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Home My WebLink About7407_Pitt_C&DLandfillInc_CDLF_Phase1_Phase2_June2022GW_FID1756473_20221229DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D DENR USE ONLY ❑Paper Report [:]Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Smith Gardner, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Seth C. Rickerts, P.G. E-mail: Seth@smithgardnerinc.com Phone: 919-828-0577 x 135 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) C&D Disposal, Inc. 802 Recycling Lane. Greenville, NC 74-07 .0500 June 13-15 & 27-28, 2022 27834 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Seth C. Rickerts, P.G. Project Geologist 919-828-0577 x 135 Facility Representative Names(Prin) Title (Area Code) Telephone Number �Docu igned y. 12/29/2022 I Affix NC Licensed/ Professional Geologist Seal Signature 3BDate 8305C978EA4E6... 14 N. Boylan Ave. Raleigh, NC 27603 Facility Representative Address F-1370 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 \ ,`%"ll'i 3t/Jy11 �,,0, , "GENs fi C �- SEAL 12/�9/2022 2'758 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D June 2022 Groundwater Monitoring Report COD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-20016 7407- CDLF- 2009 Prepared for: CGD Disposal, Inc. 802 Recycling Lane Greenville, North Carolina 27834 December 2022 Prepared by: NCLIC.NO.F-13�0 (ENGINEERING) SMITH GARDNER 14 N. Boylan Avenue, Raleigh NC 27663 1919.828.057? O 2022 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D June 2022 Groundwater Monitoring Report COD Disposal, Inc. NC Solid Waste Permit 7407-CDLF-2001 O 7407- CDLF- 2009 Prepared For: COD Disposal, Inc. Greenville, North Carolina S+G Project No. EJERECYCLING-21-2 DocuSigned by: 5DD73DOAEAB2442... Daniel Pantaleo Environmental Technician DocuSigned by:: SC�A G. iZ1e", 3B83O5C978EA4E6... Seth C. Rickerts, P.G. Project Geologist December2022 c� S�cOY�y� SEAL 1242922022 2758 NC LIC.1\10113�0 (ENGINEERING) SMITH GARDNER 14 N. Boylan Avenue, Raleigh NC 27683 1919.828.05?? DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D CSD Disposal, Inc. NC Solid Waste Permit No. 7407- CDLF- 2001 & 7407- CDLF- 2009 June 2022 Groundwater Monitoring Report Table of Contents Page 1.0 INTRODUCTION...............................................................................................................1 2.0 SITE GEOLOGY.................................................................................................................1 3.0 SAMPLING LOCATIONS...................................................................................................1 4.0 SAMPLING PROCEDURES...............................................................................................2 5.0 FIELD & LABORATORY RESULTS....................................................................................2 5.1 Field Results........................................................................................................... 2 5.2 Laboratory Analysis................................................................................................ 2 5.3 Laboratory Results................................................................................................. 3 5.3.1 Inorganic Constituents................................................................................ 3 5.3.2 Organic Constituents.................................................................................. 4 5.3.3 Surface Water Results................................................................................ 4 6.0 GROUNDWATER CHARACTERIZATION............................................................................4 7.0 CONCLUSIONS................................................................................................................5 FIGURE Figure 1 Groundwater Potentiometric Map TABLES Table 1 Groundwater Elevation Table 2 Field Parameters Table 3 Monitoring Results Table 4 MNA Parameter Results Table 5 Velocity and Conductivity Data APPENDICES Appendix A Well Logs Appendix B Laboratory Analytical Report Appendix C Time Vs. Concentration Graphs CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Table of Contents Page i DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 1.0 INTRODUCTION C&D Disposal, Inc., located at 802 Recycling Lane, Greenville, North Carolina, operates a C&D Landfill under Solid Waste Permit #7407- CDLF- 2001 and #7407- CDLF- 2009. The site is currently required to submit semi-annual groundwater monitoring reports to NCDEQ. The facility contains two unlined construction & demolition (C&D) landfill units. Phase 2 is currently active. Phase 1 has ceased accepting waste and entered final closure in late 2022. The Facility was developed in two non-contiguous footprints, Phases 1 and 2 approximately midway between US 264, i.e., a localized topographic divide, and Grindle Creek. The phases became operational in May 2001 and August 2009, respectively. Phase 1 was the regional repository for flood -damage debris after Hurricane Floyd in 1999. Phase 2 was a staging area, where flood -debris was stored temporarily. Both areas were used for agriculture, and a former railroad corridor traverses the site, including the Phase 2 footprint. This report presents the results from the semi-annual monitoring event conducted June 13-15 and 27-28, 2022 and includes a field procedure summary, laboratory analyses, summary tables and groundwater characterization. 2.0 SITE GEOLOGY Historical literature and available geologic maps indicate that C&D Landfill, Inc. sits within the NC Coastal Plain. The coastal plain is characterized as an eastward thickening wedge of sedimentary layers that alternate between sandy aquifers and aquitard. Information taken from The Geologic Map of North Carolina, 1985 shows that the C&D landfill is underlain by the Yorktown Formation, which is described as "fossiliferous clay with varying amounts of fine-grained sand, silty sand, sandy silt, silty clay, and blueish gray shell material". Groundwater in the upper -most aquifer generally flows through unconsolidated sediments. Recharge occurs generally in the northern portion of the site and is limited on slopes. Groundwater flows generally south where it discharges into tributaries of Grindle Creek. The groundwater potentiometric surface generally reflects a subdued expression of the surface topography. Local conditions are considered typical for the coastal plain region. Ground water depths generally range from 3 ft to 12 ft below ground surface (bgs) across the facility. There are minor seasonal variations in the flow pattern, but overall flow direction is consistent. 3.0 SAMPLING LOCATIONS The groundwater monitoring network consists of eighteen shallow and four deep wells totaling (22) groundwater monitoring wells. MW-IS (upgradient of phase I); MW-1D, MW-2D, MW-2S, MW-3D, MW-3S and MW-3A, MW-4, MW-5, MW-6, MW-7, and MW-8 (downgradient of phase 1); MW-9A, MW-16, and MW-17 (upgradient of phase 11); MW-10, MW-11, MW-12S, MW-13, MW-14D, MW-14S, and MW-15 (downgradient of phase II); the network also includes four surface water CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Page 1 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D locations (SW-1, SW-2, SW-3, and SW-4). It should be noted that SW-1 and SW-2 were unable to be sampled by Environment 1 personnel this event. Figure 1 illustrates all sampling locations. Available well logs for the groundwater monitoring wells are included in Appendix A. 4.0 SAMPLING PROCEDURES Environment 1 personnel performed the monitoring event across two mobilizations, June 13-15. 2022 and June 27-28, 2022. Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (DENR, DWM) and the approved site Water Quality Monitoring Plan'. The monitoring network includes wells: MW-IS, MW-ID, MW-2S, MW-2D, MW-3A, MW-3S, MW-3D, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-14D, MW-15, MW-16 and MW-17, aswell as surface water monitoring points SW-1 through SW-4. Monitoring wells MW-1S and MW-1D serve as the upgradient background locations for the site. Each well was gauged to determine groundwater depth and then purged three well volumes or until dry. Groundwater depths from this event, as well as other well details are presented in Table 1. Samples were collected by Environment 1, Inc. in laboratory prepared containers for the specified analytical procedures. Groundwater samples and quality control blanks, were properly preserved, placed on ice and transported to the laboratory facility within the specified hold times for each analysis. 5.0 FIELD B LABORATORY RESULTS 5.1 Field Results Temperature, pH, turbidity, specific conductance, ORP, and dissolved oxygen were measured in the field at the time of sampling via direct read instruments. Field results from this sampling event are presented in Table 2. All monitoring well locations exhibited turbidities less than 10 NTUs during this event. 5.2 Laboratory Analysis Ground and surface water samples were transported to Environment 1, Inc., a North Carolina certified laboratory for Appendix II metals and VOC analysis. Samples were also analyzed for additional C&D parameters, alkalinity, sulfide, chloride, total dissolved solids and tetrahydrofuran. The laboratory report including the full list of analytes is presented as Appendix B. 1 Water Quality Monitoring Plan Amendment, C&D Landfill, Inc., CDLF (Phases 1 and 2) prepared for C&D Landfill, Inc., by David Garrett and Associates, Revised May 2008. CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Page 2 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 5.3 Laboratory Results Analytical results were compared to Rule 15A NCAC 2L.0200 (21- Standard) and/or the NC Groundwater Interim Maximum Allowable Concentration. Surface water results were compared with the NCAC 2B Standard for Class C waters (213 Standards). Most constituent concentrations were either below the method detection limit (MDL) or were reported as "J-values". J-values are identified by the laboratory as "estimated values between the MDL and the MRL". 5.3.1 Inorganic Constituents Seven inorganic constituents were reported at concentrations above their 2L Standard this event. • Arsenic (MW-2S, MW-3A, MW-3S, MW-5, MW-7, MW-8, MW-12S, MW-14S, and MW-16); • Barium (MW-3S); • Chromium (MW-2S, MW-3A, MW-3S, MW-5, MW-7, MW-8, MW-10, MW- 12S, MW-14S, and MW-16) • Cobalt (MW-2, MW-3A, MW-3S, MW-5, MW-6, MW-7, MW-8, MW-10, MW- 11, MW-12S, MW-13, and MW-14S); • Iron (MW-1D, MW-IS, MW-2D, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW- 6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW- 15, MW-16, and MW-17); • Manganese (MW-1 D, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-15, MW- 16, and MW-17); and • Vanadium (MW-3S, MW-5, MW-10, MW-12S, MW-14S and MW-16). As MW-IS and MW-1D are upgradient of Phase 1 and MW-17 is upgradient of Phase 2, exceedances in these wells indicate that detected constituents may be due to naturally occurring conditions. Detections are summarized in Table 3. CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Page 3 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 5.3.2 OrOanic Constituents Five organic constituents were detected above their 2L Standards during this sampling event. Detections are summarized in Table 3. • 1,2-Dibromoethane (MW-12S); • 1,4-Dioxane (MW-IS, MW-2S, MW-3A, MW-3S, MW-5, MW-6, MW-7, MW- 8, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-15, and MW-16); • Benzene (MW-10, MW-12S, and MW-14S); • Naphthalene (MW-3S); and • Vinyl Chloride (MW-10, MW-12S, MW-13 and MW-14S). 5.3.3 Surface Water Results One inorganic constituent was detected above the NC213 standards in surface water samples during this event. • Copper (SW-3 and SW-4). No organic constituents were detected above their NC2B standards in surface water samples collected this event. Surface water detections are provided on Table 3. 6.0 GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater data from the most recent sampling event. The data indicates that groundwater is flowing generally south towards tributaries of Grindle Creek. This is consistent with groundwater flow patterns previously reported for the site. The potentiometric surface map is included as Figure 1. Groundwater flow velocities during the sampling event were calculated using the equation: V = Ki/n where: K = hydraulic conductivity i = groundwater gradient n = porosity Calculated groundwater velocities ranged from 0.00053 ft/day (MW-11) to 0.02320 ft/day (MW- 10) averaging 0.02071 ft/day. Flow velocities and calculated gradients are included in Table 5. CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Page 4 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 7.0 CONCLUSIONS Analytical results are generally consistent with past sampling events. Iron and manganese were detected in most samples collected this event, including in background wells above their respective NC21- and NCGWP standards. Due to the low turbidity values, and the exceedances noted in upgradient wells, it is likely that some of these inorganic exceedances can be attributed to metals in the soil naturally occurring at concentrations greater than their pertinent groundwater standards. 1,4-Dioxane, benzene, and vinyl chloride were detected again in multiple monitoring wells above their NC21- standards this sampling event. Although not exceeding regulatory limits, 1,2- Dichloroethane and 1,2-cis-Dichloroethylene were present in multiple wells this event. The continued presence of these organochlorides as well as vinyl chloride provide some evidence that reductive dichlorination via natural attenuation may be occurring onsite. The exceedance of the hydrocarbon naphthalene was seen for the first time during the fall 2021 event and has occurred again during this event in monitoring well MW-3S. Naphthalene was also present in MW-2S, MW- 3A, MW-6, MW-10, and MW-12S as J-tagged values during this event. This will be closely monitored during the next sampling event. A Corrective Action Plan to address organic exceedances was submitted to the NCDEQ and accepted August 16, 2022. This plan included an evaluation of natural attenuation that indicated that natural attenuation is occurring at the site along with landfill capping. This corrective action plan is currently being implemented and a corrective action effectiveness report will be submitted under a separate letter every five years with the first being submitted in Fall 2025. The next groundwater monitoring event is scheduled for Fall 2022. A report with laboratory analysis will be submitted to NCDEQ in accordance with 15A NCAC 13B .0544. 2 Re: Groundwater Corrective Action Plan, C&D Landfill, Inc. From Ms. Jaclynn Drummond to Mr. Judson Whitehurst, August 16, 2022 CSD Disposal, Inc. June 2022 Groundwater Monitoring Report December 2022 Page 5 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D FIGURES June 2022 Groundwater Monitoring Report EBB Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 4 MW-17= TOC= 20.74 DTW= 8.98 GWE= 11.76 �MW-16 TOC= 19.16 DTW= 8.13 A91GWE= LEGEND NOTES EXISTING 10' CONTOUR 1. GROUNDWATER DATA COLLECTED BY ENVIRONMENT 1, INC. z 950- (SEE REFERENCE 2) JUNE 2022. w m �' MW-9A EXISTING 2' CONTOUR TOC- 20.58 (SEE REFERENCE 2) REFERENCES o o DTW= 7.9 APPROXIMATE PROPERTY LINE 1. PARCEL BOUNDARIES FROM PITT COUNTY GIS DEPARTMENT. J 0 GWE= 12.68 - - (SEE REFERENCE i) 2. FLOOD HAZARD INFORMATION FROM NORTH CAROLINA FLOODPLAIN z MAPPING PROGRAM, FEMA FIRM MAP NO. 3720562800L, EFFECTIVE FLOOD HAZARD AREAS ZONE AE DATE JUNE 19, 2020. (SEE REFERENCE 3) 3. AERIAL IMAGERY DATED 2016 FROM PITT COUNTY GIS DEPARTMENT p R< APPROXIMATE GROUNDWATER SURFACE CONTOUR 0 200' 400' N o . . SW-1 SURFACEW,4TER MONITORING a LOCATION o N - MW_8* INDICATES ELEVATION NOT USED FOR CONTOURING --- �` M W-1 A GROUNDWATER MONITORING WELL N - Y TOC TOP OF CASING ELEVATION m DTW DEPTH TO WATER o C� z OWE GROUNDWATER ELEVA77ON F a ID4. 0 MW-15 T61rD MW-1 D*TOC= 19.67 81C= 21.14DTW= 7.53 .1 - ��,' G80W= 9.53 GWE= 22.14 :�, E= 11.61 IMW-14Si TOC= 16.60. DTW= 6.1 GWE= 10.50 Ar R 3 nF `� MW-1S TOC= 20.91 DTW= 9.35 GWE= 11.56E "�► MW-11 TOC= 14.49 MW-14D* DTW= 4.82 TOC= 17.45 GWE= 9.67 DTW= 7.21 GWE= 10.24 MW-4 TOC=18.42 DTW= 7.64 GWE= 10.78 SW-1 MW-7 / )C= 19.40 fW= 9.2 NE= 10.20 MW-8* TOC= 21.21 DTW= 10.27 r� GWE= 10.94 MW-13 MW-12S MW-3S MW-6 TOC= 20.69 TOC= 16.18 TOC= 23.02 TOC= 20.03 DTW= 10.54 DTW= 5.35 DTW= 12.8 DTW= 10.23 ' GWE= 10.15 GWE= 10.83 ' GWE= 10.22" GWE= 9.80 P, �r I SW-3 _ MW-5 _ - "MW-3D* r. TOC= 22.83, MW-3 MW-2D* MW-2S SW-2 DTW= 13.97 TOC= 21.93 - - - TOC= 21.80 / TOC= 21.44 GWE= 8.86 DTW= 12.00 DTW= 13.47- - DTW= 11.6.65 GWE= 9.93 /GWE= 8.33 GWE= 9.79 1�) co M 0 m w w a w z z W o (n N Q N w Z w U W o N N O N C) 0 Ci a c� C-i W z C- z O N J J Z N ... N O C . . z z CL z J W Cr o � C" CM Q c- O z O CM 22 Smith Gardn , Inc. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This Page Intentionally Left Blank DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D TABLES June 2022 Groundwater Monitoring Report CRD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D SMITH GARDNER .• - C.; •No V . I D. . Well Well Installation Date Well Diameter (inches) Total Well Depth (ft bgs) Ground Surface Elevation (ft amsl TOC Elevation (ft amsl) Depth toElevation Water (ft) Water Table (ft bgs) Screen Interval (feet bgs) M W-1 D 10/ 13/ 2000 2 33.75 17.4 1 21.14 9.53 11.61 40- 50 MW-1 S 5/2/2001 2 17.21 17.59 20.91 9.35 11.56 3-13 MW-2D 10/11/2000 2 38.17 17.97 21.8 13.47 8.33 39-49 MW-2S 5/3/2001 2 16.57 18.45 21.44 11.65 9.79 3-13 M W- 3A 8/ 10/ 2009 2 23.44 19.13 21.93 12 9.93 5- 20 MW-3D 10/13/2000 2 52.3 19.37 22.83 13.97 8.86 40-50 MW-3S 8/6/2007 2 22.24 19.37 23.02 12.8 10.22 8-18 M W- 4 5/3/2001 2 15.98 14.83 18.42 7.64 10.78 3-13 M W- 5 11 / 19/ 2002 2 9.5 14.8 17.9 7.1 10.80 3-18 MW-6 5/3/2001 2 16.65 16.87 20.03 10.23 9.80 3-13 M W- 7 5/3/2001 2 16.33 16.03 19.4 9.2 10.20 3-13 MW-8 11/5/2002 2 20.26 18.3 21.21 10.27 10.94 3-18 M W- 9A 8/ 7/ 2009 2 23.17 17.64 20.58 7.9 12.68 5- 20 M W-10 8/ 6/ 2009 2 22.73 14.16 16.61 4.81 11.80 5- 20 MW-11 8/6/2009 2 23.84 11.60 14.49 4.82 9.67 5-20 MW-12S 8/7/2009 2 22.93 1 13.72 16.18 5.35 10.83 5-20 M W-13 8/ 7/ 2009 2 20.68 18.12 20.69 10.54 10.15 5- 20 MW-14D 12/17/2002 2 41.92 14.54 17.45 7.21 10.24 35-40 M W-14S 12/ 18/ 2002 2 23.12 13.9 16.6 6.1 10.50 5- 20 M W-15 12/ 18/ 2002 2 22.14 13.9 19.67 7.53 12.14 5- 20 MW-16 6/16/2017 2 22.73 NA 19.16 8.13 11.03 NA M W-17 12/ 9/ 2002 2 22.25 18.18 20.74 8.98 11.76 5- 20 Note: 1. Well installation, depth, elevations, and screened interval from David Garrett Boring Logs E�. D.F D#e 1f 3012OZ MRgectAGardAdEr itairrr,2GarrindErK/tntainglpats\EEydirrj5.Jm2C2$irU2022EEb-)dirUTdJEs)dEx DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D SMITH GARDNER Ffdd Pawdas W. D.F DAe 1N301M Well ID pH (SU) Temperature (OCelsius) Specific Conductivity (uMhos/cm) Dissolved Oxygen ORP (mv) Turbidity (NTU) M W-1 D 7.3 23 384 1 50 7.04 M W-1 S 6.2 23 1481 1.89 100 7.72 MW-2D 7.4 24 460 1.01 85 6.41 M W- 2S 6.7 22 2916 1.55 120 6.06 M W- 3A 6.8 20 3190 1.44 166 4.68 MW-3D 7.6 21 533 1.97 126 - M W- 3S 6.8 22 3678 0.52 157 5.22 MW-4 6.1 21 437 1.89 59 9.54 M W- 5 6.9 26 1370 4.6 - - MW-6 6.9 22 1786 3.55 60 9.73 M W- 7 6.7 25 1850 2.1 82 8.72 MW-8 6.8 22 3592 2.48 163 8.69 M W- 9A 6.9 21 660 1.03 127 6.23 MW-10 6.5 21 2094 1.36 132 6.03 M W-11 6.9 24 1352 3.23 92 7.67 MW-12S 6.7 25 3590 2.21 158 4.62 MW-13 6.2 23 1648 1.74 130 8.22 MW-14D 7.4 25 524 2.23 123 1.19 MW-14S 6.6 26 2711 1.36 147 8.38 MW-15 5.6 23 1095 1.04 -3 7.74 M W-16 6.4 29 1714 2.16 120 4.36 M W-17 6 24 610 1.26 113 3.74 SW-1 - - - - - - SW-2 - - - - - - SW- 3 7.2 23 1150 1.86 118 59.8 SW-4 7.5 29 816 1.59 92 40.9 Note: 1. Field Parameters measured by Environment 1 on June 13-15, 27-28, 2022 2. Bold indicates a turbidity exceeding 10 NTU. 3. SW-1, and SW-2 were unable to be sampled this event. [tTTi711��"{iilP�f�ZtT.T Dili 11[�� •i �e C:u� \�.:CTIi��.�.Ti=fa//�[.0 �e :I►Iag:CTllii7CiC�!�!i DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D SMITH GARDNER Tafie3 Y= DteWl9"elY Mtitoirgl�nJfs EERxjdirgl-sill JmI13-11527-4M Monitoring Results Station Name Units NC2L NC7B NC2B-P MW-1D MW-1S MW-2D MW-2S MW-3A MW-3D MW-3S Sample Date 6/13/2022 6/13/2022 6/13/2022 6/13/2022 6/14/2022 6/14/2022 6/14/2022 Furans Tetrahydrofuran ug/1 NE NE NE 7.21 1.54 28.9 25.2 32.4 Metals Antimony ug/1 1 NE 5300 0.08 J 0.59 J 0.14 J 0.14 J 0.22 J 0.09 J 0.16 J Arsenic ug/1 10 150 NE 1.9 J 0.94 J 1.11 14 28 0.34 J 22 Barium ug/1 700 NE 21000 30 153 1 15.8 394 549 1 10.6 774 Ber lium ug/1 4 6.5 NE 0.02J 0.06J 0.02J 0.04J 0.04J Cadmium ug/1 2 8.8 NE 0.081 0.28J Chromium ug/I 10 NE NE 0.5 J 1.9 J 0.2 J 12 19 22 Cobalt ug/1 1 NE 4 0.09 J 0.22 J 0.05 J 2.3 6.4 BUL 3.9 Copper ug/I 1000 3.1 NE 0.68J 3J 0.151 0.45J 0.74J 0.08J 0.2J Iron ug/1 300 NE NE 3887 457 1384 14074 18940 101 24921 Lead ug/I 15 25 NE 0.24 J 0.82 J 0.111 0.12 J 0.16 J BDL 0.111 Manganese ug/1 50 NE NE 70 35 43 892 732 0.31 J 1476 Nickel ug/I 100 88 NE 0.52J 1.8J 0.15J 2.2J 3.8J 0.34J 4.1J Selenium ug/1 20 5 NE 0.21 J 0.82 J BF11 0.84 J 11 0.2 J 0.99 J Thallium ug/1 2 0.47 NE 0.11J 0.21J 0.02J 0.051 0.02J Tin ug/1 2000 NE NE BDL BDI ;DL BDL Vanadium ug/1 7 NE NE 0.68 J 3 0.22 J 6 7 0.36 J 8 Zinc ug/1 1000 81 1 NE 3.3J 3.8J 3.3J 2.3J 1.6J 19 2.8J Nutrients IN Nitrite (as N) mg/1 NE NE NE 4.37 0.22 0.16 0.19 0.37 Organics 1,1,2,2-Tetrachloroethane ug/1 0.2 NE NE 0.08 J 0.06 J 0.06 J 1,2-cis-Dichloroethylene ug/1 70 NE NE 1,2-Dibromoethane ug/1 0.02 NE NE 1,2-Dichloroethane ug/1 0.4 NE NE 0.06J 0.04J 0.091 1,2-Dichloropropane ug/1 0.6 NE NE BDL 0.06J 1,4-Dioxane ug/I 3 NE NE 35.3 67.6 82 118 Acenaphthene ug/1 80 NE NE 6.49 J BI Acetone ug/1 6000 NE NE BDL 11.5 J Alkalinity,Total (as CaCO3) mg/1 NE NE NE 755 232 900 1010 6100 226 1460 Benzene u /1 1 NE NE BDL BDI BDL 0.36J 0.881 BDL 2.3 Carbon Disulfide ug/I 700 NE NE BDL BDI BDL BDI BDL 'DL Chloride mg/1 NE NE NE 15 104 13 136 198 22 214 Ethylbenzene ug/I 600 NE NE )L BDL SDL BD BDL DL BDL Naphthalene ug/1 6 NE NE t BDL BDL 2.65 J 0.92 J t " 7 Sulfate mg/1 NE NE NE BL 383 26.2 360 134 B- 11.3 Toluene ug/1 600 NE NE BDL BDL '3DL BDL 0.31 J Total Dissolved Solids mg/1 NE NE NE 210 1133 270 1900 320 1900 Vinyl chloride ug/1 0.03 NE NE BDL BDL OL BDL BDL Xylenes ug/1 500 NE NE BDL BDL SDL BDL BDL NOTES: ug/L=micrograms per liter BOLD= Const it uent exceeds NCACO2L or OVVP regulatory limits BOLD =Constituent exceeds NCA002B or 2B Protection regulatory limits J =Lab estimated concentration BDL = constituent is bel m I aboratory detection I im its NA=Not Analyzed MRge}d.Qt bAcerKbitmr62QnrdAdaMitairgP4its1EHljdirj.5Jire2 2,%nrgMEB§.dirgTsUeAs, DocuSign Envelope ID: 3C8509C9-30CA-4C23-661B-5E8AB648F13D SMITH GARDNER TEde3 MtitairgFffitJts EERx)dirgL-A-dll Jlxet-11527-4M Monitorina Results Station Name Units NC2L NL2B NC2B-P MW-4 MW-5 MW-6 MW-7 MW-8 MW-9A MW-10 MW-11 MW-12S MW-13 MW-14D MW-14S MW-15 MW-16 MW-17 SW-3 SW-4 Sample Date 6/15/2022 6/15/2022 6/15/2022 6/15/2022 6/15/2022 6/27/2022 6/27/2022 6/27/2022 6/27/2022 6/27/2022 6/28/2022 6/28/2022 6/28/2022 6/28/2022 6/28/2022 6/16/2022 6/16/2022 Furans Tetrahydrofuran ug/l NE NE NE 8.17 7.65 8.67 19.9 27.7 44 48.3 12.1 31.9 3.32 1.85 Metals Antimony ug/l 1 NE 5300 0.11 0.4 J 0.06 J 0.08 J 0.12 J 0.04 J 0.111 0.38 J 0.25 J 0.19 J 0.25 J 0.46 J 0.22 J 0.81 J 2.3 Arsenic u /I 10 150 NE 0.75 J 24 9 19 27 0.28 J 10 1 6.7 45 5 0.43 J 20 5.6 13 0.85 J 5.6 2.6 J Barium ug/l 700 NE 1 21000 59.6 276 1 487 564 572 1 61.2 339 97.2 525 246 1 8.9J 348 260 460 70.5 1 124 60.7 Beryllium ug/I 4 6.5 NE 0.09 J 0.41 J 0.02 J 0.04 J 0.02 J 0.02 J 0.09 J 0.06 J 0.04 J 0.04 J 0.04 J 0.12 J 0.05 J 0.05 J 0.24 J 0.39 J Cadmium u /I 2 8.8 NE BDL 0.31 J BDL BDI BDL DL 0.14 J 0.05 J BDL 0.3 J 0.65 J Chromium u /I 10 NE NE 1.91 19 7.8 11 24 0.2J 36 4.7J 52 4.4J 25 5.5 17 2.1J 3.2J 2.4J Cobalt u /I 1 NE 4 0.15J 4.1 2 14 2.6 0.14J 2.5 1.1 3.8 2.6 BUL 1.8 0.72J 0.76J 0.091 1.7 1 Copper u/ I 1000 3.1 N E 0.191 8 J 0.44 J 0.35 J 0.15 J 0.12 J 0.191 0.06 J 0.05 J 11 0.28 J 0.21 J 2 J 0.94 J 0.62 J 16 13 Iron ug/I 300 NE NE 3473 50590 14443 45321 38181 4135 311 11478 2079 9327 22J 1930 2111 36106 1169 BE, BDL Lead ug/I 15 25 NE 0.3J 6.7 0.151 0.08J 0.05J 0.05J 0.191 0.08J 0.05J 0.54J 0.05J 0.19J 1.3J 0.75J 0.2J 3.6J 3.6J Man anese ug/l 50 NE NE 54 376 1 742 806 911 230 226 326 633 308 11 691 212 477 169 1 BD BDL Nickel ug/I 100 88 NE 0.26J 9.91 1.6J 1.91 1.8J 0.15J 3.4J 1.5J 3.6J 4.1 J 0.14J 2.4J 1.5J 2J 0.26J 1.11 1.8J Selenium ug/l 20 5 NE 0.49J 0.54J 3DL BDL BDL BDL 1.91 0.76J 2J 2.4J - 1.11 1.7J 1.8J 0.35J 0.91 0.21 J Thallium ug/I 2 0.47 NE 0.14J 0.12J BDL 0.04J BDL 0.16J 0.29J 0.1 J 0.04J 0.111 0.02J 0.24J 0.08J 0.11 0.06J Tin ug/l 2000 NE NE BDL 275 0.111 BDL 0.28J BDL 3J 0.39J 0.14J 0.08J 0.3J 12.2J BDI BD BDL Vanadium ug/I 7 NE NE 3 28 7 2 4 0.2J 14 4 36 6 0.34J 10 6 15 3 5 9 Zinc ug/1 1000 81 NE 0.84 J 35 2.8 J 1.5 J 0.89 J 0.4 J 0.21 J 1.6 J 10 1 0.74 J 0.74 J 227 1.8 J 0.21 J 12 5.6 J Nutrients Nitrite (as N) mg/1 NE NE NE 0.06 0.84 0.25 0.27 0.37 Organics 1,1,2,2-Tetrachloroethane ug/l 0.2 NE NE 0.08 J 1,2-cis-Dichloroethylene ug/I 70 NE NE 0.36J 2.25J 1,2-Dibromoethane ug/l 0.02 NE NE 0.08J 1,2-Dichloroethane ug/I 0.4 NE NE 0.02 J 0.04 J 0.11 0.13 J 0.16 J 0.18 J 0.11 0.02 J 0.16 J 1,2-Dichloropropane ug/l 0.6 NE NE BI 0.04 J BDI 0.06 J 0.11 0.05 J 0.04 J BDL 0.06 J 1,4-Dioxane ug/I 3 NE NE 42.4 8.66 4.33 84.8 18.5 22.1 34.6 13.9 14.6 9.33 73.2 Acenaphthene ug/l 80 NE NE BDL 3DL -,)L 3DL BDL Acetone u /I 6000 NE NE L 18.5J 13.2J 12.2J 10.8J 15.3J Alkalinity, Total (as CaCO3) mg/I NE NE NE 605 388 840 1015 7200 248 950 508 1510 584 320 1160 160 432 13 Benzene u /I 1 NE NE BDL BDL BDL BDL BDL BDI 0.78J 0.75J 2.52 1.23 BDL 1.68 BDL 0.53J Carbon Disulfide ug/I 700 NE NE BDL BDI BDL BC BDL BDL BDL BDL 0.53 J 0.27 J 1- 0.24 J Chloride mg/I NE NE NE 14 1 55 65 67 168 12 142 49 220 1 84 63 140 61 128 1 23 Ethylbenzene ug/I 600 NE NE BI BDI BDL BDL BDL BDL B BDL 0.27J I Naphthalene ug/I 6 NE NE BDL BDI 2.41 J BDL 6L 1.24J a 1.44J u. BDL BDL Sulfate mg/I NE NE NE 59.5 229 127 88.8 244 100 185 266 252 140 1 312 1 178 265 301 Toluene ug/I 600 NE NE BDL BDL BDL BDL BDL BDL 0.75J BDL BDL 0.24J BDL 0.29J BDL Total Dissolved Solids mg/I NE NE NE 250 820 BDL 430 1500 1100 1900 1100 300 1500 550 1100 470 Vinyl chloride ug/I 1 0.03 NE NE BDL BDL 0.14J BDL 1 1.4 2.08 BDL 1.26 BDL BDL Xylenes ug/I 500 NE NE BDL BDL BDL BDL 0.68J BDL BDL BDL^' NOTES ug/L = micrograms per liter BOLD = Constituent exceeds NCA002L or GWP regulatory limits BaD =Constituent exceeds NCACO2B or 2B Protection regulatory limits J = Lab estimated concentration BDL =constituent is below laboratory detection limits NA= Not Analyzed By 93 ate W/9 MRgeid,aarW.cerKbitmr620ardAdffMntairgP4iftEHljdirj.5Jr 212,%irgMEBr� dirUTsU nAs DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61 B-5E8AB648F1 3D 93 SMITH GARDNER �me��e4 T WMkritcnrgR9Jts EER§.ydirgla-dll JLre13-1527--4M DL Unit MW-IS MW-ID MW-2D MW-2S MW-3A MW-3D MW-3S MW-4 MNL5 MW 6 MW-7 MW-8 MW-9A MW-10 MW-11 MW-12S MW-13 MW-14D MW-14S MW-15 MW-16 MW-17 Acetic Acid 0.12 mg/L 2.4J 0.31 J 2.5J 3.4J 0.62J 3.2J 0.38J 2.8J 0.46J 0.41 J 3J 3 3.7J 0.31 J 2.5J 2.3J 0.31 J 2.5J 0.27J 1.9J 0.23J Butyric Acid 0.58 mg/L tiuL JUL 0.58J 0.61 J -JL BUL BOL bL)L 0.18J bL)L bL)L bDL A BDL JUL 0.18J BDL BDL Ethane 0.172 ug/L 0.479 J 0.443 J 0.232 J 0.199 J 0.204 J BDL 0.314 J BDL BDL BDL BDL 0.221 J 0.235 J 3DL BDL BDL 0.188 J BDL 0.226 J 0.196 J Ethene 0.241 ug/L 0.43J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.328J 0.408J 0.317J BDL 1.23 0.273J BDL HexanoicAcid 0.58 mg/L 2.3J BDL 0.11 1.91 1.91 BDL 2.5J BDL BDL BDL 0.26J BDL 0.085J 0.065J 0.59J BDL BDL 1.1 J 0.29J BDL Hydrogen 0.49 nM 0.82J 1.1 J 0.78J 0.79J 0.51 J 0.62J 0.72J 0.79J BDL 0.82J 0.75J 0.88J 2.4 2.2 1.7J 2.8 2.2 1.8J 1.2J 2.6 1.6J 1.3J Lactic Acid 0.27 mg/L 4.1 J 18 9.6 5.5 6.9 16 4.8J 0.63 3.3J 2.8 0.75 5.5 1.2 2.3J 1.7 3J 2.1 J 9.5 2.5J 1.2 2.1 J BDL Methane (Dissolved) 1.98 ug/L 16.4 306 35.1 1800 3010 19.2 3780 308 999 846 201 3040 90.1 3680 112 3540 1520 2.91 J 1970 2320 2670 404 Pentanoic Acid 0.056 m /L BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.096J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NoteS: Data from Pace Analytical report numbers 222061806 & 222063033 J =Lab estimated concentration BDL =constituent is below I aboratory detection limits ug/L=micrograms per liter mg1L = milligrams per liter MDL- Method Detection Limit MRge:AO( drt6eMmtairg\2(aMne<aMritairgRputAEER34diro5Jim2M*rg2112EE§ irO1deoJw DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D SMITH GARDNER Hydraulic Hydraulic Velocity Well Conductivity K Effective Gradient v (feet/day) Porosity n i (feet/day) M W- 3A 0.805 0.08 0.004 0.03924 MW-10 0.116 0.05 0.010 0.02320 MW-11 0.009 0.04 0.002 0.00053 MW-12S 1 0.322 1 0.06 1 0.004 0.01986 Note: 1. Hydraulic conductivity and effective porosity values from historical Wood Inc. groundwater monitoring reports 2. Velocity calculated based on the modified Darcy equation: v = (KI)/n W.3j Cite OW29'= MNectslGardl dEN,tntc ro2G rrM.dEKkntaingRpctslEB7�dinj5.Jm2Mgairg=EEfbcjdirgT@Hes)ds( DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Appendix A Well Logs June 2022 Groundwater Monitoring Report CRD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. AlfW-I d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.40 �t Equipment CME 750 Drilling Method 3-114" Hollow AugeisNater Level, TOB NA sz Date Started iom2100 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 Comments Plowed field. cool sunny weather Total Depth mo Date of Observation 1omwoo Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Medium dense buff -white, slightly silty, I I I I I I I I I I I I I I I moist 16,00 I I I I I I I I I I I I - - 14.00 I I I I I I I I 1 I I l I I I - - - 3.5 3 i i I i I i S i I 4.0 SAND: Loose, green -gray, silty and clayey, wet 4 SM 5 I I I I I I I I I I -- - 12.00 t I I I I I I I I i S t I I I I I I I I I 7.5 - - 10.00 ' I I ' ' ' —Y SILT: Medium stiff, gray -green, fine sandy and clayey, with heavy shell hash (turritellas) wet, 8.5 2 i i i i ; —_ medium plasticity 1 SM 8.00 i i i i i — 1 I I— I I I I I i I I I I — 6.00 4WV I I I I I I I I I I I S ! S 5 t I I I I I I I I I I — - — 4.00 1 I I I I I I I I t I I I 1 1 I I I I I I — 13.5 3 I I I I — 4 s I I I I — M L- 1 I I 1 I C L 2,00 1 I I I I — — 0.00 3 I S I I I I 1 I 1 I I I I I I I I I I I I I I I — — — — I I I I 1 I I I I I I 18.5 — 18,5 4 ♦ CLAY: Medium stiff, gray -green, plastic gumbo -2.00 4 clay, moist CL 6 I I I I 1 I I I I I I I I I I I I I I I 4 00 I I I I I I I 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I 1 I I I I I I I I I I 1 I 23.5 4 I I I 5 I I ' I I ' I CL 7 I I I I I I I I DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. A4W--1 d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project CSD Landfill, Inc. (Pitt County) Ground Elevation 17.40 Equipment CME 750 Drilling Method 3-114" Hollow AugelhlVater Level, TOB NA Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 r.nmmPntG Pinwed field- cool sunnv weather Total DeDth sox Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction -8.00 i i ; i CLAY: Medium stiff, gray -green, plastic gumbo 'ANNULUS GROUTED i f S I I I I I I I 1 I I I I I day, moist -10.00 I I I I I I 1 1 I I I I I I I I I I I I I I I I I I 28.5 3CL I I I I I I I I I I 1 3 -12.00 I I I I 1 I I I I I I I 1 I I I I I I I I 1 I I I 31.5 -14.00 SILTYSAND: Dense, partly cemented, black- - ' ' green speckled, variably clayey, silty, moist, hard — ' layer at 36 to 38 feet, very hard below 45 feet -16.00 I 1 I I I I s -7. -• 33.5 6 22 I I I I ! — SM Bentonite 18 I I I r I I Seal -18.00 I I I 7 I I I I I I I ! t S I I I I I 1 1 I I I I I - - -20.00 3 I 1 f t I I I I I I I I I I I I I I I 1 I I I I I I I I I I I - - 38.5 31 I I I 1 I I I 15 I - SM -22.00 I - 24 I I I I I I I I I I I I I I I 1 I - -24.007. I I I I I I I I I I 1 I - I I I I I I I I 1 1 I l I I I I - Sand Pack I - SM -26.00 1 43.5 501.1— I I ! I I I - I I 1 I I 1 I I I I I 1 I I I 77 0.010" 28.00 i i i i i Slotted I I I 7 I I I I I I Screen -30.00 .JII W I I I i ! I I I I I I I I I I t 48.5 50115 I I I I I I I I I S 7. SM -32.00 — ' I I I ' I t Boring Terminated at 50 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. MW-1 s Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C8D Landfill, Inc. (Pitt County) Ground Elevation 17.59 Equipment CME 75 Drilling Method 4.11NO ID HSA Water Level, TOB NA sz Date Started 05102/01 Date Ended 05/02/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 5.59 s Comments Lockino cover with 3.32' stickup Total Depth 13.0 Date of Observation 5/116/01 Elev. SPT Data and Strata Depths. Lithology Description and USCS Code Piez. Construction 1 I I I ! SILTY SAND: Loose, tan -brown, moist [ I I , - Concrete I i I I I pad 16.00 I t I I I • I I I I I SM Bentonite I I I I 1 - Seal 14.00 I I I I I I I I I I I I I I f I I I I I ] i I 1 I - - 12.00— I I I I I I I l } ! I I I I I I I • = - I I I I I I I 3 ! S I I I I I I - - 10.00 I I I I 1 I 8.0 - 0.010" . • . SAND: Loose, tan, fine to medium Slotted 1 Screen I I ! ! $W g.00 ! I 3 I I I I 1 I ! I ! - 6.00 3 5 ! I I I I 1 1 I 1 I I I I I I I I I I I I I I 1 I I I 1 I I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 3 Client and Project C&D Landfill, inc. (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-718" rotary -mud Water Level, TOB 6.6 a Date Started 1019100 Date Ended 10111100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Degth 70.o Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction F I I I I . ' . • - SAND: Loose, tan -yellow, variably silty sand 16.00 { I I I I I I 1 1 I I I I I I I I I I I I I I I I - I I I I I I I I I I 1 3.5 14.00 3.5 16 ' ' CLAY: Medium stiff, tan range, very sandy, silty, e ; slightly plastic, moist, crumbly CL 8 I i I I i I I i 1 I i I I i I I SM 12.00 I I I l I I I ' I I I I I I I 1 1 I I I I I I I i I 75 i D.00 ' SAND: Medium dense, tan, subangular, f - c well ; graded (boring collapsed at 13.6 feet when casing Bentonite- 8.5 5 i pulled, redrilled with 41l4" hollow stem auger) Cement 6 I f I I I � $p- Grout 8 SM 8.00 I I 1 ! I I I I I I - 6.00 I I I I I I 1 I I I I I I I I I I I I I I I S F E 12.5 - �- -, CLAYEY SILT: Medium stiff, gray -green, fine — sandy, with heavy shell hash (whole turritellas), 13.5 3 — moist, moderately plastic 4 00 3 � I I r I I �— CL- 4 I I I I I ML I I I I 1 t I I I I \— I I I I { I I I I I \- 2.00 I I 1 I \ I I ! I I \ — I I I I I 0.00 i I r I I I I I I 1 1 t I I I \— I I I 1 I 16.5 2 a I I 1 I 2 , I i I i I i I i \— iiL- ML -2.00 3 , I I I I I \— I I 1 I I I I I I I \— I I 1 1 I I I I I I �— I I 1 I I I I I I I \ µ -4.00 I 1 I I I 22.5 CLAY: Medium stiff, gray -green, plastic gumbo I I I I I I I I I I clay, moist 23.5 2 -6.00 2 ' I ' I I I I CL 4 I I I I I DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 3 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.97 n Equipment CME 750 Drilling Method 3-7/8" rotarrmud Water Level, TOB 6.6 a Date Started io/woo Date Ended 10/11/00 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Depth 70A Date of Observation 1of16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code PEez. Construction 1 I I I CLAY: Medium stiff, gray -green, plastic gumbo i f i i i day, moist -8.00 I I I I i I I I I I I I I I I I I I I I -10.00 I I I I I I I I I I I I I I I I f 7 f f 1 28.5 2 I I I I l I I ' I I 2 , I I 1 I I CL 3 I I I I I I I I -12.00 I I I I I I 1 I [ I I I I I I I I I I I I I I l ? i i I I I I I I I I -14.00 I I I I l S i I I I I I I I I I I E S I I I I I I 33.5 _3604 33.5 1 I 1 I 1 I i I i = SILT: Stiff, gray -green, fine sandy, clayey, fi I I I I — - interlayered with sand SM 8 I I I I I — I _- Bentonite — Seal -18.00 7 I I I I I I I I I I - - i 37.0 _ 1 I I I I I , Sand Pack = — SILT: Hard, black -green speckled, clayey, fine ' — sandy, moist, moderately plastic, scattered -20.00 ; I i I i I i I i I — - pelecypod shell hash 38.5 5 ' — ' ' ' — 4 I 1 I I I ML 29 -22.00 I I I I I I I 1 I I I I I I I I 1 I I I - - - - -24 00 I I I I I I I I I I I I I I I I 1 - - = I I I I I I I I I 1 - 0.01 a' - Slotted Screen MIL 43.5 10 26.00 20- 27 I I I I I I I I 1 1 — - -28 00 I I I I I I I I 1 I I I I I I I I I I I I I I I 1 I - = - -30.00 I I I I I I I I I I I I I I I I I I I I 1 I 1 I I _- - — - - 48.5 22 I I I I I I I I I 1 49.038 - 5M Bentonite SAND: Very dense (partly cemented), black -green 501.2 i i i i i speckled, clayey, silty, fine glauconite nodules Seal DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 3 of 3 Client and Project C&D Landfill, Inc, (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-7/8" rotary -mud Water Level, TOB 6.6 Date Started iomoo Date Ended 10/11100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 7.9 z Comments Plowed field. cool sunny weather Total Depth 70.o Date of Observation 10M6100 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Very dense (partly cemented), black -green 1 I I I I I E I I I I - speckled, clayey, silty, fine glauconite nodules -3-4.00 I 1 I I I I I I I I 53.5 50/ t I i 36.00 i I i - SM -38.00 I I ! I I I - I I I I I I I I I I I I I I I I I r I 1 57.4 - - ' SAND: Medium dense, green -black speckled, 40.00 i i i i i silty, clayey, fine grained, wet 58.5 6 I I I I I I I I F 7 I I I i 8C 7 42.00 I I I I I I I I Boring .• collapsed below50 I r I 61.5 , ' . feet CLAY: Medium stiff to very hard, gray -green, fine -44.00 i i i I I I I I I I r i ! I I I I I I I sandy, silty, moderately plastic 63.5 5 I I I I I I r s I I I I I -46.00 6 I I I ° I I I CL 5 I I I I I I i l I I I I I i I -48 00 I I I I I I I I I I I I I 7 r r ! F I I I I I I i I I i I I -_^•� I I I I I I I I I I I l k t ! I I I 1 I I I I I I 68.5 40 38 ; CL -s7 nn 501.5 I I t r I I Boring Terminated at 70 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. MW-2s Engineering and Geology Depths in feet, referenced 6.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 1 s.45 Equipment CME 75 Drilling Method 4114" ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Finn Bore & core Logged by David Garrett Stabilized Level 7.91 Comments Locking cover with 2.99' stickup Total Depth 13.o Date of Observation 5116101 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 i i i i i - • - SILTY SAND. Loose, tan -brown, moist Concrete I I i I I I I I I I Prdut l I I I I ! I I I I t — SM Bentonite 16.00 I I I ' I I ' ! I I 1 I I .. - Sea[ 14.00 l 3 I I I I 1 I I I I I 1 I I I I I I 1 - 12.00 I I I I I I I I I I I I ' 1 t I - I I I I I I I I I I 7.0 - SAND: Loose, tan, fine to medium, wet I I 1 I I I I 1 i I . ' 0.019, 10.00 I I Slotted 1 I I I I I I ! 1 I I I SVV Screen 6 W00 V 1 t I I I t I I I ! I I I I I I I I I I I I I I I I I I I [ • 6'00 I I I I i i Boring Terminated at 131eet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. M 3d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-1v4" Hollow AugaiNater Level, TOB 3.0 Q Date Started 10112l00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Comments Plowed field. cool sunnv weather Total Depth 50.0 Date of Observation 10/16/00 Elev, SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I I r I CLAY: Stiff, bright yellow -orange, fine sandy, silty, 1 I I I S I moist I I I S I 18.00 I 1 I I I I I I I 1 I I I I I I I I I I I i ! i I I I I i I I I I I I I Caved 16.00 3.5 4 + I i i i 4.0 SAND: Medium dense, tan -yellow, silty, trace of 4 I i I i I i I i I CL M 6 I I I I I f day, moist 14.00 I I I I I I I I f i I I I I I I I I 1 i 7.0 ' 12 00 I I SAND: Medium dense, tan -buff, well graded fine I to coarse, wet I I I I 4 S I I I 6.5 4 I I I I I I 10.00 5 * I i I i I i I i SW I I i 3 I I I I I I I I I I 1 1 I I I I 8.00 1 I ! ! I I I I I I I I I I I I I I I I 6.00 I I I 1 I 1 I I I I I I I I I 13.5 2 ' ' 14.0 - I I I I SILT: Stiff, gray -green, fine sandy and clayey, with 4 I M L- 4 I i i I i i — - rr heavy shell hash (tuitellas) wet, medium plastic CL 4.00 I I I I I I I I I I I I I I I I 1 1 1 1 — - - 2,00 I I I I I I I I I I I I I I I I I 1 I I I i 16.5 2 I I I I I 1 I I I I - 0•DD 2 CL 4 I I I I I I 1 I I I I I I I I — - - - -2.00 I I I I I I I I I I I I I 1 I I 1 1 I 1 I I I I r I I I I I I I I I - - - - - -4.00 I i I i 1 i I i I i 23.5 — CLAY: Medium stiff, gray -green, plastic gumbo 23.5 2 5 Gay, moist CL 7 I I I I 1 1 I I I I I DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. MW-3d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 r `1 Equipment CME 750 Drilling Method 4-114" Hollow AugekWater Level, TOB 3.0 a Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Y Comments Plowed field, cool sunny weather Total Depth 50.0 Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez, Construction _g 00 ' CLAY: Medium stiff, gray -green, plastic gumbo Bentonite- : day, moist Cement I I I I I r i I I I I I Grout -8.00 I I I I I I ! I I I I 27.5 - - SILTYSAND: Medium dense to dense, partly .. cemented, black -green speckled, variably clayey, 28.5 3 - silty, moist, very hard drilling (cemented) below 38 6 * i i i i feet, glauconitic SM -10.00 5 ! 3 1 I I I I I I I I I -- 12.00 F I I I I I 1 I I 1 I I I I I I I I I I I I I I I 77 - - -14.00 I I I I I I I I I I I I I I I I I I I I I I 33.5 5 I I I I I 18 I I I I I I SM 20 I I I ' - - _18.00 I I I I I _ Bentonite I I I I I I I I I I I I I I I I I I I I - Seal -18.00 I I I I I I I I I I I I 1 I 1 I I I I I I I I I I 38.5 15 I I I I I I I 1 1 1 I I 1 I I I - -20.00 501.3 i I I i I I i 1 1 i l r i I I _ - - SM I I I 1 s f I I - .. -22.00 I I I s I I I 1 I l I I - - Sand Pack -24.00 I I 1 I I 1 1 3 F I SM 43.5 501.5 I 1 I I 1 I f 1 I I -26.00 I 1 1 I I I I I 1 ! ! I I I 0.010" I I I I I Slotted 1 1 1 I r I 1 ! 1 1 I I - -- - Screen V W 1 1 I I I I I I I I 3 f I I I I - - 48,gyp .5 2943 1 I 1 I r I I I I 1 1 1 I I I -30.00 1 ! SM 501.5 Boring Terminated at 50 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. MW-3s Engineering and Geology Depths in feet, referenced b.g.s- Page 1 of 1 Client and Project CAD Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-11,V Hollow AugeliNater Level, TOB 3.9 s Date Started 815107 Date Ended 815107 Water Level, 24 Hr. NA Drilling Firm Bore A Core Logged by Aaron Hill Stabilized Level NA Comments Renlaces former MW-9s Total Depth 20.o Date of Observation NA Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I t ' SILTY CLAY: St'df, bright yellow -orange, fine 1 I I I 1.2 sandy, silty. moist 18.00 1.0 12 + Bentonite- — 16 i i i i — SILTY SAND: Med. dense, brown w! orange ML_ Cement I .. mottle, fine -medium texture CL Grout 21 I I I I I - I I I I I I 33 — Bentonite 16.00 3.5 14 ' i ' i ' i i ' i SAND: Tan, silty, fine texture, moist Seal 11 i i i i i SM- 11 I I I I 1 ML 14.00 I I I I I - 6.0 7 I I i I i I i I i • Sand Pack 11 i i i i 7.1 SM 12.00 11 ; SAND: Medium dense, tan -gray, well graded fine ' to medium texture, wet '• 0.010" 8.5 4 Slotted 4 SW Screen 10.00 4 I I i ! I i I I i I I i I t sM 8 00 I I I 1 1 I I I I I I I I I 7 ! I - I I I I I I I I I I I I r t S 12.9 - I I i I i I i t i CLAYEY SILT: Stiff, gray -green, fine sandy and 6.00 13.5 2 1 _ _ clayey, with heavy shell hash (turritellas) wet, 3 medium plasticity SM 3 I I I S I I 4.00 I I I I I I I I I I \ W I I E I I I I I i I I I I I I I I i t I 2.00 I I I I I \- I I 5 I I 18.5 4 I I ! I I — 5 I \ CL_ 0.� 5 I I F I I I _ Boring Terminated at 20 feet MIL r-111 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/10/09 Date Ended 08/10/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 21.93 Total Depth 20.0 Boring No. MW-3A Page 1 of 1 Ground Elevation 19.13 Water Level, TOB 5.9 Water Level, 24 Hr. NA Stabilized Level 11.4 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 Eli] -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF CLAYEY SAND: Topsoil with roots Bentonite- 1.0 3 1.6 Cement Grout 5 SM 0 - 3' SILTY SAND: Loose orange sli. clayey, fine - medium, trace of roots, sli. moist 3.5 4 - Bentonite Seal 4 -_ sM 3-4' 5 SZ 6.0 7 SM 7 8.5 SAND: Medium dense, tan -buff, 8.5 5 s well graded fine to coarse, SW moist -wet Sand Pack 4-20' 12.9 :. . — �- SILTY CLAY: Stiff, gray -green, 13.5 3 fine sandy, with heavy shell \- hash (turritellas) wet, medium ML- 4 plasticity CL 0.010" Slotted Screen 5 - 20' �- 18.5 2 \- M L- 2 — �— Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. MW-4 Engineering and Geology Depths in feet, referenced b.g.s. Page i of i Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 14.83 Equipment CME 75 Drilling Method 4-114~ ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 3.35 Comments leckinn cover with 3.59'stickuo Total Der)th 13.o Date of Observation wiwo1 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction _ .. - SILTY SAND: Loose, tan -brown, moist Concrete I I I I I .. Pad 14.00 ' ' ' ' ' — I I I I I I I Grout I I 1 I I I - — SM Bentonite I Seal 12.00 I I .. I I I I I I I I 1 I I l I I I — 10.00 I I I I I I I I I 1 1 1 I I I l I I I I — I I I I I I I I 1 I I 6.0 — SAND: Loose, tan, fine to medium, wet i i $.00 I 1 I I I I I ! f I I - - 1 t I 1 t I I 1 I I I 0.010" Slotted 6.00 W Screen I I I i i I I I I I I I I I I • SW 4.00 I I I I I I I I I I I I ! I I - 2.00 I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. MW-5 Engineering and Geology Depths in feet, referenced b.g.s_ Page 1 of 1 Client and Project C&D Landfill, Inc. (Phase 1) Ground Elevation 14,.80 Equipment Mobile 6-53 ATUrilling Method 4-1147 Hollow AugeidVater Level, TOB 3.6 Date Started 11M9102 Date Ended 11/19/02 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 3.9 Comments wooded area, cool sunny weatherTotal Depth 20.o Date of Observation 11/27/02 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Loose, tan, silty, fine to medium, dry ` Bentonite- I Cement 14.00 i ; i i Grout 1.0 4 4 i i i i SM 6 S I I I I I I Bentonite 2.9 Seal 12.00 i i i i i SAND: Medium dense, tan -buff, medium to 3.5 9 I I I 1 coarse, wet (fluvial) 3V ' I � 14 i i i i SW 10.00 16 I I I I I I I I I I S I 5.6 ' SAND: Loose to medium dense, tan -buff, fine to 6.1) 9 coarse, wet, trace of silt (fluvial) $.00 9 i i i i sM 4 I k I I I I I 3 t I I I I I I 8.1 Sand Pack I CLAYEY SAND: Loose, green -gray, silty, wet, 6.00 8.5 4 3 I . � sampled as distinct sand layers with plastic clay lenses (channel or near -shore deposits) SC 4 I \- I I ! I I \ \- I �- 4'00\- 0.01 a, \- ••• Slotted l I I I I Screen 2•00 3 I I I I 1 13.5 3 I i i i ....... .\- 4 i i i i \-\- SC 0.00 4\-\- i-- * Locking steel cover w! 3 foot \- •\ stickup �, -2.00 I I I I I I I I 1 I \- I I 1 I I I I I I I 18.4 Deep SILTY CLAY: Stiff, gray -green, var. sandy, shell 4.00 18.5 3 i i i i i marine 4 1 i i i i hash, moist, plastic ** CL_ deposits (Yorktown 6 i i i Boring Termat 20 feet CHinated Grp.) DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring No. MW-6 Engineering and Geology Depths in feet, referenced b.g-s. Page 1 of 1 Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16"87 Equipment CME 75 Drilling Method 411,C ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 6.68 Comments Lockina cover with 3.16" stickup Total Depth 13.o Date of Observation 5116/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I SILTY SAND: Loose, tan, moist Concrete pad 16.00 I — I I ! I I I - - Grout I I f I I SM Bentonite — Seal 14.00 I l f I I I I I I I 1 I I I I - 12.00 3 1 I I I I ! I I I . . — I I 1 ! I I I I I 1 6.0 - SAND: Loose, tan, fine to medium, wet I I I I I i 0.00 I I I I I 1 I I ! I • I I I I I 1 I I I I • 0.010" ' Slotted 8.00 i i i r i Screen I 1 1 I I I I I I I F I 1 I I I - SVj b 00 I I I I I I I - 1 I l I I I I I I I - 1 1 I I I I - Boring Terminated at 13 feet 4.00 - DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Boring No. AM-7 Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16.03 Equipment CME 75 Drilling Method 4-1►47 ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 5.29 ('nmmAntS Lne-kinn cover with 3.37' stickup Total Depth 13.o Date of Observation 5/16/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SILTY SAND: Loose, tan, moist Concrete I I I I I •• P I I I I I — Grout 14.00 1 ; r ; I ; I ; I ;77 SM Bentonfte I I I E I I I I I i Seal 12.00 I I I I I I I I I I I I I I I I S 5 1 i - I I I I ! I I I I 5.0 - - I SAND: Loose, tan, fine to medium, wot 10.00 I I S ! t I I I I I I 1 I I I I I 1 I I I I I I I I I 1 I I I I I I I 0.010" I I I I 1 Slotted Screen I SW 6.00 I 1 I I 1 I I 4D0 I 1 I I I I 1 i I I Boring Terminated at 13 feet DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P. G., P.E. Boring .No. AM-8 Engineering and Geology Depths in feet, referenced b-g.s. Page 1 of 1 Client and Project CSD Landfill, Inc. (Phase 1) Ground Elevation 18.30 Equipment Mobile 13-53 ATDrilling Method 4-114" Hollow AugeliJVater Level, TOB 7.3 s Date Started 11/18/02 Date Ended 11/18/02 Water Level, 24 Hr. 7.3 Drilling Firm Bore S Core Logged by David Garrett Stabilized Level 7.3 ('OMMentS wooded area- cool sunny weatherTotal ❑eoth 20.o Date of Observation 11/27/02 Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 SAND: Loose, tan, slightly silty, fine to medium, ` Bentonite- ' dry Cement Grout - 2 i i r i SW 16.00 3 I , I I , f I I , I I , I I , I - Bentonite Seal 3.5 3 I s I I I I 14.00 3 i i i i t - SW 4 I I I I I I I I I I I I I 1 f - I I I I I 6.3 ' 12.00 6.0 4 �' 4 SAND: Medium dense, tan -buff, medium to SW 4 I I I I f I I I :. coarse, wet 10.00 i ! i I i I i I i I 8 4 Sand Pack _ . • SAND: Loose to medium dense, tan -buff, fine to 8.5 7 8 I I i I i I i I , ' ' coarse, wet, trace of slit Sw 8.00 I 1 I I I - I I I I I Slotted I I I I 1 Screen W 6.00 I I I I I I I I I I I I 1 1 1 • 13.5 4 I I I 1 I I I - 4.00 4 I i i i i SW 4 I I 1 I I I Locking I , , , , • steel cover _ wl 3 foot 2.00 I I I : = I stickup I i I I i I 1 i I I s i I i I 17.6 ." SILTY CLAY: Mod. stiff, gray -green, var. sandy, 0.00 i i i heavy shell hash (turritellas) moist, plastic '• CL- " Deep 18.5 3 l• ; I i I i I i I CH marine deposits 4 I I 1 I I 1 I (Ye rkiown 6 Boring Terminated at 20 feet Fm.) DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.58 Total Depth 20.0 Boring No. MW-9A Page 1 of 1 Ground Elevation 17.64 Water Level, TOB 3.1 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -16 -14 -12 -10 -8 -6 -4 -2 -0 -2 N = 0 20 40 60 80 100 BPF 77 SILTY SAND: FILL with brick 1.0 3 77 and concrete fragments Bentonite- Cement Grout 4 2.1 SM 0-3' 5 XX CLAY: Med. stiff, orange -tan - gray (mottled), fine sandy, very 3.5 10 moist Bentonite Seal 12 CIL 3 - 4' 13 Ir 5.9 SAND: Medium dense, light 6.0 5 ♦ 5 gray -buff, sli. silty, well graded SW- 6 fine to medium, wet SM 85 4 5 SW- 5 SM Sand Pack 4-20' 13.5 4 13.7 _ 4 — SILTY CLAY: Med. stiff, gray- ML- 5 green, sli. fine sandy, with CL �- heavy shell hash (turritellas) 0.010" Slotted — wet, medium plasticity Screen 5 - 20' �- Artesian water press. at 12 feet 18.5 2 \- M L- 2 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.61 Total Depth 20.0 Boring No. MW-10 Page 1 of 1 Ground Elevation 14.16 Water Level, TOB 2.7 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 W -0 -2 -4 N = 0 20 40 60 80 100 BPF SILT: Soft, dark brown, fine 1 sandy, organic, very moist Bentonite- 1.0 Cement Grout 1 2.1 ML 0-3' 5 SAND: Med. dense, tan -buff, uniform fine grained, wet t t 3.5 9 Bentonite Seal 13 SP 3-4' 12 Ir 6.0 9 12 7.1 SW 2 8.0 SAND: Loose, tan -buff, sli. silty —_ SILTY CLAY: Soft, gray -green, 8.5 3 sli. fine sandy, with heavy shell 2ML- \ hash (turritellas) wet, distict CL sand and clay layers Sand Pack 4-20' 13.5 3 �- 2 — M L- 3 CL \- 0.010" Slotted Screen 5 - 20' �- 18.5 3 \- M L- 3 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 14.49 Total Depth 20.0 Boring No. MW-11 Page 1 of 1 Ground Elevation 11.60 Water Level, TOB 6.1 Water Level, 24 Hr. NA Stabilized Level 3.1 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data M -8 -6 -4 -2 -0 -2 -4 -6 -8 N = 0 20 40 60 80 100 BPF SAND: Loose, dark brown, silty, 2 fine - medium, tr. clay, moist Bentonite- 1.0 Cement Grout 2 SM >0-3' 3 2.9 CLAY: Very soft, green -gray, 3.5 1 silty, fine sandy, w/ turritella Bentonite Seal shell hash, wet ��- 3 - 4' o 5.5 CLAY: Soft - med. stiff, gray- 6.0 2 Sz 3 green, fine sandy, very silty, ML- 2 with shell hash (turritellas) wet, CL very sandy layer w/ large shell fragments at 9.5 - 10 feet 8.5 4 5 SC- 6 CL Sand Pack 4-20' 13.5 5 5 14.5 MH- $ SILTY CLAY: Med. stiff, gray- CH — green, sli. fine sandy, wet, very 0.010" Slotted plastic Screen 5 - 20' 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.18 Total Depth 20.0 Boring No. MW-12S Page 1 of 1 Ground Elevation 13.72 Water Level, TOB 2.1 Water Level, 24 Hr. NA Stabilized Level 5.3 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 z. N = 0 20 40 60 80 100 BPF SAND: FILL, Loose, brown, 1.0 1 silty, moist (drilling pad) Bentonite- Cement Grout 2 2 0 SM sz 0 - 3' SAND: Loose, tan -gray. sli. 5 silty, fine -medium, black 3.5 10 decayed organic debris, wet Bentonite Seal 12 SW- 3-4' 13 SM 7W 6.0 5 9 SW 10 SM 8.5 5 • Loose, white, clean "sugar sand" 7 T 9.5 SP 3 10.0 �- SILTY CLAY: Med. stiff, gray- Sand Pack green, sli. fine sandy, moist, w/ 4 - 20' _— shells, very plastic 13.5 3 5 CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.69 Total Depth 20.0 Boring No. MW-13 Page 1 of 1 Ground Elevation 18.12 Water Level, TOB 5.1 Water Level, 24 Hr. NA Stabilized Level 8.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 -10 -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF SILTY SAND: Loose, brown, 1.0 2 fine -medium, w/ clay, roots, dry Bentonite- 3 (perimeter embankment fill) gW_ Cement Grout0 - 3' 3 - SM 3.5 3 4.0 Bentonite Seal CLAYEY SAND: Loose, tan, SC 3 - 4' 5 fine -medium, w/ wood, moist 5.7 - SILTY SAND: Very loose, tan- 6.0 1 1 brown, w/ tr. clay, wood SM 1 _ 8.1 �_ SILTY CLAY: Stiff, green -gray, 8.5 7 9 _— sli. fine sand w/wood Y, ML- 10 C L \_ Sand Pack — 4-20' 12.5 �- �- SILTY CLAY: Stiff, gray -green, 13.5 5 sli. fine sandy, w/ heavy shell 6 — hash (turritellas), moist, very MH- 6 plastic CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 4 \- M H- 5 Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 1 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 -2 -0 W -4 -6 -8 -10 N = 0 20 40 60 80 100 BPF . SILTY SAND: Medium dense 1.0 ♦ tan -brown, fine to medium Convertedfrom 5 SM piezometer 5 B-23d 3.1 3.5 6 SAND: Medium dense, tan, 10 medium to coarse SP 9 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 • dense, dark gray 3 _I SC 5 12.7 Bentonite- Cement Grout �- SILTY CLAY: Stiff, dark gray, 13.5 4 l \- fine sand layers, shell layers, 0-32' 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL 18.5 4 * �_ 6 CH 23.5 5 CH 6 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 2 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -14 -16 -18 - 20 - 22 - 24 N = 0 20 40 60 80 100 BPF \- SILTY CLAY: Stiff, dark gray, fine sand layers, shell layers, becomes sandy with shell hash below 28.4 feet 28.5 21 : \- 16 CL Bentonite Seal 32-33' 32.8 �- SAND: Very dense, dark gray, 33.5 50/A silty, glauconitic, shell hash SM Sand Pack 33-40' 0.0101, Slotted Screen 35-40' 29 38.5 50/.5 Boring Terminated at 40.0 feet SM DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/18/02 Date Ended 12/18/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 16.60 Total Depth 20.0 Boring No. MW-14S Page 1 of 1 Ground Elevation 13.90 Water Level, TOB 3.0 Water Level, 24 Hr. 2.2 Stabilized Level 2.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 -6 N = 0 20 40 60 80 100 BPF SILTY SAND: Medium dense Convertedfrom 1.0 tan -brown, fine to medium piezometer B-23s 5 SM 5 Bentonite- 3.1 _ sz Cement Grout SAND: Medium dense, tan, 3.5 6 0-1' 10 medium to coarse SP Bentonite Seal 9 1-3' 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 dense, dark gray 3 Sc 5 12.7 Sand Pack 3-20' -- SILTY CLAY: Stiff, dark gray, 13.5 4 l \— fine sand layers, shell layers, 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL \- 0.010" Slotted Screen 5-20' 18.5 4 \— s ? Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. MW-15s (OLD B-23s) Engineering and Geology Page 1 of 1 Client and Project CAD Landfill, Inc. (Phase 2) Ground Elevation 13.90 Equipment Detrich 0-10 Drilling Method 3-114" HSA Water Level, TOB 3.0 Date Started 12/18/02 Date Ended 12 I8102 Water Level, 24 Hr. 2.2 Drilling Firm Bare & care, inc. Logged by David Garrett Stabilized Level 1.4 Comments Lagged area, cool sunny weather Total Depth 20.0 Date of Observation 1116103 All deaths are given in feet and referenced b.a.s. Depth and Elev. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data -0 - 2 12.00 - 4 10.00 - g 8.00 - 8 6.00 - 10 4.00 - 12 2.00 - 14 0.00 - 16 -2.00 - 18 -4.00 — 20 -6.00 i I l i i i i + � I i i I i i i i i BLANK: No samples taken - please see log fpr &23d Sz Bentonite- Cement Grout Bentonite Seal ' i I I i i Sand Pack 3 ' 0.0101, (} t E F e ! i i Slotted Screen DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. MW-17 (OLD B-20) M I I I Engineering and Geology Page I of 1 Client and Project C&D Landfill, Inc. (Phase 2) Ground Elevation 18.18 Equipment Detrich D•10 Drilling Method 3-1/4" NSA Water Level, TOB 3.7" Date Started 12/09/02 Date Ended 12109/02 Water Level, 24 Hr. 3.9 Drilling Firm sore & Core, Inc. Logged by David Garrett Stabilized Level 4.1 Comments Logged area, cool Manny weather Total Depth 20.0 Date of Observation 1115103 All depths are given in feet and referenced b.g.s. Depth and Elev.1. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data - a 1 B_oa — 16.00 — 14.00 — 6 12.00 — 8 10.00 — 10 8.00 — 12 6.00 — 14 4.00 — 16 2.00 = 18 0.00 - 20 .. SILTY SAND: Medium Sentonite- ; i dense, dark brown, fine Cement Grout 3 grained SM 5 1 — Bentonite Seal � SAND: Medium dense to dense, tan -brown, SW 19 I i fine to medium 8 14 0i ! i i ! SW 21 ! I 9 12 SW 14 I f � I i Sand Pack 3 SW SAND: Medium dense, [ fine to medium, trace of i { silt E f f� �{ 0.01 01, I I i Slotted Screen 3 a E f ! ! SILTY CLAY: Medium 5 I stiff, trace of shells ML-CL DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D D SOIL CLASSIFICATION P .AND REMARKS T H SEE KEY SYMBOL SHEET FOR EXPLANATION OF (ft) SYMBOLS AND ABBREVIATIONS BELOW. 0 Sandy topsoilirootmat ndfil--- l-debris/gravel - and san----- d --------� La _ _ _ COASTAL PLAIN: Orange -tan -to gray__, dry to moist_, clayey and silty SAND (SM) C-OAST-AT P-1-Tan--a-a-nd -wh-t-m-ist-to-sa-tur-ate-d-- L E SAMPLES PL (%) NM.(%) LL (%) E L I (Rec") G E D T N-COUNT ♦ FINES (%) E V E Y or N N P Rcc%MQD% 0 SPT (bpf) D (ft) T E 6"- 6"- 6"- 6" 10 20 30 40 50 60 70 80 90 100 15.0 5 slightly silty, tine to coarse SAND (SP) with trace rounded 10.0 fine gravel 1 . 10 5.0 15 YORKTOWN FORMATION: Dark gray to gray -green, 0.0 saturated, silty, fine to medium SAND (SM) with thin (0,1-0.2) lenses and layers of dark gray -green, fat CLAY (CH) 20 Boring terminated at 20.0 feet. -5.0 G n :7 a 3 25 0.0 d .a a a a n 30 15.0 35 -1 1 �- -20.0 40 -1 1 F- -25.0 45 -30.0 CONTRACTOR: Regional Probing Services -Larry Opper LOGGED BY: M. Lear EQUIPMENT: Geoprobe 5410 DRILL METHOD: Direct Push HOLE DIAMETER: 4" WELL: Stickup 2.9' Size 2" CLOSURE METHOD: Installed Monitering Well MW-16. REMARKS: Well developed by purging approximately 3 well volumes via bailer and pump. Static water level measured at 7,45 ft below TOC. 0 10 20 30 40 50 60 70 80 90 100 GEOTECHNICAL BORING RECORD BORING NO.: MW-16 PROJECT: EJE Recycling LOCATION: Greenville, NC DRILLED: June 16, 2017 PROJECT NO.: 6468-17-7070 PAGE 1 OF 1 IEWED BY: amec faster wheeler ► DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D David Garrett, P.G., P.E. Engineering and Geology .,Client and Project C&D Landfill, Inc. (phases 3 and 4) Equipment CIVIE 450 Drilling Method 4 1vvv H$A Date Started 12114101 Date Ended 12/14/01 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments :.iamg2u aiea5 cioal rarliny weather Total Depth 15.0 All dent :- are ,;:al: ,l__� _s_..__i.td r � � �kl iT.CI pelf l�if�rl'�.��YV`ii N.w.sx OLD B-Is (BG) Page 1 of 1 Ground Elevation 17.19 Water Level, TOE 1.5 Water Level, 24 Hr. 1.4 Stabilized Level 1.6 Date of Observation 12/27/01 Depth and Elegy. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezom2ter Constuction Data 0 r 16.00 2 14.00 4 12.00 6 10.00 8 8.00 10 6.00 12 4.00 14 SAND: Loose, gray- 2 I I I - brown, variably silty, 3 4 moist, trace of clay and a i ! . organics SM I Bentonite- 3 6 ' SP- Cement Grout 7 i I SM 2 SILT: Soft, dark bra.,.n, 2 clayey, decayed 2 — organics (channel Bentonite Seal -= deposits) 2 I — 1 I i ML 2 — Sand Pack 0.0101, 2 i I i i - - — ML Slotted Screen DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Appendix Laboratory Analytical Report June 2022 Groundwater Monitoring Report CRD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 R 7407- CDLF- 2009 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D EINT'kou��uMO� A kgNrlfuuaAd 114 OAKMONT CDRIVF GnEENVILLE, N.C. 27868 C & D DISPOSAL, INC. MA. atMSON WHITEHURST 802 RECYCLING LANE Cr'REENVILLE, NC 27834 Drinking water TDt 37715 Wastewater ID, 10 FAX (252) 756-0633 ID##: 6003 A DATE COLLECTED: 06/13/22 DATE REPORTED : 10/13/22 REVIEWED BY. NW-18 MW-1D MW-28 NW-2D Trip Analysis Method QARAMZTRR9 MDL MRL Blank Date Analyot Code PH (field measurement), Unite 6.2 7.3 6.7 7.4 06/13/22 PJC 4500HB-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 4.37 --- U 06/15/22 TRJ 353.2 R$-93 Nitrate+Nitrite as N, mg/1 0.04 0.04 0.22 --- V 06/20/22 K83 353.2 R2-93 Alkalinity (to pH 4.5), mg CnCD3/1 1.0 2.0 232 755 1010 900 06/20/22 D1J 232OH-11 Chloride, mg/l 2.0 1.0 104 15 136 13 06/20/22 HCE 4500CLB-ll Total Dissolved Residue, mg/1 10 10 1133 210 270 06/14/22 DIJ D5907-13 Total Dissolved Residue, mgll 10 10 1900 05/16/22 HMV D5307-13 sulfate, mg/1 5.0 5.0 383 --- U 360 26+2 06/21/22 MTM 45009042911 Antimony, qg/l 0,03 1.0 0.59 J 0.08.7 0.14 J 0.14 J 06/30/23 NAB EPA200.8 Arsenic, ug/1 0.08 5.0 0.94 J 1.9 a 14 1.iJ 06/30/22 NAB EPA2DD.8 Barium, ug/1 0.04 20.0 253 30.0 394 15,6 07/01/22 HAD EPA200.8 Beryllium, Ug/l 0.02 1.0 0.06 J 0.02 J 0.02 J --- (7 07/05/22 LFJ UPA200.8 Cadmium, ug/1 0.04 1.0 0.28 J 0.08 J --- U --- U 06/30/22 NAE EPA200.8 Cobalt, u9/1 0,02 1.0 0.22.7 0.09.7 2.3 0.a5 J 06/30/22 NAB EPA200.8 Total Chromium, ug/1 0.12 5.0 1.91 0.50 J 12 0.20 J 06/30/22 NAB EPA200,8 Copper, ug/1 0.04 10.0 3 J 0.68,7 0.49 J 0.15 J 07/01/22 NAB 6PA200.8 iron, ug/l 4.96 50.D 457 3987 14074 1384 06/20/22 LFJ EPA200.7 Manganese, ug/1 0.$1 10.6 35 70 892 43 06/2D/22 LFJ 8PA200,7 Lead, ug/1 0.03 5.0 0.82 J 0.24 J 0.12 J 0.11 J 07/01/22 MAE EPA200,8 mercury, ug/1 0.65 0.20 --- u --- ❑ -- V --- U 06/23/22 MTM 245.1 R3-34 Nickel, ug/1 0.03 10.0 1.8 J 0.52 J 2.2 J 0.15 J 07/01/22 NAB EPA200.8 Selenium, ug/1 0.05 10.D 0.82 J 0.21 J 0.84 J --- to 06/3D/22 NAB EPA200,8 silver, ug/1 D.22 5.0 --- V --- U --- U --- U 07/01/22 NAB EPA200.8 Thallium, ug/1 0,02 1,0 0.21 J 0.11 J 0.02 J --- U 07/05/22 LFJ EPA200,9 Tin, ug/1 D.05 100.0 --- U --- U --- U --- U 05/3D/22 NAB SPA200,8 vanadium, ug/1 0.04 1.0 3 0.60 J $ 0.22 J 06/3D/22 NAB EPA200.8 zinc, ug/1 D.17 20.0 3.0 J 3.3 J 2.3 J 3.3 J 07/01/22 NAB EPAZ00.8 sull"ids, ug/1 100 3000 --- D --- ❑ --- V --- V 06/17/22 LFJ 450092D•11 Conductivity (at 25C), uNhae/am 1.0 1.0 3481 394 2916 460 06/13/22 P.7c 2510E-11 Dissolved Oxygen, mg/1 0.1 0.1 1.89 1.00 1.55 1.01 06/13/22 PJC 450000-16 TemperaCUY4, °C 23 23 22 24 06/13/22 PJC 255OH-10 Static Water Level, foot 9.35 9.53 11.65 13.47 06/13/22 PJC wall Depth, Feet 17.21 33.75 16.57 38.17 06/13/22 PJC ORP, my +100 +50 +120 +85 06/13/22 NN# 2580E-11 Turbidity (Field), NTU 1.0 1.0 7.72 7.04 6.06 6.41 06/13/22 PJC 2130E-21 All QC requirements were not mete M Blank reaUlt exceeded method conatant weigtt Criteria. J - Estimated value between the MDL and MRL, U - Below ALL puentitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D llw��P0�Vq 114 OAKMONT DRIVE GREENVILLE, N,G, 27858 Drinking Water Inc 3771$ Wastewater Yb: 10 FAX (252) 7F" Or-,V. CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. MMSON WHITEHURST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 06/1.3/22 DATE EXTRACTED: 06/16/22 DATE ANALYZED: 06/17/22 REVIEWED BY: �L DATE REPORTED: 10/13/22 BASE/NEUTRAL COMPOtMDS EPA METHOD 8270E R6(18) PARAMETERS, ug/1 MDL MRL Mw-1s MW-1D MW-25 MW-2D 1. Acenaphthene 2,66 10.000 --- U - U " ' U - U a - Batlmated value between the MDL and MRL, U . Below ALL quantitation Limitd. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 1p�o)I��VW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 Drinking water IW 37715 Wastewater TP: 10 I'I1UHL tZb.-} ,.._,. „ FAX (252) 756-0633 IP CLIENT: C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED EY: LANDFILL EPA METHOD CLIENT ANALYST: DATE COLLECTED: DINE ANALYZED: DATE REPORTS]?: APPENDIX I3 8260D R4(18) ID: 600-1 A JAP 06/1.3/22 06/22/22 10/13/22 Page: 1 Trip NW-28 MW-lD MW-78 MW-3D PARAMETERS, u9/1 MDL MAIL 03.ank 1. Chloromethane 0.77 3.000 --- U -- V --- V --- U --- U 2, vinyl Chloride 0.12 0.200 --- U ___ U --- V --- U --- U 3. Bromomethans 0.67 10.00o --- U --- V --- V -,- V '-- U 4, Chloroethrne 0.48 10.000 --- U --- U --- U --- U --- V S. Triahlorafluoromethane 0.24 1.000 --- U --- ❑ --- U -'- U --- U 6, 1,1-Diahloro*thane 0,17 5.000 --- V --- U --- V --- ❑ --- U 7. Acetone 9.06 100.000 --- U --- U _._ U ... U ••• U 6. Iodomethane 0.26 10.000 --- U ... V --- U --- V --- U 3. Carbon Did%'Itide 0.23 100.000 -- V - - V - - U ❑ "-- ❑ 10. Methylene Chloride 0.64 1.006 --- U --- U --- V --- U - U 11. trans-1,2-Dichloroathaae 0,23 5.006 -.- U --- U -- V "-- U --- U 12, 1,1-Dichloroathane 0.20 51000 --- U --- U --- U U -- U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- U --- U --- U 14, Cia-1,2-Pichloroethena 0.25 5.000 --- U --- U --- U .1, U --- V 15. 2-Butanone 2.21 200,000 --- U --- U --- U --- U .__ V 16. Bromochloromethans 0.27 3.000 --- V --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- V --- U --- U --- U IS. 1,1,1-Trichlorcathans 0.19 11000 --- U --- U --- U --• U --- U 19. Carbon Tetrachloride 0.04 0.2DO --- V --- u --- V --- U --- U 20. Benzene 0.24 1.000 --- U .-- t1 0.36 d --- U --- U 21. 1,2-Diahlorcethane 0.02 01200 --- V --- V O.D6 J -•- U --- U 22. Trichloraethone 0.23 1.000 --- U --- U --- U --- U --- V 23. 1,2-Dichloropropans 0.04 0.200 --- U --- U --- ❑ - " V " - U 24. 8romadichloromethane 0.04 0,200 --- V --- U U --- U --- U 25. Cid-1,3-Dichloroprogane 0.06 0.200 --- U --- U --- U ""- U --- U 26. 4-Methyl-2-Pantanons 1.19 100,000 --- U --- U -- V U --- U 27. Tolvene O.23 1.000 --- U --- V --- ❑ --- U --- U 20. trane-1,3-Diahloropropaae 0.04 0.200 --- U --- U -•- U -"" U -`- V 29, 1,1.2-TrLehlorcethana 0.03 0.200 --- U --- U --- U --- U --- U 30. Tetr4ahloroethana 0,10 0.200 --- U --- U --- V ^-- U --- V 31, 2-Hexanons 1.57 50,000 --- ❑ --- U --- U --- ❑ U 32. Dibromochloromethane 0.03 0.200 --_ V --- V --- V --- U --• U 33, 1,2-Dibromoethane 0.03 0.200 --- U --- U --- U --- U --- U 34. Chlorohenzena 0130 3.000 -"- V --- U -= U --- U 1$, 1,1,1,2-Tetr%chlorasth&na 0.22 11000 --- U --- U --- U --- U U 36. Sthylbenzens 0,21 1.000 --- V --- 0 --- U --- U --- U 37. xylem• 0.6e 5,e00 --- ❑ --- ❑ --- u 38. Dihromamethane 0.28 10.000 --- V --- U --" U --- ❑ "-' ❑ 39. Styrene 0.19 1.000 --- U --- U --- U ... U --- U 40. aramoform 0.20 3.000 --- V --- U --- U -'- U --- U 41. 1,1,2,2-Tetrachloro#than* 0.03 0.200 --- V --- ❑ 0.0E S .-- U --- U 43. 1.2,3-Triahloropropans 0.09 0.200 •-- U --- V --- U --- U --- U 43. 1,4-Dichlorohenztnt 0.39 1.000 --- U --- V --- U --- U --- U 44, 1,2-Diohlorobenzene 0.32 5.000 --- U --- U --- U --- V --- V 45. 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- V --- V --- U --- V --- U 46, Acrylonitriia 2.72 2001000 --- U --- U --- U --- V U 47, trana-1,4-DiCh2oro_2-Hutene 0.42 100.000 --- U --- V --- U --' ❑ - U 48. Acroltin 1.97 4,000 --- U --- U --- U --- V --- U J a Eatimated value between the MDL end NRL, U - Below ALL puantitetion Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D L uA,ARMN �, �W�UWP(0� �ON)d 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE. N.C. 27858 FAX (252) 756-6633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 002 RECYCLING LANE ANALYST: ,IAP GREENVILLE, NC 27834 DATE COLLECTED: 06/13/22 Page: 2 DATE ANALYZED; 06/22/22 DATE REPORTED: 10/13/22 REVIEWED BY; LANDFILL APPENDIX II EPA METHOD 8260D R4(18) NW-18 Mw-1D MW-22 MW-2D Trip PARAM6T3R8, u9/1 MDL MRL Blank 49. Allyl chloride 0.20 10.000 --- U --- U --- V " " U ... U 50, ghloroprene 0,21 20.000 --- U --- U --- U --, U --- U 51. 1,3-Dichlorgbenzene 0.42 5.000 -"- U --- U •-- V "-" "' U 52. DichlorodLfluorammthane 0.51 5.000 --- U --- U --- U --- u "-- U 53, 1,3-Dichloropropane 0.28 1,000 --- U ••- U --- V --- U --- U 84. 2,2-Dichloropropane 0.17 25.000 --- U ^-- V --- --- U -'" U 55. 1,1-Dichlvranragene 0,22 5.000 --- U ••• U -- U U --- U 56, Bthyl Methacrylata 0.16 20,000 --- U --- U --- U --- U •-- U 57. HexachiorobutPdiens 0,10 0.200 --- U --- U --- U --- U --- U 58. lmobutyl Alcohol 12.80 200.000 ••• U --- U --- U --- U -^- U 59. Methacrylonttrile 1.93 100.000 --- V U --- Ti --- U --- U 60, Mmthyl Mathacrylate 0.25 30,000 ••• U --- U --- U -- U U 61. Naphthalmrim 0.47 6,000 --- U --- U 2.65 7 --- U ••• U 62, Propionitrile 3.26 150,000 ••• U --" U --- U --- U --- U 63. 1,2,4-TXich1orohenzene 0.50 10.0D0 --- U --- U --- U --- U ... U 64, Acetonitrile 36.29 55.000 --- U --" U --- U ••• U U 65. Tetrakhydr4Euran 0.39 1.000 1.54 7.21 28.9D --- U --- U 66. 1,4-Dioxane 2.71 3.000 35.34 --- U 67.60 ••. U --- U j • natimaeed value between the EQDL and MRL, U - Below ALL QMantitation Limits. n°O?n N DocuSi , cn w m c m CD w 0 � n c _ u> - 07 o o 00 m 3 o '0 0 m . �' C w cn w cD m0 6 w u lvtow 77 m C tv. ... M io-o�or.ovwor iov N p rm— r-- Uj IYd J 000 r �am►/G�t ' C O zM M o m M b �C�zM 0 ON cl) l IH a l�7 Uj n71 A �-! a H IJ s I�J Vti. 1 O f O D m N Ln n - - EE: m m -' = t O - Z: -i O �m m M TOTAL CHLORINE, mg/I C7 m n OR ug/I AT COLLECTION 0 m 0 o z c n z z < M C� Cj N C TEMPERATURE,°C co {cil co � �� AT COLLECTION I a o Cn Cfj z z #OFCONTAINERS A W W W A r <': Field H ti ..... ...... Nitrate+Nitrite n b alinity W Chloride d ...... ..... ...... .... a TDS I M gt Sulfate Y m m m O' AL Metals � n7 2 0 Sulfide ..... _Ir M zi u hv c 1 d Con t Y "C I � n cn ( ...... DO b c _ c Temperature er atur e I Field Parameter <> 8270E Dup. 1 8270E Dup. 2 G� 8270E Dup. 3 I G) 8260D App. II C� cn �, PARAMETERS/TESTS a �_ f T w > M o C-) r O " CD z C CD C'i7 D D -I Z 2 n Z O �„ _ = z r m m M y�y�Z O 1 GO O �_ n D r o P o m w C t� ID < _ v ^r n \ p r Z7 Z � m M f l O \.� p Z m Y �,i - l m 0 D 5 m Z n > '� n Z N � n O MrD cli 5� D O cn M z O n m cn m O 1 W m D z O M z D m M l n my z 0 m O z C5 _ N DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61 B-5E8AB648F1 3D 04 n yc.� M Z m N;0 Rocn Z ;\ _ w w W N N - _ m m = om ry w C7 Ln C7 w r+ t7 ►+ m r �p �"� V] Cn r.? �o r n o b J 0 0 n o o r�zo n n �. ZZ s� D '.. N rrujv , - z A P. mmJ D O w ii :r. Go O � z m i cn O m � � V 71 - N o = o _ m =i o CD 7 , m m m FTF TOTAL CHLORINE, mg/I C m m m OR ug/I AT COLLECTION v, 0 0 0 n z O < C� �, C' 1 '0 TEMPERATURE, °C JJ v� AT COLLECTION m C) w w #OFCONTAINERS zO ARAM 8260D App. II 2 ti7 4� 8260D App. II ORP 0 0 V'0 8270E B/N 4� n m �m b cf t7 G kA re oC � T S i� > c) w> = PARAMETERS/TESTS ft m > -0m n oz 77 -n E C� 07 i+ C5 Z _ m m 0 7�J or c = ZO m n Z cscn n M G= cn O z m m -Z m C fCrl ero' 0� Z UDi -n CD ?� O Cn < Z N 2 Z r D S zZj m o D T D mD U) -i 77 p Z n D -I n r O OZ m m Z n n �{3 C DD z 0 m Z cn C � D O { —ni C" C) G z o m Z --I O c� 0 z 0 rn DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D a G�nwkooRRffi� `�v 4(n carp Me 2� Drinking Slater ID: 37715 Wastewater IP, 10 114 OAKMONT DRIVE GREENVILL.E, N.C. 27858 C & D DiSPOSAL, INC. MR- JTIDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756.0633 ID#: 6003 A DATE COLLECTED: 06/14/22 DATE REPORTED : 07/12/22 �4 REVIEWED BY: � MW-39 NW-3D MW-3A Analysis Method PARAMBTHRB MDL MRL Date Analyst Code pm {field measurementl, Unite 6.8 7.6 6.0 06/14/22 JWT 450ONE-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 0.37 0.19 0.16 O0/20/22 KX& 353.2 R2-93 Alkalinity (ta pH 4.5), mg CeCO3/1 1.0 1.0 1460 224 610Q 06/20/22 DTJ 212OB-11 Chloride, mg/l 1.0 1.0 214 22 196 06/20/22 RCE 4509CLa-11 Total Dissolved Residue, mg/l 10 10 1900 320 06/16/22 HMV 05907-13 Total Dissolved Residue, my/l 10 30 M 1700 06/20/22 HMV D5907-1$ B.0 5.0 11.3 --- U 134 06/21/22 MTM 45009042211 Sulfate, mg/l 0.03 1.0 0.26 J 0.09 J 0.22 J 06/30/22 NAB NPA200.8 Antimony, ug/1 Areanic, ug/l 0.06 $.0 $2 0.34 J 20 O6/30/22 HAD NPA200.6 Barium, ug/1 0.04 20.0 774 10.6 549 07/01/22 NAB BPA700.9 Beryllium, ug/l 0.02 1.0 0.04 J --- U 0.04 J 07/05/22 LFJ EPA200.6 Cadmium, ug/l 0.04 1.0 --- U --- U --- U 06/30/22 NAB EPA200.8 Cobalt, ug/1 0.02 1.0 3.9 --- U 6.4 06/30/22 NAB $BA200.B Total Chromium, ug/l 0.12 5.0 22 --- U 19 06/30/22 NAB BPA200.$ 0.04 10.0 0.20 J 0.0$.T 0,74 J 07/01/22 NAB F.PA200.6 Copper, u9/1 iron, 4.96 50.0 24921 30 J 16940 06/20/27 LFJ EPA200.7 ug/l Manganese, ug/l 0.31 10.0 1476 0,31 J 732 06/20/22 LFJ aPA200.7 0.03 5.0 0.11.3 --- U 0.16 J 07/01/22 NAB 19PA200.$ Lead, ug/l 0.05 0,20 --- U --- U --- U 06/23/22 MTM 245.1 R3-94 Mercury, U1/1 0.03 10.0 4.11 0.34 J 3.6 J 07/01/22 NAB EPA200.$ Nickel, ug/l 0.05 10.0 0.99 J 0.20 J 1,0 J D6/30/22 NAB 8PA20O•S 6elenium, ug/1 5.0 --- U --- U --- U 07/01/22 NAB EPA200.6 Silver, %Ag/l 0.22 0.02 1.4 --- U 0.07 J 0.05 J 07/05/27 LFJ EPA200.9 Thallium, ug/1 U --- U 06/30/22 NAB EPA200.0 Tin, ug/1 0.05 100.0 --- U --- Vanadium, ug/1 0,04 1.0 6 0.36 J 7 06/30/22 NAB 9PA200-a Zinc, ug/l 0.17 10.0 2.8 J 19 1.6 J 07/O1/22 NAV BPA200.S Sulfide, ug/1 100 1000 --- U --- U --- U 06/17/22 LFJ 450002D-11 Conductivity (at 7$c), uMhaa/cm 1.0 1.0 3670 531 3190 06/14/22 NNa 2510E-11 Dissolved Oxygen, mg/1 0.1 0.1 0.52 1.97 1.44 06/14/22 NN1C 450000-16 22 21 20 06/24/22 JWT 25SOR-10 Temperature, °C 12,00 13,97 12.00 06/14/22 JWT Static Water Level, feet Well Depth, feet 22.24 52.30 23.44 06/14/22 JWT +157 +129 +166 06/14/22 JWT 25BOB-11 ORP, my Turbidity (Field), NTU 1.0 2.0 5.22 --- U 4.66 06/14/22 JWT 21301-11 J . notimated value between t" MDL and MRL, U = Below ALL Qu*ttitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Emlwquhfilmfly `d, A(n-wpo-aNM Drinking Water IDL 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHZTEHURST 802 RECYCLING LANE GREENVILLE, HC 27834 REVIEWED BY; f I BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(16) MW3S PARAMETERS, UV/1 MPL tdRL 1. Aaensphhhene 2.66 10.004 - D PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID; 6003 A ANALYST; HIC DATE COLLECTED: 06/14/22 DATE EXTRACTED: 06/16/22 DATE ANALYZED: 06/17/22 DATE REPORTED: 07/12/22 NW-3D MW-3A --- D 6.49 J a - 8etim2tad value between the MDL and MRLr D . @eloW ALL 0uarttit¢Cion Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D NUME `fin Mqa o 1 PHONE (25?) 'r,9s-6208 114 OAKMONT DRIVF- FAX (252) GREENVILLE, N,C 27858 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 x mR. .7t7DSON WHITEHURST 802 RECYCLING LANE ANALYST: TAP GREENVILLE, NC 27834 DATE COLLECTED: 06/14/22 Page: 1 DATE REPORTED: 10/13/22 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Data Analyzed 66/23/22 06/22/22 06/22/22 06/22/22 M47-30 MW-317 MW-3A Trip PARAMETERS, ug/i MDL MRL Blank 1. chloromethans 0.77 3.00D --- u ••• V --- u --- U 2. vinyl chloride 0.12 4.200 --- U --- u --- u '"" u 3. BromomethaAw 0.67 10.000 --- U •-- u --- U --- V 4. Chloroathans 0.49 10.000 a --- a --- u -•- V S. Trichloro€luoromethanm 0,24 1.000 ••^ U --- u --- u --- u 6. 1,1-Dichloro0thsne 0.17 5.000 u --- U "-- u ••- U 1. Acetone 3.06 100.000 11.50 J --- u --- u --- u 0, iodomethans 0.26 10.000 --- u ""- U --- U "` u 9. Catbon Disul€idm D.23 100.000 --- U u --- U -•• u 19, Methylene Chloride 0.64 1.000 ••. U •-- U '"' V " - u 11. tram-1,2-Dichloroethene 0.23 5,000 --- u --" u --- u 12. 1,1-Dichloroethane 0.20 5.000 •-- V --' V '-- u --- u 13, vinyl Acetats 0.20 50.000 --- U -"• u --" u •"- U 14• Cis-1,2-Dichloroethene 0,25 5.000 ••- V u " ' V U 15. 2-Butknone 2.21 100.000 --- u --- u --- U -" u 16, Sromochloromethane 0,21 3.000 --- a --- V ... V '•' u 17. Chloroform 0.25 5.000 -^^ V "- u --- u --- u 10, 1,1,1-Trichloroathans D.19 1.000 --- U -- U _•• t1 --- U 19, Carbon Tstrachloride 0,04 01200 --- V •-^ A --- u '-- u 20. Barissne 0.24 1.000 2.30 --- 11 0.Be J --- V 21. 1,2-Diohloroethan0 0.02 0.200 0.09 J --- U 0,04 ,7 -'- u 22, Trichlorosthens 0.23 1.000 --- u --- u --- U --- u 23. 1,2-Dich1oropYOP4n0 0.04 0.200 0.09 J --- u --- u -"` Ai 24. 13runtodichloromethAA6 0.04 0.200 --- U --• u --- u --- u 25, Cis-1,3-DiChloropropsns 0.06 0.200 --• U -" U 26. 4-Methyl-2-Perttanbne 1.29 100A00 --- U --- u --- u --- U 27. Tolueno D,23 1.000 0.31 J .•• u --- V "•• V 28, tram-1,3-DichloXopropene 0.04 0,200 --- u --- u u --- u 29, 1,1,2-Trichloroethans 0,03 0.200 --- V --- u V ••. V 30, Tetrachlorosthens 0.20 0,200 --- V --- V '-- u --- u 31, 2-Hsxan0n1b 1,57 50.000 __. U --- u __. u •-- u 32, Dibromoohloromethane 0.03 0,200 --- V --- u -'- u 33, 1,2-DibrOMOethane 0L03 0.200 --- u --- u "-- u --• u 34. Chlorohenzene 0.30 3,000 --- II u --- u --- U 35. l,l,l,a-Teerachlorosthane 0.22 1.000 ••• u u ••• u --- V 36. Ethylbenzen■ 0.21 1.050 --- u --- u --- u --- u $7• xylsnss 0.68 5.000 ••• u u --- V --- U 3B. ❑ibromomethane 0.20 1,0.000 --- u --- u --` u --- u 39. Styrene 0.19 1.000 --^ U u '"- V 40. sromoform 0.20 3.000 --- u `-" u -". u --- u 41. 1,1,2,2-Tetr"hloroathans 0.03 0,200 0,06 J --- u 0.06 J --- U 42. 1,2,3-Trichloropropane 0.09 0.200 --- V --- ❑ --- U --- U 43. 1,4-Dich1or0b9A;0n0 0.39 1.000 --" u --- v --- u --- u 44. 1,2-Diohlorobenzone 0.32 5.000 ^-^ U --- V --- u -'- U 45, 1,2-Dibromo-3.Chloropropane 0.07 0.200 -"- U --• u --- A7 --• V 46. Aory2Onitrile 2.72 200.000 --- U --" U -"- U --- U 47. Crane-1,4•DiOhloro"2-autsnm 0,42 100.000 --- u " " V -'" u J - ZS tilRated value between the KDL and MRL, u - Below ALL ¢uantitation LimitY. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Elau" n(MR(m m OC t17 h - ' K' O)WM '@0 114 OAKMONT DRIVE GREENVILLE, N.C. 27B58 PHONE (252) 756.6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 X MR. JUDSON WHITEHURST 802 RECYCLING VANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 06/14/22 DATE REPORTED: 10/13/22 REVIEWED BY: ; LANDFILL APPENDIX IY EPA METHOD 8260D R4(18) npte Analysed 06/23/22 06/2a/22 06/22/22 06/22/22 mw-38 Mw-30 NW -AA Trip PARAMP,TERs, ug/1 MDL KRL Blank 40. Atrolein 1,97 4.000 --- U --- U --" U 49. Allyl Chloride 0.20 10.000 --- U -" U --- V --- U 50, Chloroprene 0.21 20.000 -•- V --- U -,- U --- V 51. 1,3-Diahlorabenzene 0.41 5.000 --- U --- U --- U --- U 52, Dieh1orodifl4orPmethans 0.51 5.000 --- U --- U - U --- U 53. 2, 3 "DichlaraprOpAn* 0.28 1.000 --- U --- U --- U --- U 54, 2,2-Dichlogopxopane 0.27 15,000 --- U --- U --- U -" U 55, 1,1-Dichlorcpxopefle 0.22 5.000 --- U --- U --- U --- U 56. Sthyl Methek=Ylata 0.16 10.000 '-- U - U --- U --' U 57. Hexachlorohutadiane 0.10 0.200 --- U --- D --- U --- U 58, Isobutyl A?Cohol 22.80 1001000 --- U --- U --- U --- A 59, Methacrylanitrile 1.93 100.000 --- V --- U --- U --- U 60. Methyl Methperylats 0.25 10,000 --- U --- U --- U '-- U 61, Naphthalene 0.47 6.000 7.00 --- U 0.92 J --- U 62. Fropionitrile 3,z6 1$0.000 U --- U --- U --- U 63, 1,2,4-Trichlorobenznns 0.50 10.000 --- U --- U --- u --- U 64. ACatbnitrile 36.29 55.000 --- U --- U " - U -'- U 65, Tetrahydrofuran 0.39 1.000 32.40 --- U 25.20 --- U 66. 1,4-Dioxane 2.71 3.000 118.00 --- U 92.00 --- U Page: 2 i . $atimated value between the MDL and MRL, U z A510W ALL Quantitation Limits. NGFE: EPA METHOD 8260D R4 (18): MW-3S received at pH >2. DocuSi 0 M ut m m z 10 C) Ln Ci'i co c5so�?(It y11 CIIVCIVpC iU. IOU , rD _ co m T -- 4 O � CQ7 r G1 � ..� GTSA � N ��• �y QO G� S F. 0 0 �y ?� m m TC rAL CHLORINE, mgn m OR ug/l AT COLLECT}V �E �,rrV 1..i cn TEMPERATURE,'C z C n Z m f' AT COLLEC HON rn <n in D # QR CONTAINERS i w Field DH = v Nitrate+Nitrite Alkalinity ALL ��} Chloride TDS m m m Sulfate Y "d metals sulfilie Coda ctivit DO .. ,'; # ,s; „t r#' ; . Telra erature Field Parameter . 8270E Dup. 1 L� s : 8270E Dup. 2 Y C7� 8270E Dup. 3 C tf" 8260D A . I1 rn cn n PARAMETERSrrESTS z } t-n22 a [} Z fil /\cn ni «y Z d FIR 77 C Li l ay -n I"YI S7 ` Z m :5E ] �# y o M y n rM o C p m y 5 hi hi DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61 B-5E8AB648F1 3D 0 ti 0 m m { ZD-0 z a 0 O0 w n r m > C CA a C� rn r c C��Q~ �J i�'rea r�x a'�'' c a Eu r W y y+ n [7 lG) 1 W� Fn -A d CSC C"r IM1 4 _ 1 F --- � �i ■X_ m m TOTAL CHLORINE, mgll C� m OR ug(i AT COLLECTION vn 0 c Q 7. c f5� 0 C x [n TEMPERATURE, 'C f" ' AT COLLECTION m o u CD z ff OF CONTAINERS w w w € s}, ,?'; 8260D App. 112 C� 8260D A . 113 M 0 r # 1 01,1141 �w IL m m_ rn ,. rrt b -TT � u P 7 } AT + �A- iti } {Y CO C-1 PARAMETER5ffE5TSi o = 3n F. y �x p z •� F. � c ; �x z 7r5 m z. cn _ Tu a a 50 m „ rn o m m U7 � C' m cn O C rnn rm In rtl m 4 0 I 2 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 OAKMC)N7 OLIVE fiREENVILLE. N G. 2T856 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking water ID: 3771S Wastewater ID: 10 FAX (252) 766- 015 ID#: 6003 DATE COLLECTED: 06/15/22 DATE REPORTED : 10/13/22 REVIEWED BY: NW-4 MW-5 MW-6 taw-7 MW-8 Anelybis Method PARAMETERS MDL MRL Date Analyst Cade PH (field measurement), Units 6.2 619 6.9 6,7 6.8 06/15/22 PJC 45DOND•11 Nitrate4witrite as N, mg/1 0.04 0.04 --- V MISSING 0,84 0.25 --- V 06/21/22 $39 353.2 R3-93 Alkalinity (to pH 4.5), mg CaCO3/1 1.0 1.0 605 38$ 040 1019 7200 06/20/22 DIJ 2320E-11 Chloride, mg/1 110 1.0 14 55 6$ 67 168 06/20/22 HCB 4509CLB-11 Total Dissolved Aasiduer mg/l 10 10 250 $20 06/16/22 HMV D5907-13 Total Dissolved Residue, mg/1 10 10 M 1100 M 1200 M 2000 06/20/22 HMV D5901-13 sulfate, m5/1 5.0 5.0 59.5 229 127 06/21/22 MTM 4500SO42311 sulfate, mg/1 5.0 5,0 88.0 244 96/30/22 MTM 45008042011 Antimony, ug/l 0.03 1.0 0,10 J 06/30/22 NAB EPA200.8 Aptimony, ug/1 0.03 1.0 0-40 J 0.06 J 0,0$ J 0.12 J 07/05/22 LFJ EPA200.6 Arsenic, ug/1 0.00 5.0 0,75 J 06/30/22 NAB BPA200.8 Arsenio, ug/1 0.08 $,0 24 9 19 27 07/01/22 NAB BPA200.8 Barium, ug/1 q.04 10.0 50,6 07/01/22 NAB BPA200.8 Barium, ug/1 0.04 10A 276 407 564 572 07/05/32 LFd EPA200.8 Beryllium, ug/1 0.02 1.0 0,09 J 0.41 1 0.02 J 0.04 J 0,02 J 07/05/22 LPJ BPA200.8 Cadmigm, ug/1 0.04 2A --- C 06/30/22 NAB EPA200.8 Cadmium, ug/l 0,04 1.0 0.31 J --- ❑ --- U --- U 07/01/22 NAB SPA200.8 Cobalt, ug/l 0.02 1A 0.15,7 06/30/22 NAB EPA200.8 Cobalt, u9/1 0,02 1.0 4.1 2.0 14 2.6 01101/22 NAB EPA200.8 Total Chromium, ug/l 0.12 5.0 1.91 06/30/22 NAB EPA200.8 Total Chromium, ug/l 0.12 5.0 19 7.0 11 24 07/01/22 NAB 'EPA200.8 Copper, ug/1 0.04 10.0 0.19.I 8 J 0.44 J 0.35 J 0.15 a D7/01/22 NAB EPA200.8 Iron, ug/1 4.9$ 50.0 3473 50$90 14443 45321 30181 09/20/22 LFJ EPA200.7 Manganese, ug/1 0.31 10.0 54 376 742 806 911 06/20/22 LFJ BPA200.7 Lead, ug/1 0.01 5.0 0.30 J 6.7 0.15 J 0.08 J 0.05 J 07/01/22 NAB EPA200,0 mercury, u9/1 0.05 0,20 --- U --- U --- V --- U --- U 09/23/22 MTM 245.1 R3.94 Nickel, vg/1 0.03 10.0 0.26 1 9.91 l.dJ 1.9J 1,0J 07/01/22 NAB RRAa00.8 Selenium, ug/1 0.05 10.0 0.49 J 06/30/22 NAB EPA200.8 Selenium, ug/1 0.05 10.0 0.541 -- V --- U --- U 07/01/22 NAB RRA200,0 Silver, u9/1 0.22 5.0 --- U --- U --- U --- U --- U 07/01/22 NAB EPA200.8 Thallium, ug/1 0,92 1.0 0.14 J 0.12 J --- U 0.04 J --- U 07/05/22 LFJ EpA200,8 Tin, ug/1 0.0$ 100.0 --- U 04/30/22 NAB EPA200.8 Tin, ug/1 D.05 100.0 275 a.11 J --- U 0.28 J 07/05/27 LFJ EPA200.8 vanadium, ug/1 D.04 1,0 3 Q$/30/22 NAB EPA200.0 Vanadium, ug/1 0.04 1.0 20 7 2 4 07/01/22 NAB EPA200.9 zinc, ug/1 0.17 20.0 0,84 J 33 2.8 J 1.5 J 0.89 J 07/01/22 NAB BPA200.8 Sulfide, ug/1 1g0 1000 --- U HIBBING --- U --- V --- U 06/17/22 1,FJ 4500s2D-11 Conductivity ;at 25c}, uMhos/cm 1.0 1.0 437 1370 2796 1850 3592 06/15/22 FCC 2510E-11 Dissolved Oxygen, mg/1 0.1 6,1 1.83 MI85ING 3.55 2.10 2.40 06/15/22 F.IC 4500Da-16 Temperature, °C 21 29 22 25 22 06/15/22 F,7C 25SOD-10 statin water Level, feet 7.64 7.10 10.33 9.29 10.27 06/15/22 PJC Wall Depth, feet 15.4$ 9.50 16.65 16.33 20,26 06/15/22 PJC All 0C regu1r*M6nte were not matt M Blank result exceeded method constAnt weight criteria. J . Satimated value between the MDL and MRL, V . Below ALI, QUantitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D LA 114 OAKMONT DRIVE GREFNVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVXLLE, NC 27834 PARAMETERS GRP, my Turbidity (riaiw, , NTU Mw-4 Mw-5 MDL MRL +59 MISSING 1.0 1.0 9.54 MISSING wi,ist NMtax 261 to PHONE (252) 756-6208 FAX (252) 756-0633 Tn#: 6003 DATE COLLECTED: 06/15/22 DATE REPORTER : 10/13/22 N REVIEWED BY: Mw-6 MW-7 Mw-8 Analysis H4thod Late Analyst Cod* +6u +a2 +163 06/15/22 P.TC 25608-11 9.73 8.72 8.69 06/15/22 P.TC 21300-11 All QC requirement& were not mats M Blank result exceeded method constant weight criteria. G . Estimated vale between the MLL And MRL, u . Below ALL Quantitatian Limits, DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 OAKMONT DRIVE GREENVILLE. N.C. 27858, Drinking Wet#Y IVI 37115 Wa+ltewater IDI 10 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 SIR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: HIC GREENV'ILLE, NC 27834 DATE COLLECTED: 06/15/22 DATE EXTRACTED: 06/16/22 DATE REPORTED: 10/13/22 REVIEWED BY:�' BA9E/N'EUTRAL COMPOUNDS EPA METHOD 8270E R6(18) Date Analysed 06/17/22 09/20/22 06/20/22 06/20/22 mW-4 NW-6 mW-7 mW-8 PARAMETERS, Uq/1 MDL XRL 1, Acenaphthen■ 2.66 10.000 --- ❑ '"' a --- u --- ❑ a . satimated Value between the MOL and MRL, ii . Below ALL auantitatian Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D LNV0�(jo 2 1[h t�-001Nv, �U I�IN 00 114 OAKMONT DRIVE GREENVILLE, N.C_ 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY! �y LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking Water 1D, 3771$ Wastewater Mt 10 FAX (252) 756 0633 CLIENT ID: 6003 ANALYST: ,7AP DATE COLLECTED: 06/15/22 Page: I DATE REPORTED: 10/13/22 PARAMETERS, uU/1 Date MDL Analyzed: MR1, 06/22/22 MW-4 06/22/22 mw-6 06/22/22 NW-7 06/23/22 NW-8 06/23/22 Trip Rlank 1. Chloromathans 0,77 1.000 --- U --- U --- U --- U --- U 2. vinyl Chloride 0.12 0.200 --- U --- U --- U --- U --- U 3. Bromomethene 0,67 10.000 --- U --- U --- U --- ❑ --- U 4. Chloxoothanw 0.40 30,000 --• U --- U --- U --- U --- U 5, TriOhlQrofluoromethRn4 0.24 1.000 --- U •-- U --- U --- U --- U 6. 1,1-Diahloroethene 0.17 51000 --- U --- D --- U --- U --- U 1. Acetone 9.06 100,000 --- U --- U --- U 10.50 J --- U 0. lodomethane 0.26 10,000 --• U --- U --- U --- Ti --- 9. Carbon Disulfide 0.23 100,000 --- U --- U --- U --- U --- U 10. Methylene chloride 0.64 1.000 --- U --- U --- U --- U --- U 11. trans-2,2-Dichloroathene 0.23 5.000 --- U --- U --- U --- U --- U 12, 1,1-Dichloroethans 0.20 5.000 --- U --- U --- U ,- U --- U 13. vinyl Acetate 0.20 50,000 --- U U --- U --- U --- U 14. Cie-1,2-Dichloroethsne 0.25 5.000 --- U --- U --- U --- U --- U 15. 2-Butanons 2.21 100,000 --- U --- U --- U --- U --- U 16, Bromochloremethane 0.27 3.000 --` U --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U --- U --- U 18. 1,1,1-Trichloroethans 0,19 1.000 U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0,200 --- U --^ U --- U --- U --- U 20, Benzene 0.24 2.000 U - U --- U --- U --- U 21. 1,2-Diehlorcethane 0.02 0,200 --- U --- U --- U 0.04 J --- U 22, Trichloroethene 0.23 1.000 --- U --- U --- U --- U --- U 23. 1,2-Dtchloropropane 0.04 0,200 --- tr --- U --- U 0.04 J --- U 24. Bromodichlor0Metheee 0.04 0.200 --- U --- U --- U --- U --- U 25, Cie-1,3-Dichloropropene 0.06 0.200 --- U --- U --- U -- U --- U 26. 4-Methy2-2-Peht4fl4Sle 1.19 100.000 --- U --- U --- U --- U --- U 27. Toluene 0,23 1,000 - it --- U --- U -` U --- U 26. trans-1,3-Diohloropropene 0.04 0.200 --- U --- U --- U --- U `-_ o 29, 1,1,2-Triohloroathana 0.03 0.200 --- U --- U --- U --- U --- U 30. Tetr6Chlb4rOethe86 0.10 0.200 --- U --- U --- U --- U --- U 31, 2,[38xanone 1.51 50,000 --- U --- U --- U --- U --- U 32. DibrbNl4C1710Y4meChane 0.03 0.200 --- U --- U --- U --- U .-- U 33. 1,2-Dibromoethans 0.01 0.200 •-- U --- U -- U --- U ^- U 34. Chl*raben2ene 0.30 3.000 --- U --- U •-- U --- U __- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.000 --- U --- U --- U --- U --- U 35, Ethylbenzene 0.21 1.000 --- U --- U --- U --- U .-- U 37. %ylene■ 0.68 5.000 --- U --- U --- U --- U --- U 18, Dibromomathane 0.29 10.000 --- U --- U --- U --- U --- U 39. Styrene 0.19 1.000 --- U --- U --- U --- U `-' V 40. Bromoform 0.20 3.000 --- U --- U --- U --- U --- U 41. 1.1,2,2-Tetrachloroethane 0.03 0,200 --- U --- U --- U 0109 LT --- U 42. 1,2,3-TriCh1*ro9r0Pan8 0.09 0.200 --- U --- U --- U --- U --- U 43, 1,4-Dichlorobenzens 0.39 1.000 --- U --- U --- U U --- U 44. 1,2-DiCh14S4benZene 0.32 5.000 --- U --- U --- U --- U --- U 45, 1,2-Dibromo-3-Ch2oropropdnd 0.0'7 0.200 --- U --- U --- U - U --- U 46. Acrylonitrile 2.72 200.0D0 --- U --- U U --- U --- U 47, trans-1,4-Dichloro-2-Butend 0.42 100,004 --- u --- U --- U --- U --- U J s Estimated value between the NDL and NRL, U - Below ALL Quantitatian Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D I R000 q Own NO 114 OAKMONT DRIVE GREENVILLP. N.C. 27868 CLIENT: C & D DISPOSAL, INC. MR. J=SON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BYt LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking Water M 37715 Wastewater ID: 10 PHIGf4L-. t"'-'2} FAX (252) 756-0633 CLIENT TD; 6003 ANALYST: JAP DATE COLLECTED: 06/15/22 Page: 2 DATE REPORTED: 10/13/22 Date Analyzed: 06/22/22 06/22/22 06/22/22 06/23/22 06/23/22 MW"4 MW-6 bsw-7 NW-B Trip PARAMETERS, ug/1 MDL XRL Blank 48. Acralein 1.37 4.000 --- U --- U --- U -"' U --- U 49. Allyl Chloride 0,20 10.000 --- U --- U --- tl --- U --- U 30. Chloroprena 0.21 20.000 ... U --- U --- U --- U --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U --- U --- U --- U -"' U 52. Aighlorodieluor0methan9 0.51 5.000 --- U --- U --- [1 --- U U 53. 1,3-Dichloropropane 0.20 1.000 --- U --- U --- U --- U --- U 54. a, 2-Dichlorayropane 0.17 15.000 --- U --- U --- U --- V " - U 55. 1,1-D14hlaropropens 0.22 5.000 --- U --- U --- U --- U --- V 56. $thyl Methacrylat• 0.16 10.000 --- U --- U --- U --- U --- U 57. Hexachlorobutadiene 0.10 0.200 --- U --- V --- U --- U --- U 58, ieobutyl Alcohol 12,80 100.000 - U --- U --- U --- U --- U 39. Nethar-rylonitrile 1.93 100.000 --- U --- U --- U --- U --- U 60. mathyl Hathaorylate 0.25 30.000 -- U --- U --- U --- V --- U 61. Ndphthalena 0.47 6.000 --- U 2.41 J --- ❑ --- U --- U 62. Prapionitrile 3.26 150.000 --- U --- U --- U --- U --- U 63. 1,2,4-Trichlorobenxene 0.50 10.000 --- U --- U --- U --- U --- U 64. ACetonitrile 36.29 55.000-- U --- U --- V --- U --- U 65. Tatrahydrvluran 0.39 1.000 --- U 7.65 8.67 19.90 --- U 66, 1,4-Dioxane 2.71 3.000 --- U 8.66 4.33 64.00 U U - Satimatrd value between the NDL and MRL, V - Below ALL puantitation Limits. NOTE: EPA METHOD 8200❑ Ito (18): MW-8 rcccived at pl l }2. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D rn m m m B n Cw rr c z o j. FR �Q vi fad ='O a C p OC 01 _ n � - - e+ 1 m w TOTAL CHLORINE, mg1l b OR ugll AT COLLECTION i•� TEMPERATURE, °C O m " 1-11 ` AT COLLECTION CrJ 0 a z � OF CONTAINERS m 4h w w w to in Field ptl � Nitlrate+NitriteAlkalin K Vw .tChloride "0 TDS Sulfate Metals4*4 air' �; ::�:�,,: 'ii'::. .�,;�#t•� Sulfide Il'. C.v.7f 's}r ..�: :v:`y�`AL A %';#"+' #' ES Condnetivit Y as �mga #v' 'rrsrrr Temp eYatUCe F �C Field Parameter 8270E Dup. 1 Y G� 8270E Du 2 > C] p. 8270E Dup. 3 .. ssVr,{� 'r#° #% �h 'dry, r 8260D A pp• II rr.�,, ry PARAMETER5ITESTS _ m m p O � � � � rrnn cn w tQ r ��* m O k, Q cea r it y m �m-� 70 In m FD �C� y0 �DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D o W r) o NP r rc 1 m m- 4 7 Q C" GC ch � w m xa Vrgp� r m , m �1 y ^ 4 N a r n .4za q �.. o m mm !' y rr W JJ rri CD a m rri TOTAL CHLORINE, mgH i� A.wr' ti OR ugll AT COLLI=CTION 14 V TEMPERATURE, "C AT COLLECTION Z 0 O ' �„ r �„ k., ff OF CONTAINERS Cr3 x a � 4L w w w in cn cc 87.60D App. II 2 CD c� rnr'#;. rr,•;;: $260D App. II 3 cn m 8260D App. ] I 4 tilf•itif :is�}}i;$: :r t�F� 'v1{V' 4fih+ 01VC > 8270E B/N V) rn rn F in Cf5 w cr 41 Q m cr P? O cr Cti < T 4 0 C- � 2- cl, ib � cn w 3 W � `-° °i �' w c, PARAMETERWESTS m CD CD .. C'S C�17 4 2 N rn m[n cn V •� t7 = O p I .Fn is fl 10 R c7 T r m � p p n z LU1' 4 m Q 4 T DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Nowb� r NNW- 1- 114 OAKMONT DRIVE GAEENVILLE, N-C. 27858 C & D DISPOSAL, INC. MR, =SON WHITEHURST 802 RECYCLING LAN9 GREENVILLE, ETC 27834 PARAMETERS Nitr* to*K'trits as N, m9/1 sulfide, ug/l C4rtduttivttY fat 25c), uHhos/cm Dissolved Oxygen, mg/1 Temperature, 'C static Water Level, fast Well Depth, feet NW-5 MDL MRL Analysis MethQd Date Analyst Coda Drinking Water TD, 3771$ Wastewater 1D: 10 FAX (252) 756-063,', ID#! 6003 DATE COLLECTED: 06/16/22 DATE REPORTED : 10/13/22 REVIEWED BY: 0.04 0.04 0.06 06/21/22 xES 353.2 R2-93 100 1000 --- ❑ 06/17/22 LPJ 450Os2D-11 1.0 1.0 1657 06/16/22 2JC 2510B-21 0.1 9.1 4.60 06/16/22 PJC 45000G-16 as 06/16/22 7JC 2550E-10 7.10 06/16/22 Pic 9.$0 06/16/22 PJC J - Estimated veYue between the MDL and MAL, C . Below ALL Ruantitativn Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D l3 U kWou Poo T AB do 114 OAKMO147 DRIVE GRFENVILLE, N.C. 27858 ,T Drinking water TD, 37715 wastewater SD: 10 i= I li d f_ t,�:)�) r'It] I,C".1tj FAX (252) 756.0833 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 MR. =80N WHITEHURST 802 RECYCLING LANE ANALYST: L7AF GREENVILLE, NC 27834 DATE COLLECTED: 06/16/22 Page: I DATE ANALYZED: 06/23/22 DATE REPORTED: 10/13/22 REVIEWED BY LANDPILL APPENDIX II EPA METHOD 8260D R4(18) PARANSTUR8, ug/1 Mr. MRL KW-5 1. Chloromethane 0.77 1,000 --- U 2, Vinyl Chloride 0.12 0.200 --- U 3. Bromomethana 0.¢7 10.000 --- U 4. Chloroathana 0.48 10.000 -- U 5, Trichlorofluoromethans 0.24 1.000 --- U 6. 1,1-Dichlorcethefta 0.17 $.000 --- U 7. Acetone 9.06 200.000 -- U a. I0domethana 0.26 10.000 -•- U 9. Carbon Disulfide 0,23 100.000 U 10, Mathylene Chloride 0.64 1.000 --- U 11. trana-1,2-Dichlorcathene 0.23 5,000 --- U 12. 1,1-Dichloroethan6 0.20 5.000 --- U 13, Vinyl Acetate 0.70 $0,000 --- U 14. Cie-1,2-DichloYoethehe 0.25 5.000 --- U 15, 2-Butanone 2.21 100.00D --- U 16. SYvm4ohloromethene 0.27 3.000 --- V 17. Chlorofcrm 0.25 5.ODD --- U 18. 1,1,1-Trichloroethane 0.19 1.000 --- V 19, Carbon Tetrachloride 0,04 0.200 --- U 20. Benzene 0.24 1.000 --- U 21, 1,2-Dichloroethane 0102 0.2DO 0.02 S 22. Trichloroethene 0.23 1.000 --- U 23, 1,2-pichloroprcpane 0.04 0.200 --- U 24. Bromodichlorometharia 0.04 0.200 --- U 25. Cie-1,3-Dichloropropene 0.06 0.200 -- t! 26. 4-Methyl-2-Pentanons 1.19 100.000 --- U 27. TolUene 0.23 lA00 --- U 26. trans-1,3-DiehloropYOpene 0.04 0.200 --- U 29, 1,1.2-Trichloroethane 0.03 0,200 --- U 30. Tat rachloroatheme 0.10 0.200 --- U 31. 2-Hexanons 1.57 50.000 --- U 32. Dibromochloromethane 0,03 0.200 --- U 33. 1,2-Dibromoathana 0.03 0.200 --- U 34, Rhlorobenzene 0.30 3.000 --- U 35. 1,1,1,2-Tetrachlorcethane 0.22 1.000 --- U 36. ®thylbenzene 0.21 1.000 --- U 37, xylanea 0.68 5.090 --- U 38L Dibromomethans 0.28 10.00D --- U 39, Styrane 0.19 1,000 --- U 40. BromcPorm 0.20 3.000 --- U 41, 1,1,2,2-Tetrachloroathans 0.03 0.200 --- U 42. 1,2,3-Trichloropropane 0.09 0.2DD --- U 43. 1,4-Dichlorobenzens 0.39 1.000 --- U 44. 1,2-%ChlorotenlRene 0.32 5.000 --- U 45. 1,2-Dibromo-3-Chloropropans 0.07 01200 U 46. Acrylonitrile 2.72 200.DOo --- U 47, tYana-1,4-Diahloro-2-19utana 0.42 100,000 --- V 4B. Acrolairi 1.97 4,000 --- U J - Estimated value between the MDL and 1ARL, U - Below ALL Vuantitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 OAKMONT DRIVE GREENVILLE, N_G. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEXURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; LANDFILL APPENDIX II EPA METHOD 8260D R4{18) Drinking Water IDi 37715 }}rr Wastewater ID, 10 PHC11 J L FAX (252) 756-OU CLIENT ID: 6003 ANALYST: TAP DATE COLLECTED: 06/16/22 Page: 2 DATE ANALYZED; 06/23/22 DATE REPORTED: 10/13/22 PARAMETERS, ug/l MDL MRL KW - 49. Allyl chloride 0.20 10.000 --- U 50, Chloroprene 0.21 20,0to --- U 51. 1,3-Dichlorohanzene 0.41 5.000 U 52. Dichlorodiflueromethane 0,51 5.000 --- U 53, l,3-DichiaroprapaAv 0.20 1,000 --- U 54. 2,2-Dichloropropane 0.17 15.000 --- U 5$. 1,1-DichlorvpYOp4Y1• 0.22 $.000 --- U 56. Ethyl Methaerylate 0.16 10.000 --- U 57. }texa4hl0#ObuCediene 0,10 0.200 --- U 50, Imobutyl Alcohol 12.80 100.040 --- U 59. Methacrylonitrile 1.93 100.DDO --- U 60. Methyl Methacryldtb 0.25 30�000 --- U 61. Naphthalene 0.47 6.D00 --- U $2, Propionitrile 3.26 150.000 --- U 63. 1,2,4-Trichldr4benzene 0.50 10.000 -^- U 64, Rdetonitrila 36.29 55.000 -- U 65. TetrahydrofUran 0.39 1.000 8.17 56. 1,4-D14xene 2.71 3.000 42.40 d - Satimated value between the MDL and :QRL, U - gelew ALL 4uantitation Limits. DocuSign Envelope ID: 3C85( Ln C cn fn a" m ED 9C9 OCA-z C23-E i E8AB648F13D Ln N � J W m A TOTAL CHLORINE, mgll d ' Ofi ugll AT COLLECTION m o Q 4 x ' TEMPERATURE,' < ATCOLLECTION ran 0 m 0 OF CONTAINERS C-) �• 0 C-) r G1 C iC�3i O y rn v -rn U7 �a ( y m " m C n7 m y cn C5 a C-) LJ"k z MW PARAMETERSITESTS I 0 � m Q Z _ rtro _ m mi m cn O m r m f � _ O N Q O m n 0 z DocuSign Envelope CI ID: 3C8509C9-30CA-4C23-B61 m B-5E8AB648F1 3D p 'a e r� cn N R° • c ! u7 06 O m y� G] G? C,� f"} r Z5 p-J 0 rro A w o'Or t: a m m m m 1W m m TOTAL CHLORINE.mgll �j o m m m OR ugll AT COLLECTION L�1 � � v - Z � C7 TEMPERATURE,°C m m ATCOLLECTION m O ri OF CONTAINERS Z Z rz } PARAMETERS/TESTS K Tm Q 2 cl p r O rn r�r (n r !� 1� " 4 r � c rrrr O 2 a 9 q 2 o m m z � 0 r i- rQ DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D knwdroo MUNO [IV t A �-)QP0m UNd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 602 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 ID#1 6003 C DATE COLLECTED: 06/16/22 DATE REPORTED : 10/13/22 �r REVIEWED BY: SW-1 SW-2 SW-3 SW-4 Trip Analysis Method PARAMETERS MDL MRL Blank DAtb Analyst Cado PH (Bald meanurement), units MISSING MISSING 7.2 7.5 96/16/22 PJc 4500HB-11 Antimony, uq/1 0.03 2.0 MISSING MISSING 0.61I7 2.3 07/05/22 LFJ EPA200,9 Axaenic, ug/l 0.08 5.0 MISSING MISSING 5.6 2.6 J 07/11/22 NAB EPA200.8 Barium, ug/1 0.04 10.0 MISSING MISSING 124 07/11/22 NAB EPA20O.B Barium, ug/l 0.04 10.0 $0.7 07/05/22 LFJ EPA200.8 50ryllium, u9/1 0.02 1,0 MISSING MISSING 0.24,7 0.39 J 07/05/22 LFJ EPA200.8 Cadmium, ug/l 0.04 2.0 MISSING MISSING 0.30 0 0.65 J 07/05/22 LFJ EPA200.8 robAlC, U5/1 0.02 1,0 MISSING MISSING 1.7 1.0 07/D5/22 LFJ EPA200.8 Total Chromium, ug/I 0.12 5.0 MISSING MISSING 3.2J 2.4 J 07/05/22 LFJ EPA200.0 copper, u9/1 0.04 10.0 MISSING MISSINQ 16 13 07/05/22 LFJ EPA200.8 Lead, ug/l 0.03 5.0 MISSING MISSING 3.6J 3.6J 07/05/22 LFJ $PA200.8 Nickel, µg/1 0.03 10.0 MISSING MISSING 1.1 J 1.a J 07/05/22 LFJ EPA200.8 Selenium, ug/1 0.05 10.0 MISSING MISSING 0.90 J 0,21 J 07/11/22 NAB EPA200.9 Silver, ug/1 0.22 5.0 MISSING MISSING --- D --- V 07/05/22 LFJ EPA200.8 Thallium, ug/1 0.02 110 MISSING MISSING 0.10 J 0.06 J 67/05/22 LFJ EPA200.S vanadium, ug/1 0.04 1.0 M19AINO MISSING 5 9 07/05/22 LNJ 2PA200.8 Zinc, ug/1 0.17 20.0 MISSING MISSING 12 6 A J 07/09/22 LFJ EPA200.S C!pnduntivity (at 25c), uMhoe/cm 1.0 1.0 MISSING MISSING 1i50 816 06/16/22 PJC 2510E-11 Dissolved Oxygen, mg/1 0.1 0.1 MISSING MISSING 1.86 1.59 08/16/22 PJC 45000G-16 TamperAture, 'C MISSING MISSING 23 29 06/16/22 PJC 2550E-10 ORP, my MISSING MISSING +118 +92 05/15/22 PJC 2590E-11 Turbidity (Field), NTv 1.0 1.0 MISSING MISSING 59.80 40.90 06/16/22 PJC 21308-21 All QC rrquiremintM Were not met: M Blank re0u2t exCBadad method tondtant weight criteria. J . gntimated value between the MDL and MRL, ❑ - Below ALL Quantitatipn Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 OAKMONT DRIVE iREENVII*LE, N.C. 27858 CLIENT: C & D D15POSAL, INC. MR. JUDSON WHITEHURST $02 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDVILL APPENnsx II EPA METHOD 8260D R4(18) Drinking water IDi 37725 WAisteWRter M, 10 (FAX (2r,`-') 7' CLIENT ID: 6003 C ANALYST: JAP DATE COLLECTED: 06/16/22 Page: 1 DATE ANALYZED: 06/23/22 DATE REPORTED: 10/13/22 PARAMETERS, u9/1 M0L MRL SW-3 SW-4 Trip Elank 1. Chloromethane 0.77 3.000 --- U --- U "-' U 2. Vinyl Chloride 0.12 0.200 •-- U --- U __- U 3. Eromomethane 0.61 10,000 --- V --- U --- V 4, Chlovoothane 0.48 10.000 --- U -" U --- U 5. Trichlorofluoromethana 0.24 1.000 --- U -^- U --- U 6, 1,1-Dichloroathens 0.17 5.000 --- U --- U --- U 7. Ace tone 9.06 100.000 --- U --- U --- U 0. Iodomethane 0.26 10.0DO --- U --- U "'- U 9, Carbon Diouliide 0.23 100.004 --- U -" U --- U 10. Methylene Chloride 0.64 1.D00 --- U --- U --- U 11, trans-1,2-Diahloroethene 5.000 --- U -•• V --- U 12. 1,1-Diahloroethane 0.20 5.000 --- U --- V --- U 13, vinyl Acetate 0,29 50.000 --- U - U --- U 14. Cie-1,2-Dichlvroethene 0.25 5.000 --- t1 --- V --- U 15, 2-Butanone 2.21 100.000 --- U U --- U lG. hrcmaahloromethane 0.27 3.000 --- U --- U --- U 17. Chloroform 0.25 5,006 --- V --- U --- U i9. 1,1,1-Triahloroethane 0119 1.000 --- U --- U --- U 29. Carbon Tetrachloride 0.04 0,200 ^-- v --- ❑ --- v 20. Benzene 0.24 1.000 --- U •-- U ___ U 21. 1,2-Dichloroethane D.02 0.2G0 --- U --- U =-- V 22. triahloraethana 0,23 1.ODO --- U •-- U " ' U 23. 1,2-DichlorOprop6AO 0.04 01200 --- U --- U U 24, Dromadichloromethane 0.04 0.200 --- ❑ --- U --- U 25. Cie-1,3-DiChlorogr*pene 0.06 0.200 --- U --- U -`- U 25, 4-Methyl-2-Pentanone 1.29 100.000 --- U --- V --- U 27. Toluene 0,21 1.000 --- U --- V --- U 20. tran4-1,3-Dichloropropene 0.04 01200 --- U --- V --- U 29. 1,1,2-Tri4h14r04thane 0.03 0.200 --- V --- U --- U 30, Tatrachloroethene 0.10 0,200 --- U --- U --- U 31. 2-Hexanone 1.57 5D.000 --- U --- U --- U 32, Dibromochloramothana 0.03 0.200 --- U --- U --- V 33. 1,2-Dibromaathane 0.03 0.200 --- V --- U --- U 34, Chlorohenzene 0.30 3.000 --- U --- U --- V 35. 111,1,2-Tetrachloroethane 0.22 1.00D --- V --- U --" V 36• Ethylbenzene 0.21 1.000 --- U --- U --- U 37. Rylenen 0.68 5.000 --- U --- V --- U 38. Dibrom0methAne 0,28 10.000 --- U --- U --- U 39, Styrene 0.19 1.000 --- U --- v --- u 40. BrotaoC4rm 0.20 3.000 --- U ••- V --- U 41, 1,1,2,2•ToLeaChioroethane 0.03 01200 --- U --- U --- U 42, 1,2,3-Trichloropropane 0.09 0.200 -•' U --- U '^^ U 43. 1,4-Dieh2orobenLene 0.39 1.000 --- V --- U -"' U 44, 1,2-Dichlorobancene 0.32 5.000 --- V --- U ^-- U 45. 1,2-Dibrom4-3-❑hloropropans 0.07 0.200 --- U --- U --^ U 46, ACrylonitrile 2.72 200400 --- U --- U U 47. trmne-1,4-Aiphlorp"2-Butene 0.42 100.000 --- U --- U '-' U &$, ACrolein 2.97 4,000 --- U --- U --- U S . $etimeted value between the MDL and MRL, U - eelaw ALL Quantitation Limita, DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D kin'O'nnum ' kc�ouo00 n. d 114 OAKMONT DRIVE GREENVILLE, N.G, 27858 �WIIIW4= V*iktawktiL' rDL to PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 C MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 06/16/22 Page: 2 DATE ANALYZED: 06/23/22 DATE REPORTED: 10/13/22 REVIEWED BY: LANDFILL APPENDIX IT EPA METHOD 8260D R4(18) PARAMETERS, u9/1 MDL MRL Sw-3 SW-4 Trip Blank 49. Allyl Chloride 0.20 x0.060 --- U --- U -•- U 50. Chloragrwne 9.21 20.000 --- U --- U --- U 51. 1,3-DichlDrobenzane 0.41 5.006 --- U --- U --- U 52. Dichlorodilluoromethane 0.51 5.000 --- U ••• U " U 53. 1.3-Die hiorbpropane 0.29 1.000 --- U --- U --- U 54, 2,2-Dichloropropans 0.17 15.000 -•• U U --- U 55. 1,1-Dichloropropene 0122 S.000 --- U ... U --- U $5, Ethyl Methacryldte 0.16 10.000 ••• U --- U --- U 57. Hexachlorobutadlene 0.10 0.200 --- U --- U --- U 50. iaobutyl Alcohol 12.8D 100.000 --- U --- U --- U 59. M6thagrylonitrile 1.93 100.000 --- U --- U --- V 60. Methyl Methacrylmte 0.25 30.000 --- U --- U --- U 61, Naphthalene 0.47 6.000 --- U --- U --- U 62. Propionitrile 3.26 150.D00 --- U --- U --- U 63. 1,2,4-Trichlorobanaene 0.50 10,600 --- U --- U --- U 64. Acetonitrile 26,29 55.000 --- U --- U --- U 65. Tetrahydra£uran 0.39 1.000 1.85 --- U -•• U 66. 1,4-Dioxane 2,71 3.000 U --- tt --- U J . Estimated value between the MDL and MRL, U . 6e10W ALL 4uantitation Limita. DocuSign Envelope ID: 3C8509C9-30CA-4C23-661B-5E8AB648F13D to Q ZI w 3 3 C CD Q w ca ro 9 4 � O �!r (n � m CD w � w b CD o T Z) CD L o M are M-V C CP 0 is 25 fit" ' Ch�• p L cn J Vi �1 � L01 m 71 it �. m m m TOTAL CHLORINE. rrg/1 OR ugl! AT COLLEC TIC}N C j � L L _ �.r� � _m _m TEMPERATunE, °C o C ATCOLLECTION m Q vi —nn ch 0OF CONTAINERS -4 um vA ut 1 laid H "Al" Metals b . Do � Z Y +_' i`'i,s•ii } r�+ #;'+ py :yI}§+ Temperature "ti m m m ?€t 'rs i �fiy :, +. t 8260 Dup. 1 8260 DUP. 2 _ 8260 Dup. 3 C17 h 8260 Dup. 4J. G� pp. VfivA 8260D Apo. 112 8260D App. 113 ORP Field Parameter Y "� cY cn pARAMETERSITESTS am _ Cam" 27 P C C C oo c n mt7 YiR x m r. ca m CD � T m NM iz Cm-)m Cam? c7 Pri 2 b 475 b ry r■ 0- DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D . 1 00 �Rwnnma' `dQ k k(-fU')l.tV6h'*a 114 OAKMONT DRIVE GRLENVILLE. N_G. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 MW-9A 14W-16 PARAMETERS MDL MRL PH (field measurement), Unite 6.4 6.5 Nitrate+Nitrite as N, mg/1 0.04 0.04 --- V --- V Alkalinity Ito pH 4.5), m9 CsCO3/1 1.0 1,D 240 950 Chloride, mg/1 1.0 1.0 12 142 Total Dissolved Residue, mg/1 10 10 430 1500 Total DiagolVed Radidue, mg/1 10 10 sulfate, mg/1 5.0 5.0 100 185 Antioony, u9/1 0.0$ 1.0 0.04 J 0.11 J Arsenic, ug/1 0.09 5.0 0.29 J 10 Barium, ug/1 D.04 10.0 61.2 Barium, ug/1 0.04 10.0 339 Beryllium, ug/1 0.02 1.0 0.02 J D,OB J Cadmium, ug/1 0.04 1.0 --- U --- U COb4lt, ug/1 0102 1.0 0.14 1 2.5 Total Chromium, ug/1 0.12 5.0 0.20 J 36 Copper, Ug/1 0.04 1010 0.12 J 0.29 J Iron, ug/1 4.96 50.0 4135 311 Manganese, ug/l 0.31 10.0 230 226 Lead, ug/1 0.03 5.0 0.05 J 0.19 J moreury, ug/1 0,02 0.20 TESTED TESTED Nickel, ug/1 0.03 10.0 0,1S J 3.4 J ,selenium, ug/1 0.05 10.0 --- U 1.9 J silver, ug/1 0.22 5.0 --- 11 --- V Thallium, ug/l 0.02 1.0 0.16 J 0,24 J Tin, ug/l 0.05 190.0 --- u 3.0 1 vanadium, ug/l 0.04 1.0 0.20 J 14 Zino, ug/1 0,17 10.0 --- U 0.40 J 6ulfida, vg/1 100 1000 --- U --- U Conductivity Oat 25c), uMh00/Om 1.0 1.0 66D 2094 Dissolved Oxygen, mg/l 0.2 0.1 1.03 1.36 ToMpexaturs, °C 21 21 static water Level, feet 7.90 4.81 Wall Depth, feet 23.17 22.73 ORP, y0., 1.03 1,.36 Turbidity (hield), NTV 1.0 1.0 6.23 6.03 PHONE (252) 751a-6208 FAX (252) 756-00'1'' ID#; 6003 B DATE COLLECTED: 06/27/22 DATE REPORTED ; 10/13/22 REVIEWED BY9 MW-11 MW-13 Mw-12a Analydid Method Date Analyst Code 6.9 5.2 6,1 06/27/22 JWT 4500HB-11 --- U --- V ••. U 06/W.2a TRJ 353.2 R2-93 508 594 1510 07/05/22 HCE 232OU-11 49 84 290 07/05/22 EMv 45000LB-12 1100 06/20/22 HCH A5901-13 1100 1900 06/30/22 BLV D5907-13 .766 140 252 07/05/22 MTp 4500S042E11 0.30 J 0.19 J 0,25 J 07/03/22 LFJ EPA200.9 6,7 5.0 45 07/11/22 NAB EPA200.8 97.2 07/09/22 LFJ EPA2D0.6 246 525 07/11/22 NAB SPA200,8 0.06 J 0.04 J 0,04 J 07/05/22 LFJ EPA200.6 .-. V --- U --- U 07/05/22 LFJ EPA200,6 1.1 2.6 31$ 07/05/22 LY1 hPA200.6 4.7 7 4.4 J 52 07/05/22 LPJ RPA200.6 0.46 J 1 J 0.o5 J 07/05/22 LFJ 8PA200.8 11478 9327 2079 06/29/22 LFJ HPA200,7 326 300 633 06/29/22 LPJ EPA200,7 0.00 J 0,54 J 0,05 J 07/05/22 LFJ EPA200.B TESTED TBBTLD TASTED 1.5 J 4.1 J 3.6 1 07/05/22 LFJ ERA200.8 D•76 a 2.4.T 2.0J 07/11/22 NAB EFA200.6 --- U --- U --- V 07/05/22 LFJ EPA200.8 D.lo 1 0.11 J 0.04 J 07/05/22 LFJ EPA200.6 0.39 J 0.08 J 0.14.7 07/05/22 LFJ EPA200.0 4 6 36 07/05/22 LFJ BPA200.8 0.21 J 10 1.6 J 0'7/06/22 LFJ EPA200.8 --- U --- U --- D 06/29/22 LFJ 450092p-11 1352 1646 3590 06/27/22 JWT 2510E-11 3.23 1,74 2.21 06/27/22 JWT 450000-16 24 23 25 06/87/22 JWT 2550E-10 4.82 10.54 5.35 06/27/22 JWT 23,64 20.60 22.93 06/27/22 JWT 3.23 1,14 2.21 06/27/22 JWT 25808-11 7.67 0.22 4.62 06/27/22 JWT 213OA-11 All QC requirements were nOt mete M flank result exceeded method constant weight oxiteria. J - Estimated value between the MDL and MRL, U - Below ALL ¢uantitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D f flwko m(gM `'6, dN�(�P(0) �bu, 1 114 OAKMONT DRIVE GREENVILLE, N.0 27858 CLIENT! C & D DISPOSAL, INC. MR, .7UD80N WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: y BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: HIC DATE COLLECTED: 06/27/22 DATE EXTRACTED: 06/30/22 DATE ANALYZED: 06/30/22 DATE REPORTED: 10/1.3/22 7ARAMETSRB, vg/1 MDL MRL NW-9A HW-10 NW-11 M,W-13 MW-120 1. ACOnaphthOr:O 2.66 10.000 U U -- ❑ -__ ❑ U J . Estimated value between the MbL and MRL, U + Below ALL Quantination Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D E IN w 'H T @ w 0N� `d, �1@ �)�'P0T A �" V� 114 DAKNIONT DRIVE RHONE (252) -756-6208 GREENVILLE, N.C. 27858 VAX (252) 750.0633 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING VANE GREENVILLE, NC 27834 REVIEWED D'Y : LANDFILL APPENDIX 11 EPA METHOD 8260D R4 (18) CLIENT IV; 6003 H ANALYST: JAP DATE COLLBCTE17 : 0 6/ 2 7/ 2 2 Page: 1 DATE REPORTED: 1.0/13/22 PARAMETERS, V9/1 Data MDL Analyzed MRL 01/01/22 MW-10 07/01/22 NW-13 07/0$/22 HW•12e 07/01/22 Trip Blank 1. Chloromethane 0.77 3.000 --- U --- U --- V --- U 2. Vinyl Chloride 0.12 0.200 0.14 J 2.00 1.40 --- U 3, aromomethane 0.67 10.000 •-- U --- U --- D --- U 4. Chlorosthane 0.48 10.000 --- U --- U - U --- U S. Trichlorofluoromethan* 0.24 1.000 --- U --- tr --- U --- U 6. 1,1-❑iehloroethene 0.17 5.000 --- U --- U --- V --- U 7. Acetone 9.06 100.000 --- U --- U 12.20 J --- U S. ladomethane 0.26 10.000 --- U --- V --- V --- V 9. Carbon Disulfide 0.21 100.000 --- U 0.53 J --- U --- U 10. Mtithylane Chloride 0.64 1.000 --- U --- U --- V --- U 11• trana-1,2-Dichloroethene 0.23 $,000 - U --- U --- U --= U 12. 1,1-Dlobioro*thaae 0.20 5.000 --- U - U --- V --- V 13. Vinyl Acetate 0,20 $0.000 - U --- U --- 13 --- u 14. Cis-1,2-Diohloraethene 0.25 5.000 -- U 2.25 J 0.35 J --- U 15, 2-Butanone 2.21 100.000 --- U --- U --- U --- U 16. BrOmochloromethan• 0.27 3.000 --- U --- U --- U --- U 27. Chloroform 0.25 5.000 --- U --- V --- U --- U 18. 1,1,1-Triehloroethan* 0.19 1.000 --- U --- U --- U --- V 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U --- o 20. Benzene 0.24 1.000 0.70 J 1.23 2.52 --- U 21, 1,2-P14hlproethans 0.02 0.200 0.10 J 0.18 J 0.16 J 0 22. Trichloroathene 0.23 1.000 --- U --- U --- U --- U 23, 1,2-Pichloropropane 0.04 0.200 --- U 0.05 4 0.10 J --- U 24. Bromodichloromethene 0.04 0.200 --- U --- U --- V --- U 25, Cie-1,3 Dichloropropens 0.06 0.200 -- U •-• U --- U --- U 26, 4-Methyl-2-Pantanone 1.19 100.000 --- U --- U --- U --- U 27, Toluene 0.23 11000 --- U -•- U 0.7$ J --- U 22. trana-1,3-Dichloropropene 0.04 0,200 --- U --- U --- U --- V 29. 1,1,2-`Prichloro*t11an* 0.03 0.200 --- U _-- U --- U --- U 30. Tetrachloroathene 0.10 0.200 --- U --- U --- U --- U 32. 2-H*xanona 1.37 50.000 --- U --- V --- U --- U 32. Dibromochloromathana 0,03 0.200 --- 0 --- U --- U --- U 33. 1,2-Dihrpmoethane 0.03 0.200 --- U --- U D.02 J --- U 34. Chlorobanx*nn 0.30 3.000 --- U --- U --- U --- U 35. 141,1,2-Tetr4kahloroethane 0.22 1.000 --- U --- U --- U --- U 36. Uthylbenzens 0.21 1,000 --- U --- U --- U --- U 37. xylenes 0.68 5.000 --- U --- U 0.69 J --- V 30. DibromomAthans 0.28 10,000 --- U --- U --- U --• U 39. Styrene 0.19 1.000 --- U V --- U --- V 40. Brooloform 0.20 3.000 --- U --- U --- U •-• V 'kl, 1,1,2,2-Tatrachlorosthane 0.03 0.200 --- U --- U --- U --- U 42. 1,2,3-Trichlor4propans 0.09 0.200 --- U --- U --- U --- V 43. 1,4-Dichlorobanzone 0.39 1.000 --- U --- U --- U --- U 44, 1,2-Diohlorobenzene 0.32 5.000 --- V --- U --- U U 45. 1,3-Dibromo-3-Chloropropans 0.07 0.200 --- U --- U --- U --- U 46, Acrylonitrile 2.72 300.000 --- V --- U --- U - U 47. trans-1,4-Diehloro-2-Butsne 0.42 100.000 --- U --- U --- U --- U J . Astimated value between the MDL and MRL, U - Balo,4 ALL 4uantitation TAMita. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �nTOMIER@" t �N(�@rPo@�ta1�gd 114 OAKMON i DRIVE GREENVILLE, N.C, 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST B02 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY:C/ '4tonbl.r ZR 10 PHONE (252) 756,69M3 FAX (252) 756,0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 06/27/22 Page: 2 DATE REVOLTED: 10/13/22 LANDFILL APPENDIX II EPA =TROD 8260D R4 (18) Data AnalyZad 07/01/22 07/01/22 07/05/22 07/01/22 MW-10 Kw-13 MW-120 Trip PARAMRTRAS, ug/l td1]L MRL Blank 48. Aeroleiri 1.97 4.000 --- U --- U --- U --- U 49. Allyl Chloride 0,20 10.000 .-- U --- U --- U --- U 50. Ch1orvp9*n* 0.31 20.000 --- U --- U --- U --- D 51. 1,3-DichlorobOnl*ne 0.41 5.000 --- U __- t1 --- V --- U $2. DiChlorodifluoromethane 0.51 5,000 --- V --- U --- V --- tf 53. 1,3-DichloropYOpene 0.20 1.000 --- U --- U --- V "'" U 54. 2,2-D14hloroprvpant 0.17 15.000 --- U --- U --- U --- U 55, 1.1-DiChloropropene 0.22 5.000 --- U --- U --- U --- U 56. 6thy1 Methacrylatt 0.16 10.000 --- V --- U --- U --- U 67. Roxach2crabutadiene 0.10 0.200 --- U --- U --- U 11 58. 1gobutyl Alcohol 12.80 100.000 --- U --- V --- V --- U 59. Kathacxylonitrile 1.93 100.000 --- U --- U --- U --- U 60. Methyl Kethacrylate 0.25 30.000 --- U --- V -,- u --- U 61. Naphthalene 0.47 6.000 1.24 7 - U 1.44 J --- V 62. Propianitrile 3.26 150.000 --- U --- U -'" U " " U 63. 2,2,4-Trich1vr017*n4*r.e 4.50 10.000 --- U --- V --- U --- U 64. Acetonitrile 36.29 55.000 --- U --- U --- [S --- V 65, Tatrehydraturan 0.39 1.000 27,70 12.10 48.30 --- U 66. 1,4-DiOAGne 2.71 3.000 18.50 13.90 14.60 --- U J - gakimated value between the MDL and HRL, U . Below ALL putntitttiOn LimiCe. NOTL:: E M METHOD 8260D R4 (18): MW-125 received at pH >2. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Hwumfiimm� U h . off p6m'(51-IM0 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT. C & D DISPOSAL, INC. MR. &TUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY:!_� LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 75R•0633 CLIENT ID: 6003 C ANALYST. TAP DATE COLLECTED: 06/27/22 Page: 1 DATE ANALYZED: 07/01/22 DATE REPORTED: 10/13/22 PARAMBTBRB, U9/1 MDL MRL MW-9A 1. Ch10romethane 0.77 3.000 --- 2. vinyl Chloride 0,12 0.200 --- U 3, Eromomethane D.67 10.000 --- U 4. Chloraethene 0,49 10.000 --- D 5, Trich1nr0flu0rQM*thane 0.24 1,000 -•- U 6. 1,1-Dichloroethene 0.17 5.000 --- U 7, Acetone 9.06 100.000 --- U S. lodomethane 0.26 10.000 --- U 9. carbon Disulfide 0.23 100.000 --- U 10. M*Lhylene Chloride 0.64 1.000 --- U 11, trans-1,2-Dichlordethene 0.23 5,000 --- U 12. 1,1-Dichlorosthans 0120 5.00D --- U 13, Vinyl Acetate 0.20 50.0D0 --- t1 14. Cir-1,2-Dichlorcethene 0�25 5.000 --- U 15. 2-Butanona 2.21 100.DOO U 16. aramoahloromethans 0.27 3.000 U 17, Chloroform 0.25 5.000 --• V 18. 1,1,1-Trichloroothane 0.19 i.D00 - -- V 19, Carbon Tetrachloride D.04 a.200 --- U 20. Benzene 0.24 1.000 --- V 21, 1,2-Dichloroetharie 0.02 D.200 --- V 22. Tric1110Y44thene 0.23 1.000 --- U 21. 1,2-Dichlcropropans 0.04 0.200 --- U 24. sromodiphloromethana 0104 0.200 --- U 25, Cie-1,3-Dichloropropene 0105 0.200 --. U 26. 4-14ethyl-2-Pentanone 1119 100.000 --- U 27. Toluene 0123 1,000 •-- U 29L trans-1,3-Dichloropropens 0.04 0.200 --- ❑ 29. 1,1,2-Triahloroethane 0,03 0.200 --- U 10. Tetrachloroethens 0.10 0.200 --- U 31. 2-Hexanone 1.57 50.000 --- U 32. Dibromochloromethane O.D3 E 200 --- U 33. 1,2-Dibromosthans 0.03 01200 --- U 34, chlorobenzene 0.30 3.000 --- ❑ 35. 1,1,1,2-Tstrachlorosthane 0.77 1.000 --- U 36. Ethylbenzens 0.21 1.000 --- v 37. Hylenes 0,68 5.000 --- V 38. Dibromamethane 0.28 10.000 --- U 39. Styrene 0.19 1.000 --- U 40, gromolorm 0.20 3.000 --- U 41. 1,1,2,2-Tetra0h1oroethane 0.03 0.209 --- tl 42. 1,2,3-Trichloropropane 0.09 0.200 --- U 43. 1,4-Dich14z4benzene 0.39 1.000 --- U 44. 1,2-Dichlorobenzens 0.32 5.000 --- U 45. 1,2-Dibromo-3-chloropropane 0,07 0.200 --- U 46. Acrylonitrile 2.72 200.090 --- ❑ 47. trana-1,4-Dichlorc-2-Butane 0,42 100,000 ^-- U 48. Acrolsin 1.97 4.000 --- U J • Estimated value between the MDL and MRL, U - Below ALL 4utntitation Limits, DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 0AK(v101,4'( ORNE GREENVILLE, N-C. 27858 CLIENT; C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking water lba 37715 Wantewater ID: 10 FAX (252) 756-0633 CLIENT ID: 6003 C ANALYST- 67AP DATE COLLECTED: 06/27/22 DATE ANALYZED: 07/01/22 DATE REPORTED: 10/13/22 PARMETERB, of/1 MDL MRL MW-QA 49. Allyl Chloride 0.24 10.000 --- u 50, Chloropxene 0.21 20.000 --- v 51. 0.41 5,400 --- u 52. Diehlorodifluoromethans 0.51 5.000 --- u 53. 1,3-D1chlvroPvoPane 0.75 1.000 --- ❑ 54. 2,2-Diphlaropropane 0.17 15.000 --- u 55. 1,1-D14hloroprppene 0,22 5.000 --- u 56. Ethyl Methacrylats 0.16 10.000 --- u 57. HexACh1crQk)utadiene 0.10 0.200 --- u 59. Isabutyl AlCOh41 12.80 100,000 --- U 59. Methoexylonitrile 1.93 100.000 --- u 60. Methyl MethaCrylACO 0.25 30.000 --- V 61. Naphthalene 0.47 6.DD0 --- u 62. Propionitrile 3.26 150,000 --- u $3, 1,2,4-Trichlorobenzene 0.5D 10.D00 --- u 64. Acetonitrile 36.29 $5.000 --- u 65, Tetxahydrnfuran 0.39 1.000 --- u 66. 1,4-Dioxane 2.71 3.000 --- ❑ Page: 2 S + Estimated value between the MDL and MRL, ❑ e Below ALL QuantitatiOn LiMita. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Ann Baynor Environment 1 PO Box 7085 Greenville, NC 27858 Sample Matrix WW Sample Type Samplers P.M./P.C. Element One Inc. 6319-D Carolina Beach Rd. Wilmington, NC 28412 Phone: 910 793-0128 Fax: 910 792-6863 ellab@ellab.com FINAL REPORT OF ANALYSES July 20, 2022 Client Project Name: 6003 C & D Disposal Client Project Number E1 Project Number e38940 Method EPA 245.1 Date Received 07/15/2022 DL, mg/L 0.0002 Time Received 1120 Date Analyzed 07/15/2022 Received by LLB Delivered by Client eOne ID Client Sample ID Da#e Time 38940-13 6003-C&D Disposal MW9-A 38940-14 6003-C&D Disposal MW-10 38940-15 6003-C&D Disposal MW-11 38940-16 6003-C&D Disposal MW-13 38940-17 6003-C&D Disposal MW-12S 38940-18 6003-C&D Disposal MW9-15 38940-19 6003-C&D Disposal MW-16 38940-20 6003-C&D Disposal MW-17 38940-21 6003-C&D Disposal MW-14S 38940-22 6003-C&D Disposal MW-14D ,0 Ken Smlth, Laboratory Director Mercury Result Unit Dil Sampled Sampled < 0.0002 mg/L 1 06/27/2022 1011 < 0.0002 mg/L 1 06/27/2022 1116 < 0.0002 mg/L 1 06/27/2022 1216 < 0.0002 mg/L 1 06/27/2022 1400 * 0.0002 mg/L 1 06/27/2022 1303 < 0.0002 mg/L 1 06/28/2022 1417 < 0.0002 mg/L 1 06/28/2022 1330 < 0.0002 mg/L 1 06/28/2022 1017 < 0.0002 mg/L 1 06/28/2022 1214 < 0.0002 mg/L 1 06/28/2022 1121 38940 Environment 1 Hg Report Compiled by NC Certifications: DW 37788 and DWQ DENR 604 Page 1 of 1 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D m� CD �u z - (D -o CD O a CDo d o en O N Ch s O 0 G) CD 0' N X' (n CD CD x 5' Q O Q c w CD G) 0 0 D —I CD T cc a O m V-I 0 0� oI o o I W D 0 0 C� C. 0 oI o p W =CL Q 0 N > C d t7 t7 p i g z u,io' o m w CD x7 A z < � z > r tom" t�" y ° 0 m m O O I C X C Q co Q. rf w •� o� 0 m Z z V N N N N N C7CO-Q t3 i' N N t i ca r cn O N N N NrQ N w CD 0 CD D E3 CD Type' O L O D D N w a, z 0 Matrix2 CL o CD v D <. m #Cntrs i i Free =0 o 0 m x Chlorine m a mCD -0 (D«_ 0 o 0 0� =ate 7 Q� m z z CD 0 CD 0 v' cn D o z O a I m D n Cn m x CD r- m I m m CL Container Type, Plastic or Glass I None ❑ ❑ ❑ ° a a m � :3 (D — j Ascorbic en N cn Q CD Q jNkSA m � o (D m n 0' W- m sz g• a NaOH H2SO4 HNO3 F, (� (� HCI CD -o r o Cr = ro E5 CD C k sCD w a M D x rn O OD CSi w �' ts DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D m C� 0 a 0 0 CD a- N v XC' C N C� C w rn 0 x m rn Q G) 0 c Q CD 0 0 D m u� D 0 CD 0 Jc;%I o C3, C. Q 0 c;r\I0) o D Q 0 0 C4 w O w ClO� w w CD O p, i n n � m-a w t7 t7 t7 3 o o D t7 k7 .� C7 p 0 Z Z I p pl p d O Cn O o rn 0 1 m Z w D r o., _. o C z E--� r r 7a D r- m o 0 m Z p D p 0 @ n z cs' D Z --I a � z � v o 1 OC% 011 011 0 N N N N wizT` N p� 0 O a Yin O N tN tj N N <D I D W 11-0 73 3 as a v Type I= 1 a N 0- w 0 E m Q. Z o 0 o CD Q Maui K e c' v _� @ D J # Cntrs Free ;0 a 1 D -V m Chlorine �' o M a [D < 3 m A) 0 m O o tU Q = Z �7 rL Z C a m —� a Y J 1 �. Cn v -C x a CD —� o• Z O m C D w CO CD N CD c CD m a jContainer Type, Plastic or Glass None ❑ ❑ ❑ ° LO c� m m m �o Ascorbic Nam CD < CL � 0- � a ..� NaOH fD r -n H2SOa HNO3 HCl . W m C) -V r � 3 � o LS CD 3 d W CD o � N os CO <:7,-) 0 D v X (D N � 0-) '* CD 01 w DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Fn z 10 Fn z 10 w i . m 4;d 0 j N m tp 0 .2 n� ,. Q, n. tirJ Ll 4�] m n m m � TOTAL CHLORINE, mgll C7 rn Fr m OR Ug/I AT COLLECTION Lo 'T' TEMPEHATURE,"G O _ AT COLLECTION m o G7 G1 co � O #f OF CONTAINERS ny � � �` ••" v 'lF # ,,.,�� :},:sr; . Field 014 Nitrate+l�iitrite f) V J � h}' }%!l'• ��+' 'tiV '.5r Alk81Y,1t Vim,.Chloride Fw1 TDS fa {#' #;#g'; Ss4'}�" •#s'r'}; Sulfate m {mi, m , g 3r;:s Metals ItAi "MR , Sulfide �i •d Conductivity P. 1� Ytl V cn Temperature Field Parameter ,.j?? €, 8270E Du 1 > 4� s . 8270E Dup.2 > G� 9270E Dup. 3 > �] 8260D App. 11 uo co e, PARAMETERS/TESTS i: Li Li L7 D rn {") n f^i 5 [his O xp F. Cps P 0 O m m rn rn !n c ' m C"S r O > Q � m rn C�? o DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D O Ik w a 77 _a co co eb m cn o_ Co M w CD z Ul 01 cm �a 0 d° %�o n T m ID m � m Q ra w e � to i W o [ems CIS !? M �+ r� to d �I 1V m m m m b m TOTAL CHLORINE, mgll i—I jj d m m OR ugll AT COLLECTION Q [ S '�A � TEMPERATURE,°C A � AT COLLECTION etas 4 by # OF CONTAINERS INN' ORP ;M1;{�, ;o�.rfi'r. :�r'vi';� .v.'r;v�;.�� y'�f•: rri m m C7 yr crti cn 0i PARAMETERSfTESTS am O L L m . Cr n C (`��}1' ice' Q C-7 Z 4/a T rll U Do 771 rp W 1'fm rm m O fji � ?� Ls „ m Q (' m O orri r y 1 � n m Z r T Cy] C• x z 7 R t: ZO4r�r a—• J; y n Pr 3 G W DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D tl,7 N @ oo r V coi i r �q'j ��' -eon 114 OAKMONT DRIVE (3REF 1VILLE, N.0 27868 ID#: 6003 D Drinking Water IUs 37715 Wastewater ID: 10 H-IUNE G, FAX (2 _ ; C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE DATE COLLECTED: 06/28/22 GREENVILLE, NC 27834 DATE REPORTED : 10/13/22 REVIEWED BY: MW-11 HW-15 Mw-16 NW-17 MW-149 Analysis Method PARAMETERS MGL MRL hate Analyst Code PH afield measurement), Unite 5.6 8.4 6.0 6.6 06/28/22 PJC 4500RD-11 Nitrate4Nitrite as N, mg/l 0.04 0.04 0137 • U --- U --- U 06/30/22 TRJ 353.2 R2-93 Alkalinity (to pR 4.5), 1ng CaCO3/1 1.0 1.0 160 432 13 1160 07/05/22 HCE 232OR-11 Chloride, TAY/1 1,0 2.0 61 128 23 140 07/05/22 HMV 4500CLB-ll Total Dissolved Residue, mg/l 10 10 550 1100 470 1500 06/30/22 BLV D5P07-13 sulfate, mg/1 5.0 5A 170 295 301 312 07/05/22 MTM 45009042811 Antimony, ug/1 0.03 1.0 0.46 J 0.22 J 0.25 J 97/0$/22 LFJ EPA200.9 Anti=nY, µg/i 9.03 1.0 --- U OB/03/22 NAB RPA200.8 Arsenio, ug/l 0.o8 S.0 5.6 13 20 07/11/22 NAB EPA200.8 AraaniC, Ug/1 0.09 5.0 0.85 J OB/03/22 NAB RPA200.8 Barium, ug/1 0.04 10.0 260 460 348 01/11/22 NAB EPA200.8 Barium, ug/l 0.04 10.0 70.5 00/03/22 NAB EPA200.6 Beryllium, ug/1 0.02 1.0 0.23 J 0.0$ J 0.04 J 07/05/22 LFJ EPA200.8 Beryllium, Ug/1 0.02 1.0 0.05 J 00/26/22 NAB EPA200.9 cadmium, ug/l 0.04 1.0 0.24 J 0.05 J --- U 07/05/22 LFJ EPA200.8 Cadmium, Ug/1 0.04 1.0 --- U 00/03/22 HAD RPA200.0 Cobalt, ug/l 0.02 1.0 0.72 J 0.76,T 1.8 01/05/22 LFJ EPA200.8 Cobalt, Ug/l 0.02 1.0 0.08 J 08/03/22 NAB 3PA200.8 Total Chromium, Ug/1 0.12 5.0 5.5 17 25 01/05/22 LFJ EFA200.0 Total Chromium, ug/l 0.12 5,0 2.I J 08/03/22 NAB EPA290,9 Capper, ug/1 0.04 10.0 2 J 0.94 J 0,21 J 07/05/22 LVJ EPA200.8 Copper, ug/1 0.04 10.0 0.92 J 09/03/22 NAB ZPA20o.a Iron, u9/1 4.96 50.0 2111 36106 2269 1930 07/12/22 LrT SPA200.7 Manganese, ug/l 0.31 10.0 212 477 169 692 07/12/22 LFJ EPA200.7 Lead, ug/l 0.03 5.0 1.1 J 0.75 J 0,19.T 07/05/22 LVJ EPA200.9 Lend, ug/l 0.03 5.0 0,20 J 09/03/22 NAR EPA200.8 Mercury, ug/l 0.02 0.20 T,9,9TED TH9TED TESTED TEBTRT+ Nickel, ug/l 0.03 10.0 1.5 J 2.0 J 2.4 J 07/05/22 LFJ EPA200.8 Nickel, Ug/1 6.03 10.0 0.26 J 08/03/22 NAB HPA200.8 Selenium, ug/1 0-05 10.0 1.7 J 1.8 J 1.1 J 07/22/27 NAB EPA200.a 8a1en1=' Ug/l 0.05 10.0 0.35 J 05/03/22 NAB SPA209.0 silver, ug/1 0.22 5.0 --- U --- U --- U 07/05/a2 AF.7 EPA200.8 Bllver, ug/l 0.22 510 --- U 09/03/22 NAB RPA200.9 ThalliuM, U9 0 0.02 1.0 0.24 J 0.08 J 9.02 J 07/05/22 LFJ EPA200.0 Thallium, ug/l 0102 1.6 --- U 90/03/22 NAB 13P4290.8 Tin, Ug/1 0.05 100.0 12.2 J --- U 0.30 J 07/05/22 LFJ RPA200.8 Tin, ug/l 0,65 100.0 --- U 08/03/22 NAS EPA200.8 Vanadium, uq/1 0.04 1.0 6 15 10 07/05/22 LFJ EPA200.0 Vanadium, ug/1 0.04 1.0 3 08/03/22 NAB EPA200.8 zinc, ug/1 0.17 10.0 227 07/12/22 NAB EPA200.8 Zinc, US/1 0.17 10.9 1.8 J 0.74 J 07/00/22 Lis EP2200.8 zinc, ug/1 0.17 10.0 0,21 J 00/03/22 NAB 6PA200.9 All QC requir*menu were not met, M Blank result exceeded method Constant weight criteria. J - Estimated value b6tween the KPL and MRL, V R Below ALL ouantitation Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 114 OAKMONT DRIVE GREENVILLE, N.C, 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking Water In, 37715 wastewater IDi 10 FAX (252) "` ID#: 6003 D DATE COLLECTED: 06/28/22 DATE REPORT-ED : 10/13/22 REVIEWED BY: MW-11 MW-15 MW-16 MW-17 MW-143 Analysis Method PARAMRTER8 MDL MRL Date Analyst Code sulfide, ug/1 1D0 1000 --- ❑ --- U --- U --- U 06/29/22 LFJ 4g001M-11 Conductivity (at 25c), uMhoa/cm 1.0 1.0 1095 1114 610 2711 06/20/22 PJC 251OD-21 Dissolved Oxygen, mg/1 0.1 0.1 1.04 2.16 1.26 1.36 06/20/22 PiC 4500OG-16 Temperature, °C 23 29 24 26 06/20/22 PJC 255OP-10 Static Wat4r Level, feet 7.53 8.13 8.98 5,10 06/28/22 PaC Well Depth, feet 22.14 22.73 22.25 23.12 06/2u/22 Pic OR", my -3 +120 +113 +147 06/28/22 FJC 250OB-11 Turbidity (Field), NT❑ 1.0 110 7.74 4.36 2.74 0.38 06/20/22 Pic 213OB-11 All QC requirementa were not mats M mlank rebult •xceedid method conotant weight criteria. d . Hntimated value between the MDL and MRL, U e B61OW ALL UUantitatipn Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D L nT0�(0 M1 in 0F0(0-jWbV 1 114 OAKMONT DRIVE GREENVILLE, N.G. 27658 C & D DISPOSAL, INC. MR- JUDSON WHITEHURST 602 RECYCLING LANE GREENVILLE, NC 27834 ';Ik 1 PHONE (252) 756-6200 FAX (252� 756-+7£t33 ID#: 6003 D DATE COLLECTED: 06/28/22 DATE REPORTED : 10/1.3/22 REVIEWED BY: MW-14D Trip Analysis Method PARAMETERS MAL MRL Blank Date Analyat Code PH (field measurement), Unite 7.4 06/28/22 PJC 4509HB-11 Nitrats+Nitrite ae N, mg/1 0.04 0.04 0,27 06/30/22 TRJ 353.2 R2-93 Alkalinity (to pH 4.5), mg CAC03/1 1.0 1.0 320 07/05/22 HCE 2320E-11 Chloride, mg/l 2.0 1.0 63 07/0$/22 HMV 45DOCLB-ll Total Dissolved Residue, mg/1 10 10 300 06/30/22 BLV ❑5947-13 Sulfate, mg/1 5.0 5.0 --- U 07/05/22 MTN 45000042811 Antimony, ug/1 0,03 1.0 --- U D7/05/22 LFJ HPA200.6 Arsenic, ug/1 0.0E 5.0 0.43 J 07/11/22 NAB 8YA200.B Barium, ug/1 0.04 10.0 9.5 S 07/05/22 LFJ EPA200.8 Beryllium, 09/1 0.02 1.0 --- U 07/05/22 LPJ 8PA200.8 cadmium, uq/1 0.04 1.0 --- U 07/05/22 LFJ EPA200.8 Cobalt, ug/1 0.02 1.0 --- V 07/05/22 LFJ EPA200.9 Total Chromium, u9/1 0.12 5.0 --- U 07/95/22 LFJ EPA200.8 Copper, ug/1 0.04 10.0 0.28 J 07/05/22 LFJ EP4200,9 Iran, ug/l 4.9E 50.0 22 J 07/12/22 LFJ HPA200.7 Mangansss, ug/1 0.31 10.0 1 J 07/12/22 LFJ EPA200.7 Lead, uq/1 0.03 5.0 0.051 07/0$/22 LFJ SPA200.0 Mercury, ug/1 0,02 0.20 THST8D Nickel, uq/1 0.03 10.0 0,14,7 07/05/22 LFJ HPA200.8 selenium, ug/1 0.05 10.0 --- U 07/11/22 NAB 8PA200.e silver, ug/l 0.22 5.0 --- U 07/05/22 LF.T HPA200.8 Thallium, ug/1 0,02 1.0 --- U 07/OS/22 LP`J BPA200.8 Tin, ug/1 0.05 100.0 --- U 07/05/22 LFT HPA200.8 Vanadium, ug/1 0.04 1.0 0.34 J 07/05/22 LFJ EPA200.9 Zinc, 4g/1 0.17 10,0 0.74 J 07/08/22 LFJ EPA20O.B Sulfide, ug/1 100 1000 --- ❑ 06/29/22 LFJ 450062n-11 Conductivity (at 25c). uMhos/cm 1.0 1.0 524 06/20/22 PJC 25108.11 Disaclvsd Oxygen, mg/1 0.1 0.1 2.23 06/28/22 PJC 45009a-16 Temperat%4t*r °a 25 06/22/22 PJC 25SOB-20 Static Water LOV61, f0at 7.21 05/28/22 PJC Well 0@pth, feet 41.92 06/29/22 PJC ORP, my +122 06/28/2a PJC 2580E-11 Turbidity (Yield(, NTU 1.0 1.0 1.19 06/29/22 PJC 21948-}1 J w Estimated value between the NDL and MRL, U - Below ALL QU*ntitati4n Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D l nvcook ugff''t hawo- 6�duAN 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: BASE/NHUTRAL COMPOUNDS EPA METHOD 8270E R6 (18) 4P��ivakar tris �0 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: HIC DATE COLLECTED: 06/28/22 DATE EXTRACTED: 06/30/22 DATE REPORTED: 10/13/22 Data Analysed 06/30/22 06/30/22 D7/01/22 01/01/22 07/01/22 M14-15 r4w-26 riw-17 MW-140 NW-14D BARAMETERai ug/l MDL MRL 1. Acenaphthene 2.66 10.000 --- V --- V --- V --- V --- V J v Estimated VAYL1ibetwtan the 74Db and MRL, V - Below ALL ounntitatian Limits. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 5 . �Fl-nlTt. Ile 114 OAKMONT DRIVE GHEENVILLE, N.C. 2785e CLIENT: C & D DISPOSAL, INC. MR. alDSON WHITEHURST 802 RECYCLING LANE Gl2EENVILLE, NC 27634 4 REVIEWED BY: LANDFILL APPENDIX 11 7PA METHOD 82 6 0D R4 (18 ) PHONE (252) 756-6206 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: .7AP DATE COLLECTED: 06/28/22 Page; I DATE ANALYZED: 07/01/22 DATE REPORTED: 10/13/22 Mw-11 MFI-15 6iw-l6 NW-17 mw-14.9 QRRAMETER9, U9/1 MDT, MRL 1. Chlcromethmns 0.77 3.000 --- U --- U --- U --- U ... U 2. Vinyl Chloride 0.12 0.200 --- U --- U --- U --- U 1,26 3. 5 mpo:nethmne 0,67 10,000 --- U --- U --- U --- U --- U 4. Chloroethane 0.40 10.000 --- U --- U --- V --- U --- U 5, Trichlarofluoromethane 0.24 1.000 --- U --- U --- U --- U .__ U 6. 1,1-Diohloroethene 0.17 5.000 --- U --- U --- U --- U --- U 7. Acetone 9.06 100.000 11.20 .7 .-- U 15.30 J --- U 10.90 .7 9. lodomethane 0.26 10.000 --- U --- U .._ U --- U - V 9. Carbon Disulfide 0.23 100,000 .-- U --- U U 0.24 J --- U 10. Methylene Chloride 0.64 1.000 --- U --- U --- U --- U ••• U 11, tram-1,2-Dichloroethene 0.23 5.000 --- U --_ U --- U -_- U --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U --- U •"' U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- U -__ U --- U 14. cis-1.2-Dichloroethena 0,25 5.000 --- U --- U --- U --- U ... U 15. 2-eutanone 2.21 100.000 --- U --- U --- U --- V --- U 16. Bromachloromethan0 0.27 3.000 --- U --- U --- U --- U --- U 17. Chlorotorm 0.25 5.000 _._ U U --- U ••• U --- U 18. 1,1,1-Trichlorosthane 0.19 1.000 --- U --- U _-- U U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- V --- U --- U _ U 20. Een2mne 0.24 1.000 0.75 J --- U 0.53 J --- U 1.60 21, 1,2-Diohloroethpne 0.02 0.200 0.13 J 0.02 J 0.L6 J --- U 0.10 J 22. Trichlgrcathene 0.23 1.000 --- U --- U --- U .-- U --- U 23. 1,2-Dichloropropanm 0.04 0.200 0.06 J --- U 0.06 J --- ❑ 0.04 1 24, 9romgdichloromsthane 0.04 01200 --- U --- U •-- U --- U --- U 25. Cie-1,3-DiPh1oropropena 0.06 0.200 --- U --- U --- U --- U --- U 26. 4-Mathy2-2-Pentanons 1.19 100.000 --- U --- U --- V --- U --- U 27. Toluene 0.23 1.000 --- U --- ❑ 0.29 J --- 0 0,24 a 28, trans-1,3-Dichloropropane 0.04 0.200 U --- U --- U •'_ U --- U 29, 1,1,2-Trichlarosthana 0.03 0,200 --- U --- U --- U --- U --- U 30. Tatrachloroathene 0.10 0.200 --» U --- U --- U »»- U --- U 31, 2-Rexanone 1.57 $0.000 --- U --- U --- U --' U --' U 32. Dibromoahloromethane O.D3 0.200 --- U --- U --- U --- U --- U 33, 1,2-bibromoethane 0.03 0.200 --- U --- U - - U u " ' U 34. Chlarobenzene 0.30 3,000 --- U --- U --- U --- U --- U 35, 1,1,1,2•Tetrachloroethane 0,22 1.000 --- U --- U --- U --- U --- U 36. Sthylbenzene 0.21 1.000 --_ U --- U 0.27 J ••. U --' U $7. Xylehes 0,68 5.000 --- U --- U --- U U ••• U 38. Dibramomethane 0.28 10,000 --- U --- U --- U "_" U ^-- ❑ 39. Styrene 0.19 1.000 --- V --- U --- U -- U ... U 40. 3romgform 0.30 3.000 --- U --- U --- U --- U ___ ❑ 41, 1,1,2,2-Tetrach1croathane 0,03 0.20D --- U --- U --- U --- U --- U 42, 1,2,3-Trichloroprop9ne 0.09 0.200 --- U --- U --- U --- U --- U 43. 1,4-Dich1orohmntans 0,39 2.000 --- U --- U --- U -«- V --- U 44, 1,2-Dichlorobsnxene 0.32 5.000 --- U --- U --- U --- U --- U 45. 1,2-Pihromo-3-Chloropropans 0.07 0.700 --- U - U --- U --- U --- U 46, acrylonitril■ 2,72 200.000 --- V --- U --- o --- U --- U 47. trans-1,4-Dichloro-2-8utenm 0.42 100,000 --- U --- U --- U --- U --- U 48. Acrclain 1.97 4.000 --- U --- U --- U --- ❑ --- U J w Estimated Value betwoen the MDL and MRL, U • 3e10w ALL Quantitation Lim1tB. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Enw,onalm(IM ��u bo� ow P-0 vd. �" (@d 114 OAKMONT DRIVE GREENVILLE, N.C. 2785E CLIENT: C & D DISPOSAL, INC. M.R. JUDSON WHITEXURS'T 802 RtCYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; LANDFTLL APPENDIX II 9VA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST; JAP DATE COLLECTED: 06/28/22 Page: 2 DATE ANALYZED: 07/01./22 DATE REPORTED: 10/13/22 PARAMETBRB, ug/1 MDL Z&RL NW-11 MW-15 KW-16 MW-17 MW-148 49. Allyl Chloride 0,26 10.000 --- U --- U --- U --- ❑ --- U $0, Chloroprene 0.21 20.000 --- V --- U -" V --- U -- U 51. 1,3-Dichlorobenzene 0,41 5.000 --- U --- U --- U --- U --- U $2. DichlorbdiflUa roMethen• 0.51 5.000 --- U --- V --- U --- U --- U 53. 1,3-1)1phloropropano 0,28 1.000 - -- V - -- V - -- U - U --- U 54. 2,2-DiahloroproPene 0.11 15.000 --- U --- ❑ --- U --- U U 55, 1,l-Dichloroprop9na 0.22 5.000 --- V --- U --- U --- V --- U 56. Ethyl Mathaarylate 0.16 10,000 --- V `-- U --- U --- U --- V 57, xexachlorobutadient 0,10 0.200 --- U --- U --- V --- U - u 50. Ifabutyl Alcohol 12.80 100.000 --- U --- V --- U --- U --- U 59, Methacrylonitrile 1.93 100,000 --- U --- U --- U --- V --- U 60. M*thyl Kathacrylate 0.25 30.000 --- U - - D --- U --- U --- U 61. Naphthalene 0.47 6.000 --- V --- U -- U --- U --- V 62. Prop icnitrile 3.26 150.000 --- U --- iS --- U --- U --- V 93. 1,2,4-Trichlorobonsene 0.50 10.000 --- U --- V --- U --- V --- U 64. ACetonlerile 36.29 55.000 --- U --- U --- U --- U --- U 65. 7etrahydrofuran 0.39 1,000 44.00 --- U 3.32 --- U 31.80 66. 1,4-Dioxane 2.71 3.000 22.10 9.33 73.30 --- V 14,60 a - Eetimtted value between the MDL and MHL, U - Below ALL Quantitation Limits. NOTE. EPA METHOD 9260D R4 (18): MW-35 received at pH >2. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D kmW'H'mnmM 'df, VA do 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JIMSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking WntBr ID: 37715 wastewater FD: 10 FAX (252) 756-0� CLIENT ID: 6003 D ANALYST: TAP DATE COLLECTED: 06/28/22 DATE ANALYZED: 07/01/22 DATE REPORTED: 10/13/22 PARAMETWE , ug/1 MDL HRL MW-14D Trip Blank 1. Chloromethana 0.77 3.440 --- a --- u 2, Vinyl Ch10rtdo 0.12 0.200 --- u --- V 3, eromcmethans O.67 10,000 -" U --- u 4, Chloroathane 0.48 10.000 - u --- u 5. Trichlorogluoromethane 0.24 1.000 --- U ^^- u 6, 1,1-Dichloroethane 0.17 $,600 --- V --- u 7. Acetone 9.06 100.000 --- u --- ❑ $, Iodomethane 0.26 10.000 --- u --- u 9. Carbon Disulfide 0.23 100.000 0,27 J --- V 16. Methylene Chloride 0.64 1,000 --- V - V 12. trans-1,2-Dichlorcethene 0.23 5.000 --- u --- V 12, 1,1-Dichl0roathane 0.20 5.00C V --- u 23. Vinyl Aeatate 6.20 50.000 --- u --- V 14. Cis-1,2-bichloroathene 0.25 5.000 --- V --- u 25. 2-8ukanone 2.21 100.000 --- u --- V 16. BromochlOroMothafie 0.27 3.006 --- V --- u 17. Chlorotorm 6.25 5.000 --- u ''- V 16. 1,1,1-Trichlor0ethane 0.19 1,000 --- V U 19. CarbarL Tatrachloride 0.04 0.200 --- V ••- u 20, Benzene 0.24 1.000 --- V --- u 21, 1,2-Diahloroethane 0.02 0.200 --- Ti ••- Q 22, Trichloroethene 0.23 1.000 --- V --- u 23. 1,2-piohloropropana 0.04 0.200 --- u --- V 24. BromodiChloroM*thane 0.04 0.200 '•• V --- u 25, C1s-1,3-Dichloropropenc 0.06 01200 --- u --- U 26. 4-Methyl-3-pentanone 1.19 100.000 --• V --- V 27. Toluene 0.23 11000 --- u --- V 28. trafts-1,3-Dichlaropropana 0.04 0.200 --- u --- V 29. 1,1,2-Trichloroethane 0.03 0,200 --- V --- u 30, Totraehloroathene 0.10 0.200 --- u --- V 11. 2-Hexanone 1.57 50,000 --- u --- u 32. Dibxomo0hloromethane 0.03 0.200 --- u --- V 33. 1,2-Dibromoathane 0.03 0.200 --- V --- u 34. Chlorobanzene 0.30 3.000 --- U --- V 3$. 1,1,1,2-Tatrachloroethane 0.22 1,006 --- V --- u 36. Ethylbenzane 0.21 2.000 --- u ^^- u 37, xylenes 0.68 5.000 --- V u 39. Dibromomethane 0.28 10.000 --- u --- u 39. styrone 0.19 1.000 --- ❑ •• V 40. Bramororm 0.20 3.000 --- a --- u 41, 1,1,2,2-Tmtrachloroathana 0.03 0.200 --- u --- V 42. 1,2,3-TxtuhloroPrppane 0.09 0.200 --- V --- u 43, 1,4-Dichlorobenrene 0.39 1.000 --- V --- u 44. 1,2-Djehlorobenzene 0.32 5.000 --- u --- V 45. 1,2-bibromo-3-Chloropropane 0.07 0,200 --- U --- u 46. Aerylppitrile 2.72 200.000 --- u --- V 41, trans-1,4-Dichloro-2-Butene 0.42 100.000 --- V u 48. ACrolalft 1.97 4.000 --- u --- V Page: 3 a - Batimated VAlue between the MDL and MRL, V . Below ALL QuantitatiOn LiMite. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D NVVU'Om n� `fin ��O(�Co)�P01N"'-�(P�� 'q 114 OAKMONT DRIVE GREENVILLC, N.G. 27858 CLIENT: C & D DISPOSAL, INC. MR- JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Z7 REVIEWED BY: LANDFILL APPENDIX 11 EPA METHOD 8260D R4(18) Drinking Water IDi 37715 4fastewater ID, 10 PHONE (252) 751 FAX (252) 75': CLIENT ID: 6003 A ,ANALYST: JAP DATE COLLECTED: 06/28/22 DATE ANALYZED: 07/01/22 DATE REPORTED: 10/13/22 PARAMETERS, ug/1 MDL MRL Mw-14❑ Trip Blank 49. Allyl Chloride 0.20 10.000 --- U --- U 50. Chloroprene 0.21 20.000 --- U --- U $1. 1,3.171chlorobinxene 0.41 5.000 --- U ••- U 52. Di ehIoxodi[luarometharLe 0.51 5.000 U --- U 53. 1,3.1DichluvoiPrpg4np 0.2$ 1.000 -- U --- U 54, 2,2-DichIoropropane 0.17 25.000 --- U --- U 55. 1,1-Dichlorppropene 0.22 5.000 --- U --- U 56, Ethyl Methacryldta 0.16 10,000 --- U --- v 57. Hex4Ch1grobptadiene 0.10 0.200 --- U --- U 58. Ieobutyl Alcohol 12.60 100.000 --- U U 59, Methaarylonitrile 1.93 100.000 --- U --- 60. Methyl Methaeryl4te 0.25 30.000 --- U --- U 61, Naphphalene 0.47 $1000 --- U --- 62. ProgionitriX* 3.26 150.000 --- U --- U 67, 1,2,4-Trichlarobanxene 0.50 10.000 --- U --- U 64. Acetanitriie 36.29 55.000 --- U --- U 6$. TenrahydroEuran 0.39 1.000 - U - D 66. 1,4-Dioxans 2.71 3.000 --- U --- U Page: 4 ,7 . Estimated value between the MDL and MRL, U s HelaW ALL QUarititation Limits. DocuSi( m w � d m a z 0 Cif D3C8509C9 WW A 4C23 B61B 5E8AB648F13D ,a 4n °o n i„ .� - - - - �, n -0 f } Fn r r �O0" C' Q do pi�pp � W #� S A � T1 Y rn rFl Ma1 m fn � mm � rn m TOTAL CHLDRINE, mg/1 p m OR ugll AT COLLECTION TEMPERATURE, uC AT COMECTION m O 3 # OF CONTAINERS Nftrate+Nitrite n `Q fir,. '. ��r.�:. �t ;s�: �f'#a �� , Alkalinity #'stir %y'i trh} #:rr, s :r Chloride TDS 6 v x#. fC; Sulfate MM Mr `lfn ,:'s '€ Metals INN �''' �'" ` %? Sulfide Conductivity '9 Temperature Field Parameter Sz60 Dup. 2 8270E r=r+: 8270E Dup. 2 > 47 8270E Dup. 3 4� cn ul n PARAMETERStfESTS n c� S cn C cp�r, o� U Lj L I n ao ) M _ p F v-, n S M m z { C � O S M m L7 n li Z Q C� m .-•j '� A r�r M N S 2 O o Do C S LZ DocuSi v m K Lrl Y+ CD {p C ) cr CD 4 � CS N _O CJ N CD SO Lb w m C) a � N z M En 1 ID 3C8509C9 30CA 4C23 B616 5E8AB648F13D y„ ve rn ope _ d ky1 o (—S m cf/ Fr �y 7ON -CS � � K h Lil ' m m - M 1� m -4 m m m 70TAL CHLORINE, mg/l p m m OR ug/I AT COLLECTION �n 0 t 4irl TEMPERATURE, °C r� 1 ATCOLLECTlON tr O # OF CONTAINERS � MA : 826OD APP. 11 t�J k7 s � 8260D Apo. II 2 C� u 8260 App. 113 ?r. :: n € 82601) App. II 4 G LL ORP 'o mW mi f.:tArh :�rdlh s:t'z t:sr; F,M1s€ 8270E BIH > �] jay Y 1� \ III i-' PARAMETERS/TESTS o � � [3 m n m a �_ m � C7 � C7 O � � O � X cn O m �0 7C m �y m z 21- Q m � � A- N DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D aceAna lytical Deliver To Mark Oliveira LELAP CERTIFICATE NUMBER: 01955 DOD-ELAP ACCREDITATION NUMBER: 74960 ANALYTICAL RESULTS •:I Pace Analytical Gulf Coast 7979 Innovation Park Dr. Baton Rouge, LA 70820 (225) 769-4900 Report Date 06/29/2022 Report Y 222061806 �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III Project C&D Disposal 7407 Samples Collected 6/13/22 - 6/16/22 Environment 1, Inc 114 Oakmont Drive Greenville, NC 27835 (252)756-6208 PJ LA Testing Ek3D ELAP Additional Recipients NONE Pace Gulf Coast Report#: 222061806 Page 1 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D .PaceMahlca! Report#: 222061806 Project ID: C&D Disposal 7407 Laboratory Endorsement Report Date: 06/29/2022 Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non -compliant QC Result (See Q Flag Application Report) " Indicates a non -compliant or not applicable QC recovery or RPD — see narrative E Organics - The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% L Reporting Limits adjusted to meet risk -based limit. P RPD between primary and confirmation result is greater than 40 DL Diluted analysis — when appended to Client Sample ID Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. Authorized Signature Pace Gulf Coast Report 222061806 Pace Gulf Coast Report#: 222061806 Page 2 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Certifications Certification Certification Number DOD ELAP 74960 Alabama 01955 Arkansas 88-0655 Colorado 01955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky 95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Oklahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 Washington C929 USDA Soil Permit P330-16-00234 Pace Gulf Coast Report#: 222061806 Page 3 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D .PaceMahlca! Report#: 222061806 Project ID: C&D Disposal 7407 Case Narrative Client: Environment 1, Inc. Report: 222061806 Report Date: 06/29/2022 Pace Analytical Gulf Coast received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below. VOLATILES GAS CHROMATOGRAPHY In the AM20_B_H2 analysis for batch 743861, the Hydrogen result in the closing CCV was below acceptance criteria In the EPA RSK175 analysis for analytical batch 743616, Methane was detected at an estimated concentration in the method blank. This is probable laboratory contamination. Pace Gulf Coast Report#: 222061806 Page 4 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Summary Lab ID Client ID Matrix Collect Date Receive Date 22206180601 MW-1 S Water 6/13/22 11:06 6/17/22 10:15 22206180602 MW-1 D Water 6/13/22 10:30 6/17/22 10:15 22206180603 MW-2S Water 6/13/22 12:47 6/17/22 10:15 22206180604 MW-2D Water 6/13/22 11:58 6/17/22 10:15 22206180605 MW-3S Water 6/14/22 12:30 6/17/22 10:15 22206180606 MW-3D Water 6/14/22 11:53 6/17/22 10:15 22206180607 MW-3A Water 6/14/22 11:11 6/17/22 10:15 22206180608 MW-4 Water 6/15/22 13:30 6/17/22 10:15 22206180609 MW-6 Water 6/15/22 11:36 6/17/22 10:15 22206180610 MW-7 Water 6/15/22 12:42 6/17/22 10:15 22206180611 MW-8 Water 6/15/22 10:09 6/17/22 10:15 22206180612 MW-5 Water 6/16/22 09:46 6/17/22 10:15 22206180613 MW-1S Bubble Strip 6/13/22 11:06 6/17/22 10:15 22206180614 MW-1D Bubble Strip 6/13/22 10:30 6/17/22 10:15 22206180615 MW-2S Bubble Strip 6/13/22 12:47 6/17/22 10:15 22206180616 MW-2D Bubble Strip 6/13/22 11:58 6/17/22 10:15 22206180617 MW-3S Bubble Strip 6/14/22 12:30 6/17/22 10:15 22206180618 MW-3D Bubble Strip 6/14/22 11:53 6/17/22 10:15 22206180619 MW-3A Bubble Strip 6/14/22 11:11 6/17/22 10:15 22206180620 MW-4 Bubble Strip 6/15/22 13:30 6/17/22 10:15 22206180621 MW-6 Bubble Strip 6/15/22 11:36 6/17/22 10:15 22206180622 MW-7 Bubble Strip 6/15/22 12:42 6/17/22 10:15 22206180623 MW-8 Bubble Strip 6/15/22 10:09 6/17/22 10:15 Pace Gulf Coast Report#: 222061806 Page 5 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Detect Summary Results and Detection Limits are adjusted for dilution and moisture when applicable AM23G Lab ID Client ID Parameter Units Result Dil. %Moist 22206180601 MW-1 S Acetic Acid mg/L 2.4J 10 NA 22206180601 MW-1 S Hexanoic Acid mg/L 2.3J 10 NA 22206180601 MW-1 S Lactic Acid mg/L 4.1 J 10 NA 22206180602 MW-1 D Lactic Acid mg/L 18 5 NA 22206180603 MW-2S Acetic Acid mg/L 2.5J 10 NA 22206180603 MW-2S Butyric Acid mg/L 0.58J 10 NA 22206180603 MW-2S Hexanoic Acid mg/L 1.91 10 NA 22206180603 MW-2S Lactic Acid mg/L 5.5 10 NA 22206180604 MW-21D Acetic Acid mg/L 0.31J 1 NA 22206180604 MW-21D Hexanoic Acid mg/L 0.101 1 NA 22206180604 MW-21D Lactic Acid mg/L 9.6 1 NA 22206180605 MW-3S Acetic Acid mg/L 3.2J 10 NA 22206180605 MW-3S Hexanoic Acid mg/L 2.5J 10 NA 22206180605 MW-3S Lactic Acid mg/L 4.8J 10 NA 22206180606 MW-31D Acetic Acid mg/L 0.62J 5 NA 22206180606 MW-31D Lactic Acid mg/L 16 5 NA 22206180607 MW-3A Acetic Acid mg/L 3.4J 10 NA 22206180607 MW-3A Butyric Acid mg/L 0.61J 10 NA 22206180607 MW-3A Hexanoic Acid mg/L 1.91 10 NA 22206180607 MW-3A Lactic Acid mg/L 6.9 10 NA 22206180608 MW-4 Acetic Acid mg/L 0.38J 1 NA 22206180608 MW-4 Lactic Acid mg/L 0.63 1 NA 22206180609 MW-6 Acetic Acid mg/L 0.46J 1 NA 22206180609 MW-6 Butyric Acid mg/L 0.18J 1 NA 22206180609 MW-6 Lactic Acid mg/L 2.8 1 NA 22206180610 MW-7 Acetic Acid mg/L 0.41J 1 NA 22206180610 MW-7 Hexanoic Acid mg/L 0.26J 1 NA 22206180610 MW-7 Lactic Acid mg/L 0.75 1 NA 22206180610 MW-7 Pentanoic Acid mg/L 0.096J 1 NA 22206180611 MW-8 Acetic Acid mg/L 3.OJ 10 NA 22206180611 MW-8 Lactic Acid mg/L 5.5 10 NA 22206180612 MW-5 Acetic Acid mg/L 2.8J 10 NA 22206180612 MW-5 Lactic Acid mg/L 3.3J 10 NA AM20GAX Lab ID Client ID Parameter Units Result Dil. %Moist 22206180613 MW-1S Hydrogen nM 0.82J 1 NA 22206180614 MW-1D Hydrogen nM 1.11 1 NA 22206180615 MW-2S Hydrogen nM 0.79J 1 NA Pace Gulf Coast Report#: 222061806 Page 6 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Detect Summary (Continued) Results and Detection Limits are adjusted for dilution and moisture when applicable AM20GAX Lab ID Client ID Parameter Units Result Dil. %Moist 22206180616 MW-21D Hydrogen nM 0.78J 1 NA 22206180617 MW-3S Hydrogen nM 0.72J 1 NA 22206180618 MW-31D Hydrogen nM 0.62J 1 NA 22206180619 MW-3A Hydrogen nM 0.51J 1 NA 22206180620 MW-4 Hydrogen nM 0.79J 1 NA 22206180621 MW-6 Hydrogen nM 0.82J 1 NA 22206180622 MW-7 Hydrogen nM 0.75J 1 NA 22206180623 MW-8 Hydrogen nM 0.88J 1 NA EPA RSK175 Lab ID Client ID Parameter Units Result Dil. %Moist 22206180601 MW-1 S Ethane ug/L 0.479J 1 NA 22206180601 MW-1 S Ethene ug/L 0.430J 1 NA 22206180601 MW-1 S Methane ug/L 16.4 1 NA 22206180602 MW-1 D Ethane ug/L 0.443J 1 NA 22206180602 MW-1 D Methane ug/L 306 1 NA 22206180603 MW-2S Ethane ug/L 0.1991 1 NA 22206180603 MW-2S Methane ug/L 1800 1 NA 22206180604 MW-21D Ethane ug/L 0.232J 1 NA 22206180604 MW-21D Methane ug/L 35.1 1 NA 22206180605 MW-3S Ethane ug/L 0.314J 1 NA 22206180605 MW-3S Methane ug/L 3780 1 NA 22206180606 MW-31D Methane ug/L 19.2 1 NA 22206180607 MW-3A Ethane ug/L 0.204J 1 NA 22206180607 MW-3A Methane ug/L 3010 1 NA 22206180608 MW-4 Methane ug/L 308 1 NA 22206180609 MW-6 Methane ug/L 846 1 NA 22206180610 MW-7 Methane ug/L 201 1 NA 22206180611 MW-8 Ethane ug/L 0.221J 1 NA 22206180611 MW-8 Methane ug/L 3040 1 NA 22206180612 MW-5 Methane ug/L 999 1 NA Pace Gulf Coast Report#: 222061806 Page 7 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-1 c Collect Date 06/13/2022 11:06 Lab ID 22206180601 •7 Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2213:05 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 2AJ 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58U 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 2.3J 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 4.1J 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2212:13 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.479J 0.172 1.00 ug/L 74-85-1 Ethene 0.430J 0.241 1.00 ug/L 74-82-8 Methane 16.4 1.98 5.00 ug/L MW-1 D Collect Date 06/13/2022 10:30 Lab ID 22206180602 Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 5 06/24/2217:08 743987 SLL2 NA CAS# Parameter 64-19-7 Acetic Acid 107-92-6 Butyric Acid 142-62-1 Hexanoic Acid 646-07-1 i-Hexanoic Acid 503-74-2 i-Pentanoic Acid 50-21-5 Lactic Acid 109-52-4 Pentanoic Acid 79-09-4 Propionic Acid 127-17-3 Pyruvic Acid Result DL LOQ Units 0.62U 0.62 2.5 mg/L 0.29U 0.29 2.5 mg/L 0.29U 0.29 2.5 mg/L 0.28U 0.28 2.5 mg/L 0.30U 0.30 2.5 mg/L 18 0.27 2.5 mg/L 0.28U 0.28 2.5 mg/L 0.27U 0.27 2.5 mg/L 0.30U 0.30 2.5 mg/L Pace Gulf Coast Report#: 222061806 Page 8 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-1 D Collect Date 06/13/2022 10:30 Lab ID 22206180602 Receive Date 06/17/2022 10:15 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2212:24 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.443J 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 306 1.98 5.00 ug/L MW-25 Collect Date 06/13/2022 12:47 Lab ID 22206180603 Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2213:48 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 2.5J 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58J 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 1.91 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 5.5 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2212:35 743616 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.1991 0.172 1.00 0.241 U 0.241 1.00 1800 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222061806 Page 9 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-2D Collect Date 06/13/2022 11:58 Lab ID 22206180604 Receive Date 06/17/2022 10:15 Matrix Water 3G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2214:10 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.31J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.101 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 9.6 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2212:46 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.232J 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 35.1 1.98 5.00 ug/L Collect Date 06/14/2022 12:30 Lab ID 22206180605 MW�35 Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2215:07 743719 SLL2 NA CAS# Parameter 64-19-7 Acetic Acid 107-92-6 Butyric Acid 142-62-1 Hexanoic Acid 646-07-1 i-Hexanoic Acid 503-74-2 i-Pentanoic Acid 50-21-5 Lactic Acid 109-52-4 Pentanoic Acid 79-09-4 Propionic Acid 127-17-3 Pyruvic Acid Result DL LOQ Units 3.2J 1.2 5.0 mg/L 0.58U 0.58 5.0 mg/L 2.5J 0.58 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.61 U 0.61 5.0 mg/L 4.8J 0.53 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.53U 0.53 5.0 mg/L 0.60U 0.60 5.0 mg/L Pace Gulf Coast Report#: 222061806 Page 10 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-3S•7 Collect Date 06/14/2022 12:30 Lab ID 22206180605 Receive Date 06/17/2022 10:15 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2212:58 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.314J 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 3780 1.98 5.00 ug/L Collect Date 06/14/2022 11:53 Lab ID 22206180606 MW-3� Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 5 06/24/2217:30 743987 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.62J 0.62 2.5 mg/L 107-92-6 Butyric Acid 0.29U 0.29 2.5 mg/L 142-62-1 Hexanoic Acid 0.29U 0.29 2.5 mg/L 646-07-1 i-Hexanoic Acid 0.28U 0.28 2.5 mg/L 503-74-2 i-Pentanoic Acid 0.30U 0.30 2.5 mg/L 50-21-5 Lactic Acid 16 0.27 2.5 mg/L 109-52-4 Pentanoic Acid 0.28U 0.28 2.5 mg/L 79-09-4 Propionic Acid 0.27U 0.27 2.5 mg/L 127-17-3 Pyruvic Acid 0.30U 0.30 2.5 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2213:09 743616 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.172U 0.172 1.00 0.241 U 0.241 1.00 19.2 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222061806 Page 11 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-3A Collect Date 06/14/2022 11:11 Lab ID 22206180607 Receive Date 06/17/2022 10:15 Matrix Water AM23G "Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2215:51 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 3.4J 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.61J 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 1.91 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 6.9 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2213:20 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.204J 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 3010 1.98 5.00 ug/L Collect Date 06/15/2022 13:30 Lab ID 22206180608 MW-4 Receive Date 06/17/2022 10:15 Matrix Water 3G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2216:12 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.38J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.058U 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 0.63 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L Pace Gulf Coast Report#: 222061806 Page 12 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results Collect Date 06/15/2022 13:30 Lab ID 22206180608 MW�4 Receive Date 06/17/2022 10:15 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2213:32 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 308 1.98 5.00 ug/L c Collect Date 06/15/2022 11:36 Lab ID 22206180609 MW-V Receive Date 06/17/2022 10:15 Matrix Water AM23G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2216:34 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.46J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.18J 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.058U 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 2.8 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2213:43 743616 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.172U 0.172 1.00 0.241 U 0.241 1.00 846 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222061806 Page 13 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results Collect Date 06/15/2022 12:42 Lab ID 22206180610 MW�% Receive Date 06/17/2022 10:15 Matrix Water 3G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2217:38 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.41J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.26J 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 0.75 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.096J 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2213:54 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 201 1.98 5.00 ug/L MW-8 Collect Date 06/15/2022 10:09 Lab ID 22206180611 Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2218:00 743719 SLL2 NA CAS# Parameter 64-19-7 Acetic Acid 107-92-6 Butyric Acid 142-62-1 Hexanoic Acid 646-07-1 i-Hexanoic Acid 503-74-2 i-Pentanoic Acid 50-21-5 Lactic Acid 109-52-4 Pentanoic Acid 79-09-4 Propionic Acid 127-17-3 Pyruvic Acid Result DL LOQ Units 3.OJ 1.2 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.61 U 0.61 5.0 mg/L 5.5 0.53 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.53U 0.53 5.0 mg/L 0.60U 0.60 5.0 mg/L Pace Gulf Coast Report#: 222061806 Page 14 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-Q Collect Date 06/15/2022 10:09 Lab ID 22206180611 v Receive Date 06/17/2022 10:15 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2214:06 743616 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.221J 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 3040 1.98 5.00 ug/L Collect Date 06/16/2022 09:46 Lab ID 22206180612 MW-G Receive Date 06/17/2022 10:15 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 06/23/2218:22 743719 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 2.8J 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58U 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 0.58U 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 3.3J 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/20/2214:17 743616 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.172U 0.172 1.00 0.241 U 0.241 1.00 999 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222061806 Page 15 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-1 c Collect Date 06/13/2022 11:06 Lab ID 22206180613 •7 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 08:56 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.82J 0.49 1.9 nM MW-1 D Collect Date 06/13/2022 10:30 Lab ID 22206180614 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 09:08 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 1.11 0.49 1.9 nM MW-2S Collect Date 06/13/2022 12:47 Lab ID 22206180615 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 09:20 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.79J 0.49 1.9 nM Collect Date 06/13/2022 11:58 Lab ID 22206180616 MW-2D Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 09:32 743861 LMB NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ Units 0.78J 0.49 1.9 nM Pace Gulf Coast Report#: 222061806 Page 16 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-3S•7 Collect Date 06/14/2022 12:30 Lab ID 22206180617 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 09:47 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.72J 0.49 1.9 nM MW-3D Collect Date 06/14/2022 11:53 Lab ID 22206180618 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 09:59 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.62J 0.49 1.9 nM Collect Date 06/14/2022 11:11 Lab ID 22206180619 MW�3A Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/22 10:15 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.51J 0.49 1.9 nM Collect Date 06/15/2022 13:30 Lab ID 22206180620 MW�4 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2210:29 743861 LMB NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ Units 0.79J 0.49 1.9 nM Pace Gulf Coast Report#: 222061806 Page 17 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 Sample Results MW-c Collect Date 06/15/2022 11:36 Lab ID 22206180621 v Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2210:41 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.82J 0.49 1.9 nM Collect Date 06/15/2022 12:42 Lab ID 22206180622 MW�7 Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2211:45 743861 LMB NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 0.75J 0.49 1.9 nM Collect Date 06/15/2022 10:09 Lab ID 22206180623 MW-Q Receive Date 06/17/2022 10:15 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 06/23/2211:57 743861 LMB NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ Units 0.881 0.49 1.9 nM Pace Gulf Coast Report#: 222061806 Page 18 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 General Chemistry QC Summary Analytical Batch Client ID MB743719 LCS743719 LCSD743719 743719 Lab ID 2361449 2361450 2361451 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 06/23/22 12:22 06/23/22 12:00 06/23/22 16:55 Matrix Water Water Water AM23G Units mg/L Spike Result %R Control Spike Result %R RPD RPD Result DL Added Limits%R Added Limit Acetic Acid 64-19-7 0.12U 0.12 2.0 2.0 102 70 - 130 2.0 2.0 101 1 20 Butyric Acid 107-92-6 0.058U 0.058 2.0 1.9 94 70 - 130 2.0 1.8 88 7 20 Hexanoic Acid 142-62-1 0.058U 0.058 2.0 1.8 92 70 - 130 2.0 1.8 92 1 20 i-Hexanoic Acid 646-07-1 0.056U 0.056 2.0 2.6 128 70 - 130 2.0 2.5 123 4 20 i-Pentanoic Acid 503-74-2 0.061 U 0.061 2.0 1.8 90 70 - 130 2.0 1.7 87 4 20 Lactic Acid 50-21-5 0.053U 0.053 2.0 2.4 118 70 - 130 2.0 2.3 114 4 20 Pentanoic Acid 109-52-4 0.056U 0.056 2.0 1.7 86 70 - 130 2.0 1.7 84 2 20 Propionic Acid 79-09-4 0.053U 0.053 2.0 2.0 102 70 - 130 2.0 2.0 100 1 20 Pyruvic Acid 127-17-3 0.060U 0.060 2.0 1.8 89 70 - 130 2.0 1.8 90 2 20 Analytical Batch Client ID MB743987 LCS743987 743987 Lab ID 2363237 2363238 Sample Type MB LCS Prep Date NA NA Analysis Date 06/24/22 13:33 06/24/22 13:11 Matrix Water Water AM23G Units mg/L Spike Result %R Control Result DL Added Limits%R Acetic Acid 64-19-7 0.12U 0.12 2.0 1.8 93 70 - 130 Butyric Acid 107-92-6 0.058U 0.058 2.0 1.9 93 70 - 130 Hexanoic Acid 142-62-1 0.058U 0.058 2.0 1.9 97 70 - 130 i-Hexanoic Acid 646-07-1 0.056U 0.056 2.0 2.4 120 70 - 130 i-Pentanoic Acid 503-74-2 0.061 U 0.061 2.0 1.7 83 70 - 130 Lactic Acid 50-21-5 0.053U 0.053 2.0 2.3 113 70 - 130 Pentanoic Acid 109-52-4 0.056U 0.056 2.0 1.8 89 70 - 130 Propionic Acid 79-09-4 0.053U 0.053 2.0 1.9 93 70 - 130 Pyruvic Acid 127-17-3 0.060U 0.060 2.0 1.91 96 1 70 - 130 Pace Gulf Coast Report#: 222061806 Page 19 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222061806 Project ID: C&D Disposal 7407 Report Date: 06/29/2022 General Chromatography QC Summary Analytical Batch Client ID MB743861 LCS743861 LCSD743861 743861 Lab ID 2362478 2362479 2362480 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 06/23/22 08:44 06/23/22 08:19 06/23/22 08:32 Matrix Bubble Strip Bubble Strip Bubble Strip AM20GAX Units nM Spike Result %R Control Spike Result %R RPD RPD Result DL Added Limits%R Added Limit Hydrogen 1333-74-0 0.49U 1 0.491 121 9.21 77 1 70 - 130 1 121 8.7 174 1 5 1 20 Analytical Batch Client ID MB743616 LCS743616 LCSD743616 743616 Lab ID 2360940 2360941 2360942 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 06/20/22 10:30 06/20/22 09:56 06/20/22 10:08 Matrix Water Water Water EPA RSK175 Units ug/L Spike I Result %R Control Spike Result %R RPDT30 Result DL Added Limits%R Added Ethane 74-84-0 0.172U 0.172 97.1 73.0 75 70 - 130 97.1 85.4 88 16Ethene 74-85-1 0.241U 0.241 120 89.2 74 70-130 120 103 86 14Methane 74-82-8 2.97J 1.98 384 302 79 70-130 384 355 92 16 Pace Gulf Coast Report#: 222061806 Page 20 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D aceAnalyJFlcal - 79791nnovst n Park Drive I Salon Rouge, IA 70520 7402 72a169.490o I vaxv.9m1.cam GRAIN OF CUSTODY RECORD Client ID: E t - Enwranrnent 1, Inc SDG: 222D61806 PM: RV\te ReportTO1 Client: nv:rofl "en I- T1t-. Address: j ir{ Ct w- 62eli ile, Nl' Z}%SS Contact .(k ol„retr.,\ Phone: Email: �,�Iuli,retr��nf:ro�n !1L.CAM Bill To: Client fnwr2A#rnek I --TA&. Address_ 11q Pr: ve, &-eeenOie., N(- Z794sr Contact: Mmk DliytM%, Phone: T. Z-756-LZoB Emaih Mlofr�r Dnr:rvnrn i4 iAt Eon^ Anal iaai Re nests J3 Method Custody Seal: tiled. ❑ Yes ❑ No Jntact: Yes ❑ Na Temperature: p � 1~Y 5 i1- J 0 Dissoived Analysis Requested ❑ Field Filtered ❑ Lab Filtered P.D. Number Project NamerHumber ` (L Sampred By, P66 (i, J ��lf w Metric, Date The c� nt a Sample Description co Aarers Preservative f Notes GOAL 10 6 1 ""- K I0-3�' x 1414-J r2.4'7 x MV- Z I}:5S X ,Aw 2�1 6 1q-zz IT30 (AV- 35 11;65 ?c l/-3D (� 110 ,C pu-' t3 3c' -/- MV -L( lj-u 7 tA\J-(, 12'ff 7� �'(-J fDi )o.01 7K MU � �3 9' ff �a' G• .lEy X Xq- i AlrbilI Number: Turn Around Time(Business Days): ❑ RtJSH6 Days astandard (per contra quote) ulahed by{SignIKMQ Daierlme¢ (.Z£ �.0C3PP4 Retelaed by lSlgWurej QaMT"a. Notes: � I � VON I c e mlid- i4tl �� wtcifil. Vn L,l(,;y sk"Apt Yf rohtJ� i j einqui ed 5g,elu�C} Rtterveeh Signalurej Lta[y�m: e Tic z J Od ReUqulshed hy.{--VnaWee} nalrlTlma' ReceMedh nadurej 6alrJTme: 'Matrix: W = Water, S=Solid, L=Liqu■icl, TT=Tissue. x '- Requires prior approval. Rush charges may apply. We cannot accept verbal changes. Please emai wdltan changes to your PAGC Protect Manager. -jr V 647 1/F -S 07O�r�J Pace Gulf Coast Report#: 222061806 Page 21 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D rvauAnalytical' SAMPLE RECEIVING CHECKLIST IIIIIIIIII III SAMPLE DELIVERY GROUP 222061806 CHECKLIST YES NO Client PM IRV% Transport Method Samples received with proper thermal preservation? *❑ ❑ E1 - Environrrent 1, Inc. F®DC Radioactivity is <1600 cpm? If no, record cpm value in notes section. COC relinquished and complete (including samplelDs, collect times, and sampler)? *❑ *❑ ❑ ❑ Profile Number Received By 290471 I/bane, DDdie N. All containers received in good condition and within hold time? All sample labels and containers received match the chain of custody? .�I❑ *❑ ❑ ❑ Line Item(s) Receive Date(s) 1 - IVEELLVFA 06/17/22 2- Hydrogen Preservative added to any containers? ❑ /❑ If received, was headspace for VOC water containers < 6mm? *❑ ❑ Samples collected in containers provided by Pace Gulf Coast? 0 ❑ COOLERS DISCREPANCIES LAB PRESERVATIONS Airbill Thermometer ID E42 Temp °C None None 3.6 NOTES Revision 1.6 Page 1 of 1 Pace Gulf Coast Report#: 222061806 Page 22 of 22 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D aceAna lytical Deliver To Mark Oliveira LELAP CERTIFICATE NUMBER: 01955 DOD-ELAP ACCREDITATION NUMBER: 74960 ANALYTICAL RESULTS •:I Pace Analytical Gulf Coast 7979 Innovation Park Dr. Baton Rouge, LA 70820 (225) 769-4900 Report Date 07/12/2022 Report Y 222063033 �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III Project C&D Disposal / 7407 Samples Collected 6/27/22 - 6/28/22 Environment 1, Inc 114 Oakmont Drive Greenville, NC 27835 (252)756-6208 PJ LA Testing Ek3D ELAP Additional Recipients NONE Pace Gulf Coast Report#: 222063033 Page 1 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D .PaceMahlca! Report#: 222063033 Project ID: C&D Disposal / 7407 Laboratory Endorsement Report Date: 07/12/2022 Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non -compliant QC Result (See Q Flag Application Report) " Indicates a non -compliant or not applicable QC recovery or RPD — see narrative E Organics - The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% L Reporting Limits adjusted to meet risk -based limit. P RPD between primary and confirmation result is greater than 40 DL Diluted analysis — when appended to Client Sample ID Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. Authorized Signature Pace Gulf Coast Report 222063033 Pace Gulf Coast Report#: 222063033 Page 2 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Certifications Certification Certification Number DOD ELAP 74960 Alabama 01955 Arkansas 88-0655 Colorado 01955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky 95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Oklahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 Washington C929 USDA Soil Permit P330-16-00234 Pace Gulf Coast Report#: 222063033 Page 3 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D .PaceMahlca! Report#: 222063033 Project ID: C&D Disposal / 7407 Case Narrative Client: Environment 1, Inc. Report: 222063033 Report Date: 07/12/2022 Pace Analytical Gulf Coast received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below. VOLATILES GAS CHROMATOGRAPHY In the AM20_BS H2 analysis for analytical batch 744492, the closing CCV did not meet acceptance criteria. All other QCs are within control limits In the EPA RSK175 analysis for analytical batch 745093, Ethane was detected at an estimated concentration in the method blank. This is probable laboratory contamination. Pace Gulf Coast Report#: 222063033 Page 4 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Summary Lab ID Client ID Matrix Collect Date Receive Date 22206303301 MW-9A Water 6/27/22 10:11 6/29/22 10:00 22206303302 MW-10 Water 6/27/22 11:16 6/29/22 10:00 22206303303 MW-11 Water 6/27/22 12:16 6/29/22 10:00 22206303304 MW-12S Water 6/27/22 13:03 6/29/22 10:00 22206303305 MW-13 Water 6/27/22 14:00 6/29/22 10:00 22206303306 MW-14S Water 6/28/22 12:14 6/29/22 10:00 22206303307 MW-14D Water 6/28/22 11:29 6/29/22 10:00 22206303308 MW-15 Water 6/28/22 14:17 6/29/22 10:00 22206303309 MW-16 Water 6/28/22 13:30 6/29/22 10:00 22206303310 MW-9A Bubble Strip 6/27/22 10:11 6/29/22 10:00 22206303311 MW-10 Bubble Strip 6/27/22 11:16 6/29/22 10:00 22206303312 MW-12S Bubble Strip 6/27/22 12:16 6/29/22 10:00 22206303313 MW-13 Bubble Strip 6/27/22 14:00 6/29/22 10:00 22206303314 MW-14S Bubble Strip 6/28/22 12:14 6/29/22 10:00 22206303315 MW-14D Bubble Strip 6/28/22 11:29 6/29/22 10:00 22206303316 MW-15 Bubble Strip 6/28/22 14:17 6/29/22 10:00 22206303317 MW-16 Bubble Strip 6/28/22 13:30 6/29/22 10:00 22206303318 MW-17 Bubble Strip 6/28/22 10:17 6/29/22 10:00 22206303319 MW-17 Water 6/28/22 10:17 6/30/22 09:58 22206303320 MW-11 Bubble Strip 6/27/22 12:16 6/30/22 09:58 Pace Gulf Coast Report#: 222063033 Page 5 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Detect Summary Results and Detection Limits are adjusted for dilution and moisture when applicable AM23G Lab ID Client ID Parameter Units Result Dil. %Moist 22206303301 MW-9A Acetic Acid mg/L 3.0 1 NA 22206303301 MW-9A Hexanoic Acid mg/L 0.085J 1 NA 22206303301 MW-9A Lactic Acid mg/L 1.2 1 NA 22206303302 MW-10 Acetic Acid mg/L 3.7,1 10 NA 22206303302 MW-10 Lactic Acid mg/L 2.3J 10 NA 22206303303 MW-11 Acetic Acid mg/L 0.31J 1 NA 22206303303 MW-11 Hexanoic Acid mg/L 0.065J 1 NA 22206303303 MW-11 Lactic Acid mg/L 1.7 1 NA 22206303304 MW-12S Acetic Acid mg/L 2.5,1 10 NA 22206303304 MW-12S Hexanoic Acid mg/L 0.59J 10 NA 22206303304 MW-12S Lactic Acid mg/L 3.OJ 10 NA 22206303305 MW-13 Acetic Acid mg/L 2.3,1 10 NA 22206303305 MW-13 Lactic Acid mg/L 2.1J 10 NA 22206303306 MW-14S Acetic Acid mg/L 2.5,1 10 NA 22206303306 MW-14S Hexanoic Acid mg/L 1.11 10 NA 22206303306 MW-14S Lactic Acid mg/L 2.5,1 10 NA 22206303307 MW-14D Acetic Acid mg/L 0.31J 1 NA 22206303307 MW-14D Lactic Acid mg/L 9.5 1 NA 22206303308 MW-15 Acetic Acid mg/L 0.27J 1 NA 22206303308 MW-15 Butyric Acid mg/L 0.18J 1 NA 22206303308 MW-15 Hexanoic Acid mg/L 0.29J 1 NA 22206303308 MW-15 Lactic Acid mg/L 1.2 1 NA 22206303309 MW-16 Acetic Acid mg/L 1.91 10 NA 22206303309 MW-16 Lactic Acid mg/L 2.1J 10 NA 22206303319 MW-17 Acetic Acid mg/L 0.23J 1 NA AM20GAX Lab ID Client ID Parameter Units Result Dil. %Moist 22206303310 MW-9A Hydrogen nM 2.4 1 NA 22206303311 MW-10 Hydrogen nM 2.2 1 NA 22206303312 MW-12S Hydrogen nM 2.8 1 NA 22206303313 MW-13 Hydrogen nM 2.2 1 NA 22206303314 MW-14S Hydrogen nM 1.2J 1 NA 22206303315 MW-14D Hydrogen nM 1.8J 1 NA 22206303316 MW-15 Hydrogen nM 2.6 1 NA 22206303317 MW-16 Hydrogen nM 1.6J 1 NA 22206303318 MW-17 Hydrogen nM 1.3J 1 NA 22206303320 MW-11 Hydrogen nM 1.7J 1 NA EPA RSK175 Lab ID Client ID Parameter Units Result Dil. %Moist 22206303301 MW-9A Methane ug/L 90.1 1 NA Pace Gulf Coast Report#: 222063033 Page 6 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Detect Summary (Continued) Results and Detection Limits are adjusted for dilution and moisture when applicable EPA RSK175 Lab ID Client ID Parameter Units Result Dil. %Moist 22206303302 MW-10 Methane ug/L 3680 1 NA 22206303303 MW-11 Ethane ug/L 0.235J 1 NA 22206303303 MW-11 Ethene ug/L 0.328J 1 NA 22206303303 MW-11 Methane ug/L 112 1 NA 22206303304 MW-12S Ethene ug/L 0.408J 1 NA 22206303304 MW-12S Methane ug/L 3540 1 NA 22206303305 MW-13 Ethene ug/L 0.317J 1 NA 22206303305 MW-13 Methane ug/L 1520 1 NA 22206303306 MW-14S Ethane ug/L 0.188J 1 NA 22206303306 MW-14S Ethene ug/L 1.23 1 NA 22206303306 MW-14S Methane ug/L 1970 1 NA 22206303307 MW-14D Methane ug/L 2.91J 1 NA 22206303308 MW-15 Ethene ug/L 0.273J 1 NA 22206303308 MW-15 Methane ug/L 2320 1 NA 22206303309 MW-16 Ethane ug/L 0.226J 1 NA 22206303309 MW-16 Methane ug/L 2670 1 NA 22206303319 MW-17 Ethane ug/L 0.196J 1 NA 22206303319 MW-17 Methane ug/L 404 1 NA Pace Gulf Coast Report#: 222063033 Page 7 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-9A Collect Date 06/27/2022 10:11 Lab ID 22206303301 Receive Date 06/29/2022 10:00 Matrix Water 3G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/06/2211:50 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 3.0 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.085J 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 1.2 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2213:33 745093 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 90.1 1.98 5.00 ug/L MW-1 O Collect Date 06/27/2022 11:16 Lab ID 22206303302 Receive Date 06/29/2022 10:00 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 07/06/2212:12 744740 SLL2 NA CAS# Parameter 64-19-7 Acetic Acid 107-92-6 Butyric Acid 142-62-1 Hexanoic Acid 646-07-1 i-Hexanoic Acid 503-74-2 i-Pentanoic Acid 50-21-5 Lactic Acid 109-52-4 Pentanoic Acid 79-09-4 Propionic Acid 127-17-3 Pyruvic Acid Result DL LOQ Units 3.7J 1.2 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.61 U 0.61 5.0 mg/L 2.3J 0.53 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.53U 0.53 5.0 mg/L 0.60U 0.60 5.0 mg/L Pace Gulf Coast Report#: 222063033 Page 8 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-1 O Collect Date 06/27/2022 11:16 Lab ID 22206303302 Receive Date 06/29/2022 10:00 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2214:42 744837 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 3680 1.98 5.00 ug/L Collect Date 06/27/2022 12:16 Lab ID 22206303303 MW�1 1 Receive Date 06/29/2022 10:00 Matrix Water AM23G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/06/2212:34 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.31J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.065J 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 1.7 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2214:53 744837 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.235J 0.172 1.00 0.328J 0.241 1.00 112 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222063033 Page 9 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-12S Collect Date 06/27/2022 13:03 Lab ID 22206303304 Receive Date 06/29/2022 10:00 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 07/06/2212:55 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 2.5J 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58U 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 0.591 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 3.OJ 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2215:04 744837 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.408J 0.241 1.00 ug/L 74-82-8 Methane 3540 1.98 5.00 ug/L MW-1 3 Collect Date 06/27/2022 14:00 Lab ID 22206303305 Receive Date 06/29/2022 10:00 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 07/06/2213:17 744740 SLL2 NA CAS# Parameter 64-19-7 Acetic Acid 107-92-6 Butyric Acid 142-62-1 Hexanoic Acid 646-07-1 i-Hexanoic Acid 503-74-2 i-Pentanoic Acid 50-21-5 Lactic Acid 109-52-4 Pentanoic Acid 79-09-4 Propionic Acid 127-17-3 Pyruvic Acid Result DL LOQ Units 2.3J 1.2 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.58U 0.58 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.61 U 0.61 5.0 mg/L 2.1J 0.53 5.0 mg/L 0.56U 0.56 5.0 mg/L 0.53U 0.53 5.0 mg/L 0.60U 0.60 5.0 mg/L Pace Gulf Coast Report#: 222063033 Page 10 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-1 3 Collect Date 06/27/2022 14:00 Lab ID 22206303305 Receive Date 06/29/2022 10:00 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2215:16 744837 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.317J 0.241 1.00 ug/L 74-82-8 Methane 1520 1.98 5.00 ug/L MW-14S Collect Date 06/28/2022 12:14 Lab ID 22206303306 Receive Date 06/29/2022 10:00 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 07/06/2213:38 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 2.5J 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58U 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 1.1J 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 2.5J 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2215:27 744837 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.188J 0.172 1.00 1.23 0.241 1.00 1970 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222063033 Page 11 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-14D Collect Date 06/28/2022 11:29 Lab ID 22206303307 Receive Date 06/29/2022 10:00 Matrix Water 13G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/06/2214:00 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.31J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.058U 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 9.5 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2215:38 744837 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.241 U 0.241 1.00 ug/L 74-82-8 Methane 2.91J 1.98 5.00 ug/L MW-1 5 Collect Date 06/28/2022 14:17 Lab ID 22206303308 Receive Date 06/29/2022 10:00 Matrix Water 13G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/06/2214:21 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.27J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.181 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.29J 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 1.2 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L Pace Gulf Coast Report#: 222063033 Page 12 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-1 5 Collect Date 06/28/2022 14:17 Lab ID 22206303308 Receive Date 06/29/2022 10:00 Matrix Water EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2215:50 744837 LMB NA CAS# Parameter Result DL LOQ Units 74-84-0 Ethane 0.172U 0.172 1.00 ug/L 74-85-1 Ethene 0.273J 0.241 1.00 ug/L 74-82-8 Methane 2320 1.98 5.00 ug/L Collect Date 06/28/2022 13:30 Lab ID 22206303309 MW-1 s Receive Date 06/29/2022 10:00 Matrix Water AM23G *Results and limits are adjusted for dilution. Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 10 07/06/2216:11 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 1.91 1.2 5.0 mg/L 107-92-6 Butyric Acid 0.58U 0.58 5.0 mg/L 142-62-1 Hexanoic Acid 0.58U 0.58 5.0 mg/L 646-07-1 i-Hexanoic Acid 0.56U 0.56 5.0 mg/L 503-74-2 i-Pentanoic Acid 0.61 U 0.61 5.0 mg/L 50-21-5 Lactic Acid 2.1J 0.53 5.0 mg/L 109-52-4 Pentanoic Acid 0.56U 0.56 5.0 mg/L 79-09-4 Propionic Acid 0.53U 0.53 5.0 mg/L 127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2216:01 744837 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.226J 0.172 1.00 0.241 U 0.241 1.00 2670 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222063033 Page 13 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-9A Collect Date 06/27/2022 10:11 Lab ID 22206303310 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 07:56 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 2.4 0.49 1.9 nM MW-1 O Collect Date 06/27/2022 11:16 Lab ID 22206303311 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 08:08 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 2.2 0.49 1.9 nM MW-12S Collect Date 06/27/2022 12:16 Lab ID 22206303312 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 08:20 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 2.8 0.49 1.9 nM MW-1 3 Collect Date 06/27/2022 14:00 Lab ID 22206303313 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 08:33 744492 AWE NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ Units 2.2 0.49 1.9 nM Pace Gulf Coast Report#: 222063033 Page 14 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-14S Collect Date 06/28/2022 12:14 Lab ID 22206303314 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 08:45 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 1.2J 0.49 1.9 nM MW-14D Collect Date 06/28/2022 11:29 Lab ID 22206303315 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 09:04 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 1.8J 0.49 1.9 nM Collect Date 06/28/2022 14:17 Lab ID 22206303316 MW-15 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 09:17 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 2.6 0.49 1.9 nM Collect Date 06/28/2022 13:30 Lab ID 22206303317 MW-1C Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 09:29 744492 AWE NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ Units 1.6J 0.49 1.9 n M Pace Gulf Coast Report#: 222063033 Page 15 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-1 7 Collect Date 06/28/2022 10:17 Lab ID 22206303318 Receive Date 06/29/2022 10:00 Matrix Bubble Strip AM20GAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 09:41 744492 AWE NA CAS# Parameter Result DL LOQ Units 1333-74-0 Hydrogen 1.3J 0.49 1.9 nM MW-1 7 Collect Date 06/28/2022 10:17 Lab ID 22206303319 Receive Date 06/30/2022 09:58 Matrix Water AM23G Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/06/2216:33 744740 SLL2 NA CAS# Parameter Result DL LOQ Units 64-19-7 Acetic Acid 0.23J 0.12 0.50 mg/L 107-92-6 Butyric Acid 0.058U 0.058 0.50 mg/L 142-62-1 Hexanoic Acid 0.058U 0.058 0.50 mg/L 646-07-1 i-Hexanoic Acid 0.056U 0.056 0.50 mg/L 503-74-2 i-Pentanoic Acid 0.061 U 0.061 0.50 mg/L 50-21-5 Lactic Acid 0.053U 0.053 0.50 mg/L 109-52-4 Pentanoic Acid 0.056U 0.056 0.50 mg/L 79-09-4 Propionic Acid 0.053U 0.053 0.50 mg/L 127-17-3 Pyruvic Acid 0.060U 0.060 0.50 mg/L EPA RSK175 Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/07/2216:12 744837 LMB NA CAS# Parameter 74-84-0 Ethane 74-85-1 Ethene 74-82-8 Methane Result DL LOQ 0.196J 0.172 1.00 0.241 U 0.241 1.00 404 1.98 5.00 Units ug/L ug/L ug/L Pace Gulf Coast Report#: 222063033 Page 16 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 Sample Results MW-1 1 Collect Date 06/27/2022 12:16 Lab ID 22206303320 Receive Date 06/30/2022 09:58 Matrix Bubble Strip OGAX Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture NA NA NA 1 07/01/22 09:54 744492 AWE NA CAS# Parameter 1333-74-0 Hydrogen Result DL LOQ 1.7J 0.49 1.9 Units nM Pace Gulf Coast Report#: 222063033 Page 17 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 General Chemistry QC Summary Analytical Batch Client ID MB744740 LCS744740 LCSD744740 744740 Lab ID 2367364 2367365 2367366 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 07/06/22 10:46 07/06/22 15:05 07/06/22 19:47 Matrix Water Water Water AM23G Units mg/L Spike Result %R Control Spike Result %R RPD RPD Result DL Added Limits%R Added Limit Acetic Acid 64-19-7 0.12U 0.12 2.0 2.0 102 70 - 130 2.0 2.0 101 1 20 Butyric Acid 107-92-6 0.058U 0.058 2.0 1.8 89 70 - 130 2.0 1.8 92 3 20 Hexanoic Acid 142-62-1 0.058U 0.058 2.0 1.6 81 70 - 130 2.0 1.8 89 9 20 i-Hexanoic Acid 646-07-1 0.056U 0.056 2.0 2.4 119 70 - 130 2.0 2.3 113 5 20 i-Pentanoic Acid 503-74-2 0.061 U 0.061 2.0 1.6 81 70 - 130 2.0 1.5 76 7 20 Lactic Acid 50-21-5 0.053U 0.053 2.0 2.5 123 70 - 130 2.0 2.6 129 5 20 Pentanoic Acid 109-52-4 0.056U 0.056 2.0 1.7 83 70 - 130 2.0 1.7 83 0 20 Propionic Acid 79-09-4 0.053U 0.053 2.0 1.9 95 70 - 130 2.0 2.0 98 3 20 Pyruvic Acid 127-17-3 0.060U 0.060 2.0 1.8 88 70 - 130 2.0 1.9 95 8 20 Pace Gulf Coast Report#: 222063033 Page 18 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �aceAnaltrcal Report#: 222063033 Project ID: C&D Disposal / 7407 Report Date: 07/12/2022 General Chromatography QC Summary Analytical Batch Client ID MB744492 LCS744492 LCSD744492 744492 Lab ID 2365855 2365856 2365857 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 07/01/22 07:44 07/01/22 07:19 07/01/22 07:32 Matrix Bubble Strip Bubble Strip Bubble Strip AM20GAX Units nM Spike Result %R Control Spike Result %R RPD RPD Result DL Added Limits%R Added Limit Hydrogen 1333-74-0 0.49U 1 0.491 121 101 87 1 70 - 130 1 121 9.7 182 1 5 1 20 Analytical Batch Client ID MB744837 LCS744837 LCSD744837 744837 Lab ID 2367927 2367928 2367929 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 07/07/22 14:30 07/07/22 13:56 07/07/22 14:07 Matrix Water Water Water EPA RSK175 Units ug/L Spike I Result %R Control Spike Result %R RPDT30 Result DL Added Limits%R Added Ethane 74-84-0 0.172U 0.172 97.1 108 111 70 - 130 97.1 103 106 5 Ethene 74-85-1 0.241U 0.241 120 133 111 70-130 120 129 108 3 Methane 74-82-8 1.98U 1.98 384 402 105 70-130 384 381 99 5 Analytical Batch Client ID MB745093 LCS745093 LCSD745093 745093 Lab ID 2369049 2369050 2369051 Sample Type MB LCS LCSD Prep Date NA NA NA Analysis Date 07/07/22 06:42 07/07/22 05:58 07/07/22 06:09 Matrix Water Water Water EPA RSK175 Units ug/L Spike I Result %R Control Spike Result %R RPDT30 Result DL Added Limits%R Added Ethane 74-84-0 0.204J 0.172 97.1 110 113 70 - 130 97.1 111 114 1 Ethene 74-85-1 0.241 U 0.241 120 136 113 70-130120 136 113 0 Methane 74-82-8 1.98U 1.98 384 424 110 70-130 384 416 108 2 Pace Gulf Coast Report#: 222063033 Page 19 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 6► ? CHAIN -CIF -CUSTODY Analytical Request Document W1USE ONLY- Affix Wori PlaceAnalytical Chant !D:. El - Envifonrr+snt 4 ! : Chain -of -Custody is a LEGAL DOCUMENT - Canpfele all releuenl fields Company: Blilirg Information; SOG: 222063033 ALLl1VI�a�SMP�I-�rZi1L SHAD Container Preservative Tj RVVe +�r�1 • PreservalaeT s 1 rMricadd, 2 suth�ricar 3 h YPe (i I i d,! 1 ydrochlaric aeA.14}sadrum hydrvKiee, L51+.n4L11— , (G)xnv*am4. 13] sodium bi€ulfate, (Sl sodium thiosulrate, (9j hexane, (Al ascorbic acid, (a) arnmoniurn sulfate, (C) ammonnrmtTdroxide, (D)TSP, I014inpreserved,101 Ocher Re art Taf �A i p f'�{l k 011 Ve't(8.-- 1 Email ol,Yai�a�[i V'•ronMa .Y �t�L Copy TO; Site Collection rnfo}Address_ Customer Projjeect Name/Nurnbec Stake: lCotlnlywcity: Time Zone Collected: Analyses lab prof ie/Line; Lab sarmple Receipt Checklist: dC� Vi5 Srx1 I � I" C' f L I IpTI [MT1 Icr r fFT Custody Seals PresentlSntaCt Y !! NA Custody Signatures Present Y H NA Phone:2-52-75b-620$ Site/Facillty104: Campliaw Monitoring? Email: M.6j oel rak@ t*r w;rrn,.uyln Yes Ho f ] I ] CalLectar signature Present Y H NA Bottler Lntact Y H HA Correct Bottles Y }1 FLh Collectedilly{printj: PurthaseOrdeFP: DW PWS10TO: ��EE�� P,�Girk` 3.- &k%e,6j Quote lv OW location Corte; 4 5uffieient Volume Y N HA samples Received: on Ice Y N HA Voa - Hl adspace Acceptable Y N HA Collected 4 (signature): turnaround Date Requir _ Immediately Packed on 6ce: r {-' { Yes [ ]No 1.15aA Regulated Soils Y H VA samplas in Bolding Time Y H VA Residual Chlorine Present Y H NA Sample Disposal: Rush: Fierd Filtered {lf applicable]: ( ] Oispose as appropriate I I Return [ j Same Day { ] Next Day [ I Yes [ I No CL Strips: I ] Archne: [ 12 Day f ] 3 0ay f ] 4 Day ( ] S Day Analysis: Sample PE Acceptable Y H NA ( ]Bold: IErpedite Charges Apply} � 7f � � PH oz Sulfide pPresent Y rf IrA read Acetate Strips: Matrix Codes IJnsert in Matrix bM belowl: Drinking Water (OW}, Ground Water{GW], Wastewater (WW), Product (P), Sodj%lid (SLI, ofl (01-), Wipe {WPI, Air (ARk, Tissue (TS], Bioassay (a), Vapor (Vl, Other(OTl d i Ap uge ONLY; Gals sample A ! C.Nments : Customer Sample 10 Matrix * Camp / Co©ected (or Composite End Res Nof Grab Composite Start) cl Ctns -1 Date Time 6 to Ti W -- k V w &11 6/2 ri(v" 10.1( A II l .� 1,1q- IU 1i]I&A l t,r - l l ti2 lL 1 Mw- Ins 4- 1, / tr-13 TOO?�3 M1J- It{ C5 $28fZ2 iZrJLJF> M 2:17 '6 J,30 V ;o' 17,E t;' Customer Remarks Special Conditions J Possible Hazards.' Type of €e Used: Wet Blue Dry None SHORT HOLDS PRESENT 102 hours]: Y N N/A Lab Sample Temperalure J a: 1 Temp Blank Received: Y N NA Packing Material Used: Lab Tracking Il; f6k6 WX1 2777628 Therm lDR: (� Q r'� i Cooler 1 Temp Upon Receipt. oc rFt,7dl,,- r..-lple�s) screened J<50D cpm): Y N NA sample(sl screened {c540gPm]; Y N NA received via: - Cooker 1 Thernt Carr- Factor: �aC rEDEX UPS Client Courier Paee Courier Cooler 1 Corrected Temp: oC Comments: Relinquished by/Company: Isigaature] Oate{fime: Rece]Ved by/Company: (Signature) Date/Time: MTJL LAB USE ONEI+ Table At: ��✓1 ]� )V.406-�rs].s r G ' fJ�r , l ��l y 3. C F[1� .( Ammurm: Template: elinuished by/Company: (Signature) Date/rime: d[Received �8 b /Can ; Sc] DateITitne: Trip Blank Received: Y N NA lRefeived Prelogin: PM: HCL Ve0H TVOther Relinquished Company: (Signature) Datefrime: bylCompany: (Signature) Date/Time: Non Confcrmance{sl: Page: PB: YES / NO of: Pace Gulf Coast Report#: 222063033 Page 20 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D �faceAnalyfical'SAMPLE RECEIVING CHECKLIST 1111111IIIIIIIIII SAMPLE DELIVERY GROUP 222063033 CHECKLIST YES NO Client PM RvVe Transport Method Samples received with proper thermal preservation? *❑ ❑ E1 - Environrrent 1, Inc. UPS Radioactivity is <1600 cpm? If no, record cpm value in notes section. COC relinquished and complete (including samplelDs, collect times, and sampler)? *❑ *❑ ❑ ❑ Profile Number Received By 290471 Fbberts, George S. All containers received in good condition and within hold time? All sample labels and containers received match the chain of custody? .�I❑ *❑ ❑ ❑ Line Item(s) Receive Date(s) 1 - IVE£LLVFA 06/29/22 2- Hydrogen 06/30/22 Preservative added to any containers? ❑ *❑ If received, was headspace for VOC water containers < 6mm? *❑ ❑ Samples collected in containers provided by Pace Gulf Coast? 0 ❑ COOLERS DISCREPANCIES LAB PRESERVATIONS Airbill Thermometer ID E42 Temp °C None None 3.6 NOTES Revision 1.6 Page 1 of 1 Pace Gulf Coast Report#: 222063033 Page 21 of 21 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D Appendix C Time vs. Concentration Graphs June 2022 Groundwater Monitoring Report CRD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D This page intentionally left blank. DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D BE MW-12S Organochlorides 9 8 7 6 nq c — 6 c O c 4 v c O u 3 2 1 0 Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 t Tetrachloroethene (CAS 127-18-4) --*—Trichloroethene (CAS 79-01-6) --0-1,2-Dichloroethane t cis-1,2-Dichloroethene --*—Vinyl chloride DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D BE MW-11 Organochlorides 0.8 0.7 0.6 0.5 3 C_ C O ;+ 0.4 o N C U 0.3 0.2 0.1 0 Jul DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D EJE MW-10 Organochlorides 2.5 c U c 1 O U 0.5 0 Jul DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 1.6 1.4 1.2 1 0 0.8 u 0.6 0.4 0.2 0 Jul-09 BE MW-8 Organochlorides Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 t Tetrachloroethene (CAS 127-18-4) tTrichloroethene(CAS 79-01-6) t 1,2-Dichloroethane tcis-1,2-Dichloroethene Vinyl chloride DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D 3 2.5 2 m c 0 c w c 0 1 0.5 0 Jul-09 BE MW-3S Organochlorides Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar 23 --*--Tetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) 1,2-Dichloroethane f cis-1,2-Dichloroethene Vinyl chloride DocuSign Envelope ID: 3C8509C9-30CA-4C23-B61B-5E8AB648F13D BE MW-3A Organochlorides 1.2 0.8 0 0.6 c v c 0 u 0.4 0.2 0 • • • • • • • • r • • till • •• Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Ott-21 Mar-23 +Tetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) t1,2-Dichloroethane +cis-1,2-Dichloroethene —0--Vinyl chloride