20061-Glenburnie Prj-Limited Phase II ESA 11.20.15 Final

Geological Resources, Inc.
November 20, 2015
Columbia Development
1845 St. Julian Place
Columbia, South Carolina 29204
Attn: Ms. Meredith Jewell
Re: Limited Phase II Environmental Site Assessment
2116 South Glenburnie Road
New Bern, North Carolina 28562
GRI Project No. 3841
Dear Ms. Jewell:
Attached for your review is the Limited Phase II Environmerr[al Site Assessment Report for the
above referenced property located in New Bern, North Carolina. We appreciate the opportunity
to provide these services to you. If you require additional information, please contact the
undersigned at [phone].
cc:
3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT
2116 SOUTH GLENBURNIE ROAD
NEW BERN, NORTH CAROLINA
CRAVEN COUNTY
GRI PROJECT NO.3841
Prepared For:
Columbia Development
1845 St. Julian Place
Columbia, South Carolina 29204
Prepared By:
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
November 20, 2015

Limited Phase II Environmental Site Assessment
2116 South Glenburnie Road
New Bern, North Carolina
GRI Job No. 3841
Table of Contents
Section
Page No.
1.0 Introduction and Background....................................................................................................1
2.0 Phase II Groundwater Sampling Activities...............................................................................2
2.1 Ground Water Sample Collection........................................................................................ 2
2.2 Groundwater Results............................................................................................................ 5
3.0 Phase II ESA Data Summary......................................................................................................8
4.0 Signatures of Environmental Professionals.............................................................................10
5.0 Qualifications of Environmental Professionals Conducting the Phase II ESA ................... I I
Tables
Table 1 Summary of Ground Water Sample Analytical Results
Figures
Figure 1 Site Location Map
Figure 2 Sampling Location Map #1
Figure 3 Sampling Location Map #2
Appendices
Appendix A Laboratory Analytical Reports
Appendix B Curriculum Vitae
Limited Phase II Environmental Site Assessment Page i
2116 South Glenburnie Road
New Bern, North Carolina

Limited Phase II Environmental Site Assessment
2116 South Glenburnie Road
New Bern, North Carolina
GRI Job No. 3841
1.0 Introduction and Background
Geological Resources, Inc. (GRI) has completed limited Phase II Environmental Site Assessment
(ESA) activities on eleven of 20 parcels in the vicinity of 2115 South Glenburnie Road in New
Bern, Craven County, North Carolina. The subject site totals approximately 34.60 acres of land.
Limited Phase II ESA assessments were performed on select parcels to investigate Recognized
Environmental Conditions (RECs) identified in a May 12, 2015 Phase I ESA and an August 28,
2015 Phase I ESA completed by ECS Carolinas, LLP. A site location map is included as Figure
1 and sampling location maps are included as Figure 2 and Figure 3. The results of the
assessment activities are presented below.
Limited Phase II Environmental Site Assessment Page 1
2116 South Glenburnie Road
New Bern, North Carolina

2.0 Phase II Groundwater Sampling Activities
On October 27 and 28, 2015 and November 9, 2015, GRI conducted limited Phase II ESA
groundwater sampling activities to assess ground water conditions at the following locations:
• Clarke Power Services (3511 Dr. Martin Luther King, Jr. [DMLKJ] Drive) — oil/water
separator (OWS), septic system, floor drains
• West Marine (3601 DMLKJ Drive) — floor drains
• Former Fulcher Tire Sales & Service (3605 DMLKJ Drive) — historic use as a tire sales
and service facility
• Badcock Furniture (2116 South Glenburnie Road) — due to off -site dry cleaner to east
• Residence (3608 Trent Road) — possible heating oil underground storage tank (UST)
• Residence (3612 Trent Road) — possible heating oil UST
• Residence (3700 Trent Road) — heating oil UST
• Residence (3702 Trent Road) — possible heating oil UST
• Residence (3704 Trent Road) — possible heating oil UST
• Residence (3706 Trent Road) — possible heating oil UST
• Residence (3708 Trent Road) — possible heating oil UST
Phase II ESA sampling locations are shown on Figure 2 and Figure 3.
2.1 Ground Water Sample Collection
GRI used direct -push technology to advance seventeen borings at the above -referenced sampling
locations and utilized discrete ground water sampling techniques to collect a ground water
sample from each boring. GRI contacted the public utility locator and used a private utility
locator to clear subsurface utilities. A description of sampling locations and laboratory analyses
are provided below.
Clarke Power Service
Discrete ground water samples were collected in the vicinity of the OWS (Clark OWS), floor
drains (Clark Floor Drains West and Clark Floor Drains East), the septic system (Clark Septic),
and the wash bay (Clark Wash Bay). The ground water samples were analyzed for volatile
organic compounds (VOCs) by EPA Method 8260B, polynuclear aromatic hydrocarbons (PAHs)
by 8270D, and 8 RCRA Metals by EPA Methods 6010C/7440A.
Limited Phase II Environmental Site Assessment Page 2
2116 South Glenburnie Road
New Bern, North Carolina

West Marine
Discrete ground water samples were collected in the vicinity of an unknown tank to the east of
the site structure (WM Unknown Tank) and to the south of the site structure (WM Rear). The
ground water samples were analyzed for VOCs, PAHs, and 8 RCRA Metals.
Former Fulcher Tire & Service
Discrete ground water samples were collected in the central location of the former facility
(Fulcher Center) and along the western boundary of the site and down gradient of the former
structure (Fulcher DG). The ground water samples were analyzed for VOCs, PAHs, and 8
RCRA Metals.
Badcock Furniture
A discrete ground water sample (Badcock) was collected to the east of the site structure near
South Glenburnie Road in an attempt to determine if the off -site dry cleaner to the east of
Badcock Furniture had impacted the subject site. The ground water sample was analyzed for
VOCs.
3608 Trent Road
A discrete ground water sample (3608 Trent) was collected in the vicinity of the heating oil
aboveground storage tank (AST) in an attempt to determine if the current AST or a current or
former heating oil UST had impacted ground water at the site. The ground water sample was
analyzed for VOCs and PAHs.
3612 Trent Road
A discrete ground water sample (3612 Trent) was collected to the northeast of the residence in an
attempt to determine if a current or former heating oil UST had impacted ground water at the
site. The ground water sample was analyzed for VOCs and PAHs.
Limited Phase II Environmental Site Assessment Page 3
2116 South Glenburnie Road
New Bern, North Carolina

3700 Trent Road
A discrete ground water sample (3700 Trent) was collected along the north side of the residence
in an attempt to determine if a current or former heating oil UST had impacted ground water at
the site. The ground water sample was analyzed for VOCs and PAHs.
3702 Trent Road
A discrete ground water sample (3702 Trent) was collected along the north side of the residence
in an attempt to determine if the existing heating oil UST had impacted ground water at the site.
The ground water sample was analyzed for VOCs and PAHs.
3704 Trent Road
A discrete ground water sample (3704 Trent) was collected along the north side of the residence
in an attempt to determine if a current or former heating oil UST had impacted ground water at
the site. The ground water sample was analyzed for VOCs and PAHs.
3706 Trent Road
A discrete ground water sample (3706) was collected along the north side of the residence in an
attempt to determine if a current or former heating oil UST had impacted ground water at the
site. The ground water sample was analyzed for VOCs and PAHs.
3708 Trent Road
A discrete ground water sample (3708) was collected on the north side of the residence in an
attempt to determine if a current or former heating oil UST had impacted ground water at the
site. The ground water sample was analyzed for VOCs and PAHs.
Background
A discrete ground water sample (Background) was collected in a field located to the east of an
access road located to the south of DMLKJ Drive and to the north of Trent Road. The ground
water sample was analyzed for 8 RCRA Metals.
Limited Phase II Environmental Site Assessment Page 4
2116 South Glenburnie Road
New Bern, North Carolina

Prior to sampling, water was purged from the discrete sampling points using polyethylene tubing
and a peristaltic pump. The groundwater samples were placed into laboratory supplied bottles
upon collection, properly labeled, placed in coolers with ice, and sent to Accutest Laboratories
located in Orlando, Florida under standard chain -of -custody protocol for laboratory analysis.
Laboratory analytical data sheets for groundwater samples and chain -of -custody documentation
for this site are provided in Appendix A. The analytical results are discussed below.
2.2 Groundwater Results
Clarke Power Service
One or more detectable or estimated VOCs and PAHs were reported in ground water samples
Clark OWS, Clark Floor Drains West, Clark Floor Drains East, Clark Septic, and Clark Wash
Bay. The concentration of tetrachloroethylene reported in ground water sample Clark Floor
Drain East exceeded the maximum allowable concentration (MAC) as specified in T15A NCAC
2L.0202. Based on the exceedance of the MAC, a release of tetrachloroethylene has occurred
and represents a REC at the site.
One or more concentrations of arsenic, barium, chromium, lead, and mercury were reported
above the MACs in ground water samples Clark OWS, Clark Floor Drains West, Clark Floor
Drains East, Clark Septic, and Clark Wash Bay. However, the reported concentrations are below
the concentrations reported in the background sample. Therefore, the detected metals reported in
ground water samples are assumed to be naturally occurring and not an REC.
West Marine
With the exception of an estimate concentration of carbon disulfide reported in ground water
sample WM Rear, there were no detections of VOCs or PAHs in the WM Unknown Tank or
WM Rear groundwater samples. Based on the lack of detected constituents, the unknown UST
does not represent a REC at this time.
One or more concentrations of arsenic, barium, chromium, lead, and mercury were reported
above the MACs in ground water samples WM Unknown Tank and WM Rear. However, the
Limited Phase II Environmental Site Assessment Page 5
2116 South Glenburnie Road
New Bern, North Carolina

reported concentrations are below the concentrations reported in the background sample.
Therefore, the detected metals reported in ground water samples are assumed to be naturally
occurring and not an REC.
Former Fulcher Tire & Service
Estimated concentrations of carbon disulfide were reported in ground water samples Fulcher
Center and Fulcher DG. In addition, tetrachloroethylene exceeded the MAC in ground water
sample Fulcher DG. Based on the exceedance of the MAC, a release of tetrachloroethylene has
occurred and represents a REC at the site.
One or more concentrations of arsenic, chromium, and lead were reported above the MACs in
ground water samples Fulcher Center and Fulcher DG. However, the reported concentrations are
below the concentrations reported in the background sample. Therefore, the detected metals
reported in ground water samples are assumed to be naturally occurring and not an REC.
Badcock Furniture
There were no detections of VOCs in the Badcock groundwater sample collected to the east of
the site structure near South Glenburnie Road. Therefore, it appears that the dry cleaner to the
east of Badcock Furniture does not represent a REC to the subject site at this time.
3608 Trent Road
There were no detections of VOCs or PAHs in the 3608 Trent groundwater sample. Therefore, it
appears that a release of heating oil has not occurred at the site.
3612 Trent Road
There were no detections of VOCs or PAHs in the 3612 Trent groundwater sample. Therefore, it
appears that a release of heating oil has not occurred at the site.
3700 Trent Road
There were no detections of VOCs or PAHs in the 3700 Trent groundwater sample. Therefore, it
appears that a release of heating oil has not occurred at the site.
Limited Phase II Environmental Site Assessment Page 6
2116 South Glenburnie Road
New Bern, North Carolina

3702 Trent Road
There were no detections of VOCs or PAHs in the 3702 Trent groundwater sample. Therefore, it
appears that a release of heating oil has not occurred from the existing UST. Based on the lack
of detected constituents, the heating oil UST does not represent a REC at this time.
3704 Trent Road
Detectable or estimated petroleum compounds were reported in ground water sample 3704 Trent.
The concentrations of naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded the
MACs. Based on the exceedance of the MACs, a release has occurred and represents a REC at
the site.
3706 Trent Road
Detectable or estimated petroleum compounds were reported in ground water sample 3706. The
concentrations of naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded the
MACs. Based on the exceedance of the MACs, a release has occurred and represents a REC at
the site.
3708 Trent Road
There were no detections of VOCs or PAHs in the 3708 groundwater sample collected at the site.
Therefore, it appears that a release of heating oil has not occurred.
Background
Concentrations of arsenic, barium, chromium, lead, and mercury were reported above the MACs
for the Background ground water sample. The exceedance of the MACs appears to indicate high
levels of naturally occurring metals in ground water in the area.
Results of the groundwater analyses are summarized on Table 1 and the sample locations are
depicted on Figure 2 and Figure 3.
Limited Phase II Environmental Site Assessment Page 7
2116 South Glenburnie Road
New Bern, North Carolina

3.0 Phase II ESA Data Summary
• The concentration of tetrachloroethylene reported in ground water sample Clark Floor
Drain East exceeded the MAC. Based on the exceedance of the MAC, a release of
tetrachloroethylene has occurred and represents a REC at the Clarke Power Service site.
• With the exception of an estimate concentration of carbon disulfide reported in ground
water sample WM Rear, there were no detections of VOCs or PAHs in the WM
Unknown Tank or WM Rear groundwater samples. Based on the lack of detected
constituents, the unknown UST at West Marine does not represent a REC at this time.
• The concentration of tetrachloroethylene reported in ground water sample Fulcher DG
exceeded the MAC. Based on the exceedance of the MAC, a release of
tetrachloroethylene has occurred and represents a REC at the former Fulcher Tire &
Service site.
• There were no detections of VOCs in the Badcock groundwater sample collected to the
east of the site structure near South Glenburnie Road. Therefore, it appears that the dry
cleaner to the east of Badcock Furniture does not represent a REC to the subject site at
this time.
• Based on the lack of detections of VOCs or PAHs in ground water samples from 3608
Trent Road, 3612 Trent Road, 3700 Trent Road, and 3708 Trent Road, it appears that a
release of heating oil has not occurred at these residences.
• There were no detections of VOCs or PAHs in the 3702 Trent groundwater sample.
Therefore, it appears that a release of heating oil has not occurred from the existing UST
located at the 3702 Trent Road residence. Based on the lack of detected constituents, the
heating oil UST does not represent a REC at this time.
Limited Phase II Environmental Site Assessment Page 8
2116 South Glenburnie Road
New Bern, North Carolina

• Concentrations of naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene reported
in ground water sample 3704 Trent exceeded the MACs. Based on the exceedance of the
MACs, a release has occurred and represents a REC at the 3704 Trent Road residence.
• Concentrations of naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene reported
in ground water sample 3706 exceeded the MACs. Based on the exceedance of the
MACs, a release has occurred and represents a REC at the 3706 Trent Road residence.
• The concentrations arsenic, barium, chromium, lead, and mercury reported in ground
water samples throughout the site are below the concentrations reported in the
background sample. Therefore, the detected metals reported in ground water samples are
assumed to be naturally occurring and not an REC.
Limited Phase II Environmental Site Assessment Page 9
2116 South Glenburnie Road
New Bern, North Carolina

I
4.0 Signatures of Environmental Professionals
that, to the best of my professional knowledge d belief, I meet the definition of
nental Professional as defined in Section 312.10 of 4 0 CFR 312, and have the specific
tions based on education, training, and experience W assess a property of the nature,
and setting of the subject Site. I have developed d performed the all appropriate
in conformance with the standards and practices set forth for the environmental
anal in 40 CFR Part 312.
Reviewed by:

5.0 Qualifications of Environmental Professionals Conducting the Phase II ESA
James Wellons, PG, Project Manager, has over 19 years of experience in environmental site
assessments, soil and ground water investigations, and nationwide emergency response facilitator
of chemical releases.
Randy Smith, PG, Project Manager, has over 22 years of experience in conducting
environmental site assessments, soil and ground water investigations and remediation across the
United States.
Curriculum vitae for each individual are included in Appendix B.
Limited Phase II Environmental Site Assessment Page 11
2116 South Glenburnie Road
New Bern, North Carolina

Tables

TABLE 1
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
2116 SOUTH GLENBURNIE ROAD
NEW BERN, NORTH CAROLINA
Date : 11/18/15
Analytical Method 4
EPA Method 8260B
EPA Method 8270D
EPA Method 601 OC/7470A
Contaminant of Concern
71
N
1
o
o
Date
o
�,
r.
Well ID
Collected
W
Z
(mm/dd/yy)
MAC ( /l)
1
600
600
500
20
0.7
6
1
30
10
700
2
10
15
1
20
20
GCL (µg/1)
5,000
260,000
84,500
85,500
20,000
700
6,000
1,000
12,500
NS
700,000
NS
10,000
15,000
NS
NS
20,000
Clark OWS
10/27/15
<0.20
<0.40
<0.20
0.61 J
<0.30
<0.33
<1.0
<0.60
<0.60
<100
<2,000
<50
963
380
1.2
<100
<100
Clark Floor
10/27/15
<0.20
0.57 J
<0.20
0.76 J
<0.30
<0.33
<1.0
<0.48
<0.48
113
<2,000
<50
621
203
0.58
<100
<100
Drains West
Clark Floor
10/27/15
<0.20
<0.40
0.49 J
2.3 J
<0.30
2.2
<1.0
<0.53
<0.53
25.5
664
<5.0
571
314
1.2
<10
<10
Drains East
Clark Septic
10/27/15
<0.20
0.76 J
0.22 J
1.0 J
<0.30
<0.33
<1.0
<0.61
<0.61
72.5
707
<10
833
321
0.97
<20
<20
Clark Wash
10/27/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.54
<0.55
41.9
456
<10
623
274
0.69
<20
<20
Bay
WM Unknown
10/27/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.63
<0.63
29.4
1,070
<5.0
373
290
1.5
<10
<10
Tank
WM Rear
10/27/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.57
<0.57
28.8
358
<5.0
451
182
0.63
<10
<10
Fulcher Center
10/27/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.56
<0.56
40.7
337
<5.0
396
205
0.70
<10
<10
Fulcher DG
10/27/15
<0.20
<0.40
<0.20
<0.51
<0.30
18.6
<1.0
<0.56
<0.56
14.5
228
<5.0
220
75.7
<0.50
<10
<10
Badcock
10/28/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
3608 Trent
11/09/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.42
<0.42
NR
NR
NR
NR
NR
NR
NR
NR
3612 Trent
10/28/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.56
<0.56
NR
NR
NR
NR
NR
NR
NR
NR
3700 Trent
10/28/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<0.63
<0.63
NR
NR
NR
NR
NR
NR
NR
NR
3702 Trent
10/28/15
<0.20
<0.40
<0.20
<0.51
<0.30
<0.33
<1.0
<5.0
<5.0
NR
NR
NR
NR
NR
NR
NR
NR
3704 Trent
10/28/15
<0.20
<0.40
4.5
<0.51
<0.30
<0.33
52.1
137
167
NR
NR
NR
NR
NR
NR
NR
NR
3706
10/28/15
<0.20
<0.80
13.8
7.9
<0.60
<0.65
154
328
447
NR
NR
NR
NR
NR
NR
NR
NR
3708
10/28/15
<0.20
<0.40
1 <0.20
<0.51
1 <0.30
1 <0.33
1 <1.0
1 <0.66
1 <0.66
NR
NR
NR
NR
NR
NR
NR
NR
Background
10/28/15
NR
NR
I NR
NR
I NR
I NR
I NR
I NR
I NR
320
2,290
<50
2,310
1,380
1.6
<100
<100
Notes:
• µg/1- micrograms per liter
• MAC - Maximum Allowable Concentration
• GCL - Gross contamination level; NS - Not specified; NR - Analysis not requested
• J - Estimated value between the laboratory reporting limit and the method detection limit
• < - Less than the method detection limit specified in the laboratory report
• Concentrations in bold exceeded the MAC
1 of 1

Figures

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SITE LOCATION
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0 1,000 2,000 4,000
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Feet
SCALE: 1 INCH = 2,000 FEET TRENT
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MAP CENTER LOCATION
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LATITUDE: 35.096850' N
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' FIGURE 1 '•�
f SITE LOCATION MAP
2116 SOUTH GLENBURNIE ROAD
NEW BERN, CRAVEN COUNTY, '•
'' NORTH CAROLINA
• , CQ;; GRI PROJECT NO. 3841
.. PREPARED BY:
GEOLOGICAL RESOURCES, INC.
Nov NOVEMBER 20, 2015
— Ciao,,"
Geological Resources, Inc. t _

LEGEND
- - - -
SUBJECT PROPERTY
BOUNDARY LINE
ADJACENT PROPERTY
BOUNDARY LINE
BUILDING FOOTPRINT
FD ®
FLOOR DRAIN
ows
OIL -WATER SEPARATOR
Q
MONITORING WELL
®
TEMPORARY MONITORING WELL
<0.20
BENZENE
<0.40
TOL UENE
<0.20
ETHYLBENZENE
0.61 J
XYLENES
<0.30
MTSE
<0.33
TE TRA CHL OR OE TH YL ENE
<1.0
NAPHTHALENE
<0.60
1-METHYLN4PHTHALENE
<0.60
2-METHYLNAPHTHALENE
<100
ARSENIC
<2,000
BAR/UM
963
CHROMIUM
380
LEAD
1.2
MERCURY
CONCENTRATIONS /N ag/L
<0.20 LESS THAN THE METHOD DETECT/ON LIMIT
SPECIFIED /N THE LABORATORY REPORT
✓" ESTIMATED VALUE
'WR" ANAL PSIS NOT REQUESTED
CONCENTRATIONS /N BOLD EXCEEDED THE MAC
MAC - MAX/MUM ALLOWABLE CONCENTRA770N
Note:
1. This Site Map is based on data from the
Craven County GIS of NC.
2. These parcels were not professionally
surveyed; locations of features are
approximate.
Pepsi-Co/a
Distribution
Strike
\ /
\ Zone
AA oho/t
F/
m� KING JR
/ pR•
by 1,
oU�E�PRp / • •' A pha/� 1
6 Clarke Power 1
// Services
lo
Q C/ark 0WS
<0.20 \� O 0 1
01GNY� I 0.57 OWS 1
5 / 1 0.76 J C/ark Floor "0 Clark F/oar
I
<0.30 Drains West FD
/ 1 I ®
<0.33 Drains East
1 <1.0
I 1 <0.48 1
<0.48
1 113 Clork
<2,000 Septic
1 I 621
1 oe C 0 <0.20
1 0.76 J
O I <0.20 Wosh Boy_ 0.22 J
Q <0.40 ® Z.30
I I <0.20
<0.51 Z.33
<1.0
<0.30
I <0.33 <0.61
<0.61
Nationwide I o.ss AS.h72.5
Ol�� 07
Insurance
V
`♦ WM Unknown
♦ ♦ Tank
♦ West 0
Fu/cher Fu/cher `Marine
<0.20 DG Center Shop
<0.40
<0.20
1&6 \
<0.30 WY Rear
<1.0 <0.20 Grove
0.56 <0.40
0.56 <0.20
14.5 <0.51
228 <0.30 i
220 <0.33 _
75.7 <1.0
<0.50 <0.56
<0.56 _
40.7
337
396
205
0.70 --Tre�
es/W000ed
EZ Mini
Storage
41.9 833
).20 321
).40 I 456 0.97
F0 623
W 1 274
SB&T
Bonk
0.69 1
� I1
Q I 1
I- es/Wooded 1
1 I
1 1
1
NR- - _ _ _ _
NR - -
1 NR
NR
1 NR
NR
NR
NR Field
1 _ inn
SAMPLING L OCA T/ON MAP #1
0 40 80 160 2116 South G/enburnie Road
New Bern, Craven County, NC
6R( IN FEET ) GRI Project No. J841
Geological Resources, Inc. 1 inch = 80 ft Dote: 11120115 Drown by. ECH I Figure: 2

LEGEND
- - - -
SUBJECT PROPERTY
BOUNDARY LINE
ADJACENT PROPERTY
BOUNDARY LINE
BUILDING FOOTPRINT
®
TEMPORARY MONITORING WELL
<o.zo
BENZENE
<0.40
TOL UENE
<o.zo
ETHYLBENZENE
<0.51
XYLENES
<0.3o
MTBE
<0.33
TETRACHLOROETHYLENE
a.o
NAPHTHALENE
NR
1-METHYLNAPHTHALENE
NR
2-METHYLNAPHTHALENE
NR
ARSENIC
NR
BARIUM
NR
CHROMIUM
NR
LEAD
NR
MERCURY
CONCENTRA TIONS IN ,ug/L
<0.20 LESS THAN THE METHOD DETECTION LIMIT
SPECIFIED IN THE LABORATORY REPORT
✓" ESTIMATED VALUE
"NR" ANALYSIS NOT REQUESTED
CONCENTRATIONS IN BOLD EXCEEDED THE MAC
MAC - MAXIMUM ALLOWABLE CONCENTRATION
Note:
1. This Site Mop is based on data from the
Craven County GIS of NC.
2. These parcels were not professionally
surveyed- locations of features ore
approximate.
Background
EZ Mini I
Storage 1
1
1 I 1
I 1
1
1
1
I
1 1
1 1
I I
1 1
J 1 1
I I
1 1
I 1
I
Field
Go5
1 �
1
1 _
1 Gras
1 1
I
1 1 I 1 zo -Residential Propert/es- 1
40 ► I 1
T �-�J70830 1
33 3706 1 I ►
Trent 1
.0 ► ® I 37066
4 1 --G...
1
88 ► <0.20 ® 13702 Trent 1 1 I
R <0.80 ► <0.20 ® 13700 Tren t ►
R 13.8 1 <0.40 <0.20 0 1
R 7.9 4.5 ► <0.4
<0.60 <0.51 0 <0.20 I 3612 Tren t I
R 1 <0.20 1
R _ <0.85 <0.30 3 <0.51 1 <0.20 1
328 521I <0.33
NR NR
NR NR
NR
I _
�1 C-)
O
1 �
<0.20 1
<0.40
<0.20 Z
1 <0.51 Badcock
<0.30 0 9
<0.33
I NR 1 =
NR �
NR �> I
NR Asphalt
NR
I NR Bcdcock C I
I NR Furniture
NR
Store II
T ees/Wooded Is
E�
I •�
1 _ -
I
1
♦ 1
I I
/
♦ 1
♦ 1
♦
♦ 1
1 -
ICrc ven
County
1 Board of
1 ---T,, es/WoodEd I Education
1
I I
1
1
1 I <0.20
I <0.40
� <0.20
3608 Tren t <0.51
<0.30
<0.33
1 <1.0
<0.42
<0.42
I NR
1 NR
NR
_ NR
NR
-NT RL7AD
SAMPLING L OCA T/ON MAP ,¢K2
0 50 100 200 2116 South G/enburnie Road
New Bern, Craven County, NC
6R( IN FEET ) GRI Project No. 3841
Geological Resources, Inc. 1 inch = 100 ft Date: 11120115 Drown by. ECH I Figure: 3

Appendices

Appendix A
Laboratory Analytical Reports

Southeast
■ ,o�N,ccuTEST
L A© OR AT OR E E 5
Technical Report for
GRI (Geological Resources Inc.)
2116 E Glenburnie Rd, New Bern, NC
3841 / 1775
Accutest Job Number: FA28901
Sampl i ng Dates: 10/27/ 15 - 10/28/ 15
Report to:
e Hardcopy 2.0
Automated Report
1
GRI
3502 Hayes Rd
Monroe, NC 28110
j wel I ons@geol ogi cal resourcesi nc. com; carri ekenned @geol ogi cal resourcesi nc. com;
jj r@geol ogi cal resourcesi nc. com; [e-mail]
ATTN: James Wellon
Total number of pages in report: 143
��Q AC Fp
2 �srcrr
Test results contained within this data package meet the requirements Norm Farmer
of the National Environmental Laboratory Accreditation Program Technical Director
and/or state specific certification programs as applicable.
CI i ent Service contact: M una Mohammed 407-425-6700
Certifications: FL (E83510), LA (03051), KS(E-10327), IA (366), IL (200063), NC (573), NJ(FL002), SC (96038001)
DoD ELAP (L-A-13 1-2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
http://www.ac)cutest.com
■■ 1 of 143
ACCUTEST
FA28907

Sections:
Table of Contents
-1-
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
5
Section3: Sample Results........................................................................................................
9
3.1: FA28901-1: CLARK OWS...........................................................................................
10
3.2: FA28901-2: CLARK FLOOR DRAINS WEST...........................................................
15
3.3: FA28901-3: CLARK FLOOR DRAINS EAST............................................................
20
3.4: FA28901-4: CLARK SEPTIC......................................................................................
25
3.5: FA28901-5: CLARK WASH BAY...............................................................................
30
3.6: FA28901-6: WM UNKNOWN TANK.........................................................................
35
3.7: FA28901-7: WM REAR...............................................................................................
40
3.8: FA28901-8: FULCHER CENTER...............................................................................
45
3.9: FA28901-9: FULCHER DG.........................................................................................
50
3.10: FA28901-10: BADCOCK...........................................................................................
55
3.11: FA28901-11: 3612 TRENT.........................................................................................
57
3.12: FA28901-12: 3700 TRENT........................................................................................
61
3.13: FA28901-13: 3702 TRENT........................................................................................
65
3.14: FA28901-14: 3704 TRENT........................................................................................
69
3.15: FA28901-15: 3706......................................................................................................
73
3.16: FA28901-16: 3708......................................................................................................
77
3.17: FA28901-17: BACKGROUND..................................................................................
81
Section4: Misc. Forms............................................................................................................
82
4.1: Chain of Custody...........................................................................................................
83
Section 5: GC/MS Volatiles - QC Data Summaries..............................................................
87
5.1: Method Blank Summary................................................................................................
88
5.2: Blank Spike Summary...................................................................................................
96
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
104
Section 6: GC/MS Semi-volatiles - QC Data Summaries.....................................................
6.1: Method Blank Summary................................................................................................
113
6.2: Blank Spike Summary...................................................................................................
119
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
123
Section 7: Metals Analysis - QC Data Summaries................................................................
127
7.1: Prep QC MP29604: Hg..................................................................................................
128
7.2: Prep QC MP29608: Hg..................................................................................................
133
7.3: Prep QC MP29610: As,Ba,Cd,Cr,Pb,Se,Ag..................................................................
138
■■ 2 of 143
ACCUTEST
FA28907

Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA28901
2116 E Glenburnie Rd, New Bern, NC
Project No: 3841/1775
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA28901-1
10/27/15
13:30 DG
10/29/15
AQ
Ground Water
CLARK OWS
FA28901-2
10/27/15
13:40 DG
10/29/15
AQ
Ground Water
CLARK FLOOR DRAINS WEST
FA28901-3
10/27/15
13:53 DG
10/29/15
AQ
Ground Water
CLARK FLOOR DRAINS EAST
FA28901-4
10/27/15
14:29 DG
10/29/15
AQ
Ground Water
CLARK SEPTIC
FA28901-5
10/27/15
14:54 DG
10/29/15
AQ
Ground Water
CLARK WASH BAY
FA28901-6
10/27/15
15:31 DG
10/29/15
AQ
Ground Water
WM UNKNOWN TANK
FA28901-7
10/27/15
15:44 DG
10/29/15
AQ
Ground Water
WM REAR
FA28901-8
10/27/15
15:59 DG
10/29/15
AQ
Ground Water
FULCHER CENTER
FA28901-9
10/27/15
16:12 DG
10/29/15
AQ
Ground Water
FULCHER DG
FA28901-10
10/28/15
09:01 DG
10/29/15
AQ
Ground Water
BADCOCK
FA28901-11
10/28/15
09:51 DG
10/29/15
AQ
Ground Water
3612 TRENT
FA28901-12
10/28/15
10:17 DG
10/29/15
AQ
Ground Water
3700 TRENT
FA28901-13
10/28/15
11:04 DG
10/29/15
AQ
Ground Water
3702 TRENT
■ 3 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No: FA28901
2116 E Glenburnie Rd, New Bern, NC
Project No: 3841/1775
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA28901-14 10/28/15 11:29 DG 10/29/15 AQ Ground Water 3704 TRENT
FA28901-15 10/28/15 11:56 DG 10/29/15 AQ Ground Water 3706
FA28901-16 10/28/15 12:45 DG 10/29/15 AQ Ground Water 3708
FA28901-17 10/28/15 13:13 DG 10/29/15 AQ Ground Water BACKGROUND
■ 4 of 143
E ACCUTEST
FA28901

Summary of Hits
Job Number: FA28901
Account: GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Collected: 10/27/15 thru 10/28/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA28901-1 CLARK OWS
1,2,4-Trimethylbenzene
0.22 J
Xylene (total)
0.61 J
Chromium a
963
Lead
380
Mercury
1.2
FA28901-2 CLARK FLOOR DRAINS WEST
Carbon Disulfide b
0.42 J
Toluene b
0.57 J
1,2,4-Trimethylbenzene b
0.27 J
Xylene (total) b
0.76 J
Arsenic a
113
Chromium a
621
Lead
203
Mercury
0.58
FA28901-3 CLARK FLOOR DRAINS EAST
Ethylbenzene b
0.49 J
Tetrachloroethylene b
2.2
Xylene (total) b
2.3 J
Phenanthrene
0.59 J
Arsenic
25.5
Barium
664
Chromium
571
Lead
314
Mercury
1.2
FA28901-4 CLARK SEPTIC
Carbon Disulfide b
0.45 J
Ethylbenzene b
0.22 J
Toluene b
0.76 J
1,2,4-Trimethylbenzene b
0.29 J
Xylene (total) b
1.0 J
Arsenic a
72.5
Barium a
707
Chromium a
833
Lead
321
Mercury
0.97
2.0
0.20
ug/1
SW846 8260B
3.0
0.51
ug/1
SW846 8260B
100
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
2.0
0.29
ug/1
SW846 8260B
1.0
0.40
ug/1
SW846 8260B
2.0
0.20
ug/1
SW846 8260B
3.0
0.51
ug/1
SW846 8260B
100
ug/1
SW846 6010C
100
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
1.0
0.20
ug/1
SW846 8260B
1.0
0.33
ug/1
SW846 8260B
3.0
0.51
ug/1
SW846 8260B
5.3
0.55
ug/1
SW846 8270D
10
ug/1
SW846 6010C
200
ug/1
SW846 6010C
10
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
2.0
0.29
ug/1
SW846 8260B
1.0
0.20
ug/1
SW846 8260B
1.0
0.40
ug/1
SW846 8260B
2.0
0.20
ug/1
SW846 8260B
3.0
0.51
ug/1
SW846 8260B
20
ug/1
SW846 6010C
400
ug/1
SW846 6010C
20
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
Page 1 of 4
■■ 5 of 143
ACCUTEST
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Summary of Hits
Job Number: FA28901
Account: GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Collected: 10/27/15 thru 10/28/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA28901-5
CLARK WASH BAY
Carbon Disulfide
b 0.34 J
Arsenic a
41.9
Barium a
456
Chromium a
623
Lead
274
Mercury
0.69
FA28901-6
WM UNKNOWN TANK
Arsenic
29.4
Barium
1070
Chromium
373
Lead
290
Mercury
1.5
FA28901-7
WM REAR
Carbon Disulfide
0.32 J
Arsenic
28.8
Barium
358
Chromium
451
Lead
182
Mercury
0.63
FA28901-8
FULCHER CENTER
Carbon Disulfide
0.44 J
Arsenic
40.7
Barium
337
Chromium
396
Lead
205
Mercury
0.70
FA28901-9
FULCHER DG
Carbon Disulfide
0.53 J
Tetrachloroethylene 18.6
Arsenic
14.5
Barium
228
Chromium
220
Lead
75.7
2.0
0.29
ug/1
SW846 8260B
20
ug/1
SW846 6010C
400
ug/1
SW846 6010C
20
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
10
ug/1
SW846 6010C
200
ug/1
SW846 6010C
10
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
2.0
0.29
ug/1
SW846 8260B
10
ug/1
SW846 6010C
200
ug/1
SW846 6010C
10
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
2.0
0.29
ug/1
SW846 8260B
10
ug/1
SW846 6010C
200
ug/1
SW846 6010C
10
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
0.50
ug/1
SW846 7470A
2.0
0.29
ug/1
SW846 8260B
1.0
0.33
ug/1
SW846 8260B
10
ug/1
SW846 6010C
200
ug/1
SW846 6010C
10
ug/1
SW846 6010C
5.0
ug/1
SW846 6010C
Page 2 of 4
■■ 6 of 143
ACCUTEST
FA28907

Summary of Hits
Job Number: FA28901
Account: GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Collected: 10/27/15 thru 10/28/15
,ab Sample ID Client Sample ID Result/
Lnalyte Qual RL MDL Units Method
FA28901-10 BADCOCK
No hits reported in this sample.
FA28901-11 3612 TRENT
No hits reported in this sample.
FA28901-12 3700 TRENT
No hits reported in this sample.
FA28901-13 3702 TRENT
No hits reported in this sample.
FA28901-14 3704 TRENT
n-Butylbenzene
14.4
1.0
0.22
ug/1
SW846 8260B
Ethylbenzene
4.5
1.0
0.20
ug/1
SW846 8260B
Isopropylbenzene
11.5
1.0
0.20
ug/1
SW846 8260B
Methylcyclohexane
2.7
1.0
0.22
ug/1
SW846 8260B
4-Methyl-2-pentanone (MIBK)
40.6
5.0
1.0
ug/1
SW846 8260B
Naphthalene
52.1
5.0
1.0
ug/1
SW846 8260B
n-Propylbenzene
22.7
1.0
0.20
ug/1
SW846 8260B
1,2,4-Trichlorobenzene
0.94 J
1.0
0.50
ug/1
SW846 8260B
1,2,4-Trimethylbenzene
65.9
2.0
0.20
ug/1
SW846 8260B
Acenaphthene
6.0
5.3
0.53
ug/1
SW846 8270D
Fluorene
15.7
5.3
0.53
ug/1
SW846 8270D
1-Methylnaphthalene
137
21
2.1
ug/1
SW846 8270D
2-Methylnaphthalene
167
21
2.1
ug/1
SW846 8270D
Naphthalene
30.5
5.3
0.53
ug/1
SW846 8270D
Phenanthrene
26.0
5.3
0.55
ug/1
SW846 8270D
Pyrene
1.0 J
5.3
0.58
ug/1
SW846 8270D
FA28901-15 3706
n-Butylbenzene
8.3
2.0
0.45
ug/1
SW846 8260B
Ethylbenzene
13.8
2.0
0.40
ug/1
SW846 8260B
Isopropylbenzene
9.2
2.0
0.40
ug/1
SW846 8260B
Methylcyclohexane
3.2
2.0
0.45
ug/1
SW846 8260B
Naphthalene
154
10
2.0
ug/1
SW846 8260B
n-Propylbenzene
21.7
2.0
0.40
ug/1
SW846 8260B
1,2,4-Trimethylbenzene
147
10
1.0
ug/1
SW846 8260B
1,3,5-Trimethylbenzene
42.5
4.0
0.45
ug/1
SW846 8260B
Page 3 of 4
■■ 7 of 143
ACCUTEST
FA28907

Summary of Hits
Job Number: FA28901
Account: GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Collected: 10/27/15 thru 10/28/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Xylene (total)
7.9
6.0
1.0
ug/1
SW846 8260B
Acenaphthene
25.9
6.1
0.61
ug/1
SW846 8270D
Anthracene
6.3
6.1
0.61
ug/1
SW846 8270D
Fluoranthene
1.7 J
6.1
0.61
ug/1
SW846 8270D
Fluorene
31.7
6.1
0.61
ug/1
SW846 8270D
1-Methylnaphthalene
328
24
2.4
ug/1
SW846 8270D
2-Methylnaphthalene
447
24
2.4
ug/1
SW846 8270D
Naphthalene
147
24
2.4
ug/1
SW846 8270D
Phenanthrene
56.3
6.1
0.63
ug/1
SW846 8270D
Pyrene
3.7 J
6.1
0.67
ug/1
SW846 8270D
FA28901-16 3708
No hits reported in this sample.
FA28901-17 BACKGROUND
Arsenic
320
100
ug/1
SW846 6010C
Barium
2290
2000
ug/1
SW846 6010C
Chromium
2310
100
ug/1
SW846 6010C
Lead
1380
50
ug/1
SW846 6010C
Mercury
1.6
0.50
ug/1
SW846 7470A
(a) Elevated reporting limit(s) due to matrix interference.
(b) Sample was not preserved to a pH < 2; reported results are considered minimum values.
Page 4 of 4
■ 8 of 143
E ACCUTEST
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Section 3
Southeast
ACCUTEST
L A B O RAT D R I ES
Sample Results
Report of Analysis
■ ,i 9 of 143
ACCUTEBT
FA28901 `A ... A I..

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK OWS
Lab Sample ID: FA28901-1 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36794.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 10 of 143
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Accutest Laboratories
Report of Analysis
'lient Sample ID: CLARK OWS
,ab Sample ID: FA28901-1 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
0.22
2.0
0.20
ug/1 J
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
0.61
3.0
0.51
ug/1 J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
79-125%
2037-26-5
Toluene-D8
96%
85-112%
460-00-4
4-Bromofluorobenzene
95%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 11 of 143
ACCUTEST
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK OWS
Lab Sample ID: FA28901-1 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684444.D 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run # 1 840 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
60
12
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.0
0.60
ug/1
95-57-8
2-Chlorophenol
ND
6.0
0.60
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.0
0.60
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.0
0.60
ug/1
51-28-5
2,4-Dinitrophenol
ND
30
6.0
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
12
2.5
ug/1
95-48-7
2-Methylphenol
ND
6.0
0.60
ug/1
3&4-Methylphenol
ND
6.0
1.2
ug/1
88-75-5
2-Nitrophenol
ND
6.0
1.0
ug/1
100-02-7
4-Nitrophenol
ND
30
6.0
ug/1
87-86-5
Pentachlorophenol
ND
30
6.0
ug/1
108-95-2
Phenol
ND
6.0
0.60
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.0
0.75
ug/1
83-32-9
Acenaphthene
ND
6.0
0.60
ug/1
208-96-8
Acenaphthylene
ND
6.0
0.60
ug/1
120-12-7
Anthracene
ND
6.0
0.60
ug/1
56-55-3
Benzo(a)anthracene
ND
6.0
0.60
ug/1
50-32-8
Benzo(a)pyrene
ND
6.0
0.60
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.0
0.69
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.0
0.79
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.0
0.81
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.0
0.76
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.0
1.2
ug/1
106-47-8
4-Chloroaniline
ND
6.0
0.60
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.0
0.75
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.0
0.82
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.0
0.60
ug/1
91-58-7
2-Chloronaphthalene
ND
6.0
0.60
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.0
0.68
ug/1
218-01-9
Chrysene
ND
6.0
0.60
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.0
0.81
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 12 of 143
ACCUTEST
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Accutest Laboratories
Report of Analysis
lient Sample ID: CLARK OWS
gab Sample ID: FA28901-1 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.0
0.60
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.0
0.62
ug/1
84-66-2
Diethyl Phthalate
ND
6.0
1.7
ug/1
131-11-3
Dimethyl Phthalate
ND
6.0
1.2
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.0
1.2
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.0
1.2
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.0
0.69
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.0
0.82
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.0
1.2
ug/1
206-44-0
Fluoranthene
ND
6.0
0.60
ug/1
86-73-7
Fluorene
ND
6.0
0.60
ug/1
118-74-1
Hexachlorobenzene
ND
6.0
0.75
ug/1
87-68-3
Hexachlorobutadiene
ND
6.0
0.71
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.0
1.2
ug/1
67-72-1
Hexachloroethane
ND
6.0
0.81
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.0
0.75
ug/1
78-59-1
Isophorone
ND
6.0
0.61
ug/1
90-12-0
1-Methylnaphthalene
ND
6.0
0.60
ug/1
91-57-6
2-Methylnaphthalene
ND
6.0
0.60
ug/1
91-20-3
Naphthalene
ND
6.0
0.60
ug/1
98-95-3
Nitrobenzene
ND
6.0
0.62
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.0
0.69
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.0
0.70
ug/1
85-01-8
Phenanthrene
ND
6.0
0.61
ug/1
129-00-0
Pyrene
ND
6.0
0.65
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
29%
14-67%
4165-62-2
Phenol-d5
23%
10-50%
118-79-6
2,4,6-Tribromophenol
76%
33-118%
4165-60-0
Nitrobenzene-d5
62%
42-108%
321-60-8
2-Fluorobiphenyl
68%
40-106%
1718-51-0
Terphenyl-dl4
66%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 13 of 143
E ACCUTEST
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Accutest Laboratories
Report of Analysis Page 1 of 1 j
Client Sample ID: CLARK OWS
Lab Sample ID: FA28901-1 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic a < 100 100
ug/1
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Barium a < 2000 2000
ug/l
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Cadmium a < 50 50
ug/l
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Chromium a 963 100
ug/l
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Lead 380 5.0
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 5
Mercury 1.2 0.50
ug/l
1
11/03/15
11/03/15
JL
SW846 7470A 1
SW846 7470A 4
Selenium a < 100 100
ug/l
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Silver a < 100 100
ug/l
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Instrument QC Batch: MA12759
(4) Prep QC Batch: MP29608
(5) Prep QC Batch: MP29610
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
■ 14 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK FLOOR DRAINS WEST
Lab Sample ID: FA28901-2 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36795.13 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.42
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 15 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: CLARK FLOOR DRAINS WEST
,ab Sample ID: FA28901-2 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
0.57
1.0
0.40
ug/1 J
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
0.27
2.0
0.20
ug/1 J
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
0.76
3.0
0.51
ug/1 J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
79-125%
2037-26-5
Toluene-D8
98%
85-112%
460-00-4
4-Bromofluorobenzene
96%
83-118%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
Page 2 of 2 N
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 16 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK FLOOR DRAINS WEST
Lab Sample ID: FA28901-2 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684445.D 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run # 1 1040 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
48
9.6
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
4.8
0.48
ug/1
95-57-8
2-Chlorophenol
ND
4.8
0.48
ug/1
120-83-2
2,4-Dichlorophenol
ND
4.8
0.48
ug/1
105-67-9
2,4-Dimethylphenol
ND
4.8
0.48
ug/1
51-28-5
2,4-Dinitrophenol
ND
24
4.8
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
9.6
2.1
ug/1
95-48-7
2-Methylphenol
ND
4.8
0.48
ug/1
3&4-Methylphenol
ND
4.8
0.96
ug/1
88-75-5
2-Nitrophenol
ND
4.8
0.84
ug/1
100-02-7
4-Nitrophenol
ND
24
4.8
ug/1
87-86-5
Pentachlorophenol
ND
24
4.8
ug/1
108-95-2
Phenol
ND
4.8
0.48
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
4.8
0.60
ug/1
83-32-9
Acenaphthene
ND
4.8
0.48
ug/1
208-96-8
Acenaphthylene
ND
4.8
0.48
ug/1
120-12-7
Anthracene
ND
4.8
0.48
ug/1
56-55-3
Benzo(a)anthracene
ND
4.8
0.48
ug/1
50-32-8
Benzo(a)pyrene
ND
4.8
0.48
ug/1
205-99-2
Benzo(b)fluoranthene
ND
4.8
0.56
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
4.8
0.63
ug/1
207-08-9
Benzo(k)fluoranthene
ND
4.8
0.66
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
4.8
0.61
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
4.8
0.96
ug/1
106-47-8
4-Chloroaniline
ND
4.8
0.48
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
4.8
0.61
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
4.8
0.66
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
4.8
0.48
ug/1
91-58-7
2-Chloronaphthalene
ND
4.8
0.48
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
4.8
0.55
ug/1
218-01-9
Chrysene
ND
4.8
0.49
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
4.8
0.65
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 17 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: CLARK FLOOR DRAINS WEST
gab Sample ID: FA28901-2 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
4.8
0.48
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
4.8
0.50
ug/1
84-66-2
Diethyl Phthalate
ND
4.8
1.4
ug/1
131-11-3
Dimethyl Phthalate
ND
4.8
0.96
ug/1
84-74-2
Di-n-butyl Phthalate
ND
4.8
0.96
ug/1
117-84-0
Di-n-octyl Phthalate
ND
4.8
0.96
ug/1
121-14-2
2,4-Dinitrotoluene
ND
4.8
0.56
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
4.8
0.66
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
4.8
0.96
ug/1
206-44-0
Fluoranthene
ND
4.8
0.48
ug/1
86-73-7
Fluorene
ND
4.8
0.48
ug/1
118-74-1
Hexachlorobenzene
ND
4.8
0.61
ug/1
87-68-3
Hexachlorobutadiene
ND
4.8
0.58
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
4.8
0.96
ug/1
67-72-1
Hexachloroethane
ND
4.8
0.66
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
4.8
0.61
ug/1
78-59-1
Isophorone
ND
4.8
0.49
ug/1
90-12-0
1-Methylnaphthalene
ND
4.8
0.48
ug/1
91-57-6
2-Methylnaphthalene
ND
4.8
0.48
ug/1
91-20-3
Naphthalene
ND
4.8
0.48
ug/1
98-95-3
Nitrobenzene
ND
4.8
0.50
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
4.8
0.56
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
4.8
0.57
ug/1
85-01-8
Phenanthrene
ND
4.8
0.49
ug/1
129-00-0
Pyrene
ND
4.8
0.53
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
38%
14-67%
4165-62-2
Phenol-d5
30%
10-50%
118-79-6
2,4,6-Tribromophenol
85%
33-118%
4165-60-0
Nitrobenzene-d5
61%
42-108%
321-60-8
2-Fluorobiphenyl
67%
40-106%
1718-51-0
Terphenyl-dl4
72%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 18 of 143
E ACCUTEST
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Report of Analysis Page 1 of 1 N
Client Sample ID: CLARK FLOOR DRAINS WEST
Lab Sample ID: FA28901-2 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic a 113 100
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Barium a < 2000 2000
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Cadmium a < 50 50
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Chromium a 621 100
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Lead 203 5.0
ug/I
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 5
Mercury 0.58 0.50
ug/I
1
11/03/15
11/03/15
7L
SW846 7470A 1
SW846 7470A 4
Selenium a < 100 100
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Silver a < 100 100
ug/I
10
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Instrument QC Batch: MA12759
(4) Prep QC Batch: MP29608
(5) Prep QC Batch: MP29610
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
■ 19 of 143
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Report of Analysis Page 1 of 2
Client Sample ID: CLARK FLOOR DRAINS EAST
Lab Sample ID: FA28901-3 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36796.13 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
0.49
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 20 of 143
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Report of Analysis
'lient Sample ID: CLARK FLOOR DRAINS EAST
,ab Sample ID: FA28901-3 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
2.2
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
2.3
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
97%
83-118%
J
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
Page 2 of 2 w
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 21 of 143
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Report of Analysis Page 1 of 2
Client Sample ID: CLARK FLOOR DRAINS EAST
Lab Sample ID: FA28901-3 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684446.D 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run # 1 940 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
53
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.3
0.53
ug/1
95-57-8
2-Chlorophenol
ND
5.3
0.53
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.3
0.53
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.3
0.53
ug/l
51-28-5
2,4-Dinitrophenol
ND
27
5.3
ug/l
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.3
ug/1
95-48-7
2-Methylphenol
ND
5.3
0.53
ug/1
3&4-Methylphenol
ND
5.3
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.3
0.93
ug/1
100-02-7
4-Nitrophenol
ND
27
5.3
ug/1
87-86-5
Pentachlorophenol
ND
27
5.3
ug/1
108-95-2
Phenol
ND
5.3
0.53
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.3
0.67
ug/1
83-32-9
Acenaphthene
ND
5.3
0.53
ug/l
208-96-8
Acenaphthylene
ND
5.3
0.53
ug/1
120-12-7
Anthracene
ND
5.3
0.53
ug/1
56-55-3
Benzo(a)anthracene
ND
5.3
0.53
ug/1
50-32-8
Benzo(a)pyrene
ND
5.3
0.53
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.3
0.62
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.3
0.70
ug/l
207-08-9
Benzo(k)fluoranthene
ND
5.3
0.73
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.3
0.68
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.3
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.3
0.53
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.3
0.67
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.3
0.73
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.3
0.54
ug/1
91-58-7
2-Chloronaphthalene
ND
5.3
0.53
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.3
0.61
ug/1
218-01-9
Chrysene
ND
5.3
0.54
ug/l
53-70-3
Dibenzo(a,h)anthracene
ND
5.3
0.72
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 22 of 143
ACCUTEST
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Accutest Laboratories
Report of Analysis
lient Sample ID: CLARK FLOOR DRAINS EAST
gab Sample ID: FA28901-3 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.3
0.53
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
5.3
0.55
ug/l
84-66-2
Diethyl Phthalate
ND
5.3
1.5
ug/l
131-11-3
Dimethyl Phthalate
ND
5.3
1.1
ug/l
84-74-2
Di-n-butyl Phthalate
ND
5.3
1.1
ug/l
117-84-0
Di-n-octyl Phthalate
ND
5.3
1.1
ug/l
121-14-2
2,4-Dinitrotoluene
ND
5.3
0.62
ug/l
606-20-2
2, 6-Dinitrotoluene
ND
5.3
0.73
ug/l
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.3
1.1
ug/l
206-44-0
Fluoranthene
ND
5.3
0.53
ug/l
86-73-7
Fluorene
ND
5.3
0.53
ug/l
118-74-1
Hexachlorobenzene
ND
5.3
0.67
ug/l
87-68-3
Hexachlorobutadiene
ND
5.3
0.64
ug/l
77-47-4
Hexachlorocyclopentadiene
ND
5.3
1.1
ug/l
67-72-1
Hexachloroethane
ND
5.3
0.73
ug/l
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.3
0.67
ug/l
78-59-1
Isophorone
ND
5.3
0.54
ug/l
90-12-0
1-Methylnaphthalene
ND
5.3
0.53
ug/l
91-57-6
2-Methylnaphthalene
ND
5.3
0.53
ug/l
91-20-3
Naphthalene
ND
5.3
0.53
ug/l
98-95-3
Nitrobenzene
ND
5.3
0.56
ug/l
621-64-7
N-Nitrosodi-n-propylamine
ND
5.3
0.62
ug/l
86-30-6
N-Nitrosodiphenylamine
ND
5.3
0.63
ug/l
85-01-8
Phenanthrene
0.59
5.3
0.55
ug/l J
129-00-0
Pyrene
ND
5.3
0.58
ug/l
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
44%
14-67%
4165-62-2
Phenol-d5
32%
10-50%
118-79-6
2,4,6-Tribromophenol
104%
33-118%
4165-60-0
Nitrobenzene-d5
80%
42-108%
321-60-8
2-Fluorobiphenyl
84%
40-106%
1718-51-0
Terphenyl-dl4
75%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 23 of 143
E ACCUTEST
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Accutest Laboratories
Report of Analysis
Client Sample ID: CLARK FLOOR DRAINS EAST
Lab Sample ID: FA28901-3 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 25.5 10
Barium 664 200
Cadmium < 5.0 5.0
Chromium 571 10
Lead 314 5.0
Mercury 1.2 0.50
Selenium < 10 10
Silver < 10 10
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29608
(4) Prep QC Batch: MP29610
RL = Reporting Limit
Page 1 of 1 w
Units DF Prep Analyzed By Method Prep Method
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
JL
SW846 7470A 1
SW846 7470A 3
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/1
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■ 24 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK SEPTIC
Lab Sample ID: FA28901-4 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36797.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.45
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
0.22
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 25 of 143
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Report of Analysis
'lient Sample ID: CLARK SEPTIC
,ab Sample ID: FA28901-4 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
0.76
1.0
0.40
ug/1 J
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
0.29
2.0
0.20
ug/1 J
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
1.0
3.0
0.51
ug/1 J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
102%
79-125%
2037-26-5
Toluene-D8
97%
85-112%
460-00-4
4-Bromofluorobenzene
97%
83-118%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
Page 2 of 2 a
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 26 of 143
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Report of Analysis Page 1 of 2
Client Sample ID: CLARK SEPTIC
Lab Sample ID: FA28901-4 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684448.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 820 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
61
12
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.1
0.61
ug/1
95-57-8
2-Chlorophenol
ND
6.1
0.61
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.1
0.61
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.1
0.61
ug/1
51-28-5
2,4-Dinitrophenol
ND
30
6.1
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
12
2.6
ug/1
95-48-7
2-Methylphenol
ND
6.1
0.61
ug/1
3&4-Methylphenol
ND
6.1
1.2
ug/1
88-75-5
2-Nitrophenol
ND
6.1
1.1
ug/1
100-02-7
4-Nitrophenol
ND
30
6.1
ug/1
87-86-5
Pentachlorophenol
ND
30
6.1
ug/1
108-95-2
Phenol
ND
6.1
0.61
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.1
0.77
ug/1
83-32-9
Acenaphthene
ND
6.1
0.61
ug/1
208-96-8
Acenaphthylene
ND
6.1
0.61
ug/1
120-12-7
Anthracene
ND
6.1
0.61
ug/1
56-55-3
Benzo(a)anthracene
ND
6.1
0.61
ug/1
50-32-8
Benzo(a)pyrene
ND
6.1
0.61
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.1
0.71
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.1
0.80
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.1
0.83
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.1
0.77
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.1
1.2
ug/1
106-47-8
4-Chloroaniline
ND
6.1
0.61
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.1
0.77
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.1
0.84
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.1
0.61
ug/1
91-58-7
2-Chloronaphthalene
ND
6.1
0.61
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.1
0.70
ug/1
218-01-9
Chrysene
ND
6.1
0.62
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.1
0.83
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 27 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: CLARK SEPTIC
gab Sample ID: FA28901-4 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.1
0.61
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.1
0.64
ug/1
84-66-2
Diethyl Phthalate
ND
6.1
1.7
ug/1
131-11-3
Dimethyl Phthalate
ND
6.1
1.2
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.1
1.2
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.1
1.2
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.1
0.71
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.1
0.84
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.1
1.2
ug/1
206-44-0
Fluoranthene
ND
6.1
0.61
ug/1
86-73-7
Fluorene
ND
6.1
0.61
ug/1
118-74-1
Hexachlorobenzene
ND
6.1
0.77
ug/1
87-68-3
Hexachlorobutadiene
ND
6.1
0.73
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.1
1.2
ug/1
67-72-1
Hexachloroethane
ND
6.1
0.83
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.1
0.77
ug/1
78-59-1
Isophorone
ND
6.1
0.62
ug/1
90-12-0
1-Methylnaphthalene
ND
6.1
0.61
ug/1
91-57-6
2-Methylnaphthalene
ND
6.1
0.61
ug/1
91-20-3
Naphthalene
ND
6.1
0.61
ug/1
98-95-3
Nitrobenzene
ND
6.1
0.64
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.1
0.71
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.1
0.72
ug/1
85-01-8
Phenanthrene
ND
6.1
0.63
ug/1
129-00-0
Pyrene
ND
6.1
0.67
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
42%
14-67%
4165-62-2
Phenol-d5
32%
10-50%
118-79-6
2,4,6-Tribromophenol
92%
33-118%
4165-60-0
Nitrobenzene-d5
69%
42-108%
321-60-8
2-Fluorobiphenyl
75%
40-106%
1718-51-0
Terphenyl-dl4
72%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 28 of 143
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Report of Analysis Page 1 of 1 P
Client Sample ID: CLARK SEPTIC
Lab Sample ID: FA28901-4 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic a 72.5 20
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Barium a 707 400
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Cadmium a < 10 10
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Chromium a 833 20
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Lead 321 5.0
ug/I
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 5
Mercury 0.97 0.50
ug/I
1
11/03/15
11/03/15
7L
SW846 7470A 1
SW846 7470A 4
Selenium a < 20 20
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Silver a < 20 20
ug/I
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Instrument QC Batch: MA12759
(4) Prep QC Batch: MP29608
(5) Prep QC Batch: MP29610
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
■ 29 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK WASH BAY
Lab Sample ID: FA28901-5 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36798.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.34
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 30 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
'lient Sample ID: CLARK WASH BAY
,ab Sample ID: FA28901-5 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
102%
79-125%
2037-26-5
Toluene-D8
98%
85-112%
460-00-4
4-Bromofluorobenzene
96%
83-118%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 31 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: CLARK WASH BAY
Lab Sample ID: FA28901-5 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684449.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 920 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
54
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.4
0.54
ug/1
95-57-8
2-Chlorophenol
ND
5.4
0.54
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.4
0.54
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.4
0.54
ug/1
51-28-5
2,4-Dinitrophenol
ND
27
5.4
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.3
ug/1
95-48-7
2-Methylphenol
ND
5.4
0.54
ug/1
3&4-Methylphenol
ND
5.4
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.4
0.95
ug/1
100-02-7
4-Nitrophenol
ND
27
5.4
ug/1
87-86-5
Pentachlorophenol
ND
27
5.4
ug/1
108-95-2
Phenol
ND
5.4
0.54
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.4
0.68
ug/1
83-32-9
Acenaphthene
ND
5.4
0.54
ug/1
208-96-8
Acenaphthylene
ND
5.4
0.54
ug/1
120-12-7
Anthracene
ND
5.4
0.54
ug/1
56-55-3
Benzo(a)anthracene
ND
5.4
0.54
ug/1
50-32-8
Benzo(a)pyrene
ND
5.4
0.54
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.4
0.63
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.4
0.72
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.4
0.74
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.4
0.69
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.4
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.4
0.54
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.4
0.69
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.4
0.75
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.4
0.55
ug/1
91-58-7
2-Chloronaphthalene
ND
5.4
0.54
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.4
0.62
ug/1
218-01-9
Chrysene
ND
5.4
0.55
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.4
0.74
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 32 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: CLARK WASH BAY
gab Sample ID: FA28901-5 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.4
0.54
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.4
0.57
ug/1
84-66-2
Diethyl Phthalate
ND
5.4
1.5
ug/1
131-11-3
Dimethyl Phthalate
ND
5.4
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.4
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.4
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.4
0.63
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.4
0.75
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.4
1.1
ug/1
206-44-0
Fluoranthene
ND
5.4
0.54
ug/1
86-73-7
Fluorene
ND
5.4
0.55
ug/1
118-74-1
Hexachlorobenzene
ND
5.4
0.68
ug/1
87-68-3
Hexachlorobutadiene
ND
5.4
0.65
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.4
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.4
0.74
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.4
0.69
ug/1
78-59-1
Isophorone
ND
5.4
0.56
ug/1
90-12-0
1-Methylnaphthalene
ND
5.4
0.54
ug/1
91-57-6
2-Methylnaphthalene
ND
5.4
0.55
ug/1
91-20-3
Naphthalene
ND
5.4
0.54
ug/1
98-95-3
Nitrobenzene
ND
5.4
0.57
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.4
0.63
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.4
0.64
ug/1
85-01-8
Phenanthrene
ND
5.4
0.56
ug/1
129-00-0
Pyrene
ND
5.4
0.59
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
42%
14-67%
4165-62-2
Phenol-d5
32%
10-50%
118-79-6
2,4,6-Tribromophenol
91%
33-118%
4165-60-0
Nitrobenzene-d5
71%
42-108%
321-60-8
2-Fluorobiphenyl
77%
40-106%
1718-51-0
Terphenyl-dl4
75%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 33 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 1 P
Client Sample ID: CLARK WASH BAY
Lab Sample ID: FA28901-5 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic a 41.9 20
ug/1
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Barium a 456 400
ug/l
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Cadmium a < 10 10
ug/l
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Chromium a 623 20
ug/l
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Lead 274 5.0
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 5
Mercury 0.69 0.50
ug/l
1
11/03/15
11/03/15
7L
SW846 7470A 1
SW846 7470A 4
Selenium a < 20 20
ug/l
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
Silver a < 20 20
ug/l
2
11/03/15
11/04/15
LM
SW846 6010C 3
SW846 3010A 5
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Instrument QC Batch: MA12759
(4) Prep QC Batch: MP29608
(5) Prep QC Batch: MP29610
(a) Elevated reporting limit(s) due to matrix interference.
RL = Reporting Limit
■ 34 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: WM UNKNOWN TANK
Lab Sample ID: FA28901-6 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36799.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 35 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: WM UNKNOWN TANK
,ab Sample ID: FA28901-6 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
103%
79-125%
2037-26-5
Toluene-D8
90%
85-112%
460-00-4
4-Bromofluorobenzene
94%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 36 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: WM UNKNOWN TANK
Lab Sample ID: FA28901-6 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684487.13 1 11/05/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 800 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
63
13
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.3
0.63
ug/1
95-57-8
2-Chlorophenol
ND
6.3
0.63
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.3
0.63
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.3
0.63
ug/1
51-28-5
2,4-Dinitrophenol
ND
31
6.3
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
13
2.7
ug/1
95-48-7
2-Methylphenol
ND
6.3
0.63
ug/1
3&4-Methylphenol
ND
6.3
1.3
ug/1
88-75-5
2-Nitrophenol
ND
6.3
1.1
ug/1
100-02-7
4-Nitrophenol
ND
31
6.3
ug/1
87-86-5
Pentachlorophenol
ND
31
6.3
ug/1
108-95-2
Phenol
ND
6.3
0.63
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.3
0.79
ug/1
83-32-9
Acenaphthene
ND
6.3
0.63
ug/1
208-96-8
Acenaphthylene
ND
6.3
0.63
ug/1
120-12-7
Anthracene
ND
6.3
0.63
ug/1
56-55-3
Benzo(a)anthracene
ND
6.3
0.63
ug/1
50-32-8
Benzo(a)pyrene
ND
6.3
0.63
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.3
0.73
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.3
0.83
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.3
0.85
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.3
0.79
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.3
1.3
ug/1
106-47-8
4-Chloroaniline
ND
6.3
0.63
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.3
0.79
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.3
0.86
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.3
0.63
ug/1
91-58-7
2-Chloronaphthalene
ND
6.3
0.63
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.3
0.72
ug/1
218-01-9
Chrysene
ND
6.3
0.64
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.3
0.85
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 37 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: WM UNKNOWN TANK
gab Sample ID: FA28901-6 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.3
0.63
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.3
0.65
ug/1
84-66-2
Diethyl Phthalate
ND
6.3
1.8
ug/1
131-11-3
Dimethyl Phthalate
ND
6.3
1.3
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.3
1.3
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.3
1.3
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.3
0.73
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.3
0.86
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.3
1.3
ug/1
206-44-0
Fluoranthene
ND
6.3
0.63
ug/1
86-73-7
Fluorene
ND
6.3
0.63
ug/1
118-74-1
Hexachlorobenzene
ND
6.3
0.79
ug/1
87-68-3
Hexachlorobutadiene
ND
6.3
0.75
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.3
1.3
ug/1
67-72-1
Hexachloroethane
ND
6.3
0.85
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.3
0.79
ug/1
78-59-1
Isophorone
ND
6.3
0.64
ug/1
90-12-0
1-Methylnaphthalene
ND
6.3
0.63
ug/1
91-57-6
2-Methylnaphthalene
ND
6.3
0.63
ug/1
91-20-3
Naphthalene
ND
6.3
0.63
ug/1
98-95-3
Nitrobenzene
ND
6.3
0.65
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.3
0.72
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.3
0.74
ug/1
85-01-8
Phenanthrene
ND
6.3
0.64
ug/1
129-00-0
Pyrene
ND
6.3
0.68
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
42%
14-67%
4165-62-2
Phenol-d5
31%
10-50%
118-79-6
2,4,6-Tribromophenol
82%
33-118%
4165-60-0
Nitrobenzene-d5
68%
42-108%
321-60-8
2-Fluorobiphenyl
71%
40-106%
1718-51-0
Terphenyl-dl4
69%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 38 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
Client Sample ID: WM UNKNOWN TANK
Lab Sample ID: FA28901-6 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 29.4 10
Barium 1070 200
Cadmium < 5.0 5.0
Chromium 373 10
Lead 290 5.0
Mercury 1.5 0.50
Selenium < 10 10
Silver < 10 10
(1) Instrument QC Batch: MA12753
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29604
(4) Prep QC Batch: MP29610
RL = Reporting Limit
Page 1 of 1
Units DF Prep Analyzed By Method Prep Method
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/02/15
11/02/15
JL
SW846 7470A 1
SW846 7470A 3
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■ 39 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: WM REAR
Lab Sample ID: FA28901-7 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36800.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.32
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 40 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
'lient Sample ID: WM REAR
,ab Sample ID: FA28901-7 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
102%
79-125%
2037-26-5
Toluene-D8
92%
85-112%
460-00-4
4-Bromofluorobenzene
97%
83-118%
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 41 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: WM REAR
Lab Sample ID: FA28901-7 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684452.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 880 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
57
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.7
0.57
ug/1
95-57-8
2-Chlorophenol
ND
5.7
0.57
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.7
0.57
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.7
0.57
ug/1
51-28-5
2,4-Dinitrophenol
ND
28
5.7
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.4
ug/1
95-48-7
2-Methylphenol
ND
5.7
0.57
ug/1
3&4-Methylphenol
ND
5.7
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.7
1.0
ug/1
100-02-7
4-Nitrophenol
ND
28
5.7
ug/1
87-86-5
Pentachlorophenol
ND
28
5.7
ug/1
108-95-2
Phenol
ND
5.7
0.57
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.7
0.71
ug/1
83-32-9
Acenaphthene
ND
5.7
0.57
ug/1
208-96-8
Acenaphthylene
ND
5.7
0.57
ug/1
120-12-7
Anthracene
ND
5.7
0.57
ug/1
56-55-3
Benzo(a)anthracene
ND
5.7
0.57
ug/1
50-32-8
Benzo(a)pyrene
ND
5.7
0.57
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.7
0.66
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.7
0.75
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.7
0.78
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.7
0.72
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.7
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.7
0.57
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.7
0.72
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.7
0.78
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.7
0.57
ug/1
91-58-7
2-Chloronaphthalene
ND
5.7
0.57
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.7
0.65
ug/1
218-01-9
Chrysene
ND
5.7
0.58
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.7
0.77
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 42 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
Tent Sample ID: WM REAR
,ab Sample ID: FA28901-7 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No. Compound Result RL MDL Units Q
132-64-9
Dibenzofuran
ND
5.7
0.57
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.7
0.59
ug/1
84-66-2
Diethyl Phthalate
ND
5.7
1.6
ug/1
131-11-3
Dimethyl Phthalate
ND
5.7
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.7
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.7
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.7
0.66
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.7
0.78
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.7
1.1
ug/1
206-44-0
Fluoranthene
ND
5.7
0.57
ug/1
86-73-7
Fluorene
ND
5.7
0.57
ug/1
118-74-1
Hexachlorobenzene
ND
5.7
0.72
ug/1
87-68-3
Hexachlorobutadiene
ND
5.7
0.68
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.7
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.7
0.78
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.7
0.72
ug/1
78-59-1
Isophorone
ND
5.7
0.58
ug/1
90-12-0
1-Methylnaphthalene
ND
5.7
0.57
ug/1
91-57-6
2-Methylnaphthalene
ND
5.7
0.57
ug/1
91-20-3
Naphthalene
ND
5.7
0.57
ug/1
98-95-3
Nitrobenzene
ND
5.7
0.59
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.7
0.66
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.7
0.67
ug/1
85-01-8
Phenanthrene
ND
5.7
0.58
ug/1
129-00-0
Pyrene
ND
5.7
0.62
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
44%
14-67%
4165-62-2
Phenol-d5
34%
10-50%
118-79-6
2,4,6-Tribromophenol
93%
33-118%
4165-60-0
Nitrobenzene-d5
72%
42-108%
321-60-8
2-Fluorobiphenyl
79%
40-106%
1718-51-0
Terphenyl-dl4
72%
39-121%
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■ 43 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
Client Sample ID: WM REAR
Lab Sample ID: FA28901-7 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 28.8 10
Barium 358 200
Cadmium < 5.0 5.0
Chromium 451 10
Lead 182 5.0
Mercury 0.63 0.50
Selenium < 10 10
Silver < 10 10
(1) Instrument QC Batch: MA12753
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29604
(4) Prep QC Batch: MP29610
RL = Reporting Limit
Page 1 of 1 P
Units DF Prep Analyzed By Method Prep Method
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/02/15
11/02/15
JL
SW846 7470A 1
SW846 7470A 3
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■ 44 of 143
■ ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: FULCHER CENTER
Lab Sample ID: FA28901-8 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P3680LD 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.44
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
00
■■ 45 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: FULCHER CENTER
,ab Sample ID: FA28901-8 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
103%
79-125%
2037-26-5
Toluene-D8
90%
85-112%
460-00-4
4-Bromofluorobenzene
96%
83-118%
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 46 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: FULCHER CENTER
Lab Sample ID: FA28901-8 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684453.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 890 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
56
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.6
0.56
ug/1
95-57-8
2-Chlorophenol
ND
5.6
0.56
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.6
0.56
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.6
0.56
ug/1
51-28-5
2,4-Dinitrophenol
ND
28
5.6
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.4
ug/1
95-48-7
2-Methylphenol
ND
5.6
0.56
ug/1
3&4-Methylphenol
ND
5.6
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.6
0.99
ug/1
100-02-7
4-Nitrophenol
ND
28
5.6
ug/1
87-86-5
Pentachlorophenol
ND
28
5.6
ug/1
108-95-2
Phenol
ND
5.6
0.56
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.6
0.71
ug/1
83-32-9
Acenaphthene
ND
5.6
0.56
ug/1
208-96-8
Acenaphthylene
ND
5.6
0.56
ug/1
120-12-7
Anthracene
ND
5.6
0.56
ug/1
56-55-3
Benzo(a)anthracene
ND
5.6
0.56
ug/1
50-32-8
Benzo(a)pyrene
ND
5.6
0.56
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.6
0.65
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.6
0.74
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.6
0.77
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.6
0.71
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.6
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.6
0.56
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.6
0.71
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.6
0.78
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.6
0.57
ug/1
91-58-7
2-Chloronaphthalene
ND
5.6
0.56
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.6
0.64
ug/1
218-01-9
Chrysene
ND
5.6
0.57
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.6
0.76
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
i"
■■ 47 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: FULCHER CENTER
gab Sample ID: FA28901-8 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.6
0.56
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.6
0.59
ug/1
84-66-2
Diethyl Phthalate
ND
5.6
1.6
ug/1
131-11-3
Dimethyl Phthalate
ND
5.6
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.6
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.6
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.6
0.66
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.6
0.78
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.6
1.1
ug/1
206-44-0
Fluoranthene
ND
5.6
0.56
ug/1
86-73-7
Fluorene
ND
5.6
0.56
ug/1
118-74-1
Hexachlorobenzene
ND
5.6
0.71
ug/1
87-68-3
Hexachlorobutadiene
ND
5.6
0.67
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.6
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.6
0.77
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.6
0.71
ug/1
78-59-1
Isophorone
ND
5.6
0.57
ug/1
90-12-0
1-Methylnaphthalene
ND
5.6
0.56
ug/1
91-57-6
2-Methylnaphthalene
ND
5.6
0.56
ug/1
91-20-3
Naphthalene
ND
5.6
0.56
ug/1
98-95-3
Nitrobenzene
ND
5.6
0.59
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.6
0.65
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.6
0.66
ug/1
85-01-8
Phenanthrene
ND
5.6
0.58
ug/1
129-00-0
Pyrene
ND
5.6
0.61
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
37%
14-67%
4165-62-2
Phenol-d5
27%
10-50%
118-79-6
2,4,6-Tribromophenol
82%
33-118%
4165-60-0
Nitrobenzene-d5
60%
42-108%
321-60-8
2-Fluorobiphenyl
67%
40-106%
1718-51-0
Terphenyl-dl4
72%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
00
■ 48 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
Client Sample ID: FULCHER CENTER
Lab Sample ID: FA28901-8 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 40.7 10
Barium 337 200
Cadmium < 5.0 5.0
Chromium 396 10
Lead 205 5.0
Mercury 0.70 0.50
Selenium < 10 10
Silver < 10 10
(1) Instrument QC Batch: MA12753
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29604
(4) Prep QC Batch: MP29610
RL = Reporting Limit
Page 1 of 1 w
Units DF Prep Analyzed By Method Prep Method
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/02/15
11/02/15
JL
SW846 7470A 1
SW846 7470A 3
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■ 49 of 143
■ ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: FULCHER DG
Lab Sample ID: FA28901-9 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36802.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
0.53
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 50 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
'lient Sample ID: FULCHER DG
,ab Sample ID: FA28901-9 Date Sampled: 10/27/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
18.6
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
79-125%
2037-26-5
Toluene-D8
94%
85-112%
460-00-4
4-Bromofluorobenzene
95%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 51 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: FULCHER DG
Lab Sample ID: FA28901-9 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684454.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run # 1 900 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
56
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.6
0.56
ug/1
95-57-8
2-Chlorophenol
ND
5.6
0.56
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.6
0.56
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.6
0.56
ug/1
51-28-5
2,4-Dinitrophenol
ND
28
5.6
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.4
ug/1
95-48-7
2-Methylphenol
ND
5.6
0.56
ug/1
3&4-Methylphenol
ND
5.6
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.6
0.98
ug/1
100-02-7
4-Nitrophenol
ND
28
5.6
ug/1
87-86-5
Pentachlorophenol
ND
28
5.6
ug/1
108-95-2
Phenol
ND
5.6
0.56
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.6
0.70
ug/1
83-32-9
Acenaphthene
ND
5.6
0.56
ug/1
208-96-8
Acenaphthylene
ND
5.6
0.56
ug/1
120-12-7
Anthracene
ND
5.6
0.56
ug/1
56-55-3
Benzo(a)anthracene
ND
5.6
0.56
ug/1
50-32-8
Benzo(a)pyrene
ND
5.6
0.56
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.6
0.64
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.6
0.73
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.6
0.76
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.6
0.71
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.6
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.6
0.56
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.6
0.70
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.6
0.77
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.6
0.56
ug/1
91-58-7
2-Chloronaphthalene
ND
5.6
0.56
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.6
0.64
ug/1
218-01-9
Chrysene
ND
5.6
0.56
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.6
0.75
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 52 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: FULCHER DG
gab Sample ID: FA28901-9 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.6
0.56
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.6
0.58
ug/1
84-66-2
Diethyl Phthalate
ND
5.6
1.6
ug/1
131-11-3
Dimethyl Phthalate
ND
5.6
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.6
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.6
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.6
0.65
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.6
0.77
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.6
1.1
ug/1
206-44-0
Fluoranthene
ND
5.6
0.56
ug/1
86-73-7
Fluorene
ND
5.6
0.56
ug/1
118-74-1
Hexachlorobenzene
ND
5.6
0.70
ug/1
87-68-3
Hexachlorobutadiene
ND
5.6
0.67
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.6
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.6
0.76
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.6
0.70
ug/1
78-59-1
Isophorone
ND
5.6
0.57
ug/1
90-12-0
1-Methylnaphthalene
ND
5.6
0.56
ug/1
91-57-6
2-Methylnaphthalene
ND
5.6
0.56
ug/1
91-20-3
Naphthalene
ND
5.6
0.56
ug/1
98-95-3
Nitrobenzene
ND
5.6
0.58
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.6
0.64
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.6
0.66
ug/1
85-01-8
Phenanthrene
ND
5.6
0.57
ug/1
129-00-0
Pyrene
ND
5.6
0.61
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
40%
14-67%
4165-62-2
Phenol-d5
29%
10-50%
118-79-6
2,4,6-Tribromophenol
89%
33-118%
4165-60-0
Nitrobenzene-d5
67%
42-108%
321-60-8
2-Fluorobiphenyl
75%
40-106%
1718-51-0
Terphenyl-dl4
79%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 53 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
Client Sample ID: FULCHER DG
Lab Sample ID: FA28901-9 Date Sampled: 10/27/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 14.5 10
Barium 228 200
Cadmium < 5.0 5.0
Chromium 220 10
Lead 75.7 5.0
Mercury < 0.50 0.50
Selenium < 10 10
Silver < 10 10
(1) Instrument QC Batch: MA12753
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29604
(4) Prep QC Batch: MP29610
RL = Reporting Limit
to
Page 1 of 1 P
Units DF Prep Analyzed By Method Prep Method
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/02/15
11/02/15
JL
SW846 7470A 1
SW846 7470A 3
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■ 54 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: BADCOCK
Lab Sample ID: FA28901-10 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36803.D 1 11/04/15 KM n/a n/a VP1367
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
3
0
■■ 55 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: BADCOCK
,ab Sample ID: FA28901-10 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
104%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
79-125%
2037-26-5
Toluene-D8
97%
85-112%
460-00-4
4-Bromofluorobenzene
97%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 56 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3612 TRENT
Lab Sample ID: FA28901-11 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P36920.D 1 11/09/15 KM n/a n/a VP1371
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/I
71-43-2
Benzene
ND
1.0
0.20
ug/I
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/I
75-25-2
Bromoform
ND
1.0
0.32
ug/I
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/I
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/I
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/I
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/I
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/I
75-00-3
Chloroethane
ND
2.0
0.50
ug/I
67-66-3
Chloroform
ND
1.0
0.30
ug/I
110-82-7
Cyclohexane
ND
1.0
0.20
ug/I
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/I
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/I
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/I
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/I
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/I
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/I
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/I
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/I
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/I
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/I
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/I
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/I
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/I
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/I
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/I
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/I
591-78-6
2-Hexanone
ND
10
2.0
ug/I
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/I
79-20-9
Methyl Acetate
ND
20
5.0
ug/I
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/I
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 57 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3612 TRENT
,ab Sample ID: FA28901-11 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
102%
83-118%
17060-07-0
1,2-Dichloroethane-D4
99%
79-125%
2037-26-5
Toluene-D8
98%
85-112%
460-00-4
4-Bromofluorobenzene
102%
83-118%
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■ 58 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3612 TRENT
Lab Sample ID: FA28901-11 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684455.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run # 1 900 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
56
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.6
0.56
ug/1
95-57-8
2-Chlorophenol
ND
5.6
0.56
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.6
0.56
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.6
0.56
ug/1
51-28-5
2,4-Dinitrophenol
ND
28
5.6
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.4
ug/1
95-48-7
2-Methylphenol
ND
5.6
0.56
ug/1
3&4-Methylphenol
ND
5.6
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.6
0.98
ug/1
100-02-7
4-Nitrophenol
ND
28
5.6
ug/1
87-86-5
Pentachlorophenol
ND
28
5.6
ug/1
108-95-2
Phenol
ND
5.6
0.56
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.6
0.70
ug/1
83-32-9
Acenaphthene
ND
5.6
0.56
ug/1
208-96-8
Acenaphthylene
ND
5.6
0.56
ug/1
120-12-7
Anthracene
ND
5.6
0.56
ug/1
56-55-3
Benzo(a)anthracene
ND
5.6
0.56
ug/1
50-32-8
Benzo(a)pyrene
ND
5.6
0.56
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.6
0.64
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.6
0.73
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.6
0.76
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.6
0.71
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.6
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.6
0.56
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.6
0.70
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.6
0.77
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.6
0.56
ug/1
91-58-7
2-Chloronaphthalene
ND
5.6
0.56
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.6
0.64
ug/1
218-01-9
Chrysene
ND
5.6
0.56
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.6
0.75
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 59 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
lient Sample ID: 3612 TRENT
gab Sample ID: FA28901-11 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.6
0.56
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.6
0.58
ug/1
84-66-2
Diethyl Phthalate
ND
5.6
1.6
ug/1
131-11-3
Dimethyl Phthalate
ND
5.6
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.6
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.6
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.6
0.65
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.6
0.77
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.6
1.1
ug/1
206-44-0
Fluoranthene
ND
5.6
0.56
ug/1
86-73-7
Fluorene
ND
5.6
0.56
ug/1
118-74-1
Hexachlorobenzene
ND
5.6
0.70
ug/1
87-68-3
Hexachlorobutadiene
ND
5.6
0.67
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.6
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.6
0.76
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.6
0.70
ug/1
78-59-1
Isophorone
ND
5.6
0.57
ug/1
90-12-0
1-Methylnaphthalene
ND
5.6
0.56
ug/1
91-57-6
2-Methylnaphthalene
ND
5.6
0.56
ug/1
91-20-3
Naphthalene
ND
5.6
0.56
ug/1
98-95-3
Nitrobenzene
ND
5.6
0.58
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.6
0.64
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.6
0.66
ug/1
85-01-8
Phenanthrene
ND
5.6
0.57
ug/1
129-00-0
Pyrene
ND
5.6
0.61
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
31%
14-67%
4165-62-2
Phenol-d5
24%
10-50%
118-79-6
2,4,6-Tribromophenol
66%
33-118%
4165-60-0
Nitrobenzene-d5
67%
42-108%
321-60-8
2-Fluorobiphenyl
69%
40-106%
1718-51-0
Terphenyl-dl4
53%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 60 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3700 TRENT
Lab Sample ID: FA28901-12 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36826.D 1 11/05/15 KM n/a n/a VP1368
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropan
b ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 61 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3700 TRENT
,ab Sample ID: FA28901-12 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/I
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/I
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/I
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
83-118%
17060-07-0
1,2-Dichloroethane-D4
104%
79-125%
2037-26-5
Toluene-D8
97%
85-112%
460-00-4
4-Bromofluorobenzene
95%
83-118%
(a) Combined vials 1,2 due to sediment.
(b) Associated CCV outside control limits.
Insufficient sample for reanalysis.
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 62 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3700 TRENT
Lab Sample ID: FA28901-12 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0684456.13 1 11/04/15 MV 11/02/15 OP58175 SL3741
Run #2
Initial Volume Final Volume
Run #1 800 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
63
13
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.3
0.63
ug/1
95-57-8
2-Chlorophenol
ND
6.3
0.63
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.3
0.63
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.3
0.63
ug/1
51-28-5
2,4-Dinitrophenol
ND
31
6.3
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
13
2.7
ug/1
95-48-7
2-Methylphenol
ND
6.3
0.63
ug/1
3&4-Methylphenol
ND
6.3
1.3
ug/1
88-75-5
2-Nitrophenol
ND
6.3
1.1
ug/1
100-02-7
4-Nitrophenol
ND
31
6.3
ug/1
87-86-5
Pentachlorophenol
ND
31
6.3
ug/1
108-95-2
Phenol
ND
6.3
0.63
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.3
0.79
ug/1
83-32-9
Acenaphthene
ND
6.3
0.63
ug/1
208-96-8
Acenaphthylene
ND
6.3
0.63
ug/1
120-12-7
Anthracene
ND
6.3
0.63
ug/1
56-55-3
Benzo(a)anthracene
ND
6.3
0.63
ug/1
50-32-8
Benzo(a)pyrene
ND
6.3
0.63
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.3
0.73
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.3
0.83
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.3
0.85
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.3
0.79
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.3
1.3
ug/1
106-47-8
4-Chloroaniline
ND
6.3
0.63
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.3
0.79
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.3
0.86
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.3
0.63
ug/1
91-58-7
2-Chloronaphthalene
ND
6.3
0.63
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.3
0.72
ug/1
218-01-9
Chrysene
ND
6.3
0.64
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.3
0.85
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
j
N
■ 63 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
lient Sample ID: 3700 TRENT
gab Sample ID: FA28901-12 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.3
0.63
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.3
0.65
ug/1
84-66-2
Diethyl Phthalate
ND
6.3
1.8
ug/1
131-11-3
Dimethyl Phthalate
ND
6.3
1.3
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.3
1.3
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.3
1.3
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.3
0.73
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.3
0.86
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.3
1.3
ug/1
206-44-0
Fluoranthene
ND
6.3
0.63
ug/1
86-73-7
Fluorene
ND
6.3
0.63
ug/1
118-74-1
Hexachlorobenzene
ND
6.3
0.79
ug/1
87-68-3
Hexachlorobutadiene
ND
6.3
0.75
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.3
1.3
ug/1
67-72-1
Hexachloroethane
ND
6.3
0.85
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.3
0.79
ug/1
78-59-1
Isophorone
ND
6.3
0.64
ug/1
90-12-0
1-Methylnaphthalene
ND
6.3
0.63
ug/1
91-57-6
2-Methylnaphthalene
ND
6.3
0.63
ug/1
91-20-3
Naphthalene
ND
6.3
0.63
ug/1
98-95-3
Nitrobenzene
ND
6.3
0.65
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.3
0.72
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.3
0.74
ug/1
85-01-8
Phenanthrene
ND
6.3
0.64
ug/1
129-00-0
Pyrene
ND
6.3
0.68
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
25%
14-67%
4165-62-2
Phenol-d5
21%
10-50%
118-79-6
2,4,6-Tribromophenol
50%
33-118%
4165-60-0
Nitrobenzene-d5
65%
42-108%
321-60-8
2-Fluorobiphenyl
66%
40-106%
1718-51-0
Terphenyl-dl4
64%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 64 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3702 TRENT
Lab Sample ID: FA28901-13 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36827.D 1 11/05/15 KM n/a n/a VP1368
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropan
b ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 65 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3702 TRENT
,ab Sample ID: FA28901-13 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/I
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/I
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/I
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
105%
79-125%
2037-26-5
Toluene-D8
94%
85-112%
460-00-4
4-Bromofluorobenzene
93%
83-118%
(a) Combined vials 1,3 due to sediment.
(b) Associated CCV outside control limits.
Insufficient sample for reanalysis.
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 66 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3702 TRENT
Lab Sample ID: FA28901-13 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a X043264.13 1 11/04/15 MV 11/04/15 OP58211 SX1956
Run #2
Initial Volume Final Volume
Run # 1 100 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
500
100
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
50
5.0
ug/1
95-57-8
2-Chlorophenol
ND
50
5.0
ug/1
120-83-2
2,4-Dichlorophenol
ND
50
5.0
ug/1
105-67-9
2,4-Dimethylphenol
ND
50
5.0
ug/1
51-28-5
2,4-Dinitrophenol
ND
250
50
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
100
21
ug/1
95-48-7
2-Methylphenol
ND
50
5.0
ug/1
3&4-Methylphenol
ND
50
10
ug/1
88-75-5
2-Nitrophenol
ND
50
8.8
ug/1
100-02-7
4-Nitrophenol
ND
250
50
ug/1
87-86-5
Pentachlorophenol
ND
250
50
ug/1
108-95-2
Phenol
ND
50
5.0
ug/1
88-06-2
2,4,6-Trichlorophenol
ND
50
6.3
ug/1
83-32-9
Acenaphthene
ND
50
5.0
ug/1
208-96-8
Acenaphthylene
ND
50
5.0
ug/1
120-12-7
Anthracene
ND
50
5.0
ug/1
56-55-3
Benzo(a)anthracene
ND
50
5.0
ug/1
50-32-8
Benzo(a)pyrene
ND
50
5.0
ug/1
205-99-2
Benzo(b)fluoranthene
ND
50
5.8
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
50
6.6
ug/1
207-08-9
Benzo(k)fluoranthene
ND
50
6.8
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
50
6.4
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
50
10
ug/1
106-47-8
4-Chloroaniline
ND
50
5.0
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
50
6.3
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
50
6.9
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
50
5.0
ug/1
91-58-7
2-Chloronaphthalene
ND
50
5.0
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
50
5.7
ug/1
218-01-9
Chrysene
ND
50
5.1
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
50
6.8
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
j
w
■■ 67 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: 3702 TRENT
gab Sample ID: FA28901-13 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
50
5.0
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
50
5.2
ug/1
84-66-2
Diethyl Phthalate
ND
50
14
ug/1
131-11-3
Dimethyl Phthalate
ND
50
10
ug/1
84-74-2
Di-n-butyl Phthalate
ND
50
10
ug/1
117-84-0
Di-n-octyl Phthalate
ND
50
10
ug/1
121-14-2
2,4-Dinitrotoluene
ND
50
5.8
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
50
6.9
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
50
10
ug/1
206-44-0
Fluoranthene
ND
50
5.0
ug/1
86-73-7
Fluorene
ND
50
5.0
ug/1
118-74-1
Hexachlorobenzene
ND
50
6.3
ug/1
87-68-3
Hexachlorobutadiene
ND
50
6.0
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
50
10
ug/1
67-72-1
Hexachloroethane
ND
50
6.8
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
50
6.3
ug/1
78-59-1
Isophorone
ND
50
5.1
ug/1
90-12-0
1-Methylnaphthalene
ND
50
5.0
ug/1
91-57-6
2-Methylnaphthalene
ND
50
5.0
ug/1
91-20-3
Naphthalene
ND
50
5.0
ug/1
98-95-3
Nitrobenzene
ND
50
5.2
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
50
5.8
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
50
5.9
ug/1
85-01-8
Phenanthrene
ND
50
5.1
ug/1
129-00-0
Pyrene
ND
50
5.5
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
30%
14-67%
4165-62-2
Phenol-d5
21%
10-50%
118-79-6
2,4,6-Tribromophenol
62%
33-118%
4165-60-0
Nitrobenzene-d5
63%
42-108%
321-60-8
2-Fluorobiphenyl
62%
40-106%
1718-51-0
Terphenyl-d14
69%
39-121%
(a) Elevated reporting limit due to matrix interference, dilution required during sample prep.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 68 of 143
E ACCUTEST
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3704 TRENT
Lab Sample ID: FA28901-14 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 P3692LD 1 11/09/15 KM n/a n/a VP1371
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
14.4
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
4.5
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
11.5
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 69 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3704 TRENT
,ab Sample ID: FA28901-14 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
2.7
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) 40.6
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
52.1
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
22.7
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
0.94
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
65.9
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
79-125%
2037-26-5
Toluene-D8
96%
85-112%
460-00-4
4-Bromofluorobenzene
119%
83-118%
J
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■ 70 of 143
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Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3704 TRENT
Lab Sample ID: FA28901-14 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 X043265.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
Run #2 X043276.13
4
11/05/15
MV
11/04/15
OP58211
SX1957
Initial Volume Final Volume
Run # 1 940 ml 1.0 ml
Run #2 940 ml 1.0 ml
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
53
11
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
5.3
0.53
ug/1
95-57-8
2-Chlorophenol
ND
5.3
0.53
ug/1
120-83-2
2,4-Dichlorophenol
ND
5.3
0.53
ug/1
105-67-9
2,4-Dimethylphenol
ND
5.3
0.53
ug/1
51-28-5
2,4-Dinitrophenol
ND
27
5.3
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
11
2.3
ug/1
95-48-7
2-Methylphenol
ND
5.3
0.53
ug/1
3&4-Methylphenol
ND
5.3
1.1
ug/1
88-75-5
2-Nitrophenol
ND
5.3
0.93
ug/1
100-02-7
4-Nitrophenol
ND
27
5.3
ug/1
87-86-5
Pentachlorophenol
ND
27
5.3
ug/1
108-95-2
Phenol
ND
5.3
0.53
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
5.3
0.67
ug/1
83-32-9
Acenaphthene
6.0
5.3
0.53
ug/1
208-96-8
Acenaphthylene
ND
5.3
0.53
ug/1
120-12-7
Anthracene
ND
5.3
0.53
ug/1
56-55-3
Benzo(a)anthracene
ND
5.3
0.53
ug/1
50-32-8
Benzo(a)pyrene
ND
5.3
0.53
ug/1
205-99-2
Benzo(b)fluoranthene
ND
5.3
0.62
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
5.3
0.70
ug/1
207-08-9
Benzo(k)fluoranthene
ND
5.3
0.73
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.3
0.68
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.3
1.1
ug/1
106-47-8
4-Chloroaniline
ND
5.3
0.53
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.3
0.67
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
5.3
0.73
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.3
0.54
ug/1
91-58-7
2-Chloronaphthalene
ND
5.3
0.53
ug/1
7005-72-3
4-ChlorophenylPhenyl Ether
ND
5.3
0.61
ug/1
218-01-9
Chrysene
ND
5.3
0.54
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
5.3
0.72
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
j
■■ 71 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: 3704 TRENT
gab Sample ID: FA28901-14 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
5.3
0.53
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
5.3
0.55
ug/1
84-66-2
Diethyl Phthalate
ND
5.3
1.5
ug/1
131-11-3
Dimethyl Phthalate
ND
5.3
1.1
ug/1
84-74-2
Di-n-butyl Phthalate
ND
5.3
1.1
ug/1
117-84-0
Di-n-octyl Phthalate
ND
5.3
1.1
ug/1
121-14-2
2,4-Dinitrotoluene
ND
5.3
0.62
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
5.3
0.73
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.3
1.1
ug/1
206-44-0
Fluoranthene
ND
5.3
0.53
ug/1
86-73-7
Fluorene
15.7
5.3
0.53
ug/1
118-74-1
Hexachlorobenzene
ND
5.3
0.67
ug/1
87-68-3
Hexachlorobutadiene
ND
5.3
0.64
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
5.3
1.1
ug/1
67-72-1
Hexachloroethane
ND
5.3
0.73
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
5.3
0.67
ug/1
78-59-1
Isophorone
ND
5.3
0.54
ug/1
90-12-0
1-Methylnaphthalene
137 a
21
2.1
ug/1
91-57-6
2-Methylnaphthalene
167 a
21
2.1
ug/1
91-20-3
Naphthalene
30.5
5.3
0.53
ug/1
98-95-3
Nitrobenzene
ND
5.3
0.56
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
5.3
0.62
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
5.3
0.63
ug/1
85-01-8
Phenanthrene
26.0
5.3
0.55
ug/1
129-00-0
Pyrene
1.0
5.3
0.58
ug/1 J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
30%
35%
14-67%
4165-62-2
Phenol-d5
24%
28%
10-50%
118-79-6
2,4,6-Tribromophenol
85%
68%
33-118%
4165-60-0
Nitrobenzene-d5
79%
87%
42-108%
321-60-8
2-Fluorobiphenyl
67%
76%
40-106%
1718-51-0
Terphenyl-dl4
69%
80%
39-121%
(a) Result is from Run# 2
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 72 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3706
Lab Sample ID: FA28901-15 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 P36847.D
2
11/06/15
KM
n/a
n/a
VP1369
Run #2 P36829.D
5
11/05/15
KM
n/a
n/a
VP1368
Purge Volume
Run # 1 5.0 ml
Run #2 5.0 ml
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
50
20
ug/1
71-43-2
Benzene
ND
2.0
0.40
ug/1
75-27-4
Bromodichloromethane
ND
2.0
0.43
ug/1
75-25-2
Bromoform
ND
2.0
0.65
ug/1
78-93-3
2-Butanone (MEK)
ND
10
2.3
ug/1
104-51-8
n-Butylbenzene
8.3
2.0
0.45
ug/1
75-15-0
Carbon Disulfide
ND
4.0
0.59
ug/1
56-23-5
Carbon Tetrachloride
ND
2.0
0.56
ug/1
108-90-7
Chlorobenzene
ND
2.0
0.40
ug/1
75-00-3
Chloroethane
ND
4.0
1.0
ug/1
67-66-3
Chloroform
ND
2.0
0.60
ug/1
110-82-7
Cyclohexane
ND
2.0
0.40
ug/1
124-48-1
Dibromochloromethane
ND
2.0
0.40
ug/1
96-12-8
1,2-Dibromo-3-chloropropan
a ND
4.0
1.2
ug/1
106-93-4
1,2-Dibromoethane
ND
4.0
0.83
ug/1
75-71-8
Dichlorodifluoromethane
ND
4.0
1.0
ug/1
95-50-1
1,2-Dichlorobenzene
ND
2.0
0.44
ug/1
541-73-1
1,3-Dichlorobenzene
ND
2.0
0.43
ug/1
106-46-7
1,4-Dichlorobenzene
ND
2.0
0.49
ug/1
75-34-3
1, 1 -Dichloroethane
ND
2.0
0.40
ug/1
107-06-2
1,2-Dichloroethane
ND
2.0
0.40
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
2.0
0.54
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
2.0
0.44
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
2.0
0.42
ug/1
78-87-5
1,2-Dichloropropane
ND
2.0
0.51
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
2.0
0.50
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
2.0
0.52
ug/1
100-41-4
Ethlbenzene
13.8
2.0
0.40
ug/1
591-78-6
2-Hexanone
ND
20
4.0
ug/1
98-82-8
Isopropylbenzene
9.2
2.0
0.40
ug/1
79-20-9
Methyl Acetate
ND
40
10
ug/1
74-83-9
Methyl Bromide
ND
4.0
1.0
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 73 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3706
,ab Sample ID: FA28901-15 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
4.0
1.0
ug/1
108-87-2
Methylcyclohexane
3.2
2.0
0.45
ug/1
75-09-2
Methylene Chloride
ND
10
4.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
10
2.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
2.0
0.60
ug/1
91-20-3
Naphthalene
154
10
2.0
ug/1
103-65-1
n-Propylbenzene
21.7
2.0
0.40
ug/1
100-42-5
Styrene
ND
2.0
0.56
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
2.0
0.45
ug/1
127-18-4
Tetrachloroethylene
ND
2.0
0.65
ug/1
108-88-3
Toluene
ND
2.0
0.80
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
2.0
1.0
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
2.0
0.51
ug/1
79-00-5
1,1,2-Trichloroethane
ND
2.0
0.63
ug/1
79-01-6
Trichloroethylene
ND
2.0
0.43
ug/1
75-69-4
Trichlorofluoromethane
ND
4.0
1.0
ug/1
95-63-6
1,2,4-Trimethylbenzene
147 b
10
1.0
ug/1
108-67-8
1,3,5-Trimethylbenzene
42.5
4.0
0.45
ug/1
75-01-4
Vinyl Chloride
ND
2.0
0.50
ug/1
1330-20-7
Xylene (total)
7.9
6.0
1.0
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
99%
98%
79-125%
2037-26-5
Toluene-D8
96%
96%
85-112%
460-00-4
4-Bromofluorobenzene
100%
93%
83-118%
(a) Associated CCV outside control limits.
(b) Result is from Run# 2
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■ 74 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3706
Lab Sample ID: FA28901-15 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 X043266.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
Run #2 X043277.13
4
11/05/15
MV
11/04/15
OP58211
SX1957
Initial Volume Final Volume
Run #1 820 ml 1.0 ml
Run #2 820 ml 1.0 ml
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
61
12
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.1
0.61
ug/1
95-57-8
2-Chlorophenol
ND
6.1
0.61
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.1
0.61
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.1
0.61
ug/1
51-28-5
2,4-Dinitrophenol
ND
30
6.1
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
12
2.6
ug/1
95-48-7
2-Methylphenol
ND
6.1
0.61
ug/1
3&4-Methylphenol
ND
6.1
1.2
ug/1
88-75-5
2-Nitrophenol
ND
6.1
1.1
ug/1
100-02-7
4-Nitrophenol
ND
30
6.1
ug/1
87-86-5
Pentachlorophenol
ND
30
6.1
ug/1
108-95-2
Phenol
ND
6.1
0.61
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.1
0.77
ug/1
83-32-9
Acenaphthene
25.9
6.1
0.61
ug/1
208-96-8
Acenaphthylene
ND
6.1
0.61
ug/1
120-12-7
Anthracene
6.3
6.1
0.61
ug/1
56-55-3
Benzo(a)anthracene
ND
6.1
0.61
ug/1
50-32-8
Benzo(a)pyrene
ND
6.1
0.61
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.1
0.71
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.1
0.80
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.1
0.83
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.1
0.77
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.1
1.2
ug/1
106-47-8
4-Chloroaniline
ND
6.1
0.61
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.1
0.77
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.1
0.84
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.1
0.61
ug/1
91-58-7
2-Chloronaphthalene
ND
6.1
0.61
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.1
0.70
ug/1
218-01-9
Chrysene
ND
6.1
0.62
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.1
0.83
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
j
■■ 75 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
lient Sample ID: 3706
gab Sample ID: FA28901-15 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.1
0.61
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.1
0.64
ug/1
84-66-2
Diethyl Phthalate
ND
6.1
1.7
ug/1
131-11-3
Dimethyl Phthalate
ND
6.1
1.2
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.1
1.2
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.1
1.2
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.1
0.71
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.1
0.84
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.1
1.2
ug/1
206-44-0
Fluoranthene
1.7
6.1
0.61
ug/1 J
86-73-7
Fluorene
31.7
6.1
0.61
ug/1
118-74-1
Hexachlorobenzene
ND
6.1
0.77
ug/1
87-68-3
Hexachlorobutadiene
ND
6.1
0.73
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.1
1.2
ug/1
67-72-1
Hexachloroethane
ND
6.1
0.83
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.1
0.77
ug/1
78-59-1
Isophorone
ND
6.1
0.62
ug/1
90-12-0
1-Methylnaphthalene
328 a
24
2.4
ug/1
91-57-6
2-Methylnaphthalene
447 a
24
2.4
ug/1
91-20-3
Naphthalene
147 a
24
2.4
ug/1
98-95-3
Nitrobenzene
ND
6.1
0.64
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.1
0.71
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.1
0.72
ug/1
85-01-8
Phenanthrene
56.3
6.1
0.63
ug/1
129-00-0
Pyrene
3.7
6.1
0.67
ug/1 J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
46%
52%
14-67%
4165-62-2
Phenol-d5
33%
41%
10-50%
118-79-6
2,4,6-Tribromophenol
115%
92%
33-118%
4165-60-0
Nitrobenzene-d5
71%
89%
42-108%
321-60-8
2-Fluorobiphenyl
70%
86%
40-106%
1718-51-0
Terphenyl-dl4
77%
93%
39-121%
(a) Result is from Run# 2
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 76 of 143
M ACCUTEST
FA28901 LA...A-1-

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3708
Lab Sample ID: FA28901-16 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P36830.D 1 11/05/15 KM n/a n/a VP1368
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropan
b ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 77 of 143
ACCUTEST
FA28907

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3708
,ab Sample ID: FA28901-16 Date Sampled: 10/28/15
Ratrix: AQ - Ground Water Date Received: 10/29/ 15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/I
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/I
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/I
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
97%
79-125%
2037-26-5
Toluene-D8
96%
85-112%
460-00-4
4-Bromofluorobenzene
96%
83-118%
(a) Combined vials 1,2 due to sediment
(b) Associated CCV outside control limits.
Insufficient sample for reanalysis.
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■ 78 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3708
Lab Sample ID: FA28901-16 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X043267.13 1 11/04/15 MV 11/04/15 OP58211 SX1956
Run #2
Initial Volume Final Volume
Run #1 760 ml 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
66
13
ug/1
59-50-7
4-Chloro-3-methyl Phenol
ND
6.6
0.66
ug/1
95-57-8
2-Chlorophenol
ND
6.6
0.66
ug/1
120-83-2
2,4-Dichlorophenol
ND
6.6
0.66
ug/1
105-67-9
2,4-Dimethylphenol
ND
6.6
0.66
ug/1
51-28-5
2,4-Dinitrophenol
ND
33
6.6
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
13
2.8
ug/1
95-48-7
2-Methylphenol
ND
6.6
0.66
ug/1
3&4-Methylphenol
ND
6.6
1.3
ug/1
88-75-5
2-Nitrophenol
ND
6.6
1.2
ug/1
100-02-7
4-Nitrophenol
ND
33
6.6
ug/1
87-86-5
Pentachlorophenol
ND
33
6.6
ug/1
108-95-2
Phenol
ND
6.6
0.66
ug/1
88-06-2
2, 4, 6-Trichlorophenol
ND
6.6
0.83
ug/1
83-32-9
Acenaphthene
ND
6.6
0.66
ug/1
208-96-8
Acenaphthylene
ND
6.6
0.66
ug/1
120-12-7
Anthracene
ND
6.6
0.66
ug/1
56-55-3
Benzo(a)anthracene
ND
6.6
0.66
ug/1
50-32-8
Benzo(a)pyrene
ND
6.6
0.66
ug/1
205-99-2
Benzo(b)fluoranthene
ND
6.6
0.76
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
6.6
0.87
ug/1
207-08-9
Benzo(k)fluoranthene
ND
6.6
0.90
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
6.6
0.84
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
6.6
1.3
ug/1
106-47-8
4-Chloroaniline
ND
6.6
0.66
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
6.6
0.83
ug/1
111-44-4
bis(2-Chloroethyl)ether
ND
6.6
0.91
ug/1
108-60-1
bis(2-Chloroisopropyl)ether
ND
6.6
0.66
ug/1
91-58-7
2-Chloronaphthalene
ND
6.6
0.66
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
6.6
0.75
ug/1
218-01-9
Chrysene
ND
6.6
0.67
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
6.6
0.89
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 79 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
lient Sample ID: 3708
gab Sample ID: FA28901-16 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Method: SW846 8270D SW846 3510C Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
ABN Special List
CAS No.
Compound
Result
RL
MDL
Units Q
132-64-9
Dibenzofuran
ND
6.6
0.66
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
6.6
0.69
ug/1
84-66-2
Diethyl Phthalate
ND
6.6
1.9
ug/1
131-11-3
Dimethyl Phthalate
ND
6.6
1.3
ug/1
84-74-2
Di-n-butyl Phthalate
ND
6.6
1.3
ug/1
117-84-0
Di-n-octyl Phthalate
ND
6.6
1.3
ug/1
121-14-2
2,4-Dinitrotoluene
ND
6.6
0.77
ug/1
606-20-2
2, 6-Dinitrotoluene
ND
6.6
0.91
ug/1
117-81-7
bis(2-Ethylhexyl)phthalate
ND
6.6
1.3
ug/1
206-44-0
Fluoranthene
ND
6.6
0.66
ug/1
86-73-7
Fluorene
ND
6.6
0.66
ug/1
118-74-1
Hexachlorobenzene
ND
6.6
0.83
ug/1
87-68-3
Hexachlorobutadiene
ND
6.6
0.79
ug/1
77-47-4
Hexachlorocyclopentadiene
ND
6.6
1.3
ug/1
67-72-1
Hexachloroethane
ND
6.6
0.90
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
6.6
0.83
ug/1
78-59-1
Isophorone
ND
6.6
0.67
ug/1
90-12-0
1-Methylnaphthalene
ND
6.6
0.66
ug/1
91-57-6
2-Methylnaphthalene
ND
6.6
0.66
ug/1
91-20-3
Naphthalene
ND
6.6
0.66
ug/1
98-95-3
Nitrobenzene
ND
6.6
0.69
ug/1
621-64-7
N-Nitrosodi-n-propylamine
ND
6.6
0.76
ug/1
86-30-6
N-Nitrosodiphenylamine
ND
6.6
0.78
ug/1
85-01-8
Phenanthrene
ND
6.6
0.68
ug/1
129-00-0
Pyrene
ND
6.6
0.72
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
38%
14-67%
4165-62-2
Phenol-d5
29%
10-50%
118-79-6
2,4,6-Tribromophenol
65%
33-118%
4165-60-0
Nitrobenzene-d5
57%
42-108%
321-60-8
2-Fluorobiphenyl
59%
40-106%
1718-51-0
Terphenyl-dl4
78%
39-121%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■ 80 of 143
E ACCUTEST
FA28901

Accutest Laboratories
Report of Analysis
Client Sample ID: BACKGROUND
Lab Sample ID: FA28901-17 Date Sampled: 10/28/15
Matrix: AQ - Ground Water Date Received: 10/29/ 15
Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Total Metals Analysis
Analyte Result RL
Arsenic 320 100
Barium 2290 2000
Cadmium < 50 50
Chromium 2310 100
Lead 1380 50
Mercury 1.6 0.50
Selenium < 100 100
Silver < 100 100
(1) Instrument QC Batch: MA12755
(2) Instrument QC Batch: MA12757
(3) Prep QC Batch: MP29608
(4) Prep QC Batch: MP29610
RL = Reporting Limit
Page 1 of 1
Units DF Prep Analyzed By Method Prep Method
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
JL
SW846 7470A 1
SW846 7470A 3
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
ug/l
1
11/03/15
11/03/15
LM
SW846 6010C 2
SW846 3010A 4
■■ 81 of 143
ACCUTEST
FA28907

Section 4
Southeast
E ACCUTEST
L A B O RAT D R I ES
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
■ ,i 82 of 143
E ACCUTEST
FA28901 `"a°RA-1 -

No Accutest Laboratories Southeast FAZ8901
Chain of Custody Accutest JOB # PAGE EAOF a
CC UTEST 4405 Vineland Road, Suite C-15„ FI Orlando, 32811
L A e o R A T o R I e e 1 LL. 4V -4LJ-tl /W
www,accutest.com
Acoutest Quote
Client/Reponfing Information
Pro ect Intonation[
Analytical
information
Matdx C es
Company Name R
Prolect Name: �1� GlenN ltr n
t
i'p
J
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eW- Drlel&g Water
eW-Ground Weler
ww- water
5w - Sudece water
80-9n11
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a -oil
LIO. Other Liquid
AIR - Air
SOL-O thheer S.Ild
Add..
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(Ate. oA
CI a state G >
city Afe state NC
Proled Contact J T4e�e S E.sil
ft)..t #
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Fax #
Sampler(.) Name(.) (Prim dl -
Client Purchase Order # 5
se�tesa
Field ID / Point of Collection
Oe
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Comments
/Remarks
Approved By: ! Rush Code
10 Days Standard
❑ 7Day RUSH
❑ S Day RUSH ._
❑ 3 Day EMERGENCY
❑ 2 Day EMERGENCY
© 1 Day EMERGENCY --„_,=
❑ OTHER _.._—
Emergency or Rush T/A Data Available VIA Email or Lablink
❑ COMMERCIAL"A" (RESULTS ONLY)
(�/�� �T T
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each chance cossession.
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RelinquishI� by Sa er:
Date Time:
Received Byy RelinAlllshed
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Received By: Relinquished
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Received By:
8
Lab Use Only: Custody Seal in Place: Y N TernBlank Provided: Y N Preserved where Applicable: Y N Total # of Coolers: Cooler Temperature s Celsius: 3.1 .0 z_
FA28901: Chain of Custody
Page 1 of 4
0
■ ,i 83 of 143
ACCUTEST
FA28901 `....A OR15

00
■.4cc
Client ! Re
Company Name
Add —
CI
Prgeet Contact
Phone#
Swplm(9) Name(a) (Pdnted)
A.Weet
Semple #
Fleli
17
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❑ 10 Days Slender
❑ 7 Day RUSH
❑ 5 Day RUSH
❑ 3 Day EMERGEI
❑ 2 Day EMERGEI
❑ 1 bey EMERGEI
❑ OTHER'
Emergency or Ri
Relingaigped by pl
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Relinquished by:
5
Lab Use Only: Custt
FA28901: Chain of Custody
Page 2 of 4
■ ,i 84 of 143
ACC UTEBT
FA28901 `"°°"A— I..

ACCUTEST LABORATORIES SAMPLE.RECEIPT CONFIRMATION
ACCUTEST'S JOB NUMBER: E y- A Z?j 4 d (
CLIENT: PROJECT: 3
DATE/TIME RECEIVED: (�-2`t-15- Oq'.3�
(MM/DD/YY 24:00) NUMBER OF COOLERS RECEIVED:
METHOD OF DELIVERY: AER UPS
ACCUTEST COURIER DELIVERY OTHER:
AHtBILLNUMBERS: 043 0172-
l 57957, g?36 /ZS53 2i94 OEi/ z
COOLER INFORMATION
TEMPERATURE INFORMATION
CUSTODY SEAL NOT PRESENT OR NOT INTACT
IR THERM ID I CORR. FACTOR
CHAIN OF CUSTODY NOT RECEIVED (COC)
OBSERVED TEMPS: �. 3. ° 3. Z
ANALYSIS REQUESTED is UNCLEAR OR MISSING
CORRECTED TEMPS: .0 3:0
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
SAMPLE INFORMATION
TEMPERATURE CRITERIA NOT MET
INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
TRIP BLANK INFORMATION
INSUFFICIENT VOLUME FOR ANALYSIS
TRIP BLANK PROVIDED
DATES/TIMES ON COC DO NOT MATCH SAMPLE LABEL
TRIP BLANK NOT PROVIDED
ID'S ON COC DO NOT MATCH LABEL
TRIP BLANK NOT ON COC
VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
TRIP BLANK INTACT
BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
TRIP BLANK NOT INTACT
5<O
BOTTLES RECEIVED FOR ANALYSIS REQUESTED
RECEIVED WATER TRIP BLANK
UNCLEAR FILTERING OR COMPOSITING INSTRUCTIONS
RECI' 'NTn SOIL, TRIP BLANK
SAMPLE CONTAINER(S) RECEIVED -BROKEN
5035 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
MISC. INFORMATION
BULK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS
NUMBER OF ENCORES ? 25-GRAM 5 GRAM
% SOLIDS JAR NOT RECEIVED
NUMBER OF 5035 FIELD KITS ?
RESIDUAL CHLORINE PRESENT LOT#
NUMBER OF LAB FILTERED METALS ?
(APPLICABLE TO EPA 600 SERIES OR NORTH CAROLINA ORGANICS)
pH PAPER LOT#S WIDI HC 131225
NARROW RANGE 036I33 OTHER (specify) 405 23p0I0
SUMMARY OF COMMENTS: S,1tlpL�
Flu :j. & ( ,tA, N p6 Qom; s
c'k06W(
BD-,nZ r_ A, �E1,4 OUV,". —
TECHNICIAN SIGNATURE/DATE l�IH t<J'�C�r /U 3G-IS REVIEWER SIGNATURE/DA
NF 10114 YELLOWSHEET110514.Xis
FA28901: Chain of Custody
Page 3 of 4
■ ,i 85 of 143
E ACCUTEBT
FA28901 `..... I..

a
THU - 29 OCT 3.0w .
.Z1 8053 9196 0864 STANDARD OVERNIDHT
• C 0662
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FA289O1: Chain of Custody
Page 4 of 4
■■ 86 of 143
ACCUTEST
FA28901 LA ... ATO""`

Section 5
Southeast
ACCUTECT
L A H 0 R A T O R i E 5
GUMS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
■ ,i 87 of 143
E ACCUTEBT
FA28901 `..... I..

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1367-MB
P36783.D
1
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples:
Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/l
75-25-2
Bromoform
ND
1.0
0.32
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.0
ug/l
■ 88 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1367-MB
P36783.D
1
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/l
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/l
100-42-5
Styrene
ND
1.0
0.28
ug/l
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.22
ug/l
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.26
ug/l
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/l
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/l
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/l
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
98%
83-118%
17060-07-0
1,2-Dichloroethane-D4
98%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
101%
83-118%
■ 89 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1368-MB
P36814.D
1
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-12, FA28901-13, FA28901-15, FA28901-16
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/l
75-25-2
Bromoform
ND
1.0
0.32
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.0
ug/l
■ 90 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1368-MB
P36814.D
1
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples:
FA28901-12, FA28901-13, FA28901-15, FA28901-16
Method: SW846 8260B
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/l
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/l
100-42-5
Styrene
ND
1.0
0.28
ug/l
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.22
ug/l
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.26
ug/l
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/l
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/l
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/l
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
103%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
95%
83-118%
■■ 91 of 143
ACCUTEST
FA28907

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1369-MB
P36846.D
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-15
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/l
75-25-2
Bromoform
ND
1.0
0.32
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.0
ug/l
■■ 92 of 143
ACCUTEST
FA28907

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1369-MB
P36846.D
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples:
FA28901-15
Method: SW846 8260B
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/l
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/l
100-42-5
Styrene
ND
1.0
0.28
ug/l
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.22
ug/l
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.26
ug/l
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/l
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/l
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
98%
79-125%
2037-26-5
Toluene-D8
97%
85-112%
460-00-4
4-Bromofluorobenzene
97%
83-118%
■ 93 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1371-MB
P36914.D
1
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-11, FA28901-14
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/l
75-25-2
Bromoform
ND
1.0
0.32
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.0
ug/l
■ 94 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1371-MB
P36914.D
1
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples:
FA28901-11, FA28901-14
Method: SW846 8260B
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/l
91-20-3
Naphthalene
ND
5.0
1.0
ug/l
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/l
100-42-5
Styrene
ND
1.0
0.28
ug/l
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.22
ug/l
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.26
ug/l
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/l
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/l
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/l
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
97%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
102%
83-118%
■■ 95 of 143
ACCUTEST
FA28907

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1367-BS
P36782.D
1
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples:
Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
Spike BSP BSP
CAS No. Compound ug/l ug/l % Limits
67-64-1
Acetone
125
115
92
50-147
71-43-2
Benzene
25
23.2
93
81-122
75-27-4
Bromodichloromethane
25
23.9
96
79-123
75-25-2
Bromoform
25
22.2
89
66-123
78-93-3
2-Butanone (MEK)
125
116
93
56-143
104-51-8
n-Butylbenzene
25
24.9
100
79-126
75-15-0
Carbon Disulfide
25
21.7
87
66-148
56-23-5
Carbon Tetrachloride
25
26.3
105
76-136
108-90-7
Chlorobenzene
25
24.8
99
82-124
75-00-3
Chloroethane
25
28.1
112
62-144
67-66-3
Chloroform
25
24.0
96
80-124
110-82-7
Cyclohexane
25
25.8
103
73-138
124-48-1
Dibromochloromethane
25
23.0
92
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
20.7
83
64-123
106-93-4
1,2-Dibromoethane
25
23.6
94
75-120
75-71-8
Dichlorodifluoromethane
25
32.0
128
42-167
95-50-1
1,2-Dichlorobenzene
25
23.9
96
82-124
541-73-1
1,3-Dichlorobenzene
25
25.2
101
84-125
106-46-7
1,4-Dichlorobenzene
25
24.1
96
78-120
75-34-3
1, 1 -Dichloroethane
25
25.1
100
81-122
107-06-2
1,2-Dichloroethane
25
23.0
92
75-125
75-35-4
1, 1 -Dichloroethylene
25
24.7
99
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
22.3
89
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
25.3
101
76-127
78-87-5
1,2-Dichloropropane
25
24.1
96
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
24.0
96
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
24.4
98
80-120
100-41-4
Ethylbenzene
25
24.9
100
81-121
591-78-6
2-Hexanone
125
109
87
61-129
98-82-8
Isopropylbenzene
25
25.9
104
83-132
79-20-9
Methyl Acetate
125
107
86
65-126
74-83-9
Methyl Bromide
25
26.8
107
59-143
74-87-3
Methyl Chloride
25
28.0
112
50-159
108-87-2
Methylcyclohexane
25
27.0
108
76-129
75-09-2
Methylene Chloride
25
23.1
92
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
112
90
66-122
* = Outside of Control Limits.
■■ 96 of 143
ACCUTEST
FA28907

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1367-BS
P36782.D
1
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
Spike
BSP
BSP
CAS No.
Compound
ug/1
ug/l
%
Limits
1634-04-4
Methyl Tert Butyl Ether
25
22.5
90
72-117
91-20-3
Naphthalene
25
23.1
92
63-132
103-65-1
n-Propylbenzene
25
26.3
105
82-133
100-42-5
Styrene
25
24.1
96
78-119
79-34-5
1,1,2,2-Tetrachloroethane
25
21.8
87
72-120
127-18-4
Tetrachloroethylene
25
26.8
107
76-135
108-88-3
Toluene
25
24.6
98
80-120
120-82-1
1,2,4-Trichlorobenzene
25
22.4
90
73-129
71-55-6
1, 1, 1-Trichloroethane
25
23.9
96
75-130
79-00-5
1,1,2-Trichloroethane
25
22.0
88
76-119
79-01-6
Trichloroethylene
25
24.3
97
81-126
75-69-4
Trichlorofluoromethane
25
31.3
125
71-156
95-63-6
1,2,4-Trimethylbenzene
25
24.3
97
79-120
108-67-8
1,3,5-Trimethylbenzene
25
24.1
96
79-120
75-01-4
Vinyl Chloride
25
29.7
119
69-159
1330-20-7
Xylene (total)
75
74.9
100
80-126
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
96%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
79-125%
2037-26-5
Toluene-D8
101%
85-112%
460-00-4
4-Bromofluorobenzene
100%
83-118%
* = Outside of Control Limits.
■■ 97 of 143
ACCUTEST
FA28907

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1368-BS
P36813.D
1
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples:
FA28901-12, FA28901-13, FA28901-15, FA28901-16
Spike BSP BSP
CAS No. Compound ug/l ug/l % Limits
67-64-1
Acetone
125
110
88
50-147
71-43-2
Benzene
25
23.5
94
81-122
75-27-4
Bromodichloromethane
25
24.4
98
79-123
75-25-2
Bromoform
25
21.9
88
66-123
78-93-3
2-Butanone (MEK)
125
109
87
56-143
104-51-8
n-Butylbenzene
25
23.6
94
79-126
75-15-0
Carbon Disulfide
25
22.1
88
66-148
56-23-5
Carbon Tetrachloride
25
28.0
112
76-136
108-90-7
Chlorobenzene
25
23.9
96
82-124
75-00-3
Chloroethane
25
28.7
115
62-144
67-66-3
Chloroform
25
24.1
96
80-124
110-82-7
Cyclohexane
25
24.6
98
73-138
124-48-1
Dibromochloromethane
25
22.6
90
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
19.4
78
64-123
106-93-4
1,2-Dibromoethane
25
22.3
89
75-120
75-71-8
Dichlorodifluoromethane
25
35.0
140
42-167
95-50-1
1,2-Dichlorobenzene
25
23.7
95
82-124
541-73-1
1,3-Dichlorobenzene
25
24.7
99
84-125
106-46-7
1,4-Dichlorobenzene
25
24.1
96
78-120
75-34-3
1, 1 -Dichloroethane
25
25.2
101
81-122
107-06-2
1,2-Dichloroethane
25
23.6
94
75-125
75-35-4
1, 1 -Dichloroethylene
25
25.3
101
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
22.4
90
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
24.9
100
76-127
78-87-5
1,2-Dichloropropane
25
23.5
94
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
23.4
94
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
23.2
93
80-120
100-41-4
Ethylbenzene
25
24.1
96
81-121
591-78-6
2-Hexanone
125
98.2
79
61-129
98-82-8
Isopropylbenzene
25
25.4
102
83-132
79-20-9
Methyl Acetate
125
105
84
65-126
74-83-9
Methyl Bromide
25
26.9
108
59-143
74-87-3
Methyl Chloride
25
29.8
119
50-159
108-87-2
Methylcyclohexane
25
27.3
109
76-129
75-09-2
Methylene Chloride
25
23.7
95
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
102
82
66-122
* = Outside of Control Limits.
Method: SW846 8260B
■ 98 of 143
E ACC UTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1368-BS
P36813.D
1
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples:
FA28901-12, FA28901-13, FA28901-15, FA28901-16
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
1634-04-4
Methyl Tert Butyl Ether
25
22.8
91
72-117
91-20-3
Naphthalene
25
22.4
90
63-132
103-65-1
n-Propylbenzene
25
25.0
100
82-133
100-42-5
Styrene
25
23.5
94
78-119
79-34-5
1,1,2,2-Tetrachloroethane
25
20.0
80
72-120
127-18-4
Tetrachloroethylene
25
27.4
110
76-135
108-88-3
Toluene
25
23.9
96
80-120
120-82-1
1,2,4-Trichlorobenzene
25
22.5
90
73-129
71-55-6
1, 1, 1-Trichloroethane
25
24.9
100
75-130
79-00-5
1,1,2-Trichloroethane
25
21.0
84
76-119
79-01-6
Trichloroethylene
25
24.9
100
81-126
75-69-4
Trichlorofluoromethane
25
34.0
136
71-156
95-63-6
1,2,4-Trimethylbenzene
25
23.3
93
79-120
108-67-8
1,3,5-Trimethylbenzene
25
23.3
93
79-120
75-01-4
Vinyl Chloride
25
31.0
124
69-159
1330-20-7
Xylene (total)
75
72.4
97
80-126
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
102%
83-118%
17060-07-0
1,2-Dichloroethane-D4
97%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
94%
83-118%
* = Outside of Control Limits.
Method: SW846 8260B
■ 99 of 143
E ACC UTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1369-BS
P36845.D
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-15
CAS No. Compound
Spike BSP BSP
ug/l ug/l % Limits
67-64-1
Acetone
125
115
92
50-147
71-43-2
Benzene
25
25.7
103
81-122
75-27-4
Bromodichloromethane
25
26.4
106
79-123
75-25-2
Bromoform
25
25.3
101
66-123
78-93-3
2-Butanone (MEK)
125
104
83
56-143
104-51-8
n-Butylbenzene
25
26.6
106
79-126
75-15-0
Carbon Disulfide
25
24.3
97
66-148
56-23-5
Carbon Tetrachloride
25
30.8
123
76-136
108-90-7
Chlorobenzene
25
26.7
107
82-124
75-00-3
Chloroethane
25
26.8
107
62-144
67-66-3
Chloroform
25
26.8
107
80-124
110-82-7
Cyclohexane
25
27.4
110
73-138
124-48-1
Dibromochloromethane
25
25.3
101
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
20.7
83
64-123
106-93-4
1,2-Dibromoethane
25
25.6
102
75-120
75-71-8
Dichlorodifluoromethane
25
31.2
125
42-167
95-50-1
1,2-Dichlorobenzene
25
26.1
104
82-124
541-73-1
1,3-Dichlorobenzene
25
27.6
110
84-125
106-46-7
1,4-Dichlorobenzene
25
26.3
105
78-120
75-34-3
1, 1 -Dichloroethane
25
28.1
112
81-122
107-06-2
1,2-Dichloroethane
25
25.4
102
75-125
75-35-4
1, 1 -Dichloroethylene
25
27.8
ill
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
24.1
96
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
28.0
112
76-127
78-87-5
1,2-Dichloropropane
25
25.6
102
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
26.2
105
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
26.0
104
80-120
100-41-4
Ethylbenzene
25
27.1
108
81-121
591-78-6
2-Hexanone
125
98.2
79
61-129
98-82-8
Isopropylbenzene
25
28.6
114
83-132
79-20-9
Methyl Acetate
125
116
93
65-126
74-83-9
Methyl Bromide
25
25.6
102
59-143
74-87-3
Methyl Chloride
25
25.8
103
50-159
108-87-2
Methylcyclohexane
25
29.8
119
76-129
75-09-2
Methylene Chloride
25
25.6
102
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
101
81
66-122
* = Outside of Control Limits.
■ 100 of 143
E ACC UTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1369-BS
P36845.D
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-15
CAS No. Compound
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
79-34-5
1,1,2,2-Tetrachloroethane
127-18-4
Tetrachloroethylene
108-88-3
Toluene
120-82-1
1,2,4-Trichlorobenzene
71-55-6
1, 1, 1-Trichloroethane
79-00-5
1,1,2-Trichloroethane
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
108-67-8
1,3,5-Trimethylbenzene
75-01-4
Vinyl Chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1, 2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
* = Outside of Control Limits.
Spike
BSP
BSP
ug/l
ug/l
%
Limits
25
24.6
98
72-117
25
24.3
97
63-132
25
28.1
112
82-133
25
26.1
104
78-119
25
22.3
89
72-120
25
30.1
120
76-135
25
27.0
108
80-120
25
24.7
99
73-129
25
27.1
108
75-130
25
23.7
95
76-119
25
27.4
110
81-126
25
31.1
124
71-156
25
25.8
103
79-120
25
27.5
110
69-159
75
81.8
109
80-126
BSP Limits
101%
83-118%
97%
79-125%
100%
85-112%
96%
83-118%
■■ 101 of 143
ACCUTEST
FA28907

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1371-BS
P36913.D
1
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-11, FA28901-14
CAS No. Compound
Spike BSP BSP
ug/1 ug/1 % Limits
67-64-1
Acetone
125
134
107
50-147
71-43-2
Benzene
25
26.2
105
81-122
75-27-4
Bromodichloromethane
25
27.5
110
79-123
75-25-2
Bromoform
25
27.1
108
66-123
78-93-3
2-Butanone (MEK)
125
122
98
56-143
104-51-8
n-Butylbenzene
25
27.0
108
79-126
75-15-0
Carbon Disulfide
25
23.9
96
66-148
56-23-5
Carbon Tetrachloride
25
27.3
109
76-136
108-90-7
Chlorobenzene
25
26.2
105
82-124
75-00-3
Chloroethane
25
30.4
122
62-144
67-66-3
Chloroform
25
26.5
106
80-124
110-82-7
Cyclohexane
25
27.5
110
73-138
124-48-1
Dibromochloromethane
25
27.1
108
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
25.3
101
64-123
106-93-4
1,2-Dibromoethane
25
26.5
106
75-120
75-71-8
Dichlorodifluoromethane
25
33.3
133
42-167
95-50-1
1,2-Dichlorobenzene
25
26.7
107
82-124
541-73-1
1,3-Dichlorobenzene
25
26.4
106
84-125
106-46-7
1,4-Dichlorobenzene
25
26.4
106
78-120
75-34-3
1, 1 -Dichloroethane
25
27.5
110
81-122
107-06-2
1,2-Dichloroethane
25
25.7
103
75-125
75-35-4
1, 1 -Dichloroethylene
25
27.5
110
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
25.3
101
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
29.2
117
76-127
78-87-5
1,2-Dichloropropane
25
25.7
103
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
26.2
105
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
28.4
114
80-120
100-41-4
Ethylbenzene
25
26.6
106
81-121
591-78-6
2-Hexanone
125
123
98
61-129
98-82-8
Isopropylbenzene
25
27.5
110
83-132
79-20-9
Methyl Acetate
125
125
100
65-126
74-83-9
Methyl Bromide
25
26.5
106
59-143
74-87-3
Methyl Chloride
25
29.1
116
50-159
108-87-2
Methylcyclohexane
25
29.7
119
76-129
75-09-2
Methylene Chloride
25
27.3
109
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
125
100
66-122
* = Outside of Control Limits.
■■ 102 of 143
M ACCUTEST
FA28901 LA...A - 1-

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1371-BS
P36913.D
1
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples:
FA28901-11, FA28901-14
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
1634-04-4
Methyl Tert Butyl Ether
25
26.5
106
72-117
91-20-3
Naphthalene
25
26.8
107
63-132
103-65-1
n-Propylbenzene
25
28.1
112
82-133
100-42-5
Styrene
25
26.0
104
78-119
79-34-5
1,1,2,2-Tetrachloroethane
25
24.9
100
72-120
127-18-4
Tetrachloroethylene
25
27.2
109
76-135
108-88-3
Toluene
25
26.3
105
80-120
120-82-1
1,2,4-Trichlorobenzene
25
26.5
106
73-129
71-55-6
1, 1, 1-Trichloroethane
25
26.7
107
75-130
79-00-5
1,1,2-Trichloroethane
25
25.9
104
76-119
79-01-6
Trichloroethylene
25
27.5
110
81-126
75-69-4
Trichlorofluoromethane
25
28.2
113
71-156
95-63-6
1,2,4-Trimethylbenzene
25
26.1
104
79-120
108-67-8
1,3,5-Trimethylbenzene
25
25.7
103
79-120
75-01-4
Vinyl Chloride
25
29.3
117
69-159
1330-20-7
Xylene (total)
75
79.9
107
80-126
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
102%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
79-125%
2037-26-5
Toluene-D8
100%
85-112%
460-00-4
4-Bromofluorobenzene
99%
83-118%
* = Outside of Control Limits.
Method: SW846 8260B
■ 103 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA28738-3MS
P36804.13
10
11/04/15
KM
n/a
n/a
VP1367
FA28738-3MSD
P36805.13
10
11/04/15
KM
n/a
n/a
VP1367
FA28738-3
P36791.13
10
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples:
Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
FA28738-3
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
67-64-1
Acetone
ND
1250
983
79
1250
1070
86
8
50-147/21
71-43-2
Benzene
ND
250
261
104
250
262
105
0
81-122/14
75-27-4
Bromodichloromethane
ND
250
256
102
250
239
96
7
79-123/19
75-25-2
Bromoform
ND
250
225
90
250
201
80
11
66-123/21
78-93-3
2-Butanone(MEK)
ND
1250
1050
84
1250
1100
88
5
56-143/18
104-51-8
n-Butylbenzene
ND
250
256
102
250
251
100
2
79-126/16
75-15-0
Carbon Disulfide
ND
250
186
74
250
161
64*
14
66-148/23
56-23-5
Carbon Tetrachloride
ND
250
305
122
250
281
112
8
76-136/23
108-90-7
Chlorobenzene
ND
250
271
108
250
268
107
1
82-124/14
75-00-3
Chloroethane
ND
250
234
94
250
221
88
6
62-144/20
67-66-3
Chloroform
ND
250
273
109
250
267
107
2
80-124/15
110-82-7
Cyclohexane
ND
250
278
111
250
271
108
3
73-138/18
124-48-1
Dibromochloromethane
ND
250
240
96
250
216
86
11
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
ND
250
224
90
250
223
89
0
64-123/18
106-93-4
1,2-Dibromoethane
ND
250
261
104
250
264
106
1
75-120/13
75-71-8
Dichlorodifluoromethane
ND
250
287
115
250
283
113
1
42-167/19
95-50-1
1,2-Dichlorobenzene
ND
250
261
104
250
263
105
1
82-124/14
541-73-1
1,3-Dichlorobenzene
ND
250
273
109
250
267
107
2
84-125/14
106-46-7
1,4-Dichlorobenzene
ND
250
264
106
250
258
103
2
78-120/15
75-34-3
1, 1 -Dichloroethane
17.5
250
303
114
250
298
112
2
81-122/15
107-06-2
1,2-Dichloroethane
5.6 J
250
272
107
250
278
109
2
75-125/14
75-35-4
1, 1 -Dichloroethylene
706
250
881
70* a
250
869
65* a
1
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
ND
250
252
101
250
248
99
2
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
ND
250
292
117
250
276
110
6
76-127/17
78-87-5
1,2-Dichloropropane
ND
250
266
106
250
257
103
3
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
ND
250
248
99
250
221
88
12
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
ND
250
246
98
250
219
88
12
80-120/22
100-41-4
Ethylbenzene
ND
250
266
106
250
269
108
1
81-121/14
591-78-6
2-Hexanone
ND
1250
1020
82
1250
1030
82
1
61-129/18
98-82-8
Isopropylbenzene
ND
250
283
113
250
277
111
2
83-132/15
79-20-9
Methyl Acetate
ND
1250
1190
95
1250
1270
102
7
65-126/18
74-83-9
Methyl Bromide
ND
250
226
90
250
219
88
3
59-143/19
74-87-3
Methyl Chloride
ND
250
247
99
250
235
94
5
50-159/19
108-87-2
Methylcyclohexane
ND
250
293
117
250
289
116
1
76-129/17
75-09-2
Methylene Chloride
ND
250
276
110
250
269
108
3
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
1250
1070
86
1250
1100
88
3
66-122/16
* = Outside of Control Limits.
■ 104 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A28738-3MS
P36804.13
10
11/04/15
KM
n/a
n/a
VP1367
'A28738-3MSD
P36805.13
10
11/04/15
KM
n/a
n/a
VP1367
'A28738-3
P36791.13
10
11/04/15
KM
n/a
n/a
VP1367
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-10
FA28738-3
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l %
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
250
261
104
250
259
104
1
72-117/14
91-20-3
Naphthalene
ND
250
256
102
250
268
107
5
63-132/25
103-65-1
n-Propylbenzene
ND
250
279
112
250
271
108
3
82-133/15
100-42-5
Styrene
ND
250
258
103
250
260
104
1
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
ND
250
238
95
250
238
95
0
72-120/14
127-18-4
Tetrachloroethylene
8.7 J
250
297
115
250
299
116
1
76-135/16
108-88-3
Toluene
ND
250
265
106
250
267
107
1
80-120/14
120-82-1
1,2,4-Trichlorobenzene
ND
250
248
99
250
251
100
1
73-129/20
71-55-6
1, 1, 1-Trichloroethane
33.6
250
311
111
250
305
109
2
75-130/16
79-00-5
1,1,2-Trichloroethane
ND
250
245
98
250
247
99
1
76-119/14
79-01-6
Trichloroethylene
93.8
250
365
108
250
354
104
3
81-126/15
75-69-4
Trichlorofluoromethane
ND
250
278
111
250
274
110
1
71-156/21
95-63-6
1,2,4-Trimethylbenzene
ND
250
256
102
250
255
102
0
79-120/18
108-67-8
1,3,5-Trimethylbenzene
ND
250
258
103
250
250
100
3
79-120/19
75-01-4
Vinyl Chloride
ND
250
251
100
250
249
100
1
69-159/18
1330-20-7
Xylene (total)
ND
750
809
108
750
799
107
1
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA28738-3
Limits
1868-53-7
Dibromofluoromethane
99%
101%
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
100%
103%
99%
79-125%
2037-26-5
Toluene-D8
98%
99%
99%
85-112%
460-00-4
4-Bromofluorobenzene
94%
95%
96%
83-118%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
■■ 105 of 143
ACCUTEST
FA28907

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA28901-15MS
P36835.13
5
11/05/15
KM
n/a
n/a
VP1368
FA28901-15MSD
P36836.13
5
11/05/15
KM
n/a
n/a
VP1368
FA28901-15
P36829.13
5
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples:
FA28901-12, FA28901-13, FA28901-15, FA28901-16
CAS No. Compound
FA28901-15 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8260B
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
67-64-1
Acetone
ND
625
446
71
625
431
69
3
50-147/21
71-43-2
Benzene
ND
125
119
95
125
114
91
4
81-122/14
75-27-4
Bromodichloromethane
ND
125
110
88
125
101
81
9
79-123/19
75-25-2
Bromoform
ND
125
82.5
66
125
78.3
63*
5
66-123/21
78-93-3
2-Butanone(MEK)
ND
625
459
73
625
464
74
1
56-143/18
104-51-8
n-Butylbenzene
5.4
125
119
91
125
117
89
2
79-126/16
75-15-0
Carbon Disulfide
ND
125
89.8
72
125
75.1
60*
18
66-148/23
56-23-5
Carbon Tetrachloride
ND
125
136
109
125
115
92
17
76-136/23
108-90-7
Chlorobenzene
ND
125
122
98
125
118
94
3
82-124/14
75-00-3
Chloroethane
ND
125
132
106
125
125
100
5
62-144/20
67-66-3
Chloroform
ND
125
120
96
125
118
94
2
80-124/15
110-82-7
Cyclohexane
ND
125
126
101
125
114
91
10
73-138/18
124-48-1
Dibromochloromethane
ND
125
93.7
75*
125
87.8
70*
7
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
ND
125
99.6
80
125
95.2
76
5
64-123/18
106-93-4
1,2-Dibromoethane
ND
125
117
94
125
117
94
0
75-120/13
75-71-8
Dichlorodifluoromethane
ND
125
155
124
125
140
112
10
42-167/19
95-50-1
1,2-Dichlorobenzene
ND
125
118
94
125
114
91
3
82-124/14
541-73-1
1,3-Dichlorobenzene
ND
125
125
100
125
120
96
4
84-125/14
106-46-7
1,4-Dichlorobenzene
ND
125
120
96
125
115
92
4
78-120/15
75-34-3
1, 1 -Dichloroethane
ND
125
126
101
125
121
97
4
81-122/15
107-06-2
1,2-Dichloroethane
ND
125
119
95
125
114
91
4
75-125/14
75-35-4
1, 1 -Dichloroethylene
ND
125
124
99
125
117
94
6
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
ND
125
114
91
125
ill
89
3
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
ND
125
129
103
125
119
95
8
76-127/17
78-87-5
1,2-Dichloropropane
ND
125
118
94
125
116
93
2
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
ND
125
ill
89
125
98.6
79
12
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
ND
125
ill
89
125
97.0
78*
13
80-120/22
100-41-4
Ethylbenzene
8.0
125
129
97
125
126
94
2
81-121/14
591-78-6
2-Hexanone
ND
625
451
72
625
440
70
2
61-129/18
98-82-8
Isopropylbenzene
5.8
125
133
102
125
128
98
4
83-132/15
79-20-9
Methyl Acetate
ND
625
545
87
625
546
87
0
65-126/18
74-83-9
Methyl Bromide
ND
125
129
103
125
120
96
7
59-143/19
74-87-3
Methyl Chloride
ND
125
133
106
125
114
91
15
50-159/19
108-87-2
Methylcyclohexane
1.9
J 125
133
105
125
126
99
5
76-129/17
75-09-2
Methylene Chloride
ND
125
120
96
125
112
90
7
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
625
476
76
625
472
76
1
66-122/16
* = Outside of Control Limits.
■■ 106 of 143
ACCUTEST
FA28907

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A28901-15MS
P36835.13
5
11/05/15
KM
n/a
n/a
VP1368
'A28901-15MSD
P36836.13
5
11/05/15
KM
n/a
n/a
VP1368
'A28901-15
P36829.13
5
11/05/15
KM
n/a
n/a
VP1368
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-12, FA28901-13, FA28901-15, FA28901-16
FA28901-15 Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l
Q ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
125
115
92
125
110
88
4
72-117/14
91-20-3
Naphthalene
97.8
125
220
98
125
219
97
0
63-132/25
103-65-1
n-Propylbenzene
13.0
125
140
102
125
131
94
7
82-133/15
100-42-5
Styrene
ND
125
117
94
125
112
90
4
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
ND
125
112
90
125
112
90
0
72-120/14
127-18-4
Tetrachloroethylene
ND
125
137
110
125
130
104
5
76-135/16
108-88-3
Toluene
ND
125
120
96
125
117
94
3
80-120/14
120-82-1
1,2,4-Trichlorobenzene
ND
125
113
90
125
112
90
1
73-129/20
71-55-6
1, 1, 1-Trichloroethane
ND
125
124
99
125
119
95
4
75-130/16
79-00-5
1,1,2-Trichloroethane
ND
125
121
97
125
118
94
3
76-119/14
79-01-6
Trichloroethylene
ND
125
128
102
125
118
94
8
81-126/15
75-69-4
Trichlorofluoromethane
ND
125
154
123
125
145
116
6
71-156/21
95-63-6
1,2,4-Trimethylbenzene
147
125
276
103
125
261
91
6
79-120/18
108-67-8
1,3,5-Trimethylbenzene
24.9
125
145
96
125
137
90
6
79-120/19
75-01-4
Vinyl Chloride
ND
125
136
109
125
129
103
5
69-159/18
1330-20-7
Xylene (total)
4.3
J 375
370
98
375
360
95
3
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA28901-15
Limits
1868-53-7
Dibromofluoromethane
101%
101%
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
97%
97%
98%
79-125%
2037-26-5
Toluene-D8
98%
97%
96%
85-112%
460-00-4
4-Bromofluorobenzene
95%
94%
93%
83-118%
* = Outside of Control Limits.
■■ 107 of 143
ACCUTEST
FA28907

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA28966-lMS
P36867.13
1
11/06/15
KM
n/a
n/a
VP1369
FA28966-1MSD
P36868.13
1
11/06/15
KM
n/a
n/a
VP1369
FA28966-1
P36855.13
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples:
FA28901-15
CAS No. Compound
FA28966-1 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8260B
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
67-64-1
Acetone
25 U
125
117
94
125
ill
89
5
50-147/21
71-43-2
Benzene
1.0 U
25
28.8
115
25
27.9
112
3
81-122/14
75-27-4
Bromodichloromethane
1.0 U
25
30.0
120
25
28.3
113
6
79-123/19
75-25-2
Bromoform
1.0 U
25
25.8
103
25
25.3
101
2
66-123/21
78-93-3
2-Butanone(MEK)
5.0 U
125
113
90
125
117
94
3
56-143/18
104-51-8
n-Butylbenzene
1.0 U
25
28.0
112
25
27.3
109
3
79-126/16
75-15-0
Carbon Disulfide
2.0 U
25
23.9
96
25
22.1
88
8
66-148/23
56-23-5
Carbon Tetrachloride
1.0 U
25
35.4
142*
25
32.3
129
9
76-136/23
108-90-7
Chlorobenzene
1.0 U
25
29.9
120
25
29.4
118
2
82-124/14
75-00-3
Chloroethane
2.0 U
25
22.3
89
25
22.0
88
1
62-144/20
67-66-3
Chloroform
1.0 U
25
30.0
120
25
29.9
120
0
80-124/15
110-82-7
Cyclohexane
1.0 U
25
30.5
122
25
28.7
115
6
73-138/18
124-48-1
Dibromochloromethane
1.0 U
25
27.4
110
25
26.3
105
4
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
2.0 U
25
23.6
94
25
24.9
100
5
64-123/18
106-93-4
1,2-Dibromoethane
2.0 U
25
28.9
116
25
28.8
115
0
75-120/13
75-71-8
Dichlorodifluoromethane
2.0 U
25
29.4
118
25
28.8
115
2
42-167/19
95-50-1
1,2-Dichlorobenzene
1.0 U
25
29.7
119
25
29.2
117
2
82-124/14
541-73-1
1,3-Dichlorobenzene
1.0 U
25
31.3
125
25
29.7
119
5
84-125/14
106-46-7
1,4-Dichlorobenzene
1.0 U
25
30.0
120
25
29.2
117
3
78-120/15
75-34-3
1, 1 -Dichloroethane
1.0 U
25
31.2
125*
25
29.8
119
5
81-122/15
107-06-2
1,2-Dichloroethane
1.0 U
25
30.2
121
25
29.6
118
2
75-125/14
75-35-4
1, 1 -Dichloroethylene
1.0 U
25
30.1
120
25
29.8
119
1
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
1.0U
25
27.8
ill
25
27.2
109
2
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
1.0 U
25
31.0
124
25
30.1
120
3
76-127/17
78-87-5
1,2-Dichloropropane
1.0 U
25
28.3
113
25
27.3
109
4
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
1.0 U
25
25.8
103
25
24.3
97
6
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
1.0 U
25
25.5
102
25
23.8
95
7
80-120/22
100-41-4
Ethylbenzene
1.0 U
25
30.0
120
25
29.5
118
2
81-121/14
591-78-6
2-Hexanone
10 U
125
112
90
125
114
91
2
61-129/18
98-82-8
Isopropylbenzene
1.0 U
25
31.9
128
25
30.7
123
4
83-132/15
79-20-9
Methyl Acetate
20 U
125
129
103
125
130
104
1
65-126/18
74-83-9
Methyl Bromide
2.0 U
25
22.2
89
25
22.5
90
1
59-143/19
74-87-3
Methyl Chloride
2.0 U
25
25.1
100
25
23.1
92
8
50-159/19
108-87-2
Methylcyclohexane
1.0 U
25
33.4
134*
25
31.5
126
6
76-129/17
75-09-2
Methylene Chloride
5.0 U
25
28.8
115
25
27.8
ill
4
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
5.0 U
125
118
94
125
119
95
1
66-122/16
* = Outside of Control Limits.
■ 108 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A28966-lMS
P36867.13
1
11/06/15
KM
n/a
n/a
VP1369
'A28966-1MSD
P36868.13
1
11/06/15
KM
n/a
n/a
VP1369
'A28966-1
P36855.13
1
11/06/15
KM
n/a
n/a
VP1369
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-15
FA28966-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
1.0 U
25
27.7
111
25
28.3
113
2
72-117/14
91-20-3
Naphthalene
5.0 U
25
29.5
118
25
30.2
121
2
63-132/25
103-65-1
n-Propylbenzene
1.0 U
25
30.5
122
25
29.3
117
4
82-133/15
100-42-5
Styrene
1.0 U
25
25.4
102
25
24.8
99
2
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
1.0 U
25
24.7
99
25
25.1
100
2
72-120/14
127-18-4
Tetrachloroethylene
1.0 U
25
33.9
136*
25
32.9
132
3
76-135/16
108-88-3
Toluene
1.0 U
25
29.4
118
25
28.8
115
2
80-120/14
120-82-1
1,2,4-Trichlorobenzene
1.0 U
25
28.1
112
25
28.8
115
2
73-129/20
71-55-6
1, 1, 1-Trichloroethane
1.0 U
25
31.7
127
25
31.2
125
2
75-130/16
79-00-5
1,1,2-Trichloroethane
1.0 U
25
26.2
105
25
25.5
102
3
76-119/14
79-01-6
Trichloroethylene
1.0 U
25
30.3
121
25
30.1
120
1
81-126/15
75-69-4
Trichlorofluoromethane
2.0 U
25
29.4
118
25
28.1
112
5
71-156/21
108-67-8
1,3,5-Trimethylbenzene
2.0 U
25
28.4
114
25
26.7
107
6
79-120/19
75-01-4
Vinyl Chloride
1.0 U
25
24.7
99
25
23.6
94
5
69-159/18
1330-20-7
Xylene(total)
3.0 U
75
89.9
120
75
87.2
116
3
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA28966-1
Limits
1868-53-7
Dibromofluoromethane
103%
102%
104%
83-118%
17060-07-0
1,2-Dichloroethane-D4
101%
102%
101%
79-125%
2037-26-5
Toluene-D8
98%
98%
97%
85-112%
460-00-4
4-Bromofluorobenzene
92%
91%
93%
83-118%
* = Outside of Control Limits.
■ 109 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA28961-2MS
P36926.13
10
11/09/15
KM
n/a
n/a
VP1371
FA28961-2MSD
P36927.13
10
11/09/15
KM
n/a
n/a
VP1371
FA28961-2
P36916.13
10
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples:
FA28901-11, FA28901-14
CAS No. Compound
FA28961-2 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8260B
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
67-64-1
Acetone
1690
1250
2820
90
1250
2840
92
1
50-147/21
71-43-2
Benzene
ND
250
242
97
250
238
95
2
81-122/14
75-27-4
Bromodichloromethane
ND
250
236
94
250
218
87
8
79-123/19
75-25-2
Bromoform
ND
250
195
78
250
190
76
3
66-123/21
78-93-3
2-Butanone(MEK)
99.1
1250
1190
87
1250
1250
92
5
56-143/18
104-51-8
n-Butylbenzene
ND
250
250
100
250
244
98
2
79-126/16
75-15-0
Carbon Disulfide
16.6
J 250
196
72
250
187
68
5
66-148/23
56-23-5
Carbon Tetrachloride
ND
250
258
103
250
238
95
8
76-136/23
108-90-7
Chlorobenzene
ND
250
254
102
250
248
99
2
82-124/14
75-00-3
Chloroethane
ND
250
307
123
250
311
124
1
62-144/20
67-66-3
Chloroform
ND
250
246
98
250
243
97
1
80-124/15
110-82-7
Cyclohexane
ND
250
246
98
250
242
97
2
73-138/18
124-48-1
Dibromochloromethane
ND
250
219
88
250
199
80
10
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
ND
250
231
92
250
243
97
5
64-123/18
106-93-4
1,2-Dibromoethane
ND
250
260
104
250
253
101
3
75-120/13
75-71-8
Dichlorodifluoromethane
ND
250
326
130
250
319
128
2
42-167/19
95-50-1
1,2-Dichlorobenzene
ND
250
255
102
250
252
101
1
82-124/14
541-73-1
1,3-Dichlorobenzene
ND
250
258
103
250
251
100
3
84-125/14
106-46-7
1,4-Dichlorobenzene
ND
250
253
101
250
250
100
1
78-120/15
75-34-3
1, 1 -Dichloroethane
ND
250
250
100
250
248
99
1
81-122/15
107-06-2
1,2-Dichloroethane
9.9
J 250
240
92
250
239
92
0
75-125/14
75-35-4
1, 1 -Dichloroethylene
ND
250
246
98
250
246
98
0
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
ND
250
234
94
250
234
94
0
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
ND
250
264
106
250
254
102
4
76-127/17
78-87-5
1,2-Dichloropropane
ND
250
237
95
250
238
95
0
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
ND
250
232
93
250
208
83
11
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
ND
250
256
102
250
228
91
12
80-120/22
100-41-4
Ethylbenzene
ND
250
258
103
250
250
100
3
81-121/14
591-78-6
2-Hexanone
ND
1250
1170
94
1250
1200
96
3
61-129/18
98-82-8
Isopropylbenzene
ND
250
261
104
250
257
103
2
83-132/15
79-20-9
Methyl Acetate
ND
1250
1180
94
1250
1210
97
3
65-126/18
74-83-9
Methyl Bromide
29.8
250
306
110
250
305
110
0
59-143/19
74-87-3
Methyl Chloride
429
250
639
84
250
631
81
1
50-159/19
108-87-2
Methylcyclohexane
ND
250
273
109
250
266
106
3
76-129/17
75-09-2
Methylene Chloride
23.6
J 250
253
92
250
250
91
1
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
1250
1200
96
1250
1220
98
2
66-122/16
* = Outside of Control Limits.
■ 110 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A28961-2MS
P36926.13
10
11/09/15
KM
n/a
n/a
VP1371
'A28961-2MSD
P36927.13
10
11/09/15
KM
n/a
n/a
VP1371
'A28961-2
P36916.13
10
11/09/15
KM
n/a
n/a
VP1371
The QC reported here applies to the following samples: Method: SW846 8260B
FA28901-11, FA28901-14
FA28961-2
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
250
244
98
250
248
99
2
72-117/14
91-20-3
Naphthalene
ND
250
255
102
250
270
108
6
63-132/25
103-65-1
n-Propylbenzene
ND
250
265
106
250
256
102
3
82-133/15
100-42-5
Styrene
ND
250
242
97
250
235
94
3
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
ND
250
244
98
250
249
100
2
72-120/14
127-18-4
Tetrachloroethylene
ND
250
260
104
250
259
104
0
76-135/16
108-88-3
Toluene
ND
250
253
101
250
246
98
3
80-120/14
120-82-1
1,2,4-Trichlorobenzene
ND
250
253
101
250
254
102
0
73-129/20
71-55-6
1, 1, 1-Trichloroethane
ND
250
248
99
250
247
99
0
75-130/16
79-00-5
1,1,2-Trichloroethane
ND
250
252
101
250
247
99
2
76-119/14
79-01-6
Trichloroethylene
ND
250
259
104
250
250
100
4
81-126/15
75-69-4
Trichlorofluoromethane
ND
250
288
115
250
282
113
2
71-156/21
95-63-6
1,2,4-Trimethylbenzene
ND
250
253
101
250
246
98
3
79-120/18
108-67-8
1,3,5-Trimethylbenzene
ND
250
248
99
250
243
97
2
79-120/19
75-01-4
Vinyl Chloride
ND
250
273
109
250
270
108
1
69-159/18
1330-20-7
Xylene (total)
ND
750
764
102
750
744
99
3
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA28961-2
Limits
1868-53-7
Dibromofluoromethane
100%
100%
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
95%
95%
101%
79-125%
2037-26-5
Toluene-D8
99%
99%
98%
85-112%
460-00-4
4-Bromofluorobenzene
100%
100%
103%
83-118%
* = Outside of Control Limits.
■■ 111 of 143
M A DMUTEST
FA28901 LA...A - 1-

Section 6
Southeast
■,N.ccuTEST
L A H OR AT OR E E 5
GUMS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
■■ 112 of 143
ACCUTEST

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58175-MB
L0684426.13
1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples:
Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
50
10
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
5.0
0.50
ug/l
95-57-8
2-Chlorophenol
ND
5.0
0.50
ug/l
120-83-2
2,4-Dichlorophenol
ND
5.0
0.50
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.0
0.50
ug/l
51-28-5
2,4-Dinitrophenol
ND
25
5.0
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
10
2.1
ug/1
95-48-7
2-Methylphenol
ND
5.0
0.50
ug/1
3&4-Methylphenol
ND
5.0
1.0
ug/l
88-75-5
2-Nitrophenol
ND
5.0
0.88
ug/1
100-02-7
4-Nitrophenol
ND
25
5.0
ug/1
87-86-5
Pentachlorophenol
ND
25
5.0
ug/1
108-95-2
Phenol
ND
5.0
0.50
ug/1
88-06-2
2,4,6-Trichlorophenol
ND
5.0
0.63
ug/l
83-32-9
Acenaphthene
ND
5.0
0.50
ug/l
208-96-8
Acenaphthylene
ND
5.0
0.50
ug/l
120-12-7
Anthracene
ND
5.0
0.50
ug/l
56-55-3
Benzo(a)anthracene
ND
5.0
0.50
ug/l
50-32-8
Benzo(a)pyrene
ND
5.0
0.50
ug/l
205-99-2
Benzo(b)fluoranthene
ND
5.0
0.58
ug/l
191-24-2
Benzo(g,h,i)perylene
ND
5.0
0.66
ug/l
207-08-9
Benzo(k)fluoranthene
ND
5.0
0.68
ug/l
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.0
0.64
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.0
1.0
ug/1
106-47-8
4-Chloroaniline
ND
5.0
0.50
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.0
0.63
ug/l
111-44-4
bis(2-Chloroethyl)ether
ND
5.0
0.69
ug/l
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.0
0.50
ug/1
91-58-7
2-Chloronaphthalene
ND
5.0
0.50
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
5.0
0.57
ug/l
218-01-9
Chrysene
ND
5.0
0.51
ug/l
53-70-3
Dibenzo(a,h)anthracene
ND
5.0
0.68
ug/l
132-64-9
Dibenzofuran
ND
5.0
0.50
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
5.0
0.52
ug/l
84-66-2
Diethyl Phthalate
ND
5.0
1.4
ug/l
131-11-3
Dimethyl Phthalate
ND
5.0
1.0
ug/l
■ 113 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P58175-MB
L0684426.13
1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples: Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
CAS No. Compound
84-74-2
Di-n-butyl Phthalate
117-84-0
Di-n-octyl Phthalate
121-14-2
2,4-Dinitrotoluene
606-20-2
2, 6-Dinitrotoluene
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno(1,2,3-cd)pyrene
78-59-1
Isophorone
90-12-0
1-M ethylnaphthalene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3
Nitrobenzene
621-64-7
N-Nitrosodi-n-propylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanthrene
129-00-0
Pyrene
CAS No. Surrogate Recoveries
Result
RL
MDL
Units Q
ND
5.0
1.0
ug/1
ND
5.0
1.0
ug/1
ND
5.0
0.58
ug/1
ND
5.0
0.69
ug/1
ND
5.0
1.0
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.63
ug/1
ND
5.0
0.60
ug/1
ND
5.0
1.0
ug/1
ND
5.0
0.68
ug/1
ND
5.0
0.63
ug/1
ND
5.0
0.51
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.52
ug/1
ND
5.0
0.58
ug/1
ND
5.0
0.59
ug/1
ND
5.0
0.51
ug/1
ND
5.0
0.55
ug/1
Limits
367-12-4
2-Fluorophenol
44%
14-67%
4165-62-2
Phenol-d5
31%
10-50%
118-79-6
2,4,6-Tribromophenol
89%
33-118%
4165-60-0
Nitrobenzene-d5
71%
42-108%
321-60-8
2-Fluorobiphenyl
79%
40-106%
1718-51-0
Terphenyl-d14
84%
39-121%
CAS No. Tentatively Identified Compounds R.T.
Total TIC, Semi -Volatile a
Est. Conc. Units Q
0 ug/1
■ 114 of 143
E ACCUTEST
FA28901

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58175-MB
L0684426.13
1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples:
Method:
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
(a) No TICS detected.
■■ 115 of 143
ACCUTEST
FA28907

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
DP58211-MB
X043257.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples: Method: SW846 8270D
FA28901-13, FA28901-14, FA28901-15, FA28901-16
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
50
10
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
5.0
0.50
ug/l
95-57-8
2-Chlorophenol
ND
5.0
0.50
ug/l
120-83-2
2,4-Dichlorophenol
ND
5.0
0.50
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.0
0.50
ug/l
51-28-5
2,4-Dinitrophenol
ND
25
5.0
ug/1
534-52-1
4,6-Dinitro-o-cresol
ND
10
2.1
ug/1
95-48-7
2-Methylphenol
ND
5.0
0.50
ug/1
3&4-Methylphenol
ND
5.0
1.0
ug/l
88-75-5
2-Nitrophenol
ND
5.0
0.88
ug/1
100-02-7
4-Nitrophenol
ND
25
5.0
ug/1
87-86-5
Pentachlorophenol
ND
25
5.0
ug/1
108-95-2
Phenol
ND
5.0
0.50
ug/1
88-06-2
2,4,6-Trichlorophenol
ND
5.0
0.63
ug/l
83-32-9
Acenaphthene
ND
5.0
0.50
ug/l
208-96-8
Acenaphthylene
ND
5.0
0.50
ug/l
120-12-7
Anthracene
ND
5.0
0.50
ug/l
56-55-3
Benzo(a)anthracene
ND
5.0
0.50
ug/l
50-32-8
Benzo(a)pyrene
ND
5.0
0.50
ug/l
205-99-2
Benzo(b)fluoranthene
ND
5.0
0.58
ug/l
191-24-2
Benzo(g,h,i)perylene
ND
5.0
0.66
ug/l
207-08-9
Benzo(k)fluoranthene
ND
5.0
0.68
ug/l
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.0
0.64
ug/1
85-68-7
Butyl Benzyl Phthalate
ND
5.0
1.0
ug/1
106-47-8
4-Chloroaniline
ND
5.0
0.50
ug/1
111-91-1
bis(2-Chloroethoxy)methane
ND
5.0
0.63
ug/l
111-44-4
bis(2-Chloroethyl)ether
ND
5.0
0.69
ug/l
108-60-1
bis(2-Chloroisopropyl)ether
ND
5.0
0.50
ug/1
91-58-7
2-Chloronaphthalene
ND
5.0
0.50
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
5.0
0.57
ug/l
218-01-9
Chrysene
ND
5.0
0.51
ug/l
53-70-3
Dibenzo(a,h)anthracene
ND
5.0
0.68
ug/l
132-64-9
Dibenzofuran
ND
5.0
0.50
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
5.0
0.52
ug/l
84-66-2
Diethyl Phthalate
ND
5.0
1.4
ug/l
131-11-3
Dimethyl Phthalate
ND
5.0
1.0
ug/l
■■ 116 of 143
ACCUTEST
FA28907

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P58211-MB
X043257.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples: Method: SW846 8270D
FA28901-13, FA28901-14, FA28901-15, FA28901-16
CAS No. Compound
84-74-2
Di-n-butyl Phthalate
117-84-0
Di-n-octyl Phthalate
121-14-2
2,4-Dinitrotoluene
606-20-2
2, 6-Dinitrotoluene
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno(1,2,3-cd)pyrene
78-59-1
Isophorone
90-12-0
1-M ethylnaphthalene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3
Nitrobenzene
621-64-7
N-Nitrosodi-n-propylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanthrene
129-00-0
Pyrene
CAS No. Surrogate Recoveries
Result
RL
MDL
Units Q
ND
5.0
1.0
ug/l
ND
5.0
1.0
ug/l
ND
5.0
0.58
ug/l
ND
5.0
0.69
ug/l
ND
5.0
1.0
ug/l
ND
5.0
0.50
ug/1
ND
5.0
0.50
ug/1
ND
5.0
0.63
ug/1
ND
5.0
0.60
ug/l
ND
5.0
1.0
ug/1
ND
5.0
0.68
ug/1
ND
5.0
0.63
ug/1
ND
5.0
0.51
ug/1
ND
5.0
0.50
ug/l
ND
5.0
0.50
ug/l
ND
5.0
0.50
ug/l
ND
5.0
0.52
ug/l
ND
5.0
0.58
ug/l
ND
5.0
0.59
ug/l
ND
5.0
0.51
ug/l
ND
5.0
0.55
ug/l
Limits
367-12-4
2-Fluorophenol
43%
14-67%
4165-62-2
Phenol-d5
31%
10-50%
118-79-6
2,4,6-Tribromophenol
71%
33-118%
4165-60-0
Nitrobenzene-d5
72%
42-108%
321-60-8
2-Fluorobiphenyl
68%
40-106%
1718-51-0
Terphenyl-d14
83%
39-121%
CAS No. Tentatively Identified Compounds R.T.
563-80-4 2-Butanone, 3-methyl-
2.33
Est. Conc. Units Q
38 ug/l JN
■■ 117 of 143
M ACCUTEST
FA28901 LA...A-1-

Method Blank Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58211-MB
X043257.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples: Method:
FA28901-13, FA28901-14, FA28901-15, FA28901-16
CAS No.
Tentatively Identified Compounds
R.T.
Est. Conc.
Units
Q
594-36-5
Butane, 2-chloro-2-methyl-
2.38
11
ug/1
JN
1000152-79-7Cyclopentane,
1,2,3,4,5-pentamethyl-
4.64
12
ug/1
JN
49622-18-6
Decane, 3,3,4-trimethyl-
4.86
5.1
ug/1
JN
4291-79-6
Cyclohexane, 1-methyl-2-propyl-
4.88
5.1
ug/1
JN
Total TIC, Semi -Volatile
71.2
ug/1
J
■ 118 of 143
E ACCUTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58175-BS
L0684425.13
1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples:
Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
65-85-0
Benzoic Acid
100
14.1
14
10-69
59-50-7
4-Chloro-3-methyl Phenol
50
37.1
74
54-103
95-57-8
2-Chlorophenol
50
40.8
82
52-98
120-83-2
2,4-Dichlorophenol
50
40.4
81
53-103
105-67-9
2,4-Dimethylphenol
50
27.4
55
43-90
51-28-5
2,4-Dinitrophenol
100
77.5
78
44-112
534-52-1
4,6-Dinitro-o-cresol
100
108
108
66-121
95-48-7
2-Methylphenol
50
33.8
68
43-90
3&4-Methylphenol
100
62.1
62
36-88
88-75-5
2-Nitrophenol
50
39.6
79
53-102
100-02-7
4-Nitrophenol
100
42.9
43
18-62
87-86-5
Pentachlorophenol
100
117
117*
61-115
108-95-2
Phenol
50
19.7
39
19-56
88-06-2
2,4,6-Trichlorophenol
50
47.4
95
59-107
83-32-9
Acenaphthene
50
47.7
95
61-107
208-96-8
Acenaphthylene
50
44.4
89
60-104
120-12-7
Anthracene
50
48.3
97
65-108
56-55-3
Benzo(a)anthracene
50
48.3
97
66-111
50-32-8
Benzo(a)pyrene
50
47.1
94
62-107
205-99-2
Benzo(b)fluoranthene
50
47.2
94
65-114
191-24-2
Benzo(g,h,i)perylene
50
48.6
97
66-116
207-08-9
Benzo(k)fluoranthene
50
48.2
96
65-114
101-55-3
4-BromophenylPhenyl Ether
50
50.5
101
65-109
85-68-7
Butyl Benzyl Phthalate
50
45.9
92
65-112
106-47-8
4-Chloroaniline
50
37.7
75
49-105
111-91-1
bis(2-Chloroethoxy)methane
50
28.9
58
51-102
111-44-4
bis(2-Chloroethyl)ether
50
41.8
84
53-100
108-60-1
bis(2-Chloroisopropyl)ether
50
40.7
81
45-106
91-58-7
2-Chloronaphthalene
50
44.0
88
57-103
7005-72-3
4-ChlorophenylPhenyl Ether
50
45.2
90
62-105
218-01-9
Chrysene
50
50.0
100
66-111
53-70-3
Dibenzo(a,h)anthracene
50
48.7
97
66-119
132-64-9
Dibenzofuran
50
46.6
93
61-106
91-94-1
3,3'-Dichlorobenzidine
50
48.5
97
46-117
84-66-2
Diethyl Phthalate
50
45.3
91
64-108
131-11-3
Dimethyl Phthalate
50
45.0
90
63-106
* = Outside of Control Limits.
■ 119 of 143
E ACC UTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P58175-BS
L0684425.13
1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples: Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
Spike
BSP
BSP
CAS No.
Compound
ug/1
ug/l
%
Limits
84-74-2
Di-n-butyl Phthalate
50
48.0
96
65-107
117-84-0
Di-n-octyl Phthalate
50
47.3
95
62-118
121-14-2
2,4-Dinitrotoluene
50
46.0
92
61-110
606-20-2
2,6-Dinitrotoluene
50
44.3
89
63-108
117-81-7
bis(2-Ethylhexyl)phthalate
50
46.7
93
61-117
206-44-0
Fluoranthene
50
47.4
95
63-106
86-73-7
Fluorene
50
46.7
93
62-108
118-74-1
Hexachlorobenzene
50
49.7
99
63-108
87-68-3
Hexachlorobutadiene
50
33.7
67
42-102
77-47-4
Hexachlorocyclopentadiene
50
39.4
79
39-102
67-72-1
Hexachloroethane
50
33.3
67
42-100
193-39-5
Indeno(1,2,3-cd)pyrene
50
48.6
97
64-119
78-59-1
Isophorone
50
37.3
75
43-87
90-12-0
1-Methylnaphthalene
50
40.6
81
53-102
91-57-6
2-Methylnaphthalene
50
38.5
77
51-102
91-20-3
Naphthalene
50
37.0
74
47-100
98-95-3
Nitrobenzene
50
37.1
74
50-104
621-64-7
N-Nitrosodi-n-propylamine
50
40.8
82
52-104
86-30-6
N-Nitrosodiphenylamine
50
46.9
94
64-108
85-01-8
Phenanthrene
50
49.7
99
66-110
129-00-0
Pyrene
50
45.8
92
64-113
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
53%
14-67%
4165-62-2
Phenol-d5
37%
10-50%
118-79-6
2,4,6-Tribromophenol
94%
33-118%
4165-60-0
Nitrobenzene-d5
73%
42-108%
321-60-8
2-Fluorobiphenyl
87%
40-106%
1718-51-0
Terphenyl-d14
97%
39-121%
* = Outside of Control Limits.
■ 120 of 143
E ACC UTEST
FA28901

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58211-BS
X043256.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples:
FA28901-13, FA28901-14, FA28901-15, FA28901-16
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
65-85-0
Benzoic Acid
100
12.8
13
10-69
59-50-7
4-Chloro-3-methyl Phenol
50
36.1
72
54-103
95-57-8
2-Chlorophenol
50
33.7
67
52-98
120-83-2
2,4-Dichlorophenol
50
36.7
73
53-103
105-67-9
2,4-Dimethylphenol
50
26.4
53
43-90
51-28-5
2,4-Dinitrophenol
100
65.0
65
44-112
534-52-1
4,6-Dinitro-o-cresol
100
79.0
79
66-121
95-48-7
2-Methylphenol
50
28.7
57
43-90
3&4-Methylphenol
100
51.4
51
36-88
88-75-5
2-Nitrophenol
50
37.8
76
53-102
100-02-7
4-Nitrophenol
100
31.6
32
18-62
87-86-5
Pentachlorophenol
100
85.9
86
61-115
108-95-2
Phenol
50
14.8
30
19-56
88-06-2
2,4,6-Trichlorophenol
50
39.1
78
59-107
83-32-9
Acenaphthene
50
38.9
78
61-107
208-96-8
Acenaphthylene
50
36.6
73
60-104
120-12-7
Anthracene
50
38.6
77
65-108
56-55-3
Benzo(a)anthracene
50
39.1
78
66-111
50-32-8
Benzo(a)pyrene
50
39.3
79
62-107
205-99-2
Benzo(b)fluoranthene
50
39.1
78
65-114
191-24-2
Benzo(g,h,i)perylene
50
33.9
68
66-116
207-08-9
Benzo(k)fluoranthene
50
38.5
77
65-114
101-55-3
4-BromophenylPhenyl Ether
50
37.4
75
65-109
85-68-7
Butyl Benzyl Phthalate
50
38.8
78
65-112
106-47-8
4-Chloroaniline
50
36.6
73
49-105
111-91-1
bis(2-Chloroethoxy)methane
50
37.3
75
51-102
111-44-4
bis(2-Chloroethyl)ether
50
34.8
70
53-100
108-60-1
bis(2-Chloroisopropyl)ether
50
37.5
75
45-106
91-58-7
2-Chloronaphthalene
50
36.7
73
57-103
7005-72-3
4-ChlorophenylPhenyl Ether
50
37.6
75
62-105
218-01-9
Chrysene
50
41.1
82
66-111
53-70-3
Dibenzo(a,h)anthracene
50
39.3
79
66-119
132-64-9
Dibenzofuran
50
38.7
77
61-106
91-94-1
3,3'-Dichlorobenzidine
50
40.1
80
46-117
84-66-2
Diethyl Phthalate
50
38.7
77
64-108
131-11-3
Dimethyl Phthalate
50
37.9
76
63-106
* = Outside of Control Limits.
Method: SW846 8270D
■■ 121 of 143
M A DMUTEST
FA28901 LA...A - 1-

Blank Spike Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58211-BS
X043256.1)
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples:
FA28901-13, FA28901-14, FA28901-15, FA28901-16
Spike
BSP
BSP
CAS No.
Compound
ug/l
ug/l
%
Limits
84-74-2
Di-n-butyl Phthalate
50
39.2
78
65-107
117-84-0
Di-n-octyl Phthalate
50
36.0
72
62-118
121-14-2
2,4-Dinitrotoluene
50
40.2
80
61-110
606-20-2
2,6-Dinitrotoluene
50
38.0
76
63-108
117-81-7
bis(2-Ethylhexyl)phthalate
50
38.7
77
61-117
206-44-0
Fluoranthene
50
38.2
76
63-106
86-73-7
Fluorene
50
39.2
78
62-108
118-74-1
Hexachlorobenzene
50
37.4
75
63-108
87-68-3
Hexachlorobutadiene
50
34.1
68
42-102
77-47-4
Hexachlorocyclopentadiene
50
29.1
58
39-102
67-72-1
Hexachloroethane
50
31.6
63
42-100
193-39-5
Indeno(1,2,3-cd)pyrene
50
38.0
76
64-119
78-59-1
Isophorone
50
36.2
72
43-87
90-12-0
1-Methylnaphthalene
50
38.5
77
53-102
91-57-6
2-Methylnaphthalene
50
36.7
73
51-102
91-20-3
Naphthalene
50
35.2
70
47-100
98-95-3
Nitrobenzene
50
37.2
74
50-104
621-64-7
N-Nitrosodi-n-propylamine
50
36.4
73
52-104
86-30-6
N-Nitrosodiphenylamine
50
38.2
76
64-108
85-01-8
Phenanthrene
50
37.9
76
66-110
129-00-0
Pyrene
50
37.7
75
64-113
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
43%
14-67%
4165-62-2
Phenol-d5
30%
10-50%
118-79-6
2,4,6-Tribromophenol
75%
33-118%
4165-60-0
Nitrobenzene-d5
71%
42-108%
321-60-8
2-Fluorobiphenyl
72%
40-106%
1718-51-0
Terphenyl-d14
81%
39-121%
* = Outside of Control Limits.
Method: SW846 8270D
■■ 122 of 143
ACCUTEST
FA28907

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58175-MS
L0684435.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
OP58175-MSD
L0684436.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
FA28818-6
L0684434.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples:
Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
FA28818-6
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
65-85-0
Benzoic Acid
47 U
189
88.5
47
189
74.6
40
17
10-69/39
59-50-7
4-Chloro-3-methyl Phenol
4.7 U
94.3
74.2
79
94.3
73.0
77
2
54-103/23
95-57-8
2-Chlorophenol
4.7 U
94.3
78.2
83
94.3
74.3
79
5
52-98/25
120-83-2
2,4-Dichlorophenol
4.7 U
94.3
71.9
76
94.3
70.2
74
2
53-103/26
105-67-9
2,4-Dimethylphenol
4.7 U
94.3
55.5
59
94.3
55.5
59
0
43-90/27
51-28-5
2,4-Dinitrophenol
24 U
189
144
76
189
145
77
1
44-112/25
534-52-1
4,6-Dinitro-o-cresol
9.4 U
189
200
106
189
196
104
2
66-121/23
95-48-7
2-Methylphenol
4.7 U
94.3
71.3
76
94.3
66.5
70
7
43-90/28
3&4-Methylphenol
4.7 U
189
141
75
189
129
68
9
36-88/28
88-75-5
2-Nitrophenol
4.7 U
94.3
69.2
73
94.3
69.7
74
1
53-102/29
100-02-7
4-Nitrophenol
24 U
189
143
76*
189
115
61
22
18-62/33
87-86-5
Pentachlorophenol
24 U
189
210
111
189
203
108
3
61-115/26
108-95-2
Phenol
4.7 U
94.3
56.4
60*
94.3
45.9
49
21
19-56/35
88-06-2
2,4,6-Trichlorophenol
4.7 U
94.3
86.2
91
94.3
81.6
86
5
59-107/23
83-32-9
Acenaphthene
4.7 U
94.3
91.2
97
94.3
86.6
92
5
61-107/22
208-96-8
Acenaphthylene
4.7 U
94.3
84.3
89
94.3
81.5
86
3
60-104/22
120-12-7
Anthracene
4.7 U
94.3
91.1
97
94.3
88.4
94
3
65-108/20
56-55-3
Benzo(a)anthracene
4.7 U
94.3
89.3
95
94.3
87.1
92
2
66-111/22
50-32-8
Benzo(a)pyrene
4.7 U
94.3
84.8
90
94.3
84.9
90
0
62-107/23
205-99-2
Benzo(b)fluoranthene
4.7 U
94.3
84.2
89
94.3
84.9
90
1
65-114/23
191-24-2
Benzo(g, h, i)perylene
4.7 U
94.3
87.8
93
94.3
89.1
94
1
66-116/23
207-08-9
Benzo(k)fluoranthene
4.7 U
94.3
86.0
91
94.3
86.5
92
1
65-114/24
101-55-3
4-Bromophenyl Phenyl Ether
4.7 U
94.3
91.8
97
94.3
88.8
94
3
65-109/23
85-68-7
Butyl Benzyl Phthalate
4.7 U
94.3
87.6
93
94.3
86.5
92
1
65-112/24
106-47-8
4-Chloroaniline
4.7 U
94.3
61.8
66
94.3
49.5
52
22
49-105/27
111-91-1
bis(2-Chloroethoxy)methane
4.7 U
94.3
54.0
57
94.3
53.1
56
2
51-102/28
111-44-4
bis(2-Chloroethyl)ether
4.7 U
94.3
75.4
80
94.3
73.5
78
3
53-100/27
108-60-1
bis(2-Chloroisopropyl)ether
4.7 U
94.3
77.4
82
94.3
73.9
78
5
45-106/26
91-58-7
2-Chloronaphthalene
4.7 U
94.3
84.4
89
94.3
80.3
85
5
57-103/23
7005-72-3
4-Chlorophenyl Phenyl Ether
4.7 U
94.3
85.7
91
94.3
82.7
88
4
62-105/20
218-01-9
Chrysene
4.7 U
94.3
92.3
98
94.3
90.9
96
2
66-111/22
53-70-3
Dibenzo(a,h)anthracene
4.7 U
94.3
88.2
93
94.3
87.3
93
1
66-119/24
132-64-9
Dibenzofuran
4.7 U
94.3
85.6
91
94.3
84.1
89
2
61-106/21
91-94-1
3,3'-Dichlorobenzidine
4.7 U
94.3
77.6
82
94.3
70.8
75
9
46-117/29
84-66-2
Diethyl Phthalate
4.7 U
94.3
86.2
91
94.3
83.3
88
3
64-108/21
131-11-3
Dimethyl Phthalate
4.7 U
94.3
86.0
91
94.3
84.9
90
1
63-106/22
* = Outside of Control Limits.
■ 123 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58175-MS
L0684435.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
OP58175-MSD
L0684436.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
FA28818-6
L0684434.1) 1
11/03/15
MV
11/02/15
OP58175
SL3740
The QC reported here applies to the following samples:
Method: SW846 8270D
FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7, FA28901-8, FA28901-9,
FA28901-11, FA28901-12
FA28818-6
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
84-74-2
Di-n-butyl Phthalate
4.7 U
94.3
91.2
97
94.3
89.5
95
2
65-107/21
117-84-0
Di-n-octyl Phthalate
4.7 U
94.3
85.8
91
94.3
85.8
91
0
62-118/24
121-14-2
2,4-Dinitrotoluene
4.7 U
94.3
87.3
93
94.3
83.2
88
5
61-110/21
606-20-2
2,6-Dinitrotoluene
4.7 U
94.3
81.7
87
94.3
78.6
83
4
63-108/21
117-81-7
bis(2-Ethylhexyl)phthalate
4.7 U
94.3
87.8
93
94.3
87.4
93
0
61-117/23
206-44-0
Fluoranthene
4.7 U
94.3
87.7
93
94.3
85.5
91
3
63-106/21
86-73-7
Fluorene
4.7 U
94.3
89.5
95
94.3
86.5
92
3
62-108/20
118-74-1
Hexachlorobenzene
4.7 U
94.3
89.8
95
94.3
90.8
96
1
63-108/22
87-68-3
Hexachlorobutadiene
4.7 U
94.3
66.0
70
94.3
63.7
68
4
42-102/28
77-47-4
Hexachlorocyclopentadiene
4.7 U
94.3
69.9
74
94.3
70.4
75
1
39-102/29
67-72-1
Hexachloroethane
4.7 U
94.3
67.0
71
94.3
63.2
67
6
42-100/29
193-39-5
Indeno(1,2,3-cd)pyrene
4.7 U
94.3
85.8
91
94.3
85.9
91
0
64-119/24
78-59-1
Isophorone
4.7 U
94.3
71.2
75
94.3
70.1
74
2
43-87/25
90-12-0
1-Methylnaphthalene
4.7 U
94.3
75.5
80
94.3
74.7
79
1
53-102/27
91-57-6
2-Methylnaphthalene
4.7 U
94.3
69.7
74
94.3
69.1
73
1
51-102/26
91-20-3
Naphthalene
4.7 U
94.3
67.7
72
94.3
68.0
72
0
47-100/29
98-95-3
Nitrobenzene
4.7 U
94.3
70.1
74
94.3
68.4
73
2
50-104/28
621-64-7
N-Nitrosodi-n-propylamine
4.7 U
94.3
76.5
81
94.3
73.3
78
4
52-104/25
86-30-6
N-Nitrosodiphenylamine
4.7 U
94.3
90.4
96
94.3
88.7
94
2
64-108/23
85-01-8
Phenanthrene
4.7 U
94.3
93.3
99
94.3
90.1
96
3
66-110/21
129-00-0
Pyrene
4.7 U
94.3
86.4
92
94.3
83.7
89
3
64-113/23
CAS No.
Surrogate Recoveries
MS
MSD
FA28818-6
Limits
367-12-4
2-Fluorophenol
71%* a
60%
38%
14-67%
4165-62-2
Phenol-d5
61% * a
50%
27%
10-50%
118-79-6
2,4,6-Tribromophenol
97%
95%
91%
33-118%
4165-60-0
Nitrobenzene-d5
71%
71%
64%
42-108%
321-60-8
2-Fluorobiphenyl
86%
83%
72%
40-106%
1718-51-0
Terphenyl-d14
93%
91%
72%
39-121%
(a) Outside control limits.
* = Outside of Control Limits.
■ 124 of 143
E ACC UTEST
FA28901

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58211-MS
X043259.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
OP58211-MSD
X043260.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
FA28922-17
X043258.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples:
FA28901-13, FA28901-14, FA28901-15, FA28901-16
CAS No. Compound
FA28922-17 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8270D
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
100
29.5
30
100
33.1
33
12
10-69/39
59-50-7
4-Chloro-3-methyl Phenol
ND
50
34.4
69
50
33.6
67
2
54-103/23
95-57-8
2-Chlorophenol
ND
50
31.5
63
50
29.5
59
7
52-98/25
120-83-2
2,4-Dichlorophenol
ND
50
33.9
68
50
32.3
65
5
53-103/26
105-67-9
2,4-Dimethylphenol
ND
50
25.2
50
50
24.7
49
2
43-90/27
51-28-5
2,4-Dinitrophenol
ND
100
67.7
68
100
66.6
67
2
44-112/25
534-52-1
4,6-Dinitro-o-cresol
ND
100
77.1
77
100
74.3
74
4
66-121/23
95-48-7
2-Methylphenol
ND
50
29.2
58
50
27.6
55
6
43-90/28
3&4-Methylphenol
ND
100
57.3
57
100
54.1
54
6
36-88/28
88-75-5
2-Nitrophenol
ND
50
33.9
68
50
32.8
66
3
53-102/29
100-02-7
4-Nitrophenol
ND
100
47.4
47
100
42.5
43
11
18-62/33
87-86-5
Pentachlorophenol
ND
100
79.2
79
100
77.2
77
3
61-115/26
108-95-2
Phenol
ND
50
20.8
42
50
18.4
37
12
19-56/35
88-06-2
2,4,6-Trichlorophenol
ND
50
35.0
70
50
33.9
68
3
59-107/23
83-32-9
Acenaphthene
ND
50
36.2
72
50
35.2
70
3
61-107/22
208-96-8
Acenaphthylene
ND
50
34.2
68
50
33.3
67
3
60-104/22
120-12-7
Anthracene
ND
50
35.8
72
50
35.3
71
1
65-108/20
56-55-3
Benzo(a)anthracene
ND
50
36.5
73
50
35.7
71
2
66-111/22
50-32-8
Benzo(a)pyrene
ND
50
37.4
75
50
36.1
72
4
62-107/23
205-99-2
Benzo(b)fluoranthene
ND
50
37.5
75
50
36.3
73
3
65-114/23
191-24-2
Benzo(g, h, i)perylene
ND
50
30.4
61*
50
28.9
58*
5
66-116/23
207-08-9
Benzo(k)fluoranthene
ND
50
37.4
75
50
35.6
71
5
65-114/24
101-55-3
4-BromophenylPhenyl Ether
ND
50
35.5
71
50
34.0
68
4
65-109/23
85-68-7
Butyl Benzyl Phthalate
ND
50
37.1
74
50
36.5
73
2
65-112/24
106-47-8
4-Chloroaniline
ND
50
33.7
67
50
32.5
65
4
49-105/27
111-91-1
bis(2-Chloroethoxy)methane
ND
50
33.2
66
50
32.2
64
3
51-102/28
111-44-4
bis(2-Chloroethyl)ether
ND
50
31.7
63
50
30.3
61
5
53-100/27
108-60-1
bis(2-Chloroisopropyl)ether
ND
50
33.6
67
50
32.6
65
3
45-106/26
91-58-7
2-Chloronaphthalene
ND
50
34.5
69
50
33.1
66
4
57-103/23
7005-72-3
4-ChlorophenylPhenyl Ether
ND
50
35.8
72
50
34.4
69
4
62-105/20
218-01-9
Chrysene
ND
50
38.2
76
50
36.9
74
3
66-111/22
53-70-3
Dibenzo(a,h)anthracene
ND
50
35.4
71
50
34.5
69
3
66-119/24
132-64-9
Dibenzofuran
ND
50
36.2
72
50
34.9
70
4
61-106/21
91-94-1
3,3'-Dichlorobenzidine
ND
50
35.6
71
50
33.0
66
8
46-117/29
84-66-2
Diethyl Phthalate
ND
50
36.3
73
50
35.2
70
3
64-108/21
131-11-3
Dimethyl Phthalate
ND
50
35.9
72
50
34.4
69
4
63-106/22
* = Outside of Control Limits.
■■ 125 of 143
M A DMUTEST
FA28901 LA...A - 1-

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA28901
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P58211-MS
X043259.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
)P58211-MSD
X043260.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
'A28922-17
X043258.13
1
11/04/15
MV
11/04/15
OP58211
SX1956
The QC reported here applies to the following samples: Method: SW846 8270D
FA28901-13, FA28901-14, FA28901-15, FA28901-16
FA28922-17 Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l
Q ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
84-74-2
Di-n-butyl Phthalate
ND
50
37.4
75
50
37.0
74
1
65-107/21
117-84-0
Di-n-octyl Phthalate
ND
50
36.0
72
50
35.3
71
2
62-118/24
121-14-2
2,4-Dinitrotoluene
ND
50
37.7
75
50
36.5
73
3
61-110/21
606-20-2
2,6-Dinitrotoluene
ND
50
35.4
71
50
33.9
68
4
63-108/21
117-81-7
bis(2-Ethylhexyl)phthalate
1.1
J 50
37.7
73
50
36.8
71
2
61-117/23
206-44-0
Fluoranthene
ND
50
36.3
73
50
35.0
70
4
63-106/21
86-73-7
Fluorene
ND
50
37.2
74
50
35.6
71
4
62-108/20
118-74-1
Hexachlorobenzene
ND
50
35.2
70
50
33.9
68
4
63-108/22
87-68-3
Hexachlorobutadiene
ND
50
32.8
66
50
29.9
60
9
42-102/28
77-47-4
Hexachlorocyclopentadiene
ND
50
28.9
58
50
29.8
60
3
39-102/29
67-72-1
Hexachloroethane
ND
50
30.7
61
50
28.4
57
8
42-100/29
193-39-5
Indeno(1,2,3-cd)pyrene
ND
50
33.6
67
50
33.4
67
1
64-119/24
78-59-1
Isophorone
ND
50
33.7
67
50
32.9
66
2
43-87/25
90-12-0
1-Methylnaphthalene
ND
50
36.5
73
50
35.0
70
4
53-102/27
91-57-6
2-Methylnaphthalene
ND
50
33.6
67
50
32.7
65
3
51-102/26
91-20-3
Naphthalene
ND
50
32.9
66
50
31.0
62
6
47-100/29
98-95-3
Nitrobenzene
ND
50
33.3
67
50
31.9
64
4
50-104/28
621-64-7
N-Nitrosodi-n-propylamine
ND
50
34.1
68
50
33.2
66
3
52-104/25
86-30-6
N-Nitrosodiphenylamine
ND
50
35.8
72
50
35.4
71
1
64-108/23
85-01-8
Phenanthrene
ND
50
36.3
73
50
35.6
71
2
66-110/21
129-00-0
Pyrene
ND
50
36.2
72
50
35.2
70
3
64-113/23
CAS No.
Surrogate Recoveries
MS
MSD
FA28922-17
Limits
367-12-4
2-Fluorophenol
50%
45%
33%
14-67%
4165-62-2
Phenol-d5
42%
37%
23%
10-50%
118-79-6
2,4,6-Tribromophenol
70%
66%
59%
33-118%
4165-60-0
Nitrobenzene-d5
64%
61%
58%
42-108%
321-60-8
2-Fluorobiphenyl
66%
64%
57%
40-106%
1718-51-0
Terphenyl-d14
77%
74%
73%
39-121%
* = Outside of Control Limits.
■■ 126 of 143
ACCUTEST
FA28907

Section 7
Southeast
ACCUTEST
L A B O RAT 0 R I ES
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
■ ,i 127 of 143
E ACCUTEBT
FA28901 `..... I..

BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29604 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date:
MB
letal RL IDL MDL raw final
Mercury 0.50 .03 .03 0.0084 <0.50
Associated samples MP29604: FA28901-6, FA28901-7, FA28901-8, FA28901-9
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
N
Page 1
■ 128 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29604 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28922-17 QC FA28922-17 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWSI % Rec Limits
Mercury 0.0 0.0 NC 0-20 0.0 3.0 3 100.0 80-120
Associated samples MP29604: FA28901-6, FA28901-7, FA28901-8, FA28901-9
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
V
i
N
N
Page 1
■ 129 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29604 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28922-17 Spikelot MSD QC
letal Original MSD HGFLWSI % Rec RPD Limit
Mercury 0.0 3.1 3 103.3 3.3 20
Associated samples MP29604: FA28901-6, FA28901-7, FA28901-8, FA28901-9
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
V
W
Page 2
■ 130 of 143
E ACC UTEST
FA28901

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29604 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
BSP Spikelot QC
letal Result HGFLWSI o Rec Limits
Mercury 3.0 3 100.0 80-120
Associated samples MP29604: FA28901-6, FA28901-7, FA28901-8, FA28901-9
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
W
Page 1
■■ 131 of 143
M ACCUTEST
FA28901 LA...A - 1-

SERIAL DILUTION RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29604 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28922-17 QC
letal Original SDL 1:5 oDIF Limits
Mercury 0.00 0.00 NC 0-10
Associated samples MP29604: FA28901-6, FA28901-7, FA28901-8, FA28901-9
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
Page 1
■■ 132 of 143
M ACCUTEST
FA28901 LA...A - 1-

BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29608 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
MB
letal RL IDL MDL raw final
Mercury 0.50 .03 .03 0.016 <0.50
Associated samples MP29608: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
W
Page 1
■ 133 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29608 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date:
FA28901-3 QC FA28901-3 Spikelot QC
letal Original DUP RPD Limits Original MS HGFLWSI % Rec Limits
Mercury 1.2 1.1 8.7 0-20 1.2 3.7 3 83.3 80-120
Associated samples MP29608: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
V
N
N
Page 1
■ 134 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29608 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28901-3 Spikelot MSD QC
letal Original MSD HGFLWSI % Rec RPD Limit
Mercury 1.2 3.8 3 86.7 2.7 20
Associated samples MP29608: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
V
N
N
Page 2
■■ 135 of 143
ACCUTEST
FA28907

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29608 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
BSP Spikelot QC
letal Result HGFLWSI o Rec Limits
Mercury 3.0 3 100.0 80-120
Associated samples MP29608: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
N
W
Page 1
■■ 136 of 143
ACCUTEST
FA28907

SERIAL DILUTION RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29608 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28901-3 QC
letal Original SDL 1:5 oDIF Limits
Mercury 1.18 1.27 7.6 0-10
Associated samples MP29608: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
N
Page 1
■■ 137 of 143
M ACCUTEST
FA28901 LA...A - 1-

BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
MB
letal RL IDL MDL raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3 -0.80 <10
Barium 200 1 1 -0.10 <200
Beryllium 4.0 .2 .2
Cadmium 5.0 .2 .2 0.0 <5.0
Calcium 1000 50 50
Chromium 10 1 1 0.0 <10
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 17 17
Lead 5.0 1 1.1 -0.10 <5.0
Magnesium 5000 35 35
Manganese 15 .5 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 200 200
Selenium 10 2.4 2.9 1.7 <10
Silver 10 .7 .7 0.20 <10
Sodium 10000 500 500
Strontium 10 .5 .5
Thallium 10 1.1 1.4
Tin 50 .9 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP29610: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7,
FA28901-8, FA28901-9, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
W
Page 1
■ 138 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28868-3 QC FA28868-3 Spikelot QC
letal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum am
Antimony am
Arsenic 0.0 0.0
NC
0-20
0.0
1970
2000
98.5
80-120
Barium 73.9 72.5
1.9
0-20
73.9
2160
2000
104.3
80-120
Beryllium am
Cadmium 0.0 0.0
NC
0-20
0.0
50.4
50
100.8
80-120
Calcium am
Chromium 5.2 5.1
1.9
0-20
5.2
209
200
101.9
80-120
Cobalt am
Copper am
Iron am
Lead 1.6 1.3
20.7
(a) 0-20
1.6
497
500
99.1
80-120
Magnesium am
Manganese am
Molybdenum
Nickel am
Potassium am
Selenium 0.0 0.0
NC
0-20
0.0
1980
2000
99.0
80-120
Silver 0.0 0.0
NC
0-20
0.0
48.8
50
97.6
80-120
Sodium am
Strontium
Thallium am
Tin
Titanium
Vanadium am
Zinc am
Associated samples MP29610: FA28901-1,
FA28901-2,
FA28901-3,
FA28901-4,
FA28901-5,
FA28901-6, FA28901-7,
FA28901-8, FA28901-9, FA28901-17
Results < IDL are shown as zero for calculation
purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside
of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low
duplicate
and sample
concentrations.
V
W
N
Page 1
■ 139 of 143
E ACC UTEST
FA28901

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
FA28868-3 Spikelot MSD QC
letal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum am
Antimony am
Arsenic 0.0 1960 2000 98.0 0.5 20
Barium 73.9 2150 2000 103.8 0.5 20
Beryllium am
Cadmium 0.0 50.2 50 100.4 0.4 20
Calcium am
Chromium 5.2 210 200 102.4 0.5 20
Cobalt am
Copper am
Iron am
Lead 1.6 494 500 98.5 0.6 20
Magnesium am
Manganese am
Molybdenum
Nickel am
Potassium am
Selenium 0.0 1970 2000 98.5 0.5 20
Silver 0.0 48.5 50 97.0 0.6 20
Sodium am
Strontium
Thallium am
Tin
Titanium
Vanadium am
Zinc am
Associated samples MP29610: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7,
FA28901-8, FA28901-9, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
V
W
N
Page 2
■ 140 of 143
E ACC UTEST
FA28901

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
BSP Spikelot QC
letal Result MPFLICP2 % Rec Limits
Aluminum am
Antimony am
Arsenic 2010 2000 100.5 80-120
Barium 2100 2000 105.0 80-120
Beryllium am
Cadmium 51.4 50 102.8 80-120
Calcium am
Chromium 208 200 104.0 80-120
Cobalt am
Copper am
Iron am
Lead 494 500 98.8 80-120
Magnesium am
Manganese am
Molybdenum
Nickel am
Potassium am
Selenium 2020 2000 101.0 80-120
Silver 50.0 50 100.0 80-120
Sodium am
Strontium
Thallium am
Tin
Titanium
Vanadium am
Zinc am
Associated samples MP29610: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7,
FA28901-8, FA28901-9, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
V
W
W
Page 1
■■ 141 of 143
ACCUTEST
FA28907

SERIAL DILUTION RESULTS SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/l
Prep Date:
FA28868-3 QC
letal Original SDL 1:5 %DIF Limits
Aluminum am
Antimony am
Arsenic 0.00 0.00 NC 0-10
Barium 73.9 76.9 4.1 0-10
Beryllium am
Cadmium 0.00 0.00 NC 0-10
Calcium am
Chromium 5.20 5.00 3.8 0-10
Cobalt am
Copper am
Iron am
Lead 1.60 0.00 100.0(a) 0-10
Magnesium am
Manganese am
Molybdenum
Nickel am
Potassium am
Selenium 0.00 0.00 NC 0-10
Silver 0.00 0.00 NC 0-10
Sodium am
Strontium
Thallium am
Tin
Titanium
Vanadium am
Zinc am
Associated samples MP29610: FA28901-1, FA28901-2, FA28901-3, FA28901-4, FA28901-5, FA28901-6, FA28901-7,
FA28901-8, FA28901-9, FA28901-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
v
W
Page 1
■■ 142 of 143
M ACCUTEST
FA28901 LA...A - 1-

POST DIGESTATE SPIKE SUMMARY
Login Number: FA28901
Account: GRINCC - GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
QC Batch ID: MP29610 Methods: SW846 6010C
Matrix Type: AQUEOUS Units: ug/1
Prep Date:
Sample Final FA28868-3 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l o Rec Limits
Aluminum
Antimony
Arsenic
9.8
10
101.1
0.2
5
100
101.1
80-120
Barium
9.8
10
73.9 72.422
336.3
.2
12.5
250
105.6
80-120
Beryllium
Cadmium
9.8
10
50.2
0.2
2.5
50
100.4
80-120
Calcium
Chromium
9.8
10
5.2 5.096
55.4
0.2
2.5
50
100.6
80-120
Cobalt
Copper
Iron
Lead
9.8
10
1.6 1.568
49.4
.2
2.5
50
95.7
80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
9.8
10
97
0.2
5
100
97.0
80-120
Silver
9.8
10
45.5
0.2
2.5
50
91.0
80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated
samples
MP29610: FA28901-1,
FA28901-2,
FA28901-3,
FA28901-4, FA28901-5,
FA28901-6,
FA28901-7,
FA28901-8,
FA28901-9,
FA28901-17
Results < IDL
are
shown as zero
for calculation purposes
(*) Outside
of QC
limits
(**) Corr.
sample
result = Raw
* (sample volume
/ final
volume)
(anr) Analyte
not
requested
V
W
C71
Page 1
■ 143 of 143
E ACC UTEST
FA28901

e Hardcopy 2.0
Automated Report
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
Technical Report for
GRI (Geological Resources Inc.)
2116 E Glenburnie Rd, New Bern, NC
3841/1775
Accutest Job Number: FA29125
Sampling Date: 11/09/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
com;
ATTN: James Wellon
com;
Total number of pages in report: 22
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
sine. com
Norm Farmer
Technical Director
Client Service contact: Muna Mohammed 407-425-6700
com;
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
http://www.accutest.com
■■ 1 of 22
ACCUTEST
FA29125

Table of Contents
Sections:
-I-
Section1: Sample Summary...................................................................................................
Section2: Summary of Hits....................................................................................................
Section3: Sample Results........................................................................................................
3.1: FA29125-1: 3608 TRENT............................................................................................
Section4: Misc. Forms............................................................................................................
4.1: Chain of Custody...........................................................................................................
Section 5: GUMS Volatiles - QC Data Summaries..............................................................
5.1: Method Blank Summary................................................................................................
5.2: Blank Spike Summary...................................................................................................
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section 6: GUMS Semi-volatiles - QC Data Summaries.....................................................
6.1: Method Blank Summary................................................................................................
6.2: Blank Spike Summary...................................................................................................
3
4
5
6
9
10
13
14
16
18
20
21
22
2 of 22
ACCUTEST
FA29125

Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA29125
2116 E Glenburnie Rd, New Bern, NC
Project No: 3841/1775
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA29125-1 11/09/15 14:54 DG 11/10/15 AQ Ground Water 3608 TRENT
■ 3 of 22
E ACCUTEST
FA29125 LPBORATOR15

Summary of Hits
Job Number:
FA29125
Account:
GRI (Geological Resources Inc.)
Project:
2116 E Glenburnie Rd, New Bern, NC
Collected:
11/09/ 15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA29125-1 3608 TRENT
No hits reported in this sample.
Page 1 of l
4 of 22
ACCUTEST
FA29125

Section 3
Southeast
■,ZS,ccuTEST
L A H OR AT OR E E 5
Sample Results
Report of Analysis
■■ 5 of 22
ACCUTEST«
FA29125 `"a°""'- E.

Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID: 3608 TRENT
Lab Sample ID: FA29125-1 Date Sampled: 11/09/15
Matrix: AQ - Ground Water Date Received: I l/10/15
Method: SW846 8260B Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a P37009.D 1 11/12/15 KM n/a n/a VP1374
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/1
71-43-2
Benzene
ND
1.0
0.20
ug/1
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/1
75-25-2
Bromoform
ND
1.0
0.32
ug/1
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/1
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/1
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/1
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/1
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/1
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/1
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/1
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/1
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/1
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/1
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/1
156-59-2
cis-1,2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5
cis- 1, 3 -Dichloropropene
ND
1.0
0.25
ug/1
10061-02-6
trans- 1, 3 -Dichloropropene
ND
1.0
0.26
ug/1
100-41-4
Ethlbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/1
79-20-9
Methyl Acetate
ND
20
5.0
ug/1
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 6 of 22
ACCUTEST
FA29125

Accutest Laboratories
Report of Analysis
'lient Sample ID: 3608 TRENT
,ab Sample ID: FA29125-1 Date Sampled: 11/09/15
Ratrix: AQ - Ground Water Date Received: I l/10/15
lthod: SW846 8260B Percent Solids: n/a
'roject: 2116 E Glenburnie Rd, New Bern, NC
VOA Special List
CAS No. Compound Result RL MDL Units Q
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/1
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/1
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/1
108-10-1
4-Methyl-2-pentanone (MIBK) ND
5.0
1.0
ug/1
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1 -Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
83-118%
17060-07-0
1,2-Dichloroethane-D4
104%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
100%
83-118%
(a) Sample was not preserved to a pH < 2.
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 7 of 22
ACCUTEST
FA29125

Accutest Laboratories
Report of Analysis
Client Sample ID: 3608 TRENT
Lab Sample ID: FA29125-1 Date Sampled: 11/09/15
Matrix: AQ - Ground Water Date Received: I l/10/15
Method: SW846 8270D BY SIM SW846 3510C Percent Solids: n/a
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 W090100.1) 1 11/11/15 NJ 11/11/15 OP58301 SW4100
Run #2
Initial Volume Final Volume
Run #1 950 ml 1.0 ml
Run #2
BN PAH List
CAS No.
Compound
Result
RL
MDL
Units Q
83-32-9
Acenaphthene
ND
1.1
0.42
ug/1
208-96-8
Acenaphthylene
ND
1.1
0.42
ug/1
120-12-7
Anthracene
ND
1.1
0.26
ug/1
56-55-3
Benzo(a)anthracene
ND
0.21
0.042
ug/1
50-32-8
Benzo(a)pyrene
ND
0.21
0.042
ug/1
205-99-2
Benzo(b)fluoranthene
ND
0.21
0.042
ug/1
191-24-2
Benzo(g, h, i)perylene
ND
0.21
0.042
ug/1
207-08-9
Benzo(k)fluoranthene
ND
0.21
0.042
ug/1
218-01-9
Chrysene
ND
0.21
0.042
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
0.21
0.042
ug/1
206-44-0
Fluoranthene
ND
1.1
0.26
ug/1
86-73-7
Fluorene
ND
L I
0.42
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.21
0.042
ug/1
90-12-0
1-Methylnaphthalene
ND
1.1
0.42
ug/1
91-57-6
2-Methylnaphthalene
ND
1.1
0.42
ug/1
91-20-3
Naphthalene
ND
1.1
0.42
ug/1
85-01-8
Phenanthrene
ND
1.1
0.26
ug/1
129-00-0
Pyrene
ND
1.1
0.26
ug/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
4165-60-0
Nitrobenzene-d5
75%
42-108%
321-60-8
2-Fluorobiphenyl
77%
40-106%
1718-51-0
Terphenyl-d14
84%
39-121%
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 8 of 22
ACCUTEST
FA29125

Section 4
Southeast
E ACCUTEST
L A B O RAT D R I ES
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
■■ 9 of 22
ACCUTEST
FA29125 LPBDRATOR15

.® Accutest Laboratories Noutneast
Chain of Custody Accutest JOB #(A AlP SAGEj__OF_f_
EACGCUTEST 4405 Vineland Road, Suite C-15 Orlando, 32811
LABORATORIES TLL- 407-425-6700 • FAX: [phone]
www.accutest.com
CCUte$t Dote
Re
Client/ orti Information ,;,,..„ rn J ..,
yName
y Project Information
Anal ical Information
-�
Matrix Codes
Company (3
Project Name: [ l-� Nd
po
rJ
N
DW- Ddnldng Water
GW-Ground Water
SW WW ace - Water
water
so -loll
sL-Sludge
of -oil
LIO - Other Liquid
AIR - Air
SOL - Other Shcd
WP - Wide
Address
�.tt ++
OIL! 4. werlwr��e_�
Cit State Zi �+
ciry
Protect Contact E-mail
rwAPT
prgact# ;yy,
3
Ph°ne#
Fax N
Sampler(S) Name(s) (Punted)
il, r l (AOO
Client Purchase Order #
I
Accutaet
S #
Field ID / Point of Collection
snma�eo
nix
T oP p
a:
Crete l9-151
H
(�
6�r
v
:at,TURNAROUND
IL
TIME Business Days)Data
Deliverable
Information
°'.'i,
r
Comments
/Remarks
10 Days Standard Approved By: ! Rush Code-
❑ 7 Day RUSH _
5 Day RUSH
❑ 3 Day EMERGENCY
❑ 2 Day EMERGENCY _
❑ 1 Day EMERGENCY
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Emergency or Rush T/A Data Available VIA Email or Lablink
COMMERCIAL "A" (RESULTS ONLY)
COMMERCIAL "B" (RESULTS PLUS QC)
REDT1 (EPA LEVEL 3)
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EDD'S
Sam
le Custodv must be documented
below
each time samples chancie possossion.
includina courier delivery
Reli lshed b
pier:
Date Time: p
Received By: Relinquished
15
by :
Date Time:
Rec Tved By:
Relinquished by:
5
Date Time:
Received By:
6 7
Relinquished by:
Date Time:
Received By:
1 8
Lab Use Only: Custody Seal in Place: Y N Temp Blank Provided: Y N Preserved where Applicable:Y N Total # of Coolers: Cooler Temperature (s) Celsius:
FA29125: Chain of Custody
Page 1 of 3
0
■■ 10 of 22
E ACCUTEBT
FA29125 LABORATOR15

ACppCUTEjST LABORATORIES SAMPLE RECEIPT CONFIRMATIION
ACCUTEST'SJOB NUMBER : /ti I
CLIENT: 6d, 1 PROJECT: /
_
DATE/TIME RECEIVED: I� IO -I S _ (MM/DD/VY 24:00) NUMBER OF COOLERS RECEIVED:
METHOD OF DELIVERY: FEDEX UPS
ACCUTEST COURIER DELIVERY OTHER:
AIRBILL NUMBERS: 01043 `J 7-f g
COOLER INFORMATION
TEMPERATURE INFORMATION
CUSTODY SEAL NOT PRESENT OR NOT INTACT
IR THERM ID�_ CORR. FACTOR •- (i,
CHAIN OF CUSTODY NOT RECEIVED (COC)
OBSERVED TEMPS: 3-6
NCORRECTED
ANALYSIS REQUESTED IS UNCLEAR OR MISSING
TEMPS: • 2
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
SAMPLE INFORMATION
TEMPERATURE CRITERIA NOT MET .
INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
TRIP BLANK INFORMATION
INSUFFICIENT VOLUME FOR ANALYSIS
TRIP BLANK PROVIDED
DATES/CIMES ON COC DO NOT MATCH SAMPLE LABEL
TRIP BLANK NOT PROVIDED
ID'S ON COC DO NOT MATCH LABEL
TRIP BLANK NOT ON COC
VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
TRIP BLANK INTACT
BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
TRIP BLANK NOT INTACT
NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED
RECEIVED WATER TRIP BLANK
UNCLEAR FILTERING OR COMPOSITING INSTRUCTIONS
RECEIVED SOIL TRIP BLANK
SAMPLE CONTAINER(S) RECEIVED BROKEN
5035 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
MISC. INFORMATION
BULK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS
NUMBER OF ENCORES ? 25-GRAM 5-GRAM
% SOLIDS JAR NOT RECEIVED
NUMBER OF 5035 FIELD KITS ?
RESIDUAL CHLORINE PRESENT LOT#
NUMBER OF LAB FILTERED METALS ?
(APPLICABLE TO EPA 600 SERIES OR NORTH CAROLINA ORGANICS)
pH PAPER LOT#s WIDI HC 131225
NARROW RANGE AO36133_ OTHER (specify) 4057230010
SUMMARY OF COMMENTS: I/Ab
hfL 6,2
TECHNICIAN SIGNATURE/DATE
REVIEWER SIGNATURE/DATE-
NF 10/14
YELLOWSHEET110514.xis
FA29125: Chain of Custody
Page 2 of 3
■■ 11 of 22
ACCUTEST
FA29125

ORIGIN 1D=PGVA SHIP DATE= OSNOVIS
ACTWGT 11 .90 LB
CRD lPDS 1621
;DIRS= 11x9x11 IN
BILL SENDER
UNITED STATES US
TO SAMPLE RECEIVING
ACCUTEST LABS411
4405 VINELAND RD g
STE C15
ORLANDO FL 32811
�Q0 425-6700 REF;
• Pa. Rrv1:
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TUE -10 NOV 3:00P
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FA29125: Chain of Custody
Page 3 of 3
■■ 12 of 22
ACCUTEST
FA29125 LA...AT— E.

Section 5
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
GUMS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
■■ 13 of 22
ACCUTEST•
FA29125 "°°""'°""•

Method Blank Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1374-MB
P36997.D
1
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples: Method: SW846 8260B
FA29125-1
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
ND
25
10
ug/l
71-43-2
Benzene
ND
1.0
0.20
ug/l
75-27-4
Bromodichloromethane
ND
1.0
0.22
ug/l
75-25-2
Bromoform
ND
1.0
0.32
ug/l
78-93-3
2-Butanone (MEK)
ND
5.0
1.2
ug/l
104-51-8
n-Butylbenzene
ND
1.0
0.22
ug/1
75-15-0
Carbon Disulfide
ND
2.0
0.29
ug/1
56-23-5
Carbon Tetrachloride
ND
1.0
0.28
ug/1
108-90-7
Chlorobenzene
ND
1.0
0.20
ug/l
75-00-3
Chloroethane
ND
2.0
0.50
ug/1
67-66-3
Chloroform
ND
1.0
0.30
ug/1
110-82-7
Cyclohexane
ND
1.0
0.20
ug/1
124-48-1
Dibromochloromethane
ND
1.0
0.20
ug/1
96-12-8
1,2-Dibromo-3-chloropropane
ND
2.0
0.61
ug/l
106-93-4
1,2-Dibromoethane
ND
2.0
0.42
ug/l
75-71-8
Dichlorodifluoromethane
ND
2.0
0.50
ug/l
95-50-1
1,2-Dichlorobenzene
ND
1.0
0.22
ug/l
541-73-1
1,3-Dichlorobenzene
ND
1.0
0.22
ug/l
106-46-7
1,4-Dichlorobenzene
ND
1.0
0.25
ug/l
75-34-3
1, 1 -Dichloroethane
ND
1.0
0.20
ug/l
107-06-2
1,2-Dichloroethane
ND
1.0
0.20
ug/l
75-35-4
1, 1 -Dichloroethylene
ND
1.0
0.27
ug/l
156-59-2
cis- 1, 2-Dichloroethylene
ND
1.0
0.22
ug/1
156-60-5
trans- 1, 2-Dichloroethylene
ND
1.0
0.21
ug/1
78-87-5
1,2-Dichloropropane
ND
1.0
0.25
ug/1
10061-01-5 cis- 1, 3-Dichloropropene
ND
1.0
0.25
ug/l
10061-02-6 trans- 1, 3-Dichloropropene
ND
1.0
0.26
ug/l
100-41-4
Ethylbenzene
ND
1.0
0.20
ug/1
591-78-6
2-Hexanone
ND
10
2.0
ug/1
98-82-8
Isopropylbenzene
ND
1.0
0.20
ug/l
79-20-9
Methyl Acetate
ND
20
5.0
ug/l
74-83-9
Methyl Bromide
ND
2.0
0.50
ug/l
74-87-3
Methyl Chloride
ND
2.0
0.50
ug/l
108-87-2
Methylcyclohexane
ND
1.0
0.22
ug/l
75-09-2
Methylene Chloride
ND
5.0
2.0
ug/l
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
5.0
1.0
ug/l
■■ 14 of 22
ACCUTEST«
FA29125

Method Blank Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1374-MB
P36997.D
1
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples: Method: SW846 8260B
FA29125-1
CAS No.
Compound
Result
RL
MDL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
1.0
0.30
ug/1
91-20-3
Naphthalene
ND
5.0
1.0
ug/1
103-65-1
n-Propylbenzene
ND
1.0
0.20
ug/1
100-42-5
Styrene
ND
1.0
0.28
ug/1
79-34-5
1,1,2,2-Tetrachloroethane
ND
1.0
0.22
ug/1
127-18-4
Tetrachloroethylene
ND
1.0
0.33
ug/1
108-88-3
Toluene
ND
1.0
0.40
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
1.0
0.50
ug/1
71-55-6
1, 1, 1-Trichloroethane
ND
1.0
0.26
ug/1
79-00-5
1,1,2-Trichloroethane
ND
1.0
0.31
ug/1
79-01-6
Trichloroethylene
ND
1.0
0.22
ug/1
75-69-4
Trichlorofluoromethane
ND
2.0
0.50
ug/1
95-63-6
1,2,4-Trimethylbenzene
ND
2.0
0.20
ug/1
108-67-8
1,3,5-Trimethylbenzene
ND
2.0
0.22
ug/1
75-01-4
Vinyl Chloride
ND
1.0
0.25
ug/1
1330-20-7
Xylene (total)
ND
3.0
0.51
ug/1
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
100%
83-118%
17060-07-0
1,2-Dichloroethane-D4
102%
79-125%
2037-26-5
Toluene-D8
99%
85-112%
460-00-4
4-Bromofluorobenzene
102%
83-118%
CAS No.
Tentatively Identified Compounds
R.T.
Est.
Conc. Units Q
Total TIC, Volatile a
0
ug/1
(a) No TICS detected.
15 of 22
ACCUTEST
FA29125

Blank Spike Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1374-BS
P36996.D
1
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples: Method: SW846 8260B
FA29125-1
CAS No. Compound
Spike BSP BSP
ug/1 ug/1 % Limits
67-64-1
Acetone
125
114
91
50-147
71-43-2
Benzene
25
25.6
102
81-122
75-27-4
Bromodichloromethane
25
27.2
109
79-123
75-25-2
Bromoform
25
25.5
102
66-123
78-93-3
2-Butanone (MEK)
125
114
91
56-143
104-51-8
n-Butylbenzene
25
27.2
109
79-126
75-15-0
Carbon Disulfide
25
23.0
92
66-148
56-23-5
Carbon Tetrachloride
25
28.3
113
76-136
108-90-7
Chlorobenzene
25
26.2
105
82-124
75-00-3
Chloroethane
25
30.0
120
62-144
67-66-3
Chloroform
25
26.3
105
80-124
110-82-7
Cyclohexane
25
27.2
109
73-138
124-48-1
Dibromochloromethane
25
26.7
107
78-122
96-12-8
1,2-Dibromo-3-chloropropane
25
22.2
89
64-123
106-93-4
1,2-Dibromoethane
25
25.5
102
75-120
75-71-8
Dichlorodifluoromethane
25
34.0
136
42-167
95-50-1
1,2-Dichlorobenzene
25
26.2
105
82-124
541-73-1
1,3-Dichlorobenzene
25
26.3
105
84-125
106-46-7
1,4-Dichlorobenzene
25
26.3
105
78-120
75-34-3
1, 1 -Dichloroethane
25
27.1
108
81-122
107-06-2
1,2-Dichloroethane
25
25.6
102
75-125
75-35-4
1, 1 -Dichloroethylene
25
27.1
108
78-137
156-59-2
cis- 1, 2-Dichloroethylene
25
24.9
100
78-120
156-60-5
trans- 1, 2-Dichloroethylene
25
28.5
114
76-127
78-87-5
1,2-Dichloropropane
25
25.3
101
76-124
10061-01-5 cis- 1, 3-Dichloropropene
25
25.9
104
75-118
10061-02-6 trans- 1, 3-Dichloropropene
25
27.8
111
80-120
100-41-4
Ethylbenzene
25
26.7
107
81-121
591-78-6
2-Hexanone
125
109
87
61-129
98-82-8
Isopropylbenzene
25
27.8
111
83-132
79-20-9
Methyl Acetate
125
116
93
65-126
74-83-9
Methyl Bromide
25
26.6
106
59-143
74-87-3
Methyl Chloride
25
27.6
110
50-159
108-87-2
Methylcyclohexane
25
29.5
118
76-129
75-09-2
Methylene Chloride
25
26.5
106
69-135
108-10-1
4-Methyl-2-pentanone (MIBK)
125
113
90
66-122
* = Outside of Control Limits.
■■ 16 of 22
ACCUTEST«
FA29125

Blank Spike Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VP1374-BS
P36996.D
1
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples: Method: SW846 8260B
FA29125-1
CAS No. Compound
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
79-34-5
1,1,2,2-Tetrachloroethane
127-18-4
Tetrachloroethylene
108-88-3
Toluene
120-82-1
1,2,4-Trichlorobenzene
71-55-6
1, 1, 1-Trichloroethane
79-00-5
1,1,2-Trichloroethane
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
75-01-4
Vinyl Chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
* = Outside of Control Limits.
Spike
BSP
BSP
ug/l
ug/l
%
Limits
25
25.6
102
72-117
25
24.5
98
63-132
25
27.5
110
82-133
25
25.8
103
78-119
25
23.1
92
72-120
25
27.5
110
76-135
25
26.4
106
80-120
25
26.2
105
73-129
25
27.2
109
75-130
25
25.2
101
76-119
25
26.9
108
81-126
25
28.3
113
71-156
25
26.3
105
79-120
25
25.9
104
79-120
25
28.6
114
69-159
75
80.8
108
80-126
BSP Limits
100% 83-118%
101% 79-125%
100% 85-112%
99% 83-118%
■■ 17 of 22
ACCUTEST
FA29125

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA29094-4MS
P37018.13
50
11/12/15
KM
n/a
n/a
VP1374
FA29094-4MSD
P37019.13
50
11/12/15
KM
n/a
n/a
VP1374
FA29094-4
P37005.13
50
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples:
FA29125-1
CAS No. Compound
FA29094-4 Spike MS
ug/l Q ug/l ug/l
Method: SW846 8260B
MS Spike MSD MSD Limits
% ug/l ug/l % RPD Rec/RPD
67-64-1
Acetone
1300 U
6250
5910
95
6250
5580
89
6
50-147/21
71-43-2
Benzene
50 U
1250
1360
109
1250
1350
108
1
81-122/14
75-27-4
Bromodichloromethane
50 U
1250
1510
121
1250
1470
118
3
79-123/19
75-25-2
Bromoform
50 U
1250
1360
109
1250
1320
106
3
66-123/21
78-93-3
2-Butanone(MEK)
250 U
6250
5740
92
6250
5770
92
1
56-143/18
104-51-8
n-Butylbenzene
50 U
1250
1420
114
1250
1340
107
6
79-126/16
75-15-0
Carbon Disulfide
100 U
1250
1130
90
1250
1070
86
5
66-148/23
56-23-5
Carbon Tetrachloride
50 U
1250
1550
124
1250
1480
118
5
76-136/23
108-90-7
Chlorobenzene
50 U
1250
1390
111
1250
1370
110
1
82-124/14
75-00-3
Chloroethane
100 U
1250
1530
122
1250
1540
123
1
62-144/20
67-66-3
Chloroform
50 U
1250
1410
113
1250
1390
111
1
80-124/15
110-82-7
Cyclohexane
50 U
1250
1420
114
1250
1330
106
7
73-138/18
124-48-1
Dibromochloromethane
50 U
1250
1410
113
1250
1390
111
1
78-122/19
96-12-8
1,2-Dibromo-3-chloropropane
100 U
1250
1290
103
1250
1320
106
2
64-123/18
106-93-4
1,2-Dibromoethane
100 U
1250
1330
106
1250
1350
108
1
75-120/13
75-71-8
Dichlorodifluoromethane
100 U
1250
1790
143
1250
1760
141
2
42-167/19
95-50-1
1,2-Dichlorobenzene
50 U
1250
1440
115
1250
1370
110
5
82-124/14
541-73-1
1,3-Dichlorobenzene
50 U
1250
1450
116
1250
1370
110
6
84-125/14
106-46-7
1,4-Dichlorobenzene
50 U
1250
1400
112
1250
1380
110
1
78-120/15
75-34-3
1, 1 -Dichloroethane
50 U
1250
1410
113
1250
1390
ill
1
81-122/15
107-06-2
1,2-Dichloroethane
50 U
1250
1430
114
1250
1420
114
1
75-125/14
75-35-4
1, 1 -Dichloroethylene
50 U
1250
1380
110
1250
1360
109
1
78-137/18
156-59-2
cis- 1, 2-Dichloroethylene
3000
1250
4170
94
1250
4060
85
3
78-120/15
156-60-5
trans- 1, 2-Dichloroethylene
50 U
1250
1480
118
1250
1470
118
1
76-127/17
78-87-5
1,2-Dichloropropane
50 U
1250
1330
106
1250
1300
104
2
76-124/14
10061-01-5 cis- 1, 3-Dichloropropene
50 U
1250
1370
110
1250
1330
106
3
75-118/23
10061-02-6 trans- 1, 3-Dichloropropene
50 U
1250
1470
118
1250
1420
114
3
80-120/22
100-41-4
Ethylbenzene
50 U
1250
1430
114
1250
1400
112
2
81-121/14
591-78-6
2-Hexanone
500 U
6250
5650
90
6250
5680
91
1
61-129/18
98-82-8
Isopropylbenzene
50 U
1250
1460
117
1250
1430
114
2
83-132/15
79-20-9
Methyl Acetate
1000 U
6250
6110
98
6250
6420
103
5
65-126/18
74-83-9
Methyl Bromide
100 U
1250
1410
113
1250
1370
110
3
59-143/19
74-87-3
Methyl Chloride
100 U
1250
1490
119
1250
1460
117
2
50-159/19
108-87-2
Methylcyclohexane
50 U
1250
1550
124
1250
1490
119
4
76-129/17
75-09-2
Methylene Chloride
250 U
1250
1470
118
1250
1460
117
1
69-135/16
108-10-1
4-Methyl-2-pentanone (MIBK)
250 U
6250
5620
90
6250
5820
93
3
66-122/16
* = Outside of Control Limits.
■■ 18 of 22
M A DMUTEST
FA29125 LPBDRATOR15

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
'A29094-4MS
P37018.13
50
11/12/15
KM
n/a
n/a
VP1374
'A29094-4MSD
P37019.13
50
11/12/15
KM
n/a
n/a
VP1374
'A29094-4
P37005.13
50
11/12/15
KM
n/a
n/a
VP1374
The QC reported here applies to the following samples: Method: SW846 8260B
FA29125-1
FA29094-4
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
50 U
1250
1340
107
1250
1360
109
1
72-117/14
91-20-3
Naphthalene
250 U
1250
1350
108
1250
1350
108
0
63-132/25
103-65-1
n-Propylbenzene
50 U
1250
1490
119
1250
1440
115
3
82-133/15
100-42-5
Styrene
50 U
1250
1350
108
1250
1360
109
1
78-119/23
79-34-5
1,1,2,2-Tetrachloroethane
50 U
1250
1250
100
1250
1240
99
1
72-120/14
127-18-4
Tetrachloroethylene
50 U
1250
1450
116
1250
1360
109
6
76-135/16
108-88-3
Toluene
50 U
1250
1380
110
1250
1360
109
1
80-120/14
120-82-1
1,2,4-Trichlorobenzene
50 U
1250
1400
112
1250
1370
110
2
73-129/20
71-55-6
1, 1, 1-Trichloroethane
50 U
1250
1480
118
1250
1410
113
5
75-130/16
79-00-5
1,1,2-Trichloroethane
50 U
1250
1310
105
1250
1330
106
2
76-119/14
79-01-6
Trichloroethylene
1820
1250
3210
111
1250
3120
104
3
81-126/15
75-69-4
Trichlorofluoromethane
100 U
1250
1550
124
1250
1510
121
3
71-156/21
95-63-6
1,2,4-Trimethylbenzene
100 U
1250
1450
116
1250
1390
111
4
79-120/18
108-67-8
1,3,5-Trimethylbenzene
100 U
1250
1390
111
1250
1340
107
4
79-120/19
75-01-4
Vinyl Chloride
50 U
1250
1440
115
1250
1420
114
1
69-159/18
1330-20-7
Xylene (total)
150 U
3750
4290
114
3750
4180
ill
3
80-126/15
CAS No.
Surrogate Recoveries
MS
MSD
FA29094-4
Limits
1868-53-7
Dibromofluoromethane
101%
103%
102%
83-118%
17060-07-0
1,2-Dichloroethane-D4
106%
107%
102%
79-125%
2037-26-5
Toluene-D8
98%
97%
99%
85-112%
460-00-4
4-Bromofluorobenzene
98%
98%
101%
83-118%
* = Outside of Control Limits.
■■ 19 of 22
M A DMUTEST
FA29125 LPBDRATOR15

Section 6
Southeast
■,N.ccuTEST
L A H OR AT OR E E 5
GUMS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
■■ 20 of 22
ACCUTEST
FA29125

Method Blank Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58301-MB
W090098.D
1
11/11/15
NJ
11/11/15
OP58301
SW4100
The QC reported here applies to the following samples: Method: SW846 8270D BY SIM
FA29125-1
CAS No.
Compound
Result
RL
MDL
Units Q
83-32-9
Acenaphthene
ND
1.0
0.40
ug/l
208-96-8
Acenaphthylene
ND
1.0
0.40
ug/l
120-12-7
Anthracene
ND
1.0
0.25
ug/l
56-55-3
Benzo(a)anthracene
ND
0.20
0.040
ug/l
50-32-8
Benzo(a)pyrene
ND
0.20
0.040
ug/l
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.040
ug/1
191-24-2
Benzo(g,h,i)perylene
ND
0.20
0.040
ug/1
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.040
ug/1
218-01-9
Chrysene
ND
0.20
0.040
ug/l
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.040
ug/1
206-44-0
Fluoranthene
ND
1.0
0.25
ug/1
86-73-7
Fluorene
ND
1.0
0.40
ug/1
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.040
ug/1
90-12-0
1-Methylnaphthalene
ND
1.0
0.40
ug/l
91-57-6
2-Methylnaphthalene
ND
1.0
0.40
ug/l
91-20-3
Naphthalene
ND
1.0
0.40
ug/l
85-01-8
Phenanthrene
ND
1.0
0.25
ug/l
129-00-0
Pyrene
ND
1.0
0.25
ug/l
CAS No.
Surrogate Recoveries
Limits
4165-60-0
Nitrobenzene-d5
68%
42-108%
321-60-8
2-Fluorobiphenyl
67%
40-106%
1718-51-0
Terphenyl-dl4
104%
39-121%
Rz
■■ 21 of 22
ACCUTEST
FA29125

Blank Spike Summary
Job Number: FA29125
Account: GRINCC GRI (Geological Resources Inc.)
Project: 2116 E Glenburnie Rd, New Bern, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP58301-BS a
W090097.D
1
11/11/15
NJ
11/11/15
OP58301
SW4100
The QC reported here applies to the following samples: Method: SW846 8270D BY SIM
FA29125-1
Spike
BSP BSP
CAS No.
Compound
ug/1
ug/1
%
Limits
83-32-9
Acenaphthene
10
8.3
83
56-101
208-96-8
Acenaphthylene
10
7.8
78
54-104
120-12-7
Anthracene
5
4.1
82
67-106
56-55-3
Benzo(a)anthracene
5
4.4
88
65-106
50-32-8
Benzo(a)pyrene
5
4.3
86
58-111
205-99-2
Benzo(b)fluoranthene
5
4.5
90
59-113
191-24-2
Benzo(g,h,i)perylene
5
4.2
84
43-112
207-08-9
Benzo(k)fluoranthene
5
4.7
94
58-110
218-01-9
Chrysene
5
4.7
94
66-107
53-70-3
Dibenzo(a,h)anthracene
5
4.0
80
40-113
206-44-0
Fluoranthene
10
8.6
86
64-110
86-73-7
Fluorene
10
8.6
86
60-106
193-39-5
Indeno(1,2,3-cd)pyrene
5
4.2
84
44-112
90-12-0
1-Methylnaphthalene
10
8.5
85
54-105
91-57-6
2-Methylnaphthalene
10
7.8
78
53-105
91-20-3
Naphthalene
10
7.9
79
56-105
85-01-8
Phenanthrene
10
9.0
90
62-105
129-00-0
Pyrene
10
9.4
94
62-109
CAS No.
Surrogate Recoveries
BSP
Limits
4165-60-0
Nitrobenzene-d5
82%
42-108%
321-60-8
2-Fluorobiphenyl
85%
40-106%
1718-51-0
Terphenyl-d14
97%
39-121%
(a) Insufficient sample for MS/MSD.
* = Outside of Control Limits.
Cn
i1a
■■ 22 of 22
ACCUTEST«
FA29125

Appendix B
Curriculum Vitae

QUALIFICATIONS OF ENVIRONMENTAL PROFESSIONALS
James E. Wellons, III, P.G., Compliance, Emergency Response, and Real Estate Manager
Professional Experience:
ASTM Standard Phase I and Phase II Environmental Site Assessments for general
commercial, car and truck maintenance facilities, trucking terminals, light and heavy
industrial, chemical plants, health care, multi -family residential, and office buildings
throughout the United States. Clients have included financial institutions, major retailers,
major industrial companies, major trucking companies, and real estate developers and
owners.
Assisted major trucking company with terminal property acquisitions by performing or
overseeing numerous Phase I and II environmental site assessments throughout the
United States, obtaining No Further Action for sites with soil and/or ground water
contamination, and determining escrows to be used for soil and/or ground water
remediation and site closure.
Completed Spill Prevention, Control and Countermeasures Plans for major trucking
company, chemical plants, and the Charlotte -Douglas International Airport.
Completed Storm Water Pollution Prevention Plans for chemical plants, a major trucking
company, and three Charlotte Area Transit System facilities.
Completed yearly preparation of over 100 SARA Title III / Tier II reports for a major
trucking company.
Managed third party contractor to perform nationwide compliance testing of underground
and aboveground storage tank systems for major trucking company.
Certifications:
OSHA Certified 40-Hour HAZWOPER
OSHA Certified Annual 8-Hour HAZWOPER Refresher
Certified Professional Geologist — North Carolina #1647, 1998
Registered Professional Geologist — South Carolina #2236, 2000
Education:
B.S., 1992, Geology, Appalachian State University, Boone, NC
Graduate Courses 1992-1995, Geology, East Carolina University, Greenville, NC

Randall A. Smith, P.G., Project Manager
Professional Experience:
ASTM Standard Phase I and Phase II Environmental Site Assessments for
industrial/manufacturing facilities, undeveloped real estate, and lending institutions
throughout the southwest and central United States.
Environmental assessment of underground storage tank and inactive hazardous waste
sites. Work included subsurface data acquisition and interpretation, regulatory
compliance and remediation; report preparation and review; field supervision of
environmental drilling and remedial excavations, perform soils and ground water
sampling, interaction with clients and regulators.
Certifications:
OSHA Certified 40-Hour HAZWOPER
OSHA Certified Annual 8-Hour HAZWOPER Refresher
Certified Professional Geologist — North Carolina #1262, 1993
Registered Professional Geologist — South Carolina #2323, 2003
Professional Geologist — Virginia 2801001711, 2006
Education:
B.S., 1979, Geology, University of Miami, Coral Gables, FL
M.S. 1981, Geophysics, Purdue University, West Lafayette, IN.