10061_OPR_Final Grade Soil Assessment Report_OPR

Via Email
November 30, 2022 NCDEQ – Division of Waste Management Brownfields Program
1646 Mail Service Center Raleigh, North Carolina 27699-1646 Attn: Ms. Carolyn Minnich
Re: Final Grade Soil Assessment Report Old Pineville Road Charlotte, North Carolina Brownfields Project No. 10061-06-060
H&H Project No. BOU-012 Dear Carolyn:
Enclosed please find a copy of the Final Grade Soil Assessment Report prepared for the Old Pineville Road Brownfields property located in Charlotte, Mecklenburg County. Should you have any questions or need additional information, please do not hesitate to contact us at [phone].

Sincerely,
Hart & Hickman, PC
Alexis McKenzie, PE Joe Gentilcore Senior Project Engineer Assistant Project Scientist

Enclosure cc: Mr. Michael Bender, Boulevard Real Estate Advisors (via email)

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Final Grade Soil Assessment Report Old Pineville Road Old Pineville Townhomes Charlotte, North Carolina Brownfields Project No. 10061-06-060 H&H Job No. BOU-012 Table of Contents
1.0 Introduction .............................................................................................................................1
2.0 Final Grade Soil Assessment Activities .................................................................................2
2.1 Final Grade Soil Sampling Methodology ..............................................................................2
2.2 Final Grade Soil Sampling Results ........................................................................................4
2.3 Risk Calculations ...................................................................................................................5
3.0 Summary and Conclusions ....................................................................................................6
List of Tables

Table 1 Summary of Final Grade Soil Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map
Appendices Appendix A Laboratory Analytical Reports
Appendix B Risk Calculator Summary Pages
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Final Grade Soil Assessment Report Old Pineville Road Old Pineville Townhomes Charlotte, North Carolina Brownfields Project No. 10061-06-060 H&H Job No. BOU-012 1.0 Introduction

Hart & Hickman, P.C. (H&H) has prepared this Final Grade Soil Assessment Report for the Old
Pineville Road Brownfields property (Brownfields Project No. 10061-06-060) located at 4928
Old Pineville Road and 649 Scholtz Road in Charlotte, Mecklenburg County, North Carolina
(Site or subject Site). The redevelopment is known as Old Pineville Townhomes and is being
developed with for-sale residential townhomes by Ryan Homes, an NVR company. The Site
was developed with fifteen (15) townhome complexes including one 3-unit townhome complex,
one 4-unit townhome complex, five 7-unit townhome complexes, and eight 8-unit townhome
complexes for a total of 106 individual residential townhome units. A Site location map is
included as Figure 1.

In accordance with the North Carolina Department of Environmental Quality (DEQ) approved
Environmental Management Plan (EMP) dated January 3, 2020 H&H prepared a Final Grade
Soil Sampling Work Plan (Work Plan) dated October 10, 2022. The Work Plan received DEQ
approval in a letter dated October 11, 2022. Final grade soil sampling was conducted at the Site
in areas that are not covered with buildings, sidewalks, concrete or asphaltic paved (hardscape)
surfaces, or a minimum of two feet of demonstrably clean fill soil. H&H completed final grade
soil sampling activities to evaluate the potential for impacts in shallow soil within unpaved areas.
A discussion of the final grade soil assessment activities is provided in the following sections.
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2.0 Final Grade Soil Assessment Activities

The Site is predominately covered with impervious surfaces including the townhome building
footprints, paved roadways, and walkways. Limited landscaped and/or grassy lawn areas are
located along the central portion of the Site. The townhomes located on the northern and
southern Site boundaries do not have lawns and have minimal landscaping near the residential
entries. A Site Map is included as Figure 2 and general surface conditions and boring locations
are shown on Figure 3.

On October 27, 2022 and November 2, 2022, H&H completed final grade soil assessment
activities. Final grade soil sampling activities were conducted at the Site to evaluate potential
direct exposure risks to future Site occupants and workers from shallow soil in landscaped areas.
The soil sampling activities were conducted in general accordance with the DEQ Inactive
Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup (Guidelines) dated
January 2020, the most recent versions of U.S. Environmental Protection Agency (EPA) Region
IV Laboratory Services and Applied Science Division (LSASD) Field Branches Quality System
and Technical Procedures guidance, and the DEQ-approved Work Plan.

2.1 Final Grade Soil Sampling Methodology

Based on review of the Site Plan and observations at the Site, landscaped areas in the central and
eastern portions of the Site were divided into fifteen (15) final grade evaluation areas (FG-1
through FG-15). Three to five shallow soil borings were advanced within each final grade
evaluation area for collection of aliquot soil samples from each shallow soil boring. Soil sample
aliquots collected from each evaluation area were homogenized to form one composite soil
sample to represent shallow soil conditions within that evaluation area. The final grade
evaluation areas and approximate locations of the aliquot soil borings are shown in Figure 3.

Aliquot soil borings were advanced from the surface to approximately two feet below the ground
surface (ft bgs) using a decontaminated stainless-steel hand auger. During boring advancement,
continuous soil samples were collected from the center of the hand auger bucket. Soil samples
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were described for lithologic purposes and observed for obvious evidence of staining and
unusual odors. Each soil aliquot was screened for the presence of volatile organic vapors using a
calibrated photoionization detector (PID). Site soils were generally moist, medium stiff, reddish-
brown clayey silt and field personnel did not observe the presence of staining, odor, or other
obvious evidence of impacts.

Remaining portions of the aliquot soil samples were homogenized to form a composite soil
sample representative of each evaluation area for a total of fifteen (15) composite final grade soil
samples. Soil samples selected for laboratory analysis were collected directly into laboratory
supplied glassware, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Waypoint
Analytical, a North Carolina certified laboratory, under standard chain of custody protocols for
analysis. Composite soil samples were submitted for laboratory analysis of semi-volatile organic
compounds (SVOCs) by EPA Method 8270 and Resource Conservation and Recovery Act
(RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199.

In addition, one grab sample was collected from an undisturbed portion of one aliquot soil
sample collected in each evaluation area for a total of fifteen (15) grab soil samples that were
submitted for analysis of volatile organic compounds (VOCs) by EPA Method 8260. Field
screening results did not identify obvious presence of impacts in any aliquot soil sample,
therefore the grab sample collected for VOC analysis from each final grade evaluation area was
collected from the 1 to 2 ft bgs sample interval from a randomly selected aliquot soil boring.

For quality assurance and quality control purposes (QA/QC), H&H collected one duplicate
composite sample (FG-DUP) from evaluation area FG-6 for SVOCs and RCRA metals plus
hexavalent chromium. H&H also collected a duplicate representative grab sample from the
aliquot where VOCs were collected in the same section.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil boring locations were estimated
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using a hand-held global positioning system (GPS) unit.

2.2 Final Grade Soil Sampling Results

A tabular summary of final grade soil sample laboratory analytical results is presented in Table
1. The laboratory analytical results were compared to the DEQ Preliminary Soil Remediation
Goals (PSRGs) for Residential use dated July 2022. In addition to the PSRGs, metals results are
compared to published concentrations for naturally occurring metals in soil. A copy of the
laboratory analytical report and chain of custody record is provided in Appendix A.

VOCs
Laboratory analytical results indicate several VOCs were detected above the laboratory method
detection limits but below the DEQ Residential PSRGs. Acetone, acrolein, bromomethane,
carbon disulfide, chloromethane, and ethanol were detected at trace concentrations in select soil
samples. No other VOCs were detected above laboratory method detection limits in final grade
soil samples collected at the Site.

SVOCs
Final grade soil sample analytical results indicate that estimated (J-flag) concentrations of
butylbenzylphthalate were detected in final grade evaluation area soil samples FG-DUP and FG-
12 (0.395 J milligrams per kilogram (mg/kg) and 0.213 J mg/kg, respectively), well below the
Residential PSRG of 290 mg/kg. Please note, butylbenzylphthalate was not detected in the
parent sample FG-6 from which evaluation area FG-DUP was collected. Fluoranthene was
detected at an estimated (J-flag) concentration in soil sample FG-12 (0.193 J mg/kg), which is
well below the Residential PSRG of 480 mg/kg. No other SVOCs were detected above
laboratory method detection limits in any final grade soil samples collected at the Site.

Metals
As anticipated, each of the analyzed metals, with the exception of hexavalent chromium, was
detected at concentrations above laboratory method detection limits in all of the final grade soil
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samples collected at the Site. Arsenic was detected in each sample at concentrations ranging
from 0.742 mg/kg in FG-3 to 2.54 mg/kg in FG-14. Although the detected arsenic
concentrations in each soil sample exceed the Residential PSRG of 0.68 mg/kg, the detected
concentrations are consistent with regional background metals concentrations. Therefore, the
concentrations of arsenic appear to be naturally occurring. No other metals were detected at
concentrations exceeding the Residential PSRGs or regional background concentrations.

2.3 Risk Calculations

The DEQ PSRGs used for comparison to the laboratory analytical results are very conservative
and based upon a carcinogenic target risk (TCR) of 1 x 10-6 for potential carcinogenic effects and
a non-carcinogenic target hazard quotient (THQ) of 0.2 for potential noncarcinogenic effects.
The DEQ and Environmental Protection Agency (EPA) acceptable risks for potential
carcinogenic risks is a cumulative lifetime incremental carcinogenic risk (LICR) of 1 x 10-4 and a
cumulative Hazard Index (HI) of 1.0 for noncarcinogenic risks. H&H utilized the DEQ Risk
Calculator dated July 2022 to further evaluate cumulative risks to residential occupants based on
the final grade soil sample analytical results.

The highest concentration of each compound detected in any final grade soil sample was used to
model a hypothetical worst-case exposure risk under a residential use scenario. Please note that
although metals concentrations, specifically arsenic, are consistent with background conditions,
these concentrations were also included in the risk calculator.

The risk calculator results indicate a residential use worst-case cumulative LICR of 3.8 x 10-6
and a cumulative HI of 0.13. The results of the risk calculator indicate the calculated cumulative
carcinogenic and noncarcinogenic risks are well below the acceptable risk levels of 1 x 10-4 and
1.0, respectively. A copy of the completed DEQ Risk Calculator is provided as Appendix B.

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3.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the Old Pineville Road Brownfields
property located at 4928 Old Pineville Road and 649 Scholtz Road in Charlotte, North Carolina.
The final grade soil sampling activities were conducted in accordance with the DEQ Brownfields
approved Work Plan dated October 10, 2022. Final grade soil sampling activities included the
collection of soil samples to evaluate the potential for impacts in areas at the Site that are not
covered by demonstrably clean fill soil, building foundations, sidewalks, or asphaltic or concrete
parking areas and driveways following redevelopment.

Laboratory analytical results indicate that several VOCs were detected at concentrations above
the laboratory method detection limits but below the DEQ Residential PSRGs in the soil samples
collected at the Site. In addition, butylbenzylphthalate and fluoranthene were detected in select
samples at concentrations above the laboratory method detection limit, but well below the
Residential PSRGs.

Several metals were detected above laboratory method detection limits in each final grade soil
sample collected at the Site. Arsenic was detected at concentrations above the DEQ Residential
PSRG in each soil sample, however the detected concentrations are within the range of naturally
occurring background concentrations. No other metals were detected at concentrations above the
Residential PSRGs or regional background concentrations.

To evaluate potential cumulative risks for residential use at the Site, H&H calculated worst-case
cumulative risks using the highest concentrations of compounds detected in the final grade
samples. The results of the risk calculator indicate that the calculated cumulative LICR for the
final grade soil samples is 3.8 x 10-6 and the cumulative HI is 0.13. Thus, the calculated risks do
not exceed acceptable risk levels for a residential use exposure scenario.
Table 1Summary of Final Grade Soil Analytical DataOld Pineville RoadCharlotte, North CarolinaBrownfields Project No. 10061-06-060H&H Job No. BOU-012Sample IDDateSample TypeComposite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite GrabDepth (ft bgs)0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 Range MeanUnitsVOCs (8260D)AcetoneNA0.038NA0.021 JNA0.038NA0.019 JNA0.029NA NA0.027 0.044NA0.031NA0.028 14,000-- --AcroleinNA0.002 JNA <0.001 NA <0.001 NA <0.001 NA <0.001 NA NA <0.001 <0.001 NA <0.001 NA <0.0010.031-- --BromomethaneNA<0.002 NA <0.002 NA <0.002 NA <0.002 NA <0.002 NA NA <0.002 <0.002 NA <0.002 NA <0.0021.4-- --Carbon disulfideNA<0.0008 NA <0.0008 NA0.002 JNA <0.0008 NA <0.0009 NA NA <0.0008 <0.0008 NA0.004 JNA <0.0008160-- --ChloromethaneNA<0.0008 NA <0.0008 NA <0.0008 NA <0.0008 NA <0.0009 NA NA <0.0008 <0.0008 NA <0.0008 NA <0.000823-- --EthanolNA<0.018 NA <0.016 NA <0.018 NA <0.018 NA <0.019 NA NA <0.018 <0.018 NA <0.018 NA <0.017 NE -- --SVOCs (8270E)Butylbenzylphthalate<0.145NA<0.136NA<0.145 NA <0.148 NA <0.153 NA <0.1470.395 JNA NA <0.148 NA <0.143 NA290-- --Fluoranthene<0.158NA<0.148NA<0.158 NA <0.161 NA <0.167 NA <0.160 <0.161 NA NA <0.161 NA <0.155 NA480-- --Metals (6020B/7471B/7199)Arsenic2.42NA1.43NA0.742NA1.68NA1.82NA1.67 1.48NA NA2.07NA1.35NA0.68 1.0 - 18 4.8Barium74.0NA107NA98.2NA63.2NA69.6NA53.9 46.1NA NA34.5NA49.0NA3,100 50 - 1,000 356Cadmium0.177 JNA0.0871 JNA0.0337 JNA0.0528 JNA0.0957 JNA0.0578 J 0.0616 JNA NA0.0627 JNA0.0502 JNA1.4 1.0 - 10 4.3Chromium (total)46.9NA40.8NA30.7NA35.9NA42.9NA39.9 33.5NA NA36.6NA42.5NA NE7.0 - 300 65Hexavalent Chromium<0.182NA<0.170NA<0.182 NA <0.185 NA <0.197 NA <0.184 <0.185 NA NA <0.187 NA <0.178 NA0.31 NS NSTrivalent Chromium46.9NA40.8NA30.7NA35.9NA42.9NA39.9 33.5NA NA36.6NA42.5NA23,000 NS NSLead20.0NA10.3NA4.34NA11.2NA14.9NA10.2 10.4NA NA11.6NA8.62NA400 ND - 50 16Mercury0.0612NA0.0424NA0.0624NA0.0725NA0.0738NA0.102 0.0937NA NA0.105NA0.102NA4.7 0.03 - 0.52 0.121Selenium0.731NA0.365NA0.202 JNA0.582NA0.663NA0.755 0.638NA NA0.727NA0.621NA78 <0.1 - 0.8 0.42Silver0.0264 JNA0.0357 JNA0.0248 JNA0.0188 JNA0.0402 JNA0.0268 J 0.0161 JNA NA0.0190 JNA0.0198 JNA78 ND - 5.0 NSNotes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) (July 2022). 2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations are for Southeastern & Conteminous US soils. With the exception of metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds;ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgRegional Background Metals in Soils (2)0-2 1-2FG-3FG-211/2/202211/2/202211/2/202210/27/202210/27/2022Residential PSRGs (1)FG-111/2/2022GrabCompositeFG-811/2/202211/2/2022FG-7FG-6 / FG-DUPFG-5FG-4https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Boulevard Realty Estate Advisors (BOU)/BOU‐012  4928 Old Pineville Rd/Final Grade/Tables/Data Table_Old Pineville Road11/30/2022Table 1 (Page 1 of 2) Hart & Hickman, PC
Table 1Summary of Final Grade Soil Analytical DataOld Pineville RoadCharlotte, North CarolinaBrownfields Project No. 10061-06-060H&H Job No. BOU-012Sample IDDateSample TypeCompostie Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite GrabDepth (ft bgs)0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 Range MeanUnitsVOCs (8260D)AcetoneNA0.025 JNA0.042NA0.022 JNA0.045NA0.029NA0.025NA0.021 J 14,000-- --AcroleinNA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.0010.031-- --BromomethaneNA <0.002 NA0.002 JNA <0.002 NA <0.002 NA <0.002 NA <0.002 NA <0.0021.4-- --Carbon disulfideNA <0.0009 NA0.001 JNA <0.0008 NA <0.0009 NA <0.0009 NA <0.0008 NA <0.0008160-- --ChloromethaneNA <0.0009 NA0.001 JNA <0.0008 NA <0.0008 NA <0.0009 NA <0.0008 NA <0.000823-- --EthanolNA <0.019 NA <0.018 NA0.237 JNA <0.018 NA <0.018 NA <0.017 NA <0.017 NE -- --SVOCs (8270E)Butylbenzylphthalate<0.157 NA <0.149 NA <0.146 NA0.213 JNA <0.153 NA <0.142 NA <0.140 NA290-- --Fluoranthene<0.171 NA <0.163 NA <0.159 NA0.193 JNA <0.166 NA <0.154 NA <0.152 NA480-- --Metals (6020B/7471B/7199)Arsenic1.74NA0.844NA1.73NA1.80NA2.11NA2.54NA0.953NA0.68 1.0 - 18 4.8Barium60.6NA90.3NA41.0NA49.9NA40.5NA73.3NA73.0NA3,100 50 - 1,000 356Cadmium0.0897 JNA0.0953 JNA0.105 JNA0.0881 JNA0.0613 JNA0.147 JNA0.0484 JNA1.4 1.0 - 10 4.3Chromium (total)43.8NA48.8NA33.5NA36.0NA41.5NA40.8NA38.6NA NE7.0 - 300 65Hexavalent Chromium<0.196 NA <0.188 NA <0.182 NA <0.189 NA <0.191 NA <0.177 NA <0.180 NA0.31 NS NSTrivalent Chromium43.8NA48.8NA33.5NA36.0NA41.5NA40.8NA38.6NA23,000 NS NSLead13.4NA4.88NA9.21NA12.4NA10.8NA13.5NA5.24NA400 ND - 50 16Mercury0.153NA0.0960NA0.0830NA0.0837NA0.101NA0.179NA0.0717NA4.7 0.03 - 0.52 0.121Selenium0.721NA0.473NA0.715NA0.668NA0.768NA0.778NA0.414NA78 <0.1 - 0.8 0.42Silver0.0235 JNA0.0224 JNA0.0158 JNA0.0431 JNA0.0298 JNA0.0638 JNA0.0160 JNA78 ND - 5.0 NSNotes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) (July 2022). 2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations are for Southeastern & Conteminous US soils. With the exception of metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds;ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. 11/2/2022FG-1511/2/2022FG-1411/2/2022FG-1311/2/2022FG-1211/2/2022FG-1111/2/2022FG-10Regional Background Metals in Soils (2)mg/kgResidential PSRGs (1)11/2/2022FG-9https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Boulevard Realty Estate Advisors (BOU)/BOU‐012  4928 Old Pineville Rd/Final Grade/Tables/Data Table_Old Pineville Road11/30/2022Table 1 (Page 2 of 2) Hart & Hickman, PC
SITE LOCATION MAP
OLD PINEVILLE ROAD
4928 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
6-18-2021 0
1NVR-010
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
7.5 MINUTE SERIES (TOPOGRAPHIC)
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
CHARLOTTE WEST, NORTH CAROLINA 1996
SITE
REVISION NO. 0
JOB NO. NVR-010
DATE: 6-21-21
FIGURE NO. 2
OLD PINEVILLE ROAD
4928 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
PROPOSED BUILDING FOOTPRINT
UNIT NUMBERF
F
F
F
F
F
F
F
F
F
F
F
F
F
H G
E D C B A
H G
E D C B A
H G
E D C B A
H G
E D C B A H G
E D C B A
H G
E D C B A
H G
E D C B A
H G
E D C B A
A
B
C
A
B
C
D
A
B
C
D
E
G
A B C D E
G
A B C D E
G
A B C D E
G
A B C D E
G
ANSTON DRI
V
E
TODDWICK P
L
A
C
EBIRCHAM DRIVETHORNDALE LANESCHLOTZ RO
A
D OLD PINEVILLE ROADNOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2021).
2.DEVELOPMENT PLAN BASED ON SITE PLAN PROVIDED BY
BOHLER ENGINEERING (STAMPED 12/24/19).
BUILDING 1001
BUILDING 1002
BUILDING 1003
BUILDING 1007
BUILDING 1011
BUILDING 1006
BUILDING 1005
BUILDING 1004
BUILDING 1008
BUILDING 1009
BUILDING 1010
BUILDING 1015
BUILDING 1014
BUILDING 1013
BUILDING 1012
M:\AAA_DRAFTING\NVR\NVR-010-Old Pineville Road\Site Plan.dwg, FIG 2, 6/21/2021 11:19:59 AM, SVincent
REVISION NO. 0
JOB NO. BOU-012
DATE: 11-30-22
FIGURE NO. 3
OLD PINEVILLE ROAD
4928 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLING MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
BUILDING FOOTPRINT
AIR CONDITIONING COMPRESSOR
LOCATION
GRASS/YARD AREA
LANDSCAPED AREA
ALIQUOT SOIL SAMPLE LOCATION
ANSTON DRI
V
E
TODDWICK P
L
A
C
EBIRCHAM DRIVETHORNDALE LANESCHOLTZ RO
A
D OLD PINEVILLE ROADNOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2022).
2.DEVELOPMENT PLAN BASED ON SITE PLAN PROVIDED BY
BOHLER ENGINEERING (STAMPED 12/24/19).
BUILDING 1001
BUILDING 1002
BUILDING 1003
BUILDING 1007
BUILDING 1011
BUILDING 1006
BUILDING 1005
BUILDING 1004
BUILDING 1008
BUILDING 1009
BUILDING 1010
BUILDING 1015
BUILDING 1014
BUILDING 1013
BUILDING 1012
FG-2
FG-5
FG-7 FG-9 FG-11
FG-13
FG-15
FG-3
FG-6
FG-8
FG-10
FG-14
FG-12
FG-4
FG-1
S:\AAA-Master Projects\NVR, Inc\NVR-010 OPR\Final Grade\Work Plan\Figures\Site Plan.dwg, FIG 3, 11/30/2022 1:18:09 PM, amckenzie

Appendix A
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/10/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-301-0017 Client Project Description: BOU-012
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/28/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 43
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-301-0017
Page 2 of 43
Report Number:
Sample Summary Table
Client Project Description:
22-301-0017
BOU-012
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
10/27/2022 10:25Solids 91754 FG-2 10/28/2022 15:35
10/27/2022 10:25Solids 91754 FG-2 10/28/2022 15:35 SW-7199 WP MTN -
10/27/2022 10:25Solids 91754 FG-2 10/28/2022 15:35 6020B WP MTN -
10/27/2022 10:45Solids 91755 FG-3 10/28/2022 15:35
10/27/2022 10:45Solids 91755 FG-3 10/28/2022 15:35 SW-7199 WP MTN -
10/27/2022 10:45Solids 91755 FG-3 10/28/2022 15:35 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 43
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0017
Report Limit
Project:BOU-012
V 91754FG-2
1.43 11/04/2022 21:176020BArsenicmg/Kg - dry 0.104
107 11/04/2022 21:176020BBariummg/Kg - dry 0.051
J0.0871 11/04/2022 21:176020BCadmiummg/Kg - dry 0.0313
40.8 11/04/2022 21:176020BChromiummg/Kg - dry 0.140
10.3 11/04/2022 21:176020BLeadmg/Kg - dry 0.0375
0.365 11/04/2022 21:176020BSeleniummg/Kg - dry 0.124
J0.0357 11/04/2022 21:176020BSilvermg/Kg - dry 0.0081
0.0424 10/31/2022 16:137471BMercury (Total)mg/Kg - dry 0.0145
J0.021 10/31/2022 13:518260DAcetonemg/Kg - dry 0.002
17.4 11/04/2022 11:19SW-DRYWT Moisture %
V 91755FG-3
0.742 11/04/2022 21:226020BArsenicmg/Kg - dry 0.110
98.2 11/04/2022 21:226020BBariummg/Kg - dry 0.055
J0.0337 11/04/2022 21:226020BCadmiummg/Kg - dry 0.0334
30.7 11/04/2022 21:226020BChromiummg/Kg - dry 0.149
4.34 11/04/2022 21:226020BLeadmg/Kg - dry 0.0400
J0.202 11/04/2022 21:226020BSeleniummg/Kg - dry 0.133
J0.0248 11/04/2022 21:226020BSilvermg/Kg - dry 0.0087
0.0624 10/31/2022 16:157471BMercury (Total)mg/Kg - dry 0.0155
0.038 10/31/2022 14:188260DAcetonemg/Kg - dry 0.003
J0.002 10/31/2022 14:188260DCarbon Disulfide mg/Kg - dry 0.0008
22.6 11/04/2022 11:19SW-DRYWT Moisture %
Page 4 of 43

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: BOU-012 Lab Report Number: 22-301-0017
Date: 11/9/2022
Metals Analyses Method 6020B Sample 91802 (COMP-5 (2-4)) Analyte: Barium
QC Batch No: L647316/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Chromium
QC Batch No: L647584/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Lead
QC Batch No: L647316/L646697 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Selenium QC Batch No: L647316/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 QC Batch No: L647181 Insoluble Hexavalent Chromium spike data.
Page 5 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.4 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.170 mg/Kg - dry 0.170 0.243Chromium, Hexavalent 1 11/04/22 14:19 SW-7199SAR
1.43 mg/Kg - dry 0.104 0.303Arsenic 5 11/04/22 21:17 6020BCPW
107 mg/Kg - dry 0.051 0.302Barium 5 11/04/22 21:17 6020BCPW
0.0871 J mg/Kg - dry 0.0313 0.303Cadmium 5 11/04/22 21:17 6020BCPW
40.8 mg/Kg - dry 0.140 0.302
Chromium 5 11/04/22 21:17 6020BBKN
10.3 mg/Kg - dry 0.0375 0.303Lead 5 11/04/22 21:17 6020BCPW
0.0424 mg/Kg - dry 0.0145 0.0363Mercury (Total)1 10/31/22 16:13 7471BEDV
0.365 mg/Kg - dry 0.124 0.302Selenium 5 11/04/22 21:17 6020BCPW
0.0357 J mg/Kg - dry 0.0081 0.303Silver 5 11/04/22 21:17 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.021 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/31/22 13:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 13:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 13:51 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 13:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 13:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 13:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 13:51 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 13:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 13:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 13:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 13:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 13:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 13:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 13:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 13:51 V25732TBL
<0.016 mg/Kg - dry 0.016 0.302Ethanol 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 13:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 13:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 13:51 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 13:51 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 13:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 13:51 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 13:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 13:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 13:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 13:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 13:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 13:51 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 13:511 TBL V25732
Surrogate: Dibromofluoromethane 108 Limits: 84-123%10/31/22 13:511 TBL V25732
Surrogate: Toluene-d8 92.6 Limits: 76-129%10/31/22 13:511 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.140 mg/Kg - dry 0.140 0.799Acenaphthene 1 11/04/22 22:37 V25983JMV
<0.127 mg/Kg - dry 0.127 0.799Acenaphthylene 1 11/04/22 22:37 V25983JMV
<0.184 mg/Kg - dry 0.184 0.799Aniline 1 11/04/22 22:37 V25983JMV
<0.173 mg/Kg - dry 0.173 0.799Anthracene 1 11/04/22 22:37 V25983JMV
<0.168 mg/Kg - dry 0.168 0.799
Benzo(a)anthracene 1 11/04/22 22:37 V25983JMV
<0.177 mg/Kg - dry 0.177 0.799Benzo(a)pyrene 1 11/04/22 22:37 V25983JMV
<0.176 mg/Kg - dry 0.176 0.799Benzo(b)fluoranthene 1 11/04/22 22:37 V25983JMV
<0.164 mg/Kg - dry 0.164 0.799Benzo(g,h,i)perylene 1 11/04/22 22:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.165 mg/Kg - dry 0.165 0.799Benzo(k)fluoranthene 1 11/04/22 22:37 V25983JMV
<0.702 mg/Kg - dry 0.702 2.42Benzoic Acid 1 11/04/22 22:37 V25983JMV
<0.127 mg/Kg - dry 0.127 0.799Benzyl alcohol 1 11/04/22 22:37 V25983JMV
<0.142 mg/Kg - dry 0.142 0.799Bis(2-Chloroethoxy)methane 1 11/04/22 22:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.799Bis(2-Chloroethyl)ether 1 11/04/22 22:37 V25983JMV
<0.164 mg/Kg - dry 0.164 0.399Bis(2-Chloroisopropyl)ether 1 11/04/22 22:37 V25983JMV
<0.145 mg/Kg - dry 0.145 0.799Bis(2-ethylhexyl)phthalate 1 11/04/22 22:37 V25983JMV
<0.131 mg/Kg - dry 0.131 0.7994-Bromophenyl phenyl ether 1 11/04/22 22:37 V25983JMV
<0.136 mg/Kg - dry 0.136 0.399
Butyl benzyl phthalate 1 11/04/22 22:37 V25983JMV
<0.111 mg/Kg - dry 0.111 0.7994-Chloro-3-methylphenol 1 11/04/22 22:37 V25983JMV
<0.135 mg/Kg - dry 0.135 0.3994-Chloroaniline 1 11/04/22 22:37 V25983JMV
<0.140 mg/Kg - dry 0.140 0.7992-Chloronaphthalene 1 11/04/22 22:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.7992-Chlorophenol 1 11/04/22 22:37 V25983JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 11/04/22 22:37 V25983JMV
<0.171 mg/Kg - dry 0.171 0.799Chrysene 1 11/04/22 22:37 V25983JMV
<0.278 mg/Kg - dry 0.278 0.799
Dibenz(a,h)anthracene 1 11/04/22 22:37 V25983JMV
<0.144 mg/Kg - dry 0.144 0.799Dibenzofuran 1 11/04/22 22:37 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7991,2-Dichlorobenzene 1 11/04/22 22:37 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7991,3-Dichlorobenzene 1 11/04/22 22:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.3991,4-Dichlorobenzene 1 11/04/22 22:37 V25983JMV
<0.177 mg/Kg - dry 0.177 0.7993,3'-Dichlorobenzidine 1 11/04/22 22:37 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7992,4-Dichlorophenol 1 11/04/22 22:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.217 mg/Kg - dry 0.217 0.799Diethyl phthalate 1 11/04/22 22:37 V25983JMV
<0.210 mg/Kg - dry 0.210 0.799Dimethyl phthalate 1 11/04/22 22:37 V25983JMV
<0.130 mg/Kg - dry 0.130 0.3992,4-Dimethylphenol 1 11/04/22 22:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.799Di-n-butyl phthalate 1 11/04/22 22:37 V25983JMV
<0.290 mg/Kg - dry 0.290 1.824,6-Dinitro-2-methylphenol 1 11/04/22 22:37 V25983JMV
<0.629 mg/Kg - dry 0.629 1.822,4-Dinitrophenol 1 11/04/22 22:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7992,4-Dinitrotoluene 1 11/04/22 22:37 V25983JMV
<0.130 mg/Kg - dry 0.130 0.7992,6-Dinitrotoluene 1 11/04/22 22:37 V25983JMV
<0.173 mg/Kg - dry 0.173 0.399
Di-n-Octyl Phthalate 1 11/04/22 22:37 V25983JMV
<0.148 mg/Kg - dry 0.148 0.799Fluoranthene 1 11/04/22 22:37 V25983JMV
<0.154 mg/Kg - dry 0.154 0.799Fluorene 1 11/04/22 22:37 V25983JMV
<0.128 mg/Kg - dry 0.128 0.799Hexachlorobenzene 1 11/04/22 22:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.799Hexachlorobutadiene 1 11/04/22 22:37 V25983JMV
<0.190 mg/Kg - dry 0.190 0.799Hexachlorocyclopentadiene 1 11/04/22 22:37 V25983JMV
<0.095 mg/Kg - dry 0.095 0.799Hexachloroethane 1 11/04/22 22:37 V25983JMV
<0.216 mg/Kg - dry 0.216 0.799
Indeno(1,2,3-cd)pyrene 1 11/04/22 22:37 V25983JMV
<0.231 mg/Kg - dry 0.231 0.799Isophorone 1 11/04/22 22:37 V25983JMV
<0.128 mg/Kg - dry 0.128 0.7991-Methylnaphthalene 1 11/04/22 22:37 V25983JMV
<0.121 mg/Kg - dry 0.121 0.7992-Methylnaphthalene 1 11/04/22 22:37 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7992-Methylphenol 1 11/04/22 22:37 V25983JMV
<0.102 mg/Kg - dry 0.102 0.7993&4 Methylphenol 1 11/04/22 22:37 V25983JMV
<0.174 mg/Kg - dry 0.174 0.799Naphthalene 1 11/04/22 22:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91754 Matrix:
10/27/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.117 mg/Kg - dry 0.117 0.7992-Nitroaniline 1 11/04/22 22:37 V25983JMV
<0.145 mg/Kg - dry 0.145 0.7993-Nitroaniline 1 11/04/22 22:37 V25983JMV
<0.112 mg/Kg - dry 0.112 0.3994-Nitroaniline 1 11/04/22 22:37 V25983JMV
<0.140 mg/Kg - dry 0.140 0.399Nitrobenzene 1 11/04/22 22:37 V25983JMV
<0.107 mg/Kg - dry 0.107 0.7992-Nitrophenol 1 11/04/22 22:37 V25983JMV
<0.141 mg/Kg - dry 0.141 0.7994-Nitrophenol 1 11/04/22 22:37 V25983JMV
<0.318 mg/Kg - dry 0.318 0.799N-Nitrosodimethylamine 1 11/04/22 22:37 V25983JMV
<0.219 mg/Kg - dry 0.219 0.799N-Nitrosodiphenylamine 1 11/04/22 22:37 V25983JMV
<0.142 mg/Kg - dry 0.142 0.799
N-Nitroso-di-n-propylamine 1 11/04/22 22:37 V25983JMV
<0.420 mg/Kg - dry 0.420 1.21Pentachlorophenol 1 11/04/22 22:37 V25983JMV
<0.251 mg/Kg - dry 0.251 0.799Phenanthrene 1 11/04/22 22:37 V25983JMV
<0.135 mg/Kg - dry 0.135 0.799Phenol 1 11/04/22 22:37 V25983JMV
<0.162 mg/Kg - dry 0.162 0.799Pyrene 1 11/04/22 22:37 V25983JMV
<0.095 mg/Kg - dry 0.095 0.399Pyridine 1 11/04/22 22:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.7991,2,4-Trichlorobenzene 1 11/04/22 22:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.799
2,4,5-Trichlorophenol 1 11/04/22 22:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7992,4,6-Trichlorophenol 1 11/04/22 22:37 V25983JMV
8270ESurrogate: Phenol-d5 74.2 Limits: 34-121%11/04/22 22:371 JMV
Surrogate: 2-Fluorobiphenyl 85.5 Limits: 44-115%11/04/22 22:371 JMV V25983
Surrogate: 2-Fluorophenol 76.9 Limits: 35-115%11/04/22 22:371 JMV V25983
Surrogate: Nitrobenzene-d5 79.5 Limits: 37-122%11/04/22 22:371 JMV V25983
Surrogate: 4-Terphenyl-d14 94.6 Limits: 54-127%11/04/22 22:371 JMV V25983
Surrogate: 2,4,6-Tribromophenol 71.8 Limits: 39-132%11/04/22 22:371 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.182 mg/Kg - dry 0.182 0.258Chromium, Hexavalent 1 11/04/22 15:03 SW-7199SAR
0.742 mg/Kg - dry 0.110 0.323Arsenic 5 11/04/22 21:22 6020BCPW
98.2 mg/Kg - dry 0.055 0.322Barium 5 11/04/22 21:22 6020BCPW
0.0337 J mg/Kg - dry 0.0334 0.323Cadmium 5 11/04/22 21:22 6020BCPW
30.7 mg/Kg - dry 0.149 0.322
Chromium 5 11/04/22 21:22 6020BBKN
4.34 mg/Kg - dry 0.0400 0.323Lead 5 11/04/22 21:22 6020BCPW
0.0624 mg/Kg - dry 0.0155 0.0388Mercury (Total)1 10/31/22 16:15 7471BEDV
0.202 J mg/Kg - dry 0.133 0.322Selenium 5 11/04/22 21:22 6020BCPW
0.0248 J mg/Kg - dry 0.0087 0.323Silver 5 11/04/22 21:22 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.038 mg/Kg - dry 0.003 0.025Acetone 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 10/31/22 14:18 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 14:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 14:18 V25732TBL
0.002 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 14:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 10/31/22 14:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 10/31/22 14:18 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 14:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 14:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 14:18 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 14:18 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 14:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 14:18 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 10/31/22 14:18 V25732TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 10/31/22 14:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 14:18 V25732TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 14:18 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 14:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 14:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 14:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 14:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 14:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 14:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 14:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 14:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 14:18 V25732
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%10/31/22 14:181 TBL V25732
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/31/22 14:181 TBL V25732
Surrogate: Toluene-d8 93.2 Limits: 76-129%10/31/22 14:181 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.149 mg/Kg - dry 0.149 0.852Acenaphthene 1 11/04/22 23:00 V25983JMV
<0.135 mg/Kg - dry 0.135 0.852Acenaphthylene 1 11/04/22 23:00 V25983JMV
<0.196 mg/Kg - dry 0.196 0.852Aniline 1 11/04/22 23:00 V25983JMV
<0.184 mg/Kg - dry 0.184 0.852Anthracene 1 11/04/22 23:00 V25983JMV
<0.179 mg/Kg - dry 0.179 0.852
Benzo(a)anthracene 1 11/04/22 23:00 V25983JMV
<0.189 mg/Kg - dry 0.189 0.852Benzo(a)pyrene 1 11/04/22 23:00 V25983JMV
<0.188 mg/Kg - dry 0.188 0.852Benzo(b)fluoranthene 1 11/04/22 23:00 V25983JMV
<0.175 mg/Kg - dry 0.175 0.852Benzo(g,h,i)perylene 1 11/04/22 23:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.177 mg/Kg - dry 0.177 0.852Benzo(k)fluoranthene 1 11/04/22 23:00 V25983JMV
<0.749 mg/Kg - dry 0.749 2.58Benzoic Acid 1 11/04/22 23:00 V25983JMV
<0.135 mg/Kg - dry 0.135 0.852Benzyl alcohol 1 11/04/22 23:00 V25983JMV
<0.152 mg/Kg - dry 0.152 0.852Bis(2-Chloroethoxy)methane 1 11/04/22 23:00 V25983JMV
<0.138 mg/Kg - dry 0.138 0.852Bis(2-Chloroethyl)ether 1 11/04/22 23:00 V25983JMV
<0.175 mg/Kg - dry 0.175 0.426Bis(2-Chloroisopropyl)ether 1 11/04/22 23:00 V25983JMV
<0.155 mg/Kg - dry 0.155 0.852Bis(2-ethylhexyl)phthalate 1 11/04/22 23:00 V25983JMV
<0.140 mg/Kg - dry 0.140 0.8524-Bromophenyl phenyl ether 1 11/04/22 23:00 V25983JMV
<0.145 mg/Kg - dry 0.145 0.426
Butyl benzyl phthalate 1 11/04/22 23:00 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8524-Chloro-3-methylphenol 1 11/04/22 23:00 V25983JMV
<0.144 mg/Kg - dry 0.144 0.4264-Chloroaniline 1 11/04/22 23:00 V25983JMV
<0.149 mg/Kg - dry 0.149 0.8522-Chloronaphthalene 1 11/04/22 23:00 V25983JMV
<0.126 mg/Kg - dry 0.126 0.8522-Chlorophenol 1 11/04/22 23:00 V25983JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 11/04/22 23:00 V25983JMV
<0.183 mg/Kg - dry 0.183 0.852Chrysene 1 11/04/22 23:00 V25983JMV
<0.297 mg/Kg - dry 0.297 0.852
Dibenz(a,h)anthracene 1 11/04/22 23:00 V25983JMV
<0.153 mg/Kg - dry 0.153 0.852Dibenzofuran 1 11/04/22 23:00 V25983JMV
<0.121 mg/Kg - dry 0.121 0.8521,2-Dichlorobenzene 1 11/04/22 23:00 V25983JMV
<0.125 mg/Kg - dry 0.125 0.8521,3-Dichlorobenzene 1 11/04/22 23:00 V25983JMV
<0.125 mg/Kg - dry 0.125 0.4261,4-Dichlorobenzene 1 11/04/22 23:00 V25983JMV
<0.189 mg/Kg - dry 0.189 0.8523,3'-Dichlorobenzidine 1 11/04/22 23:00 V25983JMV
<0.123 mg/Kg - dry 0.123 0.8522,4-Dichlorophenol 1 11/04/22 23:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.232 mg/Kg - dry 0.232 0.852Diethyl phthalate 1 11/04/22 23:00 V25983JMV
<0.224 mg/Kg - dry 0.224 0.852Dimethyl phthalate 1 11/04/22 23:00 V25983JMV
<0.139 mg/Kg - dry 0.139 0.4262,4-Dimethylphenol 1 11/04/22 23:00 V25983JMV
<0.138 mg/Kg - dry 0.138 0.852Di-n-butyl phthalate 1 11/04/22 23:00 V25983JMV
<0.310 mg/Kg - dry 0.310 1.944,6-Dinitro-2-methylphenol 1 11/04/22 23:00 V25983JMV
<0.671 mg/Kg - dry 0.671 1.942,4-Dinitrophenol 1 11/04/22 23:00 V25983JMV
<0.124 mg/Kg - dry 0.124 0.8522,4-Dinitrotoluene 1 11/04/22 23:00 V25983JMV
<0.139 mg/Kg - dry 0.139 0.8522,6-Dinitrotoluene 1 11/04/22 23:00 V25983JMV
<0.184 mg/Kg - dry 0.184 0.426
Di-n-Octyl Phthalate 1 11/04/22 23:00 V25983JMV
<0.158 mg/Kg - dry 0.158 0.852Fluoranthene 1 11/04/22 23:00 V25983JMV
<0.165 mg/Kg - dry 0.165 0.852Fluorene 1 11/04/22 23:00 V25983JMV
<0.136 mg/Kg - dry 0.136 0.852Hexachlorobenzene 1 11/04/22 23:00 V25983JMV
<0.126 mg/Kg - dry 0.126 0.852Hexachlorobutadiene 1 11/04/22 23:00 V25983JMV
<0.202 mg/Kg - dry 0.202 0.852Hexachlorocyclopentadiene 1 11/04/22 23:00 V25983JMV
<0.102 mg/Kg - dry 0.102 0.852Hexachloroethane 1 11/04/22 23:00 V25983JMV
<0.231 mg/Kg - dry 0.231 0.852
Indeno(1,2,3-cd)pyrene 1 11/04/22 23:00 V25983JMV
<0.246 mg/Kg - dry 0.246 0.852Isophorone 1 11/04/22 23:00 V25983JMV
<0.136 mg/Kg - dry 0.136 0.8521-Methylnaphthalene 1 11/04/22 23:00 V25983JMV
<0.129 mg/Kg - dry 0.129 0.8522-Methylnaphthalene 1 11/04/22 23:00 V25983JMV
<0.125 mg/Kg - dry 0.125 0.8522-Methylphenol 1 11/04/22 23:00 V25983JMV
<0.109 mg/Kg - dry 0.109 0.8523&4 Methylphenol 1 11/04/22 23:00 V25983JMV
<0.186 mg/Kg - dry 0.186 0.852Naphthalene 1 11/04/22 23:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 43
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0017
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/28/2022
BOU-012
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91755 Matrix:
10/27/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.124 mg/Kg - dry 0.124 0.8522-Nitroaniline 1 11/04/22 23:00 V25983JMV
<0.155 mg/Kg - dry 0.155 0.8523-Nitroaniline 1 11/04/22 23:00 V25983JMV
<0.120 mg/Kg - dry 0.120 0.4264-Nitroaniline 1 11/04/22 23:00 V25983JMV
<0.149 mg/Kg - dry 0.149 0.426Nitrobenzene 1 11/04/22 23:00 V25983JMV
<0.114 mg/Kg - dry 0.114 0.8522-Nitrophenol 1 11/04/22 23:00 V25983JMV
<0.151 mg/Kg - dry 0.151 0.8524-Nitrophenol 1 11/04/22 23:00 V25983JMV
<0.339 mg/Kg - dry 0.339 0.852N-Nitrosodimethylamine 1 11/04/22 23:00 V25983JMV
<0.233 mg/Kg - dry 0.233 0.852N-Nitrosodiphenylamine 1 11/04/22 23:00 V25983JMV
<0.152 mg/Kg - dry 0.152 0.852
N-Nitroso-di-n-propylamine 1 11/04/22 23:00 V25983JMV
<0.448 mg/Kg - dry 0.448 1.29Pentachlorophenol 1 11/04/22 23:00 V25983JMV
<0.268 mg/Kg - dry 0.268 0.852Phenanthrene 1 11/04/22 23:00 V25983JMV
<0.144 mg/Kg - dry 0.144 0.852Phenol 1 11/04/22 23:00 V25983JMV
<0.173 mg/Kg - dry 0.173 0.852Pyrene 1 11/04/22 23:00 V25983JMV
<0.102 mg/Kg - dry 0.102 0.426Pyridine 1 11/04/22 23:00 V25983JMV
<0.138 mg/Kg - dry 0.138 0.8521,2,4-Trichlorobenzene 1 11/04/22 23:00 V25983JMV
<0.124 mg/Kg - dry 0.124 0.852
2,4,5-Trichlorophenol 1 11/04/22 23:00 V25983JMV
<0.124 mg/Kg - dry 0.124 0.8522,4,6-Trichlorophenol 1 11/04/22 23:00 V25983JMV
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%11/04/22 23:001 JMV
Surrogate: 2-Fluorobiphenyl 88.0 Limits: 44-115%11/04/22 23:001 JMV V25983
Surrogate: 2-Fluorophenol 78.7 Limits: 35-115%11/04/22 23:001 JMV V25983
Surrogate: Nitrobenzene-d5 82.6 Limits: 37-122%11/04/22 23:001 JMV V25983
Surrogate: 4-Terphenyl-d14 96.4 Limits: 54-127%11/04/22 23:001 JMV V25983
Surrogate: 2,4,6-Tribromophenol 72.7 Limits: 39-132%11/04/22 23:001 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 21 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Metals Analyses
6020B
L647316,L647584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L646697
Associated Lab Samples: 91754, 91755
LRB-L646697 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/04/22 20:470.2500.0855<0.0855mg/KgArsenic
11/04/22 20:470.2500.042<0.042mg/KgBarium
11/04/22 20:470.2500.0259<0.0259mg/KgCadmium
11/04/22 20:470.2500.116<0.116mg/KgChromium
11/04/22 20:470.2500.0310<0.0310mg/KgLead
11/04/22 20:470.2500.103<0.103mg/KgSelenium
11/04/22 20:470.2500.0067<0.0067mg/KgSilver
LCS-L646697Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1002.492.50mg/KgArsenic 80-120
1045.225.00mg/KgBarium 80-120
1010.5040.500mg/KgCadmium 80-120
1045.205.00mg/KgChromium 80-120
1022.562.50mg/KgLead 80-120
99.04.935.00mg/KgSelenium 80-120
1020.5110.500mg/KgSilver 80-120
V 91802-MS-L646697 V 91802-MSD-L646697Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.77 91.03.252.442.420.564mg/KgArsenic 110 75-125 15.9 80
113 -450*1084.874.84135mg/KgBarium -550*75-125 4.5 80
0.550 1000.5410.4870.4840.0660mg/KgCadmium 97.0 75-125 1.6 80
70.5 683*44.44.874.8437.4mg/KgChromium 144*75-125 45.4 80
Page 1 of 20* QC Fail Date:11/10/2022 12:15 PM
Page 22 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Metals Analyses
6020B
L647316,L647584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L646697
V 91802-MS-L646697 V 91802-MSD-L646697Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
14.6 186*16.92.442.4210.1mg/KgLead 279*75-125 14.6 80
2.48 48.0*2.804.874.840.133mg/KgSelenium 55.0*75-125 12.1 80
0.482 95.00.5040.4870.4840.0205mg/KgSilver 99.0 75-125 4.4 80
V 91802-PDS-L646697Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/04/22 23:1983.00.999mg/KgArsenic
11/04/22 23:1996.015.1mg/KgBarium
11/04/22 23:191000.237mg/KgCadmium
11/07/22 20:381014.20mg/KgChromium
11/04/22 23:1995.02.05mg/KgLead
11/04/22 23:1980.01.84mg/KgSelenium
11/04/22 23:1997.00.225mg/KgSilver
Page 2 of 20* QC Fail Date:11/10/2022 12:15 PM
Page 23 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V25742QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V25715
Associated Lab Samples: 91754, 91755
LRB-V25715 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/31/22 15:220.03000.0120<0.0120mg/KgMercury (Total)
LCS-V25715Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1020.4250.417mg/KgMercury (Total)80-120
V 91828-MS-V25715 V 91828-MSD-V25715Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.427 1020.4240.4170.417<0.0120mg/KgMercury (Total)102 80-120 0.7 20
V 91828-PDS-V25715Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/31/22 15:381020.213mg/KgMercury (Total)
Page 3 of 20Date:11/10/2022 12:15 PM
Page 24 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91754, 91755
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0200.002<0.002mg/KgAcetone
10/31/22 12:570.0200.001<0.001mg/KgAcrolein
10/31/22 12:570.0200.0008<0.0008mg/KgAcrylonitrile
10/31/22 12:570.0050.0006<0.0006mg/KgBenzene
10/31/22 12:570.0050.0005<0.0005mg/KgBromobenzene
10/31/22 12:570.0050.0008<0.0008mg/KgBromochloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromodichloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromoform
10/31/22 12:570.0100.001<0.001mg/KgBromomethane
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Butylbenzene
10/31/22 12:570.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/31/22 12:570.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/31/22 12:570.0050.0006<0.0006mg/KgCarbon Disulfide
10/31/22 12:570.0050.001<0.001mg/KgCarbon Tetrachloride
10/31/22 12:570.0050.0007<0.0007mg/KgChlorobenzene
10/31/22 12:570.0050.0009<0.0009mg/KgChlorodibromomethane
10/31/22 12:570.0100.0009<0.0009mg/KgChloroethane
10/31/22 12:570.0050.001<0.001mg/KgChloroform
10/31/22 12:570.0100.0006<0.0006mg/KgChloromethane
10/31/22 12:570.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/31/22 12:570.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/31/22 12:570.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/31/22 12:570.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/31/22 12:570.0050.0006<0.0006mg/KgDibromomethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 20Date:11/10/2022 12:15 PM
Page 25 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91754, 91755
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/31/22 12:570.0100.001<0.001mg/KgDichlorodifluoromethane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/31/22 12:570.0050.001<0.001mg/Kg1,2-Dichloroethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/31/22 12:570.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/31/22 12:570.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/31/22 12:570.0050.001<0.001mg/Kg2,2-Dichloropropane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/31/22 12:570.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/31/22 12:570.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/31/22 12:570.2500.014<0.014mg/KgEthanol
10/31/22 12:570.0050.0006<0.0006mg/KgEthylbenzene
10/31/22 12:570.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/31/22 12:570.0100.0008<0.0008mg/KgHexachlorobutadiene
10/31/22 12:570.0100.0007<0.0007mg/Kgn-Hexane
10/31/22 12:570.0200.0006<0.0006mg/Kg2-Hexanone
10/31/22 12:570.0050.0005<0.0005mg/KgIsopropylbenzene
10/31/22 12:570.0050.001<0.001mg/Kg4-Isopropyl toluene
10/31/22 12:570.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/31/22 12:570.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/31/22 12:570.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/31/22 12:570.0100.001<0.001mg/KgMethylene Chloride
10/31/22 12:570.0100.0010<0.0010mg/KgNaphthalene
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 20Date:11/10/2022 12:15 PM
Page 26 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91754, 91755
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.001<0.001mg/KgStyrene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTetrachloroethene
10/31/22 12:570.0050.0007<0.0007mg/KgToluene
10/31/22 12:570.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/31/22 12:570.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTrichloroethene
10/31/22 12:570.0100.002<0.002mg/KgTrichlorofluoromethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/31/22 12:570.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Acetate
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Chloride
10/31/22 12:570.0050.0005<0.0005mg/Kgo-Xylene
10/31/22 12:570.0100.001<0.001mg/Kgm,p-Xylene
10/31/22 12:574-Bromofluorobenzene (S)101 70-130
10/31/22 12:57Dibromofluoromethane (S)97.6 84-123
10/31/22 12:57Toluene-d8 (S)93.6 76-129
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.095 95.389.60.0890.100mg/KgAcetone 29-198 6.1 20
Page 6 of 20Date:11/10/2022 12:15 PM
Page 27 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031040.1040.100mg/KgAcrolein 70-130 0.9 20
0.115 1151100.1100.100mg/KgAcrylonitrile 65-134 4.4 20
0.048 97.61000.0500.050mg/KgBenzene 74-127 2.4 20
0.043 86.091.40.0450.050mg/KgBromobenzene 73-125 6.0 20
0.054 1081070.0530.050mg/KgBromochloromethane 72-134 1.2 20
0.055 1101120.0550.050mg/KgBromodichloromethane 75-122 1.0 20
0.055 1101090.0540.050mg/KgBromoform 66-135 1.2 20
0.059 1201250.0620.050mg/KgBromomethane 20-180 4.5 20
0.040 81.089.20.0440.050mg/Kgn-Butylbenzene 65-135 9.6 20
0.041 82.290.20.0450.050mg/Kgsec-Butyl benzene 66-131 9.2 20
0.040 81.287.00.0430.050mg/Kgtert-Butyl benzene 67-132 6.8 20
0.045 91.495.60.0470.050mg/KgCarbon Disulfide 61-129 4.4 20
0.045 91.295.00.0470.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.044 88.291.80.0450.050mg/KgChlorobenzene 74-118 4.0 20
0.051 1031030.0510.050mg/KgChlorodibromomethane 73-122 0.0 20
0.049 99.41040.0510.050mg/KgChloroethane 33-149 4.3 20
0.049 98.01000.0500.050mg/KgChloroform 73-127 2.0 20
0.055 1101110.0550.050mg/KgChloromethane 45-143 0.7 20
0.040 81.886.60.0430.050mg/Kg2-Chlorotoluene 67-124 5.7 20
0.040 81.886.60.0430.050mg/Kg4-Chlorotoluene 71-126 5.7 20
0.055 1111130.0560.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.2 20
0.061 1241280.0640.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.4 20
0.055 1111130.0560.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.054 1091150.0570.050mg/KgDibromomethane 74-133 5.1 20
0.044 89.290.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.041 83.686.40.0430.050mg/Kg1,3-Dichlorobenzene 71-120 3.2 20
Page 7 of 20Date:11/10/2022 12:15 PM
Page 28 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.045 91.21010.0500.050mg/KgDichlorodifluoromethane 26-146 9.8 20
0.048 96.81020.0510.050mg/Kg1,1-Dichloroethane 74-127 5.2 20
0.051 1031030.0510.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.898.60.0490.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.050 1021070.0530.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.048 96.81010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.053 1061090.0540.050mg/Kg1,2-Dichloropropane 73-130 2.4 20
0.052 1051070.0530.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.045 91.294.40.0470.050mg/Kg2,2-Dichloropropane 50-142 3.4 20
0.043 86.894.80.0470.050mg/Kg1,1-Dichloropropene 71-130 8.8 20
0.055 1111130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.056 1131120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.984 78.792.01.151.25mg/KgEthanol 70-130 15.5 20
0.044 88.490.40.0450.050mg/KgEthylbenzene 74-128 2.2 20
0.109 1091090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.039 79.887.40.0430.050mg/KgHexachlorobutadiene 64-125 9.0 20
0.048 96.81010.0500.050mg/Kgn-Hexane 70-130 3.8 20
0.054 1091070.0530.050mg/Kg2-Hexanone 61-157 2.2 20
0.039 79.487.00.0430.050mg/KgIsopropylbenzene 68-126 9.1 20
0.039 79.885.80.0420.050mg/Kg4-Isopropyl toluene 68-129 7.2 20
0.052 1051190.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 12.8 20
0.057 1141170.0580.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.7 20
0.052 10491.40.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 13.2 20
0.052 1051090.0540.050mg/KgMethylene Chloride 74-129 3.9 20
0.050 1021080.0530.050mg/KgNaphthalene 57-157 5.7 20
Page 8 of 20Date:11/10/2022 12:15 PM
Page 29 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.889.60.0440.050mg/Kgn-Propylbenzene 67-130 6.6 20
0.047 94.097.60.0480.050mg/KgStyrene 77-121 3.7 20
0.045 90.691.60.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.055 1101140.0570.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.046 92.696.20.0480.050mg/KgTetrachloroethene 68-130 3.8 20
0.047 94.298.20.0490.050mg/KgToluene 71-129 4.1 20
0.045 91.096.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.7 20
0.046 92.897.80.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.2 20
0.044 88.092.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.3 20
0.053 1081080.0540.050mg/Kg1,1,2-Trichloroethane 70-133 0.3 20
0.049 98.21050.0520.050mg/KgTrichloroethene 75-133 6.5 20
0.045 90.096.60.0480.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.056 1141150.0570.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.041 83.887.20.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.9 20
0.040 81.687.40.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.8 20
0.058 1171200.0590.050mg/KgVinyl Acetate 60-140 1.8 20
0.050 1011040.0520.050mg/KgVinyl Chloride 48-147 2.9 20
0.045 90.894.60.0470.050mg/Kgo-Xylene 74-126 4.0 20
0.087 87.490.90.0900.100mg/Kgm,p-Xylene 75-124 3.9 20
97.099.44-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)84-123
93.693.0Toluene-d8 (S)76-129
Page 9 of 20Date:11/10/2022 12:15 PM
Page 30 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91754, 91755
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.6600.116<0.116mg/KgAcenaphthene
11/04/22 16:380.6600.105<0.105mg/KgAcenaphthylene
11/04/22 16:380.6600.152<0.152mg/KgAniline
11/04/22 16:380.6600.143<0.143mg/KgAnthracene
11/04/22 16:380.6600.139<0.139mg/KgBenzo(a)anthracene
11/04/22 16:380.6600.147<0.147mg/KgBenzo(a)pyrene
11/04/22 16:380.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/04/22 16:380.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/04/22 16:380.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/04/22 16:382.000.580<0.580mg/KgBenzoic Acid
11/04/22 16:380.6600.105<0.105mg/KgBenzyl alcohol
11/04/22 16:380.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/04/22 16:380.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/04/22 16:380.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/04/22 16:380.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/04/22 16:380.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/04/22 16:380.3300.113<0.113mg/KgButyl benzyl phthalate
11/04/22 16:380.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/04/22 16:380.3300.112<0.112mg/Kg4-Chloroaniline
11/04/22 16:380.6600.116<0.116mg/Kg2-Chloronaphthalene
11/04/22 16:380.6600.098<0.098mg/Kg2-Chlorophenol
11/04/22 16:381.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/04/22 16:380.6600.142<0.142mg/KgChrysene
11/04/22 16:380.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/04/22 16:380.6600.119<0.119mg/KgDibenzofuran
11/04/22 16:380.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/04/22 16:380.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 20Date:11/10/2022 12:15 PM
Page 31 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91754, 91755
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/04/22 16:380.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/04/22 16:380.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/04/22 16:380.6600.180<0.180mg/KgDiethyl phthalate
11/04/22 16:380.6600.174<0.174mg/KgDimethyl phthalate
11/04/22 16:380.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/04/22 16:380.6600.107<0.107mg/KgDi-n-butyl phthalate
11/04/22 16:381.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/04/22 16:381.500.520<0.520mg/Kg2,4-Dinitrophenol
11/04/22 16:380.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/04/22 16:380.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/04/22 16:380.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/04/22 16:380.6600.123<0.123mg/KgFluoranthene
11/04/22 16:380.6600.128<0.128mg/KgFluorene
11/04/22 16:380.6600.106<0.106mg/KgHexachlorobenzene
11/04/22 16:380.6600.097<0.097mg/KgHexachlorobutadiene
11/04/22 16:380.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/04/22 16:380.6600.079<0.079mg/KgHexachloroethane
11/04/22 16:380.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/04/22 16:380.6600.191<0.191mg/KgIsophorone
11/04/22 16:380.6600.106<0.106mg/Kg1-Methylnaphthalene
11/04/22 16:380.6600.100<0.100mg/Kg2-Methylnaphthalene
11/04/22 16:380.6600.097<0.097mg/Kg2-Methylphenol
11/04/22 16:380.6600.084<0.084mg/Kg3&4 Methylphenol
11/04/22 16:380.6600.144<0.144mg/KgNaphthalene
11/04/22 16:380.6600.096<0.096mg/Kg2-Nitroaniline
11/04/22 16:380.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 20Date:11/10/2022 12:15 PM
Page 32 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91754, 91755
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.3300.093<0.093mg/Kg4-Nitroaniline
11/04/22 16:380.3300.116<0.116mg/KgNitrobenzene
11/04/22 16:380.6600.088<0.088mg/Kg2-Nitrophenol
11/04/22 16:380.6600.117<0.117mg/Kg4-Nitrophenol
11/04/22 16:380.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/04/22 16:380.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/04/22 16:380.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/04/22 16:381.000.347<0.347mg/KgPentachlorophenol
11/04/22 16:380.6600.208<0.208mg/KgPhenanthrene
11/04/22 16:380.6600.112<0.112mg/KgPhenol
11/04/22 16:380.6600.134<0.134mg/KgPyrene
11/04/22 16:380.3300.079<0.079mg/KgPyridine
11/04/22 16:380.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/04/22 16:380.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/04/22 16:380.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/04/22 16:382-Fluorobiphenyl (S)85.0 44-115
11/04/22 16:382-Fluorophenol (S)75.3 35-115
11/04/22 16:38Nitrobenzene-d5 (S)81.4 37-122
11/04/22 16:384-Terphenyl-d14 (S)94.6 54-127
11/04/22 16:382,4,6-Tribromophenol (S)74.4 39-132
11/04/22 16:38Phenol-d5 (S)71.4 34-121
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.61.431.67mg/KgAcenaphthene 40-123
84.41.411.67mg/KgAcenaphthylene 32-132
Page 12 of 20Date:11/10/2022 12:15 PM
Page 33 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1302.171.67mg/KgAniline 12-197
91.61.531.67mg/KgAnthracene 47-123
89.81.501.67mg/KgBenzo(a)anthracene 49-126
97.61.631.67mg/KgBenzo(a)pyrene 45-129
95.21.591.67mg/KgBenzo(b)fluoranthene 45-132
86.81.451.67mg/KgBenzo(g,h,i)perylene 43-134
92.21.541.67mg/KgBenzo(k)fluoranthene 47-132
41.60.6951.67mg/KgBenzoic Acid 10-83
88.61.481.67mg/KgBenzyl alcohol 29-122
79.01.321.67mg/KgBis(2-Chloroethoxy)methane 36-121
83.21.391.67mg/KgBis(2-Chloroethyl)ether 31-120
88.01.471.67mg/KgBis(2-Chloroisopropyl)ether 33-131
96.41.611.67mg/KgBis(2-ethylhexyl)phthalate 51-133
92.21.541.67mg/Kg4-Bromophenyl phenyl ether 46-124
94.01.571.67mg/KgButyl benzyl phthalate 48-132
76.61.281.67mg/Kg4-Chloro-3-methylphenol 45-122
81.41.361.67mg/Kg4-Chloroaniline 17-106
85.61.431.67mg/Kg2-Chloronaphthalene 41-114
85.01.421.67mg/Kg2-Chlorophenol 34-121
89.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121
89.21.491.67mg/KgChrysene 50-124
99.41.661.67mg/KgDibenz(a,h)anthracene 45-134
85.61.431.67mg/KgDibenzofuran 44-120
79.01.321.67mg/Kg1,2-Dichlorobenzene 33-117
76.61.281.67mg/Kg1,3-Dichlorobenzene 30-115
77.81.301.67mg/Kg1,4-Dichlorobenzene 31-115
76.01.271.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 20Date:11/10/2022 12:15 PM
Page 34 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2,4-Dichlorophenol 40-122
89.81.501.67mg/KgDiethyl phthalate 50-124
89.21.491.67mg/KgDimethyl phthalate 48-124
1011.691.67mg/Kg2,4-Dimethylphenol 30-127
98.21.641.67mg/KgDi-n-butyl phthalate 51-128
83.81.401.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
80.81.351.67mg/Kg2,4-Dinitrophenol 27-129
91.61.531.67mg/Kg2,4-Dinitrotoluene 48-126
89.81.501.67mg/Kg2,6-Dinitrotoluene 46-124
96.41.611.67mg/KgDi-n-Octyl Phthalate 45-140
85.01.421.67mg/KgFluoranthene 50-127
88.61.481.67mg/KgFluorene 43-125
89.81.501.67mg/KgHexachlorobenzene 45-122
75.41.261.67mg/KgHexachlorobutadiene 32-123
70.01.171.67mg/KgHexachlorocyclopentadiene 32-117
76.01.271.67mg/KgHexachloroethane 28-117
88.61.481.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
64.01.071.67mg/KgIsophorone 30-122
71.81.201.67mg/Kg1-Methylnaphthalene 40-119
71.81.201.67mg/Kg2-Methylnaphthalene 38-122
88.61.481.67mg/Kg2-Methylphenol 32-122
77.81.301.67mg/Kg3&4 Methylphenol 34-119
71.81.201.67mg/KgNaphthalene 35-123
92.21.541.67mg/Kg2-Nitroaniline 44-127
91.61.531.67mg/Kg3-Nitroaniline 33-119
91.01.521.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 14 of 20Date:11/10/2022 12:15 PM
Page 35 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
74.21.241.67mg/Kg2-Nitrophenol 36-123
92.21.541.67mg/Kg4-Nitrophenol 30-132
70.01.171.67mg/KgN-Nitrosodimethylamine 10-146
1101.831.67mg/KgN-Nitrosodiphenylamine 38-127
83.81.401.67mg/KgN-Nitroso-di-n-propylamine 36-120
1041.741.67mg/KgPentachlorophenol 25-133
90.41.511.67mg/KgPhenanthrene 50-121
80.21.341.67mg/KgPhenol 34-121
88.61.481.67mg/KgPyrene 47-127
62.81.051.67mg/KgPyridine 10-80
72.41.211.67mg/Kg1,2,4-Trichlorobenzene 34-118
85.61.431.67mg/Kg2,4,5-Trichlorophenol 41-124
86.21.441.67mg/Kg2,4,6-Trichlorophenol 39-126
87.42-Fluorobiphenyl (S)44-115
78.92-Fluorophenol (S)35-115
72.4Nitrobenzene-d5 (S)37-122
94.04-Terphenyl-d14 (S)54-127
78.02,4,6-Tribromophenol (S)39-132
74.4Phenol-d5 (S)34-121
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.36 81.41.341.671.67<0.116mg/KgAcenaphthene 80.2 40-123 1.4 20
1.34 80.21.331.671.67<0.105mg/KgAcenaphthylene 79.6 32-132 0.7 20
1.42 85.01.421.671.67<0.152mg/KgAniline 85.0 12-197 0.0 20
Page 15 of 20Date:11/10/2022 12:15 PM
Page 36 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.441.671.67<0.143mg/KgAnthracene 86.2 47-123 0.6 20
1.42 85.01.441.671.67<0.139mg/KgBenzo(a)anthracene 86.2 49-126 1.3 20
1.55 92.81.581.671.67<0.147mg/KgBenzo(a)pyrene 94.6 45-129 1.9 20
1.46 87.41.481.671.67<0.146mg/KgBenzo(b)fluoranthene 88.6 45-132 1.3 20
1.35 80.81.381.671.67<0.136mg/KgBenzo(g,h,i)perylene 82.6 43-134 2.1 20
1.48 88.61.501.671.67<0.137mg/KgBenzo(k)fluoranthene 89.8 47-132 1.3 20
1.22 73.01.141.671.67<0.580mg/KgBenzoic Acid 68.2 10-83 6.7 20
1.44 86.21.381.671.67<0.105mg/KgBenzyl alcohol 82.6 29-122 4.2 20
1.26 75.41.241.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 74.2 36-121 1.6 20
1.32 79.01.241.671.67<0.107mg/KgBis(2-Chloroethyl)ether 74.2 31-120 6.2 20
1.39 83.21.321.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 79.0 33-131 5.1 20
1.53 91.61.561.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 93.4 51-133 1.9 20
1.44 86.21.431.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 85.6 46-124 0.6 20
1.52 91.01.521.671.67<0.113mg/KgButyl benzyl phthalate 91.0 48-132 0.0 20
1.25 74.81.251.671.67<0.092mg/Kg4-Chloro-3-methylphenol 74.8 45-122 0.0 20
1.23 73.61.241.671.67<0.112mg/Kg4-Chloroaniline 74.2 17-106 0.8 20
1.35 80.81.351.671.67<0.116mg/Kg2-Chloronaphthalene 80.8 41-114 0.0 20
1.38 82.61.311.671.67<0.098mg/Kg2-Chlorophenol 78.4 34-121 5.2 20
1.42 85.01.401.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 83.8 45-121 1.4 20
1.46 87.41.451.671.67<0.142mg/KgChrysene 86.8 50-124 0.6 20
1.50 89.81.511.671.67<0.230mg/KgDibenz(a,h)anthracene 90.4 45-134 0.6 20
1.34 80.21.331.671.67<0.119mg/KgDibenzofuran 79.6 44-120 0.7 20
1.22 73.01.171.671.67<0.094mg/Kg1,2-Dichlorobenzene 70.0 33-117 4.1 20
1.20 71.81.141.671.67<0.097mg/Kg1,3-Dichlorobenzene 68.2 30-115 5.1 20
1.21 72.41.151.671.67<0.097mg/Kg1,4-Dichlorobenzene 68.8 31-115 5.0 20
0.795 47.60.8791.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 52.6 22-121 10.0 20
Page 16 of 20Date:11/10/2022 12:15 PM
Page 37 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.27 76.01.261.671.67<0.095mg/Kg2,4-Dichlorophenol 75.4 40-122 0.7 20
1.42 85.01.431.671.67<0.180mg/KgDiethyl phthalate 85.6 50-124 0.7 20
1.42 85.01.401.671.67<0.174mg/KgDimethyl phthalate 83.8 48-124 1.4 30
1.55 92.81.571.671.67<0.108mg/Kg2,4-Dimethylphenol 94.0 30-127 1.2 20
1.54 92.21.551.671.67<0.107mg/KgDi-n-butyl phthalate 92.8 51-128 0.6 20
1.37 82.01.431.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 85.6 29-132 4.2 20
1.59 95.21.551.671.67<0.520mg/Kg2,4-Dinitrophenol 92.8 27-129 2.5 20
1.38 82.61.421.671.67<0.096mg/Kg2,4-Dinitrotoluene 85.0 48-126 2.8 20
1.37 82.01.401.671.67<0.108mg/Kg2,6-Dinitrotoluene 83.8 46-124 2.1 20
1.51 90.41.571.671.67<0.143mg/KgDi-n-Octyl Phthalate 94.0 45-140 3.8 20
1.32 79.01.341.671.67<0.123mg/KgFluoranthene 80.2 50-127 1.5 20
1.39 83.21.371.671.67<0.128mg/KgFluorene 82.0 43-125 1.4 20
1.39 83.21.411.671.67<0.106mg/KgHexachlorobenzene 84.4 45-122 1.4 20
1.18 70.61.131.671.67<0.097mg/KgHexachlorobutadiene 67.6 32-123 4.3 20
1.18 70.61.151.671.67<0.157mg/KgHexachlorocyclopentadiene 68.8 32-117 2.5 20
1.19 71.21.121.671.67<0.079mg/KgHexachloroethane 67.0 28-117 6.0 20
1.38 82.61.391.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 83.2 45-133 0.7 20
1.03 61.61.021.671.67<0.191mg/KgIsophorone 61.0 30-122 0.9 20
1.15 68.81.171.671.67<0.106mg/Kg1-Methylnaphthalene 70.0 40-119 1.7 20
1.16 69.41.161.671.67<0.100mg/Kg2-Methylnaphthalene 69.4 38-122 0.0 20
1.36 81.41.341.671.67<0.097mg/Kg2-Methylphenol 80.2 32-122 1.4 20
1.23 73.61.191.671.67<0.084mg/Kg3&4 Methylphenol 71.2 34-119 3.3 20
1.14 68.21.141.671.67<0.144mg/KgNaphthalene 68.2 35-123 0.0 20
1.47 88.01.471.671.67<0.096mg/Kg2-Nitroaniline 88.0 44-127 0.0 20
1.40 83.81.421.671.67<0.120mg/Kg3-Nitroaniline 85.0 33-119 1.4 20
1.35 80.81.411.671.67<0.093mg/Kg4-Nitroaniline 84.4 63-147 4.3 20
Page 17 of 20Date:11/10/2022 12:15 PM
Page 38 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.11 66.41.101.671.67<0.116mg/KgNitrobenzene 65.8 34-122 0.9 20
1.17 70.01.171.671.67<0.088mg/Kg2-Nitrophenol 70.0 32-123 0.0 20
1.45 86.81.441.671.67<0.117mg/Kg4-Nitrophenol 86.2 30-132 0.6 20
1.11 66.41.061.671.67<0.263mg/KgN-Nitrosodimethylamine 63.4 10-146 4.6 30
1.61 96.41.661.671.67<0.181mg/KgN-Nitrosodiphenylamine 99.4 38-127 3.0 20
1.30 77.81.271.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 76.0 36-120 2.3 20
1.70 1021.751.671.67<0.347mg/KgPentachlorophenol 105 25-133 2.8 20
1.40 83.81.421.671.67<0.208mg/KgPhenanthrene 85.0 50-121 1.4 20
1.27 76.01.241.671.67<0.112mg/KgPhenol 74.2 34-121 2.3 20
1.42 85.01.451.671.67<0.134mg/KgPyrene 86.8 47-127 2.0 20
0.741 44.30.6941.671.67<0.079mg/KgPyridine 41.5 10-80 6.5 20
1.14 68.21.111.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 66.4 34-118 2.6 20
1.37 82.01.361.671.67<0.096mg/Kg2,4,5-Trichlorophenol 81.4 41-124 0.7 20
1.35 80.81.361.671.67<0.096mg/Kg2,4,6-Trichlorophenol 81.4 39-126 0.7 20
80.82-Fluorobiphenyl (S)80.2 44-115
73.32-Fluorophenol (S)70.5 35-115
68.8Nitrobenzene-d5 (S)66.4 37-122
89.84-Terphenyl-d14 (S)89.2 54-127
70.62,4,6-Tribromophenol (S)71.4 39-132
70.3Phenol-d5 (S)66.9 34-121
Page 18 of 20Date:11/10/2022 12:15 PM
Page 39 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L647181QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L646942
Associated Lab Samples: 91754, 91755
LRB-L646942 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/04/22 13:580.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L646942Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1034.114.00mg/KgChromium, Hexavalent 80-120
V 91754-DUP-L646942Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 14:300.4<0.200< 0.200mg/KgChromium, Hexavalent
V 91754-MS-L646942 V 91754-MSD-L646942Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
36.1 90.257474140.0< 0.141mg/KgChromium, Hexavalent 77.4 75-125
Page 19 of 20Date:11/10/2022 12:15 PM
Page 40 of 43
Quality Control Data
22-301-0017Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
Dry Weight Determination
SW-DRYWT
V25892QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91770-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:195.716.215.3%Moisture
V 91773-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:190.519.819.7%Moisture
Page 20 of 20Date:11/10/2022 12:15 PM
Page 41 of 43
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-301-0017
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Asia Blakeborough Date & Time:10/28/2022 16:33:21
Special precautions or instructions included?
Comments:
Page 42 of 43
Page 43 of 43

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/17/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-307-0011 Client Project Description: BOU-012
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/3/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 170
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-307-0011
Page 2 of 170
Report Number:
Sample Summary Table
Client Project Description:
22-307-0011
BOU-012
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/02/2022 12:15Solids 92342 FG-1 11/03/2022 08:56
11/02/2022 12:15Solids 92342 FG-1 11/03/2022 08:56 6020B WP MTN -
11/02/2022 12:15Solids 92342 FG-1 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 12:30Solids 92343 FG-4 11/03/2022 08:56
11/02/2022 12:30Solids 92343 FG-4 11/03/2022 08:56 6020B WP MTN -
11/02/2022 12:30Solids 92343 FG-4 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 12:50Solids 92344 FG-5 11/03/2022 08:56
11/02/2022 12:50Solids 92344 FG-5 11/03/2022 08:56 6020B WP MTN -
11/02/2022 12:50Solids 92344 FG-5 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:00Solids 92345 FG-6 11/03/2022 08:56
11/02/2022 13:00Solids 92345 FG-6 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:00Solids 92345 FG-6 11/03/2022 08:56 6020B WP MTN -
11/02/2022 13:10Solids 92346 FG-7 11/03/2022 08:56
11/02/2022 13:10Solids 92346 FG-7 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:10Solids 92346 FG-7 11/03/2022 08:56 6020B WP MTN -
11/02/2022 13:20Solids 92347 FG-8 11/03/2022 08:56
11/02/2022 13:20Solids 92347 FG-8 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:20Solids 92347 FG-8 11/03/2022 08:56 6020B WP MTN -
11/02/2022 13:30Solids 92348 FG-9 11/03/2022 08:56
11/02/2022 13:30Solids 92348 FG-9 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:30Solids 92348 FG-9 11/03/2022 08:56 6020B WP MTN -
11/02/2022 13:40Solids 92349 FG-10 11/03/2022 08:56
11/02/2022 13:40Solids 92349 FG-10 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:40Solids 92349 FG-10 11/03/2022 08:56 6020B WP MTN -
11/02/2022 13:50Solids 92350 FG-11 11/03/2022 08:56
11/02/2022 13:50Solids 92350 FG-11 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 13:50Solids 92350 FG-11 11/03/2022 08:56 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 170
Report Number:
Sample Summary Table
Client Project Description:
22-307-0011
BOU-012
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/02/2022 14:00Solids 92351 FG-12 11/03/2022 08:56
11/02/2022 14:00Solids 92351 FG-12 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 14:00Solids 92351 FG-12 11/03/2022 08:56 6020B WP MTN -
11/02/2022 14:15Solids 92352 FG-13 11/03/2022 08:56
11/02/2022 14:15Solids 92352 FG-13 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 14:15Solids 92352 FG-13 11/03/2022 08:56 6020B WP MTN -
11/02/2022 14:30Solids 92353 FG-14 11/03/2022 08:56
11/02/2022 14:30Solids 92353 FG-14 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 14:30Solids 92353 FG-14 11/03/2022 08:56 6020B WP MTN -
11/02/2022 14:45Solids 92354 FG-15 11/03/2022 08:56
11/02/2022 14:45Solids 92354 FG-15 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022 14:45Solids 92354 FG-15 11/03/2022 08:56 6020B WP MTN -
11/02/2022Solids 92355 FG-DUP 11/03/2022 08:56
11/02/2022Solids 92355 FG-DUP 11/03/2022 08:56 SW-7199 WP MTN -
11/02/2022Solids 92355 FG-DUP 11/03/2022 08:56 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 170
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-307-0011
Report Limit
Project:BOU-012
V 92342FG-1
2.42 11/14/2022 22:306020BArsenicmg/Kg - dry 0.110
74.0 11/11/2022 22:356020BBariummg/Kg - dry 0.055
J0.177 11/14/2022 22:306020BCadmiummg/Kg - dry 0.0334
46.9 11/14/2022 22:356020BChromiummg/Kg - dry 0.749
20.0 11/11/2022 22:356020BLeadmg/Kg - dry 0.0400
0.731 11/14/2022 22:306020BSeleniummg/Kg - dry 0.133
J0.0264 11/16/2022 18:056020BSilvermg/Kg - dry 0.0087
0.0612 11/10/2022 15:017471BMercury (Total)mg/Kg - dry 0.0155
0.038 11/06/2022 22:428260DAcetonemg/Kg - dry 0.003
J0.002 11/06/2022 22:428260DAcroleinmg/Kg - dry 0.001
22.6 11/08/2022 18:09SW-DRYWT Moisture %
V 92343FG-4
1.68 11/14/2022 22:406020BArsenicmg/Kg - dry 0.113
63.2 11/11/2022 22:496020BBariummg/Kg - dry 0.056
J0.0528 11/14/2022 22:406020BCadmiummg/Kg - dry 0.0340
35.9 11/14/2022 22:456020BChromiummg/Kg - dry 0.763
11.2 11/14/2022 22:406020BLeadmg/Kg - dry 0.0407
0.582 11/14/2022 22:406020BSeleniummg/Kg - dry 0.135
J0.0188 11/16/2022 18:196020BSilvermg/Kg - dry 0.0088
0.0725 11/10/2022 15:037471BMercury (Total)mg/Kg - dry 0.0158
J0.019 11/06/2022 23:098260DAcetonemg/Kg - dry 0.003
24.0 11/08/2022 18:09SW-DRYWT Moisture %
V 92344FG-5
1.82 11/14/2022 22:496020BArsenicmg/Kg - dry 0.116
69.6 11/11/2022 22:536020BBariummg/Kg - dry 0.058
J0.0957 11/14/2022 22:496020BCadmiummg/Kg - dry 0.0351
42.9 11/14/2022 22:556020BChromiummg/Kg - dry 0.788
14.9 11/14/2022 22:496020BLeadmg/Kg - dry 0.0421
0.663 11/14/2022 22:496020BSeleniummg/Kg - dry 0.139
J0.0402 11/16/2022 18:246020BSilvermg/Kg - dry 0.0091
0.0738 11/10/2022 15:067471BMercury (Total)mg/Kg - dry 0.0163
0.029 11/06/2022 23:368260DAcetonemg/Kg - dry 0.003
26.4 11/08/2022 18:09SW-DRYWT Moisture %
V 92345FG-6
1.67 11/14/2022 23:086020BArsenicmg/Kg - dry 0.112
Page 5 of 170
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-307-0011
Report Limit
Project:BOU-012
V 92345FG-6
53.9 11/11/2022 22:586020BBariummg/Kg - dry 0.055
J0.0578 11/14/2022 23:086020BCadmiummg/Kg - dry 0.0338
39.9 11/14/2022 23:136020BChromiummg/Kg - dry 0.757
10.2 11/14/2022 23:086020BLeadmg/Kg - dry 0.0404
0.755 11/14/2022 23:086020BSeleniummg/Kg - dry 0.134
J0.0268 11/16/2022 18:306020BSilvermg/Kg - dry 0.0087
0.102 11/10/2022 15:147471BMercury (Total)mg/Kg - dry 0.0157
0.027 11/07/2022 00:048260DAcetonemg/Kg - dry 0.003
23.4 11/08/2022 18:09SW-DRYWT Moisture %
V 92346FG-7
2.07 11/14/2022 23:186020BArsenicmg/Kg - dry 0.112
34.5 11/11/2022 23:026020BBariummg/Kg - dry 0.055
J0.0627 11/14/2022 23:186020BCadmiummg/Kg - dry 0.0339
36.6 11/14/2022 23:236020BChromiummg/Kg - dry 0.760
11.6 11/14/2022 23:186020BLeadmg/Kg - dry 0.0406
0.727 11/14/2022 23:186020BSeleniummg/Kg - dry 0.134
J0.0190 11/16/2022 18:356020BSilvermg/Kg - dry 0.0088
0.105 11/10/2022 15:177471BMercury (Total)mg/Kg - dry 0.0157
0.031 11/08/2022 20:348260DAcetonemg/Kg - dry 0.003
J0.004 11/08/2022 20:348260DCarbon Disulfide mg/Kg - dry 0.0008
23.7 11/08/2022 18:09SW-DRYWT Moisture %
V 92347FG-8
1.35 11/14/2022 23:286020BArsenicmg/Kg - dry 0.108
49.0 11/11/2022 23:076020BBariummg/Kg - dry 0.054
J0.0502 11/14/2022 23:286020BCadmiummg/Kg - dry 0.0327
42.5 11/14/2022 23:336020BChromiummg/Kg - dry 0.734
8.62 11/14/2022 23:286020BLeadmg/Kg - dry 0.0392
0.621 11/14/2022 23:286020BSeleniummg/Kg - dry 0.130
J0.0198 11/16/2022 18:406020BSilvermg/Kg - dry 0.0085
0.102 11/10/2022 15:197471BMercury (Total)mg/Kg - dry 0.0152
0.028 11/08/2022 21:018260DAcetonemg/Kg - dry 0.003
21.0 11/08/2022 18:09SW-DRYWT Moisture %
V 92348FG-9
1.74 11/14/2022 23:376020BArsenicmg/Kg - dry 0.119
60.6 11/11/2022 23:116020BBariummg/Kg - dry 0.059
Page 6 of 170
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-307-0011
Report Limit
Project:BOU-012
V 92348FG-9
J0.0897 11/14/2022 23:376020BCadmiummg/Kg - dry 0.0360
43.8 11/14/2022 23:436020BChromiummg/Kg - dry 0.806
13.4 11/14/2022 23:376020BLeadmg/Kg - dry 0.0431
0.721 11/14/2022 23:376020BSeleniummg/Kg - dry 0.143
J0.0235 11/16/2022 18:466020BSilvermg/Kg - dry 0.0093
0.153 11/10/2022 15:227471BMercury (Total)mg/Kg - dry 0.0167
J0.025 11/08/2022 21:298260DAcetonemg/Kg - dry 0.003
28.1 11/08/2022 18:09SW-DRYWT Moisture %
V 92349FG-10
0.844 11/14/2022 23:476020BArsenicmg/Kg - dry 0.113
90.3 11/11/2022 23:156020BBariummg/Kg - dry 0.056
J0.0953 11/14/2022 23:476020BCadmiummg/Kg - dry 0.0343
48.8 11/14/2022 23:536020BChromiummg/Kg - dry 0.769
4.88 11/14/2022 23:476020BLeadmg/Kg - dry 0.0411
0.473 11/14/2022 23:476020BSeleniummg/Kg - dry 0.136
J0.0224 11/16/2022 18:516020BSilvermg/Kg - dry 0.0089
0.0960 11/10/2022 15:247471BMercury (Total)mg/Kg - dry 0.0159
0.042 11/08/2022 21:568260DAcetonemg/Kg - dry 0.003
J0.002 11/08/2022 21:568260DBromomethanemg/Kg - dry 0.002
J0.001 11/08/2022 21:568260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 11/08/2022 21:568260DChloromethanemg/Kg - dry 0.0008
24.6 11/08/2022 18:09SW-DRYWT Moisture %
V 92350FG-11
1.73 11/15/2022 00:066020BArsenicmg/Kg - dry 0.111
41.0 11/11/2022 23:206020BBariummg/Kg - dry 0.055
J0.105 11/15/2022 00:066020BCadmiummg/Kg - dry 0.0335
33.5 11/15/2022 00:116020BChromiummg/Kg - dry 0.752
9.21 11/15/2022 00:066020BLeadmg/Kg - dry 0.0402
0.715 11/15/2022 00:066020BSeleniummg/Kg - dry 0.133
J0.0158 11/16/2022 18:576020BSilvermg/Kg - dry 0.0087
0.0830 11/10/2022 15:277471BMercury (Total)mg/Kg - dry 0.0156
J0.022 11/08/2022 22:238260DAcetonemg/Kg - dry 0.003
J0.237 11/08/2022 22:238260DEthanolmg/Kg - dry 0.018
22.9 11/08/2022 18:09SW-DRYWT Moisture %
Page 7 of 170
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-307-0011
Report Limit
Project:BOU-012
V 92351FG-12
1.80 11/15/2022 00:156020BArsenicmg/Kg - dry 0.115
49.9 11/11/2022 23:246020BBariummg/Kg - dry 0.057
J0.0881 11/15/2022 00:156020BCadmiummg/Kg - dry 0.0348
36.0 11/15/2022 00:216020BChromiummg/Kg - dry 0.779
12.4 11/15/2022 00:156020BLeadmg/Kg - dry 0.0416
0.668 11/15/2022 00:156020BSeleniummg/Kg - dry 0.138
J0.0431 11/16/2022 19:026020BSilvermg/Kg - dry 0.0090
0.0837 11/10/2022 15:297471BMercury (Total)mg/Kg - dry 0.0161
0.045 11/08/2022 22:518260DAcetonemg/Kg - dry 0.003
J0.213 11/11/2022 18:168270EButyl benzyl phthalate mg/Kg - dry 0.151
J0.193 11/11/2022 18:168270EFluoranthenemg/Kg - dry 0.165
25.6 11/08/2022 18:09SW-DRYWT Moisture %
V 92352FG-13
2.11 11/15/2022 00:256020BArsenicmg/Kg - dry 0.116
40.5 11/11/2022 23:286020BBariummg/Kg - dry 0.057
J0.0613 11/15/2022 00:256020BCadmiummg/Kg - dry 0.0350
41.5 11/15/2022 00:316020BChromiummg/Kg - dry 0.785
10.8 11/15/2022 00:256020BLeadmg/Kg - dry 0.0420
0.768 11/15/2022 00:256020BSeleniummg/Kg - dry 0.139
J0.0298 11/16/2022 19:076020BSilvermg/Kg - dry 0.0091
0.101 11/10/2022 15:327471BMercury (Total)mg/Kg - dry 0.0163
0.029 11/08/2022 23:188260DAcetonemg/Kg - dry 0.003
26.2 11/08/2022 18:09SW-DRYWT Moisture %
V 92353FG-14
2.54 11/15/2022 00:356020BArsenicmg/Kg - dry 0.108
73.3 11/11/2022 23:426020BBariummg/Kg - dry 0.053
J0.147 11/15/2022 00:356020BCadmiummg/Kg - dry 0.0325
40.8 11/15/2022 00:416020BChromiummg/Kg - dry 0.729
13.5 11/15/2022 00:356020BLeadmg/Kg - dry 0.0389
0.778 11/15/2022 00:356020BSeleniummg/Kg - dry 0.129
J0.0638 11/16/2022 19:226020BSilvermg/Kg - dry 0.0084
0.179 11/10/2022 15:347471BMercury (Total)mg/Kg - dry 0.0151
0.025 11/08/2022 23:468260DAcetonemg/Kg - dry 0.003
20.5 11/08/2022 18:09SW-DRYWT Moisture %
Page 8 of 170
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-307-0011
Report Limit
Project:BOU-012
V 92354FG-15
0.953 11/15/2022 00:466020BArsenicmg/Kg - dry 0.106
73.0 11/11/2022 23:476020BBariummg/Kg - dry 0.053
J0.0484 11/15/2022 00:466020BCadmiummg/Kg - dry 0.0321
38.6 11/15/2022 00:516020BChromiummg/Kg - dry 0.720
5.24 11/15/2022 00:466020BLeadmg/Kg - dry 0.0385
0.414 11/15/2022 00:466020BSeleniummg/Kg - dry 0.127
J0.0160 11/16/2022 19:286020BSilvermg/Kg - dry 0.0083
0.0717 11/10/2022 15:377471BMercury (Total)mg/Kg - dry 0.0149
J0.021 11/09/2022 00:138260DAcetonemg/Kg - dry 0.002
19.5 11/08/2022 18:09SW-DRYWT Moisture %
V 92355FG-DUP
1.48 11/15/2022 01:046020BArsenicmg/Kg - dry 0.112
46.1 11/11/2022 23:516020BBariummg/Kg - dry 0.056
J0.0616 11/15/2022 01:046020BCadmiummg/Kg - dry 0.0340
33.5 11/15/2022 19:426020BChromiummg/Kg - dry 0.152
10.4 11/15/2022 01:046020BLeadmg/Kg - dry 0.0407
0.638 11/15/2022 01:046020BSeleniummg/Kg - dry 0.135
J0.0161 11/16/2022 19:336020BSilvermg/Kg - dry 0.0088
0.0937 11/10/2022 15:467471BMercury (Total)mg/Kg - dry 0.0158
0.044 11/09/2022 00:408260DAcetonemg/Kg - dry 0.003
J0.395 11/11/2022 20:318270EButyl benzyl phthalate mg/Kg - dry 0.148
23.9 11/08/2022 18:09SW-DRYWT Moisture %
Page 9 of 170

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: BOU-012 Lab Report Number: 22-307-0011
Date: 11/17/2022
Metals Analyses Method 6020B Sample 87550 (345723) Analyte: Silver
QC Batch No: L649337/L647906 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 87550 (345723)
Analyte: Barium QC Batch No: L648608/L647906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 87550 (345723) Analyte: Chromium
QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are
required. Sample 92342 (FG-1) Analyte: Chromium
QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are
required.
Sample 92343 (FG-4) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are
required.
Sample 92344 (FG-5) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92345 (FG-6) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Page 10 of 170

Sample 92346 (FG-7)
Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92347 (FG-8)
Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92348 (FG-9)
Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92349 (FG-10)
Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required. Sample 92350 (FG-11)
Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required. Sample 92351 (FG-12) Analyte: Chromium QC Batch No: L648858/L647906
One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92352 (FG-13) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Sample 92353 (FG-14) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required. Sample 92354 (FG-15) Analyte: Chromium QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are required.
Page 11 of 170

Sample 92355 (FG-DUP) Analyte: Chromium
QC Batch No: L648858/L647906 One or more Internal Standards are outside method acceptance criteria. Re-analysis and/or sample dilutions are
required.
Sample 87550 (345723) Analyte: Lead
QC Batch No: L648858/L647906 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 QC Batch No: L649235
Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium.
QC Batch No: L649235
Insoluble Hexavalent Chromium spike data. Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acetone QC Batch No: V26116/V25973 CCV result above control limits but within method parameters. LCS and LCSD recovered within parameters.
Results are reported but considered estimated. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 92164 (SB-DUP) Analyte: Benzoic Acid QC Batch No: V26276/V26175 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 92164 (SB-DUP)
Analyte: Hexachlorocyclopentadiene QC Batch No: V26276/V26175 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 92164 (SB-DUP)
Analyte: N-Nitrosodiphenylamine QC Batch No: V26276/V26175 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 92351 (FG-12) QC Batch No: V26355/V26228 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits for several analytes. Sample 92351 (FG-12) Analyte: Benzoic Acid
Page 12 of 170

QC Batch No: V26355/V26228
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 92351 (FG-12)
Analyte: Hexachlorocyclopentadiene QC Batch No: V26355/V26228
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Matrix spike recovery is outside control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.

Page 13 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.6 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.182 mg/Kg - dry 0.182 0.258Chromium, Hexavalent 1 11/16/22 19:19 SW-7199SAR
2.42 mg/Kg - dry 0.110 0.323Arsenic 5 11/14/22 22:30 6020BBKN
74.0 mg/Kg - dry 0.055 0.322Barium 5 11/11/22 22:35 6020BBKN
0.177 J mg/Kg - dry 0.0334 0.323Cadmium 5 11/14/22 22:30 6020BBKN
46.9 mg/Kg - dry 0.749 1.61
Chromium 25 11/14/22 22:35 6020BBKN
20.0 mg/Kg - dry 0.0400 0.323Lead 5 11/11/22 22:35 6020BBKN
0.0612 mg/Kg - dry 0.0155 0.0388Mercury (Total)1 11/10/22 15:01 7471BEDV
0.731 mg/Kg - dry 0.133 0.322Selenium 5 11/14/22 22:30 6020BBKN
0.0264 J mg/Kg - dry 0.0087 0.323Silver 5 11/16/22 18:05 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
0.038 mg/Kg - dry 0.003 0.025Acetone 1 11/06/22 22:42 V25974TBL
0.002 J mg/Kg - dry 0.001 0.025Acrolein 1 11/06/22 22:42 V25974TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/06/22 22:42 V25974TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/06/22 22:42 V25974TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/06/22 22:42 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/06/22 22:42 V25974TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/06/22 22:42 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/06/22 22:42 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/06/22 22:42 V25974TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/06/22 22:42 V25974TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/06/22 22:42 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/06/22 22:42 V25974TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/06/22 22:42 V25974TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/06/22 22:42 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/06/22 22:42 V25974TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/06/22 22:42 V25974TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/06/22 22:42 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/06/22 22:42 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/06/22 22:42 V25974TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/06/22 22:42 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/06/22 22:42 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/06/22 22:42 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/06/22 22:42 V25974TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/06/22 22:42 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/06/22 22:42 V25974
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%11/06/22 22:421 TBL V25974
Surrogate: Dibromofluoromethane 114 Limits: 84-123%11/06/22 22:421 TBL V25974
Surrogate: Toluene-d8 119 Limits: 76-129%11/06/22 22:421 TBL V25974
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.149 mg/Kg - dry 0.149 0.852Acenaphthene 1 11/11/22 14:31 V26276JMV
<0.135 mg/Kg - dry 0.135 0.852Acenaphthylene 1 11/11/22 14:31 V26276JMV
<0.196 mg/Kg - dry 0.196 0.852Aniline 1 11/11/22 14:31 V26276JMV
<0.184 mg/Kg - dry 0.184 0.852Anthracene 1 11/11/22 14:31 V26276JMV
<0.179 mg/Kg - dry 0.179 0.852
Benzo(a)anthracene 1 11/11/22 14:31 V26276JMV
<0.189 mg/Kg - dry 0.189 0.852Benzo(a)pyrene 1 11/11/22 14:31 V26276JMV
<0.188 mg/Kg - dry 0.188 0.852Benzo(b)fluoranthene 1 11/11/22 14:31 V26276JMV
<0.175 mg/Kg - dry 0.175 0.852Benzo(g,h,i)perylene 1 11/11/22 14:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.177 mg/Kg - dry 0.177 0.852Benzo(k)fluoranthene 1 11/11/22 14:31 V26276JMV
<0.749 mg/Kg - dry 0.749 2.58Benzoic Acid 1 11/11/22 14:31 V26276JMV
<0.135 mg/Kg - dry 0.135 0.852Benzyl alcohol 1 11/11/22 14:31 V26276JMV
<0.152 mg/Kg - dry 0.152 0.852Bis(2-Chloroethoxy)methane 1 11/11/22 14:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.852Bis(2-Chloroethyl)ether 1 11/11/22 14:31 V26276JMV
<0.175 mg/Kg - dry 0.175 0.426Bis(2-Chloroisopropyl)ether 1 11/11/22 14:31 V26276JMV
<0.155 mg/Kg - dry 0.155 0.852Bis(2-ethylhexyl)phthalate 1 11/11/22 14:31 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8524-Bromophenyl phenyl ether 1 11/11/22 14:31 V26276JMV
<0.145 mg/Kg - dry 0.145 0.426
Butyl benzyl phthalate 1 11/11/22 14:31 V26276JMV
<0.119 mg/Kg - dry 0.119 0.8524-Chloro-3-methylphenol 1 11/11/22 14:31 V26276JMV
<0.144 mg/Kg - dry 0.144 0.4264-Chloroaniline 1 11/11/22 14:31 V26276JMV
<0.149 mg/Kg - dry 0.149 0.8522-Chloronaphthalene 1 11/11/22 14:31 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8522-Chlorophenol 1 11/11/22 14:31 V26276JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 11/11/22 14:31 V26276JMV
<0.183 mg/Kg - dry 0.183 0.852Chrysene 1 11/11/22 14:31 V26276JMV
<0.297 mg/Kg - dry 0.297 0.852
Dibenz(a,h)anthracene 1 11/11/22 14:31 V26276JMV
<0.153 mg/Kg - dry 0.153 0.852Dibenzofuran 1 11/11/22 14:31 V26276JMV
<0.121 mg/Kg - dry 0.121 0.8521,2-Dichlorobenzene 1 11/11/22 14:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8521,3-Dichlorobenzene 1 11/11/22 14:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.4261,4-Dichlorobenzene 1 11/11/22 14:31 V26276JMV
<0.189 mg/Kg - dry 0.189 0.8523,3'-Dichlorobenzidine 1 11/11/22 14:31 V26276JMV
<0.123 mg/Kg - dry 0.123 0.8522,4-Dichlorophenol 1 11/11/22 14:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.232 mg/Kg - dry 0.232 0.852Diethyl phthalate 1 11/11/22 14:31 V26276JMV
<0.224 mg/Kg - dry 0.224 0.852Dimethyl phthalate 1 11/11/22 14:31 V26276JMV
<0.139 mg/Kg - dry 0.139 0.4262,4-Dimethylphenol 1 11/11/22 14:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.852Di-n-butyl phthalate 1 11/11/22 14:31 V26276JMV
<0.310 mg/Kg - dry 0.310 1.944,6-Dinitro-2-methylphenol 1 11/11/22 14:31 V26276JMV
<0.671 mg/Kg - dry 0.671 1.942,4-Dinitrophenol 1 11/11/22 14:31 V26276JMV
<0.124 mg/Kg - dry 0.124 0.8522,4-Dinitrotoluene 1 11/11/22 14:31 V26276JMV
<0.139 mg/Kg - dry 0.139 0.8522,6-Dinitrotoluene 1 11/11/22 14:31 V26276JMV
<0.184 mg/Kg - dry 0.184 0.426
Di-n-Octyl Phthalate 1 11/11/22 14:31 V26276JMV
<0.158 mg/Kg - dry 0.158 0.852Fluoranthene 1 11/11/22 14:31 V26276JMV
<0.165 mg/Kg - dry 0.165 0.852Fluorene 1 11/11/22 14:31 V26276JMV
<0.136 mg/Kg - dry 0.136 0.852Hexachlorobenzene 1 11/11/22 14:31 V26276JMV
<0.126 mg/Kg - dry 0.126 0.852Hexachlorobutadiene 1 11/11/22 14:31 V26276JMV
<0.202 mg/Kg - dry 0.202 0.852Hexachlorocyclopentadiene 1 11/11/22 14:31 V26276JMV
<0.102 mg/Kg - dry 0.102 0.852Hexachloroethane 1 11/11/22 14:31 V26276JMV
<0.231 mg/Kg - dry 0.231 0.852
Indeno(1,2,3-cd)pyrene 1 11/11/22 14:31 V26276JMV
<0.246 mg/Kg - dry 0.246 0.852Isophorone 1 11/11/22 14:31 V26276JMV
<0.136 mg/Kg - dry 0.136 0.8521-Methylnaphthalene 1 11/11/22 14:31 V26276JMV
<0.129 mg/Kg - dry 0.129 0.8522-Methylnaphthalene 1 11/11/22 14:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8522-Methylphenol 1 11/11/22 14:31 V26276JMV
<0.109 mg/Kg - dry 0.109 0.8523&4 Methylphenol 1 11/11/22 14:31 V26276JMV
<0.186 mg/Kg - dry 0.186 0.852Naphthalene 1 11/11/22 14:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-1
92342 Matrix:
11/2/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.124 mg/Kg - dry 0.124 0.8522-Nitroaniline 1 11/11/22 14:31 V26276JMV
<0.155 mg/Kg - dry 0.155 0.8523-Nitroaniline 1 11/11/22 14:31 V26276JMV
<0.120 mg/Kg - dry 0.120 0.4264-Nitroaniline 1 11/11/22 14:31 V26276JMV
<0.149 mg/Kg - dry 0.149 0.426Nitrobenzene 1 11/11/22 14:31 V26276JMV
<0.114 mg/Kg - dry 0.114 0.8522-Nitrophenol 1 11/11/22 14:31 V26276JMV
<0.151 mg/Kg - dry 0.151 0.8524-Nitrophenol 1 11/11/22 14:31 V26276JMV
<0.339 mg/Kg - dry 0.339 0.852N-Nitrosodimethylamine 1 11/11/22 14:31 V26276JMV
<0.233 mg/Kg - dry 0.233 0.852N-Nitrosodiphenylamine 1 11/11/22 14:31 V26276JMV
<0.152 mg/Kg - dry 0.152 0.852
N-Nitroso-di-n-propylamine 1 11/11/22 14:31 V26276JMV
<0.448 mg/Kg - dry 0.448 1.29Pentachlorophenol 1 11/11/22 14:31 V26276JMV
<0.268 mg/Kg - dry 0.268 0.852Phenanthrene 1 11/11/22 14:31 V26276JMV
<0.144 mg/Kg - dry 0.144 0.852Phenol 1 11/11/22 14:31 V26276JMV
<0.173 mg/Kg - dry 0.173 0.852Pyrene 1 11/11/22 14:31 V26276JMV
<0.102 mg/Kg - dry 0.102 0.426Pyridine 1 11/11/22 14:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.8521,2,4-Trichlorobenzene 1 11/11/22 14:31 V26276JMV
<0.124 mg/Kg - dry 0.124 0.852
2,4,5-Trichlorophenol 1 11/11/22 14:31 V26276JMV
<0.124 mg/Kg - dry 0.124 0.8522,4,6-Trichlorophenol 1 11/11/22 14:31 V26276JMV
8270ESurrogate: Phenol-d5 72.7 Limits: 34-121%11/11/22 14:311 JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%11/11/22 14:311 JMV V26276
Surrogate: 2-Fluorophenol 76.0 Limits: 35-115%11/11/22 14:311 JMV V26276
Surrogate: Nitrobenzene-d5 83.8 Limits: 37-122%11/11/22 14:311 JMV V26276
Surrogate: 4-Terphenyl-d14 110 Limits: 54-127%11/11/22 14:311 JMV V26276
Surrogate: 2,4,6-Tribromophenol 81.4 Limits: 39-132%11/11/22 14:311 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.0 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.185 mg/Kg - dry 0.185 0.264Chromium, Hexavalent 1 11/16/22 19:30 SW-7199SAR
1.68 mg/Kg - dry 0.113 0.329Arsenic 5 11/14/22 22:40 6020BBKN
63.2 mg/Kg - dry 0.056 0.328Barium 5 11/11/22 22:49 6020BBKN
0.0528 J mg/Kg - dry 0.0340 0.329Cadmium 5 11/14/22 22:40 6020BBKN
35.9 mg/Kg - dry 0.763 1.64
Chromium 25 11/14/22 22:45 6020BBKN
11.2 mg/Kg - dry 0.0407 0.329Lead 5 11/14/22 22:40 6020BBKN
0.0725 mg/Kg - dry 0.0158 0.0395Mercury (Total)1 11/10/22 15:03 7471BEDV
0.582 mg/Kg - dry 0.135 0.328Selenium 5 11/14/22 22:40 6020BBKN
0.0188 J mg/Kg - dry 0.0088 0.329Silver 5 11/16/22 18:19 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
0.019 J mg/Kg - dry 0.003 0.026Acetone 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/06/22 23:09 V25974TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/06/22 23:09 V25974TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/06/22 23:09 V25974TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/06/22 23:09 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/06/22 23:09 V25974TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/06/22 23:09 V25974TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/06/22 23:09 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/06/22 23:09 V25974TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/06/22 23:09 V25974TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/06/22 23:09 V25974TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/06/22 23:09 V25974TBL
<0.018 mg/Kg - dry 0.018 0.328Ethanol 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/06/22 23:09 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/06/22 23:09 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/06/22 23:09 V25974TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/06/22 23:09 V25974TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/06/22 23:09 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/06/22 23:09 V25974TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/06/22 23:09 V25974TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/06/22 23:09 V25974TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/06/22 23:09 V25974TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25973 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/06/22 23:09 V25974TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/06/22 23:09 V25974TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/06/22 23:09 V25974TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/06/22 23:09 V25974
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%11/06/22 23:091 TBL V25974
Surrogate: Dibromofluoromethane 118 Limits: 84-123%11/06/22 23:091 TBL V25974
Surrogate: Toluene-d8 120 Limits: 76-129%11/06/22 23:091 TBL V25974
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.152 mg/Kg - dry 0.152 0.868Acenaphthene 1 11/11/22 14:53 V26276JMV
<0.138 mg/Kg - dry 0.138 0.868Acenaphthylene 1 11/11/22 14:53 V26276JMV
<0.200 mg/Kg - dry 0.200 0.868Aniline 1 11/11/22 14:53 V26276JMV
<0.188 mg/Kg - dry 0.188 0.868Anthracene 1 11/11/22 14:53 V26276JMV
<0.182 mg/Kg - dry 0.182 0.868
Benzo(a)anthracene 1 11/11/22 14:53 V26276JMV
<0.193 mg/Kg - dry 0.193 0.868Benzo(a)pyrene 1 11/11/22 14:53 V26276JMV
<0.192 mg/Kg - dry 0.192 0.868Benzo(b)fluoranthene 1 11/11/22 14:53 V26276JMV
<0.178 mg/Kg - dry 0.178 0.868Benzo(g,h,i)perylene 1 11/11/22 14:53 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.180 mg/Kg - dry 0.180 0.868Benzo(k)fluoranthene 1 11/11/22 14:53 V26276JMV
<0.763 mg/Kg - dry 0.763 2.63Benzoic Acid 1 11/11/22 14:53 V26276JMV
<0.138 mg/Kg - dry 0.138 0.868Benzyl alcohol 1 11/11/22 14:53 V26276JMV
<0.155 mg/Kg - dry 0.155 0.868Bis(2-Chloroethoxy)methane 1 11/11/22 14:53 V26276JMV
<0.140 mg/Kg - dry 0.140 0.868Bis(2-Chloroethyl)ether 1 11/11/22 14:53 V26276JMV
<0.178 mg/Kg - dry 0.178 0.434Bis(2-Chloroisopropyl)ether 1 11/11/22 14:53 V26276JMV
<0.157 mg/Kg - dry 0.157 0.868Bis(2-ethylhexyl)phthalate 1 11/11/22 14:53 V26276JMV
<0.143 mg/Kg - dry 0.143 0.8684-Bromophenyl phenyl ether 1 11/11/22 14:53 V26276JMV
<0.148 mg/Kg - dry 0.148 0.434
Butyl benzyl phthalate 1 11/11/22 14:53 V26276JMV
<0.121 mg/Kg - dry 0.121 0.8684-Chloro-3-methylphenol 1 11/11/22 14:53 V26276JMV
<0.147 mg/Kg - dry 0.147 0.4344-Chloroaniline 1 11/11/22 14:53 V26276JMV
<0.152 mg/Kg - dry 0.152 0.8682-Chloronaphthalene 1 11/11/22 14:53 V26276JMV
<0.129 mg/Kg - dry 0.129 0.8682-Chlorophenol 1 11/11/22 14:53 V26276JMV
<0.165 mg/Kg - dry 0.165 1.324-Chlorophenyl phenyl ether 1 11/11/22 14:53 V26276JMV
<0.186 mg/Kg - dry 0.186 0.868Chrysene 1 11/11/22 14:53 V26276JMV
<0.302 mg/Kg - dry 0.302 0.868
Dibenz(a,h)anthracene 1 11/11/22 14:53 V26276JMV
<0.156 mg/Kg - dry 0.156 0.868Dibenzofuran 1 11/11/22 14:53 V26276JMV
<0.124 mg/Kg - dry 0.124 0.8681,2-Dichlorobenzene 1 11/11/22 14:53 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8681,3-Dichlorobenzene 1 11/11/22 14:53 V26276JMV
<0.128 mg/Kg - dry 0.128 0.4341,4-Dichlorobenzene 1 11/11/22 14:53 V26276JMV
<0.193 mg/Kg - dry 0.193 0.8683,3'-Dichlorobenzidine 1 11/11/22 14:53 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8682,4-Dichlorophenol 1 11/11/22 14:53 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.236 mg/Kg - dry 0.236 0.868Diethyl phthalate 1 11/11/22 14:53 V26276JMV
<0.228 mg/Kg - dry 0.228 0.868Dimethyl phthalate 1 11/11/22 14:53 V26276JMV
<0.142 mg/Kg - dry 0.142 0.4342,4-Dimethylphenol 1 11/11/22 14:53 V26276JMV
<0.140 mg/Kg - dry 0.140 0.868Di-n-butyl phthalate 1 11/11/22 14:53 V26276JMV
<0.315 mg/Kg - dry 0.315 1.974,6-Dinitro-2-methylphenol 1 11/11/22 14:53 V26276JMV
<0.684 mg/Kg - dry 0.684 1.972,4-Dinitrophenol 1 11/11/22 14:53 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8682,4-Dinitrotoluene 1 11/11/22 14:53 V26276JMV
<0.142 mg/Kg - dry 0.142 0.8682,6-Dinitrotoluene 1 11/11/22 14:53 V26276JMV
<0.188 mg/Kg - dry 0.188 0.434
Di-n-Octyl Phthalate 1 11/11/22 14:53 V26276JMV
<0.161 mg/Kg - dry 0.161 0.868Fluoranthene 1 11/11/22 14:53 V26276JMV
<0.168 mg/Kg - dry 0.168 0.868Fluorene 1 11/11/22 14:53 V26276JMV
<0.139 mg/Kg - dry 0.139 0.868Hexachlorobenzene 1 11/11/22 14:53 V26276JMV
<0.128 mg/Kg - dry 0.128 0.868Hexachlorobutadiene 1 11/11/22 14:53 V26276JMV
<0.206 mg/Kg - dry 0.206 0.868Hexachlorocyclopentadiene 1 11/11/22 14:53 V26276JMV
<0.104 mg/Kg - dry 0.104 0.868Hexachloroethane 1 11/11/22 14:53 V26276JMV
<0.235 mg/Kg - dry 0.235 0.868
Indeno(1,2,3-cd)pyrene 1 11/11/22 14:53 V26276JMV
<0.251 mg/Kg - dry 0.251 0.868Isophorone 1 11/11/22 14:53 V26276JMV
<0.139 mg/Kg - dry 0.139 0.8681-Methylnaphthalene 1 11/11/22 14:53 V26276JMV
<0.131 mg/Kg - dry 0.131 0.8682-Methylnaphthalene 1 11/11/22 14:53 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8682-Methylphenol 1 11/11/22 14:53 V26276JMV
<0.111 mg/Kg - dry 0.111 0.8683&4 Methylphenol 1 11/11/22 14:53 V26276JMV
<0.189 mg/Kg - dry 0.189 0.868Naphthalene 1 11/11/22 14:53 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-4
92343 Matrix:
11/2/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.127 mg/Kg - dry 0.127 0.8682-Nitroaniline 1 11/11/22 14:53 V26276JMV
<0.157 mg/Kg - dry 0.157 0.8683-Nitroaniline 1 11/11/22 14:53 V26276JMV
<0.122 mg/Kg - dry 0.122 0.4344-Nitroaniline 1 11/11/22 14:53 V26276JMV
<0.152 mg/Kg - dry 0.152 0.434Nitrobenzene 1 11/11/22 14:53 V26276JMV
<0.116 mg/Kg - dry 0.116 0.8682-Nitrophenol 1 11/11/22 14:53 V26276JMV
<0.153 mg/Kg - dry 0.153 0.8684-Nitrophenol 1 11/11/22 14:53 V26276JMV
<0.346 mg/Kg - dry 0.346 0.868N-Nitrosodimethylamine 1 11/11/22 14:53 V26276JMV
<0.238 mg/Kg - dry 0.238 0.868N-Nitrosodiphenylamine 1 11/11/22 14:53 V26276JMV
<0.155 mg/Kg - dry 0.155 0.868
N-Nitroso-di-n-propylamine 1 11/11/22 14:53 V26276JMV
<0.456 mg/Kg - dry 0.456 1.32Pentachlorophenol 1 11/11/22 14:53 V26276JMV
<0.273 mg/Kg - dry 0.273 0.868Phenanthrene 1 11/11/22 14:53 V26276JMV
<0.147 mg/Kg - dry 0.147 0.868Phenol 1 11/11/22 14:53 V26276JMV
<0.176 mg/Kg - dry 0.176 0.868Pyrene 1 11/11/22 14:53 V26276JMV
<0.104 mg/Kg - dry 0.104 0.434Pyridine 1 11/11/22 14:53 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8681,2,4-Trichlorobenzene 1 11/11/22 14:53 V26276JMV
<0.126 mg/Kg - dry 0.126 0.868
2,4,5-Trichlorophenol 1 11/11/22 14:53 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8682,4,6-Trichlorophenol 1 11/11/22 14:53 V26276JMV
8270ESurrogate: Phenol-d5 74.6 Limits: 34-121%11/11/22 14:531 JMV
Surrogate: 2-Fluorobiphenyl 93.4 Limits: 44-115%11/11/22 14:531 JMV V26276
Surrogate: 2-Fluorophenol 79.0 Limits: 35-115%11/11/22 14:531 JMV V26276
Surrogate: Nitrobenzene-d5 88.6 Limits: 37-122%11/11/22 14:531 JMV V26276
Surrogate: 4-Terphenyl-d14 106 Limits: 54-127%11/11/22 14:531 JMV V26276
Surrogate: 2,4,6-Tribromophenol 76.3 Limits: 39-132%11/11/22 14:531 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.4 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.197 mg/Kg - dry 0.197 0.279Chromium, Hexavalent 1 11/16/22 19:41 SW-7199SAR
1.82 mg/Kg - dry 0.116 0.340Arsenic 5 11/14/22 22:49 6020BBKN
69.6 mg/Kg - dry 0.058 0.339Barium 5 11/11/22 22:53 6020BBKN
0.0957 J mg/Kg - dry 0.0351 0.340Cadmium 5 11/14/22 22:49 6020BBKN
42.9 mg/Kg - dry 0.788 1.70
Chromium 25 11/14/22 22:55 6020BBKN
14.9 mg/Kg - dry 0.0421 0.340Lead 5 11/14/22 22:49 6020BBKN
0.0738 mg/Kg - dry 0.0163 0.0408Mercury (Total)1 11/10/22 15:06 7471BEDV
0.663 mg/Kg - dry 0.139 0.339Selenium 5 11/14/22 22:49 6020BBKN
0.0402 J mg/Kg - dry 0.0091 0.340Silver 5 11/16/22 18:24 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
0.029 mg/Kg - dry 0.003 0.027Acetone 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/06/22 23:36 V25976TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 11/06/22 23:36 V25976TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/06/22 23:36 V25976TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/06/22 23:36 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/06/22 23:36 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 11/06/22 23:36 V25976TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/06/22 23:36 V25976TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/06/22 23:36 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/06/22 23:36 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/06/22 23:36 V25976TBL
<0.019 mg/Kg - dry 0.019 0.339Ethanol 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/06/22 23:36 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 11/06/22 23:36 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 11/06/22 23:36 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/06/22 23:36 V25976TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/06/22 23:36 V25976TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/06/22 23:36 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/06/22 23:36 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/06/22 23:36 V25976TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/06/22 23:36 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 11/06/22 23:36 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/06/22 23:36 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/06/22 23:36 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/06/22 23:36 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/06/22 23:36 V25976
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%11/06/22 23:361 TBL V25976
Surrogate: Dibromofluoromethane 117 Limits: 84-123%11/06/22 23:361 TBL V25976
Surrogate: Toluene-d8 118 Limits: 76-129%11/06/22 23:361 TBL V25976
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.157 mg/Kg - dry 0.157 0.896Acenaphthene 1 11/11/22 15:16 V26276JMV
<0.142 mg/Kg - dry 0.142 0.896Acenaphthylene 1 11/11/22 15:16 V26276JMV
<0.206 mg/Kg - dry 0.206 0.896Aniline 1 11/11/22 15:16 V26276JMV
<0.194 mg/Kg - dry 0.194 0.896Anthracene 1 11/11/22 15:16 V26276JMV
<0.188 mg/Kg - dry 0.188 0.896
Benzo(a)anthracene 1 11/11/22 15:16 V26276JMV
<0.199 mg/Kg - dry 0.199 0.896Benzo(a)pyrene 1 11/11/22 15:16 V26276JMV
<0.198 mg/Kg - dry 0.198 0.896Benzo(b)fluoranthene 1 11/11/22 15:16 V26276JMV
<0.184 mg/Kg - dry 0.184 0.896Benzo(g,h,i)perylene 1 11/11/22 15:16 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.186 mg/Kg - dry 0.186 0.896Benzo(k)fluoranthene 1 11/11/22 15:16 V26276JMV
<0.788 mg/Kg - dry 0.788 2.72Benzoic Acid 1 11/11/22 15:16 V26276JMV
<0.142 mg/Kg - dry 0.142 0.896Benzyl alcohol 1 11/11/22 15:16 V26276JMV
<0.160 mg/Kg - dry 0.160 0.896Bis(2-Chloroethoxy)methane 1 11/11/22 15:16 V26276JMV
<0.145 mg/Kg - dry 0.145 0.896Bis(2-Chloroethyl)ether 1 11/11/22 15:16 V26276JMV
<0.184 mg/Kg - dry 0.184 0.448Bis(2-Chloroisopropyl)ether 1 11/11/22 15:16 V26276JMV
<0.163 mg/Kg - dry 0.163 0.896Bis(2-ethylhexyl)phthalate 1 11/11/22 15:16 V26276JMV
<0.148 mg/Kg - dry 0.148 0.8964-Bromophenyl phenyl ether 1 11/11/22 15:16 V26276JMV
<0.153 mg/Kg - dry 0.153 0.448
Butyl benzyl phthalate 1 11/11/22 15:16 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8964-Chloro-3-methylphenol 1 11/11/22 15:16 V26276JMV
<0.152 mg/Kg - dry 0.152 0.4484-Chloroaniline 1 11/11/22 15:16 V26276JMV
<0.157 mg/Kg - dry 0.157 0.8962-Chloronaphthalene 1 11/11/22 15:16 V26276JMV
<0.133 mg/Kg - dry 0.133 0.8962-Chlorophenol 1 11/11/22 15:16 V26276JMV
<0.171 mg/Kg - dry 0.171 1.364-Chlorophenyl phenyl ether 1 11/11/22 15:16 V26276JMV
<0.192 mg/Kg - dry 0.192 0.896Chrysene 1 11/11/22 15:16 V26276JMV
<0.312 mg/Kg - dry 0.312 0.896
Dibenz(a,h)anthracene 1 11/11/22 15:16 V26276JMV
<0.161 mg/Kg - dry 0.161 0.896Dibenzofuran 1 11/11/22 15:16 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8961,2-Dichlorobenzene 1 11/11/22 15:16 V26276JMV
<0.132 mg/Kg - dry 0.132 0.8961,3-Dichlorobenzene 1 11/11/22 15:16 V26276JMV
<0.132 mg/Kg - dry 0.132 0.4481,4-Dichlorobenzene 1 11/11/22 15:16 V26276JMV
<0.199 mg/Kg - dry 0.199 0.8963,3'-Dichlorobenzidine 1 11/11/22 15:16 V26276JMV
<0.130 mg/Kg - dry 0.130 0.8962,4-Dichlorophenol 1 11/11/22 15:16 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.244 mg/Kg - dry 0.244 0.896Diethyl phthalate 1 11/11/22 15:16 V26276JMV
<0.236 mg/Kg - dry 0.236 0.896Dimethyl phthalate 1 11/11/22 15:16 V26276JMV
<0.146 mg/Kg - dry 0.146 0.4482,4-Dimethylphenol 1 11/11/22 15:16 V26276JMV
<0.145 mg/Kg - dry 0.145 0.896Di-n-butyl phthalate 1 11/11/22 15:16 V26276JMV
<0.326 mg/Kg - dry 0.326 2.044,6-Dinitro-2-methylphenol 1 11/11/22 15:16 V26276JMV
<0.706 mg/Kg - dry 0.706 2.042,4-Dinitrophenol 1 11/11/22 15:16 V26276JMV
<0.131 mg/Kg - dry 0.131 0.8962,4-Dinitrotoluene 1 11/11/22 15:16 V26276JMV
<0.146 mg/Kg - dry 0.146 0.8962,6-Dinitrotoluene 1 11/11/22 15:16 V26276JMV
<0.194 mg/Kg - dry 0.194 0.448
Di-n-Octyl Phthalate 1 11/11/22 15:16 V26276JMV
<0.167 mg/Kg - dry 0.167 0.896Fluoranthene 1 11/11/22 15:16 V26276JMV
<0.173 mg/Kg - dry 0.173 0.896Fluorene 1 11/11/22 15:16 V26276JMV
<0.144 mg/Kg - dry 0.144 0.896Hexachlorobenzene 1 11/11/22 15:16 V26276JMV
<0.132 mg/Kg - dry 0.132 0.896Hexachlorobutadiene 1 11/11/22 15:16 V26276JMV
<0.213 mg/Kg - dry 0.213 0.896Hexachlorocyclopentadiene 1 11/11/22 15:16 V26276JMV
<0.107 mg/Kg - dry 0.107 0.896Hexachloroethane 1 11/11/22 15:16 V26276JMV
<0.243 mg/Kg - dry 0.243 0.896
Indeno(1,2,3-cd)pyrene 1 11/11/22 15:16 V26276JMV
<0.259 mg/Kg - dry 0.259 0.896Isophorone 1 11/11/22 15:16 V26276JMV
<0.144 mg/Kg - dry 0.144 0.8961-Methylnaphthalene 1 11/11/22 15:16 V26276JMV
<0.135 mg/Kg - dry 0.135 0.8962-Methylnaphthalene 1 11/11/22 15:16 V26276JMV
<0.131 mg/Kg - dry 0.131 0.8962-Methylphenol 1 11/11/22 15:16 V26276JMV
<0.115 mg/Kg - dry 0.115 0.8963&4 Methylphenol 1 11/11/22 15:16 V26276JMV
<0.195 mg/Kg - dry 0.195 0.896Naphthalene 1 11/11/22 15:16 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-5
92344 Matrix:
11/2/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.131 mg/Kg - dry 0.131 0.8962-Nitroaniline 1 11/11/22 15:16 V26276JMV
<0.163 mg/Kg - dry 0.163 0.8963-Nitroaniline 1 11/11/22 15:16 V26276JMV
<0.126 mg/Kg - dry 0.126 0.4484-Nitroaniline 1 11/11/22 15:16 V26276JMV
<0.157 mg/Kg - dry 0.157 0.448Nitrobenzene 1 11/11/22 15:16 V26276JMV
<0.120 mg/Kg - dry 0.120 0.8962-Nitrophenol 1 11/11/22 15:16 V26276JMV
<0.158 mg/Kg - dry 0.158 0.8964-Nitrophenol 1 11/11/22 15:16 V26276JMV
<0.357 mg/Kg - dry 0.357 0.896N-Nitrosodimethylamine 1 11/11/22 15:16 V26276JMV
<0.245 mg/Kg - dry 0.245 0.896N-Nitrosodiphenylamine 1 11/11/22 15:16 V26276JMV
<0.160 mg/Kg - dry 0.160 0.896
N-Nitroso-di-n-propylamine 1 11/11/22 15:16 V26276JMV
<0.471 mg/Kg - dry 0.471 1.36Pentachlorophenol 1 11/11/22 15:16 V26276JMV
<0.282 mg/Kg - dry 0.282 0.896Phenanthrene 1 11/11/22 15:16 V26276JMV
<0.152 mg/Kg - dry 0.152 0.896Phenol 1 11/11/22 15:16 V26276JMV
<0.182 mg/Kg - dry 0.182 0.896Pyrene 1 11/11/22 15:16 V26276JMV
<0.107 mg/Kg - dry 0.107 0.448Pyridine 1 11/11/22 15:16 V26276JMV
<0.145 mg/Kg - dry 0.145 0.8961,2,4-Trichlorobenzene 1 11/11/22 15:16 V26276JMV
<0.130 mg/Kg - dry 0.130 0.896
2,4,5-Trichlorophenol 1 11/11/22 15:16 V26276JMV
<0.131 mg/Kg - dry 0.131 0.8962,4,6-Trichlorophenol 1 11/11/22 15:16 V26276JMV
8270ESurrogate: Phenol-d5 69.7 Limits: 34-121%11/11/22 15:161 JMV
Surrogate: 2-Fluorobiphenyl 86.7 Limits: 44-115%11/11/22 15:161 JMV V26276
Surrogate: 2-Fluorophenol 71.8 Limits: 35-115%11/11/22 15:161 JMV V26276
Surrogate: Nitrobenzene-d5 77.7 Limits: 37-122%11/11/22 15:161 JMV V26276
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%11/11/22 15:161 JMV V26276
Surrogate: 2,4,6-Tribromophenol 75.1 Limits: 39-132%11/11/22 15:161 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.4 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.184 mg/Kg - dry 0.184 0.261Chromium, Hexavalent 1 11/16/22 19:52 SW-7199SAR
1.67 mg/Kg - dry 0.112 0.326Arsenic 5 11/14/22 23:08 6020BBKN
53.9 mg/Kg - dry 0.055 0.326Barium 5 11/11/22 22:58 6020BBKN
0.0578 J mg/Kg - dry 0.0338 0.326Cadmium 5 11/14/22 23:08 6020BBKN
39.9 mg/Kg - dry 0.757 1.63
Chromium 25 11/14/22 23:13 6020BBKN
10.2 mg/Kg - dry 0.0404 0.326Lead 5 11/14/22 23:08 6020BBKN
0.102 mg/Kg - dry 0.0157 0.0392Mercury (Total)1 11/10/22 15:14 7471BEDV
0.755 mg/Kg - dry 0.134 0.326Selenium 5 11/14/22 23:08 6020BBKN
0.0268 J mg/Kg - dry 0.0087 0.326Silver 5 11/16/22 18:30 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
0.027 mg/Kg - dry 0.003 0.026Acetone 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/07/22 00:04 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/07/22 00:04 V25976TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/07/22 00:04 V25976TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/07/22 00:04 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/07/22 00:04 V25976TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/07/22 00:04 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/07/22 00:04 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/07/22 00:04 V25976TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/07/22 00:04 V25976TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/07/22 00:04 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/07/22 00:04 V25976TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/07/22 00:04 V25976TBL
<0.018 mg/Kg - dry 0.018 0.326Ethanol 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/07/22 00:04 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/07/22 00:04 V25976TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/07/22 00:04 V25976TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/07/22 00:04 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/07/22 00:04 V25976TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/07/22 00:04 V25976TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/07/22 00:04 V25976TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/07/22 00:04 V25976TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25975 11/06/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/07/22 00:04 V25976TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/07/22 00:04 V25976TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/07/22 00:04 V25976TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/07/22 00:04 V25976
Surrogate: 4-Bromofluorobenzene 111 Limits: 70-130%11/07/22 00:041 TBL V25976
Surrogate: Dibromofluoromethane 116 Limits: 84-123%11/07/22 00:041 TBL V25976
Surrogate: Toluene-d8 121 Limits: 76-129%11/07/22 00:041 TBL V25976
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.151 mg/Kg - dry 0.151 0.861Acenaphthene 1 11/11/22 15:38 V26276JMV
<0.137 mg/Kg - dry 0.137 0.861Acenaphthylene 1 11/11/22 15:38 V26276JMV
<0.198 mg/Kg - dry 0.198 0.861Aniline 1 11/11/22 15:38 V26276JMV
<0.186 mg/Kg - dry 0.186 0.861Anthracene 1 11/11/22 15:38 V26276JMV
<0.181 mg/Kg - dry 0.181 0.861
Benzo(a)anthracene 1 11/11/22 15:38 V26276JMV
<0.191 mg/Kg - dry 0.191 0.861Benzo(a)pyrene 1 11/11/22 15:38 V26276JMV
<0.190 mg/Kg - dry 0.190 0.861Benzo(b)fluoranthene 1 11/11/22 15:38 V26276JMV
<0.177 mg/Kg - dry 0.177 0.861Benzo(g,h,i)perylene 1 11/11/22 15:38 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.178 mg/Kg - dry 0.178 0.861Benzo(k)fluoranthene 1 11/11/22 15:38 V26276JMV
<0.757 mg/Kg - dry 0.757 2.61Benzoic Acid 1 11/11/22 15:38 V26276JMV
<0.137 mg/Kg - dry 0.137 0.861Benzyl alcohol 1 11/11/22 15:38 V26276JMV
<0.154 mg/Kg - dry 0.154 0.861Bis(2-Chloroethoxy)methane 1 11/11/22 15:38 V26276JMV
<0.139 mg/Kg - dry 0.139 0.861Bis(2-Chloroethyl)ether 1 11/11/22 15:38 V26276JMV
<0.177 mg/Kg - dry 0.177 0.430Bis(2-Chloroisopropyl)ether 1 11/11/22 15:38 V26276JMV
<0.156 mg/Kg - dry 0.156 0.861Bis(2-ethylhexyl)phthalate 1 11/11/22 15:38 V26276JMV
<0.142 mg/Kg - dry 0.142 0.8614-Bromophenyl phenyl ether 1 11/11/22 15:38 V26276JMV
<0.147 mg/Kg - dry 0.147 0.430
Butyl benzyl phthalate 1 11/11/22 15:38 V26276JMV
<0.120 mg/Kg - dry 0.120 0.8614-Chloro-3-methylphenol 1 11/11/22 15:38 V26276JMV
<0.146 mg/Kg - dry 0.146 0.4304-Chloroaniline 1 11/11/22 15:38 V26276JMV
<0.151 mg/Kg - dry 0.151 0.8612-Chloronaphthalene 1 11/11/22 15:38 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8612-Chlorophenol 1 11/11/22 15:38 V26276JMV
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 11/11/22 15:38 V26276JMV
<0.185 mg/Kg - dry 0.185 0.861Chrysene 1 11/11/22 15:38 V26276JMV
<0.300 mg/Kg - dry 0.300 0.861
Dibenz(a,h)anthracene 1 11/11/22 15:38 V26276JMV
<0.155 mg/Kg - dry 0.155 0.861Dibenzofuran 1 11/11/22 15:38 V26276JMV
<0.123 mg/Kg - dry 0.123 0.8611,2-Dichlorobenzene 1 11/11/22 15:38 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8611,3-Dichlorobenzene 1 11/11/22 15:38 V26276JMV
<0.127 mg/Kg - dry 0.127 0.4301,4-Dichlorobenzene 1 11/11/22 15:38 V26276JMV
<0.191 mg/Kg - dry 0.191 0.8613,3'-Dichlorobenzidine 1 11/11/22 15:38 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8612,4-Dichlorophenol 1 11/11/22 15:38 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.234 mg/Kg - dry 0.234 0.861Diethyl phthalate 1 11/11/22 15:38 V26276JMV
<0.227 mg/Kg - dry 0.227 0.861Dimethyl phthalate 1 11/11/22 15:38 V26276JMV
<0.140 mg/Kg - dry 0.140 0.4302,4-Dimethylphenol 1 11/11/22 15:38 V26276JMV
<0.139 mg/Kg - dry 0.139 0.861Di-n-butyl phthalate 1 11/11/22 15:38 V26276JMV
<0.313 mg/Kg - dry 0.313 1.964,6-Dinitro-2-methylphenol 1 11/11/22 15:38 V26276JMV
<0.678 mg/Kg - dry 0.678 1.962,4-Dinitrophenol 1 11/11/22 15:38 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8612,4-Dinitrotoluene 1 11/11/22 15:38 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8612,6-Dinitrotoluene 1 11/11/22 15:38 V26276JMV
<0.186 mg/Kg - dry 0.186 0.430
Di-n-Octyl Phthalate 1 11/11/22 15:38 V26276JMV
<0.160 mg/Kg - dry 0.160 0.861Fluoranthene 1 11/11/22 15:38 V26276JMV
<0.167 mg/Kg - dry 0.167 0.861Fluorene 1 11/11/22 15:38 V26276JMV
<0.138 mg/Kg - dry 0.138 0.861Hexachlorobenzene 1 11/11/22 15:38 V26276JMV
<0.127 mg/Kg - dry 0.127 0.861Hexachlorobutadiene 1 11/11/22 15:38 V26276JMV
<0.204 mg/Kg - dry 0.204 0.861Hexachlorocyclopentadiene 1 11/11/22 15:38 V26276JMV
<0.103 mg/Kg - dry 0.103 0.861Hexachloroethane 1 11/11/22 15:38 V26276JMV
<0.233 mg/Kg - dry 0.233 0.861
Indeno(1,2,3-cd)pyrene 1 11/11/22 15:38 V26276JMV
<0.249 mg/Kg - dry 0.249 0.861Isophorone 1 11/11/22 15:38 V26276JMV
<0.138 mg/Kg - dry 0.138 0.8611-Methylnaphthalene 1 11/11/22 15:38 V26276JMV
<0.130 mg/Kg - dry 0.130 0.8612-Methylnaphthalene 1 11/11/22 15:38 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8612-Methylphenol 1 11/11/22 15:38 V26276JMV
<0.110 mg/Kg - dry 0.110 0.8613&4 Methylphenol 1 11/11/22 15:38 V26276JMV
<0.187 mg/Kg - dry 0.187 0.861Naphthalene 1 11/11/22 15:38 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-6
92345 Matrix:
11/2/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.126 mg/Kg - dry 0.126 0.8612-Nitroaniline 1 11/11/22 15:38 V26276JMV
<0.156 mg/Kg - dry 0.156 0.8613-Nitroaniline 1 11/11/22 15:38 V26276JMV
<0.121 mg/Kg - dry 0.121 0.4304-Nitroaniline 1 11/11/22 15:38 V26276JMV
<0.151 mg/Kg - dry 0.151 0.430Nitrobenzene 1 11/11/22 15:38 V26276JMV
<0.115 mg/Kg - dry 0.115 0.8612-Nitrophenol 1 11/11/22 15:38 V26276JMV
<0.152 mg/Kg - dry 0.152 0.8614-Nitrophenol 1 11/11/22 15:38 V26276JMV
<0.343 mg/Kg - dry 0.343 0.861N-Nitrosodimethylamine 1 11/11/22 15:38 V26276JMV
<0.236 mg/Kg - dry 0.236 0.861N-Nitrosodiphenylamine 1 11/11/22 15:38 V26276JMV
<0.154 mg/Kg - dry 0.154 0.861
N-Nitroso-di-n-propylamine 1 11/11/22 15:38 V26276JMV
<0.453 mg/Kg - dry 0.453 1.31Pentachlorophenol 1 11/11/22 15:38 V26276JMV
<0.271 mg/Kg - dry 0.271 0.861Phenanthrene 1 11/11/22 15:38 V26276JMV
<0.146 mg/Kg - dry 0.146 0.861Phenol 1 11/11/22 15:38 V26276JMV
<0.174 mg/Kg - dry 0.174 0.861Pyrene 1 11/11/22 15:38 V26276JMV
<0.103 mg/Kg - dry 0.103 0.430Pyridine 1 11/11/22 15:38 V26276JMV
<0.139 mg/Kg - dry 0.139 0.8611,2,4-Trichlorobenzene 1 11/11/22 15:38 V26276JMV
<0.125 mg/Kg - dry 0.125 0.861
2,4,5-Trichlorophenol 1 11/11/22 15:38 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8612,4,6-Trichlorophenol 1 11/11/22 15:38 V26276JMV
8270ESurrogate: Phenol-d5 75.1 Limits: 34-121%11/11/22 15:381 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%11/11/22 15:381 JMV V26276
Surrogate: 2-Fluorophenol 80.5 Limits: 35-115%11/11/22 15:381 JMV V26276
Surrogate: Nitrobenzene-d5 87.4 Limits: 37-122%11/11/22 15:381 JMV V26276
Surrogate: 4-Terphenyl-d14 107 Limits: 54-127%11/11/22 15:381 JMV V26276
Surrogate: 2,4,6-Tribromophenol 80.8 Limits: 39-132%11/11/22 15:381 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.7 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.187 mg/Kg - dry 0.187 0.266Chromium, Hexavalent 1 11/16/22 11:29 SW-7199SAR
2.07 mg/Kg - dry 0.112 0.328Arsenic 5 11/14/22 23:18 6020BBKN
34.5 mg/Kg - dry 0.055 0.327Barium 5 11/11/22 23:02 6020BBKN
0.0627 J mg/Kg - dry 0.0339 0.328Cadmium 5 11/14/22 23:18 6020BBKN
36.6 mg/Kg - dry 0.760 1.64
Chromium 25 11/14/22 23:23 6020BBKN
11.6 mg/Kg - dry 0.0406 0.328Lead 5 11/14/22 23:18 6020BBKN
0.105 mg/Kg - dry 0.0157 0.0393Mercury (Total)1 11/10/22 15:17 7471BEDV
0.727 mg/Kg - dry 0.134 0.327Selenium 5 11/14/22 23:18 6020BBKN
0.0190 J mg/Kg - dry 0.0088 0.328Silver 5 11/16/22 18:35 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.031 mg/Kg - dry 0.003 0.026Acetone 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/08/22 20:34 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 20:34 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/08/22 20:34 V26116TBL
0.004 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/08/22 20:34 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 20:34 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 20:34 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 20:34 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 20:34 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/08/22 20:34 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 20:34 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 20:34 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 20:34 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 20:34 V26116TBL
<0.018 mg/Kg - dry 0.018 0.327Ethanol 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/08/22 20:34 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 20:34 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 20:34 V26116TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 20:34 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 20:34 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/08/22 20:34 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 20:34 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/08/22 20:34 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/08/22 20:34 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/08/22 20:34 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/08/22 20:34 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/08/22 20:34 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/08/22 20:34 V26116
Surrogate: 4-Bromofluorobenzene 99.3 Limits: 70-130%11/08/22 20:341 TBL V26116
Surrogate: Dibromofluoromethane 101 Limits: 84-123%11/08/22 20:341 TBL V26116
Surrogate: Toluene-d8 99.5 Limits: 76-129%11/08/22 20:341 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.152 mg/Kg - dry 0.152 0.865Acenaphthene 1 11/11/22 16:01 V26276JMV
<0.137 mg/Kg - dry 0.137 0.865Acenaphthylene 1 11/11/22 16:01 V26276JMV
<0.199 mg/Kg - dry 0.199 0.865Aniline 1 11/11/22 16:01 V26276JMV
<0.187 mg/Kg - dry 0.187 0.865Anthracene 1 11/11/22 16:01 V26276JMV
<0.182 mg/Kg - dry 0.182 0.865
Benzo(a)anthracene 1 11/11/22 16:01 V26276JMV
<0.192 mg/Kg - dry 0.192 0.865Benzo(a)pyrene 1 11/11/22 16:01 V26276JMV
<0.191 mg/Kg - dry 0.191 0.865Benzo(b)fluoranthene 1 11/11/22 16:01 V26276JMV
<0.178 mg/Kg - dry 0.178 0.865Benzo(g,h,i)perylene 1 11/11/22 16:01 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.179 mg/Kg - dry 0.179 0.865Benzo(k)fluoranthene 1 11/11/22 16:01 V26276JMV
<0.760 mg/Kg - dry 0.760 2.62Benzoic Acid 1 11/11/22 16:01 V26276JMV
<0.137 mg/Kg - dry 0.137 0.865Benzyl alcohol 1 11/11/22 16:01 V26276JMV
<0.154 mg/Kg - dry 0.154 0.865Bis(2-Chloroethoxy)methane 1 11/11/22 16:01 V26276JMV
<0.140 mg/Kg - dry 0.140 0.865Bis(2-Chloroethyl)ether 1 11/11/22 16:01 V26276JMV
<0.178 mg/Kg - dry 0.178 0.432Bis(2-Chloroisopropyl)ether 1 11/11/22 16:01 V26276JMV
<0.157 mg/Kg - dry 0.157 0.865Bis(2-ethylhexyl)phthalate 1 11/11/22 16:01 V26276JMV
<0.142 mg/Kg - dry 0.142 0.8654-Bromophenyl phenyl ether 1 11/11/22 16:01 V26276JMV
<0.148 mg/Kg - dry 0.148 0.432
Butyl benzyl phthalate 1 11/11/22 16:01 V26276JMV
<0.121 mg/Kg - dry 0.121 0.8654-Chloro-3-methylphenol 1 11/11/22 16:01 V26276JMV
<0.146 mg/Kg - dry 0.146 0.4324-Chloroaniline 1 11/11/22 16:01 V26276JMV
<0.152 mg/Kg - dry 0.152 0.8652-Chloronaphthalene 1 11/11/22 16:01 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8652-Chlorophenol 1 11/11/22 16:01 V26276JMV
<0.165 mg/Kg - dry 0.165 1.314-Chlorophenyl phenyl ether 1 11/11/22 16:01 V26276JMV
<0.186 mg/Kg - dry 0.186 0.865Chrysene 1 11/11/22 16:01 V26276JMV
<0.301 mg/Kg - dry 0.301 0.865
Dibenz(a,h)anthracene 1 11/11/22 16:01 V26276JMV
<0.155 mg/Kg - dry 0.155 0.865Dibenzofuran 1 11/11/22 16:01 V26276JMV
<0.123 mg/Kg - dry 0.123 0.8651,2-Dichlorobenzene 1 11/11/22 16:01 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8651,3-Dichlorobenzene 1 11/11/22 16:01 V26276JMV
<0.127 mg/Kg - dry 0.127 0.4321,4-Dichlorobenzene 1 11/11/22 16:01 V26276JMV
<0.192 mg/Kg - dry 0.192 0.8653,3'-Dichlorobenzidine 1 11/11/22 16:01 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8652,4-Dichlorophenol 1 11/11/22 16:01 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.235 mg/Kg - dry 0.235 0.865Diethyl phthalate 1 11/11/22 16:01 V26276JMV
<0.228 mg/Kg - dry 0.228 0.865Dimethyl phthalate 1 11/11/22 16:01 V26276JMV
<0.141 mg/Kg - dry 0.141 0.4322,4-Dimethylphenol 1 11/11/22 16:01 V26276JMV
<0.140 mg/Kg - dry 0.140 0.865Di-n-butyl phthalate 1 11/11/22 16:01 V26276JMV
<0.314 mg/Kg - dry 0.314 1.974,6-Dinitro-2-methylphenol 1 11/11/22 16:01 V26276JMV
<0.681 mg/Kg - dry 0.681 1.972,4-Dinitrophenol 1 11/11/22 16:01 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8652,4-Dinitrotoluene 1 11/11/22 16:01 V26276JMV
<0.141 mg/Kg - dry 0.141 0.8652,6-Dinitrotoluene 1 11/11/22 16:01 V26276JMV
<0.187 mg/Kg - dry 0.187 0.432
Di-n-Octyl Phthalate 1 11/11/22 16:01 V26276JMV
<0.161 mg/Kg - dry 0.161 0.865Fluoranthene 1 11/11/22 16:01 V26276JMV
<0.167 mg/Kg - dry 0.167 0.865Fluorene 1 11/11/22 16:01 V26276JMV
<0.138 mg/Kg - dry 0.138 0.865Hexachlorobenzene 1 11/11/22 16:01 V26276JMV
<0.127 mg/Kg - dry 0.127 0.865Hexachlorobutadiene 1 11/11/22 16:01 V26276JMV
<0.205 mg/Kg - dry 0.205 0.865Hexachlorocyclopentadiene 1 11/11/22 16:01 V26276JMV
<0.103 mg/Kg - dry 0.103 0.865Hexachloroethane 1 11/11/22 16:01 V26276JMV
<0.234 mg/Kg - dry 0.234 0.865
Indeno(1,2,3-cd)pyrene 1 11/11/22 16:01 V26276JMV
<0.250 mg/Kg - dry 0.250 0.865Isophorone 1 11/11/22 16:01 V26276JMV
<0.138 mg/Kg - dry 0.138 0.8651-Methylnaphthalene 1 11/11/22 16:01 V26276JMV
<0.131 mg/Kg - dry 0.131 0.8652-Methylnaphthalene 1 11/11/22 16:01 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8652-Methylphenol 1 11/11/22 16:01 V26276JMV
<0.111 mg/Kg - dry 0.111 0.8653&4 Methylphenol 1 11/11/22 16:01 V26276JMV
<0.188 mg/Kg - dry 0.188 0.865Naphthalene 1 11/11/22 16:01 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-7
92346 Matrix:
11/2/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.126 mg/Kg - dry 0.126 0.8652-Nitroaniline 1 11/11/22 16:01 V26276JMV
<0.157 mg/Kg - dry 0.157 0.8653-Nitroaniline 1 11/11/22 16:01 V26276JMV
<0.122 mg/Kg - dry 0.122 0.4324-Nitroaniline 1 11/11/22 16:01 V26276JMV
<0.152 mg/Kg - dry 0.152 0.432Nitrobenzene 1 11/11/22 16:01 V26276JMV
<0.116 mg/Kg - dry 0.116 0.8652-Nitrophenol 1 11/11/22 16:01 V26276JMV
<0.153 mg/Kg - dry 0.153 0.8654-Nitrophenol 1 11/11/22 16:01 V26276JMV
<0.344 mg/Kg - dry 0.344 0.865N-Nitrosodimethylamine 1 11/11/22 16:01 V26276JMV
<0.237 mg/Kg - dry 0.237 0.865N-Nitrosodiphenylamine 1 11/11/22 16:01 V26276JMV
<0.154 mg/Kg - dry 0.154 0.865
N-Nitroso-di-n-propylamine 1 11/11/22 16:01 V26276JMV
<0.454 mg/Kg - dry 0.454 1.31Pentachlorophenol 1 11/11/22 16:01 V26276JMV
<0.272 mg/Kg - dry 0.272 0.865Phenanthrene 1 11/11/22 16:01 V26276JMV
<0.146 mg/Kg - dry 0.146 0.865Phenol 1 11/11/22 16:01 V26276JMV
<0.175 mg/Kg - dry 0.175 0.865Pyrene 1 11/11/22 16:01 V26276JMV
<0.103 mg/Kg - dry 0.103 0.432Pyridine 1 11/11/22 16:01 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8651,2,4-Trichlorobenzene 1 11/11/22 16:01 V26276JMV
<0.126 mg/Kg - dry 0.126 0.865
2,4,5-Trichlorophenol 1 11/11/22 16:01 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8652,4,6-Trichlorophenol 1 11/11/22 16:01 V26276JMV
8270ESurrogate: Phenol-d5 79.6 Limits: 34-121%11/11/22 16:011 JMV
Surrogate: 2-Fluorobiphenyl 102 Limits: 44-115%11/11/22 16:011 JMV V26276
Surrogate: 2-Fluorophenol 85.0 Limits: 35-115%11/11/22 16:011 JMV V26276
Surrogate: Nitrobenzene-d5 95.2 Limits: 37-122%11/11/22 16:011 JMV V26276
Surrogate: 4-Terphenyl-d14 113 Limits: 54-127%11/11/22 16:011 JMV V26276
Surrogate: 2,4,6-Tribromophenol 79.9 Limits: 39-132%11/11/22 16:011 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.0 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.178 mg/Kg - dry 0.178 0.253Chromium, Hexavalent 1 11/16/22 12:13 SW-7199SAR
1.35 mg/Kg - dry 0.108 0.316Arsenic 5 11/14/22 23:28 6020BBKN
49.0 mg/Kg - dry 0.054 0.316Barium 5 11/11/22 23:07 6020BBKN
0.0502 J mg/Kg - dry 0.0327 0.316Cadmium 5 11/14/22 23:28 6020BBKN
42.5 mg/Kg - dry 0.734 1.58
Chromium 25 11/14/22 23:33 6020BBKN
8.62 mg/Kg - dry 0.0392 0.316Lead 5 11/14/22 23:28 6020BBKN
0.102 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 11/10/22 15:19 7471BEDV
0.621 mg/Kg - dry 0.130 0.316Selenium 5 11/14/22 23:28 6020BBKN
0.0198 J mg/Kg - dry 0.0085 0.316Silver 5 11/16/22 18:40 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.028 mg/Kg - dry 0.003 0.025Acetone 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/08/22 21:01 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 21:01 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/08/22 21:01 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/08/22 21:01 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 21:01 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 21:01 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/08/22 21:01 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 21:01 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 21:01 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 21:01 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 21:01 V26116TBL
<0.017 mg/Kg - dry 0.017 0.316Ethanol 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/08/22 21:01 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 21:01 V26116TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 21:01 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/08/22 21:01 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 21:01 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/08/22 21:01 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/08/22 21:01 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/08/22 21:01 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/08/22 21:01 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/08/22 21:01 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/08/22 21:01 V26116
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%11/08/22 21:011 TBL V26116
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/08/22 21:011 TBL V26116
Surrogate: Toluene-d8 102 Limits: 76-129%11/08/22 21:011 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.146 mg/Kg - dry 0.146 0.835Acenaphthene 1 11/11/22 16:23 V26276JMV
<0.132 mg/Kg - dry 0.132 0.835Acenaphthylene 1 11/11/22 16:23 V26276JMV
<0.192 mg/Kg - dry 0.192 0.835Aniline 1 11/11/22 16:23 V26276JMV
<0.181 mg/Kg - dry 0.181 0.835Anthracene 1 11/11/22 16:23 V26276JMV
<0.175 mg/Kg - dry 0.175 0.835
Benzo(a)anthracene 1 11/11/22 16:23 V26276JMV
<0.186 mg/Kg - dry 0.186 0.835Benzo(a)pyrene 1 11/11/22 16:23 V26276JMV
<0.184 mg/Kg - dry 0.184 0.835Benzo(b)fluoranthene 1 11/11/22 16:23 V26276JMV
<0.172 mg/Kg - dry 0.172 0.835Benzo(g,h,i)perylene 1 11/11/22 16:23 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.173 mg/Kg - dry 0.173 0.835Benzo(k)fluoranthene 1 11/11/22 16:23 V26276JMV
<0.734 mg/Kg - dry 0.734 2.53Benzoic Acid 1 11/11/22 16:23 V26276JMV
<0.132 mg/Kg - dry 0.132 0.835Benzyl alcohol 1 11/11/22 16:23 V26276JMV
<0.149 mg/Kg - dry 0.149 0.835Bis(2-Chloroethoxy)methane 1 11/11/22 16:23 V26276JMV
<0.135 mg/Kg - dry 0.135 0.835Bis(2-Chloroethyl)ether 1 11/11/22 16:23 V26276JMV
<0.172 mg/Kg - dry 0.172 0.417Bis(2-Chloroisopropyl)ether 1 11/11/22 16:23 V26276JMV
<0.151 mg/Kg - dry 0.151 0.835Bis(2-ethylhexyl)phthalate 1 11/11/22 16:23 V26276JMV
<0.137 mg/Kg - dry 0.137 0.8354-Bromophenyl phenyl ether 1 11/11/22 16:23 V26276JMV
<0.143 mg/Kg - dry 0.143 0.417
Butyl benzyl phthalate 1 11/11/22 16:23 V26276JMV
<0.116 mg/Kg - dry 0.116 0.8354-Chloro-3-methylphenol 1 11/11/22 16:23 V26276JMV
<0.141 mg/Kg - dry 0.141 0.4174-Chloroaniline 1 11/11/22 16:23 V26276JMV
<0.146 mg/Kg - dry 0.146 0.8352-Chloronaphthalene 1 11/11/22 16:23 V26276JMV
<0.124 mg/Kg - dry 0.124 0.8352-Chlorophenol 1 11/11/22 16:23 V26276JMV
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 11/11/22 16:23 V26276JMV
<0.179 mg/Kg - dry 0.179 0.835Chrysene 1 11/11/22 16:23 V26276JMV
<0.291 mg/Kg - dry 0.291 0.835
Dibenz(a,h)anthracene 1 11/11/22 16:23 V26276JMV
<0.150 mg/Kg - dry 0.150 0.835Dibenzofuran 1 11/11/22 16:23 V26276JMV
<0.119 mg/Kg - dry 0.119 0.8351,2-Dichlorobenzene 1 11/11/22 16:23 V26276JMV
<0.123 mg/Kg - dry 0.123 0.8351,3-Dichlorobenzene 1 11/11/22 16:23 V26276JMV
<0.123 mg/Kg - dry 0.123 0.4171,4-Dichlorobenzene 1 11/11/22 16:23 V26276JMV
<0.186 mg/Kg - dry 0.186 0.8353,3'-Dichlorobenzidine 1 11/11/22 16:23 V26276JMV
<0.121 mg/Kg - dry 0.121 0.8352,4-Dichlorophenol 1 11/11/22 16:23 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.227 mg/Kg - dry 0.227 0.835Diethyl phthalate 1 11/11/22 16:23 V26276JMV
<0.220 mg/Kg - dry 0.220 0.835Dimethyl phthalate 1 11/11/22 16:23 V26276JMV
<0.136 mg/Kg - dry 0.136 0.4172,4-Dimethylphenol 1 11/11/22 16:23 V26276JMV
<0.135 mg/Kg - dry 0.135 0.835Di-n-butyl phthalate 1 11/11/22 16:23 V26276JMV
<0.303 mg/Kg - dry 0.303 1.904,6-Dinitro-2-methylphenol 1 11/11/22 16:23 V26276JMV
<0.658 mg/Kg - dry 0.658 1.902,4-Dinitrophenol 1 11/11/22 16:23 V26276JMV
<0.122 mg/Kg - dry 0.122 0.8352,4-Dinitrotoluene 1 11/11/22 16:23 V26276JMV
<0.136 mg/Kg - dry 0.136 0.8352,6-Dinitrotoluene 1 11/11/22 16:23 V26276JMV
<0.181 mg/Kg - dry 0.181 0.417
Di-n-Octyl Phthalate 1 11/11/22 16:23 V26276JMV
<0.155 mg/Kg - dry 0.155 0.835Fluoranthene 1 11/11/22 16:23 V26276JMV
<0.162 mg/Kg - dry 0.162 0.835Fluorene 1 11/11/22 16:23 V26276JMV
<0.134 mg/Kg - dry 0.134 0.835Hexachlorobenzene 1 11/11/22 16:23 V26276JMV
<0.123 mg/Kg - dry 0.123 0.835Hexachlorobutadiene 1 11/11/22 16:23 V26276JMV
<0.198 mg/Kg - dry 0.198 0.835Hexachlorocyclopentadiene 1 11/11/22 16:23 V26276JMV
<0.100 mg/Kg - dry 0.100 0.835Hexachloroethane 1 11/11/22 16:23 V26276JMV
<0.226 mg/Kg - dry 0.226 0.835
Indeno(1,2,3-cd)pyrene 1 11/11/22 16:23 V26276JMV
<0.241 mg/Kg - dry 0.241 0.835Isophorone 1 11/11/22 16:23 V26276JMV
<0.134 mg/Kg - dry 0.134 0.8351-Methylnaphthalene 1 11/11/22 16:23 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8352-Methylnaphthalene 1 11/11/22 16:23 V26276JMV
<0.122 mg/Kg - dry 0.122 0.8352-Methylphenol 1 11/11/22 16:23 V26276JMV
<0.107 mg/Kg - dry 0.107 0.8353&4 Methylphenol 1 11/11/22 16:23 V26276JMV
<0.182 mg/Kg - dry 0.182 0.835Naphthalene 1 11/11/22 16:23 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-8
92347 Matrix:
11/2/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.122 mg/Kg - dry 0.122 0.8352-Nitroaniline 1 11/11/22 16:23 V26276JMV
<0.151 mg/Kg - dry 0.151 0.8353-Nitroaniline 1 11/11/22 16:23 V26276JMV
<0.118 mg/Kg - dry 0.118 0.4174-Nitroaniline 1 11/11/22 16:23 V26276JMV
<0.146 mg/Kg - dry 0.146 0.417Nitrobenzene 1 11/11/22 16:23 V26276JMV
<0.112 mg/Kg - dry 0.112 0.8352-Nitrophenol 1 11/11/22 16:23 V26276JMV
<0.148 mg/Kg - dry 0.148 0.8354-Nitrophenol 1 11/11/22 16:23 V26276JMV
<0.332 mg/Kg - dry 0.332 0.835N-Nitrosodimethylamine 1 11/11/22 16:23 V26276JMV
<0.229 mg/Kg - dry 0.229 0.835N-Nitrosodiphenylamine 1 11/11/22 16:23 V26276JMV
<0.149 mg/Kg - dry 0.149 0.835
N-Nitroso-di-n-propylamine 1 11/11/22 16:23 V26276JMV
<0.439 mg/Kg - dry 0.439 1.27Pentachlorophenol 1 11/11/22 16:23 V26276JMV
<0.263 mg/Kg - dry 0.263 0.835Phenanthrene 1 11/11/22 16:23 V26276JMV
<0.141 mg/Kg - dry 0.141 0.835Phenol 1 11/11/22 16:23 V26276JMV
<0.169 mg/Kg - dry 0.169 0.835Pyrene 1 11/11/22 16:23 V26276JMV
<0.100 mg/Kg - dry 0.100 0.417Pyridine 1 11/11/22 16:23 V26276JMV
<0.135 mg/Kg - dry 0.135 0.8351,2,4-Trichlorobenzene 1 11/11/22 16:23 V26276JMV
<0.121 mg/Kg - dry 0.121 0.835
2,4,5-Trichlorophenol 1 11/11/22 16:23 V26276JMV
<0.122 mg/Kg - dry 0.122 0.8352,4,6-Trichlorophenol 1 11/11/22 16:23 V26276JMV
8270ESurrogate: Phenol-d5 81.1 Limits: 34-121%11/11/22 16:231 JMV
Surrogate: 2-Fluorobiphenyl 102 Limits: 44-115%11/11/22 16:231 JMV V26276
Surrogate: 2-Fluorophenol 86.5 Limits: 35-115%11/11/22 16:231 JMV V26276
Surrogate: Nitrobenzene-d5 96.4 Limits: 37-122%11/11/22 16:231 JMV V26276
Surrogate: 4-Terphenyl-d14 113 Limits: 54-127%11/11/22 16:231 JMV V26276
Surrogate: 2,4,6-Tribromophenol 80.8 Limits: 39-132%11/11/22 16:231 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.1 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.196 mg/Kg - dry 0.196 0.278Chromium, Hexavalent 1 11/16/22 14:17 SW-7199SAR
1.74 mg/Kg - dry 0.119 0.348Arsenic 5 11/14/22 23:37 6020BBKN
60.6 mg/Kg - dry 0.059 0.347Barium 5 11/11/22 23:11 6020BBKN
0.0897 J mg/Kg - dry 0.0360 0.348Cadmium 5 11/14/22 23:37 6020BBKN
43.8 mg/Kg - dry 0.806 1.74
Chromium 25 11/14/22 23:43 6020BBKN
13.4 mg/Kg - dry 0.0431 0.348Lead 5 11/14/22 23:37 6020BBKN
0.153 mg/Kg - dry 0.0167 0.0417Mercury (Total)1 11/10/22 15:22 7471BEDV
0.721 mg/Kg - dry 0.143 0.347Selenium 5 11/14/22 23:37 6020BBKN
0.0235 J mg/Kg - dry 0.0093 0.348Silver 5 11/16/22 18:46 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.025 J mg/Kg - dry 0.003 0.027Acetone 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 21:29 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 11/08/22 21:29 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 21:29 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 21:29 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 11/08/22 21:29 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 21:29 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 21:29 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 21:29 V26116TBL
<0.019 mg/Kg - dry 0.019 0.347Ethanol 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/08/22 21:29 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 11/08/22 21:29 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 21:29 V26116TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 11/08/22 21:29 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 21:29 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.013
1,2,3-Trichlorobenzene 1 11/08/22 21:29 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 11/08/22 21:29 V26116TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 21:29 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 11/08/22 21:29 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 11/08/22 21:29 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 11/08/22 21:29 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/08/22 21:29 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/08/22 21:29 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/08/22 21:29 V26116
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%11/08/22 21:291 TBL V26116
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/08/22 21:291 TBL V26116
Surrogate: Toluene-d8 100 Limits: 76-129%11/08/22 21:291 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.161 mg/Kg - dry 0.161 0.917Acenaphthene 1 11/11/22 16:46 V26276JMV
<0.146 mg/Kg - dry 0.146 0.917Acenaphthylene 1 11/11/22 16:46 V26276JMV
<0.211 mg/Kg - dry 0.211 0.917Aniline 1 11/11/22 16:46 V26276JMV
<0.198 mg/Kg - dry 0.198 0.917Anthracene 1 11/11/22 16:46 V26276JMV
<0.193 mg/Kg - dry 0.193 0.917
Benzo(a)anthracene 1 11/11/22 16:46 V26276JMV
<0.204 mg/Kg - dry 0.204 0.917Benzo(a)pyrene 1 11/11/22 16:46 V26276JMV
<0.203 mg/Kg - dry 0.203 0.917Benzo(b)fluoranthene 1 11/11/22 16:46 V26276JMV
<0.189 mg/Kg - dry 0.189 0.917Benzo(g,h,i)perylene 1 11/11/22 16:46 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.190 mg/Kg - dry 0.190 0.917Benzo(k)fluoranthene 1 11/11/22 16:46 V26276JMV
<0.806 mg/Kg - dry 0.806 2.78Benzoic Acid 1 11/11/22 16:46 V26276JMV
<0.146 mg/Kg - dry 0.146 0.917Benzyl alcohol 1 11/11/22 16:46 V26276JMV
<0.164 mg/Kg - dry 0.164 0.917Bis(2-Chloroethoxy)methane 1 11/11/22 16:46 V26276JMV
<0.148 mg/Kg - dry 0.148 0.917Bis(2-Chloroethyl)ether 1 11/11/22 16:46 V26276JMV
<0.189 mg/Kg - dry 0.189 0.458Bis(2-Chloroisopropyl)ether 1 11/11/22 16:46 V26276JMV
<0.166 mg/Kg - dry 0.166 0.917Bis(2-ethylhexyl)phthalate 1 11/11/22 16:46 V26276JMV
<0.151 mg/Kg - dry 0.151 0.9174-Bromophenyl phenyl ether 1 11/11/22 16:46 V26276JMV
<0.157 mg/Kg - dry 0.157 0.458
Butyl benzyl phthalate 1 11/11/22 16:46 V26276JMV
<0.128 mg/Kg - dry 0.128 0.9174-Chloro-3-methylphenol 1 11/11/22 16:46 V26276JMV
<0.155 mg/Kg - dry 0.155 0.4584-Chloroaniline 1 11/11/22 16:46 V26276JMV
<0.161 mg/Kg - dry 0.161 0.9172-Chloronaphthalene 1 11/11/22 16:46 V26276JMV
<0.136 mg/Kg - dry 0.136 0.9172-Chlorophenol 1 11/11/22 16:46 V26276JMV
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 11/11/22 16:46 V26276JMV
<0.197 mg/Kg - dry 0.197 0.917Chrysene 1 11/11/22 16:46 V26276JMV
<0.319 mg/Kg - dry 0.319 0.917
Dibenz(a,h)anthracene 1 11/11/22 16:46 V26276JMV
<0.165 mg/Kg - dry 0.165 0.917Dibenzofuran 1 11/11/22 16:46 V26276JMV
<0.131 mg/Kg - dry 0.131 0.9171,2-Dichlorobenzene 1 11/11/22 16:46 V26276JMV
<0.135 mg/Kg - dry 0.135 0.9171,3-Dichlorobenzene 1 11/11/22 16:46 V26276JMV
<0.135 mg/Kg - dry 0.135 0.4581,4-Dichlorobenzene 1 11/11/22 16:46 V26276JMV
<0.204 mg/Kg - dry 0.204 0.9173,3'-Dichlorobenzidine 1 11/11/22 16:46 V26276JMV
<0.133 mg/Kg - dry 0.133 0.9172,4-Dichlorophenol 1 11/11/22 16:46 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.250 mg/Kg - dry 0.250 0.917Diethyl phthalate 1 11/11/22 16:46 V26276JMV
<0.242 mg/Kg - dry 0.242 0.917Dimethyl phthalate 1 11/11/22 16:46 V26276JMV
<0.150 mg/Kg - dry 0.150 0.4582,4-Dimethylphenol 1 11/11/22 16:46 V26276JMV
<0.148 mg/Kg - dry 0.148 0.917Di-n-butyl phthalate 1 11/11/22 16:46 V26276JMV
<0.333 mg/Kg - dry 0.333 2.094,6-Dinitro-2-methylphenol 1 11/11/22 16:46 V26276JMV
<0.723 mg/Kg - dry 0.723 2.092,4-Dinitrophenol 1 11/11/22 16:46 V26276JMV
<0.134 mg/Kg - dry 0.134 0.9172,4-Dinitrotoluene 1 11/11/22 16:46 V26276JMV
<0.150 mg/Kg - dry 0.150 0.9172,6-Dinitrotoluene 1 11/11/22 16:46 V26276JMV
<0.198 mg/Kg - dry 0.198 0.458
Di-n-Octyl Phthalate 1 11/11/22 16:46 V26276JMV
<0.171 mg/Kg - dry 0.171 0.917Fluoranthene 1 11/11/22 16:46 V26276JMV
<0.178 mg/Kg - dry 0.178 0.917Fluorene 1 11/11/22 16:46 V26276JMV
<0.147 mg/Kg - dry 0.147 0.917Hexachlorobenzene 1 11/11/22 16:46 V26276JMV
<0.135 mg/Kg - dry 0.135 0.917Hexachlorobutadiene 1 11/11/22 16:46 V26276JMV
<0.218 mg/Kg - dry 0.218 0.917Hexachlorocyclopentadiene 1 11/11/22 16:46 V26276JMV
<0.110 mg/Kg - dry 0.110 0.917Hexachloroethane 1 11/11/22 16:46 V26276JMV
<0.248 mg/Kg - dry 0.248 0.917
Indeno(1,2,3-cd)pyrene 1 11/11/22 16:46 V26276JMV
<0.265 mg/Kg - dry 0.265 0.917Isophorone 1 11/11/22 16:46 V26276JMV
<0.147 mg/Kg - dry 0.147 0.9171-Methylnaphthalene 1 11/11/22 16:46 V26276JMV
<0.139 mg/Kg - dry 0.139 0.9172-Methylnaphthalene 1 11/11/22 16:46 V26276JMV
<0.134 mg/Kg - dry 0.134 0.9172-Methylphenol 1 11/11/22 16:46 V26276JMV
<0.118 mg/Kg - dry 0.118 0.9173&4 Methylphenol 1 11/11/22 16:46 V26276JMV
<0.200 mg/Kg - dry 0.200 0.917Naphthalene 1 11/11/22 16:46 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-9
92348 Matrix:
11/2/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.134 mg/Kg - dry 0.134 0.9172-Nitroaniline 1 11/11/22 16:46 V26276JMV
<0.166 mg/Kg - dry 0.166 0.9173-Nitroaniline 1 11/11/22 16:46 V26276JMV
<0.129 mg/Kg - dry 0.129 0.4584-Nitroaniline 1 11/11/22 16:46 V26276JMV
<0.161 mg/Kg - dry 0.161 0.458Nitrobenzene 1 11/11/22 16:46 V26276JMV
<0.123 mg/Kg - dry 0.123 0.9172-Nitrophenol 1 11/11/22 16:46 V26276JMV
<0.162 mg/Kg - dry 0.162 0.9174-Nitrophenol 1 11/11/22 16:46 V26276JMV
<0.365 mg/Kg - dry 0.365 0.917N-Nitrosodimethylamine 1 11/11/22 16:46 V26276JMV
<0.251 mg/Kg - dry 0.251 0.917N-Nitrosodiphenylamine 1 11/11/22 16:46 V26276JMV
<0.164 mg/Kg - dry 0.164 0.917
N-Nitroso-di-n-propylamine 1 11/11/22 16:46 V26276JMV
<0.482 mg/Kg - dry 0.482 1.39Pentachlorophenol 1 11/11/22 16:46 V26276JMV
<0.289 mg/Kg - dry 0.289 0.917Phenanthrene 1 11/11/22 16:46 V26276JMV
<0.155 mg/Kg - dry 0.155 0.917Phenol 1 11/11/22 16:46 V26276JMV
<0.186 mg/Kg - dry 0.186 0.917Pyrene 1 11/11/22 16:46 V26276JMV
<0.110 mg/Kg - dry 0.110 0.458Pyridine 1 11/11/22 16:46 V26276JMV
<0.148 mg/Kg - dry 0.148 0.9171,2,4-Trichlorobenzene 1 11/11/22 16:46 V26276JMV
<0.133 mg/Kg - dry 0.133 0.917
2,4,5-Trichlorophenol 1 11/11/22 16:46 V26276JMV
<0.134 mg/Kg - dry 0.134 0.9172,4,6-Trichlorophenol 1 11/11/22 16:46 V26276JMV
8270ESurrogate: Phenol-d5 62.8 Limits: 34-121%11/11/22 16:461 JMV
Surrogate: 2-Fluorobiphenyl 81.3 Limits: 44-115%11/11/22 16:461 JMV V26276
Surrogate: 2-Fluorophenol 66.4 Limits: 35-115%11/11/22 16:461 JMV V26276
Surrogate: Nitrobenzene-d5 72.3 Limits: 37-122%11/11/22 16:461 JMV V26276
Surrogate: 4-Terphenyl-d14 89.8 Limits: 54-127%11/11/22 16:461 JMV V26276
Surrogate: 2,4,6-Tribromophenol 66.1 Limits: 39-132%11/11/22 16:461 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.6 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.188 mg/Kg - dry 0.188 0.267Chromium, Hexavalent 1 11/16/22 14:27 SW-7199SAR
0.844 mg/Kg - dry 0.113 0.332Arsenic 5 11/14/22 23:47 6020BBKN
90.3 mg/Kg - dry 0.056 0.331Barium 5 11/11/22 23:15 6020BBKN
0.0953 J mg/Kg - dry 0.0343 0.332Cadmium 5 11/14/22 23:47 6020BBKN
48.8 mg/Kg - dry 0.769 1.66
Chromium 25 11/14/22 23:53 6020BBKN
4.88 mg/Kg - dry 0.0411 0.332Lead 5 11/14/22 23:47 6020BBKN
0.0960 mg/Kg - dry 0.0159 0.0398Mercury (Total)1 11/10/22 15:24 7471BEDV
0.473 mg/Kg - dry 0.136 0.331Selenium 5 11/14/22 23:47 6020BBKN
0.0224 J mg/Kg - dry 0.0089 0.332Silver 5 11/16/22 18:51 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.042 mg/Kg - dry 0.003 0.026Acetone 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/08/22 21:56 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 21:56 V26116TBL
0.002 J
mg/Kg - dry 0.002 0.013
Bromomethane 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/08/22 21:56 V26116TBL
0.001 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/08/22 21:56 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 21:56 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 21:56 V26116TBL
0.001 J mg/Kg - dry 0.0008 0.013Chloromethane 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 21:56 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 21:56 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 21:56 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/08/22 21:56 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 21:56 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 21:56 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 21:56 V26116TBL
<0.018 mg/Kg - dry 0.018 0.331Ethanol 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/08/22 21:56 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 21:56 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 21:56 V26116TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 21:56 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 21:56 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/08/22 21:56 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 21:56 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/08/22 21:56 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 11/08/22 21:56 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/08/22 21:56 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/08/22 21:56 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/08/22 21:56 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/08/22 21:56 V26116
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%11/08/22 21:561 TBL V26116
Surrogate: Dibromofluoromethane 103 Limits: 84-123%11/08/22 21:561 TBL V26116
Surrogate: Toluene-d8 100 Limits: 76-129%11/08/22 21:561 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.153 mg/Kg - dry 0.153 0.875Acenaphthene 1 11/11/22 17:09 V26276JMV
<0.139 mg/Kg - dry 0.139 0.875Acenaphthylene 1 11/11/22 17:09 V26276JMV
<0.201 mg/Kg - dry 0.201 0.875Aniline 1 11/11/22 17:09 V26276JMV
<0.189 mg/Kg - dry 0.189 0.875Anthracene 1 11/11/22 17:09 V26276JMV
<0.184 mg/Kg - dry 0.184 0.875
Benzo(a)anthracene 1 11/11/22 17:09 V26276JMV
<0.194 mg/Kg - dry 0.194 0.875Benzo(a)pyrene 1 11/11/22 17:09 V26276JMV
<0.193 mg/Kg - dry 0.193 0.875Benzo(b)fluoranthene 1 11/11/22 17:09 V26276JMV
<0.180 mg/Kg - dry 0.180 0.875Benzo(g,h,i)perylene 1 11/11/22 17:09 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.181 mg/Kg - dry 0.181 0.875Benzo(k)fluoranthene 1 11/11/22 17:09 V26276JMV
<0.769 mg/Kg - dry 0.769 2.65Benzoic Acid 1 11/11/22 17:09 V26276JMV
<0.139 mg/Kg - dry 0.139 0.875Benzyl alcohol 1 11/11/22 17:09 V26276JMV
<0.156 mg/Kg - dry 0.156 0.875Bis(2-Chloroethoxy)methane 1 11/11/22 17:09 V26276JMV
<0.141 mg/Kg - dry 0.141 0.875Bis(2-Chloroethyl)ether 1 11/11/22 17:09 V26276JMV
<0.180 mg/Kg - dry 0.180 0.437Bis(2-Chloroisopropyl)ether 1 11/11/22 17:09 V26276JMV
<0.159 mg/Kg - dry 0.159 0.875Bis(2-ethylhexyl)phthalate 1 11/11/22 17:09 V26276JMV
<0.144 mg/Kg - dry 0.144 0.8754-Bromophenyl phenyl ether 1 11/11/22 17:09 V26276JMV
<0.149 mg/Kg - dry 0.149 0.437
Butyl benzyl phthalate 1 11/11/22 17:09 V26276JMV
<0.122 mg/Kg - dry 0.122 0.8754-Chloro-3-methylphenol 1 11/11/22 17:09 V26276JMV
<0.148 mg/Kg - dry 0.148 0.4374-Chloroaniline 1 11/11/22 17:09 V26276JMV
<0.153 mg/Kg - dry 0.153 0.8752-Chloronaphthalene 1 11/11/22 17:09 V26276JMV
<0.130 mg/Kg - dry 0.130 0.8752-Chlorophenol 1 11/11/22 17:09 V26276JMV
<0.167 mg/Kg - dry 0.167 1.334-Chlorophenyl phenyl ether 1 11/11/22 17:09 V26276JMV
<0.188 mg/Kg - dry 0.188 0.875Chrysene 1 11/11/22 17:09 V26276JMV
<0.305 mg/Kg - dry 0.305 0.875
Dibenz(a,h)anthracene 1 11/11/22 17:09 V26276JMV
<0.157 mg/Kg - dry 0.157 0.875Dibenzofuran 1 11/11/22 17:09 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8751,2-Dichlorobenzene 1 11/11/22 17:09 V26276JMV
<0.129 mg/Kg - dry 0.129 0.8751,3-Dichlorobenzene 1 11/11/22 17:09 V26276JMV
<0.129 mg/Kg - dry 0.129 0.4371,4-Dichlorobenzene 1 11/11/22 17:09 V26276JMV
<0.194 mg/Kg - dry 0.194 0.8753,3'-Dichlorobenzidine 1 11/11/22 17:09 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8752,4-Dichlorophenol 1 11/11/22 17:09 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.238 mg/Kg - dry 0.238 0.875Diethyl phthalate 1 11/11/22 17:09 V26276JMV
<0.230 mg/Kg - dry 0.230 0.875Dimethyl phthalate 1 11/11/22 17:09 V26276JMV
<0.143 mg/Kg - dry 0.143 0.4372,4-Dimethylphenol 1 11/11/22 17:09 V26276JMV
<0.141 mg/Kg - dry 0.141 0.875Di-n-butyl phthalate 1 11/11/22 17:09 V26276JMV
<0.318 mg/Kg - dry 0.318 1.994,6-Dinitro-2-methylphenol 1 11/11/22 17:09 V26276JMV
<0.689 mg/Kg - dry 0.689 1.992,4-Dinitrophenol 1 11/11/22 17:09 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8752,4-Dinitrotoluene 1 11/11/22 17:09 V26276JMV
<0.143 mg/Kg - dry 0.143 0.8752,6-Dinitrotoluene 1 11/11/22 17:09 V26276JMV
<0.189 mg/Kg - dry 0.189 0.437
Di-n-Octyl Phthalate 1 11/11/22 17:09 V26276JMV
<0.163 mg/Kg - dry 0.163 0.875Fluoranthene 1 11/11/22 17:09 V26276JMV
<0.169 mg/Kg - dry 0.169 0.875Fluorene 1 11/11/22 17:09 V26276JMV
<0.140 mg/Kg - dry 0.140 0.875Hexachlorobenzene 1 11/11/22 17:09 V26276JMV
<0.129 mg/Kg - dry 0.129 0.875Hexachlorobutadiene 1 11/11/22 17:09 V26276JMV
<0.208 mg/Kg - dry 0.208 0.875Hexachlorocyclopentadiene 1 11/11/22 17:09 V26276JMV
<0.105 mg/Kg - dry 0.105 0.875Hexachloroethane 1 11/11/22 17:09 V26276JMV
<0.237 mg/Kg - dry 0.237 0.875
Indeno(1,2,3-cd)pyrene 1 11/11/22 17:09 V26276JMV
<0.253 mg/Kg - dry 0.253 0.875Isophorone 1 11/11/22 17:09 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8751-Methylnaphthalene 1 11/11/22 17:09 V26276JMV
<0.132 mg/Kg - dry 0.132 0.8752-Methylnaphthalene 1 11/11/22 17:09 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8752-Methylphenol 1 11/11/22 17:09 V26276JMV
<0.112 mg/Kg - dry 0.112 0.8753&4 Methylphenol 1 11/11/22 17:09 V26276JMV
<0.190 mg/Kg - dry 0.190 0.875Naphthalene 1 11/11/22 17:09 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-10
92349 Matrix:
11/2/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.128 mg/Kg - dry 0.128 0.8752-Nitroaniline 1 11/11/22 17:09 V26276JMV
<0.159 mg/Kg - dry 0.159 0.8753-Nitroaniline 1 11/11/22 17:09 V26276JMV
<0.123 mg/Kg - dry 0.123 0.4374-Nitroaniline 1 11/11/22 17:09 V26276JMV
<0.153 mg/Kg - dry 0.153 0.437Nitrobenzene 1 11/11/22 17:09 V26276JMV
<0.117 mg/Kg - dry 0.117 0.8752-Nitrophenol 1 11/11/22 17:09 V26276JMV
<0.155 mg/Kg - dry 0.155 0.8754-Nitrophenol 1 11/11/22 17:09 V26276JMV
<0.348 mg/Kg - dry 0.348 0.875N-Nitrosodimethylamine 1 11/11/22 17:09 V26276JMV
<0.240 mg/Kg - dry 0.240 0.875N-Nitrosodiphenylamine 1 11/11/22 17:09 V26276JMV
<0.156 mg/Kg - dry 0.156 0.875
N-Nitroso-di-n-propylamine 1 11/11/22 17:09 V26276JMV
<0.460 mg/Kg - dry 0.460 1.33Pentachlorophenol 1 11/11/22 17:09 V26276JMV
<0.275 mg/Kg - dry 0.275 0.875Phenanthrene 1 11/11/22 17:09 V26276JMV
<0.148 mg/Kg - dry 0.148 0.875Phenol 1 11/11/22 17:09 V26276JMV
<0.177 mg/Kg - dry 0.177 0.875Pyrene 1 11/11/22 17:09 V26276JMV
<0.105 mg/Kg - dry 0.105 0.437Pyridine 1 11/11/22 17:09 V26276JMV
<0.141 mg/Kg - dry 0.141 0.8751,2,4-Trichlorobenzene 1 11/11/22 17:09 V26276JMV
<0.127 mg/Kg - dry 0.127 0.875
2,4,5-Trichlorophenol 1 11/11/22 17:09 V26276JMV
<0.128 mg/Kg - dry 0.128 0.8752,4,6-Trichlorophenol 1 11/11/22 17:09 V26276JMV
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%11/11/22 17:091 JMV
Surrogate: 2-Fluorobiphenyl 98.2 Limits: 44-115%11/11/22 17:091 JMV V26276
Surrogate: 2-Fluorophenol 81.1 Limits: 35-115%11/11/22 17:091 JMV V26276
Surrogate: Nitrobenzene-d5 90.4 Limits: 37-122%11/11/22 17:091 JMV V26276
Surrogate: 4-Terphenyl-d14 107 Limits: 54-127%11/11/22 17:091 JMV V26276
Surrogate: 2,4,6-Tribromophenol 75.1 Limits: 39-132%11/11/22 17:091 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.9 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.182 mg/Kg - dry 0.182 0.259Chromium, Hexavalent 1 11/16/22 14:38 SW-7199SAR
1.73 mg/Kg - dry 0.111 0.324Arsenic 5 11/15/22 00:06 6020BBKN
41.0 mg/Kg - dry 0.055 0.324Barium 5 11/11/22 23:20 6020BBKN
0.105 J mg/Kg - dry 0.0335 0.324Cadmium 5 11/15/22 00:06 6020BBKN
33.5 mg/Kg - dry 0.752 1.62
Chromium 25 11/15/22 00:11 6020BBKN
9.21 mg/Kg - dry 0.0402 0.324Lead 5 11/15/22 00:06 6020BBKN
0.0830 mg/Kg - dry 0.0156 0.0389Mercury (Total)1 11/10/22 15:27 7471BEDV
0.715 mg/Kg - dry 0.133 0.324Selenium 5 11/15/22 00:06 6020BBKN
0.0158 J mg/Kg - dry 0.0087 0.324Silver 5 11/16/22 18:57 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.022 J mg/Kg - dry 0.003 0.025Acetone 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/08/22 22:23 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 22:23 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/08/22 22:23 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 22:23 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 22:23 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 22:23 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 22:23 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/08/22 22:23 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 22:23 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 22:23 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 22:23 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 22:23 V26116TBL
0.237 J mg/Kg - dry 0.018 0.324Ethanol 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/08/22 22:23 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 22:23 V26116TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 22:23 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 22:23 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/08/22 22:23 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 22:23 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/08/22 22:23 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/08/22 22:23 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/08/22 22:23 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/08/22 22:23 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/08/22 22:23 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/08/22 22:23 V26116
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/08/22 22:231 TBL V26116
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/08/22 22:231 TBL V26116
Surrogate: Toluene-d8 101 Limits: 76-129%11/08/22 22:231 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.150 mg/Kg - dry 0.150 0.856Acenaphthene 1 11/11/22 17:31 V26276JMV
<0.136 mg/Kg - dry 0.136 0.856Acenaphthylene 1 11/11/22 17:31 V26276JMV
<0.197 mg/Kg - dry 0.197 0.856Aniline 1 11/11/22 17:31 V26276JMV
<0.185 mg/Kg - dry 0.185 0.856Anthracene 1 11/11/22 17:31 V26276JMV
<0.180 mg/Kg - dry 0.180 0.856
Benzo(a)anthracene 1 11/11/22 17:31 V26276JMV
<0.190 mg/Kg - dry 0.190 0.856Benzo(a)pyrene 1 11/11/22 17:31 V26276JMV
<0.189 mg/Kg - dry 0.189 0.856Benzo(b)fluoranthene 1 11/11/22 17:31 V26276JMV
<0.176 mg/Kg - dry 0.176 0.856Benzo(g,h,i)perylene 1 11/11/22 17:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 82 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.177 mg/Kg - dry 0.177 0.856Benzo(k)fluoranthene 1 11/11/22 17:31 V26276JMV
<0.752 mg/Kg - dry 0.752 2.59Benzoic Acid 1 11/11/22 17:31 V26276JMV
<0.136 mg/Kg - dry 0.136 0.856Benzyl alcohol 1 11/11/22 17:31 V26276JMV
<0.153 mg/Kg - dry 0.153 0.856Bis(2-Chloroethoxy)methane 1 11/11/22 17:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.856Bis(2-Chloroethyl)ether 1 11/11/22 17:31 V26276JMV
<0.176 mg/Kg - dry 0.176 0.428Bis(2-Chloroisopropyl)ether 1 11/11/22 17:31 V26276JMV
<0.155 mg/Kg - dry 0.155 0.856Bis(2-ethylhexyl)phthalate 1 11/11/22 17:31 V26276JMV
<0.141 mg/Kg - dry 0.141 0.8564-Bromophenyl phenyl ether 1 11/11/22 17:31 V26276JMV
<0.146 mg/Kg - dry 0.146 0.428
Butyl benzyl phthalate 1 11/11/22 17:31 V26276JMV
<0.119 mg/Kg - dry 0.119 0.8564-Chloro-3-methylphenol 1 11/11/22 17:31 V26276JMV
<0.145 mg/Kg - dry 0.145 0.4284-Chloroaniline 1 11/11/22 17:31 V26276JMV
<0.150 mg/Kg - dry 0.150 0.8562-Chloronaphthalene 1 11/11/22 17:31 V26276JMV
<0.127 mg/Kg - dry 0.127 0.8562-Chlorophenol 1 11/11/22 17:31 V26276JMV
<0.163 mg/Kg - dry 0.163 1.304-Chlorophenyl phenyl ether 1 11/11/22 17:31 V26276JMV
<0.184 mg/Kg - dry 0.184 0.856Chrysene 1 11/11/22 17:31 V26276JMV
<0.298 mg/Kg - dry 0.298 0.856
Dibenz(a,h)anthracene 1 11/11/22 17:31 V26276JMV
<0.154 mg/Kg - dry 0.154 0.856Dibenzofuran 1 11/11/22 17:31 V26276JMV
<0.122 mg/Kg - dry 0.122 0.8561,2-Dichlorobenzene 1 11/11/22 17:31 V26276JMV
<0.126 mg/Kg - dry 0.126 0.8561,3-Dichlorobenzene 1 11/11/22 17:31 V26276JMV
<0.126 mg/Kg - dry 0.126 0.4281,4-Dichlorobenzene 1 11/11/22 17:31 V26276JMV
<0.190 mg/Kg - dry 0.190 0.8563,3'-Dichlorobenzidine 1 11/11/22 17:31 V26276JMV
<0.124 mg/Kg - dry 0.124 0.8562,4-Dichlorophenol 1 11/11/22 17:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.233 mg/Kg - dry 0.233 0.856Diethyl phthalate 1 11/11/22 17:31 V26276JMV
<0.225 mg/Kg - dry 0.225 0.856Dimethyl phthalate 1 11/11/22 17:31 V26276JMV
<0.140 mg/Kg - dry 0.140 0.4282,4-Dimethylphenol 1 11/11/22 17:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.856Di-n-butyl phthalate 1 11/11/22 17:31 V26276JMV
<0.311 mg/Kg - dry 0.311 1.954,6-Dinitro-2-methylphenol 1 11/11/22 17:31 V26276JMV
<0.674 mg/Kg - dry 0.674 1.952,4-Dinitrophenol 1 11/11/22 17:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8562,4-Dinitrotoluene 1 11/11/22 17:31 V26276JMV
<0.140 mg/Kg - dry 0.140 0.8562,6-Dinitrotoluene 1 11/11/22 17:31 V26276JMV
<0.185 mg/Kg - dry 0.185 0.428
Di-n-Octyl Phthalate 1 11/11/22 17:31 V26276JMV
<0.159 mg/Kg - dry 0.159 0.856Fluoranthene 1 11/11/22 17:31 V26276JMV
<0.166 mg/Kg - dry 0.166 0.856Fluorene 1 11/11/22 17:31 V26276JMV
<0.137 mg/Kg - dry 0.137 0.856Hexachlorobenzene 1 11/11/22 17:31 V26276JMV
<0.126 mg/Kg - dry 0.126 0.856Hexachlorobutadiene 1 11/11/22 17:31 V26276JMV
<0.203 mg/Kg - dry 0.203 0.856Hexachlorocyclopentadiene 1 11/11/22 17:31 V26276JMV
<0.102 mg/Kg - dry 0.102 0.856Hexachloroethane 1 11/11/22 17:31 V26276JMV
<0.232 mg/Kg - dry 0.232 0.856
Indeno(1,2,3-cd)pyrene 1 11/11/22 17:31 V26276JMV
<0.247 mg/Kg - dry 0.247 0.856Isophorone 1 11/11/22 17:31 V26276JMV
<0.137 mg/Kg - dry 0.137 0.8561-Methylnaphthalene 1 11/11/22 17:31 V26276JMV
<0.129 mg/Kg - dry 0.129 0.8562-Methylnaphthalene 1 11/11/22 17:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8562-Methylphenol 1 11/11/22 17:31 V26276JMV
<0.110 mg/Kg - dry 0.110 0.8563&4 Methylphenol 1 11/11/22 17:31 V26276JMV
<0.186 mg/Kg - dry 0.186 0.856Naphthalene 1 11/11/22 17:31 V26276JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-11
92350 Matrix:
11/2/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26175 11/09/22 10:30
<0.125 mg/Kg - dry 0.125 0.8562-Nitroaniline 1 11/11/22 17:31 V26276JMV
<0.155 mg/Kg - dry 0.155 0.8563-Nitroaniline 1 11/11/22 17:31 V26276JMV
<0.121 mg/Kg - dry 0.121 0.4284-Nitroaniline 1 11/11/22 17:31 V26276JMV
<0.150 mg/Kg - dry 0.150 0.428Nitrobenzene 1 11/11/22 17:31 V26276JMV
<0.115 mg/Kg - dry 0.115 0.8562-Nitrophenol 1 11/11/22 17:31 V26276JMV
<0.151 mg/Kg - dry 0.151 0.8564-Nitrophenol 1 11/11/22 17:31 V26276JMV
<0.341 mg/Kg - dry 0.341 0.856N-Nitrosodimethylamine 1 11/11/22 17:31 V26276JMV
<0.234 mg/Kg - dry 0.234 0.856N-Nitrosodiphenylamine 1 11/11/22 17:31 V26276JMV
<0.153 mg/Kg - dry 0.153 0.856
N-Nitroso-di-n-propylamine 1 11/11/22 17:31 V26276JMV
<0.450 mg/Kg - dry 0.450 1.30Pentachlorophenol 1 11/11/22 17:31 V26276JMV
<0.269 mg/Kg - dry 0.269 0.856Phenanthrene 1 11/11/22 17:31 V26276JMV
<0.145 mg/Kg - dry 0.145 0.856Phenol 1 11/11/22 17:31 V26276JMV
<0.173 mg/Kg - dry 0.173 0.856Pyrene 1 11/11/22 17:31 V26276JMV
<0.102 mg/Kg - dry 0.102 0.428Pyridine 1 11/11/22 17:31 V26276JMV
<0.138 mg/Kg - dry 0.138 0.8561,2,4-Trichlorobenzene 1 11/11/22 17:31 V26276JMV
<0.124 mg/Kg - dry 0.124 0.856
2,4,5-Trichlorophenol 1 11/11/22 17:31 V26276JMV
<0.125 mg/Kg - dry 0.125 0.8562,4,6-Trichlorophenol 1 11/11/22 17:31 V26276JMV
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%11/11/22 17:311 JMV
Surrogate: 2-Fluorobiphenyl 94.6 Limits: 44-115%11/11/22 17:311 JMV V26276
Surrogate: 2-Fluorophenol 80.8 Limits: 35-115%11/11/22 17:311 JMV V26276
Surrogate: Nitrobenzene-d5 89.2 Limits: 37-122%11/11/22 17:311 JMV V26276
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%11/11/22 17:311 JMV V26276
Surrogate: 2,4,6-Tribromophenol 75.1 Limits: 39-132%11/11/22 17:311 JMV V26276
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.6 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.189 mg/Kg - dry 0.189 0.268Chromium, Hexavalent 1 11/16/22 15:11 SW-7199SAR
1.80 mg/Kg - dry 0.115 0.336Arsenic 5 11/15/22 00:15 6020BBKN
49.9 mg/Kg - dry 0.057 0.336Barium 5 11/11/22 23:24 6020BBKN
0.0881 J mg/Kg - dry 0.0348 0.336Cadmium 5 11/15/22 00:15 6020BBKN
36.0 mg/Kg - dry 0.779 1.68
Chromium 25 11/15/22 00:21 6020BBKN
12.4 mg/Kg - dry 0.0416 0.336Lead 5 11/15/22 00:15 6020BBKN
0.0837 mg/Kg - dry 0.0161 0.0403Mercury (Total)1 11/10/22 15:29 7471BEDV
0.668 mg/Kg - dry 0.138 0.336Selenium 5 11/15/22 00:15 6020BBKN
0.0431 J mg/Kg - dry 0.0090 0.336Silver 5 11/16/22 19:02 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.045 mg/Kg - dry 0.003 0.026Acetone 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 22:51 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/08/22 22:51 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 11/08/22 22:51 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 22:51 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 22:51 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 22:51 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 22:51 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 11/08/22 22:51 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 22:51 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 22:51 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 22:51 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 22:51 V26116TBL
<0.018 mg/Kg - dry 0.018 0.336Ethanol 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/08/22 22:51 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/08/22 22:51 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 22:51 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/08/22 22:51 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 22:51 V26116TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 22:51 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 22:51 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/08/22 22:51 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 22:51 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 22:51 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/08/22 22:51 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 11/08/22 22:51 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 89 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 22:51 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/08/22 22:51 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/08/22 22:51 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/08/22 22:51 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/08/22 22:51 V26116
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/08/22 22:511 TBL V26116
Surrogate: Dibromofluoromethane 102 Limits: 84-123%11/08/22 22:511 TBL V26116
Surrogate: Toluene-d8 99.0 Limits: 76-129%11/08/22 22:511 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.155 mg/Kg - dry 0.155 0.888Acenaphthene 1 11/11/22 18:16 V26355JMV
<0.141 mg/Kg - dry 0.141 0.888Acenaphthylene 1 11/11/22 18:16 V26355JMV
<0.204 mg/Kg - dry 0.204 0.888Aniline 1 11/11/22 18:16 V26355JMV
<0.192 mg/Kg - dry 0.192 0.888Anthracene 1 11/11/22 18:16 V26355JMV
<0.186 mg/Kg - dry 0.186 0.888
Benzo(a)anthracene 1 11/11/22 18:16 V26355JMV
<0.197 mg/Kg - dry 0.197 0.888Benzo(a)pyrene 1 11/11/22 18:16 V26355JMV
<0.196 mg/Kg - dry 0.196 0.888Benzo(b)fluoranthene 1 11/11/22 18:16 V26355JMV
<0.182 mg/Kg - dry 0.182 0.888Benzo(g,h,i)perylene 1 11/11/22 18:16 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 90 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.184 mg/Kg - dry 0.184 0.888Benzo(k)fluoranthene 1 11/11/22 18:16 V26355JMV
<0.779 mg/Kg - dry 0.779 2.69Benzoic Acid 1 11/11/22 18:16 V26355JMV
<0.141 mg/Kg - dry 0.141 0.888Benzyl alcohol 1 11/11/22 18:16 V26355JMV
<0.158 mg/Kg - dry 0.158 0.888Bis(2-Chloroethoxy)methane 1 11/11/22 18:16 V26355JMV
<0.143 mg/Kg - dry 0.143 0.888Bis(2-Chloroethyl)ether 1 11/11/22 18:16 V26355JMV
<0.182 mg/Kg - dry 0.182 0.444Bis(2-Chloroisopropyl)ether 1 11/11/22 18:16 V26355JMV
<0.161 mg/Kg - dry 0.161 0.888Bis(2-ethylhexyl)phthalate 1 11/11/22 18:16 V26355JMV
<0.146 mg/Kg - dry 0.146 0.8884-Bromophenyl phenyl ether 1 11/11/22 18:16 V26355JMV
0.213 J
mg/Kg - dry 0.151 0.444
Butyl benzyl phthalate 1 11/11/22 18:16 V26355JMV
<0.124 mg/Kg - dry 0.124 0.8884-Chloro-3-methylphenol 1 11/11/22 18:16 V26355JMV
<0.150 mg/Kg - dry 0.150 0.4444-Chloroaniline 1 11/11/22 18:16 V26355JMV
<0.155 mg/Kg - dry 0.155 0.8882-Chloronaphthalene 1 11/11/22 18:16 V26355JMV
<0.132 mg/Kg - dry 0.132 0.8882-Chlorophenol 1 11/11/22 18:16 V26355JMV
<0.169 mg/Kg - dry 0.169 1.344-Chlorophenyl phenyl ether 1 11/11/22 18:16 V26355JMV
<0.190 mg/Kg - dry 0.190 0.888Chrysene 1 11/11/22 18:16 V26355JMV
<0.309 mg/Kg - dry 0.309 0.888
Dibenz(a,h)anthracene 1 11/11/22 18:16 V26355JMV
<0.159 mg/Kg - dry 0.159 0.888Dibenzofuran 1 11/11/22 18:16 V26355JMV
<0.127 mg/Kg - dry 0.127 0.8881,2-Dichlorobenzene 1 11/11/22 18:16 V26355JMV
<0.130 mg/Kg - dry 0.130 0.8881,3-Dichlorobenzene 1 11/11/22 18:16 V26355JMV
<0.131 mg/Kg - dry 0.131 0.4441,4-Dichlorobenzene 1 11/11/22 18:16 V26355JMV
<0.197 mg/Kg - dry 0.197 0.8883,3'-Dichlorobenzidine 1 11/11/22 18:16 V26355JMV
<0.128 mg/Kg - dry 0.128 0.8882,4-Dichlorophenol 1 11/11/22 18:16 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 91 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.241 mg/Kg - dry 0.241 0.888Diethyl phthalate 1 11/11/22 18:16 V26355JMV
<0.233 mg/Kg - dry 0.233 0.888Dimethyl phthalate 1 11/11/22 18:16 V26355JMV
<0.145 mg/Kg - dry 0.145 0.4442,4-Dimethylphenol 1 11/11/22 18:16 V26355JMV
<0.143 mg/Kg - dry 0.143 0.888Di-n-butyl phthalate 1 11/11/22 18:16 V26355JMV
<0.322 mg/Kg - dry 0.322 2.024,6-Dinitro-2-methylphenol 1 11/11/22 18:16 V26355JMV
<0.698 mg/Kg - dry 0.698 2.022,4-Dinitrophenol 1 11/11/22 18:16 V26355JMV
<0.129 mg/Kg - dry 0.129 0.8882,4-Dinitrotoluene 1 11/11/22 18:16 V26355JMV
<0.145 mg/Kg - dry 0.145 0.8882,6-Dinitrotoluene 1 11/11/22 18:16 V26355JMV
<0.192 mg/Kg - dry 0.192 0.444
Di-n-Octyl Phthalate 1 11/11/22 18:16 V26355JMV
0.193 J mg/Kg - dry 0.165 0.888Fluoranthene 1 11/11/22 18:16 V26355JMV
<0.172 mg/Kg - dry 0.172 0.888Fluorene 1 11/11/22 18:16 V26355JMV
<0.142 mg/Kg - dry 0.142 0.888Hexachlorobenzene 1 11/11/22 18:16 V26355JMV
<0.131 mg/Kg - dry 0.131 0.888Hexachlorobutadiene 1 11/11/22 18:16 V26355JMV
<0.211 mg/Kg - dry 0.211 0.888Hexachlorocyclopentadiene 1 11/11/22 18:16 V26355JMV
<0.106 mg/Kg - dry 0.106 0.888Hexachloroethane 1 11/11/22 18:16 V26355JMV
<0.240 mg/Kg - dry 0.240 0.888
Indeno(1,2,3-cd)pyrene 1 11/11/22 18:16 V26355JMV
<0.256 mg/Kg - dry 0.256 0.888Isophorone 1 11/11/22 18:16 V26355JMV
<0.142 mg/Kg - dry 0.142 0.8881-Methylnaphthalene 1 11/11/22 18:16 V26355JMV
<0.134 mg/Kg - dry 0.134 0.8882-Methylnaphthalene 1 11/11/22 18:16 V26355JMV
<0.130 mg/Kg - dry 0.130 0.8882-Methylphenol 1 11/11/22 18:16 V26355JMV
<0.114 mg/Kg - dry 0.114 0.8883&4 Methylphenol 1 11/11/22 18:16 V26355JMV
<0.193 mg/Kg - dry 0.193 0.888Naphthalene 1 11/11/22 18:16 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 92 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-12
92351 Matrix:
11/2/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.130 mg/Kg - dry 0.130 0.8882-Nitroaniline 1 11/11/22 18:16 V26355JMV
<0.161 mg/Kg - dry 0.161 0.8883-Nitroaniline 1 11/11/22 18:16 V26355JMV
<0.125 mg/Kg - dry 0.125 0.4444-Nitroaniline 1 11/11/22 18:16 V26355JMV
<0.155 mg/Kg - dry 0.155 0.444Nitrobenzene 1 11/11/22 18:16 V26355JMV
<0.119 mg/Kg - dry 0.119 0.8882-Nitrophenol 1 11/11/22 18:16 V26355JMV
<0.157 mg/Kg - dry 0.157 0.8884-Nitrophenol 1 11/11/22 18:16 V26355JMV
<0.353 mg/Kg - dry 0.353 0.888N-Nitrosodimethylamine 1 11/11/22 18:16 V26355JMV
<0.243 mg/Kg - dry 0.243 0.888N-Nitrosodiphenylamine 1 11/11/22 18:16 V26355JMV
<0.158 mg/Kg - dry 0.158 0.888
N-Nitroso-di-n-propylamine 1 11/11/22 18:16 V26355JMV
<0.466 mg/Kg - dry 0.466 1.34Pentachlorophenol 1 11/11/22 18:16 V26355JMV
<0.279 mg/Kg - dry 0.279 0.888Phenanthrene 1 11/11/22 18:16 V26355JMV
<0.150 mg/Kg - dry 0.150 0.888Phenol 1 11/11/22 18:16 V26355JMV
<0.180 mg/Kg - dry 0.180 0.888Pyrene 1 11/11/22 18:16 V26355JMV
<0.106 mg/Kg - dry 0.106 0.444Pyridine 1 11/11/22 18:16 V26355JMV
<0.143 mg/Kg - dry 0.143 0.8881,2,4-Trichlorobenzene 1 11/11/22 18:16 V26355JMV
<0.129 mg/Kg - dry 0.129 0.888
2,4,5-Trichlorophenol 1 11/11/22 18:16 V26355JMV
<0.129 mg/Kg - dry 0.129 0.8882,4,6-Trichlorophenol 1 11/11/22 18:16 V26355JMV
8270ESurrogate: Phenol-d5 73.1 Limits: 34-121%11/11/22 18:161 JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%11/11/22 18:161 JMV V26355
Surrogate: 2-Fluorophenol 78.1 Limits: 35-115%11/11/22 18:161 JMV V26355
Surrogate: Nitrobenzene-d5 83.2 Limits: 37-122%11/11/22 18:161 JMV V26355
Surrogate: 4-Terphenyl-d14 109 Limits: 54-127%11/11/22 18:161 JMV V26355
Surrogate: 2,4,6-Tribromophenol 74.6 Limits: 39-132%11/11/22 18:161 JMV V26355
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 93 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.2 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.191 mg/Kg - dry 0.191 0.271Chromium, Hexavalent 1 11/16/22 15:22 SW-7199SAR
2.11 mg/Kg - dry 0.116 0.339Arsenic 5 11/15/22 00:25 6020BBKN
40.5 mg/Kg - dry 0.057 0.338Barium 5 11/11/22 23:28 6020BBKN
0.0613 J mg/Kg - dry 0.0350 0.339Cadmium 5 11/15/22 00:25 6020BBKN
41.5 mg/Kg - dry 0.785 1.69
Chromium 25 11/15/22 00:31 6020BBKN
10.8 mg/Kg - dry 0.0420 0.339Lead 5 11/15/22 00:25 6020BBKN
0.101 mg/Kg - dry 0.0163 0.0407Mercury (Total)1 11/10/22 15:32 7471BEDV
0.768 mg/Kg - dry 0.139 0.338Selenium 5 11/15/22 00:25 6020BBKN
0.0298 J mg/Kg - dry 0.0091 0.339Silver 5 11/16/22 19:07 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 94 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.029 mg/Kg - dry 0.003 0.027Acetone 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 23:18 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 11/08/22 23:18 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/08/22 23:18 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 23:18 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 23:18 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 95 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 11/08/22 23:18 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 23:18 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 23:18 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 23:18 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 23:18 V26116TBL
<0.018 mg/Kg - dry 0.018 0.338Ethanol 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/08/22 23:18 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 96 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 11/08/22 23:18 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 11/08/22 23:18 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 23:18 V26116TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 23:18 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/08/22 23:18 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 23:18 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 23:18 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/08/22 23:18 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 11/08/22 23:18 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 97 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 23:18 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/08/22 23:18 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/08/22 23:18 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/08/22 23:18 V26116
Surrogate: 4-Bromofluorobenzene 99.3 Limits: 70-130%11/08/22 23:181 TBL V26116
Surrogate: Dibromofluoromethane 102 Limits: 84-123%11/08/22 23:181 TBL V26116
Surrogate: Toluene-d8 100 Limits: 76-129%11/08/22 23:181 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.157 mg/Kg - dry 0.157 0.895Acenaphthene 1 11/11/22 19:24 V26355JMV
<0.142 mg/Kg - dry 0.142 0.895Acenaphthylene 1 11/11/22 19:24 V26355JMV
<0.205 mg/Kg - dry 0.205 0.895Aniline 1 11/11/22 19:24 V26355JMV
<0.193 mg/Kg - dry 0.193 0.895Anthracene 1 11/11/22 19:24 V26355JMV
<0.188 mg/Kg - dry 0.188 0.895
Benzo(a)anthracene 1 11/11/22 19:24 V26355JMV
<0.199 mg/Kg - dry 0.199 0.895Benzo(a)pyrene 1 11/11/22 19:24 V26355JMV
<0.197 mg/Kg - dry 0.197 0.895Benzo(b)fluoranthene 1 11/11/22 19:24 V26355JMV
<0.184 mg/Kg - dry 0.184 0.895Benzo(g,h,i)perylene 1 11/11/22 19:24 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 98 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.185 mg/Kg - dry 0.185 0.895Benzo(k)fluoranthene 1 11/11/22 19:24 V26355JMV
<0.785 mg/Kg - dry 0.785 2.71Benzoic Acid 1 11/11/22 19:24 V26355JMV
<0.142 mg/Kg - dry 0.142 0.895Benzyl alcohol 1 11/11/22 19:24 V26355JMV
<0.159 mg/Kg - dry 0.159 0.895Bis(2-Chloroethoxy)methane 1 11/11/22 19:24 V26355JMV
<0.144 mg/Kg - dry 0.144 0.895Bis(2-Chloroethyl)ether 1 11/11/22 19:24 V26355JMV
<0.184 mg/Kg - dry 0.184 0.447Bis(2-Chloroisopropyl)ether 1 11/11/22 19:24 V26355JMV
<0.162 mg/Kg - dry 0.162 0.895Bis(2-ethylhexyl)phthalate 1 11/11/22 19:24 V26355JMV
<0.147 mg/Kg - dry 0.147 0.8954-Bromophenyl phenyl ether 1 11/11/22 19:24 V26355JMV
<0.153 mg/Kg - dry 0.153 0.447
Butyl benzyl phthalate 1 11/11/22 19:24 V26355JMV
<0.125 mg/Kg - dry 0.125 0.8954-Chloro-3-methylphenol 1 11/11/22 19:24 V26355JMV
<0.151 mg/Kg - dry 0.151 0.4474-Chloroaniline 1 11/11/22 19:24 V26355JMV
<0.157 mg/Kg - dry 0.157 0.8952-Chloronaphthalene 1 11/11/22 19:24 V26355JMV
<0.133 mg/Kg - dry 0.133 0.8952-Chlorophenol 1 11/11/22 19:24 V26355JMV
<0.170 mg/Kg - dry 0.170 1.364-Chlorophenyl phenyl ether 1 11/11/22 19:24 V26355JMV
<0.192 mg/Kg - dry 0.192 0.895Chrysene 1 11/11/22 19:24 V26355JMV
<0.311 mg/Kg - dry 0.311 0.895
Dibenz(a,h)anthracene 1 11/11/22 19:24 V26355JMV
<0.161 mg/Kg - dry 0.161 0.895Dibenzofuran 1 11/11/22 19:24 V26355JMV
<0.128 mg/Kg - dry 0.128 0.8951,2-Dichlorobenzene 1 11/11/22 19:24 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8951,3-Dichlorobenzene 1 11/11/22 19:24 V26355JMV
<0.132 mg/Kg - dry 0.132 0.4471,4-Dichlorobenzene 1 11/11/22 19:24 V26355JMV
<0.199 mg/Kg - dry 0.199 0.8953,3'-Dichlorobenzidine 1 11/11/22 19:24 V26355JMV
<0.129 mg/Kg - dry 0.129 0.8952,4-Dichlorophenol 1 11/11/22 19:24 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 99 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.243 mg/Kg - dry 0.243 0.895Diethyl phthalate 1 11/11/22 19:24 V26355JMV
<0.235 mg/Kg - dry 0.235 0.895Dimethyl phthalate 1 11/11/22 19:24 V26355JMV
<0.146 mg/Kg - dry 0.146 0.4472,4-Dimethylphenol 1 11/11/22 19:24 V26355JMV
<0.144 mg/Kg - dry 0.144 0.895Di-n-butyl phthalate 1 11/11/22 19:24 V26355JMV
<0.325 mg/Kg - dry 0.325 2.034,6-Dinitro-2-methylphenol 1 11/11/22 19:24 V26355JMV
<0.704 mg/Kg - dry 0.704 2.032,4-Dinitrophenol 1 11/11/22 19:24 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8952,4-Dinitrotoluene 1 11/11/22 19:24 V26355JMV
<0.146 mg/Kg - dry 0.146 0.8952,6-Dinitrotoluene 1 11/11/22 19:24 V26355JMV
<0.193 mg/Kg - dry 0.193 0.447
Di-n-Octyl Phthalate 1 11/11/22 19:24 V26355JMV
<0.166 mg/Kg - dry 0.166 0.895Fluoranthene 1 11/11/22 19:24 V26355JMV
<0.173 mg/Kg - dry 0.173 0.895Fluorene 1 11/11/22 19:24 V26355JMV
<0.143 mg/Kg - dry 0.143 0.895Hexachlorobenzene 1 11/11/22 19:24 V26355JMV
<0.132 mg/Kg - dry 0.132 0.895Hexachlorobutadiene 1 11/11/22 19:24 V26355JMV
<0.212 mg/Kg - dry 0.212 0.895Hexachlorocyclopentadiene 1 11/11/22 19:24 V26355JMV
<0.107 mg/Kg - dry 0.107 0.895Hexachloroethane 1 11/11/22 19:24 V26355JMV
<0.242 mg/Kg - dry 0.242 0.895
Indeno(1,2,3-cd)pyrene 1 11/11/22 19:24 V26355JMV
<0.258 mg/Kg - dry 0.258 0.895Isophorone 1 11/11/22 19:24 V26355JMV
<0.143 mg/Kg - dry 0.143 0.8951-Methylnaphthalene 1 11/11/22 19:24 V26355JMV
<0.135 mg/Kg - dry 0.135 0.8952-Methylnaphthalene 1 11/11/22 19:24 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8952-Methylphenol 1 11/11/22 19:24 V26355JMV
<0.115 mg/Kg - dry 0.115 0.8953&4 Methylphenol 1 11/11/22 19:24 V26355JMV
<0.195 mg/Kg - dry 0.195 0.895Naphthalene 1 11/11/22 19:24 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 100 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-13
92352 Matrix:
11/2/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.131 mg/Kg - dry 0.131 0.8952-Nitroaniline 1 11/11/22 19:24 V26355JMV
<0.162 mg/Kg - dry 0.162 0.8953-Nitroaniline 1 11/11/22 19:24 V26355JMV
<0.126 mg/Kg - dry 0.126 0.4474-Nitroaniline 1 11/11/22 19:24 V26355JMV
<0.157 mg/Kg - dry 0.157 0.447Nitrobenzene 1 11/11/22 19:24 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8952-Nitrophenol 1 11/11/22 19:24 V26355JMV
<0.158 mg/Kg - dry 0.158 0.8954-Nitrophenol 1 11/11/22 19:24 V26355JMV
<0.356 mg/Kg - dry 0.356 0.895N-Nitrosodimethylamine 1 11/11/22 19:24 V26355JMV
<0.245 mg/Kg - dry 0.245 0.895N-Nitrosodiphenylamine 1 11/11/22 19:24 V26355JMV
<0.159 mg/Kg - dry 0.159 0.895
N-Nitroso-di-n-propylamine 1 11/11/22 19:24 V26355JMV
<0.470 mg/Kg - dry 0.470 1.36Pentachlorophenol 1 11/11/22 19:24 V26355JMV
<0.281 mg/Kg - dry 0.281 0.895Phenanthrene 1 11/11/22 19:24 V26355JMV
<0.151 mg/Kg - dry 0.151 0.895Phenol 1 11/11/22 19:24 V26355JMV
<0.181 mg/Kg - dry 0.181 0.895Pyrene 1 11/11/22 19:24 V26355JMV
<0.107 mg/Kg - dry 0.107 0.447Pyridine 1 11/11/22 19:24 V26355JMV
<0.144 mg/Kg - dry 0.144 0.8951,2,4-Trichlorobenzene 1 11/11/22 19:24 V26355JMV
<0.130 mg/Kg - dry 0.130 0.895
2,4,5-Trichlorophenol 1 11/11/22 19:24 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8952,4,6-Trichlorophenol 1 11/11/22 19:24 V26355JMV
8270ESurrogate: Phenol-d5 86.8 Limits: 34-121%11/11/22 19:241 JMV
Surrogate: 2-Fluorobiphenyl 102 Limits: 44-115%11/11/22 19:241 JMV V26355
Surrogate: 2-Fluorophenol 92.2 Limits: 35-115%11/11/22 19:241 JMV V26355
Surrogate: Nitrobenzene-d5 102 Limits: 37-122%11/11/22 19:241 JMV V26355
Surrogate: 4-Terphenyl-d14 116 Limits: 54-127%11/11/22 19:241 JMV V26355
Surrogate: 2,4,6-Tribromophenol 86.8 Limits: 39-132%11/11/22 19:241 JMV V26355
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 101 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.5 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.177 mg/Kg - dry 0.177 0.251Chromium, Hexavalent 1 11/16/22 15:33 SW-7199SAR
2.54 mg/Kg - dry 0.108 0.314Arsenic 5 11/15/22 00:35 6020BBKN
73.3 mg/Kg - dry 0.053 0.314Barium 5 11/11/22 23:42 6020BBKN
0.147 J mg/Kg - dry 0.0325 0.314Cadmium 5 11/15/22 00:35 6020BBKN
40.8 mg/Kg - dry 0.729 1.57
Chromium 25 11/15/22 00:41 6020BBKN
13.5 mg/Kg - dry 0.0389 0.314Lead 5 11/15/22 00:35 6020BBKN
0.179 mg/Kg - dry 0.0151 0.0377Mercury (Total)1 11/10/22 15:34 7471BEDV
0.778 mg/Kg - dry 0.129 0.314Selenium 5 11/15/22 00:35 6020BBKN
0.0638 J mg/Kg - dry 0.0084 0.314Silver 5 11/16/22 19:22 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 102 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.025 mg/Kg - dry 0.003 0.025Acetone 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/08/22 23:46 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/08/22 23:46 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/08/22 23:46 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/08/22 23:46 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/08/22 23:46 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 103 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/08/22 23:46 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/08/22 23:46 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/08/22 23:46 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/08/22 23:46 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/08/22 23:46 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/08/22 23:46 V26116TBL
<0.017 mg/Kg - dry 0.017 0.314Ethanol 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/08/22 23:46 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/08/22 23:46 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 104 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/08/22 23:46 V26116TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/08/22 23:46 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/08/22 23:46 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/08/22 23:46 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/08/22 23:46 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/08/22 23:46 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 105 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/08/22 23:46 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/08/22 23:46 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/08/22 23:46 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/08/22 23:46 V26116
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%11/08/22 23:461 TBL V26116
Surrogate: Dibromofluoromethane 106 Limits: 84-123%11/08/22 23:461 TBL V26116
Surrogate: Toluene-d8 102 Limits: 76-129%11/08/22 23:461 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.145 mg/Kg - dry 0.145 0.830Acenaphthene 1 11/11/22 19:46 V26355JMV
<0.132 mg/Kg - dry 0.132 0.830Acenaphthylene 1 11/11/22 19:46 V26355JMV
<0.191 mg/Kg - dry 0.191 0.830Aniline 1 11/11/22 19:46 V26355JMV
<0.179 mg/Kg - dry 0.179 0.830Anthracene 1 11/11/22 19:46 V26355JMV
<0.174 mg/Kg - dry 0.174 0.830
Benzo(a)anthracene 1 11/11/22 19:46 V26355JMV
<0.184 mg/Kg - dry 0.184 0.830Benzo(a)pyrene 1 11/11/22 19:46 V26355JMV
<0.183 mg/Kg - dry 0.183 0.830Benzo(b)fluoranthene 1 11/11/22 19:46 V26355JMV
<0.171 mg/Kg - dry 0.171 0.830Benzo(g,h,i)perylene 1 11/11/22 19:46 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 106 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.172 mg/Kg - dry 0.172 0.830Benzo(k)fluoranthene 1 11/11/22 19:46 V26355JMV
<0.729 mg/Kg - dry 0.729 2.52Benzoic Acid 1 11/11/22 19:46 V26355JMV
<0.132 mg/Kg - dry 0.132 0.830Benzyl alcohol 1 11/11/22 19:46 V26355JMV
<0.148 mg/Kg - dry 0.148 0.830Bis(2-Chloroethoxy)methane 1 11/11/22 19:46 V26355JMV
<0.134 mg/Kg - dry 0.134 0.830Bis(2-Chloroethyl)ether 1 11/11/22 19:46 V26355JMV
<0.171 mg/Kg - dry 0.171 0.415Bis(2-Chloroisopropyl)ether 1 11/11/22 19:46 V26355JMV
<0.150 mg/Kg - dry 0.150 0.830Bis(2-ethylhexyl)phthalate 1 11/11/22 19:46 V26355JMV
<0.137 mg/Kg - dry 0.137 0.8304-Bromophenyl phenyl ether 1 11/11/22 19:46 V26355JMV
<0.142 mg/Kg - dry 0.142 0.415
Butyl benzyl phthalate 1 11/11/22 19:46 V26355JMV
<0.116 mg/Kg - dry 0.116 0.8304-Chloro-3-methylphenol 1 11/11/22 19:46 V26355JMV
<0.140 mg/Kg - dry 0.140 0.4154-Chloroaniline 1 11/11/22 19:46 V26355JMV
<0.145 mg/Kg - dry 0.145 0.8302-Chloronaphthalene 1 11/11/22 19:46 V26355JMV
<0.123 mg/Kg - dry 0.123 0.8302-Chlorophenol 1 11/11/22 19:46 V26355JMV
<0.158 mg/Kg - dry 0.158 1.264-Chlorophenyl phenyl ether 1 11/11/22 19:46 V26355JMV
<0.178 mg/Kg - dry 0.178 0.830Chrysene 1 11/11/22 19:46 V26355JMV
<0.289 mg/Kg - dry 0.289 0.830
Dibenz(a,h)anthracene 1 11/11/22 19:46 V26355JMV
<0.149 mg/Kg - dry 0.149 0.830Dibenzofuran 1 11/11/22 19:46 V26355JMV
<0.118 mg/Kg - dry 0.118 0.8301,2-Dichlorobenzene 1 11/11/22 19:46 V26355JMV
<0.122 mg/Kg - dry 0.122 0.8301,3-Dichlorobenzene 1 11/11/22 19:46 V26355JMV
<0.122 mg/Kg - dry 0.122 0.4151,4-Dichlorobenzene 1 11/11/22 19:46 V26355JMV
<0.184 mg/Kg - dry 0.184 0.8303,3'-Dichlorobenzidine 1 11/11/22 19:46 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8302,4-Dichlorophenol 1 11/11/22 19:46 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 107 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.226 mg/Kg - dry 0.226 0.830Diethyl phthalate 1 11/11/22 19:46 V26355JMV
<0.218 mg/Kg - dry 0.218 0.830Dimethyl phthalate 1 11/11/22 19:46 V26355JMV
<0.135 mg/Kg - dry 0.135 0.4152,4-Dimethylphenol 1 11/11/22 19:46 V26355JMV
<0.134 mg/Kg - dry 0.134 0.830Di-n-butyl phthalate 1 11/11/22 19:46 V26355JMV
<0.301 mg/Kg - dry 0.301 1.894,6-Dinitro-2-methylphenol 1 11/11/22 19:46 V26355JMV
<0.654 mg/Kg - dry 0.654 1.892,4-Dinitrophenol 1 11/11/22 19:46 V26355JMV
<0.121 mg/Kg - dry 0.121 0.8302,4-Dinitrotoluene 1 11/11/22 19:46 V26355JMV
<0.135 mg/Kg - dry 0.135 0.8302,6-Dinitrotoluene 1 11/11/22 19:46 V26355JMV
<0.179 mg/Kg - dry 0.179 0.415
Di-n-Octyl Phthalate 1 11/11/22 19:46 V26355JMV
<0.154 mg/Kg - dry 0.154 0.830Fluoranthene 1 11/11/22 19:46 V26355JMV
<0.161 mg/Kg - dry 0.161 0.830Fluorene 1 11/11/22 19:46 V26355JMV
<0.133 mg/Kg - dry 0.133 0.830Hexachlorobenzene 1 11/11/22 19:46 V26355JMV
<0.122 mg/Kg - dry 0.122 0.830Hexachlorobutadiene 1 11/11/22 19:46 V26355JMV
<0.197 mg/Kg - dry 0.197 0.830Hexachlorocyclopentadiene 1 11/11/22 19:46 V26355JMV
<0.099 mg/Kg - dry 0.099 0.830Hexachloroethane 1 11/11/22 19:46 V26355JMV
<0.225 mg/Kg - dry 0.225 0.830
Indeno(1,2,3-cd)pyrene 1 11/11/22 19:46 V26355JMV
<0.240 mg/Kg - dry 0.240 0.830Isophorone 1 11/11/22 19:46 V26355JMV
<0.133 mg/Kg - dry 0.133 0.8301-Methylnaphthalene 1 11/11/22 19:46 V26355JMV
<0.125 mg/Kg - dry 0.125 0.8302-Methylnaphthalene 1 11/11/22 19:46 V26355JMV
<0.122 mg/Kg - dry 0.122 0.8302-Methylphenol 1 11/11/22 19:46 V26355JMV
<0.106 mg/Kg - dry 0.106 0.8303&4 Methylphenol 1 11/11/22 19:46 V26355JMV
<0.181 mg/Kg - dry 0.181 0.830Naphthalene 1 11/11/22 19:46 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 108 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-14
92353 Matrix:
11/2/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.121 mg/Kg - dry 0.121 0.8302-Nitroaniline 1 11/11/22 19:46 V26355JMV
<0.150 mg/Kg - dry 0.150 0.8303-Nitroaniline 1 11/11/22 19:46 V26355JMV
<0.117 mg/Kg - dry 0.117 0.4154-Nitroaniline 1 11/11/22 19:46 V26355JMV
<0.145 mg/Kg - dry 0.145 0.415Nitrobenzene 1 11/11/22 19:46 V26355JMV
<0.111 mg/Kg - dry 0.111 0.8302-Nitrophenol 1 11/11/22 19:46 V26355JMV
<0.147 mg/Kg - dry 0.147 0.8304-Nitrophenol 1 11/11/22 19:46 V26355JMV
<0.330 mg/Kg - dry 0.330 0.830N-Nitrosodimethylamine 1 11/11/22 19:46 V26355JMV
<0.227 mg/Kg - dry 0.227 0.830N-Nitrosodiphenylamine 1 11/11/22 19:46 V26355JMV
<0.148 mg/Kg - dry 0.148 0.830
N-Nitroso-di-n-propylamine 1 11/11/22 19:46 V26355JMV
<0.436 mg/Kg - dry 0.436 1.26Pentachlorophenol 1 11/11/22 19:46 V26355JMV
<0.261 mg/Kg - dry 0.261 0.830Phenanthrene 1 11/11/22 19:46 V26355JMV
<0.140 mg/Kg - dry 0.140 0.830Phenol 1 11/11/22 19:46 V26355JMV
<0.168 mg/Kg - dry 0.168 0.830Pyrene 1 11/11/22 19:46 V26355JMV
<0.099 mg/Kg - dry 0.099 0.415Pyridine 1 11/11/22 19:46 V26355JMV
<0.134 mg/Kg - dry 0.134 0.8301,2,4-Trichlorobenzene 1 11/11/22 19:46 V26355JMV
<0.121 mg/Kg - dry 0.121 0.830
2,4,5-Trichlorophenol 1 11/11/22 19:46 V26355JMV
<0.121 mg/Kg - dry 0.121 0.8302,4,6-Trichlorophenol 1 11/11/22 19:46 V26355JMV
8270ESurrogate: Phenol-d5 77.5 Limits: 34-121%11/11/22 19:461 JMV
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%11/11/22 19:461 JMV V26355
Surrogate: 2-Fluorophenol 83.5 Limits: 35-115%11/11/22 19:461 JMV V26355
Surrogate: Nitrobenzene-d5 90.4 Limits: 37-122%11/11/22 19:461 JMV V26355
Surrogate: 4-Terphenyl-d14 112 Limits: 54-127%11/11/22 19:461 JMV V26355
Surrogate: 2,4,6-Tribromophenol 83.8 Limits: 39-132%11/11/22 19:461 JMV V26355
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 109 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.5 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.180 mg/Kg - dry 0.180 0.257Chromium, Hexavalent 1 11/16/22 15:44 SW-7199SAR
0.953 mg/Kg - dry 0.106 0.311Arsenic 5 11/15/22 00:46 6020BBKN
73.0 mg/Kg - dry 0.053 0.310Barium 5 11/11/22 23:47 6020BBKN
0.0484 J mg/Kg - dry 0.0321 0.311Cadmium 5 11/15/22 00:46 6020BBKN
38.6 mg/Kg - dry 0.720 1.55
Chromium 25 11/15/22 00:51 6020BBKN
5.24 mg/Kg - dry 0.0385 0.311Lead 5 11/15/22 00:46 6020BBKN
0.0717 mg/Kg - dry 0.0149 0.0373Mercury (Total)1 11/10/22 15:37 7471BEDV
0.414 mg/Kg - dry 0.127 0.310Selenium 5 11/15/22 00:46 6020BBKN
0.0160 J mg/Kg - dry 0.0083 0.311Silver 5 11/16/22 19:28 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 110 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.021 J mg/Kg - dry 0.002 0.024Acetone 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 11/09/22 00:13 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/09/22 00:13 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/09/22 00:13 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/09/22 00:13 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/09/22 00:13 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/09/22 00:13 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 111 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/09/22 00:13 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/09/22 00:13 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/09/22 00:13 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/09/22 00:13 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/09/22 00:13 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/09/22 00:13 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/09/22 00:13 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/09/22 00:13 V26116TBL
<0.017 mg/Kg - dry 0.017 0.310Ethanol 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/09/22 00:13 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/09/22 00:13 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 112 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/09/22 00:13 V26116TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/09/22 00:13 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/09/22 00:13 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/09/22 00:13 V26116TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/09/22 00:13 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/09/22 00:13 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 113 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/09/22 00:13 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/09/22 00:13 V26116TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/09/22 00:13 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/09/22 00:13 V26116
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/09/22 00:131 TBL V26116
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/09/22 00:131 TBL V26116
Surrogate: Toluene-d8 99.2 Limits: 76-129%11/09/22 00:131 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.144 mg/Kg - dry 0.144 0.819Acenaphthene 1 11/11/22 20:09 V26355JMV
<0.130 mg/Kg - dry 0.130 0.819Acenaphthylene 1 11/11/22 20:09 V26355JMV
<0.188 mg/Kg - dry 0.188 0.819Aniline 1 11/11/22 20:09 V26355JMV
<0.177 mg/Kg - dry 0.177 0.819Anthracene 1 11/11/22 20:09 V26355JMV
<0.172 mg/Kg - dry 0.172 0.819
Benzo(a)anthracene 1 11/11/22 20:09 V26355JMV
<0.182 mg/Kg - dry 0.182 0.819Benzo(a)pyrene 1 11/11/22 20:09 V26355JMV
<0.181 mg/Kg - dry 0.181 0.819Benzo(b)fluoranthene 1 11/11/22 20:09 V26355JMV
<0.168 mg/Kg - dry 0.168 0.819Benzo(g,h,i)perylene 1 11/11/22 20:09 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 114 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.170 mg/Kg - dry 0.170 0.819Benzo(k)fluoranthene 1 11/11/22 20:09 V26355JMV
<0.720 mg/Kg - dry 0.720 2.48Benzoic Acid 1 11/11/22 20:09 V26355JMV
<0.130 mg/Kg - dry 0.130 0.819Benzyl alcohol 1 11/11/22 20:09 V26355JMV
<0.146 mg/Kg - dry 0.146 0.819Bis(2-Chloroethoxy)methane 1 11/11/22 20:09 V26355JMV
<0.132 mg/Kg - dry 0.132 0.819Bis(2-Chloroethyl)ether 1 11/11/22 20:09 V26355JMV
<0.168 mg/Kg - dry 0.168 0.409Bis(2-Chloroisopropyl)ether 1 11/11/22 20:09 V26355JMV
<0.149 mg/Kg - dry 0.149 0.819Bis(2-ethylhexyl)phthalate 1 11/11/22 20:09 V26355JMV
<0.135 mg/Kg - dry 0.135 0.8194-Bromophenyl phenyl ether 1 11/11/22 20:09 V26355JMV
<0.140 mg/Kg - dry 0.140 0.409
Butyl benzyl phthalate 1 11/11/22 20:09 V26355JMV
<0.114 mg/Kg - dry 0.114 0.8194-Chloro-3-methylphenol 1 11/11/22 20:09 V26355JMV
<0.139 mg/Kg - dry 0.139 0.4094-Chloroaniline 1 11/11/22 20:09 V26355JMV
<0.144 mg/Kg - dry 0.144 0.8192-Chloronaphthalene 1 11/11/22 20:09 V26355JMV
<0.121 mg/Kg - dry 0.121 0.8192-Chlorophenol 1 11/11/22 20:09 V26355JMV
<0.156 mg/Kg - dry 0.156 1.244-Chlorophenyl phenyl ether 1 11/11/22 20:09 V26355JMV
<0.176 mg/Kg - dry 0.176 0.819Chrysene 1 11/11/22 20:09 V26355JMV
<0.285 mg/Kg - dry 0.285 0.819
Dibenz(a,h)anthracene 1 11/11/22 20:09 V26355JMV
<0.147 mg/Kg - dry 0.147 0.819Dibenzofuran 1 11/11/22 20:09 V26355JMV
<0.117 mg/Kg - dry 0.117 0.8191,2-Dichlorobenzene 1 11/11/22 20:09 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8191,3-Dichlorobenzene 1 11/11/22 20:09 V26355JMV
<0.121 mg/Kg - dry 0.121 0.4091,4-Dichlorobenzene 1 11/11/22 20:09 V26355JMV
<0.182 mg/Kg - dry 0.182 0.8193,3'-Dichlorobenzidine 1 11/11/22 20:09 V26355JMV
<0.119 mg/Kg - dry 0.119 0.8192,4-Dichlorophenol 1 11/11/22 20:09 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 115 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.223 mg/Kg - dry 0.223 0.819Diethyl phthalate 1 11/11/22 20:09 V26355JMV
<0.216 mg/Kg - dry 0.216 0.819Dimethyl phthalate 1 11/11/22 20:09 V26355JMV
<0.134 mg/Kg - dry 0.134 0.4092,4-Dimethylphenol 1 11/11/22 20:09 V26355JMV
<0.132 mg/Kg - dry 0.132 0.819Di-n-butyl phthalate 1 11/11/22 20:09 V26355JMV
<0.298 mg/Kg - dry 0.298 1.864,6-Dinitro-2-methylphenol 1 11/11/22 20:09 V26355JMV
<0.645 mg/Kg - dry 0.645 1.862,4-Dinitrophenol 1 11/11/22 20:09 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8192,4-Dinitrotoluene 1 11/11/22 20:09 V26355JMV
<0.134 mg/Kg - dry 0.134 0.8192,6-Dinitrotoluene 1 11/11/22 20:09 V26355JMV
<0.177 mg/Kg - dry 0.177 0.409
Di-n-Octyl Phthalate 1 11/11/22 20:09 V26355JMV
<0.152 mg/Kg - dry 0.152 0.819Fluoranthene 1 11/11/22 20:09 V26355JMV
<0.159 mg/Kg - dry 0.159 0.819Fluorene 1 11/11/22 20:09 V26355JMV
<0.131 mg/Kg - dry 0.131 0.819Hexachlorobenzene 1 11/11/22 20:09 V26355JMV
<0.121 mg/Kg - dry 0.121 0.819Hexachlorobutadiene 1 11/11/22 20:09 V26355JMV
<0.195 mg/Kg - dry 0.195 0.819Hexachlorocyclopentadiene 1 11/11/22 20:09 V26355JMV
<0.098 mg/Kg - dry 0.098 0.819Hexachloroethane 1 11/11/22 20:09 V26355JMV
<0.222 mg/Kg - dry 0.222 0.819
Indeno(1,2,3-cd)pyrene 1 11/11/22 20:09 V26355JMV
<0.237 mg/Kg - dry 0.237 0.819Isophorone 1 11/11/22 20:09 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8191-Methylnaphthalene 1 11/11/22 20:09 V26355JMV
<0.124 mg/Kg - dry 0.124 0.8192-Methylnaphthalene 1 11/11/22 20:09 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8192-Methylphenol 1 11/11/22 20:09 V26355JMV
<0.105 mg/Kg - dry 0.105 0.8193&4 Methylphenol 1 11/11/22 20:09 V26355JMV
<0.178 mg/Kg - dry 0.178 0.819Naphthalene 1 11/11/22 20:09 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 116 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-15
92354 Matrix:
11/2/2022 14:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.120 mg/Kg - dry 0.120 0.8192-Nitroaniline 1 11/11/22 20:09 V26355JMV
<0.149 mg/Kg - dry 0.149 0.8193-Nitroaniline 1 11/11/22 20:09 V26355JMV
<0.115 mg/Kg - dry 0.115 0.4094-Nitroaniline 1 11/11/22 20:09 V26355JMV
<0.144 mg/Kg - dry 0.144 0.409Nitrobenzene 1 11/11/22 20:09 V26355JMV
<0.110 mg/Kg - dry 0.110 0.8192-Nitrophenol 1 11/11/22 20:09 V26355JMV
<0.145 mg/Kg - dry 0.145 0.8194-Nitrophenol 1 11/11/22 20:09 V26355JMV
<0.326 mg/Kg - dry 0.326 0.819N-Nitrosodimethylamine 1 11/11/22 20:09 V26355JMV
<0.224 mg/Kg - dry 0.224 0.819N-Nitrosodiphenylamine 1 11/11/22 20:09 V26355JMV
<0.146 mg/Kg - dry 0.146 0.819
N-Nitroso-di-n-propylamine 1 11/11/22 20:09 V26355JMV
<0.431 mg/Kg - dry 0.431 1.24Pentachlorophenol 1 11/11/22 20:09 V26355JMV
<0.258 mg/Kg - dry 0.258 0.819Phenanthrene 1 11/11/22 20:09 V26355JMV
<0.139 mg/Kg - dry 0.139 0.819Phenol 1 11/11/22 20:09 V26355JMV
<0.166 mg/Kg - dry 0.166 0.819Pyrene 1 11/11/22 20:09 V26355JMV
<0.098 mg/Kg - dry 0.098 0.409Pyridine 1 11/11/22 20:09 V26355JMV
<0.132 mg/Kg - dry 0.132 0.8191,2,4-Trichlorobenzene 1 11/11/22 20:09 V26355JMV
<0.119 mg/Kg - dry 0.119 0.819
2,4,5-Trichlorophenol 1 11/11/22 20:09 V26355JMV
<0.120 mg/Kg - dry 0.120 0.8192,4,6-Trichlorophenol 1 11/11/22 20:09 V26355JMV
8270ESurrogate: Phenol-d5 81.4 Limits: 34-121%11/11/22 20:091 JMV
Surrogate: 2-Fluorobiphenyl 102 Limits: 44-115%11/11/22 20:091 JMV V26355
Surrogate: 2-Fluorophenol 87.7 Limits: 35-115%11/11/22 20:091 JMV V26355
Surrogate: Nitrobenzene-d5 94.6 Limits: 37-122%11/11/22 20:091 JMV V26355
Surrogate: 4-Terphenyl-d14 117 Limits: 54-127%11/11/22 20:091 JMV V26355
Surrogate: 2,4,6-Tribromophenol 84.7 Limits: 39-132%11/11/22 20:091 JMV V26355
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 117 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.9 %Moisture 1 11/08/22 18:09 SW-DRYWTAMB
<0.185 mg/Kg - dry 0.185 0.262Chromium, Hexavalent 1 11/16/22 15:55 SW-7199SAR
1.48 mg/Kg - dry 0.112 0.329Arsenic 5 11/15/22 01:04 6020BBKN
46.1 mg/Kg - dry 0.056 0.328Barium 5 11/11/22 23:51 6020BBKN
0.0616 J mg/Kg - dry 0.0340 0.329Cadmium 5 11/15/22 01:04 6020BBKN
33.5 mg/Kg - dry 0.152 0.328
Chromium 5 11/15/22 19:42 6020BCPW
10.4 mg/Kg - dry 0.0407 0.329Lead 5 11/15/22 01:04 6020BBKN
0.0937 mg/Kg - dry 0.0158 0.0394Mercury (Total)1 11/10/22 15:46 7471BEDV
0.638 mg/Kg - dry 0.135 0.328Selenium 5 11/15/22 01:04 6020BBKN
0.0161 J mg/Kg - dry 0.0088 0.329Silver 5 11/16/22 19:33 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 118 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
0.044 mg/Kg - dry 0.003 0.026Acetone 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 11/09/22 00:40 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/09/22 00:40 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/09/22 00:40 V26116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/09/22 00:40 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/09/22 00:40 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/09/22 00:40 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/09/22 00:40 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 119 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/09/22 00:40 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/09/22 00:40 V26116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/09/22 00:40 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/09/22 00:40 V26116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/09/22 00:40 V26116TBL
<0.018 mg/Kg - dry 0.018 0.328Ethanol 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/09/22 00:40 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 120 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/09/22 00:40 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/09/22 00:40 V26116TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/09/22 00:40 V26116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/09/22 00:40 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 11/09/22 00:40 V26116TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/09/22 00:40 V26116TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/09/22 00:40 V26116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/09/22 00:40 V26116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 121 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26115 11/08/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/09/22 00:40 V26116TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/09/22 00:40 V26116TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/09/22 00:40 V26116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/09/22 00:40 V26116
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/09/22 00:401 TBL V26116
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/09/22 00:401 TBL V26116
Surrogate: Toluene-d8 99.4 Limits: 76-129%11/09/22 00:401 TBL V26116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.152 mg/Kg - dry 0.152 0.867Acenaphthene 1 11/11/22 20:31 V26355JMV
<0.137 mg/Kg - dry 0.137 0.867Acenaphthylene 1 11/11/22 20:31 V26355JMV
<0.199 mg/Kg - dry 0.199 0.867Aniline 1 11/11/22 20:31 V26355JMV
<0.187 mg/Kg - dry 0.187 0.867Anthracene 1 11/11/22 20:31 V26355JMV
<0.182 mg/Kg - dry 0.182 0.867
Benzo(a)anthracene 1 11/11/22 20:31 V26355JMV
<0.193 mg/Kg - dry 0.193 0.867Benzo(a)pyrene 1 11/11/22 20:31 V26355JMV
<0.191 mg/Kg - dry 0.191 0.867Benzo(b)fluoranthene 1 11/11/22 20:31 V26355JMV
<0.178 mg/Kg - dry 0.178 0.867Benzo(g,h,i)perylene 1 11/11/22 20:31 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 122 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.180 mg/Kg - dry 0.180 0.867Benzo(k)fluoranthene 1 11/11/22 20:31 V26355JMV
<0.762 mg/Kg - dry 0.762 2.63Benzoic Acid 1 11/11/22 20:31 V26355JMV
<0.137 mg/Kg - dry 0.137 0.867Benzyl alcohol 1 11/11/22 20:31 V26355JMV
<0.155 mg/Kg - dry 0.155 0.867Bis(2-Chloroethoxy)methane 1 11/11/22 20:31 V26355JMV
<0.140 mg/Kg - dry 0.140 0.867Bis(2-Chloroethyl)ether 1 11/11/22 20:31 V26355JMV
<0.178 mg/Kg - dry 0.178 0.433Bis(2-Chloroisopropyl)ether 1 11/11/22 20:31 V26355JMV
<0.157 mg/Kg - dry 0.157 0.867Bis(2-ethylhexyl)phthalate 1 11/11/22 20:31 V26355JMV
<0.143 mg/Kg - dry 0.143 0.8674-Bromophenyl phenyl ether 1 11/11/22 20:31 V26355JMV
0.395 J
mg/Kg - dry 0.148 0.433
Butyl benzyl phthalate 1 11/11/22 20:31 V26355JMV
<0.121 mg/Kg - dry 0.121 0.8674-Chloro-3-methylphenol 1 11/11/22 20:31 V26355JMV
<0.147 mg/Kg - dry 0.147 0.4334-Chloroaniline 1 11/11/22 20:31 V26355JMV
<0.152 mg/Kg - dry 0.152 0.8672-Chloronaphthalene 1 11/11/22 20:31 V26355JMV
<0.129 mg/Kg - dry 0.129 0.8672-Chlorophenol 1 11/11/22 20:31 V26355JMV
<0.165 mg/Kg - dry 0.165 1.314-Chlorophenyl phenyl ether 1 11/11/22 20:31 V26355JMV
<0.186 mg/Kg - dry 0.186 0.867Chrysene 1 11/11/22 20:31 V26355JMV
<0.302 mg/Kg - dry 0.302 0.867
Dibenz(a,h)anthracene 1 11/11/22 20:31 V26355JMV
<0.156 mg/Kg - dry 0.156 0.867Dibenzofuran 1 11/11/22 20:31 V26355JMV
<0.124 mg/Kg - dry 0.124 0.8671,2-Dichlorobenzene 1 11/11/22 20:31 V26355JMV
<0.127 mg/Kg - dry 0.127 0.8671,3-Dichlorobenzene 1 11/11/22 20:31 V26355JMV
<0.128 mg/Kg - dry 0.128 0.4331,4-Dichlorobenzene 1 11/11/22 20:31 V26355JMV
<0.193 mg/Kg - dry 0.193 0.8673,3'-Dichlorobenzidine 1 11/11/22 20:31 V26355JMV
<0.125 mg/Kg - dry 0.125 0.8672,4-Dichlorophenol 1 11/11/22 20:31 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 123 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.236 mg/Kg - dry 0.236 0.867Diethyl phthalate 1 11/11/22 20:31 V26355JMV
<0.228 mg/Kg - dry 0.228 0.867Dimethyl phthalate 1 11/11/22 20:31 V26355JMV
<0.141 mg/Kg - dry 0.141 0.4332,4-Dimethylphenol 1 11/11/22 20:31 V26355JMV
<0.140 mg/Kg - dry 0.140 0.867Di-n-butyl phthalate 1 11/11/22 20:31 V26355JMV
<0.315 mg/Kg - dry 0.315 1.974,6-Dinitro-2-methylphenol 1 11/11/22 20:31 V26355JMV
<0.683 mg/Kg - dry 0.683 1.972,4-Dinitrophenol 1 11/11/22 20:31 V26355JMV
<0.126 mg/Kg - dry 0.126 0.8672,4-Dinitrotoluene 1 11/11/22 20:31 V26355JMV
<0.141 mg/Kg - dry 0.141 0.8672,6-Dinitrotoluene 1 11/11/22 20:31 V26355JMV
<0.187 mg/Kg - dry 0.187 0.433
Di-n-Octyl Phthalate 1 11/11/22 20:31 V26355JMV
<0.161 mg/Kg - dry 0.161 0.867Fluoranthene 1 11/11/22 20:31 V26355JMV
<0.168 mg/Kg - dry 0.168 0.867Fluorene 1 11/11/22 20:31 V26355JMV
<0.139 mg/Kg - dry 0.139 0.867Hexachlorobenzene 1 11/11/22 20:31 V26355JMV
<0.128 mg/Kg - dry 0.128 0.867Hexachlorobutadiene 1 11/11/22 20:31 V26355JMV
<0.206 mg/Kg - dry 0.206 0.867Hexachlorocyclopentadiene 1 11/11/22 20:31 V26355JMV
<0.104 mg/Kg - dry 0.104 0.867Hexachloroethane 1 11/11/22 20:31 V26355JMV
<0.235 mg/Kg - dry 0.235 0.867
Indeno(1,2,3-cd)pyrene 1 11/11/22 20:31 V26355JMV
<0.250 mg/Kg - dry 0.250 0.867Isophorone 1 11/11/22 20:31 V26355JMV
<0.139 mg/Kg - dry 0.139 0.8671-Methylnaphthalene 1 11/11/22 20:31 V26355JMV
<0.131 mg/Kg - dry 0.131 0.8672-Methylnaphthalene 1 11/11/22 20:31 V26355JMV
<0.127 mg/Kg - dry 0.127 0.8672-Methylphenol 1 11/11/22 20:31 V26355JMV
<0.111 mg/Kg - dry 0.111 0.8673&4 Methylphenol 1 11/11/22 20:31 V26355JMV
<0.189 mg/Kg - dry 0.189 0.867Naphthalene 1 11/11/22 20:31 V26355JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 124 of 170
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-307-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/03/2022
BOU-012
Report Date : 11/17/2022
Sample ID :
Lab No :
Sampled:FG-DUP
92355 Matrix:
11/2/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V26228 11/09/22 10:30
<0.127 mg/Kg - dry 0.127 0.8672-Nitroaniline 1 11/11/22 20:31 V26355JMV
<0.157 mg/Kg - dry 0.157 0.8673-Nitroaniline 1 11/11/22 20:31 V26355JMV
<0.122 mg/Kg - dry 0.122 0.4334-Nitroaniline 1 11/11/22 20:31 V26355JMV
<0.152 mg/Kg - dry 0.152 0.433Nitrobenzene 1 11/11/22 20:31 V26355JMV
<0.116 mg/Kg - dry 0.116 0.8672-Nitrophenol 1 11/11/22 20:31 V26355JMV
<0.153 mg/Kg - dry 0.153 0.8674-Nitrophenol 1 11/11/22 20:31 V26355JMV
<0.345 mg/Kg - dry 0.345 0.867N-Nitrosodimethylamine 1 11/11/22 20:31 V26355JMV
<0.237 mg/Kg - dry 0.237 0.867N-Nitrosodiphenylamine 1 11/11/22 20:31 V26355JMV
<0.155 mg/Kg - dry 0.155 0.867
N-Nitroso-di-n-propylamine 1 11/11/22 20:31 V26355JMV
<0.455 mg/Kg - dry 0.455 1.31Pentachlorophenol 1 11/11/22 20:31 V26355JMV
<0.273 mg/Kg - dry 0.273 0.867Phenanthrene 1 11/11/22 20:31 V26355JMV
<0.147 mg/Kg - dry 0.147 0.867Phenol 1 11/11/22 20:31 V26355JMV
<0.176 mg/Kg - dry 0.176 0.867Pyrene 1 11/11/22 20:31 V26355JMV
<0.104 mg/Kg - dry 0.104 0.433Pyridine 1 11/11/22 20:31 V26355JMV
<0.140 mg/Kg - dry 0.140 0.8671,2,4-Trichlorobenzene 1 11/11/22 20:31 V26355JMV
<0.126 mg/Kg - dry 0.126 0.867
2,4,5-Trichlorophenol 1 11/11/22 20:31 V26355JMV
<0.126 mg/Kg - dry 0.126 0.8672,4,6-Trichlorophenol 1 11/11/22 20:31 V26355JMV
8270ESurrogate: Phenol-d5 77.8 Limits: 34-121%11/11/22 20:311 JMV
Surrogate: 2-Fluorobiphenyl 98.8 Limits: 44-115%11/11/22 20:311 JMV V26355
Surrogate: 2-Fluorophenol 81.7 Limits: 35-115%11/11/22 20:311 JMV V26355
Surrogate: Nitrobenzene-d5 89.2 Limits: 37-122%11/11/22 20:311 JMV V26355
Surrogate: 4-Terphenyl-d14 113 Limits: 54-127%11/11/22 20:311 JMV V26355
Surrogate: 2,4,6-Tribromophenol 77.8 Limits: 39-132%11/11/22 20:311 JMV V26355
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 125 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Metals Analyses
6020B
L648608,L648858,L649090,L649337QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L647906
Associated Lab Samples: 92342, 92343, 92344, 92345, 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-L647906 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/14/22 22:110.2500.0855<0.0855mg/KgArsenic
11/11/22 22:220.2500.042<0.042mg/KgBarium
11/14/22 22:110.2500.0259<0.0259mg/KgCadmium
11/14/22 22:110.2500.116<0.116mg/KgChromium
11/11/22 22:220.2500.0310<0.0310mg/KgLead
11/14/22 22:110.2500.103<0.103mg/KgSelenium
11/16/22 17:510.2500.0067<0.0067mg/KgSilver
LCS-L647906Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.02.442.50mg/KgArsenic 80-120
89.04.435.00mg/KgBarium 80-120
97.00.4850.500mg/KgCadmium 80-120
1095.435.00mg/KgChromium 80-120
96.02.402.50mg/KgLead 80-120
97.04.865.00mg/KgSelenium 80-120
93.00.4650.500mg/KgSilver 80-120
L 87550-MS-L647906 L 87550-MSD-L647906Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.81 90.02.812.492.340.695mg/KgArsenic 85.0 75-125 0.0 80
7.54 73.0*8.234.994.684.13mg/KgBarium 82.0 75-125 8.7 80
0.881 95.00.9240.4990.4680.438mg/KgCadmium 97.0 75-125 4.7 80
6.02 93.05.974.994.681.65mg/KgChromium 87.0 75-125 0.8 80
Page 1 of 42Date:11/17/2022 12:34 PM
Page 126 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Metals Analyses
6020B
L648608,L648858,L649090,L649337QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L647906
L 87550-MS-L647906 L 87550-MSD-L647906Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
13.6 51.0*14.32.492.3412.4mg/KgLead 76.0 75-125 5.0 80
4.16 89.04.294.994.68<0.103mg/KgSelenium 86.0 75-125 3.0 80
0.334 70.0*0.3070.4990.4680.0081mg/KgSilver 60.0*75-125 8.4 80
L 87550-PDS-L647906Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/15/22 01:401101.43mg/KgArsenic
11/12/22 00:161012.90mg/KgBarium
11/15/22 01:401060.306mg/KgCadmium
11/15/22 20:041032.69mg/KgChromium
11/15/22 01:401042.57mg/KgLead
11/15/22 01:401092.67mg/KgSelenium
11/16/22 19:5599.00.243mg/KgSilver
Page 2 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 127 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V26234QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V26193
Associated Lab Samples: 92342, 92343, 92344, 92345, 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-V26193 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/10/22 14:400.03000.0120<0.0120mg/KgMercury (Total)
LCS-V26193Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.4330.417mg/KgMercury (Total)80-120
V 92245-MS-V26193 V 92245-MSD-V26193Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.445 96.00.4510.4170.4170.0444mg/KgMercury (Total)98.0 80-120 1.3 20
V 92245-PDS-V26193Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/10/22 14:561010.233mg/KgMercury (Total)
Page 3 of 42Date:11/17/2022 12:34 PM
Page 128 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
Associated Lab Samples: 92342, 92343
LRB-V25973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0200.002<0.002mg/KgAcetone
11/06/22 14:050.0200.001<0.001mg/KgAcrolein
11/06/22 14:050.0200.0008<0.0008mg/KgAcrylonitrile
11/06/22 14:050.0050.0006<0.0006mg/KgBenzene
11/06/22 14:050.0050.0005<0.0005mg/KgBromobenzene
11/06/22 14:050.0050.0008<0.0008mg/KgBromochloromethane
11/06/22 14:050.0050.001<0.001mg/KgBromodichloromethane
11/06/22 14:050.0050.001<0.001mg/KgBromoform
11/06/22 14:050.0100.001<0.001mg/KgBromomethane
11/06/22 14:050.0050.0005<0.0005mg/Kgn-Butylbenzene
11/06/22 14:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/06/22 14:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/06/22 14:050.0050.0006<0.0006mg/KgCarbon Disulfide
11/06/22 14:050.0050.001<0.001mg/KgCarbon Tetrachloride
11/06/22 14:050.0050.0007<0.0007mg/KgChlorobenzene
11/06/22 14:050.0050.0009<0.0009mg/KgChlorodibromomethane
11/06/22 14:050.0100.0009<0.0009mg/KgChloroethane
11/06/22 14:050.0050.001<0.001mg/KgChloroform
11/06/22 14:050.0100.0006<0.0006mg/KgChloromethane
11/06/22 14:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/06/22 14:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/06/22 14:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/06/22 14:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/06/22 14:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/06/22 14:050.0050.0006<0.0006mg/KgDibromomethane
11/06/22 14:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/06/22 14:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 42Date:11/17/2022 12:34 PM
Page 129 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
Associated Lab Samples: 92342, 92343
LRB-V25973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/06/22 14:050.0100.001<0.001mg/KgDichlorodifluoromethane
11/06/22 14:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/06/22 14:050.0050.001<0.001mg/Kg1,2-Dichloroethane
11/06/22 14:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/06/22 14:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/06/22 14:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/06/22 14:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/06/22 14:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/06/22 14:050.0050.001<0.001mg/Kg2,2-Dichloropropane
11/06/22 14:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/06/22 14:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/06/22 14:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/06/22 14:050.2500.014<0.014mg/KgEthanol
11/06/22 14:050.0050.0006<0.0006mg/KgEthylbenzene
11/06/22 14:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/06/22 14:050.0100.0008<0.0008mg/KgHexachlorobutadiene
11/06/22 14:050.0100.0007<0.0007mg/Kgn-Hexane
11/06/22 14:050.0200.0006<0.0006mg/Kg2-Hexanone
11/06/22 14:050.0050.0005<0.0005mg/KgIsopropylbenzene
11/06/22 14:050.0050.001<0.001mg/Kg4-Isopropyl toluene
11/06/22 14:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/06/22 14:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/06/22 14:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/06/22 14:050.0100.001<0.001mg/KgMethylene Chloride
11/06/22 14:050.0100.0010<0.0010mg/KgNaphthalene
11/06/22 14:050.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 42Date:11/17/2022 12:34 PM
Page 130 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
Associated Lab Samples: 92342, 92343
LRB-V25973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0050.001<0.001mg/KgStyrene
11/06/22 14:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/06/22 14:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/06/22 14:050.0050.0009<0.0009mg/KgTetrachloroethene
11/06/22 14:050.0050.0007<0.0007mg/KgToluene
11/06/22 14:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/06/22 14:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/06/22 14:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/06/22 14:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/06/22 14:050.0050.0009<0.0009mg/KgTrichloroethene
11/06/22 14:050.0100.002<0.002mg/KgTrichlorofluoromethane
11/06/22 14:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/06/22 14:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/06/22 14:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/06/22 14:050.0100.0005<0.0005mg/KgVinyl Acetate
11/06/22 14:050.0100.0005<0.0005mg/KgVinyl Chloride
11/06/22 14:050.0050.0005<0.0005mg/Kgo-Xylene
11/06/22 14:050.0100.001<0.001mg/Kgm,p-Xylene
11/06/22 14:054-Bromofluorobenzene (S)109 70-130
11/06/22 14:05Dibromofluoromethane (S)112 84-123
11/06/22 14:05Toluene-d8 (S)117 76-129
LCS-V25973 LCSD-V25973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.089 89.395.30.0950.100mg/KgAcetone 29-198 6.5 20
Page 6 of 42Date:11/17/2022 12:34 PM
Page 131 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
LCS-V25973 LCSD-V25973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.076 76.476.20.0760.100mg/KgAcrolein 70-130 0.2 20
0.091 91.691.90.0910.100mg/KgAcrylonitrile 65-134 0.3 20
0.046 92.092.20.0460.050mg/KgBenzene 74-127 0.2 20
0.054 1081070.0530.050mg/KgBromobenzene 73-125 0.9 20
0.037 75.673.00.0360.050mg/KgBromochloromethane 72-134 3.4 20
0.044 88.090.80.0450.050mg/KgBromodichloromethane 75-122 3.1 20
0.050 1011060.0530.050mg/KgBromoform 66-135 5.4 20
0.043 87.884.80.0420.050mg/KgBromomethane 20-180 3.4 20
0.054 1101110.0550.050mg/Kgn-Butylbenzene 65-135 1.6 20
0.054 1081090.0540.050mg/Kgsec-Butyl benzene 66-131 0.9 20
0.053 1081090.0540.050mg/Kgtert-Butyl benzene 67-132 1.4 20
0.032 65.264.60.0320.050mg/KgCarbon Disulfide 61-129 0.9 20
0.040 81.283.40.0410.050mg/KgCarbon Tetrachloride 64-143 2.6 20
0.043 87.691.40.0450.050mg/KgChlorobenzene 74-118 4.2 20
0.049 99.21000.0500.050mg/KgChlorodibromomethane 73-122 0.8 20
0.035 70.071.60.0350.050mg/KgChloroethane 33-149 2.2 20
0.038 77.280.60.0400.050mg/KgChloroform 73-127 4.3 20
0.039 79.479.60.0390.050mg/KgChloromethane 45-143 0.2 20
0.052 1051090.0540.050mg/Kg2-Chlorotoluene 67-124 3.9 20
0.052 1051090.0540.050mg/Kg4-Chlorotoluene 71-126 4.1 20
0.043 86.083.40.0410.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.0 20
0.054 1091150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.1 20
0.049 98.61000.0500.050mg/Kg1,2-Dibromoethane 70-132 1.4 20
0.038 77.479.60.0390.050mg/KgDibromomethane 74-133 2.8 20
0.053 1071100.0550.050mg/Kg1,2-Dichlorobenzene 72-123 2.5 20
0.052 1051090.0540.050mg/Kg1,3-Dichlorobenzene 71-120 3.3 20
Page 7 of 42Date:11/17/2022 12:34 PM
Page 132 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
LCS-V25973 LCSD-V25973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1061080.0540.050mg/Kg1,4-Dichlorobenzene 71-123 2.6 20
0.035 70.478.20.0390.050mg/KgDichlorodifluoromethane 26-146 10.4 20
0.037 74.874.40.0370.050mg/Kg1,1-Dichloroethane 74-127 0.5 20
0.044 88.290.20.0450.050mg/Kg1,2-Dichloroethane 68-128 2.2 20
0.037 74.478.00.0390.050mg/Kg1,1-Dichloroethene 67-149 4.7 20
0.039 79.480.80.0400.050mg/Kgcis-1,2-Dichloroethene 76-134 1.7 20
0.038 76.279.80.0390.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.038 77.674.00.0370.050mg/Kg1,2-Dichloropropane 73-130 4.7 20
0.046 92.095.60.0470.050mg/Kg1,3-Dichloropropane 75-124 3.8 20
0.039 79.682.20.0410.050mg/Kg2,2-Dichloropropane 50-142 3.2 20
0.036 72.271.00.0350.050mg/Kg1,1-Dichloropropene 71-130 1.6 20
0.040 80.482.00.0410.050mg/Kgcis-1,3-Dichloropropene 71-125 1.9 20
0.042 84.683.80.0410.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.9 20
1.20 96.091.21.141.25mg/KgEthanol 70-130 5.1 20
0.045 91.093.40.0460.050mg/KgEthylbenzene 74-128 2.6 20
0.082 82.781.70.0810.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.2 20
0.054 1101140.0570.050mg/KgHexachlorobutadiene 64-125 4.1 20
0.036 73.872.60.0360.050mg/Kgn-Hexane 70-130 1.6 20
0.057 1151170.0580.050mg/Kg2-Hexanone 61-157 2.4 20
0.052 1041060.0530.050mg/KgIsopropylbenzene 68-126 1.9 20
0.052 1061080.0530.050mg/Kg4-Isopropyl toluene 68-129 1.8 20
0.046 93.293.20.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.0 20
0.041 83.481.00.0400.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.9 20
0.052 1051040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 1.1 20
0.040 80.279.60.0390.050mg/KgMethylene Chloride 74-129 0.7 20
0.052 1061080.0530.050mg/KgNaphthalene 57-157 1.8 20
Page 8 of 42Date:11/17/2022 12:34 PM
Page 133 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25973
LCS-V25973 LCSD-V25973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.054 1091090.0540.050mg/Kgn-Propylbenzene 67-130 0.0 20
0.046 92.698.20.0490.050mg/KgStyrene 77-121 5.8 20
0.046 93.695.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.4 20
0.055 1111080.0530.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.7 20
0.036 73.075.40.0370.050mg/KgTetrachloroethene 68-130 3.2 20
0.035 71.471.20.0350.050mg/KgToluene 71-129 0.2 20
0.055 1101100.0540.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.3 20
0.056 1121120.0550.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.3 20
0.040 81.683.00.0410.050mg/Kg1,1,1-Trichloroethane 67-131 1.7 20
0.046 93.294.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.037 75.075.00.0370.050mg/KgTrichloroethene 75-133 0.0 20
0.040 81.686.00.0430.050mg/KgTrichlorofluoromethane 44-146 5.2 20
0.060 1211250.0620.050mg/Kg1,2,3-Trichloropropane 60-137 3.2 20
0.053 1071090.0540.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.2 20
0.053 1081080.0530.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.0 20
0.036 73.868.80.0340.050mg/KgVinyl Acetate 60-140 7.0 20
0.034 69.273.00.0360.050mg/KgVinyl Chloride 48-147 5.3 20
0.047 94.699.20.0490.050mg/Kgo-Xylene 74-126 4.7 20
0.090 90.694.20.0940.100mg/Kgm,p-Xylene 75-124 3.8 20
1051064-Bromofluorobenzene (S)70-130
111109Dibromofluoromethane (S)84-123
112111Toluene-d8 (S)76-129
Page 9 of 42Date:11/17/2022 12:34 PM
Page 134 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
Associated Lab Samples: 92344, 92345
LRB-V25975 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0200.002<0.002mg/KgAcetone
11/06/22 14:050.0200.001<0.001mg/KgAcrolein
11/06/22 14:050.0200.0008<0.0008mg/KgAcrylonitrile
11/06/22 14:050.0050.0006<0.0006mg/KgBenzene
11/06/22 14:050.0050.0005<0.0005mg/KgBromobenzene
11/06/22 14:050.0050.0008<0.0008mg/KgBromochloromethane
11/06/22 14:050.0050.001<0.001mg/KgBromodichloromethane
11/06/22 14:050.0050.001<0.001mg/KgBromoform
11/06/22 14:050.0100.001<0.001mg/KgBromomethane
11/06/22 14:050.0050.0005<0.0005mg/Kgn-Butylbenzene
11/06/22 14:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/06/22 14:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/06/22 14:050.0050.0006<0.0006mg/KgCarbon Disulfide
11/06/22 14:050.0050.001<0.001mg/KgCarbon Tetrachloride
11/06/22 14:050.0050.0007<0.0007mg/KgChlorobenzene
11/06/22 14:050.0050.0009<0.0009mg/KgChlorodibromomethane
11/06/22 14:050.0100.0009<0.0009mg/KgChloroethane
11/06/22 14:050.0050.001<0.001mg/KgChloroform
11/06/22 14:050.0100.0006<0.0006mg/KgChloromethane
11/06/22 14:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/06/22 14:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/06/22 14:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/06/22 14:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/06/22 14:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/06/22 14:050.0050.0006<0.0006mg/KgDibromomethane
11/06/22 14:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/06/22 14:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 42Date:11/17/2022 12:34 PM
Page 135 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
Associated Lab Samples: 92344, 92345
LRB-V25975 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/06/22 14:050.0100.001<0.001mg/KgDichlorodifluoromethane
11/06/22 14:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/06/22 14:050.0050.001<0.001mg/Kg1,2-Dichloroethane
11/06/22 14:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/06/22 14:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/06/22 14:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/06/22 14:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/06/22 14:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/06/22 14:050.0050.001<0.001mg/Kg2,2-Dichloropropane
11/06/22 14:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/06/22 14:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/06/22 14:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/06/22 14:050.2500.014<0.014mg/KgEthanol
11/06/22 14:050.0050.0006<0.0006mg/KgEthylbenzene
11/06/22 14:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/06/22 14:050.0100.0008<0.0008mg/KgHexachlorobutadiene
11/06/22 14:050.0100.0007<0.0007mg/Kgn-Hexane
11/06/22 14:050.0200.0006<0.0006mg/Kg2-Hexanone
11/06/22 14:050.0050.0005<0.0005mg/KgIsopropylbenzene
11/06/22 14:050.0050.001<0.001mg/Kg4-Isopropyl toluene
11/06/22 14:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/06/22 14:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/06/22 14:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/06/22 14:050.0100.001<0.001mg/KgMethylene Chloride
11/06/22 14:050.0100.0010<0.0010mg/KgNaphthalene
11/06/22 14:050.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 11 of 42Date:11/17/2022 12:34 PM
Page 136 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
Associated Lab Samples: 92344, 92345
LRB-V25975 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/06/22 14:050.0050.001<0.001mg/KgStyrene
11/06/22 14:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/06/22 14:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/06/22 14:050.0050.0009<0.0009mg/KgTetrachloroethene
11/06/22 14:050.0050.0007<0.0007mg/KgToluene
11/06/22 14:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/06/22 14:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/06/22 14:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/06/22 14:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/06/22 14:050.0050.0009<0.0009mg/KgTrichloroethene
11/06/22 14:050.0100.002<0.002mg/KgTrichlorofluoromethane
11/06/22 14:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/06/22 14:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/06/22 14:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/06/22 14:050.0100.0005<0.0005mg/KgVinyl Acetate
11/06/22 14:050.0100.0005<0.0005mg/KgVinyl Chloride
11/06/22 14:050.0050.0005<0.0005mg/Kgo-Xylene
11/06/22 14:050.0100.001<0.001mg/Kgm,p-Xylene
11/06/22 14:054-Bromofluorobenzene (S)109 70-130
11/06/22 14:05Dibromofluoromethane (S)112 84-123
11/06/22 14:05Toluene-d8 (S)117 76-129
LCS-V25975 LCSD-V25975Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.089 89.395.30.0950.100mg/KgAcetone 29-198 6.5 20
Page 12 of 42Date:11/17/2022 12:34 PM
Page 137 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
LCS-V25975 LCSD-V25975Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.076 76.476.20.0760.100mg/KgAcrolein 70-130 0.2 20
0.091 91.691.90.0910.100mg/KgAcrylonitrile 65-134 0.3 20
0.046 92.092.20.0460.050mg/KgBenzene 74-127 0.2 20
0.054 1081070.0530.050mg/KgBromobenzene 73-125 0.9 20
0.037 75.673.00.0360.050mg/KgBromochloromethane 72-134 3.4 20
0.044 88.090.80.0450.050mg/KgBromodichloromethane 75-122 3.1 20
0.050 1011060.0530.050mg/KgBromoform 66-135 5.4 20
0.043 87.884.80.0420.050mg/KgBromomethane 20-180 3.4 20
0.054 1101110.0550.050mg/Kgn-Butylbenzene 65-135 1.6 20
0.054 1081090.0540.050mg/Kgsec-Butyl benzene 66-131 0.9 20
0.053 1081090.0540.050mg/Kgtert-Butyl benzene 67-132 1.4 20
0.032 65.264.60.0320.050mg/KgCarbon Disulfide 61-129 0.9 20
0.040 81.283.40.0410.050mg/KgCarbon Tetrachloride 64-143 2.6 20
0.043 87.691.40.0450.050mg/KgChlorobenzene 74-118 4.2 20
0.049 99.21000.0500.050mg/KgChlorodibromomethane 73-122 0.8 20
0.035 70.071.60.0350.050mg/KgChloroethane 33-149 2.2 20
0.038 77.280.60.0400.050mg/KgChloroform 73-127 4.3 20
0.039 79.479.60.0390.050mg/KgChloromethane 45-143 0.2 20
0.052 1051090.0540.050mg/Kg2-Chlorotoluene 67-124 3.9 20
0.052 1051090.0540.050mg/Kg4-Chlorotoluene 71-126 4.1 20
0.043 86.083.40.0410.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.0 20
0.054 1091150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.1 20
0.049 98.61000.0500.050mg/Kg1,2-Dibromoethane 70-132 1.4 20
0.038 77.479.60.0390.050mg/KgDibromomethane 74-133 2.8 20
0.053 1071100.0550.050mg/Kg1,2-Dichlorobenzene 72-123 2.5 20
0.052 1051090.0540.050mg/Kg1,3-Dichlorobenzene 71-120 3.3 20
Page 13 of 42Date:11/17/2022 12:34 PM
Page 138 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
LCS-V25975 LCSD-V25975Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1061080.0540.050mg/Kg1,4-Dichlorobenzene 71-123 2.6 20
0.035 70.478.20.0390.050mg/KgDichlorodifluoromethane 26-146 10.4 20
0.037 74.874.40.0370.050mg/Kg1,1-Dichloroethane 74-127 0.5 20
0.044 88.290.20.0450.050mg/Kg1,2-Dichloroethane 68-128 2.2 20
0.037 74.478.00.0390.050mg/Kg1,1-Dichloroethene 67-149 4.7 20
0.039 79.480.80.0400.050mg/Kgcis-1,2-Dichloroethene 76-134 1.7 20
0.038 76.279.80.0390.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.038 77.674.00.0370.050mg/Kg1,2-Dichloropropane 73-130 4.7 20
0.046 92.095.60.0470.050mg/Kg1,3-Dichloropropane 75-124 3.8 20
0.039 79.682.20.0410.050mg/Kg2,2-Dichloropropane 50-142 3.2 20
0.036 72.271.00.0350.050mg/Kg1,1-Dichloropropene 71-130 1.6 20
0.040 80.482.00.0410.050mg/Kgcis-1,3-Dichloropropene 71-125 1.9 20
0.042 84.683.80.0410.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.9 20
1.20 96.091.21.141.25mg/KgEthanol 70-130 5.1 20
0.045 91.093.40.0460.050mg/KgEthylbenzene 74-128 2.6 20
0.082 82.781.70.0810.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.2 20
0.054 1101140.0570.050mg/KgHexachlorobutadiene 64-125 4.1 20
0.036 73.872.60.0360.050mg/Kgn-Hexane 70-130 1.6 20
0.057 1151170.0580.050mg/Kg2-Hexanone 61-157 2.4 20
0.052 1041060.0530.050mg/KgIsopropylbenzene 68-126 1.9 20
0.052 1061080.0530.050mg/Kg4-Isopropyl toluene 68-129 1.8 20
0.046 93.293.20.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.0 20
0.041 83.481.00.0400.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.9 20
0.052 1051040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 1.1 20
0.040 80.279.60.0390.050mg/KgMethylene Chloride 74-129 0.7 20
0.052 1061080.0530.050mg/KgNaphthalene 57-157 1.8 20
Page 14 of 42Date:11/17/2022 12:34 PM
Page 139 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25976QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25975
LCS-V25975 LCSD-V25975Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.054 1091090.0540.050mg/Kgn-Propylbenzene 67-130 0.0 20
0.046 92.698.20.0490.050mg/KgStyrene 77-121 5.8 20
0.046 93.695.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.4 20
0.055 1111080.0530.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.7 20
0.036 73.075.40.0370.050mg/KgTetrachloroethene 68-130 3.2 20
0.035 71.471.20.0350.050mg/KgToluene 71-129 0.2 20
0.055 1101100.0540.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.3 20
0.056 1121120.0550.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.3 20
0.040 81.683.00.0410.050mg/Kg1,1,1-Trichloroethane 67-131 1.7 20
0.046 93.294.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.037 75.075.00.0370.050mg/KgTrichloroethene 75-133 0.0 20
0.040 81.686.00.0430.050mg/KgTrichlorofluoromethane 44-146 5.2 20
0.060 1211250.0620.050mg/Kg1,2,3-Trichloropropane 60-137 3.2 20
0.053 1071090.0540.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.2 20
0.053 1081080.0530.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.0 20
0.036 73.868.80.0340.050mg/KgVinyl Acetate 60-140 7.0 20
0.034 69.273.00.0360.050mg/KgVinyl Chloride 48-147 5.3 20
0.047 94.699.20.0490.050mg/Kgo-Xylene 74-126 4.7 20
0.090 90.694.20.0940.100mg/Kgm,p-Xylene 75-124 3.8 20
1051064-Bromofluorobenzene (S)70-130
111109Dibromofluoromethane (S)84-123
112111Toluene-d8 (S)76-129
Page 15 of 42Date:11/17/2022 12:34 PM
Page 140 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
Associated Lab Samples: 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-V26115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/08/22 20:070.0200.002<0.002mg/KgAcetone
11/08/22 20:070.0200.001<0.001mg/KgAcrolein
11/08/22 20:070.0200.0008<0.0008mg/KgAcrylonitrile
11/08/22 20:070.0050.0006<0.0006mg/KgBenzene
11/08/22 20:070.0050.0005<0.0005mg/KgBromobenzene
11/08/22 20:070.0050.0008<0.0008mg/KgBromochloromethane
11/08/22 20:070.0050.001<0.001mg/KgBromodichloromethane
11/08/22 20:070.0050.001<0.001mg/KgBromoform
11/08/22 20:070.0100.001<0.001mg/KgBromomethane
11/08/22 20:070.0050.0005<0.0005mg/Kgn-Butylbenzene
11/08/22 20:070.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/08/22 20:070.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/08/22 20:070.0050.0006<0.0006mg/KgCarbon Disulfide
11/08/22 20:070.0050.001<0.001mg/KgCarbon Tetrachloride
11/08/22 20:070.0050.0007<0.0007mg/KgChlorobenzene
11/08/22 20:070.0050.0009<0.0009mg/KgChlorodibromomethane
11/08/22 20:070.0100.0009<0.0009mg/KgChloroethane
11/08/22 20:070.0050.001<0.001mg/KgChloroform
11/08/22 20:070.0100.0006<0.0006mg/KgChloromethane
11/08/22 20:070.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/08/22 20:070.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/08/22 20:070.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/08/22 20:070.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/08/22 20:070.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/08/22 20:070.0050.0006<0.0006mg/KgDibromomethane
11/08/22 20:070.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/08/22 20:070.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 16 of 42Date:11/17/2022 12:34 PM
Page 141 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
Associated Lab Samples: 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-V26115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/08/22 20:070.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/08/22 20:070.0100.001<0.001mg/KgDichlorodifluoromethane
11/08/22 20:070.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/08/22 20:070.0050.001<0.001mg/Kg1,2-Dichloroethane
11/08/22 20:070.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/08/22 20:070.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/08/22 20:070.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/08/22 20:070.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/08/22 20:070.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/08/22 20:070.0050.001<0.001mg/Kg2,2-Dichloropropane
11/08/22 20:070.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/08/22 20:070.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/08/22 20:070.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/08/22 20:070.2500.014<0.014mg/KgEthanol
11/08/22 20:070.0050.0006<0.0006mg/KgEthylbenzene
11/08/22 20:070.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/08/22 20:070.0100.0008<0.0008mg/KgHexachlorobutadiene
11/08/22 20:070.0100.0007<0.0007mg/Kgn-Hexane
11/08/22 20:070.0200.0006<0.0006mg/Kg2-Hexanone
11/08/22 20:070.0050.0005<0.0005mg/KgIsopropylbenzene
11/08/22 20:070.0050.001<0.001mg/Kg4-Isopropyl toluene
11/08/22 20:070.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/08/22 20:070.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/08/22 20:070.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/08/22 20:070.0100.001<0.001mg/KgMethylene Chloride
11/08/22 20:070.0100.0010<0.0010mg/KgNaphthalene
11/08/22 20:070.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 17 of 42Date:11/17/2022 12:34 PM
Page 142 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
Associated Lab Samples: 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-V26115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/08/22 20:070.0050.001<0.001mg/KgStyrene
11/08/22 20:070.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/08/22 20:070.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/08/22 20:070.0050.0009<0.0009mg/KgTetrachloroethene
11/08/22 20:070.0050.0007<0.0007mg/KgToluene
11/08/22 20:070.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/08/22 20:070.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/08/22 20:070.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/08/22 20:070.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/08/22 20:070.0050.0009<0.0009mg/KgTrichloroethene
11/08/22 20:070.0100.002<0.002mg/KgTrichlorofluoromethane
11/08/22 20:070.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/08/22 20:070.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/08/22 20:070.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/08/22 20:070.0100.0005<0.0005mg/KgVinyl Acetate
11/08/22 20:070.0100.0005<0.0005mg/KgVinyl Chloride
11/08/22 20:070.0050.0005<0.0005mg/Kgo-Xylene
11/08/22 20:070.0100.001<0.001mg/Kgm,p-Xylene
11/08/22 20:074-Bromofluorobenzene (S)101 70-130
11/08/22 20:07Dibromofluoromethane (S)101 84-123
11/08/22 20:07Toluene-d8 (S)100 76-129
LCS-V26115 LCSD-V26115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.091 91.493.30.0930.100mg/KgAcetone 29-198 2.0 20
Page 18 of 42Date:11/17/2022 12:34 PM
Page 143 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
LCS-V26115 LCSD-V26115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.108 1081010.1010.100mg/KgAcrolein 70-130 6.6 20
0.102 10290.40.0900.100mg/KgAcrylonitrile 65-134 12.0 20
0.046 92.692.00.0460.050mg/KgBenzene 74-127 0.6 20
0.046 92.090.40.0450.050mg/KgBromobenzene 73-125 1.7 20
0.045 91.688.80.0440.050mg/KgBromochloromethane 72-134 3.1 20
0.045 91.088.00.0440.050mg/KgBromodichloromethane 75-122 3.3 20
0.049 98.291.40.0450.050mg/KgBromoform 66-135 7.1 20
0.042 85.692.20.0460.050mg/KgBromomethane 20-180 7.4 20
0.045 90.695.20.0470.050mg/Kgn-Butylbenzene 65-135 4.9 20
0.045 90.894.60.0470.050mg/Kgsec-Butyl benzene 66-131 4.0 20
0.043 87.691.40.0450.050mg/Kgtert-Butyl benzene 67-132 4.2 20
0.043 86.490.00.0450.050mg/KgCarbon Disulfide 61-129 4.0 20
0.041 83.688.00.0440.050mg/KgCarbon Tetrachloride 64-143 5.1 20
0.045 90.092.00.0460.050mg/KgChlorobenzene 74-118 2.1 20
0.045 90.286.60.0430.050mg/KgChlorodibromomethane 73-122 4.0 20
0.041 82.486.20.0430.050mg/KgChloroethane 33-149 4.5 20
0.047 95.096.80.0480.050mg/KgChloroform 73-127 1.8 20
0.036 73.876.00.0380.050mg/KgChloromethane 45-143 2.9 20
0.045 90.693.40.0460.050mg/Kg2-Chlorotoluene 67-124 3.0 20
0.045 90.893.60.0460.050mg/Kg4-Chlorotoluene 71-126 3.0 20
0.046 92.291.60.0450.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.6 20
0.044 88.884.00.0420.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.5 20
0.047 95.295.20.0470.050mg/Kg1,2-Dibromoethane 70-132 0.0 20
0.046 93.087.20.0430.050mg/KgDibromomethane 74-133 6.4 20
0.047 94.695.00.0470.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.045 91.694.60.0470.050mg/Kg1,3-Dichlorobenzene 71-120 3.2 20
Page 19 of 42Date:11/17/2022 12:34 PM
Page 144 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
LCS-V26115 LCSD-V26115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.691.60.0450.050mg/Kg1,4-Dichlorobenzene 71-123 4.4 20
0.040 80.885.60.0420.050mg/KgDichlorodifluoromethane 26-146 5.7 20
0.045 91.491.00.0450.050mg/Kg1,1-Dichloroethane 74-127 0.4 20
0.048 97.291.80.0450.050mg/Kg1,2-Dichloroethane 68-128 5.7 20
0.045 90.690.40.0450.050mg/Kg1,1-Dichloroethene 67-149 0.2 20
0.043 87.288.20.0440.050mg/Kgcis-1,2-Dichloroethene 76-134 1.1 20
0.042 85.687.20.0430.050mg/Kgtrans-1,2-Dichloroethene 73-132 1.8 20
0.047 95.890.00.0450.050mg/Kg1,2-Dichloropropane 73-130 6.2 20
0.048 96.893.00.0460.050mg/Kg1,3-Dichloropropane 75-124 4.0 20
0.044 88.091.60.0450.050mg/Kg2,2-Dichloropropane 50-142 4.0 20
0.045 90.890.60.0450.050mg/Kg1,1-Dichloropropene 71-130 0.2 20
0.046 93.093.20.0460.050mg/Kgcis-1,3-Dichloropropene 71-125 0.2 20
0.049 98.495.60.0470.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.8 20
1.46 11797.61.221.25mg/KgEthanol 70-130 17.9 20
0.044 88.488.40.0440.050mg/KgEthylbenzene 74-128 0.0 20
0.096 96.295.00.0950.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.2 20
0.045 91.695.40.0470.050mg/KgHexachlorobutadiene 64-125 4.0 20
0.047 95.498.80.0490.050mg/Kgn-Hexane 70-130 3.5 20
0.045 91.482.80.0410.050mg/Kg2-Hexanone 61-157 9.8 20
0.043 86.690.60.0450.050mg/KgIsopropylbenzene 68-126 4.5 20
0.045 90.495.40.0470.050mg/Kg4-Isopropyl toluene 68-129 5.3 20
0.041 83.879.20.0390.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.6 20
0.046 92.890.80.0450.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.1 20
0.050 10296.60.0480.050mg/Kg4-Methyl-2-Pentanone 57-162 5.2 20
0.044 89.489.20.0440.050mg/KgMethylene Chloride 74-129 0.2 20
0.047 95.691.00.0450.050mg/KgNaphthalene 57-157 4.9 20
Page 20 of 42Date:11/17/2022 12:34 PM
Page 145 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26115
LCS-V26115 LCSD-V26115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.692.80.0460.050mg/Kgn-Propylbenzene 67-130 3.5 20
0.045 91.295.20.0470.050mg/KgStyrene 77-121 4.2 20
0.042 85.294.80.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 10.6 20
0.044 89.886.80.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.042 84.291.20.0450.050mg/KgTetrachloroethene 68-130 7.9 20
0.043 87.689.00.0440.050mg/KgToluene 71-129 1.5 20
0.049 99.092.80.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 6.4 20
0.046 92.694.60.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.1 20
0.045 90.292.20.0460.050mg/Kg1,1,1-Trichloroethane 67-131 2.1 20
0.045 90.490.00.0450.050mg/Kg1,1,2-Trichloroethane 70-133 0.4 20
0.044 89.693.80.0460.050mg/KgTrichloroethene 75-133 4.5 20
0.043 86.092.60.0460.050mg/KgTrichlorofluoromethane 44-146 7.3 20
0.045 91.883.60.0410.050mg/Kg1,2,3-Trichloropropane 60-137 9.3 20
0.044 89.689.80.0440.050mg/Kg1,2,4-Trimethylbenzene 69-129 0.2 20
0.044 89.092.40.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.057 1151130.0560.050mg/KgVinyl Acetate 60-140 1.5 20
0.042 85.892.60.0460.050mg/KgVinyl Chloride 48-147 7.6 20
0.045 91.092.40.0460.050mg/Kgo-Xylene 74-126 1.5 20
0.087 87.791.00.0910.100mg/Kgm,p-Xylene 75-124 3.6 20
10197.24-Bromofluorobenzene (S)70-130
101100Dibromofluoromethane (S)84-123
102100Toluene-d8 (S)76-129
Page 21 of 42Date:11/17/2022 12:34 PM
Page 146 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
Associated Lab Samples: 92342, 92343, 92344, 92345, 92346, 92347, 92348, 92349, 92350
LRB-V26175 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/10/22 12:130.6600.116<0.116mg/KgAcenaphthene
11/10/22 12:130.6600.105<0.105mg/KgAcenaphthylene
11/10/22 12:130.6600.152<0.152mg/KgAniline
11/10/22 12:130.6600.143<0.143mg/KgAnthracene
11/10/22 12:130.6600.139<0.139mg/KgBenzo(a)anthracene
11/10/22 12:130.6600.147<0.147mg/KgBenzo(a)pyrene
11/10/22 12:130.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/10/22 12:130.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/10/22 12:130.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/10/22 12:132.000.580<0.580mg/KgBenzoic Acid
11/10/22 12:130.6600.105<0.105mg/KgBenzyl alcohol
11/10/22 12:130.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/10/22 12:130.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/10/22 12:130.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/10/22 12:130.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/10/22 12:130.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/10/22 12:130.3300.113<0.113mg/KgButyl benzyl phthalate
11/10/22 12:130.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/10/22 12:130.3300.112<0.112mg/Kg4-Chloroaniline
11/10/22 12:130.6600.116<0.116mg/Kg2-Chloronaphthalene
11/10/22 12:130.6600.098<0.098mg/Kg2-Chlorophenol
11/10/22 12:131.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/10/22 12:130.6600.142<0.142mg/KgChrysene
11/10/22 12:130.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/10/22 12:130.6600.119<0.119mg/KgDibenzofuran
11/10/22 12:130.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/10/22 12:130.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 22 of 42Date:11/17/2022 12:34 PM
Page 147 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
Associated Lab Samples: 92342, 92343, 92344, 92345, 92346, 92347, 92348, 92349, 92350
LRB-V26175 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/10/22 12:130.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/10/22 12:130.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/10/22 12:130.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/10/22 12:130.6600.180<0.180mg/KgDiethyl phthalate
11/10/22 12:130.6600.174<0.174mg/KgDimethyl phthalate
11/10/22 12:130.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/10/22 12:130.6600.107<0.107mg/KgDi-n-butyl phthalate
11/10/22 12:131.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/10/22 12:131.500.520<0.520mg/Kg2,4-Dinitrophenol
11/10/22 12:130.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/10/22 12:130.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/10/22 12:130.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/10/22 12:130.6600.123<0.123mg/KgFluoranthene
11/10/22 12:130.6600.128<0.128mg/KgFluorene
11/10/22 12:130.6600.106<0.106mg/KgHexachlorobenzene
11/10/22 12:130.6600.097<0.097mg/KgHexachlorobutadiene
11/10/22 12:130.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/10/22 12:130.6600.079<0.079mg/KgHexachloroethane
11/10/22 12:130.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/10/22 12:130.6600.191<0.191mg/KgIsophorone
11/10/22 12:130.6600.106<0.106mg/Kg1-Methylnaphthalene
11/10/22 12:130.6600.100<0.100mg/Kg2-Methylnaphthalene
11/10/22 12:130.6600.097<0.097mg/Kg2-Methylphenol
11/10/22 12:130.6600.084<0.084mg/Kg3&4 Methylphenol
11/10/22 12:130.6600.144<0.144mg/KgNaphthalene
11/10/22 12:130.6600.096<0.096mg/Kg2-Nitroaniline
11/10/22 12:130.6600.120<0.120mg/Kg3-Nitroaniline
Page 23 of 42Date:11/17/2022 12:34 PM
Page 148 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
Associated Lab Samples: 92342, 92343, 92344, 92345, 92346, 92347, 92348, 92349, 92350
LRB-V26175 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/10/22 12:130.3300.093<0.093mg/Kg4-Nitroaniline
11/10/22 12:130.3300.116<0.116mg/KgNitrobenzene
11/10/22 12:130.6600.088<0.088mg/Kg2-Nitrophenol
11/10/22 12:130.6600.117<0.117mg/Kg4-Nitrophenol
11/10/22 12:130.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/10/22 12:130.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/10/22 12:130.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/10/22 12:131.000.347<0.347mg/KgPentachlorophenol
11/10/22 12:130.6600.208<0.208mg/KgPhenanthrene
11/10/22 12:130.6600.112<0.112mg/KgPhenol
11/10/22 12:130.6600.134<0.134mg/KgPyrene
11/10/22 12:130.3300.079<0.079mg/KgPyridine
11/10/22 12:130.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/10/22 12:130.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/10/22 12:130.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/10/22 12:132-Fluorobiphenyl (S)97.6 44-115
11/10/22 12:132-Fluorophenol (S)82.8 35-115
11/10/22 12:13Nitrobenzene-d5 (S)88.0 37-122
11/10/22 12:134-Terphenyl-d14 (S)105 54-127
11/10/22 12:132,4,6-Tribromophenol (S)78.3 39-132
11/10/22 12:13Phenol-d5 (S)78.0 34-121
LCS-V26175Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.61.581.67mg/KgAcenaphthene 40-123
93.41.561.67mg/KgAcenaphthylene 32-132
Page 24 of 42Date:11/17/2022 12:34 PM
Page 149 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
LCS-V26175Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1422.371.67mg/KgAniline 12-197
1031.721.67mg/KgAnthracene 47-123
1011.691.67mg/KgBenzo(a)anthracene 49-126
1081.811.67mg/KgBenzo(a)pyrene 45-129
95.81.601.67mg/KgBenzo(b)fluoranthene 45-132
99.41.661.67mg/KgBenzo(g,h,i)perylene 43-134
97.01.621.67mg/KgBenzo(k)fluoranthene 47-132
58.20.9721.67mg/KgBenzoic Acid 10-83
98.81.651.67mg/KgBenzyl alcohol 29-122
89.21.491.67mg/KgBis(2-Chloroethoxy)methane 36-121
88.01.471.67mg/KgBis(2-Chloroethyl)ether 31-120
97.01.621.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1071.781.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1021.711.67mg/Kg4-Bromophenyl phenyl ether 46-124
1041.741.67mg/KgButyl benzyl phthalate 48-132
90.41.511.67mg/Kg4-Chloro-3-methylphenol 45-122
88.01.471.67mg/Kg4-Chloroaniline 17-106
96.41.611.67mg/Kg2-Chloronaphthalene 41-114
94.01.571.67mg/Kg2-Chlorophenol 34-121
1011.691.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1021.701.67mg/KgChrysene 50-124
1101.831.67mg/KgDibenz(a,h)anthracene 45-134
94.01.571.67mg/KgDibenzofuran 44-120
85.01.421.67mg/Kg1,2-Dichlorobenzene 33-117
82.01.371.67mg/Kg1,3-Dichlorobenzene 30-115
81.41.361.67mg/Kg1,4-Dichlorobenzene 31-115
78.41.311.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 25 of 42Date:11/17/2022 12:34 PM
Page 150 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
LCS-V26175Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.41.511.67mg/Kg2,4-Dichlorophenol 40-122
99.41.661.67mg/KgDiethyl phthalate 50-124
1001.671.67mg/KgDimethyl phthalate 48-124
1131.891.67mg/Kg2,4-Dimethylphenol 30-127
1091.821.67mg/KgDi-n-butyl phthalate 51-128
98.81.651.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1081.801.67mg/Kg2,4-Dinitrophenol 27-129
98.21.641.67mg/Kg2,4-Dinitrotoluene 48-126
97.61.631.67mg/Kg2,6-Dinitrotoluene 46-124
98.81.651.67mg/KgDi-n-Octyl Phthalate 45-140
95.81.601.67mg/KgFluoranthene 50-127
95.81.601.67mg/KgFluorene 43-125
95.21.591.67mg/KgHexachlorobenzene 45-122
82.61.381.67mg/KgHexachlorobutadiene 32-123
87.41.461.67mg/KgHexachlorocyclopentadiene 32-117
81.41.361.67mg/KgHexachloroethane 28-117
99.41.661.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
69.41.161.67mg/KgIsophorone 30-122
82.01.371.67mg/Kg1-Methylnaphthalene 40-119
82.01.371.67mg/Kg2-Methylnaphthalene 38-122
95.21.591.67mg/Kg2-Methylphenol 32-122
86.81.451.67mg/Kg3&4 Methylphenol 34-119
80.21.341.67mg/KgNaphthalene 35-123
1001.671.67mg/Kg2-Nitroaniline 44-127
95.21.591.67mg/Kg3-Nitroaniline 33-119
1021.711.67mg/Kg4-Nitroaniline 63-147
77.21.291.67mg/KgNitrobenzene 34-122
Page 26 of 42Date:11/17/2022 12:34 PM
Page 151 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
LCS-V26175Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.21.341.67mg/Kg2-Nitrophenol 36-123
1001.671.67mg/Kg4-Nitrophenol 30-132
69.41.161.67mg/KgN-Nitrosodimethylamine 10-146
1202.001.67mg/KgN-Nitrosodiphenylamine 38-127
91.01.521.67mg/KgN-Nitroso-di-n-propylamine 36-120
1161.941.67mg/KgPentachlorophenol 25-133
1011.691.67mg/KgPhenanthrene 50-121
88.61.481.67mg/KgPhenol 34-121
1011.681.67mg/KgPyrene 47-127
62.81.051.67mg/KgPyridine 10-80
80.21.341.67mg/Kg1,2,4-Trichlorobenzene 34-118
98.21.641.67mg/Kg2,4,5-Trichlorophenol 41-124
98.21.641.67mg/Kg2,4,6-Trichlorophenol 39-126
97.62-Fluorobiphenyl (S)44-115
84.02-Fluorophenol (S)35-115
79.6Nitrobenzene-d5 (S)37-122
1054-Terphenyl-d14 (S)54-127
85.82,4,6-Tribromophenol (S)39-132
79.8Phenol-d5 (S)34-121
V 92164-MS-V26175 V 92164-MSD-V26175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.44 86.71.571.671.66<0.116mg/KgAcenaphthene 94.0 40-123 8.6 20
1.54 92.71.661.671.66<0.105mg/KgAcenaphthylene 99.4 32-132 7.5 20
1.91 1152.101.671.66<0.152mg/KgAniline 126 12-197 9.4 20
Page 27 of 42Date:11/17/2022 12:34 PM
Page 152 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
V 92164-MS-V26175 V 92164-MSD-V26175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.66 1001.841.671.66<0.143mg/KgAnthracene 110 47-123 10.2 20
1.69 1021.851.671.66<0.139mg/KgBenzo(a)anthracene 111 49-126 9.0 20
1.76 1061.921.671.66<0.147mg/KgBenzo(a)pyrene 115 45-129 8.6 20
1.72 90.91.841.671.660.210mg/KgBenzo(b)fluoranthene 97.6 45-132 6.7 20
1.56 93.91.691.671.66<0.136mg/KgBenzo(g,h,i)perylene 101 43-134 8.0 20
1.51 90.91.671.671.66<0.137mg/KgBenzo(k)fluoranthene 100 47-132 10.0 20
1.57 94.51.681.671.66<0.105mg/KgBenzyl alcohol 101 29-122 6.7 20
1.41 84.91.471.671.66<0.118mg/KgBis(2-Chloroethoxy)methane 88.0 36-121 4.1 20
1.44 86.71.561.671.66<0.107mg/KgBis(2-Chloroethyl)ether 93.4 31-120 8.0 20
1.58 95.11.641.671.66<0.136mg/KgBis(2-Chloroisopropyl)ether 98.2 33-131 3.7 20
1.73 1041.921.671.66<0.120mg/KgBis(2-ethylhexyl)phthalate 115 51-133 10.4 20
1.60 96.31.781.671.66<0.109mg/Kg4-Bromophenyl phenyl ether 107 46-124 10.6 20
1.71 1031.911.671.66<0.113mg/KgButyl benzyl phthalate 114 48-132 11.0 20
1.41 84.91.471.671.66<0.092mg/Kg4-Chloro-3-methylphenol 88.0 45-122 4.1 20
1.32 79.51.451.671.66<0.112mg/Kg4-Chloroaniline 86.8 17-106 9.3 20
1.54 92.71.671.671.66<0.116mg/Kg2-Chloronaphthalene 100 41-114 8.0 20
1.45 87.31.481.671.66<0.098mg/Kg2-Chlorophenol 88.6 34-121 2.0 20
1.55 93.31.761.671.66<0.126mg/Kg4-Chlorophenyl phenyl ether 105 45-121 12.6 20
1.72 94.81.871.671.660.145mg/KgChrysene 103 50-124 8.3 20
1.68 1011.861.671.66<0.230mg/KgDibenz(a,h)anthracene 111 45-134 10.1 20
1.53 92.11.681.671.66<0.119mg/KgDibenzofuran 101 44-120 9.3 20
1.35 81.31.441.671.66<0.094mg/Kg1,2-Dichlorobenzene 86.2 33-117 6.4 20
1.30 78.31.391.671.66<0.097mg/Kg1,3-Dichlorobenzene 83.2 30-115 6.6 20
1.31 78.91.381.671.66<0.097mg/Kg1,4-Dichlorobenzene 82.6 31-115 5.2 20
1.17 70.41.441.671.66<0.147mg/Kg3,3'-Dichlorobenzidine 86.2 22-121 20.6*20
1.32 79.51.341.671.66<0.095mg/Kg2,4-Dichlorophenol 80.2 40-122 1.5 20
Page 28 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 153 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
V 92164-MS-V26175 V 92164-MSD-V26175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.54 92.71.711.671.66<0.180mg/KgDiethyl phthalate 102 50-124 10.4 20
1.57 94.51.721.671.66<0.174mg/KgDimethyl phthalate 103 48-124 9.1 30
1.81 1091.941.671.66<0.108mg/Kg2,4-Dimethylphenol 116 30-127 6.9 20
1.71 1031.921.671.66<0.107mg/KgDi-n-butyl phthalate 115 51-128 11.5 20
0.962 57.90.9851.671.66<0.240mg/Kg4,6-Dinitro-2-methylphenol 58.9 29-132 2.3 20
0.656 39.50.6291.671.66<0.520mg/Kg2,4-Dinitrophenol 37.6 27-129 4.2 20
1.51 90.91.681.671.66<0.096mg/Kg2,4-Dinitrotoluene 101 48-126 10.6 20
1.53 92.11.661.671.66<0.108mg/Kg2,6-Dinitrotoluene 99.4 46-124 8.1 20
1.63 98.11.791.671.66<0.143mg/KgDi-n-Octyl Phthalate 107 45-140 9.3 20
1.61 96.91.761.671.66<0.123mg/KgFluoranthene 105 50-127 8.9 20
1.52 91.51.701.671.66<0.128mg/KgFluorene 102 43-125 11.1 20
1.55 93.31.711.671.66<0.106mg/KgHexachlorobenzene 102 45-122 9.8 20
1.38 83.11.431.671.66<0.097mg/KgHexachlorobutadiene 85.6 32-123 3.5 20
1.28 77.11.381.671.66<0.079mg/KgHexachloroethane 82.6 28-117 7.5 20
1.58 95.11.721.671.66<0.179mg/KgIndeno(1,2,3-cd)pyrene 103 45-133 8.4 20
1.09 65.61.131.671.66<0.191mg/KgIsophorone 67.6 30-122 3.6 20
1.46 73.71.511.671.660.235mg/Kg1-Methylnaphthalene 76.3 40-119 3.3 20
1.51 71.31.561.671.660.325mg/Kg2-Methylnaphthalene 73.9 38-122 3.2 20
1.48 89.11.621.671.66<0.097mg/Kg2-Methylphenol 97.0 32-122 9.0 20
1.35 81.31.441.671.66<0.084mg/Kg3&4 Methylphenol 86.2 34-119 6.4 20
1.41 72.21.471.671.660.211mg/KgNaphthalene 75.3 35-123 4.1 20
1.61 96.91.751.671.66<0.096mg/Kg2-Nitroaniline 105 44-127 8.3 20
1.48 89.11.671.671.66<0.120mg/Kg3-Nitroaniline 100 33-119 12.0 20
1.61 96.91.781.671.66<0.093mg/Kg4-Nitroaniline 107 63-147 10.0 20
1.26 75.91.311.671.66<0.116mg/KgNitrobenzene 78.4 34-122 3.8 20
1.03 62.01.001.671.66<0.088mg/Kg2-Nitrophenol 59.8 32-123 2.9 20
Page 29 of 42Date:11/17/2022 12:34 PM
Page 154 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26276QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26175
V 92164-MS-V26175 V 92164-MSD-V26175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.07 64.41.071.671.66<0.117mg/Kg4-Nitrophenol 64.0 30-132 0.0 20
1.10 66.21.181.671.66<0.263mg/KgN-Nitrosodimethylamine 70.6 10-146 7.0 30
1.88 1132.161.671.66<0.181mg/KgN-Nitrosodiphenylamine 129 38-127 13.8 20
1.48 89.11.541.671.66<0.118mg/KgN-Nitroso-di-n-propylamine 92.2 36-120 3.9 20
1.21 72.81.201.671.66<0.347mg/KgPentachlorophenol 71.8 25-133 0.8 20
1.71 1031.891.671.66<0.208mg/KgPhenanthrene 113 50-121 10.0 20
1.38 83.11.491.671.66<0.112mg/KgPhenol 89.2 34-121 7.6 20
1.78 97.81.911.671.660.155mg/KgPyrene 105 47-127 7.0 20
0.936 56.31.011.671.66<0.079mg/KgPyridine 60.4 10-80 7.6 20
1.30 78.31.361.671.66<0.107mg/Kg1,2,4-Trichlorobenzene 81.4 34-118 4.5 20
1.35 81.31.371.671.66<0.096mg/Kg2,4,5-Trichlorophenol 82.0 41-124 1.4 20
1.22 73.41.261.671.66<0.096mg/Kg2,4,6-Trichlorophenol 75.4 39-126 3.2 20
94.52-Fluorobiphenyl (S)99.4 44-115
75.32-Fluorophenol (S)74.1 35-115
77.7Nitrobenzene-d5 (S)79.6 37-122
1044-Terphenyl-d14 (S)111 54-127
61.52,4,6-Tribromophenol (S)64.8 39-132
74.4Phenol-d5 (S)78.3 34-121
Page 30 of 42Date:11/17/2022 12:34 PM
Page 155 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
Associated Lab Samples: 92351, 92352, 92353, 92354, 92355
LRB-V26228 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/11/22 10:440.6600.116<0.116mg/KgAcenaphthene
11/11/22 10:440.6600.105<0.105mg/KgAcenaphthylene
11/11/22 10:440.6600.152<0.152mg/KgAniline
11/11/22 10:440.6600.143<0.143mg/KgAnthracene
11/11/22 10:440.6600.139<0.139mg/KgBenzo(a)anthracene
11/11/22 10:440.6600.147<0.147mg/KgBenzo(a)pyrene
11/11/22 10:440.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/11/22 10:440.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/11/22 10:440.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/11/22 10:442.000.580<0.580mg/KgBenzoic Acid
11/11/22 10:440.6600.105<0.105mg/KgBenzyl alcohol
11/11/22 10:440.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/11/22 10:440.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/11/22 10:440.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/11/22 10:440.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/11/22 10:440.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/11/22 10:440.3300.113<0.113mg/KgButyl benzyl phthalate
11/11/22 10:440.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/11/22 10:440.3300.112<0.112mg/Kg4-Chloroaniline
11/11/22 10:440.6600.116<0.116mg/Kg2-Chloronaphthalene
11/11/22 10:440.6600.098<0.098mg/Kg2-Chlorophenol
11/11/22 10:441.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/11/22 10:440.6600.142<0.142mg/KgChrysene
11/11/22 10:440.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/11/22 10:440.6600.119<0.119mg/KgDibenzofuran
11/11/22 10:440.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/11/22 10:440.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 31 of 42Date:11/17/2022 12:34 PM
Page 156 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
Associated Lab Samples: 92351, 92352, 92353, 92354, 92355
LRB-V26228 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/11/22 10:440.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/11/22 10:440.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/11/22 10:440.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/11/22 10:440.6600.180<0.180mg/KgDiethyl phthalate
11/11/22 10:440.6600.174<0.174mg/KgDimethyl phthalate
11/11/22 10:440.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/11/22 10:440.6600.107<0.107mg/KgDi-n-butyl phthalate
11/11/22 10:441.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/11/22 10:441.500.520<0.520mg/Kg2,4-Dinitrophenol
11/11/22 10:440.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/11/22 10:440.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/11/22 10:440.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/11/22 10:440.6600.123<0.123mg/KgFluoranthene
11/11/22 10:440.6600.128<0.128mg/KgFluorene
11/11/22 10:440.6600.106<0.106mg/KgHexachlorobenzene
11/11/22 10:440.6600.097<0.097mg/KgHexachlorobutadiene
11/11/22 10:440.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/11/22 10:440.6600.079<0.079mg/KgHexachloroethane
11/11/22 10:440.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/11/22 10:440.6600.191<0.191mg/KgIsophorone
11/11/22 10:440.6600.106<0.106mg/Kg1-Methylnaphthalene
11/11/22 10:440.6600.100<0.100mg/Kg2-Methylnaphthalene
11/11/22 10:440.6600.097<0.097mg/Kg2-Methylphenol
11/11/22 10:440.6600.084<0.084mg/Kg3&4 Methylphenol
11/11/22 10:440.6600.144<0.144mg/KgNaphthalene
11/11/22 10:440.6600.096<0.096mg/Kg2-Nitroaniline
11/11/22 10:440.6600.120<0.120mg/Kg3-Nitroaniline
Page 32 of 42Date:11/17/2022 12:34 PM
Page 157 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
Associated Lab Samples: 92351, 92352, 92353, 92354, 92355
LRB-V26228 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/11/22 10:440.3300.093<0.093mg/Kg4-Nitroaniline
11/11/22 10:440.3300.116<0.116mg/KgNitrobenzene
11/11/22 10:440.6600.088<0.088mg/Kg2-Nitrophenol
11/11/22 10:440.6600.117<0.117mg/Kg4-Nitrophenol
11/11/22 10:440.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/11/22 10:440.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/11/22 10:440.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/11/22 10:441.000.347<0.347mg/KgPentachlorophenol
11/11/22 10:440.6600.208<0.208mg/KgPhenanthrene
11/11/22 10:440.6600.112<0.112mg/KgPhenol
11/11/22 10:440.6600.134<0.134mg/KgPyrene
11/11/22 10:440.3300.079<0.079mg/KgPyridine
11/11/22 10:440.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/11/22 10:440.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/11/22 10:440.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/11/22 10:442-Fluorobiphenyl (S)105 44-115
11/11/22 10:442-Fluorophenol (S)89.1 35-115
11/11/22 10:44Nitrobenzene-d5 (S)95.2 37-122
11/11/22 10:444-Terphenyl-d14 (S)108 54-127
11/11/22 10:442,4,6-Tribromophenol (S)89.7 39-132
11/11/22 10:44Phenol-d5 (S)83.1 34-121
LCS-V26228Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1011.681.67mg/KgAcenaphthene 40-123
1021.701.67mg/KgAcenaphthylene 32-132
Page 33 of 42Date:11/17/2022 12:34 PM
Page 158 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
LCS-V26228Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1622.711.67mg/KgAniline 12-197
1081.811.67mg/KgAnthracene 47-123
1071.781.67mg/KgBenzo(a)anthracene 49-126
1151.921.67mg/KgBenzo(a)pyrene 45-129
1031.721.67mg/KgBenzo(b)fluoranthene 45-132
1071.781.67mg/KgBenzo(g,h,i)perylene 43-134
1041.731.67mg/KgBenzo(k)fluoranthene 47-132
66.41.111.67mg/KgBenzoic Acid 10-83
1041.741.67mg/KgBenzyl alcohol 29-122
92.81.551.67mg/KgBis(2-Chloroethoxy)methane 36-121
85.01.421.67mg/KgBis(2-Chloroethyl)ether 31-120
1011.681.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1131.881.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1081.801.67mg/Kg4-Bromophenyl phenyl ether 46-124
1101.841.67mg/KgButyl benzyl phthalate 48-132
94.01.571.67mg/Kg4-Chloro-3-methylphenol 45-122
98.21.641.67mg/Kg4-Chloroaniline 17-106
1021.701.67mg/Kg2-Chloronaphthalene 41-114
99.41.661.67mg/Kg2-Chlorophenol 34-121
1111.851.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1061.771.67mg/KgChrysene 50-124
1171.951.67mg/KgDibenz(a,h)anthracene 45-134
1011.681.67mg/KgDibenzofuran 44-120
85.61.431.67mg/Kg1,2-Dichlorobenzene 33-117
83.21.391.67mg/Kg1,3-Dichlorobenzene 30-115
81.41.361.67mg/Kg1,4-Dichlorobenzene 31-115
91.01.521.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 34 of 42Date:11/17/2022 12:34 PM
Page 159 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
LCS-V26228Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.41.561.67mg/Kg2,4-Dichlorophenol 40-122
1071.791.67mg/KgDiethyl phthalate 50-124
1111.861.67mg/KgDimethyl phthalate 48-124
1202.001.67mg/Kg2,4-Dimethylphenol 30-127
1141.911.67mg/KgDi-n-butyl phthalate 51-128
1031.721.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1111.851.67mg/Kg2,4-Dinitrophenol 27-129
1071.781.67mg/Kg2,4-Dinitrotoluene 48-126
1071.791.67mg/Kg2,6-Dinitrotoluene 46-124
1051.751.67mg/KgDi-n-Octyl Phthalate 45-140
1011.681.67mg/KgFluoranthene 50-127
1071.781.67mg/KgFluorene 43-125
1021.711.67mg/KgHexachlorobenzene 45-122
85.01.421.67mg/KgHexachlorobutadiene 32-123
89.81.501.67mg/KgHexachlorocyclopentadiene 32-117
82.61.381.67mg/KgHexachloroethane 28-117
1051.761.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
71.21.191.67mg/KgIsophorone 30-122
85.61.431.67mg/Kg1-Methylnaphthalene 40-119
85.01.421.67mg/Kg2-Methylnaphthalene 38-122
98.21.641.67mg/Kg2-Methylphenol 32-122
91.61.531.67mg/Kg3&4 Methylphenol 34-119
82.01.371.67mg/KgNaphthalene 35-123
1081.811.67mg/Kg2-Nitroaniline 44-127
1071.791.67mg/Kg3-Nitroaniline 33-119
1121.871.67mg/Kg4-Nitroaniline 63-147
80.21.341.67mg/KgNitrobenzene 34-122
Page 35 of 42Date:11/17/2022 12:34 PM
Page 160 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
LCS-V26228Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.21.391.67mg/Kg2-Nitrophenol 36-123
1071.781.67mg/Kg4-Nitrophenol 30-132
66.41.111.67mg/KgN-Nitrosodimethylamine 10-146
1262.101.67mg/KgN-Nitrosodiphenylamine 38-127
94.61.581.67mg/KgN-Nitroso-di-n-propylamine 36-120
1141.901.67mg/KgPentachlorophenol 25-133
1071.781.67mg/KgPhenanthrene 50-121
92.81.551.67mg/KgPhenol 34-121
1071.791.67mg/KgPyrene 47-127
63.41.061.67mg/KgPyridine 10-80
82.61.381.67mg/Kg1,2,4-Trichlorobenzene 34-118
1071.781.67mg/Kg2,4,5-Trichlorophenol 41-124
1061.771.67mg/Kg2,4,6-Trichlorophenol 39-126
1012-Fluorobiphenyl (S)44-115
85.82-Fluorophenol (S)35-115
81.4Nitrobenzene-d5 (S)37-122
1084-Terphenyl-d14 (S)54-127
89.42,4,6-Tribromophenol (S)39-132
81.3Phenol-d5 (S)34-121
V 92351-MS-V26228 V 92351-MSD-V26228Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.40 83.81.601.671.67<0.116mg/KgAcenaphthene 95.8 40-123 13.3 20
1.42 85.01.711.671.67<0.105mg/KgAcenaphthylene 102 32-132 18.5 20
1.86 1112.391.671.67<0.152mg/KgAniline 143 12-197 24.9*20
Page 36 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 161 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
V 92351-MS-V26228 V 92351-MSD-V26228Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.67 1001.901.671.67<0.143mg/KgAnthracene 114 47-123 12.8 20
1.68 1011.891.671.67<0.139mg/KgBenzo(a)anthracene 113 49-126 11.7 20
1.82 1092.041.671.67<0.147mg/KgBenzo(a)pyrene 122 45-129 11.3 20
1.68 1011.821.671.67<0.146mg/KgBenzo(b)fluoranthene 109 45-132 8.0 20
1.65 98.81.841.671.67<0.136mg/KgBenzo(g,h,i)perylene 110 43-134 10.8 20
1.58 94.61.791.671.67<0.137mg/KgBenzo(k)fluoranthene 107 47-132 12.4 20
<0.580 0.0*<0.5801.671.67<0.580mg/KgBenzoic Acid 0.0 10-83 0.0 20
1.43 85.61.671.671.67<0.105mg/KgBenzyl alcohol 100 29-122 15.4 20
1.27 76.01.511.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 90.4 36-121 17.2 20
1.31 78.41.441.671.67<0.107mg/KgBis(2-Chloroethyl)ether 86.2 31-120 9.4 20
1.39 83.21.711.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 102 33-131 20.6*20
1.79 1071.991.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 119 51-133 10.5 20
1.62 97.01.841.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 110 46-124 12.7 20
1.74 94.61.881.671.670.159mg/KgButyl benzyl phthalate 103 48-132 7.7 20
1.39 83.21.581.671.67<0.092mg/Kg4-Chloro-3-methylphenol 94.6 45-122 12.7 20
1.31 78.41.541.671.67<0.112mg/Kg4-Chloroaniline 92.2 17-106 16.1 20
1.43 85.61.741.671.67<0.116mg/Kg2-Chloronaphthalene 104 41-114 19.5 20
1.34 80.21.641.671.67<0.098mg/Kg2-Chlorophenol 98.2 34-121 20.1*20
1.59 95.21.811.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 108 45-121 12.9 20
1.67 1001.891.671.67<0.142mg/KgChrysene 113 50-124 12.3 20
1.80 1082.001.671.67<0.230mg/KgDibenz(a,h)anthracene 120 45-134 10.5 20
1.45 86.81.681.671.67<0.119mg/KgDibenzofuran 101 44-120 14.6 20
1.21 72.41.501.671.67<0.094mg/Kg1,2-Dichlorobenzene 89.8 33-117 21.4*20
1.17 70.01.461.671.67<0.097mg/Kg1,3-Dichlorobenzene 87.4 30-115 22.0*20
1.17 70.01.441.671.67<0.097mg/Kg1,4-Dichlorobenzene 86.2 31-115 20.6*20
1.29 77.21.491.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 89.2 22-121 14.3 20
Page 37 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 162 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
V 92351-MS-V26228 V 92351-MSD-V26228Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.33 79.61.551.671.67<0.095mg/Kg2,4-Dichlorophenol 92.8 40-122 15.2 20
1.58 94.61.781.671.67<0.180mg/KgDiethyl phthalate 107 50-124 11.9 20
1.57 94.01.831.671.67<0.174mg/KgDimethyl phthalate 110 48-124 15.2 30
1.64 98.21.831.671.67<0.108mg/Kg2,4-Dimethylphenol 110 30-127 10.9 20
1.75 1051.861.671.67<0.107mg/KgDi-n-butyl phthalate 111 51-128 6.0 20
1.46 87.41.381.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 82.6 29-132 5.6 20
1.30 77.80.6051.671.67<0.520mg/Kg2,4-Dinitrophenol 36.2 27-129 72.9*20
1.56 93.41.761.671.67<0.096mg/Kg2,4-Dinitrotoluene 105 48-126 12.0 20
1.53 91.61.821.671.67<0.108mg/Kg2,6-Dinitrotoluene 109 46-124 17.3 20
1.67 1001.841.671.67<0.143mg/KgDi-n-Octyl Phthalate 110 45-140 9.6 20
1.64 89.51.801.671.670.144mg/KgFluoranthene 99.1 50-127 9.3 20
1.53 91.61.751.671.67<0.128mg/KgFluorene 105 43-125 13.4 20
1.57 94.01.801.671.67<0.106mg/KgHexachlorobenzene 108 45-122 13.6 20
1.25 74.81.491.671.67<0.097mg/KgHexachlorobutadiene 89.2 32-123 17.5 20
0.389 23.2*1.001.671.67<0.157mg/KgHexachlorocyclopentadiene 59.8 32-117 87.9*20
1.15 68.81.421.671.67<0.079mg/KgHexachloroethane 85.0 28-117 21.0*20
1.64 98.21.841.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 110 45-133 11.4 20
0.980 58.61.201.671.67<0.191mg/KgIsophorone 71.8 30-122 20.1*20
1.21 72.41.441.671.67<0.106mg/Kg1-Methylnaphthalene 86.2 40-119 17.3 20
1.23 73.61.441.671.67<0.100mg/Kg2-Methylnaphthalene 86.2 38-122 15.7 20
1.35 80.81.611.671.67<0.097mg/Kg2-Methylphenol 96.4 32-122 17.5 20
1.22 73.01.481.671.67<0.084mg/Kg3&4 Methylphenol 88.6 34-119 19.2 20
1.17 70.01.411.671.67<0.144mg/KgNaphthalene 84.4 35-123 18.6 20
1.58 94.61.831.671.67<0.096mg/Kg2-Nitroaniline 110 44-127 14.6 20
1.54 92.21.761.671.67<0.120mg/Kg3-Nitroaniline 105 33-119 13.3 20
1.63 97.61.811.671.67<0.093mg/Kg4-Nitroaniline 108 63-147 10.4 20
Page 38 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 163 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V26355QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V26228
V 92351-MS-V26228 V 92351-MSD-V26228Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.14 68.21.421.671.67<0.116mg/KgNitrobenzene 85.0 34-122 21.8*20
1.16 69.41.431.671.67<0.088mg/Kg2-Nitrophenol 85.6 32-123 20.8*20
1.55 92.81.721.671.67<0.117mg/Kg4-Nitrophenol 103 30-132 10.3 20
1.02 61.01.311.671.67<0.263mg/KgN-Nitrosodimethylamine 78.4 10-146 24.8 30
1.92 1152.151.671.67<0.181mg/KgN-Nitrosodiphenylamine 129 38-127 11.3 20
1.30 77.81.611.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 96.4 36-120 21.3*20
1.69 1011.921.671.67<0.347mg/KgPentachlorophenol 115 25-133 12.7 20
1.70 1021.881.671.67<0.208mg/KgPhenanthrene 113 50-121 10.0 20
1.24 74.21.521.671.67<0.112mg/KgPhenol 91.0 34-121 20.2*20
1.78 1071.991.671.67<0.134mg/KgPyrene 119 47-127 11.1 20
0.949 56.81.221.671.67<0.079mg/KgPyridine 73.0 10-80 24.9*20
1.19 71.21.441.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 86.2 34-118 19.0 20
1.58 94.61.781.671.67<0.096mg/Kg2,4,5-Trichlorophenol 107 41-124 11.9 20
1.47 88.01.791.671.67<0.096mg/Kg2,4,6-Trichlorophenol 107 39-126 19.6 20
84.42-Fluorobiphenyl (S)102 44-115
71.72-Fluorophenol (S)83.8 35-115
68.8Nitrobenzene-d5 (S)82.0 37-122
1054-Terphenyl-d14 (S)119 54-127
73.22,4,6-Tribromophenol (S)86.8 39-132
66.9Phenol-d5 (S)79.0 34-121
Page 39 of 42* QC Fail Date:11/17/2022 12:34 PM
Page 164 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L649235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L648524
Associated Lab Samples: 92342, 92343, 92344, 92345
LRB-L648524 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/16/22 16:380.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L648524Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.53.944.00mg/KgChromium, Hexavalent 80-120
V 92332-DUP-L648524Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/16/22 17:302.4<0.207< 0.207mg/KgChromium, Hexavalent
V 92332-MS-L648524 V 92332-MSD-L648524Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
5.46 13.5*38270840.2< 0.142mg/KgChromium, Hexavalent 53.9 75-125
Page 40 of 42Date:11/17/2022 12:34 PM
Page 165 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L649103QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L648525
Associated Lab Samples: 92346, 92347, 92348, 92349, 92350, 92351, 92352, 92353, 92354, 92355
LRB-L648525 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/16/22 11:070.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L648525Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.03.764.00mg/KgChromium, Hexavalent 80-120
V 92346-DUP-L648525Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/16/22 11:401.4<0.200< 0.200mg/KgChromium, Hexavalent
V 92346-MS-L648525 V 92346-MSD-L648525Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
36.7 88.450864241.5< 0.143mg/KgChromium, Hexavalent 79.1 75-125
Page 41 of 42Date:11/17/2022 12:34 PM
Page 166 of 170
Quality Control Data
22-307-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-012
Dry Weight Determination
SW-DRYWT
V26113QC Analytical Batch:
Analysis Method:
Analysis Description:
V 92338-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/08/22 18:096.720.021.4%Moisture
V 92340-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/08/22 18:092.721.422.0%Moisture
Page 42 of 42Date:11/17/2022 12:34 PM
Page 167 of 170
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-307-0011
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Paula Blakeborough Date & Time:11/03/2022 11:06:36
Special precautions or instructions included?
Comments:
Page 168 of 170
Page 169 of 170
Page 170 of 170

Appendix B
Risk Calculator Summary Pages
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Soil (Worst Case)
North Carolina Department of Environmental Quality
Risk Calculator
Old Pineville Road
Old Pineville Rd & Scholtz Rd
DWM Brownfields
10061-06-060
July 2022
May 2022 EPA RSL Table
Prepared By:H&H
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 10061-06-060
Exposure Unit ID: Final Grade Soil (Worst Case)
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 10061-06-060
Exposure Unit ID: Final Grade Soil (Worst Case)
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.045 67-64-1 Acetone mg/kg
0.002 107-02-8 Acrolein mg/kg
2.54 7440-38-2 Arsenic, Inorganic mg/kg
107 7440-39-3 Barium mg/kg
0.002 74-83-9 Bromomethane mg/kg
0.177 7440-43-9 Cadmium (Diet)mg/kg
0.004 75-15-0 Carbon Disulfide mg/kg
0.001 74-87-3 Chloromethane mg/kg
48.8 16065-83-1 Chromium(III), Insoluble Salts mg/kg
20 7439-92-1 ~Lead and Compounds mg/kg
0.179 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.395 85-68-7 ~Butyl Benzyl Phthalate mg/kg
0.193 206-44-0 ~Fluoranthene mg/kg
0.778 7782-49-2 Selenium mg/kg
0.0638 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 10061-06-060
Exposure Unit ID: Final Grade Soil (Worst Case)
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 3.8E-06 1.3E-01 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 10061-06-060
Exposure Unit ID: Final Grade Soil (Worst Case)
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentratio
n (mg/kg)
Dermal
Concentratio
n (mg/kg)
Inhalation
Concentratio
n (mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.045 0.045 0.045 6.4E-07 6.4E-07
107-02-8 Acrolein 0.002 0.002 0.002 5.1E-05 1.3E-02 1.3E-02
7440-38-2 Arsenic, Inorganic 2.54 2.54 2.54 3.3E-06 4.6E-07 6.6E-11 3.8E-06 6.5E-02 7.7E-03 2.7E-06 7.3E-02
7440-39-3 Barium 107 107 107 6.8E-03 3.5E-06 6.8E-03
74-83-9 Bromomethane 0.002 0.002 0.002 1.8E-05 1.2E-04 1.4E-04
7440-43-9 Cadmium (Diet)0.177 0.177 0.177 1.9E-12 1.9E-12 2.3E-02 2.1E-03 2.9E-07 2.5E-02
75-15-0 Carbon Disulfide 0.004 0.004 0.004 5.1E-07 1.7E-06 2.3E-06
74-87-3 Chloromethane 0.001 0.001 0.001 3.4E-06 3.4E-06
16065-83-1 Chromium(III), Insoluble Salts 48.8 48.8 48.8 4.2E-04 4.2E-04
7439-92-1 ~Lead and Compounds 20 20 20 <SL**<SL**<SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.179 0.179 0.179 7.6E-03 9.6E-09 7.6E-03
85-68-7 ~Butyl Benzyl Phthalate 0.395 0.395 0.395 1.1E-09 3.0E-10 1.4E-09 2.5E-05 6.0E-06 3.1E-05
206-44-0 ~Fluoranthene 0.193 0.193 0.193 6.2E-05 1.9E-05 8.1E-05
7782-49-2 Selenium 0.778 0.778 0.778 2.0E-03 6.3E-10 2.0E-03
7440-22-4 Silver 0.0638 0.0638 0.0638 1.6E-04 1.6E-04
Cumulative:3.8E-06 1.3E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening
level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator