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HomeMy WebLinkAbout3901_Granville_Oxford_MSWLF_Unit2_Sept22GW_FID1771850_20230201hart 'L hickman ■ SMARTER ENVIRONMENTAL SOLUTIONS Via E-Mail sbray@garTett-moore.com January 30, 2023 Garrett & Moore, Inc. 1029 West South Street Raleigh, NC 27603 Attn: Mr. Stefan Bray, PE Re: Water Quality Monitoring Report — September/October 2022 Granville County Oxford Unit 2 Landfill Oxford, Granville County, NC Facility Permit No. 3 901 -MSWLF-2012 H&H Job No. GMI-005 Dear Stefan: Hart & Hickman, PC (H&H) is submitting the attached Water Quality Monitoring Report — September/October 2022 documenting sample results for the Oxford Unit 2 Landfill for the second semiannual sampling event of 2022. H&H appreciates the opportunity to work with you on this project. If you have any questions or require additional information, please do not hesitate to contact us at 704-586-0007. Very truly yours, Hart & Hickman, PC Jason Soban, PG Project Manager Jeffrey 011ison Project Environmental Scientist 2923 South Tryon Street, Suite 100 Charlotte, NC 28203 704_S86.0007 main 3921 Sunset Ridge Rd, Suite 301 Raleigh, NC 27607 www.harthickman.com 919.847.4241 main I DENR USE 0 NLT t ❑Paper Report ❑Eiectronic Data - Email CO (data loaded: Yes / No Doc/Event #: 'NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reoortina Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6) Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g naturally occurring, off -site source, pre-existing condition, etc.) Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i) Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information T Name of entity submitting data (laboratory, consultant, facility owner): Garrett & Moore, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Stefan Brav Phone: 919-792-1903 E-mail: sbray@garrett-moore.com NC Landfill Rule: Actual sampling dates (e g., Facility name: Facility Address: Facility Permit # ( 0500 or 1600) October 20-24, 2006) Granville County 6854 Landfill Road 3901- September 29 & October 5, Oxford Landfill Unit 2 Oxford, NC 27565 MSWLF-2012 1600 :2022 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring Assessment Monitoring ❑ Corrective Action TIx e of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wellsIGroundwater monitoring data from private water supply wells ❑Leachate monitoring data E, Surface water monitoring data ❑ Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Jason Soban, PG Consultant for Facility (704) 887-4622 Facility Representative Name (Print) Title (Area Code) Telephone Number Affix NC Licensed/ Professional Geologist Seal Signature/ Date 2923 S Tryon Street, Suite 100, Charlotte, NC 28203 Facility Representative Address C-1269 (Engineering) 245 (Geology) NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Water Quality Monitoring Report September/October 2022 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 January 30, 2023 GARRETTmr� ;a MOORE 2 Enginearinq for the Power and Waste Industries hart � hickman SMARTER ENVIRONMENTAL SOLUTIONS 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd , Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919,847.4241 main Water Quality Monitoring Report — September/October 2022 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 Table of Contents Section Pate 1.0 Introduction.................................................................................................................I 1.1 Site Information........................................................................................................1 1.2 Regulatory Status......................................................................................................2 1.3 Groundwater Monitoring Program...........................................................................2 1.4 Surface Water Monitoring Program.........................................................................3 2.0 Water Quality Monitoring Activities........................................................................4 2.1 Water Level Measurements......................................................................................4 2.2 Groundwater Sampling Methods..............................................................................4 2.3 Surface Water Sampling Methods............................................................................5 2.4 Sample Equipment Management..............................................................................5 2.5 Sample Handling and Laboratory Analyses .............................................................5 3.0 Water Quality Monitoring Results............................................................................7 3.1 Groundwater Flow and Hydraulic Gradient .............................................................7 3.2 Groundwater Analytical Results...............................................................................8 3.3 Surface Water Analytical Results.............................................................................9 3.4 Quality Assurance/Quality Control Results ..............................................................9 4.0 Conclusions ................................................................................................................11 i https://harthick.shuepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit2/2022 Second Half GWM/GML005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx Id hart hickman SMARTER ENVIRONMENTAL SOLUTIONS List of Tables Table 1 Summary of Well Construction Details Table 2 Summary of Groundwater Elevations Table 3 Summary of Field Parameters Table 4 Summary of Groundwater Flow Velocity Table 5 Summary of Groundwater and Surface Water Analytical Results List of Figures Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Groundwater Potentiometric Map (October 5, 2022) List of Appendices Appendix A Groundwater and Surface Water Sampling Records Appendix B Laboratory Analytical Reports Appendix C Summary of Historical Groundwater Elevations Appendix D Summary of Historical Constituents in Groundwater Appendix E Summary of Historical Constituents in Surface Water ii https://harthick.shaepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 ■ Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx hart : h i C km a n SMARTER ENVIRONMENTAL SOLUTIONS Water Quality Monitoring Report — September/October 2022 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 1.0 Introduction This Water Quality Monitoring Report (Report) has been prepared by Hart & Hickman, PC (H&H) to document the methods and results of semi-annual groundwater and surface water monitoring activities conducted at the Granville County Oxford Unit 2 Landfill located at 6584 Landfill Road, Oxford, Granville County, North Carolina. A site location map is included as Figure 1. Water quality monitoring at the site was performed in general accordance with the Water Quality Monitoring Plan (WQMP; March 2019) which was approved by the North Carolina Department of Environmental Quality (DEQ) Solid Waste Section (SWS). 1.1 Site Information The Granville County Oxford Landfill consists of two separate waste disposal units (Unit 1 and Unit 2). The facility is owned and operated by Granville County under Permit Numbers 3901- CDLF-1997 (Unit 1) and 3901-MSWLF-2012 (Unit 2) issued by DEQ SWS. The permitted facility consists of approximately 283 acres, of which approximately 29 acres constitutes the Unit 1 waste unit and 37.3 acres constitutes the Unit 2 waste unit. A site layout map that depicts the facility features is included as Figure 2. The Oxford Unit 1 Landfill is a former unlined municipal solid waste (MSW) landfill originally permitted for disposal of domestic, institutional, industrial, agricultural, and demolition wastes. The Oxford Unit 1 Landfill was closed in 1997. Between 1997 and 2017, the facility disposed of construction and demolition (C&D) waste on top of the closed MSW landfill in accordance with the Transition Plan dated 1994. The subject Oxford Unit 2 Landfill is a Subtitle-D MSW landfill which was permitted to operate in February 2013 and began receiving waste in May 2013. This Report covers water quality monitoring conducted at the Oxford Unit 2 Landfill. A separate Water Quality Monitoring Report will be submitted for the Oxford Unit 1 Landfill. 1 https://harthick.shmepoint.com/sites/MwtuFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx Ad hart hickman SMARTER ENVIRONMENTAL SOLUTION5 1.2 Regulatory Status The Granville County Oxford Unit 2 Landfill is currently in a Detection Monitoring Program. Water quality monitoring is completed following the North Carolina Administrative Code Title 15A-Environmental Quality Chapter 13 Sub -Chapter B Solid Waste Management Rule (NCSWMR) § 1633. Statistical analyses of the laboratory data when required is prepared following the required compliance demonstration of the NCSWMR Rule .1632(g), (h), and (i). 1.3 Groundwater Monitoring Program The groundwater monitoring program at the Oxford Unit 2 Landfill consists of the following six monitoring wells: MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Monitoring well MW- 7 is located south and upgradient of the landfill and serves as a background location. Compliance monitoring well MW-8 serves to monitor groundwater conditions downgradient of the leachate tank area which is located south to southwest and upgradient of the landfill. Compliance monitoring wells MW-9, MW-10, MW-11, and NES-2S are located along the northern downgradient side of the landfill. Groundwater samples are collected semi-annually for analysis of North Carolina Solid Waste Management Rules Appendix I list of constituents (hereafter referred to as Appendix I constituents) plus 1,4-doxane. A summary of the well locations and sample analyses for the semi-annual sampling events is provided below. The monitoring well locations and other site features are identified on Figure 2. A summary of well construction details is provided in Table 1. Well ID Classification First Half Analyses Second Half Analyses MW-7 Background App. I + 1,4-Dioxane App. I + 1,4-Dioxane MW-8 Compliance App. I + 1,4-Dioxane App. I + 1,4-Dioxane MW-9 Compliance App. I + 1,4-Dioxane App. I + 1,4-Dioxane MW-10 Compliance App. I + 1,4-Dioxane App. I + 1,4-Dioxane MW-11 Compliance App. I + 1,4-Dioxane App. I + 1,4-Dioxane NES-2S Compliance App. I + 1,4-Dioxane App. I + 1,4-Dioxane 2 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 1.4 Surface Water Monitoring Program The surface water monitoring program at the Oxford Unit 2 Landfill consists of collecting samples from two locations which are located upstream (SW-3) and downstream (SW-4) of the waste unit. The sampling points are situated along an unnamed tributary to Little Grassy Creek which runs along the eastern and northern side of the landfill. Little Grassy Creek is classified as a Class C (Aquatic Life and Secondary Recreation) stream. The locations of the surface water monitoring points are identified on Figure 2. Surface water samples are collected semi-annually and analyzed for NC Appendix I constituents plus 1,4-dioxane. https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 2.0 Water Quality Monitoring Activities 2.1 Water Level Measurements On October 5, 2022, H&H measured depth -to -water and total depths in monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Depth -to -water measurements were collected from the top -of -casing utilizing a decontaminated electronic water level indicator. Depth -to -water measurements were made after the wells were opened for a sufficient period of time to allow water levels to equilibrate with atmospheric pressure. Water level measurements and calculated groundwater elevations are presented in Table 2. 2.2 Groundwater Sampling Methods On September 29 and October 5, 2022, H&H collected groundwater samples from site monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Groundwater sampling activities began on September 29, 2022; however, due to severe weather conditions related to a tropical storm the sampling event was completed on October 5, 2022. Monitoring well MW-7 serves as the upgradient background well for the facility, and monitoring wells MW-8, MW-9, MW-10, MW-11, and NES-2S serve as compliance monitoring wells. The groundwater samples were collected and handled in accordance with the sampling protocols included in the site WQMP as well as the DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling document. Monitoring wells were purged utilizing a peristaltic pump under low flow (<200 milliliters/minute) conditions. Water levels were recorded during the purging process to ensure the pump rate did not cause significant drawdown of the water column, and samples were collected following stabilization of field parameters over three consecutive readings. Field measurements of pH, temperature, specific conductance, oxygen reduction potential (ORP), and dissolved oxygen (DO) were measured using a YSI Pro Plus water quality meter. Turbidity was measured using a Hach 2100Q turbidity meter. A summary of the final field parameters recorded prior to sample collection are presented in Table 3. Copies of groundwater sampling forms containing pertinent 4 14 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx SMARTER ENVIRONMENTAL SOLUTIONS information recorded in the field during purging and sampling at each monitoring well are provided in Appendix A. The results of the field -measured water quality parameters indicate that the values measured in groundwater collected from site monitoring wells were within applicable stabilization criteria. Groundwater at the site is slightly acidic to slightly basic based on the pH values measured in the field (5.92 to 7.82 Standard Units). Specific conductance values in site groundwater ranged from 168.0 (MW-11) to 392.1 (MW-7) microsiemens per centimeter (µS/cm). Turbidity values ranged from 0.74 (MW-8) to 9.72 (MW-11) nephelometric turbidity units (NTUs). 2.3 Surface Water Sampling Methods On October 5, 2022, H&H collected surface water samples from sample locations SW-3 and SW- 4 (Figure 2). Surface water samples were collected in general accordance with the WQMP as well as the DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling document. Field parameters were measured during sample collection and copies of surface water sampling forms are provided in Appendix A. A summary of field parameters recorded prior to sample collection is provided in Table 3. 2.4 Sample Equipment Management All reusable sampling equipment (e.g., water level indicator) was properly decontaminated between sampling locations with a non -phosphate soap and water wash, followed by multiple rinses with distilled water. New disposable nitrile or latex gloves were worn during all sampling activities. Disposable sampling equipment/material was discarded after each use. 2.5 Sample Handling and Laboratory Analyses Upon sample collection, samples for laboratory analysis were placed directly into dedicated laboratory -supplied sample bottles, labeled, and placed into ice -filled coolers. A chain -of -custody record was completed and included sample description, analyses required, matrix, sample 5 14 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx SMARTER ENVIRONMENTAL SOLUTIONS container information, and date and time of sample collection. The samples were transported on ice, under standard protocol, to Pace Analytical Services, Inc. (Pace) in Huntersville, North Carolina. Pace is a North Carolina -certified laboratory. The laboratory analytical reports and chain -of -custody records for the September/October 2022 sampling event are included in Appendix B. A summary of samples collected during the subject reporting period is provided below. The groundwater samples from monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S were analyzed for NC Appendix I constituents plus 1,4-dioxane. The surface water samples from SW-1 and SW- 2 were analyzed for NC Appendix I constituents plus 1,4-dioxane. 0 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 3.0 Water Quality Monitoring Results Groundwater and surface water monitoring activities were conducted at the site on September 29 and October 5, 2022. Groundwater and surface water samples were collected and analyzed in accordance with the DEQ approved WQMP. The monitoring results are discussed in the following sections. 3.1 Groundwater Flow and Hydraulic Gradient A summary of monitoring well gauging and water level elevation data is provided in Table 2. Historical groundwater elevation data is provided in Appendix C. Groundwater flow direction, average hydraulic gradient, and average interstitial flow velocity were derived from water -level measurements recorded during the September/October 2022 sampling event. A potentiometric map generated from the October 5, 2022 gauging event is provided as Figure 3. The October 2022 water levels are within the range of historical seasonal fluctuations observed at the site. Consistent with historical trends, the overall direction of shallow groundwater flow at the site is generally to the north to northwest towards an unnamed tributary to Little Grassy Creek. The hydraulic gradient in the vicinity of each well was derived by dividing the elevation difference between water table elevations measured at the monitoring wells and proximal potentiometric contour lines, by the perpendicular horizontal distance between the wells and potentiometric contours (Figure 3 and Table 4). The potentiometric contours indicate an average hydraulic gradient of approximately 0.013 ft/ft. Results of in -situ slug testing reported by others (LaBella Associates, 2021) indicate an average hydraulic conductivity value in the bedrock aquifer of approximately 4.43 feet/day. Using the horizontal hydraulic gradient measurements, the individual estimate of hydraulic conductivity, and an assumed effective porosity of 0.15 (LaBella Associates, 2021), the range of average interstitial groundwater flow velocities for the shallow bedrock aquifer was calculated using the following equation: Vx = (K/ne) x dh/dl. https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Where: Vx = average interstitial groundwater flow velocity; K = hydraulic conductivity; ne = effective porosity; and, dh/d1= horizontal hydraulic gradient Average linear flow velocities are estimated to range between approximately 70.37 to 997.69 feet/year (approximately 0.193 to 2.733 feet/day) with a geometric mean of approximately 140.68 feet/year (0.385 feet/day). These values are consistent with prior monitoring events. Table 4 summarizes the data used to calculate the average interstitial groundwater flow velocity in the vicinity of each monitoring well. 3.2 Groundwater Analytical Results Semi-annual groundwater sampling consisted of collecting samples from six site monitoring wells. A summary of groundwater constituent detections from the September/October 2022 sampling event is provided in Table 5. Historical analytical results are presented in Appendix D. A summary of groundwater results is provided below. Organic Anal The analytical results indicate VOCs 2-butanone, 1,4-dioxane, and 2-hexanone were detected at concentrations above MDLs in one or more wells during the September/October 2022 sampling event. The VOC detections do not exceed their respective North Carolina 2L Groundwater Standards (2L Standards). Inorganic Analyses The analytical results indicate metals antimony, arsenic, barium, cadmium, chromium, cobalt, copper, lead, nickel, selenium, and vanadium were detected at concentrations above MDLs in one or more wells during the September/October 2022 sampling event. The metal detections do not exceed their respective North Carolina 2L Groundwater Standards (2L Standards). https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 3.3 Surface Water Analytical Results Semi-annual surface water sampling consisted of collecting samples from two locations, one upstream (SW-3) and one downstream (SW-4) location. A summary of surface water constituent detections from the October 2022 sampling event is provided in Table 5. Historical analytical results are presented in Appendix E. A discussion of the results for the October 2022 sampling event is provided below. Organic Anal The analytical results indicate that VOCs were not detected at concentrations above MDLs in either surface water sample collected during the September/October 2022 sampling event. Inorganic Anal The analytical results indicate arsenic, barium, beryllium, chromium, cobalt, copper, lead, nickel, selenium, vanadium, and zinc were detected above the laboratory MDL in one or both of the surface water samples collected during the October 2022 sampling event. Copper (5.1 µg/L) was detected at a concentration above its 2B Standard (4.35 µg/L) in the sample collected from downstream location SW-4, and concentrations are similar to historical detections at this location. No other inorganic constituents were detected above MDLs during the October 2022 sampling event. 3.4 Quality Assurance/Quality Control Results Quality assurance procedures and protocols for sampling activities were conducted in general accordance with the DEQ approved WQMP. Quality assurance samples included the collection of a trip blank and field blank sample. Samples were received by the lab in good condition and met holding times and preservation requirements. Based upon a review of the data packages, no significant quality assurance/quality control (QA/QC) issues were identified for the laboratory analyses. In summary, the QA/QC results indicate that the data collected during the semi-annual monitoring event is suitable for its intended purpose. 0 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Trip Blanks Laboratory -filled trip blanks accompanied the sampling team during sampling and the transport of VOC samples to the laboratory. The trip blank samples serve as a QC check on potential external contamination and/or cross -contamination between VOC water samples during shipping and storage. The trip blank sample was analyzed for Appendix I VOCs and 1,4-dioxane. The results indicate no constituents were detected above laboratory MDLs. Fiala Rlanke A field blank sample was collected in the field by exposing laboratory -supplied deionized water to the sampling environment. The field blank is used to evaluate the potential for contamination of a sample by site contaminants from a source not associated with the samples collected. The field blank sample was analyzed for Appendix I constituents plus 1,4-dioxane. The field blank sample was non -detect with the exception of a low concentration of chromium. A total of four samples collected during the monitoring event indicate low-level concentrations similar to the detected concentration of chromium in the field blank sample. The detected concentrations of chromium in the field blank and site samples are well below groundwater 2L Standards and surface water 2B Standards. The detected concentration of chromium in the field blank sample is not considered to impact the conclusions of this report. 10 https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 4.0 Conclusions The analytical results for groundwater and surface water samples collected during the September/October 2022 event indicate no constituents were detected at concentrations above standards with the exception of copper in downstream surface water sample SW-4. The detected concentration of copper was slightly above its 2B Standard, but similar to historical concentrations detected at the location. Copper will continue to be monitored for evidence of increasing or sustained concentrations in exceedance of groundwater and/or surface water standards. Based on the water quality monitoring results, the Granville County Oxford Unit 2 Landfill will remain in the Detection Monitoring Program. The next semi-annual sampling event will be conducted in March 2023. 11 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Sept-Oct 2022.docx SMARTER ENVIRONMENTAL SOLUTIONS Table 1 Summary of Well Construction Details Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Ground TOC Top of Top Bottom Bottom Auger Total Depth Total Depth Screened Well ID Date Installed Northing Easting Elevation Elevation Screen Screen Screen Screen Refusal Comments (ft BGS) (ft BTOC) Lithology (ft AMSL) (ft AMSL) (ft BGS) (Ft BTOC) (Ft BGS) (Ft BTOC) (ft BGS) Background Well Units MW-7 7/28/2008 953292.1160 2112043.44800 531.24 534.24 34.50 37.50 19.50 22.50 34.50 37.50 34.50 Saprolite 1 & 2 MW-8 7/18/2012 953360.2000 2111527.6910 500.57 503.31 25.00 20.00 10.00 12.74 20.00 22.74 1.00 Bedrock Unit 2 Compliance MW-9 10/6/2008 954799.7410 2112842.3890 485.05 487.51 40.00 43.00 20.00 22.46 40.00 42.46 1.50 Bedrock Unit 2 Compliance MW-10 10/2/2008 955136.0000 2112571.1750 481.81 484.92 30.00 32.90 15.00 18.11 30.00 33.11 6.00 Bedrock Unit 2 Compliance MW-11 10/5/2008 954795.8510 2111957.0410 476.43 478.72 20.00 22.90 5.00 7.30 20.00 22.30 6.00 Bedrock Unit 2 Compliance MW-12 8/1/2008 954077.4350 2112567.4920 519.29 521.30 50.00 52.30 40.00 42.00 50.00 52.00 31.00 Bedrock Not Sampled Unit 2 Compliance & NES-2S 5/1/2004 955091.2902 2111945.3411 474.53 477.20 21.50 24.17 11.00 13.67 21.00 23.67 9.00 Saprolite 1 Unit 1 Performance Notes: Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. ft = feet; AMSL = above mean sea level; AGS = above ground surface TOC = top of casing; BTOC = below top of casing; * = estimated value https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 1 (Page 1 of 1) Hart & Hickman, PC Table 2 Summary of Groundwater Elevations Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Well ID Total Depth (ft BTOC) TOC Elevation (ft AMSL) October 5, 2022 Depth To Groundwater (ft BTOC) Groundwater Elevation (ft AMSL) MW-7 37.50 534.24 26.72 507.52 MW-8 22.74 503.31 3.09 500.22 MW-9 42.46 487.51 9.45 478.06 MW-10 33.11 484.92 8.35 476.57 MW-11 22.30 478.72 5.20 473.52 NES-2S 23.67 477.20 4.97 472.23 Notes: Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. TOC = top of casing; ft BTOC = feet below top of casing ft AMSL= feet above mean sea level Table 2 (Page 1 of 11) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Hart & Hickman, PC Table 3 Summary of Field Parameters Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Sample ID Sample Date Field Parameter Results Units Groundwater MW-7 9/29/2022 Conductivity 392.1 PS/CM Dissolved Oxygen 2.07 mg/I Oxidation Reduction Potential 118.3 mV pH 6.31 S.U. Temperature 18.1 °C Turbidity 9.11 NTU MW-8 10/5/2022 Conductivity 243.7 PS/CM Dissolved Oxygen 0.24 mg/I Oxidation Reduction Potential 17.6 mV pH 7.82 S.U. Temperature 23.5 oC Turbidity 0.74 NTU MW-9 10/5/2022 Conductivity 362.6 PS/CM Dissolved Oxygen 0.64 mg/I Oxidation Reduction Potential 52.4 mV pH 7.27 S.U. Temperature 19.9 oC Turbidity 4.63 NTU MW-10 10/5/2022 Conductivity 238.6 PS/CM Dissolved Oxygen 1.46 mg/I Oxidation Reduction Potential 23.8 mV pH 6.78 S.U. Temperature 18.9 oC Turbidity 9.68 NTU MW-11 10/5/2022 Conductivity 168.0 PS/CM Dissolved Oxygen 1.53 mg/I Oxidation Reduction Potential 86.7 mV pH 5.92 S.U. Temperature 18.5 oC Turbidity 9.72 NTU NES-2S 9/29/2022 Conductivity 269.5 PS/CM Dissolved Oxygen 0.26 mg/I Oxidation Reduction Potential 61.4 mV pH 6.34 S.U. Temperature 17.5 oC Turbidity 1.61 NTU Table 3 (Page 1 of 2) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 3 Summary of Field Parameters Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Sample ID Sample Date Field Parameter Results Units Surface Water SW-3 10/5/2022 Conductivity 57.6 PS/cm Dissolved Oxygen 7.11 mg/I Oxidation Reduction Potential 67.9 mV pH 7.19 S.U. Temperature 14.9 °C Turbidity 41.7 NTU SW-4 10/5/2022 Conductivity 106.5 PS/cm Dissolved Oxygen 5.55 mg/I Oxidation Reduction Potential 70.7 mV pH 7.07 S.U. Temperature 17.9 oC Turbidity 250 NTU Notes: S.U. = standard units; °C = degrees Celsius; pS/cm = microsiemens per centimeter NTU = nephelometric turbidity unit; mg/L = milligrams per liter; mV = millivolts ORP = oxidation reduction potential Table 3 (Page 2 of 2) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 4 Summary of Groundwater Flow Velocity Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Well ID Hydraulic Conductivity ��� (ft/day) Groundwater Elevation (ft AMSL) Reference Elevation (ft AMSL) Delta Elevation (ft) Map Length (ft) Hydraulic Gradient (ft/ft) Effective Porosity(') Groundwater Flow Velocity (ft/day) Groundwater Flow Velocity (ft/year) MW-7 4.43 507.52 505.00 2.52 27.23 0.093 0.15 2.733 997.69 MW-8 4.43 500.22 500.00 0.22 33.70 0.007 0.15 0.193 70.37 MW-9 4.43 478.06 480.00 1.94 147.60 0.013 0.15 0.388 141.68 MW-10 4.43 476.57 475.00 1.57 143.87 0.011 0.15 0.322 117.63 MW-11 4.43 473.52 475.00 1.48 172.50 0.009 0.15 0.253 92.49 NES-2S 4.43 472.23 475.00 2.77 416.82 0.007 0.15 0.196 71.64 Minimum -- -- -- -- 0.007 -- 0.193 70.37 Maximum -- -- -- -- 0.093 -- 2.733 997.69 Geometric Mean -- -- -- -- 0.013 -- 0.385 140.68 Notes: 1) Hydraulic conductivity and porosity values from Labella Associates Water Quality Monitoring Report - February 2021 Event. Hydraulic conductivity is based on the geometric mean of bedrock wells at the facility in 2019 and the effective porosity value for fractured bedrock was estimated at 15%. ft = feet; ft/day = feet per day; ft/year = feet per year AMSL = feet above mean sea level; -- = not applicable Vx = (K/ne) x dh/dl Vx = groundwater flow velocity K = hydraulic conductivity ne = effective porosity dh/dl = hydraulic gradient Table 4 (Page 1 of 1) Hart & Hickman, PC Table 5 Summary of Groundwater and Surface Water Analytical Results Granville County Oxford Unit 2 Landfill Butner, North Carolina H&H Job No. GMI-005 Well ID Sample Date Parameter 7(0.9si-LI)t Standard (pg/L) Source Groundwater MW-7 09/29/22 Barium 4.3 J 700 NC 2L 2-Butanone (MEK) 5.1 4,000 NC 2L 1,4-Dioxane 1.7 J 3 NC 2L MW-8 10/05/22 2-Butanone (MEK) 11.4 4,000 NC 2L Arsenic 1.4 10 NC 2L Barium 38.3 700 NC 2L Copper 12.3 1,000 NC 2L MW-9 10/05/22 Antimony 0.28 J 1 NC 2L Arsenic 0.37 J 10 NC 2L Barium 78.4 700 NC 2L 2-Butanone (MEK) 7.7 4,000 NC 2L Cadmium 0.15 J 2 NC 2L Cobalt 0.052 J 1 NC 2L Copper 1.2 J 1,000 NC 2L 2-Hexanone 0.71 J 40 NC 2L Selenium 0.27 J 20 NC 2L Vanadium 3.1 7 NC 2L MW-10 10/05/22 Arsenic 0.33 J 10 NC 2L Barium 51.2 700 NC 2L Chromium 0.54 J 10 NC 2L Cobalt 0.73 J 1 NC 2L Lead 0.12 J 15 NC 2L Nickel 0.58 J 100 NC 2L Vanadium 1.7 7 NC 2L MW-11 10/05/22 Arsenic 0.19 J 10 NC 2L Barium 28.6 700 NC 2L Chromium 0.54 J 10 NC 2L Cobalt 1.0 1 NC 2L Lead 0.14 J 15 NC 2L Nickel 2.6 100 NC 2L Vanadium 1.1 7 NC 2L NES-2S 09/29/22 Barium 33.7 700 NC 2L Surface Water SW-3 10/05/22 Arsenic 0.28 J 340 NC 2B Barium 19.5 21,000 ISTV (3) Chromium 0.91 J 109.85 (4) NC 2B Cobalt 0.27 J 16 ISTV I3) Hardness 13,400 NE NE Lead 0.42 J 6.85(4) NC 2B Vanadium 2.1 NE NE SW-4 10/05/22 Arsenic 1.2 340 NC 2B Barium 40.8 21,000 ISTV (3) Beryllium 0.10 65 NC 2B Chromium 5.0 213.71 (4) NC 2B Cobalt 2.1 16 ISTV (3) Copper 5.1 4.35(4) NC 2B Lead 1.6 17.17(4) NC 2B Nickel 2.5 170.04 (4) NC 2B Hardness 30,200 NE NE Selenium 0.26 J 5.00 NC 2B Vanadium 14.2 NE NE Zinc 9.8 J 42.49(4) NC 2L Notes: 1. NC 2L Standards are the Title 15A NCAC 02L .0202 Groundwater Standards dated April 1, 2022. 2. 15A NCAC 2B Water Quality Standards (213 Standards) for Surface Water (Class C Waters) dated July 2 3. No 2B Standard established; therefore, the value shown is the North Carolina In -Stream Target Values for Surface Waters (ISTV; July 26, 2021) 4. Acute 2B Standard is hardness dependent and was calculated using the respective measured hardness Only detected compounds are presented in this table. pg/L = micrograms per liter; -- = not applicable; NE = Not Established Table 5 (Page 1 of 1) Hart & Hickman, PC APPROXIMATE LIMITS OF WASTE UNIT 1 l 4 "Y j 4 ^^^^ERTY BOUNDARY APPROXIMATE SrERr (4_ LIMITS OF WASTE UNIT 2 i USGS The National Map: National Boundaries Dataset, 3DEP Elevation Program, Geographic Names Information System, National Hydrography Dataset, National Land Cover Database, National Structures Dataset, and National Transportation Dataset; USGS Global Ecosystems; U.S. Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S. Department of State Humanitarian Information Unit; and NOAA National Centers for Environmental Information, U.S. Coastal Relief Model. Data refreshed August, 2021. TITLE o 2,000 4,000 SITE LOCATION MAP NPROJECT SCALE IN FEET OXFORD LANDFILL GRANVILLE COUNTY U.S.G.S. QUADRANGLE MAP OXFORD, NORTH CAROLINA 2923 South Tryon Street - Suite 100 BEREA, NORTH CAROLINA2019 hart hickman Charlotte, North Carolina28203 704-586-0007 (p) 704-586-0373 (t) OXFORD, NORTH CAROLINA 2019 SMARTER E NVrFro 7jMENT LL soLUVONs License # C-1269 / # C-245 Geology 3 QUADRANGLE DATE: 11-21-22 REVISION NO: 0 7.5 MINUTE SERIES (TOPOGRAPHIC) JOB NO: GMI-004 FIGURE NO: 1 T. 4661, GO 150' 7n 490 506 7 'o _ _ •r �/ // y � I I , _ • ��-•��-,� �90 �`.,.-� /��'�' J r /// /ram/1 // 1 r /- � ,� do 46 ib 16 ! ram... -� � I � 1 ��� •. I :�26 I \ ,� 1 \ � 1 j - \ '�.... Ig r li l I it \ ter/ � / // � r \ \ �'\ � ��✓ (/� � I 1 v\ ^\ 1 530 .7v IAA )S 1Y � LEGEND k SITE PROPERTY BOUNDARY . �s[ + APPROXIMATE LIMITS OF WASTE SURFACE WATER FEATURE t '�••. GROUNDWATER MONITORING WELL SURFACE WATER SAMPLE POINT (473.52) GROUNDWATER ELEVATION (FT MSL) GROUNDWATER ELEVATION CONTOUR 500 I w `• '` •1 '• (FT MSL) APPROXIMATE GROUNDWATER FLOW DIRECTION t; ti ti APPROXIMATE LOCATION OF UNNAMED TRIBUTARY r r OF LITTLE GRASSY CREEK NES-2S (472.23) e MW-4R (476.57) - NOTES: MW-5R SW-2 t;. �' � ` a Y4 1. APPROXIMATE LIMITS OF WASTE AND LOCATIONS OF MW-11 _ MW-9 , �` .�� ENVIRONMENTAL MONITORING POINTS OBTAINED FROM MW-6R (473.52) (478.06) LABELLA GROUNDWATER MONITORING REPORTS. UNIT 2 480 2. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2021. - i f UNIT 1. ` 4$5 SW-3 MW-2ti_ MW�R 485 490 490 _ 1 495 sW-1 495 500 . .. _ — MW-8. 505 ouu.z2) MW-7 (507.52) APPROXIMATE 0 500 1,000 505 SCALE IN FEET - - GROUNDWATER POTENTIOMETRIC MAP _ (OCTOBER 5, 2022) _ - PROE` OXFORD LANDFILL UNIT 2 GRANVILLE COUNTY OXFORD, NORTH CAROLINA = - h a rt h i c k ma n 2923 100 Tryon Strcct-Screen- • 282 Charlotte, North Carolina 28203 out,, 704 586 0007(p) 704 586 0373(I) _ MW-1A SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology DATE: 12-28-22 REVISION NO. 0 - - —k, OB NO. GMI-005 FIGURE NO. 3 Appendix A Groundwater and Surface Water Sampling Records 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS hart hickman i — SMARTER ENVIRONMENTAL SOLUTIONS Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Job No: G/-� ( • 0!��f LOW -FLOW GROUNDWATER Turb. +/- 10% (<10 NTUs for metals) Well ID: Water Level: slight or stable SAMPLING RECORD drawdown during purging Well Location: ©X, L Facility Name: 0x -no) n,k Date: Top of Casing Elevation (ft msl): Casing Material: U _ _ Volume of Water Per Well Volume: gallons Total Well Depth (ftTOC): Depth to Water (ftTOC); t-C. - Well Diameter: 2 `` Sampling Personnel: C'C_1141r'�: Screen Interval (ftTOC): / • S - `l. S Type of Pump: ['► `� Tubing Material: �—D Pump/Tubing set at: �— 3 C� ft o USz ", r i, 6_s Azd,^ot t,u5.r 4v6rn3 ; i L. <_[t. Weather Conditions: cA [�U • 4 "' NOTES: H ,+ h , w 3 7. SZ �. GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity t Time Levelly Pum ed` Rate I n lmgm (°C� S/cm SU �xy mV NTU Ll 3 i ;? . o? 22_U 2.33 5� 3rC� 3 ;�_3� !� 47.5 I l-5 I-� • �z t �70U '� _- v r �c • 3 3 17. Q [� . ��L_ _ II K • ` 1 I 7 3?5-b 2 IL-7 !K Z- 3�r_ , -t_ 117. ]_� •SV ?_ .oL( M 3 3 9�. 1 ty. f 01?. io 1`3.3i fZ-Zc?�Crr`�' 7'C1 7 Other Sample Parameters: Sampled at: \- -�'U Parameters taken with: YSz Pr- h,S (R, A4­ ftert U-L Sample Delivered to; PCn� f755 r )'Ec by A _ at Field Filtration: ()Yes Q No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): \/Q(-S (-< V=f cWkO) AeAJS 'L.�/�I� DI,-, ttun l /7/'n�+tie �3`GR� w1 CAlor &4 &SZ1C I "SABBB Master Templatefforms - 2022 Forms\Law Flow Groundwater sampung rorm.put---^•--••-• • - ••- •- --- -- Last Updated 2/1412022 Procedure for Groundwater Sampling, dated April 26, 2017. hart i hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Stabilization Criteria DO +/- 0.3 mg/1 Turb. +/-10% (<10 NTUs) S. Cond. +/- 3% ORP +/- 10 mV pH +/- 0.1 unit Job No: L_fA 1 .0 L1 Well ID: yV - lb Well Location: X�[ d N C Facility Name: QAV-111 L E V n i-i I Date: S Z -2' Top of Casing Elevation (ft msl). (�, 'J Casing Material: 1-' V- Volume of Water Per Well Volume: Total Well Depth (ft): - % - Depth to Water (ft): 3• 0 Well Diameter: Z" Sampling Personnel 5 SU1)Y(S l U i7 Type of Pump: eAn I C- Tubing Material: L Q P L Pump/Tubing set at: Weather Conditions: ' n- a V, V. Ctk_6L �'� S NOTES: GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Time Levet Pumped Rate [mp111 r� �� _ 3 • I7'1 U. �f t, �? 4.1 3 ►a �� Other Sample Parameters: _ Sampled at: LAE Sample Delivered to: &ZL _ Temp. S. Cond. pH ORP Turbidity LQ Slcm Lalu� Lnv_l (NTU) 23-5- 2K '�-�?�.L i�.t� c•��l Parameters taken with: S j ND PV Or L J A ( Piro � , +VVjrrl'Si 0V1_A-Q M by ' -i _ at Field Filtration: ( ) Yes ( X ) No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): ,&10 ) - 1� r i File: S:VWA-Master Templates\Forms-Groundwater1ow Flow Groundwater Sampling Record Date:1/21/2016 hart *- hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Job No: (') i-' E I. d U S- Well ID: Well Location: Facility Name: L A L r U n 1-1 i Date: 10 � 5 /22 Top of Casing Elevat- (ft msl): 9'61 - 5-1 Casing Materi \V'(2., Volume of Water Per Well Volume: Total Well Depth (ft}: r `� 15'Depth to Water (ft):' i' &� ' L�S Well Diameter: Sampling Personnel: S S 0 Y) V1 Type of Pump:Tubing Material: �_ 1� l_ Pump/Tubing set at: �JIQ`�' ft. Stabilization Criteria DO +/- 0.3 mg/1 Turb. +/- 10% (<10 NTUs) S. Cond. +/- 3% ORP +/- 10 mV pH +/- 0.1 unit Weather Conditions: 4-s-VU IV2l4 0--•i' U Gig NOTES: GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity im Level Pumoed Rate (Mg/1) C—Cl Slcm (SU) (MV) (NTU) 1 t� -C1 n (D - 3 `1 _ Ll _-Jvb I �I Jo• i�4 3 :.,"�c -�� �rT 3{n �f .-5 -aL4 Sta c: VC0 h r �,La�+ 3 't- .��i S3 �t 7,-- 7 i 4-154 tZ°a Q - (og 1 Ui'6l ,3ib 2-.10 Li 3 Other Sample Parameters: Sampled at: ILA Parameters taken with:""( Sample Delivered to: DLL , by [At�t� �• at Field Filtration: ( ) Yes ( X ) No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives)_ [- i 4) , ;1 X yy1/ File: SMAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Date:1/21/2016 hart i hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Facility Name: bc-F L` UI t ► # Top of Casing Elevation (ft msl): Z Job No: (_")M I - 1) � S' Well ID: M V\) — ((U Well Location:tYcl Date: f G -2, Casing Material: S'1{i i Volume of Water Per Well Volume: _ 3_ U 7) Stabilization Criteria DO +/- 0.3 mg/1 Turb. +/-10% (<10 NTUs) S. Cond. +/- 3% ORP +/-10 mV pH +/- 0.1 unit Total Well Depth (ft): �� Sampling Personnel: a �y✓ln S Depth to Water (ft):. C 1� - , Well Diameter: Type of Pulnp: PQ.V Tubing Material: L- IDPt Pump/Tubing set at: ?10 ft. Weather Conditions: �ti4yl 11 tI , I�� Q-�tr �� `� ` NOTES: W el I YXI, j _ Ut,1 N t I -(u." lC_ I'" w tl-, Si Et-la-Ce.. -fr i I`f o _ 5 -j�-;` i i i r�_�— GROUNDWATER SAMPLING PARAMETERS ` '` �f i 016 _ Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate [mgLI LCj IS/Cm SU (MV) Nf TU) e>.LAO rnl_/min 1 V( M G ??r7.L? U 52- ia.L L'L.S-ct -0t I I ug- E.. e I -1st + ' Lt L4 •`& z 1� '� 2 j cl 3 . I L 0 cb 4fb E 1'b0 1 •4 l❑ 1` . 41 IS t. La is Y2 2 t� �,ctry fl �}v3•Y� U Other Sample Parameters: Sampled at: i l Parameters taken with: , r..p)V ! P rb plus yy it �( { t�} 1 _Wy-joi4 •ice Sample Delivered to: o by L 0U I`1 I eA at Field Filtration: ( ) Yes ( X ) No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): y0-�_�1 File: S:\W-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Dale:1 /21 /2016 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Job No: L— I\4 1 0 U S Well ID: "V'V - I ( Well Location: t) K_{ Facility Name: OK"Y3 L F 0 V1 Date: I U% S 22 Top of Casing Elevation (ft msl): U{ L), -2- Casing Material: P V , Volume of Water Per Well Volume: Total Well Depth (ft): ; C1L) Depth to Water (ft): S l7 Well Diameter: 2 " Sampling Personnel: r r '-h, cly Type of Pump:. P &V I $ht.bt L Tubing Material: nl�{ Pump/Tubing set at: # ft. Stabilization Criteria DO +/- 0.3 mg/1 Turb. +/- 10% (<10 NTUs) S. Cond. +/- 3% ORP +/- 10 mV pH +/- 0.1 unit Weather Conditions: -,Lk Vlt t jl _C -'Qkr'W U-y S NOTES: we 11 Amn& t y k-4 i' �i-wt i i Sr•l I� �1 GROUNDWATER SAMPLING PARAMETERS �� �G�'vG►-'E-�'`� �`'� I2 Water Volume Pumping DO Temp. S. Cond. pH ❑RP Turbidity Time Level Pumped Rate (mall] (Ij S/cm) LIUL imV] (NTQJ la all C 1�t! Mthnin g24 iFi• 190-. �u - II I 1a 32 t - ;Do mi, 9, -a Q i+ . Cl i Lou -1, ir,_ sue. C' 12L35' Z 1) cc i i U-1- 6 ia3'� i to t ut� I lb ArI L `� `I ? `i S16 ,.3 1. SY) -- I.b 1rr `l `7L i� H. 1 A f. Lid '.Z-H eta ^� t eJ 1 S .a 1 . s 1 to `p 5 `1 "t_ dh Ca • �} �Z ► •• •�3 EDWi Other Sample Parameters: Sampled at: i s S S Parameters taken with: S i Pty, VL l 9 i 'w L ILI I E Sample Delivered to: P G+- -e by , ( I -K A--V i _ _ at Field Filtration: ( ) Yes ( X ) No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Date:1/21/2016 hart -== hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Facility Name: c?-K4rJ U' : � I 00 Job No: Well ID: Well Location: (19.1411 0,21 Date: q /7-4 /1-1, Top of Casing Elevation (ft msl): 4r?7. ZO Casing Material: lyc Volume of Water Per Well Volumegallons Total Well Depth (ftTOC): 2� • Depth to Water (ftTOC): Well Diameter: Sampling Personnel:,!'af��w- , ~- Screen Interval (ftTOC): Type of Pump: Tubing Material: , L p I Pump/Tubing set at: ft Weather Conditions: ��/`Cr( rnR �" 76vl NOTES: "^`'� A.'-L-mot Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Turb. +/- 10% (<10 NTUs for metals) Water Level: slight or stable drawdown during purging GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate LM&IM1°Cl(US/cm) -= (mV) NTUTUI 2GS 5 6 .. 3.s" afi CHI �9-0"L- 1 0 7.5? 271.E ��_ �1y.7 �— �1 / Z2S c, Cy..?3 / 7 C 2 70.5� .. � 7 1 E—L e" `LG 17 S•- Z64--S A - Other Sample Parameters: Sampled at:__/.1�Z Parameters taken with: �1�T _���, %•fS r_1���I�� i�tic r��-Z , rt, Sample Delivered to: F'-'e- by 0- J at Field Filtration: Q Yes Q No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): VC"CS (Sr� /1�.��(� 2-Svn.L rrl A"� - l,,,,, �2So nL U[ r'Lttar �!r ��' 2SOn•G vR -MS I !�C n rwu c� l.. ttug 'S5 _ .�, 4 G�c� �.r t/� S r 1ev►C �t l ,c3 S h �r tl.,..._ �71-Pur G i e.T S �! • 4 r "S:1BBB Master Templates\Forms -2022 Forms1ow Flow Groundwater Sampling Form,pdf' Stabilization criteria guidelines from the EPA SESD Operating Last Updated: 211412022 Procedure for Groundwater Sampling, dated April 26, 2017 hart ` hickman SMARTER ENVIRONMENTAL SOLUTIONS Job No.: GM1.005 Site Name: Oxford LF Unit 2 Surface Water Sampling Form GENERAL INFORMATION Location No.: SW-3 Location: Oxford, NC Date: 10/05/22 Sample Type (0) Grab (❑) Composite (❑) Other Sampling Equipment (❑) Dedicated (❑) Decontaminated (❑) Bailer (❑) Pump Material (❑) PVC (❑) Stainless Steel (❑) Teflon (❑) Other Decontamination Method: Alconox and DI Water Rinse - Note samples were collected directly into sample containers, thus no decontamination was needed. LOCATION INFORMATION Coordinates: Sample Location Dimentions Width NA Depth to Stream Bed NA PURGING INFORMATION Time pH (SU) Temp. (°C) S. Cond. (umhos/cm) Redox Turbidity (NTU) 16:55 7.11 14.9 57.6 67.9 41.7 Weather Conditions: Sunny, Clear, 60s Sample Condition: (❑✓) Clear (❑) Cloudy (❑) Other: Field Filtration: (❑) Yes (❑) No Containers (Types, Numbers, Preservatives): Appendix I, Hardness, 1-4 Dioxane Comments: DO = 7.11 mg/L Sample Collector: E Dye, J Johns File: SW Sampling Log, SW Form Date: 2/20/2018 Odor: Date:10/5/22 Time:16:55 hart ` hickman SMARTER ENVIRONMENTAL SOLUTIONS Job No.: GM1.005 Site Name: Oxford LF Unit 2 Surface Water Sampling Form GENERAL INFORMATION Location No.: SW-4 Location: Oxford, NC Date: 10/05/22 Sample Type (0) Grab (❑) Composite (❑) Other Sampling Equipment (❑) Dedicated (❑) Decontaminated (❑) Bailer (❑) Pump Material (❑) PVC (❑) Stainless Steel (❑) Teflon (❑) Other Decontamination Method: Alconox and DI Water Rinse - Note samples were collected directly into sample containers, thus no decontamination was needed. LOCATION INFORMATION Coordinates: Sample Location Dimentions Width NA Depth to Stream Bed NA PURGING INFORMATION Time pH (SU) Temp. (°C) S. Cond. (umhos/cm) Redox Turbidity (NTU) 15:50 7.19 17.9 106.5 70.7 250 Weather Conditions: Sunny, Clear 60s Sample Condition: (❑) Clear (❑✓) Cloudy (❑) Other: Field Filtration: (❑) Yes (❑✓ ) No Containers (Types, Numbers, Preservatives): Appendix I, Hardness, 1-4 Dioxane Comments: DO = 5.55 mg/L Sample Collector: E Dye, J Johns File: SW Sampling Log, SW Form Date: 2/20/2018 Odor: Date:10/5/22 Time:15:50 Appendix B Laboratory Analytical Reports 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 27, 2022 Jeffrey 011ison Hart & Hickman 3921 Sunset Ridge Rd. Ste. 301 Raleigh, NC 27607 RE: Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Dear Jeffrey 011ison: Enclosed are the analytical results for sample(s) received by the laboratory between October 06, 2022 and October 07, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte A revised laboratory report is being submitted on 11/1/22 to report all missing analytes. A revised report is being issued on 11/8/22 to add missing 8260 compounds. If you have any questions concerning this report, please feel free to contact me. Sincerely, -� &-I-- Taylor M Cannon taylor.cannon@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Lab ID Sample ID Matrix Date Collected Date Received 92630054001 MW-8 Water 10/05/2213:45 10/06/2214:19 92630054002 MW-9 Water 10/05/2214:40 10/06/2214:19 92630054003 MW-10 Water 10/05/2211:40 10/06/2214:19 92630054004 MW-11 Water 10/05/2212:55 10/06/2214:19 92630054005 SW-3 Water 10/05/2216:55 10/06/2214:19 92630054006 SW-4 Water 10/05/2215:50 10/06/2214:19 92630054007 Field Blank -Unit 2 Water 10/05/22 17:25 10/06/22 14:19 92630054008 Trip Blank Water 10/05/22 00:00 10/07/22 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: GMI-005 Oxford LF Unit 2 92630054 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92630054001 MW-8 EPA6020B DBB1 15 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054002 MW-9 EPA6020B DBB1 15 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054003 MW-10 EPA6020B DBB1 15 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054004 MW-11 EPA6020B DBB1 15 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054005 SW-3 EPA6020B DBB1 16 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054006 SW-4 EPA6020B DBB1 16 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054007 Field Blank -Unit 2 EPA 6020E CRW 15 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92630054008 Trip Blank EPA 8260D LMB 63 PASI-C EPA 8260D Mod. LMB 3 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-8 Lab ID: 92630054001 Collected: 10/05/22 13:45 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:22 7440-36-0 Arsenic 1.4 ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:22 7440-38-2 Barium 38.3 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:22 7440-39-3 Beryllium ND ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:22 7440-41-7 Cadmium ND ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:22 7440-43-9 Chromium ND ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:22 7440-47-3 Cobalt ND ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:22 7440-48-4 Copper 12.3 ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:22 7440-50-8 Lead ND ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:22 7439-92-1 Nickel ND ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:22 7440-02-0 Selenium ND ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:22 7782-49-2 Silver ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:22 7440-22-4 Thallium ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:22 7440-28-0 Vanadium ND ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:22 7440-62-2 Zinc ND ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:22 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/10/22 21:19 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/10/22 21:19 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/10/22 21:19 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/10/22 21:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/10/22 21:19 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/10/22 21:19 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/10/22 21:19 74-83-9 v2 2-Butanone (MEK) 11.4 ug/L 5.0 4.0 1 10/10/22 21:19 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/10/22 21:19 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/10/22 21:19 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/10/22 21:19 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/10/22 21:19 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/10/22 21:19 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/10/22 21:19 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/10/22 21:19 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/10/22 21:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/10/22 21:19 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/10/22 21:19 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/10/22 21:19 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/10/22 21:19 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/10/22 21:19 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/10/22 21:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/10/22 21:19 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/10/22 21:19 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/10/22 21:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/10/22 21:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/10/22 21:19 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-8 Lab ID: 92630054001 Collected: 10/05/22 13:45 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 95 % 70-130 105 % 70-130 97 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 99 % 70-130 99 % 70-130 0.36 1 10/10/22 21:19 10061-01-5 0.36 1 10/10/22 21:19 10061-02-6 0.30 1 10/10/22 21:19 100-41-4 0.48 1 10/10/22 21:19 591-78-6 9.7 1 10/10/22 21:19 74-88-4 2.0 1 10/10/22 21:19 75-09-2 2.7 1 10/10/22 21:19 108-10-1 0.29 1 10/10/22 21:19 100-42-5 0.31 1 10/10/22 21:19 630-20-6 0.22 1 10/10/22 21:19 79-34-5 0.29 1 10/10/22 21:19 127-18-4 0.48 1 10/10/22 21:19 108-88-3 0.33 1 10/10/22 21:19 71-55-6 0.32 1 10/10/22 21:19 79-00-5 0.38 1 10/10/22 21:19 79-01-6 0.30 1 10/10/22 21:19 75-69-4 0.26 1 10/10/22 21:19 96-18-4 1.3 1 10/10/22 21:19 108-05-4 0.39 1 10/10/22 21:19 75-01-4 0.34 1 10/10/22 21:19 1330-20-7 1 10/10/22 21:19 460-00-4 1 10/10/22 21:19 17060-07-0 1 10/10/22 21:19 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 21:01 123-91-1 10/10/22 21:01 17060-07-0 10/10/22 21:01 2037-26-5 Page 6 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-9 Lab ID: 92630054002 Collected: 10/05/22 14:40 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony 0.28J ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:26 7440-36-0 Arsenic 0.37J ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:26 7440-38-2 Barium 78.4 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:26 7440-39-3 Beryllium ND ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:26 7440-41-7 Cadmium 0.15J ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:26 7440-43-9 Chromium ND ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:26 7440-47-3 Cobalt 0.052J ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:26 7440-48-4 Copper 1.2.1 ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:26 7440-50-8 Lead ND ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:26 7439-92-1 Nickel ND ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:26 7440-02-0 Selenium 0.27J ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:26 7782-49-2 Silver ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:26 7440-22-4 Thallium ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:26 7440-28-0 Vanadium 3.1 ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:26 7440-62-2 Zinc ND ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:26 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/10/22 21:37 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/10/22 21:37 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/10/22 21:37 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/10/22 21:37 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/10/22 21:37 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/10/22 21:37 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/10/22 21:37 74-83-9 v2 2-Butanone (MEK) 7.7 ug/L 5.0 4.0 1 10/10/22 21:37 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/10/22 21:37 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/10/22 21:37 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/10/22 21:37 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/10/22 21:37 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/10/22 21:37 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/10/22 21:37 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/10/22 21:37 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/10/22 21:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/10/22 21:37 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/10/22 21:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/10/22 21:37 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/10/22 21:37 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/10/22 21:37 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/10/22 21:37 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/10/22 21:37 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/10/22 21:37 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/10/22 21:37 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/10/22 21:37 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/10/22 21:37 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-9 Lab ID: 92630054002 Collected: 10/05/22 14:40 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.71J ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 98 % 70-130 103 % 70-130 98 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 98 % 70-130 96 % 70-130 0.36 1 10/10/22 21:37 10061-01-5 0.36 1 10/10/22 21:37 10061-02-6 0.30 1 10/10/22 21:37 100-41-4 0.48 1 10/10/22 21:37 591-78-6 9.7 1 10/10/22 21:37 74-88-4 2.0 1 10/10/22 21:37 75-09-2 2.7 1 10/10/22 21:37 108-10-1 0.29 1 10/10/22 21:37 100-42-5 0.31 1 10/10/22 21:37 630-20-6 0.22 1 10/10/22 21:37 79-34-5 0.29 1 10/10/22 21:37 127-18-4 0.48 1 10/10/22 21:37 108-88-3 0.33 1 10/10/22 21:37 71-55-6 0.32 1 10/10/22 21:37 79-00-5 0.38 1 10/10/22 21:37 79-01-6 0.30 1 10/10/22 21:37 75-69-4 0.26 1 10/10/22 21:37 96-18-4 1.3 1 10/10/22 21:37 108-05-4 0.39 1 10/10/22 21:37 75-01-4 0.34 1 10/10/22 21:37 1330-20-7 1 10/10/22 21:37 460-00-4 1 10/10/22 21:37 17060-07-0 1 10/10/22 21:37 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 21:20 123-91-1 10/10/22 21:20 17060-07-0 10/10/22 21:20 2037-26-5 Page 8 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-10 Lab ID: 92630054003 Collected: 10/05/22 11:40 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:30 7440-36-0 Arsenic 0.33J ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:30 7440-38-2 Barium 51.2 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:30 7440-39-3 Beryllium ND ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:30 7440-41-7 Cadmium ND ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:30 7440-43-9 Chromium 0.54J ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:30 7440-47-3 Cobalt 0.73J ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:30 7440-48-4 Copper ND ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:30 7440-50-8 Lead 0.12J ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:30 7439-92-1 Nickel 0.581 ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:30 7440-02-0 Selenium ND ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:30 7782-49-2 Silver ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:30 7440-22-4 Thallium ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:30 7440-28-0 Vanadium 1.7 ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:30 7440-62-2 Zinc ND ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:30 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/10/22 21:55 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/10/22 21:55 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/10/22 21:55 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/10/22 21:55 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/10/22 21:55 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/10/22 21:55 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/10/22 21:55 74-83-9 v2 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/10/22 21:55 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/10/22 21:55 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/10/22 21:55 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/10/22 21:55 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/10/22 21:55 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/10/22 21:55 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/10/22 21:55 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/10/22 21:55 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/10/22 21:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/10/22 21:55 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/10/22 21:55 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/10/22 21:55 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/10/22 21:55 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/10/22 21:55 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/10/22 21:55 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/10/22 21:55 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/10/22 21:55 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/10/22 21:55 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/10/22 21:55 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/10/22 21:55 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-10 Lab ID: 92630054003 Collected: 10/05/22 11:40 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 96 % 70-130 109 % 70-130 102 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 95 % 70-130 99 % 70-130 0.36 1 10/10/22 21:55 10061-01-5 0.36 1 10/10/22 21:55 10061-02-6 0.30 1 10/10/22 21:55 100-41-4 0.48 1 10/10/22 21:55 591-78-6 9.7 1 10/10/22 21:55 74-88-4 2.0 1 10/10/22 21:55 75-09-2 2.7 1 10/10/22 21:55 108-10-1 0.29 1 10/10/22 21:55 100-42-5 0.31 1 10/10/22 21:55 630-20-6 0.22 1 10/10/22 21:55 79-34-5 0.29 1 10/10/22 21:55 127-18-4 0.48 1 10/10/22 21:55 108-88-3 0.33 1 10/10/22 21:55 71-55-6 0.32 1 10/10/22 21:55 79-00-5 0.38 1 10/10/22 21:55 79-01-6 0.30 1 10/10/22 21:55 75-69-4 0.26 1 10/10/22 21:55 96-18-4 1.3 1 10/10/22 21:55 108-05-4 0.39 1 10/10/22 21:55 75-01-4 0.34 1 10/10/22 21:55 1330-20-7 1 10/10/22 21:55 460-00-4 1 10/10/22 21:55 17060-07-0 1 10/10/22 21:55 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 21:40 123-91-1 10/10/22 21:40 17060-07-0 10/10/22 21:40 2037-26-5 Page 10 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-11 Lab ID: 92630054004 Collected: 10/05/22 12:55 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:34 7440-36-0 Arsenic 0.191 ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:34 7440-38-2 Barium 28.6 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:34 7440-39-3 Beryllium ND ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:34 7440-41-7 Cadmium ND ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:34 7440-43-9 Chromium 0.54J ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:34 7440-47-3 Cobalt 1.0 ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:34 7440-48-4 Copper ND ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:34 7440-50-8 Lead 0.14J ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:34 7439-92-1 Nickel 2.6 ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:34 7440-02-0 Selenium ND ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:34 7782-49-2 Silver ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:34 7440-22-4 Thallium ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:34 7440-28-0 Vanadium 1.1 ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:34 7440-62-2 Zinc ND ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:34 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/10/22 22:13 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/10/22 22:13 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/10/22 22:13 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/10/22 22:13 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/10/22 22:13 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/10/22 22:13 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/10/22 22:13 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/10/22 22:13 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/10/22 22:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/10/22 22:13 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/10/22 22:13 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/10/22 22:13 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/10/22 22:13 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/10/22 22:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/10/22 22:13 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/10/22 22:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/10/22 22:13 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/10/22 22:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/10/22 22:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/10/22 22:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/10/22 22:13 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/10/22 22:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/10/22 22:13 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/10/22 22:13 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/10/22 22:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/10/22 22:13 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/10/22 22:13 78-87-5 Date: 12/27/2022 02:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 11 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: MW-11 Lab ID: 92630054004 Collected: 10/05/22 12:55 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 93 % 70-130 107 % 70-130 101 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 95 % 70-130 99 % 70-130 0.36 1 10/10/22 22:13 10061-01-5 0.36 1 10/10/22 22:13 10061-02-6 0.30 1 10/10/22 22:13 100-41-4 0.48 1 10/10/22 22:13 591-78-6 9.7 1 10/10/22 22:13 74-88-4 2.0 1 10/10/22 22:13 75-09-2 2.7 1 10/10/22 22:13 108-10-1 0.29 1 10/10/22 22:13 100-42-5 0.31 1 10/10/22 22:13 630-20-6 0.22 1 10/10/22 22:13 79-34-5 0.29 1 10/10/22 22:13 127-18-4 0.48 1 10/10/22 22:13 108-88-3 0.33 1 10/10/22 22:13 71-55-6 0.32 1 10/10/22 22:13 79-00-5 0.38 1 10/10/22 22:13 79-01-6 0.30 1 10/10/22 22:13 75-69-4 0.26 1 10/10/22 22:13 96-18-4 1.3 1 10/10/22 22:13 108-05-4 0.39 1 10/10/22 22:13 75-01-4 0.34 1 10/10/22 22:13 1330-20-7 1 10/10/22 22:13 460-00-4 1 10/10/22 22:13 17060-07-0 1 10/10/22 22:13 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 21:59 123-91-1 10/10/22 21:59 17060-07-0 10/10/22 21:59 2037-26-5 Page 12 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: SW-3 Lab ID: 92630054005 Collected: 10/05/22 16:55 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Hardness, Total(SM 2340B) Vanadium Zinc 8260D MSV Low Level Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1.2-Dichloroethene Date: 12/27/2022 02:52 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:38 7440-36-0 0.28J ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:38 7440-38-2 19.5 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:38 7440-39-3 ND ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:38 7440-41-7 ND ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:38 7440-43-9 0.911 ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:38 7440-47-3 0.27J ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:38 7440-48-4 ND ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:38 7440-50-8 0.42J ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:38 7439-92-1 ND ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:38 7440-02-0 ND ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:38 7782-49-2 ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:38 7440-22-4 ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:38 7440-28-0 13400 ug/L 541 541 1 10/11/22 15:06 10/11/22 22:38 2.1 ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:38 7440-62-2 ND ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:38 7440-66-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 10/10/22 22:31 67-64-1 ND ug/L 10.0 1.8 1 10/10/22 22:31 107-13-1 ND ug/L 1.0 0.34 1 10/10/22 22:31 71-43-2 ND ug/L 1.0 0.47 1 10/10/22 22:31 74-97-5 ND ug/L 1.0 0.31 1 10/10/22 22:31 75-27-4 ND ug/L 1.0 0.34 1 10/10/22 22:31 75-25-2 ND ug/L 2.0 1.7 1 10/10/22 22:31 74-83-9 ND ug/L 5.0 4.0 1 10/10/22 22:31 78-93-3 ND ug/L 2.0 0.36 1 10/10/22 22:31 75-15-0 ND ug/L 1.0 0.33 1 10/10/22 22:31 56-23-5 ND ug/L 1.0 0.28 1 10/10/22 22:31 108-90-7 ND ug/L 1.0 0.65 1 10/10/22 22:31 75-00-3 ND ug/L 1.0 0.43 1 10/10/22 22:31 67-66-3 ND ug/L 1.0 0.54 1 10/10/22 22:31 74-87-3 ND ug/L 2.0 0.34 1 10/10/22 22:31 96-12-8 ND ug/L 1.0 0.36 1 10/10/22 22:31 124-48-1 ND ug/L 1.0 0.27 1 10/10/22 22:31 106-93-4 ND ug/L 1.0 0.39 1 10/10/22 22:31 74-95-3 ND ug/L 1.0 0.34 1 10/10/22 22:31 95-50-1 ND ug/L 1.0 0.33 1 10/10/22 22:31 106-46-7 ND ug/L 1.0 0.56 1 10/10/22 22:31 110-57-6 ND ug/L 1.0 0.37 1 10/10/22 22:31 75-34-3 ND ug/L 1.0 0.32 1 10/10/22 22:31 107-06-2 ND ug/L 1.0 0.35 1 10/10/22 22:31 75-35-4 ND ug/L 1.0 0.38 1 10/10/22 22:31 156-59-2 ND ug/L 1.0 0.40 1 10/10/22 22:31 156-60-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 13 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: SW-3 Lab ID: 92630054005 Collected: 10/05/22 16:55 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y�:i111 e7 �, 6yyL91 �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 94 % 70-130 107 % 70-130 104 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 96 % 70-130 95 % 70-130 0.36 1 10/10/22 22:31 78-87-5 0.36 1 10/10/22 22:31 10061-01-5 0.36 1 10/10/22 22:31 10061-02-6 0.30 1 10/10/22 22:31 100-41-4 0.48 1 10/10/22 22:31 591-78-6 9.7 1 10/10/22 22:31 74-88-4 2.0 1 10/10/22 22:31 75-09-2 2.7 1 10/10/22 22:31 108-10-1 0.29 1 10/10/22 22:31 100-42-5 0.31 1 10/10/22 22:31 630-20-6 0.22 1 10/10/22 22:31 79-34-5 0.29 1 10/10/22 22:31 127-18-4 0.48 1 10/10/22 22:31 108-88-3 0.33 1 10/10/22 22:31 71-55-6 0.32 1 10/10/22 22:31 79-00-5 0.38 1 10/10/22 22:31 79-01-6 0.30 1 10/10/22 22:31 75-69-4 0.26 1 10/10/22 22:31 96-18-4 1.3 1 10/10/22 22:31 108-05-4 0.39 1 10/10/22 22:31 75-01-4 0.34 1 10/10/22 22:31 1330-20-7 1 10/10/22 22:31 460-00-4 1 10/10/22 22:31 17060-07-0 1 10/10/22 22:31 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 22:18 123-91-1 10/10/22 22:18 17060-07-0 10/10/22 22:18 2037-26-5 Page 14 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: SW-4 Lab ID: 92630054006 Collected: 10/05/22 15:50 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Hardness, Total(SM 2340B) Vanadium Zinc 8260D MSV Low Level Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1.2-Dichloroethene Date: 12/27/2022 02:52 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 1.0 0.20 1 10/11/22 15:06 10/11/22 22:41 7440-36-0 1.2 ug/L 1.0 0.087 1 10/11/22 15:06 10/11/22 22:41 7440-38-2 40.8 ug/L 1.0 0.21 1 10/11/22 15:06 10/11/22 22:41 7440-39-3 0.10 ug/L 0.10 0.050 1 10/11/22 15:06 10/11/22 22:41 7440-41-7 ND ug/L 0.20 0.060 1 10/11/22 15:06 10/11/22 22:41 7440-43-9 5.0 ug/L 1.0 0.50 1 10/11/22 15:06 10/11/22 22:41 7440-47-3 2.1 ug/L 1.0 0.050 1 10/11/22 15:06 10/11/22 22:41 7440-48-4 5.1 ug/L 2.0 1.1 1 10/11/22 15:06 10/11/22 22:41 7440-50-8 1.6 ug/L 1.0 0.077 1 10/11/22 15:06 10/11/22 22:41 7439-92-1 2.5 ug/L 1.0 0.42 1 10/11/22 15:06 10/11/22 22:41 7440-02-0 0.26J ug/L 2.0 0.072 1 10/11/22 15:06 10/11/22 22:41 7782-49-2 ND ug/L 0.40 0.070 1 10/11/22 15:06 10/11/22 22:41 7440-22-4 ND ug/L 0.47 0.050 1 10/11/22 15:06 10/11/22 22:41 7440-28-0 30200 ug/L 541 541 1 10/11/22 15:06 10/11/22 22:41 14.2 ug/L 1.0 0.25 1 10/11/22 15:06 10/11/22 22:41 7440-62-2 9.81 ug/L 10.0 2.7 1 10/11/22 15:06 10/11/22 22:41 7440-66-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 10/10/22 22:50 67-64-1 ND ug/L 10.0 1.8 1 10/10/22 22:50 107-13-1 ND ug/L 1.0 0.34 1 10/10/22 22:50 71-43-2 ND ug/L 1.0 0.47 1 10/10/22 22:50 74-97-5 ND ug/L 1.0 0.31 1 10/10/22 22:50 75-27-4 ND ug/L 1.0 0.34 1 10/10/22 22:50 75-25-2 ND ug/L 2.0 1.7 1 10/10/22 22:50 74-83-9 ND ug/L 5.0 4.0 1 10/10/22 22:50 78-93-3 ND ug/L 2.0 0.36 1 10/10/22 22:50 75-15-0 ND ug/L 1.0 0.33 1 10/10/22 22:50 56-23-5 ND ug/L 1.0 0.28 1 10/10/22 22:50 108-90-7 ND ug/L 1.0 0.65 1 10/10/22 22:50 75-00-3 ND ug/L 1.0 0.43 1 10/10/22 22:50 67-66-3 ND ug/L 1.0 0.54 1 10/10/22 22:50 74-87-3 ND ug/L 2.0 0.34 1 10/10/22 22:50 96-12-8 ND ug/L 1.0 0.36 1 10/10/22 22:50 124-48-1 ND ug/L 1.0 0.27 1 10/10/22 22:50 106-93-4 ND ug/L 1.0 0.39 1 10/10/22 22:50 74-95-3 ND ug/L 1.0 0.34 1 10/10/22 22:50 95-50-1 ND ug/L 1.0 0.33 1 10/10/22 22:50 106-46-7 ND ug/L 1.0 0.56 1 10/10/22 22:50 110-57-6 ND ug/L 1.0 0.37 1 10/10/22 22:50 75-34-3 ND ug/L 1.0 0.32 1 10/10/22 22:50 107-06-2 ND ug/L 1.0 0.35 1 10/10/22 22:50 75-35-4 ND ug/L 1.0 0.38 1 10/10/22 22:50 156-59-2 ND ug/L 1.0 0.40 1 10/10/22 22:50 156-60-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 15 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: SW-4 Lab ID: 92630054006 Collected: 10/05/22 15:50 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) E:Y�:i111 e7 �, 6yyL91 �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 93 % 70-130 108 % 70-130 99 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 98 % 70-130 102 % 70-130 0.36 1 10/10/22 22:50 78-87-5 0.36 1 10/10/22 22:50 10061-01-5 0.36 1 10/10/22 22:50 10061-02-6 0.30 1 10/10/22 22:50 100-41-4 0.48 1 10/10/22 22:50 591-78-6 9.7 1 10/10/22 22:50 74-88-4 2.0 1 10/10/22 22:50 75-09-2 2.7 1 10/10/22 22:50 108-10-1 0.29 1 10/10/22 22:50 100-42-5 0.31 1 10/10/22 22:50 630-20-6 0.22 1 10/10/22 22:50 79-34-5 0.29 1 10/10/22 22:50 127-18-4 0.48 1 10/10/22 22:50 108-88-3 0.33 1 10/10/22 22:50 71-55-6 0.32 1 10/10/22 22:50 79-00-5 0.38 1 10/10/22 22:50 79-01-6 0.30 1 10/10/22 22:50 75-69-4 0.26 1 10/10/22 22:50 96-18-4 1.3 1 10/10/22 22:50 108-05-4 0.39 1 10/10/22 22:50 75-01-4 0.34 1 10/10/22 22:50 1330-20-7 1 10/10/22 22:50 460-00-4 1 10/10/22 22:50 17060-07-0 1 10/10/22 22:50 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 22:37 123-91-1 10/10/22 22:37 17060-07-0 10/10/22 22:37 2037-26-5 Page 16 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: Field Blank -Unit 2 Lab ID: 92630054007 Collected: 10/05/22 17:25 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 1.0 0.20 1 10/18/2215:48 10/19/2216:10 7440-36-0 Arsenic ND ug/L 1.0 0.087 1 10/18/2215:48 10/19/2216:10 7440-38-2 Barium ND ug/L 1.0 0.21 1 10/18/2215:48 10/19/2216:10 7440-39-3 Beryllium ND ug/L 0.10 0.050 1 10/18/2215:48 10/19/2216:10 7440-41-7 Cadmium ND ug/L 0.20 0.060 1 10/18/2215:48 10/19/2216:10 7440-43-9 Chromium 0.78J ug/L 1.0 0.50 1 10/18/2215:48 10/19/2216:10 7440-47-3 Cobalt ND ug/L 1.0 0.050 1 10/18/2215:48 10/19/2216:10 7440-48-4 Copper ND ug/L 2.0 1.1 1 10/18/2215:48 10/19/2216:10 7440-50-8 Lead ND ug/L 1.0 0.077 1 10/18/2215:48 10/19/2216:10 7439-92-1 Nickel ND ug/L 1.0 0.42 1 10/18/2215:48 10/19/2216:10 7440-02-0 Selenium ND ug/L 2.0 0.072 1 10/18/2215:48 10/19/2216:10 7782-49-2 Silver ND ug/L 0.40 0.070 1 10/18/2215:48 10/19/2216:10 7440-22-4 Thallium ND ug/L 0.47 0.050 1 10/18/2215:48 10/19/2216:10 7440-28-0 Vanadium ND ug/L 1.0 0.25 1 10/18/2215:48 10/19/2216:10 7440-62-2 Zinc ND ug/L 10.0 2.7 1 10/18/2215:48 10/19/2216:10 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/10/22 20:43 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/10/22 20:43 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/10/22 20:43 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/10/22 20:43 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/10/22 20:43 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/10/22 20:43 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/10/22 20:43 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/10/22 20:43 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/10/22 20:43 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/10/22 20:43 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/10/22 20:43 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/10/22 20:43 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/10/22 20:43 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/10/22 20:43 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/10/22 20:43 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/10/22 20:43 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/10/22 20:43 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/10/22 20:43 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/10/22 20:43 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/10/22 20:43 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/10/22 20:43 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/10/22 20:43 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/10/22 20:43 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/10/22 20:43 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/10/22 20:43 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/10/22 20:43 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/10/22 20:43 78-87-5 Date: 12/27/2022 02:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 17 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: Field Blank -Unit 2 Lab ID: 92630054007 Collected: 10/05/22 17:25 Received: 10/06/22 14:19 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 12/27/2022 02:52 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 95 % 70-130 104 % 70-130 103 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 102 % 70-130 107 % 70-130 0.36 1 10/10/22 20:43 10061-01-5 0.36 1 10/10/22 20:43 10061-02-6 0.30 1 10/10/22 20:43 100-41-4 0.48 1 10/10/22 20:43 591-78-6 9.7 1 10/10/22 20:43 74-88-4 2.0 1 10/10/22 20:43 75-09-2 2.7 1 10/10/22 20:43 108-10-1 0.29 1 10/10/22 20:43 100-42-5 0.31 1 10/10/22 20:43 630-20-6 0.22 1 10/10/22 20:43 79-34-5 0.29 1 10/10/22 20:43 127-18-4 0.48 1 10/10/22 20:43 108-88-3 0.33 1 10/10/22 20:43 71-55-6 0.32 1 10/10/22 20:43 79-00-5 0.38 1 10/10/22 20:43 79-01-6 0.30 1 10/10/22 20:43 75-69-4 0.26 1 10/10/22 20:43 96-18-4 1.3 1 10/10/22 20:43 108-05-4 0.39 1 10/10/22 20:43 75-01-4 0.34 1 10/10/22 20:43 1330-20-7 1 10/10/22 20:43 460-00-4 1 10/10/22 20:43 17060-07-0 1 10/10/22 20:43 2037-26-5 0.86 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/10/22 20:04 123-91-1 10/10/22 20:04 17060-07-0 10/10/22 20:04 2037-26-5 Page 18 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: Trip Blank Lab ID: 92630054008 Collected: 10/05/22 00:00 Received: 10/07/22 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/09/22 00:02 67-64-1 Benzene ND ug/L 1.0 0.34 1 10/09/22 00:02 71-43-2 Bromobenzene ND ug/L 1.0 0.29 1 10/09/22 00:02 108-86-1 Bromochloromethane ND ug/L 1.0 0.47 1 10/09/22 00:02 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/09/22 00:02 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/09/22 00:02 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/09/22 00:02 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/09/22 00:02 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/09/22 00:02 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/09/22 00:02 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/09/22 00:02 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/09/22 00:02 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/09/22 00:02 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.32 1 10/09/22 00:02 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.32 1 10/09/22 00:02 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/09/22 00:02 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/09/22 00:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/09/22 00:02 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/09/22 00:02 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/09/22 00:02 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 10/09/22 00:02 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/09/22 00:02 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 10/09/22 00:02 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/09/22 00:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/09/22 00:02 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/09/22 00:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/09/22 00:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/09/22 00:02 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 10/09/22 00:02 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 10/09/22 00:02 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 10/09/22 00:02 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 10/09/22 00:02 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/09/22 00:02 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/09/22 00:02 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.31 1 10/09/22 00:02 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 10/09/22 00:02 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 10/09/22 00:02 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 10/09/22 00:02 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.41 1 10/09/22 00:02 99-87-6 Methylene Chloride ND ug/L 5.0 2.0 1 10/09/22 00:02 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 10/09/22 00:02 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.42 1 10/09/22 00:02 1634-04-4 Naphthalene ND ug/L 1.0 0.64 1 10/09/22 00:02 91-20-3 Styrene ND ug/L 1.0 0.29 1 10/09/22 00:02 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 10/09/22 00:02 630-20-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 Sample: Trip Blank Lab ID: 92630054008 Collected: 10/05/22 00:00 Received: 10/07/22 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 10/09/22 00:02 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 10/09/22 00:02 127-18-4 Toluene ND ug/L 1.0 0.48 1 10/09/22 00:02 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.81 1 10/09/22 00:02 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 10/09/22 00:02 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 10/09/22 00:02 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 10/09/22 00:02 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 10/09/22 00:02 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 10/09/22 00:02 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 10/09/22 00:02 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 10/09/22 00:02 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 10/09/22 00:02 75-01-4 Xylene (Total) ND ug/L 1.0 0.34 1 10/09/22 00:02 1330-20-7 m&p-Xylene ND ug/L 2.0 0.71 1 10/09/22 00:02 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 10/09/22 00:02 95-47-6 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 1 10/09/22 00:02 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 10/09/22 00:02 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 10/09/22 00:02 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 10/10/22 20:42 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 10/10/22 20:42 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 10/10/22 20:42 2037-26-5 Date: 12/27/2022 02:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 QC Batch: 729379 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006 METHOD BLANK: 3798239 Matrix: Water Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006 Blank Reporting Parameter Units Result Limit MDL Analyzed Antimony ug/L ND 1.0 0.20 10/11/22 20:54 Arsenic ug/L 0.111 1.0 0.087 10/11/22 20:54 Barium ug/L ND 1.0 0.21 10/11/22 20:54 Beryllium ug/L ND 0.10 0.050 10/11/22 20:54 Cadmium ug/L ND 0.20 0.060 10/11/22 20:54 Chromium ug/L ND 1.0 0.50 10/11/22 20:54 Cobalt ug/L ND 1.0 0.050 10/11/22 20:54 Copper ug/L ND 2.0 1.1 10/11/22 20:54 Hardness, Total(SM 2340B) ug/L ND 541 541 10/11/22 20:54 Lead ug/L ND 1.0 0.077 10/11/22 20:54 Nickel ug/L ND 1.0 0.42 10/11/22 20:54 Selenium ug/L ND 2.0 0.072 10/11/22 20:54 Silver ug/L ND 0.40 0.070 10/11/22 20:54 Thallium ug/L ND 0.47 0.050 10/11/22 20:54 Vanadium ug/L ND 1.0 0.25 10/11/22 20:54 Zinc ug/L ND 10.0 2.7 10/11/22 20:54 LABORATORY CONTROL SAMPLE: Parameter 3798240 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 50 50.0 100 80-120 Arsenic ug/L 50 49.7 99 80-120 Barium ug/L 50 49.6 99 80-120 Beryllium ug/L 50 53.4 107 80-120 Cadmium ug/L 50 51.5 103 80-120 Chromium ug/L 50 50.9 102 80-120 Cobalt ug/L 50 52.1 104 80-120 Copper ug/L 50 51.5 103 80-120 Hardness, Total(SM 2340B) ug/L 16500 17400 105 80-120 Lead ug/L 50 51.2 102 80-120 Nickel ug/L 50 51.6 103 80-120 Selenium ug/L 50 49.9 100 80-120 Silver ug/L 25 26.5 106 80-120 Thallium ug/L 25 26.1 104 80-120 Vanadium ug/L 50 52.4 105 80-120 Zinc ug/L 50 51.5 103 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3798241 3798242 MS MSD 92628841001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 50 50 50.1 50.1 100 100 75-125 0 20 Arsenic ug/L 0.30J 50 50 48.3 48.9 96 97 75-125 1 20 Barium ug/L 2.6 50 50 53.3 54.1 101 103 75-125 2 20 Beryllium ug/L ND 50 50 49.8 50.9 100 102 75-125 2 20 Cadmium ug/L ND 50 50 51.0 51.0 102 102 75-125 0 20 Chromium ug/L 1.0 50 50 51.9 52.1 102 102 75-125 0 20 Cobalt ug/L 0.35J 50 50 52.3 52.7 104 105 75-125 1 20 Copper ug/L ND 50 50 51.9 52.5 103 104 75-125 1 20 Hardness, Total(SM 2340B) ug/L 31100 16500 16500 47400 47900 98 101 75-125 1 20 Lead ug/L 0.20J 50 50 51.1 52.0 102 104 75-125 2 20 Nickel ug/L 0.53J 50 50 51.7 52.0 102 103 75-125 1 20 Selenium ug/L ND 50 50 49.0 49.7 98 99 75-125 1 20 Silver ug/L ND 25 25 25.8 25.9 103 104 75-125 1 20 Thallium ug/L ND 25 25 25.7 26.2 103 105 75-125 2 20 Vanadium ug/L 1.9 50 50 53.6 54.3 103 105 75-125 1 20 Zinc ug/L 4.OJ 50 50 53.9 54.4 100 101 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 QC Batch: 730852 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92630054007 METHOD BLANK: 3805255 Associated Lab Samples: 92630054007 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 1.0 0.20 10/19/2216:02 Arsenic ug/L ND 1.0 0.087 10/19/2216:02 Barium ug/L ND 1.0 0.21 10/19/2216:02 Beryllium ug/L ND 0.10 0.050 10/19/2216:02 Cadmium ug/L ND 0.20 0.060 10/19/2216:02 Chromium ug/L ND 1.0 0.50 10/19/2216:02 Cobalt ug/L ND 1.0 0.050 10/19/2216:02 Copper ug/L ND 2.0 1.1 10/19/2216:02 Lead ug/L ND 1.0 0.077 10/19/2216:02 Nickel ug/L ND 1.0 0.42 10/19/2216:02 Selenium ug/L ND 2.0 0.072 10/19/2216:02 Silver ug/L ND 0.40 0.070 10/19/2216:02 Thallium ug/L ND 0.47 0.050 10/19/2216:02 Vanadium ug/L ND 1.0 0.25 10/19/2216:02 Zinc ug/L ND 10.0 2.7 10/19/2216:02 LABORATORY CONTROL SAMPLE: Parameter 3805256 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 50 51.5 103 80-120 Arsenic ug/L 50 51.1 102 80-120 Barium ug/L 50 51.8 104 80-120 Beryllium ug/L 50 52.5 105 80-120 Cadmium ug/L 50 52.2 104 80-120 Chromium ug/L 50 53.4 107 80-120 Cobalt ug/L 50 53.2 106 80-120 Copper ug/L 50 52.2 104 80-120 Lead ug/L 50 51.1 102 80-120 Nickel ug/L 50 52.8 106 80-120 Selenium ug/L 50 50.6 101 80-120 Silver ug/L 25 25.2 101 80-120 Thallium ug/L 25 25.6 103 80-120 Vanadium ug/L 50 51.4 103 80-120 Zinc ug/L 50 52.4 105 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GMI-005 Oxford LF Unit 2 92630054 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3805257 3805258 MS MSD 92630054007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 50 50 52.4 51.8 105 104 75-125 1 20 Arsenic ug/L ND 50 50 50.7 50.6 101 101 75-125 0 20 Barium ug/L ND 50 50 51.9 51.0 104 102 75-125 2 20 Beryllium ug/L ND 50 50 52.7 52.9 105 106 75-125 0 20 Cadmium ug/L ND 50 50 52.3 51.2 105 102 75-125 2 20 Chromium ug/L 0.78J 50 50 53.1 52.8 105 104 75-125 1 20 Cobalt ug/L ND 50 50 52.3 52.6 105 105 75-125 0 20 Copper ug/L ND 50 50 52.4 52.6 103 104 75-125 0 20 Lead ug/L ND 50 50 51.1 51.2 102 102 75-125 0 20 Nickel ug/L ND 50 50 53.4 53.1 107 106 75-125 1 20 Selenium ug/L ND 50 50 50.9 50.9 102 102 75-125 0 20 Silver ug/L ND 25 25 25.2 25.3 101 101 75-125 0 20 Thallium ug/L ND 25 25 25.9 25.6 103 102 75-125 1 20 Vanadium ug/L ND 50 50 53.8 51.0 108 102 75-125 5 20 Zinc ug/L ND 50 50 51.4 51.3 102 102 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 QC Batch: 728945 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92630054008 METHOD BLANK: 3796233 Associated Lab Samples: 92630054008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 10/08/22 16:47 1,1,1-Trichloroethane ug/L ND 1.0 0.33 10/08/22 16:47 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 10/08/22 16:47 1,1,2-Trichloroethane ug/L ND 1.0 0.32 10/08/22 16:47 1,1-Dichloroethane ug/L ND 1.0 0.37 10/08/22 16:47 1,1-Dichloroethene ug/L ND 1.0 0.35 10/08/22 16:47 1,1-Dichloropropene ug/L ND 1.0 0.43 10/08/22 16:47 1,2,3-Trichlorobenzene ug/L ND 1.0 0.81 10/08/22 16:47 1,2,3-Trichloropropane ug/L ND 1.0 0.26 10/08/22 16:47 1,2,4-Trichlorobenzene ug/L ND 1.0 0.64 10/08/22 16:47 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 10/08/22 16:47 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 10/08/22 16:47 1,2-Dichlorobenzene ug/L ND 1.0 0.34 10/08/22 16:47 1,2-Dichloroethane ug/L ND 1.0 0.32 10/08/22 16:47 1,2-Dichloropropane ug/L ND 1.0 0.36 10/08/22 16:47 1,3-Dichlorobenzene ug/L ND 1.0 0.34 10/08/22 16:47 1,3-Dichloropropane ug/L ND 1.0 0.28 10/08/22 16:47 1,4-Dichlorobenzene ug/L ND 1.0 0.33 10/08/22 16:47 2,2-Dichloropropane ug/L ND 1.0 0.39 10/08/22 16:47 2-Butanone (MEK) ug/L ND 5.0 4.0 10/08/22 16:47 2-Chlorotoluene ug/L ND 1.0 0.32 10/08/22 16:47 2-Hexanone ug/L ND 5.0 0.48 10/08/22 16:47 4-Chlorotoluene ug/L ND 1.0 0.32 10/08/22 16:47 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 10/08/22 16:47 Acetone ug/L ND 25.0 5.1 10/08/22 16:47 Benzene ug/L ND 1.0 0.34 10/08/22 16:47 Bromobenzene ug/L ND 1.0 0.29 10/08/22 16:47 Bromochloromethane ug/L ND 1.0 0.47 10/08/22 16:47 Bromodichloromethane ug/L ND 1.0 0.31 10/08/22 16:47 Bromoform ug/L ND 1.0 0.34 10/08/22 16:47 Bromomethane ug/L ND 2.0 1.7 10/08/22 16:47 v2 Carbon tetrachloride ug/L ND 1.0 0.33 10/08/22 16:47 Chlorobenzene ug/L ND 1.0 0.28 10/08/22 16:47 Chloroethane ug/L ND 1.0 0.65 10/08/22 16:47 Chloroform ug/L ND 1.0 0.43 10/08/22 16:47 Chloromethane ug/L ND 1.0 0.54 10/08/22 16:47 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 10/08/22 16:47 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 10/08/22 16:47 Dibromochloromethane ug/L ND 1.0 0.36 10/08/22 16:47 Dibromomethane ug/L ND 1.0 0.39 10/08/22 16:47 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 40 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 METHOD BLANK: 3796233 Associated Lab Samples: 92630054008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.35 10/08/22 16:47 Diisopropyl ether ug/L ND 1.0 0.31 10/08/22 16:47 Ethylbenzene ug/L ND 1.0 0.30 10/08/22 16:47 Hexachloro-1,3-butadiene ug/L ND 2.0 1.5 10/08/22 16:47 m&p-Xylene ug/L ND 2.0 0.71 10/08/22 16:47 Methyl-tert-butyl ether ug/L ND 1.0 0.42 10/08/22 16:47 Methylene Chloride ug/L ND 5.0 2.0 10/08/22 16:47 Naphthalene ug/L ND 1.0 0.64 10/08/22 16:47 o-Xylene ug/L ND 1.0 0.34 10/08/22 16:47 p-Isopropyltoluene ug/L ND 1.0 0.41 10/08/22 16:47 Styrene ug/L ND 1.0 0.29 10/08/22 16:47 Tetrachloroethene ug/L ND 1.0 0.29 10/08/22 16:47 Toluene ug/L ND 1.0 0.48 10/08/22 16:47 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 10/08/22 16:47 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 10/08/22 16:47 Trichloroethene ug/L ND 1.0 0.38 10/08/22 16:47 Trichlorofluoromethane ug/L ND 1.0 0.30 10/08/22 16:47 Vinyl acetate ug/L ND 2.0 1.3 10/08/22 16:47 Vinyl chloride ug/L ND 1.0 0.39 10/08/22 16:47 Xylene (Total) ug/L ND 1.0 0.34 10/08/22 16:47 1,2-Dichloroethane-d4 (S) % 109 70-130 10/08/22 16:47 4-Bromofluorobenzene (S) % 93 70-130 10/08/22 16:47 Toluene-d8 (S) % 100 70-130 10/08/22 16:47 LABORATORY CONTROL SAMPLE: 3796234 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 46.4 93 70-130 1,1,1-Trichloroethane ug/L 50 47.2 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,2-Trichloroethane ug/L 50 46.8 94 70-130 1,1-Dichloroethane ug/L 50 47.5 95 70-130 1,1-Dichloroethene ug/L 50 53.2 106 70-130 1,1-Dichloropropene ug/L 50 50.8 102 70-130 1,2,3-Trichlorobenzene ug/L 50 44.1 88 70-130 1,2,3-Trichloropropane ug/L 50 52.3 105 70-130 1,2,4-Trichlorobenzene ug/L 50 43.7 87 70-130 1,2-Dibromo-3-chloropropane ug/L 50 45.0 90 70-131 1,2-Dibromoethane (EDB) ug/L 50 48.1 96 70-130 1,2-Dichlorobenzene ug/L 50 48.2 96 70-130 1,2-Dichloroethane ug/L 50 48.8 98 70-130 1,2-Dichloropropane ug/L 50 48.7 97 70-130 1,3-Dichlorobenzene ug/L 50 47.4 95 70-130 1,3-Dichloropropane ug/L 50 49.0 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 LABORATORY CONTROL SAMPLE: Parameter 3796234 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 47.6 95 70-130 2,2-Dichloropropane ug/L 50 45.0 90 68-135 2-Butanone (MEK) ug/L 100 112 112 70-134 2-Chlorotoluene ug/L 50 47.9 96 70-130 2-Hexanone ug/L 100 112 112 70-131 4-Chlorotoluene ug/L 50 49.0 98 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 108 108 70-130 Acetone ug/L 100 118 118 70-133 Benzene ug/L 50 43.3 87 70-130 Bromobenzene ug/L 50 46.5 93 70-130 Bromochloromethane ug/L 50 47.8 96 70-130 Bromodichloromethane ug/L 50 45.8 92 70-130 Bromoform ug/L 50 44.4 89 70-130 Bromomethane ug/L 50 39.3 79 45-151 v3 Carbon tetrachloride ug/L 50 41.9 84 70-130 Chlorobenzene ug/L 50 48.4 97 70-130 Chloroethane ug/L 50 50.5 101 39-152 Chloroform ug/L 50 48.1 96 70-130 Chloromethane ug/L 50 56.7 113 58-130 cis-1,2-Dichloroethene ug/L 50 47.4 95 70-130 cis-1,3-Dichloropropene ug/L 50 45.6 91 70-130 Dibromochloromethane ug/L 50 43.8 88 70-130 Dibromomethane ug/L 50 44.8 90 70-130 Dichlorodifluoromethane ug/L 50 58.1 116 54-133 Diisopropyl ether ug/L 50 50.4 101 70-130 Ethylbenzene ug/L 50 48.3 97 70-130 Hexachloro-1,3-butadiene ug/L 50 44.2 88 70-135 m&p-Xylene ug/L 100 96.5 96 70-130 Methyl-tert-butyl ether ug/L 50 48.0 96 70-130 Methylene Chloride ug/L 50 48.4 97 66-130 Naphthalene ug/L 50 46.3 93 70-130 o-Xylene ug/L 50 47.2 94 70-130 p-Isopropyltoluene ug/L 50 48.3 97 70-130 Styrene ug/L 50 47.2 94 70-130 Tetrachloroethene ug/L 50 44.7 89 70-130 Toluene ug/L 50 47.2 94 70-130 trans-1,2-Dichloroethene ug/L 50 50.0 100 70-130 trans- 1,3-Dichloropropene ug/L 50 45.7 91 70-130 Trichloroethene ug/L 50 48.2 96 70-130 Trichlorofluoromethane ug/L 50 48.9 98 62-130 Vinyl acetate ug/L 100 104 104 70-144 Vinyl chloride ug/L 50 59.0 118 62-130 Xylene (Total) ug/L 150 144 96 70-130 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8(S) % 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3796235 MS 92629971006 Spike Parameter Units Result Conc. 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3- chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 3796236 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits ug/L ND 20 20 21.1 21.5 106 108 70-141 ug/L ND 20 20 22.8 22.9 114 115 70-150 ug/L ND 20 20 23.7 22.8 119 114 69-142 ug/L ND 20 20 21.2 22.5 106 112 70-138 ug/L ND 20 20 22.9 23.3 114 116 70-150 ug/L ND 20 20 25.5 25.2 127 126 70-156 ug/L ND 20 20 24.5 24.2 123 121 70-150 ug/L ND 20 20 19.0 20.5 95 102 70-148 ug/L ND 20 20 21.9 22.1 110 111 70-140 ug/L ND 20 20 18.6 19.8 93 99 70-146 ug/L ND 20 20 18.6 20.1 93 100 68-146 Max RPD RPD Qual 2 30 1 30 4 30 6 30 2 30 1 30 1 30 8 30 1 30 6 30 8 30 ug/L ND 20 20 21.4 22.6 107 113 70-138 6 30 ug/L ND 20 20 22.4 22.4 112 112 70-141 0 30 ug/L ND 20 20 22.0 23.0 110 115 69-143 4 30 ug/L ND 20 20 22.5 23.1 113 116 68-156 2 30 ug/L ND 20 20 22.1 22.8 110 114 70-143 3 30 ug/L ND 20 20 21.6 22.6 108 113 70-138 5 30 ug/L ND 20 20 22.1 21.7 110 109 70-142 2 30 ug/L ND 20 20 21.2 21.3 106 106 52-170 0 30 ug/L ND 40 40 46.5 48.3 116 121 60-157 4 30 ug/L ND 20 20 21.6 22.4 108 112 70-147 3 30 ug/L ND 40 40 43.9 46.3 110 116 68-146 5 30 ug/L ND 20 20 22.3 22.6 112 113 70-142 1 30 ug/L ND 40 40 44.8 49.6 112 124 70-141 10 30 ug/L ND 40 40 48.0 50.3 120 126 58-157 5 30 ug/L ND 20 20 21.2 21.2 106 106 70-142 0 30 ug/L ND 20 20 21.6 22.0 108 110 70-143 2 30 ug/L ND 20 20 22.2 22.6 111 113 70-146 2 30 ug/L ND 20 20 20.8 22.5 104 112 70-139 8 30 ug/L ND 20 20 19.9 19.7 100 98 64-140 1 30 ug/L ND 20 20 20.4 20.8 102 104 28-192 2 30 v3 ug/L ND 20 20 21.2 21.3 106 106 70-148 0 30 ug/L ND 20 20 22.3 22.5 112 113 70-141 1 30 ug/L ND 20 20 26.2 26.2 131 131 58-191 0 30 ug/L ND 20 20 23.0 22.8 115 114 70-148 1 30 ug/L ND 20 20 29.3 28.5 146 142 43-162 3 30 ug/L ND 20 20 22.7 23.2 113 115 68-151 2 30 ug/L ND 20 20 20.4 22.0 102 110 70-139 8 30 ug/L ND 20 20 19.1 20.4 95 102 70-144 7 30 ug/L ND 20 20 20.8 22.0 104 110 70-139 5 30 ug/L ND 20 20 27.0 27.0 135 135 39-171 0 30 ug/L ND 20 20 23.5 23.9 117 119 67-142 2 30 ug/L ND 20 20 22.1 22.2 111 111 70-143 0 30 ug/L ND 20 20 20.5 21.0 102 105 64-163 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3796235 3796236 MS MSD 92629971006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 40 40 44.6 44.8 112 112 70-144 0 30 Methyl-tert-butyl ether ug/L ND 20 20 21.5 22.2 107 111 65-143 3 30 Methylene Chloride ug/L ND 20 20 24.3 23.5 121 118 62-149 3 30 Naphthalene ug/L ND 20 20 18.2 19.9 91 100 67-147 9 30 o-Xylene ug/L ND 20 20 22.3 21.4 112 107 70-145 4 30 p-Isopropyltoluene ug/L ND 20 20 22.4 22.6 112 113 70-147 1 30 Styrene ug/L ND 20 20 22.0 21.1 110 106 70-143 4 30 Tetrachloroethene ug/L ND 20 20 21.2 22.3 106 112 70-145 5 30 Toluene ug/L ND 20 20 22.1 23.7 110 118 70-142 7 30 trans-1,2-Dichloroethene ug/L ND 20 20 23.6 24.0 118 120 70-151 2 30 trans-1,3-Dichloropropene ug/L ND 20 20 20.7 22.2 103 111 70-139 7 30 Trichloroethene ug/L ND 20 20 23.0 23.6 115 118 62-146 3 30 Trichlorofluoromethane ug/L ND 20 20 24.1 24.6 121 123 63-153 2 30 Vinyl acetate ug/L ND 40 40 45.6 47.0 114 118 61-162 3 30 Vinyl chloride ug/L ND 20 20 28.6 28.2 143 141 61-163 1 30 Xylene (Total) ug/L ND 60 60 67.0 66.1 112 110 70-143 1 30 1,2-Dichloroethane-d4 (S) % 98 97 70-130 4-Bromofluorobenzene (S) % 103 97 70-130 Toluene-d8 (S) % 100 105 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 QC Batch: 729191 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006, 92630054007 METHOD BLANK: 3797522 Matrix: Water Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006, 92630054007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 10/10/22 19:48 1,1,1-Trichloroethane ug/L ND 1.0 0.33 10/10/22 19:48 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 10/10/22 19:48 1,1,2-Trichloroethane ug/L ND 1.0 0.32 10/10/22 19:48 1,1-Dichloroethane ug/L ND 1.0 0.37 10/10/22 19:48 1,1-Dichloroethene ug/L ND 1.0 0.35 10/10/22 19:48 1,2,3-Trichloropropane ug/L ND 1.0 0.26 10/10/22 19:48 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 10/10/22 19:48 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 10/10/22 19:48 1,2-Dichlorobenzene ug/L ND 1.0 0.34 10/10/22 19:48 1,2-Dichloroethane ug/L ND 1.0 0.32 10/10/22 19:48 1,2-Dichloropropane ug/L ND 1.0 0.36 10/10/22 19:48 1,4-Dichlorobenzene ug/L ND 1.0 0.33 10/10/22 19:48 2-Butanone (MEK) ug/L ND 5.0 4.0 10/10/22 19:48 2-Hexanone ug/L ND 5.0 0.48 10/10/22 19:48 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 10/10/22 19:48 Acetone ug/L ND 25.0 5.1 10/10/22 19:48 Acrylonitrile ug/L ND 10.0 1.8 10/10/22 19:48 Benzene ug/L ND 1.0 0.34 10/10/22 19:48 Bromochloromethane ug/L ND 1.0 0.47 10/10/22 19:48 Bromodichloromethane ug/L ND 1.0 0.31 10/10/22 19:48 Bromoform ug/L ND 1.0 0.34 10/10/22 19:48 Bromomethane ug/L ND 2.0 1.7 10/10/22 19:48 Carbon disulfide ug/L ND 2.0 0.36 10/10/22 19:48 Carbon tetrachloride ug/L ND 1.0 0.33 10/10/22 19:48 Chlorobenzene ug/L ND 1.0 0.28 10/10/22 19:48 Chloroethane ug/L ND 1.0 0.65 10/10/22 19:48 Chloroform ug/L ND 1.0 0.43 10/10/22 19:48 Chloromethane ug/L ND 1.0 0.54 10/10/22 19:48 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 10/10/22 19:48 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 10/10/22 19:48 Dibromochloromethane ug/L ND 1.0 0.36 10/10/22 19:48 Dibromomethane ug/L ND 1.0 0.39 10/10/22 19:48 Ethylbenzene ug/L ND 1.0 0.30 10/10/22 19:48 lodomethane ug/L ND 20.0 9.7 10/10/22 19:48 Methylene Chloride ug/L ND 5.0 2.0 10/10/22 19:48 Styrene ug/L ND 1.0 0.29 10/10/22 19:48 Tetrachloroethene ug/L ND 1.0 0.29 10/10/22 19:48 Toluene ug/L ND 1.0 0.48 10/10/22 19:48 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 10/10/22 19:48 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 METHOD BLANK: 3797522 Matrix: Water Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006, 92630054007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 10/10/22 19:48 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 10/10/22 19:48 Trichloroethene ug/L ND 1.0 0.38 10/10/22 19:48 Trichlorofluoromethane ug/L ND 1.0 0.30 10/10/22 19:48 Vinyl acetate ug/L ND 2.0 1.3 10/10/22 19:48 Vinyl chloride ug/L ND 1.0 0.39 10/10/22 19:48 Xylene (Total) ug/L ND 1.0 0.34 10/10/22 19:48 1,2-Dichloroethane-d4 (S) % 104 70-130 10/10/22 19:48 4-Bromofluorobenzene (S) % 95 70-130 10/10/22 19:48 Toluene-d8 (S) % 106 70-130 10/10/22 19:48 LABORATORY CONTROL SAMPLE: Parameter 3797523 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 48.0 96 70-130 1,1,1-Trichloroethane ug/L 50 45.7 91 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.9 110 70-130 1,1,2-Trichloroethane ug/L 50 46.3 93 70-130 1,1-Dichloroethane ug/L 50 47.7 95 70-130 1,1-Dichloroethene ug/L 50 51.3 103 70-130 1,2,3-Trichloropropane ug/L 50 53.3 107 70-130 1,2-Dibromo-3-chloropropane ug/L 50 42.6 85 70-131 1,2-Dibromoethane (EDB) ug/L 50 47.0 94 70-130 1,2-Dichlorobenzene ug/L 50 45.5 91 70-130 1,2-Dichloroethane ug/L 50 47.2 94 70-130 1,2-Dichloropropane ug/L 50 48.2 96 70-130 1,4-Dichlorobenzene ug/L 50 46.2 92 70-130 2-Butanone (MEK) ug/L 100 107 107 70-134 2-Hexanone ug/L 100 106 106 70-131 4-Methyl-2-pentanone (MIBK) ug/L 100 104 104 70-130 Acetone ug/L 100 111 111 70-133 Acrylonitrile ug/L 250 284 114 70-130 Benzene ug/L 50 44.0 88 70-130 Bromochloromethane ug/L 50 47.7 95 70-130 Bromodichloromethane ug/L 50 45.1 90 70-130 Bromoform ug/L 50 45.9 92 70-130 Bromomethane ug/L 50 36.2 72 45-151 Carbon disulfide ug/L 50 50.9 102 70-130 Carbon tetrachloride ug/L 50 42.3 85 70-130 Chlorobenzene ug/L 50 47.2 94 70-130 Chloroethane ug/L 50 50.1 100 39-152 Chloroform ug/L 50 48.0 96 70-130 Chloromethane ug/L 50 57.3 115 58-130 cis-1,2-Dichloroethene ug/L 50 46.5 93 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 40 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 LABORATORY CONTROL SAMPLE: Parameter 3797523 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 50 45.7 91 70-130 Dibromochloromethane ug/L 50 42.9 86 70-130 Dibromomethane ug/L 50 45.8 92 70-130 Ethylbenzene ug/L 50 49.5 99 70-130 lodomethane ug/L 100 82.5 82 53-141 Methylene Chloride ug/L 50 49.4 99 66-130 Styrene ug/L 50 48.4 97 70-130 Tetrachloroethene ug/L 50 45.2 90 70-130 Toluene ug/L 50 46.3 93 70-130 trans-1,2-Dichloroethene ug/L 50 49.8 100 70-130 trans- 1,3-Dichloropropene ug/L 50 45.7 91 70-130 trans-1,4-Dichloro-2-butene ug/L 50 55.4 111 57-185 Trichloroethene ug/L 50 47.4 95 70-130 Trichlorofluoromethane ug/L 50 48.5 97 62-130 Vinyl acetate ug/L 100 103 103 70-144 Vinyl chloride ug/L 50 58.3 117 62-130 Xylene (Total) ug/L 150 148 99 70-130 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 107 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 3797573 Units 35750833008 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 0.31U 20 19.8 99 70-141 1,1,1-Trichloroethane ug/L 0.331-1 20 21.3 107 70-150 1,1,2,2-Tetrachloroethane ug/L 0.221-1 20 20.4 102 69-142 1,1,2-Trichloroethane ug/L 0.321-1 20 21.2 106 70-138 1,1-Dichloroethane ug/L 0.371-1 20 22.0 108 70-150 1,1-Dichloroethene ug/L 0.351-1 20 24.2 121 70-156 1,2,3-Trichloropropane ug/L 0.261-1 20 19.7 98 70-140 1,2-Dibromo-3-chloropropane ug/L 0.341-1 20 17.8 89 68-146 1,2-Dibromoethane (EDB) ug/L 0.271-1 20 20.1 100 70-138 1,2-Dichlorobenzene ug/L 0.341-1 20 20.8 104 70-141 1,2-Dichloroethane ug/L 0.321-1 20 20.2 101 69-143 1,2-Dichloropropene ug/L 0.361-1 20 20.7 104 68-156 1,4-Dichlorobenzene ug/L 0.331-1 20 21.1 105 70-142 2-Butanone (MEK) ug/L 4.01-1 40 42.0 105 60-157 2-Hexanone ug/L 0.481-1 40 40.5 101 68-146 4-Methyl-2-pentanone (MIBK) ug/L 2.71-1 40 42.8 107 70-141 Acetone ug/L 5.1 U 40 45.5 114 58-157 Acrylonitrile ug/L 1.81-1 100 112 112 69-147 Benzene ug/L 0.38J 20 20.0 98 70-142 Bromochloromethane ug/L 0.471-1 20 21.0 105 70-146 Bromodichloromethane ug/L 0.31 U 20 19.5 97 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 MATRIX SPIKE SAMPLE: Parameter 3797573 Units 35750833008 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromoform ug/L 0.34U 20 17.8 89 64-140 Bromomethane ug/L 1.7U 20 19.3 96 28-192 v3 Carbon disulfide ug/L 0.36U 20 24.8 124 70-151 Carbon tetrachloride ug/L 0.33U 20 20.0 100 70-148 Chlorobenzene ug/L 0.28U 20 20.9 105 70-141 Chloroethane ug/L 0.65U 20 24.0 120 58-191 Chloroform ug/L 0.43U 20 21.1 106 70-148 Chloromethane ug/L 0.54U 20 24.9 124 43-162 cis-1,2-Dichloroethene ug/L 0.38U 20 20.4 102 68-151 cis-1,3-Dichloropropene ug/L 0.36U 20 19.5 97 70-139 Dibromochloromethane ug/L 0.36U 20 18.5 92 70-144 Dibromomethane ug/L 0.39U 20 20.3 102 70-139 Ethylbenzene ug/L 0.30U 20 20.5 102 70-143 lodomethane ug/L 9.7U 40 32.9 82 35-171 Methylene Chloride ug/L 2.OU 20 21.9 109 62-149 Styrene ug/L 0.29U 20 18.9 94 70-143 Tetrachloroethene ug/L 0.29U 20 20.8 104 70-145 Toluene ug/L 0.48U 20 21.4 106 70-142 trans-1,2-Dichloroethene ug/L 0.40U 20 22.9 115 70-151 trans- 1,3-Dichloropropene ug/L 0.36U 20 19.9 100 70-139 trans-1,4-Dichloro-2-butene ug/L 0.56U 20 16.7 83 51-159 Trichloroethene ug/L 0.38U 20 22.0 110 62-146 Trichlorofluoromethane ug/L 0.30U 20 23.1 115 63-153 Vinyl acetate ug/L 1.3U 40 42.1 105 61-162 Vinyl chloride ug/L 4.3 20 30.1 129 61-163 Xylene (Total) ug/L 0.34U 60 60.2 100 70-143 1,2-Dichloroethane-d4 (S) % 94 70-130 4-Bromofluorobenzene (S) % 94 70-130 Toluene-d8 (S) % 103 70-130 SAMPLE DUPLICATE: 3797572 Parameter Units 35750833004 Dup Result Result 1,1,1,2-Tetrachloroethane ug/L 0.31 U 1,1,1-Trichloroethane ug/L 0.331-1 1,1,2,2-Tetrachloroethane ug/L 0.221-1 1,1,2-Trichloroethane ug/L 0.321-1 1,1-Dichloroethane ug/L 0.371-1 1,1-Dichloroethene ug/L 0.351-1 1,2,3-Trichloropropane ug/L 0.261-1 1,2-Dibromo-3-chloropropane ug/L 0.341-1 1,2-Dibromoethane (EDB) ug/L 0.271-1 1,2-Dichlorobenzene ug/L 0.341-1 1,2-Dichloroethane ug/L 0.321-1 1,2-Dichloropropene ug/L 0.361-1 RPD Max RPD ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 SAMPLE DUPLICATE: 3797572 Parameter Units 35750833004 Result Dup Result 1,4-Dichlorobenzene ug/L 0.54J 0.51J 2-Butanone (MEK) ug/L 4.OU ND 2-Hexanone ug/L 0.48U ND 4-Methyl-2-pentanone (MIBK) ug/L 2.7U ND Acetone ug/L 5.1U ND Acrylonitrile ug/L 1.8U ND Benzene ug/L 0.34U ND Bromochloromethane ug/L 0.47U ND Bromodichloromethane ug/L 0.31U ND Bromoform ug/L 0.34U ND Bromomethane ug/L 1.7U ND Carbon disulfide ug/L 0.36U ND Carbon tetrachloride ug/L 0.33U ND Chlorobenzene ug/L 0.28U ND Chloroethane ug/L 0.65U ND Chloroform ug/L 0.43U ND Chloromethane ug/L 0.54U ND cis-1,2-Dichloroethene ug/L 0.38U ND cis-1,3-Dichloropropene ug/L 0.36U ND Dibromochloromethane ug/L 0.36U ND Dibromomethane ug/L 0.39U ND Ethylbenzene ug/L 0.30U ND lodomethane ug/L 9.7U ND Methylene Chloride ug/L 2.OU ND Styrene ug/L 0.29U ND Tetrachloroethene ug/L 0.29U ND Toluene ug/L 0.48U ND trans-1,2-Dichloroethene ug/L 0.40U ND trans- 1,3-Dichloropropene ug/L 0.36U ND trans-1,4-Dichloro-2-butene ug/L 0.56U ND Trichloroethene ug/L 0.38U ND Trichlorofluoromethane ug/L 0.30U ND Vinyl acetate ug/L 1.3U ND Vinyl chloride ug/L 0.39U ND Xylene (Total) ug/L 0.34U ND 1,2-Dichloroethane-d4 (S) % 104 103 4-Bromofluorobenzene (S) % 93 94 Toluene-d8(S) % 108 99 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 v2 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 40 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 QC Batch: 729188 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006, 92630054007, 92630054008 METHOD BLANK: 3797501 Matrix: Water Associated Lab Samples: 92630054001, 92630054002, 92630054003, 92630054004, 92630054005, 92630054006, 92630054007, 92630054008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 10/10/22 14:01 1,2-Dichloroethane-d4 (S) % 106 70-130 10/10/22 14:01 Toluene-d8 (S) % 106 70-130 10/10/22 14:01 LABORATORY CONTROL SAMPLE: 3797502 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 18.1 91 70-130 1,2-Dichloroethane-d4 (S) % 106 70-130 Toluene-d8 (S) % 107 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3797503 3797504 MS MSD 92630055003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 11.0 20 20 27.9 31.6 84 103 63-136 12 30 1,2-Dichloroethane-d4 (S) % 103 98 70-130 30 Toluene-d8 (S) % 100 97 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 40 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALIFIERS Project: GMI-005 Oxford LF Unit 2 Pace Project No.: 92630054 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2022 02:52 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GMI-005 Oxford LF Unit 2 92630054 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92630054001 MW-8 EPA 3010A 729379 EPA 6020B 729465 92630054002 MW-9 EPA 3010A 729379 EPA 6020B 729465 92630054003 MW-10 EPA 3010A 729379 EPA 6020B 729465 92630054004 MW-11 EPA 3010A 729379 EPA 6020B 729465 92630054005 SW-3 EPA 3010A 729379 EPA 6020B 729465 92630054006 SW-4 EPA 3010A 729379 EPA 6020B 729465 92630054007 Field Blank -Unit 2 EPA 3010A 730852 EPA 6020B 731147 92630054001 MW-8 EPA 8260D 729191 92630054002 MW-9 EPA 8260D 729191 92630054003 MW-10 EPA 8260D 729191 92630054004 MW-11 EPA 8260D 729191 92630054005 SW-3 EPA 8260D 729191 92630054006 SW-4 EPA 8260D 729191 92630054007 Field Blank -Unit 2 EPA 8260D 729191 92630054008 Trip Blank EPA 8260D 728945 92630054001 MW-8 EPA 8260D Mod. 729188 92630054002 MW-9 EPA 8260D Mod. 729188 92630054003 MW-10 EPA 8260D Mod. 729188 92630054004 MW-11 EPA 8260D Mod. 729188 92630054005 SW-3 EPA 8260D Mod. 729188 92630054006 SW-4 EPA 8260D Mod. 729188 92630054007 Field Blank -Unit 2 EPA 8260D Mod. 729188 92630054008 Trip Blank EPA 8260D Mod. 729188 Date: 12/27/2022 02:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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Ie���t�euya�E P of 40 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 November 01, 2022 Jeffrey 011ison Hart & Hickman 3921 Sunset Ridge Rd. Ste. 301 Raleigh, NC 27607 RE: Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Dear Jeffrey 011ison: Enclosed are the analytical results for sample(s) received by the laboratory on September 30, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Gulf Coast • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte A revised laboratory report is being submitted on 11/1/22 to report MDLs and applicable J values, per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni for Taylor M Cannon taylor.cannon@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoD ELAP Certification #: 6429-01 Florida Certification #: E87854 Illinois Certification #: 004585 Kansas Certification #: E-10354 Louisiana/LELAP Certification #: 01955 North Carolina Certification #: 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification #: C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Lab ID Sample ID Matrix Date Collected Date Received 92628588001 MW-3RR Water 09/29/2212:10 09/30/22 10:30 92628588002 MW-5R Water 09/29/2215:34 09/30/22 10:30 92628588003 MW-7 Water 09/29/22 12:20 09/30/22 10:30 92628588004 NES-2S Water 09/29/2215:26 09/30/22 10:30 92628588005 SW-1 Water 09/29/2218:45 09/30/22 10:30 92628588006 SW-2 Water 09/29/2218:10 09/30/22 10:30 92628588008 TRIP BLANK Water 09/29/22 00:00 09/30/22 10:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: GM1.004/.005 OXFORD LANDFILL 92628588 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92628588001 MW-3RR EPA 601 OD DEC, RDT 16 PASI-A EPA 6020E CRW 1 PASI-A EPA 7470A NMP 1 PASI-A EPA 8260D LMB 51 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2011 MAB2 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A 92628588002 MW-5R AM20GAX LMB 1 GCLA RSK-175 LMB 1 GCLA EPA 601 OD DEC, RDT 16 PASI-A EPA 6020E CRW 1 PASI-A EPA 7470A NMP 1 PASI-A EPA 8260D LMB 51 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2011 MAB2 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 3 PASI-A 92628588003 MW-7 AM20GAX LMB 1 GCLA RSK-175 LMB 1 GCLA EPA 601 OD DEC, RDT 16 PASI-A EPA 6020E CRW 1 PASI-A EPA 7470A NMP 1 PASI-A EPA 8260D LMB 51 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2011 MAB2 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 3 PASI-A 92628588004 NES-2S AM20GAX LMB 1 GCLA RSK-175 LMB 1 GCLA EPA 601 OD DEC, RDT 14 PASI-A EPA 6020E CRW 1 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 3 PASI-A 92628588005 SW-1 EPA 601 OD DEC, RDT 15 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 6020E CRW 1 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92628588006 SW-2 EPA 601 OD DEC, RDT 15 PASI-A EPA 6020E CRW 1 PASI-A EPA 8260D LMB 50 PASI-C EPA 8260D Mod. LMB 3 PASI-C 92628588008 TRIP BLANK EPA 8260D SAS 51 PASI-C EPA 8260D Mod. LMB 3 PASI-C GCLA = Pace Analytical Gulf Coast PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-3RR Lab ID: 92628588001 Collected: 09/29/22 12:10 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:00 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 19:59 7440-38-2 Barium 43.5 ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:00 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:00 7440-41-7 Cadmium 0.55.1 ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:00 7440-43-9 Chromium ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:00 7440-47-3 Cobalt 9.5 ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:00 7440-48-4 Copper ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:00 7440-50-8 Iron 3210 ug/L 50.0 41.5 1 10/05/22 01:02 10/05/22 22:00 7439-89-6 Lead ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 19:59 7439-92-1 Manganese 3480 ug/L 5.0 3.4 1 10/05/22 01:02 10/05/22 22:00 7439-96-5 Nickel ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:00 7440-02-0 Selenium ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 19:59 7782-49-2 Silver ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:00 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:00 7440-62-2 Zinc ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:00 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 17:37 7440-28-0 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 11/01/2022 12:12 PM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 10/05/2211:57 10/06/2213:46 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 0.51J ug/L 1.0 ND ug/L 1.0 2.1 ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 10/04/22 16:26 67-64-1 1.8 1 10/04/22 16:26 107-13-1 0.34 1 10/04/22 16:26 71-43-2 0.47 1 10/04/22 16:26 74-97-5 0.31 1 10/04/22 16:26 75-27-4 0.34 1 10/04/22 16:26 75-25-2 1.7 1 10/04/22 16:26 74-83-9 4.0 1 10/04/22 16:26 78-93-3 0.36 1 10/04/22 16:26 75-15-0 0.33 1 10/04/22 16:26 56-23-5 0.28 1 10/04/22 16:26 108-90-7 0.65 1 10/04/22 16:26 75-00-3 0.43 1 10/04/22 16:26 67-66-3 0.54 1 10/04/22 16:26 74-87-3 0.34 1 10/04/22 16:26 96-12-8 0.36 1 10/04/22 16:26 124-48-1 0.27 1 10/04/22 16:26 106-93-4 0.39 1 10/04/22 16:26 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v3 v3 v2,v3 Page 6 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-3RR Lab ID: 92628588001 Collected: 09/29/22 12:10 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 11/01/2022 12:12 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 10/04/2216:26 95-50-1 ND ug/L 1.0 0.33 1 10/04/2216:26 106-46-7 ND ug/L 1.0 0.56 1 10/04/2216:26 110-57-6 ND ug/L 1.0 0.37 1 10/04/2216:26 75-34-3 ND ug/L 1.0 0.32 1 10/04/2216:26 107-06-2 ND ug/L 1.0 0.35 1 10/04/2216:26 75-35-4 ND ug/L 1.0 0.38 1 10/04/2216:26 156-59-2 ND ug/L 1.0 0.40 1 10/04/2216:26 156-60-5 ND ug/L 1.0 0.36 1 10/04/2216:26 78-87-5 ND ug/L 1.0 0.36 1 10/04/22 16:26 10061-01-5 ND ug/L 1.0 0.36 1 10/04/2216:26 10061-02-6 ND ug/L 1.0 0.30 1 10/04/2216:26 100-41-4 ND ug/L 5.0 0.48 1 10/04/2216:26 591-78-6 ND ug/L 20.0 9.7 1 10/04/2216:26 74-88-4 ND ug/L 5.0 2.0 1 10/04/2216:26 75-09-2 ND ug/L 5.0 2.7 1 10/04/2216:26 108-10-1 ND ug/L 1.0 0.29 1 10/04/2216:26 100-42-5 ND ug/L 1.0 0.31 1 10/04/2216:26 630-20-6 ND ug/L 1.0 0.22 1 10/04/2216:26 79-34-5 ND ug/L 1.0 0.29 1 10/04/2216:26 127-18-4 ND ug/L 10.0 3.5 1 10/04/2216:26 109-99-9 ND ug/L 1.0 0.48 1 10/04/2216:26 108-88-3 ND ug/L 1.0 0.33 1 10/04/2216:26 71-55-6 ND ug/L 1.0 0.32 1 10/04/2216:26 79-00-5 ND ug/L 1.0 0.38 1 10/04/2216:26 79-01-6 ND ug/L 1.0 0.30 1 10/04/2216:26 75-69-4 ND ug/L 1.0 0.26 1 10/04/2216:26 96-18-4 ND ug/L 2.0 1.3 1 10/04/2216:26 108-05-4 ND ug/L 1.0 0.39 1 10/04/2216:26 75-01-4 ND ug/L 1.0 0.34 1 10/04/2216:26 1330-20-7 98 % 70-130 1 10/04/2216:26 460-00-4 97 % 70-130 1 10/04/2216:26 17060-07-0 101 % 70-130 1 10/04/2216:26 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 70.2 ug/L 2.0 0.86 1 10/01/2219:15 123-91-1 100 % 70-130 1 10/01 /22 19:15 17060-07-0 92 % 70-130 1 10/01 /22 19:15 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 205 mg/L 5.0 5.0 1 10/01 /22 19:14 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-3RR Parameters Lab ID: 92628588001 Collected: Report Results Units Limit 09/29/22 12:10 MDL DF Received: 09/30/22 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 399 mg/L 25.0 25.0 1 10/01/22 11:16 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 41.7 mg/L 1.0 0.60 1 09/30/2217:50 16887-00-6 Sulfate 42.4 mg/L 1.0 0.50 1 09/30/2217:50 14808-79-8 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-5R Lab ID: 92628588002 Collected: 09/29/22 15:34 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX Pace Analytical Gulf Coast Hydrogen 1.0J nM 1.9 0.49 1 10/05/2210:02 1333-74-0 Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane 63 ug/L 5.0 2.0 1 10/05/22 08:04 74-82-8 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:14 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:30 7440-38-2 Barium 56.0 ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:14 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:14 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:14 7440-43-9 Chromium ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:14 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:14 7440-48-4 Copper ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:14 7440-50-8 Iron 116 ug/L 50.0 41.5 1 10/05/22 01:02 10/05/22 22:14 7439-89-6 Lead ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 20:30 7439-92-1 Manganese 335 ug/L 5.0 3.4 1 10/05/22 01:02 10/05/22 22:14 7439-96-5 Nickel ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:14 7440-02-0 Selenium ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:30 7782-49-2 Silver ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:14 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:14 7440-62-2 Zinc ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:14 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 18:04 7440-28-0 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 10/05/2211:57 10/06/2213:48 7439-97-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/04/22 16:44 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/04/22 16:44 107-13-1 Benzene 0.35J ug/L 1.0 0.34 1 10/04/22 16:44 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/04/22 16:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/04/22 16:44 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/04/22 16:44 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/04/22 16:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/04/22 16:44 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/04/22 16:44 75-15-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-5R Lab ID: 92628588002 Collected: 09/29/22 15:34 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Carbon tetrachloride ND ug/L 1.0 0.33 1 10/04/22 16:44 56-23-5 Chlorobenzene 1.9 ug/L 1.0 0.28 1 10/04/22 16:44 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/04/22 16:44 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/04/22 16:44 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/04/22 16:44 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/04/22 16:44 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/04/22 16:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/04/22 16:44 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/04/22 16:44 74-95-3 1,2-Dichlorobenzene 1.4 ug/L 1.0 0.34 1 10/04/22 16:44 95-50-1 1,4-Dichlorobenzene 0.96J ug/L 1.0 0.33 1 10/04/22 16:44 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/04/22 16:44 110-57-6 1,1-Dichloroethane 1.1 ug/L 1.0 0.37 1 10/04/22 16:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/04/22 16:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/04/22 16:44 75-35-4 cis-1,2-Dichloroethene 1.9 ug/L 1.0 0.38 1 10/04/22 16:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/04/22 16:44 156-60-5 1,2-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 16:44 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 16:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 16:44 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 10/04/22 16:44 100-41-4 2-Hexanone ND ug/L 5.0 0.48 1 10/04/22 16:44 591-78-6 lodomethane ND ug/L 20.0 9.7 1 10/04/22 16:44 74-88-4 Methylene Chloride ND ug/L 5.0 2.0 1 10/04/22 16:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 10/04/22 16:44 108-10-1 Styrene ND ug/L 1.0 0.29 1 10/04/22 16:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 10/04/22 16:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 10/04/22 16:44 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 10/04/22 16:44 127-18-4 Tetrahydrofuran ND ug/L 10.0 3.5 1 10/04/22 16:44 109-99-9 Toluene ND ug/L 1.0 0.48 1 10/04/22 16:44 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 10/04/22 16:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 10/04/22 16:44 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 10/04/22 16:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 10/04/22 16:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 10/04/22 16:44 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 10/04/22 16:44 108-05-4 Vinyl chloride 0.591 ug/L 1.0 0.39 1 10/04/22 16:44 75-01-4 Xylene (Total) ND ug/L 1.0 0.34 1 10/04/22 16:44 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 10/04/22 16:44 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 10/04/22 16:44 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 10/04/22 16:44 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-5R Lab ID: 92628588002 Collected: 09/29/22 15:34 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 65.1 ug/L 2.0 0.86 1 10/01/22 19:34 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 10/01/22 19:34 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 10/01/22 19:34 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 182 mg/L 5.0 5.0 1 10/01/22 16:03 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 326 mg/L 25.0 25.0 1 10/01/22 11:16 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 52.3 mg/L 1.0 0.60 1 09/30/2219:09 16887-00-6 Nitrate as N ND mg/L 0.10 0.060 1 09/30/22 19:09 14797-55-8 Sulfate 8.5 mg/L 1.0 0.50 1 09/30/2219:09 14808-79-8 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-7 Lab ID: 92628588003 Collected: 09/29/22 12:20 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX Pace Analytical Gulf Coast Hydrogen 9.2 nM 1.9 0.49 1 10/05/2210:14 1333-74-0 Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane ND ug/L 5.0 2.0 1 10/05/22 08:15 74-82-8 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:18 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:34 7440-38-2 Barium 4.3J ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:18 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:18 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:18 7440-43-9 Chromium ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:18 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:18 7440-48-4 Copper ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:18 7440-50-8 Iron 472 ug/L 50.0 41.5 1 10/05/22 01:02 10/05/22 22:18 7439-89-6 Lead ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 20:34 7439-92-1 Manganese 20.9 ug/L 5.0 3.4 1 10/05/22 01:02 10/05/22 22:18 7439-96-5 Nickel ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:18 7440-02-0 Selenium ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:34 7782-49-2 Silver ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:18 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:18 7440-62-2 Zinc ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:18 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 18:08 7440-28-0 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 10/05/2211:57 10/06/2213:50 7439-97-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/04/22 17:02 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/04/22 17:02 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/04/22 17:02 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/04/22 17:02 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/04/22 17:02 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/04/22 17:02 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/04/22 17:02 74-83-9 2-Butanone (MEK) 5.1 ug/L 5.0 4.0 1 10/04/22 17:02 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/04/22 17:02 75-15-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-7 Lab ID: 92628588003 Collected: 09/29/22 12:20 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Carbon tetrachloride ND ug/L 1.0 0.33 1 10/04/22 17:02 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/04/22 17:02 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/04/22 17:02 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/04/22 17:02 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/04/22 17:02 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/04/22 17:02 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/04/22 17:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/04/22 17:02 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/04/22 17:02 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/04/22 17:02 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/04/22 17:02 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/04/22 17:02 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/04/22 17:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:02 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/04/22 17:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/04/22 17:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/04/22 17:02 156-60-5 1,2-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:02 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:02 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:02 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 10/04/22 17:02 100-41-4 2-Hexanone ND ug/L 5.0 0.48 1 10/04/22 17:02 591-78-6 lodomethane ND ug/L 20.0 9.7 1 10/04/22 17:02 74-88-4 Methylene Chloride ND ug/L 5.0 2.0 1 10/04/22 17:02 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 10/04/22 17:02 108-10-1 Styrene ND ug/L 1.0 0.29 1 10/04/22 17:02 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 10/04/22 17:02 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 10/04/22 17:02 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 10/04/22 17:02 127-18-4 Tetrahydrofuran ND ug/L 10.0 3.5 1 10/04/22 17:02 109-99-9 Toluene ND ug/L 1.0 0.48 1 10/04/22 17:02 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 10/04/22 17:02 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:02 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 10/04/22 17:02 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 10/04/22 17:02 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 10/04/22 17:02 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 10/04/22 17:02 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 10/04/22 17:02 75-01-4 Xylene (Total) ND ug/L 1.0 0.34 1 10/04/22 17:02 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 10/04/22 17:02 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 10/04/22 17:02 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 10/04/22 17:02 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: MW-7 Lab ID: 92628588003 Collected: 09/29/22 12:20 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 1.7J ug/L 2.0 0.86 1 10/01/22 19:53 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 10/01/22 19:53 17060-07-0 Toluene-d8 (S) 113 % 70-130 1 10/01/22 19:53 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 144 mg/L 5.0 5.0 1 10/01/22 16:29 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 246 mg/L 25.0 25.0 1 10/01/22 11:16 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 7.6 mg/L 1.0 0.60 1 09/30/2218:37 16887-00-6 Nitrate as N 0.24 mg/L 0.10 0.060 1 09/30/22 18:37 14797-55-8 Sulfate 41.2 mg/L 1.0 0.50 1 09/30/2218:37 14808-79-8 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: NES-2S Lab ID: 92628588004 Collected: 09/29/22 15:26 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX Pace Analytical Gulf Coast Hydrogen 0.78J nM 1.9 0.49 1 10/05/2210:26 1333-74-0 Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane 74 ug/L 5.0 2.0 1 10/05/22 08:27 74-82-8 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:21 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:37 7440-38-2 Barium 33.7 ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:21 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:21 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:21 7440-43-9 Chromium ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:21 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:21 7440-48-4 Copper ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:21 7440-50-8 Lead ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 20:37 7439-92-1 Nickel ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:21 7440-02-0 Selenium ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:37 7782-49-2 Silver ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:21 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:21 7440-62-2 Zinc ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:21 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 18:12 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/04/22 17:21 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/04/22 17:21 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/04/22 17:21 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/04/22 17:21 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/04/22 17:21 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/04/22 17:21 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/04/22 17:21 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/04/22 17:21 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/04/22 17:21 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/04/22 17:21 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/04/22 17:21 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/04/22 17:21 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/04/22 17:21 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/04/22 17:21 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/04/22 17:21 96-12-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: NES-2S Lab ID: 92628588004 Collected: 09/29/22 15:26 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Dibromochloromethane ND ug/L 1.0 0.36 1 10/04/22 17:21 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/04/22 17:21 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/04/22 17:21 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/04/22 17:21 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/04/22 17:21 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/04/22 17:21 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/04/22 17:21 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:21 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 10/04/22 17:21 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 10/04/22 17:21 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 10/04/22 17:21 156-60-5 1,2-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:21 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:21 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 10/04/22 17:21 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 10/04/22 17:21 100-41-4 2-Hexanone ND ug/L 5.0 0.48 1 10/04/22 17:21 591-78-6 lodomethane ND ug/L 20.0 9.7 1 10/04/22 17:21 74-88-4 Methylene Chloride ND ug/L 5.0 2.0 1 10/04/22 17:21 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 10/04/22 17:21 108-10-1 Styrene ND ug/L 1.0 0.29 1 10/04/22 17:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 10/04/22 17:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 10/04/22 17:21 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 10/04/22 17:21 127-18-4 Toluene ND ug/L 1.0 0.48 1 10/04/22 17:21 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 10/04/22 17:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:21 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 10/04/22 17:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 10/04/22 17:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 10/04/22 17:21 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 10/04/22 17:21 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 10/04/22 17:21 75-01-4 Xylene (Total) ND ug/L 1.0 0.34 1 10/04/22 17:21 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 10/04/22 17:21 460-00-4 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 10/04/22 17:21 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 10/04/22 17:21 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 10/01/22 20:12 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 10/01/22 20:12 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 10/01/22 20:12 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: NES-2S Lab ID: 92628588004 Collected: 09/29/22 15:26 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 77.4 mg/L 5.0 5.0 1 10/01/22 16:40 300.0 IC anions 48hr Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 10.4 mg/L 1.0 0.60 1 09/30/2218:53 16887-00-6 Nitrate as N 0.20 mg/L 0.10 0.060 1 09/30/22 18:53 14797-55-8 Sulfate 30.1 mg/L 1.0 0.50 1 09/30/2218:53 14808-79-8 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: SW-1 Lab ID: 92628588005 Collected: 09/29/22 18:45 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Hardness, Total(SM 2340B) Vanadium Zinc Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:25 7440-36-0 ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:48 7440-38-2 23.5 ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:25 7440-39-3 ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:25 7440-41-7 ND ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:25 7440-43-9 ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:25 7440-47-3 ND ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:25 7440-48-4 ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:25 7440-50-8 ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 20:48 7439-92-1 ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:25 7440-02-0 ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:48 7782-49-2 ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:25 7440-22-4 32700 ug/L 662 131 1 10/05/22 01:02 10/05/22 22:25 ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:25 7440-62-2 ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:25 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 18:16 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/04/22 17:39 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/04/22 17:39 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/04/22 17:39 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/04/22 17:39 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/04/22 17:39 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/04/22 17:39 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/04/22 17:39 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/04/22 17:39 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/04/22 17:39 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/04/22 17:39 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/04/22 17:39 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/04/22 17:39 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/04/22 17:39 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/04/22 17:39 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/04/22 17:39 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/04/22 17:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/04/22 17:39 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/04/22 17:39 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/04/22 17:39 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/04/22 17:39 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/04/22 17:39 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/04/22 17:39 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:39 107-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. v2 Page 18 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: SW-1 Lab ID: 92628588005 Collected: 09/29/22 18:45 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 11/01/2022 12:12 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.35 1 10/04/2217:39 75-35-4 ND ug/L 1.0 0.38 1 10/04/2217:39 156-59-2 ND ug/L 1.0 0.40 1 10/04/2217:39 156-60-5 ND ug/L 1.0 0.36 1 10/04/2217:39 78-87-5 ND ug/L 1.0 0.36 1 10/04/22 17:39 10061-01-5 ND ug/L 1.0 0.36 1 10/04/2217:39 10061-02-6 ND ug/L 1.0 0.30 1 10/04/2217:39 100-41-4 ND ug/L 5.0 0.48 1 10/04/2217:39 591-78-6 ND ug/L 20.0 9.7 1 10/04/2217:39 74-88-4 ND ug/L 5.0 2.0 1 10/04/2217:39 75-09-2 ND ug/L 5.0 2.7 1 10/04/2217:39 108-10-1 ND ug/L 1.0 0.29 1 10/04/2217:39 100-42-5 ND ug/L 1.0 0.31 1 10/04/2217:39 630-20-6 ND ug/L 1.0 0.22 1 10/04/2217:39 79-34-5 ND ug/L 1.0 0.29 1 10/04/2217:39 127-18-4 ND ug/L 1.0 0.48 1 10/04/2217:39 108-88-3 ND ug/L 1.0 0.33 1 10/04/2217:39 71-55-6 ND ug/L 1.0 0.32 1 10/04/2217:39 79-00-5 ND ug/L 1.0 0.38 1 10/04/2217:39 79-01-6 ND ug/L 1.0 0.30 1 10/04/2217:39 75-69-4 ND ug/L 1.0 0.26 1 10/04/2217:39 96-18-4 ND ug/L 2.0 1.3 1 10/04/2217:39 108-05-4 ND ug/L 1.0 0.39 1 10/04/2217:39 75-01-4 ND ug/L 1.0 0.34 1 10/04/2217:39 1330-20-7 97 % 70-130 1 10/04/2217:39 460-00-4 101 % 70-130 1 10/04/2217:39 17060-07-0 101 % 70-130 1 10/04/2217:39 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 10/01/22 20:31 123-91-1 102 % 70-130 1 10/01 /22 20:31 17060-07-0 104 % 70-130 1 10/01 /22 20:31 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: SW-2 Lab ID: 92628588006 Collected: 09/29/22 18:10 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Hardness, Total(SM 2340B) Vanadium Zinc Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 5.0 3.0 1 10/05/22 01:02 10/05/22 22:28 7440-36-0 ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:51 7440-38-2 25.3 ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:28 7440-39-3 ND ug/L 1.0 0.70 1 10/05/22 01:02 10/05/22 22:28 7440-41-7 ND ug/L 1.0 0.40 1 10/05/22 01:02 10/05/22 22:28 7440-43-9 ND ug/L 5.0 3.7 1 10/05/22 01:02 10/05/22 22:28 7440-47-3 ND ug/L 5.0 3.6 1 10/05/22 01:02 10/05/22 22:28 7440-48-4 ND ug/L 5.0 4.3 1 10/05/22 01:02 10/05/22 22:28 7440-50-8 ND ug/L 5.0 4.5 1 10/05/22 01:02 10/10/22 20:51 7439-92-1 ND ug/L 5.0 3.5 1 10/05/22 01:02 10/05/22 22:28 7440-02-0 ND ug/L 10.0 4.7 1 10/05/22 01:02 10/10/22 20:51 7782-49-2 ND ug/L 5.0 2.5 1 10/05/22 01:02 10/05/22 22:28 7440-22-4 62300 ug/L 662 131 1 10/05/22 01:02 10/05/22 22:28 ND ug/L 5.0 3.9 1 10/05/22 01:02 10/05/22 22:28 7440-62-2 ND ug/L 10.0 9.5 1 10/05/22 01:02 10/05/22 22:28 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.47 0.050 1 10/05/22 09:53 10/10/22 18:20 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 10/04/22 17:58 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 10/04/22 17:58 107-13-1 Benzene ND ug/L 1.0 0.34 1 10/04/22 17:58 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 10/04/22 17:58 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 10/04/22 17:58 75-27-4 Bromoform ND ug/L 1.0 0.34 1 10/04/22 17:58 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 10/04/22 17:58 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 10/04/22 17:58 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 10/04/22 17:58 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 10/04/22 17:58 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 10/04/22 17:58 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 10/04/22 17:58 75-00-3 Chloroform ND ug/L 1.0 0.43 1 10/04/22 17:58 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 10/04/22 17:58 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 10/04/22 17:58 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 10/04/22 17:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 10/04/22 17:58 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 10/04/22 17:58 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 10/04/22 17:58 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 10/04/22 17:58 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 10/04/22 17:58 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 10/04/22 17:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 10/04/22 17:58 107-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. v2 Page 20 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: SW-2 Lab ID: 92628588006 Collected: 09/29/22 18:10 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 11/01/2022 12:12 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.35 1 10/04/2217:58 75-35-4 ND ug/L 1.0 0.38 1 10/04/2217:58 156-59-2 ND ug/L 1.0 0.40 1 10/04/2217:58 156-60-5 ND ug/L 1.0 0.36 1 10/04/2217:58 78-87-5 ND ug/L 1.0 0.36 1 10/04/22 17:58 10061-01-5 ND ug/L 1.0 0.36 1 10/04/2217:58 10061-02-6 ND ug/L 1.0 0.30 1 10/04/2217:58 100-41-4 ND ug/L 5.0 0.48 1 10/04/2217:58 591-78-6 ND ug/L 20.0 9.7 1 10/04/2217:58 74-88-4 ND ug/L 5.0 2.0 1 10/04/2217:58 75-09-2 ND ug/L 5.0 2.7 1 10/04/2217:58 108-10-1 ND ug/L 1.0 0.29 1 10/04/2217:58 100-42-5 ND ug/L 1.0 0.31 1 10/04/2217:58 630-20-6 ND ug/L 1.0 0.22 1 10/04/2217:58 79-34-5 ND ug/L 1.0 0.29 1 10/04/2217:58 127-18-4 ND ug/L 1.0 0.48 1 10/04/2217:58 108-88-3 ND ug/L 1.0 0.33 1 10/04/2217:58 71-55-6 ND ug/L 1.0 0.32 1 10/04/2217:58 79-00-5 ND ug/L 1.0 0.38 1 10/04/2217:58 79-01-6 ND ug/L 1.0 0.30 1 10/04/2217:58 75-69-4 ND ug/L 1.0 0.26 1 10/04/2217:58 96-18-4 ND ug/L 2.0 1.3 1 10/04/2217:58 108-05-4 ND ug/L 1.0 0.39 1 10/04/2217:58 75-01-4 ND ug/L 1.0 0.34 1 10/04/2217:58 1330-20-7 96 % 70-130 1 10/04/2217:58 460-00-4 100 % 70-130 1 10/04/2217:58 17060-07-0 103 % 70-130 1 10/04/2217:58 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 10/01/22 20:50 123-91-1 101 % 70-130 1 10/01 /22 20:50 17060-07-0 106 % 70-130 1 10/01 /22 20:50 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: TRIP BLANK Lab ID: 92628588008 Collected: 09/29/22 00:00 Received: 09/30/22 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Date: 11/01/2022 12:12 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 10/02/2219:23 67-64-1 ND ug/L 10.0 1.8 1 10/02/2219:23 107-13-1 ND ug/L 1.0 0.34 1 10/02/2219:23 71-43-2 ND ug/L 1.0 0.47 1 10/02/2219:23 74-97-5 ND ug/L 1.0 0.31 1 10/02/2219:23 75-27-4 ND ug/L 1.0 0.34 1 10/02/2219:23 75-25-2 ND ug/L 2.0 1.7 1 10/02/2219:23 74-83-9 ND ug/L 5.0 4.0 1 10/02/2219:23 78-93-3 ND ug/L 2.0 0.36 1 10/02/2219:23 75-15-0 ND ug/L 1.0 0.33 1 10/02/2219:23 56-23-5 ND ug/L 1.0 0.28 1 10/02/2219:23 108-90-7 ND ug/L 1.0 0.65 1 10/02/2219:23 75-00-3 ND ug/L 1.0 0.43 1 10/02/2219:23 67-66-3 ND ug/L 1.0 0.54 1 10/02/2219:23 74-87-3 ND ug/L 2.0 0.34 1 10/02/2219:23 96-12-8 ND ug/L 1.0 0.36 1 10/02/2219:23 124-48-1 ND ug/L 1.0 0.27 1 10/02/2219:23 106-93-4 ND ug/L 1.0 0.39 1 10/02/2219:23 74-95-3 ND ug/L 1.0 0.34 1 10/02/2219:23 95-50-1 ND ug/L 1.0 0.33 1 10/02/2219:23 106-46-7 ND ug/L 1.0 0.56 1 10/02/2219:23 110-57-6 ND ug/L 1.0 0.37 1 10/02/2219:23 75-34-3 ND ug/L 1.0 0.32 1 10/02/2219:23 107-06-2 ND ug/L 1.0 0.35 1 10/02/2219:23 75-35-4 ND ug/L 1.0 0.38 1 10/02/2219:23 156-59-2 ND ug/L 1.0 0.40 1 10/02/2219:23 156-60-5 ND ug/L 1.0 0.36 1 10/02/2219:23 78-87-5 ND ug/L 1.0 0.36 1 10/02/22 19:23 10061-01-5 ND ug/L 1.0 0.36 1 10/02/2219:23 10061-02-6 ND ug/L 1.0 0.30 1 10/02/2219:23 100-41-4 ND ug/L 5.0 0.48 1 10/02/2219:23 591-78-6 ND ug/L 20.0 9.7 1 10/02/2219:23 74-88-4 ND ug/L 5.0 2.0 1 10/02/2219:23 75-09-2 ND ug/L 5.0 2.7 1 10/02/2219:23 108-10-1 ND ug/L 1.0 0.29 1 10/02/2219:23 100-42-5 ND ug/L 1.0 0.31 1 10/02/2219:23 630-20-6 ND ug/L 1.0 0.22 1 10/02/2219:23 79-34-5 ND ug/L 1.0 0.29 1 10/02/2219:23 127-18-4 ND ug/L 10.0 3.5 1 10/02/2219:23 109-99-9 ND ug/L 1.0 0.48 1 10/02/2219:23 108-88-3 ND ug/L 1.0 0.33 1 10/02/2219:23 71-55-6 ND ug/L 1.0 0.32 1 10/02/2219:23 79-00-5 ND ug/L 1.0 0.38 1 10/02/2219:23 79-01-6 ND ug/L 1.0 0.30 1 10/02/2219:23 75-69-4 ND ug/L 1.0 0.26 1 10/02/2219:23 96-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IN Page 22 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Sample: TRIP BLANK Parameters Lab ID: 92628588008 Collected: Report Results Units Limit 09/29/22 00:00 MDL DF Received: 09/30/22 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Vinyl acetate ND ug/L 2.0 1.3 1 10/02/22 19:23 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 10/02/22 19:23 75-01-4 Xylene (Total) ND ug/L 1.0 0.34 1 10/02/22 19:23 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 10/02/22 19:23 460-00-4 1,2-Dichloroethane-d4 (S) 114 % 70-130 1 10/02/22 19:23 17060-07-0 Toluene-d8 (S) 110 % 70-130 1 10/02/22 19:23 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 10/01/22 15:05 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 10/01/22 15:05 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 10/01/22 15:05 2037-26-5 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 751115 Analysis Method: AM20GAX QC Batch Method: AM20GAX Analysis Description: Indicator Gases Bubble Strip H2 Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92628588002, 92628588003, 92628588004 METHOD BLANK: 2403342 Matrix: Air Associated Lab Samples: 92628588002, 92628588003, 92628588004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Hydrogen nM ND 1.9 0.49 10/05/22 06:35 LABORATORY CONTROL SAMPLE & LCSD: 2403343 2403344 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Hydrogen nM 12 12 11 98 95 70-130 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 751162 Analysis Method: RSK-175 QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92628588002, 92628588003, 92628588004 METHOD BLANK: 2403704 Matrix: Water Associated Lab Samples: 92628588002, 92628588003, 92628588004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Methane ug/L ND 5.0 2.0 10/05/22 06:10 LABORATORY CONTROL SAMPLE & LCSD: 2403705 2403706 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Methane ug/L 380 330 330 87 87 70-130 0 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727674 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003 METHOD BLANK: 3789251 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 10/06/2213:00 LABORATORY CONTROL SAMPLE: 3789252 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.5 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3789253 3789254 MS MSD 92628412001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.1 2.2 84 87 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727880 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 METHOD BLANK: 3790578 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.0 10/05/22 21:46 Arsenic ug/L ND 10.0 4.7 10/10/2219:52 Barium ug/L ND 5.0 3.5 10/05/22 21:46 Beryllium ug/L ND 1.0 0.70 10/05/22 21:46 Cadmium ug/L ND 1.0 0.40 10/05/22 21:46 Chromium ug/L ND 5.0 3.7 10/10/2219:52 Cobalt ug/L ND 5.0 3.6 10/05/22 21:46 Copper ug/L ND 5.0 4.3 10/05/22 21:46 Hardness, Total(SM 2340B) ug/L ND 662 131 10/05/22 21:46 Iron ug/L ND 50.0 41.5 10/05/22 21:46 Lead ug/L ND 5.0 4.5 10/10/2219:52 Manganese ug/L ND 5.0 3.4 10/05/22 21:46 Nickel ug/L ND 5.0 3.5 10/05/22 21:46 Selenium ug/L ND 10.0 4.7 10/10/2219:52 Silver ug/L ND 5.0 2.5 10/05/22 21:46 Vanadium ug/L ND 5.0 3.9 10/05/22 21:46 Zinc ug/L ND 10.0 9.5 10/05/22 21:46 LABORATORY CONTROL SAMPLE: 3790579 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 496 99 80-120 Arsenic ug/L 500 476 95 80-120 Barium ug/L 500 487 97 80-120 Beryllium ug/L 500 490 98 80-120 Cadmium ug/L 500 494 99 80-120 Chromium ug/L 500 495 99 80-120 Cobalt ug/L 500 505 101 80-120 Copper ug/L 500 523 105 80-120 Hardness, Total(SM 2340B) ug/L 33100 32900 99 80-120 Iron ug/L 5000 4920 98 80-120 Lead ug/L 500 494 99 80-120 Manganese ug/L 500 514 103 80-120 Nickel ug/L 500 502 100 80-120 Selenium ug/L 500 483 97 80-120 Silver ug/L 250 234 93 80-120 Vanadium ug/L 500 536 107 80-120 Zinc ug/L 500 502 100 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 MATRIX SPIKE & MATRIX SPIKE Parameter DUPLICATE: 3790580 MS 92628588001 Spike Units Result Conc. MSD Spike Conc. 3790581 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Antimony ug/L ND 500 500 514 506 103 101 75-125 1 20 Arsenic ug/L ND 500 500 498 491 99 97 75-125 2 20 Barium ug/L 43.5 500 500 546 532 100 98 75-125 3 20 Beryllium ug/L ND 500 500 509 498 102 100 75-125 2 20 Cadmium ug/L 0.55J 500 500 520 514 104 103 75-125 1 20 Chromium ug/L ND 500 500 520 502 104 100 75-125 3 20 Cobalt ug/L 9.5 500 500 518 512 102 100 75-125 1 20 Copper ug/L ND 500 500 534 517 107 103 75-125 3 20 Hardness, Total(SM 2340B) ug/L 95000 33100 33100 131000 127000 110 97 75-125 3 20 Iron ug/L 3210 5000 5000 8340 8170 102 99 75-125 2 20 Lead ug/L ND 500 500 487 481 97 96 75-125 1 20 Manganese ug/L 3480 500 500 4090 3980 121 100 75-125 3 20 Nickel ug/L ND 500 500 510 505 101 100 75-125 1 20 Selenium ug/L ND 500 500 518 510 103 102 75-125 2 20 Silver ug/L ND 250 250 241 237 96 95 75-125 2 20 Vanadium ug/L ND 500 500 553 537 110 107 75-125 3 20 Zinc ug/L ND 500 500 522 514 103 101 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727920 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 METHOD BLANK: 3790630 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.47 0.050 10/10/2217:29 LABORATORY CONTROL SAMPLE: 3790631 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 25 25.6 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3790632 3790633 MS MSD 92628588001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 25 25 25.7 26.0 103 104 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727360 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92628588008 METHOD BLANK: 3787851 Associated Lab Samples: 92628588008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 10/02/22 18:47 1,1,1-Trichloroethane ug/L ND 1.0 0.33 10/02/22 18:47 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 10/02/22 18:47 1,1,2-Trichloroethane ug/L ND 1.0 0.32 10/02/22 18:47 1,1-Dichloroethane ug/L ND 1.0 0.37 10/02/22 18:47 1,1-Dichloroethene ug/L ND 1.0 0.35 10/02/22 18:47 1,2,3-Trichloropropane ug/L ND 1.0 0.26 10/02/22 18:47 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 10/02/22 18:47 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 10/02/22 18:47 1,2-Dichlorobenzene ug/L ND 1.0 0.34 10/02/22 18:47 1,2-Dichloroethane ug/L ND 1.0 0.32 10/02/22 18:47 1,2-Dichloropropane ug/L ND 1.0 0.36 10/02/22 18:47 1,4-Dichlorobenzene ug/L ND 1.0 0.33 10/02/22 18:47 2-Butanone (MEK) ug/L ND 5.0 4.0 10/02/22 18:47 2-Hexanone ug/L ND 5.0 0.48 10/02/22 18:47 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 10/02/22 18:47 Acetone ug/L ND 25.0 5.1 10/02/22 18:47 Acrylonitrile ug/L ND 10.0 1.8 10/02/22 18:47 Benzene ug/L ND 1.0 0.34 10/02/22 18:47 Bromochloromethane ug/L ND 1.0 0.47 10/02/22 18:47 Bromodichloromethane ug/L ND 1.0 0.31 10/02/22 18:47 Bromoform ug/L ND 1.0 0.34 10/02/22 18:47 Bromomethane ug/L ND 2.0 1.7 10/02/22 18:47 Carbon disulfide ug/L ND 2.0 0.36 10/02/22 18:47 Carbon tetrachloride ug/L ND 1.0 0.33 10/02/22 18:47 Chlorobenzene ug/L ND 1.0 0.28 10/02/22 18:47 Chloroethane ug/L ND 1.0 0.65 10/02/22 18:47 Chloroform ug/L ND 1.0 0.43 10/02/22 18:47 Chloromethane ug/L ND 1.0 0.54 10/02/22 18:47 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 10/02/22 18:47 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 10/02/22 18:47 Dibromochloromethane ug/L ND 1.0 0.36 10/02/22 18:47 Dibromomethane ug/L ND 1.0 0.39 10/02/22 18:47 Ethylbenzene ug/L ND 1.0 0.30 10/02/22 18:47 lodomethane ug/L ND 20.0 9.7 10/02/22 18:47 Methylene Chloride ug/L ND 5.0 2.0 10/02/22 18:47 Styrene ug/L ND 1.0 0.29 10/02/22 18:47 Tetrachloroethene ug/L ND 1.0 0.29 10/02/22 18:47 Tetrahydrofuran ug/L ND 10.0 3.5 10/02/22 18:47 Toluene ug/L ND 1.0 0.48 10/02/22 18:47 IK Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 48 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 METHOD BLANK: 3787851 Matrix: Water Associated Lab Samples: 92628588008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.40 10/02/22 18:47 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 10/02/22 18:47 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 10/02/22 18:47 Trichloroethene ug/L ND 1.0 0.38 10/02/22 18:47 Trichlorofluoromethane ug/L ND 1.0 0.30 10/02/22 18:47 Vinyl acetate ug/L ND 2.0 1.3 10/02/22 18:47 Vinyl chloride ug/L ND 1.0 0.39 10/02/22 18:47 Xylene (Total) ug/L ND 1.0 0.34 10/02/22 18:47 1,2-Dichloroethane-d4 (S) % 118 70-130 10/02/22 18:47 4-Bromofluorobenzene (S) % 96 70-130 10/02/22 18:47 Toluene-d8 (S) % 111 70-130 10/02/22 18:47 LABORATORY CONTROL SAMPLE: 3787852 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,1-Trichloroethane ug/L 50 54.3 109 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.7 109 70-130 1,1,2-Trichloroethane ug/L 50 53.1 106 70-130 1,1-Dichloroethane ug/L 50 53.0 106 70-130 1,1-Dichloroethene ug/L 50 54.3 109 70-130 1,2,3-Trichloropropane ug/L 50 54.7 109 70-130 1,2-Dibromo-3-chloropropane ug/L 50 53.7 107 70-131 1,2-Dibromoethane (EDB) ug/L 50 52.8 106 70-130 1,2-Dichlorobenzene ug/L 50 52.3 105 70-130 1,2-Dichloroethane ug/L 50 55.6 111 70-130 1,2-Dichloropropane ug/L 50 50.9 102 70-130 1,4-Dichlorobenzene ug/L 50 51.2 102 70-130 2-Butanone (MEK) ug/L 100 106 106 70-134 2-Hexanone ug/L 100 114 114 70-131 4-Methyl-2-pentanone (MIBK) ug/L 100 108 108 70-130 Acetone ug/L 100 106 106 70-133 Acrylonitrile ug/L 250 272 109 70-130 Benzene ug/L 50 47.2 94 70-130 Bromochloromethane ug/L 50 52.1 104 70-130 Bromodichloromethane ug/L 50 52.5 105 70-130 Bromoform ug/L 50 52.3 105 70-130 Bromomethane ug/L 50 45.0 90 45-151 Carbon disulfide ug/L 50 48.1 96 70-130 Carbon tetrachloride ug/L 50 51.6 103 70-130 Chlorobenzene ug/L 50 52.6 105 70-130 Chloroethane ug/L 50 57.6 115 39-152 IK Chloroform ug/L 50 53.6 107 70-130 Chloromethane ug/L 50 50.0 100 58-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 LABORATORY CONTROL SAMPLE: Parameter 3787852 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 54.6 109 70-130 cis-1,3-Dichloropropene ug/L 50 55.1 110 70-130 Dibromochloromethane ug/L 50 55.1 110 70-130 Dibromomethane ug/L 50 45.3 91 70-130 Ethylbenzene ug/L 50 52.4 105 70-130 lodomethane ug/L 100 107 107 53-141 Methylene Chloride ug/L 50 54.0 108 66-130 Styrene ug/L 50 52.3 105 70-130 Tetrachloroethene ug/L 50 49.5 99 70-130 Tetrahydrofuran ug/L 500 570 114 70-130 Toluene ug/L 50 49.0 98 70-130 trans-1,2-Dichloroethene ug/L 50 53.8 108 70-130 trans- 1,3-Dichloropropene ug/L 50 55.4 111 70-130 trans-1,4-Dichloro-2-butene ug/L 50 55.3 111 57-185 Trichloroethene ug/L 50 49.4 99 70-130 Trichlorofluoromethane ug/L 50 46.1 92 62-130 Vinyl acetate ug/L 100 115 115 70-144 Vinyl chloride ug/L 50 51.9 104 62-130 Xylene (Total) ug/L 150 158 105 70-130 1,2-Dichloroethane-d4 (S) % 111 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 100 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787853 MS 92628486006 Spike Parameter Units Result Conc. MSD Spike Conc. 3787854 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 20.6 21.6 103 108 70-141 5 30 1,1,1-Trichloroethane ug/L ND 20 20 26.5 25.3 132 126 70-150 5 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.5 22.2 108 111 69-142 3 30 1,1,2-Trichloroethane ug/L ND 20 20 23.5 22.1 118 110 70-138 6 30 1,1-Dichloroethane ug/L ND 20 20 24.9 24.0 125 120 70-150 4 30 1,1-Dichloroethene ug/L ND 20 20 26.5 26.0 132 130 70-156 2 30 1,2,3-Trichloropropane ug/L ND 20 20 21.4 20.3 107 102 70-140 5 30 1,2-Dibromo-3- ug/L ND 20 20 22.1 22.3 111 112 68-146 1 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 21.3 22.9 107 114 70-138 7 30 1,2-Dichlorobenzene ug/L ND 20 20 20.3 22.0 102 110 70-141 8 30 1,2-Dichloroethane ug/L ND 20 20 24.8 23.4 124 117 69-143 6 30 1,2-Dichloropropane ug/L ND 20 20 23.0 23.6 115 118 68-156 3 30 1,4-Dichlorobenzene ug/L ND 20 20 20.4 20.4 102 102 70-142 0 30 2-Butanone (MEK) ug/L ND 40 40 47.1 43.1 118 108 60-157 9 30 2-Hexanone ug/L ND 40 40 45.2 46.2 113 115 68-146 2 30 4-Methyl-2-pentanone ug/L ND 40 40 41.4 43.2 104 108 70-141 4 30 (MIBK) Acetone ug/L ND 40 40 48.4 45.8 121 115 58-157 5 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787853 3787854 MS MSD 92628486006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acrylonitrile ug/L ND 100 100 123 117 123 117 69-147 4 30 Benzene ug/L ND 20 20 21.5 21.1 108 106 70-142 2 30 Bromochloromethane ug/L ND 20 20 25.0 23.7 125 118 70-146 6 30 Bromodichloromethane ug/L ND 20 20 23.5 22.2 117 111 70-139 6 30 Bromoform ug/L ND 20 20 20.4 20.5 102 103 64-140 0 30 Bromomethane ug/L ND 20 20 23.8 21.8 119 109 28-192 9 30 Carbon disulfide ug/L ND 20 20 24.0 23.2 120 116 70-151 4 30 Carbon tetrachloride ug/L ND 20 20 26.3 25.3 131 127 70-148 4 30 Chlorobenzene ug/L ND 20 20 21.6 22.4 108 112 70-141 4 30 Chloroethane ug/L ND 20 20 31.9 29.4 159 147 58-191 8 30 IK,v1 Chloroform ug/L ND 20 20 25.1 23.8 125 119 70-148 5 30 Chloromethane ug/L ND 20 20 25.1 23.9 125 119 43-162 5 30 cis-1,2-Dichloroethene ug/L ND 20 20 25.7 24.6 128 123 68-151 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 23.4 23.4 117 117 70-139 0 30 Dibromochloromethane ug/L ND 20 20 22.5 21.1 112 106 70-144 6 30 Dibromomethane ug/L ND 20 20 19.0 19.5 95 97 70-139 2 30 Ethylbenzene ug/L ND 20 20 22.6 22.8 113 114 70-143 1 30 lodomethane ug/L ND 40 40 49.1 46.0 123 115 35-171 6 30 Methylene Chloride ug/L ND 20 20 23.3 22.9 117 114 62-149 2 30 Styrene ug/L ND 20 20 20.8 21.4 104 107 70-143 3 30 Tetrachloroethene ug/L ND 20 20 19.5 20.9 97 104 70-145 7 30 Tetrahydrofuran ug/L ND 200 200 244 226 122 113 69-144 8 30 Toluene ug/L ND 20 20 21.3 21.8 107 109 70-142 2 30 trans-1,2-Dichloroethene ug/L ND 20 20 26.0 24.5 130 122 70-151 6 30 trans-1,3-Dichloropropene ug/L ND 20 20 23.7 23.3 119 116 70-139 2 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 18.8 18.8 94 94 51-159 0 30 Trichloroethene ug/L ND 20 20 22.0 22.6 110 113 62-146 3 30 Trichlorofluoromethane ug/L ND 20 20 24.3 23.8 121 119 63-153 2 30 Vinyl acetate ug/L ND 40 40 50.1 46.7 125 117 61-162 7 30 v1 Vinyl chloride ug/L ND 20 20 27.2 26.3 136 132 61-163 3 30 Xylene (Total) ug/L ND 60 60 65.0 66.8 108 111 70-143 3 30 1,2-Dichloroethane-d4 (S) % 122 111 70-130 4-Bromofluorobenzene (S) % 99 99 70-130 Toluene-d8 (S) % 100 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727685 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 METHOD BLANK: 3789304 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 10/04/22 23:46 1,1,1-Trichloroethane ug/L ND 1.0 0.33 10/04/22 23:46 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 10/04/22 23:46 1,1,2-Trichloroethane ug/L ND 1.0 0.32 10/04/22 23:46 1,1-Dichloroethane ug/L ND 1.0 0.37 10/04/22 23:46 1,1-Dichloroethene ug/L ND 1.0 0.35 10/04/22 23:46 1,2,3-Trichloropropane ug/L ND 1.0 0.26 10/04/22 23:46 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 10/04/22 23:46 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 10/04/22 23:46 1,2-Dichlorobenzene ug/L ND 1.0 0.34 10/04/22 23:46 1,2-Dichloroethane ug/L ND 1.0 0.32 10/04/22 23:46 1,2-Dichloropropane ug/L ND 1.0 0.36 10/04/22 23:46 1,4-Dichlorobenzene ug/L ND 1.0 0.33 10/04/22 23:46 2-Butanone (MEK) ug/L ND 5.0 4.0 10/04/22 23:46 2-Hexanone ug/L ND 5.0 0.48 10/04/22 23:46 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 10/04/22 23:46 Acetone ug/L ND 25.0 5.1 10/04/22 23:46 Acrylonitrile ug/L ND 10.0 1.8 10/04/22 23:46 Benzene ug/L ND 1.0 0.34 10/04/22 23:46 Bromochloromethane ug/L ND 1.0 0.47 10/04/22 23:46 Bromodichloromethane ug/L ND 1.0 0.31 10/04/22 23:46 Bromoform ug/L ND 1.0 0.34 10/04/22 23:46 Bromomethane ug/L ND 2.0 1.7 10/04/22 23:46 Carbon disulfide ug/L ND 2.0 0.36 10/04/22 23:46 Carbon tetrachloride ug/L ND 1.0 0.33 10/04/22 23:46 Chlorobenzene ug/L ND 1.0 0.28 10/04/22 23:46 Chloroethane ug/L ND 1.0 0.65 10/04/22 23:46 Chloroform ug/L ND 1.0 0.43 10/04/22 23:46 Chloromethane ug/L ND 1.0 0.54 10/04/22 23:46 v2 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 10/04/22 23:46 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 10/04/22 23:46 Dibromochloromethane ug/L ND 1.0 0.36 10/04/22 23:46 Dibromomethane ug/L ND 1.0 0.39 10/04/22 23:46 Ethylbenzene ug/L ND 1.0 0.30 10/04/22 23:46 lodomethane ug/L ND 20.0 9.7 10/04/22 23:46 Methylene Chloride ug/L ND 5.0 2.0 10/04/22 23:46 Styrene ug/L ND 1.0 0.29 10/04/22 23:46 Tetrachloroethene ug/L ND 1.0 0.29 10/04/22 23:46 Tetrahydrofuran ug/L ND 10.0 3.5 10/04/22 23:46 Toluene ug/L ND 1.0 0.48 10/04/22 23:46 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 METHOD BLANK: 3789304 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.40 10/04/22 23:46 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 10/04/22 23:46 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 10/04/22 23:46 Trichloroethene ug/L ND 1.0 0.38 10/04/22 23:46 Trichlorofluoromethane ug/L ND 1.0 0.30 10/04/22 23:46 Vinyl acetate ug/L ND 2.0 1.3 10/04/22 23:46 Vinyl chloride ug/L ND 1.0 0.39 10/04/22 23:46 Xylene (Total) ug/L ND 1.0 0.34 10/04/22 23:46 1,2-Dichloroethane-d4 (S) % 95 70-130 10/04/22 23:46 4-Bromofluorobenzene (S) % 97 70-130 10/04/22 23:46 Toluene-d8 (S) % 102 70-130 10/04/22 23:46 LABORATORY CONTROL SAMPLE: Parameter 3789305 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.3 105 70-130 1,1,1-Trichloroethane ug/L 50 46.8 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.6 99 70-130 1,1,2-Trichloroethane ug/L 50 50.2 100 70-130 1,1-Dichloroethane ug/L 50 44.9 90 70-130 1,1-Dichloroethene ug/L 50 44.1 88 70-130 1,2,3-Trichloropropane ug/L 50 48.4 97 70-130 1,2-Dibromo-3-chloropropane ug/L 50 52.3 105 70-131 1,2-Dibromoethane (EDB) ug/L 50 51.1 102 70-130 1,2-Dichlorobenzene ug/L 50 50.6 101 70-130 1,2-Dichloroethane ug/L 50 43.0 86 70-130 1,2-Dichloropropane ug/L 50 48.1 96 70-130 1,4-Dichlorobenzene ug/L 50 48.7 97 70-130 2-Butanone (MEK) ug/L 100 96.9 97 70-134 2-Hexanone ug/L 100 106 106 70-131 4-Methyl-2-pentanone (MIBK) ug/L 100 99.0 99 70-130 Acetone ug/L 100 96.5 97 70-133 Acrylonitrile ug/L 250 249 99 70-130 Benzene ug/L 50 45.5 91 70-130 Bromochloromethane ug/L 50 47.5 95 70-130 Bromodichloromethane ug/L 50 48.1 96 70-130 Bromoform ug/L 50 54.0 108 70-130 Bromomethane ug/L 50 46.7 93 45-151 Carbon disulfide ug/L 50 45.7 91 70-130 Carbon tetrachloride ug/L 50 50.4 101 70-130 Chlorobenzene ug/L 50 49.4 99 70-130 Chloroethane ug/L 50 45.6 91 39-152 Chloroform ug/L 50 45.0 90 70-130 Chloromethane ug/L 50 42.6 85 58-130 v3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 LABORATORY CONTROL SAMPLE: Parameter 3789305 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 45.2 90 70-130 cis-1,3-Dichloropropene ug/L 50 51.5 103 70-130 Dibromochloromethane ug/L 50 51.2 102 70-130 Dibromomethane ug/L 50 48.5 97 70-130 Ethylbenzene ug/L 50 48.7 97 70-130 lodomethane ug/L 100 101 101 53-141 Methylene Chloride ug/L 50 46.9 94 66-130 Styrene ug/L 50 52.0 104 70-130 Tetrachloroethene ug/L 50 49.1 98 70-130 Tetrahydrofuran ug/L 500 492 98 70-130 Toluene ug/L 50 45.8 92 70-130 trans-1,2-Dichloroethene ug/L 50 47.0 94 70-130 trans- 1,3-Dichloropropene ug/L 50 50.9 102 70-130 trans-1,4-Dichloro-2-butene ug/L 50 44.7 89 57-185 Trichloroethene ug/L 50 50.8 102 70-130 Trichlorofluoromethane ug/L 50 42.6 85 62-130 Vinyl acetate ug/L 100 102 102 70-144 Vinyl chloride ug/L 50 46.5 93 62-130 Xylene (Total) ug/L 150 148 99 70-130 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 97 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3789306 MS 92628588001 Spike Parameter Units Result Conc. MSD Spike Conc. 3789307 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 26.1 26.0 131 130 70-141 1 30 1,1,1-Trichloroethane ug/L ND 20 20 25.1 24.7 126 124 70-150 2 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 25.1 25.4 125 127 69-142 1 30 1,1,2-Trichloroethane ug/L ND 20 20 25.2 23.3 126 116 70-138 8 30 1,1-Dichloroethane ug/L ND 20 20 23.3 23.2 117 116 70-150 0 30 1,1-Dichloroethene ug/L ND 20 20 24.1 23.7 120 118 70-156 2 30 1,2,3-Trichloropropane ug/L ND 20 20 24.7 23.0 123 115 70-140 7 30 1,2-Dibromo-3- ug/L ND 20 20 26.6 26.7 133 133 68-146 0 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 26.1 25.6 130 128 70-138 2 30 1,2-Dichlorobenzene ug/L ND 20 20 25.0 25.0 125 125 70-141 0 30 1,2-Dichloroethane ug/L ND 20 20 22.5 22.9 112 114 69-143 2 30 1,2-Dichloropropane ug/L ND 20 20 24.7 24.3 124 121 68-156 2 30 1,4-Dichlorobenzene ug/L ND 20 20 25.1 25.2 125 126 70-142 0 30 2-Butanone (MEK) ug/L ND 40 40 53.5 47.9 134 120 60-157 11 30 2-Hexanone ug/L ND 40 40 54.4 52.6 136 131 68-146 4 30 4-Methyl-2-pentanone ug/L ND 40 40 49.7 46.5 124 116 70-141 7 30 (MIBK) Acetone ug/L ND 40 40 56.6 51.2 142 128 58-157 10 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3789306 3789307 MS MSD 92628588001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acrylonitrile ug/L ND 100 100 129 124 129 124 69-147 4 30 Benzene ug/L ND 20 20 23.6 22.4 118 112 70-142 5 30 Bromochloromethane ug/L ND 20 20 25.7 24.8 128 124 70-146 4 30 Bromodichloromethane ug/L ND 20 20 25.2 24.3 126 122 70-139 4 30 Bromoform ug/L ND 20 20 26.8 25.7 134 128 64-140 4 30 Bromomethane ug/L ND 20 20 24.2 23.0 121 115 28-192 5 30 v3 Carbon disulfide ug/L ND 20 20 22.5 22.4 113 112 70-151 0 30 Carbon tetrachloride ug/L ND 20 20 26.2 25.6 131 128 70-148 2 30 Chlorobenzene ug/L 0.51J 20 20 25.6 26.4 126 129 70-141 3 30 Chloroethane ug/L ND 20 20 24.2 24.1 121 121 58-191 0 30 v3 Chloroform ug/L 2.1 20 20 25.2 24.6 116 113 70-148 2 30 Chloromethane ug/L ND 20 20 23.7 22.9 118 114 43-162 3 30 v3 cis-1,2-Dichloroethene ug/L ND 20 20 23.9 23.8 120 119 68-151 0 30 cis-1,3-Dichloropropene ug/L ND 20 20 26.0 24.7 130 123 70-139 5 30 Dibromochloromethane ug/L ND 20 20 26.5 26.3 132 131 70-144 1 30 Dibromomethane ug/L ND 20 20 26.1 24.4 131 122 70-139 7 30 Ethylbenzene ug/L ND 20 20 25.1 25.0 126 125 70-143 1 30 lodomethane ug/L ND 40 40 48.9 47.1 122 118 35-171 4 30 Methylene Chloride ug/L ND 20 20 24.9 24.4 125 122 62-149 2 30 Styrene ug/L ND 20 20 26.3 25.9 132 130 70-143 2 30 Tetrachloroethene ug/L ND 20 20 24.2 24.7 121 123 70-145 2 30 Tetrahydrofuran ug/L ND 200 200 251 244 126 122 69-144 3 30 Toluene ug/L ND 20 20 24.4 23.1 122 116 70-142 5 30 trans-1,2-Dichloroethene ug/L ND 20 20 24.2 24.6 121 123 70-151 2 30 trans-1,3-Dichloropropene ug/L ND 20 20 26.2 25.2 131 126 70-139 4 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 16.1 19.6 80 98 51-159 20 30 Trichloroethene ug/L ND 20 20 26.2 24.8 131 124 62-146 6 30 Trichlorofluoromethane ug/L ND 20 20 22.5 23.1 112 115 63-153 3 30 Vinyl acetate ug/L ND 40 40 50.9 47.5 127 119 61-162 7 30 Vinyl chloride ug/L ND 20 20 25.4 25.2 127 126 61-163 1 30 Xylene (Total) ug/L ND 60 60 75.1 75.4 125 126 70-143 0 30 1,2-Dichloroethane-d4 (S) % 97 94 70-130 4-Bromofluorobenzene (S) % 100 102 70-130 Toluene-d8 (S) % 99 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727317 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92628588008 METHOD BLANK: 3787732 Matrix: Water Associated Lab Samples: 92628588008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 10/01/22 14:07 1,2-Dichloroethane-d4 (S) % 104 70-130 10/01/22 14:07 Toluene-d8 (S) % 105 70-130 10/01/22 14:07 LABORATORY CONTROL SAMPLE: 3787733 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 18.2 91 70-130 1,2-Dichloroethane-d4 (S) % 101 70-130 Toluene-d8(S) % 102 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787734 3787735 MS MSD 92628458008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 21.3 22.0 106 110 63-136 3 30 1,2-Dichloroethane-d4 (S) % 105 106 70-130 30 Toluene-d8 (S) % 107 105 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727318 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 METHOD BLANK: 3787736 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004, 92628588005, 92628588006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 10/01/22 14:08 1,2-Dichloroethane-d4 (S) % 90 70-130 10/01/22 14:08 Toluene-d8 (S) % 99 70-130 10/01/22 14:08 LABORATORY CONTROL SAMPLE: 3787737 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 18.9 94 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 Toluene-d8(S) % 102 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787738 3787739 MS MSD 92628458030 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 21.0 19.0 105 95 63-136 10 30 1,2-Dichloroethane-d4 (S) % 108 102 70-130 30 Toluene-d8 (S) % 104 106 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727323 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004 METHOD BLANK: 3787752 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 5.0 10/01/22 14:58 LABORATORY CONTROL SAMPLE: 3787753 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 50.3 101 80-120 LABORATORY CONTROL SAMPLE: 3787754 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 51.0 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787755 3787756 MS MSD 92628237001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 mg/L 26.3 50 50 75.1 74.5 98 96 80-120 1 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787757 3787758 MS MSD 92628237002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 mg/L 26.0 50 50 78.3 77.9 105 104 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727291 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003 METHOD BLANK: 3787639 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 25.0 10/01/22 11:15 LABORATORY CONTROL SAMPLE: 3787640 Spike LCS Parameter Units Conc. Result Total Dissolved Solids mg/L 250 256 SAMPLE DUPLICATE: 3787641 92628085001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 6460000 ug/L 6600 LCS % Rec % Rec Limits Qualifiers 102 90-110 Max RPD RPD Qualifiers 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 48 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 QC Batch: 727186 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004 METHOD BLANK: 3787305 Matrix: Water Associated Lab Samples: 92628588001, 92628588002, 92628588003, 92628588004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride mg/L ND 1.0 0.60 09/30/2216:18 Nitrate as N mg/L ND 0.10 0.060 09/30/22 16:18 Sulfate mg/L ND 1.0 0.50 09/30/2216:18 LABORATORY CONTROL SAMPLE: 3787306 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 48.1 96 90-110 Nitrate as N mg/L 2.5 2.4 95 90-110 Sulfate mg/L 50 48.5 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3787307 3787308 MS MSD 92628482001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride mg/L 4.7 50 50 52.9 53.3 96 97 90-110 1 10 Nitrate as N mg/L 0.50 2.5 2.5 3.0 3.0 99 99 90-110 1 10 Sulfate mg/L 3.2 50 50 51.6 52.1 97 98 90-110 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /01 /2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GM1.004/.005 OXFORD 92628588 LANDFILL Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92628588002 MW-5R AM20GAX 751115 92628588003 MW-7 AM20GAX 751115 92628588004 NES-2S AM20GAX 751115 92628588002 MW-5R RSK-175 751162 92628588003 MW-7 RSK-175 751162 92628588004 NES-2S RSK-175 751162 92628588001 MW-3RR EPA 3010A 727880 EPA 6010D 727892 92628588002 MW-5R EPA 3010A 727880 EPA 6010D 727892 92628588003 MW-7 EPA 3010A 727880 EPA 6010D 727892 92628588004 NES-2S EPA 3010A 727880 EPA 6010D 727892 92628588005 SW-1 EPA 3010A 727880 EPA 6010D 727892 92628588006 SW-2 EPA 3010A 727880 EPA 6010D 727892 92628588001 MW-3RR EPA 3010A 727920 EPA 6020B 728088 92628588002 MW-5R EPA 3010A 727920 EPA 6020B 728088 92628588003 MW-7 EPA 3010A 727920 EPA 6020B 728088 92628588004 NES-2S EPA 3010A 727920 EPA 6020B 728088 92628588005 SW-1 EPA 3010A 727920 EPA 6020B 728088 92628588006 SW-2 EPA 3010A 727920 EPA 6020B 728088 92628588001 MW-3RR EPA 7470A 727674 EPA 7470A 728041 92628588002 MW-5R EPA 7470A 727674 EPA 7470A 728041 92628588003 MW-7 EPA 7470A 727674 EPA 7470A 728041 92628588001 MW-3RR EPA 8260D 727685 92628588002 MW-5R EPA 8260D 727685 92628588003 MW-7 EPA 8260D 727685 92628588004 NES-2S EPA 8260D 727685 92628588005 SW-1 EPA 8260D 727685 92628588006 SW-2 EPA 8260D 727685 92628588008 TRIP BLANK EPA 8260D 727360 92628588001 MW-3RR EPA 8260D Mod. 727318 92628588002 MW-5R EPA 8260D Mod. 727318 92628588003 MW-7 EPA 8260D Mod. 727318 92628588004 NES-2S EPA 8260D Mod. 727318 92628588005 SW-1 EPA 8260D Mod. 727318 92628588006 SW-2 EPA 8260D Mod. 727318 92628588008 TRIP BLANK EPA 8260D Mod. 727317 92628588001 MW-3RR SM 2320B-2011 727323 92628588002 MW-5R SM 2320B-2011 727323 92628588003 MW-7 SM 2320B-2011 727323 92628588004 NES-2S SM 2320E-2011 727323 92628588001 MW-3RR SM 2540C-2011 727291 92628588002 MW-5R SM 2540C-2011 727291 92628588003 MW-7 SM 2540C-2011 727291 92628588001 MW-3RR EPA 300.0 Rev 2.1 1993 727186 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2022 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 48 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: GM1.004/.005 OXFORD LANDFILL Pace Project No.: 92628588 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92628588002 MW-511 EPA 300.0 Rev 2.1 1993 727186 92628588003 MW-7 EPA 300.0 Rev 2.1 1993 727186 92628588004 NES-2S EPA 300.0 Rev 2.1 1993 727186 Date: 11/01/2022 12:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 45 of 48 DG# Title: ENV�FRWHUNI-0003 v04—S . a . mple Conditid Upon Receipt Co. P tabomory receiving samples: Ashkille.4. EdenCxreenwood[] Huntersville[I RalelghL] Mecl,--;--,*'F-r—J r-' S a m pie Cc pdftioFi ClIent Narne: U13Dn Re eipt Project N., W011:92628588 Courier: ed EX OUPS E]USPS kht cCommercialPace []0thbr: 926281,588 1 Custedy.SeaVl?resent? []yes XN a Seals Intact? []Yes )000 Pad04Na;e!10b 006ble WraDBubble Bags E:]Nonc ❑ Other Th4 0 H-6 bm*td-h'. Type orice; et E]BILe CoolerTeino"4 I 1.7 Correction Factor; Add/Subtract ('C) Cooler temp Corrected (T) . USOA Regulated Soil ( ZN/A, water.Lg6rn;pl el Did sarnplesior.ig!na(e tn.a quarandne ZWfthin the Udi .SfAtqr.'C-A ,orsc (check rnafos)?.MYes 014a ?d W-ihiri Rush Turn An 3. Date/InWals Persion.E.*amt."ins contents- LLI �0 Ls ftldgk3l Tissue Ffbzent Dyes E]No EIPJA [Wane Te rnp should be above freezing to V�c ElSampleswohemp-criti2fia-. Samples on ice, cooftrigpirotem. has begun. Did samples origipatorpm a foreign source (internationally, includirig Hawaii and Puerto FRO? nYes rIN6 Correc! dontali*rs Used? 91 as []N6 []N/A 6. -Pace Cantaineirs-Used7P Wes NaQ C]N/A Contairters Intact? MyLis [:]No EIN/A 7. I)Walvedanalysil,! Samples Field FRergd3i I- - yes- No '!rt3 ©N/A 8. 5a,mp!wLaWs Mitch COC21. es -Eig. [jNJA 9. Matrix: UIP 01anK Fresent? PqYr EltYo EJN/A 11. Trip BlanIcCustody Seals present? Erfes EIND ONfa COMMENTS/SAMPLE DISCREPANCY i - Lot 10 Of split CObtairiers- CLIENT NOTIFICATIONIRESOWTION Pe*rj.c�ontacted,. Project Manager SCURF Review: r;'494' rolwiii&�i a' A%Y , '�G . ,- . Date/Ti me: Date: uaxe; Quaftrax ID: 69614 Page 1 of 2 Page 46 of 48 1' ''c ' DC# Title; ENV.FRM-HUN9-0084 01 Tech Spec Sample Condition Upon Receipt i —r K,.tb=n Effective pate: 0511212022 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 {water] 00C, LLHg "Bottom half of box is to list number of bottles ***Check all. unpreserved Nitrates for chlorine Project N ON: 92628588 PM: TIIC Due Date: 10/07/22 CLIENT: 92-Hart_Ral U " z u 41b E W _ z cn L! a 'J E v Z ca Z c [J n o M a m Z C 7 U c o 0_ N a m Z v a C 7 rL ..4 rl m ry v 00 ry = V rl Ln 4 a IL V 0 Z n m a m z ¢ N U a !E v a. m n n a Lf a 7 a m a R tx r j 3 2 i' ? E W a v N u a 41 l7 M u a y n N = E .�� l7 a 2 ¢ J rn t� 4 ,d ? Z W Q E of t7 o = M 0 z cNn NQ. Z O > a C7 z v d O a 0 C O 7 v 0 o = yy P o0� 2 o u tx7 a li ?. m N uWt ��„ ? VNu�lJE N C. re O VI V d Opp M m diL. a J Q a N O VI N = a -y W n. C Q Eu m n r/n 3 l XN (� 3-1 1 XN 3 3 1 1 3 a 3 5 � is I �! t g 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot N Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I Out of hold, lncorrect preservative, out of temp, incorrect containers) Qualtrax Document ID: 70677 Page 2 of 2 Page 47 of 48 a� It 'S rz (WA) a+Lugg,) lenpsa�j MNV t3 c� i sel alellaSleFucl'JO Anu�ieVM atvl•N a��y7ary Pa+losslp OW2Agaus%O`(l p •l Olc* Aq %;B; 4 G9LB hq OOA "4;0 N�p41aY1 N v a EGZS12N `Q 2 HOEN m N IDN EONH apgLH ra.vasa:eu� SL+7Htl11i0� d0 i n'alc:Nno� irdv;ai 3"kll\IS c � f0 4 � F !n ❑ C �1 .L 3 idltr> � a � ii � (ik�l � sor � a,v� cas} 3Qm n ;o wZ1wi o a m Q ° o a s o "@ a "os awoSKpH c� Q m q N FF 15 M � v G= M L 4 M❑ P 6 O V be O a a t Lu n �? e a R � 9 1 OS q N a' (wm Felu SRl LLeg �appO Paleag FtKil�rrl {wti) mr Uo D "^ Imu `n .5, - u D n Page 48 of 48 Appendix C Summary of Historical Groundwater Elevations 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix C Summary of Historical Groundwater Elevations Granville County Oxford Unit 2 Landfill Oxford North Carolina H&H Job No. GMI-005 Date Groundwater Elevations (ft AMSL) Background Downgradient MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S 06/13/12 513.48 503.31 479.70 477.42 473.20 468.81 08/22/12 509.73 500.82 477.97 475.31 471.50 469.36 09/25/12 508.45 499.85 478.10 475.06 471.86 469.30 10/17/12 507.95 499.90 478.00 474.23 471.04 467.98 08/06/13 514.33 499.92 478.81 475.32 472.80 469.29 02/25/14 511.75 499.91 480.34 476.26 473.47 470.28 08/12/14 511.98 500.16 479.91 476.54 473.42 470.29 03/12/15 516.39 499.99 479.73 476.47 473.66 470.63 08/18/15 512.39 499.86 478.41 474.92 472.17 469.25 02/16/16 515.79 499.90 481.44 476.37 474.12 471.15 08/10/16 514.29 499.82 478.86 475.51 472.91 470.40 02/14/17 510.89 496.36 479.36 475.97 472.77 468.85 08/23/17 508.84 499.61 477.86 474.74 472.02 469.80 02/07/18 505.74 499.86 479.88 476.25 473.54 471.40 08/14/18 510.22 499.95 478.22 475.31 473.57* 470.81 02/05/19 515.74 500.01 480.72 476.63 474.03 472.18 08/07/19 512.11 500.15 478.86 475.75 473.09 472.31 09/04/19 NM NM NM 475.09 NM NM 02/12/20 511.37 499.99 481.41 477.10 475.06 472.76 03/19/20 512.89 NM NM 476.33 473.90 471.82 04/23/20 NM NM NM NM NM 472.06 08/26/20 512.24 499.98 479.78 476.64 473.97 453.00 09/29/20 NM N M NM 476.76 NM NM 02/10/21 517.28 499.88 481.52 476.92 474.32 472.06 08/18/21 511.96 500.19 478.96 475.95 473.13 471.20 02/15/22 507.49 500.10 479.40 476.18 473.22 471.26 10/05/22 507.52 500.22 478.06 476.57 473.52 472.23 Notes: Groundwater elevations from June 2012 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Groundwater elevations from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. ft AMSL = ft above mean sea level -- = not applicable; NM = not measured Appendix C (Page 1 of 1) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables.xlsx Appendix D Summary of Historical Constituents in Groundwater 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Inorganics Antimony 02/15/22 3 --- ND ND ND ND --- NC2L = 1 fag/L 10/05/22 3.0 <5.0 <1.0 0.28 J <1.0 <1.0 <5.0 Arsenic 03/12/15 2.5 4.2 J ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND NC2L = 10 ug/L 02/18/16 2.5 ND ND 2.7 ND 3.9 J ND 08/11/16 2.5 ND ND ND 3.1 J 3.2 J ND 02/14/17 5 ND ND ND ND ND ND 08/23/17 5 ND ND ND ND ND ND 02/06/18 --- ND ND ND ND ND ND 08/16/18 5 ND ND ND ND NM ND 02/05/19 5 ND ND ND ND ND ND 08/08/19 5 ND ND ND ND ND ND 02/14/20 4.7 ND ND ND ND ND --- 03/19/20 4.7 ND NS NS NS NS ND 08/26/20 4.7 ND ND ND ND ND J 5.2 J 02/10/21 4.7 4.7 J 5.5 J ND ND --- ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 4.7 5.9 J 4.9 J 5.4 J ND ND NA 10/05/22 4.7 <10.0 1.4 0.37 J 0.33 J 0.19 J <10.0 Barium 06/13/12 --- 9.2 J 36.8 J 59.2 J 48.2 J 30.6 J 31.4 J 08/22/12 --- ND 37.3 J 60.9 J 58.9 J 85 J 28.2 J NC2L = 700 ug/L 09/25/12 --- 10.3 J 40.8 J 64.2 J 72.7 J 43.8 J 30.5 J 10/17/12 --- 24.2 J 57.3 J 65.1 J 48.7 J 110 28 J 08/06/13 --- ND 37.1 J 66.5 J 36.8 J 28.5 J 24.8 J 02/25/14 --- ND 43.6 J 65 J 41.1 J 20.3 J 58.6 J 08/13/14 5 6.2 J 52.7 J 72.7 J 40.7 J 19.7 J 21.7 J 03/12/15 2.5 9.8 J 47.9 J 76.3 J 49.1 J 19.1 J 35.5 J 08/18/15 --- 11 J 45.6 J 72.1 J 43.5 J 20.5 J 31.3 J 02/18/16 2.5 14.8 J 59.5 J 76.1 J 54.2 J 31.8 J 28.6 J 08/11/16 2.5 6.2 J 42.9 J 81 J 61.2 J 49.9 J 31.1 J 02/14/17 2.5 11.8 J 41.9 J 89 J 46.2 J 40.8 J 27.6 J 08/23/17 2.5 25.2 J 42.6 J 126 40.8 J 51.4 J 33.8 J 02/06/18 --- 19.3 J 62.6 J 90.7 J 47.1 J 33.9 J 25.4 J 08/16/18 2.5 3.8 J 40.3 J 68.9 J 47.5 J NM 25.8 J 02/05/19 2.5 4 J 39.8 78 59.4 27.7 19.6 08/08/19 2.5 4.5 J 40.2 71.4 60.5 30.1 ND 02/14/20 1 11 39.3 85 47.2 45 --- 03/19/20 1 NS NS NS NS NS 31.8 08/26/20 3.5 8.8 37.9 73.7 49.3 35.6 32.4 02/10/21 3.5 ND 40.1 76.3 60.6 31.2 ND 08/17/21 --- --- 37.0 76.2 50.2 27.0 --- 02/15/22 3.5 3.8 J 37.5 76.5 37.5 29.0 NA 10/05/22 3.5 4.3 J 38.3 78.4 51.2 28.6 33.7 Cadmium 08/23/17 0.5 ND ND ND 0.56 J ND ND 02/06/18 --- ND ND ND ND 0.59 J ND NC2L = 2 Ng/L 08/16/18 0.5 ND ND ND ND NM ND 02/05/19 0.5 ND ND ND ND ND ND 08/08/19 0.5 ND ND ND ND ND ND 02/14/20 0.4 ND ND ND ND 0.45 J --- 03/19/20 0.4 NS NS NS NS NS ND 08/26/20 0.4 ND ND ND ND ND ND 02/10/21 0.4 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.4 ND ND ND ND ND NA 10/05/22 0.40 <1.0 <0.20 0.15 J <0.20 <0.20 <1.0 Appendix D (Page 1 of6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Chromium 06/13/12 --- ND ND ND 10.9 ND ND 08/22/12 --- ND ND ND 10.4 18.3 ND NC21- = 10 pg/L 09/25/12 --- ND ND ND 10.3 ND ND 10/17/12 --- ND ND ND 15.8 20.9 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 --- ND ND ND 5.1 J ND ND 03/12/15 2.5 ND 3 J ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 2.5 ND ND ND ND ND 3 J 08/11/16 2.5 2.8 J ND ND 4.3 J 6.3 J ND 02/14/17 2.5 ND ND ND ND 4.4 J ND 08/23/17 2.5 ND ND ND ND 4.5 J ND 02/06/18 --- 4.4 J ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NM ND 02/05/19 2.5 ND ND ND ND ND ND 08/08/19 2.5 ND ND ND 1 J ND ND 02/14/20 1 3 J ND 1.6 J 2.6 J 8.8 --- 03/19/20 1 NS NS NS NS NS ND 08/26/20 3.7 ND ND ND ND ND ND 02/10/21 3.7 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.7 ND ND ND ND ND NA 10/05/22 3.7 <5.0 <1.0 <1.0 0.54 J 0.54 J <5.0 Cobalt 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND ND ND ND ND ND NC21- = 1 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- 10.3 ND ND ND 12.4 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5 ND ND ND ND ND ND 03/12/15 2.5 ND ND ND ND ND 3.6 J 08/18/15 --- ND ND ND ND ND ND 02/18/16 2.5 ND ND ND ND ND ND 08/11/16 2.5 ND ND ND ND ND ND 02/14/17 2.5 ND ND ND ND ND 3.2 J 08/23/17 2.5 ND ND ND ND ND ND 02/06/18 --- 3.4 J ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NM ND 02/05/19 2.5 ND ND ND ND ND ND 08/08/19 2.5 ND ND ND ND 1.2 J ND 02/14/20 1.1 2.7 J ND ND ND 3.9 J --- 03/19/20 1.1 NS NS NS NS NS 4.1 J 08/26/20 3.6 ND ND ND ND ND ND 02/10/21 3.6 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.6 ND ND ND ND ND NA 10/05/22 3.6 <5.0 <1.0 0.052 J 0.73 J 1.0 <5.0 Copper 06/13/12 --- ND ND ND 46 ND ND 08/22/12 --- ND ND ND 56.2 19.8 ND NC21- = 1,000 pg/L 09/25/12 --- 7.4 J ND ND 63.6 5.7 J ND 10/17/12 --- 19.9 7.6 J ND 35.5 23.1 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND 7.9 J ND ND 08/13/14 5 ND 11.6 ND 13.4 ND ND 03/12/15 2.5 ND 47 ND 6 J ND 3.3 J 08/18/15 --- 2.8 J 26.6 ND 12.3 ND 4.3 J 02/18/16 2.5 ND 7.8 J ND ND ND ND 08/11/16 2.5 ND 30.7 ND 14.6 4.5 J 2.7 J 02/14/17 2.5 ND 16.6 3.2 J 9.9 J 4.9 J 3.9 J 08/23/17 2.5 8.8 J 6.4 J ND 6.4 J 4.5 J ND 02/06/18 --- 18.6 133 3.7 J 5.4 J ND ND 08/16/18 2.5 ND 24.7 ND 3.6 J NM ND 02/05/19 2.5 ND 11 ND 3 J ND ND 08/08/19 2.5 2.5 J 8.3 ND 6.9 ND ND 02/14/20 2.1 5.5 11.8 ND 4.6 J 17.6 --- 03/19/20 2.1 NS NS NS NS NS ND 08/26/20 4.3 ND 10.9 ND 5.6 ND ND 02/10/21 4.3 ND 7.8 ND 4.5 J ND ND 08/17/21 --- --- 4.6 J ND 8.7 ND --- 02/15/22 4.3 ND 4.5 J ND ND ND NA 10/05/22 1.1 <5.0 12.3 1.2 J 1 <2.0 <2.0 <5.0 Appendix D (Page 2 of6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Iron 02/06/18 --- 9990 1500 1190 1670 1630 353 08/16/18 25 340 --- --- --- NM --- NC21- = 300 pg/L 02/05/19 25 183 --- --- --- --- --- 08/08/19 25 176 --- --- --- --- --- 02/14/20 19.5 3750 --- --- --- --- --- Resample 03/19/20 0.9 1310 NS NS NS ND NS 08/26/20 41.5 1570 --- --- --- --- 1030 02/10/21 41.5 --- --- --- --- -- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA Lead 02/14/17 2.5 ND ND ND ND 2.9 J ND 08/23/17 2.5 ND ND ND ND ND ND NC21- = 15 pg/L 02/06/18 2.5 ND ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NM ND 02/14/20 1.6 ND 1.8 J 1.9 J ND 4.2 J --- 03/19/20 1.6 NS NS NS NS NS ND 02/10/21 1.6 ND ND ND ND ND --- 08/17/21 --- --- ND ND ND ND --- 02/15/22 4.5 ND ND ND ND ND --- 10/05/22 4.5 <5.0 <1.0 <1.0 0.12 J 0.14 J <5.0 Manganese 02/06/18 --- 241 394 53 25.8 J 410 411 08/16/18 2.5 6.7 J --- --- --- NM --- NC2L = 50 pg/L 02/05/19 2.5 5.5 --- --- --- --- --- 08/08/19 2.5 6 --- --- --- --- --- 02/14/20 0.9 85.8 --- --- --- --- --- Resample 03/19/20 0.9 26.4 NS NS NS ND NS 08/26/20 3.4 35.2 --- --- --- --- 431 02/10/21 3.4 --- --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA Nickel 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND ND ND ND 6.1 J ND NC2L = 100 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND 6.9 J 8.9 J ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5 ND ND ND ND ND ND 03/12/15 2.5 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND 2.7 J ND 02/18/16 2.5 ND ND ND ND 2.9 J ND 08/11/16 2.5 ND ND ND ND 6.2 J ND 02/14/17 2.5 ND ND ND ND 5.2 J ND 08/23/17 2.5 5.2 J ND ND 2.8 J 5.8 J ND 02/06/18 --- 5.9 J ND ND ND 3.4 J ND 08/16/18 2.5 ND ND ND ND NM ND 02/05/19 2.5 ND ND ND ND 2.7 J ND 08/08/19 2.5 0.93 J ND ND 1.6 J 3.2 J ND 02/14/20 0.9 2.5 J ND ND 1.3 J 16 --- 03/19/20 0.9 NS NS NS NS NS 1.5 J 08/26/20 3.5 ND ND ND ND 4 J ND 02/10/21 3.5 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.5 --- ND ND ND ND NA 10/05/22 3.5 <5.0 <1.0 <1.0 0.58 J 2.6 <5.0 Selenium 02/15/22 4.7 --- ND ND ND ND --- NC2L = 20 pg/L 10/05/22 4.7 <10.0 <2.0 0.27 J <2.0 <2.0 <10.0 Appendix D (Page 3 of6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Thallium 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND 6.8 6.8 ND ND ND NC21- = 2 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND ND ND ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5.4 ND ND ND ND ND ND 03/12/15 5 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 5 ND ND ND ND ND ND 08/11/16 5 ND ND ND ND ND ND 02/14/17 0.02 0.039 J 0.059 J ND ND ND ND 08/23/17 0.02 0.04 J 0.044 J ND ND 0.021 J ND 02/06/18 --- ND 0.034 J ND ND ND ND 08/16/18 0.02 ND ND ND ND NM ND 02/05/19 0.06 ND ND ND ND ND ND 08/08/19 0.06 ND ND ND ND ND ND 02/14/20 0.06 ND ND ND ND ND --- 03/19/20 0.06 NS NS NS NS NS ND 08/26/20 0.05 ND ND ND ND ND ND 02/10/21 0.05 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.05 ND ND ND ND ND NA 10/05/22 0.050 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 Total Dissolved Solids, Dissolved 08/26/20 25000 262000 --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- NC 2L = 500,000 pg/L 02/10/21 25000 274000 --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA Vanadium 06/13/12 --- 5.2 J ND ND 27.8 17.3 J 11 J 08/22/12 --- ND ND ND 30.2 69.5 9 J NC21- = 7 pg/L 09/25/12 --- 8.3 J ND ND 33.4 16.5 J 8.2 J 10/17/12 --- 29.7 ND ND 19.5 J 63.8 J 6.2 J 08/06/13 --- ND ND ND ND 9.2 J ND 02/25/14 --- ND ND ND 10.2 J ND ND 08/13/14 5 ND ND ND 11.8 J ND ND 03/12/15 2.5 ND 4.4 J 7.3 J 5 J ND 6.7 J 08/18/15 --- 6.1 J ND ND 6.5 J 3.6 J 9.1 J 02/18/16 2.5 ND 2.9 J ND ND ND ND 08/11/16 2.5 ND ND 5.8 J 10 J 14.3 J 6.6 J 02/14/17 2.5 ND ND 5.2 J 4 J 9.1 J 5.4 J 08/23/17 2.5 18.6 J ND 2.6 J 4.6 J 11.9 J 6.4 J 02/06/18 --- 23.5 J 3.4 J 4.4 J 4.7 J 3.3 J ND 08/16/18 2.5 ND ND ND 2.9 J NM 2.5 J 02/05/19 2.5 ND ND ND 2.9 J ND ND 08/08/19 2.5 2.2 J ND ND 5.3 1.8 ND Resample 09/04/19 1.3 NS NS NS ND NS NS 02/14/20 1.3 9.2 ND 3.4 J 5.5 13.3 --- 03/19/20 1.3 7.9 J NS NS 3.2 J ND 5.6 Resample 04/23/20 1.3 NS NS NS NS NS 3 J 08/26/20 3.9 4.4 J ND ND 5.5 ND ND 09/29/20 3.9 --- --- --- ND --- --- 02/10/21 3.9 ND ND ND 4.4 J ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.9 ND ND ND ND ND NA 10/05/22 3.9 <5.0 <1.0 3.1 1.7 1.1 <5.0 Zinc 06/13/12 --- ND ND ND 10.5 ND ND 08/22/12 --- ND ND 32 31 21.9 10.6 NC21-= 1,000 pg/L 09/25/12 --- 11.7 ND ND 14.8 ND ND 10/17/12 --- 32.5 ND ND 10.5 29 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 10 ND ND ND ND ND ND 03/12/15 5 9.8 B 10.9 B 10.7 B 8.7 B 7.8 B 9.9 B 08/18/15 --- 8.9 B ND ND ND ND 5.2 B 02/18/16 5 ND 13.1 ND ND ND 8.6 J 08/11/16 5 7.2 J 5.4 J ND 19.5 11.7 8.7 J 02/14/17 5 7 J 6 J 5.4 J 5.3 J 8.3 J 6 J 08/23/17 5 18 ND 6.3 J 5.1 J 15.5 6.9 J 02/06/18 --- ND ND ND ND ND ND 08/16/18 5 ND ND ND ND NM ND 02/05/19 5 ND ND ND ND ND ND 08/08/19 5 ND ND ND ND ND ND 02/14/20 3.9 9.6 J ND ND ND 20.2 --- 03/19/20 3.9 NS NS NS NS NS ND 08/26/20 9.5 ND ND ND ND ND ND 02/10/21 9.5 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 9.5 ND ND ND ND ND NA 10/05/22 9.5 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 Appendix D (Page 4 of 6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Organics 1,4-Dioxane 08/16/18 1.9 ND ND ND ND NM ND 02/05/19 1.9 ND ND ND ND ND ND NC21- = 3 ug/L 08/08/19 1.9 ND ND ND ND ND ND 02/14/20 1.2 ND ND ND ND ND ND 08/26/20 1.2 ND ND ND ND ND ND 02/10/21 1.2 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.86 ND ND ND ND ND --- 10/05/22 0.86 1.7 J <2.0 <2.0 <2.0 <2.0 <2.0 2-Butanone (MEK) 02/15/22 4 --- ND ND ND ND --- NC21- = 4,000 pg/L 10/05/22 4.0 5.1 11.4 7.7 <5.0 <5.0 <5.0 2-Hexanone 02/15/22 0.48 --- ND ND ND ND --- NC21- = 40 Ng/L 10/05/22 0.48 <5.0 <5.0 0.71 J <5.0 <5.0 <5.0 Chloromethane 02/15/22 0.54 --- ND ND ND ND --- NC21- = 3 Ng/L 10/05/22 0.86 <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 cis-1,2-Dichloroethene 08/18/15 5 0.71 J 0.36 J ND ND ND ND 02/18/16 5 ND ND ND ND ND ND NC21- = 70 ug/L 08/11/16 5 ND ND ND ND ND ND 02/14/17 0.19 ND ND ND ND ND ND 08/23/17 0.19 ND ND ND ND ND ND 02/06/18 0.19 ND ND ND ND ND ND 08/16/18 0.19 ND ND ND ND NM ND 02/05/19 0.29 ND ND ND ND ND ND 08/08/19 0.29 ND ND ND ND ND ND 02/14/20 0.29 ND ND ND ND ND ND 08/26/20 0.29 ND ND ND ND ND ND 02/10/21 0.29 --- ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.38 ND ND ND ND ND --- 10/05/22 0.38 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Methylene Chloride 02/14/17 0.97 ND ND ND ND ND ND 08/23/17 0.97 ND ND ND ND ND ND NC21- = 5 pg/L 02/06/18 --- 0 ND ND ND ND ND 08/16/18 0.97 ND 0 ND ND ND ND 02/05/19 3.7 ND ND 0 ND ND ND 08/08/19 3.7 ND ND ND ND ND ND 02/14/20 3.7 ND ND ND ND ND ND 08/26/20 3.7 ND ND ND ND ND ND 02/10/21 3.7 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 2 ND ND ND ND ND --- 10/05/22 2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Sulfate 08/26/20 500 53300 --- --- --- --- -- 02/10/21 500 65000 --- --- --- --- 24900 NC21- = 250,000 ug/L 08/17/21 --- NA NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- I NA NA NA NA NA NA Appendix D (Page 5 of6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Trichlorofluoromethane 06/13/12 --- ND ND ND ND 0.78 B 0.85 B 08/22/12 --- ND ND ND ND ND ND NC2L = 2,000 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND ND ND ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 --- ND ND ND ND ND ND 03/12/15 0.2 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 0.2 ND ND ND ND ND ND 08/11/16 0.2 ND ND ND ND ND ND 02/14/17 0.2 ND ND ND ND ND ND 08/23/17 0.2 ND ND ND ND ND ND 02/06/18 --- ND ND ND ND ND ND 08/16/18 0.2 ND ND ND ND NM ND 02/05/19 0.31 ND ND ND ND ND ND 08/08/19 0.31 ND ND ND ND ND ND 02/14/20 0.31 ND ND ND ND ND ND 08/26/20 0.31 ND ND ND ND ND ND 02/10/21 0.31 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.3 ND ND ND ND ND --- 10/05/22 0.30 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Notes: Analytical results from September June 2012 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. The March 19, 2020 sampling event was a resampling event for MW-7, MW-10, and MW-11; however, it was the initial 2020 semiannual sampling event for NES-2S. NC 2L Standards are the Title 15A NCAC 02L.0202 Groundwater Standards dated April 1, 2022. Bold concentrations exceed the NC2L Standard for groundwater. Detections of cis- 1,2-dichloroethylene in MW-7 and MW-8 in August 2015 are suspect. Results for the Unit 1 MW-7 sample, collected in concurrence with the Unit 2 sample, was reported as non -detect for cis-1,2-dichloroethylene. NES-2S 8/17/21 sample data shown in table collected on 8/18/21. NES-2S and MW-7 09/29/2022 sample data show in in table collected on 10/05/2022. All concentrations are in micrograms per liter (Ng/L). ND = not detected; RL = reporting limit; NM = not measured; NS = not samples; NE = not established; --- = data not available/not reported; B = blank -qualified data, result is expected to be biased high based on concentrations in the blank; NA = not analyzed/not available; J = Estimated value between the MDL and the MRL; MDL = laboratory method detection limit; MRL = laboratory method reporting limit. Appendix D (Page 6 of6) https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, Pl.l Appendix E Summary of Historical Constituents in Surface Water 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Inorganics Arsenic 03/12/15 2.5 ND ND 08/19/15 2.5 ND ND NC2B 340 pq/L 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 02/14/17 5 ND ND 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND 6.1 J 08/08/19 4.7 ND ND 02/14/20 4.7 ND ND 08/26/20 4.7 ND 7.2 J 02/10/21 4.7 4.7 J Dry 08/17/21 --- ND ND 02/15/22 4.7 ND ND 10/05/22 0.087 0.28 J 1.2 Barium 08/13/14 5 22.1 J 33.9 J 03/12/15 2.5 22.5 J 24.6 J ISTV �3)= 21,000 pg/L 08/19/15 2.5 23.9 J 32.7 J 02/18/16 2.5 22 J 26.3 J 08/11/16 2.5 23.4 J 26.5 J 02/14/17 2.5 18.6 J 21.4 J 08/23/17 2.5 32.3 J 33.3 J 02/06/18 2.5 23.7 J 32.3 J 08/16/18 2.5 24.2 J 38.2 J 02/05/19 2.5 22.9 23.1 08/08/19 1 23.3 44.5 02/14/20 1 26.5 29.3 08/26/20 3.5 21.2 47.5 02/10/21 3.5 18.8 DRY 08/17/21 --- 19.9 28.5 02/15/22 3.5 16.6 29.7 10/05/22 0.21 19.5 40.8 Beryllium 08/11/16 0.5 ND ND 02/14/17 0.5 ND ND NC2B 65 pq/L 08/23/17 0.5 ND ND 02/06/18 0.5 ND ND 08/16/18 0.5 ND ND 02/05/19 0.5 ND ND 08/08/19 0.2 ND ND 02/14/20 0.2 ND ND 08/26/20 0.7 ND ND 02/10/21 0.7 ND DRY 08/17/21 --- ND ND 02/15/22 0.7 ND ND 10/05/22 0.050 <0.10 0.10 Chromium 08/13/14 5 ND ND 03/12/15 2.5 ND 2.6 J NC2B SW-3 (4) = 109.85 pg/L 08/19/15 2.5 ND ND NC2B SW-4 (4) = 213.71 pg/L 02/18/16 2.5 ND ND 08/11/16 2.5 5.2 J ND 9/13/16(5) 2.5 NS NS 02/14/17 2.5 3 J ND 08/23/17 2.5 ND ND 02/06/18 2.5 ND 2.7 J 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1 ND 2.2 J 02/14/20 1 2.6 J 3.1 J 08/26/20 3.7 ND 9.8 02/10/21 3.7 ND DRY 08/17/21 --- ND ND 02/15/22 3.7 ND ND 10/05/22 0.50 0.91 J 5.0 Cobalt 08/11/16 2.5 ND ND 02/14/17 2.5 ND ND ISTV (3) = 16 pq/L 08/23/17 2.5 ND ND 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1.1 ND 2.9 J 02/14/20 1.1 ND ND 08/26/20 3.6 ND ND 02/10/21 3.6 ND DRY 08/17/21 --- ND ND 02/15/22 3.6 ND ND 10/05/22 1 0.050 1 0.27 J 2.1 Appendix E (Page 1 of 3) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, PC Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Copper 08/13/14 5 ND ND 03/12/15 2.5 ND ND NC21B SW-314) = 2.02 pg/L 08/19/15 2.5 ND ND NC21B SW-4 (4) = 4.35 pg/L 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 9/13/16(5� 2.5 NS NS 02/14/17 2.5 ND ND 08/23/17 2.5 ND ND 02/06/18 2.5 2.7 J 3.6 J 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 2.1 2.7 J 2.7 J 02/14/20 2.1 2.8 J 2.9 J 08/26/20 4.3 ND 8.1 02/10/21 4.3 ND DRY 08/17/21 --- ND ND 02/15/22 4.3 ND ND 10/05/22 1.1 <2.0 5.1 Hardness, Total (SM 23408) 02/05/19 662 13800 17400 08/08/19 131 17400 28200 NC26 ��� = NE 02/14/20 131 10800 12300 08/26/20 131 14900 34900 02/10/21 131 --- DRY 08/17/21 --- 16500 28900 02/15/22 --- NA NA 10/05/22 541 13400 30200 Iron 02/06/18 25 1520 2920 08/16/18 25 --- --- NRWQC 12) = 1,000 uq/L 02/05/19 25 --- --- 02/14/20 19.5 --- --- 02/10/21 41.5 --- DRY 08/17/21 --- NA NA 02/15/22 --- NA NA 10/05/22 --- NA NA Lead 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 9/13/16") 2.5 NS NS 02/14/17 2.5 ND ND NC21B SW-3 (4) = 6.85 pg/L 08/23/17 2.5 ND ND NC21B SW-4 (4) = 17.17 pg/L 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1.6 ND 1.6 J 02/14/20 1.6 ND ND 08/26/20 4.5 ND ND 02/10/21 4.5 ND DRY 08/17/21 --- ND ND 02/15/22 4.5 ND ND 10/05/22 0.077 0.42 J 1.6 Manganese 02/06/18 2.5 11.6 J 25.8 J 08/16/18 2.5 --- --- NRWQC (21 = 100 pq/L 02/05/19 2.5 --- --- 02/14/20 0.9 --- --- 02/10/21 3.4 --- DRY 08/17/21 --- NA NA 02/15/22 --- NA NA 10/05/22 --- NA NA Nickel 08/13/14 5 ND ND 03/12/15 2.5 ND ND NC21B SW-3 (4) = 85.51 pg/L 08/19/15 2.5 ND ND NC21B SW-4 (4) = 170.04 pg/L 02/18/16 2.5 ND ND 08/11/16 2.5 2.8 J ND 02/14/17 2.5 ND ND 08/23/17 2.5 ND ND 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 0.9 ND 1.9 J 02/14/20 0.9 1.2 J 1.3 J 08/26/20 3.5 ND 4.3 J 02/10/21 3.5 ND DRY 08/17/21 --- ND ND 02/15/22 3.5 ND ND 10/05/22 0.42 <1.0 2.5 Selenium 08/11/16 5 ND ND 02/14/17 5 ND ND NC26 ��� = 5 pq/L 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND ND 08/08/19 4.7 ND ND 02/14/20 4.7 ND ND 08/26/20 4.7 ND ND 02/10/21 4.7 ND DRY 08/17/21 --- ND ND 02/15/22 4.7 ND ND 10/05/22 0.072 <2.0 0.26 J Appendix E (Page 2 of 3) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, PC Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Vanadium 08/13/14 5 ND 9.3 J 03/12/15 2.5 3.1 J 6.3 J NC2B �'� = NE 08/19/15 2.5 2.7 J 4.3 J 02/18/16 2.5 ND ND 08/11/16 2.5 ND 2.7 J 02/14/17 2.5 ND ND 08/23/17 2.5 4.6 J ND 02/06/18 2.5 4.3 J 8.2 J 08/16/18 2.5 3.7 J ND 02/05/19 2.5 ND ND 08/08/19 1.3 3.3 J 7.9 02/14/20 1.3 3.8 J 6.1 08/26/20 3.9 ND 24.3 02/10/21 3.9 ND DRY 08/17/21 --- ND ND 02/15/22 3.9 ND ND 10/05/22 0.25 2.1 14.2 Zinc 08/13/14 5 ND ND 03/12/15 5 8.5 B 10.8 B NC213 SW-3 (4) = 21.34 pg/L 08/19/15 5 ND ND NC26 SW-4 (4) = 42.49 pg/L 02/18/16 5 ND ND 08/11/16 5 13 5.6 J 9/13/16(5) 5 --- --- 02/14/17 5 7 J ND 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND ND 08/08/19 3.9 ND 7.2 J 02/14/20 3.9 4 J 4.7 J 08/26/20 9.5 ND 11.3 02/10/21 9.5 ND DRY 08/17/21 --- ND ND 02/15/22 9.5 ND ND 10/05/22 1 2.7 1 <10.0 1 9.8 J Organics 1,4-Dioxane 08/16/18 1.9 ND ND 02/05/19 1.9 ND ND ISTVI"= 80 pg/L 08/08/19 1.2 ND ND 02/14/20 1.2 ND ND 08/26/20 1.2 ND ND 02/10/21 1.2 ND DRY 08/17/21 --- ND ND 02/15/22 0.86 ND ND 10/05/22 0.86 <2.0 <2.0 2-Hexanone 08/11/16 0.46 ND ND 02/14/17 0.46 ND ND NC213 ��� = NE 08/23/17 0.46 ND ND 02/06/18 0.46 ND ND 08/16/18 0.46 ND ND 02/05/19 0.57 ND ND 08/08/19 0.57 ND ND 02/14/20 0.57 ND ND 08/26/20 0.57 ND ND 02/10/21 0.57 ND DRY 08/17/21 --- --- --- 02/15/22 0.48 ND ND 10/05/22 0.48 <5.0 <5.0 Methylene Chloride 08/26/20 3.7 --- 8.2 02/10/21 3.7 ND DRY ISTV (2) = 11,000 uq/L 08/17/21 --- ND ND 02/15/22 2.0 ND ND 10/05/22 2.0 <5.0 <5.0 Toluene 08/26/20 0.24 ND 0.33 J 02/10/21 0.24 ND DRY NC213 ��� = 11 pq/L 08/17/21 --- ND ND 02/15/22 0.48 ND ND 10/05/22 1 0.48 1 <1.0 I <1.0 Notes: 1. 15A NCAC 213 Water Quality Standards (213 Standards) for Surface Water (Class C) dated July 26, 2021. 2. No 213 Standard established, value shown is EPA Nationally Recommended Water Quality Criteria (NRWQC) for Aquatic Life & Human Health. 3. No 213 Standard or NWQC established, value shown is North Carolina In -Stream Target Values for Surface Waters (ISTV). 4. NC 213 Standards for hardness -dependent metals calculated using total hardness values obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - October 2022 Event (SW-3 = 13,400 ug/L; SW-4 = 30,200 ug/L). 5. The 9/13/16 sampling event was a resampling event. Analytical results from November 1996 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. Bold concentrations exceed the NC 213 Standard or ISTV. All concentrations are in micrograms per liter (pg/L). J = Estimated concentration above the laboratory method detection limit and below the laboratory method reporting limit; B = blank -qualified data; result is expected to be biased high based on concentrations in the blanks. MRL = method reporting limit; MDL = laboratory detection limit; ND = Not detected above laboratory method reporting limit NE = Not established; --- = Not Sampled/ Data not available. DRY = Surface water point considered to be dry Data shown in parentheses indicate dissolved concentrations. Appendix E (Page 3 of 3) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 Second Half GWM/Tables/Oxford Unit 2 Historic Tables Hart & Hickman, PC