinitro-2-methylphenol ND ug/kg 06/28/22 17:25 534-52-106/24/22 16:117303411
2,4-Dinitrophenol ND ug/kg 06/28/22 17:25 51-28-506/24/22 16:11183011301
2,4-Dinitrotoluene ND ug/kg 06/28/22 17:25 121-14-206/24/22 16:113651411
2,6-Dinitrotoluene ND ug/kg 06/28/22 17:25 606-20-206/24/22 16:113651341
Di-n-octylphthalate ND ug/kg 06/28/22 17:25 117-84-006/24/22 16:113651441
bis(2-Ethylhexyl)phthalate ND ug/kg 06/28/22 17:25 117-81-706/24/22 16:113651421
Fluoranthene 264J ug/kg 06/28/22 17:25 206-44-006/24/22 16:113651251
Fluorene ND ug/kg 06/28/22 17:25 86-73-706/24/22 16:113651281
Hexachloro-1,3-butadiene ND ug/kg 06/28/22 17:25 87-68-306/24/22 16:113651581
Hexachlorobenzene ND ug/kg 06/28/22 17:25 118-74-106/24/22 16:113651431
Hexachlorocyclopentadiene ND ug/kg 06/28/22 17:25 77-47-4 L2,M0,
v206/24/22 16:113652091
Hexachloroethane ND ug/kg 06/28/22 17:25 67-72-106/24/22 16:113651391
Indeno(1,2,3-cd)pyrene ND ug/kg 06/28/22 17:25 193-39-506/24/22 16:113651441
Isophorone ND ug/kg 06/28/22 17:25 78-59-106/24/22 16:113651631
1-Methylnaphthalene ND ug/kg 06/28/22 17:25 90-12-006/24/22 16:113651281
2-Methylnaphthalene ND ug/kg 06/28/22 17:25 91-57-606/24/22 16:113651461
2-Methylphenol(o-Cresol)ND ug/kg 06/28/22 17:25 95-48-706/24/22 16:113651491
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/28/22 17:25 15831-10-406/24/22 16:113651471
Naphthalene ND ug/kg 06/28/22 17:25 91-20-306/24/22 16:113651241
2-Nitroaniline ND ug/kg 06/28/22 17:25 88-74-406/24/22 16:1118302991
3-Nitroaniline ND ug/kg 06/28/22 17:25 99-09-206/24/22 16:1118302871
4-Nitroaniline ND ug/kg 06/28/22 17:25 100-01-606/24/22 16:117302781
Nitrobenzene ND ug/kg 06/28/22 17:25 98-95-306/24/22 16:113651691
2-Nitrophenol ND ug/kg 06/28/22 17:25 88-75-506/24/22 16:113651581
4-Nitrophenol ND ug/kg 06/28/22 17:25 100-02-706/24/22 16:1118307061
N-Nitrosodimethylamine ND ug/kg 06/28/22 17:25 62-75-906/24/22 16:113651231
N-Nitroso-di-n-propylamine ND ug/kg 06/28/22 17:25 621-64-706/24/22 16:113651371
N-Nitrosodiphenylamine ND ug/kg 06/28/22 17:25 86-30-606/24/22 16:113651291
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/28/22 17:25 108-60-106/24/22 16:113651741
Pentachlorophenol ND ug/kg 06/28/22 17:25 87-86-506/24/22 16:117303571
Phenanthrene 175J ug/kg 06/28/22 17:25 85-01-806/24/22 16:113651201
Phenol ND ug/kg 06/28/22 17:25 108-95-206/24/22 16:113651631
Pyrene 211J ug/kg 06/28/22 17:25 129-00-006/24/22 16:113651481
Pyridine ND ug/kg 06/28/22 17:25 110-86-106/24/22 16:113651151
1,2,4-Trichlorobenzene ND ug/kg 06/28/22 17:25 120-82-106/24/22 16:113651441
2,4,5-Trichlorophenol ND ug/kg 06/28/22 17:25 95-95-406/24/22 16:113651671
2,4,6-Trichlorophenol ND ug/kg 06/28/22 17:25 88-06-206/24/22 16:113651511
Surrogates
Nitrobenzene-d5 (S)68 %06/28/22 17:25 4165-60-006/24/22 16:1121-130 1
2-Fluorobiphenyl (S)66 %06/28/22 17:25 321-60-806/24/22 16:1119-130 1
Terphenyl-d14 (S)62 %06/28/22 17:25 1718-51-006/24/22 16:1115-130 1
Phenol-d6 (S)66 %06/28/22 17:25 13127-88-306/24/22 16:1118-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:SP-2 Lab ID:92611578001 Collected:06/23/22 15:25 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)54 %06/28/22 17:25 367-12-406/24/22 16:1118-130 1
2,4,6-Tribromophenol (S)58 %06/28/22 17:25 118-79-606/24/22 16:1118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/25/22 04:37 67-64-106/24/22 17:0818659.8 1
Benzene ND ug/kg 06/25/22 04:37 71-43-206/24/22 17:089.3 3.7 1
Bromobenzene ND ug/kg 06/25/22 04:37 108-86-106/24/22 17:089.3 3.0 1
Bromochloromethane ND ug/kg 06/25/22 04:37 74-97-506/24/22 17:089.3 2.8 1
Bromodichloromethane ND ug/kg 06/25/22 04:37 75-27-406/24/22 17:089.3 3.6 1
Bromoform ND ug/kg 06/25/22 04:37 75-25-206/24/22 17:089.3 3.3 1
Bromomethane ND ug/kg 06/25/22 04:37 74-83-9 IK06/24/22 17:0818.6 14.7 1
2-Butanone (MEK)87.2J ug/kg 06/25/22 04:37 78-93-306/24/22 17:0818644.7 1
n-Butylbenzene ND ug/kg 06/25/22 04:37 104-51-806/24/22 17:089.3 4.4 1
sec-Butylbenzene ND ug/kg 06/25/22 04:37 135-98-806/24/22 17:089.3 4.1 1
tert-Butylbenzene ND ug/kg 06/25/22 04:37 98-06-606/24/22 17:089.3 3.3 1
Carbon tetrachloride ND ug/kg 06/25/22 04:37 56-23-506/24/22 17:089.3 3.5 1
Chlorobenzene ND ug/kg 06/25/22 04:37 108-90-706/24/22 17:089.3 1.8 1
Chloroethane ND ug/kg 06/25/22 04:37 75-00-306/24/22 17:0818.6 7.2 1
Chloroform ND ug/kg 06/25/22 04:37 67-66-306/24/22 17:089.3 5.7 1
Chloromethane ND ug/kg 06/25/22 04:37 74-87-3 v106/24/22 17:0818.6 7.8 1
2-Chlorotoluene ND ug/kg 06/25/22 04:37 95-49-806/24/22 17:089.3 3.3 1
4-Chlorotoluene ND ug/kg 06/25/22 04:37 106-43-406/24/22 17:089.3 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/25/22 04:37 96-12-806/24/22 17:089.3 3.6 1
Dibromochloromethane ND ug/kg 06/25/22 04:37 124-48-106/24/22 17:089.3 5.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/25/22 04:37 106-93-406/24/22 17:089.3 4.1 1
Dibromomethane ND ug/kg 06/25/22 04:37 74-95-306/24/22 17:089.3 2.0 1
1,2-Dichlorobenzene ND ug/kg 06/25/22 04:37 95-50-106/24/22 17:089.3 3.4 1
1,3-Dichlorobenzene ND ug/kg 06/25/22 04:37 541-73-106/24/22 17:089.3 2.9 1
1,4-Dichlorobenzene ND ug/kg 06/25/22 04:37 106-46-706/24/22 17:089.3 2.4 1
Dichlorodifluoromethane ND ug/kg 06/25/22 04:37 75-71-8 v106/24/22 17:0818.6 4.0 1
1,1-Dichloroethane ND ug/kg 06/25/22 04:37 75-34-306/24/22 17:089.3 3.8 1
1,2-Dichloroethane ND ug/kg 06/25/22 04:37 107-06-206/24/22 17:089.3 6.2 1
1,1-Dichloroethene ND ug/kg 06/25/22 04:37 75-35-406/24/22 17:089.3 3.8 1
cis-1,2-Dichloroethene ND ug/kg 06/25/22 04:37 156-59-206/24/22 17:089.3 3.2 1
trans-1,2-Dichloroethene ND ug/kg 06/25/22 04:37 156-60-506/24/22 17:089.3 3.3 1
1,2-Dichloropropane ND ug/kg 06/25/22 04:37 78-87-506/24/22 17:089.3 2.8 1
1,3-Dichloropropane ND ug/kg 06/25/22 04:37 142-28-906/24/22 17:089.3 2.9 1
2,2-Dichloropropane ND ug/kg 06/25/22 04:37 594-20-706/24/22 17:089.3 3.0 1
1,1-Dichloropropene ND ug/kg 06/25/22 04:37 563-58-606/24/22 17:089.3 4.5 1
cis-1,3-Dichloropropene ND ug/kg 06/25/22 04:37 10061-01-506/24/22 17:089.3 2.5 1
trans-1,3-Dichloropropene ND ug/kg 06/25/22 04:37 10061-02-606/24/22 17:089.3 3.2 1
Diisopropyl ether ND ug/kg 06/25/22 04:37 108-20-306/24/22 17:089.3 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:SP-2 Lab ID:92611578001 Collected:06/23/22 15:25 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/25/22 04:37 100-41-406/24/22 17:089.3 4.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/25/22 04:37 87-68-306/24/22 17:0818.6 15.2 1
2-Hexanone ND ug/kg 06/25/22 04:37 591-78-606/24/22 17:0893.1 9.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/25/22 04:37 98-82-806/24/22 17:089.3 3.2 1
p-Isopropyltoluene ND ug/kg 06/25/22 04:37 99-87-606/24/22 17:089.3 4.6 1
Methylene Chloride ND ug/kg 06/25/22 04:37 75-09-206/24/22 17:0837.2 25.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/25/22 04:37 108-10-106/24/22 17:0893.1 9.0 1
Methyl-tert-butyl ether ND ug/kg 06/25/22 04:37 1634-04-406/24/22 17:089.3 3.5 1
Naphthalene ND ug/kg 06/25/22 04:37 91-20-306/24/22 17:089.3 4.9 1
n-Propylbenzene ND ug/kg 06/25/22 04:37 103-65-106/24/22 17:089.3 3.3 1
Styrene ND ug/kg 06/25/22 04:37 100-42-5 IK06/24/22 17:089.3 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/25/22 04:37 630-20-606/24/22 17:089.3 3.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/25/22 04:37 79-34-506/24/22 17:089.3 2.5 1
Tetrachloroethene ND ug/kg 06/25/22 04:37 127-18-406/24/22 17:089.3 2.9 1
Toluene 9.3 ug/kg 06/25/22 04:37 108-88-3 IK06/24/22 17:089.3 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/25/22 04:37 87-61-606/24/22 17:089.3 7.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/25/22 04:37 120-82-106/24/22 17:089.3 7.8 1
1,1,1-Trichloroethane ND ug/kg 06/25/22 04:37 71-55-606/24/22 17:089.3 4.8 1
1,1,2-Trichloroethane ND ug/kg 06/25/22 04:37 79-00-506/24/22 17:089.3 3.1 1
Trichloroethene ND ug/kg 06/25/22 04:37 79-01-606/24/22 17:089.3 2.4 1
Trichlorofluoromethane ND ug/kg 06/25/22 04:37 75-69-406/24/22 17:089.3 5.1 1
1,2,3-Trichloropropane ND ug/kg 06/25/22 04:37 96-18-406/24/22 17:089.3 4.7 1
1,2,4-Trimethylbenzene ND ug/kg 06/25/22 04:37 95-63-606/24/22 17:089.3 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/25/22 04:37 108-67-806/24/22 17:089.3 3.1 1
Vinyl acetate ND ug/kg 06/25/22 04:37 108-05-406/24/22 17:0893.1 6.8 1
Vinyl chloride ND ug/kg 06/25/22 04:37 75-01-406/24/22 17:0818.6 4.7 1
Xylene (Total)ND ug/kg 06/25/22 04:37 1330-20-706/24/22 17:0818.6 5.3 1
m&p-Xylene ND ug/kg 06/25/22 04:37 179601-23-106/24/22 17:0818.6 6.4 1
o-Xylene ND ug/kg 06/25/22 04:37 95-47-606/24/22 17:089.3 4.1 1
Surrogates
Toluene-d8 (S)100 %06/25/22 04:37 2037-26-506/24/22 17:0870-130 1
4-Bromofluorobenzene (S)100 %06/25/22 04:37 460-00-406/24/22 17:0869-134 1
1,2-Dichloroethane-d4 (S)99 %06/25/22 04:37 17060-07-006/24/22 17:0870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.9 %06/24/22 13:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:DUP-2 Lab ID:92611578002 Collected:06/23/22 00:00 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.1 mg/kg 07/07/22 13:20 7440-38-206/29/22 15:260.56 0.12 1
Barium 93.3 mg/kg 07/07/22 13:20 7440-39-306/29/22 15:260.34 0.060 1
Cadmium 1.1 mg/kg 07/07/22 13:20 7440-43-906/29/22 15:260.089 0.035 1
Chromium 7.3 mg/kg 07/07/22 13:20 7440-47-306/29/22 15:262.2 0.16 1
Lead 19.0 mg/kg 07/07/22 13:20 7439-92-106/29/22 15:260.56 0.033 1
Selenium 0.32J mg/kg 07/07/22 13:20 7782-49-206/29/22 15:260.56 0.096 1
Silver ND mg/kg 07/07/22 13:20 7440-22-406/29/22 15:260.56 0.16 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.029 mg/kg 06/30/22 09:21 7439-97-606/29/22 10:390.021 0.0091 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/29/22 09:34 83-32-906/28/22 10:003901371
Acenaphthylene ND ug/kg 06/29/22 09:34 208-96-806/28/22 10:003901371
Aniline ND ug/kg 06/29/22 09:34 62-53-306/28/22 10:003901521
Anthracene ND ug/kg 06/29/22 09:34 120-12-706/28/22 10:003901281
Benzo(a)anthracene 219J ug/kg 06/29/22 09:34 56-55-306/28/22 10:003901301
Benzo(a)pyrene 212J ug/kg 06/29/22 09:34 50-32-806/28/22 10:003901351
Benzo(b)fluoranthene 272J ug/kg 06/29/22 09:34 205-99-206/28/22 10:003901301
Benzo(g,h,i)perylene ND ug/kg 06/29/22 09:34 191-24-2 v206/28/22 10:003901511
Benzo(k)fluoranthene ND ug/kg 06/29/22 09:34 207-08-906/28/22 10:003901371
Benzoic Acid ND ug/kg 06/29/22 09:34 65-85-0 M106/28/22 10:0019508381
Benzyl alcohol ND ug/kg 06/29/22 09:34 100-51-606/28/22 10:007802961
4-Bromophenylphenyl ether ND ug/kg 06/29/22 09:34 101-55-306/28/22 10:003901501
Butylbenzylphthalate ND ug/kg 06/29/22 09:34 85-68-706/28/22 10:003901641
4-Chloro-3-methylphenol ND ug/kg 06/29/22 09:34 59-50-706/28/22 10:007802741
4-Chloroaniline ND ug/kg 06/29/22 09:34 106-47-806/28/22 10:007803061
bis(2-Chloroethoxy)methane ND ug/kg 06/29/22 09:34 111-91-106/28/22 10:003901621
bis(2-Chloroethyl) ether ND ug/kg 06/29/22 09:34 111-44-4 M106/28/22 10:003901471
2-Chloronaphthalene ND ug/kg 06/29/22 09:34 91-58-706/28/22 10:003901551
2-Chlorophenol ND ug/kg 06/29/22 09:34 95-57-806/28/22 10:003901471
4-Chlorophenylphenyl ether ND ug/kg 06/29/22 09:34 7005-72-306/28/22 10:003901451
Chrysene 225J ug/kg 06/29/22 09:34 218-01-906/28/22 10:003901421
Dibenz(a,h)anthracene ND ug/kg 06/29/22 09:34 53-70-306/28/22 10:003901501
Dibenzofuran ND ug/kg 06/29/22 09:34 132-64-906/28/22 10:003901411
1,2-Dichlorobenzene ND ug/kg 06/29/22 09:34 95-50-106/28/22 10:003901411
1,3-Dichlorobenzene ND ug/kg 06/29/22 09:34 541-73-106/28/22 10:003901381
1,4-Dichlorobenzene ND ug/kg 06/29/22 09:34 106-46-706/28/22 10:003901491
3,3'-Dichlorobenzidine ND ug/kg 06/29/22 09:34 91-94-1 IL06/28/22 10:007802641
2,4-Dichlorophenol ND ug/kg 06/29/22 09:34 120-83-206/28/22 10:003901521
Diethylphthalate ND ug/kg 06/29/22 09:34 84-66-206/28/22 10:003901431
2,4-Dimethylphenol ND ug/kg 06/29/22 09:34 105-67-906/28/22 10:003901621
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:DUP-2 Lab ID:92611578002 Collected:06/23/22 00:00 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/29/22 09:34 131-11-306/28/22 10:003901421
Di-n-butylphthalate ND ug/kg 06/29/22 09:34 84-74-206/28/22 10:003901311
4,6-Dinitro-2-methylphenol ND ug/kg 06/29/22 09:34 534-52-1 R106/28/22 10:007803641
2,4-Dinitrophenol ND ug/kg 06/29/22 09:34 51-28-506/28/22 10:00195012101
2,4-Dinitrotoluene ND ug/kg 06/29/22 09:34 121-14-206/28/22 10:003901501
2,6-Dinitrotoluene ND ug/kg 06/29/22 09:34 606-20-206/28/22 10:003901431
Di-n-octylphthalate ND ug/kg 06/29/22 09:34 117-84-006/28/22 10:003901541
bis(2-Ethylhexyl)phthalate ND ug/kg 06/29/22 09:34 117-81-706/28/22 10:003901511
Fluoranthene 449 ug/kg 06/29/22 09:34 206-44-006/28/22 10:003901341
Fluorene ND ug/kg 06/29/22 09:34 86-73-706/28/22 10:003901371
Hexachloro-1,3-butadiene ND ug/kg 06/29/22 09:34 87-68-306/28/22 10:003901691
Hexachlorobenzene ND ug/kg 06/29/22 09:34 118-74-106/28/22 10:003901521
Hexachlorocyclopentadiene ND ug/kg 06/29/22 09:34 77-47-4 R1,v206/28/22 10:003902231
Hexachloroethane ND ug/kg 06/29/22 09:34 67-72-106/28/22 10:003901491
Indeno(1,2,3-cd)pyrene ND ug/kg 06/29/22 09:34 193-39-506/28/22 10:003901541
Isophorone ND ug/kg 06/29/22 09:34 78-59-106/28/22 10:003901741
1-Methylnaphthalene ND ug/kg 06/29/22 09:34 90-12-006/28/22 10:003901371
2-Methylnaphthalene ND ug/kg 06/29/22 09:34 91-57-606/28/22 10:003901561
2-Methylphenol(o-Cresol)ND ug/kg 06/29/22 09:34 95-48-706/28/22 10:003901601
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/29/22 09:34 15831-10-4 v206/28/22 10:003901571
Naphthalene ND ug/kg 06/29/22 09:34 91-20-306/28/22 10:003901321
2-Nitroaniline ND ug/kg 06/29/22 09:34 88-74-406/28/22 10:0019503191
3-Nitroaniline ND ug/kg 06/29/22 09:34 99-09-2 IL06/28/22 10:0019503061
4-Nitroaniline ND ug/kg 06/29/22 09:34 100-01-6 IL06/28/22 10:007802971
Nitrobenzene ND ug/kg 06/29/22 09:34 98-95-306/28/22 10:003901811
2-Nitrophenol ND ug/kg 06/29/22 09:34 88-75-506/28/22 10:003901691
4-Nitrophenol ND ug/kg 06/29/22 09:34 100-02-7 v206/28/22 10:0019507541
N-Nitrosodimethylamine ND ug/kg 06/29/22 09:34 62-75-906/28/22 10:003901311
N-Nitroso-di-n-propylamine ND ug/kg 06/29/22 09:34 621-64-706/28/22 10:003901471
N-Nitrosodiphenylamine ND ug/kg 06/29/22 09:34 86-30-606/28/22 10:003901381
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/29/22 09:34 108-60-1 v106/28/22 10:003901861
Pentachlorophenol ND ug/kg 06/29/22 09:34 87-86-506/28/22 10:007803821
Phenanthrene 319J ug/kg 06/29/22 09:34 85-01-806/28/22 10:003901281
Phenol ND ug/kg 06/29/22 09:34 108-95-206/28/22 10:003901741
Pyrene 407 ug/kg 06/29/22 09:34 129-00-006/28/22 10:003901581
Pyridine ND ug/kg 06/29/22 09:34 110-86-106/28/22 10:003901231
1,2,4-Trichlorobenzene ND ug/kg 06/29/22 09:34 120-82-106/28/22 10:003901541
2,4,5-Trichlorophenol ND ug/kg 06/29/22 09:34 95-95-406/28/22 10:003901791
2,4,6-Trichlorophenol ND ug/kg 06/29/22 09:34 88-06-206/28/22 10:003901611
Surrogates
Nitrobenzene-d5 (S)67 %06/29/22 09:34 4165-60-006/28/22 10:0021-130 1
2-Fluorobiphenyl (S)64 %06/29/22 09:34 321-60-806/28/22 10:0019-130 1
Terphenyl-d14 (S)79 %06/29/22 09:34 1718-51-006/28/22 10:0015-130 1
Phenol-d6 (S)69 %06/29/22 09:34 13127-88-306/28/22 10:0018-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:DUP-2 Lab ID:92611578002 Collected:06/23/22 00:00 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)57 %06/29/22 09:34 367-12-406/28/22 10:0018-130 1
2,4,6-Tribromophenol (S)92 %06/29/22 09:34 118-79-606/28/22 10:0018-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/25/22 04:19 67-64-106/24/22 17:0820866.8 1
Benzene ND ug/kg 06/25/22 04:19 71-43-206/24/22 17:0810.4 4.1 1
Bromobenzene ND ug/kg 06/25/22 04:19 108-86-106/24/22 17:0810.4 3.4 1
Bromochloromethane ND ug/kg 06/25/22 04:19 74-97-506/24/22 17:0810.4 3.1 1
Bromodichloromethane ND ug/kg 06/25/22 04:19 75-27-406/24/22 17:0810.4 4.0 1
Bromoform ND ug/kg 06/25/22 04:19 75-25-206/24/22 17:0810.4 3.7 1
Bromomethane ND ug/kg 06/25/22 04:19 74-83-9 IK06/24/22 17:0820.8 16.4 1
2-Butanone (MEK)104J ug/kg 06/25/22 04:19 78-93-306/24/22 17:0820849.9 1
n-Butylbenzene ND ug/kg 06/25/22 04:19 104-51-806/24/22 17:0810.4 4.9 1
sec-Butylbenzene ND ug/kg 06/25/22 04:19 135-98-806/24/22 17:0810.4 4.6 1
tert-Butylbenzene ND ug/kg 06/25/22 04:19 98-06-606/24/22 17:0810.4 3.7 1
Carbon tetrachloride ND ug/kg 06/25/22 04:19 56-23-506/24/22 17:0810.4 3.9 1
Chlorobenzene ND ug/kg 06/25/22 04:19 108-90-706/24/22 17:0810.4 2.0 1
Chloroethane ND ug/kg 06/25/22 04:19 75-00-306/24/22 17:0820.8 8.0 1
Chloroform ND ug/kg 06/25/22 04:19 67-66-306/24/22 17:0810.4 6.3 1
Chloromethane ND ug/kg 06/25/22 04:19 74-87-3 v106/24/22 17:0820.8 8.7 1
2-Chlorotoluene ND ug/kg 06/25/22 04:19 95-49-806/24/22 17:0810.4 3.7 1
4-Chlorotoluene ND ug/kg 06/25/22 04:19 106-43-406/24/22 17:0810.4 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/25/22 04:19 96-12-806/24/22 17:0810.4 4.0 1
Dibromochloromethane ND ug/kg 06/25/22 04:19 124-48-106/24/22 17:0810.4 5.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/25/22 04:19 106-93-406/24/22 17:0810.4 4.6 1
Dibromomethane ND ug/kg 06/25/22 04:19 74-95-306/24/22 17:0810.4 2.2 1
1,2-Dichlorobenzene ND ug/kg 06/25/22 04:19 95-50-106/24/22 17:0810.4 3.7 1
1,3-Dichlorobenzene ND ug/kg 06/25/22 04:19 541-73-106/24/22 17:0810.4 3.2 1
1,4-Dichlorobenzene ND ug/kg 06/25/22 04:19 106-46-706/24/22 17:0810.4 2.7 1
Dichlorodifluoromethane ND ug/kg 06/25/22 04:19 75-71-8 v106/24/22 17:0820.8 4.5 1
1,1-Dichloroethane ND ug/kg 06/25/22 04:19 75-34-306/24/22 17:0810.4 4.3 1
1,2-Dichloroethane ND ug/kg 06/25/22 04:19 107-06-206/24/22 17:0810.4 6.9 1
1,1-Dichloroethene ND ug/kg 06/25/22 04:19 75-35-406/24/22 17:0810.4 4.3 1
cis-1,2-Dichloroethene ND ug/kg 06/25/22 04:19 156-59-206/24/22 17:0810.4 3.6 1
trans-1,2-Dichloroethene ND ug/kg 06/25/22 04:19 156-60-506/24/22 17:0810.4 3.6 1
1,2-Dichloropropane ND ug/kg 06/25/22 04:19 78-87-506/24/22 17:0810.4 3.1 1
1,3-Dichloropropane ND ug/kg 06/25/22 04:19 142-28-906/24/22 17:0810.4 3.2 1
2,2-Dichloropropane ND ug/kg 06/25/22 04:19 594-20-706/24/22 17:0810.4 3.4 1
1,1-Dichloropropene ND ug/kg 06/25/22 04:19 563-58-606/24/22 17:0810.4 5.0 1
cis-1,3-Dichloropropene ND ug/kg 06/25/22 04:19 10061-01-506/24/22 17:0810.4 2.8 1
trans-1,3-Dichloropropene ND ug/kg 06/25/22 04:19 10061-02-606/24/22 17:0810.4 3.6 1
Diisopropyl ether ND ug/kg 06/25/22 04:19 108-20-306/24/22 17:0810.4 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92611578
LSG-001
Sample:DUP-2 Lab ID:92611578002 Collected:06/23/22 00:00 Received:06/23/22 16:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/25/22 04:19 100-41-406/24/22 17:0810.4 4.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/25/22 04:19 87-68-306/24/22 17:0820.8 17.0 1
2-Hexanone ND ug/kg 06/25/22 04:19 591-78-606/24/22 17:0810410.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/25/22 04:19 98-82-806/24/22 17:0810.4 3.5 1
p-Isopropyltoluene ND ug/kg 06/25/22 04:19 99-87-606/24/22 17:0810.4 5.1 1
Methylene Chloride ND ug/kg 06/25/22 04:19 75-09-206/24/22 17:0841.6 28.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/25/22 04:19 108-10-106/24/22 17:0810410.0 1
Methyl-tert-butyl ether ND ug/kg 06/25/22 04:19 1634-04-406/24/22 17:0810.4 3.9 1
Naphthalene ND ug/kg 06/25/22 04:19 91-20-306/24/22 17:0810.4 5.5 1
n-Propylbenzene ND ug/kg 06/25/22 04:19 103-65-106/24/22 17:0810.4 3.7 1
Styrene ND ug/kg 06/25/22 04:19 100-42-5 IK06/24/22 17:0810.4 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/25/22 04:19 630-20-606/24/22 17:0810.4 4.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/25/22 04:19 79-34-506/24/22 17:0810.4 2.7 1
Tetrachloroethene ND ug/kg 06/25/22 04:19 127-18-406/24/22 17:0810.4 3.3 1
Toluene 7.8J ug/kg 06/25/22 04:19 108-88-3 IK06/24/22 17:0810.4 3.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/25/22 04:19 87-61-606/24/22 17:0810.4 8.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/25/22 04:19 120-82-106/24/22 17:0810.4 8.7 1
1,1,1-Trichloroethane ND ug/kg 06/25/22 04:19 71-55-606/24/22 17:0810.4 5.4 1
1,1,2-Trichloroethane ND ug/kg 06/25/22 04:19 79-00-506/24/22 17:0810.4 3.5 1
Trichloroethene ND ug/kg 06/25/22 04:19 79-01-606/24/22 17:0810.4 2.7 1
Trichlorofluoromethane ND ug/kg 06/25/22 04:19 75-69-406/24/22 17:0810.4 5.7 1
1,2,3-Trichloropropane ND ug/kg 06/25/22 04:19 96-18-406/24/22 17:0810.4 5.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/25/22 04:19 95-63-606/24/22 17:0810.4 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/25/22 04:19 108-67-806/24/22 17:0810.4 3.5 1
Vinyl acetate ND ug/kg 06/25/22 04:19 108-05-406/24/22 17:081047.6 1
Vinyl chloride ND ug/kg 06/25/22 04:19 75-01-406/24/22 17:0820.8 5.3 1
Xylene (Total)ND ug/kg 06/25/22 04:19 1330-20-706/24/22 17:0820.8 5.9 1
m&p-Xylene ND ug/kg 06/25/22 04:19 179601-23-106/24/22 17:0820.8 7.1 1
o-Xylene ND ug/kg 06/25/22 04:19 95-47-606/24/22 17:0810.4 4.6 1
Surrogates
Toluene-d8 (S)100 %06/25/22 04:19 2037-26-506/24/22 17:0870-130 1
4-Bromofluorobenzene (S)100 %06/25/22 04:19 460-00-406/24/22 17:0869-134 1
1,2-Dichloroethane-d4 (S)97 %06/25/22 04:19 17060-07-006/24/22 17:0870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.4 %06/24/22 13:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
824638
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92611578001, 92611578002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4368485
Associated Lab Samples:92611578001, 92611578002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.018 06/30/22 09:130.0078
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4368486LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.500.49 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4368487MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578001
4368488
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.5 100 80-12099 2 200.4890.037 0.53 0.52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
824633
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92611578001, 92611578002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4368465
Associated Lab Samples:92611578001, 92611578002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.49 07/07/22 12:540.11
Barium mg/kg ND 0.29 07/07/22 12:540.052
Cadmium mg/kg 0.038J 0.078 07/08/22 16:580.031
Chromium mg/kg ND 2.0 07/07/22 12:540.14
Lead mg/kg ND 0.49 07/07/22 12:540.029
Selenium mg/kg ND 0.49 07/07/22 12:540.084
Silver mg/kg ND 0.49 07/07/22 12:540.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4368466LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 45.648.4 94 80-120
Barium mg/kg 46.548.4 96 80-120
Cadmium mg/kg 47.348.4 98 80-120
Chromium mg/kg 48.448.4 100 80-120
Lead mg/kg 47.048.4 97 80-120
Selenium mg/kg 47.048.4 97 80-120
Silver mg/kg 24.824.2 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4368467MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578001
4368468
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 53.3 84 75-12576 9 2053.51.4 46.0 42.3
Barium mg/kg M153.3 100 75-125138 12 2053.5113 166 187
Cadmium mg/kg 53.3 93 75-12585 8 2053.51.0 50.6 46.7
Chromium mg/kg 53.3 97 75-12588 8 2053.58.4 59.9 55.5
Lead mg/kg 53.3 96 75-125103 5 2053.521.4 72.5 76.4
Selenium mg/kg 53.3 91 75-12586 6 2053.50.37J 49.1 46.3
Silver mg/kg 26.7 99 75-12591 8 2026.8ND 26.4 24.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
706927
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92611578001, 92611578002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3688119
Associated Lab Samples:92611578001, 92611578002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/25/22 01:221.9
1,1,1-Trichloroethane ug/kg ND 5.0 06/25/22 01:222.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/25/22 01:221.3
1,1,2-Trichloroethane ug/kg ND 5.0 06/25/22 01:221.7
1,1-Dichloroethane ug/kg ND 5.0 06/25/22 01:222.1
1,1-Dichloroethene ug/kg ND 5.0 06/25/22 01:222.1
1,1-Dichloropropene ug/kg ND 5.0 06/25/22 01:222.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/25/22 01:224.0
1,2,3-Trichloropropane ug/kg ND 5.0 06/25/22 01:222.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/25/22 01:224.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/25/22 01:221.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/25/22 01:221.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/25/22 01:222.2
1,2-Dichlorobenzene ug/kg ND 5.0 06/25/22 01:221.8
1,2-Dichloroethane ug/kg ND 5.0 06/25/22 01:223.3
1,2-Dichloropropane ug/kg ND 5.0 06/25/22 01:221.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/25/22 01:221.7
1,3-Dichlorobenzene ug/kg ND 5.0 06/25/22 01:221.6
1,3-Dichloropropane ug/kg ND 5.0 06/25/22 01:221.6
1,4-Dichlorobenzene ug/kg ND 5.0 06/25/22 01:221.3
2,2-Dichloropropane ug/kg ND 5.0 06/25/22 01:221.6
2-Butanone (MEK)ug/kg ND 100 06/25/22 01:2224.0
2-Chlorotoluene ug/kg ND 5.0 06/25/22 01:221.8
2-Hexanone ug/kg ND 50.0 06/25/22 01:224.8
4-Chlorotoluene ug/kg ND 5.0 06/25/22 01:220.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/25/22 01:224.8
Acetone ug/kg ND 100 06/25/22 01:2232.1
Benzene ug/kg ND 5.0 06/25/22 01:222.0
Bromobenzene ug/kg ND 5.0 06/25/22 01:221.6
Bromochloromethane ug/kg ND 5.0 06/25/22 01:221.5
Bromodichloromethane ug/kg ND 5.0 06/25/22 01:221.9
Bromoform ug/kg ND 5.0 06/25/22 01:221.8
Bromomethane ug/kg ND 10.0 IK06/25/22 01:227.9
Carbon tetrachloride ug/kg ND 5.0 06/25/22 01:221.9
Chlorobenzene ug/kg ND 5.0 06/25/22 01:220.96
Chloroethane ug/kg ND 10.0 06/25/22 01:223.9
Chloroform ug/kg 3.6J 5.0 06/25/22 01:223.0
Chloromethane ug/kg ND 10.0 v106/25/22 01:224.2
cis-1,2-Dichloroethene ug/kg ND 5.0 06/25/22 01:221.7
cis-1,3-Dichloropropene ug/kg ND 5.0 06/25/22 01:221.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3688119
Associated Lab Samples:92611578001, 92611578002
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 06/25/22 01:222.8
Dibromomethane ug/kg ND 5.0 06/25/22 01:221.1
Dichlorodifluoromethane ug/kg ND 10.0 v106/25/22 01:222.2
Diisopropyl ether ug/kg ND 5.0 06/25/22 01:221.4
Ethylbenzene ug/kg ND 5.0 06/25/22 01:222.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/25/22 01:228.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/25/22 01:221.7
m&p-Xylene ug/kg ND 10.0 06/25/22 01:223.4
Methyl-tert-butyl ether ug/kg ND 5.0 06/25/22 01:221.9
Methylene Chloride ug/kg ND 20.0 06/25/22 01:2213.7
n-Butylbenzene ug/kg ND 5.0 06/25/22 01:222.4
n-Propylbenzene ug/kg ND 5.0 06/25/22 01:221.8
Naphthalene ug/kg ND 5.0 06/25/22 01:222.6
o-Xylene ug/kg ND 5.0 06/25/22 01:222.2
p-Isopropyltoluene ug/kg ND 5.0 06/25/22 01:222.5
sec-Butylbenzene ug/kg ND 5.0 06/25/22 01:222.2
Styrene ug/kg ND 5.0 IK06/25/22 01:221.3
tert-Butylbenzene ug/kg ND 5.0 06/25/22 01:221.8
Tetrachloroethene ug/kg ND 5.0 06/25/22 01:221.6
Toluene ug/kg ND 5.0 IK06/25/22 01:221.4
trans-1,2-Dichloroethene ug/kg ND 5.0 06/25/22 01:221.8
trans-1,3-Dichloropropene ug/kg ND 5.0 06/25/22 01:221.7
Trichloroethene ug/kg ND 5.0 06/25/22 01:221.3
Trichlorofluoromethane ug/kg ND 5.0 06/25/22 01:222.8
Vinyl acetate ug/kg ND 50.0 06/25/22 01:223.6
Vinyl chloride ug/kg ND 10.0 06/25/22 01:222.5
Xylene (Total)ug/kg ND 10.0 06/25/22 01:222.8
1,2-Dichloroethane-d4 (S)%103 70-130 06/25/22 01:22
4-Bromofluorobenzene (S)%98 69-134 06/25/22 01:22
Toluene-d8 (S)%100 70-130 06/25/22 01:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3688120LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13001250 104 70-130
1,1,1-Trichloroethane ug/kg 13201250 105 70-130
1,1,2,2-Tetrachloroethane ug/kg 12901250 103 70-130
1,1,2-Trichloroethane ug/kg 13301250 106 70-130
1,1-Dichloroethane ug/kg 12501250 100 70-130
1,1-Dichloroethene ug/kg 13301250 107 70-130
1,1-Dichloropropene ug/kg 13401250 107 70-130
1,2,3-Trichlorobenzene ug/kg 12501250 100 65-130
1,2,3-Trichloropropane ug/kg 12901250 103 70-130
1,2,4-Trichlorobenzene ug/kg 12801250 102 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3688120LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12701250 102 70-130
1,2-Dibromo-3-chloropropane ug/kg 14701250 118 70-130
1,2-Dibromoethane (EDB)ug/kg 12501250 100 70-130
1,2-Dichlorobenzene ug/kg 12701250 102 70-130
1,2-Dichloroethane ug/kg 12401250 99 63-130
1,2-Dichloropropane ug/kg 12901250 103 70-130
1,3,5-Trimethylbenzene ug/kg 13001250 104 70-130
1,3-Dichlorobenzene ug/kg 12901250 103 70-130
1,3-Dichloropropane ug/kg 12001250 96 70-130
1,4-Dichlorobenzene ug/kg 12201250 97 70-130
2,2-Dichloropropane ug/kg 13501250 108 66-130
2-Butanone (MEK)ug/kg 26302500 105 70-130
2-Chlorotoluene ug/kg 12701250 102 70-130
2-Hexanone ug/kg 29002500 116 70-130
4-Chlorotoluene ug/kg 12601250 101 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 28202500 113 70-130
Acetone ug/kg 25902500 103 69-130
Benzene ug/kg 12201250 98 70-130
Bromobenzene ug/kg 12601250 100 70-130
Bromochloromethane ug/kg 13001250 104 70-130
Bromodichloromethane ug/kg 13001250 104 69-130
Bromoform ug/kg 13901250 111 70-130
Bromomethane ug/kg 1260 IK125010152-130
Carbon tetrachloride ug/kg 13601250 109 70-130
Chlorobenzene ug/kg 12101250 97 70-130
Chloroethane ug/kg 14701250 118 65-130
Chloroform ug/kg 12301250 99 70-130
Chloromethane ug/kg 1540 v1125012355-130
cis-1,2-Dichloroethene ug/kg 12601250 101 70-130
cis-1,3-Dichloropropene ug/kg 13301250 106 70-130
Dibromochloromethane ug/kg 12801250 103 70-130
Dibromomethane ug/kg 13301250 107 70-130
Dichlorodifluoromethane ug/kg 1520 v1125012245-156
Diisopropyl ether ug/kg 12401250 99 70-130
Ethylbenzene ug/kg 11201250 90 70-130
Hexachloro-1,3-butadiene ug/kg 12501250 100 66-130
Isopropylbenzene (Cumene)ug/kg 12201250 98 70-130
m&p-Xylene ug/kg 23602500 94 70-130
Methyl-tert-butyl ether ug/kg 11701250 94 70-130
Methylene Chloride ug/kg 10201250 82 65-130
n-Butylbenzene ug/kg 12901250 103 67-130
n-Propylbenzene ug/kg 12701250 102 70-130
Naphthalene ug/kg 13801250 110 70-130
o-Xylene ug/kg 11901250 95 70-130
p-Isopropyltoluene ug/kg 13301250 106 67-130
sec-Butylbenzene ug/kg 12801250 102 69-130
Styrene ug/kg 1190 IK12509570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3688120LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13201250 106 67-130
Tetrachloroethene ug/kg 12701250 102 70-130
Toluene ug/kg 1230 IK12509870-130
trans-1,2-Dichloroethene ug/kg 13101250 105 70-130
trans-1,3-Dichloropropene ug/kg 13601250 109 68-130
Trichloroethene ug/kg 13101250 105 70-130
Trichlorofluoromethane ug/kg 12601250 101 70-130
Vinyl acetate ug/kg 27602500 110 70-130
Vinyl chloride ug/kg 14701250 118 61-130
Xylene (Total)ug/kg 35503750 95 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%95 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3688121MATRIX SPIKE SAMPLE:
MSSpike
Result
92611736001
1,1,1,2-Tetrachloroethane ug/kg 808617 131 70-131ND
1,1,1-Trichloroethane ug/kg 864 M161714065-133ND
1,1,2,2-Tetrachloroethane ug/kg 790617 128 66-130ND
1,1,2-Trichloroethane ug/kg 816617 132 66-133ND
1,1-Dichloroethane ug/kg 795617 129 65-130ND
1,1-Dichloroethene ug/kg 926617 150 10-158ND
1,1-Dichloropropene ug/kg 916 M161714868-133ND
1,2,3-Trichlorobenzene ug/kg 260617 42 27-138ND
1,2,3-Trichloropropane ug/kg 751617 122 67-130ND
1,2,4-Trichlorobenzene ug/kg 492617 80 51-134ND
1,2,4-Trimethylbenzene ug/kg 832617 135 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 579617 94 32-130ND
1,2-Dibromoethane (EDB)ug/kg 801617 130 70-130ND
1,2-Dichlorobenzene ug/kg 795617 129 69-130ND
1,2-Dichloroethane ug/kg 780617 126 59-130ND
1,2-Dichloropropane ug/kg 841 M161713670-130ND
1,3,5-Trimethylbenzene ug/kg 857 M161713965-137ND
1,3-Dichlorobenzene ug/kg 799617 129 70-130ND
1,3-Dichloropropane ug/kg 790617 128 70-130ND
1,4-Dichlorobenzene ug/kg 768617 124 68-130ND
2,2-Dichloropropane ug/kg 801617 130 32-130ND
2-Butanone (MEK)ug/kg 15701230 124 10-13646.0J
2-Chlorotoluene ug/kg 819617 133 69-141ND
2-Hexanone ug/kg 15901230 129 10-144ND
4-Chlorotoluene ug/kg 798617 129 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 16201230 131 25-143ND
Acetone ug/kg 13501230 109 10-130ND
Benzene ug/kg 828 M161713467-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3688121MATRIX SPIKE SAMPLE:
MSSpike
Result
92611736001
Bromobenzene ug/kg 797617 129 70-130ND
Bromochloromethane ug/kg 805617 130 69-134ND
Bromodichloromethane ug/kg 745617 121 64-130ND
Bromoform ug/kg 730617 118 62-130ND
Bromomethane ug/kg 629 IK61710220-176ND
Carbon tetrachloride ug/kg 853617 138 65-140ND
Chlorobenzene ug/kg 822 M161713370-130ND
Chloroethane ug/kg 314617 51 10-130ND
Chloroform ug/kg 797617 129 63-130ND
Chloromethane ug/kg 1050 M1,v161716958-130ND
cis-1,2-Dichloroethene ug/kg 826 M161713466-130ND
cis-1,3-Dichloropropene ug/kg 783617 127 67-130ND
Dibromochloromethane ug/kg 723617 117 67-130ND
Dibromomethane ug/kg 813 M161713263-131ND
Dichlorodifluoromethane ug/kg 1090 v161717744-180ND
Diisopropyl ether ug/kg 819 M161713363-130ND
Ethylbenzene ug/kg 764617 124 66-130ND
Hexachloro-1,3-butadiene ug/kg 707617 115 64-150ND
Isopropylbenzene (Cumene)ug/kg 838 M161713669-135ND
m&p-Xylene ug/kg 15901230 129 60-133ND
Methyl-tert-butyl ether ug/kg 739617 120 65-130ND
Methylene Chloride ug/kg 554617 90 61-130ND
n-Butylbenzene ug/kg 827617 134 65-140ND
n-Propylbenzene ug/kg 832617 135 67-140ND
Naphthalene ug/kg 304617 49 15-145ND
o-Xylene ug/kg 808617 131 66-133ND
p-Isopropyltoluene ug/kg 882617 143 56-147ND
sec-Butylbenzene ug/kg 865 M161714065-139ND
Styrene ug/kg 771 IK61712570-132ND
tert-Butylbenzene ug/kg 839 M161713662-135ND
Tetrachloroethene ug/kg 825617 134 70-135ND
Toluene ug/kg 813 IK,M161713267-130ND
trans-1,2-Dichloroethene ug/kg 887 M161714469-130ND
trans-1,3-Dichloropropene ug/kg 769617 124 62-130ND
Trichloroethene ug/kg 868 M161714170-135ND
Trichlorofluoromethane ug/kg 312617 51 10-130ND
Vinyl acetate ug/kg 15901230 129 53-130ND
Vinyl chloride ug/kg 943 M161715361-148ND
Xylene (Total)ug/kg 24001860 129 63-132ND
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92611736002
3688122SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 3052.6J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND v130ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92611736002
3688122SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND IK30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND IK30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9797
4-Bromofluorobenzene (S)%9897
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
706843
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92611578001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3687481
Associated Lab Samples:92611578001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 06/28/22 16:30129
1,2-Dichlorobenzene ug/kg ND 328 06/28/22 16:30118
1,3-Dichlorobenzene ug/kg ND 328 06/28/22 16:30116
1,4-Dichlorobenzene ug/kg ND 328 06/28/22 16:30125
1-Methylnaphthalene ug/kg ND 328 06/28/22 16:30115
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 06/28/22 16:30156
2,4,5-Trichlorophenol ug/kg ND 328 06/28/22 16:30150
2,4,6-Trichlorophenol ug/kg ND 328 06/28/22 16:30135
2,4-Dichlorophenol ug/kg ND 328 06/28/22 16:30128
2,4-Dimethylphenol ug/kg ND 328 06/28/22 16:30136
2,4-Dinitrophenol ug/kg ND 1640 06/28/22 16:301010
2,4-Dinitrotoluene ug/kg ND 328 06/28/22 16:30126
2,6-Dinitrotoluene ug/kg ND 328 06/28/22 16:30120
2-Chloronaphthalene ug/kg ND 328 06/28/22 16:30130
2-Chlorophenol ug/kg ND 328 06/28/22 16:30123
2-Methylnaphthalene ug/kg ND 328 06/28/22 16:30131
2-Methylphenol(o-Cresol)ug/kg ND 328 06/28/22 16:30134
2-Nitroaniline ug/kg ND 1640 06/28/22 16:30268
2-Nitrophenol ug/kg ND 328 06/28/22 16:30142
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 06/28/22 16:30132
3,3'-Dichlorobenzidine ug/kg ND 656 IL06/28/22 16:30222
3-Nitroaniline ug/kg ND 1640 06/28/22 16:30257
4,6-Dinitro-2-methylphenol ug/kg ND 656 06/28/22 16:30306
4-Bromophenylphenyl ether ug/kg ND 328 06/28/22 16:30126
4-Chloro-3-methylphenol ug/kg ND 656 06/28/22 16:30230
4-Chloroaniline ug/kg ND 656 06/28/22 16:30257
4-Chlorophenylphenyl ether ug/kg ND 328 06/28/22 16:30122
4-Nitroaniline ug/kg ND 656 06/28/22 16:30249
4-Nitrophenol ug/kg ND 1640 06/28/22 16:30634
Acenaphthene ug/kg ND 328 06/28/22 16:30115
Acenaphthylene ug/kg ND 328 06/28/22 16:30115
Aniline ug/kg ND 328 06/28/22 16:30128
Anthracene ug/kg ND 328 06/28/22 16:30107
Benzo(a)anthracene ug/kg ND 328 06/28/22 16:30109
Benzo(a)pyrene ug/kg ND 328 06/28/22 16:30113
Benzo(b)fluoranthene ug/kg ND 328 06/28/22 16:30109
Benzo(g,h,i)perylene ug/kg ND 328 06/28/22 16:30127
Benzo(k)fluoranthene ug/kg ND 328 06/28/22 16:30115
Benzoic Acid ug/kg ND 1640 06/28/22 16:30704
Benzyl alcohol ug/kg ND 656 06/28/22 16:30248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3687481
Associated Lab Samples:92611578001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 328 06/28/22 16:30136
bis(2-Chloroethyl) ether ug/kg ND 328 06/28/22 16:30123
bis(2-Ethylhexyl)phthalate ug/kg ND 328 06/28/22 16:30127
Butylbenzylphthalate ug/kg ND 328 06/28/22 16:30138
Chrysene ug/kg ND 328 06/28/22 16:30119
Di-n-butylphthalate ug/kg ND 328 06/28/22 16:30110
Di-n-octylphthalate ug/kg ND 328 06/28/22 16:30129
Dibenz(a,h)anthracene ug/kg ND 328 06/28/22 16:30126
Dibenzofuran ug/kg ND 328 06/28/22 16:30118
Diethylphthalate ug/kg ND 328 06/28/22 16:30120
Dimethylphthalate ug/kg ND 328 06/28/22 16:30119
Fluoranthene ug/kg ND 328 06/28/22 16:30112
Fluorene ug/kg ND 328 06/28/22 16:30115
Hexachloro-1,3-butadiene ug/kg ND 328 06/28/22 16:30142
Hexachlorobenzene ug/kg ND 328 06/28/22 16:30128
Hexachlorocyclopentadiene ug/kg ND 328 v206/28/22 16:30188
Hexachloroethane ug/kg ND 328 06/28/22 16:30125
Indeno(1,2,3-cd)pyrene ug/kg ND 328 06/28/22 16:30129
Isophorone ug/kg ND 328 06/28/22 16:30146
N-Nitroso-di-n-propylamine ug/kg ND 328 06/28/22 16:30123
N-Nitrosodimethylamine ug/kg ND 328 06/28/22 16:30110
N-Nitrosodiphenylamine ug/kg ND 328 06/28/22 16:30116
Naphthalene ug/kg ND 328 06/28/22 16:30111
Nitrobenzene ug/kg ND 328 06/28/22 16:30152
Pentachlorophenol ug/kg ND 656 06/28/22 16:30321
Phenanthrene ug/kg ND 328 06/28/22 16:30107
Phenol ug/kg ND 328 06/28/22 16:30146
Pyrene ug/kg ND 328 06/28/22 16:30133
Pyridine ug/kg ND 328 06/28/22 16:30103
2,4,6-Tribromophenol (S)%46 18-130 06/28/22 16:30
2-Fluorobiphenyl (S)%49 19-130 06/28/22 16:30
2-Fluorophenol (S)%49 18-130 06/28/22 16:30
Nitrobenzene-d5 (S)%54 21-130 06/28/22 16:30
Phenol-d6 (S)%57 18-130 06/28/22 16:30
Terphenyl-d14 (S)%52 15-130 06/28/22 16:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3687482LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10201690 60 47-130
1,2-Dichlorobenzene ug/kg 10201690 60 49-130
1,3-Dichlorobenzene ug/kg 9621690 57 48-130
1,4-Dichlorobenzene ug/kg 9881690 58 49-130
1-Methylnaphthalene ug/kg 11201690 66 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3687482LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9801690 58 38-130
2,4,5-Trichlorophenol ug/kg 11401690 67 49-130
2,4,6-Trichlorophenol ug/kg 11001690 65 50-130
2,4-Dichlorophenol ug/kg 11901690 70 51-130
2,4-Dimethylphenol ug/kg 11501690 68 53-130
2,4-Dinitrophenol ug/kg 43308470 51 39-130
2,4-Dinitrotoluene ug/kg 11801690 69 53-130
2,6-Dinitrotoluene ug/kg 12401690 73 55-130
2-Chloronaphthalene ug/kg 10801690 63 48-130
2-Chlorophenol ug/kg 9341690 55 54-130
2-Methylnaphthalene ug/kg 11001690 65 57-130
2-Methylphenol(o-Cresol)ug/kg 10601690 63 50-130
2-Nitroaniline ug/kg 26903390 79 49-130
2-Nitrophenol ug/kg 9781690 58 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 9781690 58 50-130
3,3'-Dichlorobenzidine ug/kg 2480 IL33907347-130
3-Nitroaniline ug/kg 25503390 75 45-130
4,6-Dinitro-2-methylphenol ug/kg 19703390 58 50-142
4-Bromophenylphenyl ether ug/kg 12401690 73 55-130
4-Chloro-3-methylphenol ug/kg 26303390 77 52-130
4-Chloroaniline ug/kg 22703390 67 49-130
4-Chlorophenylphenyl ether ug/kg 12201690 72 53-130
4-Nitroaniline ug/kg 24003390 71 51-130
4-Nitrophenol ug/kg 57208470 67 40-130
Acenaphthene ug/kg 11901690 70 56-130
Acenaphthylene ug/kg 11301690 67 58-130
Aniline ug/kg 8341690 49 44-130
Anthracene ug/kg 11801690 70 60-130
Benzo(a)anthracene ug/kg 11701690 69 59-130
Benzo(a)pyrene ug/kg 11301690 66 57-130
Benzo(b)fluoranthene ug/kg 10901690 64 54-130
Benzo(g,h,i)perylene ug/kg 11401690 67 59-130
Benzo(k)fluoranthene ug/kg 11401690 67 54-130
Benzoic Acid ug/kg 42008470 50 19-130
Benzyl alcohol ug/kg 20803390 61 50-130
bis(2-Chloroethoxy)methane ug/kg 11301690 67 55-130
bis(2-Chloroethyl) ether ug/kg 10401690 61 53-130
bis(2-Ethylhexyl)phthalate ug/kg 14001690 82 58-130
Butylbenzylphthalate ug/kg 13201690 78 46-138
Chrysene ug/kg 12401690 73 57-130
Di-n-butylphthalate ug/kg 12801690 75 57-130
Di-n-octylphthalate ug/kg 14701690 87 57-130
Dibenz(a,h)anthracene ug/kg 11601690 68 60-130
Dibenzofuran ug/kg 12401690 73 54-130
Diethylphthalate ug/kg 12001690 71 55-130
Dimethylphthalate ug/kg 11801690 70 57-130
Fluoranthene ug/kg 13501690 80 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3687482LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12101690 72 56-130
Hexachloro-1,3-butadiene ug/kg 10301690 61 41-130
Hexachlorobenzene ug/kg 11201690 66 53-130
Hexachlorocyclopentadiene ug/kg ND L2,v31690823-130
Hexachloroethane ug/kg 9911690 58 48-130
Indeno(1,2,3-cd)pyrene ug/kg 11401690 67 61-130
Isophorone ug/kg 11901690 70 49-130
N-Nitroso-di-n-propylamine ug/kg 12401690 73 52-130
N-Nitrosodimethylamine ug/kg 8481690 50 45-130
N-Nitrosodiphenylamine ug/kg 11901690 70 56-130
Naphthalene ug/kg 10401690 61 56-130
Nitrobenzene ug/kg 11501690 68 50-130
Pentachlorophenol ug/kg 19003390 56 33-130
Phenanthrene ug/kg 12701690 75 60-130
Phenol ug/kg 10801690 64 54-130
Pyrene ug/kg 11901690 70 61-130
Pyridine ug/kg 7501690 44 35-130
2,4,6-Tribromophenol (S)%59 18-130
2-Fluorobiphenyl (S)%57 19-130
2-Fluorophenol (S)%48 18-130
Nitrobenzene-d5 (S)%61 21-130
Phenol-d6 (S)%56 18-130
Terphenyl-d14 (S)%60 15-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3687483MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578001
3687484
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1870 67 22-13059 13 301840ND12501090
1,2-Dichlorobenzene ug/kg 1870 70 23-13060 17 301840ND13001100
1,3-Dichlorobenzene ug/kg 1870 67 26-13057 18 301840ND12401040
1,4-Dichlorobenzene ug/kg 1870 69 27-13059 18 301840ND12901080
1-Methylnaphthalene ug/kg 1870 70 30-13062 14 301840ND13101140
2,2'-Oxybis(1-
chloropropane)ug/kg 1870 70 30-13057 22 301840ND13001040
2,4,5-Trichlorophenol ug/kg 1870 70 26-13063 13 301840ND13101150
2,4,6-Trichlorophenol ug/kg 1870 65 23-13059 12 301840ND12101080
2,4-Dichlorophenol ug/kg 1870 75 29-13068 12 301840ND14001240
2,4-Dimethylphenol ug/kg 1870 68 13-13061 14 301840ND12801110
2,4-Dinitrophenol ug/kg 9320 25 10-13124 6 309190ND23402200
2,4-Dinitrotoluene ug/kg 1870 69 28-13061 14 301840ND12901120
2,6-Dinitrotoluene ug/kg 1870 71 36-13062 14 301840ND13201150
2-Chloronaphthalene ug/kg 1870 68 27-13061 12 301840ND12701130
2-Chlorophenol ug/kg 1870 64 29-13054 18 301840ND1200997
2-Methylnaphthalene ug/kg 1870 70 29-13062 14 301840ND13001140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3687483MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578001
3687484
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/kg 1870 70 20-13059 18 301840ND13101090
2-Nitroaniline ug/kg 3730 78 29-13069 13 303680ND28902540
2-Nitrophenol ug/kg 1870 66 26-13057 16 301840ND12201040
3&4-Methylphenol(m&p
Cresol)ug/kg 1870 64 10-17653 19 301840ND1180981
3,3'-Dichlorobenzidine ug/kg IL37306715-13062 9 303680ND24802270
3-Nitroaniline ug/kg 3730 75 28-13067 14 303680ND28102450
4,6-Dinitro-2-methylphenol ug/kg 3730 44 15-13244 2 303680ND16501620
4-Bromophenylphenyl ether ug/kg 1870 71 35-13061 17 301840ND13201120
4-Chloro-3-methylphenol ug/kg 3730 79 30-13068 16 303680ND29302510
4-Chloroaniline ug/kg 3730 65 28-13058 12 303680ND24102140
4-Chlorophenylphenyl ether ug/kg 1870 74 32-13064 16 301840ND13801170
4-Nitroaniline ug/kg 3730 67 30-13061 11 303680ND25002240
4-Nitrophenol ug/kg 9320 60 17-13063 3 309190ND56305780
Acenaphthene ug/kg 1870 72 29-13063 15 301840ND13501160
Acenaphthylene ug/kg 1870 71 31-13063 12 301840ND13201170
Aniline ug/kg 1870 52 10-13045 15 301840ND960825
Anthracene ug/kg 1870 66 33-13058 14 301840ND12901120
Benzo(a)anthracene ug/kg 1870 66 32-13056 17 301840125J13601150
Benzo(a)pyrene ug/kg 1870 65 32-13055 16 301840ND13301130
Benzo(b)fluoranthene ug/kg 1870 64 33-13053 17 301840145J13301120
Benzo(g,h,i)perylene ug/kg 1870 64 28-13054 18 301840ND12901070
Benzo(k)fluoranthene ug/kg 1870 66 31-13055 18 301840ND12901080
Benzoic Acid ug/kg M19320510-1308 309190NDNDND
Benzyl alcohol ug/kg 3730 67 31-13064 5 303680ND24902370
bis(2-
Chloroethoxy)methane ug/kg 1870 71 30-13061 16 301840ND13201130
bis(2-Chloroethyl) ether ug/kg M118707668-13063 21 301840ND14201150
bis(2-Ethylhexyl)phthalate ug/kg 1870 79 40-13068 17 301840ND14801250
Butylbenzylphthalate ug/kg 1870 75 40-13065 16 301840ND14001190
Chrysene ug/kg 1870 71 30-13058 19 301840ND14601200
Di-n-butylphthalate ug/kg 1870 73 41-13063 16 301840ND13501150
Di-n-octylphthalate ug/kg 1870 82 42-13072 15 301840ND15401320
Dibenz(a,h)anthracene ug/kg 1870 66 27-13057 16 301840ND12401050
Dibenzofuran ug/kg 1870 75 32-13067 13 301840ND14101240
Diethylphthalate ug/kg 1870 69 40-13062 12 301840ND12901140
Dimethylphthalate ug/kg 1870 70 37-13061 15 301840ND13001120
Fluoranthene ug/kg 1870 73 26-13061 16 301840264J16201380
Fluorene ug/kg 1870 72 31-13065 12 301840ND13501200
Hexachloro-1,3-butadiene ug/kg 1870 70 20-13061 14 301840ND13001130
Hexachlorobenzene ug/kg 1870 65 29-13057 16 301840ND12101040
Hexachlorocyclopentadiene ug/kg M0,v318701310-1308 301840ND247JND
Hexachloroethane ug/kg 1870 68 21-13059 16 301840ND12701080
Indeno(1,2,3-cd)pyrene ug/kg 1870 64 28-13054 18 301840ND12701060
Isophorone ug/kg 1870 70 32-13060 17 301840ND13101100
N-Nitroso-di-n-propylamine ug/kg 1870 78 31-13065 20 301840ND14501190
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3687483MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578001
3687484
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 1870 60 20-13053 14 301840ND1120968
N-Nitrosodiphenylamine ug/kg 1870 69 32-13061 14 301840ND12801120
Naphthalene ug/kg 1870 70 30-13061 15 301840ND13001110
Nitrobenzene ug/kg 1870 77 25-13065 18 301840ND14301200
Pentachlorophenol ug/kg 3730 48 10-13047 3 303680ND17901740
Phenanthrene ug/kg 1870 68 34-13058 15 301840175J14401240
Phenol ug/kg 1870 72 14-13061 17 301840ND13301130
Pyrene ug/kg 1870 66 31-13054 19 301840211J14401200
Pyridine ug/kg 1870 51 10-13048 9 301840ND959874
2,4,6-Tribromophenol (S)%61 18-13056
2-Fluorobiphenyl (S)%64 19-13058
2-Fluorophenol (S)%56 18-13051
Nitrobenzene-d5 (S)%69 21-13062
Phenol-d6 (S)%63 18-13055
Terphenyl-d14 (S)%60 15-13054
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
707334
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92611578002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3689404
Associated Lab Samples:92611578002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 331 06/29/22 09:33130
1,2-Dichlorobenzene ug/kg ND 331 06/29/22 09:33119
1,3-Dichlorobenzene ug/kg ND 331 06/29/22 09:33117
1,4-Dichlorobenzene ug/kg ND 331 06/29/22 09:33126
1-Methylnaphthalene ug/kg ND 331 06/29/22 09:33116
2,2'-Oxybis(1-chloropropane)ug/kg ND 331 06/29/22 09:33158
2,4,5-Trichlorophenol ug/kg ND 331 06/29/22 09:33152
2,4,6-Trichlorophenol ug/kg ND 331 06/29/22 09:33136
2,4-Dichlorophenol ug/kg ND 331 06/29/22 09:33129
2,4-Dimethylphenol ug/kg ND 331 06/29/22 09:33137
2,4-Dinitrophenol ug/kg ND 1660 06/29/22 09:331020
2,4-Dinitrotoluene ug/kg ND 331 06/29/22 09:33127
2,6-Dinitrotoluene ug/kg ND 331 06/29/22 09:33121
2-Chloronaphthalene ug/kg ND 331 06/29/22 09:33131
2-Chlorophenol ug/kg ND 331 06/29/22 09:33124
2-Methylnaphthalene ug/kg ND 331 06/29/22 09:33132
2-Methylphenol(o-Cresol)ug/kg ND 331 06/29/22 09:33135
2-Nitroaniline ug/kg ND 1660 06/29/22 09:33271
2-Nitrophenol ug/kg ND 331 06/29/22 09:33143
3&4-Methylphenol(m&p Cresol)ug/kg ND 331 06/29/22 09:33133
3,3'-Dichlorobenzidine ug/kg ND 662 IL06/29/22 09:33224
3-Nitroaniline ug/kg ND 1660 06/29/22 09:33260
4,6-Dinitro-2-methylphenol ug/kg ND 662 06/29/22 09:33309
4-Bromophenylphenyl ether ug/kg ND 331 06/29/22 09:33127
4-Chloro-3-methylphenol ug/kg ND 662 06/29/22 09:33233
4-Chloroaniline ug/kg ND 662 06/29/22 09:33260
4-Chlorophenylphenyl ether ug/kg ND 331 06/29/22 09:33123
4-Nitroaniline ug/kg ND 662 06/29/22 09:33252
4-Nitrophenol ug/kg ND 1660 06/29/22 09:33640
Acenaphthene ug/kg ND 331 06/29/22 09:33116
Acenaphthylene ug/kg ND 331 06/29/22 09:33116
Aniline ug/kg ND 331 06/29/22 09:33129
Anthracene ug/kg ND 331 06/29/22 09:33108
Benzo(a)anthracene ug/kg ND 331 06/29/22 09:33110
Benzo(a)pyrene ug/kg ND 331 06/29/22 09:33114
Benzo(b)fluoranthene ug/kg ND 331 06/29/22 09:33110
Benzo(g,h,i)perylene ug/kg ND 331 06/29/22 09:33128
Benzo(k)fluoranthene ug/kg ND 331 06/29/22 09:33116
Benzoic Acid ug/kg ND 1660 06/29/22 09:33711
Benzyl alcohol ug/kg ND 662 06/29/22 09:33251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3689404
Associated Lab Samples:92611578002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 331 06/29/22 09:33137
bis(2-Chloroethyl) ether ug/kg ND 331 06/29/22 09:33124
bis(2-Ethylhexyl)phthalate ug/kg ND 331 06/29/22 09:33128
Butylbenzylphthalate ug/kg ND 331 06/29/22 09:33139
Chrysene ug/kg ND 331 06/29/22 09:33120
Di-n-butylphthalate ug/kg ND 331 06/29/22 09:33111
Di-n-octylphthalate ug/kg ND 331 06/29/22 09:33130
Dibenz(a,h)anthracene ug/kg ND 331 06/29/22 09:33127
Dibenzofuran ug/kg ND 331 06/29/22 09:33119
Diethylphthalate ug/kg ND 331 06/29/22 09:33121
Dimethylphthalate ug/kg ND 331 06/29/22 09:33120
Fluoranthene ug/kg ND 331 06/29/22 09:33113
Fluorene ug/kg ND 331 06/29/22 09:33116
Hexachloro-1,3-butadiene ug/kg ND 331 06/29/22 09:33143
Hexachlorobenzene ug/kg ND 331 06/29/22 09:33129
Hexachlorocyclopentadiene ug/kg ND 331 v206/29/22 09:33190
Hexachloroethane ug/kg ND 331 06/29/22 09:33126
Indeno(1,2,3-cd)pyrene ug/kg ND 331 06/29/22 09:33130
Isophorone ug/kg ND 331 06/29/22 09:33147
N-Nitroso-di-n-propylamine ug/kg ND 331 06/29/22 09:33124
N-Nitrosodimethylamine ug/kg ND 331 06/29/22 09:33111
N-Nitrosodiphenylamine ug/kg ND 331 06/29/22 09:33117
Naphthalene ug/kg ND 331 06/29/22 09:33112
Nitrobenzene ug/kg ND 331 06/29/22 09:33154
Pentachlorophenol ug/kg ND 662 06/29/22 09:33324
Phenanthrene ug/kg ND 331 06/29/22 09:33108
Phenol ug/kg ND 331 06/29/22 09:33147
Pyrene ug/kg ND 331 06/29/22 09:33134
Pyridine ug/kg ND 331 06/29/22 09:33104
2,4,6-Tribromophenol (S)%74 18-130 06/29/22 09:33
2-Fluorobiphenyl (S)%79 19-130 06/29/22 09:33
2-Fluorophenol (S)%73 18-130 06/29/22 09:33
Nitrobenzene-d5 (S)%80 21-130 06/29/22 09:33
Phenol-d6 (S)%82 18-130 06/29/22 09:33
Terphenyl-d14 (S)%82 15-130 06/29/22 09:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3689405LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14801690 88 47-130
1,2-Dichlorobenzene ug/kg 15001690 89 49-130
1,3-Dichlorobenzene ug/kg 14301690 85 48-130
1,4-Dichlorobenzene ug/kg 14701690 87 49-130
1-Methylnaphthalene ug/kg 15901690 94 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3689405LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 14601690 86 38-130
2,4,5-Trichlorophenol ug/kg 16001690 94 49-130
2,4,6-Trichlorophenol ug/kg 15401690 91 50-130
2,4-Dichlorophenol ug/kg 16701690 99 51-130
2,4-Dimethylphenol ug/kg 16201690 96 53-130
2,4-Dinitrophenol ug/kg 77708450 92 39-130
2,4-Dinitrotoluene ug/kg 16901690 100 53-130
2,6-Dinitrotoluene ug/kg 17201690 102 55-130
2-Chloronaphthalene ug/kg 15501690 92 48-130
2-Chlorophenol ug/kg 13801690 81 54-130
2-Methylnaphthalene ug/kg 15601690 93 57-130
2-Methylphenol(o-Cresol)ug/kg 16401690 97 50-130
2-Nitroaniline ug/kg 36803380 109 49-130
2-Nitrophenol ug/kg 14601690 87 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 14301690 85 50-130
3,3'-Dichlorobenzidine ug/kg 3180 IL33809447-130
3-Nitroaniline ug/kg 35203380 104 45-130
4,6-Dinitro-2-methylphenol ug/kg 32703380 97 50-142
4-Bromophenylphenyl ether ug/kg 16901690 100 55-130
4-Chloro-3-methylphenol ug/kg 35303380 105 52-130
4-Chloroaniline ug/kg 31903380 94 49-130
4-Chlorophenylphenyl ether ug/kg 16901690 100 53-130
4-Nitroaniline ug/kg 33003380 98 51-130
4-Nitrophenol ug/kg 76908450 91 40-130
Acenaphthene ug/kg 16101690 96 56-130
Acenaphthylene ug/kg 15701690 93 58-130
Aniline ug/kg 12601690 75 44-130
Anthracene ug/kg 15801690 94 60-130
Benzo(a)anthracene ug/kg 15901690 94 59-130
Benzo(a)pyrene ug/kg 14901690 88 57-130
Benzo(b)fluoranthene ug/kg 14701690 87 54-130
Benzo(g,h,i)perylene ug/kg 14901690 88 59-130
Benzo(k)fluoranthene ug/kg 15301690 90 54-130
Benzoic Acid ug/kg 64008450 76 19-130
Benzyl alcohol ug/kg 30103380 89 50-130
bis(2-Chloroethoxy)methane ug/kg 16701690 99 55-130
bis(2-Chloroethyl) ether ug/kg 16201690 96 53-130
bis(2-Ethylhexyl)phthalate ug/kg 19601690 116 58-130
Butylbenzylphthalate ug/kg 18601690 110 46-138
Chrysene ug/kg 16901690 100 57-130
Di-n-butylphthalate ug/kg 17501690 104 57-130
Di-n-octylphthalate ug/kg 20301690 120 57-130
Dibenz(a,h)anthracene ug/kg 15401690 91 60-130
Dibenzofuran ug/kg 16701690 99 54-130
Diethylphthalate ug/kg 16801690 99 55-130
Dimethylphthalate ug/kg 16601690 98 57-130
Fluoranthene ug/kg 17901690 106 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
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[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3689405LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 16701690 99 56-130
Hexachloro-1,3-butadiene ug/kg 15201690 90 41-130
Hexachlorobenzene ug/kg 15301690 91 53-130
Hexachlorocyclopentadiene ug/kg 418 v216902523-130
Hexachloroethane ug/kg 15001690 89 48-130
Indeno(1,2,3-cd)pyrene ug/kg 15001690 89 61-130
Isophorone ug/kg 16501690 98 49-130
N-Nitroso-di-n-propylamine ug/kg 17801690 105 52-130
N-Nitrosodimethylamine ug/kg 13401690 79 45-130
N-Nitrosodiphenylamine ug/kg 16301690 96 56-130
Naphthalene ug/kg 15001690 89 56-130
Nitrobenzene ug/kg 16301690 97 50-130
Pentachlorophenol ug/kg 26103380 77 33-130
Phenanthrene ug/kg 17001690 101 60-130
Phenol ug/kg 15901690 94 54-130
Pyrene ug/kg 16301690 97 61-130
Pyridine ug/kg 11401690 67 35-130
2,4,6-Tribromophenol (S)%90 18-130
2-Fluorobiphenyl (S)%87 19-130
2-Fluorophenol (S)%76 18-130
Nitrobenzene-d5 (S)%93 21-130
Phenol-d6 (S)%86 18-130
Terphenyl-d14 (S)%89 15-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3689406MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578002
3689407
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1990 84 22-13074 14 301940ND16701440
1,2-Dichlorobenzene ug/kg 1990 79 23-13069 15 301940ND15701350
1,3-Dichlorobenzene ug/kg 1990 79 26-13070 15 301940ND15701360
1,4-Dichlorobenzene ug/kg 1990 79 27-13069 15 301940ND15701350
1-Methylnaphthalene ug/kg 1990 85 30-13076 13 301940ND16801480
2,2'-Oxybis(1-
chloropropane)ug/kg v119909930-13086 17 301940ND19701660
2,4,5-Trichlorophenol ug/kg 1990 92 26-13082 14 301940ND18301600
2,4,6-Trichlorophenol ug/kg 1990 90 23-13078 16 301940ND17801520
2,4-Dichlorophenol ug/kg 1990 90 29-13081 13 301940ND17901570
2,4-Dimethylphenol ug/kg 1990 85 13-13074 15 301940ND16801440
2,4-Dinitrophenol ug/kg 9920 44 10-13135 23 309720ND43403450
2,4-Dinitrotoluene ug/kg 1990 93 28-13084 12 301940ND18401640
2,6-Dinitrotoluene ug/kg 1990 103 36-13091 14 301940ND20301770
2-Chloronaphthalene ug/kg 1990 90 27-13077 17 301940ND17801510
2-Chlorophenol ug/kg 1990 85 29-13073 17 301940ND16801410
2-Methylnaphthalene ug/kg 1990 85 29-13076 14 301940ND16901480
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3689406MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578002
3689407
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/kg 1990 78 20-13069 15 301940ND15601340
2-Nitroaniline ug/kg 3970 87 29-13077 14 303890ND34603000
2-Nitrophenol ug/kg 1990 102 26-13089 16 301940ND20301730
3&4-Methylphenol(m&p
Cresol)ug/kg v319907110-17663 14 301940ND14101230
3,3'-Dichlorobenzidine ug/kg IL39707715-13072 9 303890ND30702810
3-Nitroaniline ug/kg IL39708628-13079 11 303890ND34103050
4,6-Dinitro-2-methylphenol ug/kg R139706815-13249 35 303890ND27001890
4-Bromophenylphenyl ether ug/kg 1990 98 35-13084 17 301940ND19401640
4-Chloro-3-methylphenol ug/kg 3970 82 30-13074 11 303890ND32402900
4-Chloroaniline ug/kg 3970 74 28-13067 11 303890ND29202620
4-Chlorophenylphenyl ether ug/kg 1990 84 32-13075 13 301940ND16601450
4-Nitroaniline ug/kg IL39707730-13073 7 303890ND30502850
4-Nitrophenol ug/kg v399206117-13057 9 309720ND60605520
Acenaphthene ug/kg 1990 87 29-13076 15 301940ND17301480
Acenaphthylene ug/kg 1990 100 31-13077 27 301940ND20301540
Aniline ug/kg 1990 62 10-13055 14 301940ND12201060
Anthracene ug/kg 1990 82 33-13069 18 301940ND17301440
Benzo(a)anthracene ug/kg 1990 90 32-13076 16 301940219J20001690
Benzo(a)pyrene ug/kg 1990 88 32-13073 18 301940212J19601630
Benzo(b)fluoranthene ug/kg 1990 86 33-13073 16 301940272J19701690
Benzo(g,h,i)perylene ug/kg v319909128-13070 25 301940ND19401500
Benzo(k)fluoranthene ug/kg 1990 83 31-13076 10 301940ND17601600
Benzoic Acid ug/kg M19920110-1301 309720NDNDND
Benzyl alcohol ug/kg 3970 71 31-13062 15 303890ND28102420
bis(2-
Chloroethoxy)methane ug/kg 1990 80 30-13069 17 301940ND15801340
bis(2-Chloroethyl) ether ug/kg M119907568-13064 17 301940ND14801250
bis(2-Ethylhexyl)phthalate ug/kg 1990 98 40-13089 11 301940ND19401740
Butylbenzylphthalate ug/kg 1990 110 40-130100 11 301940ND21801950
Chrysene ug/kg 1990 89 30-13074 18 301940225J19801660
Di-n-butylphthalate ug/kg 1990 89 41-13079 13 301940ND17601540
Di-n-octylphthalate ug/kg 1990 105 42-13097 9 301940ND20701900
Dibenz(a,h)anthracene ug/kg 1990 82 27-13071 17 301940ND16701420
Dibenzofuran ug/kg 1990 87 32-13078 14 301940ND17301510
Diethylphthalate ug/kg 1990 90 40-13080 14 301940ND17901550
Dimethylphthalate ug/kg 1990 90 37-13079 15 301940ND17801540
Fluoranthene ug/kg 1990 77 26-13067 12 30194044919701740
Fluorene ug/kg 1990 82 31-13073 14 301940ND16301410
Hexachloro-1,3-butadiene ug/kg 1990 89 20-13078 15 301940ND17601510
Hexachlorobenzene ug/kg 1990 89 29-13078 15 301940ND17601520
Hexachlorocyclopentadiene ug/kg R1,v319904310-13024 58 301940ND849467
Hexachloroethane ug/kg 1990 78 21-13066 18 301940ND15501290
Indeno(1,2,3-cd)pyrene ug/kg 1990 88 28-13071 22 301940ND18501490
Isophorone ug/kg 1990 77 32-13067 15 301940ND15201310
N-Nitroso-di-n-propylamine ug/kg 1990 72 31-13063 15 301940ND14201230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3689406MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611578002
3689407
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 1990 65 20-13055 19 301940ND12901070
N-Nitrosodiphenylamine ug/kg 1990 93 32-13080 17 301940ND18401550
Naphthalene ug/kg 1990 84 30-13074 15 301940ND16701430
Nitrobenzene ug/kg 1990 81 25-13071 16 301940ND16201370
Pentachlorophenol ug/kg 3970 67 10-13061 12 303890ND26702370
Phenanthrene ug/kg 1990 82 34-13069 16 301940319J19401650
Phenol ug/kg 1990 81 14-13071 16 301940ND16101370
Pyrene ug/kg 1990 115 31-13086 25 30194040726802080
Pyridine ug/kg 1990 56 10-13049 17 301940ND1120945
2,4,6-Tribromophenol (S)%101 18-13091
2-Fluorobiphenyl (S)%80 19-13072
2-Fluorophenol (S)%74 18-13066
Nitrobenzene-d5 (S)%81 21-13074
Phenol-d6 (S)%80 18-13073
Terphenyl-d14 (S)%93 15-13088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92611578
LSG-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
706844
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92611578001, 92611578002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92611572001
3687487SAMPLE DUPLICATE:
Percent Moisture %37.4 N222538.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92611592002
3687488SAMPLE DUPLICATE:
Percent Moisture %16.4 N222516.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 34 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92611578
LSG-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
Pace Analytical Services, LLC
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[phone]
Page 35 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92611578
LSG-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92611578001 824633 825275SP-2 EPA 3050B EPA 6020B
92611578002 824633 825275DUP-2 EPA 3050B EPA 6020B
92611578001 824638 825249SP-2 EPA 7471B EPA 7471B
92611578002 824638 825249DUP-2 EPA 7471B EPA 7471B
92611578001 706843 707404SP-2 EPA 3546 EPA 8270E
92611578002 707334 707583DUP-2 EPA 3546 EPA 8270E
92611578001 706927 707067SP-2 EPA 5035A/5030B EPA 8260D
92611578002 706927 707067DUP-2 EPA 5035A/5030B EPA 8260D
92611578001 706844SP-2 SW-846
92611578002 706844DUP-2 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 05:11 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 39
Page 37 of 39
Page 38 of 39
Page 39 of 39

Appendix B Soil Waste Manifests