20061-SouthGlenburnieClosureRpt(1) recd 12-9-16

UST and AST CLOSURE AND REMEDIATION REPORT
SOUTH GLENBURNIE ROAD SITE — 3704 and 3706 TRENT ROAD
NEW BERN, CRAVEN COUNTY
NORTH CAROLINA
BROWNFIELDS PROJECT NO.20061-16-025
GRI PROJECT NO.3841
Prepared for:
Mr. James Rudder
North Carolina of Department of Environmental Quality
Division of Waste Management
Brownfields Program
217 West Jones Street
Raleigh, North Carolina 27603
and
Columbia Development and CDG-New Bern. LLC
1845 St. Julian Place
Columbia, South Carolina 29204
Prepared by:
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
December 9, 2016
a"Oer�5�7 -0�.
Angela Roach
Project Manager
JA o4or-P
Rae Troiano, P.G.
Project Manager
704.698-1254

PROJECT INFORMATION
• Project Name:
• Brownfields Project Number:
• Location:
• Land Use Classification:
• Consultant:
• Laboratory:
• Latitude/Longitude:
Certification
I, Rae Troiano Brown, a Licensed Geologist
contained in this report is correct and accura
Geological Resources, Inc. is licensed
certification numbers of the company are
South Glenburnie Road Site (aka Clarke Power Services)
20061-16-025
Intersection of South Glenburnie and ML King Jr. Blvd.
New Bern, Craven County
Commercial
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
Accutest Southeast Laboratories
4405 Vineland Road
Suite C-15
Orlando, Florida 32811
[phone]
State Certification Number: 573
35.0968500 North/77.1018970 West
Resources, Inc., do certify that the information
;any knowledge.
engineering in North Carolina. The

PROJECT INFORMATION
Project Name: South Glenbumie Road Site (aka Clarke Power Services)
Brownfields Project Number: 20061-16-025
Location: Intersection of South Glenburnie and ML King Jr. Blvd.
New Bern, Craven County
Land Use Classification: Commercial
Consultant: Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
Laboratory:
Latitude/Longitude:
Certification
Accutest Southeast Laboratories
4405 Vineland Road
Suite C-15
Orlando, Florida 32811
[phone]
State Certification Number: 573
35.096850' North/77.101897° West
I, Rae Troiano Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.
Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the company are C-127 and C-2727, respectively.

EXECUTIVE SUMMARY
The South Glenburnie Road Site/ Clarke Power Services Site (Brownfields Project Number 20061-16-025)
is located at the southwest intersection of South Glenburnie Road and ML King Jr. Boulevard in New Bern,
Craven County, North Carolina. Land use in the area is comprised of a mixture of commercial and
residential properties. Currently, approximately 31.62 acres owned by multiple entities are being acquired
by CDG-New Bern, LLC (CDG) for re -development into a retail shopping center.
In May 2015, during a Phase I Environmental Site Assessment (ESA), several Recognized Environmental
Concerns were identified which included historical heating oil USTs and ASTs located at the six residences
located on Trent Road. Subsequently, in November 2015, during Phase II ESA activities, temporary
monitoring wells were installed and ground water samples were collected from the residences. Laboratory
results confirmed ground water contamination at 3704 and 3706 Trent Road.
On November 30, 2016, Geological Resources, Inc. directed soil excavation in the location of the former
temporary monitoring well at 3704 Trent Road. Impacted soil was observed in the saturated zone of the
excavation, approximately 8 to 10 feet below ground surface (BGS). The final excavation was
approximately 11 feet wide by 11 feet long by 12 feet deep. The excavation basin was de -watered prior to
filling it with clean regional sand.
On November 30 and December 1, 2016, at 3706 Trent Road, soil was excavated in the location of the
former monitoring well and the hydraulic lift was excavated and removed. Impacted soil was observed in
the saturated zone approximately 7 to 11 feet BGS. The final excavation was approximately 17 feet long
by 14 feet wide by 12 feet deep. The excavation basin was de -watered prior to filling it with clean regional
sand.
On December 5, 2016, four soil samples were collected from the perimeter of the excavation areas; and,
one soil sample was collected in the former location of the hydraulic lift located at 3706 Trent Road. Soil
samples were analyzed using EPA Methods 8260 and 8270. Estimated concentrations of acetone, methyl
cyclohexane, and/or 1,2,4 trimethylbenzene were reported in three soil samples. However, none of the
estimated concentrations exceeded the Preliminary Soil Remediation Goals for protection of ground water
or Industrial Health.

On December 2, 2016, subsequent to excavation activities, temporary monitoring wells were installed at
3704 and 3706 Trent Road. Ground water samples were collected and submitted for laboratory analysis
using SW 846 8260B and 8270B. Estimated concentrations of 1-methylnaphthalene, 2- methylnaphthalene,
and 1,2,4 trimethylbenzene were reported in ground water samples collected from 3706 Trent Road.
However, none of the estimated concentrations exceeded the Maximum Allowable Concentrations or the
non-residential Ground Water Screening Levels for Vapor Intrusion
Based on these data, there are no soil violations or vapor intrusion conditions at 3704 or 3706 Trent Road.

TABLE OF CONTENTS
1.0
INTRODUCTION.........................................................................................................................1
2.0
EXCAVATION ACTIVITIES......................................................................................................1
3.0
SOIL................................................................................................................................................2
4.0
GROUND WATER........................................................................................................................3
5.0
CONCLUSIONS AND RECOMMENDATIONS.......................................................................3
6.0
LIMITATIONS.............................................................................................................................. 4
FIGURES
Figure 1:
Site Location Map
Figure 2:
South Glenburnie Overview Map
Figure 3:
Excavation Map
Figure 4:
Well Location Map
TABLES
Table 1: Summary of Soil Sample Analytical Results
Table 2: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: Excavation Photographs
Appendix B: Subsurface Boring Logs
Appendix C: Laboratory Analytical Report - Soil
Appendix D: Laboratory Analytical Report — Ground Water

1.0 INTRODUCTION
The South Glenburnie Road Site/ Clarke Power Services Site (Brownfields Project Number 20061-16-025)
(Site) is comprised of approximately 31.62 acres located at the southwest intersection of South Glenburnie
Road and ML King Jr. Boulevard in New Bern, Craven County, North Carolina (Figures 1 and 2).
Currently, the area is owned by multiple entities; however, CDG-New Bern, LLC (CDG) is in the process
of acquiring them. Subsequent to their acquisition, CDG intends to remove existing buildings and re-
develop the Site into a retail shopping center.
In May 2015, ECS Carolinas LLP conducted a Phase I Environmental Site Assessment (ESA) at the South
Glenbumie Properties and identified Recognized Environmental Concerns (RECs) that included historical
heating oil USTs and ASTs located at six Trent Road Residences.
In November 2015, as part of the Phase II ESA activities, Geological Resources, Inc. (GRI) collected
ground water samples from the Trent Road residences. Concentrations of naphthalene, 1-
methylnaphthalene and 2- methylnaphthalene reported in ground water samples collected from 3704 Trent
Road and 3706 Trent Road exceeded the Maximum Allowable Concentrations (MACS). Concentrations of
naphthalene and/or 1,2,4 trimethylbenzene exceeded the non-residential Ground Water Screening Levels
(GWSLs) for Vapor Intrusion in samples collected at 3704 and 3706 Trent Road.
In order to reduce the ground water contamination and remove concern for vapor intrusion, soil excavation
and dewatering activities were conducted at 3704 and 3706 Trent Road.
Please refer to earlier reports for details pertaining to the Phase I ESA and Phase II ESA assessments.
2.0 EXCAVATION ACTIVITIES
On November 30, 2016, the area in the former location of the ESA temporary well at 3704 Trent Road was
excavated. Impacted soil was observed toward the house, in the saturated zone of the excavation,
approximately 8 to 10 feet below ground surface (BGS). Soil was saturated approximately 5 to 6 feet BGS.
The impacted soil was removed and the excavation remained open until the end of the work day when it
was de -watered and filled with clean regional sand. The final dimensions of the excavation were
approximately 11 feet long by 11 feet wide by 12 feet deep. The property owner was on -site during
excavation activities. According to Mrs. Harrell, who lived in the house as a child, an AST was located in
the excavation area.
1

On November 30 and December 1, 2016, the area in the former location of the ESA temporary well at 3706
Trent Road was excavated. Impacted soil was observed southeast of former temporary well location and
extended toward the residence, in the saturated zone of the excavation, approximately 7 to 11 feet BGS.
Soil was saturated approximately 5 to 6 feet BGS. The impacted soil was removed and the excavation
remained open until the end of the work day when it was de -watered and filled with clean regional sand.
During excavation, a 280-gallon UST was removed. The UST was pitted and in very poor condition. The
final dimensions of the excavation were approximately 17 feet long by 14 feet wide by 12 feet deep.
On December 1, 2016, the hydraulic lift located at 3706 Trent Road was removed. The lift was overlain
by a concrete pad that was approximately 8 feet long by 8 feet wide and 6 inches thick. The lift cylinder
extended into the subsurface approximately 3 feet and was in good condition upon removal. There were
no visible signs of soil staining or leakage. The excavation area was limited to what was required to extract
the hydraulic cylinder.
The approximate excavation boundaries are shown on Figure 3. Copies of the soil and water disposal
manifests will be forwarded upon receipt. Photographs of the excavation activities are included in
Appendix A.
3.0 SOIL
On December 5, 2016, four soil samples (SS-8 (3) through SS-11 (3)) were collected from the side walls
of the excavation at 3704 Trent Road. Four soil samples (SS-12 (3) through SS-15 (3)) were collected from
the side walls of the excavation at 3706 Trent Road and one soil sample (SS-16 (3)) was collected in the
former location of the hydraulic lift. All soil samples were collected using a decontaminated hand -auger in
general accordance with the EPA standard protocol. Soil samples were taken above the seasonal high water
table, approximately 3 feet BGS. Soil samples were submitted for laboratory analysis using EPA Methods
8260 and 8270. All soil borings were properly abandoned subsequent to sample collection. Copies of the
subsurface logs are included in Appendix B.
Estimated concentrations of acetone, methyl cyclohexane, and/or 1,2,4 trimethylbenzene were reported in
soil samples SS-9 (3), SS-11 (3), and SS-12 (3). However, none of the estimated concentrations exceeded
the Preliminary Soil Remediation Goals (PSRGs) for protection of ground water or the PSRGs for Industrial
Health.
2

A summary of ground water analytical results is presented in Table 1. Soil boring locations are shown on
Figure 4. A copy of the laboratory report is included in Appendix C.
4.0 GROUND WATER
On December 2, 2016, temporary monitoring wells MW-A and MW-B were installed at 3704 and 3706
Trent Road, respectively. The monitoring wells were installed to 13 feet below ground surface and were
purged and sampled in general accordance with the EPA standard protocol. Ground water samples were
submitted for laboratory analysis using SW 846 8260B and 8270B. Both temporary monitoring wells were
properly abandoned subsequent to sample collection. Copies of the subsurface logs are included in
Appendix B.
No detectable concentrations were reported in samples collected from 3704 Trent Road (MW-A).
Estimated concentrations of 1-methylnaphthalene, 2- methylnaphthalene, and 1,2,4 trimethylbenzene were
reported in ground water samples collected from 3706 Trent Road. However, none of the estimated
concentrations exceeded the MACS or the non-residential GWSLs for Vapor Intrusion samples.
A summary of ground water analytical results is presented in Table 2. A Well Location Map is included
as Figure 4. A copy of the laboratory report is included in Appendix D.
5.0 CONCLUSIONS AND RECOMMENDATIONS
• The Site is 31.62 acres located at the southwest intersection of South Glenburnie Road and ML
King Jr. Boulevard. During a Phase I ESA and associated update report conducted in May and
August 2015, several RECs were identified that included historical heating oil USTs and ASTs
located at six Trent Road Residences.
• In November 2015, ground water assessed during a Phase II ESA reported contamination at 3704
and 3706 Trent Road that exceeded the MACS and the non-residential GWSL for vapor intrusion.
• On November 30 and December 1, 2016, the locations of the former ESA Phase I1 temporary wells
at 3704 and 3706 Trent Road were excavated.
• According to the property owner, an AST was located at 3704 Trent Road. Impacted soil was
observed in the saturated zone of the excavation, approximately 8 to 10 feet BGS. The final
excavation was approximately 11 feet wide by 11 feet long by 12 feet deep. The excavation basin
was de -watered prior to filling it with clean regional sand.
3

• On November 30 and December 1, 2016, at 3706 Trent Road, soil was excavated in the location of
the former monitoring well. Impacted soil was overserved in the saturated zone approximately 7
to 11 feet BGA. The final excavation was approximately 17 feet long by 14 feet wide by 12 feet
deep. The excavation basin was de -watered prior to filling it with clean regional sand. A 280-
gallon UST was removed during excavation.
• The hydraulic lift located at 3706 Trent Road was removed. No soil staining was observed and the
hydraulic cylinder was in good condition with no evidence of leaking.
• On December 5, 2016, four soil samples were collected from the perimeter of the UST and AST
excavation areas; and, one soil sample was collected in the former location of the hydraulic lift
located at 3706 Trent Road. Estimated concentrations of acetone, methyl cyclohexane, and/or 1,2,4
trimethylbenzene were reported in soil samples SS-9 (3), SS-11 (3), and SS-12 (3). However, none
of the estimated concentrations exceeded the PSRGs for protection of ground water or Industrial
Health.
• On December 2, 2016, temporary monitoring wells MW-A and MW-B were installed at 3704 and
3706 Trent Road, respectively. Estimated concentrations of 1-methylnaphthalene, 2-
methylnaphthalene, and 1,2,4 trimethylbenzene were reported in ground water samples collected
from 3706 Trent Road. However, none of the estimated concentrations exceeded the MACS or the
non-residential GWSLs for Vapor Intrusion.
• Based on these data, there are no soil violations or vapor intrusion conditions at 3704 or 3706 Trent
Road.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Columbia Development and CDG for specific
application to the referenced site in Craven County, North Carolina. The assessment was conducted based
on the scope of work and level of effort specified by the DEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
geology and hydrogeology practices in the State of North Carolina, available information, and our
professional judgment. No other warranty is expressed or implied.
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory reports and memo.
No additional information can logically be inferred from these data.
4

FIGURES

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f SITE LOCATION MAP
2116 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, '•
'' NORTH CAROLINA
• , CQ;; GRI PROJECT NO. 3841
.. PREPARED BY:
GEOLOGICAL RESOURCES, INC.
Nov NOVEMBER 20, 2015
— Ciao,,"
Geological Resources, Inc. t _

LEGEND
— - - — SUBJECT PROPERTY
BOUNDARY LINE
ADJACENT PROPERTY
BOUNDARY LINE
BUILDING FOOTPRINT
Note:
1. This Site Mop is based on data from the
Craven County GIS of NC.
2. These parcels were not professionally
surveyed- locations of features ore
approximate.
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ROAD
0 50 100 200 OVERVIEW MAP
2116 South Glenburnie Road
New Bern, Craven County, NC
6R( IN FEET ) GRI Project No. J841
Geological Resources, Inc. 1 inch = 100 ft Dote: 12108116 Drown by. ECH I Figure: 2

LEGEND
— - - — SUBJECT PROPERTY
BOUNDARY LINE
ADJACENT PROPERTY
BOUNDARY L/NE
BUILDING FOOTPRINT
_ . _ . _ _ _ EXCA VA T/ON AREA
® TEMPORARY MONITORING WELL
f SOIL BORING L OCA T/ON
Note:
1. This Site Map is based on data from the
Craven County GIS of NC.
2. These parcels were not professionally
surveyed- locations of features are
approximate.
I
' 1 I
-
1
I I I 1 -
I I I
I
� ► I I I
<— Residential Properties � ►
I SS-16 (3) I
1 �
1 I I 1
1 I 1 1 ► I
� ► 1 I ►
3708 ► I
I ® iI ►I SS-15 (3)
I SS-12 (3)
I' i 31 I
1 706 1
► SS-10 (3) 1
► ' �' 3704 Tren t 1
I 55-13 (3) I I
I1 SS-8 (3) L SS-14 (3) SS -II (3) 3702 Trent I 1 1 I 1
1 1 I
I I SS-9 �
(3) ► 1
► I
1 I
► 1
- 1 I
1 /
T' eN7- RO,4p
0 20 40 80 EXCA VA T/ON MAP
2116 South G/enburnie Road
New Bern, Craven County, NC
6R( IN FEET ) GRI Project No. 3841
Geological Resources, Inc. 1 inch = 40 ft Date: 12109116 Drown by. ECH I Figure: 3

LEGEND
- - - -
SUBJECT PROPERTY
BOUNDARY LINE
ADJACENT PROPERTY
BOUNDARY L/NE
BUILDING FOOTPRINT
EXCA VA T/ON AREA
®
TEMPORARY MON/TOR/NG WELL
Q
TYPE // MONITORING WELL
11 0s 15
DA TE SAMPLE COLLECTED
<0.20
BENZENE
<0.40
TOL UENE
<0.20
ETHYLBENZENE
<0.51
XYLENES
<0.30
MISE
<0.33
TE IRA CHL OR OE TH YL ENE
<1.0
NAPHTHALENE
NR
1-METHYLNAPHTYALENE
NR
2-METHYLNAPHTHALENE
NR
ARSENIC
NR
BAR/UM
NR
CHROMIUM
NR
LEAD
NR
MERCURY
CONCENTRATIONS IN agIL
<0.20 LESS THAN THE METHOD DETECTION LIMIT
SPECIFIED IN THE LABORATORY REPORT
ESTIMATED
VALUE
NR" ANAL YSIS NOT REQUESTED
CONCENTRATIONS IN BOLD EXCEEDED THE MAC
MAC - MAXIMUM ALLOWABLE CONCENTRATION
Note:
1. This Site Map is based on data from the
Craven County GIS of NC.
2. These parcels were not professionally
surveyed; locations of features are
approximate.
I
' ► I
' I 1
► I
1
� 1
' ► I ► ►
I � Residential Properties � ► I
� 1
► 1 MW-A ►
' ► ► 12 02 16 ►
1 <0.20 ►
I MW-B <0.20 ► I
1 12 02 16 I <0.25
1 <0.20 <0.56 I
1 ► 1 <0.20 <0 20 ►
► ' <0.25 1 <0.30 ►
<0.56 1 <L 0 1
<0.20 <0. 49 I
1 m.30 <0,55 ► J704 Trent
1 1 <t0 NR I 10 28 15
0-63 J NR <0.20 ►
1 I 0 82 J 1 NR <0.40 1
NR ► NR 1 4.5
I NR J706 NR <0.51 I
NR T 10 28 15 ► <0.30
► NR <0.33
<0.20
1 ► NR 52.1 /
I <0..8
1 _ „ J 13.8 187 1
7.9 1
<0.60 NR
► <0.65 L„-� ► NR I
154 NR
1 ► ,2 NR 1
1 I 447 NR 1
L NR 1 I
NR
I NR ►
NR
► NR 1
_ I I
_ I ►
_ It/
I
T' eN7- RO,4p
0 20 40 80 WELL L OCA T/ON MAP
2116 South G/enburnie Road
New Bern, Craven County, NC
6R( /N FEET ) GRI Project No. J841
Geological Resources, Inc. 1 inch = 40 ft Date: 12109116 Drown by. ECH I Figure: 4

TABLES

TABLE 1
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
SOUTH GLENBURNIE SITE
Date: 12/08/16
Analytical Method 4
SW846 8260B / 8270B
Contaminant of Concern 4
;
W
N
1
Date Collected
Sample
Z
a
Sample ID
Sample Location
Depth
W
(mm/dd/yy)
(feet)
[�
Protection of Ground Water PSRG (mg/kg)
0.0073
5.5
8.1
6.0
0.085
0.21
0.085
0.0050
Health Based PSRG - Industrial (mg/kg)
5.10
818
25.0
260
210
17.0
210
78.0
SS-8 (3')
12/05/2016
3704 Trent Road
3
<0.0013
<0.0012
<0.0011
<0.0030
<0.0012
<0.0021
<0.011
<0.0014
SS-9 (3')
12/05/2016
3704 Trent Road
3
<0.0011
<0.00095
<0.00091
<0.0024
<0.00093
<0.0017
0.0409 J
<0.0011
SS-10 (3')
12/05/2016
3704 Trent Road
3
<0.0011
<0.0010
<0.00096
<0.0025
<0.00098
<0.0018
<0.0090
<0.0012
SS-11 (3')
12/05/2016
3704 Trent Road
3
<0.0012
<0.0011
<0.0011
<0.0028
<0.0011
<0.0019
0.0166 J
<0.0013
SS-12 (3')
12/05/2016
3706 Trent Road
3
<0.0012
<0.0010
<0.0010
<0.0026
<0.0010
<0.0019
0.0121 J
<0.0012
SS-13 (3')
12/05/2016
3706 Trent Road
3
<0.0013
<0.0011
<0.0011
<0.0029
<0.0011
<0.0020
<0.010
<0.0013
SS-14 (3')
12/05/2016
3706 Trent Road
3
<0.0014
<0.0012
<0.0012
<0.0031
<0.0012
<0.0022
<0.011
<0.0014
SS-15 (3')
12/05/2016
3706 Trent Road
3
<0.0014
<0.0013
<0.0012
<0.0032
<0.0013
<0.0023
<0.012
<0.0015
3706 Trent Road
SS-16 (3')
12/05/2016
3
<0.0013
<0.0012
<0.0011
<0.0030
<0.0012
<0.0021
<0.011
<0.0014
Hydraulic Lift
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• PSRG: Preliminary Soil Remediation Goal; April 2016.
• < : Less than the method detection limit specified in the laboratory report
• J: Estimated value.
• An estimated concentration of Methycyclohexane (0.0028 J mg/Kg) was reported in SS-9(3).

TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SOUTH GLENBURNIE SITE
Analytical Method 4
SW846 8260B and 8270B
Contaminant of Concern 4
%
Date
Well ID
Collected
Sample location
(mm/dd/yy)
MAC ( /1)
1
600
600
500
20
6
6,000
100
70
0.7
70
400
1
30
GWSL - Vapor Non -Residential
(µg/1)
69.3
16,100
152
323
19,700
146
19,000,000
466,000
2,040
48.4
30.2
24.3
NE
NE
MW-A
12/02/16
3704 Trent Road
<0.20
<0.20
<0.25
<0.56
<0.20
<1.0
<10
<1.4
<0.20
<0.30
<0.50
<0.20
<0.49
<0.55
3704 TRENT
10/28/15
<0.20
<0.40
4.5
<0.51
<0.30
52.1
<10
40.6
22.7
<0.33
0.94 J
65.9
137
167
MW-B
12/02/16
3706 Trent Road
<0.20
<0.20
<0.25
<0.56
<0.20
<1.0
<10
<1.4
<0.20
<0.30
<0.50
0.29 J
0.63 J
0.82 J
3706 TRENT
10/28/15
<0.40
<0.80
13.8
7.9
<0.60
154
<20
<2.0
1 21.7
<0.65
<1.0
147
328
447
Notes:
• Results reported in micrograms per liter (µg/1).
• < : Less than the method detection limit specified in the laboratory report.
• MAC: Maximum Allowable Concentrations specified in T15A NCAC 2L.0202.
• GWSL: Ground Water Screening Level for vapor intrusion October 2016.
• NE: Not Established
• Concentrations in bold face type exceeded the MACs.
• Italicized concentrations exceeded the Non -Residential Vapor GWSLs.
Page 1 of 1

APPENDICES

Appendix A
Excavation Photographs

Js+1t �
Excavation at 3704 Trent Road.
r4
Final excavation area at 3704 Trent Road.
South Glenburnie Site
New Bern, North Carolina
Georogces, Inc.

r
a
i_.
Excavation area at 3706 Trent Road.
i
� y i
k - .
y t
st
L .i
Terminal sidewall; excavation limited to the south due
to the residence and to the east due the septic tank.
South Glenburnie Site
New Bern, North Carolina
Georagrcal Resources, Inc.

UST excavated at 3706 Trent Road.
Hydraulic lift at 3706 Trent Road.
South Glenburnie Site
6R New Bern, North Carolina
Georogrcal Resources, Inc.

Appendix B
Subsurface Boring Logs

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project SouthGlenbumie Project #: 3841
Address 3704 Trent Rd. New Bern NC
Boring Number SS-8 (3') Date Drilled 12105/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cart 94149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project#: 3841
Address 3704 Trent Rd. New Bern NC
Boring Number SS-9 (3') Date Drilled 12105116
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cart #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project#: 3841
Address 3704 Trent Rd. New Bern NC
Boring Number SS-10 (3') Date Drilled 12105/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cart #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Intewal(ft)
ppm
LITHOLOGY
0
0 -1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project M..3841
Address 3704 Trent Rd. New Bern NC
Boring Number SS-11 (3') Date Drilled 12/05/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cert #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 -1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Proect#: 3841
Address 3706 Trent Rd. New Bern NC
Boring Number SS-12 (T) Date Drilled 12/05/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cart #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project #: 3841
Address 3706 Trent Rd. New Bern NC
Boring Number SS-13 (3') Date Drilled 12/05/16
Sample Method Grab Drilling Method Hand Au er
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cert #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
_ 32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenbumie Project: #:3841
Address 3706 Trent Rd. New Bern NC
Boring Number SS-14 (T) Date Drilled 12/05/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cent #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project#: 3841
Address 3706 Trent Rd. New Bern NC
Boring Number SS-15(3') Date Drilled 12/05/16
Sample Method Grab Drilling Method Hand Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cert 94149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 - 1 Brown fine sand
2
1 - 3 Gray tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Project #: 3841
Address 3706 Trent Rd. New Bern NC
Boring Number SS-16 (3') Date Drilled 12/05/16
Sample Method Grab Drilling Method ;and Auger
Completion Details Borehole filled with onsite soil
Driller Jimmy D. Hines (NC Cart #4149-B) Log By Jimmy D. Hines
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
0 -1 Gray fine sand
2
1 - 3 Tan clayey sand
3
Soil sample taken
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Rd. Project #: 3841
Address 3706 Trent Rd. New Bern, NC
Boring Number MW-B Date Drilled 12/02/16
Sample Method Grab Drilling Method Hand Auger (4" boring)
Completion Details Abandoned with Bentonite & Capped with on -site soil after sampling.
Driller James R. Williamson (Cert. #4251-B) Log By JRW
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
2
4
wet
6
8
GW@8.63'
10
0 - 10' Tan fine sand.
8260
12
8270
10' - 12' Grey -Tan clayey sand.
14
16
18
20
22
24
26
28
30
32
34
Boring was properly abandoned with
Bentonite & Capped with on -site soil.
36
38
L
1-1
40
�L

Geological Resources, Inc. Phone: [phone]
3502 Hayes Road Fax: [phone]
Monroe, NC 28110
SUBSURFACE LOG
Project South Glenburnie Rd. Project #: 3841
Address 3704 Trent Rd. New Bern, NC
Boring Number MW-A Date Drilled 12/02/16
Sample Method Grab Drilling Method Hand Auger (4" boring)
Completion Details Abandoned with Bentonite & Capped with on -site soil after sampling.
Driller James R. Williamson (Cert. #4251-B) Log By JRW
Lab
Sample
OVA
Depth
Sample
Interval(ft)
ppm
LITHOLOGY
0
2
4
wet
6
8
GW@8.20'
10
0 - 10' Tan fine sand.
12
8260
8270
10' - 13' Grey -Tan clayey sand.
14
16
18
20
22
24
26
28
30
32
34
Boring was properly abandoned with
Bentonite & Capped with on -site soil.
36
38
40

Appendix C
Laboratory Analytical Report - Soil

5MI
ACCUTEST
Southeast
SGS ACCUTEST IS PART OF SGS, THE WORLD'S LEADING INSPECTION,
VERIFICATION, TESTING AND CERTIFICATION COMPANY.
Technical Report for
GRI (Geol ogi cal Resources Inc.)
South Glenburnie, 3511 & ML King Jr Blvd, New Burn, NC
3841
SGSAccutest Job Number: FA39257
Sampling Date: 12/05/ 16
Report to:
e-Hardcopy 2.0
Automated Report
GRI
3502 Hayes Rd
Monroe, NC 28110
rtb@geol ogi cal resourcesi nc. com; carri ekennedy@g I ogi cad resourcesi nc. com;
jj r@geol ogi cad resourcesi nc. com; [e-mail]
ATTN: Rae Brown
Total number of pages in report: 65
'? pCCRFO
2�
Test results contained within this data package meet the requirements Norm Farmer
of the National Environmental Laboratory Accreditation Program Technical Director
and/or state specific certification programs as applicable.
CI i ent Service contact: M una Mohammed 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FLO02), NY(12022), SC(96038001)
DoD ELAP(L-A-B 1-2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGSAccutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 - Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
1 of 65
SGS Accutest is the sole authority for authorizing edits or modifications to this document. T
Unauthorized modification of this report is strictly prohibited. Fn3ACCUTESES

Table of Contents
Sections:
-1-
Section1: Sample Summary...................................................................................................
Section2: Summary of Hits....................................................................................................
Section3: Sample Results .............................................................................................
3.1: FA39257-1: SS-8 (Y)....................................................................................................
3.2: FA39257-2: SS-9 (Y)....................................................................................................
3.3: FA39257-3: SS-10 (Y)..................................................................................................
3.4: FA39257-4: SS-11 (Y)..................................................................................................
3.5: FA39257-5: SS-12 (Y)..................................................................................................
3.6: FA39257-6: SS-13 (Y)..................................................................................................
3.7: FA39257-7: SS-14 (Y)..................................................................................................
3.8: FA39257-8: SS-15 (Y)..................................................................................................
3.9: FA39257-9: SS-16 (Y)..................................................................................................
Section4: Misc. Forms............................................................................................................
4.1: Chain of Custody...........................................................................................................
Section 5: GUMS Volatiles - QC Data Summaries..............................................................
5.1: Method Blank Summary................................................................................................
5.2: Blank Spike Summary...................................................................................................
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section 6: GUMS Semi-volatiles - QC Data Summaries.....................................................
6.1: Method Blank Summary................................................................................................
6.2: Blank Spike Summary...................................................................................................
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
3
4
5
6
10
14
18
22
26
30
34
38
42
43
46
47
51
55
5
60
62
64
6 2of 65
ACCUTEST
FA39257

SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA39257
South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Project No: 3841
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA39257-1
12/05/16
10:38 JDH
12/06/16
SO
Soil
SS-8 (Y)
FA39257-2
12/05/16
10:59 JDH
12/06/16
SO
Soil
SS-9 (Y)
FA39257-3
12/05/16
11:10 JDH
12/06/16
SO
Soil
SS-10 (Y)
FA39257-4
12/05/16
11:31 JDH
12/06/16
SO
Soil
SS-11 (Y)
FA39257-5
12/05/16
12:02 JDH
12/06/16
SO
Soil
SS-12 (Y)
FA39257-6
12/05/16
12:33 JDH
12/06/16
SO
Soil
SS-13 (Y)
FA39257-7
12/05/16
12:54 JDH
12/06/16
SO
Soil
SS-14 (Y)
FA39257-8
12/05/16
13:15 JDH
12/06/16
SO
Soil
SS-15 (Y)
FA39257-9
12/05/16
13:46 JDH
12/06/16
SO
Soil
SS-16 (Y)
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 65
ACCUTEST
FA39257

Summary of Hits
Job Number:
FA39257
Account:
GRI (Geological Resources Inc.)
Project:
South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Collected:
12/05/ 16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA39257-1 SS-8 (Y)
No hits reported in this sample.
FA39257-2 SS-9 (Y)
Acetone
Methylcyclohexane
1, 2, 4-Trimethylbenzene
FA39257-3 SS-10 (Y)
No hits reported in this sample.
FA39257-4 SS-11 (Y)
Acetone
FA39257-5 SS-12 (Y)
Acetone
FA39257-6 SS-13 (Y)
No hits reported in this sample.
FA39257-7 SS-14 (Y)
No hits reported in this sample.
FA39257-8 SS-15 (Y)
No hits reported in this sample.
FA39257-9 SS-16 (Y)
No hits reported in this sample.
0.0409 J 0.042 0.0085 mg/kg SW846 8260B
0.0028 J 0.0042 0.00084 mg/kg SW846 8260B
0.0021 J 0.0042 0.00084 mg/kg SW846 8260B
0.0166 J 0.048 0.0099 mg/kg SW846 8260B
0.0121 J 0.046 0.0095 mg/kg SW846 8260B
Page 1 of 1
6 4 of 65
ACCUTEST
FA39257

SG$
ACCUTEST
Southeast
Sample Results
Report of Analysis
i
,"ONE
Section 3
5 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-8 (Y )
Lab Sample ID: FA39257-1 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 82.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32742.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run #1 5.80 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.052
0.011
mg/kg
71-43-2
Benzene
ND
0.0052
0.0013
mg/kg
75-27-4
Bromodichloromethane
ND
0.0052
0.0010
mg/kg
75-25-2
Bromoform
ND
0.0052
0.0010
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.026
0.0095
mg/kg
104-51-8
n-Butylbenzene
ND
0.0052
0.0010
mg/kg
75-15-0
Carbon Disulfide
ND
0.0052
0.0010
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0052
0.0019
mg/kg
108-90-7
Chlorobenzene
ND
0.0052
0.0010
mg/kg
75-00-3
Chloroethane
ND
0.0052
0.0021
mg/kg
67-66-3
Chloroform
ND
0.0052
0.0013
mg/kg
110-82-7
Cyclohexane
ND
0.0052
0.0013
mg/kg
124-48-1
Dibromochloromethane
ND
0.0052
0.0010
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0052
0.0023
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0052
0.0010
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0052
0.0026
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0052
0.0010
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0052
0.0010
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0052
0.0011
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0052
0.0017
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0052
0.0010
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0052
0.0010
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0052
0.0012
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0052
0.0016
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0052
0.0017
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0052
0.0020
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0052
0.0010
mg/kg
100-41-4
Ethlbenzene
ND
0.0052
0.0011
mg/kg
591-78-6
2-Hexanone
ND
0.026
0.0091
mg/kg
98-82-8
Isopropylbenzene
ND
0.0052
0.0015
mg/kg
79-20-9
Methyl Acetate
ND
0.026
0.0089
mg/kg
74-83-9
Methyl Bromide
ND
0.0052
0.0027
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
lient Sample ID: SS-8 (Y )
gab Sample ID: FA39257-1 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 82.8
'roject: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0052
0.0025
mg/kg
108-87-2
Methylcyclohexane
ND
0.0052
0.0010
mg/kg
75-09-2
Methylene Chloride
ND
0.010
0.0042
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.026
0.011
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0052
0.0012
mg/kg
91-20-3
Naphthalene
ND
0.0052
0.0021
mg/kg
103-65-1
n-Propylbenzene
ND
0.0052
0.0013
mg/kg
100-42-5
Styrene
ND
0.0052
0.0010
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0052
0.0023
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0052
0.0014
mg/kg
108-88-3
Toluene
ND
0.0052
0.0012
mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0052
0.0015
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0052
0.0010
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0052
0.0019
mg/kg
79-01-6
Trichloroethylene
ND
0.0052
0.0012
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0052
0.0019
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0052
0.0010
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0052
0.0010
mg/kg
75-01-4
Vinyl Chloride
ND
0.0052
0.0017
mg/kg
1330-20-7
Xylene (total)
ND
0.016
0.0030
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
75-124%
17060-07-0
1,2-Dichloroethane-D4
112%
72-135%
2037-26-5
Toluene-D8
98%
75-126%
460-00-4
4-Bromofluorobenzene
101%
71-133%
(a) Associated BS recovery outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-8 (Y )
Lab Sample ID: FA39257-1 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 82.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689453.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run # 1 29.7 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
1.0
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.031
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.026
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.029
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.025
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.0
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.41
0.081
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.022
mg/kg
3&4-Methylphenol
ND
0.20
0.048
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.025
mg/kg
100-02-7
4-Nitrophenol
ND
1.0
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
1.0
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.024
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.025
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.026
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.029
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.024
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.022
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.026
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.028
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.024
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.041
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.028
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.031
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.036
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.029
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.028
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.026
mg/kg
218-01-9
Chrysene
ND
0.20
0.027
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.022
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 65
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SGS Accutest
Report of Analysis
Client Sample ID: SS-8 (3' )
Lab Sample ID: FA39257-1 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 82.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.026
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.41
0.041
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.041
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.041
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.41
0.081
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.026
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.41
0.041
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.025
mg/kg
86-73-7
Fluorene
ND
0.20
0.026
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.025
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.023
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.041
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.024
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.031
mg/kg
78-59-1
Isophorone
ND
0.20
0.021
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.032
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.023
mg/kg
91-20-3
Naphthalene
ND
0.20
0.031
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.027
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.039
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.025
mg/kg
129-00-0
Pyrene
ND
0.20
0.038
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
57%
40-102%
4165-62-2
Phenol-d5
61%
41-100%
118-79-6
2,4,6-Tribromophenol
97% a
42-108%
4165-60-0
Nitrobenzene-d5
65%
40-105%
321-60-8
2-Fluorobiphenyl
73%
43-107%
1718-51-0
Terphenyl-dl4
82%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 65
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SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-9 (Y )
Lab Sample ID: FA39257-2 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 81.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32743.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run #1 7.34 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
0.0409
0.042
0.0085 mg/kg J
71-43-2
Benzene
ND
0.0042
0.0011 mg/kg
75-27-4
Bromodichloromethane
ND
0.0042
0.00084 mg/kg
75-25-2
Bromoform
ND
0.0042
0.00084 mg/kg
78-93-3
2-Butanone (MEK)
ND
0.021
0.0076 mg/kg
104-51-8
n-Butylbenzene
ND
0.0042
0.00084 mg/kg
75-15-0
Carbon Disulfide
ND
0.0042
0.00084 mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0042
0.0015 mg/kg
108-90-7
Chlorobenzene
ND
0.0042
0.00084 mg/kg
75-00-3
Chloroethane
ND
0.0042
0.0017 mg/kg
67-66-3
Chloroform
ND
0.0042
0.0010 mg/kg
110-82-7
Cyclohexane
ND
0.0042
0.0010 mg/kg
124-48-1
Dibromochloromethane
ND
0.0042
0.00084 mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0042
0.0019 mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0042
0.00084 mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0042
0.0021 mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0042
0.00084 mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0042
0.00084 mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0042
0.00085 mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0042
0.0014 mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0042
0.00084 mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0042
0.00084 mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0042
0.0010 mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0042
0.0013 mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0042
0.0013 mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0042
0.0016 mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0042
0.00084 mg/kg
100-41-4
Ethlbenzene
ND
0.0042
0.00091 mg/kg
591-78-6
2-Hexanone
ND
0.021
0.0073 mg/kg
98-82-8
Isopropylbenzene
ND
0.0042
0.0012 mg/kg
79-20-9
Methyl Acetate
ND
0.021
0.0072 mg/kg
74-83-9
Methyl Bromide
ND
0.0042
0.0022 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
lient Sample ID: SS-9 (Y )
gab Sample ID: FA39257-2 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 81.3
'roject: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL Units Q
74-87-3
Methyl Chloride
ND
0.0042
0.0020 mg/kg
108-87-2
Methylcyclohexane
0.0028
0.0042
0.00084 mg/kg J
75-09-2
Methylene Chloride
ND
0.0084
0.0034 mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.021
0.0090 mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0042
0.00093 mg/kg
91-20-3
Naphthalene
ND
0.0042
0.0017 mg/kg
103-65-1
n-Propylbenzene
ND
0.0042
0.0010 mg/kg
100-42-5
Styrene
ND
0.0042
0.00084 mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0042
0.0019 mg/kg
127-18-4
Tetrachloroethylene
ND
0.0042
0.0011 mg/kg
108-88-3
Toluene
ND
0.0042
0.00095 mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0042
0.0012 mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0042
0.00084 mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0042
0.0015 mg/kg
79-01-6
Trichloroethylene
ND
0.0042
0.00098 mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0042
0.0016 mg/kg
95-63-6
1,2,4-Trimethylbenzene
0.0021
0.0042
0.00084 mg/kg J
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0042
0.00084 mg/kg
75-01-4
Vinyl Chloride
ND
0.0042
0.0014 mg/kg
1330-20-7
Xylene (total)
ND
0.013
0.0024 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
111%
72-135%
2037-26-5
Toluene-D8
97%
75-126%
460-00-4
4-Bromofluorobenzene
87%
71-133%
(a) Associated BS recovery outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
of 65
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SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-9 (Y )
Lab Sample ID: FA39257-2 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 81.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689456.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
1.0
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.030
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.026
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.028
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.025
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.0
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.40
0.081
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.022
mg/kg
3&4-Methylphenol
ND
0.20
0.048
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.025
mg/kg
100-02-7
4-Nitrophenol
ND
1.0
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
1.0
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.024
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.026
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.029
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.022
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.025
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.028
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.024
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.040
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.028
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.031
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.036
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.029
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.028
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.025
mg/kg
218-01-9
Chrysene
ND
0.20
0.027
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 12 of 65
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SGS Accutest
Report of Analysis
Client Sample ID: SS-9 (3' )
Lab Sample ID: FA39257-2 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 81.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.025
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.40
0.040
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.040
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.040
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.40
0.081
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.026
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.40
0.040
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.025
mg/kg
86-73-7
Fluorene
ND
0.20
0.026
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.025
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.023
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.040
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.031
mg/kg
78-59-1
Isophorone
ND
0.20
0.021
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.032
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.023
mg/kg
91-20-3
Naphthalene
ND
0.20
0.031
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.026
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.038
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.024
mg/kg
129-00-0
Pyrene
ND
0.20
0.038
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
55%
40-102%
4165-62-2
Phenol-d5
58%
41-100%
118-79-6
2,4,6-Tribromophenol
84% a
42-108%
4165-60-0
Nitrobenzene-d5
68%
40-105%
321-60-8
2-Fluorobiphenyl
78%
43-107%
1718-51-0
Terphenyl-dl4
60%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 65
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SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-10 (Y)
Lab Sample ID: FA39257-3 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.9
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32745.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run # 1 6.74 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.044
0.0090 mg/kg
71-43-2
Benzene
ND
0.0044
0.0011 mg/kg
75-27-4
Bromodichloromethane
ND
0.0044
0.00088 mg/kg
75-25-2
Bromoform
ND
0.0044
0.00088 mg/kg
78-93-3
2-Butanone (MEK)
ND
0.022
0.0080 mg/kg
104-51-8
n-Butylbenzene
ND
0.0044
0.00088 mg/kg
75-15-0
Carbon Disulfide
ND
0.0044
0.00088 mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0044
0.0016 mg/kg
108-90-7
Chlorobenzene
ND
0.0044
0.00088 mg/kg
75-00-3
Chloroethane
ND
0.0044
0.0018 mg/kg
67-66-3
Chloroform
ND
0.0044
0.0011 mg/kg
110-82-7
Cyclohexane
ND
0.0044
0.0011 mg/kg
124-48-1
Dibromochloromethane
ND
0.0044
0.00088 mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0044
0.0020 mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0044
0.00088 mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0044
0.0022 mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0044
0.00088 mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0044
0.00088 mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0044
0.00090 mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0044
0.0015 mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0044
0.00088 mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0044
0.00088 mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0044
0.0011 mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0044
0.0013 mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0044
0.0014 mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0044
0.0017 mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0044
0.00088 mg/kg
100-41-4
Ethlbenzene
ND
0.0044
0.00096 mg/kg
591-78-6
2-Hexanone
ND
0.022
0.0077 mg/kg
98-82-8
Isopropylbenzene
ND
0.0044
0.0012 mg/kg
79-20-9
Methyl Acetate
ND
0.022
0.0076 mg/kg
74-83-9
Methyl Bromide
ND
0.0044
0.0023 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 14 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-10 (Y)
Lab Sample ID: FA39257-3 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.9
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL Units Q
74-87-3
Methyl Chloride
ND
0.0044
0.0021 mg/kg
108-87-2
Methylcyclohexane
ND
0.0044
0.00088 mg/kg
75-09-2
Methylene Chloride
ND
0.0088
0.0035 mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.022
0.0095 mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0044
0.00098 mg/kg
91-20-3
Naphthalene
ND
0.0044
0.0018 mg/kg
103-65-1
n-Propylbenzene
ND
0.0044
0.0011 mg/kg
100-42-5
Styrene
ND
0.0044
0.00088 mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0044
0.0020 mg/kg
127-18-4
Tetrachloroethylene
ND
0.0044
0.0012 mg/kg
108-88-3
Toluene
ND
0.0044
0.0010 mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0044
0.0013 mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0044
0.00088 mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0044
0.0016 mg/kg
79-01-6
Trichloroethylene
ND
0.0044
0.0010 mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0044
0.0017 mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0044
0.00088 mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.0044
0.00088 mg/kg
75-01-4
Vinyl Chloride
ND
0.0044
0.0015 mg/kg
1330-20-7
Xylene (total)
ND
0.013
0.0025 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
110%
72-135%
2037-26-5
Toluene-D8
97%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
(a) Associated BS recovery outside control limits
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-10 (Y)
Lab Sample ID: FA39257-3 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.9
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689457.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run # 1 29.8 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
1.0
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.030
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.025
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.028
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.024
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.0
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.40
0.080
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.021
mg/kg
3&4-Methylphenol
ND
0.20
0.047
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.025
mg/kg
100-02-7
4-Nitrophenol
ND
1.0
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
1.0
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.024
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.026
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.029
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.025
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.028
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.040
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.028
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.030
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.036
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.029
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.028
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.025
mg/kg
218-01-9
Chrysene
ND
0.20
0.027
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-10 (3')
Lab Sample ID: FA39257-3 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.9
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.025
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.40
0.040
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.040
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.040
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.40
0.080
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.026
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.40
0.040
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.024
mg/kg
86-73-7
Fluorene
ND
0.20
0.026
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.025
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.022
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.040
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.031
mg/kg
78-59-1
Isophorone
ND
0.20
0.021
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.031
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.023
mg/kg
91-20-3
Naphthalene
ND
0.20
0.030
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.026
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.038
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.024
mg/kg
129-00-0
Pyrene
ND
0.20
0.037
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
60%
40-102%
4165-62-2
Phenol-d5
64%
41-100%
118-79-6
2,4,6-Tribromophenol
90% a
42-108%
4165-60-0
Nitrobenzene-d5
63%
40-105%
321-60-8
2-Fluorobiphenyl
78%
43-107%
1718-51-0
Terphenyl-dl4
84%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-11 (Y)
Lab Sample ID: FA39257-4 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 84.0
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32746.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run#1 6.16g 5.0ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
0.0166
0.048
0.0099 mg/kg J
71-43-2
Benzene
ND
0.0048
0.0012 mg/kg
75-27-4
Bromodichloromethane
ND
0.0048
0.00097 mg/kg
75-25-2
Bromoform
ND
0.0048
0.00097 mg/kg
78-93-3
2-Butanone (MEK)
ND
0.024
0.0088 mg/kg
104-51-8
n-Butylbenzene
ND
0.0048
0.00097 mg/kg
75-15-0
Carbon Disulfide
ND
0.0048
0.00097 mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0048
0.0017 mg/kg
108-90-7
Chlorobenzene
ND
0.0048
0.00097 mg/kg
75-00-3
Chloroethane
ND
0.0048
0.0019 mg/kg
67-66-3
Chloroform
ND
0.0048
0.0012 mg/kg
110-82-7
Cyclohexane
ND
0.0048
0.0012 mg/kg
124-48-1
Dibromochloromethane
ND
0.0048
0.00097 mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0048
0.0021 mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0048
0.00097 mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0048
0.0024 mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0048
0.00097 mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0048
0.00097 mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0048
0.00099 mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0048
0.0016 mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0048
0.00097 mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0048
0.00097 mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0048
0.0012 mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0048
0.0015 mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0048
0.0015 mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0048
0.0018 mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0048
0.00097 mg/kg
100-41-4
Ethlbenzene
ND
0.0048
0.0011 mg/kg
591-78-6
2-Hexanone
ND
0.024
0.0084 mg/kg
98-82-8
Isopropylbenzene
ND
0.0048
0.0014 mg/kg
79-20-9
Methyl Acetate
ND
0.024
0.0083 mg/kg
74-83-9
Methyl Bromide
ND
0.0048
0.0025 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-11 (Y)
Lab Sample ID: FA39257-4 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 84.0
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL Units Q
74-87-3
Methyl Chloride
ND
0.0048
0.0023 mg/kg
108-87-2
Methylcyclohexane
ND
0.0048
0.00097 mg/kg
75-09-2
Methylene Chloride
ND
0.0097
0.0039 mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.024
0.010 mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0048
0.0011 mg/kg
91-20-3
Naphthalene
ND
0.0048
0.0019 mg/kg
103-65-1
n-Propylbenzene
ND
0.0048
0.0012 mg/kg
100-42-5
Styrene
ND
0.0048
0.00097 mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0048
0.0021 mg/kg
127-18-4
Tetrachloroethylene
ND
0.0048
0.0013 mg/kg
108-88-3
Toluene
ND
0.0048
0.0011 mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0048
0.0014 mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0048
0.00097 mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0048
0.0017 mg/kg
79-01-6
Trichloroethylene
ND
0.0048
0.0011 mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0048
0.0018 mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0048
0.00097 mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0048
0.00097 mg/kg
75-01-4
Vinyl Chloride
ND
0.0048
0.0016 mg/kg
1330-20-7
Xylene (total)
ND
0.014
0.0028 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
97%
75-124%
17060-07-0
1,2-Dichloroethane-D4
102%
72-135%
2037-26-5
Toluene-D8
100%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
(a) Associated BS recovery outside control limits
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
99 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-11 (Y)
Lab Sample ID: FA39257-4 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 84.0
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689458.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run#1 30.2g 1.0ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
0.99
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.030
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.025
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.028
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.024
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.99
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.39
0.079
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.021
mg/kg
3&4-Methylphenol
ND
0.20
0.047
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.024
mg/kg
100-02-7
4-Nitrophenol
ND
0.99
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
0.99
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.023
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.025
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.029
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.025
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.028
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.039
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.028
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.030
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.035
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.029
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.027
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.025
mg/kg
218-01-9
Chrysene
ND
0.20
0.027
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 20 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-11 (3')
Lab Sample ID: FA39257-4 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 84.0
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.025
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.39
0.039
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.039
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.039
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.39
0.079
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.025
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.39
0.039
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.024
mg/kg
86-73-7
Fluorene
ND
0.20
0.025
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.024
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.022
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.039
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.030
mg/kg
78-59-1
Isophorone
ND
0.20
0.020
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.031
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.022
mg/kg
91-20-3
Naphthalene
ND
0.20
0.030
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.026
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.038
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.024
mg/kg
129-00-0
Pyrene
ND
0.20
0.037
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
61%
40-102%
4165-62-2
Phenol-d5
65%
41-100%
118-79-6
2,4,6-Tribromophenol
100% a
42-108%
4165-60-0
Nitrobenzene-d5
66%
40-105%
321-60-8
2-Fluorobiphenyl
78%
43-107%
1718-51-0
Terphenyl-dl4
77%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 21 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-12 (Y)
Lab Sample ID: FA39257-5 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 79.4
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32747.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run #1 6.78 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
0.0121
0.046
0.0095
mg/kg J
71-43-2
Benzene
ND
0.0046
0.0012
mg/kg
75-27-4
Bromodichloromethane
ND
0.0046
0.00093
mg/kg
75-25-2
Bromoform
ND
0.0046
0.00093
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.023
0.0084
mg/kg
104-51-8
n-Butylbenzene
ND
0.0046
0.00093
mg/kg
75-15-0
Carbon Disulfide
ND
0.0046
0.00093
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0046
0.0017
mg/kg
108-90-7
Chlorobenzene
ND
0.0046
0.00093
mg/kg
75-00-3
Chloroethane
ND
0.0046
0.0019
mg/kg
67-66-3
Chloroform
ND
0.0046
0.0011
mg/kg
110-82-7
Cyclohexane
ND
0.0046
0.0011
mg/kg
124-48-1
Dibromochloromethane
ND
0.0046
0.00093
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0046
0.0021
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0046
0.00093
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0046
0.0023
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0046
0.00093
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0046
0.00093
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0046
0.00095
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0046
0.0016
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0046
0.00093
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0046
0.00093
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0046
0.0011
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0046
0.0014
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0046
0.0015
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0046
0.0018
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0046
0.00093
mg/kg
100-41-4
Ethlbenzene
ND
0.0046
0.0010
mg/kg
591-78-6
2-Hexanone
ND
0.023
0.0081
mg/kg
98-82-8
Isopropylbenzene
ND
0.0046
0.0013
mg/kg
79-20-9
Methyl Acetate
ND
0.023
0.0080
mg/kg
74-83-9
Methyl Bromide
ND
0.0046
0.0024
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 22 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-12 (Y)
Lab Sample ID: FA39257-5 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 79.4
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0046
0.0022
mg/kg
108-87-2
Methylcyclohexane
ND
0.0046
0.00093
mg/kg
75-09-2
Methylene Chloride
ND
0.0093
0.0037
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.023
0.0099
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0046
0.0010
mg/kg
91-20-3
Naphthalene
ND
0.0046
0.0019
mg/kg
103-65-1
n-Propylbenzene
ND
0.0046
0.0012
mg/kg
100-42-5
Styrene
ND
0.0046
0.00093
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0046
0.0021
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0046
0.0012
mg/kg
108-88-3
Toluene
ND
0.0046
0.0010
mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0046
0.0014
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0046
0.00093
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0046
0.0017
mg/kg
79-01-6
Trichloroethylene
ND
0.0046
0.0011
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0046
0.0017
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0046
0.00093
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0046
0.00093
mg/kg
75-01-4
Vinyl Chloride
ND
0.0046
0.0016
mg/kg
1330-20-7
Xylene (total)
ND
0.014
0.0026
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
96%
75-124%
17060-07-0
1,2-Dichloroethane-D4
106%
72-135%
2037-26-5
Toluene-D8
99%
75-126%
460-00-4
4-Bromofluorobenzene
96%
71-133%
(a) Associated BS recovery outside control limits
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 23 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-12 (Y)
Lab Sample ID: FA39257-5 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 79.4
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689459.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run # 1 29.9 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
1.1
0.21
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.21
0.032
mg/kg
95-57-8
2-Chlorophenol
ND
0.21
0.027
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.21
0.030
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.21
0.026
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.1
0.21
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.42
0.084
mg/kg
95-48-7
2-Methylphenol
ND
0.21
0.023
mg/kg
3&4-Methylphenol
ND
0.21
0.050
mg/kg
88-75-5
2-Nitrophenol
ND
0.21
0.026
mg/kg
100-02-7
4-Nitrophenol
ND
1.1
0.17
mg/kg
87-86-5
Pentachlorophenola
ND
1.1
0.17
mg/kg
108-95-2
Phenol
ND
0.21
0.025
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.21
0.026
mg/kg
83-32-9
Acenaphthene
ND
0.21
0.027
mg/kg
208-96-8
Acenaphthylene
ND
0.21
0.026
mg/kg
120-12-7
Anthracene
ND
0.21
0.031
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.21
0.024
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.21
0.023
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.21
0.027
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.21
0.021
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.21
0.029
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.21
0.025
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.21
0.042
mg/kg
106-47-8
4-Chloroaniline
ND
0.21
0.029
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.21
0.032
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.21
0.038
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.21
0.031
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.21
0.029
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.21
0.027
mg/kg
218-01-9
Chrysene
ND
0.21
0.028
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.21
0.022
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 24 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-12 (3')
Lab Sample ID: FA39257-5 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 79.4
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.21
0.027
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.21
0.023
mg/kg
84-66-2
Diethyl Phthalate
ND
0.42
0.042
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.21
0.042
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.21
0.042
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.42
0.084
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.21
0.021
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.21
0.027
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.42
0.042
mg/kg
206-44-0
Fluoranthene
ND
0.21
0.026
mg/kg
86-73-7
Fluorene
ND
0.21
0.027
mg/kg
118-74-1
Hexachlorobenzene
ND
0.21
0.026
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.21
0.024
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.21
0.042
mg/kg
67-72-1
Hexachloroethane
ND
0.21
0.024
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.21
0.032
mg/kg
78-59-1
Isophorone
ND
0.21
0.022
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.21
0.033
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.21
0.024
mg/kg
91-20-3
Naphthalene
ND
0.21
0.032
mg/kg
98-95-3
Nitrobenzene
ND
0.21
0.028
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.21
0.022
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.21
0.040
mg/kg
85-01-8
Phenanthrene
ND
0.21
0.025
mg/kg
129-00-0
Pyrene
ND
0.21
0.039
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
58%
40-102%
4165-62-2
Phenol-d5
62%
41-100%
118-79-6
2,4,6-Tribromophenol
94% a
42-108%
4165-60-0
Nitrobenzene-d5
61%
40-105%
321-60-8
2-Fluorobiphenyl
70%
43-107%
1718-51-0
Terphenyl-dl4
74%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 25 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-13 (Y)
Lab Sample ID: FA39257-6 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 81.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32748.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run # 1 6.05 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.051
0.010
mg/kg
71-43-2
Benzene
ND
0.0051
0.0013
mg/kg
75-27-4
Bromodichloromethane
ND
0.0051
0.0010
mg/kg
75-25-2
Bromoform
ND
0.0051
0.0010
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.025
0.0092
mg/kg
104-51-8
n-Butylbenzene
ND
0.0051
0.0010
mg/kg
75-15-0
Carbon Disulfide
ND
0.0051
0.0010
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0051
0.0018
mg/kg
108-90-7
Chlorobenzene
ND
0.0051
0.0010
mg/kg
75-00-3
Chloroethane
ND
0.0051
0.0020
mg/kg
67-66-3
Chloroform
ND
0.0051
0.0012
mg/kg
110-82-7
Cyclohexane
ND
0.0051
0.0012
mg/kg
124-48-1
Dibromochloromethane
ND
0.0051
0.0010
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0051
0.0022
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0051
0.0010
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0051
0.0025
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0051
0.0010
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0051
0.0010
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0051
0.0010
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0051
0.0017
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0051
0.0010
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0051
0.0010
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0051
0.0012
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0051
0.0015
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0051
0.0016
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0051
0.0019
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0051
0.0010
mg/kg
100-41-4
Ethlbenzene
ND
0.0051
0.0011
mg/kg
591-78-6
2-Hexanone
ND
0.025
0.0088
mg/kg
98-82-8
Isopropylbenzene
ND
0.0051
0.0014
mg/kg
79-20-9
Methyl Acetate
ND
0.025
0.0087
mg/kg
74-83-9
Methyl Bromide
ND
0.0051
0.0026
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 26 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Aient Sample ID: SS-13 (Y)
gab Sample ID: FA39257-6 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 81.7
'roject: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0051
0.0024
mg/kg
108-87-2
Methylcyclohexane
ND
0.0051
0.0010
mg/kg
75-09-2
Methylene Chloride
ND
0.010
0.0040
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.025
0.011
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0051
0.0011
mg/kg
91-20-3
Naphthalene
ND
0.0051
0.0020
mg/kg
103-65-1
n-Propylbenzene
ND
0.0051
0.0013
mg/kg
100-42-5
Styrene
ND
0.0051
0.0010
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0051
0.0022
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0051
0.0013
mg/kg
108-88-3
Toluene
ND
0.0051
0.0011
mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0051
0.0015
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0051
0.0010
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0051
0.0018
mg/kg
79-01-6
Trichloroethylene
ND
0.0051
0.0012
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0051
0.0019
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0051
0.0010
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0051
0.0010
mg/kg
75-01-4
Vinyl Chloride
ND
0.0051
0.0017
mg/kg
1330-20-7
Xylene (total)
ND
0.015
0.0029
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
115%
72-135%
2037-26-5
Toluene-D8
100%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
(a) Associated BS recovery outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 27 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-13 (Y)
Lab Sample ID: FA39257-6 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 81.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689460.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run # 1 29.6 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
1.0
0.21
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.21
0.031
mg/kg
95-57-8
2-Chlorophenol
ND
0.21
0.026
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.21
0.029
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.21
0.025
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.0
0.21
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.41
0.083
mg/kg
95-48-7
2-Methylphenol
ND
0.21
0.022
mg/kg
3&4-Methylphenol
ND
0.21
0.049
mg/kg
88-75-5
2-Nitrophenol
ND
0.21
0.026
mg/kg
100-02-7
4-Nitrophenol
ND
1.0
0.17
mg/kg
87-86-5
Pentachlorophenola
ND
1.0
0.17
mg/kg
108-95-2
Phenol
ND
0.21
0.024
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.21
0.025
mg/kg
83-32-9
Acenaphthene
ND
0.21
0.027
mg/kg
208-96-8
Acenaphthylene
ND
0.21
0.026
mg/kg
120-12-7
Anthracene
ND
0.21
0.030
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.21
0.024
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.21
0.022
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.21
0.026
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.21
0.021
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.21
0.029
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.21
0.024
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.21
0.041
mg/kg
106-47-8
4-Chloroaniline
ND
0.21
0.029
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.21
0.031
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.21
0.037
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.21
0.030
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.21
0.028
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.21
0.026
mg/kg
218-01-9
Chrysene
ND
0.21
0.028
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.21
0.022
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 28 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-13 (3')
Lab Sample ID: FA39257-6 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 81.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.21
0.026
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.21
0.023
mg/kg
84-66-2
Diethyl Phthalate
ND
0.41
0.041
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.21
0.041
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.21
0.041
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.41
0.083
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.21
0.021
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.21
0.026
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.41
0.041
mg/kg
206-44-0
Fluoranthene
ND
0.21
0.025
mg/kg
86-73-7
Fluorene
ND
0.21
0.026
mg/kg
118-74-1
Hexachlorobenzene
ND
0.21
0.026
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.21
0.023
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.21
0.041
mg/kg
67-72-1
Hexachloroethane
ND
0.21
0.024
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.21
0.032
mg/kg
78-59-1
Isophorone
ND
0.21
0.021
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.21
0.032
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.21
0.023
mg/kg
91-20-3
Naphthalene
ND
0.21
0.032
mg/kg
98-95-3
Nitrobenzene
ND
0.21
0.027
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.21
0.022
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.21
0.039
mg/kg
85-01-8
Phenanthrene
ND
0.21
0.025
mg/kg
129-00-0
Pyrene
ND
0.21
0.039
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
58%
40-102%
4165-62-2
Phenol-d5
62%
41-100%
118-79-6
2,4,6-Tribromophenol
93% a
42-108%
4165-60-0
Nitrobenzene-d5
62%
40-105%
321-60-8
2-Fluorobiphenyl
71%
43-107%
1718-51-0
Terphenyl-dl4
73%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 29 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-14 (Y)
Lab Sample ID: FA39257-7 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 a Y32763.1)
1
12/07/16
AD
n/a
n/a
VY1300
Run #2 b Y32749.1)
1
12/06/16
EP
n/a
n/a
VY1299
Initial Weight Final Volume
Run # 1 5.47 g 5.0 ml
Run #2 4.36 g 5.0 ml
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.055
0.011
mg/kg
71-43-2
Benzene
ND
0.0055
0.0014
mg/kg
75-27-4
Bromodichloromethane
ND
0.0055
0.0011
mg/kg
75-25-2
Bromoform
ND
0.0055
0.0011
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.027
0.0099
mg/kg
104-51-8
n-Butylbenzene
ND
0.0055
0.0011
mg/kg
75-15-0
Carbon Disulfide
ND
0.0055
0.0011
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0055
0.0019
mg/kg
108-90-7
Chlorobenzene
ND
0.0055
0.0011
mg/kg
75-00-3
Chloroethane
ND
0.0055
0.0022
mg/kg
67-66-3
Chloroform
ND
0.0055
0.0013
mg/kg
110-82-7
Cyclohexane
ND
0.0055
0.0013
mg/kg
124-48-1
Dibromochloromethane
ND
0.0055
0.0011
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0055
0.0024
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0055
0.0011
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0055
0.0027
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0055
0.0011
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0055
0.0011
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0055
0.0011
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0055
0.0018
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0055
0.0011
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0055
0.0011
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0055
0.0013
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0055
0.0017
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0055
0.0017
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0055
0.0021
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0055
0.0011
mg/kg
100-41-4
Ethlbenzene
ND
0.0055
0.0012
mg/kg
591-78-6
2-Hexanone
ND
0.027
0.0095
mg/kg
98-82-8
Isopropylbenzene
ND
0.0055
0.0015
mg/kg
79-20-9
Methyl Acetate
ND
0.027
0.0094
mg/kg
74-83-9
Methyl Bromide
ND
0.0055
0.0028
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-14 (Y)
Lab Sample ID: FA39257-7 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0055
0.0026
mg/kg
108-87-2
Methylcyclohexane
ND
0.0055
0.0011
mg/kg
75-09-2
Methylene Chloride
ND
0.011
0.0044
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.027
0.012
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0055
0.0012
mg/kg
91-20-3
Naphthalene
ND
0.0055
0.0022
mg/kg
103-65-1
n-Propylbenzene
ND
0.0055
0.0014
mg/kg
100-42-5
Styrene
ND
0.0055
0.0011
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0055
0.0024
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0055
0.0014
mg/kg
108-88-3
Toluene
ND
0.0055
0.0012
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.0055
0.0016
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0055
0.0011
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0055
0.0020
mg/kg
79-01-6
Trichloroethylene
ND
0.0055
0.0013
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0055
0.0020
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0055
0.0011
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0055
0.0011
mg/kg
75-01-4
Vinyl Chloride
ND
0.0055
0.0018
mg/kg
1330-20-7
Xylene (total)
ND
0.016
0.0031
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
94%
75-124%
17060-07-0
1,2-Dichloroethane-D4
102%
0% c
72-135%
2037-26-5
Toluene-D8
100%
100%
75-126%
460-00-4
4-Bromofluorobenzene
103%
106%
71-133%
(a) Sample was prepared from a bulk container.
(b) Confirmation run for surrogate recoveries.
(c) Outside control limits due to matrix interference.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-14 (Y)
Lab Sample ID: FA39257-7 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689461.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run#1 30.0g 1.0ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
0.99
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.030
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.025
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.028
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.024
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.99
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.40
0.080
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.021
mg/kg
3&4-Methylphenol
ND
0.20
0.047
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.025
mg/kg
100-02-7
4-Nitrophenol
ND
0.99
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
0.99
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.024
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.026
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.029
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.025
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.028
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.040
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.028
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.030
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.036
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.029
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.027
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.025
mg/kg
218-01-9
Chrysene
ND
0.20
0.027
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 32 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-14 (3')
Lab Sample ID: FA39257-7 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.8
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.025
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.40
0.040
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.040
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.040
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.40
0.080
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.025
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.40
0.040
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.024
mg/kg
86-73-7
Fluorene
ND
0.20
0.025
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.025
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.022
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.040
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.031
mg/kg
78-59-1
Isophorone
ND
0.20
0.020
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.031
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.022
mg/kg
91-20-3
Naphthalene
ND
0.20
0.030
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.026
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.038
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.024
mg/kg
129-00-0
Pyrene
ND
0.20
0.037
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
55%
40-102%
4165-62-2
Phenol-d5
58%
41-100%
118-79-6
2,4,6-Tribromophenol
88% a
42-108%
4165-60-0
Nitrobenzene-d5
58%
40-105%
321-60-8
2-Fluorobiphenyl
68%
43-107%
1718-51-0
Terphenyl-dl4
69%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-15 (Y)
Lab Sample ID: FA39257-8 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32750.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run #1 5.25 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.057
0.012
mg/kg
71-43-2
Benzene
ND
0.0057
0.0014
mg/kg
75-27-4
Bromodichloromethane
ND
0.0057
0.0011
mg/kg
75-25-2
Bromoform
ND
0.0057
0.0011
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.028
0.010
mg/kg
104-51-8
n-Butylbenzene
ND
0.0057
0.0011
mg/kg
75-15-0
Carbon Disulfide
ND
0.0057
0.0011
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0057
0.0020
mg/kg
108-90-7
Chlorobenzene
ND
0.0057
0.0011
mg/kg
75-00-3
Chloroethane
ND
0.0057
0.0023
mg/kg
67-66-3
Chloroform
ND
0.0057
0.0014
mg/kg
110-82-7
Cyclohexane
ND
0.0057
0.0014
mg/kg
124-48-1
Dibromochloromethane
ND
0.0057
0.0011
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0057
0.0025
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0057
0.0011
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0057
0.0028
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0057
0.0011
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0057
0.0011
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0057
0.0012
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0057
0.0019
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0057
0.0011
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0057
0.0011
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0057
0.0014
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0057
0.0017
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0057
0.0018
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0057
0.0022
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0057
0.0011
mg/kg
100-41-4
Ethlbenzene
ND
0.0057
0.0012
mg/kg
591-78-6
2-Hexanone
ND
0.028
0.0099
mg/kg
98-82-8
Isopropylbenzene
ND
0.0057
0.0016
mg/kg
79-20-9
Methyl Acetate
ND
0.028
0.0098
mg/kg
74-83-9
Methyl Bromide
ND
0.0057
0.0029
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Aient Sample ID: SS-15 (Y)
gab Sample ID: FA39257-8 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 83.7
'roject: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0057
0.0027
mg/kg
108-87-2
Methylcyclohexane
ND
0.0057
0.0011
mg/kg
75-09-2
Methylene Chloride
ND
0.011
0.0046
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.028
0.012
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0057
0.0013
mg/kg
91-20-3
Naphthalene
ND
0.0057
0.0023
mg/kg
103-65-1
n-Propylbenzene
ND
0.0057
0.0014
mg/kg
100-42-5
Styrene
ND
0.0057
0.0011
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0057
0.0025
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0057
0.0015
mg/kg
108-88-3
Toluene
ND
0.0057
0.0013
mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0057
0.0017
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0057
0.0011
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0057
0.0021
mg/kg
79-01-6
Trichloroethylene
ND
0.0057
0.0013
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0057
0.0021
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0057
0.0011
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0057
0.0011
mg/kg
75-01-4
Vinyl Chloride
ND
0.0057
0.0019
mg/kg
1330-20-7
Xylene (total)
ND
0.017
0.0032
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
104%
75-124%
17060-07-0
1,2-Dichloroethane-D4
111%
72-135%
2037-26-5
Toluene-D8
98%
75-126%
460-00-4
4-Bromofluorobenzene
97%
71-133%
(a) Associated BS recovery outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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35 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-15 (Y)
Lab Sample ID: FA39257-8 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689462.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
0.98
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.029
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.025
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.028
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.024
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.98
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.39
0.078
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.021
mg/kg
3&4-Methylphenol
ND
0.20
0.046
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.024
mg/kg
100-02-7
4-Nitrophenol
ND
0.98
0.16
mg/kg
87-86-5
Pentachlorophenola
ND
0.98
0.16
mg/kg
108-95-2
Phenol
ND
0.20
0.023
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.025
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.025
mg/kg
120-12-7
Anthracene
ND
0.20
0.028
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.025
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.20
0.020
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.027
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.039
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.027
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.030
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.035
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.20
0.028
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.027
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.025
mg/kg
218-01-9
Chrysene
ND
0.20
0.026
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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36 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-15 (3')
Lab Sample ID: FA39257-8 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 83.7
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.20
0.025
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.022
mg/kg
84-66-2
Diethyl Phthalate
ND
0.39
0.039
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.039
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.039
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.39
0.078
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.20
0.020
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.20
0.025
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.39
0.039
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.024
mg/kg
86-73-7
Fluorene
ND
0.20
0.025
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.024
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.022
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.039
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.030
mg/kg
78-59-1
Isophorone
ND
0.20
0.020
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.031
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.022
mg/kg
91-20-3
Naphthalene
ND
0.20
0.030
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.026
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.021
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.037
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.024
mg/kg
129-00-0
Pyrene
ND
0.20
0.037
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
63%
40-102%
4165-62-2
Phenol-d5
65%
41-100%
118-79-6
2,4,6-Tribromophenol
101% a
42-108%
4165-60-0
Nitrobenzene-d5
68%
40-105%
321-60-8
2-Fluorobiphenyl
79%
43-107%
1718-51-0
Terphenyl-dl4
80%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-16 (Y)
Lab Sample ID: FA39257-9 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 89.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y32751.1) 1 12/06/16 EP n/a n/a VY1299
Run #2
Initial Weight Final Volume
Run # 1 5.31 g 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
0.053
0.011
mg/kg
71-43-2
Benzene
ND
0.0053
0.0013
mg/kg
75-27-4
Bromodichloromethane
ND
0.0053
0.0011
mg/kg
75-25-2
Bromoform
ND
0.0053
0.0011
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.026
0.0096
mg/kg
104-51-8
n-Butylbenzene
ND
0.0053
0.0011
mg/kg
75-15-0
Carbon Disulfide
ND
0.0053
0.0011
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0053
0.0019
mg/kg
108-90-7
Chlorobenzene
ND
0.0053
0.0011
mg/kg
75-00-3
Chloroethane
ND
0.0053
0.0021
mg/kg
67-66-3
Chloroform
ND
0.0053
0.0013
mg/kg
110-82-7
Cyclohexane
ND
0.0053
0.0013
mg/kg
124-48-1
Dibromochloromethane
ND
0.0053
0.0011
mg/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
0.0053
0.0023
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0053
0.0011
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0053
0.0026
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0053
0.0011
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0053
0.0011
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0053
0.0011
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0053
0.0018
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0053
0.0011
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0053
0.0011
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0053
0.0013
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
0.0053
0.0016
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0053
0.0017
mg/kg
10061-01-5
cis- 1, 3 -Dichloropropene
ND
0.0053
0.0020
mg/kg
10061-02-6
trans- 1, 3 -Dichloropropene
ND
0.0053
0.0011
mg/kg
100-41-4
Ethlbenzene
ND
0.0053
0.0011
mg/kg
591-78-6
2-Hexanone
ND
0.026
0.0092
mg/kg
98-82-8
Isopropylbenzene
ND
0.0053
0.0015
mg/kg
79-20-9
Methyl Acetate
ND
0.026
0.0090
mg/kg
74-83-9
Methyl Bromide
ND
0.0053
0.0027
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Aient Sample ID: SS-16 (Y)
gab Sample ID: FA39257-9 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8260B Percent Solids: 89.3
'roject: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
VOA Special List
CAS No.
Compound
Result
RL
MDL
Units Q
74-87-3
Methyl Chloride
ND
0.0053
0.0025
mg/kg
108-87-2
Methylcyclohexane
ND
0.0053
0.0011
mg/kg
75-09-2
Methylene Chloride
ND
0.011
0.0042
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.026
0.011
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0053
0.0012
mg/kg
91-20-3
Naphthalene
ND
0.0053
0.0021
mg/kg
103-65-1
n-Propylbenzene
ND
0.0053
0.0013
mg/kg
100-42-5
Styrene
ND
0.0053
0.0011
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0053
0.0023
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0053
0.0014
mg/kg
108-88-3
Toluene
ND
0.0053
0.0012
mg/kg
120-82-1
1,2,4-Trichlorobenzene a
ND
0.0053
0.0016
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0053
0.0011
mg/kg
79-00-5
1,1,2-Trichloroethane
ND
0.0053
0.0019
mg/kg
79-01-6
Trichloroethylene
ND
0.0053
0.0012
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0053
0.0020
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0053
0.0011
mg/kg
108-67-8
1, 3, 5-Trimethylbenzene
ND
0.0053
0.0011
mg/kg
75-01-4
Vinyl Chloride
ND
0.0053
0.0018
mg/kg
1330-20-7
Xylene (total)
ND
0.016
0.0030
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
104%
75-124%
17060-07-0
1,2-Dichloroethane-D4
107%
72-135%
2037-26-5
Toluene-D8
97%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
(a) Associated BS recovery outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: SS-16 (Y)
Lab Sample ID: FA39257-9 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 89.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0689463.13 1 12/07/16 MV 12/07/16 OP62980 SL3935
Run #2
Initial Weight Final Volume
Run#1 30.0g 1.0ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid a
ND
0.93
0.19
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.19
0.028
mg/kg
95-57-8
2-Chlorophenol
ND
0.19
0.024
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.19
0.026
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.19
0.023
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.93
0.19
mg/kg
534-52-1
4,6-Dinitro-o-cresol a
ND
0.37
0.075
mg/kg
95-48-7
2-Methylphenol
ND
0.19
0.020
mg/kg
3&4-Methylphenol
ND
0.19
0.044
mg/kg
88-75-5
2-Nitrophenol
ND
0.19
0.023
mg/kg
100-02-7
4-Nitrophenol
ND
0.93
0.15
mg/kg
87-86-5
Pentachlorophenola
ND
0.93
0.15
mg/kg
108-95-2
Phenol
ND
0.19
0.022
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.19
0.023
mg/kg
83-32-9
Acenaphthene
ND
0.19
0.024
mg/kg
208-96-8
Acenaphthylene
ND
0.19
0.023
mg/kg
120-12-7
Anthracene
ND
0.19
0.027
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.19
0.022
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.19
0.020
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.19
0.024
mg/kg
191-24-2
Benzo(g, h, i)perylene
ND
0.19
0.019
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.19
0.026
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.19
0.022
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.19
0.037
mg/kg
106-47-8
4-Chloroaniline
ND
0.19
0.026
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.19
0.028
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.19
0.033
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.19
0.027
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.19
0.026
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.19
0.024
mg/kg
218-01-9
Chrysene
ND
0.19
0.025
mg/kg
53-70-3
Dibenzo(a,h)anthracene
ND
0.19
0.020
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 40 of 65
ACCUTEST
FA39257

SGS Accutest
Report of Analysis
Client Sample ID: SS-16 (3')
Lab Sample ID: FA39257-9 Date Sampled: 12/05/16
Matrix: SO - Soil Date Received: 12/06/ 16
Method: SW846 8270D SW846 3550C Percent Solids: 89.3
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
0.19
0.024
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.19
0.021
mg/kg
84-66-2
Diethyl Phthalate
ND
0.37
0.037
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.19
0.037
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.19
0.037
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.37
0.075
mg/kg
121-14-2
2,4-Dinitrotoluene
ND
0.19
0.019
mg/kg
606-20-2
2, 6-Dinitrotoluene
ND
0.19
0.024
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.37
0.037
mg/kg
206-44-0
Fluoranthene
ND
0.19
0.023
mg/kg
86-73-7
Fluorene
ND
0.19
0.024
mg/kg
118-74-1
Hexachlorobenzene
ND
0.19
0.023
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.19
0.021
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.19
0.037
mg/kg
67-72-1
Hexachloroethane
ND
0.19
0.022
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.19
0.029
mg/kg
78-59-1
Isophorone
ND
0.19
0.019
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.19
0.029
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.19
0.021
mg/kg
91-20-3
Naphthalene
ND
0.19
0.028
mg/kg
98-95-3
Nitrobenzene
ND
0.19
0.025
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.19
0.020
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.19
0.036
mg/kg
85-01-8
Phenanthrene
ND
0.19
0.023
mg/kg
129-00-0
Pyrene
ND
0.19
0.035
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
56%
40-102%
4165-62-2
Phenol-d5
59%
41-100%
118-79-6
2,4,6-Tribromophenol
88% a
42-108%
4165-60-0
Nitrobenzene-d5
61%
40-105%
321-60-8
2-Fluorobiphenyl
71%
43-107%
1718-51-0
Terphenyl-dl4
69%
45-119%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 41 of 65
ACCUTEST
FA39257

SGSi
ACCUTEST
Southeast
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
i
Section 4
�r%6 42 of 65ACCUTEST
FA39257

o
FAM,®s■■e■■■o■■■M■M■■■■���■
©
■■®■■■■■■■u■■■■■■n■■■■■■■■■■■�
®
■■M■■■■■■■n■■■■■■u©■■■■■■■■■■�
■
■
FA39257: Chain of Custody
Page 1 of 3
6 43of 65
ACCUTEST
FA39257

SGS ACCUTEST - ORLANDO SAMPLE RECEIPT CONFIRMATION
SGS ACCUTEST'S JOB NUMBER: YA3q,257
CLIENT: PROJECT: 3V/
DATErrIME RECEIVED: /21(.r/Mp //OO (MM/DD/YY 24:001 NUMBER OF COOLERS RECEIVED:
METHOD OF DELIVERY: FEDEX UPS
ACCUTEST COURIER DELIVERY OTHER:
AIRBH.L NUMBERS: SOSf; gig(, g3U(e
COOLER INFORMATION
TEMPERATURE INFORMATION
SEAL NOT PRESENT OR NOT INTACT
/ CORR. FACTOR _ D.
CHAIN OF CUSTODY NOT RECEIVED (COC)
PIRT.ERMID_
OBSERVED TEMPS: r'/ I?
HCUSTODY
ANALYSIS REQUESTED IS UNCLEAR OR MISSING
CORRECTED TEMPS: 4. L (USED FOR LIMS)
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
SAMPLE INFORMATION
TEMPERATURE CRITERIA NOT MET
INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
TRIP BLANK INFORMATION
INSUFFICIENT VOLUME FOR ANALYSIS
TRIP BLANK PROVIDED
DATESTIMES ON COC DO NOT MATCH SAMPLE LABEL
TRIP BLANK NOT PROVIDED
ID'S ON COC DO NOT (HATCH LABEL
X
TRIP BLANK NOT ON COC
VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
TRIP BLANK INTACT
BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
TRIP BLANK NOT INTACT
NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED
RECEIVED WATER TRIP BLANK
FILTERING OR COMPOSITING INSTRUCTIONS
RECEIVED SOIL TRIP BLANK
-.
SAMPLE CONTAINER(S) RECEIVED BROKEN - -
5035 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
MISC. INFORMATION
]UNCLEAR
BULK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS
NUMBER OF ENCORES? 25-GRAM_ 5-CRAM
% SOLIDS JAR NOT RECEIVED
NUMBER OF 5035 FIELD KITS ?
RESIDUAL CHLORINE PRESENT LOT#
NUMBER OF LAB FILTERED METALS ?
(APPLICABLE TO EPA 400 SERIES OR NORTH CAROLPIA ORGANICS)
TEST STRIP LOT#s pH 0-3 230315
pH 10-12 219813A OTHER (specify)
SUMMARY OF COMMENTS:
TECHNICIAN SIGNATURE/DAT REVIEWERSIGNATUREMATE
NF 02/16 - receipt confirmation 020116.xis
FA39257: Chain of Custody
Page 2 of 3
6 44of 65
ACCUTEST
FA39257

0
FA39257: Chain of Custody
Page 3 of 3
6 45of 65
ACCUTEST
FA39257

SG$
ACCUTEST
Southeast
GUMS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
0
Section 5
�r%6 46 of 65ACCUTEST
FA39257

Method Blank Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1299-MB
Y32741.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
50
10
ug/kg
71-43-2
Benzene
ND
5.0
1.3
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.0
ug/kg
78-93-3
2-Butanone (MEK)
ND
25
9.1
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
75-15-0
Carbon Disulfide
ND
5.0
1.0
ug/kg
56-23-5
Carbon Tetrachloride
ND
5.0
1.8
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.0
ug/kg
67-66-3
Chloroform
ND
5.0
1.2
ug/kg
110-82-7
Cyclohexane
ND
5.0
1.2
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
2.2
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
2.5
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
5.0
1.0
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
5.0
1.0
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
5.0
1.7
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
5.0
1.0
ug/kg
156-59-2
cis- 1, 2-Dichloroethylene
ND
5.0
1.2
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
5.0
1.5
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.6
ug/kg
10061-01-5 cis- 1, 3-Dichloropropene
ND
5.0
1.9
ug/kg
10061-02-6 trans- 1, 3-Dichloropropene
ND
5.0
1.0
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.1
ug/kg
591-78-6
2-Hexanone
ND
25
8.7
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.4
ug/kg
79-20-9
Methyl Acetate
ND
25
8.6
ug/kg
74-83-9
Methyl Bromide
ND
5.0
2.6
ug/kg
74-87-3
Methyl Chloride
ND
5.0
2.4
ug/kg
108-87-2
Methylcyclohexane
ND
5.0
1.0
ug/kg
75-09-2
Methylene Chloride
ND
10
4.0
ug/kg
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
25
11
ug/kg
6 47 of 65
ACCUTEST
FA39257

Method Blank Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1299-MB
Y32741.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.1
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.2
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
2.2
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
5.0
1.1
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.5
ug/kg
71-55-6
1, 1, 1-Trichloroethane
ND
5.0
1.0
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.8
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.2
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
1.9
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
75-01-4
Vinyl Chloride
ND
5.0
1.7
ug/kg
1330-20-7
Xylene (total)
ND
15
2.9
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
103%
72-135%
2037-26-5
Toluene-D8
101%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
6 48 of 65
ACCUTEST
FA39257

Method Blank Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1300-MB
Y32762.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-7
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
50
10
ug/kg
71-43-2
Benzene
ND
5.0
1.3
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.0
ug/kg
78-93-3
2-Butanone (MEK)
ND
25
9.1
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
75-15-0
Carbon Disulfide
ND
5.0
1.0
ug/kg
56-23-5
Carbon Tetrachloride
ND
5.0
1.8
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.0
ug/kg
67-66-3
Chloroform
ND
5.0
1.2
ug/kg
110-82-7
Cyclohexane
ND
5.0
1.2
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
2.2
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
2.5
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
5.0
1.0
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
5.0
1.0
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
5.0
1.7
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
5.0
1.0
ug/kg
156-59-2
cis- 1, 2-Dichloroethylene
ND
5.0
1.2
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
5.0
1.5
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.6
ug/kg
10061-01-5 cis- 1, 3-Dichloropropene
ND
5.0
1.9
ug/kg
10061-02-6 trans- 1, 3-Dichloropropene
ND
5.0
1.0
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.1
ug/kg
591-78-6
2-Hexanone
ND
25
8.7
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.4
ug/kg
79-20-9
Methyl Acetate
ND
25
8.6
ug/kg
74-83-9
Methyl Bromide
ND
5.0
2.6
ug/kg
74-87-3
Methyl Chloride
ND
5.0
2.4
ug/kg
108-87-2
Methylcyclohexane
ND
5.0
1.0
ug/kg
75-09-2
Methylene Chloride
ND
10
4.0
ug/kg
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
25
11
ug/kg
6 49 of 65
ACCUTEST
FA39257

Method Blank Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1300-MB
Y32762.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples:
FA39257-7
Method: SW846 8260B
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.1
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.2
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
2.2
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
5.0
1.1
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.5
ug/kg
71-55-6
1, 1, 1-Trichloroethane
ND
5.0
1.0
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.8
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.2
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
1.9
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
75-01-4
Vinyl Chloride
ND
5.0
1.7
ug/kg
1330-20-7
Xylene (total)
ND
15
2.9
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
98%
75-124%
17060-07-0
1,2-Dichloroethane-D4
99%
72-135%
2037-26-5
Toluene-D8
100%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
50 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1299-BS
Y32740.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
67-64-1
Acetone
250
168
67
61-152
71-43-2
Benzene
50
51.4
103
76-126
75-27-4
Bromodichloromethane
50
52.5
105
74-130
75-25-2
Bromoform
50
52.2
104
76-127
78-93-3
2-Butanone (MEK)
250
223
89
75-137
104-51-8
n-Butylbenzene
50
39.6
79
71-128
75-15-0
Carbon Disulfide
50
49.3
99
72-122
56-23-5
Carbon Tetrachloride
50
54.0
108
78-133
108-90-7
Chlorobenzene
50
48.9
98
81-129
75-00-3
Chloroethane
50
46.3
93
68-133
67-66-3
Chloroform
50
50.8
102
72-123
110-82-7
Cyclohexane
50
52.8
106
73-126
124-48-1
Dibromochloromethane
50
52.2
104
76-127
96-12-8
1,2-Dibromo-3-chloropropane
50
47.4
95
70-137
106-93-4
1,2-Dibromoethane
50
50.2
100
77-126
75-71-8
Dichlorodifluoromethane
50
46.7
93
68-168
95-50-1
1,2-Dichlorobenzene
50
46.7
93
80-129
541-73-1
1,3-Dichlorobenzene
50
43.0
86
81-129
106-46-7
1,4-Dichlorobenzene
50
42.0
84
76-130
75-34-3
1, 1 -Dichloroethane
50
52.5
105
73-125
107-06-2
1,2-Dichloroethane
50
52.4
105
74-128
75-35-4
1, 1 -Dichloroethylene
50
49.3
99
81-136
156-59-2
cis- 1, 2-Dichloroethylene
50
49.3
99
74-126
156-60-5
trans- 1, 2-Dichloroethylene
50
58.9
118
70-127
78-87-5
1,2-Dichloropropane
50
51.4
103
74-125
10061-01-5 cis- 1, 3-Dichloropropene
50
51.4
103
80-123
10061-02-6 trans- 1, 3-Dichloropropene
50
55.6
111
75-131
100-41-4
Ethylbenzene
50
47.3
95
77-123
591-78-6
2-Hexanone
250
236
94
72-133
98-82-8
Isopropylbenzene
50
49.5
99
80-136
79-20-9
Methyl Acetate
250
308
123
67-137
74-83-9
Methyl Bromide
50
48.9
98
65-139
74-87-3
Methyl Chloride
50
44.1
88
71-144
108-87-2
Methylcyclohexane
50
52.5
105
75-128
75-09-2
Methylene Chloride
50
50.5
101
74-137
108-10-1
4-Methyl-2-pentanone (MIBK)
250
257
103
76-132
* = Outside of Control Limits.
51 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1299-BS
Y32740.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
CAS No. Compound
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
79-34-5
1,1,2,2-Tetrachloroethane
127-18-4
Tetrachloroethylene
108-88-3
Toluene
120-82-1
1,2,4-Trichlorobenzene
71-55-6
1, 1, 1-Trichloroethane
79-00-5
1,1,2-Trichloroethane
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
75-01-4
Vinyl Chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
(a) Sporadic marginal failure.
* = Outside of Control Limits.
Spike
BSP
BSP
ug/kg
ug/kg
%
Limits
50
59.9
120
77-120
50
49.4
99
79-129
50
45.6
91
80-135
50
49.0
98
78-125
50
49.5
99
71-126
50
45.0
90
79-130
50
49.3
99
76-124
50
35.5
71* a
78-130
50
48.6
97
70-129
50
52.1
104
74-124
50
48.2
96
75-128
50
50.3
101
73-145
50
45.3
91
74-123
50
45.8
92
73-122
50
48.3
97
76-141
150
148
99
80-129
BSP Limits
103% 75-124%
100% 72-135%
100% 75-126%
98% 71-133%
52 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1300-BS
Y32761.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples:
FA39257-7
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
67-64-1
Acetone
250
195
78
61-152
71-43-2
Benzene
50
54.1
108
76-126
75-27-4
Bromodichloromethane
50
57.5
115
74-130
75-25-2
Bromoform
50
62.8
126
76-127
78-93-3
2-Butanone (MEK)
250
252
101
75-137
104-51-8
n-Butylbenzene
50
56.2
112
71-128
75-15-0
Carbon Disulfide
50
54.3
109
72-122
56-23-5
Carbon Tetrachloride
50
56.2
112
78-133
108-90-7
Chlorobenzene
50
54.3
109
81-129
75-00-3
Chloroethane
50
57.7
115
68-133
67-66-3
Chloroform
50
52.0
104
72-123
110-82-7
Cyclohexane
50
55.5
111
73-126
124-48-1
Dibromochloromethane
50
59.4
119
76-127
96-12-8
1,2-Dibromo-3-chloropropane
50
58.7
117
70-137
106-93-4
1,2-Dibromoethane
50
56.1
112
77-126
75-71-8
Dichlorodifluoromethane
50
52.3
105
68-168
95-50-1
1,2-Dichlorobenzene
50
55.7
ill
80-129
541-73-1
1,3-Dichlorobenzene
50
55.3
ill
81-129
106-46-7
1,4-Dichlorobenzene
50
54.3
109
76-130
75-34-3
1, 1 -Dichloroethane
50
53.9
108
73-125
107-06-2
1,2-Dichloroethane
50
54.3
109
74-128
75-35-4
1, 1 -Dichloroethylene
50
55.7
ill
81-136
156-59-2
cis- 1, 2-Dichloroethylene
50
51.6
103
74-126
156-60-5
trans- 1, 2-Dichloroethylene
50
59.9
120
70-127
78-87-5
1,2-Dichloropropane
50
54.4
109
74-125
10061-01-5 cis- 1, 3-Dichloropropene
50
55.4
Ill
80-123
10061-02-6 trans- 1, 3-Dichloropropene
50
60.2
120
75-131
100-41-4
Ethylbenzene
50
54.3
109
77-123
591-78-6
2-Hexanone
250
277
ill
72-133
98-82-8
Isopropylbenzene
50
56.7
113
80-136
79-20-9
Methyl Acetate
250
305
122
67-137
74-83-9
Methyl Bromide
50
53.7
107
65-139
74-87-3
Methyl Chloride
50
52.1
104
71-144
108-87-2
Methylcyclohexane
50
56.4
113
75-128
75-09-2
Methylene Chloride
50
55.2
110
74-137
108-10-1
4-Methyl-2-pentanone (MIBK)
250
291
116
76-132
* = Outside of Control Limits.
Method: SW846 8260B
53 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1300-BS
Y32761.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples:
FA39257-7
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
1634-04-4
Methyl Tert Butyl Ether
50
52.6
105
77-120
91-20-3
Naphthalene
50
60.5
121
79-129
103-65-1
n-Propylbenzene
50
54.7
109
80-135
100-42-5
Styrene
50
56.4
113
78-125
79-34-5
1,1,2,2-Tetrachloroethane
50
54.0
108
71-126
127-18-4
Tetrachloroethylene
50
56.3
113
79-130
108-88-3
Toluene
50
52.9
106
76-124
120-82-1
1,2,4-Trichlorobenzene
50
56.1
112
78-130
71-55-6
1, 1, 1-Trichloroethane
50
51.6
103
70-129
79-00-5
1,1,2-Trichloroethane
50
55.4
111
74-124
79-01-6
Trichloroethylene
50
54.9
110
75-128
75-69-4
Trichlorofluoromethane
50
59.9
120
73-145
95-63-6
1,2,4-Trimethylbenzene
50
54.5
109
74-123
108-67-8
1,3,5-Trimethylbenzene
50
53.3
107
73-122
75-01-4
Vinyl Chloride
50
51.6
103
76-141
1330-20-7
Xylene (total)
150
172
115
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
100%
72-135%
2037-26-5
Toluene-D8
99%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
* = Outside of Control Limits.
Method: SW846 8260B
54 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA39257-4MS
Y32752.D
1
12/06/16
EP
n/a
n/a
VY1299
FA39257-4MSD
Y32753.1)
1
12/06/16
EP
n/a
n/a
VY1299
FA39257-4
Y32746.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples:
Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
FA39257-4
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
67-64-1
Acetone
16.6 J
365
249
64
358
237
62
5
61-152/27
71-43-2
Benzene
ND
72.9
59.0
81
71.5
59.1
83
0
76-126/26
75-27-4
Bromodichloromethane
ND
72.9
60.5
83
71.5
61.4
86
1
74-130/25
75-25-2
Bromoform
ND
72.9
61.9
85
71.5
58.6
82
5
76-127/26
78-93-3
2-Butanone (MEK)
ND
365
276
76
358
284
79
3
75-137/25
104-51-8
n-Butylbenzene
ND
72.9
55.7
76
71.5
56.0
78
1
71-128/35
75-15-0
Carbon Disulfide
ND
72.9
59.8
82
71.5
57.9
81
3
72-122/29
56-23-5
Carbon Tetrachloride
ND
72.9
54.3
74*
71.5
54.7
76*
1
78-133/29
108-90-7
Chlorobenzene
ND
72.9
60.4
83
71.5
60.3
84
0
81-129/29
75-00-3
Chloroethane
ND
72.9
53.7
74
71.5
50.5
71
6
68-133/29
67-66-3
Chloroform
ND
72.9
60.4
83
71.5
61.0
85
1
72-123/26
110-82-7
Cyclohexane
ND
72.9
49.8
68*
71.5
48.6
68*
2
73-126/32
124-48-1
Dibromochloromethane
ND
72.9
61.1
84
71.5
61.3
86
0
76-127/27
96-12-8
1,2-Dibromo-3-chloropropane
ND
72.9
58.0
80
71.5
57.9
81
0
70-137/29
106-93-4
1,2-Dibromoethane
ND
72.9
63.7
87
71.5
62.2
87
2
77-126/26
75-71-8
Dichlorodifluoromethane
ND
72.9
45.6
63*
71.5
45.0
63*
1
68-168/29
95-50-1
1,2-Dichlorobenzene
ND
72.9
60.5
83
71.5
60.6
85
0
80-129/32
541-73-1
1,3-Dichlorobenzene
ND
72.9
60.4
83
71.5
60.5
85
0
81-129/33
106-46-7
1,4-Dichlorobenzene
ND
72.9
61.0
84
71.5
59.9
84
2
76-130/32
75-34-3
1, 1 -Dichloroethane
ND
72.9
60.7
83
71.5
62.8
88
3
73-125/27
107-06-2
1,2-Dichloroethane
ND
72.9
64.5
88
71.5
64.4
90
0
74-128/23
75-35-4
1, 1 -Dichloroethylene
ND
72.9
59.9
82
71.5
57.3
80*
4
81-136/28
156-59-2
cis- 1, 2-Dichloroethylene
ND
72.9
60.1
82
71.5
60.4
84
0
74-126/26
156-60-5
trans- 1, 2-Dichloroethylene
ND
72.9
66.6
91
71.5
69.2
97
4
70-127/27
78-87-5
1,2-Dichloropropane
ND
72.9
62.4
86
71.5
61.6
86
1
74-125/25
10061-01-5 cis- 1, 3-Dichloropropene
ND
72.9
62.3
85
71.5
62.2
87
0
80-123/26
10061-02-6 trans- 1, 3-Dichloropropene
ND
72.9
64.8
89
71.5
64.5
90
0
75-131/28
100-41-4
Ethylbenzene
ND
72.9
59.7
82
71.5
59.4
83
1
77-123/31
591-78-6
2-Hexanone
ND
365
296
81
358
290
81
2
72-133/26
98-82-8
Isopropylbenzene
ND
72.9
58.3
80
71.5
58.0
81
1
80-136/32
79-20-9
Methyl Acetate
ND
365
492
135
358
588
164*
18
67-137/30
74-83-9
Methyl Bromide
ND
72.9
57.6
79
71.5
53.0
74
8
65-139/31
74-87-3
Methyl Chloride
ND
72.9
54.4
75
71.5
52.4
73
4
71-144/27
108-87-2
Methylcyclohexane
ND
72.9
46.1
63*
71.5
45.4
63*
2
75-128/31
75-09-2
Methylene Chloride
ND
72.9
76.8
105
71.5
73.8
103
4
74-137/28
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
365
331
91
358
324
91
2
76-132/26
* = Outside of Control Limits.
55 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A39257-4MS
Y32752.D
1
12/06/16
EP
n/a
n/a
VY1299
'A39257-4MSD
Y32753.1)
1
12/06/16
EP
n/a
n/a
VY1299
'A39257-4
Y32746.1)
1
12/06/16
EP
n/a
n/a
VY1299
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-8, FA39257-9
FA39257-4
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
72.9
66.0
90
71.5
72.7
102
10
77-120/24
91-20-3
Naphthalene
ND
72.9
59.9
82
71.5
59.7
83
0
79-129/33
103-65-1
n-Propylbenzene
ND
72.9
59.1
81
71.5
59.5
83
1
80-135/33
100-42-5
Styrene
ND
72.9
60.8
83
71.5
60.7
85
0
78-125/30
79-34-5
1,1,2,2-Tetrachloroethane
ND
72.9
62.8
86
71.5
62.3
87
1
71-126/30
127-18-4
Tetrachloroethylene
ND
72.9
58.8
81
71.5
58.8
82
0
79-130/31
108-88-3
Toluene
ND
72.9
58.9
81
71.5
57.9
81
2
76-124/30
120-82-1
1,2,4-Trichlorobenzene
ND
72.9
58.1
80
71.5
59.1
83
2
78-130/34
71-55-6
1, 1, 1-Trichloroethane
ND
72.9
55.2
76
71.5
56.8
79
3
70-129/27
79-00-5
1,1,2-Trichloroethane
ND
72.9
65.3
90
71.5
62.8
88
4
74-124/28
79-01-6
Trichloroethylene
ND
72.9
58.5
80
71.5
57.8
81
1
75-128/27
75-69-4
Trichlorofluoromethane
ND
72.9
55.0
75
71.5
59.5
83
8
73-145/31
95-63-6
1,2,4-Trimethylbenzene
ND
72.9
60.2
83
71.5
60.9
85
1
74-123/34
108-67-8
1,3,5-Trimethylbenzene
ND
72.9
59.1
81
71.5
58.7
82
1
73-122/33
75-01-4
Vinyl Chloride
ND
72.9
52.4
72*
71.5
52.4
73*
0
76-141/27
1330-20-7
Xylene (total)
ND
219
185
85
215
185
86
0
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA39257-4
Limits
1868-53-7
Dibromofluoromethane
105%
103%
97%
75-124%
17060-07-0
1,2-Dichloroethane-D4
101%
104%
102%
72-135%
2037-26-5
Toluene-D8
99%
99%
100%
75-126%
460-00-4
4-Bromofluorobenzene
98%
98%
99%
71-133%
* = Outside of Control Limits.
56 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA39303-lMS
Y32773.D
1
12/07/16
AD
n/a
n/a
VY1300
FA39303-1MSD
Y32774.D
1
12/07/16
AD
n/a
n/a
VY1300
FA39303-1
Y32767.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples:
FA39257-7
CAS No. Compound
FA39303-1 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
67-64-1
Acetone
ND
298
198
66
300
172
57*
14
61-152/27
71-43-2
Benzene
ND
59.7
60.1
101
59.9
57.5
96
4
76-126/26
75-27-4
Bromodichloromethane
ND
59.7
62.7
105
59.9
61.3
102
2
74-130/25
75-25-2
Bromoform
ND
59.7
58.7
98
59.9
58.6
98
0
76-127/26
78-93-3
2-Butanone (MEK)
ND
298
236
79
300
215
72*
9
75-137/25
104-51-8
n-Butylbenzene
ND
59.7
65.2
109
59.9
58.6
98
11
71-128/35
75-15-0
Carbon Disulfide
ND
59.7
67.2
113
59.9
54.2
90
21
72-122/29
56-23-5
Carbon Tetrachloride
ND
59.7
60.4
101
59.9
57.7
96
5
78-133/29
108-90-7
Chlorobenzene
ND
59.7
62.6
105
59.9
58.5
98
7
81-129/29
75-00-3
Chloroethane
ND
59.7
64.8
109
59.9
63.2
105
2
68-133/29
67-66-3
Chloroform
ND
59.7
63.2
106
59.9
57.5
96
9
72-123/26
110-82-7
Cyclohexane
ND
59.7
57.9
97
59.9
56.1
94
3
73-126/32
124-48-1
Dibromochloromethane
ND
59.7
62.2
104
59.9
62.5
104
0
76-127/27
96-12-8
1,2-Dibromo-3-chloropropane
ND
59.7
55.4
93
59.9
53.7
90
3
70-137/29
106-93-4
1,2-Dibromoethane
ND
59.7
62.9
105
59.9
58.8
98
7
77-126/26
75-71-8
Dichlorodifluoromethane
ND
59.7
58.7
98
59.9
62.9
105
7
68-168/29
95-50-1
1,2-Dichlorobenzene
ND
59.7
63.2
106
59.9
57.6
96
9
80-129/32
541-73-1
1,3-Dichlorobenzene
ND
59.7
64.5
108
59.9
59.8
100
8
81-129/33
106-46-7
1,4-Dichlorobenzene
ND
59.7
65.3
109
59.9
57.8
96
12
76-130/32
75-34-3
1, 1 -Dichloroethane
ND
59.7
64.9
109
59.9
60.2
100
8
73-125/27
107-06-2
1,2-Dichloroethane
ND
59.7
62.4
105
59.9
59.8
100
4
74-128/23
75-35-4
1, 1 -Dichloroethylene
ND
59.7
69.7
117
59.9
54.5
91
24
81-136/28
156-59-2
cis- 1, 2-Dichloroethylene
ND
59.7
61.2
103
59.9
55.4
92
10
74-126/26
156-60-5
trans- 1, 2-Dichloroethylene
ND
59.7
70.2
118
59.9
62.8
105
11
70-127/27
78-87-5
1,2-Dichloropropane
ND
59.7
61.5
103
59.9
59.6
99
3
74-125/25
10061-01-5 cis- 1, 3-Dichloropropene
ND
59.7
61.4
103
59.9
60.2
100
2
80-123/26
10061-02-6 trans- 1, 3-Dichloropropene
ND
59.7
66.0
111
59.9
63.3
106
4
75-131/28
100-41-4
Ethylbenzene
ND
59.7
62.0
104
59.9
58.5
98
6
77-123/31
591-78-6
2-Hexanone
ND
298
257
86
300
246
82
4
72-133/26
98-82-8
Isopropylbenzene
ND
59.7
63.0
106
59.9
59.4
99
6
80-136/32
79-20-9
Methyl Acetate
ND
298
370
124
300
369
123
0
67-137/30
74-83-9
Methyl Bromide
ND
59.7
60.3
101
59.9
58.5
98
3
65-139/31
74-87-3
Methyl Chloride
ND
59.7
54.9
92
59.9
52.4
87
5
71-144/27
108-87-2
Methylcyclohexane
ND
59.7
58.7
98
59.9
59.1
99
1
75-128/31
75-09-2
Methylene Chloride
ND
59.7
69.2
116
59.9
65.6
109
5
74-137/28
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
298
279
94
300
268
89
4
76-132/26
* = Outside of Control Limits.
57 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A39303-lMS
Y32773.D
1
12/07/16
AD
n/a
n/a
VY1300
'A39303-1MSD
Y32774.D
1
12/07/16
AD
n/a
n/a
VY1300
'A39303-1
Y32767.D
1
12/07/16
AD
n/a
n/a
VY1300
The QC reported here applies to the following samples: Method: SW846 8260B
FA39257-7
FA39303-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
59.7
61.9
104
59.9
58.5
98
6
77-120/24
91-20-3
Naphthalene
ND
59.7
56.2
94
59.9
50.8
85
10
79-129/33
103-65-1
n-Propylbenzene
ND
59.7
65.4
110
59.9
60.6
101
8
80-135/33
100-42-5
Styrene
ND
59.7
63.7
107
59.9
59.9
100
6
78-125/30
79-34-5
1,1,2,2-Tetrachloroethane
ND
59.7
59.6
100
59.9
56.6
94
5
71-126/30
127-18-4
Tetrachloroethylene
ND
59.7
59.4
100
59.9
57.2
95
4
79-130/31
108-88-3
Toluene
ND
59.7
61.2
103
59.9
57.8
96
6
76-124/30
120-82-1
1,2,4-Trichlorobenzene
ND
59.7
62.8
105
59.9
54.2
90
15
78-130/34
71-55-6
1, 1, 1-Trichloroethane
ND
59.7
59.2
99
59.9
56.0
93
6
70-129/27
79-00-5
1,1,2-Trichloroethane
ND
59.7
61.4
103
59.9
59.8
100
3
74-124/28
79-01-6
Trichloroethylene
34.5
59.7
80.9
78
59.9
77.4
72*
4
75-128/27
75-69-4
Trichlorofluoromethane
ND
59.7
72.0
121
59.9
64.8
108
11
73-145/31
95-63-6
1,2,4-Trimethylbenzene
ND
59.7
65.8
110
59.9
60.4
101
9
74-123/34
108-67-8
1,3,5-Trimethylbenzene
ND
59.7
63.9
107
59.9
58.9
98
8
73-122/33
75-01-4
Vinyl Chloride
ND
59.7
56.7
95
59.9
55.2
92
3
76-141/27
1330-20-7
Xylene (total)
ND
179
197
110
180
185
103
6
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA39303-1
Limits
1868-53-7
Dibromofluoromethane
102%
101%
101%
75-124%
17060-07-0
1,2-Dichloroethane-D4
103%
104%
110%
72-135%
2037-26-5
Toluene-D8
98%
101%
102%
75-126%
460-00-4
4-Bromofluorobenzene
101%
99%
107%
71-133%
* = Outside of Control Limits.
58 of 65
ACCUTEST
FA39257

SG$
ACCUTEST
Southeast
GUMS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
Section 6
0
59 of 65
ACCUTEST
FA39257

Method Blank Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62980-MB
L0689450.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples:
Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
170
25
ug/kg
95-57-8
2-Chlorophenol
ND
170
21
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
23
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
20
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
18
ug/kg
3&4-Methylphenol
ND
170
39
ug/kg
88-75-5
2-Nitrophenol
ND
170
21
ug/kg
100-02-7
4-Nitrophenol
ND
830
130
ug/kg
87-86-5
Pentachlorophenol
ND
830
130
ug/kg
108-95-2
Phenol
ND
170
20
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
20
ug/kg
83-32-9
Acenaphthene
ND
170
21
ug/kg
208-96-8
Acenaphthylene
ND
170
21
ug/kg
120-12-7
Anthracene
ND
170
24
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
19
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
18
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
21
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
23
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
19
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
106-47-8
4-Chloroaniline
ND
170
23
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
25
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
30
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
170
24
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
23
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
21
ug/kg
218-01-9
Chrysene
ND
170
22
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
18
ug/kg
132-64-9
Dibenzofuran
ND
170
21
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
18
ug/kg
84-66-2
Diethyl Phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl Phthalate
ND
170
33
ug/kg
60 of 65
ACCUTEST
FA39257

Method Blank Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P62980-MB
L0689450.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples: Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
CAS No. Compound
Result RL MDL Units Q
117-84-0
Di-n-octyl Phthalate
ND
170
33
ug/kg
84-74-2
Di-n-butyl Phthalate
ND
330
67
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
170
17
ug/kg
606-20-2
2,6-Dinitrotoluene
ND
170
21
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
20
ug/kg
86-73-7
Fluorene
ND
170
21
ug/kg
118-74-1
Hexachlorobenzene
ND
170
21
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
19
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
170
33
ug/kg
67-72-1
Hexachloroethane
ND
170
19
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
26
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
90-12-0
1-Methylnaphthalene
ND
170
26
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
19
ug/kg
91-20-3
Naphthalene
ND
170
25
ug/kg
98-95-3
Nitrobenzene
ND
170
22
ug/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
170
18
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
32
ug/kg
85-01-8
Phenanthrene
ND
170
20
ug/kg
129-00-0
Pyrene
ND
170
31
ug/kg
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
58%
40-102%
4165-62-2
Phenol-d5
62%
41-100%
118-79-6
2,4,6-Tribromophenol
94%
42-108%
4165-60-0
Nitrobenzene-d5
65%
40-105%
321-60-8
2-Fluorobiphenyl
71%
43-107%
1718-51-0
Terphenyl-d14
77%
45-119%
61 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 1 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62980-BS
L0689449.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples:
Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
65-85-0
Benzoic Acid
3330
3310
99
36-118
59-50-7
4-Chloro-3-methyl Phenol
1670
1330
80
52-108
95-57-8
2-Chlorophenol
1670
1240
74
48-104
120-83-2
2,4-Dichlorophenol
1670
1380
83
51-105
105-67-9
2,4-Dimethylphenol
1670
1070
64
43-96
51-28-5
2,4-Dinitrophenol
3330
2600
78
40-119
534-52-1
4,6-Dinitro-o-cresol
3330
2940
88
64-121
95-48-7
2-Methylphenol
1670
1100
66
46-107
3&4-Methylphenol
3330
1890
57
44-111
88-75-5
2-Nitrophenol
1670
1420
85
49-104
100-02-7
4-Nitrophenol
3330
2160
65
56-116
87-86-5
Pentachlorophenol
3330
3080
92
61-114
108-95-2
Phenol
1670
1040
62
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1450
87
56-109
83-32-9
Acenaphthene
1670
1140
68
56-109
208-96-8
Acenaphthylene
1670
1200
72
56-106
120-12-7
Anthracene
1670
1230
74
61-110
56-55-3
Benzo(a)anthracene
1670
1280
77
66-111
50-32-8
Benzo(a)pyrene
1670
1340
80
59-104
205-99-2
Benzo(b)fluoranthene
1670
1440
86
67-113
191-24-2
Benzo(g,h,i)perylene
1670
1300
78
67-113
207-08-9
Benzo(k)fluoranthene
1670
1220
73
67-114
101-55-3
4-Bromophenyl phenyl ether
1670
1440
86
62-110
85-68-7
Butyl benzyl phthalate
1670
1450
87
65-113
106-47-8
4-Chloroaniline
1670
1290
77
30-115
111-91-1
bis(2-Chloroethoxy)methane
1670
961
58
48-105
111-44-4
bis(2-Chloroethyl)ether
1670
1050
63
46-103
108-60-1
bis(2-Chloroisopropyl)ether
1670
1050
63
40-110
91-58-7
2-Chloronaphthalene
1670
1270
76
53-106
7005-72-3
4-Chlorophenyl phenyl ether
1670
1160
70
58-106
218-01-9
Chrysene
1670
1260
76
65-112
53-70-3
Dibenzo(a,h)anthracene
1670
1460
88
68-115
132-64-9
Dibenzofuran
1670
1250
75
57-108
91-94-1
3,3'-Dichlorobenzidine
1670
1380
83
36-114
84-66-2
Diethyl Phthalate
1670
1270
76
61-109
131-11-3
Dimethyl Phthalate
1670
1310
79
59-108
* = Outside of Control Limits.
62 of 65
ACCUTEST
FA39257

Blank Spike Summary Page 2 of 2
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P62980-BS
L0689449.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples: Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
117-84-0
Di-n-octyl Phthalate
1670
1420
85
64-119
84-74-2
Di-n-butyl Phthalate
1670
1380
83
63-108
121-14-2
2,4-Dinitrotoluene
1670
1380
83
59-109
606-20-2
2,6-Dinitrotoluene
1670
1300
78
61-107
117-81-7
bis(2-Ethylhexyl)phthalate
1670
1430
86
64-115
206-44-0
Fluoranthene
1670
1270
76
60-108
86-73-7
Fluorene
1670
1210
73
58-109
118-74-1
Hexachlorobenzene
1670
1360
82
59-111
87-68-3
Hexachlorobutadiene
1670
1250
75
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1580
95
49-110
67-72-1
Hexachloroethane
1670
1010
61
40-105
193-39-5
Indeno(1,2,3-cd)pyrene
1670
1530
92
66-116
78-59-1
Isophorone
1670
1160
70
42-89
90-12-0
1-Methylnaphthalene
1670
1220
73
49-106
91-57-6
2-Methylnaphthalene
1670
1270
76
47-106
91-20-3
Naphthalene
1670
1090
65
44-104
98-95-3
Nitrobenzene
1670
1060
64
43-108
621-64-7
N-Nitrosodi-n-propylamine
1670
985
59
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1390
83
62-110
85-01-8
Phenanthrene
1670
1230
74
63-111
129-00-0
Pyrene
1670
1490
89
65-115
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
62%
40-102%
4165-62-2
Phenol-d5
62%
41-100%
118-79-6
2,4,6-Tribromophenol
85%
42-108%
4165-60-0
Nitrobenzene-d5
60%
40-105%
321-60-8
2-Fluorobiphenyl
71%
43-107%
1718-51-0
Terphenyl-d14
74%
45-119%
* = Outside of Control Limits.
63 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62980-MS
L0689454.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
OP62980-MSD
L0689455.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
FA39257-1
L0689453.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples:
Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
FA39257-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
3970
3820
96
3990
4660
117
20
36-118/41
59-50-7
4-Chloro-3-methyl Phenol
ND
1990
1550
78
1990
1800
90
15
52-108/21
95-57-8
2-Chlorophenol
ND
1990
1470
74
1990
1610
81
9
48-104/26
120-83-2
2,4-Dichlorophenol
ND
1990
1630
82
1990
1810
91
10
51-105/27
105-67-9
2,4-Dimethylphenol
ND
1990
1330
67
1990
1470
74
10
43-96/23
51-28-5
2,4-Dinitrophenol
ND
3970
1810
46
3990
2130
53
16
40-119/32
534-52-1
4,6-Dinitro-o-cresol
ND
3970
2260
57*
3990
2620
66
15
64-121/29
95-48-7
2-Methylphenol
ND
1990
1330
67
1990
1500
75
12
46-107/24
3&4-Methylphenol
ND
3970
2200
55
3990
2610
65
17
44-111/24
88-75-5
2-Nitrophenol
ND
1990
1690
85
1990
1780
89
5
49-104/27
100-02-7
4-Nitrophenol
ND
3970
2400
60
3990
3040
76
24*
56-116/23
87-86-5
Pentachlorophenol
ND
3970
3420
86
3990
4260
107
22
61-114/23
108-95-2
Phenol
ND
1990
1190
60
1990
1330
67
11
45-110/24
88-06-2
2,4,6-Trichlorophenol
ND
1990
1640
83
1990
1950
98
17
56-109/25
83-32-9
Acenaphthene
ND
1990
1320
66
1990
1590
80
19
56-109/23
208-96-8
Acenaphthylene
ND
1990
1400
70
1990
1650
83
16
56-106/23
120-12-7
Anthracene
ND
1990
1440
72
1990
1770
89
21
61-110/21
56-55-3
Benzo(a)anthracene
ND
1990
1440
72
1990
1810
91
23
66-111/23
50-32-8
Benzo(a)pyrene
ND
1990
1470
74
1990
1890
95
25*
59-104/23
205-99-2
Benzo(b)fluoranthene
ND
1990
1510
76
1990
1930
97
24
67-113/24
191-24-2
Benzo(g, h, i)perylene
ND
1990
1450
73
1990
1930
97
28*
67-113/21
207-08-9
Benzo(k)fluoranthene
ND
1990
1420
71
1990
1740
87
20
67-114/22
101-55-3
4-Bromophenyl phenyl ether
ND
1990
1710
86
1990
2000
100
16
62-110/21
85-68-7
Butyl benzyl phthalate
ND
1990
1720
87
1990
2100
105
20
65-113/20
106-47-8
4-Chloroaniline
ND
1990
1460
73
1990
1890
95
26
30-115/30
111-91-1
bis(2-Chloroethoxy)methane
ND
1990
1170
59
1990
1270
64
8
48-105/24
111-44-4
bis(2-Chloroethyl)ether
ND
1990
1270
64
1990
1330
67
5
46-103/27
108-60-1
bis(2-Chloroisopropyl)ether
ND
1990
1200
60
1990
1300
65
8
40-110/25
91-58-7
2-Chloronaphthalene
ND
1990
1380
69
1990
1600
80
15
53-106/23
7005-72-3
4-Chlorophenyl phenyl ether
ND
1990
1350
68
1990
1630
82
19
58-106/21
218-01-9
Chrysene
ND
1990
1450
73
1990
1800
90
22
65-112/25
53-70-3
Dibenzo(a,h)anthracene
ND
1990
1570
79
1990
2000
100
24*
68-115/23
132-64-9
Dibenzofuran
ND
1990
1450
73
1990
1820
91
23*
57-108/22
91-94-1
3,3'-Dichlorobenzidine
ND
1990
1700
86
1990
2180
109
25
36-114/28
84-66-2
Diethyl Phthalate
ND
1990
1450
73
1990
1810
91
22*
61-109/20
131-11-3
Dimethyl Phthalate
ND
1990
1530
77
1990
1860
93
19
59-108/20
* = Outside of Control Limits.
64 of 65
ACCUTEST
FA39257

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA39257
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3511 & ML King Jr Blvd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62980-MS
L0689454.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
OP62980-MSD
L0689455.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
FA39257-1
L0689453.13
1
12/07/16
MV
12/07/16
OP62980
SL3935
The QC reported here applies to the following samples:
Method: SW846 8270D
FA39257-1, FA39257-2, FA39257-3, FA39257-4, FA39257-5, FA39257-6, FA39257-7, FA39257-8, FA39257-9
FA39257-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
117-84-0
Di-n-octyl Phthalate
ND
1990
1670
84
1990
2030
102
19
64-119/21
84-74-2
Di-n-butyl Phthalate
ND
1990
1520
77
1990
1950
98
25*
63-108/19
121-14-2
2,4-Dinitrotoluene
ND
1990
1570
79
1990
1960
98
22*
59-109/20
606-20-2
2,6-Dinitrotoluene
ND
1990
1470
74
1990
1780
89
19
61-107/22
117-81-7
bis(2-Ethylhexyl)phthalate
ND
1990
1680
85
1990
2030
102
19
64-115/23
206-44-0
Fluoranthene
ND
1990
1260
63
1990
1670
84
28*
60-108/25
86-73-7
Fluorene
ND
1990
1410
71
1990
1700
85
19
58-109/21
118-74-1
Hexachlorobenzene
ND
1990
1620
82
1990
1960
98
19
59-111/21
87-68-3
Hexachlorobutadiene
ND
1990
1470
74
1990
1500
75
2
41-108/27
77-47-4
Hexachlorocyclopentadiene
ND
1990
1090
55
1990
1000
50
9
49-110/31
67-72-1
Hexachloroethane
ND
1990
1110
56
1990
1170
59
5
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
ND
1990
1620
82
1990
2070
104
24*
66-116/22
78-59-1
Isophorone
ND
1990
1420
71
1990
1570
79
10
42-89/22
90-12-0
1-Methylnaphthalene
ND
1990
1440
72
1990
1560
78
8
49-106/26
91-57-6
2-Methylnaphthalene
ND
1990
1510
76
1990
1840
92
20
47-106/27
91-20-3
Naphthalene
ND
1990
1320
66
1990
1410
71
7
44-104/27
98-95-3
Nitrobenzene
ND
1990
1300
65
1990
1380
69
6
43-108/25
621-64-7
N-Nitrosodi-n-propylamine
ND
1990
1100
55
1990
1260
63
14
48-108/27
86-30-6
N-Nitrosodiphenylamine
ND
1990
1710
86
1990
2020
101
17
62-110/21
85-01-8
Phenanthrene
ND
1990
1410
71
1990
1770
89
23*
63-111/22
129-00-0
Pyrene
ND
1990
1680
85
1990
1980
99
16
65-115/25
CAS No.
Surrogate Recoveries
MS
MSD
FA39257-1
Limits
367-12-4
2-Fluorophenol
63%
77%
57%
40-102%
4165-62-2
Phenol-d5
61%
76%
61%
41-100%
118-79-6
2,4,6-Tribromophenol
87%
108%
97%
a
42-108%
4165-60-0
Nitrobenzene-d5
64%
74%
65%
40-105%
321-60-8
2-Fluorobiphenyl
69%
85%
73%
43-107%
1718-51-0
Terphenyl-d14
77%
93%
82%
45-119%
(a) Associated CCV outside control limits.
* = Outside of Control Limits.
65 of 65
ACCUTEST
FA39257

Appendix D
Laboratory Analytical Report — Ground Water

5MI
ACCUTEST
Southeast 1
SGS ACCUTEST IS PART OF SGS, THE WORLD'S LEADING INSPECTION,
VERIFICATION, TESTING AND CERTIFICATION COMPANY.
Technical Report for
GRI (Geological Resources Inc.)
South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
3841
SGS Accutest Job Number: FA39209
Sampling Date: 12/02/ 16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
.com;
com;
ATTN: Rae Brown
Total number of pages in report: 31
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
e-Hardcopy 2.0
Automated Report
sine. com
Norm Farmer
Technical Director
Client Service contact: Muna Mohammed 407-425-6700
com;
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FLO02), NY(12022), SC(96038001)
DoD ELAP(L-A-13 L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
-SGS
1 31
SGS Accutest is the sole authority for authorizing edits or modifications to this document. ACCUTEST
Unauthorized modification of this report is strictly prohibited. FA39209

Table of Contents
-I-
Section1: Sample Summary...................................................................................................
Section2: Summary of Hits....................................................................................................
Section3: Sample Results........................................................................................................
3.1: FA39209-1: MW-A.......................................................................................................
3.2: FA39209-2: MW-B.......................................................................................................
Section4: Misc. Forms............................................................................................................
4.1: Chain of Custody...........................................................................................................
Section 5: GUMS Volatiles - QC Data Summaries..............................................................
5.1: Method Blank Summary................................................................................................
5.2: Blank Spike Summary...................................................................................................
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section 6: GUMS Semi-volatiles - QC Data Summaries.....................................................
6.1: Method Blank Summary................................................................................................
6.2: Blank Spike Summary...................................................................................................
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Sections:
3
4
5
60
14
15
18
19
21
23
25
26
28
30
2of 31
ACCUTESTEST
FA39209

SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA39209
South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Project No: 3841
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA39209-1 12/02/16 10:18 JW 12/03/16 AQ Ground Water MW-A
FA39209-2 12/02/16 09:23 JW 12/03/16 AQ Ground Water MW-B
3of 31
ACCUTESTEST
FA39209

Summary of Hits Page i of I
Job Number: FA39209
Account: GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Collected: 12/02/ 16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA39209-1 MW-A
No hits reported in this sample.
FA39209-2 MW-B
1,2,4-Trimethylbenzene 0.29 J 1.0 0.20 ug/1 SW846 8260B
1-Methylnaphthalene 0.63 J 5.8 0.58 ug/1 SW846 8270D
2-Methylnaphthalene 0.82 J 5.8 0.65 ug/1 SW846 8270D
4of 31
ACCUTESTEST
FA39209

SG$
ACCUTEST
Southeast
Sample Results
Report of Analysis
i
,"ONE
Section 3
5of 31
ACCUTESTEST
FA39209

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: MW-A
Lab Sample ID: FA39209-1 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8260B Percent Solids: n/a
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0099319.D 1 12/05/16 KM n/a n/a VN4523
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.24
ug/1
75-25-2
Bromoform
ND
1.0
0.46
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
2.6
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.43
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.23
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.30
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.63
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.26
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.26
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
0.81
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.33
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.27
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.24
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.39
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.26
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.28
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.22
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.31
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.33
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.34
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.25
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.33
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6of 31
ACCUTESTEST
FA39209

SGS Accutest
Report of Analysis
'lient Sample ID: MW-A
,ab Sample ID: FA39209-1 Date Sampled: 12/02/16
Ratrix: AQ - Ground Water Date Received: 12/03/ 16
lthod: SW846 8260B Percent Solids: n/a
'roject: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.23
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.4
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.20
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.24
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.33
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.30
ug/1
108-88-3
Toluene
ND
1.0
0.20
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
2.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.20
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.37
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.27
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
1.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
1.0
0.20
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.31
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.56
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
97%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
79-125%
2037-26-5
Toluene-D8
98%
85-112%
460-00-4
4-Bromofluorobenzene
102%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
7of 31
ACCUTESTEST
FA39209

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: MW-A
Lab Sample ID: FA39209-1 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X050943.13 1 12/06/16 MV 12/05/16 OP62944 SX2179
Run #2
Initial Volume Final Volume
Run # 1 1020 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
49
9.8
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
4.9
0.73
ug/1
95-57-8
2-Chlorophenol
ND
4.9
0.63
ug/1
120-83-2
2,4-Dichlorophenol
ND
4.9
0.62
ug/1
105-67-9
2,4-Dimethylphenol
ND
4.9
0.68
ug/1
51-28-5
2,4-Dinitrophenol a
ND
25
4.9
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
9.8
2.0
ug/1
95-48-7
2-Methylphenol
ND
4.9
0.57
ug/1
3&4-Methylphenol
ND
4.9
1.0
ug/1
88-75-5
2-Nitrophenol
ND
4.9
0.61
ug/1
100-02-7
4-Nitrophenol
ND
25
4.9
ug/1
87-86-5
Pentachlorophenol
ND
25
4.9
ug/1
108-95-2
Phenol
ND
4.9
0.49
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
4.9
0.85
ug/1
83-32-9
Acenaphthene
ND
4.9
0.55
ug/1
208-96-8
Acenaphthylene
ND
4.9
0.56
ug/1
120-12-7
Anthracene
ND
4.9
0.60
ug/1
56-55-3
Benzo(a)anthracene
ND
4.9
0.49
ug/1
50-32-8
Benzo(a)pyrene
ND
4.9
0.49
ug/1
205-99-2
Benzo(b)fluoranthene
ND
4.9
0.53
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
4.9
0.49
ug/1
207-08-9
Benzo(k)fluoranthene
ND
4.9
0.62
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
4.9
0.49
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
4.9
0.98
ug/1
106-47-8
4-Chloroaniline
ND
4.9
0.70
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
4.9
0.66
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
4.9
0.68
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
4.9
0.67
ug/1
91-58-7
2-Chloronaphthalene
ND
4.9
0.49
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
4.9
0.57
ug/1
218-01-9
Chrysene
ND
4.9
0.52
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
4.9
0.74
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8of 31
ACCUTESTEST
FA39209

SGS Accutest
Report of Analysis
lient Sample ID: MW-A
gab Sample ID: FA39209-1 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
4.9
0.66
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
4.9
0.49
ug/1
84-66-2
Diethyl Phthalate
ND
4.9
0.98
ug/1
131-11-3
Dimethyl Phthalate
ND
4.9
0.98
ug/1
84-74-2
Di-n-butyl Phthalate
ND
4.9
0.98
ug/1
117-84-0
Di-n-octyl Phthalate
ND
4.9
0.98
ug/1
121-14-2
2,4-Dinitrotoluene
ND
4.9
0.62
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
4.9
0.57
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
4.9
0.98
ug/1
206-44-0
Fluoranthene
ND
4.9
0.49
ug/1
86-73-7
Fluorene
ND
4.9
0.64
ug/1
118-74-1
Hexachlorobenzene
ND
4.9
0.54
ug/1
87-68-3
Hexachlorobutadiene
ND
4.9
0.50
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
4.9
0.98
ug/1
67-72-1
Hexachloroethane
ND
4.9
0.50
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
4.9
0.49
ug/1
78-59-1
Isophorone
ND
4.9
0.66
ug/1
90-12-0
1-Methylnaphthalene
ND
4.9
0.49
ug/1
91-57-6
2-Methylnaphthalene
ND
4.9
0.55
ug/1
91-20-3
Naphthalene
ND
4.9
0.49
ug/1
98-95-3
Nitrobenzene
ND
4.9
0.64
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
4.9
0.57
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
4.9
0.68
ug/1
85-01-8
Phenanthrene
ND
4.9
0.58
ug/1
129-00-0
Pyrene
ND
4.9
0.54
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
35%
14-67%
4165-62-2
Phenol-d5
22%
10-50%
118-79-6
2,4,6-Tribromophenol
75%
33-118%
4165-60-0
Nitrobenzene-d5
72%
42-108%
321-60-8
2-Fluorobiphenyl
71%
40-106%
1718-51-0
Terphenyl-dl4
70%
39-121%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9of 31
ACCUTESTEST
FA39209

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: MW-B
Lab Sample ID: FA39209-2 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8260B Percent Solids: n/a
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 N0099320.1) 1 12/05/16 KM n/a n/a VN4523
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.24
ug/1
75-25-2
Bromoform
ND
1.0
0.46
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
2.6
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.43
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.23
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.30
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.63
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.26
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.26
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
0.81
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.33
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.27
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.24
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.39
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.26
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.28
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.22
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.31
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.33
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.34
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.25
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.33
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
ACCUTESUTEST
FA39209

SGS Accutest
Report of Analysis
'lient Sample ID: MW-B
,ab Sample ID: FA39209-2 Date Sampled: 12/02/16
Ratrix: AQ - Ground Water Date Received: 12/03/ 16
lthod: SW846 8260B Percent Solids: n/a
'roject: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.23
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.4
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.20
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.24
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.33
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.30
ug/1
108-88-3
Toluene
ND
1.0
0.20
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
2.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.20
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.37
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.27
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
0.29
1.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
1.0
0.20
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.31
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.56
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
95%
83-118%
17060-07-0
1,2-Dichloroethane-D4
99%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
103%
83-118%
J
Page 2 of 2 N
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
11 of 31
ACCUTEST
FA39209

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID: MW-B
Lab Sample ID: FA39209-2 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X050944.13 1 12/06/16 MV 12/05/16 OP62944 SX2179
Run #2
Initial Volume Final Volume
Run #1 860 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
58
12
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.8
0.86
ug/1
95-57-8
2-Chlorophenol
ND
5.8
0.74
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.8
0.73
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.8
0.81
ug/1
51-28-5
2,4-Dinitrophenol a
ND
29
5.8
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
12
2.3
ug/1
95-48-7
2-Methylphenol
ND
5.8
0.67
ug/1
3&4-Methylphenol
ND
5.8
1.2
ug/1
88-75-5
2-Nitrophenol
ND
5.8
0.72
ug/1
100-02-7
4-Nitrophenol
ND
29
5.8
ug/1
87-86-5
Pentachlorophenol
ND
29
5.8
ug/1
108-95-2
Phenol
ND
5.8
0.58
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.8
1.0
ug/1
83-32-9
Acenaphthene
ND
5.8
0.65
ug/1
208-96-8
Acenaphthylene
ND
5.8
0.67
ug/1
120-12-7
Anthracene
ND
5.8
0.71
ug/1
56-55-3
Benzo(a)anthracene
ND
5.8
0.58
ug/1
50-32-8
Benzo(a)pyrene
ND
5.8
0.58
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.8
0.63
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.8
0.58
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.8
0.73
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.8
0.58
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.8
1.2
ug/1
106-47-8
4-Chloroaniline
ND
5.8
0.83
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.8
0.79
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.8
0.81
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.8
0.80
ug/1
91-58-7
2-Chloronaphthalene
ND
5.8
0.58
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.8
0.67
ug/1
218-01-9
Chrysene
ND
5.8
0.61
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.8
0.88
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 12 of 31
ACCUTEST
FA39209

SGS Accutest
Report of Analysis
lient Sample ID: MW-B
gab Sample ID: FA39209-2 Date Sampled: 12/02/16
Matrix: AQ - Ground Water Date Received: 12/03/ 16
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.8
0.78
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.8
0.58
ug/1
84-66-2
Diethyl Phthalate
ND
5.8
1.2
ug/1
131-11-3
Dimethyl Phthalate
ND
5.8
1.2
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.8
1.2
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.8
1.2
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.8
0.73
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.8
0.68
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.8
1.2
ug/1
206-44-0
Fluoranthene
ND
5.8
0.58
ug/1
86-73-7
Fluorene
ND
5.8
0.76
ug/1
118-74-1
Hexachlorobenzene
ND
5.8
0.63
ug/1
87-68-3
Hexachlorobutadiene
ND
5.8
0.60
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.8
1.2
ug/1
67-72-1
Hexachloroethane
ND
5.8
0.59
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.8
0.58
ug/1
78-59-1
Isophorone
ND
5.8
0.78
ug/1
90-12-0
1-Methylnaphthalene
0.63
5.8
0.58
ug/1 J
91-57-6
2-Methylnaphthalene
0.82
5.8
0.65
ug/1 J
91-20-3
Naphthalene
ND
5.8
0.58
ug/1
98-95-3
Nitrobenzene
ND
5.8
0.76
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.8
0.68
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.8
0.81
ug/1
85-01-8
Phenanthrene
ND
5.8
0.69
ug/1
129-00-0
Pyrene
ND
5.8
0.64
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
34%
14-67%
4165-62-2
Phenol-d5
22%
10-50%
118-79-6
2,4,6-Tribromophenol
69%
33-118%
4165-60-0
Nitrobenzene-d5
64%
42-108%
321-60-8
2-Fluorobiphenyl
65%
40-106%
1718-51-0
Terphenyl-dl4
68%
39-121%
(a) Associated CCV outside control limits.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
ACCUTESUTEST
FA39209

SGSi
ACCUTEST
Southeast
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
i
Section 4
of 31
ACCUTEST
FA39209

S
SGS Accutest Southeast r" 3yaoy1
SGACCUTEST Chain of Custody SGS ACCUTEST JOB #: PAGE OF- LA
I TFT-.407-42s-0i00 FAX: [phone]
www.u��N.ar.ro�n
SGS Accutest Quote #
SKIFF #
Client/Reporting Information ffM
_
Project Information
"Q",;
Analytical Information_
`
Matrix Codes
Company Name:
G. i I'r
Project Name:
S 6/1✓M
(
°w
U
.ea
-•l
DW - UnnkIng
Water
GW -Ground
Water
WW - Water
SW • Surface
Water
SO - Soil
SL- Sludge
Ot - Oil
LIQ - Other
Liquid
-
AIR Air
Address:
Street
4 q -P 3 7e I r -i- 1` �,
City: State: Zip:
a ' Al C G
I a
V� l e
Project Contact: Email:
Project#
q i
Phone #:
�� J43 - /
Fax #
Sampler(s) Name(a ?-eq'g t t/; I 1 ..;i j e1
Sam ler 1: m ler 2:
Client Purchase Order If
1
SGS
Accutest
Sample #
Field ID / Point of Collection
CO -ON
CONTAINER
INFORMATION
DATE
W-x
Torussnux,co or
nprrleg
-
o d
s
LAB USE ONLY
/ a
lo;
sR w
1,
q
)(
x
Turnaround Time (Business da s
10 Day (Business) Approved By: / Date:
7 Day
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3 Day RUSH
2 Day RUSH _
t Day RUSH _
Other
Rush T/A Data Available VIA Email or Lablink
pate Deliverable Information
COMMERCIAL "A° (RESULTS ONLY)
COMMERCIAL"B" (RESU F 1 T
OREDT7 1EJP LJE}yiEL 3) � � _'(� �!
❑ FULLTt (E�'IEtlE�C� QU - V C.T / `�' '
QEDD'S CLi NC 28203 -
Comments / Remarks
Sam
le Custod must be documented
below each time Sam
le$ Change possession, Including
courier delivery.
'
Relinquis d b mpler/Affiliation
Deta Time:
Received By/Affillation
Relinquished By/Affiliation
Date Time:
Rece�ijv�d By/Affillatlon
elinquis ed by/Affiliation
5
Date Time:
Received By/Affiliation
8
Relinquished By/Affiliation
7
Date Time:
Received By/Affiliation
8
Lab Use Ool : Cooler Temperature (s) Celsius:_.
FA39209: Chain of Custody
Page 1 of 3
ACCUTEST
FA39209

SGS ACCUTE:ST - ORLANDO SAMPLE RECEIPT CONF[RMAT[ON
SGS ACCUT'EST'S JOB NUMBER: -- �b3Cj CLIENT:G7Cf-1 12-06--- 2-5 1'-� . PROJECT: 3&Lfi _
DATF,/TIMERFCEIVED: 1a-3-1h_ _�S_ (MM/DD/YY 24:00) NUMBER OF COOLERS REC'EIVED:--1
METHOD OF DELIVERY: FF.DF.X UPS ACCUTESTCOURIER DELIVERY OTHER:
AIRBILL NUMBERS: �� I 1 Sil�lLl
COOLER INFORMATION
CUSTODY SEAL NOT PRESENT OR NOT INTACT
CHAIN OF CUSTODY NOT RECEIVED (COC)
ANALYSIS REQUESTED IS UNCLEAR OR MISSING
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
TEMPER.ATi.iRF,; CRITERIA NOT MET
TRIP BLANK INFORMATION
TRIP BLANK PROVIDED
TRIP BLANK NOT PROVIDED
TRIP BLANK NOT ON COC
TRIP BLANK INTACT
TRIP BLANK NOT INTACT
RECEIVED WATER TRIP BLANK
rl RECEIVEDSOIL TRIP BLANK .
MISC. INFORMATION
NUMBER OF ENCORES? 25-GRAM S-GRAM
NUMBER OF 5035 FIELD KITS!
NUMBER OF LAB FILTERED MET'ALS'.
TEMPERATURE INFORMATION
IR THERM �1CORR. FACTOR -0.4
OBSERVED TEMPS:
CORRECTED TEMPS:(USED FOR LIMS)
SAMPLE INF'ORMATION
INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
INSUFFICIENT' VOLUME FOR ANALYSIS
DATES/TIMES ON COC DO NOT MATCH SAMPLE LABEL
ID'S ON COC DO NOT MATCH LABEL
VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED
UNCLEAR FILTERING OR COMPOSITING INSTRUCTIONS
SAMPLE CONTAINER(S) RECEIVED BROKEN
5035 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
BULK VOA SOIL IARS NOT RECEIVED WITHIN 48 HOURS
'% SOLIDS.IAR NOT RECEIVED
RESIDUAL CHLORINE PRESENT LOT-#
APPLIC kBLE rO EFA 600 SERIES OR NOR 111 CAROLlNA ORGANICS;
TEST STRIP LO T Ns pH 0-3- 230315 p H 10-12 2198F3A OTHER (Specif;r) ..-
M1LMAPYCl- ,.. d one �,ow r"L ct er -p�G "._....------
TECHNICIAN SIGNATURE/DATE 1�'3' REVIEWERSIGNATURElDATF..�-�"'��
NF 02/16
receipt confirmation 020116.xls
FA39209: Chain of Custody
Page 2 of 3
A
L
0
ACCUTESUTEST
FA39209

FA39209: Chain of Custody
Page 3 of 3
ACCUTESUTEST
FA39209

SG$
ACCUTEST
Southeast
GUMS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
0
Section 5
of 31
ACCUTEST
FA39209

Method Blank Summary Page 1 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VN4523-MB
N0099305.1)
1
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples: Method: SW846 8260B
FA39209-1, FA39209-2
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.24
ug/l
75-25-2
Bromoform
ND
1.0
0.46
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
2.6
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.43
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.23
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.30
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.63
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.26
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.26
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
0.81
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.33
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.27
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.24
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.39
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.26
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.28
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.22
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.31
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.33
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.34
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.25
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.33
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.23
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.4
ug/l
99of31
ACCUTEST
FA39209

Method Blank Summary Page 2 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VN4523-MB
N0099305.1)
1
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples: Method: SW846 8260B
FA39209-1, FA39209-2
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.20
ug/l
91-20-3
Naphthalene
1.6
5.0
1.0
ug/l J
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/l
100-42-5
Styrene
ND
1.0
0.24
ug/l
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.33
ug/l
127-18-4
Tetrachloroethylene
ND
1.0
0.30
ug/1
108-88-3
Toluene
ND
1.0
0.20
ug/1
120-82-1
1,2,4-Trichlorobenzene
0.94
2.0
0.50
ug/1 J
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.20
ug/l
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.37
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.27
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
1.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
1.0
0.20
ug/l
75-01-4
Vinyl Chloride
ND
1.0
0.31
ug/l
1330-20-7
Xylene (total)
ND
3.0
0.56
ug/l
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
96%
83-118%
17060-07-0
1,2-Dichloroethane-D4
99%
79-125%
2037-26-5
Toluene-D8
100%
85-112%
460-00-4
4-Bromofluorobenzene
102%
83-118%
6 20 of 31
ACCUTEST
FA39209

Blank Spike Summary Page 1 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VN4523-BS
N0099304.D
1
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples: Method: SW846 8260B
FA39209-1, FA39209-2
CAS No. Compound
Spike BSP BSP
ug/l ug/l % Limits
67-64-1
Acetone
125
161
129
50-147
71-43-2
Benzene
25
24.9
100
81-122
75-27-4
Bromodichloromethane
25
25.1
100
79-123
75-25-2
Bromoform
25
21.8
87
66-123
78-93-3
2-Butanone (MEK)
125
142
114
56-143
104-51-8
n-Butylbenzene
25
26.7
107
79-126
75-15-0
Carbon Disulfide
25
25.0
100
66-148
56-23-5
Carbon Tetrachloride
25
25.4
102
76-136
108-90-7
Chlorobenzene
25
25.2
101
82-124
75-00-3
Chloroethane
25
23.5
94
62-144
67-66-3
Chloroform
25
25.5
102
80-124
110-82-7
Cyclohexane
25
25.1
100
73-138
124-48-1
Dibromochloromethane
25
25.2
101
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
20.5
82
64-123
106-93-4
1,2-Dibromoethane
25
26.0
104
75-120
75-71-8
Dichlorodifluoromethane
25
24.8
99
42-167
95-50-1
1,2-Dichlorobenzene
25
25.6
102
82-124
541-73-1
1,3-Dichlorobenzene
25
25.7
103
84-125
106-46-7
1,4-Dichlorobenzene
25
26.4
106
78-120
75-34-3
1, 1 -Dichloroethane
25
25.7
103
81-122
107-06-2
1,2-Dichloroethane
25
25.5
102
75-125
75-35-4
1, 1 -Dichloroethylene
25
26.1
104
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
24.3
97
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
27.6
110
76-127
78-87-5
1,2-Dichloropropane
25
24.6
98
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
26.3
105
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
29.0
116
80-120
100-41-4
Ethylbenzene
25
25.5
102
81-121
591-78-6
2-Hexanone
125
130
104
61-129
98-82-8
Isopropylbenzene
25
26.8
107
83-132
79-20-9
Methyl Acetate
125
130
104
65-126
74-83-9
Methyl Bromide
25
26.7
107
59-143
74-87-3
Methyl Chloride
25
22.6
90
50-159
108-87-2
Methylcyclohexane
25
26.3
105
76-129
75-09-2
Methylene Chloride
25
25.9
104
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
120
96
66-122
* = Outside of Control Limits.
6 21 of 31
ACCUTEST
FA39209

Blank Spike Summary Page 2 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VN4523-BS
N0099304.D
1
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples:
FA39209-1, FA39209-2
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
1634-04-4
Methyl Tert Butyl Ether
25
23.4
94
72-117
91-20-3
Naphthalene
25
30.0
120
63-132
103-65-1
n-Propylbenzene
25
27.0
108
82-133
100-42-5
Styrene
25
26.9
108
78-119
79-34-5
1,1,2,2-Tetrachloroethane
25
24.4
98
72-120
127-18-4
Tetrachloroethylene
25
26.4
106
76-135
108-88-3
Toluene
25
27.4
110
80-120
120-82-1
1,2,4-Trichlorobenzene
25
25.7
103
73-129
71-55-6
1, 1, 1-Trichloroethane
25
24.1
96
75-130
79-00-5
1,1,2-Trichloroethane
25
25.5
102
76-119
79-01-6
Trichloroethylene
25
25.9
104
81-126
75-69-4
Trichlorofluoromethane
25
24.0
96
71-156
95-63-6
1,2,4-Trimethylbenzene
25
26.3
105
79-120
108-67-8
1,3,5-Trimethylbenzene
25
26.1
104
79-120
75-01-4
Vinyl Chloride
25
24.1
96
69-159
1330-20-7
Xylene (total)
75
78.8
105
80-126
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
99%
83-118%
17060-07-0
1,2-Dichloroethane-D4
96%
79-125%
2037-26-5
Toluene-D8
100%
85-112%
460-00-4
4-Bromofluorobenzene
100%
83-118%
* = Outside of Control Limits.
Method: SW846 8260B
6 22 of 31
ACCUTEST
FA39209

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA39177-lMS
N0099321.13
20
12/05/16
KM
n/a
n/a
VN4523
FA39177-1MSD
N0099322.13
20
12/05/16
KM
n/a
n/a
VN4523
FA39177-1
N0099318.D
20
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples:
FA39209-1, FA39209-2
CAS No. Compound
FA39177-1 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8260B
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
67-64-1
Acetone
ND
2500
2260
90
2500
2170
87
4
50-147/21
71-43-2
Benzene
ND
500
509
102
500
506
101
1
81-122/14
75-27-4
Bromodichloromethane
ND
500
510
102
500
506
101
1
79-123/19
75-25-2
Bromoform
ND
500
434
87
500
436
87
0
66-123/21
78-93-3
2-Butanone(MEK)
ND
2500
2530
101
2500
2400
96
5
56-143/18
104-51-8
n-Butylbenzene
ND
500
517
103
500
526
105
2
79-126/16
75-15-0
Carbon Disulfide
ND
500
462
92
500
486
97
5
66-148/23
56-23-5
Carbon Tetrachloride
ND
500
473
95
500
496
99
5
76-136/23
108-90-7
Chlorobenzene
ND
500
512
102
500
510
102
0
82-124/14
75-00-3
Chloroethane
ND
500
567
113
500
571
114
1
62-144/20
67-66-3
Chloroform
ND
500
528
106
500
521
104
1
80-124/15
110-82-7
Cyclohexane
ND
500
491
98
500
516
103
5
73-138/18
124-48-1
Dibromochloromethane
ND
500
509
102
500
507
101
0
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
ND
500
425
85
500
437
87
3
64-123/18
106-93-4
1,2-Dibromoethane
ND
500
542
108
500
532
106
2
75-120/13
75-71-8
Dichlorodifluoromethane
ND
500
520
104
500
540
108
4
42-167/19
95-50-1
1,2-Dichlorobenzene
ND
500
515
103
500
527
105
2
82-124/14
541-73-1
1,3-Dichlorobenzene
ND
500
512
102
500
519
104
1
84-125/14
106-46-7
1,4-Dichlorobenzene
ND
500
525
105
500
532
106
1
78-120/15
75-34-3
1, 1 -Dichloroethane
ND
500
534
107
500
528
106
1
81-122/15
107-06-2
1,2-Dichloroethane
ND
500
531
106
500
519
104
2
75-125/14
75-35-4
1, 1 -Dichloroethylene
ND
500
522
104
500
528
106
1
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
ND
500
502
100
500
492
98
2
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
ND
500
558
112
500
557
111
0
76-127/17
78-87-5
1,2-Dichloropropane
ND
500
513
103
500
502
100
2
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
ND
500
501
100
500
501
100
0
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
ND
500
563
113
500
565
113
0
80-120/22
100-41-4
Ethylbenzene
ND
500
514
103
500
518
104
1
81-121/14
591-78-6
2-Hexanone
ND
2500
2500
100
2500
2380
95
5
61-129/18
98-82-8
Isopropylbenzene
ND
500
535
107
500
548
110
2
83-132/15
79-20-9
Methyl Acetate
ND
2500
2740
110
2500
2610
104
5
65-126/18
74-83-9
Methyl Bromide
ND
500
645
129
500
646
129
0
59-143/19
74-87-3
Methyl Chloride
ND
500
503
101
500
508
102
1
50-159/19
108-87-2
Methylcyclohexane
ND
500
527
105
500
543
109
3
76-129/17
75-09-2
Methylene Chloride
43.2
J 500
534
98
500
530
97
1
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
2500
2470
99
2500
2370
95
4
66-122/16
* = Outside of Control Limits.
6 23 of 31
ACCUTEST
FA39209

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A39177-lMS
N0099321.13
20
12/05/16
KM
n/a
n/a
VN4523
'A39177-1MSD
N0099322.13
20
12/05/16
KM
n/a
n/a
VN4523
'A39177-1
N0099318.D
20
12/05/16
KM
n/a
n/a
VN4523
The QC reported here applies to the following samples: Method: SW846 8260B
FA39209-1, FA39209-2
FA39177-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
500
485
97
500
478
96
1
72-117/14
91-20-3
Naphthalene
ND
500
545
109
500
563
113
3
63-132/25
103-65-1
n-Propylbenzene
ND
500
537
107
500
543
109
1
82-133/15
100-42-5
Styrene
ND
500
540
108
500
544
109
1
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
ND
500
508
102
500
491
98
3
72-120/14
127-18-4
Tetrachloroethylene
ND
500
522
104
500
536
107
3
76-135/16
108-88-3
Toluene
ND
500
554
111
500
558
112
1
80-120/14
120-82-1
1,2,4-Trichlorobenzene
ND
500
480
96
500
489
98
2
73-129/20
71-55-6
1, 1, 1-Trichloroethane
89.8
500
581
98
500
599
102
3
75-130/16
79-00-5
1,1,2-Trichloroethane
ND
500
533
107
500
525
105
2
76-119/14
79-01-6
Trichloroethylene
2000 E
500
2490
98
500
2510
102
1
81-126/15
75-69-4
Trichlorofluoromethane
ND
500
533
107
500
541
108
1
71-156/21
95-63-6
1,2,4-Trimethylbenzene
ND
500
526
105
500
527
105
0
79-120/18
108-67-8
1,3,5-Trimethylbenzene
ND
500
517
103
500
523
105
1
79-120/19
75-01-4
Vinyl Chloride
ND
500
520
104
500
539
108
4
69-159/18
1330-20-7
Xylene (total)
ND
1500
1580
105
1500
1610
107
2
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA39177-1
Limits
1868-53-7
Dibromofluoromethane
101%
100%
96%
83-118%
17060-07-0
1,2-Dichloroethane-D4
98%
97%
100%
79-125%
2037-26-5
Toluene-D8
99%
99%
99%
85-112%
460-00-4
4-Bromofluorobenzene
100%
100%
102%
83-118%
* = Outside of Control Limits.
6 24 of 31
ACCUTEST
FA39209

SG$
ACCUTEST
Southeast
GUMS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
Section 6
0
25 of 31
ACCUTEST
FA39209

Method Blank Summary Page 1 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
DP62944-MB
X050939.1)
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples: Method: SW846 8270D
FA39209-1, FA39209-2
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
50
10
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
5.0
0.74
ug/l
95-57-8
2-Chlorophenol
ND
5.0
0.64
ug/l
120-83-2
2,4-Dichlorophenol
ND
5.0
0.63
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.0
0.70
ug/l
51-28-5
2,4-Dinitrophenol
ND
25
5.0
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
10
2.0
ug/1
95-48-7
2-Methylphenol
ND
5.0
0.58
ug/1
3&4-Methylphenol
ND
5.0
1.1
ug/l
88-75-5
2-Nitrophenol
ND
5.0
0.62
ug/1
100-02-7
4-Nitrophenol
ND
25
5.0
ug/1
87-86-5
Pentachlorophenol
ND
25
5.0
ug/1
108-95-2
Phenol
ND
5.0
0.50
ug/1
88-06-2
2,4,6-Trichlorophenol
ND
5.0
0.86
ug/l
83-32-9
Acenaphthene
ND
5.0
0.56
ug/l
208-96-8
Acenaphthylene
ND
5.0
0.58
ug/l
120-12-7
Anthracene
ND
5.0
0.61
ug/l
56-55-3
Benzo(a)anthracene
ND
5.0
0.50
ug/l
50-32-8
Benzo(a)pyrene
ND
5.0
0.50
ug/l
205-99-2
Benzo(b)fluoranthene
ND
5.0
0.54
ug/l
191-24-2
Benzo(g,h,i)perylene
ND
5.0
0.50
ug/l
207-08-9
Benzo(k)fluoranthene
ND
5.0
0.63
ug/l
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.0
0.50
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.0
1.0
ug/1
106-47-8
4-Chloroaniline
ND
5.0
0.72
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.0
0.68
ug/l
111-44-4
bis(2-Chloroethyl)ether
ND
5.0
0.69
ug/l
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.0
0.69
ug/1
91-58-7
2-Chloronaphthalene
ND
5.0
0.50
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
5.0
0.58
ug/l
218-01-9
Chrysene
ND
5.0
0.53
ug/l
53-70-3
Dibenzo(a,h)anthracene
ND
5.0
0.76
ug/l
132-64-9
Dibenzofuran
ND
5.0
0.67
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
5.0
0.50
ug/l
84-66-2
Diethyl Phthalate
ND
5.0
1.0
ug/l
131-11-3
Dimethyl Phthalate
ND
5.0
1.0
ug/l
6 26 of 31
ACCUTEST
FA39209

Method Blank Summary Page 2 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62944-MB
X050939.1)
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples: Method: SW846 8270D
FA39209-1, FA39209-2
CAS No.
Compound
Result
RL
MDL
Units Q
84-74-2
Di-n-butyl Phthalate
ND
5.0
1.0
ug/l
117-84-0
Di-n-octyl Phthalate
ND
5.0
1.0
ug/l
121-14-2
2,4-Dinitrotoluene
ND
5.0
0.63
ug/l
606-20-2
2, 6-Dinitrotoluene
ND
5.0
0.58
ug/l
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.0
1.0
ug/l
206-44-0
Fluoranthene
ND
5.0
0.50
ug/1
86-73-7
Fluorene
ND
5.0
0.65
ug/1
118-74-1
Hexachlorobenzene
ND
5.0
0.55
ug/1
87-68-3
Hexachlorobutadiene
ND
5.0
0.51
ug/l
77-47-4
Hexachlorocyclopentadiene
ND
5.0
1.0
ug/1
67-72-1
Hexachloroethane
ND
5.0
0.51
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.0
0.50
ug/1
78-59-1
Isophorone
ND
5.0
0.67
ug/1
90-12-0
1-Methylnaphthalene
ND
5.0
0.50
ug/l
91-57-6
2-Methylnaphthalene
ND
5.0
0.56
ug/l
91-20-3
Naphthalene
ND
5.0
0.50
ug/l
98-95-3
Nitrobenzene
ND
5.0
0.66
ug/l
621-64-7
N-Nitrosodi-n-propylamine
ND
5.0
0.58
ug/l
86-30-6
N-Nitrosodiphenylamine
ND
5.0
0.70
ug/l
85-01-8
Phenanthrene
ND
5.0
0.60
ug/l
129-00-0
Pyrene
ND
5.0
0.55
ug/l
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
33%
14-67%
4165-62-2
Phenol-d5
20%
10-50%
118-79-6
2,4,6-Tribromophenol
69%
33-118%
4165-60-0
Nitrobenzene-d5
71%
42-108%
321-60-8
2-Fluorobiphenyl
67%
40-106%
1718-51-0
Terphenyl-d14
68%
39-121%
Cn
3
6 27 of 31
ACCUTEST
FA39209

Blank Spike Summary Page 1 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62944-BS
X050938.1)
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples:
FA39209-1, FA39209-2
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
65-85-0
Benzoic Acid
100
16.5
17
10-69
59-50-7
4-Chloro-3-methyl Phenol
50
34.0
68
54-103
95-57-8
2-Chlorophenol
50
28.9
58
52-98
120-83-2
2,4-Dichlorophenol
50
35.0
70
53-103
105-67-9
2,4-Dimethylphenol
50
28.6
57
43-90
51-28-5
2,4-Dinitrophenol
100
81.9
82
44-112
534-52-1
4,6-Dinitro-o-cresol
100
77.3
77
66-121
95-48-7
2-Methylphenol
50
25.0
50
43-90
3&4-Methylphenol
100
44.4
44
36-88
88-75-5
2-Nitrophenol
50
34.1
68
53-102
100-02-7
4-Nitrophenol
100
35.4
35
18-62
87-86-5
Pentachlorophenol
100
67.7
68
61-115
108-95-2
Phenol
50
13.0
26
19-56
88-06-2
2,4,6-Trichlorophenol
50
37.6
75
59-107
83-32-9
Acenaphthene
50
37.4
75
61-107
208-96-8
Acenaphthylene
50
38.8
78
60-104
120-12-7
Anthracene
50
35.6
71
65-108
56-55-3
Benzo(a)anthracene
50
38.1
76
66-111
50-32-8
Benzo(a)pyrene
50
38.7
77
62-107
205-99-2
Benzo(b)fluoranthene
50
37.3
75
65-114
191-24-2
Benzo(g,h,i)perylene
50
40.0
80
66-116
207-08-9
Benzo(k)fluoranthene
50
38.3
77
65-114
101-55-3
4-BromophenylPhenyl Ether
50
36.1
72
65-109
85-68-7
Butyl Benzyl Phthalate
50
42.3
85
65-112
106-47-8
4-Chloroaniline
50
34.4
69
49-105
111-91-1
bis(2-Chloroethoxy)methane
50
34.9
70
51-102
111-44-4
bis(2-Chloroethyl)ether
50
32.1
64
53-100
108-60-1
bis(2-Chloroisopropyl)ether
50
27.0
54
45-106
91-58-7
2-Chloronaphthalene
50
34.8
70
57-103
7005-72-3
4-ChlorophenylPhenyl Ether
50
39.7
79
62-105
218-01-9
Chrysene
50
40.4
81
66-111
53-70-3
Dibenzo(a,h)anthracene
50
39.6
79
66-119
132-64-9
Dibenzofuran
50
42.5
85
61-106
91-94-1
3,3'-Dichlorobenzidine
50
41.9
84
46-117
84-66-2
Diethyl Phthalate
50
39.8
80
64-108
131-11-3
Dimethyl Phthalate
50
37.8
76
63-106
* = Outside of Control Limits.
Method: SW846 8270D
6 28 of 31
ACCUTEST
FA39209

Blank Spike Summary Page 2 of 2
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62944-BS
X050938.1)
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples: Method: SW846 8270D
FA39209-1, FA39209-2
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
84-74-2
Di-n-butyl Phthalate
50
38.8
78
65-107
117-84-0
Di-n-octyl Phthalate
50
38.9
78
62-118
121-14-2
2,4-Dinitrotoluene
50
39.2
78
61-110
606-20-2
2,6-Dinitrotoluene
50
38.0
76
63-108
117-81-7
bis(2-Ethylhexyl)phthalate
50
42.6
85
61-117
206-44-0
Fluoranthene
50
37.0
74
63-106
86-73-7
Fluorene
50
37.4
75
62-108
118-74-1
Hexachlorobenzene
50
36.2
72
63-108
87-68-3
Hexachlorobutadiene
50
29.1
58
42-102
77-47-4
Hexachlorocyclopentadiene
50
33.8
68
39-102
67-72-1
Hexachloroethane
50
21.6
43
42-100
193-39-5
Indeno(1,2,3-cd)pyrene
50
37.6
75
64-119
78-59-1
Isophorone
50
35.0
70
43-87
90-12-0
1-Methylnaphthalene
50
33.3
67
53-102
91-57-6
2-Methylnaphthalene
50
34.4
69
51-102
91-20-3
Naphthalene
50
31.5
63
47-100
98-95-3
Nitrobenzene
50
36.9
74
50-104
621-64-7
N-Nitrosodi-n-propylamine
50
31.5
63
52-104
86-30-6
N-Nitrosodiphenylamine
50
37.0
74
64-108
85-01-8
Phenanthrene
50
36.1
72
66-110
129-00-0
Pyrene
50
41.4
83
64-113
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
38%
14-67%
4165-62-2
Phenol-d5
25%
10-50%
118-79-6
2,4,6-Tribromophenol
70%
33-118%
4165-60-0
Nitrobenzene-d5
66%
42-108%
321-60-8
2-Fluorobiphenyl
69%
40-106%
1718-51-0
Terphenyl-d14
69%
39-121%
* = Outside of Control Limits.
6 29 of 31
ACCUTEST
FA39209

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP62944-MS
X050941.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
OP62944-MSD
X050942.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
FA39141-1
X050940.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples:
FA39209-1, FA39209-2
CAS No. Compound
FA39141-1 Spike MS
ug/1 Q ug/l ug/l
Method: SW846 8270D
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
189
80.7
43
189
69.9
37
14
10-69/39
59-50-7
4-Chloro-3-methyl Phenol
ND
94.3
68.0
72
94.3
57.6
61
17
54-103/23
95-57-8
2-Chlorophenol
ND
94.3
52.6
56
94.3
48.2
51*
9
52-98/25
120-83-2
2,4-Dichlorophenol
ND
94.3
65.4
69
94.3
57.9
61
12
53-103/26
105-67-9
2,4-Dimethylphenol
ND
94.3
54.3
58
94.3
48.4
51
11
43-90/27
51-28-5
2,4-Dinitrophenol
ND
189
177
94
189
157
83
12
44-112/25
534-52-1
4,6-Dinitro-o-cresol
ND
189
155
82
189
134
71
15
66-121/23
95-48-7
2-Methylphenol
ND
94.3
48.9
52
94.3
42.7
45
14
43-90/28
3&4-Methylphenol
ND
189
91.1
48
189
82.2
44
10
36-88/28
88-75-5
2-Nitrophenol
ND
94.3
62.8
67
94.3
55.6
59
12
53-102/29
100-02-7
4-Nitrophenol
ND
189
100
53
189
89.3
47
11
18-62/33
87-86-5
Pentachlorophenol
ND
189
144
76
189
121
64
17
61-115/26
108-95-2
Phenol
ND
94.3
30.8
33
94.3
28.5
30
8
19-56/35
88-06-2
2,4,6-Trichlorophenol
ND
94.3
72.8
77
94.3
64.0
68
13
59-107/23
83-32-9
Acenaphthene
ND
94.3
71.7
76
94.3
62.4
66
14
61-107/22
208-96-8
Acenaphthylene
ND
94.3
75.1
80
94.3
64.8
69
15
60-104/22
120-12-7
Anthracene
ND
94.3
73.2
78
94.3
61.3
65
18
65-108/20
56-55-3
Benzo(a)anthracene
ND
94.3
75.8
80
94.3
66.4
70
13
66-111/22
50-32-8
Benzo(a)pyrene
ND
94.3
74.4
79
94.3
65.5
69
13
62-107/23
205-99-2
Benzo(b)fluoranthene
ND
94.3
71.9
76
94.3
66.6
71
8
65-114/23
191-24-2
Benzo(g, h, i)perylene
ND
94.3
80.8
86
94.3
71.9
76
12
66-116/23
207-08-9
Benzo(k)fluoranthene
ND
94.3
76.8
81
94.3
64.8
69
17
65-114/24
101-55-3
4-Bromophenyl Phenyl Ether
ND
94.3
73.5
78
94.3
62.5
66
16
65-109/23
85-68-7
Butyl Benzyl Phthalate
ND
94.3
84.7
90
94.3
73.1
77
15
65-112/24
106-47-8
4-Chloroaniline
ND
94.3
61.4
65
94.3
52.2
55
16
49-105/27
111-91-1
bis(2-Chloroethoxy)methane
ND
94.3
64.3
68
94.3
58.2
62
10
51-102/28
111-44-4
bis(2-Chloroethyl)ether
ND
94.3
56.3
60
94.3
52.8
56
6
53-100/27
108-60-1
bis(2-Chloroisopropyl)ether
ND
94.3
47.7
51
94.3
44.5
47
7
45-106/26
91-58-7
2-Chloronaphthalene
ND
94.3
67.1
71
94.3
60.9
65
10
57-103/23
7005-72-3
4-ChlorophenylPhenyl Ether
ND
94.3
74.8
79
94.3
65.3
69
14
62-105/20
218-01-9
Chrysene
ND
94.3
78.6
83
94.3
71.6
76
9
66-111/22
53-70-3
Dibenzo(a,h)anthracene
ND
94.3
79.3
84
94.3
70.0
74
12
66-119/24
132-64-9
Dibenzofuran
ND
94.3
84.3
89
94.3
72.2
77
15
61-106/21
91-94-1
3,3'-Dichlorobenzidine
ND
94.3
66.5
70
94.3
57.4
61
15
46-117/29
84-66-2
Diethyl Phthalate
ND
94.3
78.4
83
94.3
68.1
72
14
64-108/21
131-11-3
Dimethyl Phthalate
ND
94.3
74.4
79
94.3
64.8
69
14
63-106/22
* = Outside of Control Limits.
30 of 31
ACCUTEST
FA39209

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA39209
Account: GRINCC GRI (Geological Resources Inc.)
Project: South Glenburnie; 3704 & 3706 Trent Rd, New Burn, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P62944-MS
X050941.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
)P62944-MSD
X050942.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
;A39141-1
X050940.13
1
12/06/16
MV
12/05/16
OP62944
SX2179
The QC reported here applies to the following samples:
FA39209-1, FA39209-2
CAS No. Compound
FA39141-1 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8270D
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
84-74-2
Di-n-butyl Phthalate
ND
94.3
77.4
82
94.3
66.9
71
15
65-107/21
117-84-0
Di-n-octyl Phthalate
ND
94.3
76.2
81
94.3
67.7
72
12
62-118/24
121-14-2
2,4-Dinitrotoluene
ND
94.3
75.8
80
94.3
66.5
70
13
61-110/21
606-20-2
2,6-Dinitrotoluene
ND
94.3
75.5
80
94.3
64.8
69
15
63-108/21
117-81-7
bis(2-Ethylhexyl)phthalate
ND
94.3
86.4
92
94.3
75.9
80
13
61-117/23
206-44-0
Fluoranthene
ND
94.3
72.6
77
94.3
63.1
67
14
63-106/21
86-73-7
Fluorene
ND
94.3
72.9
77
94.3
64.4
68
12
62-108/20
118-74-1
Hexachlorobenzene
ND
94.3
70.6
75
94.3
61.5
65
14
63-108/22
87-68-3
Hexachlorobutadiene
ND
94.3
66.0
70
94.3
61.7
65
7
42-102/28
77-47-4
Hexachlorocyclopentadiene
ND
94.3
65.4
69
94.3
57.7
61
13
39-102/29
67-72-1
Hexachloroethane
ND
94.3
52.4
56
94.3
50.8
54
3
42-100/29
193-39-5
Indeno(1,2,3-cd)pyrene
ND
94.3
75.6
80
94.3
69.5
74
8
64-119/24
78-59-1
Isophorone
ND
94.3
64.5
68
94.3
57.9
61
11
43-87/25
90-12-0
1-Methylnaphthalene
ND
94.3
64.7
69
94.3
58.4
62
10
53-102/27
91-57-6
2-Methylnaphthalene
ND
94.3
66.6
71
94.3
60.4
64
10
51-102/26
91-20-3
Naphthalene
ND
94.3
61.1
65
94.3
56.5
60
8
47-100/29
98-95-3
Nitrobenzene
ND
94.3
66.8
71
94.3
61.1
65
9
50-104/28
621-64-7
N-Nitrosodi-n-propylamine
ND
94.3
55.5
59
94.3
50.7
54
9
52-104/25
86-30-6
N-Nitrosodiphenylamine
ND
94.3
74.3
79
94.3
62.2
66
18
64-108/23
85-01-8
Phenanthrene
ND
94.3
72.5
77
94.3
62.6
66
15
66-110/21
129-00-0
Pyrene
ND
94.3
80.1
85
94.3
69.7
74
14
64-113/23
CAS No.
Surrogate Recoveries
MS
MSD
FA39141-1
Limits
367-12-4
2-Fluorophenol
43%
39%
29%
14-67%
4165-62-2
Phenol-d5
32%
30%
19%
10-50%
118-79-6
2,4,6-Tribromophenol
74%
61%
69%
33-118%
4165-60-0
Nitrobenzene-d5
63%
59%
56%
42-108%
321-60-8
2-Fluorobiphenyl
70%
61%
60%
40-106%
1718-51-0
Terphenyl-d14
71%
62%
67%
39-121%
* = Outside of Control Limits.
31 of 31
ACCUTEST
FA39209