SF_F_NCS000002196_20220727_FRB_PASI(1)

July 27, 2022
Ms. Sandra Bramble, RPM
Superfund Restoration and Site Evaluation Section
Superfund Division
US EPA Region IV Waste Division
61 Forsyth Street SW, 11th Floor, Atlanta, GA 30303
Subject: Preliminary Assessment (PA) Report
DAFCO Totes Site (a.k.a., Anderson Properties)
EPA ID: NCS000002196
Hudson, Caldwell County, NC
Dear Ms. Bramble,
Under authority of the Comprehensive Environmental Response, Compensation, and
Liability Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization Act of
1986 (SARA), the NC DEQ Superfund Section conducted a Preliminary Assessment (PA) at the
above site. The purpose of this investigation was to collect information concerning conditions at
the site sufficient to determine the need for additional CERCLA/SARA or other appropriate
evaluation. Based on the results of this investigation, this site is recommended for No Further
Remedial Action Planned (NFRAP) designation under CERCLA.
The scope of this investigation included reviews of NC DEQ Hazardous Waste Section
(HWS) inspection and enforcement documents from 2018 and 2019 and a 2020 removal action
conducted by a private contractor for a potentially responsible party (PRP). NC and Avery County
geographic information system (GIS) data were reviewed to identify potential groundwater
receptors near the site. Field investigation included passive soil gas (PSG) sampling, due to
historical storage and use of chlorinated volatile organic compounds (cVOCs) at the site property.
Site Description, Operational and Regulatory History and Waste Characteristics:
Site Description:
The site is a commercial/industrial property located at 2698 Hickory Boulevard, Hudson,
NC 28638. Geographic coordinates at the central part of the on-site storage area are 35.86228o N
Latitude and 81.48553o West Longitude (Refs. 3, 4, 5, 6; Figs. 1, 2A).
Ms. Bramble July 27, 2022
Page 2
The site property is a 5.42-acre parcel which forms the rear (eastern) portion of a larger,
approximately 25-acre property that constitutes the facility. The smaller parcel contains a former
truck maintenance building, and the facility parcel to the west contains a 65,000 square-foot
aluminum structure with garage bays and loading docks. The 25-acre property is bordered by
residential/undeveloped properties to the north and southeast, by a church property to the east, by
commercial property to the southwest and by Hickory Boulevard/Highway 321 to the west (Refs.
4, 5, 6; Fig. 2A).
The 25-acre site property’s original land surface elevation (mean sea level) ranged from
approximately 1180 feet at Hickory Boulevard to 1260 feet at the site’s north property line.
Facility construction apparently included excavation and re-grading within a pre-existing natural
drainage, and most of the site property now lies near-level at approximately 20 feet lower than
surrounding properties to the east, north and west. The site reportedly has a stormwater
conveyance system. Two intermittent surface drainage features exist on site, the main one running
along the south property line and the secondary one following the base of the cut slope at the
northwest edge of the facility. The two drainages combine to the southwest, and runoff is conveyed
via culvert to a pond on the southwest side of Hickory Boulevard. (Refs. 7, 8, 9).
Site Operational and Regulatory History and Waste Characteristics:
Tax records indicate that the site property was developed as a distribution warehouse
during (or prior to) 1972 (Ref. 7). The current site owner leased the site to a trucking company
from 1995 until 2009, and part of the site was in similar use in 2020 (Refs. 6, 7).
In 2015, the owners leased the western 5-acre parcel to DAFCO, a North Carolina
corporation. DAFCO fabricated wastewater treatment systems and treated and cleaned wastewater
totes for reuse. Tailored Chemical Products, Inc. (TCP) paid DAFCO to clean wastewater totes
that were delivered to the site. DAFCO had previously operated at a leased property in nearby
Lenoir, NC. However, after DAFCPO failed to pay rent the other property owner transported
approximately 9000 totes to the current site location during 2015 and 2016. Each tote contained
approximately 275 gallons of untreated wastewater. In 2016, DAFCO sold its assets to Eco-Tote
Container Services, LLC (Eco-Tote), which briefly took over DAFCO’s operations before
abandoning the site and totes. Both entities subsequently were administratively dissolved (Refs.
4, 5, 6).
DAFCO TotesNCS000002196
Preliminary Assessment
Ms. Bramble
July 27, 2022
Page 3
On May 11, 2018, the NC DEQ HWS conducted an on-site inspection in accordance with
the federal Resource Conservation and Recovery Act (RCRA). The compliance inspection was
conducted one day after the Hudson, NC Fire Chief contacted the EPA Region 4 National
Response Center (NRC), reporting that several of the wastewater totes left on the site appeared to
be leaking (Ref. 4). Also present during the inspection were personnel from the Town of Hudson,
Hudson Police and Fire departments, Caldwell County Emergency Management, a former DAFCO
representative, a US EPA On-Scene Coordinator (OSC), and a representative of the site owner
(Ref. 4).
The contents of the totes reportedly appeared to be wastewater generated from manufacture
of white glue. In 2015, Tailored Chemical Products had demonstrated through generator
knowledge that the glue and wastewater were not hazardous waste. In addition, approximately
twenty-five 55-gallon plastic containers and a 25-gallon steel container were observed on site.
Some of the 55-gallon containers were labeled as containing corrosive materials, and the steel
container was labeled as containing nitric acid. In a subsequent site visit on May 24, 2018,
approximately half of the 55-gallon containers and at least one tote were determined to contain
hazardous waste (D002) corrosive liquids, and the nitric acid tank contained a small hole. The
containers were segregated and assessed for leaks and NC HWS personnel requested that the nitric
acid container be overpacked (Refs. 4, 5).
On May 31, 2018, the HWS issued an Immediate Action Notice of Violation (IANOV) to
the site owner for RCRA violations in 1) failing to make proper hazardous waste determination
and 2) storing hazardous waste without obtaining a hazardous waste management permit. The 55-
gallon containers were subsequently removed from the site in accordance with the IANOV (Refs
4, 5).
On August 2, 2018, the NC Solid Waste Section (SWS) issued SWS NOVs to the site
owner and to Tailored Chemical, requiring an assessment and inventory of the totes and specifying
that a plan of action would need to be approved before removal. On September 6, 2018, Tailored
Chemical submitted an initial assessment plan, which the SWS determined did not fully address
the requirements of the NOV (Ref. 5).
On January 24, 2019, the SWS received analytical data from a composite sample of glue
and wastewater collected by Tailored Chemical from approximately 20 totes at the site. Analysis
for RCRA characteristic constituents identified tetrachloroethene (PCE: 2.07 mg/L) exceeding the
RCRA regulatory level (0.7 mg/L) and characterizing the material as (D039 - PCE) characteristic
hazardous waste. The SWS notified the owner and Tailored Chemical that a hazardous waste
characterization and sampling plan would need to be submitted and approved prior to any
additional characterization at the site. The SWS also notified that the containers on site would
need to be labeled as hazardous waste and transported to a RCRA-permitted treatment, storage and
disposal facility within 90 days, and that the site would need to obtain an EPA identification
number and comply with large quantity generator regulations prior to further assessment (Ref. 5).
DAFCO Totes
NCS000002196Preliminary Assessment
Ms. Bramble
July 27, 2022
Page 4
On February 19, 2019, the HWS issued an Immediate Action Notice of Violation (IANOV)
to Tailored Chemical for RCRA violations in 1) failing to make proper hazardous waste
determination and 2) storing hazardous waste without obtaining a hazardous waste management
permit. Sampling plan letters submitted in response by Tailored Chemical attorneys on March 13
and (revised) on April 2, 2019 were determined to be inadequate (Ref. 5).
In early April 2019, the US EPA met with parties involved with the site to request that the
responsible parties (PRPs) conduct an emergency response stabilization, due to the ongoing
deterioration of the totes from exposure to the elements, and their proximity to residential areas
and surface drainage. The PRPs agreed and their environmental contractor initiated the action on
April 6, 2019. During an unannounced Compliance Development Inspection on June 17, 2019,
HWS personnel observed that liquid wastes were being placed into frac tanks and solidified
sludges were being composited into a roll-off container. Waste materials were being evaluated for
PCE via Toxicity Characteristic Leaching Procedure (TCLP) (Ref.5).
On April 21, 2020, Tailored Chemical submitted their final report on the emergency
response. Hazardous tote liquids had been transported to the following permitted disposal
facilities: Dart, Charlotte NC; EQ Detroit, Detroit MI; Giant Resource Recovery, Harleyville and
Sumter, SC. Hazardous solidified tote waste had been transported to the latter three facilities and
to Michigan Disposal Waste Treatment, Belleville MI. Based on photoionization detection (PID)
readings, liquids from ninety totes were segregated, determined (by laboratory analysis) to be non-
hazardous, and transported to Shamrock Environmental, Browns Summit NC. Throughout daily
response activities, contractors had monitored wind speed and direction and air temperature and
monitored air quality at the upwind and downwind property lines by PID. Contractor, EPA and
NCDEQ personnel completed a final meeting and site walkover on February 18, 2020 (Ref. 6).
During the April 2019 site visit, HWS personnel noted that attempts were being made to
identify use of private domestic wells near the site. However, no results from this effort were
documented in the Tailored Chemical final report, or in the March 2022 (Final) HWS RCRA
Inspection Reports (Refs. 5; 6).
Groundwater Migration Pathway and Targets:
Caldwell County, NC lies within the Piedmont Physiographic Province. The piedmont
landscape is characterized by rolling surface topography with well-rounded hills and northeast-
southwest-oriented ridges, dendritic surface drainage patterns and broad, flat inter-stream areas
(Ref. 10; Fig 1).
Surface soil over the developed portion of the site is mapped as Urban Land Complex, 0-
15% slopes (Ref. 11). This description is consistent with the extensive excavation/grading that
apparently occurred during original construction of the existing on-site facility (see Site
Description).
DAFCO TotesNCS000002196
Preliminary Assessment
Ms. Bramble July 27, 2022
Page 5
The site is located within the Inner Piedmont Belt geologic region of the state. Bedrock in
and around the site is mapped as late Proterozoic to Cambrian age sillimanite mica schist (Ref. 12).
Average annual precipitation in the area is approximately 48 inches (Ref. 13). Precipitation
that does not run off to streams infiltrates the ground surface. Infiltrating water that is not lost to
evapotranspiration migrates down through the soil column to recharge the underlying aquifer. In
the piedmont, the groundwater aquifer consists of fractured bedrock and an overlying veneer of
saprolite (weathered rock). Groundwater seeps through the permeable saprolite, but migration
through competent bedrock occurs primarily via discontinuities including fractures, faults and
bedding planes. Groundwater within the saprolite migrates laterally and vertically to points of
discharge on lower hillslopes and at streams in valleys. Groundwater also enters open bedrock
fractures and typically migrates into nearby valleys by this route (Ref. 10). Based on surface
topography and drainage, groundwater beneath the site is anticipated to move in a southwesterly
direction. However, wells operating in proximity to the site in other directions could potentially
draw groundwater from beneath the site through open bedrock fractures.
The site property and properties to the north, east and immediate southwest are located
within the incorporated Town of Hudson, NC. (Ref. 7) The city of Lenoir supplies drinking water
to residences and businesses within incorporated Lenoir and Hudson (Ref. 14). The municipal
water source is a surface-water intake located on Lake Rhodhiss, approximately 9 miles south of
Hudson. The nearest community water supply well is located 3.72 miles north of the site (Ref. 9;
Fig. 1).
GIS-mapped water lines supply the (incorporated) residential neighborhood to the north of
the site (Ref. 7). Residences on Family Tree Lane and Maple Lynn Place, northwest and southeast
of the site, either have listed municipal water accounts or reportedly share with other residences
that do so. On Coy Hartley Lane, southwest across Hickory Boulevard from the site, two of three
(separately owned, adjacent) residences have water accounts; the third resident did not respond to
a written query by the NC Superfund Section, but is anticipated to share with a neighbor (Refs. 15,
16). Residences and businesses farther outside city limits that are not connected to public water
line extensions are anticipated to rely on private wells for drinking water.
Based on the absence of proximal groundwater targets, the exposure hazard posed by the
site via the groundwater migration pathway appears to be minimal.
DAFCO TotesNCS000002196
Preliminary Assessment
Ms. Bramble
July 27, 2022
Page 6
Surface Water Migration Pathway and Targets:
Two minor surface drainage features bracket the developed portion of the site property to
the northwest and south. To the southwest, just beyond Hudson Boulevard, lies a small pond
which is the probable point of entry (PPE) to the 15-mile surface water pathway. The pond drains
to Angley Creek, which then flows southeast 1.5 miles before joining Gunpowder Creek.
Gunpowder Creek flows approximately 7 miles southeast into the Lake Hickory Reservoir portion
of the Catawba River, which constitutes the remainder of the 15-mile surface water migration
pathway target distance limit (TDL)(Refs. 8, 9; Fig. 1).
The City of Hickory NC operates a municipal surface-water intake on the upper portion of
Lake Hickory Reservoir, upriver from the confluence with Gunpowder Creek. No public surface-
water intakes reportedly operate farther downstream, within the 15-mile TDL (Ref. 9).
The small pond downgradient from the site (southwest of Hickory Boulevard) is accessible
via a private road, but aerial photography indicates otherwise-limited accessibility and
development (Ref. 3). The much larger Lake Hickory Reservoir is identified as a fishery with
multiple access points, and is therefore much more likely to be routinely fished for human
consumption (Ref. 17).
The nearest downstream wetland is a 0.14-mile frontage located approximately 0.3 mile
below the PPE. Wetland mapping indicates that Angley Creek and Gunpowder Creek contain a
total of 1.1.mile of wetland frontage, most of which lies farther downstream near Hickory Lake
Reservoir (Ref. 8).
Based on the above information, the exposure hazard posed by the site via the surface water
migration pathway appears to be minimal.
Soil Exposure and Subsurface Intrusion and Air Migration Pathways and Targets:
The site is an active/semi-active commercial trucking facility. A limited number of people
were working locally on site during the initial May 2022 PA site visit, but no workers were present
when sampling activities concluded 11 days later. The site perimeter is not visibly fenced or
securely gated, except possibly against entry by vehicles. Residential properties border the site
property to the north, northwest and southeast. The property line is densely wooded and a steep
bedrock slope overlooks the site from the north. The nearest school is located approximately 0.5
mile south of the site, and no day care facilities reportedly exist within at least that radius (Refs. 3,
18).
The scope of the current PA included a passive soil gas (PSG) evaluation. PSG sampling
was conducted using a “Besure” passive soil-gas sampling kit, provided by Beacon Environmental
Services, Inc. (Appendix B).
DAFCO TotesNCS000002196Preliminary Assessment
Ms. Bramble
July 27, 2022
Page 7
PSG samplers were emplaced at six outdoor locations on the site property. PSG sampler
DT04SG was emplaced within exposed soil in an area in the northeastern portion of the site, where
stored totes had previously been visible on historical aerial photographs (Ref. 7). PSG sampler
DT01SG was emplaced at a downgradient southwest location adjacent to the site entrance. PSG
samplers DT02SG and DT03SG were placed along the south property line between the active site
parcel and residences and businesses to the south and southeast, respectively. PSG samplers
DT05SG and DT06SG were emplaced along the north property line, between the site and
residences to the north and northwest (Ref. 18; Fig. 2; Appendix A).
PSG samplers were deployed on May 26, 2022 and retrieved on June 6, 2022, after 11 days
of equilibration (Ref. 20). At each soil vapor sampling location, a 1.5 inch-diameter hole was
power-drilled into the ground surface to a depth of 1.0 foot. From the bottom of the borehole, a
0.5 inch-diameter borehole was further advanced to a total depth of 3 feet. The PSG samplers
were suspended by metal wire into the upper boreholes. Compacted aluminum foil was used to
anchor the upper sampler wires and to seal the upper boreholes from the atmosphere. Following
retrieval, samplers were secured and shipped to Beacon Environmental for VOC analysis (Ref. 18;
Appendix B).
Beacon analyzed the PSG samples using EPA Method 8260C, for chlorinated and non-
chlorinated volatile organic compounds. A duplicate analysis (DT04SGDup) was performed on
source area PSG sampler DT04SG (Appendix B).
PSG sample results are summarized in Appendix B of this report. Toluene (15.1 µg/m3;
20.8 µg/m3) was detected in PSG sampler DT04SG. All other PSG sample results were non-detect
for VOCs (Appendix B).
The NC Superfund Section evaluated the above PSG sample results using the EPA’s Vapor
Intrusion Screening Level (VISL) Calculator. None of the results exceeded Target Sub-slab/Near-
source Soil Gas concentrations, based on a Commercial Carcinogenic/Non-carcinogenic Risk of
1.0E-6 and Hazard Quotient of 0.1 (Ref. 19). Based on the above sampling results, the off-site
exposure hazard posed via the subsurface intrusion component of the soil exposure and subsurface
intrusion pathway appears to be minimal.
Preliminary Assessment Conclusions:
The site was tasked for a PA following a voluntary removal of leaking wastewater totes
from the site by one of the responsible parties, with EPA Region 4 oversight. The purpose of the
PA was to address the subsurface (vapor) intrusion exposure pathway, for which chlorinated VOCs
were the primary potential contaminant of concern at this site. Results of PSG sampling on the
periphery of the active parcels properties indicate that a minimal off-site exposure hazard exists as
a result of historic site activities.
DAFCO TotesNCS000002196
Preliminary Assessment
Ms. Bramble
July 27, 2022
Page 8
Based on current site conditions, the DAFCO Totes site is recommended for No Further
Remedial Action Planned (NFRAP) designation under CERCLA. If you have any questions,
please contact me at [e-mail] or [phone].
Sincerely,
___________________________ _______________________
Stuart F Parker, Hydrogeologist Qu Qi, Head
Federal Remediation Branch Federal Remediation Branch
NC Superfund Section NC Superfund Section
Attachments
cc: File
Janet MacDonald – letter only
DAFCO TotesNCS000002196Preliminary Assessment
DAFCO Totes (a.k.a., Anderson Family Properties)
NCS000002196
Preliminary Assessment References:
1)United States Environmental Protection Agency (EPA) 40 Code of Federal Regulations - Part300, Hazard Ranking System, July 1, 2019, Available On-line at:
https://semspub.epa.gov/work/HQ/100002489.pdf.
2)United States Environmental Protection Agency, Superfund Chemical Data Matrix, Appendix
B, Updated July 2020. Query at: https://www.epa.gov/superfund/superfund-chemical-data-
matrix-scdm-query
3)Google Maps Latitude and Longitude Determination, Aerial Map and Imagery.
https://www.google.com/maps
4)NC DEQ Hazardous Waste Section, Compliance Branch, “RCRA Inspection Report,
Anderson Family Properties, 2698 Hickory Boulevard, Hudson, NC 28638, Site EPA ID#:
NCS000002196”. June 12, 2018.
5)NC DEQ Hazardous Waste Section, Compliance Branch, “Compliance Schedule Evaluation
Report, Anderson Family Properties, 2698 Hickory Boulevard, Hudson, NC 28638, Site EPA
ID#: NCS000002196”. March 11, 2022.
6)Tailored Chemical Products, Hickory, NC: “Final Report, DAFCO Tote Site, 2698 Hickory
Boulevard, Hudson, North Carolina. April 21, 2020.
7)Caldwell County, NC Geographic Information Service (GIS), https://gis.caldwellcountync.org.
Reviewed October 20, 2021.
8)US Fish and Wildlife Service National Wetland Inventory on line Wetland Mapper. Reviewed
December 29, 2021.
https://www.fws.gov/wetlands/data/mapper.html
9)NC DEQ, DWM, Superfund Section, Inactive Hazardous Sites Branch (IHSB) ARC GIS Map
Viewer: https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html
10)Heath, Ralph, Basic Elements of Groundwater Hydrology with Reference to Conditions in
North Carolina, Parts I-II, US Geological Survey Water Resources Investigations Open-File
Report 80-44, 1980.
11)US Department of Agriculture (USDA), Natural Resources Conservation Service, Web Soil
Survey. Reviewed December 29, 2021.
https://websoilsurvey.ncrs.usda.gov/app/WebSoilSurvey.aspx
12)Goldsmith, R., Milton, Horton, D., Wright, J. W. Jr.: Geologic Map of the Charlotte 1o x 2o
Quadrangle, North Carolina and South Carolina, 1988.
DAFCO Totes
NCS000002196Preliminary Assessment
13)US National Climatic Data Center: Data Tools, 1981-2010 Normals.
https://www.ncdc.noaa.gov/cdo-web/datatools/normals
14)City of Lenoir NC Public Utilities website: https://www.cityoflenoir.com/189/Public-Utilities
15)Parker, Stuart F., NC DEQ Superfund Section: Electronic communications with Erika
Leonhart, City of Lenoir re: Municipal Water Accounts. January 3, 2022.
16)Parker, Stuart F., NC DEQ, Superfund Section: Property Access Requests and resident
responses. March 2022.
17)North Carolina Wildlife Resources Commission Fishing Areas GIS Mapping Tool:
https://www.ncpaws.org/wrcmapbook/FishingAreas.aspx
18)Parker, Stuart F., NC DEQ, Superfund Section: PA Passive Soil Gas Investigation Field Notes,
May 26 and June 6, 2022.
19)US EPA Vapor Intrusion Screening Level (VISL) Calculator output. August 5,2022.
https://epa-visl.ornl.gov/cgi-bin/visl_search
DAFCO TotesNCS000002196Preliminary Assessment

FIGURES

&3
Copyright:© 2013 National Geographic Society, i-cubed
µ
0 1 2 3 40.5
Miles
1.0 Mile
2.0 Miles
3.0 Miles
4.0 Miles
Legend:
&3 DAFCO Totes Site Location
!C Public Well (Non-Community Transient)
USA Detailed Streams
Freshwater Forested/Shrub Wetland
Freshwater Pond
Lake
Riverine
Urban Area
CALDWELL
DAFCO Totes SiteEPA ID No.: NCS000002196
Hudson, Caldwell County, NCPreliminary Assessment Figure 1: Site Location Plan
Created by: Stuart F ParkerNCDWM, Superfund SectionMarch 10, 2022
DAFCO Totes Site
Hudson, Caldwell County, NC
ID # NCS000002196
Fig. 2: Soil Gas
Sample Locations
Stuart F Parker, DWM Superfund Section, 3/10/2022.
Base map from Caldwell County GIS
0 x00 ft
Legend:
Site Property Line
PA Passive Soil Gas Sample
Probable Groundwater Migration
Outdoor Tote Storage (removed)
DT01SG
DT04SG
DT02SG DT03SG
DT05SG
DT06SG
RESIDENCES
RESIDENCES
RESIDENCES

APPENDIX A:
Sample GPS Coordinates
DAFCO Totes
NCS000002196
Passive Soil Gas Sample GPS Locations
6/6/2022
PSG Sampler Longitude Latitude
DT01SG -81.488412 35.861732
DT02SG -81.486572 35.861623
DT03SG -81.485552 35.861663
DT04SG -81.485697 35.862636
DT05SG -81.486561 35.863002
DT06SG -81.487301 35.862619

APPENDIX B:
Sample Laboratory Analytical Reports

Beacon Environmental
CERTIFICATE OF ANALYSIS
Project Description:
Forest Hill, MD 21050 USA
2203A Commerce Road, Suite 1
1.410.838.8780
Laboratory Work Order: 0006389
Beacon Proposal No.: 220506R02
Dafco Totes
Hudson, NC
Prepared for:
June 15, 2022
NC DEQ - Division of Waste Management
217 West Jones Street
Raleigh, NC 27603
Stuart Parker
Ryan W. Schneider
Senior Project Manager
All data meet requirements as specified in the Beacon Environmental Quality Assurance Project Plan and the results
relate only to the samples reported. The work performed was in accordance with ISO/IEC 17025:2017, except
compounds reported with are not included in Beacon’s scope of accreditation. This report shall not be reproduced,
except in full, without written approval of the laboratory. Release of the data contained in this data package has been
authorized by the Laboratory Director or his signee, as verified by the following signatures:
Steven C. Thornley
Laboratory Director
Peter B. Kelly
Quality Manager
BEACON-USA.COM
[TOC_1]Cover Page[TOC]
Page 1 of 56
Table of Contents
Cover Page 1
Sample Summary 4
Case Narrative 5
Analytical Results 6
Summary of Compound Detections 7
Data Summary Table 9
Data Summary Table-Concentration 10
Detailed Analytical Results 11
- Mass 12
0006389-01 - TRIP BLANK 13
0006389-02 - DT 001 SG 14
0006389-03 - DT 002 SG 15
0006389-04 - DT 003 SG 16
0006389-05 - DT 004 SG 17
0006389-06 - DT 004 SG-DUP 18
0006389-07 - DT 005 SG 19
0006389-08 - DT 006 SG 20
- Concentration 21
0006389-01 - TRIP BLANK 22
0006389-02 - DT 001 SG 23
0006389-03 - DT 002 SG 24
0006389-04 - DT 003 SG 25
0006389-05 - DT 004 SG 26
0006389-06 - DT 004 SG-DUP 27
0006389-07 - DT 005 SG 28
Page 2 of 56
Table of Contents (continued)
0006389-08 - DT 006 SG 29
QC Summaries 30
Additional QC Information 35
Sample Result Calculations 36
Equation 44
MRL Calculation Table 45
Certifications 53
Notes and Definitions 54
Sample Management Records 55
Chain of Custody 56
Page 3 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Sample Summary
Client Sample ID Received MatrixLab Sample ID Analysis
Sampler Type: Beacon Passive Sampler
0006389-01 TRIP BLANK Air06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-02 DT 001 SG Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-03 DT 002 SG Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-04 DT 003 SG Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-05 DT 004 SG Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-06 DT 004 SG-DUP Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-07 DT 005 SG Soil Gas06/07/2022 EPA 8260C
Sampler Type: Beacon Passive Sampler
0006389-08 DT 006 SG Soil Gas06/07/2022 EPA 8260C
Samples Received: 8
Samples Analyzed: 8
Project Completeness
[TOC_1]Sample Summary[TOC]
0006389 Page 4 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
[TOC_1]Case Narrative[TOC]Case Narrative
U.S. EPA Method 8260C
All samples were analyzed using thermal desorption-gas chromatography/mass spectrometry (TD-GC/MS)
instrumentation following U.S. EPA Method 8260C, with laboratory results provided in nanograms (ng) and
micrograms per cubic meter (!g/m‡). Laboratory QA/QC procedures included internal standards, surrogates, and
blanks based on EPA Method 8260C. Analyses and reporting were under BEACON’s Quality Assurance Project Plan.
Passive Soil-Gas Survey Notes
If sample locations are covered with or near the edge of an impervious surface (e.g., asphalt or concrete), the
concentrations of compounds in soil gas are higher than if the surfacing was not present. Therefore, the sample
location conditions should be considered when comparing results between locations.
Survey findings are exclusive to this project and when the spatial relationships are compared with results of other
BEACON Surveys it is necessary to incorporate information from both investigations (e.g., depth to sources, soil types,
porosity, soil moisture, presence of impervious surfacing, sample collection times).
Reporting Limits
The RLs represent a baseline above which results meet laboratory-determined limits of precision and accuracy. All
reported results are within the calibration range. The project method quantitation limit (MQL) is the limit of
quantitation (LOQ) as noted in the data tables. Beacon determined uptake rates for a suite of compounds with the
Beacon sampler for sampling in air. Beacon calculated the uptake rates for the remaining compounds using Grahams
Law of Diffusion. The reported data includes LOQ limits.
Project Details
Samples were received in proper condition and laboratory control parameters were met unless otherwise noted
below. The work performed was in accordance with ISO/IEC 17025:2017, except compounds reported with are
not included in Beacon’s scope of accreditation.
End of Case Narrative
0006389 Page 5 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analytical Results
[TOC_1]Analytical Results[TOC]
0006389 Page 6 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
[TOC_2]Summary of Compound Detections[TOC]Summary of Compound Detections- Mass
Result
Analyte
LOQ
QCAS#
EPA 8260C
(ng)
DT 004 SG0006389-05Lab Sample ID:
(ng)
Method:
File ID
Soil Gas
RT
Toluene 95108-88-3 25 C22060809.D 5.297
Result
Analyte
LOQ
QCAS#
EPA 8260C
(ng)
DT 004 SG-DUP0006389-06Lab Sample ID:
(ng)
Method:
File ID
Soil Gas
RT
Toluene 131108-88-3 25 C22060810.D 5.296
0006389 Page 7 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Summary of Compound Detections- Concentration
Result
Analyte
LOQ
QCAS#
EPA 8260C
(g/m‡)
DT 004 SG0006389-05Lab Sample ID:
(g/m‡)
Method:
File ID
Soil Gas
RT
Toluene 15.1108-88-3 3.95 C22060809.D 5.297
Result
Analyte
LOQ
QCAS#
EPA 8260C
(g/m‡)
DT 004 SG-DUP0006389-06Lab Sample ID:
(g/m‡)
Method:
File ID
Soil Gas
RT
Toluene 20.8108-88-3 3.95 C22060810.D 5.296
0006389 Page 8 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Data Summary Table- Mass
(ng)(ng)
LOQ
Compound Frequency
Max Value
Toluene 1 25 95
[TOC_2]Data Summary Table[TOC]
0006389 Page 9 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Data Summary Table- Concentration
(g/m‡)(g/m‡)
LOQ
Compound Frequency
Max Value
Toluene 1 3.95 15.1
[TOC_2]Data Summary Table-Concentration[TOC]
0006389 Page 10 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
[TOC_2]Detailed Analytical Results[TOC]
Detailed Analytical Results
0006389 Page 11 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Detailed Analytical Results- Mass
[TOC_3]- Mass[TOC]
0006389 Page 12 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-01 - TRIP BLANK[TOC]
CAS#
TRIP BLANKLab Sample ID:0006389-01
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Air
75-01-4 <10 10 06/08/2022 13:49 C22060805.DVinyl Chloride
75-35-4 <10 10 06/08/2022 13:49 C22060805.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 13:49 C22060805.DMethylene Chloride
76-13-1 <10 10 06/08/2022 13:49 C22060805.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 13:49 C22060805.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 13:49 C22060805.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 13:49 C22060805.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 13:49 C22060805.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 13:49 C22060805.DChloroform
107-06-2 <10 10 06/08/2022 13:49 C22060805.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 13:49 C22060805.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 13:49 C22060805.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 13:49 C22060805.DBenzene
79-01-6 <10 10 06/08/2022 13:49 C22060805.DTrichloroethene
123-91-1 <10 10 06/08/2022 13:49 C22060805.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 13:49 C22060805.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 13:49 C22060805.DToluene
106-93-4 <10 10 06/08/2022 13:49 C22060805.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 13:49 C22060805.DTetrachloroethene
630-20-6 <10 10 06/08/2022 13:49 C22060805.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 13:49 C22060805.DChlorobenzene
100-41-4 <25 25 06/08/2022 13:49 C22060805.DEthylbenzene
179601-23-1 <25 25 06/08/2022 13:49 C22060805.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 13:49 C22060805.Do-Xylene
96-18-4 <10 10 06/08/2022 13:49 C22060805.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 13:49 C22060805.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 13:49 C22060805.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 13:49 C22060805.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 13:49 C22060805.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 13:49 C22060805.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 13:49 C22060805.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 13:49 C22060805.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 13:49 C22060805.DNaphthalene
87-61-6 <10 10 06/08/2022 13:49 C22060805.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 13:49 C22060805.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 13:49 C22060805.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 13:49 C22060805.DTPH C10-C15ˇ
0006389 Page 13 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-02 - DT 001 SG[TOC]
CAS#
DT 001 SGLab Sample ID:0006389-02
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 14:14 C22060806.DVinyl Chloride
75-35-4 <10 10 06/08/2022 14:14 C22060806.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 14:14 C22060806.DMethylene Chloride
76-13-1 <10 10 06/08/2022 14:14 C22060806.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 14:14 C22060806.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 14:14 C22060806.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 14:14 C22060806.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 14:14 C22060806.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 14:14 C22060806.DChloroform
107-06-2 <10 10 06/08/2022 14:14 C22060806.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 14:14 C22060806.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 14:14 C22060806.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 14:14 C22060806.DBenzene
79-01-6 <10 10 06/08/2022 14:14 C22060806.DTrichloroethene
123-91-1 <10 10 06/08/2022 14:14 C22060806.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 14:14 C22060806.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 14:14 C22060806.DToluene
106-93-4 <10 10 06/08/2022 14:14 C22060806.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 14:14 C22060806.DTetrachloroethene
630-20-6 <10 10 06/08/2022 14:14 C22060806.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 14:14 C22060806.DChlorobenzene
100-41-4 <25 25 06/08/2022 14:14 C22060806.DEthylbenzene
179601-23-1 <25 25 06/08/2022 14:14 C22060806.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 14:14 C22060806.Do-Xylene
96-18-4 <10 10 06/08/2022 14:14 C22060806.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 14:14 C22060806.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 14:14 C22060806.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 14:14 C22060806.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 14:14 C22060806.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 14:14 C22060806.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 14:14 C22060806.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 14:14 C22060806.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 14:14 C22060806.DNaphthalene
87-61-6 <10 10 06/08/2022 14:14 C22060806.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 14:14 C22060806.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 14:14 C22060806.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 14:14 C22060806.DTPH C10-C15ˇ
0006389 Page 14 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-03 - DT 002 SG[TOC]
CAS#
DT 002 SGLab Sample ID:0006389-03
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 14:40 C22060807.DVinyl Chloride
75-35-4 <10 10 06/08/2022 14:40 C22060807.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 14:40 C22060807.DMethylene Chloride
76-13-1 <10 10 06/08/2022 14:40 C22060807.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 14:40 C22060807.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 14:40 C22060807.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 14:40 C22060807.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 14:40 C22060807.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 14:40 C22060807.DChloroform
107-06-2 <10 10 06/08/2022 14:40 C22060807.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 14:40 C22060807.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 14:40 C22060807.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 14:40 C22060807.DBenzene
79-01-6 <10 10 06/08/2022 14:40 C22060807.DTrichloroethene
123-91-1 <10 10 06/08/2022 14:40 C22060807.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 14:40 C22060807.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 14:40 C22060807.DToluene
106-93-4 <10 10 06/08/2022 14:40 C22060807.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 14:40 C22060807.DTetrachloroethene
630-20-6 <10 10 06/08/2022 14:40 C22060807.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 14:40 C22060807.DChlorobenzene
100-41-4 <25 25 06/08/2022 14:40 C22060807.DEthylbenzene
179601-23-1 <25 25 06/08/2022 14:40 C22060807.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 14:40 C22060807.Do-Xylene
96-18-4 <10 10 06/08/2022 14:40 C22060807.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 14:40 C22060807.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 14:40 C22060807.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 14:40 C22060807.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 14:40 C22060807.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 14:40 C22060807.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 14:40 C22060807.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 14:40 C22060807.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 14:40 C22060807.DNaphthalene
87-61-6 <10 10 06/08/2022 14:40 C22060807.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 14:40 C22060807.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 14:40 C22060807.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 14:40 C22060807.DTPH C10-C15ˇ
0006389 Page 15 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-04 - DT 003 SG[TOC]
CAS#
DT 003 SGLab Sample ID:0006389-04
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 15:05 C22060808.DVinyl Chloride
75-35-4 <10 10 06/08/2022 15:05 C22060808.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 15:05 C22060808.DMethylene Chloride
76-13-1 <10 10 06/08/2022 15:05 C22060808.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 15:05 C22060808.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 15:05 C22060808.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 15:05 C22060808.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 15:05 C22060808.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 15:05 C22060808.DChloroform
107-06-2 <10 10 06/08/2022 15:05 C22060808.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 15:05 C22060808.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 15:05 C22060808.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 15:05 C22060808.DBenzene
79-01-6 <10 10 06/08/2022 15:05 C22060808.DTrichloroethene
123-91-1 <10 10 06/08/2022 15:05 C22060808.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 15:05 C22060808.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 15:05 C22060808.DToluene
106-93-4 <10 10 06/08/2022 15:05 C22060808.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 15:05 C22060808.DTetrachloroethene
630-20-6 <10 10 06/08/2022 15:05 C22060808.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 15:05 C22060808.DChlorobenzene
100-41-4 <25 25 06/08/2022 15:05 C22060808.DEthylbenzene
179601-23-1 <25 25 06/08/2022 15:05 C22060808.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 15:05 C22060808.Do-Xylene
96-18-4 <10 10 06/08/2022 15:05 C22060808.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 15:05 C22060808.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 15:05 C22060808.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 15:05 C22060808.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 15:05 C22060808.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 15:05 C22060808.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 15:05 C22060808.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 15:05 C22060808.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 15:05 C22060808.DNaphthalene
87-61-6 <10 10 06/08/2022 15:05 C22060808.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 15:05 C22060808.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 15:05 C22060808.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 15:05 C22060808.DTPH C10-C15ˇ
0006389 Page 16 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-05 - DT 004 SG[TOC]
CAS#
DT 004 SGLab Sample ID:0006389-05
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 15:31 C22060809.DVinyl Chloride
75-35-4 <10 10 06/08/2022 15:31 C22060809.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 15:31 C22060809.DMethylene Chloride
76-13-1 <10 10 06/08/2022 15:31 C22060809.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 15:31 C22060809.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 15:31 C22060809.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 15:31 C22060809.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 15:31 C22060809.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 15:31 C22060809.DChloroform
107-06-2 <10 10 06/08/2022 15:31 C22060809.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 15:31 C22060809.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 15:31 C22060809.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 15:31 C22060809.DBenzene
79-01-6 <10 10 06/08/2022 15:31 C22060809.DTrichloroethene
123-91-1 <10 10 06/08/2022 15:31 C22060809.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 15:31 C22060809.D1,1,2-Trichloroethane
108-88-3 95 25 06/08/2022 15:31 C22060809.DToluene
106-93-4 <10 10 06/08/2022 15:31 C22060809.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 15:31 C22060809.DTetrachloroethene
630-20-6 <10 10 06/08/2022 15:31 C22060809.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 15:31 C22060809.DChlorobenzene
100-41-4 <25 25 06/08/2022 15:31 C22060809.DEthylbenzene
179601-23-1 <25 25 06/08/2022 15:31 C22060809.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 15:31 C22060809.Do-Xylene
96-18-4 <10 10 06/08/2022 15:31 C22060809.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 15:31 C22060809.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 15:31 C22060809.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 15:31 C22060809.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 15:31 C22060809.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 15:31 C22060809.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 15:31 C22060809.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 15:31 C22060809.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 15:31 C22060809.DNaphthalene
87-61-6 <10 10 06/08/2022 15:31 C22060809.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 15:31 C22060809.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 15:31 C22060809.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 15:31 C22060809.DTPH C10-C15ˇ
0006389 Page 17 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-06 - DT 004 SG-DUP[TOC]
CAS#
DT 004 SG-DUPLab Sample ID:0006389-06
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 15:57 C22060810.DVinyl Chloride
75-35-4 <10 10 06/08/2022 15:57 C22060810.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 15:57 C22060810.DMethylene Chloride
76-13-1 <10 10 06/08/2022 15:57 C22060810.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 15:57 C22060810.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 15:57 C22060810.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 15:57 C22060810.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 15:57 C22060810.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 15:57 C22060810.DChloroform
107-06-2 <10 10 06/08/2022 15:57 C22060810.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 15:57 C22060810.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 15:57 C22060810.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 15:57 C22060810.DBenzene
79-01-6 <10 10 06/08/2022 15:57 C22060810.DTrichloroethene
123-91-1 <10 10 06/08/2022 15:57 C22060810.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 15:57 C22060810.D1,1,2-Trichloroethane
108-88-3 131 25 06/08/2022 15:57 C22060810.DToluene
106-93-4 <10 10 06/08/2022 15:57 C22060810.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 15:57 C22060810.DTetrachloroethene
630-20-6 <10 10 06/08/2022 15:57 C22060810.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 15:57 C22060810.DChlorobenzene
100-41-4 <25 25 06/08/2022 15:57 C22060810.DEthylbenzene
179601-23-1 <25 25 06/08/2022 15:57 C22060810.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 15:57 C22060810.Do-Xylene
96-18-4 <10 10 06/08/2022 15:57 C22060810.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 15:57 C22060810.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 15:57 C22060810.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 15:57 C22060810.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 15:57 C22060810.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 15:57 C22060810.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 15:57 C22060810.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 15:57 C22060810.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 15:57 C22060810.DNaphthalene
87-61-6 <10 10 06/08/2022 15:57 C22060810.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 15:57 C22060810.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 15:57 C22060810.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 15:57 C22060810.DTPH C10-C15ˇ
0006389 Page 18 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-07 - DT 005 SG[TOC]
CAS#
DT 005 SGLab Sample ID:0006389-07
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 16:23 C22060811.DVinyl Chloride
75-35-4 <10 10 06/08/2022 16:23 C22060811.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 16:23 C22060811.DMethylene Chloride
76-13-1 <10 10 06/08/2022 16:23 C22060811.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 16:23 C22060811.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 16:23 C22060811.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 16:23 C22060811.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 16:23 C22060811.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 16:23 C22060811.DChloroform
107-06-2 <10 10 06/08/2022 16:23 C22060811.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 16:23 C22060811.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 16:23 C22060811.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 16:23 C22060811.DBenzene
79-01-6 <10 10 06/08/2022 16:23 C22060811.DTrichloroethene
123-91-1 <10 10 06/08/2022 16:23 C22060811.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 16:23 C22060811.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 16:23 C22060811.DToluene
106-93-4 <10 10 06/08/2022 16:23 C22060811.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 16:23 C22060811.DTetrachloroethene
630-20-6 <10 10 06/08/2022 16:23 C22060811.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 16:23 C22060811.DChlorobenzene
100-41-4 <25 25 06/08/2022 16:23 C22060811.DEthylbenzene
179601-23-1 <25 25 06/08/2022 16:23 C22060811.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 16:23 C22060811.Do-Xylene
96-18-4 <10 10 06/08/2022 16:23 C22060811.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 16:23 C22060811.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 16:23 C22060811.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 16:23 C22060811.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 16:23 C22060811.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 16:23 C22060811.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 16:23 C22060811.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 16:23 C22060811.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 16:23 C22060811.DNaphthalene
87-61-6 <10 10 06/08/2022 16:23 C22060811.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 16:23 C22060811.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 16:23 C22060811.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 16:23 C22060811.DTPH C10-C15ˇ
0006389 Page 19 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-08 - DT 006 SG[TOC]
CAS#
DT 006 SGLab Sample ID:0006389-08
(ng)(ng)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <10 10 06/08/2022 16:48 C22060812.DVinyl Chloride
75-35-4 <10 10 06/08/2022 16:48 C22060812.D1,1-Dichloroethene
75-09-2 <10 10 06/08/2022 16:48 C22060812.DMethylene Chloride
76-13-1 <10 10 06/08/2022 16:48 C22060812.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <10 10 06/08/2022 16:48 C22060812.Dtrans-1,2-Dichloroethene
1634-04-4 <25 25 06/08/2022 16:48 C22060812.DMethyl-t-butyl ether
75-34-3 <10 10 06/08/2022 16:48 C22060812.D1,1-Dichloroethane
156-59-2 <10 10 06/08/2022 16:48 C22060812.Dcis-1,2-Dichloroethene
67-66-3 <10 10 06/08/2022 16:48 C22060812.DChloroform
107-06-2 <10 10 06/08/2022 16:48 C22060812.D1,2-Dichloroethane
71-55-6 <10 10 06/08/2022 16:48 C22060812.D1,1,1-Trichloroethane
56-23-5 <10 10 06/08/2022 16:48 C22060812.DCarbon Tetrachloride
71-43-2 <25 25 06/08/2022 16:48 C22060812.DBenzene
79-01-6 <10 10 06/08/2022 16:48 C22060812.DTrichloroethene
123-91-1 <10 10 06/08/2022 16:48 C22060812.D1,4-Dioxane
79-00-5 <10 10 06/08/2022 16:48 C22060812.D1,1,2-Trichloroethane
108-88-3 <25 25 06/08/2022 16:48 C22060812.DToluene
106-93-4 <10 10 06/08/2022 16:48 C22060812.D1,2-Dibromoethane (EDB)
127-18-4 <10 10 06/08/2022 16:48 C22060812.DTetrachloroethene
630-20-6 <10 10 06/08/2022 16:48 C22060812.D1,1,1,2-Tetrachloroethane
108-90-7 <10 10 06/08/2022 16:48 C22060812.DChlorobenzene
100-41-4 <25 25 06/08/2022 16:48 C22060812.DEthylbenzene
179601-23-1 <25 25 06/08/2022 16:48 C22060812.Dp & m-Xylene
95-47-6 <25 25 06/08/2022 16:48 C22060812.Do-Xylene
96-18-4 <10 10 06/08/2022 16:48 C22060812.D1,2,3-Trichloropropane
98-82-8 <25 25 06/08/2022 16:48 C22060812.DIsopropylbenzene
108-67-8 <25 25 06/08/2022 16:48 C22060812.D1,3,5-Trimethylbenzene
95-63-6 <25 25 06/08/2022 16:48 C22060812.D1,2,4-Trimethylbenzene
541-73-1 <10 10 06/08/2022 16:48 C22060812.D1,3-Dichlorobenzene
106-46-7 <10 10 06/08/2022 16:48 C22060812.D1,4-Dichlorobenzene
95-50-1 <10 10 06/08/2022 16:48 C22060812.D1,2-Dichlorobenzene
120-82-1 <10 10 06/08/2022 16:48 C22060812.D1,2,4-Trichlorobenzene
91-20-3 <25 25 06/08/2022 16:48 C22060812.DNaphthalene
87-61-6 <10 10 06/08/2022 16:48 C22060812.D1,2,3-Trichlorobenzene
91-57-6 <25 25 06/08/2022 16:48 C22060812.D2-Methylnaphthalene
<5,000 5,000 06/08/2022 16:48 C22060812.DTPH C4-C9ˇ
<5,000 5,000 06/08/2022 16:48 C22060812.DTPH C10-C15ˇ
0006389 Page 20 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Detailed Analytical Results- Concentration
[TOC_3]- Concentration[TOC]
0006389 Page 21 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-01 - TRIP BLANK[TOC]
CAS#
TRIP BLANKLab Sample ID:0006389-01
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Air
75-01-4 <0.78 0.78 06/08/2022 13:49 C22060805.DVinyl Chloride
75-35-4 <1.91 1.91 06/08/2022 13:49 C22060805.D1,1-Dichloroethene
75-09-2 <1.80 1.80 06/08/2022 13:49 C22060805.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 13:49 C22060805.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.43 1.43 06/08/2022 13:49 C22060805.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 13:49 C22060805.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 13:49 C22060805.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 13:49 C22060805.Dcis-1,2-Dichloroethene
67-66-3 <1.80 1.80 06/08/2022 13:49 C22060805.DChloroform
107-06-2 <1.13 1.13 06/08/2022 13:49 C22060805.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 13:49 C22060805.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 13:49 C22060805.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 13:49 C22060805.DBenzene
79-01-6 <1.91 1.91 06/08/2022 13:49 C22060805.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 13:49 C22060805.D1,4-Dioxane
79-00-5 <1.91 1.91 06/08/2022 13:49 C22060805.D1,1,2-Trichloroethane
108-88-3 <3.94 3.94 06/08/2022 13:49 C22060805.DToluene
106-93-4 <1.62 1.62 06/08/2022 13:49 C22060805.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 13:49 C22060805.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 13:49 C22060805.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 13:49 C22060805.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 13:49 C22060805.DEthylbenzene
179601-23-1 <1.79 1.79 06/08/2022 13:49 C22060805.Dp & m-Xylene
95-47-6 <1.79 1.79 06/08/2022 13:49 C22060805.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 13:49 C22060805.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 13:49 C22060805.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 13:49 C22060805.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 13:49 C22060805.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 13:49 C22060805.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 13:49 C22060805.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 13:49 C22060805.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 13:49 C22060805.D1,2,4-Trichlorobenzene
91-20-3 <1.97 1.97 06/08/2022 13:49 C22060805.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 13:49 C22060805.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 13:49 C22060805.D2-Methylnaphthalene
<535 535 06/08/2022 13:49 C22060805.DTPH C4-C9ˇ
<457 457 06/08/2022 13:49 C22060805.DTPH C10-C15ˇ
0006389 Page 22 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-02 - DT 001 SG[TOC]
CAS#
DT 001 SGLab Sample ID:0006389-02
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 14:14 C22060806.DVinyl Chloride
75-35-4 <1.91 1.91 06/08/2022 14:14 C22060806.D1,1-Dichloroethene
75-09-2 <1.80 1.80 06/08/2022 14:14 C22060806.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 14:14 C22060806.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.43 1.43 06/08/2022 14:14 C22060806.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 14:14 C22060806.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 14:14 C22060806.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 14:14 C22060806.Dcis-1,2-Dichloroethene
67-66-3 <1.80 1.80 06/08/2022 14:14 C22060806.DChloroform
107-06-2 <1.13 1.13 06/08/2022 14:14 C22060806.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 14:14 C22060806.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 14:14 C22060806.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 14:14 C22060806.DBenzene
79-01-6 <1.91 1.91 06/08/2022 14:14 C22060806.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 14:14 C22060806.D1,4-Dioxane
79-00-5 <1.91 1.91 06/08/2022 14:14 C22060806.D1,1,2-Trichloroethane
108-88-3 <3.94 3.94 06/08/2022 14:14 C22060806.DToluene
106-93-4 <1.62 1.62 06/08/2022 14:14 C22060806.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 14:14 C22060806.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 14:14 C22060806.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 14:14 C22060806.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 14:14 C22060806.DEthylbenzene
179601-23-1 <1.79 1.79 06/08/2022 14:14 C22060806.Dp & m-Xylene
95-47-6 <1.79 1.79 06/08/2022 14:14 C22060806.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 14:14 C22060806.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 14:14 C22060806.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 14:14 C22060806.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 14:14 C22060806.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 14:14 C22060806.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 14:14 C22060806.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 14:14 C22060806.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 14:14 C22060806.D1,2,4-Trichlorobenzene
91-20-3 <1.97 1.97 06/08/2022 14:14 C22060806.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 14:14 C22060806.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 14:14 C22060806.D2-Methylnaphthalene
<535 535 06/08/2022 14:14 C22060806.DTPH C4-C9ˇ
<457 457 06/08/2022 14:14 C22060806.DTPH C10-C15ˇ
0006389 Page 23 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-03 - DT 002 SG[TOC]
CAS#
DT 002 SGLab Sample ID:0006389-03
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 14:40 C22060807.DVinyl Chloride
75-35-4 <1.91 1.91 06/08/2022 14:40 C22060807.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 14:40 C22060807.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 14:40 C22060807.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 14:40 C22060807.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 14:40 C22060807.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 14:40 C22060807.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 14:40 C22060807.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 14:40 C22060807.DChloroform
107-06-2 <1.13 1.13 06/08/2022 14:40 C22060807.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 14:40 C22060807.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 14:40 C22060807.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 14:40 C22060807.DBenzene
79-01-6 <1.91 1.91 06/08/2022 14:40 C22060807.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 14:40 C22060807.D1,4-Dioxane
79-00-5 <1.91 1.91 06/08/2022 14:40 C22060807.D1,1,2-Trichloroethane
108-88-3 <3.95 3.95 06/08/2022 14:40 C22060807.DToluene
106-93-4 <1.62 1.62 06/08/2022 14:40 C22060807.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 14:40 C22060807.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 14:40 C22060807.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 14:40 C22060807.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 14:40 C22060807.DEthylbenzene
179601-23-1 <1.79 1.79 06/08/2022 14:40 C22060807.Dp & m-Xylene
95-47-6 <1.79 1.79 06/08/2022 14:40 C22060807.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 14:40 C22060807.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 14:40 C22060807.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 14:40 C22060807.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 14:40 C22060807.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 14:40 C22060807.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 14:40 C22060807.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 14:40 C22060807.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 14:40 C22060807.D1,2,4-Trichlorobenzene
91-20-3 <1.97 1.97 06/08/2022 14:40 C22060807.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 14:40 C22060807.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 14:40 C22060807.D2-Methylnaphthalene
<535 535 06/08/2022 14:40 C22060807.DTPH C4-C9ˇ
<458 458 06/08/2022 14:40 C22060807.DTPH C10-C15ˇ
0006389 Page 24 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-04 - DT 003 SG[TOC]
CAS#
DT 003 SGLab Sample ID:0006389-04
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 15:05 C22060808.DVinyl Chloride
75-35-4 <1.92 1.92 06/08/2022 15:05 C22060808.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 15:05 C22060808.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 15:05 C22060808.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 15:05 C22060808.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 15:05 C22060808.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 15:05 C22060808.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 15:05 C22060808.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 15:05 C22060808.DChloroform
107-06-2 <1.13 1.13 06/08/2022 15:05 C22060808.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 15:05 C22060808.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 15:05 C22060808.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 15:05 C22060808.DBenzene
79-01-6 <1.92 1.92 06/08/2022 15:05 C22060808.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 15:05 C22060808.D1,4-Dioxane
79-00-5 <1.92 1.92 06/08/2022 15:05 C22060808.D1,1,2-Trichloroethane
108-88-3 <3.95 3.95 06/08/2022 15:05 C22060808.DToluene
106-93-4 <1.62 1.62 06/08/2022 15:05 C22060808.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 15:05 C22060808.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 15:05 C22060808.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 15:05 C22060808.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 15:05 C22060808.DEthylbenzene
179601-23-1 <1.80 1.80 06/08/2022 15:05 C22060808.Dp & m-Xylene
95-47-6 <1.80 1.80 06/08/2022 15:05 C22060808.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 15:05 C22060808.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 15:05 C22060808.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 15:05 C22060808.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 15:05 C22060808.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 15:05 C22060808.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 15:05 C22060808.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 15:05 C22060808.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 15:05 C22060808.D1,2,4-Trichlorobenzene
91-20-3 <1.98 1.98 06/08/2022 15:05 C22060808.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 15:05 C22060808.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 15:05 C22060808.D2-Methylnaphthalene
<536 536 06/08/2022 15:05 C22060808.DTPH C4-C9ˇ
<458 458 06/08/2022 15:05 C22060808.DTPH C10-C15ˇ
0006389 Page 25 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-05 - DT 004 SG[TOC]
CAS#
DT 004 SGLab Sample ID:0006389-05
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 15:31 C22060809.DVinyl Chloride
75-35-4 <1.92 1.92 06/08/2022 15:31 C22060809.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 15:31 C22060809.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 15:31 C22060809.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 15:31 C22060809.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 15:31 C22060809.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 15:31 C22060809.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 15:31 C22060809.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 15:31 C22060809.DChloroform
107-06-2 <1.13 1.13 06/08/2022 15:31 C22060809.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 15:31 C22060809.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 15:31 C22060809.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 15:31 C22060809.DBenzene
79-01-6 <1.92 1.92 06/08/2022 15:31 C22060809.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 15:31 C22060809.D1,4-Dioxane
79-00-5 <1.92 1.92 06/08/2022 15:31 C22060809.D1,1,2-Trichloroethane
108-88-3 15.1 3.95 06/08/2022 15:31 C22060809.DToluene
106-93-4 <1.62 1.62 06/08/2022 15:31 C22060809.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 15:31 C22060809.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 15:31 C22060809.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 15:31 C22060809.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 15:31 C22060809.DEthylbenzene
179601-23-1 <1.80 1.80 06/08/2022 15:31 C22060809.Dp & m-Xylene
95-47-6 <1.80 1.80 06/08/2022 15:31 C22060809.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 15:31 C22060809.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 15:31 C22060809.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 15:31 C22060809.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 15:31 C22060809.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 15:31 C22060809.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 15:31 C22060809.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 15:31 C22060809.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 15:31 C22060809.D1,2,4-Trichlorobenzene
91-20-3 <1.98 1.98 06/08/2022 15:31 C22060809.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 15:31 C22060809.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 15:31 C22060809.D2-Methylnaphthalene
<536 536 06/08/2022 15:31 C22060809.DTPH C4-C9ˇ
<458 458 06/08/2022 15:31 C22060809.DTPH C10-C15ˇ
0006389 Page 26 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-06 - DT 004 SG-DUP[TOC]
CAS#
DT 004 SG-DUPLab Sample ID:0006389-06
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 15:57 C22060810.DVinyl Chloride
75-35-4 <1.92 1.92 06/08/2022 15:57 C22060810.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 15:57 C22060810.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 15:57 C22060810.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 15:57 C22060810.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 15:57 C22060810.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 15:57 C22060810.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 15:57 C22060810.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 15:57 C22060810.DChloroform
107-06-2 <1.13 1.13 06/08/2022 15:57 C22060810.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 15:57 C22060810.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 15:57 C22060810.DCarbon Tetrachloride
71-43-2 <2.98 2.98 06/08/2022 15:57 C22060810.DBenzene
79-01-6 <1.92 1.92 06/08/2022 15:57 C22060810.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 15:57 C22060810.D1,4-Dioxane
79-00-5 <1.92 1.92 06/08/2022 15:57 C22060810.D1,1,2-Trichloroethane
108-88-3 20.8 3.95 06/08/2022 15:57 C22060810.DToluene
106-93-4 <1.62 1.62 06/08/2022 15:57 C22060810.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 15:57 C22060810.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 15:57 C22060810.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 15:57 C22060810.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 15:57 C22060810.DEthylbenzene
179601-23-1 <1.80 1.80 06/08/2022 15:57 C22060810.Dp & m-Xylene
95-47-6 <1.80 1.80 06/08/2022 15:57 C22060810.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 15:57 C22060810.D1,2,3-Trichloropropane
98-82-8 <1.90 1.90 06/08/2022 15:57 C22060810.DIsopropylbenzene
108-67-8 <1.90 1.90 06/08/2022 15:57 C22060810.D1,3,5-Trimethylbenzene
95-63-6 <1.90 1.90 06/08/2022 15:57 C22060810.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 15:57 C22060810.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 15:57 C22060810.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 15:57 C22060810.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 15:57 C22060810.D1,2,4-Trichlorobenzene
91-20-3 <1.98 1.98 06/08/2022 15:57 C22060810.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 15:57 C22060810.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 15:57 C22060810.D2-Methylnaphthalene
<536 536 06/08/2022 15:57 C22060810.DTPH C4-C9ˇ
<458 458 06/08/2022 15:57 C22060810.DTPH C10-C15ˇ
0006389 Page 27 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-07 - DT 005 SG[TOC]
CAS#
DT 005 SGLab Sample ID:0006389-07
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 16:23 C22060811.DVinyl Chloride
75-35-4 <1.92 1.92 06/08/2022 16:23 C22060811.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 16:23 C22060811.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 16:23 C22060811.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 16:23 C22060811.Dtrans-1,2-Dichloroethene
1634-04-4 <3.16 3.16 06/08/2022 16:23 C22060811.DMethyl-t-butyl ether
75-34-3 <0.74 0.74 06/08/2022 16:23 C22060811.D1,1-Dichloroethane
156-59-2 <1.19 1.19 06/08/2022 16:23 C22060811.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 16:23 C22060811.DChloroform
107-06-2 <1.13 1.13 06/08/2022 16:23 C22060811.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 16:23 C22060811.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 16:23 C22060811.DCarbon Tetrachloride
71-43-2 <2.99 2.99 06/08/2022 16:23 C22060811.DBenzene
79-01-6 <1.92 1.92 06/08/2022 16:23 C22060811.DTrichloroethene
123-91-1 <1.54 1.54 06/08/2022 16:23 C22060811.D1,4-Dioxane
79-00-5 <1.92 1.92 06/08/2022 16:23 C22060811.D1,1,2-Trichloroethane
108-88-3 <3.96 3.96 06/08/2022 16:23 C22060811.DToluene
106-93-4 <1.62 1.62 06/08/2022 16:23 C22060811.D1,2-Dibromoethane (EDB)
127-18-4 <1.54 1.54 06/08/2022 16:23 C22060811.DTetrachloroethene
630-20-6 <1.54 1.54 06/08/2022 16:23 C22060811.D1,1,1,2-Tetrachloroethane
108-90-7 <0.74 0.74 06/08/2022 16:23 C22060811.DChlorobenzene
100-41-4 <1.86 1.86 06/08/2022 16:23 C22060811.DEthylbenzene
179601-23-1 <1.80 1.80 06/08/2022 16:23 C22060811.Dp & m-Xylene
95-47-6 <1.80 1.80 06/08/2022 16:23 C22060811.Do-Xylene
96-18-4 <0.84 0.84 06/08/2022 16:23 C22060811.D1,2,3-Trichloropropane
98-82-8 <1.91 1.91 06/08/2022 16:23 C22060811.DIsopropylbenzene
108-67-8 <1.91 1.91 06/08/2022 16:23 C22060811.D1,3,5-Trimethylbenzene
95-63-6 <1.91 1.91 06/08/2022 16:23 C22060811.D1,2,4-Trimethylbenzene
541-73-1 <0.84 0.84 06/08/2022 16:23 C22060811.D1,3-Dichlorobenzene
106-46-7 <0.84 0.84 06/08/2022 16:23 C22060811.D1,4-Dichlorobenzene
95-50-1 <0.84 0.84 06/08/2022 16:23 C22060811.D1,2-Dichlorobenzene
120-82-1 <1.62 1.62 06/08/2022 16:23 C22060811.D1,2,4-Trichlorobenzene
91-20-3 <1.98 1.98 06/08/2022 16:23 C22060811.DNaphthalene
87-61-6 <1.62 1.62 06/08/2022 16:23 C22060811.D1,2,3-Trichlorobenzene
91-57-6 <2.08 2.08 06/08/2022 16:23 C22060811.D2-Methylnaphthalene
<536 536 06/08/2022 16:23 C22060811.DTPH C4-C9ˇ
<459 459 06/08/2022 16:23 C22060811.DTPH C10-C15ˇ
0006389 Page 28 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Result
Analyte
LOQ
Q
[TOC_4]0006389-08 - DT 006 SG[TOC]
CAS#
DT 006 SGLab Sample ID:0006389-08
(g/m‡)(g/m‡)Analyzed
EPA 8260CMethod:
File ID
Soil Gas
75-01-4 <0.78 0.78 06/08/2022 16:48 C22060812.DVinyl Chloride
75-35-4 <1.92 1.92 06/08/2022 16:48 C22060812.D1,1-Dichloroethene
75-09-2 <1.81 1.81 06/08/2022 16:48 C22060812.DMethylene Chloride
76-13-1 <0.71 0.71 06/08/2022 16:48 C22060812.D1,1,2-Trichlorotrifluoroethane (Fr.113)
156-60-5 <1.44 1.44 06/08/2022 16:48 C22060812.Dtrans-1,2-Dichloroethene
1634-04-4 <3.17 3.17 06/08/2022 16:48 C22060812.DMethyl-t-butyl ether
75-34-3 <0.75 0.75 06/08/2022 16:48 C22060812.D1,1-Dichloroethane
156-59-2 <1.20 1.20 06/08/2022 16:48 C22060812.Dcis-1,2-Dichloroethene
67-66-3 <1.81 1.81 06/08/2022 16:48 C22060812.DChloroform
107-06-2 <1.13 1.13 06/08/2022 16:48 C22060812.D1,2-Dichloroethane
71-55-6 <0.60 0.60 06/08/2022 16:48 C22060812.D1,1,1-Trichloroethane
56-23-5 <1.47 1.47 06/08/2022 16:48 C22060812.DCarbon Tetrachloride
71-43-2 <2.99 2.99 06/08/2022 16:48 C22060812.DBenzene
79-01-6 <1.92 1.92 06/08/2022 16:48 C22060812.DTrichloroethene
123-91-1 <1.55 1.55 06/08/2022 16:48 C22060812.D1,4-Dioxane
79-00-5 <1.92 1.92 06/08/2022 16:48 C22060812.D1,1,2-Trichloroethane
108-88-3 <3.96 3.96 06/08/2022 16:48 C22060812.DToluene
106-93-4 <1.63 1.63 06/08/2022 16:48 C22060812.D1,2-Dibromoethane (EDB)
127-18-4 <1.55 1.55 06/08/2022 16:48 C22060812.DTetrachloroethene
630-20-6 <1.55 1.55 06/08/2022 16:48 C22060812.D1,1,1,2-Tetrachloroethane
108-90-7 <0.75 0.75 06/08/2022 16:48 C22060812.DChlorobenzene
100-41-4 <1.87 1.87 06/08/2022 16:48 C22060812.DEthylbenzene
179601-23-1 <1.80 1.80 06/08/2022 16:48 C22060812.Dp & m-Xylene
95-47-6 <1.80 1.80 06/08/2022 16:48 C22060812.Do-Xylene
96-18-4 <0.85 0.85 06/08/2022 16:48 C22060812.D1,2,3-Trichloropropane
98-82-8 <1.91 1.91 06/08/2022 16:48 C22060812.DIsopropylbenzene
108-67-8 <1.91 1.91 06/08/2022 16:48 C22060812.D1,3,5-Trimethylbenzene
95-63-6 <1.91 1.91 06/08/2022 16:48 C22060812.D1,2,4-Trimethylbenzene
541-73-1 <0.85 0.85 06/08/2022 16:48 C22060812.D1,3-Dichlorobenzene
106-46-7 <0.85 0.85 06/08/2022 16:48 C22060812.D1,4-Dichlorobenzene
95-50-1 <0.85 0.85 06/08/2022 16:48 C22060812.D1,2-Dichlorobenzene
120-82-1 <1.63 1.63 06/08/2022 16:48 C22060812.D1,2,4-Trichlorobenzene
91-20-3 <1.98 1.98 06/08/2022 16:48 C22060812.DNaphthalene
87-61-6 <1.63 1.63 06/08/2022 16:48 C22060812.D1,2,3-Trichlorobenzene
91-57-6 <2.09 2.09 06/08/2022 16:48 C22060812.D2-Methylnaphthalene
<537 537 06/08/2022 16:48 C22060812.DTPH C4-C9ˇ
<460 460 06/08/2022 16:48 C22060812.DTPH C10-C15ˇ
0006389 Page 29 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
QC Information/Summary
[TOC_1]QC Summaries[TOC]
0006389 Page 30 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Soil-Gas Sample Analysis by EPA Method 8260C - Quality Control Summary
22F0022-BLK1 (Lab Blank) File ID: C22060803.D
Result
QAnalyte(ng) (ng)CAS#
LOQ
Analyzed: 6/8/22 13:05
Sampler: Beacon Passive Sampler
Vinyl Chloride 75-01-4 <10 10
1,1-Dichloroethene 75-35-4 <10 10
Methylene Chloride 75-09-2 <10 10
1,1,2-Trichlorotrifluoroethane (Fr.113)76-13-1 <10 10
trans-1,2-Dichloroethene 156-60-5 <10 10
Methyl-t-butyl ether 1634-04-4 <25 25
1,1-Dichloroethane 75-34-3 <10 10
cis-1,2-Dichloroethene 156-59-2 <10 10
Chloroform 67-66-3 <10 10
1,2-Dichloroethane 107-06-2 <10 10
1,1,1-Trichloroethane 71-55-6 <10 10
Carbon Tetrachloride 56-23-5 <10 10
Benzene 71-43-2 <25 25
Trichloroethene 79-01-6 <10 10
1,4-Dioxane 123-91-1 <10 10
1,1,2-Trichloroethane 79-00-5 <10 10
Toluene 108-88-3 <25 25
1,2-Dibromoethane (EDB)106-93-4 <10 10
Tetrachloroethene 127-18-4 <10 10
1,1,1,2-Tetrachloroethane 630-20-6 <10 10
Chlorobenzene 108-90-7 <10 10
Ethylbenzene 100-41-4 <25 25
p & m-Xylene 179601-23-1 <25 25
o-Xylene 95-47-6 <25 25
1,2,3-Trichloropropane 96-18-4 <10 10
Isopropylbenzene 98-82-8 <25 25
1,3,5-Trimethylbenzene 108-67-8 <25 25
1,2,4-Trimethylbenzene 95-63-6 <25 25
1,3-Dichlorobenzene 541-73-1 <10 10
1,4-Dichlorobenzene 106-46-7 <10 10
1,2-Dichlorobenzene 95-50-1 <10 10
1,2,4-Trichlorobenzene 120-82-1 <10 10
Naphthalene 91-20-3 <25 25
1,2,3-Trichlorobenzene 87-61-6 <10 10
2-Methylnaphthalene 91-57-6 <25 25
TPH C4-C9 <5000 5000
TPH C10-C15 <5000 5000
0006389 Page 31 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Soil-Gas Analysis by EPA 8260 - Data in Concentration - Quality Control Summary
22F0022-BLK1 (Lab Blank) File ID: C22060803.D
Result
QAnalyte(g/m‡) (g/m‡)CAS#
LOQ
Analyzed: 6/8/22 13:05
Sampler: Beacon Passive Sampler
Vinyl Chloride 75-01-4 <0.779 0.779
1,1-Dichloroethene 75-35-4 <1.91 1.91
Methylene Chloride 75-09-2 <1.80 1.80
1,1,2-Trichlorotrifluoroethane (Fr.113)76-13-1 <0.709 0.709
trans-1,2-Dichloroethene 156-60-5 <1.43 1.43
Methyl-t-butyl ether 1634-04-4 <3.16 3.16
1,1-Dichloroethane 75-34-3 <0.742 0.742
cis-1,2-Dichloroethene 156-59-2 <1.19 1.19
Chloroform 67-66-3 <1.80 1.80
1,2-Dichloroethane 107-06-2 <1.13 1.13
1,1,1-Trichloroethane 71-55-6 <0.601 0.601
Carbon Tetrachloride 56-23-5 <1.47 1.47
Benzene 71-43-2 <2.98 2.98
Trichloroethene 79-01-6 <1.91 1.91
1,4-Dioxane 123-91-1 <1.54 1.54
1,1,2-Trichloroethane 79-00-5 <1.91 1.91
Toluene 108-88-3 <3.94 3.94
1,2-Dibromoethane (EDB)106-93-4 <1.62 1.62
Tetrachloroethene 127-18-4 <1.54 1.54
1,1,1,2-Tetrachloroethane 630-20-6 <1.54 1.54
Chlorobenzene 108-90-7 <0.742 0.742
Ethylbenzene 100-41-4 <1.86 1.86
p & m-Xylene 179601-23-1 <1.79 1.79
o-Xylene 95-47-6 <1.79 1.79
1,2,3-Trichloropropane 96-18-4 <0.841 0.841
Isopropylbenzene 98-82-8 <1.90 1.90
1,3,5-Trimethylbenzene 108-67-8 <1.90 1.90
1,2,4-Trimethylbenzene 95-63-6 <1.90 1.90
1,3-Dichlorobenzene 541-73-1 <0.841 0.841
1,4-Dichlorobenzene 106-46-7 <0.841 0.841
1,2-Dichlorobenzene 95-50-1 <0.841 0.841
1,2,4-Trichlorobenzene 120-82-1 <1.62 1.62
Naphthalene 91-20-3 <1.97 1.97
1,2,3-Trichlorobenzene 87-61-6 <1.62 1.62
2-Methylnaphthalene 91-57-6 <2.08 2.08
TPH C4-C9 <535 535
TPH C10-C15 <457 457
0006389 Page 32 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Duplicate Result RPD
Analyte (ng)(ng)(%)CAS#(ng)
Sample ResultLOQ
Duplicate Sample: DT 004 SG-DUP (0006389-06) Sample: DT 004 SG (0006389-05) Average RPD: 0.9%
(ng)
LOQ
Sample Duplicate RPD Summary
Soil-Gas Sample Analysis by EPA Method 8260C
Vinyl Chloride 75-01-4 <10 <1010 10 0.0
1,1-Dichloroethene 75-35-4 <10 <1010 10 0.0
Methylene Chloride 75-09-2 <10 <1010 10 0.0
1,1,2-Trichlorotrifluoroethane (Fr.113)76-13-1 <10 <1010 10 0.0
trans-1,2-Dichloroethene 156-60-5 <10 <1010 10 0.0
Methyl-t-butyl ether 1634-04-4 <25 <2525 25 0.0
1,1-Dichloroethane 75-34-3 <10 <1010 10 0.0
cis-1,2-Dichloroethene 156-59-2 <10 <1010 10 0.0
Chloroform 67-66-3 <10 <1010 10 0.0
1,2-Dichloroethane 107-06-2 <10 <1010 10 0.0
1,1,1-Trichloroethane 71-55-6 <10 <1010 10 0.0
Carbon Tetrachloride 56-23-5 <10 <1010 10 0.0
Benzene 71-43-2 <25 <2525 25 0.0
Trichloroethene 79-01-6 <10 <1010 10 0.0
1,4-Dioxane 123-91-1 <10 <1010 10 0.0
1,1,2-Trichloroethane 79-00-5 <10 <1010 10 0.0
Toluene 108-88-3 131 95.025 25 31.9
1,2-Dibromoethane (EDB)106-93-4 <10 <1010 10 0.0
Tetrachloroethene 127-18-4 <10 <1010 10 0.0
1,1,1,2-Tetrachloroethane 630-20-6 <10 <1010 10 0.0
Chlorobenzene 108-90-7 <10 <1010 10 0.0
Ethylbenzene 100-41-4 <25 <2525 25 0.0
p & m-Xylene 179601-23-1 <25 <2525 25 0.0
o-Xylene 95-47-6 <25 <2525 25 0.0
1,2,3-Trichloropropane 96-18-4 <10 <1010 10 0.0
Isopropylbenzene 98-82-8 <25 <2525 25 0.0
1,3,5-Trimethylbenzene 108-67-8 <25 <2525 25 0.0
1,2,4-Trimethylbenzene 95-63-6 <25 <2525 25 0.0
1,3-Dichlorobenzene 541-73-1 <10 <1010 10 0.0
1,4-Dichlorobenzene 106-46-7 <10 <1010 10 0.0
1,2-Dichlorobenzene 95-50-1 <10 <1010 10 0.0
1,2,4-Trichlorobenzene 120-82-1 <10 <1010 10 0.0
Naphthalene 91-20-3 <25 <2525 25 0.0
1,2,3-Trichlorobenzene 87-61-6 <10 <1010 10 0.0
2-Methylnaphthalene 91-57-6 <25 <2525 25 0.0
TPH C4-C9 <5,000 <5,0005000 5000 0.0
TPH C10-C15 <5,000 <5,0005000 5000 0.0
0006389 Page 33 of 56
Site Name:
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NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
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2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Duplicate Result RPD
Analyte (g/m‡)(g/m‡)(%)CAS#(g/m‡)
Sample ResultLOQ
Duplicate Sample: DT 004 SG-DUP (0006389-06) Sample: DT 004 SG (0006389-05) Average RPD: 0.9%
(g/m‡)
LOQ
Sample Duplicate RPD Summary - Concentration
Soil-Gas Analysis by EPA 8260 - Data in Concentration
Vinyl Chloride 75-01-4 <0.78 <0.780.78 0.78 0.0
1,1-Dichloroethene 75-35-4 <1.92 <1.921.92 1.92 0.0
Methylene Chloride 75-09-2 <1.81 <1.811.81 1.81 0.0
1,1,2-Trichlorotrifluoroethane (Fr.113)76-13-1 <0.71 <0.710.71 0.71 0.0
trans-1,2-Dichloroethene 156-60-5 <1.44 <1.441.44 1.44 0.0
Methyl-t-butyl ether 1634-04-4 <3.16 <3.163.16 3.16 0.0
1,1-Dichloroethane 75-34-3 <0.74 <0.740.74 0.74 0.0
cis-1,2-Dichloroethene 156-59-2 <1.19 <1.191.19 1.19 0.0
Chloroform 67-66-3 <1.81 <1.811.81 1.81 0.0
1,2-Dichloroethane 107-06-2 <1.13 <1.131.13 1.13 0.0
1,1,1-Trichloroethane 71-55-6 <0.60 <0.600.60 0.60 0.0
Carbon Tetrachloride 56-23-5 <1.47 <1.471.47 1.47 0.0
Benzene 71-43-2 <2.98 <2.982.98 2.98 0.0
Trichloroethene 79-01-6 <1.92 <1.921.92 1.92 0.0
1,4-Dioxane 123-91-1 <1.54 <1.541.54 1.54 0.0
1,1,2-Trichloroethane 79-00-5 <1.92 <1.921.92 1.92 0.0
Toluene 108-88-3 20.8 15.13.95 3.95 31.8
1,2-Dibromoethane (EDB)106-93-4 <1.62 <1.621.62 1.62 0.0
Tetrachloroethene 127-18-4 <1.54 <1.541.54 1.54 0.0
1,1,1,2-Tetrachloroethane 630-20-6 <1.54 <1.541.54 1.54 0.0
Chlorobenzene 108-90-7 <0.74 <0.740.74 0.74 0.0
Ethylbenzene 100-41-4 <1.86 <1.861.86 1.86 0.0
p & m-Xylene 179601-23-1 <1.80 <1.801.80 1.80 0.0
o-Xylene 95-47-6 <1.80 <1.801.80 1.80 0.0
1,2,3-Trichloropropane 96-18-4 <0.84 <0.840.84 0.84 0.0
Isopropylbenzene 98-82-8 <1.90 <1.901.90 1.90 0.0
1,3,5-Trimethylbenzene 108-67-8 <1.90 <1.901.90 1.90 0.0
1,2,4-Trimethylbenzene 95-63-6 <1.90 <1.901.90 1.90 0.0
1,3-Dichlorobenzene 541-73-1 <0.84 <0.840.84 0.84 0.0
1,4-Dichlorobenzene 106-46-7 <0.84 <0.840.84 0.84 0.0
1,2-Dichlorobenzene 95-50-1 <0.84 <0.840.84 0.84 0.0
1,2,4-Trichlorobenzene 120-82-1 <1.62 <1.621.62 1.62 0.0
Naphthalene 91-20-3 <1.98 <1.981.98 1.98 0.0
1,2,3-Trichlorobenzene 87-61-6 <1.62 <1.621.62 1.62 0.0
2-Methylnaphthalene 91-57-6 <2.08 <2.082.08 2.08 0.0
TPH C4-C9 <536 <536536 536 0.0
TPH C10-C15 <458 <458458 458 0.0
0006389 Page 34 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Additional QC Information
[TOC_1]Additional QC Information[TOC]
0006389 Page 35 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
[TOC_2]Sample Result Calculations[TOC]
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: TRIP BLANKLab ID: 0006389-01
1.00 U U 15,847 C22060805.D 0.810Vinyl Chloride
1.00 U U 15,847 C22060805.D 0.3301,1-Dichloroethene
1.00 U U 15,847 C22060805.D 0.350Methylene Chloride
1.00 U U 15,847 C22060805.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,847 C22060805.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,847 C22060805.D 0.500Methyl-t-butyl ether
1.00 U U 15,847 C22060805.D 0.8501,1-Dichloroethane
1.00 U U 15,847 C22060805.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,847 C22060805.D 0.350Chloroform
1.00 U U 15,847 C22060805.D 0.5601,2-Dichloroethane
1.00 U U 15,847 C22060805.D 1.0501,1,1-Trichloroethane
1.00 U U 15,847 C22060805.D 0.430Carbon Tetrachloride
1.00 U U 15,847 C22060805.D 0.530Benzene
1.00 U U 15,847 C22060805.D 0.330Trichloroethene
1.00 U U 15,847 C22060805.D 0.4101,4-Dioxane
1.00 U U 15,847 C22060805.D 0.3301,1,2-Trichloroethane
1.00 U U 15,847 C22060805.D 0.400Toluene
1.00 U U 15,847 C22060805.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,847 C22060805.D 0.410Tetrachloroethene
1.00 U U 15,847 C22060805.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,847 C22060805.D 0.850Chlorobenzene
1.00 U U 15,847 C22060805.D 0.850Ethylbenzene
1.00 U U 15,847 C22060805.D 0.880p & m-Xylene
1.00 U U 15,847 C22060805.D 0.880o-Xylene
1.00 U U 15,847 C22060805.D 0.7501,2,3-Trichloropropane
1.00 U U 15,847 C22060805.D 0.830Isopropylbenzene
1.00 U U 15,847 C22060805.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,847 C22060805.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,847 C22060805.D 0.7501,3-Dichlorobenzene
1.00 U U 15,847 C22060805.D 0.7501,4-Dichlorobenzene
1.00 U U 15,847 C22060805.D 0.7501,2-Dichlorobenzene
1.00 U U 15,847 C22060805.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,847 C22060805.D 0.800Naphthalene
1.00 U U 15,847 C22060805.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,847 C22060805.D 0.7602-Methylnaphthalene
1.00 U U 15,847 C22060805.D 0.590TPH C4-C9
1.00 U U 15,847 C22060805.D 0.690TPH C10-C15
0006389 Page 36 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 001 SGLab ID: 0006389-02
1.00 U U 15,847 C22060806.D 0.810Vinyl Chloride
1.00 U U 15,847 C22060806.D 0.3301,1-Dichloroethene
1.00 U U 15,847 C22060806.D 0.350Methylene Chloride
1.00 U U 15,847 C22060806.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,847 C22060806.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,847 C22060806.D 0.500Methyl-t-butyl ether
1.00 U U 15,847 C22060806.D 0.8501,1-Dichloroethane
1.00 U U 15,847 C22060806.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,847 C22060806.D 0.350Chloroform
1.00 U U 15,847 C22060806.D 0.5601,2-Dichloroethane
1.00 U U 15,847 C22060806.D 1.0501,1,1-Trichloroethane
1.00 U U 15,847 C22060806.D 0.430Carbon Tetrachloride
1.00 U U 15,847 C22060806.D 0.530Benzene
1.00 U U 15,847 C22060806.D 0.330Trichloroethene
1.00 U U 15,847 C22060806.D 0.4101,4-Dioxane
1.00 U U 15,847 C22060806.D 0.3301,1,2-Trichloroethane
1.00 U U 15,847 C22060806.D 0.400Toluene
1.00 U U 15,847 C22060806.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,847 C22060806.D 0.410Tetrachloroethene
1.00 U U 15,847 C22060806.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,847 C22060806.D 0.850Chlorobenzene
1.00 U U 15,847 C22060806.D 0.850Ethylbenzene
1.00 U U 15,847 C22060806.D 0.880p & m-Xylene
1.00 U U 15,847 C22060806.D 0.880o-Xylene
1.00 U U 15,847 C22060806.D 0.7501,2,3-Trichloropropane
1.00 U U 15,847 C22060806.D 0.830Isopropylbenzene
1.00 U U 15,847 C22060806.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,847 C22060806.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,847 C22060806.D 0.7501,3-Dichlorobenzene
1.00 U U 15,847 C22060806.D 0.7501,4-Dichlorobenzene
1.00 U U 15,847 C22060806.D 0.7501,2-Dichlorobenzene
1.00 U U 15,847 C22060806.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,847 C22060806.D 0.800Naphthalene
1.00 U U 15,847 C22060806.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,847 C22060806.D 0.7602-Methylnaphthalene
1.00 U U 15,847 C22060806.D 0.590TPH C4-C9
1.00 U U 15,847 C22060806.D 0.690TPH C10-C15
0006389 Page 37 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 002 SGLab ID: 0006389-03
1.00 U U 15,827 C22060807.D 0.810Vinyl Chloride
1.00 U U 15,827 C22060807.D 0.3301,1-Dichloroethene
1.00 U U 15,827 C22060807.D 0.350Methylene Chloride
1.00 U U 15,827 C22060807.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,827 C22060807.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,827 C22060807.D 0.500Methyl-t-butyl ether
1.00 U U 15,827 C22060807.D 0.8501,1-Dichloroethane
1.00 U U 15,827 C22060807.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,827 C22060807.D 0.350Chloroform
1.00 U U 15,827 C22060807.D 0.5601,2-Dichloroethane
1.00 U U 15,827 C22060807.D 1.0501,1,1-Trichloroethane
1.00 U U 15,827 C22060807.D 0.430Carbon Tetrachloride
1.00 U U 15,827 C22060807.D 0.530Benzene
1.00 U U 15,827 C22060807.D 0.330Trichloroethene
1.00 U U 15,827 C22060807.D 0.4101,4-Dioxane
1.00 U U 15,827 C22060807.D 0.3301,1,2-Trichloroethane
1.00 U U 15,827 C22060807.D 0.400Toluene
1.00 U U 15,827 C22060807.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,827 C22060807.D 0.410Tetrachloroethene
1.00 U U 15,827 C22060807.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,827 C22060807.D 0.850Chlorobenzene
1.00 U U 15,827 C22060807.D 0.850Ethylbenzene
1.00 U U 15,827 C22060807.D 0.880p & m-Xylene
1.00 U U 15,827 C22060807.D 0.880o-Xylene
1.00 U U 15,827 C22060807.D 0.7501,2,3-Trichloropropane
1.00 U U 15,827 C22060807.D 0.830Isopropylbenzene
1.00 U U 15,827 C22060807.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,827 C22060807.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,827 C22060807.D 0.7501,3-Dichlorobenzene
1.00 U U 15,827 C22060807.D 0.7501,4-Dichlorobenzene
1.00 U U 15,827 C22060807.D 0.7501,2-Dichlorobenzene
1.00 U U 15,827 C22060807.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,827 C22060807.D 0.800Naphthalene
1.00 U U 15,827 C22060807.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,827 C22060807.D 0.7602-Methylnaphthalene
1.00 U U 15,827 C22060807.D 0.590TPH C4-C9
1.00 U U 15,827 C22060807.D 0.690TPH C10-C15
0006389 Page 38 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 003 SGLab ID: 0006389-04
1.00 U U 15,821 C22060808.D 0.810Vinyl Chloride
1.00 U U 15,821 C22060808.D 0.3301,1-Dichloroethene
1.00 U U 15,821 C22060808.D 0.350Methylene Chloride
1.00 U U 15,821 C22060808.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,821 C22060808.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,821 C22060808.D 0.500Methyl-t-butyl ether
1.00 U U 15,821 C22060808.D 0.8501,1-Dichloroethane
1.00 U U 15,821 C22060808.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,821 C22060808.D 0.350Chloroform
1.00 U U 15,821 C22060808.D 0.5601,2-Dichloroethane
1.00 U U 15,821 C22060808.D 1.0501,1,1-Trichloroethane
1.00 U U 15,821 C22060808.D 0.430Carbon Tetrachloride
1.00 U U 15,821 C22060808.D 0.530Benzene
1.00 U U 15,821 C22060808.D 0.330Trichloroethene
1.00 U U 15,821 C22060808.D 0.4101,4-Dioxane
1.00 U U 15,821 C22060808.D 0.3301,1,2-Trichloroethane
1.00 U U 15,821 C22060808.D 0.400Toluene
1.00 U U 15,821 C22060808.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,821 C22060808.D 0.410Tetrachloroethene
1.00 U U 15,821 C22060808.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,821 C22060808.D 0.850Chlorobenzene
1.00 U U 15,821 C22060808.D 0.850Ethylbenzene
1.00 U U 15,821 C22060808.D 0.880p & m-Xylene
1.00 U U 15,821 C22060808.D 0.880o-Xylene
1.00 U U 15,821 C22060808.D 0.7501,2,3-Trichloropropane
1.00 U U 15,821 C22060808.D 0.830Isopropylbenzene
1.00 U U 15,821 C22060808.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,821 C22060808.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,821 C22060808.D 0.7501,3-Dichlorobenzene
1.00 U U 15,821 C22060808.D 0.7501,4-Dichlorobenzene
1.00 U U 15,821 C22060808.D 0.7501,2-Dichlorobenzene
1.00 U U 15,821 C22060808.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,821 C22060808.D 0.800Naphthalene
1.00 U U 15,821 C22060808.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,821 C22060808.D 0.7602-Methylnaphthalene
1.00 U U 15,821 C22060808.D 0.590TPH C4-C9
1.00 U U 15,821 C22060808.D 0.690TPH C10-C15
0006389 Page 39 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 004 SGLab ID: 0006389-05
1.00 U U 15,815 C22060809.D 0.810Vinyl Chloride
1.00 U U 15,815 C22060809.D 0.3301,1-Dichloroethene
1.00 U U 15,815 C22060809.D 0.350Methylene Chloride
1.00 U U 15,815 C22060809.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,815 C22060809.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,815 C22060809.D 0.500Methyl-t-butyl ether
1.00 U U 15,815 C22060809.D 0.8501,1-Dichloroethane
1.00 U U 15,815 C22060809.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,815 C22060809.D 0.350Chloroform
1.00 U U 15,815 C22060809.D 0.5601,2-Dichloroethane
1.00 U U 15,815 C22060809.D 1.0501,1,1-Trichloroethane
1.00 U U 15,815 C22060809.D 0.430Carbon Tetrachloride
1.00 U U 15,815 C22060809.D 0.530Benzene
1.00 U U 15,815 C22060809.D 0.330Trichloroethene
1.00 U U 15,815 C22060809.D 0.4101,4-Dioxane
1.00 U U 15,815 C22060809.D 0.3301,1,2-Trichloroethane
1.00 95.24 15.1 15,815 C22060809.D 0.400Toluene
1.00 U U 15,815 C22060809.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,815 C22060809.D 0.410Tetrachloroethene
1.00 U U 15,815 C22060809.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,815 C22060809.D 0.850Chlorobenzene
1.00 U U 15,815 C22060809.D 0.850Ethylbenzene
1.00 U U 15,815 C22060809.D 0.880p & m-Xylene
1.00 U U 15,815 C22060809.D 0.880o-Xylene
1.00 U U 15,815 C22060809.D 0.7501,2,3-Trichloropropane
1.00 U U 15,815 C22060809.D 0.830Isopropylbenzene
1.00 U U 15,815 C22060809.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,815 C22060809.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,815 C22060809.D 0.7501,3-Dichlorobenzene
1.00 U U 15,815 C22060809.D 0.7501,4-Dichlorobenzene
1.00 U U 15,815 C22060809.D 0.7501,2-Dichlorobenzene
1.00 U U 15,815 C22060809.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,815 C22060809.D 0.800Naphthalene
1.00 U U 15,815 C22060809.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,815 C22060809.D 0.7602-Methylnaphthalene
1.00 U U 15,815 C22060809.D 0.590TPH C4-C9
1.00 U U 15,815 C22060809.D 0.690TPH C10-C15
0006389 Page 40 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 004 SG-DUPLab ID: 0006389-06
1.00 U U 15,815 C22060810.D 0.810Vinyl Chloride
1.00 U U 15,815 C22060810.D 0.3301,1-Dichloroethene
1.00 U U 15,815 C22060810.D 0.350Methylene Chloride
1.00 U U 15,815 C22060810.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,815 C22060810.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,815 C22060810.D 0.500Methyl-t-butyl ether
1.00 U U 15,815 C22060810.D 0.8501,1-Dichloroethane
1.00 U U 15,815 C22060810.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,815 C22060810.D 0.350Chloroform
1.00 U U 15,815 C22060810.D 0.5601,2-Dichloroethane
1.00 U U 15,815 C22060810.D 1.0501,1,1-Trichloroethane
1.00 U U 15,815 C22060810.D 0.430Carbon Tetrachloride
1.00 U U 15,815 C22060810.D 0.530Benzene
1.00 U U 15,815 C22060810.D 0.330Trichloroethene
1.00 U U 15,815 C22060810.D 0.4101,4-Dioxane
1.00 U U 15,815 C22060810.D 0.3301,1,2-Trichloroethane
1.00 131.32 20.8 15,815 C22060810.D 0.400Toluene
1.00 U U 15,815 C22060810.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,815 C22060810.D 0.410Tetrachloroethene
1.00 U U 15,815 C22060810.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,815 C22060810.D 0.850Chlorobenzene
1.00 U U 15,815 C22060810.D 0.850Ethylbenzene
1.00 U U 15,815 C22060810.D 0.880p & m-Xylene
1.00 U U 15,815 C22060810.D 0.880o-Xylene
1.00 U U 15,815 C22060810.D 0.7501,2,3-Trichloropropane
1.00 U U 15,815 C22060810.D 0.830Isopropylbenzene
1.00 U U 15,815 C22060810.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,815 C22060810.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,815 C22060810.D 0.7501,3-Dichlorobenzene
1.00 U U 15,815 C22060810.D 0.7501,4-Dichlorobenzene
1.00 U U 15,815 C22060810.D 0.7501,2-Dichlorobenzene
1.00 U U 15,815 C22060810.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,815 C22060810.D 0.800Naphthalene
1.00 U U 15,815 C22060810.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,815 C22060810.D 0.7602-Methylnaphthalene
1.00 U U 15,815 C22060810.D 0.590TPH C4-C9
1.00 U U 15,815 C22060810.D 0.690TPH C10-C15
0006389 Page 41 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 005 SGLab ID: 0006389-07
1.00 U U 15,801 C22060811.D 0.810Vinyl Chloride
1.00 U U 15,801 C22060811.D 0.3301,1-Dichloroethene
1.00 U U 15,801 C22060811.D 0.350Methylene Chloride
1.00 U U 15,801 C22060811.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,801 C22060811.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,801 C22060811.D 0.500Methyl-t-butyl ether
1.00 U U 15,801 C22060811.D 0.8501,1-Dichloroethane
1.00 U U 15,801 C22060811.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,801 C22060811.D 0.350Chloroform
1.00 U U 15,801 C22060811.D 0.5601,2-Dichloroethane
1.00 U U 15,801 C22060811.D 1.0501,1,1-Trichloroethane
1.00 U U 15,801 C22060811.D 0.430Carbon Tetrachloride
1.00 U U 15,801 C22060811.D 0.530Benzene
1.00 U U 15,801 C22060811.D 0.330Trichloroethene
1.00 U U 15,801 C22060811.D 0.4101,4-Dioxane
1.00 U U 15,801 C22060811.D 0.3301,1,2-Trichloroethane
1.00 U U 15,801 C22060811.D 0.400Toluene
1.00 U U 15,801 C22060811.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,801 C22060811.D 0.410Tetrachloroethene
1.00 U U 15,801 C22060811.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,801 C22060811.D 0.850Chlorobenzene
1.00 U U 15,801 C22060811.D 0.850Ethylbenzene
1.00 U U 15,801 C22060811.D 0.880p & m-Xylene
1.00 U U 15,801 C22060811.D 0.880o-Xylene
1.00 U U 15,801 C22060811.D 0.7501,2,3-Trichloropropane
1.00 U U 15,801 C22060811.D 0.830Isopropylbenzene
1.00 U U 15,801 C22060811.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,801 C22060811.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,801 C22060811.D 0.7501,3-Dichlorobenzene
1.00 U U 15,801 C22060811.D 0.7501,4-Dichlorobenzene
1.00 U U 15,801 C22060811.D 0.7501,2-Dichlorobenzene
1.00 U U 15,801 C22060811.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,801 C22060811.D 0.800Naphthalene
1.00 U U 15,801 C22060811.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,801 C22060811.D 0.7602-Methylnaphthalene
1.00 U U 15,801 C22060811.D 0.590TPH C4-C9
1.00 U U 15,801 C22060811.D 0.690TPH C10-C15
0006389 Page 42 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡ng
DFt
Calculated ResultInitial Result
Sample Result Calculation Summary (Concentration)
EPA 8260C
File ID
M C
minutes
Sampling Time Dilution
Factor
Uptake
Rate
U
Sample Name: DT 006 SGLab ID: 0006389-08
1.00 U U 15,769 C22060812.D 0.810Vinyl Chloride
1.00 U U 15,769 C22060812.D 0.3301,1-Dichloroethene
1.00 U U 15,769 C22060812.D 0.350Methylene Chloride
1.00 U U 15,769 C22060812.D 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 U U 15,769 C22060812.D 0.440trans-1,2-Dichloroethene
1.00 U U 15,769 C22060812.D 0.500Methyl-t-butyl ether
1.00 U U 15,769 C22060812.D 0.8501,1-Dichloroethane
1.00 U U 15,769 C22060812.D 0.530cis-1,2-Dichloroethene
1.00 U U 15,769 C22060812.D 0.350Chloroform
1.00 U U 15,769 C22060812.D 0.5601,2-Dichloroethane
1.00 U U 15,769 C22060812.D 1.0501,1,1-Trichloroethane
1.00 U U 15,769 C22060812.D 0.430Carbon Tetrachloride
1.00 U U 15,769 C22060812.D 0.530Benzene
1.00 U U 15,769 C22060812.D 0.330Trichloroethene
1.00 U U 15,769 C22060812.D 0.4101,4-Dioxane
1.00 U U 15,769 C22060812.D 0.3301,1,2-Trichloroethane
1.00 U U 15,769 C22060812.D 0.400Toluene
1.00 U U 15,769 C22060812.D 0.3901,2-Dibromoethane (EDB)
1.00 U U 15,769 C22060812.D 0.410Tetrachloroethene
1.00 U U 15,769 C22060812.D 0.4101,1,1,2-Tetrachloroethane
1.00 U U 15,769 C22060812.D 0.850Chlorobenzene
1.00 U U 15,769 C22060812.D 0.850Ethylbenzene
1.00 U U 15,769 C22060812.D 0.880p & m-Xylene
1.00 U U 15,769 C22060812.D 0.880o-Xylene
1.00 U U 15,769 C22060812.D 0.7501,2,3-Trichloropropane
1.00 U U 15,769 C22060812.D 0.830Isopropylbenzene
1.00 U U 15,769 C22060812.D 0.8301,3,5-Trimethylbenzene
1.00 U U 15,769 C22060812.D 0.8301,2,4-Trimethylbenzene
1.00 U U 15,769 C22060812.D 0.7501,3-Dichlorobenzene
1.00 U U 15,769 C22060812.D 0.7501,4-Dichlorobenzene
1.00 U U 15,769 C22060812.D 0.7501,2-Dichlorobenzene
1.00 U U 15,769 C22060812.D 0.3901,2,4-Trichlorobenzene
1.00 U U 15,769 C22060812.D 0.800Naphthalene
1.00 U U 15,769 C22060812.D 0.3901,2,3-Trichlorobenzene
1.00 U U 15,769 C22060812.D 0.7602-Methylnaphthalene
1.00 U U 15,769 C22060812.D 0.590TPH C4-C9
1.00 U U 15,769 C22060812.D 0.690TPH C10-C15
0006389 Page 43 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Calculations:
C = 1000 M DF
U t
where: C = concentration (g/m3)
M = mass (ng)
DF = dilution factor
t = sampling time (minutes)
U = compound specific uptake rate
Reference: Federal Register/Vol. 79, No. 125/June 30, 2014
Uptake rate determined using Graham s Law of Diffusion.
[TOC_3]Equation[TOC]
0006389 Page 44 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: TRIP BLANKLab ID: 0006389-01
1.00 15,847 10.0 0.78 0.810Vinyl Chloride
1.00 15,847 10.0 1.91 0.3301,1-Dichloroethene
1.00 15,847 10.0 1.80 0.350Methylene Chloride
1.00 15,847 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,847 10.0 1.43 0.440trans-1,2-Dichloroethene
1.00 15,847 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,847 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,847 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,847 10.0 1.80 0.350Chloroform
1.00 15,847 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,847 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,847 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,847 25.0 2.98 0.530Benzene
1.00 15,847 10.0 1.91 0.330Trichloroethene
1.00 15,847 10.0 1.54 0.4101,4-Dioxane
1.00 15,847 10.0 1.91 0.3301,1,2-Trichloroethane
1.00 15,847 25.0 3.94 0.400Toluene
1.00 15,847 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,847 10.0 1.54 0.410Tetrachloroethene
1.00 15,847 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,847 10.0 0.74 0.850Chlorobenzene
1.00 15,847 25.0 1.86 0.850Ethylbenzene
1.00 15,847 25.0 1.79 0.880p & m-Xylene
1.00 15,847 25.0 1.79 0.880o-Xylene
1.00 15,847 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,847 25.0 1.90 0.830Isopropylbenzene
1.00 15,847 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,847 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,847 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,847 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,847 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,847 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,847 25.0 1.97 0.800Naphthalene
1.00 15,847 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,847 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,847 5,000.0 535 0.590TPH C4-C9
1.00 15,847 5,000.0 457 0.690TPH C10-C15
[TOC_2]MRL Calculation Table[TOC]
0006389 Page 45 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 001 SGLab ID: 0006389-02
1.00 15,847 10.0 0.78 0.810Vinyl Chloride
1.00 15,847 10.0 1.91 0.3301,1-Dichloroethene
1.00 15,847 10.0 1.80 0.350Methylene Chloride
1.00 15,847 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,847 10.0 1.43 0.440trans-1,2-Dichloroethene
1.00 15,847 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,847 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,847 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,847 10.0 1.80 0.350Chloroform
1.00 15,847 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,847 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,847 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,847 25.0 2.98 0.530Benzene
1.00 15,847 10.0 1.91 0.330Trichloroethene
1.00 15,847 10.0 1.54 0.4101,4-Dioxane
1.00 15,847 10.0 1.91 0.3301,1,2-Trichloroethane
1.00 15,847 25.0 3.94 0.400Toluene
1.00 15,847 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,847 10.0 1.54 0.410Tetrachloroethene
1.00 15,847 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,847 10.0 0.74 0.850Chlorobenzene
1.00 15,847 25.0 1.86 0.850Ethylbenzene
1.00 15,847 25.0 1.79 0.880p & m-Xylene
1.00 15,847 25.0 1.79 0.880o-Xylene
1.00 15,847 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,847 25.0 1.90 0.830Isopropylbenzene
1.00 15,847 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,847 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,847 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,847 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,847 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,847 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,847 25.0 1.97 0.800Naphthalene
1.00 15,847 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,847 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,847 5,000.0 535 0.590TPH C4-C9
1.00 15,847 5,000.0 457 0.690TPH C10-C15
0006389 Page 46 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 002 SGLab ID: 0006389-03
1.00 15,827 10.0 0.78 0.810Vinyl Chloride
1.00 15,827 10.0 1.91 0.3301,1-Dichloroethene
1.00 15,827 10.0 1.81 0.350Methylene Chloride
1.00 15,827 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,827 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,827 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,827 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,827 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,827 10.0 1.81 0.350Chloroform
1.00 15,827 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,827 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,827 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,827 25.0 2.98 0.530Benzene
1.00 15,827 10.0 1.91 0.330Trichloroethene
1.00 15,827 10.0 1.54 0.4101,4-Dioxane
1.00 15,827 10.0 1.91 0.3301,1,2-Trichloroethane
1.00 15,827 25.0 3.95 0.400Toluene
1.00 15,827 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,827 10.0 1.54 0.410Tetrachloroethene
1.00 15,827 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,827 10.0 0.74 0.850Chlorobenzene
1.00 15,827 25.0 1.86 0.850Ethylbenzene
1.00 15,827 25.0 1.79 0.880p & m-Xylene
1.00 15,827 25.0 1.79 0.880o-Xylene
1.00 15,827 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,827 25.0 1.90 0.830Isopropylbenzene
1.00 15,827 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,827 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,827 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,827 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,827 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,827 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,827 25.0 1.97 0.800Naphthalene
1.00 15,827 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,827 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,827 5,000.0 535 0.590TPH C4-C9
1.00 15,827 5,000.0 458 0.690TPH C10-C15
0006389 Page 47 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 003 SGLab ID: 0006389-04
1.00 15,821 10.0 0.78 0.810Vinyl Chloride
1.00 15,821 10.0 1.92 0.3301,1-Dichloroethene
1.00 15,821 10.0 1.81 0.350Methylene Chloride
1.00 15,821 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,821 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,821 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,821 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,821 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,821 10.0 1.81 0.350Chloroform
1.00 15,821 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,821 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,821 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,821 25.0 2.98 0.530Benzene
1.00 15,821 10.0 1.92 0.330Trichloroethene
1.00 15,821 10.0 1.54 0.4101,4-Dioxane
1.00 15,821 10.0 1.92 0.3301,1,2-Trichloroethane
1.00 15,821 25.0 3.95 0.400Toluene
1.00 15,821 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,821 10.0 1.54 0.410Tetrachloroethene
1.00 15,821 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,821 10.0 0.74 0.850Chlorobenzene
1.00 15,821 25.0 1.86 0.850Ethylbenzene
1.00 15,821 25.0 1.80 0.880p & m-Xylene
1.00 15,821 25.0 1.80 0.880o-Xylene
1.00 15,821 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,821 25.0 1.90 0.830Isopropylbenzene
1.00 15,821 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,821 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,821 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,821 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,821 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,821 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,821 25.0 1.98 0.800Naphthalene
1.00 15,821 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,821 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,821 5,000.0 536 0.590TPH C4-C9
1.00 15,821 5,000.0 458 0.690TPH C10-C15
0006389 Page 48 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 004 SGLab ID: 0006389-05
1.00 15,815 10.0 0.78 0.810Vinyl Chloride
1.00 15,815 10.0 1.92 0.3301,1-Dichloroethene
1.00 15,815 10.0 1.81 0.350Methylene Chloride
1.00 15,815 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,815 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,815 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,815 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,815 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,815 10.0 1.81 0.350Chloroform
1.00 15,815 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,815 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,815 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,815 25.0 2.98 0.530Benzene
1.00 15,815 10.0 1.92 0.330Trichloroethene
1.00 15,815 10.0 1.54 0.4101,4-Dioxane
1.00 15,815 10.0 1.92 0.3301,1,2-Trichloroethane
1.00 15,815 25.0 3.95 0.400Toluene
1.00 15,815 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,815 10.0 1.54 0.410Tetrachloroethene
1.00 15,815 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,815 10.0 0.74 0.850Chlorobenzene
1.00 15,815 25.0 1.86 0.850Ethylbenzene
1.00 15,815 25.0 1.80 0.880p & m-Xylene
1.00 15,815 25.0 1.80 0.880o-Xylene
1.00 15,815 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,815 25.0 1.90 0.830Isopropylbenzene
1.00 15,815 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,815 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,815 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,815 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,815 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,815 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,815 25.0 1.98 0.800Naphthalene
1.00 15,815 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,815 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,815 5,000.0 536 0.590TPH C4-C9
1.00 15,815 5,000.0 458 0.690TPH C10-C15
0006389 Page 49 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 004 SG-DUPLab ID: 0006389-06
1.00 15,815 10.0 0.78 0.810Vinyl Chloride
1.00 15,815 10.0 1.92 0.3301,1-Dichloroethene
1.00 15,815 10.0 1.81 0.350Methylene Chloride
1.00 15,815 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,815 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,815 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,815 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,815 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,815 10.0 1.81 0.350Chloroform
1.00 15,815 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,815 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,815 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,815 25.0 2.98 0.530Benzene
1.00 15,815 10.0 1.92 0.330Trichloroethene
1.00 15,815 10.0 1.54 0.4101,4-Dioxane
1.00 15,815 10.0 1.92 0.3301,1,2-Trichloroethane
1.00 15,815 25.0 3.95 0.400Toluene
1.00 15,815 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,815 10.0 1.54 0.410Tetrachloroethene
1.00 15,815 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,815 10.0 0.74 0.850Chlorobenzene
1.00 15,815 25.0 1.86 0.850Ethylbenzene
1.00 15,815 25.0 1.80 0.880p & m-Xylene
1.00 15,815 25.0 1.80 0.880o-Xylene
1.00 15,815 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,815 25.0 1.90 0.830Isopropylbenzene
1.00 15,815 25.0 1.90 0.8301,3,5-Trimethylbenzene
1.00 15,815 25.0 1.90 0.8301,2,4-Trimethylbenzene
1.00 15,815 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,815 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,815 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,815 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,815 25.0 1.98 0.800Naphthalene
1.00 15,815 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,815 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,815 5,000.0 536 0.590TPH C4-C9
1.00 15,815 5,000.0 458 0.690TPH C10-C15
0006389 Page 50 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 005 SGLab ID: 0006389-07
1.00 15,801 10.0 0.78 0.810Vinyl Chloride
1.00 15,801 10.0 1.92 0.3301,1-Dichloroethene
1.00 15,801 10.0 1.81 0.350Methylene Chloride
1.00 15,801 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,801 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,801 25.0 3.16 0.500Methyl-t-butyl ether
1.00 15,801 10.0 0.74 0.8501,1-Dichloroethane
1.00 15,801 10.0 1.19 0.530cis-1,2-Dichloroethene
1.00 15,801 10.0 1.81 0.350Chloroform
1.00 15,801 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,801 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,801 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,801 25.0 2.99 0.530Benzene
1.00 15,801 10.0 1.92 0.330Trichloroethene
1.00 15,801 10.0 1.54 0.4101,4-Dioxane
1.00 15,801 10.0 1.92 0.3301,1,2-Trichloroethane
1.00 15,801 25.0 3.96 0.400Toluene
1.00 15,801 10.0 1.62 0.3901,2-Dibromoethane (EDB)
1.00 15,801 10.0 1.54 0.410Tetrachloroethene
1.00 15,801 10.0 1.54 0.4101,1,1,2-Tetrachloroethane
1.00 15,801 10.0 0.74 0.850Chlorobenzene
1.00 15,801 25.0 1.86 0.850Ethylbenzene
1.00 15,801 25.0 1.80 0.880p & m-Xylene
1.00 15,801 25.0 1.80 0.880o-Xylene
1.00 15,801 10.0 0.84 0.7501,2,3-Trichloropropane
1.00 15,801 25.0 1.91 0.830Isopropylbenzene
1.00 15,801 25.0 1.91 0.8301,3,5-Trimethylbenzene
1.00 15,801 25.0 1.91 0.8301,2,4-Trimethylbenzene
1.00 15,801 10.0 0.84 0.7501,3-Dichlorobenzene
1.00 15,801 10.0 0.84 0.7501,4-Dichlorobenzene
1.00 15,801 10.0 0.84 0.7501,2-Dichlorobenzene
1.00 15,801 10.0 1.62 0.3901,2,4-Trichlorobenzene
1.00 15,801 25.0 1.98 0.800Naphthalene
1.00 15,801 10.0 1.62 0.3901,2,3-Trichlorobenzene
1.00 15,801 25.0 2.08 0.7602-Methylnaphthalene
1.00 15,801 5,000.0 536 0.590TPH C4-C9
1.00 15,801 5,000.0 459 0.690TPH C10-C15
0006389 Page 51 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Analyte g/m‡
Calculated LOQInitial LOQ
ng
DFt
EPA 8260C
Method Detection and Reporting Limit Calculations (Concentration)
M C
minutes
Sampling Time Uptake
Rate
Dilution
Factor
U
Sample Name: DT 006 SGLab ID: 0006389-08
1.00 15,769 10.0 0.78 0.810Vinyl Chloride
1.00 15,769 10.0 1.92 0.3301,1-Dichloroethene
1.00 15,769 10.0 1.81 0.350Methylene Chloride
1.00 15,769 10.0 0.71 0.8901,1,2-Trichlorotrifluoroethane (Fr.113)
1.00 15,769 10.0 1.44 0.440trans-1,2-Dichloroethene
1.00 15,769 25.0 3.17 0.500Methyl-t-butyl ether
1.00 15,769 10.0 0.75 0.8501,1-Dichloroethane
1.00 15,769 10.0 1.20 0.530cis-1,2-Dichloroethene
1.00 15,769 10.0 1.81 0.350Chloroform
1.00 15,769 10.0 1.13 0.5601,2-Dichloroethane
1.00 15,769 10.0 0.60 1.0501,1,1-Trichloroethane
1.00 15,769 10.0 1.47 0.430Carbon Tetrachloride
1.00 15,769 25.0 2.99 0.530Benzene
1.00 15,769 10.0 1.92 0.330Trichloroethene
1.00 15,769 10.0 1.55 0.4101,4-Dioxane
1.00 15,769 10.0 1.92 0.3301,1,2-Trichloroethane
1.00 15,769 25.0 3.96 0.400Toluene
1.00 15,769 10.0 1.63 0.3901,2-Dibromoethane (EDB)
1.00 15,769 10.0 1.55 0.410Tetrachloroethene
1.00 15,769 10.0 1.55 0.4101,1,1,2-Tetrachloroethane
1.00 15,769 10.0 0.75 0.850Chlorobenzene
1.00 15,769 25.0 1.87 0.850Ethylbenzene
1.00 15,769 25.0 1.80 0.880p & m-Xylene
1.00 15,769 25.0 1.80 0.880o-Xylene
1.00 15,769 10.0 0.85 0.7501,2,3-Trichloropropane
1.00 15,769 25.0 1.91 0.830Isopropylbenzene
1.00 15,769 25.0 1.91 0.8301,3,5-Trimethylbenzene
1.00 15,769 25.0 1.91 0.8301,2,4-Trimethylbenzene
1.00 15,769 10.0 0.85 0.7501,3-Dichlorobenzene
1.00 15,769 10.0 0.85 0.7501,4-Dichlorobenzene
1.00 15,769 10.0 0.85 0.7501,2-Dichlorobenzene
1.00 15,769 10.0 1.63 0.3901,2,4-Trichlorobenzene
1.00 15,769 25.0 1.98 0.800Naphthalene
1.00 15,769 10.0 1.63 0.3901,2,3-Trichlorobenzene
1.00 15,769 25.0 2.09 0.7602-Methylnaphthalene
1.00 15,769 5,000.0 537 0.590TPH C4-C9
1.00 15,769 5,000.0 460 0.690TPH C10-C15
0006389 Page 52 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
[TOC_2]Certifications[TOC]
Project
RequiredExpiresDescriptionCertification No.Certification ID
Laboratory Certification List
Alaska CS-LAP 19-002 Alaska Department of Environmental Conservation 01/31/2023
DoD-ELAP L20-532-R1 United States Department of Defense Environmental
Laboratory Accreditation
12/31/2022
ISO/IEC 17025:2017 L20-532 General Requirements for the competence of Testing and
Calibration Laboratories
12/31/2022
NEFAP 72690/L20-533 TNI National Environmental Field Activities Program
(NEFAP)
12/31/2022
NY-NELAC 12097 New York Department of Health 04/01/2023
Utah-NELAC MD010912021-9 Utah Department of Health 12/31/2022
0006389 Page 53 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Qualifiers/Notes and Definitions
RPD Relative Percent Difference
General Definitions:
NA Not Applicable
Limit of DetectionLOD
Limit of QuantitationLOQ
QualifierQ
Dilution FactorDF
DL Detection Limit
ˇCompound not on scope of accreditation
3!Uncertainty
RRT Evaluation of Relative Retention Times in RRT Units (qualified if outside +0.06 control limits)
values are outside method/contract required QC limits+
Retention Times in MinutesRT
˘Compound not on scope of accreditation and analyzed with a one-point calibration
[TOC_2]Notes and Definitions[TOC]
0006389 Page 54 of 56
Site Name:
Site Location:
Project Manager:Reported:
NC DEQ - Division of Waste Management
217 West Jones Street
Stuart ParkerRaleigh, NC 27603
Lab Work Order:
2203A Commerce Road, Suite 1
1.410.838.8780
06/15/2022
Dafco Totes
Hudson, NC
220506R02Beacon Proposal:
CERTIFICATE OF ANALYSIS Forest Hill, MD 21050 USA
0006389
Sample Management Records
[TOC_1]Sample Management Records[TOC]
0006389 Page 55 of 56
Page 56 of 56