23068_Sir Walter Gun Club_RARpt_20211221

PREPARED FOR:
Merritt — MW1, LLC
2066 Lord Baltimore Drive
Baltimore, Maryland 21244-2501
PREPARED BY:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616
Corporate Registration for Licensing of NC Geologists No. C-145
NC Engineering Firm No. F-0176
December 21, 2021

=0
December 21, 2021
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfields Program
217 West Jones Street
Raleigh, North Carolina 27605
Attention: Mr. Brad Atkinson via email: [e-mail]
Brownfields Project Manager
Reference: Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
Dear Mr. Atkinson:
S&ME, Inc. (S&ME), on behalf of the project developer Merritt — MW1, LLC, is submitting this Remedial Action
Completion Report documenting the remedial action taken to address the lead impacted soil prior to site
development activities at the Sir Walter Gun Club site. Remedial action was performed in general accordance with
the Remedial Action Plan, dated January 15, 2021 which was submitted as part of the approved EMP for site
redevelopment. If you have any questions about this Remedial Action Completion Report, please contact the
undersigned.
Sincerely,
S&ME, Inc.
Samuel P. Watts, PG
Senior Project Manager
[e-mail]
I - 1: r5�w�
Thomas P. Raymond, P.E.
Senior Engineer
[e-mail]
cc: Nathan Robb ([e-mail]) — Merritt — MW1, LLC
Mary Katherine Stukes ([e-mail]) — Moore & Van Allen
Bruce Nicholson ([e-mail]) — North Carolina Brownfields Program
Enclosure: Remedial Action Completion Report, dated December 21, 2021
S&ME, Inc. 13201 Spring Forest Road I Raleigh, NC 27616 1 p 919.872.2660 1 www.smeinc.com

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
CERTIFICATION
Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
=©
I, Thomas P. Raymond, a Professional Engineer for S&ME, Inc., do hereby certify this Remedial Action Completion
Report was prepared by me or under my direct supervision.
SEAL =
S p
Thomas P. Raymond
Dee 21 2021 1:01 PM
I Gu t rW
Thomas P. Raymond, P.E.
Senior Engineer
NC Licensed Engineer No. 18760
S&ME, Inc. is licensed to practice engineering in North Carolina. The firm's license number is C-145.
S&ME, Inc. is licensed to practice geology in North Carolina. The firm's license number is F-0176.
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club s
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
Table of Contents
CERTIFICATION...................................................................................................................................................... ii
1.0 Introduction.......................................................................................................................1
2.0 Summary of Soil Areas Requiring Treatment.............................................................1
2.1 Soil Exceeding 5 mg/L by TCLP........................................................................................................1
2.2 Soil Exceeding Residential Lead PSRG..........................................................................................1
3.0 Remedial Activities..........................................................................................................2
3.1 Project Management, Health and Safety Plan, and Coordination.............................................2
3.2 Site Preparation....................................................................................................................................2
3.3 Soil Treatment Process with EnviroBlend®...................................................................................2
3.3.1 Soil Treated with EnviroBlend Confirmation Sampling...................................................................2
3.3.2 Soil Treated with EnviroBlend Sampling Results and Re-Treatment..............................................3
3.4 Handling & Processing Soils Exceeding Residential Lead PSRG.............................................3
3.4.1 Lateral Extent Confirmation Soil Sampling and Results.................................................................3
3.4.2 Excavated Bottoms Confirmation Soil Sampling and Results..........................................................4
3.5 Soil Placement......................................................................................................................................4
3.6 Root Balls..............................................................................................................................................5
4.0 Non -Scope Items...............................................................................................................5
5.0 Deviations from Approved EMP...................................................................................5
6.0 Conclusions and Recommendations.............................................................................6
Appendices
Appendix I —
Figures
Appendix II —
Tables
Appendix III
— Photographic Log
Appendix IV
— Analytical Laboratory Reports and Chain -of -Custody Records
Appendix V
— Preliminary Survey Plat
Appendix VI
— Waste Manifests
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club I
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
1.0 Introduction
S&ME, Inc. (S&ME) on behalf of project developer Merritt — MW1, LLC (Merritt) has prepared this Remedial Action
Completion Report for the former Sir Walter Gun Club (Brownfields Project No. 23068-19-092). The purpose of this
Remedial Action Completion Report is to document the remedial action taken to handle and treat soils with lead at
levels above 5 milligrams per liter (mg/L) analyzed by the Toxicity Characteristic Leaching Procedure (TCLP) and to
handle lead impacted soil above NCDEQ's Residential Preliminary Soil Remediation Goal (PSRG) for lead of 400
milligrams per kilogram (mg/kg). The Site Vicinity Map is attached as Figure 1.
2.0 Summary of Soil Areas Requiring Treatment
2.1 Soil Exceeding 5 mg/L by TCLP
Lead impacted soils exceeding 5 mg/L by TCLP were identified at the following on -site locations:
• 100-Yard Impact Berm
• 200-Yard Impact Berm and soil in front of the berm in the area of soil boring HA-31
• Side Berm
• Area of soil boring HA-46
The estimated total volume from these four areas was approximately 1,800 cubic yards (CY). In March 2021, prior
to on -site remedial action, a bench -level treatment study was completed to demonstrate EnviroBlend ® CS would
stabilize lead in the lead impacted soil from the former Sir Walter Gun Club site (Site) and not leach lead above
the action level required by NCDEQ. The treatability study was directed by Premier Magnesia, LLC (manufacturer
of EnviroBlend 0 CS), at their partner treatability laboratory company, Ursus Remediation Testing & Technologies
(Ursus).
S&ME collected lead impacted soil from the 200-yard berm of the former rifle range at the site and shipped the
soil samples to Ursus for a bench -level study with EnviroBlend 0 CS. Two soil samples were tested (SS-1 and
Duplicate). Laboratory analysis of the soil samples measured total lead at 2,980 milligrams per kilogram (mg/kg)
in SS-1 and 5,020 mg/kg in Duplicate. Each sample was dosed with EnviroBlend ® CS at 1%, 2% and 3% of soil by
weight.
Results indicated a 3% dosage rate stabilized the soil to well below TCLP levels for hazardous waste of 5 mg/L of
lead, and much less than the site specific NCDEQ goal of 1 mg/L lead. A 3% by weight dosage rate was
recommended. Based on the estimated quantity of lead -impacted soil and the recommended dosage rate,
approximately 54 tons of EnviroBlend ® CS were ordered for treatment of the soil.
2.2 Soil Exceeding Residential Lead PSRG
The areas impacted with lead which exceeded the Residential PSRG level of 400 mg/kg are depicted on Figure 2
(Area 1, Area 2, Area 3, and Area 4). This soil volume ranged from approximately 2,300 CY to 3,400 CY. The
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
variability of volume was based upon whether one foot of soil was removed, or 1.5 feet of soil was removed from
over the affected areas.
3.0 Remedial Activities
3.1 Project Management, Health and Safety Plan, and Coordination
Prior to conducting the remedial activities, S&ME performed the following:
Updated a previously prepared a health and safety plan to comply with currently proposed site
activities, in accordance with 29 CFR 1910.120 as required by the Occupational Safety and Health
Administration (OSHA);
Coordinated with a North Carolina certified laboratory for the proposed soil analyses with Level 2
Quality Assurance/Quality Control (QA/QC) data package; and
Marked out locations of the lead impacted soils with stakes and flagging.
3.2 Site Preparation
In July 2021, S&ME met on site with the remediation contractor, Contaminant Control, Inc. (CCI), to begin treating
the impacted soils with EnviroBlend. The EnviroBlend was delivered in approximate one cubic yard sacks, which
were staged on site under plastic sheeting cover near the proposed treatment areas. Prior to commencement of
soil treatment, the logging contractor cleared the delineated lead impacted areas of trees and heavy vegetation
without disturbing the lead impacted soils within the subsurface by leaving the root balls in place. After the areas
were cleared by the logging contractor, S&ME re -marked the delineated areas of the lead impacted soils with
stakes and flagging. Once the areas were re -marked, CCI began removing the root balls from within these areas.
Root balls from within the delineated areas with soils impacted with lead above 5 mg/L TCLP were set aside
separately for treatment with EnviroBlend. Photographs taken during the remedial activities are included in
Appendix III.
3.3 Soil Treatment Process with EnviroBlend®
Once the root balls were cleared from the areas, CCI began separating the impacted soils from the 100-yard berm,
200-yard berm, side berm, and area of HA-46 into approximate 50 CY piles. The piles were given a distinct name
and flagged/labeled in the field. The 100-yard berm was separated into six distinct piles (100P1 through 100P6),
the 200-yard berm and area in front of the 200-yard berm were separated into fourteen distinct piles (200P1
through 200P14), the side berm was separated into five distinct piles (SIDEP1 through SIDEPS), and the area of
HA-46 was separated into one distinct pile (HA46P1) for a total of twenty-six piles of impacted soil containing lead
above 5 mg/L TCLP. Each approximate 50 CY pile of lead impacted soil was then mixed with 1.5 to 2 sacks (1
cubic yard each) of EnviroBlend to achieve the proposed 3% by weight dosage rate.
3.3.1 Soil Treated with EnviroBlend Confirmation Sampling
Following treatment of each approximate 50 CY pile with EnviroBlend, S&ME utilized a decontaminated hand
auger to collect four discreet samples from each half of each 50 CY pile. The four discreet samples from each half
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
of each pile were then combined into one composite sample so that each 50 CY pile would have two composite
samples, one from each side (an A side and a B side). For example, the composite samples collected from the
100-yard berm were labeled as 100131A, 100P1 B, 100P2A, 100P213, etc. Confirmation samples were collected into
laboratory supplied containers, placed in an ice -filled cooler, and shipped under standard chain -of -custody
protocol to ENCO Laboratories for analysis of lead by the TCLP extraction EPA Method 1311 and for total lead by
SW-846 Method 6010C.
3.3.2 Soil Treated with EnviroBlend Sampling Results and Re -Treatment
Results from the initial round of confirmation sampling indicated several of the piles from the 100-yard berm and
200-yard berm needed re -treatment. Each half of a pile, represented by one composite sample, with a detected
concentration of TCLP lead above 1 mg/L (the site -specific remediation goal) was re -treated with EnviroBlend by
the methods as described in Section 3.1. Following re -treatment, the pile was re -sampled as described in Section
3.3. 7 and labeled with a -R to indicate the re-treatment/re-sampling and submitted under standard chain -of -
custody protocol to ENCO Laboratories for analysis of lead by the TCLP extraction EPA Method 1311 and for total
lead by SW-846 Method 6010C.
Results of the re-treatment/re-sampling indicated the lead was sufficiently stabilized by the EnviroBlend. Each
approximate 50 CY pile following either one or two rounds of treatment did not contain TCLP lead above 1 mg/L.
Results from the confirmation sampling of the soils treated with EnviroBlend are displayed on Table 1 in
Appendix II and analytical laboratory reports are included in Appendix IV.
3.4 Handling & Processing Soils Exceeding Residential Lead PSRG
The areas impacted with lead which exceeded the Residential PSRG level of 400 mg/kg are displayed on Figure 2
(Area 1, Area 2, Area 3, and Area 4). S&ME marked the delineated extents of these areas with stakes and flagging.
Once the areas were clearly defined, CCI began excavating approximately one foot of soil from the surface. Soils
were stockpiled within the impacted areas for direct loading and hauling to the proposed on -site placement area.
3.4.1 Lateral Extent Confirmation Soil Sampling and Results
S&ME collected confirmation sidewall samples of the lateral extent of the delineated contaminated
areas/excavation with a decontaminated hand auger. Individual, evenly distributed samples were collected
approximately 25 linear feet apart along the edge of the excavation sidewalls from approximately 0-6 inches
below the ground surface. Samples were flagged in the field, marked with a GPS, and labeled according to the
area from which they were collected. For example, confirmation sidewall samples collected from Area 1 were
labeled as Al S1 for Area 1, Sidewall 1. Sixteen sidewall samples were collected from Area 1 and the 200-yard
berm (AlS1 through AlS16), eight sidewall samples were collected from the 100-yard berm (10051 through
10058), twenty-seven sidewall samples were collected from Area 2 and the side berm (A2S1 through A2S27), eight
sidewall samples were collected from Area 3 (A3S1 through A3S8), and eighteen sidewall samples were collected
from Area 4 and the area surrounding HA-46 (A4S1 through A4S18) for a total of 77 samples. Confirmation
sidewall samples were collected into laboratory supplied containers, placed in an ice -filled cooler, and shipped
under standard chain -of -custody protocol to ENCO Laboratories for analysis of total lead by SW-846 Method
6010C.
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
Results indicated that 75 out of the 77 confirmation sidewall samples did not detect lead at concentrations above
the Residential PSRG level of 400 mg/kg. The remaining two samples, 10051 and A2S18, contained lead
concentrations above 400 mg/kg. As a result, CCI excavated laterally an additional 10 feet in these areas and
samples were collected from the new lateral extent. The samples were labeled with a -R to indicate the
resampling and submitted under standard chain -of -custody protocol to ENCO Laboratories for analysis of total
lead by SW-846 Method 6010C. Results of the samples collected from the additional lateral extents indicated that
lead was not detected above the Residential PSRG level of 400 mg/kg. Results from the lateral extent
confirmation sampling are displayed on Table 2 in Appendix II and analytical laboratory reports are included in
Appendix IV. Sample locations are depicted on Figure 2.
3.4.2 Excavated Bottoms Confirmation Soil Sampling and Results
S&ME collected confirmation samples from the bottoms of each of the excavated areas. Sampling grids were
established within each area to be approximately 25 feet by 25 feet. Each area was dimensionally flagged in the
field and given a distinct name (i.e. Al B1, representing Area 1, Base 1). Five individual evenly distributed samples
were collected from each approximate 25 feet by 25 feet area with a decontaminated hand auger and formed into
one composite soil sample. The composite soil samples were named according to the area from which they were
taken. Twenty-one base samples were collected from Area 1 and the 200-yard berm (Al B1 through Al B21), eight
base samples were collected from the 100-yard berm (100B1 through 100B8), fifty-seven base samples were
collected from Area 2 and the side berm (A2B1 through A2B57), eight base samples were collected from Area 3
(A3B1 through A3B8), and twenty-nine base samples were collected from Area 4 and the area surrounding HA-46
(A4B1 through A4B29) for a total of 123 samples. Confirmation base samples were collected into laboratory
supplied containers, placed in an ice -filled cooler, and shipped under standard chain -of -custody protocol to ENCO
Laboratories for analysis of total lead by SW-846 Method 6010C.
Results indicated that 122 out of the 123 confirmation base samples did not detect lead at concentrations above
the Residential PSRG level of 400 mg/kg. Only sample 100B2 contained lead concentrations above 400 mg/kg. As
a result, CCI excavated vertically an additional 0.5 feet in this area and a new composite sample was collected from
the additional vertical extent. The sample was labeled with a -R to indicate the resampling and submitted under
standard chain -of -custody protocol to ENCO Laboratories for analysis of total lead by SW-846 Method 6010C.
Results of the sample collected from the additional vertical extent (sample 100132-R) indicated that lead was not
detected above the Residential PSRG level of 400 mg/kg. Results from the base confirmation sampling are
displayed on Table 3 in Appendix II and analytical laboratory reports are included in Appendix IV. Sample
locations are depicted on Figure 3 and Figure 4.
3.5 Soil Placement
Once analytical results from the confirmation samples indicated the treated soils from the berms did not contain
TCLP lead above 1 mg/L and the sidewalls and bottoms of excavated areas did not contain lead above 400 mg/Kg,
the excavated soil was relocated, placed and compacted in the selected on -site placement area (Figure 5). The
soil was covered with geotextile, covered with engineered backfill, and compacted per specifications. This area
will be covered with a paved parking lot at the surface. This area is also displayed on the preliminary survey Plat
of the Brownfields property, included as Appendix V. The "soil disposal area" is encompassed by lines L168
December 21, 2021 4

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
through L198, which each have a distinct bearing and distance as shown on page 2 of the preliminary survey Plat
included as Appendix V.
3.6 Root Balls
Root balls from within the delineated areas with soils impacted with lead above 5 mg/L TCLP were set aside
separately for treatment with EnviroBlend. CCI applied EnviroBlend to the root balls and S&ME collected a
composite soil sample (Root Ball Soil) from the soils adhered to several of the root balls for analysis. The sample
was collected into laboratory supplied containers, placed in an ice -filled cooler, and shipped under standard
chain -of -custody protocol to ENCO Laboratories for analysis of lead by the TCLP extraction EPA Method 1311.
Analytical results of the Root Ball Soil sample indicated lead was not detected above the laboratory's method
detection limit of 0.155 mg/L. Once analytical results were received, CCI transported the root balls to the Great
Oak Landfill for proper disposal. Approximately 200-300 tons of root balls/vegetative debris were transported to
the Great Oak Landfill for disposal. A copy of the manifest is included in Appendix VI.
4.0 Non -Scope Items
S&ME observed an approximate 4" terra cotta pipe during the excavation of lead impacted soils from Area 2. CCI
utilized a mini excavator to trace the terra cotta pipe to a concrete septic tank located along the southern
property line. The septic tank was most likely associated with a former outbuilding and was located outside the
limit of disturbance of the proposed redevelopment activities.
S&ME observed the tank, which appeared to be in good condition and empty. S&ME collected soil samples on
the downgradient side of the septic tank and along the terracotta pipe to visually assess the soils for potential
environmental impact. Soil samples were also screened with a photoionization detector (PID) to evaluate the
presence of potential volatile organic compounds (VOCs). No discoloration of the soil or detections on the PID
were noted during the assessment. CCI broke up the concrete tank and compacted it in place to remove the void
space and the potential safety hazard. No other actions were required.
5.0 Deviations from Approved Plan/EMP
No deviations from the approved Environmental Management Plan, which included the Remedial Action Plan,
occurred during the redial activities performed at the subject site except for the following:
A small portion of the delineated areas of lead impacted soil within Areas 3 and 4 remained outside
the limit of disturbance of redevelopment activities. Silt fence and erosion control measures were
installed, which prevented CCI from excavating soil from these areas as shown on Figure 4.
Therefore, confirmation base samples were not collected from these areas. However, S&ME collected
sidewall samples from outside the limit of disturbance (A3S3, A3S4, A4S9, A4S10, and A4S11) which
indicated lead was not detected above the Residential PSRG level of 400 mg/kg.
December 21, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club I I
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
6.0 Conclusions and Recommendations
S&ME and CCI have completed the proposed remedial action to handle and treat soils with lead at levels above 5
mg/L TCLP and to handle lead impacted soil above NCDEQ's Residential PSRG for lead of 400 mg/kg at the former
Sir Walter Gun Club (Brownfields Project No. 23068-19-092). Remedial action was successfully completed in
compliance with the EMP and no further action is required at this time.
December 21, 2021

Appendices

Appendix I - Figures

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FIGURE NO.
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REFERENCE: ► �' — -
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F GIS BASE LAYERS WERE OBTAINED FROM THE 2018 NCONEMAP.COM ORTHOIMAGERY y F eye ,rL halplaR�dwthelire•• t••9nd .r.•.'
BASEMAP LAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE 0 200 r�r400' ` ' A xnG nklen
i LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY (FEET) 1
d By' Lead Impacted Soil Placement Area

Appendix II - Tables

r�
TABLET
I I Summary of EnviroBlend® Treatment Confirmation Soil Sampling Results
I E Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method P
Lead by EPA Method 6010D
(mg/Kg)
Lead by EPA Method 6010D
(mg/L)
Analyte
Total Lead
Leachable Lead - TCLP
Treatment Area
Sample ID
Date Collected
10OPlA
7/21/2021
980
<0.155
10OP1B
7/21/2021
1,000
<0.155
100P2A
7/21/2021
1,260
<0.155
100P2B
7/21/2021
1,090
<0.155
100P3A
7/21/2021
862
0.186 J
100P3B
7/21/2021
747
12.2
100P3B-R
8/4/2021
1,440
<0.155
100P4A
7/21/2021
780
<0.155
100 Yard Berm
100P4B
7/21/2021
512
12.8
100P4B-R
8/4/2021
953
<0.155
100P5A
7/21/2021
860
<0.155
100P5B
7/21/2021
801
<0.155
100P6A
7/21/2021
1,730
92.9
100P6A-R
8/4/2021
950
<0.155
100P6B
7/21/2021
1,080
20.9
100P6B-R
8/4/2021
883
<0.155
20OPlA
7/22/2021
321
<0.155
20OP1B
7/22/2021
232
1.38
200P1B-R
8/4/2021
136
<0.155
200P2A
7/22/2021
177
1.36
200P2A-R
8/4/2021
195
<0.155
200P2B
7/22/2021
146
0.784
200P3A
7/22/2021
69.7
<0.155
200P3B
7/22/2021
40.7
0.452 J
200P4A
7/22/2021
1,310
200P4A-R
8/12/2021
410
<0.155
200P4B
7/22/2021
282
0.739
200P5A
7/22/2021
267
8.87
200P5A-R
8/12/2021
142
<0.155
200P5B
7/22/2021
559
15.5
200P5B-R
8/12/2021
6,270
<0.155
200P6A
7/22/2021
306
7.79
200P6A-R
8/12/2021
228
<0.155
200P6B
7/22/2021
152
4.73
200 Yard Berm
200P6B-R
8/12/2021
118
<0.155
200P7A
7/22/2021
319
0.985
200P7B
7/22/2021
242
<0.155
200P8A
7/22/2021
202
<0.155
200P8B
7/22/2021
321
<0.155
200P9A
7/22/2021
693
3.81
200P9A-R
8/12/2021
363
<0.155
200P9B
7/22/2021
313
<0.155
20OP10A
7/22/2021
62.4
0.319 J
20OP10B
7/22/2021
55.1
<0.155
20OP11A
7/22/2021
290
<0.155
20OP11B
7/22/2021
345
8.24
200P11B-R
8/13/2021
223
<0.155
20OP12A
7/22/2021
32.7
<0.155
20OP12B
7/22/2021
44.9
0.159 J
20OP13A
7/22/2021
88.2
0.579
20OP13B
7/22/2021
67.6
1.16
200P13B-R
8/13/2021
131
<0.155
20OP14A
7/22/2021
227
0.498 J
20OP14B
7/22/2021
211
0.322 J
SIDEPIA
7/23/2021
26.5
<0.155
SIDEPIB
7/23/2021
23.9
<0.155
SIDEP2A
7/23/2021
12.6
<0.155
SIDEP2B
7/23/2021
15.3
<0.155
Berm
SIDEP3A
7/23/2021
23.1
<0.155
Side
SIDEMB
7/23/2021
28.9
<0.155
SIDEP4A
7/23/2021
0.20
<0.155
SIDEP4B
7/23/2021
32.5
<0.155
SIDEP5A
7/23/2021
17.9
<0.155
SIDEP5B
7/23/2021
24.7
<0.155
Area HA-46
HA46P1A
7/23/2021
231
<0.155
of
HA46P1B
7/23/2021
258
<0.155
Site Specific Goal for Leachable Lead
NE
1
Hazardous Waste Section Haz Waste Value
NE
5
Notes:
Soil sample concentrations are reported in mg/Kg and mg/L.
mg/Kg - milligrams per kilogram. mg/L - milligrams per liter.
Sample IDs designated with -R indicate the sample was collected following re -treatment with additional EnviroBlend®
Samples shown with F VALUE exceed the site specific goal for extractable lead by TCLP of 1 mg/L.
Samples shown with M VALUE exceed the Hazardous Waste Section Hazardous Waste Value for extractable lead by TCLP.
NE - not established.
11EgnyteDdvelsmeinc\SharedlSMElOps1EWProjects1201 N305-19-213 Merritt- Knightdale Development\Working_DocumentslSoil Treatment Remedial ActiomPost Remediation Summary ReporhTablesTost Remediaton Confirmation Soil Sampling Tables.xlsx

TABLE2
I I ! Summary of Sidewall Confirmation Soil Sampling Results
[i
- Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method
Lead by EPA Method 6010D
(mg/Kg)
Analyte
Total Lead
Treatment Area
Sample ID
Date Collected
Area 1 and
200 Yard Berm
Sidewalls
A1S1
7/26/2021
5.96
A1S2
7/26/2021
10.7
A1S3
7/26/2021
8.91
A154
7/26/2021
8.67
A1S5
7/26/2021
7.20
A1S6
7/26/2021
33.0
A1S7
7/26/2021
11.5
A1S8
7/26/2021
5.18
A1S9
7/26/2021
6.46
A1S10
7/26/2021
5.38
A1S11
7/26/2021
9.61
A1S12
7/26/2021
2.46
A1S13
7/26/2021
2.85
A1S14
7/26/2021
4.65
A1S15
7/26/2021
4.51
A1S16
7/26/2021
37.8
100 Yard Berm
Sidewalls
10051
7/26/2021
706
100S1-R
8/13/2021
9.15
100S2
7/26/2021
19.1
100S3
7/26/2021
54.8
10054
7/26/2021
10.3
100S5
7/26/2021
18.6
100S6
7/26/2021
12.2
100S7
7/26/2021
5.25
100S8
7/26/2021
7.05
Area 2 and
Side Berm
Sidewalls
A2S1
7/21/2021
6.23
A2S2
7/21/2021
5.24
A2S3
7/21/2021
15.5
A2S4
7/21/2021
12.8
A2S5
7/21/2021
16.3
A2S6
7/21/2021
12.9
A2S7
7/21/2021
16.4
A2S8
7/21/2021
22.6
A259
7/21/2021
13.0
A2S10
7/21/2021
24.8
A2S11
7/22/2021
3.28
A2S12
7/22/2021
4.85
A2S13
7/22/2021
5.52
A2S14
7/22/2021
5.75
A2S15
7/23/2021
9.35
A2S16
7/23/2021
19.3
A2S17
7/23/2021
38.5
A2S18
7/23/2021
507
A2S18-R
8/4/2021
343
A2S19
7/23/2021
82.5
A2S20
7/23/2021
39.2
A2S21
7/23/2021
7.97
A2S22
7/23/2021
5.36
A2S23
7/23/2021
10.4
A2S24
7/23/2021
5.46
A2S25
7/23/2021
34.7
A2S26
7/23/2021
20.7
A2S27
7/23/2021
14.1
Area 3
Sidewalls
A3S1
7/26/2021
7.81
A3S2
7/26/2021
9.24
A3S3
7/26/2021
11.8
A3S4
7/26/2021
11.7
A3S5
7/26/2021
4.77
A3S6
7/26/2021
5.46
A3S7
7/26/2021
13.0
A3S8
7/26/2021
8.74
Area 4 and
Area of HA-46
Sidewalls
A4S1
7/26/2021
25.7
A4S2
7/26/2021
12.7
A4S3
7/26/2021
35.5
A4S4
7/26/2021
22.1
A4S5
7/26/2021
31.9
A4S6
7/26/2021
21.4
A4S7
7/26/2021
17.3
A4S8
7/26/2021
7.99
A4S9
7/26/2021
8.42
A4S10
7/26/2021
9.82
A4S11
7/26/2021
23.8
A4S12
7/26/2021
21.9
A4S13
7/26/2021
108
A4S14
7/26/2021
10.0
A4S15
7/26/2021
28.2
A4S16
7/26/2021
73.6
A4S17
7/26/2021
6.42
A4S18
7/26/2021
48.7
Residential PSRG
400
Industrial/Commercial PSRGI
800
Notes:
Soil sample concentrations are reported in mg/Kg.
mg/Kg - milligrams per kilogram.
Sample results that exceed the Residential PSRG are shown with VALUE
Sample IDS designated with -R indicate the sample was collected following further lateral excavation.
PSRG - Preliminary Soil Remediation Goal by NCDEQ
IlEgnyteDrinesmeinclSharedlSME\Dps\ENV1Projectst2019W305-19-213 Merritt- Hnightdale DmlopmenhWorldng_D-enWSoil Treatment Remedial AdWPost Remediation Summary ReporffableatPost Remediation Confirmation Soil Sampling Tables.xlsx

TABLE3
I I Summary of Base Confirmation Soil Sampling Results
= Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method
Lead by EPA Method 6010D
(mg/Kg)
Analyte
Total Lead
Treatment Area
Sample ID
Date Collected
Area 1 and
200 Yard Berm
Base
A1131
8/26/2021
3.92
A1B2
8/26/2021
3.48
A1133
8/26/2021
2.77
A1B4
8/26/2021
8.33
A1B5
8/26/2021
13.0
A1B6
8/26/2021
5.73
A1B7
8/26/2021
10.8
A1B8
8/26/2021
37.6
A1139
8/26/2021
5.73
A1B10
8/26/2021
14.9
A1Bll
8/26/2021
3.71
AIB12
8/26/2021
6.53
AIB13
8/26/2021
17.8
AIB14
8/26/2021
8.04
AIB15
8/26/2021
7.60
AIB16
8/26/2021
115
AIB17
8/26/2021
21.5
AIB18
8/26/2021
11.6
AIB19
8/26/2021
16.5
AIB20
8/26/2021
25.1
AIB21
8/26/2021
11.1
100 Yard Berm
Base
100B1
8/24/2021
20.0
100B2
8/24/2021
406
100B2-R
9/7/2021
11.8
100B3
8/24/2021
13.4
100B4
8/24/2021
254
100B5
8/24/2021
14.0
100B6
8/24/2021
282
100B7
8/24/2021
6.84
100B8
8/24/2021
166
Area 2 and
Side Berm Base
A2B1
8/19/2021
3.62
A2B2
8/19/2021
4.36
A2B3
8/19/2021
6.27
A2B4
8/19/2021
4.88
A2B5
8/19/2021
4.51
A2B6
8/19/2021
7.30
A2B7
8/19/2021
s.88
A2B8
8/19/2021
13.0
A2B9
8/23/2021
17.4
A2B10
8/23/2021
62.5
A2B11
8/23/2021
8.05
A2B12
8/23/2021
55.9
A2B13
8/23/2021
67.8
A2B14
8/23/2021
4.95
A2B15
8/23/2021
4.48
A2B16
8/23/2021
12.4
A2B17
8/23/2021
6.20
A2B18
8/23/2021
7.21
A2B19
8/23/2021
5.56
A2B20
8/23/2021
5.34
A2B21
8/23/2021
9.16
A2B22
8/23/2021
7.02
A2B23
8/23/2021
8.54
A2B24
8/23/2021
44.6
A2B25
8/23/2021
10.3
A2B26
8/23/2021
6.92
A2B27
8/23/2021
28.3
A2B28
8/23/2021
89.2
A2B29
8/23/2021
5.90
A2B30
8/23/2021
6.16
A2B31
8/23/2021
6.33
A2B32
8/23/2021
13.7
A2B33
8/23/2021
8.08
A2B34
8/23/2021
13.8
A2B35
8/23/2021
6.25
A2B36
8/23/2021
5.87
A2B37
8/23/2021
11.3
A2B38
8/23/2021
18.9
A2B39
8/23/2021
14.3
A2B40
8/23/2021
44.2
A2B41
8/23/2021
4.86
A2B42
8/23/2021
9.83
A2B43
8/24/2021
4.29
A2B44
8/24/2021
6.70
A2B45
8/24/2021
10.4
A2B46
8/24/2021
15.9
A2B47
8/24/2021
12.7
A2B48
8/24/2021
6.27
A2B49
8/24/2021
15.1
A2B50
8/24/2021
13.4
A2B51
8/24/2021
14.9
A2B52
8/24/2021
11.3
A2B53
8/24/2021
15.4
A2B54
8/24/2021
19.2
A2B55
8/24/2021
17.2
A2B56
8/24/2021
7.29
A2B57
8/24/2021
13.7
IEgnyl D,Ivalsmein6Shomd1SME10ps1ENVlPmjocl 019W305-19-213 Mo,r d- Knighldale Developme,tWotling_DocumenlslSoil TreaMent Remedial Ado,PW Remedietion Summary Repo TablesPosl Remedietion Confirmation Soil Sampling Toble9.xl, 1 of 2

TABLE3
I I Summary of Base Confirmation Soil Sampling Results
= Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method
Lead by EPA Method 6010D
(mg/Kg)
Analyte
Total Lead
Treatment Area
Sample ID
Date Collected
Area 3
Base
A3131
8/13/2021
22.9
A3B2
8/13/2021
16.9
A3133
8/13/2021
16.2
A3B4
8/13/2021
21.9
A3B5
8/13/2021
19.3
A3B6
8/13/2021
13.1
A3137
8/13/2021
9.20
A3B8
8/13/2021
84.7
Area 4 and
Area (HA-46
Base, within Area 4)
A4131
8/16/2021
14.2
A4B2
8/16/2021
20.9
A4153
8/16/2021
64.9
A4B4
8/16/2021
13.3
A4155
8/16/2021
21.6
A4B6
8/16/2021
19.9
A4157
8/16/2021
170
A4B8
8/16/2021
11.8
A4B9
8/16/2021
27.7
A4B10
8/16/2021
19.8
A4B11
8/16/2021
45.1
A4B12
8/16/2021
22.8
A4B13
8/16/2021
32.2
A4B14
8/16/2021
6.52
A4B15
8/16/2021
27.2
A4B16
8/16/2021
86.6
A4B17
8/16/2021
21.6
A4B18
8/16/2021
49.1
A4B19
8/16/2021
9.53
A4B20
8/16/2021
25.1
A4B21
8/16/2021
13.9
A4B22
8/16/2021
27.8
A4B23
8/16/2021
8.78
A4B24
8/16/2021
48.6
A4B25
8/16/2021
7.24
A4B26
8/16/2021
19.3
A4B27
8/16/2021
96.0
A4B28
8/16/2021
5.22
A41329
8/16/2021
5.68
Residential PSRG
400
Industrial/Commercial PSRGI
800
Notes:
Soil sample concentrations are reported in mg/Kg.
mg/Kg - milligrams per kilogram.
Sample results that exceed the Residential PSRG are shown with VALUE
Sample IDs designated with -R indicate the sample was collected following further vertical excavation.
PSRG - Preliminary Soil Remediation Goal by NCDEQ
IEgny.Drlvalsmein6Shered1SME10ps1ENVlPmfeclsV019W30S19-2136lerdd-Knighldale Developme,tWotling_DooumenlslSoil TreaMent Remedial Ado,PWRemedlobon Summary Repo TablesPosl Remediabon Confirmation Soil Sampling Toble9.xl, 20f2

Appendix III - Photographic Log

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
N
O
N
6�1
1 I Photo Description (View of the stakes and flagging placed around Area 1.
N
O
N
ON
V
2 Photo Description (View of the stakes and flagging placed around Area 2.
=0
December 20, 2021

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
=0
. �R
V .srpgt ,
� i
s
s -
�' ?f 1�
-,
z
Photo Description
,
59Ui
r
9
'. R Yti
`GSM tY ..
•
,{K
Photo Description
December 20, 2021 2

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
Mea
n
"®r,
74 M. Pr
"9s
k
1
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s `�����'.- - r: .� � _ ..
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Photo Description
Igif
g
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Photo Description
•
December 20, 2021 3

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
L .
% I Photo Description
f
of the stakes and flagging placed around the side
N
O
N
V
"r
E
- `a
a= a
O
a
FHA-46.
of the stakes and flagging placed around the area of
E8 Photo Description
December 20, 2021 4

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
N
O
N
9 I Photo Description (View of delivery of the EnviroBlend to the site.
10 I Photo Description (View of the EnviroBlend staging area.
December 20, 2021 5

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
-a
December 20, 2021 6

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
=0
•
•
rt.
' a
e
ILi
S
rMAN
December 20, 2021 7

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
December 20, 2021 8

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
=0
re
..
;;;���r���'TV
r
AN % wp"V19yt
ff
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-mil% _ � p _
December 20, 2021 9

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
=0
December 20, 2021 10

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
F
�
00
N
yj
It
roc+ >
n i
r v
E
C
�
0)
_
Q
21
Photo Description
View of the stockpiled soil excavated from Area 4.
� � P
N
1.
r
N
y
�s-
Y
QJ
�
➢d -
22
Photo Description
CCI excavating lead impacted soil from Area 3.
December 20, 2021 11

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
N
O
N
L 00
�
i
E
23 Photo Description iew of the stockpiled soil excavated from Area 3.
G
3F y
j1
Ln
,n
00
a`)
a�
E
a�
t
Q
12
0)
O
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24 Photo Description View of the impacted soil placement area.
=0
December 20, 2021 12

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
N
O
55
a
N
Ln
co
ra
Y v
Hill
O
-R '�<•
O
_
i
a
25
Photo Description View of the placement of the impacted soil.
N
O
N
N
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I'
7-
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i
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(O
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m ��s
12
.ram-r�.caE •.'::.
- , ;IN
X g
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0
0
t
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.. .a.
a
26
Photo Description
iew of the placement of the impacted soil.
December 20, 2021 13

Remedial Action Completion Report
Hinton Oaks Blvd., Knightdale, North Carolina
Brownfields Project Name: Sir Walter Gun Club
Brownfields Project No.: 23068-19-092
S&ME Project No. 4305-19-213
-. ..-�44•
�� ,�' A"�' '` ' �
ml
_ � ^�✓�'��� -�:b #���. fit..:
.7.
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27
Photo Description
iew o e concre e sep is an i en i ie
excavation of Area 2.
unng e
y
�
{
ti
ram;12
28 Photo Description iew of the area from which the septic tank was removed.
December 20, 2021 14

Appendix IV - Analytical Laboratory Reports and Chain -of -Custody
Records

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, July 30, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE10948
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, July 21, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 11

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 10OPlA
Lab ID: CE10948-01
Sampled: 07/21/21 10:55
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 09:40
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:03
Client ID: 10OPlB
Lab ID: CE10948-02
Sampled: 07/21/21 11:20
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 09:54
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:25
Client ID: 300P2A
Lab ID: CE10948-03
Sampled: 07/21/21 11:45
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 09:56
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:27
Client ID: 100P213
Lab ID: CE10948-04
Sampled: 07/21/21 12:05
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 09:58
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:30
Client ID: 100P3A
Lab ID: CE10948-05
Sampled: 07/21/21 12:25
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:10
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:32
Client ID: 300P313
Lab ID: CE10948-06
Sampled: 07/21/21 12:45
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:12
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:35
Client ID: 300P4A
Lab ID: CE10948-07
Sampled: 07/21/21 13:00
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:14
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:38
Client ID: 100P413
Lab ID: CE10948-08
Sampled: 07/21/21 13:20
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:16
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:45
Client ID: 300PSA
Lab ID: CE10948-09
Sampled: 07/21/21 13:40
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:18
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:48
Client ID: 100PSB
Lab ID: CE10948-10
Sampled: 07/21/21 14:00
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:20
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:50
Client ID: 100P6A
Lab ID: CE10948-11
Sampled: 07/21/21 14:15
Received: 07/21/21 16:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:14
07/29/21 10:22
EPA 6010D
EPA 3010A
O1/17/22 01/25/22
07/29/21 15:21
07/30/21 11:53
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 11

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 300P613 Lab ID: CE10948-12 Sampled: 07/21/21 14:30 Received: 07/21/21 16:58
Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 6010D EPA 3050B
EPA 6010D EPA 3010A
O1/17/22 07/27/21 11:14 07/29/21 10:24
O1/17/22 01/25/22 07/29/21 15:21 07/30/21 11:56
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 11

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SAMPLE DETECTION SUMMARY
Client ID:
100PlA
Lab ID:
CE10948-01
Analvte
Lead - Total
Results
980
Flag
MDL
0.127
Q
0.529
Units
mg/kg dry
Method Notes
EPA 6010D
Client ID:
100PlB
Lab ID:
CE10948-02
Analvte
Lead - Total
Results
1000
Flag
MDL
0.126
PQL
0.525
Units
mg/kg dry
Method Notes
EPA 6010D
Client ID:
300P2A
Lab ID:
CE10948-03
Analvte
Lead - Total
Results
1260
Flag
MDL
0.130
PQL
0.543
Units
mg/kg dry
Method Notes
EPA 6010D
Client ID:
300P2B
Lab ID:
CE10948-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
1090
0.128
0.534
mg/kg dry
EPA 6010D
Client ID:
300P3A
Lab ID:
CE10948-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
862
0.128
0.533
mg/kg dry
EPA 6010D
Lead - TCLP
0.186
1
0.155
0.500
mg/L
EPA 6010D
Client ID:
300P3B
Lab ID:
CE10948-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
747
0.129
0.539
mg/kg dry
EPA 6010D
Lead - TCLP
12.2
0.155
0.500
mg/L
EPA 6010D
Client ID:
300P4A
Lab ID:
CE10948-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
780
0.127
0.530
mg/kg dry
EPA 6010D
Client ID:
300P4B
Lab ID:
CE10948-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
512
0.127
0.531
mg/kg dry
EPA 6010D
Lead - TCLP
12.8
0.155
0.500
mg/L
EPA 6010D
Client ID:
100PSA
Lab ID:
CE10948-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
860
0.127
0.530
mg/kg dry
EPA 6010D
Client ID:
100PSB
Lab ID:
CE10948-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
801
0.127
0.527
mg/kg dry
EPA 6010D
Client ID:
300P6A
Lab ID:
CE10948-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
1730
0.132
0.548
mg/kg dry
EPA 6010D
Lead - TCLP
92.9
0.155
0.500
mg/L
EPA 6010D
Client ID:
300P6B
Lab ID:
CE10948-12
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
1080
0.120
0.500
mg/kg dry
EPA 6010D
Lead - TCLP
20.9
0.155
0.500
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 11

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ANALYTICAL RESULTS
Description: 10OPlA Lab Sample ID:CE10948-01 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 10:55 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.55
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 980
mg/kg dry
1
0.127
0.529
1G27021
EPA 6010D
07/29/21 09:40
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:03
JDH
Description: 10OPlB Lab Sample ID:CE10948-02 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 11:20 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1000
mg/kg dry
1
0.126
0.525
1G27021
EPA 6010D
07/29/21 09:54
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:25
JDH
Description: 100P2A Lab Sample ID:CE10948-03 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 11:45 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.06
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 1260
mg/kg dry
1
0.130
0.543
1G27021
EPA 6010D
07/29/21 09:56
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:27
JDH
Description: 100P2B Lab Sample ID:CE10948-04 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 12:05 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1090
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 09:58
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:30
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 11

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ANALYTICAL RESULTS
Description: 100P3A Lab Sample ID:CE10948-05 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 12:25 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.87
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 862
mg/kg dry
1
0.128
0.533
1G27021
EPA 6010D
07/29/21 10:10
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.186 J
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:32
JDH
Description: 100P3B Lab Sample ID:CE10948-06 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 12:45 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 747
mg/kg dry
1
0.129
0.539
1G27021
EPA 6010D
07/29/21 10:12
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 12.2
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:35
JDH
Description: 100P4A Lab Sample ID:CE10948-07 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 13:00 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 780
mg/kg dry
1
0.127
0.530
1G27021
EPA 6010D
07/29/21 10:14
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:38
JDH
Description: 100P4B Lab Sample ID:CE10948-08 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 13:20 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 512
mg/kg dry
1
0.127
0.531
1G27021
EPA 6010D
07/29/21 10:16
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 12.8
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:45
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 11

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ANALYTICAL RESULTS
Description: 100P5A Lab Sample ID:CE10948-09 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 13:40 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.37
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 860
mg/kg dry
1
0.127
0.530
1G27021
EPA 6010D
07/29/21 10:18
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:48
JDH
Description: 100P5B Lab Sample ID:CE10948-10 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 14:00 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.81
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 801
mg/kg dry
1
0.127
0.527
1G27021
EPA 6010D
07/29/21 10:20
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:50
JDH
Description: 100P6A Lab Sample ID:CE10948-11 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 14:15 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 1730
mg/kg dry
1
0.132
0.548
1G27021
EPA 6010D
07/29/21 10:22
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 92.9
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:53
JDH
Description: 100P6B Lab Sample ID:CE10948-12 Received: 07/21/21 16:58
Matrix: Soil Sampled: 07/21/21 14:30 Work Order: CE10948
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 108.10
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1080
mg/kg dry
1
0.120
0.500
1G27021
EPA 6010D
07/29/21 10:24
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 20.9
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:56
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 11

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627021 - EPA 3050E
Blank (1G27021-BLK3) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27021-BS1) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:31
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.7
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27021-MS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:46
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
1160
0.529
mg/kg dry
10.8 980 NR 75-125
QM-07
Matrix Spike Dup (1G27021-MSD1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:48
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
973
0.529
mg/kg dry
10.8 980 NR 75-125 18
20
QM-07
Post Spike (1G27021-PS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:50
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.7
0.0100
mg/L
0.200 18.0 NR 80-120
QM-08
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IG29032 - EPA 3010A
Blank (1G29032-BLK3) Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 10:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
Blank (1G29032-BLK2) Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (1G29032-BS1) Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:06
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.198
0.0100
mg/L
0.200 99 80-120
Matrix Spike (1G29032-MS1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:14
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.98
0.500
mg/L
10.0 0.155 U 100 75-125
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 11

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1G29032 - EPA 3010A - Continued
Matrix Spike Dup (1G29032-MSD1) Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:17
Source: CE10948-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 9.73 0.500 mg/L 10.0 0.155 U 97 75-125 3 20
Post Spike (1G29032-PS1) Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:19
Source: CE10948-01
Analvte
Lead
Spike Source %REC
Result Flaq POL Units Level Result %REC Limits RPD
0.203 0.0100 mg/L 0.200-0.00181 101 80-120
RPD
Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 11

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 11

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, July 30, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11013
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, July 22, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 19

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P1A
Lab ID: CE11013-01
Sampled: 07/22/21 09:05
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:26
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 11:58
Client ID: 20OPlB
Lab ID: CE11013-02
Sampled: 07/22/21 09:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:28
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:01
Client ID: 200P2A
Lab ID: CE11013-03
Sampled: 07/22/21 09:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:40
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:03
Client ID: 200P213
Lab ID: CE11013-04
Sampled: 07/22/21 09:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:42
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:06
Client ID: 200P3A
Lab ID: CE11013-05
Sampled: 07/22/21 09:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:44
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:09
Client ID: 200P313
Lab ID: CE11013-06
Sampled: 07/22/21 10:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:46
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:19
Client ID: 200P4A
Lab ID: CE11013-07
Sampled: 07/22/21 10:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:48
Client ID: 200P413
Lab ID: CE11013-06
Sampled: 07/22/21 10:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:50
Client ID: 20OPSA
Lab ID: CE11013-09
Sampled: 07/22/21 10:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:01
Client ID: 200PSB
Lab ID: CE11013-10
Sampled: 07/22/21 10:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:21
Client ID: 200P6A
Lab ID: CE11013-11
Sampled: 07/22/21 10:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:23
Client ID: 20011613
Lab ID: CE11013-12
Sampled: 07/22/21 11:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:26
Client ID: 200117A
Lab ID: CE11013-13
Sampled: 07/22/21 11:05
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 19

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P713
Lab ID: CE11013-14
Sampled: 07/22/21 11:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:30
Client ID: 200P8A
Lab ID: CE11013-15
Sampled: 07/22/21 11:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:32
Client ID: 200PBB
Lab ID: CE11013-16
Sampled: 07/22/21 11:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:34
Client ID: 200P9A
Lab ID: CE11013-17
Sampled: 07/22/21 11:40
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:46
Client ID: 200P913
Lab ID: CE11013-18
Sampled: 07/22/21 11:50
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:48
Client ID: 200P10A
Lab ID: CE11013-19
Sampled: 07/22/21 12:00
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:50
Client ID: 20OP10B
Lab ID: CE11013-20
Sampled: 07/22/21 12:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:52
Client ID: 20OP11A
Lab ID: CE11013-21
Sampled: 07/22/21 13:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:54
Client ID: 20OP11B
Lab ID: CE11013-22
Sampled: 07/22/21 13:45
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:56
Client ID: 20OP12A
Lab ID: CE11013-23
Sampled: 07/22/21 14:00
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:58
Client ID: 20OP12B
Lab ID: CE11013-24
Sampled: 07/22/21 14:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:00
Client ID: 20OP13A
Lab ID: CE11013-25
Sampled: 07/22/21 14:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:02
Client ID: 20OP13B
Lab ID: CE11013-26
Sampled: 07/22/21 14:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:04
Client ID: 20OP14A
Lab ID: CE11013-27
Sampled: 07/22/21 14:40
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:43
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 19

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 20OP14B
Lab ID: CE11013-28
Sampled: 07/22/21 14:50
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:45
Client ID: A2S1
Lab ID: CE11013-29
Sampled: 07/21/21 15:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 12:56
Client ID: A2S2
Lab ID: CE11013-30
Sampled: 07/21/21 15:28
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:08
Client ID: A2S3
Lab ID: CE11013-31
Sampled: 07/21/21 15:32
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:21
Client ID: A2S4
Lab ID: CE11013-32
Sampled: 07/21/21 15:37
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:23
Client ID: A2S5
Lab ID: CE11013-33
Sampled: 07/21/21 15:42
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:26
Client ID: A2S6
Lab ID: CE11013-34
Sampled: 07/21/21 15:47
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:28
Client ID: A2S7
Lab ID: CE11013-35
Sampled: 07/21/21 15:54
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:30
Client ID: A2S8
Lab ID: CE11013-36
Sampled: 07/21/21 15:57
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1117122
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:33
Client ID: A2S9
Lab ID: CE11013-37
Sampled: 07/21/21 16:03
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:35
Client ID: A2S10
Lab ID: CE11013-38
Sampled: 07/21/21 16:07
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:37
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 19

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SAMPLE DETECTION SUMMARY
Client ID:
200P1A
Lab ID:
CE11013-01
Analvte
Lead - Total
Results
321
Flag
MDL
0.128
Q
0.535
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200PlB
Lab ID:
CE11013-02
Analvte
Lead - Total
Lead - TCLP
Results
232
1.38
Flag
MDL
0.130
0.155
Q
0.542
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P2A
Lab ID:
CE11013-03
Analvte
Lead - Total
Lead - TCLP
Results
177
1.36
Flag
MDL
0.128
0.155
Q
0.534
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P2B
Lab ID:
CE11013-04
Analvte
Lead - Total
Lead - TCLP
Results
146
0.784
Flag
MDL
0.128
0.155
Q
0.531
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P3A
Lab ID:
CE11013-05
Analvte
Lead - Total
Results
69.7
Flag
MDL
0.130
Q
0.541
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P3B
Lab ID:
CE11013-06
Analvte
Lead - Total
Lead - TCLP
Results
40.7
0.452
Flag
J
MDL
0.128
0.155
Q
0.534
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P4A
Lab ID:
CE11013-07
Analvte
Lead - Total
Results
1310
Flag
MDL
0.130
Q
0.541
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P4B
Lab ID:
CE11013-08
Analvte
Lead - Total
Results
282
Flag
MDL
0.128
Q
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200PSA
Lab ID:
CE11013-09
Analvte
Lead - Total
Results
267
Flag
MDL
0.128
PQL
0.535
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200PSB
Lab ID:
CE11013-10
Analvte
Lead - Total
Results
559
Flag
MDL
0.127
PQL
0.529
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P6A
Lab ID:
CE11013-11
Analvte
Lead - Total
Results
306
Flag
MDL
0.128
PQL
0.532
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P6B
Lab ID:
CE11013-12
Analvte
Lead - Total
Results
152
Flag
MDL
0.129
PQL
0.536
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P7A
Lab ID:
CE11013-13
Analvte
Lead - Total
Results
319
Flag
MDL
0.132
PQL
0.550
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P7B
Lab ID:
CE11013-14
Analvte
Lead - Total
Results
242
Flag
MDL
0.129
PQL
0.538
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P8A
Lab ID:
CE11013-15
Analvte
Lead - Total
Results
202
Flag
MDL
0.129
PQL
0.535
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P8B
Lab ID:
CE11013-16
Analvte
Lead - Total
Results
321
Flag
MDL
0.128
PQL
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P9A
Lab ID:
CE11013-17
Analvte
Lead - Total
Results
693
Flag
MDL
0.129
PQL
0.536
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 19

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SAMPLE DETECTION SUMMARY
Client ID: 200P9B Lab ID: CE11013-18
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 313 0.127 0.530 mq/kq dry EPA 6010D
I Client ID: 200P10A Lab ID: CE11013-19
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
62.4
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: 200P10B
Lab ID:
CE11013-20
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
55.1
0.126
0.527
mq/kq dry
EPA 6010D
I Client ID: 200P11A Lab ID: CE11013-21
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
290
0.127
0.531
mg/kg dry
EPA 6010D
Client ID: 200P11B
Lab ID:
CE11013-22
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
345
0.127
0.530
mq/kq dry
EPA 6010D
I Client ID: 200P12A Lab ID: CE11013-23
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
32.7
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: 200P12B
Lab ID:
CE11013-24
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
44.9
0.129
0.538
mq/kq dry
EPA 6010D
I Client ID: 200P13A Lab ID: CE11013-25
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
88.2
0.129
0.536
mg/kg dry
EPA 6010D
Client ID: 200P13B
Lab ID:
CE11013-26
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
67.6
0.128
0.535
mq/kq dry
EPA 6010D
I Client ID: 200P14A Lab ID: CE11013-27
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
227
0.130
0.543
mg/kg dry
EPA 6010D
Client ID: 200P14B
Lab ID:
CE11013-28
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
211
0.130
0.543
mq/kq dry
EPA 6010D
I Client ID: A2S3 Lab ID: CE11013-29
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.23
0.132
0.552
mg/kg dry
EPA 6010D
Client ID: A2S2
Lab ID:
CE11013-30
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.24
0.134
0.560
mq/kq dry
EPA 6010D
I Client ID: A2S3 Lab ID: CE11013-31
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.5
0.149
0.620
mg/kg dry
EPA 6010D
Client ID: A2S4
Lab ID:
CE11013-32
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.8
0.153
0.639
mq/kq dry
EPA 6010D
I Client ID: A2S5 Lab ID: CE11013-33
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
16.3
0.151
0.628
mg/kg dry
EPA 6010D
Client ID: A2S6
Lab ID:
CE11013-34
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.9
0.161
0.671
mq/kq dry
EPA 6010D
Client ID: A2S7 Lab ID: CE11013-35
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 16.4 0.143 0.598 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 19

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SAMPLE DETECTION SUMMARY
Client ID: A2S8 Lab ID: CE11013-36
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 22.6 0.167 0.696 mq/kq dry EPA 6010D
I Client ID: A2S9 Lab ID: CE11013-37
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
13.0
0.183
0.763
mg/kg dry
EPA 6010D
Client ID: A2S10
Lab ID:
CE11013-38
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
24.8
0.143
0.595
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 19

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ANALYTICAL RESULTS
Description: 20OPlA Lab Sample ID:CE11013-01 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.48
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 321
mg/kg dry
1
0.128
0.535
1G27021
EPA 6010D
07/29/21 10:26
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:58
JDH
Description: 20OPlB Lab Sample ID:CE11013-02 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 232
mg/kg dry
1
0.130
0.542
1G27021
EPA 6010D
07/29/21 10:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.38
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:01
JDH
Description: 200P2A Lab Sample ID:CE11013-03 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 177
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:40
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.36
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:03
JDH
Description: 200P2B Lab Sample ID:CE11013-04 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 146
mg/kg dry
1
0.128
0.531
1G27021
EPA 6010D
07/29/21 10:42
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.784
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:06
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 19

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ANALYTICAL RESULTS
Description: 200P3A Lab Sample ID:CE11013-05 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 69.7
mg/kg dry
1
0.130
0.541
1G27021
EPA 6010D
07/29/21 10:44
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:09
JDH
Description: 200P3B Lab Sample ID:CE11013-06 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.71
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 40.7
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.452 J
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:19
JDH
Description: 200P4A Lab Sample ID:CE11013-07 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.43
Metals by EPA 6000/7000 Series Methods `
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 1310 mg/kg dry 1 0.130 0.541 1G27021 EPA 6010D 07/29/21 10:48 JDH
Description: 200P4B Lab Sample ID:CE11013-08 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 282 mg/kg dry 1 0.128 0.533 1G27021 EPA 6010D 07/29/21 10:50 JDH
Description: 200P5A Lab Sample ID:CE11013-09 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.43
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Lead [7439-92-1]^
Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
267 mg/kg dry 1 0.128 0.535 1G27023 EPA 6010D 07/29/21 11:01 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 19

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ANALYTICAL RESULTS
Description: 200P5B Lab Sample ID:CE11013-10 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 559 mg/kg dry 1 0.127 0.529 1G27023 EPA 6010D 07/29/21 11:21 JDH
Description: 200P6A Lab Sample ID:CE11013-11 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 306 mg/kg dry 1 0.128 0.532 1G27023 EPA 6010D 07/29/21 11:23 JDH
Description: 200P6B Lab Sample ID:CE11013-12 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 152 mg/kg dry 1 0.129 0.536 1G27023 EPA 6010D 07/29/21 11:26 JDH
Description: 200P7A Lab Sample ID:CE11013-13 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.84
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 319 mg/kg dry 1 0.132 0.550 1G27023 EPA 6010D 07/29/21 11:28 JDH
Description: 200P7B Lab Sample ID:CE11013-14 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.99
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 242 mg/kg dry 1 0.129 0.538 1G27023 EPA 6010D 07/29/21 11:30 JDH
Description: 200P8A Lab Sample ID: CE11013-15 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 202 mg/kg dry 1 0.129 0.535 1G27023 EPA 6010D 07/29/21 11:32 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 19

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ANALYTICAL RESULTS
Description: 200P8B Lab Sample ID:CE11013-16 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 321 mg/kg dry 1 0.128 0.533 1G27023 EPA 6010D 07/29/21 11:34 JDH
Description: 200P9A Lab Sample ID:CE11013-17 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.28
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 693 mg/kg dry 1 0.129 0.536 1G27023 EPA 6010D 07/29/21 11:46 JDH
Description: 200P9B Lab Sample ID:CE11013-18 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 313 mg/kg dry 1 0.127 0.530 1G27023 EPA 6010D 07/29/21 11:48 JDH
Description: 20OP10A Lab Sample ID:CE11013-19 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.35
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 62.4 mg/kg dry 1 0.130 0.541 1G27023 EPA 6010D 07/29/21 11:50 JDH
Description: 20OP10B Lab Sample ID:CE11013-20 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.92
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 55.1 mg/kg dry 1 0.126 0.527 1G27023 EPA 6010D 07/29/21 11:52 JDH
Description: 20OP11A Lab Sample ID: CE11013-21 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.13
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 290 mg/kg dry 1 0.127 0.531 1G27023 EPA 6010D 07/29/21 11:54 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 19

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ANALYTICAL RESULTS
Description: 20OP11B Lab Sample ID:CE11013-22 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:45 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 345 mg/kg dry 1 0.127 0.530 1G27023 EPA 6010D 07/29/21 11:56 JDH
Description: 20OP12A Lab Sample ID:CE11013-23 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.36
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 32.7 mg/kg dry 1 0.130 0.541 1G27023 EPA 6010D 07/29/21 11:58 JDH
Description: 20OP12B Lab Sample ID:CE11013-24 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.90
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 44.9 mg/kg dry 1 0.129 0.538 1G27023 EPA 6010D 07/29/21 12:00 JDH
Description: 20OP13A Lab Sample ID:CE11013-25 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.33
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 88.2 mg/kg dry 1 0.129 0.536 1G27023 EPA 6010D 07/29/21 12:02 JDH
Description: 20OP13B Lab Sample ID:CE11013-26 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.42
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 67.6 mg/kg dry 1 0.128 0.535 1G27023 EPA 6010D 07/29/21 12:04 JDH
Description: 20OP14A Lab Sample ID: CE11013-27 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.12
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 227 mg/kg dry 1 0.130 0.543 1G27023 EPA 6010D 07/29/21 12:43 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 19

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ANALYTICAL RESULTS
Description: 20OP14B Lab Sample ID:CE11013-28 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 211 mg/kg dry 1 0.130 0.543 1G27023 EPA 6010D 07/29/21 12:45 JDH
Description: A2S1 Lab Sample ID:CE11013-29 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.61
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.23 mg/kg dry 1 0.132 0.552 1G27024 EPA 6010D 07/29/21 12:56 JDH
Description: A2S2 Lab Sample ID:CE11013-30 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:28 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 5.24 mg/kg dry 1 0.134 0.560 1G27024 EPA 6010D 07/29/21 13:08 JDH
Description: A2S3 Lab Sample ID:CE11013-31 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:32 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.59
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 15.5 mg/kg dry 1 0.149 0.620 1G27024 EPA 6010D 07/29/21 13:21 JDH
Description: A2S4 Lab Sample ID:CE11013-32 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:37 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.26
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.8 mg/kg dry 1 0.153 0.639 1G27024 EPA 6010D 07/29/21 13:23 JDH
Description: A2S5 Lab Sample ID:CE11013-33 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:42 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.64
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 16.3 mg/kg dry 1 0.151 0.628 1G27024 EPA 6010D 07/29/21 13:26 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 19

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ANALYTICAL RESULTS
Description: A2S6 Lab Sample ID:CE11013-34 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:47 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 74.52
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 12.9 mg/kg dry 1 0.161 0.671 1G27024 EPA 6010D 07/29/21 13:28 JDH
Description: A2S7 Lab Sample ID:CE11013-35 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:54 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.68
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 16.4 mg/kg dry 1 0.143 0.598 1G27024 EPA 6010D 07/29/21 13:30 JDH
Description: A2S8 Lab Sample ID:CE11013-36 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:57 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 71.79
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 22.6 mg/kg dry 1 0.167 0.696 1G27024 EPA 6010D 07/29/21 13:33 JDH
Description: A2S9 Lab Sample ID:CE11013-37 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:03 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.86
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.0 mg/kg dry 1.11 0.183 0.763 1G27024 EPA 6010D 07/29/21 13:35 JDH
Description: A2S10 Lab Sample ID:CE11013-38 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:07 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 24.8 mg/kg dry 1 0.143 0.595 1G27024 EPA 6010D 07/29/21 13:37 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 19

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627021 - EPA 3050E
Blank (1G27021-BLK3) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27021-BS1) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:31
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.7
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27021-MS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:46
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
1160
0.529
mg/kg dry
10.8 980 NR 75-125
QM-07
Matrix Spike Dup (1G27021-MSD1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:48
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
973
0.529
mg/kg dry
10.8 980 NR 75-125 18
20
QM-07
Post Spike (1G27021-PS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:50
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.7
0.0100
mg/L
0.200 18.0 NR 80-120
QM-08
Batch IG27023 - EPA 3050E
Blank (1G27023-BLK3) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27023-BS1) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:58
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/kg wet
10.2 111 80-120
Matrix Spike (1G27023-MS1)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:03
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
332
0.535
mg/kg dry
11.4 267 569 75-125
QM-07
Matrix Spike Dup (1G27023-MSD3)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:15
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
205
0.535
mg/kg dry
10.8 267 NR 75-125 47
20
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 19

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1G27023 - EPA 3050E - Continued
Post Spike (IG27023-PSI) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:17
Source: CE11013-09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 5.12 0.0100 mg/L 0.200 4.99 63 80-120 QM-08
Batch IG27024 - EPA 3050B
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.120
U
0.500
mg/kg wet
LCS (1G27024-BSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MSS)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (IG27024-PSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch I629032 - EPA 3010A
Blank (1G29032-BLK3)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 10:58
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
Blank (1G29032-BLK2)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
LCS (1G29032-BS1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:06
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.198
0.0100
mg/L
0.200 99 80-120
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 16 of 19

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1G29032 - EPA 3010A - Continued
Matrix Spike (1G29032-MSS)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:14
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.98
0.500
mg/L
10.0 0.155 U 100 75-125
Matrix Spike Dup (1G29032-MSD1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:17
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.73
0.500
mg/L
10.0 0.155 U 97 75-125 3
20
Post Spike (iG29032-PSI)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:19
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.203
0.0100
mg/L
0.200-0.00181 101 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 19

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-ii Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 19

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, August 4, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11013
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, July 22, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 20

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P1A
Lab ID: CE11013-01
Sampled: 07/22/21 09:05
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:26
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 11:58
Client ID: 20OPlB
Lab ID: CE11013-02
Sampled: 07/22/21 09:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:28
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:01
Client ID: 200P2A
Lab ID: CE11013-03
Sampled: 07/22/21 09:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:40
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:03
Client ID: 200P213
Lab ID: CE11013-04
Sampled: 07/22/21 09:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:42
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:06
Client ID: 200P3A
Lab ID: CE11013-05
Sampled: 07/22/21 09:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:44
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:09
Client ID: 200P313
Lab ID: CE11013-06
Sampled: 07/22/21 10:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:46
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:19
Client ID: 200P4A
Lab ID: CE11013-07
Sampled: 07/22/21 10:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:48
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 14:48
Client ID: 200P413
Lab ID: CE11013-08
Sampled: 07/22/21 10:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:50
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:02
Client ID: 20OPSA
Lab ID: CE11013-09
Sampled: 07/22/21 10:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:01
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:05
Client ID: 200PSB
Lab ID: CE11013-10
Sampled: 07/22/21 10:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:21
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:07
Client ID: 200P6A
Lab ID: CE11013-11
Sampled: 07/22/21 10:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:23
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:15
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 20

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P613
Lab ID: CE11013-12
Sampled: 07/22/21 11:00
Received: 07/22/21 16:55
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/18/22
O1/18/22 01/30/22
Prep Date/Time(s)
07/27/21 11:20
08/03/21 19:08
Analysis Date/Time(s)
07/29/21 11:26
08/04/21 15:17
Client ID: 200P7A
Lab ID: CE11013-13
Sampled: 07/22/21 11:05
Received: 07/22/21 16:55
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/18/22
O1/18/22 01/30/22
Prep Date/Time(s)
07/27/21 11:20
08/03/21 19:08
Analysis Date/Time(s)
07/29/21 11:28
08/04/21 15:20
Client ID: 200P713
Lab ID: CE11013-14
Sampled: 07/22/21 11:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/18/22
O1/18/22 01/30/22
Prep Date/Time(s)
07/27/21 11:20
08/03/21 19:08
Analysis Date/Time(s)
07/29/21 11:30
08/04/21 15:22
Client ID: 200P8A
Lab ID: CE11013-15
Sampled: 07/22/21 11:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/18/22
O1/18/22 01/30/22
Prep Date/Time(s)
07/27/21 11:20
08/03/21 19:08
Analysis Date/Time(s)
07/29/21 11:32
08/04/21 15:25
Client ID: 200P813
Lab ID: CE11013-16
Sampled: 07/22/21 11:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time
07/29/21 11:34
Client ID: 200P9A
Lab ID: CE11013-17
Sampled: 07/22/21 11:40
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:46
Client ID: 20012913
Lab ID: CE11013-18
Sampled: 07/22/21 11:50
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:48
Client ID: 20OP10A
Lab ID: CE11013-19
Sampled: 07/22/21 12:00
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:50
Client ID: 20OP10B
Lab ID: CE11013-20
Sampled: 07/22/21 12:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:52
Client ID: 20OP11A
Lab ID: CE11013-21
Sampled: 07/22/21 13:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:54
Client ID: 20OP11B
Lab ID: CE11013-22
Sampled: 07/22/21 13:45
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:56
Client ID: 20OP12A
Lab ID: CE11013-23
Sampled: 07/22/21 14:00
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 11:58
Client ID: 20OP12B
Lab ID: CE11013-24
Sampled: 07/22/21 14:10
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:00
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 20

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 20OP13A
Lab ID: CE11013-25
Sampled: 07/22/21 14:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:02
Client ID: 20OP13B
Lab ID: CE11013-26
Sampled: 07/22/21 14:30
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:04
Client ID: 20OP14A
Lab ID: CE11013-27
Sampled: 07/22/21 14:40
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:43
Client ID: 20OP14B
Lab ID: CE11013-28
Sampled: 07/22/21 14:50
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:20
Analysis Date/Time(s)
07/29/21 12:45
Client ID: A2S1
Lab ID: CE11013-29
Sampled: 07/21/21 15:20
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 12:56
Client ID: A2S2
Lab ID: CE11013-30
Sampled: 07/21/21 15:28
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:08
Client ID: A2S3
Lab ID: CE11013-31
Sampled: 07/21/21 15:32
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:21
Client ID: A2S4
Lab ID: CE11013-32
Sampled: 07/21/21 15:37
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(sl
07/29/21 13:23
Client ID: A2S5
Lab ID: CE11013-33
Sampled: 07/21/21 15:42
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1117122
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:26
Client ID: A2S6
Lab ID: CE11013-34
Sampled: 07/21/21 15:47
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:28
Client ID: A2S7
Lab ID: CE11013-35
Sampled: 07/21/21 15:54
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:30
Client ID: A2S8
Lab ID: CE11013-36
Sampled: 07/21/21 15:57
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:33
Client ID: A2S9
Lab ID: CE11013-37
Sampled: 07/21/21 16:03
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:35
Client ID: A2S10
Lab ID: CE11013-38
Sampled: 07/21/21 16:07
Received: 07/22/21 16:55
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/17/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:37
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 20

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SAMPLE DETECTION SUMMARY
Client ID: 200P1A Lab ID: CE11013-01
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 321 0.128 0.535 mq/kq dry EPA 6010D
I Client ID: 20OPlB Lab ID: CE11013-02
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
232
0.130
0.542
mg/kg dry
EPA 6010D
Lead - TCLP
1.38
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P2A
Lab ID:
CE11013-03
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
177
0.128
0.534
mg/kg dry
EPA 6010D
Lead - TCLP
1.36
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P2B
Lab ID:
CE11013-04
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
146
0.128
0.531
mg/kg dry
EPA 6010D
Lead - TCLP
0.784
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P3A
Lab ID:
CE11013-05
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
69.7
0.130
0.541
mg/kg dry
EPA 6010D
Client ID:
200P3B
Lab ID:
CE11013-06
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
40.7
0.128
0.534
mg/kg dry
EPA 6010D
Lead - TCLP
0.452
J
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P4A
Lab ID:
CE11013-07
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
1310
0.130
0.541
mg/kg dry
EPA 6010D
Lead - TCLP
8.49
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P4B
Lab ID:
CE11013-08
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
282
0.128
0.533
mg/kg dry
EPA 6010D
Lead - TCLP
0.739
0.155
0.500
mg/L
EPA 6010D
Client ID:
20OPSA
Lab ID:
CE11013-09
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
267
0.128
0.535
mg/kg dry
EPA 6010D
Lead - TCLP
8.87
0.155
0.500
mg/L
EPA 6010D
Client ID:
200PSB
Lab ID:
CE11013-10
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
559
0.127
0.529
mg/kg dry
EPA 6010D
Lead - TCLP
15.5
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P6A
Lab ID:
CE11013-11
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
306
0.128
0.532
mg/kg dry
EPA 6010D
Lead - TCLP
7.79
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P6B
Lab ID:
CE11013-12
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
152
0.129
0.536
mg/kg dry
EPA 6010D
Lead - TCLP
4.73
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P7A
Lab ID:
CE11013-13
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
319
0.132
0.550
mg/kg dry
EPA 6010D
Lead - TCLP
0.985
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P7B
Lab ID:
CE11013-14
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
242
0.129
0.538
mg/kg dry
EPA 6010D
Client ID:
200P8A
Lab ID:
CE11013-15
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
202
0.129
0.535
mg/kg dry
EPA 6010D
FINAL
This report relates only to the sample as received by
the laboratory,
and may only be reproduced
in full.
Page 5 of 20

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SAMPLE DETECTION SUMMARY
Client ID: 200P8B Lab ID: CE11013-16
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 321 0.128 0.533 mq/kq dry EPA 6010D
I Client ID: 200P9A Lab ID: CE11013-17
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
693
0.129
0.536
mg/kg dry
EPA 6010D
Client ID: 200P9B
Lab ID:
CE11013-18
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
313
0.127
0.530
mq/kq dry
EPA 6010D
I Client ID: 20OP10A Lab ID: CE11013-19
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
62.4
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: 20OP10B
Lab ID:
CE11013-20
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
55.1
0.126
0.527
mq/kq dry
EPA 6010D
I Client ID: 20OP11A Lab ID: CE11013-21
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
290
0.127
0.531
mg/kg dry
EPA 6010D
Client ID: 20OP11B
Lab ID:
CE11013-22
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
345
0.127
0.530
mq/kq dry
EPA 6010D
I Client ID: 20OP12A Lab ID: CE11013-23
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
32.7
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: 20OP12B
Lab ID:
CE11013-24
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
44.9
0.129
0.538
mq/kq dry
EPA 6010D
I Client ID: 20OP13A Lab ID: CE11013-25
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
88.2
0.129
0.536
mg/kg dry
EPA 6010D
Client ID: 20OP13B
Lab ID:
CE11013-26
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
67.6
0.128
0.535
mq/kq dry
EPA 6010D
I Client ID: 20OP14A Lab ID: CE11013-27
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
227
0.130
0.543
mg/kg dry
EPA 6010D
Client ID: 20OP14B
Lab ID:
CE11013-28
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
211
0.130
0.543
mq/kq dry
EPA 6010D
I Client ID: A2S3 Lab ID: CE11013-29
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.23
0.132
0.552
mg/kg dry
EPA 6010D
Client ID: A2S2
Lab ID:
CE11013-30
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.24
0.134
0.560
mq/kq dry
EPA 6010D
I Client ID: A2S3 Lab ID: CE11013-31
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.5
0.149
0.620
mg/kg dry
EPA 6010D
Client ID: A2S4
Lab ID:
CE11013-32
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.8
0.153
0.639
mq/kq dry
EPA 6010D
Client ID: A2S5 Lab ID: CE11013-33
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 16.3 0.151 0.628 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 20

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SAMPLE DETECTION SUMMARY
Client ID: A2S6 Lab ID: CE11013-34
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 12.9 0.161 0.671 mq/kq dry EPA 6010D
I Client ID: A2S7 Lab ID: CE11013-35
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
16.4
0.143
0.598
mg/kg dry
EPA 6010D
Client ID: A2S8
Lab ID:
CE11013-36
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
22.6
0.167
0.696
mq/kq dry
EPA 6010D
I Client ID: A2S9 Lab ID: CE11013-37
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
13.0
0.183
0.763
mg/kg dry
EPA 6010D
Client ID: A2S10
Lab ID:
CE11013-38
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
24.8
0.143
0.595
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 20

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ANALYTICAL RESULTS
Description: 20OPlA Lab Sample ID:CE11013-01 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.48
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 321
mg/kg dry
1
0.128
0.535
1G27021
EPA 6010D
07/29/21 10:26
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:58
JDH
Description: 20OPlB Lab Sample ID:CE11013-02 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 232
mg/kg dry
1
0.130
0.542
1G27021
EPA 6010D
07/29/21 10:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.38
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:01
JDH
Description: 200P2A Lab Sample ID:CE11013-03 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 177
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:40
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.36
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:03
JDH
Description: 200P2B Lab Sample ID:CE11013-04 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 146
mg/kg dry
1
0.128
0.531
1G27021
EPA 6010D
07/29/21 10:42
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.784
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:06
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 20

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ANALYTICAL RESULTS
Description: 200P3A Lab Sample ID:CE11013-05 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 69.7
mg/kg dry
1
0.130
0.541
1G27021
EPA 6010D
07/29/21 10:44
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:09
JDH
Description: 200P3B Lab Sample ID:CE11013-06 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.71
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 40.7
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.452 J
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:19
JDH
Description: 200P4A Lab Sample ID:CE11013-07 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 1310
mg/kg dry
1
0.130
0.541
1G27021
EPA 6010D
07/29/21 10:48
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 8.49
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 14:48
JDH
Description: 200P4B Lab Sample ID:CE11013-08 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 282
mg/kg dry
1
0.128
0.533
1G27021
EPA 6010D
07/29/21 10:50
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.739
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:02
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 20

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ANALYTICAL RESULTS
Description: 200P5A Lab Sample ID:CE11013-09 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 267
mg/kg dry
1
0.128
0.535
1G27023
EPA 6010D
07/29/21 11:01
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 8.87
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:05
JDH
Description: 200P5B Lab Sample ID:CE11013-10 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 559
mg/kg dry
1
0.127
0.529
1G27023
EPA 6010D
07/29/21 11:21
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 15.5
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:07
JDH
Description: 200P6A Lab Sample ID:CE11013-11 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 306
mg/kg dry
1
0.128
0.532
1G27023
EPA 6010D
07/29/21 11:23
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 7.79
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:15
JDH
Description: 200P6B Lab Sample ID:CE11013-12 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 152
mg/kg dry
1
0.129
0.536
1G27023
EPA 6010D
07/29/21 11:26
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 4.73
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:17
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 20

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ANALYTICAL RESULTS
Description: 200P7A Lab Sample ID:CE11013-13 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 319
mg/kg dry
1
0.132
0.550
1G27023
EPA 6010D
07/29/21 11:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.985
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:20
JDH
Description: 200P7B Lab Sample ID:CE11013-14 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.99
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 242
mg/kg dry
1
0.129
0.538
1G27023
EPA 6010D
07/29/21 11:30
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:22
JDH
Description: 200P8A Lab Sample ID:CE11013-15 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 202
mg/kg dry
1
0.129
0.535
1G27023
EPA 6010D
07/29/21 11:32
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:25
JDH
Description: 200P8B Lab Sample ID:CE11013-16 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 321 mg/kg dry 1 0.128 0.533 1G27023 EPA 6010D 07/29/21 11:34 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 20

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ANALYTICAL RESULTS
Description: 200P9A Lab Sample ID:CE11013-17 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.28
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 693 mg/kg dry 1 0.129 0.536 1G27023 EPA 6010D 07/29/21 11:46 JDH
Description: 200P9B Lab Sample ID:CE11013-18 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 313 mg/kg dry 1 0.127 0.530 1G27023 EPA 6010D 07/29/21 11:48 JDH
Description: 20OP10A Lab Sample ID:CE11013-19 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.35
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 62.4 mg/kg dry 1 0.130 0.541 1G27023 EPA 6010D 07/29/21 11:50 JDH
Description: 20OP10B Lab Sample ID:CE11013-20 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.92
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 55.1 mg/kg dry 1 0.126 0.527 1G27023 EPA 6010D 07/29/21 11:52 JDH
Description: 20OP11A Lab Sample ID:CE11013-21 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.13
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 290 mg/kg dry 1 0.127 0.531 1G27023 EPA 6010D 07/29/21 11:54 JDH
Description: 20OP11B Lab Sample ID: CE11013-22 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:45 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 345 mg/kg dry 1 0.127 0.530 1G27023 EPA 6010D 07/29/21 11:56 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 20

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ANALYTICAL RESULTS
Description: 20OP12A Lab Sample ID:CE11013-23 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.36
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 32.7 mg/kg dry 1 0.130 0.541 1G27023 EPA 6010D 07/29/21 11:58 JDH
Description: 20OP12B Lab Sample ID:CE11013-24 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.90
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 44.9 mg/kg dry 1 0.129 0.538 1G27023 EPA 6010D 07/29/21 12:00 JDH
Description: 20OP13A Lab Sample ID:CE11013-25 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.33
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 88.2 mg/kg dry 1 0.129 0.536 1G27023 EPA 6010D 07/29/21 12:02 JDH
Description: 20OP13B Lab Sample ID:CE11013-26 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.42
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 67.6 mg/kg dry 1 0.128 0.535 1G27023 EPA 6010D 07/29/21 12:04 JDH
Description: 20OP14A Lab Sample ID:CE11013-27 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.12
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 227 mg/kg dry 1 0.130 0.543 1G27023 EPA 6010D 07/29/21 12:43 JDH
Description: 20OP14B Lab Sample ID:CE11013-28 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 211 mg/kg dry 1 0.130 0.543 1G27023 EPA 6010D 07/29/21 12:45 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 20

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ANALYTICAL RESULTS
Description: A2S1 Lab Sample ID:CE11013-29 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.61
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 6.23 mg/kg dry 1 0.132 0.552 1G27024 EPA 6010D 07/29/21 12:56 JDH
Description: A2S2 Lab Sample ID:CE11013-30 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:28 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.24 mg/kg dry 1 0.134 0.560 1G27024 EPA 6010D 07/29/21 13:08 JDH
Description: A2S3 Lab Sample ID:CE11013-31 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:32 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.59
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 15.5 mg/kg dry 1 0.149 0.620 1G27024 EPA 6010D 07/29/21 13:21 JDH
Description: A2S4 Lab Sample ID:CE11013-32 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:37 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.26
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.8 mg/kg dry 1 0.153 0.639 1G27024 EPA 6010D 07/29/21 13:23 JDH
Description: A2S5 Lab Sample ID:CE11013-33 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:42 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.64
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 16.3 mg/kg dry 1 0.151 0.628 1G27024 EPA 6010D 07/29/21 13:26 JDH
Description: A2S6 Lab Sample ID: CE11013-34 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:47 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 74.52
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.9 mg/kg dry 1 0.161 0.671 1G27024 EPA 6010D 07/29/21 13:28 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 20

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ANALYTICAL RESULTS
Description: A2S7 Lab Sample ID:CE11013-35 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:54 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.68
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 16.4 mg/kg dry 1 0.143 0.598 1G27024 EPA 6010D 07/29/21 13:30 JDH
Description: A2S8 Lab Sample ID:CE11013-36 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:57 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 71.79
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.6 mg/kg dry 1 0.167 0.696 1G27024 EPA 6010D 07/29/21 13:33 JDH
Description: A2S9 Lab Sample ID:CE11013-37 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:03 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.86
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.0 mg/kg dry 1.11 0.183 0.763 1G27024 EPA 6010D 07/29/21 13:35 JDH
Description: A2S10 Lab Sample ID:CE11013-38 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:07 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 24.8 mg/kg dry 1 0.143 0.595 1G27024 EPA 6010D 07/29/21 13:37 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 20

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627021 - EPA 3050E
Blank (1G27021-BLK3) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27021-BS1) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:31
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.7
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27021-MS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:46
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
1160
0.529
mg/kg dry
10.8 980 NR 75-125
QM-07
Matrix Spike Dup (1G27021-MSD1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:48
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
973
0.529
mg/kg dry
10.8 980 NR 75-125 18
20
QM-07
Post Spike (1G27021-PS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:50
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.7
0.0100
mg/L
0.200 18.0 NR 80-120
QM-08
Batch IG27023 - EPA 3050E
Blank (1G27023-BLK3) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27023-BS1) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:58
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/kg wet
10.2 111 80-120
Matrix Spike (1G27023-MS1)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:03
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
332
0.535
mg/kg dry
11.4 267 569 75-125
QM-07
Matrix Spike Dup (1G27023-MSD3)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:15
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
205
0.535
mg/kg dry
10.8 267 NR 75-125 47
20
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 20

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1G27023 - EPA 3050E - Continued
Post Spike (IG27023-PSI) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:17
Source: CE11013-09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 5.12 0.0100 mg/L 0.200 4.99 63 80-120 QM-08
Batch IG27024 - EPA 3050B
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.120
U
0.500
mg/kg wet
LCS (1G27024-BSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MSS)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (IG27024-PSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch I629032 - EPA 3010A
Blank (1G29032-BLK3)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 10:58
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
Blank (1G29032-BLK2)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
LCS (1G29032-BS1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:06
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.198
0.0100
mg/L
0.200 99 80-120
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 17 of 20

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1G29032 - EPA 3010A - Continued
Matrix Spike (1G29032-MSS)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:14
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.98
0.500
mg/L
10.0 0.155 U 100 75-125
Matrix Spike Dup (1G29032-MSD1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:17
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.73
0.500
mg/L
10.0 0.155 U 97 75-125 3
20
Post Spike (iG29032-PSI)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:19
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.203
0.0100
mg/L
0.200-0.00181 101 80-120
Batch 1H03042 - EPA 3010A
Blank (lH03042-BLKI) Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (lH03042-BSI) Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:51
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.217
0.0100
mg/L
0.200 109 80-120
Matrix Spike (1H03042-MS1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:53
Source: CE11013-07
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
20.5
0.500
mg/L
10.0 8.49 120 75-125
Matrix Spike Dup (1H03042-MSD1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:56
Source: CE11013-07
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
21.2
0.500
mg/L
10.0 8.49 127 75-125 3
20
QM-07
Post Spike (1H03042-PS1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:58
Ill
Source: CE11013-07
Analvte
Lead
Spike Source %REC
Result Flaq POL Units Level Result %REC Limits RPD
0.392 0.0100 mg/L 0.200 0.170 111 80-120
RPD
Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 20

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-ii Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 20

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 5, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11013
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, July 22, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P1A
Lab ID: CE11013-01
Sampled: 07/22/21 09:05
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:26
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 11:58
Client ID: 20OPlB
Lab ID: CE11013-02
Sampled: 07/22/21 09:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:28
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:01
Client ID: 200P2A
Lab ID: CE11013-03
Sampled: 07/22/21 09:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:40
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:03
Client ID: 200P213
Lab ID: CE11013-04
Sampled: 07/22/21 09:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:42
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:06
Client ID: 200P3A
Lab ID: CE11013-05
Sampled: 07/22/21 09:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:44
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:09
Client ID: 200P313
Lab ID: CE11013-06
Sampled: 07/22/21 10:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:46
EPA 6010D
EPA 3010A
O1/18/22 01/25/22
07/29/21 15:21
07/30/21 12:19
Client ID: 200P4A
Lab ID: CE11013-07
Sampled: 07/22/21 10:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:48
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 14:48
Client ID: 200P413
Lab ID: CE11013-08
Sampled: 07/22/21 10:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:14
07/29/21 10:50
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:02
Client ID: 20OPSA
Lab ID: CE11013-09
Sampled: 07/22/21 10:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:01
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:05
Client ID: 200PSB
Lab ID: CE11013-10
Sampled: 07/22/21 10:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:21
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:07
Client ID: 200P6A
Lab ID: CE11013-11
Sampled: 07/22/21 10:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:23
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:15
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P613
Lab ID: CE11013-12
Sampled: 07/22/21 11:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:26
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:17
Client ID: 200P7A
Lab ID: CE11013-13
Sampled: 07/22/21 11:05
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:28
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:20
Client ID: 200P713
Lab ID: CE11013-14
Sampled: 07/22/21 11:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:30
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:22
Client ID: 200P8A
Lab ID: CE11013-15
Sampled: 07/22/21 11:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:32
EPA 6010D
EPA 3010A
O1/18/22 01/30/22
08/03/21 19:08
08/04/21 15:25
Client ID: 200P813
Lab ID: CE11013-16
Sampled: 07/22/21 11:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:34
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 10:19
Client ID: 200P9A
Lab ID: CE11013-17
Sampled: 07/22/21 11:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:46
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 10:33
Client ID: 200P913
Lab ID: CE11013-18
Sampled: 07/22/21 11:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:48
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 10:36
Client ID: 200P10A
Lab ID: CE11013-19
Sampled: 07/22/21 12:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:50
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 10:56
Client ID: 200P10B
Lab ID: CE11013-20
Sampled: 07/22/21 12:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:52
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 10:59
Client ID: 20OP11A
Lab ID: CE11013-21
Sampled: 07/22/21 13:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:54
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:01
Client ID: 20OP11B
Lab ID: CE11013-22
Sampled: 07/22/21 13:45
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:56
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:04
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 20OP12A
Lab ID: CE11013-23
Sampled: 07/22/21 14:00
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 11:58
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:06
Client ID: 20OP12B
Lab ID: CE11013-24
Sampled: 07/22/21 14:10
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 12:00
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:09
Client ID: 20OP13A
Lab ID: CE11013-25
Sampled: 07/22/21 14:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 12:02
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:12
Client ID: 20OP13B
Lab ID: CE11013-26
Sampled: 07/22/21 14:30
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 12:04
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:14
Client ID: 20OP14A
Lab ID: CE11013-27
Sampled: 07/22/21 14:40
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 12:43
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:17
Client ID: 20OP14B
Lab ID: CE11013-28
Sampled: 07/22/21 14:50
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/18/22
07/27/21 11:20
07/29/21 12:45
EPA 6010D
EPA 3010A
O1/18/22 01/31/22
08/04/21 16:52
08/05/21 11:19
Client ID: A2S1
Lab ID: CE11013-29
Sampled: 07/21/21 15:20
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 12:56
Client ID: A2S2
Lab ID: CE11013-30
Sampled: 07/21/21 15:28
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:08
Client ID: A2S3
Lab ID: CE11013-31
Sampled: 07/21/21 15:32
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:21
Client ID: A2S4
Lab ID: CE11013-32
Sampled: 07/21/21 15:37
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:23
Client ID: A2S5
Lab ID: CE11013-33
Sampled: 07/21/21 15:42
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:26
Client ID: A2S6
Lab ID: CE11013-34
Sampled: 07/21/21 15:47
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:28
Client ID: A2S7
Lab ID: CE11013-35
Sampled: 07/21/21 15:54
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:30
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2S8
Lab ID: CE11013-36
Sampled: 07/21/21 15:57
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:33
Client ID: A2S9
Lab ID: CE11013-37
Sampled: 07/21/21 16:03
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:35
Client ID: A2S10
Lab ID: CE11013-38
Sampled: 07/21/21 16:07
Received: 07/22/21 16:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/17/22
07/27/21 11:24
07/29/21 13:37
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 23

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SAMPLE DETECTION SUMMARY
Client ID: 200P1A Lab ID: CE11013-01
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 321 0.128 0.535 mq/kq dry EPA 6010D
I Client ID: 200PlB Lab ID: CE11013-02
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
232
0.130
0.542
mg/kg dry
EPA 6010D
Lead - TCLP
1.38
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P2A
Lab ID:
CE11013-03
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
177
0.128
0.534
mg/kg dry
EPA 6010D
Lead - TCLP
1.36
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P2B
Lab ID:
CE11013-04
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
146
0.128
0.531
mg/kg dry
EPA 6010D
Lead - TCLP
0.784
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P3A
Lab ID:
CE11013-05
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
69.7
0.130
0.541
mg/kg dry
EPA 6010D
Client ID:
200P3B
Lab ID:
CE11013-06
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
40.7
0.128
0.534
mg/kg dry
EPA 6010D
Lead - TCLP
0.452
3
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P4A
Lab ID:
CE11013-07
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
1310
0.130
0.541
mg/kg dry
EPA 6010D
Lead - TCLP
8.49
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P4B
Lab ID:
CE11013-08
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
282
0.128
0.533
mg/kg dry
EPA 6010D
Lead - TCLP
0.739
0.155
0.500
mg/L
EPA 6010D
Client ID:
200PSA
Lab ID:
CE11013-09
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
267
0.128
0.535
mg/kg dry
EPA 6010D
Lead - TCLP
8.87
0.155
0.500
mg/L
EPA 6010D
Client ID:
200PSB
Lab ID:
CE11013-10
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
559
0.127
0.529
mg/kg dry
EPA 6010D
Lead - TCLP
15.5
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P6A
Lab ID:
CE11013-11
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
306
0.128
0.532
mg/kg dry
EPA 6010D
Lead - TCLP
7.79
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P6B
Lab ID:
CE11013-12
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
152
0.129
0.536
mg/kg dry
EPA 6010D
Lead - TCLP
4.73
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P7A
Lab ID:
CE11013-13
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
319
0.132
0.550
mg/kg dry
EPA 6010D
Lead - TCLP
0.985
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P7B
Lab ID:
CE11013-14
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
242
0.129
0.538
mg/kg dry
EPA 6010D
Client ID:
200P8A
Lab ID:
CE11013-15
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
202
0.129
0.535
mg/kg dry
EPA 6010D
FINAL
This report relates only to the sample as received by
the laboratory,
and may only be reproduced
in full.
Page 6 of 23

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SAMPLE DETECTION SUMMARY
Client ID:
200P8B
Lab ID:
CE11013-16
Analvte
Lead - Total
Results
321
Flag
MDL
0.128
Q
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P9A
Lab ID:
CE11013-17
Analvte
Lead - Total
Lead - TCLP
Results
693
3.81
Flag
MDL
0.129
0.155
Q
0.536
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P9B
Lab ID:
CE11013-18
Analvte
Lead - Total
Results
313
Flag
MDL
0.127
Q
0.530
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P10A
Lab ID:
CE11013-19
Analvte
Lead - Total
Lead - TCLP
Results
62.4
0.319
Flag
3
MDL
0.130
0.155
Q
0.541
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
200P10B
Lab ID:
CE11013-20
Analvte
Lead - Total
Results
55.1
Flag
MDL
0.126
PQL
0.527
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P11A
Lab ID:
CE11013-21
Analvte
Lead - Total
Results
290
Flag
MDL
0.127
PQL
0.531
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P11B
Lab ID:
CE11013-22
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
345
0.127
0.530
mg/kg dry
EPA 6010D
Lead -TCLP
8.24
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P12A
Lab ID:
CE11013-23
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
32.7
0.130
0.541
mg/kg dry
EPA 6010D
Client ID:
200P12B
Lab ID:
CE11013-24
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
44.9
0.129
0.538
mg/kg dry
EPA 6010D
Lead - TCLP
0.159
3
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P13A
Lab ID:
CE11013-25
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
88.2
0.129
0.536
mg/kg dry
EPA 6010D
Lead - TCLP
0.579
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P13B
Lab ID:
CE11013-26
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
67.6
0.128
0.535
mg/kg dry
EPA 6010D
Lead - TCLP
1.16
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P14A
Lab ID:
CE11013-27
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
227
0.130
0.543
mg/kg dry
EPA 6010D
Lead - TCLP
0.498
3
0.155
0.500
mg/L
EPA 6010D
Client ID:
200P14B
Lab ID:
CE11013-28
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
211
0.130
0.543
mg/kg dry
EPA 6010D
Lead - TCLP
0.322
3
0.155
0.500
mg/L
EPA 6010D
Client ID:
A2S3
Lab ID:
CE11013-29
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
6.23
0.132
0.552
mg/kg dry
EPA 6010D
Client ID:
A2S2
Lab ID:
CE11013-30
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
5.24
0.134
0.560
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 23

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SAMPLE DETECTION SUMMARY
Client ID: A2S3 Lab ID: CE11013-31
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 15.5 0.149 0.620 mq/kq dry EPA 6010D
I Client ID: A2S4 Lab ID: CE11013-32
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
12.8
0.153
0.639
mg/kg dry
EPA 6010D
Client ID: A2S5
Lab ID:
CE11013-33
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
16.3
0.151
0.628
mq/kq dry
EPA 6010D
I Client ID: A2S6 Lab ID: CE11013-34
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
12.9
0.161
0.671
mg/kg dry
EPA 6010D
Client ID: A2S7
Lab ID:
CE11013-35
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
16.4
0.143
0.598
mq/kq dry
EPA 6010D
I Client ID: A2S8 Lab ID: CE11013-36
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
22.6
0.167
0.696
mg/kg dry
EPA 6010D
Client ID: A2S9
Lab ID:
CE11013-37
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
13.0
0.183
0.763
mq/kq dry
EPA 6010D
Client ID: A2S10 Lab ID: CE11013-38
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 24.8 0.143 0.595 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 23

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ANALYTICAL RESULTS
Description: 20OPlA Lab Sample ID:CE11013-01 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.48
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 321
mg/kg dry
1
0.128
0.535
1G27021
EPA 6010D
07/29/21 10:26
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 11:58
JDH
Description: 20OPlB Lab Sample ID:CE11013-02 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 232
mg/kg dry
1
0.130
0.542
1G27021
EPA 6010D
07/29/21 10:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.38
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:01
JDH
Description: 200P2A Lab Sample ID:CE11013-03 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 177
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:40
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.36
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:03
JDH
Description: 200P2B Lab Sample ID:CE11013-04 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 146
mg/kg dry
1
0.128
0.531
1G27021
EPA 6010D
07/29/21 10:42
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.784
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:06
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 23

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ANALYTICAL RESULTS
Description: 200P3A Lab Sample ID:CE11013-05 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/2109:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 69.7
mg/kg dry
1
0.130
0.541
1G27021
EPA 6010D
07/29/21 10:44
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:09
JDH
Description: 200P3B Lab Sample ID:CE11013-06 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.71
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 40.7
mg/kg dry
1
0.128
0.534
1G27021
EPA 6010D
07/29/21 10:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.452 J
mg/L
50
0.155
0.500
1G29032
EPA 6010D
07/30/21 12:19
JDH
Description: 200P4A Lab Sample ID:CE11013-07 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 1310
mg/kg dry
1
0.130
0.541
1G27021
EPA 6010D
07/29/21 10:48
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 8.49
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 14:48
JDH
Description: 200P4B Lab Sample ID:CE11013-08 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 282
mg/kg dry
1
0.128
0.533
1G27021
EPA 6010D
07/29/21 10:50
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.739
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:02
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 23

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ANALYTICAL RESULTS
Description: 200P5A Lab Sample ID:CE11013-09 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 267
mg/kg dry
1
0.128
0.535
1G27023
EPA 6010D
07/29/21 11:01
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 8.87
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:05
JDH
Description: 200P5B Lab Sample ID:CE11013-10 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 559
mg/kg dry
1
0.127
0.529
1G27023
EPA 6010D
07/29/21 11:21
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 15.5
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:07
JDH
Description: 200P6A Lab Sample ID:CE11013-11 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 10:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 306
mg/kg dry
1
0.128
0.532
1G27023
EPA 6010D
07/29/21 11:23
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 7.79
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:15
JDH
Description: 200P6B Lab Sample ID:CE11013-12 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 152
mg/kg dry
1
0.129
0.536
1G27023
EPA 6010D
07/29/21 11:26
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 4.73
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:17
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 23

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ANALYTICAL RESULTS
Description: 200P7A Lab Sample ID:CE11013-13 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:05 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 319
mg/kg dry
1
0.132
0.550
1G27023
EPA 6010D
07/29/21 11:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.985
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:20
JDH
Description: 200P7B Lab Sample ID:CE11013-14 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.99
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 242
mg/kg dry
1
0.129
0.538
1G27023
EPA 6010D
07/29/21 11:30
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:22
JDH
Description: 200P8A Lab Sample ID:CE11013-15 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 202
mg/kg dry
1
0.129
0.535
1G27023
EPA 6010D
07/29/21 11:32
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H03042
EPA 6010D
08/04/21 15:25
JDH
Description: 200P8B Lab Sample ID:CE11013-16 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.80
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 321
mg/kg dry
1
0.128
0.533
1G27023
EPA 6010D
07/29/21 11:34
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 10:19
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 23

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ANALYTICAL RESULTS
Description: 200P9A Lab Sample ID:CE11013-17 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.28
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 693
mg/kg dry
1
0.129
0.536
1G27023
EPA 6010D
07/29/21 11:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 3.81
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 10:33
JDH
Description: 200P9B Lab Sample ID:CE11013-18 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 11:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 313
mg/kg dry
1
0.127
0.530
1G27023
EPA 6010D
07/29/21 11:48
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 10:36
JDH
Description: 20OP10A Lab Sample ID:CE11013-19 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.35
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 62.4
mg/kg dry
1
0.130
0.541
1G27023
EPA 6010D
07/29/21 11:50
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.319 J
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 10:56
JDH
Description: 20OP10B Lab Sample ID:CE11013-20 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 12:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.92
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 55.1
mg/kg dry
1
0.126
0.527
1G27023
EPA 6010D
07/29/21 11:52
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 10:59
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 23

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ANALYTICAL RESULTS
Description: 20OP11A Lab Sample ID:CE11013-21 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.13
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 290
mg/kg dry
1
0.127
0.531
1G27023
EPA 6010D
07/29/21 11:54
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:01
JDH
Description: 20OP11B Lab Sample ID:CE11013-22 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 13:45 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 345
mg/kg dry
1
0.127
0.530
1G27023
EPA 6010D
07/29/21 11:56
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 8.24
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:04
JDH
Description: 20OP12A Lab Sample ID:CE11013-23 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:00 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.36
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 32.7
mg/kg dry
1
0.130
0.541
1G27023
EPA 6010D
07/29/21 11:58
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:06
JDH
Description: 20OP12B Lab Sample ID:CE11013-24 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:10 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.90
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 44.9
mg/kg dry
1
0.129
0.538
1G27023
EPA 6010D
07/29/21 12:00
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.159 J
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:09
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 23

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ANALYTICAL RESULTS
Description: 20OP13A Lab Sample ID:CE11013-25 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.33
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 88.2
mg/kg dry
1
0.129
0.536
1G27023
EPA 6010D
07/29/21 12:02
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.579
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:12
JDH
Description: 20OP13B Lab Sample ID:CE11013-26 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:30 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.42
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 67.6
mg/kg dry
1
0.128
0.535
1G27023
EPA 6010D
07/29/21 12:04
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 1.16
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:14
JDH
Description: 20OP14A Lab Sample ID:CE11013-27 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:40 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.12
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 227
mg/kg dry
1
0.130
0.543
1G27023
EPA 6010D
07/29/21 12:43
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.498 J
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:17
JDH
Description: 20OP14B Lab Sample ID:CE11013-28 Received: 07/22/21 16:55
Matrix: Soil Sampled: 07/22/21 14:50 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 211
mg/kg dry
1
0.130
0.543
1G27023
EPA 6010D
07/29/21 12:45
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.322 J
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:19
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 23

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ANALYTICAL RESULTS
Description: A2S1 Lab Sample ID:CE11013-29 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:20 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.61
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 6.23 mg/kg dry 1 0.132 0.552 1G27024 EPA 6010D 07/29/21 12:56 JDH
Description: A2S2 Lab Sample ID:CE11013-30 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:28 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.24 mg/kg dry 1 0.134 0.560 1G27024 EPA 6010D 07/29/21 13:08 JDH
Description: A2S3 Lab Sample ID:CE11013-31 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:32 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.59
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 15.5 mg/kg dry 1 0.149 0.620 1G27024 EPA 6010D 07/29/21 13:21 JDH
Description: A2S4 Lab Sample ID:CE11013-32 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:37 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.26
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.8 mg/kg dry 1 0.153 0.639 1G27024 EPA 6010D 07/29/21 13:23 JDH
Description: A2S5 Lab Sample ID:CE11013-33 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:42 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.64
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 16.3 mg/kg dry 1 0.151 0.628 1G27024 EPA 6010D 07/29/21 13:26 JDH
Description: A2S6 Lab Sample ID: CE11013-34 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:47 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 74.52
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.9 mg/kg dry 1 0.161 0.671 1G27024 EPA 6010D 07/29/21 13:28 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 23

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ANALYTICAL RESULTS
Description: A2S7 Lab Sample ID:CE11013-35 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:54 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.68
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 16.4 mg/kg dry 1 0.143 0.598 1G27024 EPA 6010D 07/29/21 13:30 JDH
Description: A2S8 Lab Sample ID:CE11013-36 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:57 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 71.79
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.6 mg/kg dry 1 0.167 0.696 1G27024 EPA 6010D 07/29/21 13:33 JDH
Description: A2S9 Lab Sample ID:CE11013-37 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:03 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.86
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.0 mg/kg dry 1.11 0.183 0.763 1G27024 EPA 6010D 07/29/21 13:35 JDH
Description: A2S10 Lab Sample ID:CE11013-38 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 16:07 Work Order: CE11013
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 24.8 mg/kg dry 1 0.143 0.595 1G27024 EPA 6010D 07/29/21 13:37 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 23

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627021 - EPA 3050E
Blank (1G27021-BLK3) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27021-BS1) Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:31
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.7
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27021-MS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:46
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
1160
0.529
mg/kg dry
10.8 980 NR 75-125
QM-07
Matrix Spike Dup (1G27021-MSD1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:48
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
973
0.529
mg/kg dry
10.8 980 NR 75-125 18
20
QM-07
Post Spike (1G27021-PS1)
Prepared: 07/27/2021 11:14 Analyzed: 07/29/2021 09:50
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.7
0.0100
mg/L
0.200 18.0 NR 80-120
QM-08
Batch IG27023 - EPA 3050E
Blank (1G27023-BLK3) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27023-BS1) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 10:58
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/kg wet
10.2 111 80-120
Matrix Spike (1G27023-MS1)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:03
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
332
0.535
mg/kg dry
11.4 267 569 75-125
QM-07
Matrix Spike Dup (1G27023-MSD3)
Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:15
Source: CE11013-09
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
205
0.535
mg/kg dry
10.8 267 NR 75-125 47
20
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 23

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1G27023 - EPA 3050E - Continued
Post Spike (IG27023-PSI) Prepared: 07/27/2021 11:20 Analyzed: 07/29/2021 11:17
Source: CE11013-09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 5.12 0.0100 mg/L 0.200 4.99 63 80-120 QM-08
Batch IG27024 - EPA 3050B
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.120
U
0.500
mg/kg wet
LCS (1G27024-BSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MSS)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (IG27024-PSI)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch I629032 - EPA 3010A
Blank (1G29032-BLK3)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 10:58
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
Blank (1G29032-BLK2)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
LCS (1G29032-BS1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:06
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.198
0.0100
mg/L
0.200 99 80-120
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 19 of 23

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1G29032 - EPA 3010A - Continued
Matrix Spike (1G29032-MSS)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:14
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.98
0.500
mg/L
10.0 0.155 U 100 75-125
Matrix Spike Dup (1G29032-MSD1)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:17
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.73
0.500
mg/L
10.0 0.155 U 97 75-125 3
20
Post Spike (iG29032-PSI)
Prepared: 07/29/2021 15:21 Analyzed: 07/30/2021 11:19
Source: CE10948-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.203
0.0100
mg/L
0.200-0.00181 101 80-120
Batch 1H03042 - EPA 3010A
Blank (lH03042-BLKI) Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (lH03042-BSI) Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:51
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.217
0.0100
mg/L
0.200 109 80-120
Matrix Spike (1H03042-MS1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:53
Source: CE11013-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
20.5
0.500
mg/L
10.0 8.49 120 75-125
Matrix Spike Dup (1H03042-MSD1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:56
Source: CE11013-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
21.2
0.500
mg/L
10.0 8.49 127 75-125 3
20
QM-07
Post Spike (1H03042-PS1)
Prepared: 08/03/2021 19:08 Analyzed: 08/04/2021 14:58
Source: CE11013-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.392
0.0100
mg/L
0.200 0.170 111 80-120
Batch IH04038 - EPA 3010A
Blank (lH04038-BLKI) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 23

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1H04038 - EPA 3010A - Continued
Blank (1H04038-BLK2) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (1H04038-BS1) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.209
0.0100
mg/L
0.200 105 80-120
Matrix Spike (1H04038-MS1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:24
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/L
10.0 0.155 U 113 75-125
Matrix Spike Dup (1H04038-MSD1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:26
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.2
0.500
mg/L
10.0 0.155 U 112 75-125 1
20
Post Spike (11-104038-PS1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:28
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.212
0.0100
mg/L
0.200 0.00262 105 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 23

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-ii Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 23

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, August 2, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11137
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, July 23, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SIDEPIA
Lab ID: CE11137-01
Sampled: 07/23/21 09:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:39
Client ID: SIDEPIB
Lab ID: CE11137-02
Sampled: 07/23/21 09:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:41
Client ID: SIDE132A
Lab ID: CE11137-03
Sampled: 07/23/21 09:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:53
Client ID: SIDEPSB
Lab ID: CE11137-04
Sampled: 07/23/21 09:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:55
Client ID: SIDE133A
Lab ID: CE11137-05
Sampled: 07/23/21 09:30
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:57
Client ID: SIDEP311
Lab ID: CE11137-06
Sampled: 07/23/21 09:40
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:59
Client ID: SIDEMA
Lab ID: CE11137-07
Sampled: 07/23/21 09:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:01
Client ID: SIDEP413
Lab ID: CE11137-08
Sampled: 07/23/21 10:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:03
Client ID: SIDEPSA
Lab ID: CE11137-09
Sampled: 07/23/21 10:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:05
Client ID: SIDEPSB
Lab ID: CE11137-10
Sampled: 07/23/21 10:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8

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SAMPLE DETECTION SUMMARY
Client ID: SIDEPIA Lab ID: CE11137-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 26.5 0.130 0.542 mq/kq dry EPA 6010D
I Client ID: SIDEPIB Lab ID: CE11137-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.9
0.129
0.537
mg/kg dry
EPA 6010D
Client ID: SIDEP2A
Lab ID:
CE11137-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.6
0.125
0.522
mq/kq dry
EPA 6010D
I Client ID: SIDEP28 Lab ID: CE11137-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.3
0.126
0.527
mg/kg dry
EPA 6010D
Client ID: SIDEP3A
Lab ID:
CE11137-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.1
0.129
0.536
mq/kq dry
EPA 6010D
I Client ID: SIDEP38 Lab ID: CE11137-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
28.9
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: SIDEP4A
Lab ID:
CE11137-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
0.200
0.00132
0.00548
mq/kq dry
EPA 6010D
I Client ID: SIDEP48 Lab ID: CE11137-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
32.5
0.128
0.533
mg/kg dry
EPA 6010D
Client ID: SIDEPSA
Lab ID:
CE11137-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.9
0.128
0.532
mq/kq dry
EPA 6010D
Client ID: SIDEP58 Lab ID: CE11137-10
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 24.7 0.128 0.534 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8

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ANALYTICAL RESULTS
Description: SIDEPIA Lab Sample ID:CE11137-01 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 26.5 mg/kg dry 1 0.130 0.542 1G27024 EPA 6010D 07/29/21 13:39 JDH
Description: SIDEPIB Lab Sample ID:CE11137-02 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.19
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 23.9 mg/kg dry 1 0.129 0.537 1G27024 EPA 6010D 07/29/21 13:41 JDH
Description: SIDEP2A Lab Sample ID:CE11137-03 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 12.6 mg/kg dry 1 0.125 0.522 1G27024 EPA 6010D 07/29/21 13:53 JDH
Description: SIDEP2B Lab Sample ID:CE11137-04 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.96
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 15.3 mg/kg dry 1 0.126 0.527 1G27024 EPA 6010D 07/29/21 13:55 JDH
Description: SIDEP3A Lab Sample ID:CE11137-05 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:30 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 23.1 mg/kg dry 1 0.129 0.536 1G27024 EPA 6010D 07/29/21 13:57 JDH
Description: SIDEP3B Lab Sample ID: CE11137-06 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:40 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.44
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 28.9 mg/kg dry 1 0.130 0.541 1G27024 EPA 6010D 07/29/21 13:59 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8

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ANALYTICAL RESULTS
Description: SIDEP4A Lab Sample ID:CE11137-07 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 0.200 mg/kg dry 0.0104 0.00132 0.00548 1G27024 EPA 6010D 07/29/21 14:01 JDH
Description: SIDEP4B Lab Sample ID:CE11137-08 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 32.5 mg/kg dry 1 0.128 0.533 1G27024 EPA 6010D 07/29/21 14:03 JDH
Description: SIDEP5A Lab Sample ID:CE11137-09 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.96
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 17.9 mg/kg dry 1 0.128 0.532 1G27024 EPA 6010D 07/29/21 14:05 JDH
Description: SIDEP5B Lab Sample ID:CE11137-10 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 24.7 mg/kg dry 1 0.128 0.534 1G27024 EPA 6010D 07/29/21 14:07 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 8

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627024 - EPA 3050E
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27024-BS1) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (1G27024-PS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8

0
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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 5, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11137
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, July 23, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 16

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SIDEPIA
Lab ID: CE11137-01
Sampled: 07/23/21 09:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/19/22
O1/19/22 01/31/22
Prep Date/Time(s)
07/27/21 11:24
08/04/21 16:52
Analysis Date/Time(s)
07/29/21 13:39
08/05/21 11:35
Client ID: SIDEPSB
Lab ID: CE11137-02
Sampled: 07/23/21 09:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/19/22
O1/19/22 01/31/22
Prep Date/Time(s)
07/27/21 11:24
08/04/21 16:52
Analysis Date/Time(s)
07/29/21 13:41
08/05/21 11:38
Client ID: SIDE132A
Lab ID: CE11137-03
Sampled: 07/23/21 09:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/19/22
O1/19/22 01/31/22
Prep Date/Time(s)
07/27/21 11:24
08/04/21 16:52
Analysis Date/Time(s)
07/29/21 13:53
08/05/21 11:41
Client ID: SIDEPSB
Lab ID: CE11137-04
Sampled: 07/23/21 09:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/19/22
O1/19/22 01/31/22
Prep Date/Time(s)
07/27/21 11:24
08/04/21 16:52
Analysis Date/Time(s)
07/29/21 13:55
08/05/21 11:43
Client ID: SIDE133A
Lab ID: CE11137-05
Sampled: 07/23/21 09:30
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time
07/29/21 13:57
Client ID: SIDEP313
Lab ID: CE11137-06
Sampled: 07/23/21 09:40
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 13:59
Client ID: SIDEMA
Lab ID: CE11137-07
Sampled: 07/23/21 09:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:01
Client ID: SIDEP413
Lab ID: CE11137-08
Sampled: 07/23/21 10:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:03
Client ID: SIDEPSA
Lab ID: CE11137-09
Sampled: 07/23/21 10:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:05
Client ID: SIDEPSB
Lab ID: CE11137-10
Sampled: 07/23/21 10:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:24
Analysis Date/Time(s)
07/29/21 14:07
Client ID: HA46P1A
Lab ID: CE11137-11
Sampled: 07/23/21 12:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:27
Client ID: HA46P1B
Lab ID: CE11137-12
Sampled: 07/23/21 13:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:38
Client ID: A2S11
Lab ID: CE11137-13
Sampled: 07/22/21 15:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 16

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2S32
Lab ID: CE11137-14
Sampled: 07/22/21 15:55
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:42
Client ID: A2S13
Lab ID: CE11137-15
Sampled: 07/22/21 16:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:03
Client ID: A2S14
Lab ID: CE11137-16
Sampled: 07/22/21 16:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:05
Client ID: A2S15
Lab ID: CE11137-17
Sampled: 07/23/21 14:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:08
Client ID: A2S16
Lab ID: CE11137-18
Sampled: 07/23/21 14:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:10
Client ID: A2S17
Lab ID: CE11137-19
Sampled: 07/23/21 14:15
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:12
Client ID: A2S18
Lab ID: CE11137-20
Sampled: 07/23/21 14:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:15
Client ID: A2S19
Lab ID: CE11137-21
Sampled: 07/23/21 14:35
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(sl
08/02/21 14:17
Client ID: A2S20
Lab ID: CE11137-22
Sampled: 07/23/21 14:40
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:19
Client ID: A2S21
Lab ID: CE11137-23
Sampled: 07/23/21 14:45
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:21
Client ID: A2S22
Lab ID: CE11137-24
Sampled: 07/23/21 14:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:23
Client ID: A2S23
Lab ID: CE11137-25
Sampled: 07/23/21 14:55
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:31
Client ID: A2S24
Lab ID: CE11137-26
Sampled: 07/23/21 15:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:33
Client ID: A2S25
Lab ID: CE11137-27
Sampled: 07/23/21 15:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:36
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 16

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2S26
Lab ID: CE11137-28
Sampled: 07/23/21 15:10
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:27
08/02/21 14:38
Client ID: A2S27
Lab ID: CE11137-29
Sampled: 07/23/21 15:15
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:27
08/02/21 14:40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 16

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SAMPLE DETECTION SUMMARY
Client ID: SIDEPIA Lab ID: CE11137-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 26.5 0.130 0.542 mq/kq dry EPA 6010D
I Client ID: SIDEPIB Lab ID: CE11137-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.9
0.129
0.537
mg/kg dry
EPA 6010D
Client ID: SIDEP2A
Lab ID:
CE11137-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.6
0.125
0.522
mq/kq dry
EPA 6010D
I Client ID: SIDEP28 Lab ID: CE11137-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.3
0.126
0.527
mg/kg dry
EPA 6010D
Client ID: SIDEP3A
Lab ID:
CE11137-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.1
0.129
0.536
mq/kq dry
EPA 6010D
I Client ID: SIDEP38 Lab ID: CE11137-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
28.9
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: SIDEP4A
Lab ID:
CE11137-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
0.200
0.00132
0.00548
mq/kq dry
EPA 6010D
I Client ID: SIDEP48 Lab ID: CE11137-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
32.5
0.128
0.533
mg/kg dry
EPA 6010D
Client ID: SIDEPSA
Lab ID:
CE11137-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.9
0.128
0.532
mq/kq dry
EPA 6010D
I Client ID: SIDEP58 Lab ID: CE11137-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
24.7
0.128
0.534
mg/kg dry
EPA 6010D
Client ID: HA46P1A
Lab ID:
CE11137-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
231
0.135
0.561
mq/kq dry
EPA 6010D
I Client ID: HA461338 Lab ID: CE11137-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
258
0.135
0.563
mg/kg dry
EPA 6010D
Client ID: A2S31
Lab ID:
CE11137-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
3.28
0.130
0.540
mq/kq dry
EPA 6010D
I Client ID: A2S12 Lab ID: CE11137-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.85
0.130
0.542
mg/kg dry
EPA 6010D
Client ID: A2S13
Lab ID:
CE11137-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.52
0.128
0.533
mq/kq dry
EPA 6010D
I Client ID: A2S14 Lab ID: CE11137-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.75
0.129
0.538
mg/kg dry
EPA 6010D
Client ID: A2S15
Lab ID:
CE11137-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.35
0.145
0.602
mq/kq dry
EPA 6010D
Client ID: A2S16 Lab ID: CE11137-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 19.3 0.154 0.643 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 16

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SAMPLE DETECTION SUMMARY
Client ID:
A2S37
Lab ID:
CE11137-19
Analvte
Lead - Total
Results
38.5
Flag
MDL
0.146
PQL
0.610
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S18
Lab ID:
CE11137-20
Analvte
Lead - Total
Results
507
Flag
MDL
0.144
PQL
0.601
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S39
Lab ID:
CE11137-21
Analvte
Lead - Total
Results
82.5
Flag
MDL
0.145
PQL
0.603
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S20
Lab ID:
CE11137-22
Analvte
Lead - Total
Results
39.2
Flag
MDL
0.135
PQL
0.564
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S21
Lab ID:
CE11137-23
Analvte
Lead - Total
Results
7.97
Flag
MDL
0.134
PQL
0.558
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S22
Lab ID:
CE11137-24
Analvte
Lead - Total
Results
5.36
Flag
MDL
0.136
PQL
0.565
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S23
Lab ID:
CE11137-25
Analvte
Lead - Total
Results
10.4
Flag
MDL
0.127
PQL
0.529
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S24
Lab ID:
CE11137-26
Analvte
Lead - Total
Results
5.46
Flag
MDL
0.132
PQL
0.549
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S25
Lab ID:
CE11137-27
Analvte
Lead - Total
Results
34.7
Flag
MDL
0.127
PQL
0.530
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S26
Lab ID:
CE11137-28
Analvte
Lead - Total
Results
20.7
Flag
MDL
0.140
PQL
0.584
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S27
Lab ID:
CE11137-29
Analvte
Lead - Total
Results
14.1
Flag
MDL
0.154
PQL
0.642
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 16

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ANALYTICAL RESULTS
Description: SIDEPIA Lab Sample ID:CE11137-01 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 26.5
mg/kg dry
1
0.130
0.542
1G27024
EPA 6010D
07/29/21 13:39
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:35
JDH
Description: SIDEPIB Lab Sample ID:CE11137-02 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.19
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 23.9
mg/kg dry
1
0.129
0.537
1G27024
EPA 6010D
07/29/21 13:41
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:38
JDH
Description: SIDEP2A Lab Sample ID:CE11137-03 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 12.6
mg/kg dry
1
0.125
0.522
1G27024
EPA 6010D
07/29/21 13:53
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:41
JDH
Description: SIDEP2B Lab Sample ID:CE11137-04 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.96
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 15.3
mg/kg dry
1
0.126
0.527
1G27024
EPA 6010D
07/29/21 13:55
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:43
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 16

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ANALYTICAL RESULTS
Description: SIDEP3A Lab Sample ID:CE11137-05 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:30 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 23.1 mg/kg dry 1 0.129 0.536 1G27024 EPA 6010D 07/29/21 13:57 JDH
Description: SIDEP3B Lab Sample ID:CE11137-06 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:40 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.44
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 28.9 mg/kg dry 1 0.130 0.541 1G27024 EPA 6010D 07/29/21 13:59 JDH
Description: SIDEP4A Lab Sample ID:CE11137-07 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 0.200 mg/kg dry 0.0104 0.00132 0.00548 1G27024 EPA 6010D 07/29/21 14:01 JDH
Description: SIDEP4B Lab Sample ID:CE11137-08 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.89
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 32.5 mg/kg dry 1 0.128 0.533 1G27024 EPA 6010D 07/29/21 14:03 JDH
Description: SIDEP5A Lab Sample ID:CE11137-09 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.96
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 17.9 mg/kg dry 1 0.128 0.532 1G27024 EPA 6010D 07/29/21 14:05 JDH
Description: SIDEP5B Lab Sample ID: CE11137-10 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 24.7 mg/kg dry 1 0.128 0.534 1G27024 EPA 6010D 07/29/21 14:07 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 16

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ANALYTICAL RESULTS
Description: HA46P1A Lab Sample ID:CE11137-11 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 12:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.19
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 231 mg/kg dry 1 0.135 0.561 1G27025 EPA 6010D 08/02/21 13:27 JDH
Description: HA46P1B Lab Sample ID:CE11137-12 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 13:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.82
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 258 mg/kg dry 1 0.135 0.563 1G27025 EPA 6010D 08/02/21 13:38 JDH
Description: A2S11 Lab Sample ID:CE11137-13 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 15:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 3.28 mg/kg dry 1 0.130 0.540 1G27025 EPA 6010D 08/02/21 13:40 JDH
Description: A2S12 Lab Sample ID:CE11137-14 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 15:55 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.26
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.85 mg/kg dry 1 0.130 0.542 1G27025 EPA 6010D 08/02/21 13:42 JDH
Description: A2S13 Lab Sample ID:CE11137-15 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 16:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.79
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 5.52 mg/kg dry 1 0.128 0.533 1G27025 EPA 6010D 08/02/21 14:03 JDH
Description: A2S14 Lab Sample ID: CE11137-16 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 16:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.94
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.75 mg/kg dry 1 0.129 0.538 1G27025 EPA 6010D 08/02/21 14:05 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 16

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ANALYTICAL RESULTS
Description: A2S15 Lab Sample ID:CE11137-17 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.02
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 9.35 mg/kg dry 1 0.145 0.602 1G27025 EPA 6010D 08/02/21 14:08 JDH
Description: A2S16 Lab Sample ID:CE11137-18 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.73
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.3 mg/kg dry 1 0.154 0.643 1G27025 EPA 6010D 08/02/21 14:10 JDH
Description: A2S17 Lab Sample ID:CE11137-19 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:15 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.95
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 38.5 mg/kg dry 1 0.146 0.610 1G27025 EPA 6010D 08/02/21 14:12 JDH
Description: A2S18 Lab Sample ID:CE11137-20 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.20
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 507 mg/kg dry 1 0.144 0.601 1G27025 EPA 6010D 08/02/21 14:15 JDH
Description: A2S19 Lab Sample ID:CE11137-21 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:35 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.93
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 82.5 mg/kg dry 1 0.145 0.603 1G27025 EPA 6010D 08/02/21 14:17 JDH
Description: A2S20 Lab Sample ID:CE11137-22 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:40 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.60
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 39.2 mg/kg dry 1 0.135 0.564 1G27025 EPA 6010D 08/02/21 14:19 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 16

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ANALYTICAL RESULTS
Description: A2S21 Lab Sample ID:CE11137-23 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:45 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 7.97 mg/kg dry 1 0.134 0.558 1G27025 EPA 6010D 08/02/21 14:21 JDH
Description: A2S22 Lab Sample ID:CE11137-24 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.36 mg/kg dry 1 0.136 0.565 1G27025 EPA 6010D 08/02/21 14:23 JDH
Description: A2S23 Lab Sample ID:CE11137-25 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:55 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 10.4 mg/kg dry 1 0.127 0.529 1G27025 EPA 6010D 08/02/21 14:31 JDH
Description: A2S24 Lab Sample ID:CE11137-26 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.06
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.46 mg/kg dry 1 0.132 0.549 1G27025 EPA 6010D 08/02/21 14:33 JDH
Description: A2S25 Lab Sample ID:CE11137-27 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 34.7 mg/kg dry 1 0.127 0.530 1G27025 EPA 6010D 08/02/21 14:36 JDH
Description: A2S26 Lab Sample ID: CE11137-28 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.55
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 20.7 mg/kg dry 1 0.140 0.584 1G27025 EPA 6010D 08/02/21 14:38 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 16

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ANALYTICAL RESULTS
Description: A2S27 Lab Sample ID:CE11137-29 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/23/21 15:15 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.91
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 14.1 mg/kg dry 1 0.154 0.642 1G27025 EPA 6010D 08/02/21 14:40 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 16

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627024 - EPA 3050E
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27024-BS1) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (1G27024-PS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
Batch IG27025 - EPA 3050E
Blank (1G27025-BLK3) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:22
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27025-BS1) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.3
0.500
mg/kg wet
10.4 99 80-120
Matrix Spike (1G27025-MS1)
Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:30
Source: CE11137-11
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
217
0.561
mg/kg dry
11.3 231 NR 75-125
QM-07
Matrix Spike Dup (1G27025-MSD3)
Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:32
Source: CE11137-11
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
198
0.561
mg/kg dry
11.3 231 NR 75-125 9
20
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 16

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627025 - EPA 3050E - Continued
Post Spike (IG27025-PSI) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:34
Source: CE11137-11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 4.08 0.0100 mg/L 0.200 3.95 65 80-120 QM-08
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1H04038 - EPA 3010A
Blank (lH04038-BLKI) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
Blank (1H04038-BLK2) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (1H04038-BSI) Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:21
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.209
0.0100
mg/L
0.200 105 80-120
Matrix Spike (1H04038-MS1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:24
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
11.3
0.500
mg/L
10.0 0.155 U 113 75-125
Matrix Spike Dup (1H04038-MSD1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:26
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
11.2
0.500
mg/L
10.0 0.155 U 112 75-125 1
20
Post Spike (lH04038-PSI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:28
Source: CE11013-16
Analvte
Lead
Spike Source %REC
Result Flaq POL Units Level Result %REC Limits RPD
0.212 0.0100 mg/L 0.200 0.00262 105 80-120
RPD
Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 16

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 16

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 5, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11167
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, July 26, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 18

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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A1S3
Lab ID: CE11167-01
Sampled: 07/26/21 09:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 11:51
Client ID: A1S2
Lab ID: CE11167-02
Sampled: 07/26/21 09:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:39
Client ID: A1S3
Lab ID: CE11167-03
Sampled: 07/26/21 09:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:42
Client ID: A1S4
Lab ID: CE11167-04
Sampled: 07/26/21 09:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:44
Client ID: A1S5
Lab ID: CE11167-05
Sampled: 07/26/21 09:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:47
Client ID: A1S6
Lab ID: CE11167-06
Sampled: 07/26/21 09:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:49
Client ID: A1S7
Lab ID: CE11167-07
Sampled: 07/26/21 09:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:51
Client ID: A1S8
Lab ID: CE11167-08
Sampled: 07/26/21 09:40
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:53
Client ID: A1S9
Lab ID: CE11167-09
Sampled: 07/26/21 09:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:55
Client ID: A1S10
Lab ID: CE11167-10
Sampled: 07/26/21 09:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:09
Client ID: A1S11
Lab ID: CE11167-11
Sampled: 07/26/21 10:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:12
Client ID: A1S12
Lab ID: CE11167-12
Sampled: 07/26/21 10:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:14
Client ID: A1S13
Lab ID: CE11167-13
Sampled: 07/26/21 10:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:16
Client ID: A1S14
Lab ID: CE11167-14
Sampled: 07/26/21 10:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:18
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 18

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A1S35
Lab ID: CE11167-15
Sampled: 07/26/21 10:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:20
Client ID: A1S16
Lab ID: CE11167-16
Sampled: 07/26/21 10:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:22
Client ID: 30051
Lab ID: CE11167-17
Sampled: 07/26/21 11:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:24
Client ID: 10052
Lab ID: CE11167-18
Sampled: 07/26/21 11:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:26
Client ID: 30053
Lab ID: CE11167-19
Sampled: 07/26/21 11:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:28
Client ID: 30054
Lab ID: CE11167-20
Sampled: 07/26/21 11:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:36
Client ID: 10055
Lab ID: CE11167-21
Sampled: 07/26/21 11:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 13:44
Client ID: 10056
Lab ID: CE11167-22
Sampled: 07/26/21 11:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(sl
08/05/21 13:54
Client ID: 10057
Lab ID: CE11167-23
Sampled: 07/26/21 11:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 13:57
Client ID: 10058
Lab ID: CE11167-24
Sampled: 07/26/21 11:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:11
Client ID: A4S1
Lab ID: CE11167-25
Sampled: 07/26/21 12:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:13
Client ID: A4S2
Lab ID: CE11167-26
Sampled: 07/26/21 12:40
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:15
Client ID: A4S3
Lab ID: CE11167-27
Sampled: 07/26/21 12:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:18
Client ID: A4S4
Lab ID: CE11167-28
Sampled: 07/26/21 12:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 18

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A4S5
Lab ID: CE11167-29
Sampled: 07/26/21 12:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:22
Client ID: A4S6
Lab ID: CE11167-30
Sampled: 07/26/21 13:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:24
Client ID: A4S7
Lab ID: CE11167-31
Sampled: 07/26/21 13:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:26
Client ID: A4S8
Lab ID: CE11167-32
Sampled: 07/26/21 13:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:28
Client ID: A4S9
Lab ID: CE11167-33
Sampled: 07/26/21 13:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:30
Client ID: A4S10
Lab ID: CE11167-34
Sampled: 07/26/21 13:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:40
Client ID: A4S11
Lab ID: CE11167-35
Sampled: 07/26/21 13:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:42
Client ID: A4S12
Lab ID: CE11167-36
Sampled: 07/26/21 13:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(sl
08/05/21 14:44
Client ID: A4S13
Lab ID: CE11167-37
Sampled: 07/26/21 13:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:46
Client ID: A4S14
Lab ID: CE11167-38
Sampled: 07/26/21 13:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:48
Client ID: A4S15
Lab ID: CE11167-39
Sampled: 07/26/21 14:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:50
Client ID: A4S16
Lab ID: CE11167-40
Sampled: 07/26/21 14:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:52
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 18

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SAMPLE DETECTION SUMMARY
Client ID: A1S3 Lab ID: CE11167-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 5.96 0.137 0.571 mq/kq dry EPA 6010D
I Client ID: A1S2 Lab ID: CE11167-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.7
0.144
0.599
mg/kg dry
EPA 6010D
Client ID: A1S3
Lab ID:
CE11167-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.91
0.139
0.579
mq/kq dry
EPA 6010D
I Client ID: A1S4 Lab ID: CE11167-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.67
0.141
0.587
mg/kg dry
EPA 6010D
Client ID: A1S5
Lab ID:
CE11167-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.20
0.132
0.548
mq/kq dry
EPA 6010D
I Client ID: A1S6 Lab ID: CE11167-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
33.0
0.146
0.609
mg/kg dry
EPA 6010D
Client ID: A1S7
Lab ID:
CE11167-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.5
0.134
0.559
mq/kq dry
EPA 6010D
I Client ID: A1S8 Lab ID: CE11167-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.18
0.146
0.610
mg/kg dry
EPA 6010D
Client ID: A1S9
Lab ID:
CE11167-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.46
0.132
0.551
mq/kq dry
EPA 6010D
I Client ID: A1S10 Lab ID: CE11167-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.38
0.138
0.573
mg/kg dry
EPA 6010D
Client ID: A1S11
Lab ID:
CE11167-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.61
0.132
0.549
mq/kq dry
EPA 6010D
I Client ID: A1S12 Lab ID: CE11167-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
2.46
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: A1S13
Lab ID:
CE11167-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
2.85
0.127
0.529
mq/kq dry
EPA 6010D
I Client ID: A1S14 Lab ID: CE11167-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.65
0.132
0.549
mg/kg dry
EPA 6010D
Client ID: A1S15
Lab ID:
CE11167-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.51
0.129
0.536
mq/kq dry
EPA 6010D
I Client ID: A1S16 Lab ID: CE11167-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
37.8
0.137
0.573
mg/kg dry
EPA 6010D
Client ID: 30051
Lab ID:
CE11167-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
706
0.131
0.544
mq/kq dry
EPA 6010D
Client ID: 30052 Lab ID: CE11167-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 19.1 0.142 0.593 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 18

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SAMPLE DETECTION SUMMARY
Client ID: 30053 Lab ID: CE11167-19
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 54.8 0.153 0.635 mq/kq dry EPA 6010D
I Client ID: 30054 Lab ID: CE11167-20
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.3
0.142
0.591
mg/kg dry
EPA 6010D
Client ID: 100SS
Lab ID:
CE11167-21
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
18.6
0.152
0.632
mq/kq dry
EPA 6010D
I Client ID: 10056 Lab ID: CE11167-22
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.2
0.129
0.539
mg/kg dry
EPA 6010D
Client ID: 30057
Lab ID:
CE11167-23
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.25
0.166
0.692
mq/kq dry
EPA 6010D
I Client ID: 100SS Lab ID: CE11167-24
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.05
0.165
0.687
mg/kg dry
EPA 6010D
Client ID: A4S1
Lab ID:
CE11167-25
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
25.7
0.143
0.594
mq/kq dry
EPA 6010D
I Client ID: A4S2 Lab ID: CE11167-26
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.7
0.175
0.731
mg/kg dry
EPA 6010D
Client ID: A4S3
Lab ID:
CE11167-27
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
35.5
0.171
0.713
mq/kq dry
EPA 6010D
I Client ID: A4S4 Lab ID: CE11167-28
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
22.1
0.167
0.697
mg/kg dry
EPA 6010D
Client ID: A4S5
Lab ID:
CE11167-29
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
31.9
0.137
0.570
mq/kq dry
EPA 6010D
I Client ID: A4S6 Lab ID: CE11167-30
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
21.4
0.154
0.643
mg/kg dry
EPA 6010D
Client ID: A4S7
Lab ID:
CE11167-31
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.3
0.135
0.562
mq/kq dry
EPA 6010D
I Client ID: A4S8 Lab ID: CE11167-32
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.99
0.133
0.553
mg/kg dry
EPA 6010D
Client ID: A4S9
Lab ID:
CE11167-33
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.42
0.157
0.654
mq/kq dry
EPA 6010D
I Client ID: A4S10 Lab ID: CE11167-34
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.82
0.130
0.543
mg/kg dry
EPA 6010D
Client ID: A4S11
Lab ID:
CE11167-35
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.8
0.148
0.617
mq/kq dry
EPA 6010D
Client ID: A4S12 Lab ID: CE11167-36
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 21.9 0.120 0.498 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 18

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SAMPLE DETECTION SUMMARY
Client ID: A4S33 Lab ID: CE11167-37
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 108 0.121 0.502 mq/kq dry EPA 6010D
I Client ID: A4S34 Lab ID: CE11167-38
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.0
0.148
0.616
mg/kg dry
EPA 6010D
Client ID: A4S15
Lab ID:
CE11167-39
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
28.2
0.133
0.554
mq/kq dry
EPA 6010D
Client ID: A4S16 Lab ID: CE11167-40
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 73.6 0.129 0.536 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 18

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ANALYTICAL RESULTS
Description: A1S1 Lab Sample ID: CE11167-01 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.59
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 5.96 mg/kg dry 1 0.137 0.571 1H04013 EPA 6010D 08/05/21 11:51 JDH
Description: A1S2 Lab Sample ID:CE11167-02 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.42
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.7 mg/kg dry 1 0.144 0.599 1H04013 EPA 6010D 08/05/21 12:39 JDH
Description: A1S3 Lab Sample ID:CE11167-03 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.40
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.91 mg/kg dry 1 0.139 0.579 1H04013 EPA 6010D 08/05/21 12:42 JDH
Description: A1S4 Lab Sample ID:CE11167-04 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.24
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.67 mg/kg dry 1 0.141 0.587 1H04013 EPA 6010D 08/05/21 12:44 JDH
Description: A1S5 Lab Sample ID:CE11167-05 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.18
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 7.20 mg/kg dry 1 0.132 0.548 1H04013 EPA 6010D 08/05/21 12:47 JDH
Description: A1S6 Lab Sample ID: CE11167-06 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.07
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 33.0 mg/kg dry 1 0.146 0.609 1H04013 EPA 6010D 08/05/21 12:49 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 18

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ANALYTICAL RESULTS
Description: A1S7 Lab Sample ID: CE11167-07 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.46
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 11.5 mg/kg dry 1 0.134 0.559 1H04013 EPA 6010D 08/05/21 12:51 JDH
Description: A1S8 Lab Sample ID:CE11167-08 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:40 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.03
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.18 mg/kg dry 1 0.146 0.610 1H04013 EPA 6010D 08/05/21 12:53 JDH
Description: A1S9 Lab Sample ID:CE11167-09 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.78
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 6.46 mg/kg dry 1 0.132 0.551 1H04013 EPA 6010D 08/05/21 12:55 JDH
Description: A1S10 Lab Sample ID:CE11167-10 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.22
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.38 mg/kg dry 1 0.138 0.573 1H04013 EPA 6010D 08/05/21 13:09 JDH
Description: A1S11 Lab Sample ID:CE11167-11 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.11
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 9.61 mg/kg dry 1 0.132 0.549 1H04013 EPA 6010D 08/05/21 13:12 JDH
Description: AIS12 Lab Sample ID: CE11167-12 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.47
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 2.46 mg/kg dry 1 0.130 0.541 1H04013 EPA 6010D 08/05/21 13:14 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 18

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ANALYTICAL RESULTS
Description: A1S13 Lab Sample ID: CE11167-13 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 2.85 mg/kg dry 1 0.127 0.529 1H04013 EPA 6010D 08/05/21 13:16 JDH
Description: A1S14 Lab Sample ID:CE11167-14 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.06
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.65 mg/kg dry 1 0.132 0.549 1H04013 EPA 6010D 08/05/21 13:18 JDH
Description: A1S15 Lab Sample ID:CE11167-15 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.24
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 4.51 mg/kg dry 1 0.129 0.536 1H04013 EPA 6010D 08/05/21 13:20 JDH
Description: A1S16 Lab Sample ID:CE11167-16 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.32
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 37.8 mg/kg dry 1 0.137 0.573 1H04013 EPA 6010D 08/05/21 13:22 JDH
Description: 100S1 Lab Sample ID:CE11167-17 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 706 mg/kg dry 1 0.131 0.544 1H04013 EPA 6010D 08/05/21 13:24 JDH
Description: 100S2 Lab Sample ID: CE11167-18 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.1 mg/kg dry 1 0.142 0.593 1H04013 EPA 6010D 08/05/21 13:26 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 18

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ANALYTICAL RESULTS
Description: 100S3 Lab Sample ID: CE11167-19 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 54.8 mg/kg dry 1 0.153 0.635 1H04013 EPA 6010D 08/05/21 13:28 JDH
Description: 100S4 Lab Sample ID:CE11167-20 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.65
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.3 mg/kg dry 1 0.142 0.591 1H04013 EPA 6010D 08/05/21 13:36 JDH
Description: 100S5 Lab Sample ID:CE11167-21 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.86
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 18.6 mg/kg dry 1.11 0.152 0.632 1H04014 EPA 6010D 08/05/21 13:44 JDH
Description: 100S6 Lab Sample ID:CE11167-22 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.75
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.2 mg/kg dry 1 0.129 0.539 1H04014 EPA 6010D 08/05/21 13:54 JDH
Description: 100S7 Lab Sample ID:CE11167-23 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.31
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 5.25 mg/kg dry 1.11 0.166 0.692 1H04014 EPA 6010D 08/05/21 13:57 JDH
Description: 100S8 Lab Sample ID:CE11167-24 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.05 mg/kg dry 1.11 0.165 0.687 1H04014 EPA 6010D 08/05/21 14:11 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 18

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ANALYTICAL RESULTS
Description: A4S1 Lab Sample ID: CE11167-25 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.12
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 25.7 mg/kg dry 1 0.143 0.594 1H04014 EPA 6010D 08/05/21 14:13 JDH
Description: A4S2 Lab Sample ID:CE11167-26 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:40 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.7 mg/kg dry 1.11 0.175 0.731 1H04014 EPA 6010D 08/05/21 14:15 JDH
Description: A4S3 Lab Sample ID:CE11167-27 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.90
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 35.5 mg/kg dry 1.11 0.171 0.713 1H04014 EPA 6010D 08/05/21 14:18 JDH
Description: A4S4 Lab Sample ID:CE11167-28 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.65
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.1 mg/kg dry 1.11 0.167 0.697 1H04014 EPA 6010D 08/05/21 14:20 JDH
Description: A4S5 Lab Sample ID:CE11167-29 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 31.9 mg/kg dry 1 0.137 0.570 1H04014 EPA 6010D 08/05/21 14:22 JDH
Description: A4S6 Lab Sample ID: CE11167-30 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.39
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.4 mg/kg dry 1.11 0.154 0.643 1H04014 EPA 6010D 08/05/21 14:24 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 18

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ANALYTICAL RESULTS
Description: A4S7 Lab Sample ID: CE11167-31 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.94
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 17.3 mg/kg dry 1 0.135 0.562 1H04014 EPA 6010D 08/05/21 14:26 JDH
Description: A4S8 Lab Sample ID:CE11167-32 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.99 mg/kg dry 1 0.133 0.553 1H04014 EPA 6010D 08/05/21 14:28 JDH
Description: A4S9 Lab Sample ID:CE11167-33 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.42 mg/kg dry 1.11 0.157 0.654 1H04014 EPA 6010D 08/05/21 14:30 JDH
Description: A4S10 Lab Sample ID:CE11167-34 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.00
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 9.82 mg/kg dry 1 0.130 0.543 1H04014 EPA 6010D 08/05/21 14:40 JDH
Description: A4S11 Lab Sample ID:CE11167-35 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 23.8 mg/kg dry 1.11 0.148 0.617 1H04014 EPA 6010D 08/05/21 14:42 JDH
Description: A4S12 Lab Sample ID:CE11167-36 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.9 mg/kg dry 1 0.120 0.498 1H04014 EPA 6010D 08/05/21 14:44 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 18

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ANALYTICAL RESULTS
Description: A4S13 Lab Sample ID: CE11167-37 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.53
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 108 mg/kg dry 1 0.121 0.502 1H04014 EPA 6010D 08/05/21 14:46 JDH
Description: A4S14 Lab Sample ID:CE11167-38 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.0 mg/kg dry 1.11 0.148 0.616 1H04014 EPA 6010D 08/05/21 14:48 JDH
Description: A4S15 Lab Sample ID:CE11167-39 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.23
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 28.2 mg/kg dry 1 0.133 0.554 1H04014 EPA 6010D 08/05/21 14:50 JDH
Description: A4S16 Lab Sample ID:CE11167-40 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.22
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 73.6 mg/kg dry 1 0.129 0.536 1H04014 EPA 6010D 08/05/21 14:52 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 18

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1HO4013 - EPA 3050E
Blank (lH04013-BLKI) Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (lH04013-BS1) Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.2
0.500
mg/kg wet
9.62 106 80-120
Matrix Spike (1H04013-MS1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:53
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.5
0.571
mg/kg dry
11.9 5.96 114 75-125
Matrix Spike Dup (1H04013-MSD1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:55
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.0
0.571
mg/kg dry
11.9 5.96 93 75-125 14
20
Post Spike (11-104013-PS1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 12:35
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.315
0.0100
mg/L
0.200 0.0981 108 80-120
Batch 1HO4014 - EPA 30505
Blank (11-104014-BLKi) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:38
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.133 U 0.556 mg/kg wet
LCS (11-104014-BSI) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:41
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.79
0.455
mg/kg wet
9.09 108 80-120
Matrix Spike (lH04014-MS1)
Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:46
Source: CE11167-21
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
36.8
0.569
mg/kg dry
11.4 18.6 160 75-125
QM-07
Matrix Spike Dup (1H04014-MSD1)
Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:48
Source: CE11167-21
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
80.1
0.569
mg/kg dry
11.4 18.6 540 75-125 74
20
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 18

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1H04014 - EPA 3050B - Continued
Post Spike (SH04014-PS3) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:50
Source: CE11167-21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.501 0.0100 mg/L 0.200 0.294 103 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 18

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 18

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, August 6, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11137
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, July 23, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 17

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SIDEPIA
Lab ID: CE11137-01
Sampled: 07/23/21 09:00
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:39
EPA 6010D
EPA 3010A
O1/19/22 01/31/22
08/04/21 16:52
08/05/21 11:35
Client ID: SIDEPSB
Lab ID: CE11137-02
Sampled: 07/23/21 09:05
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:41
EPA 6010D
EPA 3010A
O1/19/22 01/31/22
08/04/21 16:52
08/05/21 11:38
Client ID: SIDE132A
Lab ID: CE11137-03
Sampled: 07/23/21 09:10
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:53
EPA 6010D
EPA 3010A
O1/19/22 01/31/22
08/04/21 16:52
08/05/21 11:41
Client ID: SIDEPSB
Lab ID: CE11137-04
Sampled: 07/23/21 09:20
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:55
EPA 6010D
EPA 3010A
O1/19/22 01/31/22
08/04/21 16:52
08/05/21 11:43
Client ID: SIDE133A
Lab ID: CE11137-05
Sampled: 07/23/21 09:30
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:57
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:14
Client ID: SIDEP313
Lab ID: CE11137-06
Sampled: 07/23/21 09:40
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 13:59
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:29
Client ID: SIDEMA
Lab ID: CE11137-07
Sampled: 07/23/21 09:50
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 14:01
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:32
Client ID: SIDEPSB
Lab ID: CE11137-08
Sampled: 07/23/21 10:00
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 14:03
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:35
Client ID: SIDEPSA
Lab ID: CE11137-09
Sampled: 07/23/21 10:10
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 14:05
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:46
Client ID: SIDEPSB
Lab ID: CE11137-10
Sampled: 07/23/21 10:20
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:24
07/29/21 14:07
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:50
Client ID: HA46P1A
Lab ID: CE11137-11
Sampled: 07/23/21 12:50
Received: 07/23/21 16:06
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/19/22
07/27/21 11:27
08/02/21 13:27
EPA 6010D
EPA 3010A
O1/19/22 02/01/22
08/05/21 12:44
08/06/21 10:53
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 17

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: HA46P313
Lab ID: CE11137-12
Sampled: 07/23/21 13:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
EPA 6010D
Preparation
EPA 3050B
EPA 3010A
Hold Date/Time(s)
O1/19/22
O1/19/22 02/01/22
Prep Date/Time(s)
07/27/21 11:27
08/05/21 12:44
Analysis Date/Time(s)
08/02/21 13:38
08/06/21 10:56
Client ID: A2S11
Lab ID: CE11137-13
Sampled: 07/22/21 15:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:40
Client ID: A2S12
Lab ID: CE11137-14
Sampled: 07/22/21 15:55
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 13:42
Client ID: A2S13
Lab ID: CE11137-15
Sampled: 07/22/21 16:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:03
Client ID: A2S14
Lab ID: CE11137-16
Sampled: 07/22/21 16:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/18/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:05
Client ID: A2S15
Lab ID: CE11137-17
Sampled: 07/23/21 14:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:08
Client ID: A2S16
Lab ID: CE11137-18
Sampled: 07/23/21 14:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:10
Client ID: A2S17
Lab ID: CE11137-19
Sampled: 07/23/21 14:15
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:12
Client ID: A2518
Lab ID: CE11137-20
Sampled: 07/23/21 14:20
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:15
Client ID: A2S19
Lab ID: CE11137-21
Sampled: 07/23/21 14:35
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:17
Client ID: A2S20
Lab ID: CE11137-22
Sampled: 07/23/21 14:40
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:19
Client ID: A2S21
Lab ID: CE11137-23
Sampled: 07/23/21 14:45
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:21
Client ID: A2S22
Lab ID: CE11137-24
Sampled: 07/23/21 14:50
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:23
Client ID: A2S23
Lab ID: CE11137-25
Sampled: 07/23/21 14:55
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time
08/02/21 14:31
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 17

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2S24
Lab ID: CE11137-26
Sampled: 07/23/21 15:00
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:33
Client ID: A2S25
Lab ID: CE11137-27
Sampled: 07/23/21 15:05
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:36
Client ID: A2S26
Lab ID: CE11137-28
Sampled: 07/23/21 15:10
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:38
Client ID: A2S27
Lab ID: CE11137-29
Sampled: 07/23/21 15:15
Received: 07/23/21 16:06
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/19/22
Prep Date/Time(s)
07/27/21 11:27
Analysis Date/Time(s)
08/02/21 14:40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 17

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SAMPLE DETECTION SUMMARY
Client ID: SIDEPIA Lab ID: CE11137-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 26.5 0.130 0.542 mq/kq dry EPA 6010D
I Client ID: SIDEPIB Lab ID: CE11137-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.9
0.129
0.537
mg/kg dry
EPA 6010D
Client ID: SIDEP2A
Lab ID:
CE11137-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.6
0.125
0.522
mq/kq dry
EPA 6010D
I Client ID: SIDEP28 Lab ID: CE11137-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.3
0.126
0.527
mg/kg dry
EPA 6010D
Client ID: SIDEP3A
Lab ID:
CE11137-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.1
0.129
0.536
mq/kq dry
EPA 6010D
I Client ID: SIDEP38 Lab ID: CE11137-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
28.9
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: SIDEP4A
Lab ID:
CE11137-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
0.200
0.00132
0.00548
mq/kq dry
EPA 6010D
I Client ID: SIDEP48 Lab ID: CE11137-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
32.5
0.128
0.533
mg/kg dry
EPA 6010D
Client ID: SIDEPSA
Lab ID:
CE11137-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.9
0.128
0.532
mq/kq dry
EPA 6010D
I Client ID: SIDEP58 Lab ID: CE11137-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
24.7
0.128
0.534
mg/kg dry
EPA 6010D
Client ID: HA46P1A
Lab ID:
CE11137-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
231
0.135
0.561
mq/kq dry
EPA 6010D
I Client ID: HA461338 Lab ID: CE11137-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
258
0.135
0.563
mg/kg dry
EPA 6010D
Client ID: A2S31
Lab ID:
CE11137-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
3.28
0.130
0.540
mq/kq dry
EPA 6010D
I Client ID: A2S12 Lab ID: CE11137-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.85
0.130
0.542
mg/kg dry
EPA 6010D
Client ID: A2S13
Lab ID:
CE11137-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.52
0.128
0.533
mq/kq dry
EPA 6010D
I Client ID: A2S14 Lab ID: CE11137-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.75
0.129
0.538
mg/kg dry
EPA 6010D
Client ID: A2S15
Lab ID:
CE11137-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.35
0.145
0.602
mq/kq dry
EPA 6010D
Client ID: A2S16 Lab ID: CE11137-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 19.3 0.154 0.643 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 17

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SAMPLE DETECTION SUMMARY
Client ID:
A2S37
Lab ID:
CE11137-19
Analvte
Lead - Total
Results
38.5
Flag
MDL
0.146
PQL
0.610
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S18
Lab ID:
CE11137-20
Analvte
Lead - Total
Results
507
Flag
MDL
0.144
PQL
0.601
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S39
Lab ID:
CE11137-21
Analvte
Lead - Total
Results
82.5
Flag
MDL
0.145
PQL
0.603
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S20
Lab ID:
CE11137-22
Analvte
Lead - Total
Results
39.2
Flag
MDL
0.135
PQL
0.564
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S21
Lab ID:
CE11137-23
Analvte
Lead - Total
Results
7.97
Flag
MDL
0.134
PQL
0.558
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S22
Lab ID:
CE11137-24
Analvte
Lead - Total
Results
5.36
Flag
MDL
0.136
PQL
0.565
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S23
Lab ID:
CE11137-25
Analvte
Lead - Total
Results
10.4
Flag
MDL
0.127
PQL
0.529
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S24
Lab ID:
CE11137-26
Analvte
Lead - Total
Results
5.46
Flag
MDL
0.132
PQL
0.549
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S25
Lab ID:
CE11137-27
Analvte
Lead - Total
Results
34.7
Flag
MDL
0.127
PQL
0.530
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S26
Lab ID:
CE11137-28
Analvte
Lead - Total
Results
20.7
Flag
MDL
0.140
PQL
0.584
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S27
Lab ID:
CE11137-29
Analvte
Lead - Total
Results
14.1
Flag
MDL
0.154
PQL
0.642
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 17

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ANALYTICAL RESULTS
Description: SIDEPIA Lab Sample ID:CE11137-01 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 26.5
mg/kg dry
1
0.130
0.542
1G27024
EPA 6010D
07/29/21 13:39
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:35
JDH
Description: SIDEPIB Lab Sample ID:CE11137-02 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.19
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 23.9
mg/kg dry
1
0.129
0.537
1G27024
EPA 6010D
07/29/21 13:41
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:38
JDH
Description: SIDEP2A Lab Sample ID:CE11137-03 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 12.6
mg/kg dry
1
0.125
0.522
1G27024
EPA 6010D
07/29/21 13:53
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:41
JDH
Description: SIDEP2B Lab Sample ID:CE11137-04 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.96
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 15.3
mg/kg dry
1
0.126
0.527
1G27024
EPA 6010D
07/29/21 13:55
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H04038
EPA 6010D
08/05/21 11:43
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 17

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ANALYTICAL RESULTS
Description: SIDEP3A Lab Sample ID:CE11137-05 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:30 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 23.1
mg/kg dry
1
0.129
0.536
1G27024
EPA 6010D
07/29/21 13:57
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H05022
EPA 6010D
08/06/21 10:14
JDH
Description: SIDEP3B Lab Sample ID:CE11137-06 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:40 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.44
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 28.9
mg/kg dry
1
0.130
0.541
1G27024
EPA 6010D
07/29/21 13:59
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1HO5022
EPA 6010D
08/06/21 10:29
JDH
Description: SIDEP4A Lab Sample ID:CE11137-07 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/2109:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF MDL P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 0.200
mg/kg dry
0.0104 0.00132 0.00548
1G27024
EPA 6010D
07/29/21 14:01
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50 0.155 0.500
1H05022
EPA 6010D
08/06/21 10:32
JDH
Description: SIDEP4B Lab Sample ID:CE11137-08 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 32.5
mg/kg dry
1
0.128
0.533
1G27024
EPA 6010D
07/29/21 14:03
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H05022
EPA 6010D
08/06/21 10:35
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 17

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ANALYTICAL RESULTS
Description: SIDEP5A Lab Sample ID:CE11137-09 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.96
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 17.9
mg/kg dry
1
0.128
0.532
1G27024
EPA 6010D
07/29/21 14:05
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H05022
EPA 6010D
08/06/21 10:46
JDH
Description: SIDEP5B Lab Sample ID:CE11137-10 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 10:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 24.7
mg/kg dry
1
0.128
0.534
1G27024
EPA 6010D
07/29/21 14:07
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1HO5022
EPA 6010D
08/06/21 10:50
JDH
Description: HA46P1A Lab Sample ID:CE11137-11 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 12:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.19
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
—By Notes
Lead [7439-92-1]^ 231
mg/kg dry
1
0.135
0.561
1G27025
EPA 6010D
08/02/21 13:27
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H05022
EPA 6010D
08/06/21 10:53
JDH
Description: HA46P1B Lab Sample ID:CE11137-12 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 13:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.82
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 258
mg/kg dry
1
0.135
0.563
1G27025
EPA 6010D
08/02/21 13:38
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H05022
EPA 6010D
08/06/21 10:56
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 17

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ANALYTICAL RESULTS
Description: A2S11 Lab Sample ID:CE11137-13 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 15:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 3.28 mg/kg dry 1 0.130 0.540 1G27025 EPA 6010D 08/02/21 13:40 JDH
Description: A2S12 Lab Sample ID:CE11137-14 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 15:55 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.26
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.85 mg/kg dry 1 0.130 0.542 1G27025 EPA 6010D 08/02/21 13:42 JDH
Description: A2S13 Lab Sample ID:CE11137-15 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 16:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.79
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 5.52 mg/kg dry 1 0.128 0.533 1G27025 EPA 6010D 08/02/21 14:03 JDH
Description: A2S14 Lab Sample ID:CE11137-16 Received: 07/23/21 16:06
Matrix: Soil Sampled:07/22/21 16:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.94
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.75 mg/kg dry 1 0.129 0.538 1G27025 EPA 6010D 08/02/21 14:05 JDH
Description: A2S15 Lab Sample ID:CE11137-17 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.02
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 9.35 mg/kg dry 1 0.145 0.602 1G27025 EPA 6010D 08/02/21 14:08 JDH
Description: A2S16 Lab Sample ID:CE11137-18 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.73
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.3 mg/kg dry 1 0.154 0.643 1G27025 EPA 6010D 08/02/21 14:10 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 17

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ANALYTICAL RESULTS
Description: A2S17 Lab Sample ID:CE11137-19 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:15 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.95
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 38.5 mg/kg dry 1 0.146 0.610 1G27025 EPA 6010D 08/02/21 14:12 JDH
Description: A2S18 Lab Sample ID:CE11137-20 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:20 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 507 mg/kg dry 1 0.144 0.601 1G27025 EPA 6010D 08/02/21 14:15 JDH
Description: A2S19 Lab Sample ID:CE11137-21 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:35 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.93
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 82.5 mg/kg dry 1 0.145 0.603 1G27025 EPA 6010D 08/02/21 14:17 JDH
Description: A2S20 Lab Sample ID:CE11137-22 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:40 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.60
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 39.2 mg/kg dry 1 0.135 0.564 1G27025 EPA 6010D 08/02/21 14:19 JDH
Description: A2S21 Lab Sample ID:CE11137-23 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:45 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 7.97 mg/kg dry 1 0.134 0.558 1G27025 EPA 6010D 08/02/21 14:21 JDH
Description: A2S22 Lab Sample ID: CE11137-24 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:50 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.36 mg/kg dry 1 0.136 0.565 1G27025 EPA 6010D 08/02/21 14:23 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 17

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ANALYTICAL RESULTS
Description: A2S23 Lab Sample ID:CE11137-25 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 14:55 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 10.4 mg/kg dry 1 0.127 0.529 1G27025 EPA 6010D 08/02/21 14:31 JDH
Description: A2S24 Lab Sample ID:CE11137-26 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:00 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.06
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.46 mg/kg dry 1 0.132 0.549 1G27025 EPA 6010D 08/02/21 14:33 JDH
Description: A2S25 Lab Sample ID:CE11137-27 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:05 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 34.7 mg/kg dry 1 0.127 0.530 1G27025 EPA 6010D 08/02/21 14:36 JDH
Description: A2S26 Lab Sample ID:CE11137-28 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:10 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.55
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 20.7 mg/kg dry 1 0.140 0.584 1G27025 EPA 6010D 08/02/21 14:38 JDH
Description: A2S27 Lab Sample ID:CE11137-29 Received: 07/23/21 16:06
Matrix: Soil Sampled: 07/23/21 15:15 Work Order: CE11137
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.91
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 14.1 mg/kg dry 1 0.154 0.642 1G27025 EPA 6010D 08/02/21 14:40 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 17

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627024 - EPA 3050E
Blank (1G27024-BLK3) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27024-BS1) Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.6
0.500
mg/kg wet
10.3 113 80-120
Matrix Spike (1G27024-MS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 12:59
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.9 6.23 109 75-125
Matrix Spike Dup (1G27024-MSD1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:01
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.1
0.552
mg/kg dry
11.6 6.23 111 75-125 0.3
20
Post Spike (1G27024-PS1)
Prepared: 07/27/2021 11:24 Analyzed: 07/29/2021 13:03
Source: CE11013-29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.106 112 80-120
Batch IG27025 - EPA 3050E
Blank (1G27025-BLK3) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:22
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1G27025-BS1) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.3
0.500
mg/kg wet
10.4 99 80-120
Matrix Spike (1G27025-MS1)
Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:30
Source: CE11137-11
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
217
0.561
mg/kg dry
11.3 231 NR 75-125
QM-07
Matrix Spike Dup (1G27025-MSD3)
Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:32
Source: CE11137-11
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
198
0.561
mg/kg dry
11.3 231 NR 75-125 9
20
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 17

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1627025 - EPA 3050E - Continued
Post Spike (IG27025-PSI) Prepared: 07/27/2021 11:27 Analyzed: 08/02/2021 13:34
Source: CE11137-11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 4.08 0.0100 mg/L 0.200 3.95 65 80-120 QM-08
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1HO4038 - EPA 3010A
Blank (lH04038-BLKI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:14
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
Blank (1H04038-BLK2)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
LCS (IH04038-BSI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.209
0.0100
mg/L
0.200 105 80-120
Matrix Spike (1H04038-MS1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:24
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/L
10.0 0.155 U 113 75-125
Matrix Spike Dup (1H04038-MSD1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:26
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.2
0.500
mg/L
10.0 0.155 U 112 75-125 1
20
Post Spike (lH04038-PSI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:28
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.212
0.0100
mg/L
0.200 0.00262 105 80-120
Batch 1HO5022 - EPA 3010A
Blank (1H05022-BLKI) Prepared: 08/05/2021 12:44 Analyzed: 08/06/2021 10:11
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.155
U 0.500
mg/L
LCS (1H05022-BS1)
Prepared: 08/05/2021 12:44 Analyzed: 08/06/2021 10:17
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.213
0.0100
mg/L
0.200 107 80-120
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 14 of 17

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1H05022 - EPA 3010A - Continued
Matrix Spike (1H05022-MS1)
Prepared: 08/05/2021 12:44 Analyzed: 08/06/2021 10:19
Source: CE11137-05
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
10.8
0.500
mg/L
10.0 0.155 U 108 75-125
Matrix Spike Dup (1H05022-MSD1)
Prepared: 08/05/2021 12:44 Analyzed: 08/06/2021 10:22
Source: CE11137-05
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
10.3
0.500
mg/L
10.0 0.155 U 103 75-125 4
20
Post Spike (iH05022-PSI)
Prepared: 08/05/2021 12:44 Analyzed: 08/06/2021 10:24
Source: CE11137-05
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.214
0.0100
mg/L
0.200 0.000104 107 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 17

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 17

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, August 6, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11167
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, July 26, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 21

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A1S3
Lab ID: CE11167-01
Sampled: 07/26/21 09:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 11:51
Client ID: A1S2
Lab ID: CE11167-02
Sampled: 07/26/21 09:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:39
Client ID: A1S3
Lab ID: CE11167-03
Sampled: 07/26/21 09:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:42
Client ID: A1S4
Lab ID: CE11167-04
Sampled: 07/26/21 09:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:44
Client ID: A1S5
Lab ID: CE11167-05
Sampled: 07/26/21 09:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:47
Client ID: A1S6
Lab ID: CE11167-06
Sampled: 07/26/21 09:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:49
Client ID: A1S7
Lab ID: CE11167-07
Sampled: 07/26/21 09:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:51
Client ID: A1S8
Lab ID: CE11167-08
Sampled: 07/26/21 09:40
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(sl
08/05/21 12:53
Client ID: A1S9
Lab ID: CE11167-09
Sampled: 07/26/21 09:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 12:55
Client ID: A1S10
Lab ID: CE11167-10
Sampled: 07/26/21 09:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:09
Client ID: A1S11
Lab ID: CE11167-11
Sampled: 07/26/21 10:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:12
Client ID: A1S12
Lab ID: CE11167-12
Sampled: 07/26/21 10:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:14
Client ID: A1S13
Lab ID: CE11167-13
Sampled: 07/26/21 10:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:16
Client ID: A1S14
Lab ID: CE11167-14
Sampled: 07/26/21 10:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:18
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 21

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A1S35
Lab ID: CE11167-15
Sampled: 07/26/21 10:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:20
Client ID: A1S16
Lab ID: CE11167-16
Sampled: 07/26/21 10:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:22
Client ID: 30051
Lab ID: CE11167-17
Sampled: 07/26/21 11:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:24
Client ID: 30052
Lab ID: CE11167-18
Sampled: 07/26/21 11:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:26
Client ID: 30053
Lab ID: CE11167-19
Sampled: 07/26/21 11:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:28
Client ID: 30054
Lab ID: CE11167-20
Sampled: 07/26/21 11:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:39
Analysis Date/Time(s)
08/05/21 13:36
Client ID: 10055
Lab ID: CE11167-21
Sampled: 07/26/21 11:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 13:44
Client ID: 10056
Lab ID: CE11167-22
Sampled: 07/26/21 11:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 13:54
Client ID: 10057
Lab ID: CE11167-23
Sampled: 07/26/21 11:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 13:57
Client ID: 10058
Lab ID: CE11167-24
Sampled: 07/26/21 11:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:11
Client ID: A4S1
Lab ID: CE11167-25
Sampled: 07/26/21 12:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:13
Client ID: A4S2
Lab ID: CE11167-26
Sampled: 07/26/21 12:40
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:15
Client ID: A4S3
Lab ID: CE11167-27
Sampled: 07/26/21 12:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:18
Client ID: A4S4
Lab ID: CE11167-28
Sampled: 07/26/21 12:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 21

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A4S5
Lab ID: CE11167-29
Sampled: 07/26/21 12:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:22
Client ID: A4S6
Lab ID: CE11167-30
Sampled: 07/26/21 13:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:24
Client ID: A4S7
Lab ID: CE11167-31
Sampled: 07/26/21 13:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:26
Client ID: A4S8
Lab ID: CE11167-32
Sampled: 07/26/21 13:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:28
Client ID: A4S9
Lab ID: CE11167-33
Sampled: 07/26/21 13:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:30
Client ID: A4S10
Lab ID: CE11167-34
Sampled: 07/26/21 13:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:40
Client ID: A4S11
Lab ID: CE11167-35
Sampled: 07/26/21 13:35
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:42
Client ID: A4S12
Lab ID: CE11167-36
Sampled: 07/26/21 13:45
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:44
Client ID: A4S13
Lab ID: CE11167-37
Sampled: 07/26/21 13:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
01/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:46
Client ID: A4S14
Lab ID: CE11167-38
Sampled: 07/26/21 13:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:48
Client ID: A4S15
Lab ID: CE11167-39
Sampled: 07/26/21 14:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:50
Client ID: A4S16
Lab ID: CE11167-40
Sampled: 07/26/21 14:05
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:42
Analysis Date/Time(s)
08/05/21 14:52
Client ID: A4S17
Lab ID: CE11167-41
Sampled: 07/26/21 14:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:01
Client ID: A4S18
Lab ID: CE11167-42
Sampled: 07/26/21 14:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:23
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 21

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A3S3
Lab ID: CE11167-43
Sampled: 07/26/21 14:50
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:25
Client ID: A3S2
Lab ID: CE11167-44
Sampled: 07/26/21 14:55
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:27
Client ID: A3S3
Lab ID: CE11167-45
Sampled: 07/26/21 15:00
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:30
Client ID: A3S4
Lab ID: CE11167-46
Sampled: 07/26/21 15:10
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:32
Client ID: A3S5
Lab ID: CE11167-47
Sampled: 07/26/21 15:15
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:34
Client ID: A3S6
Lab ID: CE11167-48
Sampled: 07/26/21 15:20
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:37
Client ID: A3S7
Lab ID: CE11167-49
Sampled: 07/26/21 15:25
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:39
Client ID: A3S8
Lab ID: CE11167-50
Sampled: 07/26/21 15:30
Received: 07/26/21 16:49
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
O1/22/22
Prep Date/Time(s)
08/04/21 09:43
Analysis Date/Time(s)
08/06/21 11:41
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 21

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SAMPLE DETECTION SUMMARY
Client ID: A1S3 Lab ID: CE11167-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 5.96 0.137 0.571 mq/kq dry EPA 6010D
I Client ID: A1S2 Lab ID: CE11167-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.7
0.144
0.599
mg/kg dry
EPA 6010D
Client ID: A1S3
Lab ID:
CE11167-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.91
0.139
0.579
mq/kq dry
EPA 6010D
I Client ID: A1S4 Lab ID: CE11167-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.67
0.141
0.587
mg/kg dry
EPA 6010D
Client ID: A1S5
Lab ID:
CE11167-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.20
0.132
0.548
mq/kq dry
EPA 6010D
I Client ID: A1S6 Lab ID: CE11167-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
33.0
0.146
0.609
mg/kg dry
EPA 6010D
Client ID: A1S7
Lab ID:
CE11167-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.5
0.134
0.559
mq/kq dry
EPA 6010D
I Client ID: A1S8 Lab ID: CE11167-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.18
0.146
0.610
mg/kg dry
EPA 6010D
Client ID: A1S9
Lab ID:
CE11167-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.46
0.132
0.551
mq/kq dry
EPA 6010D
I Client ID: A1S10 Lab ID: CE11167-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.38
0.138
0.573
mg/kg dry
EPA 6010D
Client ID: A1S11
Lab ID:
CE11167-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.61
0.132
0.549
mq/kq dry
EPA 6010D
I Client ID: A1S12 Lab ID: CE11167-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
2.46
0.130
0.541
mg/kg dry
EPA 6010D
Client ID: A1S13
Lab ID:
CE11167-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
2.85
0.127
0.529
mq/kq dry
EPA 6010D
I Client ID: A1S14 Lab ID: CE11167-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.65
0.132
0.549
mg/kg dry
EPA 6010D
Client ID: A1S15
Lab ID:
CE11167-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.51
0.129
0.536
mq/kq dry
EPA 6010D
I Client ID: A1S16 Lab ID: CE11167-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
37.8
0.137
0.573
mg/kg dry
EPA 6010D
Client ID: 30051
Lab ID:
CE11167-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
706
0.131
0.544
mq/kq dry
EPA 6010D
Client ID: 30052 Lab ID: CE11167-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 19.1 0.142 0.593 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 21

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SAMPLE DETECTION SUMMARY
Client ID: 30053 Lab ID: CE11167-19
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 54.8 0.153 0.635 mq/kq dry EPA 6010D
I Client ID: 30054 Lab ID: CE11167-20
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.3
0.142
0.591
mg/kg dry
EPA 6010D
Client ID: 100SS
Lab ID:
CE11167-21
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
18.6
0.152
0.632
mq/kq dry
EPA 6010D
I Client ID: 10056 Lab ID: CE11167-22
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.2
0.129
0.539
mg/kg dry
EPA 6010D
Client ID: 30057
Lab ID:
CE11167-23
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.25
0.166
0.692
mq/kq dry
EPA 6010D
I Client ID: 100SS Lab ID: CE11167-24
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.05
0.165
0.687
mg/kg dry
EPA 6010D
Client ID: A4S1
Lab ID:
CE11167-25
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
25.7
0.143
0.594
mq/kq dry
EPA 6010D
I Client ID: A4S2 Lab ID: CE11167-26
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.7
0.175
0.731
mg/kg dry
EPA 6010D
Client ID: A4S3
Lab ID:
CE11167-27
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
35.5
0.171
0.713
mq/kq dry
EPA 6010D
I Client ID: A4S4 Lab ID: CE11167-28
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
22.1
0.167
0.697
mg/kg dry
EPA 6010D
Client ID: A4S5
Lab ID:
CE11167-29
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
31.9
0.137
0.570
mq/kq dry
EPA 6010D
I Client ID: A4S6 Lab ID: CE11167-30
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
21.4
0.154
0.643
mg/kg dry
EPA 6010D
Client ID: A4S7
Lab ID:
CE11167-31
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.3
0.135
0.562
mq/kq dry
EPA 6010D
I Client ID: A4S8 Lab ID: CE11167-32
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.99
0.133
0.553
mg/kg dry
EPA 6010D
Client ID: A4S9
Lab ID:
CE11167-33
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.42
0.157
0.654
mq/kq dry
EPA 6010D
I Client ID: A4S10 Lab ID: CE11167-34
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.82
0.130
0.543
mg/kg dry
EPA 6010D
Client ID: A4S11
Lab ID:
CE11167-35
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
23.8
0.148
0.617
mq/kq dry
EPA 6010D
Client ID: A4S12 Lab ID: CE11167-36
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 21.9 0.120 0.498 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 21

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SAMPLE DETECTION SUMMARY
Client ID: A4S33 Lab ID: CE11167-37
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 108 0.121 0.502 mq/kq dry EPA 6010D
I Client ID: A4S34 Lab ID: CE11167-38
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.0
0.148
0.616
mg/kg dry
EPA 6010D
Client ID: A4S15
Lab ID:
CE11167-39
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
28.2
0.133
0.554
mq/kq dry
EPA 6010D
I Client ID: A4S16 Lab ID: CE11167-40
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
73.6
0.129
0.536
mg/kg dry
EPA 6010D
Client ID: A4S17
Lab ID:
CE11167-41
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.42
0.131
0.546
mq/kq dry
EPA 6010D
I Client ID: A4S18 Lab ID: CE11167-42
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
48.7
0.134
0.557
mg/kg dry
EPA 6010D
Client ID: A3S1
Lab ID:
CE11167-43
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.81
0.130
0.542
mq/kq dry
EPA 6010D
I Client ID: A3S2 Lab ID: CE11167-44
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.24
0.129
0.539
mg/kg dry
EPA 6010D
Client ID: A3S3
Lab ID:
CE11167-45
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.8
0.130
0.541
mq/kq dry
EPA 6010D
I Client ID: A3S4 Lab ID: CE11167-46
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.7
0.126
0.526
mg/kg dry
EPA 6010D
Client ID: A3S5
Lab ID:
CE11167-47
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.77
0.128
0.535
mq/kq dry
EPA 6010D
I Client ID: A3S6 Lab ID: CE11167-48
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.46
0.128
0.535
mg/kg dry
EPA 6010D
Client ID: A3S7
Lab ID:
CE11167-49
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.0
0.142
0.590
mq/kq dry
EPA 6010D
Client ID: A3S8 Lab ID: CE11167-50
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 8.74 0.130 0.541 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 21

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ANALYTICAL RESULTS
Description: A1S1 Lab Sample ID: CE11167-01 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.59
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 5.96 mg/kg dry 1 0.137 0.571 1H04013 EPA 6010D 08/05/21 11:51 JDH
Description: A1S2 Lab Sample ID:CE11167-02 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.42
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.7 mg/kg dry 1 0.144 0.599 1H04013 EPA 6010D 08/05/21 12:39 JDH
Description: A1S3 Lab Sample ID:CE11167-03 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.40
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.91 mg/kg dry 1 0.139 0.579 1H04013 EPA 6010D 08/05/21 12:42 JDH
Description: A1S4 Lab Sample ID:CE11167-04 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.24
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.67 mg/kg dry 1 0.141 0.587 1H04013 EPA 6010D 08/05/21 12:44 JDH
Description: A1S5 Lab Sample ID:CE11167-05 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.18
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 7.20 mg/kg dry 1 0.132 0.548 1H04013 EPA 6010D 08/05/21 12:47 JDH
Description: A1S6 Lab Sample ID: CE11167-06 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.07
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 33.0 mg/kg dry 1 0.146 0.609 1H04013 EPA 6010D 08/05/21 12:49 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 21

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ANALYTICAL RESULTS
Description: A1S7 Lab Sample ID: CE11167-07 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.46
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 11.5 mg/kg dry 1 0.134 0.559 1H04013 EPA 6010D 08/05/21 12:51 JDH
Description: A1S8 Lab Sample ID:CE11167-08 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:40 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.03
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.18 mg/kg dry 1 0.146 0.610 1H04013 EPA 6010D 08/05/21 12:53 JDH
Description: A1S9 Lab Sample ID:CE11167-09 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.78
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 6.46 mg/kg dry 1 0.132 0.551 1H04013 EPA 6010D 08/05/21 12:55 JDH
Description: A1S10 Lab Sample ID:CE11167-10 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/2109:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.22
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.38 mg/kg dry 1 0.138 0.573 1H04013 EPA 6010D 08/05/21 13:09 JDH
Description: A1S11 Lab Sample ID:CE11167-11 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.11
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 9.61 mg/kg dry 1 0.132 0.549 1H04013 EPA 6010D 08/05/21 13:12 JDH
Description: AIS12 Lab Sample ID: CE11167-12 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.47
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 2.46 mg/kg dry 1 0.130 0.541 1H04013 EPA 6010D 08/05/21 13:14 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 21

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ANALYTICAL RESULTS
Description: A1S13 Lab Sample ID: CE11167-13 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 2.85 mg/kg dry 1 0.127 0.529 1H04013 EPA 6010D 08/05/21 13:16 JDH
Description: A1S14 Lab Sample ID:CE11167-14 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.06
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.65 mg/kg dry 1 0.132 0.549 1H04013 EPA 6010D 08/05/21 13:18 JDH
Description: A1S15 Lab Sample ID:CE11167-15 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.24
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 4.51 mg/kg dry 1 0.129 0.536 1H04013 EPA 6010D 08/05/21 13:20 JDH
Description: A1S16 Lab Sample ID:CE11167-16 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 10:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.32
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 37.8 mg/kg dry 1 0.137 0.573 1H04013 EPA 6010D 08/05/21 13:22 JDH
Description: 100S1 Lab Sample ID:CE11167-17 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 706 mg/kg dry 1 0.131 0.544 1H04013 EPA 6010D 08/05/21 13:24 JDH
Description: 100S2 Lab Sample ID: CE11167-18 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.1 mg/kg dry 1 0.142 0.593 1H04013 EPA 6010D 08/05/21 13:26 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 21

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ANALYTICAL RESULTS
Description: 100S3 Lab Sample ID: CE11167-19 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 54.8 mg/kg dry 1 0.153 0.635 1H04013 EPA 6010D 08/05/21 13:28 JDH
Description: 100S4 Lab Sample ID:CE11167-20 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.65
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.3 mg/kg dry 1 0.142 0.591 1H04013 EPA 6010D 08/05/21 13:36 JDH
Description: 100S5 Lab Sample ID:CE11167-21 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.86
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 18.6 mg/kg dry 1.11 0.152 0.632 1H04014 EPA 6010D 08/05/21 13:44 JDH
Description: 100S6 Lab Sample ID:CE11167-22 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.75
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.2 mg/kg dry 1 0.129 0.539 1H04014 EPA 6010D 08/05/21 13:54 JDH
Description: 100S7 Lab Sample ID:CE11167-23 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.31
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 5.25 mg/kg dry 1.11 0.166 0.692 1H04014 EPA 6010D 08/05/21 13:57 JDH
Description: 100S8 Lab Sample ID:CE11167-24 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 11:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.05 mg/kg dry 1.11 0.165 0.687 1H04014 EPA 6010D 08/05/21 14:11 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 21

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ANALYTICAL RESULTS
Description: A4S1 Lab Sample ID: CE11167-25 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.12
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 25.7 mg/kg dry 1 0.143 0.594 1H04014 EPA 6010D 08/05/21 14:13 JDH
Description: A4S2 Lab Sample ID:CE11167-26 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:40 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.7 mg/kg dry 1.11 0.175 0.731 1H04014 EPA 6010D 08/05/21 14:15 JDH
Description: A4S3 Lab Sample ID:CE11167-27 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.90
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 35.5 mg/kg dry 1.11 0.171 0.713 1H04014 EPA 6010D 08/05/21 14:18 JDH
Description: A4S4 Lab Sample ID:CE11167-28 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.65
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.1 mg/kg dry 1.11 0.167 0.697 1H04014 EPA 6010D 08/05/21 14:20 JDH
Description: A4S5 Lab Sample ID:CE11167-29 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 12:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 31.9 mg/kg dry 1 0.137 0.570 1H04014 EPA 6010D 08/05/21 14:22 JDH
Description: A4S6 Lab Sample ID: CE11167-30 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.39
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.4 mg/kg dry 1.11 0.154 0.643 1H04014 EPA 6010D 08/05/21 14:24 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 21

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ANALYTICAL RESULTS
Description: A4S7 Lab Sample ID: CE11167-31 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.94
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 17.3 mg/kg dry 1 0.135 0.562 1H04014 EPA 6010D 08/05/21 14:26 JDH
Description: A4S8 Lab Sample ID:CE11167-32 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.99 mg/kg dry 1 0.133 0.553 1H04014 EPA 6010D 08/05/21 14:28 JDH
Description: A4S9 Lab Sample ID:CE11167-33 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.42 mg/kg dry 1.11 0.157 0.654 1H04014 EPA 6010D 08/05/21 14:30 JDH
Description: A4S10 Lab Sample ID:CE11167-34 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.00
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 9.82 mg/kg dry 1 0.130 0.543 1H04014 EPA 6010D 08/05/21 14:40 JDH
Description: A4S11 Lab Sample ID:CE11167-35 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:35 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 23.8 mg/kg dry 1.11 0.148 0.617 1H04014 EPA 6010D 08/05/21 14:42 JDH
Description: A4S12 Lab Sample ID:CE11167-36 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:45 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.9 mg/kg dry 1 0.120 0.498 1H04014 EPA 6010D 08/05/21 14:44 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 21

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ANALYTICAL RESULTS
Description: A4S13 Lab Sample ID: CE11167-37 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.53
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 108 mg/kg dry 1 0.121 0.502 1H04014 EPA 6010D 08/05/21 14:46 JDH
Description: A4S14 Lab Sample ID:CE11167-38 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 13:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.25
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.0 mg/kg dry 1.11 0.148 0.616 1H04014 EPA 6010D 08/05/21 14:48 JDH
Description: A4S15 Lab Sample ID:CE11167-39 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 28.2 mg/kg dry 1 0.133 0.554 1H04014 EPA 6010D 08/05/21 14:50 JDH
Description: A4S16 Lab Sample ID:CE11167-40 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:05 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.22
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 73.6 mg/kg dry 1 0.129 0.536 1H04014 EPA 6010D 08/05/21 14:52 JDH
Description: A4S17 Lab Sample ID:CE11167-41 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.59
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 6.42 mg/kg dry 1 0.131 0.546 1H04015 EPA 6010D 08/06/21 11:01 JDH
Description: A4S18 Lab Sample ID: CE11167-42 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 48.7 mg/kg dry 1 0.134 0.557 1H04015 EPA 6010D 08/06/21 11:23 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 21

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ANALYTICAL RESULTS
Description: A3S1 Lab Sample ID: CE11167-43 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:50 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.33
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 7.81 mg/kg dry 1 0.130 0.542 1H04015 EPA 6010D 08/06/21 11:25 JDH
Description: A3S2 Lab Sample ID:CE11167-44 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 14:55 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.70
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 9.24 mg/kg dry 1 0.129 0.539 1H04015 EPA 6010D 08/06/21 11:27 JDH
Description: A3S3 Lab Sample ID:CE11167-45 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:00 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.50
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 11.8 mg/kg dry 1 0.130 0.541 1H04015 EPA 6010D 08/06/21 11:30 JDH
Description: A3S4 Lab Sample ID:CE11167-46 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:10 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.09
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 11.7 mg/kg dry 1 0.126 0.526 1H04015 EPA 6010D 08/06/21 11:32 JDH
Description: A3S5 Lab Sample ID:CE11167-47 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:15 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.41
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.77 mg/kg dry 1 0.128 0.535 1H04015 EPA 6010D 08/06/21 11:34 JDH
Description: A3S6 Lab Sample ID: CE11167-48 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:20 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.39
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 5.46 mg/kg dry 1 0.128 0.535 1H04015 EPA 6010D 08/06/21 11:37 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 21

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ANALYTICAL RESULTS
Description: A3S7 Lab Sample ID: CE11167-49 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:25 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 13.0 mg/kg dry 1 0.142 0.590 1H04015 EPA 6010D 08/06/21 11:39 JDH
Description: A3S8 Lab Sample ID:CE11167-50 Received: 07/26/21 16:49
Matrix: Soil Sampled: 07/26/21 15:30 Work Order: CE11167
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.35
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.74 mg/kg dry 1 0.130 0.541 1H04015 EPA 6010D 08/06/21 11:41 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 21

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1HO4013 - EPA 3050E
Blank (lH04013-BLKI) Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (lH04013-BS1) Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.2
0.500
mg/kg wet
9.62 106 80-120
Matrix Spike (1H04013-MS1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:53
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.5
0.571
mg/kg dry
11.9 5.96 114 75-125
Matrix Spike Dup (1H04013-MSD1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 11:55
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.0
0.571
mg/kg dry
11.9 5.96 93 75-125 14
20
Post Spike (11-104013-PS1)
Prepared: 08/04/2021 09:39 Analyzed: 08/05/2021 12:35
Source: CE11167-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.315
0.0100
mg/L
0.200 0.0981 108 80-120
Batch 1HO4014 - EPA 30505
Blank (11-104014-BLKi) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:38
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.133 U 0.556 mg/kg wet
LCS (11-104014-BSI) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:41
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.79
0.455
mg/kg wet
9.09 108 80-120
Matrix Spike (lH04014-MS1)
Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:46
Source: CE11167-21
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
36.8
0.569
mg/kg dry
11.4 18.6 160 75-125
QM-07
Matrix Spike Dup (1H04014-MSD1)
Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:48
Source: CE11167-21
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
80.1
0.569
mg/kg dry
11.4 18.6 540 75-125 74
20
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 21

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1HO4014 - EPA 3050B - Continued
Post Spike (IH04014-PS3) Prepared: 08/04/2021 09:42 Analyzed: 08/05/2021 13:50
Source: CE11167-21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.501 0.0100 mg/L 0.200 0.294 103 80-120
Batch 1HO4015 - EPA 30508
Blank (1H04015-BLK1) Prepared: 08/04/2021 09:43 Analyzed: 08/06/2021 10:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 u 0.500 mg/kg wet
LCS (1H04015-BSI) Prepared: 08/04/2021 09:43 Analyzed: 08/06/2021 11:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.6
0.500
mg/kg wet
9.71 109 80-120
Matrix Spike (1H04015-MS1)
Prepared: 08/04/2021 09:43 Analyzed: 08/06/2021 11:06
Source: CE11167-41
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.3
0.546
mg/kg dry
11.0 6.42 117 75-125
Matrix Spike Dup (1H04015-MSD1)
Prepared: 08/04/2021 09:43 Analyzed: 08/06/2021 11:08
Source: CE11167-41
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
18.4
0.546
mg/kg dry
11.6 6.42 103 75-125 5
20
Post Spike (lH04015-PSI)
Prepared: 08/04/2021 09:43 Analyzed: 08/06/2021 11:11
Source: CE11167-41
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.325
0.0100
mg/L
0.200 0.116 104 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 21

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 21

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, August 13, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11646
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, August 4, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Amanda L. Gaines For Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 9

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 300P313-11
Lab ID: CE11646-01
Sampled: 08/04/21 13:20
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:32
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 14:32
Client ID: 100P4B-R
Lab ID: CE11646-02
Sampled: 08/04/21 13:30
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:42
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 14:57
Client ID: 100P6A-R
Lab ID: CE11646-03
Sampled: 08/04/21 13:40
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:44
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 15:00
Client ID: 300P613-11
Lab ID: CE11646-04
Sampled: 08/04/21 13:50
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:46
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 15:02
Client ID: 200P113-11
Lab ID: CE11646-05
Sampled: 08/04/21 14:00
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:48
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 15:05
Client ID: 200P2A-R
Lab ID: CE11646-06
Sampled: 08/04/21 14:10
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:50
EPA 6010D
EPA 3010A
O1/31/22 02/07/22
08/11/21 14:04
08/12/21 15:07
Client ID: A2S18-R
Lab ID: CE11646-07
Sampled: 08/04/21 15:10
Received: 08/04/21 16:13
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O1/31/22
08/11/21 08:09
08/12/21 13:52
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 9

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SAMPLE DETECTION SUMMARY
Client ID:
300P3B-R
Lab ID:
CE11646-01
Analvte
Lead - Total
Results
1440
Flag
MDL
0.127
PQL
0.528
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
300P4B-R
Lab ID:
CE11646-02
Analvte
Lead - Total
Results
953
Flag
MDL
0.128
PQL
0.532
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
300P6A-R
Lab ID:
CE11646-03
Analvte
Lead - Total
Results
950
Flag
MDL
0.130
PQL
0.540
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
300P6B-R
Lab ID:
CE11646-04
Analvte
Lead - Total
Results
883
Flag
MDL
0.130
PQL
0.541
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P1B-R
Lab ID:
CE11646-05
Analvte
Lead - Total
Results
136
Flag
MDL
0.128
PQL
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P2A-R
Lab ID:
CE11646-06
Analvte
Lead - Total
Results
195
Flag
MDL
0.128
PQL
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A2S38-R
Lab ID:
CE11646-07
Analvte
Lead - Total
Results
343
Flag
MDL
0.141
PQL
0.588
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 9

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ANALYTICAL RESULTS
Description: 100P3B-R Lab Sample ID: CE11646-01 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 13:20 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.66
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 1440
mg/kg dry
1
0.127
0.528
lH11004
EPA 6010D
08/12/21 13:32
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 14:32
JDH
Description: 100P4B-R Lab Sample ID: CE11646-02 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 13:30 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 953
mg/kg dry
1
0.128
0.532
lH11004
EPA 6010D
08/12/21 13:42
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 14:57
JDH
Description: 100P6A-R Lab Sample ID: CE11646-03 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 13:40 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
I;Y Notes
Lead [7439-92-1]^ 950
mg/kg dry
1
0.130
0.540
lH11004
EPA 6010D
08/12/21 13:44
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 15:00
JDH
Description: 100P6B-R Lab Sample ID: CE11646-04 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 13:50 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.49
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 883
mg/kg dry
1
0.130
0.541
lH11004
EPA 6010D
08/12/21 13:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 15:02
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 of 9

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ANALYTICAL RESULTS
Description: 200P1B-R Lab Sample ID: CE11646-05 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 14:00 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.86
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 136
mg/kg dry
1
0.128
0.533
lH11004
EPA 6010D
08/12/21 13:48
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 15:05
JDH
Description: 200P2A-R Lab Sample ID: CE11646-06 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 14:10 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.76
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 195
mg/kg dry
1
0.128
0.533
lH11004
EPA 6010D
08/12/21 13:50
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H11022
EPA 6010D
08/12/21 15:07
JDH
Description: A2S18-R Lab Sample ID: CE11646-07 Received: 08/04/21 16:13
Matrix: Soil Sampled: 08/04/21 15:10 Work Order: CE11646
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.99
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 343 mg/kg dry 1 0.141 0.588 lH11004 EPA 6010D 08/12/21 13:52 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 of 9

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch IH11004 - EPA 3050E
Blank (11-111004-BLKI) Prepared: 08/11/2021 08:09 Analyzed: 08/12/2021 12:57
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Lead 0.108 U 0.450 mg/kg wet
LCS (1H11004-BS1) Prepared: 08/11/2021 08:09 Analyzed: 08/12/2021 13:05
Spike
Source
O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
10.1
0.500
mg/kg wet
10.4
97
80-120
Matrix Spike (1H11004-MS1)
Prepared: 08/11/2021 08:09 Analyzed: 08/12/2021 13:13
Source: CE09815-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
O/oREC
Limits RPD
Limit
Notes
Lead
128
0.798
mg/kg dry
16.3
54.0
454
75-125
QM-07
Matrix Spike Dup (1H11004-MSDl)
Prepared: 08/11/2021 08:09 Analyzed: 08/12/2021 13:15
Source: CE09815-01
Spike
Source
O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
O/oREC
Limits RPD
Limit
Notes
Lead
147
0.688
mg/kg dry
13.8
54.0
679
75-125 14
20
QM-07
Post Spike (11-111004-PS3)
Prepared: 08/11/2021 08:09 Analyzed: 08/12/2021 13:23
Source: CE09815-01
Spike
Source
O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
0.856
0.0100
mg/L
0.200
0.656
100
80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IH11022 - EPA 3010A
Blank (1H13022-BLK1) Prepared: 08/11/2021 14:05 Analyzed: 08/12/2021 14:27
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (1H11022-BSI) Prepared: 08/11/2021 14:05 Analyzed: 08/12/2021 14:34
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Lead
0.219
0.0100
mg/L
0.200 110 80-120
Matrix Spike (1H11022-MS1)
Prepared: 08/11/2021 14:05 Analyzed: 08/12/2021 14:38
Source: CE11646-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Lead
11.3
0.500
mg/L
10.0 0.155 U 113 75-125
Matrix Spike Dup (1H13022-MSD1)
Prepared: 08/11/2021 14:05 Analyzed: 08/12/2021 14:40
Source: CE11646-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
11.1
0.500
mg/L
10.0 0.155 U 111 75-125 2
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 9

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IH11022 - EPA 3010A - Continued
Post Spike (SH11022-PS1) Prepared: 08/11/2021 14:05 Analyzed: 08/12/2021 14:50
Source: CE11646-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.226 0.0100 mg/L 0.200 0.00251 112 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 9

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 of 9

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, August 23, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE12199
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, August 13, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 12

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 200P4A-R
Lab ID: CE12199-01
Sampled: 08/12/21 12:10
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 13:28
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 09:29
Client ID: 200P5A-R
Lab ID: CE12199-02
Sampled: 08/12/21 12:20
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 13:30
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 10:04
Client ID: 200P5B-R
Lab ID: CE12199-03
Sampled: 08/12/21 12:30
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 10:07
Client ID: 200P5B-R
Lab ID: CE12199-03RE1
Sampled: 08/12/21 12:30
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 14:25
Client ID: 200P6A-R
Lab ID: CE12199-04
Sampled: 08/12/21 12:40
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 13:46
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 10:09
Client ID: 200P613-11
Lab ID: CE12199-05
Sampled: 08/12/21 12:50
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 13:48
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 10:12
Client ID: 200P9A-R
Lab ID: CE12199-06
Sampled: 08/12/21 13:00
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/08/22
08/17/21 07:43
08/18/21 13:50
EPA 6010D
EPA 3010A
02/08/22 02/16/22
08/20/21 10:38
08/23/21 10:14
Client ID: 200P11B-R
Lab ID: CE12199-07
Sampled: 08/13/21 13:00
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/09/22
08/17/21 07:43
08/18/21 13:52
EPA 6010D
EPA 3010A
02/09/22 02/16/22
08/20/21 10:38
08/23/21 09:44
Client ID: 200P1313-11
Lab ID: CE12199-08
Sampled: 08/13/21 13:20
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/09/22
08/17/21 07:43
08/18/21 13:54
EPA 6010D
EPA 3010A
02/09/22 02/16/22
08/20/21 10:38
08/23/21 10:17
Client ID: 300S1-R
Lab ID: CE12199-09
Sampled: 08/13/21 13:40
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/09/22
08/17/21 07:43
08/18/21 13:56
Client ID: A3131
Lab ID: CE12199-10
Sampled: 08/13/21 11:50
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/09/22
08/17/21 07:43
08/18/21 13:58
Client ID: A3132
Lab ID: CE12199-11
Sampled: 08/13/21 12:05
Received: 08/13/21 16:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
02/09/22
08/17/21 07:43
08/18/21 14:01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 12

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A3133
Lab ID: CE12199-12
Sampled: 08/13/21 13:55
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:03
Client ID: A3134
Lab ID: CE12199-13
Sampled: 08/13/21 14:10
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:05
Client ID: A3135
Lab ID: CE12199-14
Sampled: 08/13/21 14:20
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:14
Client ID: A3136
Lab ID: CE12199-15
Sampled: 08/13/21 14:30
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:16
Client ID: A3137
Lab ID: CE12199-16
Sampled: 08/13/21 14:40
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:19
Client ID: A3138
Lab ID: CE12199-17
Sampled: 08/13/21 14:50
Received: 08/13/21 16:00
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/09/22
Prep Date/Time(s)
08/17/21 07:43
Analysis Date/Time(s)
08/18/21 14:21
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 12

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SAMPLE DETECTION SUMMARY
Client ID:
200P4A-R
Lab ID:
CE12199-01
Analvte
Lead - Total
Results
410
Flag
MDL
0.128
PQL
0.535
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200PSA-R
Lab ID:
CE12199-02
Analvte
Lead - Total
Results
142
Flag
MDL
0.127
PQL
0.528
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200PSB-R
Lab ID:
CE12199-03RE3
Analvte
Lead - Total
Results
6270
Flag
D
MDL
1.28
PQL
5.32
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P6A-R
Lab ID:
CE12199-04
Analvte
Lead - Total
Results
228
Flag
MDL
0.128
PQL
0.535
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P6B-R
Lab ID:
CE12199-05
Analvte
Lead - Total
Results
118
Flag
MDL
0.128
PQL
0.534
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P9A-R
Lab ID:
CE12199-06
Analvte
Lead - Total
Results
363
Flag
MDL
0.127
PQL
0.527
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P31B-R
Lab ID:
CE12199-07
Analvte
Lead - Total
Results
223
Flag
MDL
0.126
PQL
0.524
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
200P13B-R
Lab ID:
CE12199-08
Analvte
Lead - Total
Results
131
Flag
MDL
0.128
PQL
0.533
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
300S3-R
Lab ID:
CE12199-09
Analvte
Lead - Total
Results
9.15
Flag
MDL
0.131
PQL
0.545
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31131
Lab ID:
CE12199-10
Analvte
Lead - Total
Results
22.9
Flag
MDL
0.129
PQL
0.538
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31132
Lab ID:
CE12199-11
Analvte
Lead - Total
Results
16.9
Flag
MDL
0.131
PQL
0.548
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31133
Lab ID:
CE12199-12
Analvte
Lead - Total
Results
16.2
Flag
MDL
0.130
PQL
0.543
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31134
Lab ID:
CE12199-13
Analvte
Lead - Total
Results
21.9
Flag
MDL
0.138
PQL
0.577
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31135
Lab ID:
CE12199-14
Analvte
Lead - Total
Results
19.3
Flag
MDL
0.130
PQL
0.540
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31136
Lab ID:
CE12199-15
Analvte
Lead - Total
Results
13.1
Flag
MDL
0.130
PQL
0.540
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31137
Lab ID:
CE12199-16
Analvte
Lead - Total
Results
9.20
Flag
MDL
0.129
PQL
0.536
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A31138
Lab ID:
CE12199-17
Analvte
Lead - Total
Results
84.7
Flag
MDL
0.132
PQL
0.549
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 12

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ANALYTICAL RESULTS
Description: 200P4A-R Lab Sample ID:CE12199-01 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 12:10 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.51
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 410
mg/kg dry
1
0.128
0.535
11-117006
EPA 6010D
08/18/21 13:28
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 09:29
JDH
Description: 200P5A-R Lab Sample ID:CE12199-02 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 12:20 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.65
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 142
mg/kg dry
1
0.127
0.528
11-117006
EPA 6010D
08/18/21 13:30
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:04
JDH
Description: 200P5B-R Lab Sample ID:CE12199-03 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 12:30 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
I;Y Notes
Lead [7439-92-1]^ 6270 D
mg/kg dry
10
1.28
5.32
11-117006
EPA 6010D
08/18/21 14:25
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:07
JDH
Description: 200P6A-R Lab Sample ID:CE12199-04 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 12:40 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 228
mg/kg dry
1
0.128
0.535
11-117006
EPA 6010D
08/18/21 13:46
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:09
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 12

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ANALYTICAL RESULTS
Description: 200P6B-R Lab Sample ID:CE12199-05 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 12:50 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 118
mg/kg dry
1
0.128
0.534
11-117006
EPA 6010D
08/18/21 13:48
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Iy Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:12
JDH
Description: 200P9A-R Lab Sample ID:CE12199-06 Received: 08/13/21 16:00
Matrix: Soil Sampled:08/12/21 13:00 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.85
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 363
mg/kg dry
1
0.127
0.527
11-117006
EPA 6010D
08/18/21 13:50
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:14
JDH
Description: 200P11B-R Lab Sample ID:CE12199-07 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 13:00 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 95.45
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
I;Y Notes
Lead [7439-92-1]^ 223
mg/kg dry
1
0.126
0.524
11-117006
EPA 6010D
08/18/21 13:52
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 09:44
JDH
Description: 200P13B-R Lab Sample ID:CE12199-08 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 13:20 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.75
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 131
mg/kg dry
1
0.128
0.533
11-117006
EPA 6010D
08/18/21 13:54
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 0.155 U
mg/L
50
0.155
0.500
1H2O018
EPA 6010D
08/23/21 10:17
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 12

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ANALYTICAL RESULTS
Description: 100S1-R Lab Sample ID:CE12199-09 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 13:40 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.72
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 9.15 mg/kg dry 1 0.131 0.545 11-117006 EPA 6010D 08/18/21 13:56 JDH
Description: A3B1 Lab Sample ID:CE12199-10 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 11:50 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.92
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.9 mg/kg dry 1 0.129 0.538 1H17006 EPA 6010D 08/18/21 13:58 JDH
Description: A3B2 Lab Sample ID:CE12199-11 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 12:05 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.29
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 16.9 mg/kg dry 1 0.131 0.548 11-117006 EPA 6010D 08/18/21 14:01 JDH
Description: A3B3 Lab Sample ID:CE12199-12 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 13:55 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.11
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 16.2 mg/kg dry 1 0.130 0.543 11-117006 EPA 6010D 08/18/21 14:03 JDH
Description: A3B4 Lab Sample ID:CE12199-13 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 14:10 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.9 mg/kg dry 1 0.138 0.577 11-117006 EPA 6010D 08/18/21 14:05 JDH
Description: A3B5 Lab Sample ID:CE12199-14 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 14:20 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.56
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.3 mg/kg dry 1 0.130 0.540 11-117006 EPA 6010D 08/18/21 14:14 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 12

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ANALYTICAL RESULTS
Description: A3B6 Lab Sample ID:CE12199-15 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 14:30 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 13.1 mg/kg dry 1 0.130 0.540 11-117006 EPA 6010D 08/18/21 14:16 JDH
Description: A3B7 Lab Sample ID:CE12199-16 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 14:40 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.36
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 9.20 mg/kg dry 1 0.129 0.536 1H17006 EPA 6010D 08/18/21 14:19 JDH
Description: A3B8 Lab Sample ID:CE12199-17 Received: 08/13/21 16:00
Matrix: Soil Sampled: 08/13/21 14:50 Work Order: CE12199
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.12
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 84.7 mg/kg dry 1 0.132 0.549 11-117006 EPA 6010D 08/18/21 14:21 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 12

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch IH17006 - EPA 3050E
Blank (11-117006-BLKI) Prepared: 08/17/2021 07:43 Analyzed: 08/18/2021 11:00
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1H17006-BS1) Prepared: 08/17/2021 07:43 Analyzed: 08/18/2021 13:01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Lead
10.9
0.500
mg/kg wet
10.2 106 80-120
Matrix Spike (1H17006-MS1)
Prepared: 08/17/2021 07:43 Analyzed: 08/18/2021 13:14
Source: CE11984-02
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Lead
25.2
0.645
mg/kg dry
13.0 59.3 NR 75-125
QM-07
Matrix Spike Dup (1H17006-MSD1)
Prepared: 08/17/2021 07:43 Analyzed: 08/18/2021 13:16
Source: CE11984-02
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Lead
21.8
0.645
mg/kg dry
13.2 59.3 NR 75-125 14
20
QM-07
Post Spike (11-117006-PS1)
Prepared: 08/17/2021 07:43 Analyzed: 08/18/2021 13:19
Source: CE11984-02
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Lead
1.09
0.0100
mg/L
0.200 0.911 90 80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IH2O018 - EPA 3010A
Blank (1H2O018-BLK1) Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:17
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
Blank (1H2O018-BLK2) Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:25
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (11-12O018-BSI) Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:31
Spike Source O/oREC
RPD
Analvte
Result
Flaq POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Lead
0.187
0.0100
mg/L
0.200 94 80-120
Matrix Spike (1H2O018-MS1)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:34
Source: CE12199-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Lead
9.21
0.500
mg/L
10.0 0.155 U 92 75-125
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 12

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1H20018 - EPA 3010A - Continued
Matrix Spike (1H2O018-MS2)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:46
Source: CE12199-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.86
0.500
mg/L
10.0 0.155 U 99 75-125
Matrix Spike Dup (1H2O018-MSD1)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:36
Source: CE12199-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.50
0.500
mg/L
10.0 0.155 U 95 75-125 3
20
Matrix Spike Dup (1H2O018-MSD2)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:56
Source: CE12199-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.69
0.500
mg/L
10.0 0.155 U 97 75-125 2
20
Post Spike (SH2O018-PS1)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:39
Source: CE12199-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.188
0.0100
mg/L
0.200-0.000928 94 80-120
Post Spike (1H2O018-PS2)
Prepared: 08/20/2021 10:38 Analyzed: 08/23/2021 09:59
Source: CE12199-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.195
0.0100
mg/L
0.200 0.000226 98 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 12

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 12

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, August 24, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE12334
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, August 17, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 15

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A4131
Lab ID: CE12334-01
Sampled: 08/16/21 11:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 12:57
Client ID: A4132
Lab ID: CE12334-02
Sampled: 08/16/21 11:15
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 12:59
Client ID: A4133
Lab ID: CE12334-03
Sampled: 08/16/21 11:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:01
Client ID: A4134
Lab ID: CE12334-04
Sampled: 08/16/21 11:45
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:03
Client ID: A4135
Lab ID: CE12334-05
Sampled: 08/16/21 12:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:06
Client ID: A4136
Lab ID: CE12334-06
Sampled: 08/16/21 12:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:08
Client ID: A4137
Lab ID: CE12334-07
Sampled: 08/16/21 12:45
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:10
Client ID: A4138
Lab ID: CE12334-08
Sampled: 08/16/21 13:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:12
Client ID: A4139
Lab ID: CE12334-09
Sampled: 08/16/21 13:10
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:29
Client ID: A41310
Lab ID: CE12334-10
Sampled: 08/16/21 13:20
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:31
Client ID: A41311
Lab ID: CE12334-11
Sampled: 08/16/21 13:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:34
Client ID: A41312
Lab ID: CE12334-12
Sampled: 08/16/21 13:40
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:36
Client ID: A41313
Lab ID: CE12334-13
Sampled: 08/16/21 13:50
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:38
Client ID: A41314
Lab ID: CE12334-14
Sampled: 08/16/21 14:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:41
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 15

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A41315
Lab ID: CE12334-15
Sampled: 08/16/21 14:10
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:43
Client ID: A41316
Lab ID: CE12334-16
Sampled: 08/16/21 14:20
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:08
Analysis Date/Time(s)
08/23/21 13:45
Client ID: A41317
Lab ID: CE12334-17
Sampled: 08/16/21 14:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 13:50
Client ID: A41318
Lab ID: CE12334-18
Sampled: 08/16/21 14:40
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:09
Client ID: A41319
Lab ID: CE12334-19
Sampled: 08/16/21 14:50
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:12
Client ID: A41320
Lab ID: CE12334-20
Sampled: 08/16/21 15:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:14
Client ID: A41321
Lab ID: CE12334-21
Sampled: 08/16/21 15:20
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:16
Client ID: A41322
Lab ID: CE12334-22
Sampled: 08/16/21 15:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(sl
08/23/21 14:18
Client ID: A41323
Lab ID: CE12334-23
Sampled: 08/16/21 15:40
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:21
Client ID: A41324
Lab ID: CE12334-24
Sampled: 08/16/21 15:50
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:30
Client ID: A41325
Lab ID: CE12334-25
Sampled: 08/16/21 16:00
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:33
Client ID: A41326
Lab ID: CE12334-26
Sampled: 08/16/21 16:10
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:35
Client ID: A41327
Lab ID: CE12334-27
Sampled: 08/16/21 16:20
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:37
Client ID: A41328
Lab ID: CE12334-28
Sampled: 08/16/21 16:30
Received: 08/17/21 08:45
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/12/22
Prep Date/Time(s)
08/19/21 10:13
Analysis Date/Time(s)
08/23/21 14:39
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 15

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A41329 Lab ID: CE12334-29 Sampled: 08/16/21 16:40 Received: 08/17/21 08:45
Parameter Preparation Hold Date/Time(s)
EPA 6010D EPA 3050B 02/12/22
Prep Date/Time(s) Analysis Date/Time(s)
08/19/21 10:13 08/23/21 14:41
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 15

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SAMPLE DETECTION SUMMARY
Client ID: A481 Lab ID: CE12334-01
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 14.2 0.149 0.622 mq/kq dry EPA 6010D
I Client ID: A482 Lab ID: CE12334-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
20.9
0.147
0.611
mg/kg dry
EPA 6010D
Client ID: A483
Lab ID:
CE12334-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
64.9
0.152
0.634
mq/kq dry
EPA 6010D
I Client ID: A484 Lab ID: CE12334-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.3
0.132
0.549
mg/kg dry
EPA 6010D
Client ID: A485
Lab ID:
CE12334-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
21.6
0.155
0.648
mq/kq dry
EPA 6010D
I Client ID: A486 Lab ID: CE12334-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
19.9
0.158
0.659
mg/kg dry
EPA 6010D
Client ID: A487
Lab ID:
CE12334-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
170
0.139
0.579
mq/kq dry
EPA 6010D
I Client ID: A488 Lab ID: CE12334-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.8
0.137
0.570
mg/kg dry
EPA 6010D
Client ID: A489
Lab ID:
CE12334-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
27.7
0.156
0.649
mq/kq dry
EPA 6010D
I Client ID: A4810 Lab ID: CE12334-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
19.8
0.156
0.652
mg/kg dry
EPA 6010D
Client ID: A4811
Lab ID:
CE12334-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
45.1
0.152
0.632
mq/kq dry
EPA 6010D
I Client ID: A4812 Lab ID: CE12334-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
22.8
0.132
0.550
mg/kg dry
EPA 6010D
Client ID: A4813
Lab ID:
CE12334-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
32.2
0.162
0.676
mq/kq dry
EPA 6010D
I Client ID: A4814 Lab ID: CE12334-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.52
0.149
0.621
mg/kg dry
EPA 6010D
Client ID: A4815
Lab ID:
CE12334-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
27.2
0.138
0.576
mq/kq dry
EPA 6010D
I Client ID: A4816 Lab ID: CE12334-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
86.6
0.133
0.556
mg/kg dry
EPA 6010D
Client ID: A4817
Lab ID:
CE12334-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
21.6
0.155
0.645
mq/kq dry
EPA 6010D
Client ID: A4818 Lab ID: CE12334-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 49.1 0.156 0.650 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 15

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SAMPLE DETECTION SUMMARY
Client ID:
A4819
Lab ID:
CE12334-19
Analvte
Lead - Total
Results
9.53
Flag
MDL
0.135
Q
0.562
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4820
Lab ID:
CE12334-20
Analvte
Lead - Total
Results
25.1
Flag
MDL
0.136
PQL
0.566
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4821
Lab ID:
CE12334-21
Analvte
Lead - Total
Results
13.9
Flag
MDL
0.156
PQL
0.650
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4822
Lab ID:
CE12334-22
Analvte
Lead - Total
Results
27.8
Flag
MDL
0.149
PQL
0.621
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4823
Lab ID:
CE12334-23
Analvte
Lead - Total
Results
8.78
Flag
MDL
0.140
PQL
0.582
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4824
Lab ID:
CE12334-24
Analvte
Lead - Total
Results
48.6
Flag
MDL
0.155
PQL
0.646
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4825
Lab ID:
CE12334-25
Analvte
Lead - Total
Results
7.24
Flag
MDL
0.138
PQL
0.573
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4826
Lab ID:
CE12334-26
Analvte
Lead - Total
Results
19.3
Flag
MDL
0.133
PQL
0.554
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4827
Lab ID:
CE12334-27
Analvte
Lead - Total
Results
96.0
Flag
MDL
0.118
PQL
0.494
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4828
Lab ID:
CE12334-28
Analvte
Lead - Total
Results
5.22
Flag
MDL
0.132
PQL
0.549
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
A4829
Lab ID:
CE12334-29
Analvte
Lead - Total
Results
5.68
Flag
MDL
0.133
PQL
0.553
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 15

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ANALYTICAL RESULTS
Description: A4B1 Lab Sample ID:CE12334-01 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 11:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 14.2 mg/kg dry 1 0.149 0.622 11-119008 EPA 6010D 08/23/21 12:57 JDH
Description: A4B2 Lab Sample ID:CE12334-02 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 11:15 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.88
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 20.9 mg/kg dry 1 0.147 0.611 11-119008 EPA 6010D 08/23/21 12:59 JDH
Description: A4B3 Lab Sample ID:CE12334-03 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 11:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.82
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 64.9 mg/kg dry 1 0.152 0.634 11-119008 EPA 6010D 08/23/21 13:01 JDH
Description: A4B4 Lab Sample ID:CE12334-04 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 11:45 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.11
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.3 mg/kg dry 1 0.132 0.549 11-119008 EPA 6010D 08/23/21 13:03 JDH
Description: A4B5 Lab Sample ID:CE12334-05 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 12:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.6 mg/kg dry 1 0.155 0.648 11-119008 EPA 6010D 08/23/21 13:06 JDH
Description: A4B6 Lab Sample ID:CE12334-06 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 12:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 75.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 19.9 mg/kg dry 1 0.158 0.659 1H19008 EPA 6010D 08/23/21 13:08 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 15

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ANALYTICAL RESULTS
Description: A4B7 Lab Sample ID:CE12334-07 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 12:45 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 170 mg/kg dry 1 0.139 0.579 11-119008 EPA 6010D 08/23/21 13:10 JDH
Description: A4B8 Lab Sample ID:CE12334-08 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.77
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 11.8 mg/kg dry 1 0.137 0.570 11-119008 EPA 6010D 08/23/21 13:12 JDH
Description: A4B9 Lab Sample ID:CE12334-09 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:10 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 27.7 mg/kg dry 1 0.156 0.649 11-119008 EPA 6010D 08/23/21 13:29 JDH
Description: A4B10 Lab Sample ID:CE12334-10 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:20 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.73
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.8 mg/kg dry 1 0.156 0.652 11-119008 EPA 6010D 08/23/21 13:31 JDH
Description: A4B11 Lab Sample ID:CE12334-11 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.07
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 45.1 mg/kg dry 1 0.152 0.632 11-119008 EPA 6010D 08/23/21 13:34 JDH
Description: A4B12 Lab Sample ID:CE12334-12 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:40 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.93
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.8 mg/kg dry 1 0.132 0.550 1H19008 EPA 6010D 08/23/21 13:36 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 15

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ANALYTICAL RESULTS
Description: A4B13 Lab Sample ID:CE12334-13 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 13:50 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.95
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 32.2 mg/kg dry 1 0.162 0.676 11-119008 EPA 6010D 08/23/21 13:38 JDH
Description: A4B14 Lab Sample ID:CE12334-14 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.55
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.52 mg/kg dry 1 0.149 0.621 11-119008 EPA 6010D 08/23/21 13:41 JDH
Description: A4B15 Lab Sample ID:CE12334-15 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:10 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 27.2 mg/kg dry 1 0.138 0.576 11-119008 EPA 6010D 08/23/21 13:43 JDH
Description: A4B16 Lab Sample ID:CE12334-16 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:20 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.91
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 86.6 mg/kg dry 1 0.133 0.556 11-119008 EPA 6010D 08/23/21 13:45 JDH
Description: A4B17 Lab Sample ID:CE12334-17 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.50
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 21.6 mg/kg dry 1 0.155 0.645 11-119009 EPA 6010D 08/23/21 13:50 JDH
Description: A4B18 Lab Sample ID:CE12334-18 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:40 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.88
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 49.1 mg/kg dry 1 0.156 0.650 11-119009 EPA 6010D 08/23/21 14:09 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 15

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ANALYTICAL RESULTS
Description: A4B19 Lab Sample ID:CE12334-19 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 14:50 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.91
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 9.53 mg/kg dry 1 0.135 0.562 11-119009 EPA 6010D 08/23/21 14:12 JDH
Description: A4B20 Lab Sample ID:CE12334-20 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 15:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.40
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 25.1 mg/kg dry 1 0.136 0.566 11-119009 EPA 6010D 08/23/21 14:14 JDH
Description: A4B21 Lab Sample ID:CE12334-21 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 15:20 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.91
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 13.9 mg/kg dry 1 0.156 0.650 11-119009 EPA 6010D 08/23/21 14:16 JDH
Description: A4B22 Lab Sample ID:CE12334-22 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 15:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.47
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 27.8 mg/kg dry 1 0.149 0.621 11-119009 EPA 6010D 08/23/21 14:18 JDH
Description: A4B23 Lab Sample ID:CE12334-23 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 15:40 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.78 mg/kg dry 1 0.140 0.582 11-119009 EPA 6010D 08/23/21 14:21 JDH
Description: A4B24 Lab Sample ID:CE12334-24 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 15:50 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.41
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 48.6 mg/kg dry 1 0.155 0.646 11-119009 EPA 6010D 08/23/21 14:30 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 15

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ANALYTICAL RESULTS
Description: A4B25 Lab Sample ID:CE12334-25 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 16:00 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.24
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 7.24 mg/kg dry 1 0.138 0.573 11-119009 EPA 6010D 08/23/21 14:33 JDH
Description: A4B26 Lab Sample ID:CE12334-26 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 16:10 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.29
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.3 mg/kg dry 1 0.133 0.554 11-119009 EPA 6010D 08/23/21 14:35 JDH
Description: A4B27 Lab Sample ID:CE12334-27 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 16:20 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.46
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 96.0 mg/kg dry 0.893 0.118 0.494 11-119009 EPA 6010D 08/23/21 14:37 JDH
Description: A4B28 Lab Sample ID:CE12334-28 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 16:30 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.10
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.22 mg/kg dry 1 0.132 0.549 11-119009 EPA 6010D 08/23/21 14:39 JDH
Description: A4B29 Lab Sample ID:CE12334-29 Received: 08/17/21 08:45
Matrix: Soil Sampled:08/16/21 16:40 Work Order: CE12334
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.68 mg/kg dry 1 0.133 0.553 11-119009 EPA 6010D 08/23/21 14:41 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 15

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch IH19008 - EPA 3050E
Blank (11-119008-BLKI) Prepared: 08/19/2021 10:08 Analyzed: 08/23/2021 11:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1H19008-BS1) Prepared: 08/19/2021 10:08 Analyzed: 08/23/2021 11:42
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.82
0.500
mg/kg wet
9.71 101 80-120
Matrix Spike (1H19008-MS1)
Prepared: 08/19/2021 10:08 Analyzed: 08/23/2021 11:47
Source: CE12097-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.6
0.578
mg/kg dry
11.8 9.04 89 75-125
Matrix Spike Dup (1H19008-MSD1)
Prepared: 08/19/2021 10:08 Analyzed: 08/23/2021 11:49
Source: CE12097-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
19.3
0.578
mg/kg dry
12.2 9.04 84 75-125 2
20
Post Spike (11-119008-PS1)
Prepared: 08/19/2021 10:08 Analyzed: 08/23/2021 11:51
Source: CE12097-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.329
0.0100
mg/L
0.200 0.150 90 80-120
Batch IH19009 - EPA 30505
Blank (11-119009-BLKI) Prepared: 08/19/2021 10:13 Analyzed: 08/23/2021 11:37
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (11-119009-BSI) Prepared: 08/19/2021 10:13 Analyzed: 08/23/2021 13:47
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.8
0.500
mg/kg wet
10.3 105 80-120
Matrix Spike (1H19009-MS1)
Prepared: 08/19/2021 10:13 Analyzed: 08/23/2021 14:00
Source: CE12334-17
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
39.4
0.645
mg/kg dry
13.6 21.6 131 75-125
QM-07
Matrix Spike Dup (1H19009-MSD1)
Prepared: 08/19/2021 10:13 Analyzed: 08/23/2021 14:02
Source: CE12334-17
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
36.0
0.645
mg/kg dry
13.2 21.6 109 75-125 9
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 15

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch IH19009 - EPA 3050E - Continued
Post Spike (SH19009-PS3) Prepared: 08/19/2021 10:13 Analyzed: 08/23/2021 14:05
Source: CE12334-17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.552 0.0100 mg/L 0.200 0.352 100 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 15

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 15

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 26, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE12737
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, August 20, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2131
Lab ID: CE12737-01
Sampled: 08/19/21 12:40
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:40
Client ID: A2132
Lab ID: CE12737-02
Sampled: 08/19/21 12:50
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:43
Client ID: A2133
Lab ID: CE12737-03
Sampled: 08/19/21 13:00
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:45
Client ID: A2134
Lab ID: CE12737-04
Sampled: 08/19/21 13:10
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:47
Client ID: A2135
Lab ID: CE12737-05
Sampled: 08/19/21 13:20
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:49
Client ID: A2136
Lab ID: CE12737-06
Sampled: 08/19/21 13:30
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:52
Client ID: A2137
Lab ID: CE12737-07
Sampled: 08/19/21 13:40
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 11:54
Client ID: A2138
Lab ID: CE12737-08
Sampled: 08/19/21 13:50
Received: 08/20/21 08:20
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/15/22
Prep Date/Time(s)
08/24/21 15:53
Analysis Date/Time(s)
08/26/21 12:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8

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SAMPLE DETECTION SUMMARY
Client ID: A281 Lab ID: CE12737-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 3.62 0.131 0.545 mq/kq dry EPA 6010D
I Client ID: A282 Lab ID: CE12737-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.36
0.128
0.533
mg/kg dry
EPA 6010D
Client ID: A283
Lab ID:
CE12737-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.27
0.128
0.533
mq/kq dry
EPA 6010D
I Client ID: A284 Lab ID: CE12737-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.88
0.128
0.535
mg/kg dry
EPA 6010D
Client ID: A285
Lab ID:
CE12737-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.51
0.132
0.551
mq/kq dry
EPA 6010D
I Client ID: A286 Lab ID: CE12737-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.30
0.137
0.573
mg/kg dry
EPA 6010D
Client ID: A287
Lab ID:
CE12737-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.88
0.130
0.541
mq/kq dry
EPA 6010D
Client ID: A288 Lab ID: CE12737-08
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 13.0 0.148 0.618 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8

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ANALYTICAL RESULTS
Description: A2B1 Lab Sample ID:CE12737-01 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 12:40 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.81
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 3.62 mg/kg dry 1 0.131 0.545 11-124037 EPA 6010D 08/26/21 11:40 JDH
Description: A2B2 Lab Sample ID:CE12737-02 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 12:50 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.74
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.36 mg/kg dry 1 0.128 0.533 11-124037 EPA 6010D 08/26/21 11:43 JDH
Description: A2B3 Lab Sample ID:CE12737-03 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:00 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 6.27 mg/kg dry 1 0.128 0.533 11-124037 EPA 6010D 08/26/21 11:45 JDH
Description: A2B4 Lab Sample ID:CE12737-04 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:10 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.43
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.88 mg/kg dry 1 0.128 0.535 11-124037 EPA 6010D 08/26/21 11:47 JDH
Description: A2B5 Lab Sample ID:CE12737-05 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:20 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.74
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 4.51 mg/kg dry 1 0.132 0.551 11-124037 EPA 6010D 08/26/21 11:49 JDH
Description: A2B6 Lab Sample ID:CE12737-06 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:30 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.32
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 7.30 mg/kg dry 1 0.137 0.573 11-124037 EPA 6010D 08/26/21 11:52 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8

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ANALYTICAL RESULTS
Description: A2B7 Lab Sample ID:CE12737-07 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:40 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.50
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 8.88 mg/kg dry 0.893 0.130 0.541 11-124037 EPA 6010D 08/26/21 11:54 JDH
Description: A2B8 Lab Sample ID:CE12737-08 Received: 08/20/21 08:20
Matrix: Soil Sampled:08/19/21 13:50 Work Order: CE12737
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.85
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.0 mg/kg dry 1 0.148 0.618 11-124037 EPA 6010D 08/26/21 12:28 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 8

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1 H24037 - EPA 3050E
Blank (1H24037-BLKI) Prepared: 08/24/2021 15:53 Analyzed: 08/26/2021 10:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1H24037-BS1) Prepared: 08/24/2021 15:53 Analyzed: 08/26/2021 10:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.7
0.500
mg/kg wet
10.4 103 80-120
Matrix Spike (1H24037-MS1)
Prepared: 08/24/2021 15:53 Analyzed: 08/26/2021 10:48
Source: CE12800-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
29.1
0.529
mg/kg dry
11.5 18.3 94 75-125
Matrix Spike Dup (11-124037-MS131)
Prepared: 08/24/2021 15:53 Analyzed: 08/26/2021 10:51
Source: CE12800-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
26.1
0.529
mg/kg dry
10.2 18.3 77 75-125 11
20
Post Spike (1H24037-PS1)
Prepared: 08/24/2021 15:53 Analyzed: 08/26/2021 11:00
Source: CE12800-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.551
0.0100
mg/L
0.200 0.362 94 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, September 1, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE12913
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, August 24, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 24

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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A2139
Lab ID: CE12913-01
Sampled: 08/23/21 09:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:07
Client ID: A21310
Lab ID: CE12913-02
Sampled: 08/23/21 09:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:09
Client ID: A21311
Lab ID: CE12913-03
Sampled: 08/23/21 10:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:11
Client ID: A21312
Lab ID: CE12913-04
Sampled: 08/23/21 10:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:13
Client ID: A21313
Lab ID: CE12913-05
Sampled: 08/23/21 10:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:15
Client ID: A21314
Lab ID: CE12913-06
Sampled: 08/23/21 10:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:17
Client ID: A21315
Lab ID: CE12913-07
Sampled: 08/23/21 10:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:20
Client ID: A21316
Lab ID: CE12913-08
Sampled: 08/23/21 10:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(sl
09/01/21 10:22
Client ID: A21317
Lab ID: CE12913-09
Sampled: 08/23/21 11:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:24
Client ID: A21318
Lab ID: CE12913-10
Sampled: 08/23/21 11:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:27
Client ID: A21319
Lab ID: CE12913-11
Sampled: 08/23/21 11:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:36
Client ID: A21320
Lab ID: CE12913-12
Sampled: 08/23/21 11:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:38
Client ID: A21321
Lab ID: CE12913-13
Sampled: 08/23/21 11:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:40
Client ID: A21322
Lab ID: CE12913-14
Sampled: 08/23/21 11:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:42
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 24

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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A21323
Lab ID: CE12913-15
Sampled: 08/23/21 12:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:45
Client ID: A21324
Lab ID: CE12913-16
Sampled: 08/23/21 12:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:47
Client ID: A21325
Lab ID: CE12913-17
Sampled: 08/23/21 12:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:49
Client ID: A21326
Lab ID: CE12913-18
Sampled: 08/23/21 12:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:12
Analysis Date/Time(s)
09/01/21 10:52
Client ID: A21327
Lab ID: CE12913-19
Sampled: 08/23/21 12:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 10:56
Client ID: A21328
Lab ID: CE12913-20
Sampled: 08/23/21 12:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:15
Client ID: A21329
Lab ID: CE12913-21
Sampled: 08/23/21 13:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:17
Client ID: A21330
Lab ID: CE12913-22
Sampled: 08/23/21 13:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:20
Client ID: A21331
Lab ID: CE12913-23
Sampled: 08/23/21 13:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:22
Client ID: A21332
Lab ID: CE12913-24
Sampled: 08/23/21 13:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:24
Client ID: A21333
Lab ID: CE12913-25
Sampled: 08/23/21 13:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:27
Client ID: A21334
Lab ID: CE12913-26
Sampled: 08/23/21 13:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:39
Client ID: A21335
Lab ID: CE12913-27
Sampled: 08/23/21 14:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:41
Client ID: A21336
Lab ID: CE12913-28
Sampled: 08/23/21 14:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:44
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 24

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A21337
Lab ID: CE12913-29
Sampled: 08/23/21 14:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:46
Client ID: A21338
Lab ID: CE12913-30
Sampled: 08/23/21 14:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:48
Client ID: A21339
Lab ID: CE12913-31
Sampled: 08/23/21 14:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:51
Client ID: A21340
Lab ID: CE12913-32
Sampled: 08/23/21 14:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:53
Client ID: A21341
Lab ID: CE12913-33
Sampled: 08/23/21 15:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:55
Client ID: A21342
Lab ID: CE12913-34
Sampled: 08/23/21 15:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/19/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:57
Client ID: A21343
Lab ID: CE12913-35
Sampled: 08/24/21 10:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 11:59
Client ID: A21344
Lab ID: CE12913-36
Sampled: 08/24/21 10:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 12:36
Client ID: A21345
Lab ID: CE12913-37
Sampled: 08/24/21 10:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 12:38
Client ID: A21346
Lab ID: CE12913-38
Sampled: 08/24/21 10:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:16
Analysis Date/Time(s)
09/01/21 12:40
Client ID: A21347
Lab ID: CE12913-39
Sampled: 08/24/21 10:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 12:45
Client ID: A21348
Lab ID: CE12913-40
Sampled: 08/24/21 11:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 12:57
Client ID: A21349
Lab ID: CE12913-41
Sampled: 08/24/21 11:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:05
Client ID: A21350
Lab ID: CE12913-42
Sampled: 08/24/21 11:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 24

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A21351
Lab ID: CE12913-43
Sampled: 08/24/21 11:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:10
Client ID: A21352
Lab ID: CE12913-44
Sampled: 08/24/21 11:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:12
Client ID: A21353
Lab ID: CE12913-45
Sampled: 08/24/21 11:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:14
Client ID: A21354
Lab ID: CE12913-46
Sampled: 08/24/21 12:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:16
Client ID: A21355
Lab ID: CE12913-47
Sampled: 08/24/21 12:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:19
Client ID: A21356
Lab ID: CE12913-48
Sampled: 08/24/21 12:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:21
Client ID: A21357
Lab ID: CE12913-49
Sampled: 08/24/21 12:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:23
Client ID: 10061
Lab ID: CE12913-50
Sampled: 08/24/21 08:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:26
Client ID: 10062
Lab ID: CE12913-51
Sampled: 08/24/21 08:50
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:34
Client ID: 300133
Lab ID: CE12913-52
Sampled: 08/24/21 09:00
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:37
Client ID: 300134
Lab ID: CE12913-53
Sampled: 08/24/21 09:10
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:39
Client ID: 100B5
Lab ID: CE12913-54
Sampled: 08/24/21 09:20
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:41
Client ID: 300136
Lab ID: CE12913-55
Sampled: 08/24/21 09:30
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:43
Client ID: 300137
Lab ID: CE12913-56
Sampled: 08/24/21 09:40
Received: 08/24/21 16:46
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/20/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:45
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 24

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 300138 Lab ID: CE12913-57 Sampled: 08/24/21 09:50 Received: 08/24/21 16:46
Parameter Preparation Hold Date/Time(s)
EPA 6010D EPA 3050B 02/20/22
Prep Date/Time(s) Analysis Date/Time(s)
08/27/21 08:18 09/01/21 13:47
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 24

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SAMPLE DETECTION SUMMARY
Client ID: A289 Lab ID: CE12913-01
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 17.4 0.150 0.625 mq/kq dry EPA 6010D
I Client ID: A2810 Lab ID: CE12913-02
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
62.5
0.145
0.602
mg/kg dry
EPA 6010D
Client ID: A2811
Lab ID:
CE12913-03
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.05
0.157
0.653
mq/kq dry
EPA 6010D
I Client ID: A2812 Lab ID: CE12913-04
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
55.9
0.138
0.574
mg/kg dry
EPA 6010D
Client ID: A2813
Lab ID:
CE12913-05
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
67.8
0.119
0.497
mq/kq dry
EPA 6010D
I Client ID: A2814 Lab ID: CE12913-06
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.95
0.131
0.547
mg/kg dry
EPA 6010D
Client ID: A2815
Lab ID:
CE12913-07
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.48
0.128
0.534
mq/kq dry
EPA 6010D
I Client ID: A2816 Lab ID: CE12913-08
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.4
0.129
0.536
mg/kg dry
EPA 6010D
Client ID: A2817
Lab ID:
CE12913-09
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.20
0.137
0.569
mq/kq dry
EPA 6010D
I Client ID: A2818 Lab ID: CE12913-10
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.21
0.139
0.579
mg/kg dry
EPA 6010D
Client ID: A2819
Lab ID:
CE12913-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.56
0.122
0.510
mq/kq dry
EPA 6010D
I Client ID: A2820 Lab ID: CE12913-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.34
0.136
0.566
mg/kg dry
EPA 6010D
Client ID: A2821
Lab ID:
CE12913-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.16
0.121
0.504
mq/kq dry
EPA 6010D
I Client ID: A2822 Lab ID: CE12913-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.02
0.149
0.619
mg/kg dry
EPA 6010D
Client ID: A2823
Lab ID:
CE12913-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.54
0.138
0.574
mq/kq dry
EPA 6010D
I Client ID: A2824 Lab ID: CE12913-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
44.6
0.144
0.598
mg/kg dry
EPA 6010D
Client ID: A2825
Lab ID:
CE12913-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
10.3
0.129
0.535
mq/kq dry
EPA 6010D
Client ID: A2826 Lab ID: CE12913-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 6.92 0.127 0.530 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 24

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SAMPLE DETECTION SUMMARY
Client ID: A2827 Lab ID: CE12913-19
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 28.3 0.129 0.538 mq/kq dry EPA 6010D
I Client ID: A2828 Lab ID: CE12913-20
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
89.2
0.145
0.604
mg/kg dry
EPA 6010D
Client ID: A2829
Lab ID:
CE12913-21
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.90
0.131
0.548
mq/kq dry
EPA 6010D
I Client ID: A2830 Lab ID: CE12913-22
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.16
0.134
0.556
mg/kg dry
EPA 6010D
Client ID: A2831
Lab ID:
CE12913-23
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.33
0.118
0.492
mq/kq dry
EPA 6010D
I Client ID: A2832 Lab ID: CE12913-24
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.7
0.137
0.570
mg/kg dry
EPA 6010D
Client ID: A2833
Lab ID:
CE12913-25
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.08
0.162
0.674
mq/kq dry
EPA 6010D
I Client ID: A2834 Lab ID: CE12913-26
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.8
0.152
0.635
mg/kg dry
EPA 6010D
Client ID: A2835
Lab ID:
CE12913-27
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.25
0.154
0.641
mq/kq dry
EPA 6010D
I Client ID: A2836 Lab ID: CE12913-28
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
5.87
0.144
0.601
mg/kg dry
EPA 6010D
Client ID: A2837
Lab ID:
CE12913-29
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.3
0.149
0.621
mq/kq dry
EPA 6010D
I Client ID: A2838 Lab ID: CE12913-30
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
18.9
0.167
0.697
mg/kg dry
EPA 6010D
Client ID: A2839
Lab ID:
CE12913-31
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
14.3
0.163
0.680
mq/kq dry
EPA 6010D
I Client ID: A2840 Lab ID: CE12913-32
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
44.2
0.149
0.620
mg/kg dry
EPA 6010D
Client ID: A2841
Lab ID:
CE12913-33
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.86
0.112
0.468
mq/kq dry
EPA 6010D
I Client ID: A2842 Lab ID: CE12913-34
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
9.83
0.134
0.559
mg/kg dry
EPA 6010D
Client ID: A2843
Lab ID:
CE12913-35
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
4.29
0.131
0.547
mq/kq dry
EPA 6010D
Client ID: A2844 Lab ID: CE12913-36
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 6.70 0.139 0.581 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 24

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SAMPLE DETECTION SUMMARY
Client ID: A211345 Lab ID: CE12913-37
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 10.4 0.149 0.621 mq/kq dry EPA 6010D
I Client ID: A211346 Lab ID: CE12913-38
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.9
0.156
0.649
mg/kg dry
EPA 6010D
Client ID: A211347
Lab ID:
CE12913-39
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
12.7
0.154
0.643
mq/kq dry
EPA 6010D
I Client ID: A211348 Lab ID: CE12913-40
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.27
0.148
0.617
mg/kg dry
EPA 6010D
Client ID: A211349
Lab ID:
CE12913-41
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.1
0.170
0.709
mq/kq dry
EPA 6010D
I Client ID: A211350 Lab ID: CE12913-42
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.4
0.159
0.660
mg/kg dry
EPA 6010D
Client ID: A211351
Lab ID:
CE12913-43
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
14.9
0.162
0.676
mq/kq dry
EPA 6010D
I Client ID: A211352 Lab ID: CE12913-44
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
11.3
0.167
0.696
mg/kg dry
EPA 6010D
Client ID: A211353
Lab ID:
CE12913-45
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
15.4
0.163
0.680
mq/kq dry
EPA 6010D
I Client ID: A211354 Lab ID: CE12913-46
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
19.2
0.165
0.687
mg/kg dry
EPA 6010D
Client ID: A211355
Lab ID:
CE12913-47
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.2
0.159
0.662
mq/kq dry
EPA 6010D
I Client ID: A211356 Lab ID: CE12913-48
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.29
0.139
0.579
mg/kg dry
EPA 6010D
Client ID: A211357
Lab ID:
CE12913-49
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.7
0.138
0.574
mq/kq dry
EPA 6010D
I Client ID: 3001131 Lab ID: CE12913-50
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
20.0
0.128
0.535
mg/kg dry
EPA 6010D
Client ID: 3001132
Lab ID:
CE12913-51
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
406
0.135
0.564
mq/kq dry
EPA 6010D
I Client ID: 3001133 Lab ID: CE12913-52
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
13.4
0.142
0.592
mg/kg dry
EPA 6010D
Client ID: 3001134
Lab ID:
CE12913-53
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
254
0.137
0.572
mq/kq dry
EPA 6010D
Client ID: 100B5 Lab ID: CE12913-54
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 14.0 0.135 0.564 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 24

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SAMPLE DETECTION SUMMARY
Client ID: 30086 Lab ID: CE12913-55
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 282 0.135 0.562 mq/kq dry EPA 6010D
I Client ID: 30087 Lab ID: CE12913-56
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.84
0.136
0.567
mg/kg dry
EPA 6010D
Client ID: 30088
Lab ID:
CE12913-57
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
166
0.137
0.569
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 24

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ANALYTICAL RESULTS
Description: A2B9 Lab Sample ID:CE12913-01 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/23/2109:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 79.97
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 17.4 mg/kg dry 1 0.150 0.625 11-127014 EPA 6010D 09/01/21 10:07 JDH
Description: A2B10 Lab Sample ID:CE12913-02 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/23/2109:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 62.5 mg/kg dry 1 0.145 0.602 11-127014 EPA 6010D 09/01/21 10:09 JDH
Description: A2B11 Lab Sample ID:CE12913-03 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.57
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.05 mg/kg dry 1 0.157 0.653 11-127014 EPA 6010D 09/01/21 10:11 JDH
Description: A2B12 Lab Sample ID:CE12913-04 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.14
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 55.9 mg/kg dry 1 0.138 0.574 11-127014 EPA 6010D 09/01/21 10:13 JDH
Description: A2B13 Lab Sample ID:CE12913-05 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.05
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 67.8 mg/kg dry 0.885 0.119 0.497 11-127014 EPA 6010D 09/01/21 10:15 JDH
Description: A2B14 Lab Sample ID:CE12913-06 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.39
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 4.95 mg/kg dry 1 0.131 0.547 11-127014 EPA 6010D 09/01/21 10:17 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 24

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ANALYTICAL RESULTS
Description: A2B15 Lab Sample ID:CE12913-07 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.56
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 4.48 mg/kg dry 1 0.128 0.534 11-127014 EPA 6010D 09/01/21 10:20 JDH
Description: A2B16 Lab Sample ID:CE12913-08 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 10:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 12.4 mg/kg dry 1 0.129 0.536 11-127014 EPA 6010D 09/01/21 10:22 JDH
Description: A2B17 Lab Sample ID:CE12913-09 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.83
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 6.20 mg/kg dry 1 0.137 0.569 11-127014 EPA 6010D 09/01/21 10:24 JDH
Description: A2B18 Lab Sample ID:CE12913-10 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.37
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.21 mg/kg dry 1 0.139 0.579 11-127014 EPA 6010D 09/01/21 10:27 JDH
Description: A2B19 Lab Sample ID:CE12913-11 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.50
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 5.56 mg/kg dry 0.862 0.122 0.510 11-127014 EPA 6010D 09/01/21 10:36 JDH
Description: A2B20 Lab Sample ID:CE12913-12 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.40
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.34 mg/kg dry 1 0.136 0.566 11-127014 EPA 6010D 09/01/21 10:38 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 24

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ANALYTICAL RESULTS
Description: A2B21 Lab Sample ID:CE12913-13 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.85
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 9.16 mg/kg dry 0.885 0.121 0.504 11-127014 EPA 6010D 09/01/21 10:40 JDH
Description: A2B22 Lab Sample ID:CE12913-14 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 11:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.73
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.02 mg/kg dry 1 0.149 0.619 11-127014 EPA 6010D 09/01/21 10:42 JDH
Description: A2B23 Lab Sample ID:CE12913-15 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.17
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 8.54 mg/kg dry 1 0.138 0.574 11-127014 EPA 6010D 09/01/21 10:45 JDH
Description: A2B24 Lab Sample ID:CE12913-16 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.59
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 44.6 mg/kg dry 1 0.144 0.598 11-127014 EPA 6010D 09/01/21 10:47 JDH
Description: A2B25 Lab Sample ID:CE12913-17 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.38
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 10.3 mg/kg dry 1 0.129 0.535 11-127014 EPA 6010D 09/01/21 10:49 JDH
Description: A2B26 Lab Sample ID:CE12913-18 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.32
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.92 mg/kg dry 1 0.127 0.530 11-127014 EPA 6010D 09/01/21 10:52 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 24

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ANALYTICAL RESULTS
Description: A2B27 Lab Sample ID:CE12913-19 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 28.3 mg/kg dry 1 0.129 0.538 11-127015 EPA 6010D 09/01/21 10:56 JDH
Description: A2B28 Lab Sample ID:CE12913-20 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 12:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 89.2 mg/kg dry 1 0.145 0.604 11-127015 EPA 6010D 09/01/21 11:15 JDH
Description: A2B29 Lab Sample ID:CE12913-21 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 5.90 mg/kg dry 1 0.131 0.548 11-127015 EPA 6010D 09/01/21 11:17 JDH
Description: A2B30 Lab Sample ID:CE12913-22 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.86
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.16 mg/kg dry 1 0.134 0.556 11-127015 EPA 6010D 09/01/21 11:20 JDH
Description: A2B31 Lab Sample ID:CE12913-23 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.76
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 6.33 mg/kg dry 0.893 0.118 0.492 11-127015 EPA 6010D 09/01/21 11:22 JDH
Description: A2B32 Lab Sample ID:CE12913-24 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.72
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.7 mg/kg dry 1 0.137 0.570 11-127015 EPA 6010D 09/01/21 11:24 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 24

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ANALYTICAL RESULTS
Description: A2B33 Lab Sample ID:CE12913-25 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 74.15
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 8.08 mg/kg dry 1 0.162 0.674 11-127015 EPA 6010D 09/01/21 11:27 JDH
Description: A2B34 Lab Sample ID:CE12913-26 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 13:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.69
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.8 mg/kg dry 1 0.152 0.635 11-127015 EPA 6010D 09/01/21 11:39 JDH
Description: A2B35 Lab Sample ID:CE12913-27 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 6.25 mg/kg dry 1 0.154 0.641 11-127015 EPA 6010D 09/01/21 11:41 JDH
Description: A2B36 Lab Sample ID:CE12913-28 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.21
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.87 mg/kg dry 1 0.144 0.601 11-127015 EPA 6010D 09/01/21 11:44 JDH
Description: A2B37 Lab Sample ID:CE12913-29 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.58
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 11.3 mg/kg dry 1 0.149 0.621 11-127015 EPA 6010D 09/01/21 11:46 JDH
Description: A2B38 Lab Sample ID:CE12913-30 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 71.75
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 18.9 mg/kg dry 1 0.167 0.697 11-127015 EPA 6010D 09/01/21 11:48 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 24

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ANALYTICAL RESULTS
Description: A2B39 Lab Sample ID:CE12913-31 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.52
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 14.3 mg/kg dry 1 0.163 0.680 11-127015 EPA 6010D 09/01/21 11:51 JDH
Description: A2B40 Lab Sample ID:CE12913-32 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 14:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.68
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 44.2 mg/kg dry 1 0.149 0.620 11-127015 EPA 6010D 09/01/21 11:53 JDH
Description: A2B41 Lab Sample ID:CE12913-33 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 15:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.14
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 4.86 mg/kg dry 0.862 0.112 0.468 11-127015 EPA 6010D 09/01/21 11:55 JDH
Description: A2B42 Lab Sample ID:CE12913-34 Received: 08/24/21 16:46
Matrix: Soil Sampled:08/23/21 15:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.47
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 9.83 mg/kg dry 1 0.134 0.559 11-127015 EPA 6010D 09/01/21 11:57 JDH
Description: A2B43 Lab Sample ID:CE12913-35 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 10:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.34
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 4.29 mg/kg dry 1 0.131 0.547 11-127015 EPA 6010D 09/01/21 11:59 JDH
Description: A2B44 Lab Sample ID:CE12913-36 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 10:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.07
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.70 mg/kg dry 1 0.139 0.581 11-127015 EPA 6010D 09/01/21 12:36 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 24

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ANALYTICAL RESULTS
Description: A2B45 Lab Sample ID:CE12913-37 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 10:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.47
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 10.4 mg/kg dry 1 0.149 0.621 11-127015 EPA 6010D 09/01/21 12:38 JDH
Description: A2B46 Lab Sample ID:CE12913-38 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 10:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.09
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 15.9 mg/kg dry 1 0.156 0.649 11-127015 EPA 6010D 09/01/21 12:40 JDH
Description: A2B47 Lab Sample ID:CE12913-39 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 10:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.73
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 12.7 mg/kg dry 1 0.154 0.643 11-127016 EPA 6010D 09/01/21 12:45 JDH
Description: A2B48 Lab Sample ID:CE12913-40 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.03
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.27 mg/kg dry 1 0.148 0.617 11-127016 EPA 6010D 09/01/21 12:57 JDH
Description: A2B49 Lab Sample ID:CE12913-41 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 70.56
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 15.1 mg/kg dry 1 0.170 0.709 11-127016 EPA 6010D 09/01/21 13:05 JDH
Description: A2B50 Lab Sample ID:CE12913-42 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 75.70
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.4 mg/kg dry 1 0.159 0.660 11-127016 EPA 6010D 09/01/21 13:07 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 24

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ANALYTICAL RESULTS
Description: A2B51 Lab Sample ID:CE12913-43 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.94
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 14.9 mg/kg dry 1 0.162 0.676 11-127016 EPA 6010D 09/01/21 13:10 JDH
Description: A2B52 Lab Sample ID:CE12913-44 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 71.87
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 11.3 mg/kg dry 1 0.167 0.696 11-127016 EPA 6010D 09/01/21 13:12 JDH
Description: A2B53 Lab Sample ID:CE12913-45 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 11:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.48
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 15.4 mg/kg dry 1 0.163 0.680 11-127016 EPA 6010D 09/01/21 13:14 JDH
Description: A2B54 Lab Sample ID:CE12913-46 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 12:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.74
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 19.2 mg/kg dry 1 0.165 0.687 11-127016 EPA 6010D 09/01/21 13:16 JDH
Description: A2B55 Lab Sample ID:CE12913-47 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 12:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 75.55
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 17.2 mg/kg dry 1 0.159 0.662 11-127016 EPA 6010D 09/01/21 13:19 JDH
Description: A2B56 Lab Sample ID:CE12913-48 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 12:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 78.48
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 7.29 mg/kg dry 1 0.139 0.579 11-127016 EPA 6010D 09/01/21 13:21 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 24

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ANALYTICAL RESULTS
Description: A2B57 Lab Sample ID:CE12913-49 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/21 12:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 76.37
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 13.7 mg/kg dry 0.877 0.138 0.574 11-127016 EPA 6010D 09/01/21 13:23 JDH
Description: 100B1 Lab Sample ID:CE12913-50 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2108:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.45
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 20.0 mg/kg dry 1 0.128 0.535 11-127016 EPA 6010D 09/01/21 13:26 JDH
Description: 100B2 Lab Sample ID:CE12913-51 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2108:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.65
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 406 mg/kg dry 1 0.135 0.564 11-127016 EPA 6010D 09/01/21 13:34 JDH
Description: 100B3 Lab Sample ID:CE12913-52 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:00 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.39
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 13.4 mg/kg dry 1 0.142 0.592 11-127016 EPA 6010D 09/01/21 13:37 JDH
Description: 100B4 Lab Sample ID:CE12913-53 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:10 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.45
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 254 mg/kg dry 1 0.137 0.572 11-127016 EPA 6010D 09/01/21 13:39 JDH
Description: 100B5 Lab Sample ID:CE12913-54 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:20 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.72
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 14.0 mg/kg dry 1 0.135 0.564 11-127016 EPA 6010D 09/01/21 13:41 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 24

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ANALYTICAL RESULTS
Description: 100B6 Lab Sample ID:CE12913-55 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:30 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.00
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 282 mg/kg dry 1 0.135 0.562 11-127016 EPA 6010D 09/01/21 13:43 JDH
Description: 100B7 Lab Sample ID:CE12913-56 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:40 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 88.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 6.84 mg/kg dry 1 0.136 0.567 11-127016 EPA 6010D 09/01/21 13:45 JDH
Description: 100B8 Lab Sample ID:CE12913-57 Received: 08/24/21 16:46
Matrix: Soil Sampled: 08/24/2109:50 Work Order: CE12913
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.87
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 166 mg/kg dry 1 0.137 0.569 11-127016 EPA 6010D 09/01/21 13:47 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 24

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1H27014 - EPA 3050E
Blank (1H27014-BLKI) Prepared: 08/27/2021 08:12 Analyzed: 09/01/2021 09:36
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1H27014-BS1) Prepared: 08/27/2021 08:12 Analyzed: 09/01/2021 09:39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.99
0.500
mg/kg wet
10.0 100 80-120
Matrix Spike (1H27014-MS1)
Prepared: 08/27/2021 08:12 Analyzed: 09/01/2021 09:45
Source: CE12910-04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
22.0
0.500
mg/kg wet
9.52 17.4 49 75-125
QM-07
Matrix Spike Dup (1H27014-MSD1)
Prepared: 08/27/2021 08:12 Analyzed: 09/01/2021 09:48
Source: CE12910-04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
24.7
0.500
mg/kg wet
9.43 17.4 78 75-125 12
20
Post Spike (1H27014-PS1)
Prepared: 08/27/2021 08:12 Analyzed: 09/01/2021 09:50
Source: CE12910-04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.517
0.0100
mg/L
0.200 0.347 85 80-120
Batch IH27015 - EPA 30508
Blank (1H27015-BLKI) Prepared: 08/27/2021 08:16 Analyzed: 09/01/2021 09:33
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (11-127015-BSI) Prepared: 08/27/2021 08:16 Analyzed: 09/01/2021 10:54
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.45
0.500
mg/kg wet
9.43 100 80-120
Matrix Spike (1H27015-MS1)
Prepared: 08/27/2021 08:16 Analyzed: 09/01/2021 11:06
Source: CE12913-19
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
31.1
0.538
mg/kg dry
10.8 28.3 26 75-125
QM-07
Matrix Spike Dup (1H27015-MSD1)
Prepared: 08/27/2021 08:16 Analyzed: 09/01/2021 11:08
Source: CE12913-19
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
31.3
0.538
mg/kg dry
9.97 28.3 30 75-125 0.6
20
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 24

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch IH27015 - EPA 30505 - Continued
Post Spike (IH27015-PS3) Prepared: 08/27/2021 08:16 Analyzed: 09/01/2021 11:10
Source: CE12913-19
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.727 0.0100 mg/L 0.200 0.521 103 80-120
Batch IH27016 - EPA 30508
Blank (1H27016-BLK1) Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 09:30
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 u 0.500 mg/kg wet
LCS (1H27016-BSI) Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.86
0.500
mg/kg wet
9.80 101 80-120
Matrix Spike (1H27016-MS1)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:48
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
24.7
0.643
mg/kg dry
12.6 12.7 95 75-125
Matrix Spike Dup (1H27016-MSD1)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:50
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
22.7
0.541
mg/kg dry
10.8 12.7 92 75-125 9
20
Post Spike (iH27016-PSI)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:53
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.403
0.0100
mg/L
0.200 0.205 99 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 24

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 24

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, September 3, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE12998
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, August 26, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A3131
Lab ID: CE12998-01
Sampled: 08/26/21 09:20
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
08/27/21 08:18
Analysis Date/Time(s)
09/01/21 13:49
Client ID: A1132
Lab ID: CE12998-02
Sampled: 08/26/21 09:30
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 11:41
Client ID: A1133
Lab ID: CE12998-03
Sampled: 08/26/21 09:40
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 11:53
Client ID: A1134
Lab ID: CE12998-04
Sampled: 08/26/21 09:50
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 11:55
Client ID: A1B5
Lab ID: CE12998-05
Sampled: 08/26/21 10:00
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:43
Client ID: A1136
Lab ID: CE12998-06
Sampled: 08/26/21 10:10
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:45
Client ID: A1137
Lab ID: CE12998-07
Sampled: 08/26/21 10:20
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:47
Client ID: A1138
Lab ID: CE12998-08
Sampled: 08/26/21 10:30
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(sl
09/03/21 12:49
Client ID: A1139
Lab ID: CE12998-09
Sampled: 08/26/21 10:40
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:52
Client ID: A11310
Lab ID: CE12998-10
Sampled: 08/26/21 10:50
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:54
Client ID: A11311
Lab ID: CE12998-11
Sampled: 08/26/21 11:00
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:56
Client ID: A11312
Lab ID: CE12998-12
Sampled: 08/26/21 11:10
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 12:58
Client ID: A11313
Lab ID: CE12998-13
Sampled: 08/26/21 11:20
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:01
Client ID: A11314
Lab ID: CE12998-14
Sampled: 08/26/21 11:30
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: A31315
Lab ID: CE12998-15
Sampled: 08/26/21 11:40
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:13
Client ID: A11316
Lab ID: CE12998-16
Sampled: 08/26/21 11:50
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:15
Client ID: A1B17
Lab ID: CE12998-17
Sampled: 08/26/21 12:00
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:18
Client ID: A11318
Lab ID: CE12998-18
Sampled: 08/26/21 12:10
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:20
Client ID: A11319
Lab ID: CE12998-19
Sampled: 08/26/21 12:20
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:22
Client ID: AIB20
Lab ID: CE12998-20
Sampled: 08/26/21 12:30
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:24
Client ID: A11321
Lab ID: CE12998-21
Sampled: 08/26/21 12:40
Received: 08/26/21 14:02
Parameter
EPA 6010D
Preparation
EPA 3050B
Hold Date/Time(s)
02/22/22
Prep Date/Time(s)
09/01/21 08:48
Analysis Date/Time(s)
09/03/21 13:26
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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SAMPLE DETECTION SUMMARY
Client ID: A381 Lab ID: CE12998-01
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 3.92 0.121 0.506 mq/kq dry EPA 6010D
I Client ID: A182 Lab ID: CE12998-02
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
3.48
0.131
0.545
mg/kg dry
EPA 6010D
Client ID: A183
Lab ID:
CE12998-03
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
2.77
0.130
0.544
mq/kq dry
EPA 6010D
I Client ID: A184 Lab ID: CE12998-04
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
8.33
0.131
0.544
mg/kg dry
EPA 6010D
Client ID: A185
Lab ID:
CE12998-05
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
13.0
0.132
0.548
mq/kq dry
EPA 6010D
I Client ID: A186 Lab ID: CE12998-06
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
5.73
0.128
0.535
mg/kg dry
EPA 6010D
Client ID: A187
Lab ID:
CE12998-07
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
10.8
0.148
0.618
mq/kq dry
EPA 6010D
I Client ID: A188 Lab ID: CE12998-08
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
37.6
0.143
0.596
mg/kg dry
EPA 6010D
Client ID: A189
Lab ID:
CE12998-09
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
5.73
0.127
0.530
mq/kq dry
EPA 6010D
I Client ID: A1810 Lab ID: CE12998-10
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
14.9
0.129
0.538
mg/kg dry
EPA 6010D
Client ID: A1811
Lab ID:
CE12998-11
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
3.71
0.130
0.542
mq/kq dry
EPA 6010D
I Client ID: A1812 Lab ID: CE12998-12
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
6.53
0.131
0.544
mg/kg dry
EPA 6010D
Client ID: A1813
Lab ID:
CE12998-13
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
17.8
0.134
0.558
mq/kq dry
EPA 6010D
I Client ID: A1814 Lab ID: CE12998-14
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
8.04
0.132
0.550
mg/kg dry
EPA 6010D
Client ID: A1815
Lab ID:
CE12998-15
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
7.60
0.130
0.540
mq/kq dry
EPA 6010D
I Client ID: A1816 Lab ID: CE12998-16
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
115
0.132
0.552
mg/kg dry
EPA 6010D
Client ID: A3817
Lab ID:
CE12998-17
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Lead - Total
21.5
0.130
0.542
mq/kq dry
EPA 6010D
Client ID: A1818 Lab ID: CE12998-18
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 11.6 0.141 0.588 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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SAMPLE DETECTION SUMMARY
Client ID: A3819 Lab ID: CE12998-19
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 16.5 0.129 0.538 mq/kq dry EPA 6010D
I Client ID: A1820 Lab ID: CE12998-20
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
25.1
0.133
0.554
mg/kg dry
EPA 6010D
Client ID: A1821
Lab ID:
CE12998-21
Analvte
Results
Flag MDL
Q
Units
Method Notes
Lead - Total
11.1
0.118
0.491
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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ANALYTICAL RESULTS
Description: A1B1 Lab Sample ID:CE12998-01 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/2109:20 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.05
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 3.92 mg/kg dry 1 0.121 0.506 11-127016 EPA 6010D 09/01/21 13:49 JDH
Description: A1B2 Lab Sample ID:CE12998-02 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/2109:30 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.73
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 3.48 mg/kg dry 1 0.131 0.545 1I01012 EPA 6010D 09/03/21 11:41 JDH
Description: A1B3 Lab Sample ID:CE12998-03 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/2109:40 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.98
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 2.77 mg/kg dry 1 0.130 0.544 1I01012 EPA 6010D 09/03/21 11:53 JDH
Description: A1B4 Lab Sample ID:CE12998-04 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/2109:50 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.85
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.33 mg/kg dry 1 0.131 0.544 1I01012 EPA 6010D 09/03/21 11:55 JDH
Description: A1B5 Lab Sample ID:CE12998-05 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:00 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.16
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 13.0 mg/kg dry 1 0.132 0.548 1I01012 EPA 6010D 09/03/21 12:43 JDH
Description: A1B6 Lab Sample ID:CE12998-06 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:10 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.40
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 5.73 mg/kg dry 1 0.128 0.535 1I01012 EPA 6010D 09/03/21 12:45 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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ANALYTICAL RESULTS
Description: A1B7 Lab Sample ID:CE12998-07 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:20 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.96
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 10.8 mg/kg dry 1 0.148 0.618 1I01012 EPA 6010D 09/03/21 12:47 JDH
Description: A1B8 Lab Sample ID:CE12998-08 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:30 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 83.84
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 37.6 mg/kg dry 1 0.143 0.596 1I01012 EPA 6010D 09/03/21 12:49 JDH
Description: A1B9 Lab Sample ID:CE12998-09 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:40 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 94.42
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 5.73 mg/kg dry 1 0.127 0.530 1I01012 EPA 6010D 09/03/21 12:52 JDH
Description: A1B10 Lab Sample ID:CE12998-10 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 10:50 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.93
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 14.9 mg/kg dry 1 0.129 0.538 1I01012 EPA 6010D 09/03/21 12:54 JDH
Description: A1B11 Lab Sample ID:CE12998-11 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:00 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.21
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 3.71 mg/kg dry 1 0.130 0.542 1I01012 EPA 6010D 09/03/21 12:56 JDH
Description: A1B12 Lab Sample ID:CE12998-12 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:10 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.89
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 6.53 mg/kg dry 1 0.131 0.544 1I01012 EPA 6010D 09/03/21 12:58 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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ANALYTICAL RESULTS
Description: A1B13 Lab Sample ID:CE12998-13 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:20 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.62
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 17.8 mg/kg dry 1 0.134 0.558 1I01012 EPA 6010D 09/03/21 13:01 JDH
Description: A1B14 Lab Sample ID:CE12998-14 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:30 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.95
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 8.04 mg/kg dry 1 0.132 0.550 1I01012 EPA 6010D 09/03/21 13:03 JDH
Description: A1B15 Lab Sample ID:CE12998-15 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:40 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.54
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed —By Notes
Lead [7439-92-1]^ 7.60 mg/kg dry 1 0.130 0.540 1I01012 EPA 6010D 09/03/21 13:13 JDH
Description: A1B16 Lab Sample ID:CE12998-16 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 11:50 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.61
Metals by EPA 6000/7000 Series Methods I
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 115 mg/kg dry 1 0.132 0.552 1I01012 EPA 6010D 09/03/21 13:15 JDH
Description: A1B17 Lab Sample ID:CE12998-17 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 12:00 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-11^ 21.5 mg/kg dry 1 0.130 0.542 1I01012 EPA 6010D 09/03/21 13:18 JDH
Description: A1B18 Lab Sample ID:CE12998-18 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 12:10 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes
Lead [7439-92-1]^ 11.6 mg/kg dry 1 0.141 0.588 1I01012 EPA 6010D 09/03/21 13:20 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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ANALYTICAL RESULTS
Description: A1B19 Lab Sample ID:CE12998-19 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 12:20 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.01
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 16.5 mg/kg dry 1 0.129 0.538 1I01012 EPA 6010D 09/03/21 13:22 JDH
Description: A1B20 Lab Sample ID:CE12998-20 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 12:30 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 25.1 mg/kg dry 1 0.133 0.554 1I01012 EPA 6010D 09/03/21 13:24 JDH
Description: A1B21 Lab Sample ID:CE12998-21 Received: 08/26/21 14:02
Matrix: Soil Sampled: 08/26/21 12:40 Work Order: CE12998
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.82
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Lead [7439-92-1]^ 11.1 mg/kg dry 1 0.118 0.491 1I01012 EPA 6010D 09/03/21 13:26 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1H27016 - EPA 3050E
Blank (1H27016-BLKI) Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 09:30
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1H27016-BS1) Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
9.86
0.500
mg/kg wet
9.80 101 80-120
Matrix Spike (1H27016-MS1)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:48
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
24.7
0.643
mg/kg dry
12.6 12.7 95 75-125
Matrix Spike Dup (1H27016-MSD1)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:50
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
22.7
0.541
mg/kg dry
10.8 12.7 92 75-125 9
20
Post Spike (1H27016-PS1)
Prepared: 08/27/2021 08:18 Analyzed: 09/01/2021 12:53
Source: CE12913-39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.403
0.0100
mg/L
0.200 0.205 99 80-120
Batch 1101012 - EPA 30505
Blank (3I03012-BLK3) Prepared: 09/01/2021 08:48 Analyzed: 09/03/2021 10:35
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (1I01012-BS1) Prepared: 09/01/2021 08:48 Analyzed: 09/03/2021 11:38
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
10.8
0.500
mg/kg wet
10.3 104 80-120
Matrix Spike (1I01012-MS1)
Prepared: 09/01/2021 08:48 Analyzed: 09/03/2021 11:43
Source: CE12998-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
15.5
0.545
mg/kg dry
11.2 3.48 107 75-125
Matrix Spike Dup (3I03012-MSD1)
Prepared: 09/01/2021 08:48 Analyzed: 09/03/2021 11:46
Source: CE12998-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
13.4
0.545
mg/kg dry
10.2 3.48 97 75-125 15
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1I01012 - EPA 30505 - Continued
Post Spike (SI03012-PS1) Prepared: 09/01/2021 08:48 Analyzed: 09/03/2021 11:48
Source: CE12998-02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.275 0.0100 mg/L 0.200 0.0663 105 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, September 10, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE13708
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, September 7, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 300132-R Lab ID: CE13708-01 Sampled: 09/07/21 10:30 Received: 09/07/21 16:45
Parameter Preparation Hold Date/Time(s)
EPA 6010D EPA 3050B 03/06/22
Prep Date/Time(s) Analysis Date/Time(s)
09/09/21 07:49 09/10/21 11:03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

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SAMPLE DETECTION SUMMARY
Client ID: 10082-11 Lab ID: CE13708-03
Analvte Results Flag MDL PQL Units Method Notes
Lead - Total 11.8 0.147 0.611 mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7

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ANALYTICAL RESULTS
Description: 100B2-R Lab Sample ID:CE13708-01 Received: 09/07/21 16:45
Matrix: Soil Sampled:09/07/21 10:30 Work Order: CE13708
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.82
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 11.8 mg/kg dry 1 0.147 0.611 1I09007 EPA 6010D 09/10/21 11:03 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 1109007 - EPA 30505
Blank (1I09007-BLK3) Prepared: 09/09/2021 07:49 Analyzed: 09/10/2021 10:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (3I09007-BS1) Prepared: 09/09/2021 07:49 Analyzed: 09/10/2021 11:01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.5
0.500
mg/kg wet
10.1 104 80-120
Matrix Spike (3I09007-MS1)
Prepared: 09/09/2021 07:49 Analyzed: 09/10/2021 11:16
Source: CE13708-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
24.0
0.611
mg/kg dry
12.2 11.8 100 75-125
Matrix Spike Dup (l109007-MSD1)
Prepared: 09/09/2021 07:49 Analyzed: 09/10/2021 11:26
Source: CE13708-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
26.8
0.611
mg/kg dry
12.2 11.8 123 75-125 11
20
Post Spike (l109007-PS1)
Prepared: 09/09/2021 07:49 Analyzed: 09/10/2021 11:28
Source: CE13708-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.401
0.0100
mg/L
0.200 0.193 104 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7

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2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 5, 2021
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CE11014
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, July 22, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 7

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Root Ball Soil Lab ID: CE11014-01 Sampled: 07/21/21 15:00 Received: 07/22/21 16:SS
Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 6010D EPA 3010A O1/17/22 01/31/22 08/04/21 16:52 08/05/21 11:33
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7

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SAMPLE DETECTION SUMMARY
No positive results detected.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 7

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ANALYTICAL RESULTS
Description: Root Ball Soil Lab Sample ID:CE11014-01 Received: 07/22/21 16:55
Matrix: Soil Sampled:07/21/21 15:00 Work Order: CE11014
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids:
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 0.155 U mg/L 50 0.155 0.500 1H04038 EPA 6010D 08/05/21 11:33 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 7

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1H04038 - EPA 3010A
Blank (lH04038-BLKI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:14
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
Blank (1H04038-BLK2)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.155
U
0.500
mg/L
LCS (IH04038-BSI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.209
0.0100
mg/L
0.200 105 80-120
Matrix Spike (lH04038-MS1)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:24
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.3
0.500
mg/L
10.0 0.155 U 113 75-125
Matrix Spike Dup (11-104038-MS131)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:26
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
11.2
0.500
mg/L
10.0 0.155 U 112 75-125 1
20
Post Spike (11-104038-PSI)
Prepared: 08/04/2021 16:52 Analyzed: 08/05/2021 10:28
Source: CE11013-16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.212
0.0100
mg/L
0.200 0.00262 105 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 7

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Appendix V - Preliminary Survey Plat

I, STEPHEN B, MULLINS, CERTIFY THAT THIS PLAT WAS DRAWN UNDER
MY SUPERVISION FROM AN ACTUAL SURVEY MADE UNDER MY
SUPERVISION (DEED DESCRIPTION(S) RECORDED AS SHOWN ON
HEREON); THAT THE BOUNDARIES NOT SURVEYED ARE CLEARLY
INDICATED AS DRAWN FROM INFORMATION SHOWN ON THE FACE OF
THIS PLAT; THAT THE RATIO OF PRECISION OR POSITIONAL
ACCURACY AS CALCULATED IS 1:20,000+; AND THAT THIS PLAT WAS
PREPARED IN ACCORDANCE WITH G.S. 47-30 AS AMENDED.
I ALSO CERTIFY TO ONE OR MORE OF THE FOLLOWING:
I CERTIFY THAT THIS SURVEY IS OF ANOTHER CATEGORY, SUCH AS
THE RECOMBINATION OF EXISTING PARCELS, A COURT -ORDERED
SURVEY, OR OTHER EXEMPTION OR EXCEPTION TO THE DEFINITION
OF SUBDIVISION.
WITNESS MY ORIGINAL SIGNATURE, LICENSE NUMBER & SEAL THIS
24th DAY OF OCTOBER, A.D. 2021.
STEPHEN B. MULLINS, PROFESSIONAL LAND SURVEYOR
LICENSE NUMBER L-3059
0000000
o,po N CoA R �oo
o0
o� � ° °o`of0000000°^'` OHO
°°O` `S S/0 °° �ooc 77
f°I��I oY PLAT
N(3T Ion 05 * VEYANCE,
RE���Tp� yoo; �� �R SALES
°o A o
0
aoa y0000000000� o00
000aFN00 oB oaM0000
WAKE STONE CORPORATION
1144
WAKE STONE PROPERTY BROWNFIELDS D.B. 07, P . 13 6-13
B.M. 2007, PG. 1336-1338
COMPANY PROPERTY P.I.N. 1744-59-2979
D.B. 11171, PG, 719 BOUNDARY
B.M. 2015, PG. 381
P.I.N.1744-47-9970 30' CITY OF RALEIGH
RBF SANITARY SEWER
EASEMENT
SILVERPOINT DRIVE S 80°47,57"E 566.8B.M. 2021, PG. 1909-1910
� 2'
VARIABLE WIDTH
PRIVATE DRIVE I /- IPF
B.M. 2021, PG.1909-1910
10' CITY OF RALEIGH
WATER EASEMENT RBF RBF 20' DRAINAGE 20' DRAINAGE I -
B.M. 2021, PG.1909-1910 �'6 / EASEMENT o PRIVATE EASEMENT
C 78 RBF C� B.M. 2015, PG. 381 o I B.M. 2021, PG. 1909-1910
RBF Z I j I I I
I
20' DRAINAGE RBF Lag
EASEMENT 4, ��RBF
I I
TRACT 3
B.M. 2014, PG. 1734 / RBF 4 34 I
436 RBF RBF C5 I 9.290 ACRES I
RBF 820 I 404,663 S.F. I BROWNFIELDS
L33 RBF I B.M. 2021, PG. 1909-19101 810 I I PROPERTY
20' DRAINAGE I I I BOUNDARY
WAKE STONE CORPORATION Z I I VA IABLE WIDfTH I I N
D.B. 15868, PG. 543 PRIVATE CM ACCES
WAKE STONE PROPERTY I °'
B.M. 2015, PG. 381 COMPANY EASEMENT I I IEASEMENTI I Q
P.I.N. 1744-47-6292 D.B. 18371, PG. 719 B.M. 2014, PG. 1734 'o B.M.1021, PG. 19091r1910 I I Cl
/ B.M. 2015, PG. 381
P.I.N.1744-47-8471 I I a z
BROWNFIELDS I I o
PROPERTY T I I
50'PUBLICACCESS BOUNDARY -----' -----' /--� Z
AND CITY OF RALEIGH B' IPF \ \ JJ I
SANITARY SEWER IPF W/CAP /
EASEMENT 63.58' HINTON LAND, LLC
B.M. 2010, PG. 750 8°13'49 E 450.23' �/ - \ 1 CENTERLINE OF CREEK SCM-A D.B. 10147, PG. 682
N� L100 IS THE PROPERTY LINE BMB.M. 2021, PG. 890
30' KNIGHTDALE \ IPF
38g 65 'A B' L47-L100 .. 2021, PG. 1909-191 B.M. 2021, PG. 789
SANITARY SEWER I / \ � P.I.N. 1744-67-3392
EASEMENT No SEE o
D.B. 11722, PG. 1258 L29 � INSET'A' SCM-B
B.M. 2005, PG. 2418 a N \ B.M. 2021, PG. 1909-1910 TOCg
N_
r- r" \ \ TO°g 50' NEUSE RIVER BUFFER
°N° 0 50' NEUSE RIVER BUFFER SOIL FROM TOP OF CREEK BANK
o FROM TOP OF CREEK BANK DISPOSAL AREA BOTH SIDES
TRACT 4 I RBF BOTH SIDES 0.131 ACRES
1.103 ACRES N g, 5,706 S.F. �L182� L18B�186�18 18g
IPF
L1g LAB3 "� �e lL189 PF'.
48,064 S.F. \ 2 �2� \ /L178 119�L193�1g�191 \L190 \\ L47 A, !s/O L41 IPF jocb
B.M. 2021, PG. 1909-1910 6 / V m V19 , - 11.03' O --
8 >, �L176 �!� IPF jpGB o
\ \A L16 L196'' SOIL
\l I 11 L169 L197 DISPOSAL AREA \ \
30' KNIGHTDALE w on L19gS\E 1T4 , L171 L170 0.164 ACRES \
SANITARY SEWER Q' �--L173 540 7,143 S.F.
EASEMENT " ' ' \ ,
D.B. 11722, PG. 1258 \ S 87°2214 W 255.55; L26 \ ,,, TOTAL BROWNFIELDS \ RBF
B.M. 2005 PG. 2418 L23 \ 30' CITY OF RALEIGH `V43 ,
PROPERTY BOUNDARY AREA
' \ � L25 L21\\ \ \ SANITARY SEWER --'' / • . IPF
L24 \\ E_A�Faw�laf� 36.686ACRES -'\ IPF
L19 -B.IM 2021, PG. 1909-1910
L22 �� 1,598,051 S.F.
HINTON OAKS BLVD. \\ �, \ L20 IPF50,
R` 2 \ \ CENTERLINE OF CREEK
VARIABLE PUBLIC RM \ \ � 2 vf
B.M. 2015, PG. 381 \ °e
\ L18 \ \ IS THE PROPERTY LINE \
\ w L7-L26
B.M. 2010, PG. 750-751 / 50' NEUSE RIVER BUFFER
530 FROM TOP OF CREEK BANK
BROWNFIELDS BOTH SIDES
l
PROPERTY � �S \\ '''��
BOUNDARY \ \ \ L14 \\ TRACT \ \\
\ ,�- \ ,- 26.293ACRES\�L13 !�� \ \ \,�''� 1,145,324S.F.
VARIABLE WIDTH B.M. 2021, PG. 1909-1910 \\
20' PUBLIC \Ll l ho SCM ACCESS \\
DRAINAGE EASEMENT KNIGHTDALEVENTURES,L\ \ ly \ BM 2021, PG. ''-
////
B.M. 2015, PG. 1371 D. B. 18611, PG. 1667 \ \\ \ ,
B.M. 2015, PG. 970 \ NAD83 (2011)
P.I.N. 1744-46-9553 C8 !> ' N:746,361.86
E:2,146,479.3
\ HINTON POND ROAD IPF s 87°39'18" W
64' PUBLIC RM �s \ ,-''
B.M. 2015, PG. 1371 \
tx
/ RBF 10660
/ POND
G2 � 1016 42
\ L3 IPF IPF BROWNFIELDS
7.03 �� 1 �2 36gaz ` PROPERTY
PF BOUNDARY
IPF
REFERENCES:
MERRITT-MW1, LLC BBK MIDWAY PLANTATION, LLC
D.B. 18499, PG. 1796 \ D.B.17505, PG. 2670
B.M. 2021, PG. 1909-1910 \ TARGET CORPORATION B.M. 2006, PG. 129
B.M. 2015, PG. 970 \ D.B. 11438, PG. 1260 P.I.N. 1744-65-2987
B.M. 2015, PG. 381 \ B.M. 2005, -1127
B.M. 2010, PG. 750-751 P.I.N. 17445555-3762 \
B.M. 2014, PG. 1734-1736
P.I.N. 1744-56-6806
P.I.N. 1744-47-9093
P.I.N. 1744-47-6090
P.I.N. 1744-47-9612
MAP BASED ON SURVEY BY MCKIM &
CREED ENTITLED "ALTA/NSPS LAND
TITLE SURVEY PROPERTIES OF
CHARLES H. SILVER, JR. FOR MERRITT
PROPERTIES", DATED DECEMBER 15,
2019.
GRAPHIC SCALE
150' 0' 75' 150' 300'
1 INCH = 150 FEET
NOTES
1. NO NGS MONUMENT FOUND WITHIN 2,000 FEET OF THE SITE.
2. THE FOLLOWING INFORMATION WAS USED TO OBTAIN NC GRID NAD 83 (2011),
NAVD 88 (GEOID 12B) STATE PLANE COORDINATES (SPC) FOR THIS PROJECT:
2.1. CLASS OF SURVEY: URBAN LAND SURVEYS (CLASS A)
2.2. POSITIONAL ACCURACY: 0.03' (H), 0.07' (V)
2.3. GPS FIELD PROCEDURE: VRS
2.4. DATE OF SURVEY: 4-9-2021
2.5. DATUM/EPOCH: NAD 83 (2011), EPOCH 2O10.00
2.6. PUBLISHED DATE/FIXED CONTROL USED: VRS, NCRD
2.7. GEOID MODEL: GEOID 12B
2.8. COMBINED GRID FACTOR: 0.9999084473
2.9. UNITS: U.S. SURVEY FEET
2.10. GRID/GROUND POINT: Y(N) 746,620.70 X(E) 2,146,961.26
3. ALL DISTANCES ARE HORIZONTAL GROUND DISTANCES IN U.S. SURVEY FEET
UNLESS OTHERWISE NOTED.
4. ALL AREAS DERIVED BY THE COORDINATE COMPUTATION METHOD.
5. PROPERTY SUBJECT TO ALL EASEMENTS AND RESTRICTIONS OF RECORD. THIS
PLAT IS A CORRECT REPRESENTATION OF THE LAND PLATTED AND HAS BEEN
PREPARED IN CONFORMITY WITH NORTH CAROLINA STANDARDS, G.S. 47-30,
AND REQUIREMENTS OF LAW, BUT A NORTH CAROLINA LICENSED
ATTORNEY -AT -LAW SHOULD BE CONSULTED REGARDING CORRECT OWNERSHIP,
WIDTH, AND LOCATION OF EASEMENTS AND OTHER TITLE QUESTIONS
REVEALED BY TITLE EXAMINATION.
6. LINES NOT SURVEYED ARE SHOWN AS BROKEN LINES FROM INFORMATION
REFERENCED ON THE FACE OF THIS PLAT.
7. SUBJECT PROPERTY IS NOT LOCATED WITHIN A FLOOD HAZARD AREA
ACCORDING TO FLOOD INSURANCE RATE MAP 3720174400J DATED MAY, 02, 2006.
8. LOCATION OF UTILITIES, WHETHER PUBLIC OR PRIVATE, IS BASED UPON FIELD
LOCATION OF VISIBLE APPURTENANCES ONLY. IT IS THE CONTRACTOR'S
RESPONSIBILITY TO VERIFY LOCATION PRIOR TO COMMENCEMENT OF ANY
CONSTRUCTION. WITHERSRAVENEL CANNOT ASSUME RESPONSIBILITY FOR
MISIDENTIFICATION OR OMISSION OF UNDERGROUND UTILITIES.
9. SCM MAINTENANCE & ACCESS EASEMENT GRANTS TOWN OF KNIGHTDALE
ENTRY\ACCESS FOR INSPECTIONS AND SHOULD THERE BE AN ISSUE, FAILURE
EMERGENCE, ECT. OTHERWISE, BOTH THE EASEMENT AND SCM DEVICE ARE
TO BE MAINTAINED BY THE PROPERTY OWNER/DEVELOPER/OWNERS
ASSOCIATION.
BROWNFIELDS
PROPERTY
BOUNDARY
HINTON LAND, LLC
D.B. 10147, PG. 682
6; P.I.N.1744-66-6722
289.85'
IPF
PF _ �c,
IPF
40' PRIVATE ACCESS
EASEMENT
D.B. 11401, PG. 2634
D.B.11401, PG.2644
B.M. 2005, PG. 1125
HD DEVELOPMENT OF
MARYLAND, INC.
D.B.12800, PG.2729
B.M. 2005, PG. 1125-1128
P.I.N. 1744-66-8147
LEGEND
STREET ADDRESS 123
(IPF)-IRON PIPE FOUND
(IPF)-IRON PIPE SET
(RBF)-REBAR FOUND
(TOCB)-TOP OF CREEK BANK
(TOK)-TOWN OF KNIGHTDALE
BOUNDARY
BOUNDARY LINE NOT SURVEYED
FUTURE BUILDING LOCATION - - - - - - - - - - - - - - - - - - - - - - - - -
CENTERLINE - -
EASEMENT - -
POND
RIGHT OF WAY - - - -
RIPARIAN BUFFER
WETLAND SOIL DISPOSAL AREA

LINE TABLE
CURVE TABLE
LINE #
BEARING
DISTANCE
LINE #
BEARING
DISTANCE
LINE #
BEARING
DISTANCE
L1
N 18°28'49" W
87.75'
L71
S 87°27'27" W
19.26'
L141
S 72'1353" E
13.63'
L2
S 71 °29'20" W
167.99'
L72
S 42'35'11" W
10.89'
L142
S 17°46'07" W
10.00'
L3
N 71°35'09" E
107.11'
L73
N 85°21'03" W
21.76'
L143
N 72'13'53" W
13.63'
L4
N 53'28'19" E
60.58'
L74
N 57°38'51" W
21.00'
L143
INTENTIONALLY DELETED
L5
N 36°24'23" W
94.07'
L75
N 56'02'15" W
3.02'
L145
S 33°57'36" W
129.86'
L6
N 36'50'18" E
56.90'
L76
S 35°32'04" W
19.96'
L146
S 37'33'13" E
40.96'
L7
N 51 °14'00" W
39.74'
L77
N 75°32'27" W
18.26'
L147
N 89°56'29" E
152.40'
L8
N 68'03'19" W
21.10'
L78
S 72'1622" W
13.18'
L148
N 87°22'14" E
148.02'
L9
N 33°22'37" W
57.07'
L79
S 72°25'39" W
16.15'
L149
S 02°37'46" E
30.00'
L10
N 55°06'23" W
31.59'
L80
N 75°52'05" W
24.04'
L150
S 87°22'14" W
78.58'
L11
N 29°37'45" W
31.22'
L81
S 54°01'44" W
4.96'
L151
S 87°22'14" W
70.11'
L12
N 42°05'39" W
40.26'
L82
N 78°27'46" W
21.55'
L152
S 89°56'29" W
163.07'
L13
N 47°55'04" W
21.23'
L83
N 53°02'06" W
21.80'
L153
N 13°30'20" W
64.26'
L14
N 25°49'04" W
35.75'
L84
N 67°43'57" W
24.93'
L154
N 90°00'00" E
322.00'
L15
N 53'05'13" W
29.35'
L85
N 84°41'06" W
17.73'
L155
S 89°51'05" E
19.77'
L16
N 34'19'16" W
55.43'
L86
N 02°05'23" E
23.26'
L156
S 89'19'19" W
338.02'
L17
N 07°18'37" E
47.37'
L87
N 62°40'01" W
16.63'
L157
N 00°00'00" W
98.80'
L18
N 59°38'35" W
4.14'
L88
N 59°05'29" W
32.03'
L158
N 81 °03'56" W
257.31'
L19
N 48'1326" W
22.39'
L89
N 71 °50'30" W
20.86'
L159
N 72'18'19" W
99.38'
L20
N 17°58'02" W
32.32'
L90
N 85°25'46" W
27.51'
L160
S 33°20'48" E
83.17'
L21
N 88'1820" W
22.79'
L91
N 16°36'22" W
24.28'
L161
S 34°29'49" E
18.51'
L22
N 36°48'56" W
26.77'
L92
N 29'11'54" E
30.43'
L162
S 53°31'07" W
126.51'
L23
N 55°2841" W
17.46'
L93
N 25°08'24" W
2.88'
L163
N 53°31'07" E
71.23'
L24
N 13'14'07" W
20.87'
L94
N 65°22'24" W
10.01'
L164
N 38°20'21" W
210.79'
L25
N 36°58'57" W
22.31'
L95
N 35°12'01" W
11.09'
L165
N 75°29'51" E
323.54'
L26
N 04°01'27" E
20.36'
L96
N 64°54'09" W
18.48'
L166
N 14°30'09" W
12.50'
L27
N 04°31'22" W
116.88'
L97
S 30°20'44" W
12.40'
L167
S 75°07'54" W
332.50'
L28
N 04°31'22" W
91.74'
L98
N 85°14'00" W
22.91'
L168
S 31 °4V31" E
52.11'
L29
N 86°08'37" E
24.88'
L99
N 40°03'49" W
28.93'
L169
S 72°32'24" W
11.63'
L30
N 35°18'33" E
87.13'
L100
N 16°16'31" W
0.83'
L170
S 72°40'03" W
12.16'
L31
N 11 °16'22" W
13.55'
L101
S 72'18" 9" E
99.35'
L171
S 75'11,33" W
25.00'
L32
N 77°39'25" E
14.54'
L102
S 81 °03'56" E
305.62'
L172
S 78°42'51" W
24.01'
L33
N 80'48'12" W
216.61'
L103
S 00°00'00" E
147.11'
L173
S 77'22'11" W
24.89'
L34
N 72°14'48" W
69.97'
L104
N 85°23'59" W
77.18'
L174
S 79°06'25" W
29.78'
L35
S 17°47'02" W
30.00'
L105
N 88°54'47" W
88.17'
L175
N 07'38'10" W
35.76'
L36
N 72'1321" W
29.98'
L106
S 84°07'28" W
29.81'
L176
N 69°48'53" E
14.82'
L37
N 17°45'59" E
113.99'
L107
S 42°07'31" W
27.00'
L177
N 66°26'49" E
13.34'
L38
S 72'16'12" E
79.98'
L108
N 47°52'29" W
16.00'
L178
N 47°13'13" E
27.28'
L39
S 80°47'01" E
257.42'
L109
N 42°07'31" E
27.00'
L179
N 72°46'22" E
15.00'
L40
S 49°08'07" E
55.08'
L110
N 89°11'00" E
355.05'
L180
N 83°21'13" E
41.12'
L41
S 86°26'22" E
179.20'
1-111
N 90°00'00" W
8.85'
L181
N 74°22'27" E
21.32'
L42
S 44°5V31" E
261.69'
L112
N 88°45'02" E
64.92'
L182
N 76°59'11" E
12.20'
L43
N 73°21'17" E
185.98'
L113
N 27°01'35" E
27.86'
L183
N 80°03'45" E
43.32'
L44
S l8o03'22" E
42.51'
L114
S 62°58'25" E
22.87'
L184
N 81 °00'45" E
38.37'
L45
S 69°31'44" W
20.04'
L115
S 24°56'35" W
25.67'
L185
N 77°58'28" E
39.94'
L46
S 00°03'41" W
77.61'
L116
S 54°14'14" E
51.54'
L186
N W39'05" E
52.81'
L47
N 76°13'14" W
7.86'
L117
S 48°03'00" E
56.46'
L187
N 85°25'54" E
20.35'
L48
S 60°38'32" W
9.66'
L118
S 64°54'00" E
56.14'
L188
S 72°55'29" E
22.06'
L49
N 42°57'39" W
18.42'
L119
S 57°21'09" E
96.93'
L189
S 16'1645" W
9.58'
L50
N 14°31'17" E
9.65'
L120
S 52°01'36" E
35.10'
L190
S 73'27'12" W
19.39'
L51
N 71 °34'51" W
2.72'
L121
N 75°29'51" E
34.15'
L191
S 79°59'45" W
19.56'
L52
S 82°39'20" W
13.03'
L122
S W30'09" E
24.50'
L192
S 73°44'59" W
52.61'
L53
N 43°57'08" W
12.36'
L123
S 75°29'51" W
319.07'
L193
S 77°33'00" W
35.91'
L54
N 37°25'00" W
5.22'
L124
S W20'21" E
178.46'
L194
S 73°04'48" W
37.45'
L55
N 80'1356" W
17.70'
L125
S 81°09'56" W
42.45'
L195
S 74°40'55" W
33.19'
L56
N 25°20'59" W
17.70'
L126
N 52°21'55" W
85.41'
L196
S 77°3121" W
20.03'
L57
N 18°57'14" E
7.62'
L127
N 48'50'10" W
45.67'
L197
S 70'19'55" W
16.97'
L58
N 22'30'19" E
3.02'
L128
N 51 °52'49" W
43.02'
L198
N 23°53'05" W
39.67'
L59
N 56°42'43" W
2.04'
L129
N 12°24'23" W
62.95'
L199
N 74'1012" E
175.21'
L60
S 82°33'05" W
13.49'
L130
S 75°03'26" E
68.36'
L200
N 64°21'54" E
58.54'
L61
N 41'39'15" W
36.78'
L131
S 79°14'50" E
331.02'
L62
N 34°36'58" W
23.17'
L132
N 80'57'13" E
36.82'
L63
N 82'10'51" W
8.26'
L133
N 00°08'53" W
189.98'
L64
N 80°10'00" W
10.99'
L134
N 89°42'35" E
65.92'
L65
N 36°26'44" W
8.51'
L135
N 67°08'31" E
40.95'
L66
N 56°16'20" W
1.16'
L136
S 80°47'22" E
358.21'
L67
N 88'1502" W
3.70'
L137
S 00°00'00" E
302.52'
L68
S 55°35'25" W
31.46'
L138
N 90°00'00" E
65.57'
L69
N 77°21'15" W
32.69'
L139
N 16°58'50" E
1 110.34'
L70
I N 38°33'59" W
14.92'
L140
S 83°24'44" E
1 103.57'
N
RE
A CA R Ol°O °
0
00,
o,,0000000
SS °ooy
ID '�°o
I IN -o
PLA
T"
ONCE,
SALES
CURVE #
RADIUS
ARC LEN.
CHORD BRG.
CHORD LEN.
Cl
25.00'
39.70'
N 25°59'30" E
35.66'
C2
531.90'
167.72'
N 62°33'08" E
167.03'
C3
496.00'
103.83'
N 10'31'12" W
103.64'
C4
496.00'
2.28'
N 04°23'29" W
2.28'
C5
332.00'
49.41'
N 76°30'07" W
49.36'
C6
20.00'
31.41'
S 2713'53" E
28.28'
C7
268.00'
39.96'
S 76°30'07" E
39.92'
C8
38.50'
61.72'
N 07°35'23" E
55.32'
C9
971.50'
417.55'
N 24°43'04" W
414.34'
C10
50.00'
53.87'
S 64°49'22" W
51.30'
C11
80.17'
66.65'
N 73'1333" W
64.74'
C12
54.96'
40.65'
N 38°27'42" W
39.73'
C13
150.35'
39.46'
N 08°32'36" W
39.34'
C14
236.08'
42.52'
N 85°52'28" E
42.46'
C15
140.48'
40.52'
S 80°45'06" E
40.38'
C16
245.60'
40.49'
S 56°56'40" E
40.44'
C17
18.00'
28.27'
S 59°30'09" E
25.46'
C18
8.00'
12.57'
N 59°30'09" W
11.31'
C19
107.66'
49.73'
N 25°39'53" W
49.29'
C20
62.72'
103.82'
N 33°45'59" E
92.37'
C21
948.50'
388.23'
S 25'1720" E
385.53'
C22
288.50'
44.11'
S 76°41'07" E
44.07'
C23
93.50'
146.87'
S 45°00'00" E
132.23'
C24
23.50'
28.75'
N 54°57'05" E
26.99'
C25
15.00'
32.45'
S 28°01'12" E
26.48'
C26
35.33'
53.49'
N 46°37'22" E
48.53'
C27
26.50'
39.62'
S 47°09'51" W
36.03'
C28
116.50'
183.00'
N 45°00'00" W
164.76'
C29
33.50'
47.40'
N 40°31'58" W
43.54'
C30
311.50'
47.63'
N 76°41'07" W
47.58'

Appendix VI— Waste Manifests

-"I
EZ ProfileTm
Requested Facility: CY" - 6. (C LG.'iC, II ❑ Unsure Profile Number:
❑ Multiple Generator Locations (Attach Locations) ❑ Request Certificate of Disposal ❑ Renewal? Original Profile Number:
A. GENERATOR INFORMATION (MATERIAL ORIGIN)
I. Generator Name: #71"�TT MW-l1 LLL
2.GeneratorSiteAddress: /Z; HATOA 04KY Rw9
(City, State, ZIP) KHrr.nrp T� Z'1$,1/5-
3. County: WA'IrE
4. Contact Name: Z4rH W if i
5. Email: zdtiEiT'E'M6dZ2C."n
6. Phone: 115 - 1'L(0- 00i O 7, Fax:
B. Generator EPA ID: ❑ N/A
9. State ID: ❑ N/A
C. MATERIAL INFORMATION I /
1. Common Name: bier)- ka o v (-�t,L)5 V&e Live d�11(Y 5 1-
Describe Process(es) Generating Material: ❑ See Attached
ww�+va.l oP RdLntl3t..!/S for t- ev�loPNtuti-
a�- i�'rfvv� 6�t.t>tg�
2. Material Composition and Contaminants: ❑ See Attached
1.
592
-/pD o
3.
4.
Total comp. must be equal to or greater than 100%
Z0 00%
3. State Waste Codes: 43-N/A
4. Color: UadA
5. Physical State at 707: &Solid ❑ Liquid ❑ Other: �-
6. Free Liquid Range Percentage: to t7 N/A
7. pH: to IJ�N/A
8. Strong Odor: ❑ Yes a No Describe:
9. Flash Point: CI <140'F ❑ 140'-199'F ❑ z200' N/A
B. BILLING INFORMATION p SAME AS GENERATOR
1. Billing Name: ' .,
2. Billing Address: Laoc r
(City, State, ZIP) r
3. Contact Name: - rN
4. Email:
5. Phone: - 6. Fax:
7. WM Hauled?
❑ Yes
*0
8. P.O. Number:
9. Payment Method: [$Credit Account ❑ Cash ❑
Credit Card
D, REGULATORY INFORMATION
1. EPA Hazardous Waste?
❑ Yes*
Jd No
Code:
2. State Hazardous Waste?
❑ Yes
No
Code:
3. Is this material non -hazardous due to Treatment,
❑ Yes*
6o
Delisting, or an Exclusion?
4. Contains Underlying Hazardous Constituents?
❑ Yes*
91 No
5. From an industry regulated under Benzene NESHAP?
❑ Yes*
m o
6. Facility remediation subject to 40 CFR 63 1GGGG7
❑Yes*o
7. CERCLA or State -mandated clean-up?
❑ Yes*
�o
B. NRC or State -regulated radioactive or NORM waste?
I] Yes*
1
VJ No
*If Yes, see Addendum (page 2) for additional questions and
space.
9. Contains PCBs? 4 If Yes, answer a, b and c.
❑ Yes
0No
a. Regulated by 40 CFR 761?
❑ Yes
LINO
b. Remediation under 40 CFR 761,61 (a)?
❑ Yes
❑ No
c. Were PCB imported into the US?
❑ Yes
❑ No
10. Regulated and/or Untreated
❑ Yes
F(No
Medical/Infectious Waste?
11. Contains Asbestos?
❑ Yes
IKNo
� If Yes: ❑ Non -Friable ❑ Non -Friable - Regulated
❑
Friable
E. ANALYTICAL AND OTHER REPRESENTATIVE INFORMATION / F. SHIPPING AND DOT INFORMATION
1. Analytical attached Or Yea 1. $,One -Time Event ❑ Repeat Event/1Ongoing Business
Please identify applicable samples and/or lab reports: 2. Estimated Quantity/Unit of Measure:, �& 23V
t,o "otp.+ol-i 6, Plo r r-T M Ito I Lt °pl jons ❑ Yards ❑ Drums ❑ Gallons ❑ Other:
L.. _ I TD _ ' ( !� 415 3. Container Type and Size:
�j 4. USDOT Proper Shipping Name: WrN/A
2. Other information attached (such as MSDS)? O Yes
G. GENERATOR CERTIFICATION (PLEASE READ AND CERTIFY BY SIGNATURE)
By signing this EZ Profile"' form, I hereby certify that all information submitted in this and all attached documents contain true and accurate descriptions of this material, and that
all relevant information necessary for proper material characterization and to identify known and suspected hazards has been provided. Any analytical data attached was derived
from a sample that is representative as defined in 40 CFR 261 - Appendix 1 or by using an equivalent method. All changes occurring in the character of the material (i.e., changes
in the process or new analytical) will be identified by the Generator and be disclosed to Waste Management prior to providing the material to Waste Management.
❑ I am an Authorized Agent signing on behalf of the Generator, and I have
confirmed with the Generator that Information contained in this profile, ps well
as supportin 1ocu nisrtprovided are accurate and complete. / /
Name (Print): I`t-I rK Date: 9 ?I 4
Title: Vrslprslr</
,1i.L�1��
Company: M6UZJTi- AAW 1, f,.LG
THINK GREEN:
Certification Signature
QUESTIONS? CALL 800 963 4776 FOR ASSISTANCE Revised November 06.20200 202O WM Intellectual Property Holdings. L.L.C.