7401_PittCounty_SouthernUnit_MSWLF_July22GW_FID1742603_20221108

tiNft USE ONLY ❑Paper Repon DElectronic Data - Email CD (data loaded: Yes / No) Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste
Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NG General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
Condition, etc.).
Attach a notification table of any groundwater or sur€ace water values (hat equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NGIDENR-DWM. Solid Waste
Section. 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information _
Name of entity submitting data (laboratory, consultant, facility owner):
Groundwater Management Associates, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Codv J. Shell P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g..
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20.24, 2006)
out hem Unit of the Pitt County 31125 Landfill Road 74-01 1600 July 19-20. 2022
Municipal Solid Waste Landfill Greenville, NC 27834
Environmental Status: (Check all that apply)
❑ InitiauBackground Monitoring ❑ Detection Monitoring Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data
Surface water monitoring data ❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
j{ Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 26 surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points. dates. sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, i have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Cody J. Shell, P.G. Project Hydrogeologist 252-758-3310
Facility Representative Name (Print) Tikle (Area Code) Telephone Number
Affix NC Licensed/ ',fp C X, OZOP't Seal
• J-{ �.
Co
yes � ^"`""...�..•'
1*41140 A/Iliµf�µ�►
ifff/K*K
Signature ) J a Date
4300 Sapphire Court, Suite 100, Greenville, NC 27834
Facility Representative Address
G-121 (PG Firm License Number)
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 612009

Compounds Detected At or Above Regulatory Standards during the July 2022 Sampling Event
(7/19-20/2022) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(N9/L)
MDL
(N9/L)
NC 2L or 2B
Std* (N9/L)
IMAC
(N9/L)
MCL
(N9/L)
Groundwater Samples
MW6R
7/20/2022
1,4-Dioxane
7
0.80
3
-
-
7/20/2022
Barium Total
2010
1.10
700
-
2000
P11R
7/19/2022
Cobalt Total
5.983
1.40
1
-
-
7/19/2022
Vanadium Total
10.9
1.40
7
-
-
7/19/2022
1,4-Dioxane
83 D
4.0
3
-
-
7/20/2022
Barium Total
1090
1.10
700
-
2000
P16R
7/19/2022
Benzene
3
0.15
1
-
5
7/20/2022
Cobalt Total
2.673
1.40
1
-
-
7/20/2022
1,4-Dioxane
3.9
0.80
3
-
-
P17
7/20/2022
Cobalt Total
1.401
1.40
1
-
-
7/20/2022
1,4-Dichlorobenzene
6.3
0.19
6
-
75
7/20/2022
1,4-Dioxane
160 D
4.0
3
-
-
7/20/2022
Barium Total
1970
1.10
700
-
2000
P19
7/20/2022
Benzene
4.2
0.15
1
-
5
7/20/2022
Beryllium Total
14.4
0.160
4
-
4
7/20/2022
Cobalt Total
18.3
1.40
1
-
-
7/20/2022
Mercury Total
1.06
0.150
1
-
2
7/20/2022
Vinyl Chloride
0.751
0.32
0.03
-
2
7/19/2022
1,4-Dioxane
79 D
4.0
3
-
-
P20R
7/20/2022
Barium Total
842
1.10
700
-
2000
7/19/2022
Benzene
2.2
0.15
1
-
5
7/20/2022
Cobalt Total
2.84 J
1.40
1
-
-
7/20/2022
Beryllium Total
7.96
0.160
4
-
4
P2OD
7/20/2022
Cobalt Total
2.403
1.40
1
-
-
7/20/2022
Vanadium Total
9.793
1.40
7
-
-
P28
7/20/2022
Cobalt Total
1.823
1.400
1
-
-
7/19/2022
1,4-Dioxane
140 D
4.0
3
-
-
P29
7/19/2022
Benzene Total
2.0
0.15
1
-
5
7/20/2022
Vanadium Total
9.163
1.40
7
-
-
QA/QC Samples
Fj
FB 7/20/2022 ICobalt Total 1.433 1 1.4
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
J = The analyte was positively identified, but the value is estimated below the reporting limit.
water sampling locations (SWI and SW2).
#Value represents an EPA secondary Maximum Contaminant Level
"Hardness -dependent metal standard calculated assuming an in -stream hardness of 25 mg/L of CaCO3.
Concentrations highlighted in yellow were detected above the 2L (or 26) standards.
Concentrations highlighted in orange were detected above the IMAC.
Page 1 of 2

Compounds Detected At or Above Regulatory Standards during the July 2022 Sampling Event
(7/19-20/2022) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Preliminary analysis of cause and significance of concentrations detected at or above
groundwater or surface water standards:
1,4-Dioxane, benezene, and barium were detected at concentrations exceeding the 15A NCAC 02L
groundwater standard in multiple wells. However, these constituents were not detected at concentrations
above state standards in groundwater samples collected from just below the southern property ditch, or in
downgradient surface -water samples. These results suggest that these 1,4-dioxane, benzene, and
concentrations in excess of naturally occurring barium are not migrating off -site at this time. Further,
benzene was not detected in the sample collected from the deep monitoring well located down -gradient of
the Southern Landfill Unit (P20D). Barium was detected in this well, but the concentration (99.7 ug/L) was
well below the NCAC 02L standard and below concentrations detected in upgradient, off -site monitoring
wells. The absence of these target compounds indicates that benzene and non-native barium have not
migrated out of the Surficial/Yorktown Aquifer at the site. 1,4-Dioxane was detected in groundwater
samples collected from well P20D for the first time. The detection of this contaminant in well P20D
warrants further investigation during the next sampling event.
The detection of 1,4-dioxane and other contaminants in well P29, which is located between the Northern
and Southern Landfill Units, indicates that the Northern Unit is likely also a source for these contaminants.
Pitt County recently completed substantial cap and stormwater repairs and upgrades at the Southern Unit.
These repairs were designed to limit the infiltration of rainwater into the Southern mound and reduce
leachate volume and concentrations.
Vinyl chloride, 1,4-dichlorobenzene, and mercury (Appendix II) were also detected above the 15A NCAC
02L standards in well P19. The completed cap and stormwater upgrades are expected to reduce the
concentrations of all contaminants in groundwater downgradient of the Southern Unit. Thus, these
Page 2 of 2

PILOT STUDY UPDATE AND
JULY 2022 SEMI-ANNUAL WATER
QUALITY MONITORING EVENT
SOUTHERN PORTION OF THE
PITT COUNTY SOLID WASTE
MUNICIPAL LANDFILL
(FACILITY PERMIT # 74-01)
GREENVILLE, PITT COUNTY
PREPARED FOR
MR. TIM CORLEY, PE
ENGINEERING DEPARTMENT
PITT COUNTY
1717 WEST 5T" STREET
GREENVILLE, NC 27834
PREPARED BY
GROUNDWATER MANAGEMENT
ASSOCIATES, INC. (GMA)
4300 SAPPHIRE CT., SUITE 100
GREENVILLE, NORTH CAROLINA 27834
TELEPHONE: (2S2) 7S8-3310
NOVEMBER 7, 2022
North Carolina Corporate Engineering License (GMA —Apex, NC) #: C-0854
North Carolina Corporate Geology License (GMA — Greenville & Apex, NC) #: C-121

TABLE OF CONTENTS
1.0 INTRODUCTION..................................................................................... 1
1.1 Site Background.................................................................................. 2
1.2 Physical Setting and Hydrogeology..................................................... 2
1.3 Contaminants of Concern and Site Regulatory Status ........................ 3
2.0 1,4-DIOXANE ASSESSMENT AND PILOT STUDY UPDATE ....................... 5
3.0 JULY 2022 SEMI-ANNUAL MONITORING EVENT ................................... 7
3.1 Groundwater Hydrology.................................................................... 8
3.2 Sample Collection and Analyses........................................................ 9
3.3 Analytical Results and Discussion...................................................... 9
3.3.1 Field Quality Assurance/Quality Control Samples.....................................11
4.0 WATER LEVELS AND CONTAMINANTS THROUGH TIME ....................... 12
5.0 CONCLUSIONS AND FUTURE WORK .................................................... 12
6.0 REPORT CERTIFICATION..................................................................... 14
7.0 REFERENCES........................................................................................15
FIGURES
1. Site Layout and Existing Monitoring Network
2. Groundwater and Surface Water Sampling Locations - Southern Unit
3. Equipotential Map, July 19, 2022
4. Water Levels Through Time in Well P16R and Staff Gage SG3
5. Contaminant Concentrations Through Time in Well MW6R
6. Contaminant Concentrations Through Time in Well P20R
TABLES
1. Monitoring Well Construction and Elevations
2. Monitoring Well Water Levels and Sample Purge Volumes
3. Staff Gauge Elevations and Water Levels
4. Calculations of Groundwater Velocity
5. Field -Water Quality Parameters
6. Appendix I Target Parameters
7. Appendix II Target Parameters
8. List of Compounds Detected during the July 2022 Sampling Event

APPENDICES
Correspondence from the NC Division of Waste Management
Sampling Records
Laboratory Report and Chain -of -Custody Forms for Water Samples

1.0 INTRODUCTION
The inactive Pitt County Solid Waste Municipal Landfill (Facility Permit #74-01, Figure 1) is
comprised of a Northern Unit that closed in 1990 and a Southern Unit that reached capacity and
closed in 1995. Based on its closure date, the Southern Unit is subject to the September 1993
rules for municipal solid waste landfills (15A NCAC 13B .1600). The Northern Unit, on the other
hand, is subject to the conditions of the solid waste permit and 15A NCAC 13B .0500.
Pitt County (the County) is currently working to address 1,4-dioxane and benzene groundwater
contamination at the Southern Unit of the inactive Pitt County Solid Waste Municipal Landfill
(Facility Permit #74-01, Figure 1). In 2017, the County confirmed slight exceedances of the NC
Groundwater Quality Standard (NCAC 02L) for benzene in two groundwater samples collected
from the landfill's monitoring well network. Exceedances of the NCAC 02L groundwater
standard for 1,4-dioxane were confirmed in January 2019. Testing for 1,4-dioxane began in
response to a May 2018 directive from the North Carolina Department of Environmental Quality
(NCDEQ), Division of Waste Management (DWM), Solid Waste Section (SWS) that required all
North Carolina landfills to begin testing for the constituent as part of their routine groundwater
monitoring (Appendix A).
Groundwater contamination at the facility is believed to be related to the degradation of the
low -permeability, clay caps that cover each unit. Over time, erosion of the caps, as well as
cracking due to heating/cooling, desiccation, and/or subsidence due to decomposition of fill
material, increases the permeability of these barriers and allows infiltration of water that can
leach contaminants downward into the underlying groundwater.
Following approval from the SWS, the County has collected groundwater samples from just
beneath the southern ditch to monitor the extent of 1,4-dioxane and benzene contamination at
the facility. This ditch serves as a groundwater discharge location for the Southern Unit. To
date, 1,4-dioxane and benzene have not been detected in exceedance of the NCAC 02L
standards in these samples, which suggests that 1,4-dioxane and benzene contamination above
the NCAC 02L groundwater standard does not extend off the facility property.
On November 4, 2020, the County began construction on an extensive cap and a stormwater
system repair and upgrade project at the Southern Unit as part of an approved pilot study for
corrective action (Appendix A). These improvements are designed to greatly reduce the
infiltration of water through the cap in order to protect the groundwater from further
contamination via leaching from landfill waste. The County completed construction on
this $1.065 million project in June of 2021. The County continues to monitor groundwater and
surface water at the Southern Unit on a semi-annual schedule. The remainder of this report
presents the results of the July 2022 semi-annual monitoring event and provides an update of
the ongoing pilot study at the Southern Unit of the Pitt County Landfill.

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 2 of 16
1.1 Site Background
The Pitt County Landfill occupies approximately 156 acres along Allen Road west of the city of
Greenville, NC (Figure 1). The landfill is comprised of a Northern Unit that closed in 1990 and a
Southern Unit that reached capacity in 1995. An east -west trending railroad (Norfolk Southern
Railroad) separates the Northern and Southern Units. The Pitt County landfill is unlined, and
leachate is not collected. The Northern Unit received waste from 1974 until 1990, and the
Southern Unit received waste from 1991 until 1995. Due to the closure dates, only the
Southern Unit is subject to the September 1993 rules for municipal solid waste landfills (15A
NCAC 13B .1600). Pitt County monitors the Northern Unit in accordance with the conditions of
the solid waste permit and 15A NCAC 13B .0500.
1.2 Physical Setting and Hydrogeology
The Pitt County Landfill lies in the central portion of the Coastal Plain Physiographic Province of
North Carolina where Cretaceous to Recent age Coastal Plain sedimentary formations overlie
Mesozoic and older basement bedrock (Horton and Zullo, 1991). Coastal Plain sediments and
sedimentary rocks have significant variations in permeability and water -producing capabilities.
High -permeability strata that readily produce usable quantities of water are aquifers, and low -
permeability sediments that restrict the movement of groundwater, either into or out of
aquifers, are confining beds. Coastal Plain aquifers typically use the predominant geologic
formation name that is associated with the aquifer. The two uppermost aquifers at the Pitt
County Landfill are: the unconfined Surficial/Yorktown aquifer and the confined Peedee Aquifer.
The Surficial/Yorktown Aquifer is locally composed of fossiliferous clays and sands. The clays
within the unit tend to serve as confining layers and restrict recharge to underlying aquifers
(GMA and McGill, 2001). The Peedee Aquifer consists of unconsolidated sands and sandstones
of the of Late Cretaceous age Peedee Formation (Winner & Coble, 1996). In the western half
of Pitt County, the Peedee Aquifer lies directly beneath the Surficial/Yorktown Aquifer, and the
elevation of the top of the Peedee Aquifer is above sea level (GMA and McGill, 2001).
A detailed description of the local site hydrogeology is provided in the Water Quality Monitoring
Plan for the Southern Unit (GMA, 1994). In general, a sandy clay extends from the original land
surface beneath the landfill to varying depths of 6 to 13 feet. A portion of this clay may have
been excavated from adjacent to the Southern Unit mound and used as part of the clay cap for
the mound. Coarser, more permeable sediments (silty fine sand, clayey sand, and very clayey
sand) typically exist at depths of 10 to 16 feet. Underlying these more permeable sediments, at
a depth of approximately 16 feet below the original land surface, is a thin, discontinuous, dark
gray clay that ranges from 0.5 to 3.0 feet in thickness, with an average thickness of 1 foot.
This clay layer exists at an elevation of approximately 66 feet above mean sea level and has
previously been referred to as the "66-foot clay" (GMA, 1994). Below this clay layer lie silty,
fine sands. During the installation of deep monitoring well P20D, GMA observed a silty, clay
layer from approximately 45 to 48 feet below the land surface. Below this clay layer, GMA

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 3 of 16
observed a fine, phosphatic sand. GMA believes the deepest on -site monitoring wells (e.g.
MW1R, MW3, and P20D) may penetrate the top of the Peedee Aquifer, which is estimated to be
about 25 feet thick at the location of the landfill (GMA and McGill, 2001). We provide a general
summary of the stratigraphy below.
Average depth of strata relative
to original land surface (feet)
Lithology
0 — 9.5
sandy clay
9.5 — 16
silty fine sand, clayey sand, and very clayey sand
16 — 17
dark gray clay
17 — 45
silty, fine sand
45 — 48
silty, clay
48 — 60+
fine, phosphatic sand
1.3 Contaminants of Concern and Site Regulatory Status
As described in the introduction, the Southern Unit of the Pitt County Landfill is currently under
assessment for low-level exceedances of the NC Groundwater Quality Standard (NCAC 02L) for
benzene. The County first confirmed a slight exceedance of the NCAC 02L groundwater
standard for benzene in 2017. Since that time and following approval from the NCDEQ, DWM,
SWS, the County has collected groundwater samples from just beneath the southern ditch to
monitor the extent of benzene contamination at the facility. This ditch serves as the
groundwater discharge location for the Surficial Aquifer at Southern Unit. To date, the County
has not detected benzene in exceedance of the NCAC 02L standard in these samples, which
suggests that benzene contamination above the NCAC 02L groundwater standard does not
extend off the facility property.
Pitt County is also currently assessing the Southern Landfill Unit for exceedances of the NCAC
02L standard for 1,4-dioxane. In May 2018, the NCDEQ DWM SWS directed all North Carolina
landfills to begin testing for 1,4-dioxane as part of their routine groundwater monitoring. 1,4-
Dioxane is used primarily as a chlorinated solvent stabilizer, but it can also be found in paint
strippers, varnishes, waxes, and a variety of consumer products (USEPA, 2014a). 1,4-Dioxane
is fully miscible in water, and it migrates readily with groundwater. This compound is short-
lived in the atmosphere, but it does not volatilize rapidly from water.
1,4-Dioxane was detected at the landfill in July 2019, and the County immediately and
voluntarily chose to perform an updated potential receptor investigation to determine if any
water -supply wells might be at risk. Pitt County opted to conduct the potential receptor survey
as a proactive measure in the interest of public health. The updated potential receptor survey,
conducted by GMA in September 2018, did not identify any well being used as a drinking water
source within 2,000 feet of the facility (GMA, 2018).

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 4 of 16
Exceedances of the NCAC 02L groundwater standard for 1,4-dioxane were confirmed at the
Southern Unit of the Pitt County Landfill in January 2019. GMA suspects that the detection of
1,4-dioxane in multiple monitoring wells adjacent to the Southern Landfill Unit relates to
degradation of the integrity of one or both landfill caps and the stormwater drainage systems
designed to quickly shunt surface water off the landfill mounds. Pitt County emplaced the clay
caps above the Landfill in the mid-1990s. Over time, erosion of the cap, as well as cracking due
to heating/cooling, desiccation, and/or subsidence due to decomposition of fill material, can
increase the permeability of this type of barrier. Cap degradation has likely allowed infiltration
of water that has leached contaminants downward into the underlying groundwater.
Eliminating infiltration of water through the cap, and ensuring that the stormwater conveyance
system operates as designed, are primary goals for reducing, or eliminating, the release of
additional contaminants into the groundwater.
GMA, on behalf of the County, submitted a proposal to the SWS on June 21, 2019 to further
assess and address 1,4-dioxane contamination at the landfill. Specifically, we proposed to:
1) Delineate the vertical and horizontal extents of 1,4-dioxane by installing two additional
groundwater monitoring wells (one Type II monitoring well located between the two landfill
units and one double -cased, deep Type III monitoring well south of the Southern Mound)
and six surface water staff gauges.
2) Conduct a pilot study to document and establish the effectiveness of cap upgrades and
repairs to limit the infiltration of rainwater through the soil cap, and to evaluate if the
repairs have reduced leachate volumes and contaminant concentrations. During the pilot
study, the County proposed to:
a) conduct geophysical testing of the Southern Unit to evaluate landfill cap integrity,
b) repair any areas of concern identified by the geophysical testing,
c) inspect surface water drainage structures on the mound to ensure that they are
operating as designed, and then
d) repeat geophysical testing after cap repairs are made to document the results of the
cap repairs.
3) Install two in -stream piezometers approximately 1.5 feet below the ditch bottom at the
locations of the currently collected porewater samples. The in -stream piezometers provide
repeatable locations to collect representative groundwater samples, measure groundwater
levels, and determine any discharge relationships just below the stream bed.
The NCDEQ-SWS approved the proposed activities on June 26, 2019 (Appendix A), and the
County immediately began to implement the pilot study. We provide an update regarding the
status of the approved activities in Section 2.0 below.

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 5 of 16
2.0 1,4-DIOXANE ASSESSMENT AND PILOT STUDY UPDATE
North Carolina Administrative Code 15A NCAC 13B .1634 requires the County to characterize
the nature and extent of any release. The County began assessing the horizontal extent of 1,4-
dioxane during the January 2019 monitoring event by voluntarily sampling three additional wells
that were present at the facility, but no longer part of the required groundwater monitoring
program.
In June of 2019, the County installed the two monitoring wells and the six surface water staff
gauges described in GMA's Pilot Study proposal in June of 2019. A single -cased (Type -II)
monitoring well was installed between the Northern and Southern mounds, just north of well
P16R (Figure 1). This well, designated as well P29, is hydrologically separated from well P16R
by two drainage ditches along the railroad, and the well is screened from 7 to 12 feet below the
land surface. A 60-foot-deep, double -cased (telescoping, Type -III) groundwater monitoring
well was installed on the south side of the Southern Unit, just off the toe of the slope of the
Southern Mound (Figure 1). This well, designated as well P20D, allowed the County to further
assess the vertical extent of 1,4-dioxane at the Southern Unit. The outer casing of P20D
extends to 45 feet below land surface, and the well is screened from 50 to 60 feet below land
surface.
In accordance with the approved Pilot Plan, in August 2019, GMA also installed two shallow, in -
stream piezometers (PZ1 and PZ2) below the ditch bottom along the southern property
boundary near the locations of the historically collected porewater samples (Figure 1). Each
piezometer has a 9-inch-long screen, with the top of the screen set 1 foot below the ditch
bottom. The County uses the instream piezometers to collect representative groundwater
samples to monitor benzene migration and to evaluate groundwater discharge relationships to
the ditch.
To evaluate the integrity of the Southern Landfill Unit cap, and to provide a baseline from which
to evaluate hydrologic improvements following cap upgrades and repairs, Geo Solutions
Limited, Inc. completed electromagnetic (EM) and ground -penetrating radar (GPR) surveys of
the Southern Landfill Unit on June 26', July 15t and July 2nd 2019 (GMA, 2019). The EM survey
identified multiple areas of elevated apparent conductivity that may correspond to leachate
moving away from the landfill. Additionally, the EM survey indicated that solid waste appears to
extend beyond the toe of the slope to the edge of the gravel road in the proximity of monitoring
wells MW6R, P16R, and P20R. This finding was consistent with GMA's observations of trash
during the installation of well P20D. The GPR survey identified several areas that had only a
thin landfill cap that was completely eroded away in some locations. The identified areas
included the northwestern upper slope of the mound, the western narrow berm, and the

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 6 of 16
southern toe north of monitoring wells P28 and P19. The GPR results indicated that the
impermeable cap thickness at the Southern Landfill was, on average, 10 inches and ranged
from 0 to 30 inches. Full details of the geophysical evaluation can be found in Geo Solutions'
report, which was provided as Appendix F of the July 2019 monitoring report from GMA (GMA,
2019). A revised version of that report is included as Appendix B in the July 2021 South
Monitoring Report and Pilot Study (GMA, 2021). The revised report includes a correction to the
estimates of the thickness of the impermeable cap layer based on a corrected understanding of
cap construction at the facility. This correction did not affect the implications or conclusions of
the original geophysical evaluation.
After completion of the geophysical survey, the County contracted with an engineering firm
(The Wooten Company) to design cap repairs and stormwater upgrades that will eliminate or
greatly reduce the infiltration of precipitation into the Southern Unit. The County provided the
geophysical report to Wooten to aid their design of cap repairs and stormwater upgrades for
the facility. The Wooten Company (Wooten) resurveyed the Southern Landfill Unit in early
2020, and in June 2020, Wooten submitted a final design to the County. This design included
repairing the cap on the western end of the Southern Landfill, regrading multiple areas to
eliminate ponding on the mound, restoring the stormwater conveyance system to operate as
originally designed, and adding new drainage pipes to the southwest corner of the mound. The
County chose to make these substantial upgrades to protect the groundwater from further
contamination via leaching from landfill waste.
Construction activities commenced at the site on November 4, 2020. The County's contractor
originally anticipated completing the work by March 2021, but the project experienced
significant weather -related delays due to long periods of high rainfall from December 2020
through February 2021 (NCSCO, 2021). Repairs at the Southern Unit were completed in June
of 2021. As -built drawings for the Southern Unit cap repair and stormwater upgrades are
provided in Appendix C in the July 2021 South Monitoring Report and Pilot Study (GMA, 2021).
Following completion of the cap repairs and stormwater system upgrades, GMA contacted Geo
Solutions Limited, Inc. to complete a post -repair geophysical evaluation of the Southern Unit.
The purpose of this evaluation was to document the remedial effort of the Pitt County Landfill
by comparing the pre -repair and post -repair geophysical data. Geo Solutions completed repeat
EM and GPR surveys of the Southern Landfill Unit on August 2"d thru August 4t", 2021 (GMA,
2021).
A comparison of the EM response before and after cap improvements showed a weaker EM
response in areas where new low permeability material was placed to repair eroded areas of
the cap, and in areas where regrading was performed to improve surface water drainage
toward the catch basins (Figure 2). The weaker EM response in these locations was due to the

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 7 of 16
EM profiler being further above the waste following repairs. Based on GPR data, the most
apparent changes in landfill cap thickness from 2019 to 2021 are along the northern repaired
slope where the cap was significantly thickened (15 to 20 inches) during the recent repair
(GMA, 2021).
The areas of leachate seeps identified in 2019 appeared similar in EM response to the 2021
electromagnetic survey. It is likely too soon to see improvements at seep locations due to the
slow velocity of groundwater at this site. Future geophysical evaluations targeting only the
locations of previously identified seeps may provide a means to monitor the effectiveness of the
recently completed cap improvements. Regardless, geophysical results confirm improvements
to the landfill cap thickness and surface water drainage that should greatly reduce the
infiltration of precipitation into the Southern Landfill Unit.
The County is currently monitoring groundwater levels and contaminant concentrations to
assess the effectiveness of the cap and stormwater system upgrades, as approved by the
NCDEQ-SWS in their June 26, 2019 letter (Appendix A). Additional time will be needed to allow
time for the existing groundwater to drain from the Southern mound prior to making a full
assessment of hydraulic improvements resulting from the repair of the Southern cap. A
preliminary assessment of improvements resulting from the cap repairs is provided in Section
4.0 of this report. The County continues to monitor both the Northern and Southern Landfill
Units on their approved schedules (semi-annually for the Southern and annually for the
Northern).
3.0 JULY 2022 SEMI-ANNUAL MONITORING EVENT
GMA performed the semi-annual monitoring event at the Southern Unit on July 19 to 20, 2022.
Historically, the County has monitored the Southern Landfill Unit for the parameters
identified in Appendix I of 40 CFR Part 258 plus 1,4-dioxane on a semi-annual basis and for the
parameters listed in 40 CFR Part 258 Appendix II on an annual basis. Based on the lack of
detections of Appendix II parameters over the last 20 years, GMA, on behalf of the County,
requested that the NCDEQ SWS allow a reduction in sampling frequency for Appendix II
constituents. Specifically, we requested that the NCDEQ SWS allow the County to sample for
Appendix II constituents on a biennial basis starting in July 2022. The NCDEQ SWS approved
this request on July 2, 2020 (Appendix A). Therefore, during the July 2022 monitoring event,
the County analyzed all groundwater and surface -water samples for Appendix I parameters,
1,4-dioxane, and Appendix II parameters. Sampling procedures and analytical methods
complied with the approved Water Quality Monitoring Plan dated September 8, 1994, and
subsequent groundwater policy memos issued by the NCDEQ-SWS (Appendix A). The next
scheduled Appendix II sampling event will

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 8 of 16
occur during the July 2024 sampling event.
Twenty-eight groundwater -monitoring wells and two temporary groundwater piezometers
comprise the groundwater -monitoring network for the entire landfill facility (Figure 1, Table 1).
GMA also monitors surface water levels at fifteen locations in the ditches surrounding the site
(Table 3, Figure 1). The water -quality monitoring network used for the July 2022 semi-annual
monitoring of the Southern Unit consisted of one background monitoring well (P4), eight
shallow' wells located around the Southern Mound (P11R, P12, P16R, P17, P19, P20R, P28, and
MW6R), a deep' well located south of the Southern mound (P20D), a well located between the
Northern and Southern Landfill Unit (P29), two temporary groundwater piezometers (PZ1 and
PZ2), a hydraulically-upgradient surface water sample location (SW1), and a hydraulically-
downgradient surface water sample location (SW2) (Figure 3).
3.1 Groundwater Hydrology
GMA measured static water levels in all monitoring wells and temporary piezometers (Table 2),
and at it of the 13 staff gauges (Table 3) on July 19, 2022. GMA was unable to access staff
gauge SG2 on July 19t" due to debris at that location, and returned on July 20, 2022 to clear
the debris and measure the static water level. Staff gauge SG5 has been damaged by mowing
at the facility and has not been replaced to date. Depth to groundwater in monitoring wells at
the site ranged from approximately 1.14 to 16.05 feet below the land surface. Estimates of
groundwater velocity (Table 4) ranged from approximately 0.002 to 0.036 feet/day, or 0.73 to
13.16 feet/year. These represent relatively slow groundwater velocities.
An equipotential map prepared using these water -level measurements (Figure 3) shows that the
horizontal component of groundwater flow at the Southern Unit was generally directed to the
south and southeast. Historically, groundwater samples collected from off -site wells P4, P5,
and P6 have been used to assess background groundwater chemistry. The July 2022
equipotential map, however, indicates that groundwater elevations in these wells may be lower
than groundwater elevations in the adjacent Northern mound. This groundwater flow pattern
was also observed during the July 2021 monitoring event. Groundwater flow in this area has
likely been affected by the construction of the nearby Highway 264 overpass and changed land
usage just west of the site. Continued assessment of this finding is warranted.
During the July 2022 monitoring event, the groundwater elevation measured in well P16R was
lower than the surface water elevation at the nearby staff gauge, SG3, indicating that
groundwater from the Southern mound was not discharging to the ditch at this location. Prior
to the completion of the cap repairs and stormwater system upgrades, the opposite relationship
was true (Figure 4). Since July 2019 when a staff gauge was first installed at this location, the
groundwater elevation in well P16R had consistently been higher than the surface water
elevation at SG3, which indicated that shallow groundwater within the Southern Unit was
discharging to the ditch in this area. GMA believes that the change in the direction of shallow

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 9 of 16
groundwater flow at this location may be the first indication of hydraulic improvement resulting
from the cap repairs and stormwater improvements completed at the Southern Unit. Further
monitoring and assessment is needed to determine if this relationship continues in the future or
whether this is due to seasonal and/or annual variation in rainfall.
The groundwater elevation at instream piezometers PZ1 and PZ2 was slightly higher than the
corresponding surface water elevations at those locations during the July 2022 monitoring event
(Tables 2 and 3). The water level measurements collected at both PZ1 and PZ2 indicate that
groundwater was discharging to the southern boundary ditch in this area during the July 2022
monitoring event.
3.2 Sample Collection and Analyses
For monitoring of the Southern Unit, GMA analyzed water samples collected from eleven
monitoring wells, two temporary piezometers, and two surface water sampling locations as
shown on Figure 2. During sampling, GMA collected field water -quality parameters to
document adequate purging prior to sample collection and to aid in evaluating groundwater
chemistry at the site (Table 5). We provide copies of the well sampling records in Appendix B.
All groundwater sampling methods adhered to the procedures described in the EPA Region 4
SESD Operating Procedure for Groundwater Sampling (USEPA, 2017, SESDPROC-301-R4).
GMA transferred all samples to Environmental Conservation Laboratories, Inc. (ENCO) in ice -
filled coolers under chain -of -custody protocol for analysis of Appendix I parameters, 1,4-
dioxane, and Appendix II parameters (Tables 6 and 7). Copies of the chain -of -custody forms
and analytical reports are provided in Appendix C. Consistent with the May 29, 2018 NCDEQ-
SWS memo, ENCO analyzed the samples using EPA -approved analytical methods sufficiently
sensitive to detect the presence of regulated constituents at or below the applicable standard
(unless no such method currently exists, e.g. for vinyl chloride analysis).
3.3 Analytical Results and Discussion
Twenty-seven parameters (acetone, barium, benzene, beryllium, 2-butanone, cadmium,
chlorobenzene, chloroform, cis-1,2-dichloroethene, chromium, cobalt, copper, 1,4-
dichlorobenzene, 1,1-dichloroethene, diethylphalate, 1,4-dioxane, ethylbenzene, lead, mercury,
naphthalene, nickel; selenium, toluene, vanadium, vinyl chloride, total xylenes, and zinc) were
detected at concentrations above their method detection limits in ground and surface waters
during the July 2022 sampling event (Table 7). Nine of those constituents (barium, benzene,
beryllium, cobalt, mercury, vanadium, vinyl chloride, 1,4-dichlorobenzene, and 1,4-dioxane)
were detected at concentrations exceeding the NCAC 02L standards (Table 7).
Samples from wells P16R, P19, P20R, and P29 contained benzene (3.0 µg/L, 4.2 µg/L, 2.2 µg/L,
and 2.0 µg/L, respectively) above the 1.0 µg/L NCAC 02L groundwater standard. Importantly, ,

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 10 of 16
benzene was not detected in either in -stream piezometer sample (PZ1 and PZ2). Therefore,
there continues to be no evidence that benzene is migrating off of the landfill property at this
time.
1,4-Dioxane was detected in wells MW6R, P16R, P17, P19, P20R, and P29 (7.0 µg/L, 83 µg/L,
3.9 µg/L, 160 µg/L, 79 µg/L, and 140 µg/L, respectively) at concentrations exceeding the NCAC
02L groundwater standard of 3 µg/L. The detection of 1,4-dioxane in well P29 located between
the two landfill units indicates that 1,4-dioxane may be leaching from both the Southern and
Northern mounds. Estimated ("]-flagged) concentrations of 1,4-dioxane were also detected in
groundwater samples collected from wells P20D, the "deep" down -gradient monitoring well, and
PZ1, located in the southern ditch, but the concentrations were below the NCAC 02L
groundwater standard. This was the first detection of 1,4-dioxane in well P20D and may
indicate the beginning of migration out of the Surficial/Yorktown Aquifer. The detection of this
contaminant in well P20D warrants further investigation during the next sampling event.
Importantly, the lab did not detect 1,4-dioxane in the sample collected in the downgradient
surface water sample, SW2.
Samples from wells MW6R, P16R, P19, and P20R contained concentrations of barium (2010
µg/L, 1090 µg/L, 1970 µg/L, and 887 µg/L respectively) above the NCAC 02L standard of 700
µg/L. Barium occurs naturally in the native soils at the Pitt County Landfill as evidenced by the
ubiquitous occurrence of this alkaline metal in all samples collected at the site, including those
located in off -site areas. GMA has previously demonstrated that barium is often a constituent
of the particulate matter in many of the groundwater samples collected at the Pitt County
Landfill and that dissolved barium concentrations do not exceed the NCAC 02L standard in some
locations (GMA, 2011 and 2015). Despite the apparent natural occurrence of barium at this
site, the concentrations of barium detected in wells MW6R, MW16R, P19, and P20R are unlikely
to be solely attributable to natural sources.
Upgradient surface water sample SW1 did not contain concentrations of any constituent above
the 15A NCAC 02B surface -water standards. In recent years, multiple metals have exceeded
the standards at this location (e.g. 7 parameters above the 2B standards in July 2019, GMA
2020). Metal exceedances at this upgradient surface -water sample location corresponded with
highway construction on the adjoining parcel directly next to the SW1 sampling location. Per
the NC DOT website, construction on the bypass started in August 2016 and was completed in
November of 2019 (NC DOT, 2019). The lab did not detect any of the target parameters above
the 2B surface -water standards in the down -gradient samples for the Southern Unit (SW2).
All groundwater and surface water samples were analyzed for Appendix II constituents during
the July 2022 sampling event. Samples from well P19 contained concentrations of mercury
(1.06 µg/L) above the NCAC 02L standard of 1.0 µg/L. Mercury has been detected at other

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 11 of 16
landfill wells before, but never above the 2L standard. Additionally, this was the first time that
well P19 has been sampled for Appendix II constituents. Naphthalene and diethylphalate were
also detected in groundwater samples, but the concentrations were below the NCAC 02L
standards of 6.0 µg/L and 6,000 µg/L, respectively. Naphthalene was found in wells P19, P20R,
and P29 (1.5 µg/L, 1.5 µg/L, and 1.6 µg/L, respectively) and diethylphalate was found in well
P20R (3.4 J µg/L). Low-level detections of both naphthalene and diethylphalate are regular
occurrences in the historical data for well P20R. No Appendix II constituents were detected in
any of the surface water samples.
3.3.1 Field Quality Assurance/Quality Control Samp/es
During the July 2022 sampling event, GMA did not receive the volume of deionized (DI) water
with the sample kits necessary for both the equipment and field blank samples. The shortage
resulted from additional containers related to Appendix II sampling and a change in
methodology at ENCO labs in which an additional 1-liter amber jar was needed for each sample.
GMA used the available DI water for the field blank and as a last resort used an unopened
gallon of distilled water for the equipment blank. GMA will review sampling requirements and
procedures before the next groundwater sampling event.
Zinc, toluene, N-nitroso-diethylamine (NDEA), and carbon disulfide were detected in the
equipment blank. Methylene chloride was detected in the trip blank. GMA believes that zinc
concentrations are related to residual powder from the manufacturing process used to produce
the'powder-free' nitrile gloves that we used during sampling. Nitrile gloves are also the likely
source of the carbon disulfide detected in the equipment blank (USGS, 2012). Toluene and
methylene chloride are common laboratory contaminants related to the cleaning of glassware,
equipment, etc. (USEPA, 2014b). NDEA is a clear slightly yellow liquid used as a gasoline and
lubricant additive, antioxidant, copolymer softener, and stabilizer in plastics. Low levels of
NDEA have been found in deionized water and in ion -exchange resins (NTP, 2021). GMA
believes the NDEA detected in the equipment blank was likely from the distilled water. NDEA
was not detected in any other sample.
1,4-Dioxane, barium, carbon disulfide, cobalt, nickel, and zinc were detected in the field blank.
The sample was taken along a gravel road just after a large truck had passed by and thrown
significant dust into the air. GMA believes the dust is likely the source of the metal detections
in the sample. The source(s) of the 1,4-dioxane and carbon disulfide in the field blank sample is
(are) unknown. 1,4-Dioxane was also detected in the field blank during the January 2022
sampling event. . 1,4-Dioxane is commonly detected in landfill leachate, groundwater beneath
municipal and industrial landfills, and in landfill gas and landfill gas condensate (Mohr et al.,
2020). Beginning in 1998, landfill gas (LFG) produced from the Pitt County landfill was
collected by a third party, Enerdyne Power Systems, and sold to Vidant Medical Center (now
called ECU Health Medical Center) where it was used to fire boilers. Declining LFG volumes

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 12 of 16
resulted in the project being no longer economically viable, and Enerdyne stopped collecting
LFG at the end of 2021. Since that time, Pitt County has been running the flare approximately
every two weeks. The detections of 1,4-dioxane in field blank samples during both semi-annual
sampling events in 2022 may be related to the cessation of LFG collection at the landfill.
Additional investigation regarding this matter is warranted.
4.0 WATER LEVELS AND CONTAMINANTS THROUGH TIME
The County is currently monitoring groundwater levels and contaminant concentrations to
assess the effectiveness of the cap and stormwater system upgrades. As described in Section
3.1, the water level elevation in well P16R has historically been higher than the adjacent ditch
(SG3), but since completion of the cap repairs in June 2021 water levels in well P16R have
fallen below SG3 (Figure 4). The changed relationship between water level elevations of well
P16R and staff gage SG3 may be the first indicator that improvements are occurring. The
significance of this trend is questionable due to limited data, but well P16R is located adjacent
to formerly recognized seep locations. The County will continue to monitor for any significant
change to the landfill's groundwater system resulting from the cap repairs. At this time, the
effect of the repairs on seasonal shifts in groundwater flow patterns has not been fully
assessed.
To assess the effect of cap repairs on contaminant concentrations, primary contaminants of
concern (benzene and 1,4-dioxane) have been charted through time for downgradient wells
MW6R and P20R. Figure 5 shows benzene and 1,4-dioxane concentrations through time for
well MW6R. For MW6R, both benzene and 1,4-dioxane show relatively stable trends with some
seasonal fluctuations. Figure 6 shows benzene and 1,4-dioxane concentrations for well P20R
through time. For P20R, both benzene and 1,4-dioxane show relatively stable to slightly
increasing trends with some seasonal fluctuations. Neither well shows any significant changes
to concentration levels since cap repairs were completed. More time is needed in order to fully
assess whether the cap repairs will result in improvements of contaminant concentrations in
groundwater.
At present, it is too soon to fully assess potential hydraulic improvements or reductions in
contaminant levels resulting from the cap repairs completed at the Southern Unit. The County
will continue monitoring and allow time for the existing groundwater to drain from the Southern
mound prior to making a full assessment of any improvements resulting from the repair of the
Southern cap.

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 13 of 16
5.0 CONCLUSIONS AND FUTURE WORK
1,4-Dioxane, barium, and benzene were detected at concentrations exceeding the NCAC 02L
groundwater standards at multiple locations during the July 2022 monitoring event. However,
these constituents were not detected at concentrations above state standards in groundwater
samples collected from just below the southern property ditch, which acts as a local
groundwater discharge feature, or in the downgradient surface -water sample. These results
suggest that these 1,4-dioxane, benzene, and concentrations in excess of naturally occurring
barium are not migrating off -site at this time. Further, benzene was not detected in the sample
collected from the deep monitoring well located down -gradient of the Southern Landfill Unit
(P20D). Barium was detected in this well, but the concentration (99.7 ug/L) was well below the
NCAC 02L standard and below concentrations detected in upgradient, off -site monitoring wells.
The absence of these target compounds indicates that benzene and non-native barium have not
migrated out of the Surficial/Yorktown Aquifer at the site. During the July 2022 monitoring
event, an estimated, low-level concentration of 1,4-dioxane was detected in a groundwater
sample collected from well P20D for the first time. The presence of 1,4-dioxane in well P20D
will be confirmed during the next sampling event.
All groundwater and surface water samples were analyzed for Appendix II constituents during
the July 2022 sampling event. No detections of any new contaminants were found at the site.
No Appendix II constituents were detected in any of the surface water samples. Samples from
well P19 contained concentrations of mercury (1.06 µg/L) above the NCAC 02L standard of 1.0
µg/L. Mercury has been detected at other wells in the monitoring network before, but never
above the 2L standard. Additionally, this was the first time that well P19 has been sampled for
Appendix II constituents. Both naphthalene (P19, P20R, and P29) and diethylphalate (P20R)
had low-level detections during the July 2022 sampling event, but are regular occurrences in
the historical data. These results support the continued sampling for Appendix II constituents
at the Southern Unit on a biennial schedule.
Pitt County completed major cap and stormwater system repairs and upgrades at the Southern
Unit in June 2021 (GMA, 2021). These upgrades were part of an approved pilot study for
corrective action following detections of 1,4-dioxane and benzene above the NCAC 02L
groundwater standards. These improvements were designed to greatly reduce the infiltration
of water through the cap in order to protect the groundwater from further contamination via
leaching from landfill waste. The County is currently monitoring groundwater levels and
contaminant concentrations to assess the effectiveness of the cap and stormwater system
upgrades.
The reversal of shallow groundwater flow in the vicinity of well P16R observed during the last
two monitoring event may be the first indication of hydraulic improvement associated with the

July 2022 Semiannual Water Quality Monitoring Report
Southern Portton of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 14 of 16
cap repairs at the Southern Unit, but further assessment is needed. The County has continued
to monitor the Southern Unit to allow time for the existing groundwater to drain from the
Southern mound and to better evaluate the effects of seasonal changes and varying amounts of
precipitation on groundwater levels prior to malting a full assessment of hydraulic improvements
resulting from the cap repair. It is too soon to see reductions in contaminant levels associated
with the cap repairs. GMA suggests extending the monitoring period of the Pilot Study to July
of 2023 at a minimum so that a better assessment can be completed.
The County continues to monitor groundwater at the Southern Unit on a semi-annual schedule.
The next semi-annual monitoring event at the Pitt County Solid Waste Municipal Landfill is
scheduled for January of 2023 and will include only Appendix I of 40 CFR Part 258 parameters
plus 1,4-dioxane.
REP RT ERTIFI TI N
This report was prepared by Groundwater Management Associates, Inc. (GMA), a professional
corporation licensed to practice geology (#C-121) and engineering (#C-0854) in North Carolina.
I, Cody J. Shell, a North Carolina Licensed Geologist for GMA, do certify that the information
contained in this report is correct and accurate to the best of my knowledge.
Cody J. Shell, P.G.
Project Hydrogeologist
I
Emma H. Shipley, P.G.
Project Hydrogeologist
••.•• N C A R ►.,
MIS
SEAL
2737
Richard K. Spruill, Ph.D., P.G.
Principal Hydrogeologist

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 15 of 16
7.0 REFERENCES
Groundwater Management Associates, Inc., 1994, Water Quality Monitoring Plan for the Active
Southern Unit of the Pitt County Landfill, 71 pages.
Groundwater Management Associates, Inc., 2011, Alternative Source Demonstration Report, Pitt
County Solid Waste Municipal Landfill, Greenville, Pitt County, 8 pages.
Groundwater Management Associates, Inc., 2015, January 2015 Semi -Annual Water Quality
Monitoring Event, Greenville, Pitt County, 147 pages.
Groundwater Management Associates, Inc., 2018, Potential Receptor Survey: Northern and
Southern Units of the Pitt County Landfill, Greenville, Pitt County, 14 pages.
Groundwater Management Associates, Inc., 2019, January 2019 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 201 pages.
Groundwater Management Associates, Inc., 2021, July 2021 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 216 pages.
Groundwater Management Associates, Inc., 2022, Pilot Study Update and January 2022 Semi -
Annual Water Quality Monitoring Event (Southern Mound), Greenville, Pitt County, 172
pages.
Groundwater Management Associates, Inc. and McGill and Associates, 2001, Water Resources
Management Plan, Pitt County, North Carolina.
Horton, J.W. and V.A. Zullo, 1991, The Geology of the Carolinas: Carolina Geological Society
Fiftieth Anniversary Volume, 406 pp.
Mohr, T.K.G., DiGuiseppi, W., Hatton, J., & Anderson, 1., 2020, Environmental Investigation and
Remediation: 1,4-Dioxane and Other Solvent Stabilizers (2nd ed.). CRC Press.
https://doi.org/10.1201/9780429401428
NC DOT, 2019, Southwest Bypass Opens to Traffic ahead of Schedule,
https: //www. ncdot.aov/news/press-releases/Pages/2019/2019-11-21-pitt-cou nth
southwest-bypass-opens.asox, accessed December 4, 2019.
NCSCO, 2021, North Carolina State Climate Office, Winter Recap 2020-21: La Nina Lays Low in
a Persistent Wet Winter, https://climate.ncsu.edu/blog/2021/03/winter-recap-2020-21-la-
nina-lays-low-in-a-persistent-wet-winter/, accessed July, 20, 2021.
NTP (National Toxicology Program). 2021. Report on Carcinogens, Fifteenth Edition. Research
Triangle Park, NC: U.S. Department of Health and Human Services, Public Health Service.
https://ntp.niehs.nih.gov/go/rocl5

July 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
November 7, 2022
Page 16 of 16
USEPA, 2014a, Technical Fact Sheet — 1,4-Dioxane, Office of Solid Waste and Emergency
Response, EPA 505-F-14-011, 8 pages.
USEPA, 2014b, Laboratory Data Review for the Non -Chemist, Region 9, 59 pages.
USEPA, 2017, Operating Procedure: Groundwater Sampling, Number SESDPROC-301-R4.
Region 4 Science and Ecosystem Support Division (SESD), Athens, GA.
USGS, 2012, Program Evaluation of Volatile Organic Compound (VOC) Blank Data and
Application of Study Reporting Levels to Groundwater Data Collected for the California
GAMA Priority Basin Project, May 2004 through September 2010. Scientific
Investigations Report 2012-5139, 106 pages.
Winner, M.D. and R.W. Coble, 1996, Hydrogeologic Framework of the North Carolina Coastal
Plain, USGS Professional Paper 1404-I, 119 pages.

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75 P09 74 173
75.40� /
123 .-- 8 —8 72
2.32� �— - 80
I 80- MW5' /.
r/71
I J _
�P.24 -80 P03 70
70 80
---- PZ1 P10
69
70.05 69 - .P-08��00
(surface water) � � , 67.97��1
►� "-V- 68)
68
SG2
67.16 N
GENERAL NOTES:
1. TOPOGRAPHIC CONTOUR INTERVAL = 2.0 FEET
2. GROUNDWATER CONTOUR INTERVAL = 1.0 FOOT
3. ARROW INDICATES DIRECTION OF GROUNDWATER FLOW
4. WATER LEVEL ELEVATIONS ARE POSTED BY EACH WELL
5.( ) INDICATES DATA NOT USED FOR CONTOURING
- LEGEND -
MONITORING WELL
UNMEASURED MONITORING WELL
X ABANDONED MONITORING WELL
EPROPERTY LINE
+—t—� RAILROAD TRACKS
TOPOGRAPHIC CONTOUR
- POND
GROUNDWATER ELEVATION
CONTOUR
INDICATES DIRECTION OF
GROUNDWATER FLOW
77.31 WATER LEVEL
(FEET ABOVE SEA LEVEL)
DITCH
0 STAFF GAUGE
FIGURE 3
DATE 10/11/2022 PROJECT: 25101
DRW BY: CJS CHK BY: EHS
SCALE IN FEET
0 350 700'
1" = 350'
EQUIPOTENTIAL MAP
J U LY 19, 2022
NSA
GROUNDWATER MANAGEMENT ASSOCIATES, INC.

Water Levels in P16R and SG3 Through Time
79
78.5
J 78
cN
Q
77.5
c
0
'r- 77
c�
—
v
w 76.5
—
Cap repairs completed
76
— in June of 2021
75.5
Jul-19
Jul-20 Jul-21 Jul-22
Date
-LEGEND-
G5MA
--6—P16R SG3
GROUNDWATER MANAGEMENT ASSOCIATES, INC.
File: GMA/251XX/25101/
WATER LEVELS THROUGH TIME IN WELL P16R AND STAFF GAGE SG3
DATE: 10/10/2022
2022 JULY/FIGURES
PROJECT 25101
PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC
FIGURE 4

12
ro
0S
0.6
U
C
0
U 0A
m
c
v
= U
a
m
0
7/2411998
1,4-Dioxane concentrations through time in well MW6R
10
s
°E 7
6
O
5
c 4
u
3
2
1
0
4/10/2019 10/27/2018 5/15/2019
12/1/2019 6t18/2020 1/4/2021 7/2312021 2/8/2022 8/27/2022 3/1512023
Date
Benzene concentrations through time in well MW6R
4/19/2001 1/14/2004 10/10/2005
7/612Dag 4/1/2012 12/2712014 9/22/2017 5/18/2020 3/15/2023
Date
AGM,qA
fi=�n 0
r-
GROUNDWATER MANAGEMENT ASSOCIATES, INC.
File: D S/251CONTAMINANT CONCENTRATIONS THROUGH TIME IN WELL MW6R Date: 10/04/2022
OCthruM FIG5 COCthruTime MW6R
PROJECT 25181 PITT COUNTY, NC Figure 5

3
J
2.5
10f10/2OD6
1,4-Dioxane concentration through time in well P20R
100
90
a 80
C
0
70
60
G
°1 50
u
-
C
40
:i0
C 30
M
20
0
10
o
4/10/2018 10/27J2018 5J1512019
7/6/2009
12/1/2019 6/18/2020 1/4/2021
Date
7/23/2021 2/99022 8/27/2022 3/15/2023
Benzene concentration through time in well P20R
411J2012 12/27/2014 9/22/2017
Date
6/18/2020 3/15/2023
GMA
GROUNDWATER MANAGEMENT ASSOCIATES, INC.
File: D OCthru ime P1/ CONTAMINANT CONCENTRATIONS THROUGH TIME IN WELL P20R Date: 10/04/2022
FIG6 COCthruTime P20R
PROJECT 25181 PITT COUNTY, NC Figure 6

TABLES

Table 1. Monitoring Well Construction and Elevations
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Number
Easting
(feet)*
Northing
(feet)*
=
Lq *
U O Vf
wa
oM
a >
° W .`-°.
U
0 Uf
Ana
M�
>
W .�°.
+�+ 7
-3io°
° •� .`�°.
O
(n
-W w
a a
c °
w
O- O w°i
E
0 1.
c CO°
u
w
ao
.
W °`�°,
° wU)
= O J
O Va„)
EEa oWell
a£ W q
LU, CO
MW1R
2463487.26
676793.08
84.28
81.3
52.98
40.0
50.0
41.3
31.3
MW3
2467253.81
676198.15
81.77
79.3
47.47
35.0
45.0
44.3
34.3
MW4
2466875.66
676066.89
82.38
80.7
21.68
10.0
20.0
70.7
60.7
MW6R
2465083.71
675392.21
79.74
76.95
19.79
7.0
17.0
69.95
59.95
MW8
2464639.20
676915.58
83.21
80.42
16.79
4.0
14.0
76.42
66.42
MW8D
2464553.05
676827.15
83.08
80.17
30.91
18.0
28.0
62.17
52.17
P02
2467254.11
676191.82
83.45
79.4
19.05
11.0
15.0
68.4
64.4
PO4
2463438.60
676616.81
83.82
80.3
21.52
8.0
18.0
72.3
62.3
P05
2463490.61
676797.65
84.74
81.1
17.14
8.5
13.5
72.6
67.6
P06
2463171.35
676568.01
83.52
80.3
17.72
8.5
14.5
71.8
65.8
P07
2466875.67
676056.22
84.21
80.7
19.51
11.0
16.0
69.7
64.7
P08
2466074.39
674918.18
84.02
80.2
20.3
9.0
17.0
72.4
64.4
P09
2466189.91
675932.77
82.88
78.9
18.48
9.5
14.5
69.4
64.4
P11R
2463141.14
675651.83
84.84
81.1
19.74
13.0
16.0
68.1
65.1
P12
2463126.32
675048.53
78.21
75.1
20.61
10.5
17.5
64.6
57.6
P13
2466105.04
676161.21
83.79
80.8
18.99
11.0
16.0
69.8
64.8
P13D
2466119.99
676174.03
83.25
80.5
53.55
46.8
50.8
33.7
29.7
P15
2465472.37
676703.00
86.7
83.05
20.71
4.0
17.0
80.25
67.25
P16R
2464194.10
675837.67
86.24
83.1
17.14
11.0
14.0
72.1
69.1
P17
2463319.94
675286.12
79.18
75.1
15.08
8.0
11.0
67.1
64.1
P19
2463898.87
675403.02
82.7
77.3
18.4
9.0
13.0
68.3
64.3
P20R
2464435.49
675068.13
84.01
80.5
33.51
10.0
30.0
70.5
50.5
P20D
2464583.16
675103.79
83.32
80.3
63.02
50.0
60.0
30.3
20.3
P21
2465286.45
675904.93
80.87
76.6
15.27
8.0
11.0
68.6
65.6
P23
2465657.48
675745.22
81.73
78.2
19.53
11.0
16.0
67.2
62.2
P26
2466246.80
676940.21
83.39
81
16.39
9.0
14.0
72
67
P28
2463542.16
675278.55
76.54
73.6
10.94
3.5
8.0
70.1
65.6
P29
2464558.30
676041.26
84.16
81.2
14.96
7.0
12.0
74.2
69.2
PZ1
2464848.16
675165.00
71.24
69.6
3.39
1.0
1.8
69.8
69.1
PZ2
2464485.95
1 675009.74
1 71.69
70
3.44
1.0
1.8
70.2
69.5
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument 'RUTH' and NCGS Monuments 'MARY'. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NAVD 88.
BLS = below land surface ASL = above sea level LS = land surface

Table 2. Monitoring Well Water Levels and Sample Purge Volumes
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Elevation of
Top of
Casing*
(feet ASL)
Land
Surface
Elevation*
(feet ASL)
Total Well
Depth
below LS
(feet)
Depth to
Water
(feet)
Elevation of
Water (feet
ASL)
Height of
Water in
Well (feet)
Amount
Purged
(gallons)
Purged to
Dryness?
MW1R
7/19/22
84.28
81.3
50.0
9.54
74.74
not sampled
MW3
7/19/22
81.77
79.3
45.0
10.75
71.02
not sampled
MW4
7/19/22
82.38
80.7
20.0
7.33
75.05
not sampled
MW6111
7/19/22
79.74
76.95
17.0
8.60
71.14
11.2
5.9
no
MW8
7/19/22
83.21
80.42
14.0
8.93
74.28
not sampled
P02
7/19/22
83.45
79.4
15.0
9.56
73.89
not sampled
PO4
7/19/22
83.82
80.3
18.0
9.56
74.26
12.0
6.5
no
POS
7/19/22
84.74
81.1
13.5
8.15
76.59
not sampled
P06
7/19/22
83.52
80.3
14.5
9.31
74.21
not sampled
P07
7/19/22
84.21
80.7
16.0
9.25
74.96
not sampled
P08
7/19/22
84.02
80.2
17.0
16.05
67.97
not sampled
P09
7/19/22
82.88
78.9
14.5
7.48
75.40
not sampled
P11R
7/19/22
84.84
81.1
16.0
9.04
75.80
10.7
3.2
yes
P12
7/19/22
78.21
75.1
17.5
4.17
74.04
16.4
7.0
yes
P13
7/19/22
83.79
80.8
16.0
9.54
74.25
not sampled
P13D
7/19/22
83.25
80.5
50.8
11.39
71.86
not sampled
P1S
7/19/22
86.7
83.05
17.0
11.03
75.67
not sampled
P16R
7/19/22
86.24
83.1
14.0
9.76
76.48
7.4
2.7
yes
P17
7/19/22
79.18
75.1
11.0
5.88
73.30
9.2
3.8
yes
P19
7/19/22
82.7
77.3
13.0
8.66
74.04
9.7
3.8
yes
P20R
7/19/22
84.01
80.5
30.0
12.25
71.76
21.3
11.3
no
P20D
7/19/22
83.32
80.3
60.0
11.96
71.36
51.1
25.0
no
P21
7/19/22
80.87
76.6
11.0
7.67
73.20
not sampled
P23
7/19/22
81.73
78.2
16.0
9.41
72.32
not sampled
P26
7/19/22
83.39
81
14.0
10.59
72.80
not sampled
P28
7/19/22
76.54
73.6
8.0
4.75
71.79
6.2
3.2
no
P29
7/19/22
84.16
81.2
12.0
8.10
76.06
6.9
3.5
no
PZ12
7/19/22
71.24
69.6
1.8
1.14
70.10
2.3
0.5
no
PZ22
7/19/22
71.69
70
1.8
1.23
70.46
2.3
0.5
no
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid (NCGS) control based on ties to
NCGS Monument 'RUTH' and NCGS Monuments 'MARY'. Horizontal data referenced to NAD 83(2011). Vertical data referenced to NAVD 88.
LS = Land Surface ASL = Above Sea Level
1 MW6R also sampled using the tradidtional three well -volume purge method with a bailer.
2 A grap sample was collected at this location with a bailer.

Table 3. Staff Gauge Elevations and Water Levels
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Staff
Gauge
Date
Easting
(feet)*
Northing
(feet)*
Reference
Point
Elevation of
Reference
Point
feet ASL
Staff Gauge
Reading or
Depth to Water
Measurement
ft
Elevation of
Water
feet ASL
SG1
7/19/22
2464589.3
676053.46
4-foot mark
79.86
1.06
76.92
SG2
7/20/22
2466082.36
674856.14
4-foot mark
70.48
0.68
67.16
SG3
7/19/22
2464175.98
675874.46
4-foot mark
79.40
1.89
77.29
SG4
7/19/22
2467192.35
676705.36
4-foot mark
75.18
1.25
72.43
SGS
7/19/22
2465262.23
675928.45
3-foot mark
75.68
Missing
Missing
SG6
7/19/22
2465175.63
675356.1
4-foot mark
72.98
0.58
69.56
SG7
7/19/22
2463215.14
675010.08
3-foot mark
73.93
0.92
71.85
SG8
7/19/22
2463932.14
675059.19
3-foot mark
72.71
1.16
70.87
SG9
7/19/22
2466110.5
676143.36
3-foot mark
75.76
0.16
72.92
SG10
7/19/22
2463086.65
676845.47
3-foot mark
80.82
1.34
79.16
SGI1
7/19/22
2463169.96
676528.73
3-foot mark
80.27
0.31
77.58
SG12
7/19/22
2463583.11
676511.02
3-foot mark
79.93
0.64
77.57
SG96
7/19/22
2466366.84
676889.34
3-foot mark
76.63
1.00
74.63
PZ1-SW+
7/19/22
2464848.16
675165.00
TOC
71.24
1.19
70.05
PZ2-SW+
7/19/22
2464485.95
675009.74
TOC
71.69
1.23
70.47
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument'RUTH' and NCGS Monuments'MARY. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NAVD 88.
+ Surface water elevations determined by measuring depth to surface water from top of casing
ASL = Above Sea Level
TOC = top of casing

Table 4. Calculations of Groundwater Velocity
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Horizontal
Hydraulic
Gradient
(ft/ft)
Hydraulic
Conductivity
(ft/day)
Effective
Porosity
Horizontal
Groundwater
Velocity
(ft/day)
Horizontal
Groundwater
Velocity
(ft/year)
MW6R
7/19/22
0.012
0.50
0.29
0.021
7.79
PO4
7/19/22
0.014
0.50
0.19
0.036
13.16
P12
7/19/22
0.004
0.20
0.43
0.002
0.73
P20R
7/19/22
0.007
0.10
0.32
0.002
0.77
P28
7/19/22
0.007
0.30
0.17
0.013
4.80

Table 5. Field -Water Quality Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Sample
Date
pH
Temp-
erature
(degrees
Celsius)
Specific
Conductance
(PS/cm)
Dissolved
oxygen
(mg/L)
Turbidity during
collection of
organic samples
(ntu)
Turbidity during
collection of
metals samples
(ntu)
7/20/2022
6.72
21.6
2118
2.1
>1000
--
MW6R
7/20/2022
--
--
--
--
--
29.2
PO4
7/20/2022
4.90
17.8
62
5.8
82
--
P11R
7/19/2022
5.09
19.2
91
3.63
604
--
P12
7/20/2022
5.30
19.9
69
7.4
121
7/19/2022
6.66
20.0
5787
3.4
>1000
--
P16R
7/20/2022
--
--
--
--
--
46
P17
7/20/2022
5.27
21.8
203.7
2.8
530.0
--
P19
7/20/2022
3.93
21.2
1497
3.5
320.0
--
7/19/2022
6.16
19.3
2296
2.6
>1000
--
P20R
7/20/2022
--
--
--
--
--
37.8
P20D
7/20/2022
5.44
19.4
61.9
4.5
61.3
--
7/19/2022
5.20
24.3
66
2.6
819
--
P28
7/20/2022
--
--
--
--
--
130
7/19/2022
5.14
19.5
2281
2.9
374.0
--
P29
7/20/2022
--
--
--
--
--
12
PZ1
7/20/2022
6.14
24.70
1176.0
4.28
38.2
--
PZ2
7/20/2022
6.45
26.00
659.00
5.46
14.7
--

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
CAS
IMAC
MCL
Calculated
Number
Name
Other Names
.
;60
(Ng�L)
GWP Std
67-64-1
Acetone
2-Propanone
0
--
--
--
107-13-1
Acrylonitrile
Acrylonitrile
--
--
--
--
7440-36-0
Antimony
Antimony
1
--
6
--
7440-38-2
Arsenic
Arsenic
10
--
10
--
7440-39-3
Barium
Barium
700
--
2000
--
71-43-2
Benzene
Benzene
1
--
5
--
7440-41-7
Beryllium
Beryllium
4
--
4
--
Bromochloromethane;
Methane, bromochloro-
--
--
--
0.6
74-97-5
Chlorobromethane
Bromodichloromethane;
Methane, bromodichloro
0.6
--
80
--
75-27-4
Dichlorobromomethane
Bromoform;
75-25-2
Tribromomethane
Methane, tribromo-
4
--
80
--
7440-43-9
Cadmium
Cadmium
2
--
5
--
75-15-0
Carbon disulfide
Carbon disulfide
700
--
--
--
56-23-5
Carbon tetrachloride
Methane, tetrachloro-
0.3
--
5
--
108-90-7
Chlorobenzene
Benzene, chloro-
50
--
100
--
Chloroethane; Ethyl
75-00-3
chloride
Ethane, chloro-
3000
--
--
--
Chloroform;
67-66-3
Trichloromethane
Methane, trichloro-
70
--
80
--
7440-47-3
Chromium
Chromium
10
--
100
--
7440-48-4
Cobalt
Cobalt
1
--
--
--
7440-50-8
Copper
Copper
1000
--
1300
--
Dibromochloromethane;
Methane, dibromochloro
0.4
--
80
--
124-48-1
Chlorodibromomethane
1,2-Dibromo-3-
Propane, 1,2-dibromo-3-
96-12-8
chloro ro ane; DBCP
chloro-
0.04
--
0.2
--
1,2-Dibromoethane;
Ethane, 1,2-dibromo-
0.02
--
0.05
--
106-93-4
Ethylene dibromide; EDB
o-Dichlorobenzene; 1,2-
Benzene, 1,2-dichloro-
20
--
600
--
95-50-1
Dichlorobenzene
p-Dichlorobenzene; 1,4-
106-46-7
Dichlorobenzene
Benzene, 1,4-dichloro-
6
--
75
--
2-Butene,
110-57-6
trans-1,4-Dichloro-2-butene
E4-dichloro-,
-
-
-
-
1,1-Dichloroethane;
75-34-3
1 Eth Ididene chloride
Ethane, 1,1-dichloro-
6
--
--
--

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
IMAC
DEQ
CAS
2L
(Ng/L)
MCL
Calculated
Number
Name
Other Names
Std.
GWP Std
1,2-Dichloroethane;
Ethane, 1,2-dichloro-
04
.
--
5
--
107-06-2
Ethylene dichloride
1,1-Dichloroethylene; 1,1-
Ethene, 1,1-dichloro-
350
--
7
--
75-35-4
Dichloroethene•
cis-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(Z)
70
--
70
--
156-59-2
cis-l2-Dichloroethene
trans-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(E)
100
--
100
--
156-60-5
trans-l2-Dichloroethene
78-87-5
1,2-Dichloropropane
Propane, 1,2-dichloro-
0.6
--
5
--
cis-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-01-5
Z -
trans-1,3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-02-6
E -
100-41-4
Ethylbenzene
Benzene, ethyl-
600
--
700
--
2-Hexanone; Methyl butyl
2-Hexanone
40
--
--
--
591-78-6
ketone
7439-92-1
Lead
Lead
15
--
15
--
Methyl bromide;
Methane, bromo-
10
--
--
--
74-83-9
Bromomethane
Methyl chloride;
Methane, chloro-
3
--
--
--
74-87-3
Chloromethane
Methylene bromide;
Methane, dibromo-
--
70
--
--
74-95-3
Dibromomethane
Methylene chloride;
Methane, dichloro-
5
--
5
--
75-09-2
Dichloromethane
Methyl ethyl ketone; MEK;
78-93-3
2-Butanone
2-Butanone
4000
--
--
--
Methyl iodide;
Methane, iodo-
--
--
--
--
74-88-4
Iodomethane
4-Methyl-2-pentanone;
2-pentanone, 4-methyl-
100
--
--
--
108-10-1
Methyl isobutyl ketone
7440-02-0
Nickel
Nickel
100
--
--
--
7782-49-2
Selenium
Selenium
20
--
50
--
7440-22-4
Silver
Silver
20
--
--
--
100-42-5
Styrene
Benzene, ethenyl-
70
--
100
--
1 1 1 2-Tetrachloroethane
Ethane, 1,1,1,2-
1
630-20-6
' ' '
tetrachloro-
1 1 2 2-Tetrachloroethane
Ethane, 1,1,2,2-
0.2
79-34-5
' ' '
tetrachloro-

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standardsi
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(NgL)
GWP Std
Tetrachloroethylene;
Tetrachloroethene;
Ethene, tetrachloro-
0.7
--
5
--
127-18-4
Perch loroeth lene
7440-28-0
Thallium
Thallium
2
--
2
--
108-88-3
Toluene
Benzene, methyl-
600
--
1000
--
1,1,1-Trichloroethane;
71-55-6
Meth (chloroform
Ethane, 1,1,1-trichloro-
200
--
200
--
Trichloroethylene;
Ethene, trichloro-
3
--
5
--
79-01-6
Trichloroethene
79-00-5
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
0.6
--
5
--
Trichlorofluoromethane;
Methane,trichlorofluoro-
2000
--
--
--
75-69-4
CFC-11
96-18-4
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
0.005
--
--
--
7440-62-2
Vanadium
Vanadium
7
--
--
--
108-05-4
Vinyl acetate
Acetic acid, ethenylester
--
88
--
--
75-01-4
VIIIYI ullulluu,Ethene,
chloro-
0.03
--
2
--
7440-66-6
Zinc
Zinc
1000
--
--
--
1330-20-7
Xylene (total)
Benzene, dimethyl-
500
--
10000
All units are in micrograms per liter (pg/L)
2L STD = 15A NCAC 2L groundwater standard
'Applicable Groundwater Protection Standard is the lower of the listed standards.

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
GWP Std
Number
Name
Other Names
563-58-6
1,1-Dichloropropene
1-Propene, 1,1-dichloro-
NE
NE
NE
NE
1,2,4,5-
95-94-3
Tetra chlorobenzene
Benzene, 1,2,4,5-tetrachloro-
2
NE
NE
NE
120-82-1
1,2,4-Trichlorobenzene
Benzene, 1,2,4-trichloro-
70
NE
70
NE
1,3-Dichloropropane;
142-28-9
Trimethylene dichloride
Propane, 1,3-dichloro-
NE
NE
NE
NE
130-15-4
1,4-Naphthoquinone
1,4-Naphthalenedione
NE
NE
NE
NE
134-32-7
1-Naphthylamine
1-Naphthalenamine
NE
NE
NE
NE
2,2-Dichloropropane;
594-20-7
Isopropylidene chloride
Propane, 2,2-dichloro-
NE
NE
NE
NE
2,3,4,6-
58-90-2
Tetrachlorophenol
Phenol, 2,3,4,6-tetrachloro-
200
NE
NE
NE
2,3,7,8-TCDD; 2,3,7,8-
Tetrachlorodibenzo-p-
.0002
1746-01-6
dioxin
ng/L
NE
0.03
NE
2,4,5-T; 2,4,5-
Trichlorophenoxyacetic
Acetic acid, (2,4,5-
93-76-5
acid
trichlorophenoxy)-
NE
NE
NE
NE
95-95-4
2,4,5-Trichlorophenol
Phenol, 2,4,5-trichloro-
63
NE
NE
NE
88-06-2
2,4,6-Trichlorophenol
Phenol, 2,4,6-trichloro-
NE
4
NE
NE
2,4-D; 2,4-
Dichlorophenoxyacetic
94-75-7
acid
Acetic acid, (2,4-dichlorophenoxy)
70
NE
70
NE
120-83-2
2,4-Dichlorophenol
Phenol, 2,4-dichloro-
0.98
NE
NE
NE
2,4-Di methyl phenol; m-
105-67-9
Xylenol
Phenol, 2,4-dimethyl-
100
NE
NE
NE
51-28-5
2,4-Dinitrophenol
Phenol, 2,4-dinitro-
NE
NE
NE
NE
121-14-2
2,4-Dinitrotoluene
Benzene, 1-methyl-2,4-dinitro-
0.05
NE
NE
NE
87-65-0
1 2,6-Dichlorophenol
Phenol, 2,6-dichloro-
NE
NE
NE
NE
606-20-2
2,6-Dinitrotoluene
Benzene, 2-methyl-1,3-dinitro-
NE
NE
NE
NE
2-Acetylaminofluorene;
53-96-3
2-AAF
Acetamide, N-91-1-fluoren-2-yl-
NE
NE
NE
NE
91-58-7
2-Chloronaphthalene
Naphthalene, 2-chloro-
NE
NE
NE
NE
95-57-8
1 2-Chlorophenol
Phenol, 2-chloro-
0.4
NE
NE
NE
91-57-6
2-Methyl naphthalene
Naphthalene, 2-methyl-
30
NE
NE
NE
91-59-8
2-Naphthylamine
2-Naphthalenamine
NE
NE
NE
NE
[1,1'-Biphenyl]-4,4'-diamine,3,3'-
91-94-1
3,3'-Dichlorobenzidine
dichloro-
NE
NE
NE
NE
[1,1'-Biphenyl]-4,4'-diamine,3,3'-
119-93-7
3,3'-Dimethylbenzidine
dimethyl-
NE
NE
NE
NE
Benz[j]aceanthrylene,1,2-dihydro-
56-49-5
3-Methylcholanthrene
3-methyl-
NE
NE
NE
NE
Benzene 1,1'-(2,2-
72-54-8
4,4'-DDD
dichloroethylidene)bis[4-chloro-
0.1
NE
NE
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
GWP Std
Number
Name
Other Names
Benzene, 1,1'-
72-55-9
4,4'-DDE
(dichloroethenylidene)bis[4-chloro
NE
NE
NE
NE
Benzene, 1,1'-(2,2,2-
50-29-3
4,4'-DDT
trichloroethylidene)bis[4-chloro-
0.1
NE
NE
NE
4,6-Dinitro-o-cresol; 4,6
534-52-1
Dinitro-2-methylphenol
Phenol, 2-methyl-4,6-dinitro-
NE
NE
NE
NE
92-67-1
4-Aminobiphenyl
[1,1'-Biphenyl]-4-amine
NE
NE
NE
NE
4-Bromophenyl phenyl
101-55-3
ether
Benzene, 1-bromo-4-phenoxy-
NE
NE
NE
NE
4-Chlorophenyl phenyl
7005-72-3
ether
Benzene, 1-chloro-4-phenoxy-
NE
NE
NE
NE
99-55-8
5-Nitro-o-toluidine
Benzenamine, 2-methyl-5-nitro-
NE
NE
NE
NE
7,12-
Dimethylbenz[a]anthra
57-97-6
cene
Benz[a]anthracene, 7,12-dimethyl
NE
NE
NE
NE
83-32-9
Acenaphthene
Acenaphthylene, 1,2-dihydro-
80
NE
NE
NE
208-96-8
Acenaphthylene
Acenaphthylene
200
NE
NE
NE
Acetonitrile; Methyl
75-05-8
cyanide
Acetonitrile
NE
NE
NE
NE
98-86-2
Acetophenone
Ethanone, 1-phenyl-
700
NE
NE
NE
107-02-8
Acrolein
2-Propenal
4
NE
NE
NE
1,4:5,8-
Dimethanonaphthalene,1,2,3,4,10
,10 -hexachloro-1,4,4a,5,8,8a-
309-00-2
Aldrin
hexahydro-(1,4,4a,5,8,8a)-
0.002
NE
NE
NE
107-05-1
Allyl chloride
1-Propene, 3-chloro-
NE
NE
NE
NE
Cydohexane,1,2,3,4,5,6-
319-84-6
alpha-BHC
hexachloro-,(1a,2a,3R,4a,5' ,6' )-
NE
0.006
NE
NE
120-12-7
Anthracene
Anthracene
2000
NE
NE
NE
Benzeneethanamine,
122-09-8
alpha,alpha-dimethyl
NE
NE
NE
NE
Benzo[a]anthracene;
56-55-3
Benzanthracene
Benz[a]anthracene
0.05
NE
NE
NE
50-32-8
Benzo[a]pyrene
Benzo[a]pyrene
0.005
NE
0.2
NE
205-99-2
Benzo[b]fluoranthene
Benz[e]acephenanthrylene
0.05
NE
NE
NE
191-24-2
Benzo[ghi]perylene
Benzo[ghi]perylene
200
NE
NE
NE
207-08-9
Benzo[k]fluoranthene
Benzo[k]fluoranthene
0.5
NE
NE
NE
100-51-6
Benzyl alcohol
Benzenemethanol
700
NE
NE
NE
Cyclohexane,1,2,3,4,5,6-
319-85-7
beta-BHC
hexachloro-,(1a,2° ,3a,4' ,5a,6' )-
NE
0.02
NE
NE
Bis(2-
Ethane, 1,1'-
111-91-1
chloroethoxy)methane
[methylenebis(oxy)]bis [2-chloro-
NE
NE
NE
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
GWP Std
Number
Name
Other Names
Bis(2-chloroethyl)ether;
111-44-4
Dichloroethyl ether
Ethane, 1,1'-oxybis[2-chloro-
NE
NE
NE
0.031
Bis(2-ethylhexyl)
1,2-Benzenedicarboxylic acid,
117-81-7
phthalate
bis(2-ethylhexyl)ester
3
NE
NE
NE
Butyl benzyl phthalate;
1,2-Benzenedicarboxylicacid, butyl
85-68-7
Benzyl butyl phthalate
phenylmethyl ester
1000
NE
NE
NE
4,7-Methano-11-1-
indene,1,2,4,5,6,7,8,8- octachloro
57-74-9
Chlordane
2,3,3a,4,7,7a-hexahydro-
0.1
NE
NE
NE
Benzeneacetic acid, 4-chloro-(4-
chlorophenyl)--hydroxy-, ethyl
510-15-6
Chlorobenzilate
ester
NE
NE
NE
NE
126-99-8
Chloroprene
1,3-Butadiene, 2-chloro-
NE
NE
NE
NE
218-01-9
Chrysene
Chrysene
5
NE
NE
NE
57-12-5
Cyanide
Cyanide
70
NE
200
NE
Cyclohexane,1,2,3,4,5,6-
319-86-8
delta-BHC
hexachloro-,(1a,2a,3a,4° ,5a,6' )-
NE
NE
NE
0.019
Carbamothioic acid,bis(1-
methylethyl)-, S-(2,3-dichloro-2-
2303-16-4
Diallate
propenyl) ester
NE
NE
NE
NE
53-70-3
Dibenz[a,h]anthracene
Dibenz[a,h]anthracene
0.005
NE
NE
NE
132-64-9
Dibenzofuran
Dibenzofuran
28
NE
NE
NE
Dichlorodifluoromethan
75-71-8
e; CFC 12
Methane,dichlorodifluoro-
1000
NE
NE
NE
Bis(2-chloro-l-
methylethyl) ether; 2,2'
Dichlorodiisopropyl
ether; DCIP, See
108-60-1
footnote 4
Propane, 2,2'-oxybis[1-chloro-
NE
NE
NE
NE
2,7:3,6-Dimethanonaphth[2,3-
b]oxirene,3,4,5,6,9,9-hexachloro -
1a,2,2a,3,6,6a,7,7a-octahydro-,
60-57-1
Dieldrin
(iaa,2° ,2aa,3° ,6' ,6aa,7° ,7aa)-
0.002
NE
NE
NE
1,2-Benzenedicarboxylicacid,
84-66-2
Diethyl phthalate
diethyl ester
6000
NE
NE
NE
Phosphorodithioic acid,0,0-
dimethyl S-[2-(methylamino)-2-
60-51-5
Dimethoate
oxoethyl] ester
NE
NE
NE
NE
1,2-Benzenedicarboxylicacid,
131-11-3
Dimethyl phthalate
dimethyl ester
NE
NE
NE
NE
1,2-Benzenedicarboxylic acid,
84-74-2
Di-n-butyl phthalate
dibutyl ester
700
NE
NE
NE
1,2-Benzenedicarboxylicacid,
117-84-0
Di-n-octyl phthalate
dioctyl ester
100
NE
NE
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
Number
Name
Other Names
GWP Std
Dinoseb; DNBP; 2-sec-
Phenol, 2-(1-methylpropyl)-4,6-
88-85-7
Butyl-4,6-dinitrophenol
dinitro-
7
NE
7
NE
122-39-4
Diphenylamine
Benzenamine, N-phenyl-
NE
NE
NE
NE
Phosphorodithioic acid,0,0-diethyl
298-04-4
Disulfoton
S-[2-(ethylthio)ethyl]ester
0.3
NE
NE
NE
6,9-Methano-2,4,3-benzodiox-
athiepin,6,7,8,9,10,10 -hexachloro
1,5,5a,6,9,9a-hexahydro-, 3-
959-98-8
Endosulfan I
oxide,
40
NE
NE
NE
6,9-Methano-2,4,3-
benzodioxathiepin,6,7,8,9,10,10 -
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-
33213-65-91
Endosulfan II
oxide, (3a,5aa,6° ,9' ,9aa)-
NE
NE
NE
42
6,9-Methano-2,4,3-
benzodioxathiepin,6,7,8,9,10,10 -
hexachloro-1,5,5a,6,9,9a-
1031-07-8
Endosulfan sulfate
hexahydro-, 3,3-dioxide
40
NE
NE
NE
2,7:3,6-Dimethanonaphth[2,3-
b]oxirene, 3,4,5,6,9,9-hexachloro-
1a,2,2a,3,6,6a,7,7a-octahydro-,
72-20-8
Endrin
(1aa,2° ,2a° ,3a,6a,6a° ,7° ,7aa)-
2
NE
2
NE
1,2,4-Methenocyclo-
penta[cd]pentalene-5-
carboxaldehyde,2,2a,3,3,4,7 -
hexachlorodecahydro-
(1a,2°,2a°,4°,4a°,5°,6a°,6b°,7R*
7421-93-4
Endrin aldehyde
)-
2
NE
NE
NE
2-Propenoic acid, 2-methyl-, ethyl
97-63-2
Ethyl methacrylate
ester
NE
NE
NE
NE
62-50-0
Ethyl methanesulfonate
Methanesulfonic acid,ethyl ester
NE
NE
NE
NE
Phosphorothioic acid, 0-[4-
[(dimethylamino)sulfonyl]phenyl]-
52-85-7
Famphur
0, 0-dimethyl ester
NE
NE
NE
NE
206-44-0
Fluoranthene
Fluoranthene
300
NE
NE
NE
86-73-7
Fluorene
9H-Fluorene
300
NE
NE
NE
Cyclohexane,1,2,3,4,5,6-
58-89-9
gamma-BHC; Lindane
hexachloro-,(ia,2a,3° ,4a,5a,6° )-
0.03
NE
0.2
NE
4,7-Methano-lH-
indene,1,4,5,6,7,8,8-heptachloro-
76-44-8
Heptachlor
3a,4,7,7a-tetra hydro-
0.008
NE
0.4
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
Number
Name
Other Names
GWP Std
2,5-Methano-2H-indeno[1,2-
b]oxirene,2,3,4,5,6,7,7 -
heptachloro-ia,ib,5,5a,6,6a, -
hexahydro-
1024-57-3
Heptachlor epoxide
,(1aa,1b' ,2a,5a,5a' ,6' ,6aa)
0.004
NE
0.2
NE
118-74-1
Hexachlorobenzene
Benzene, hexachloro-
0.02
NE
1
NE
1,3-Butadiene,1,1,2,3,4,4-
87-68-3
Hexachlorobutadiene
hexachloro-
0.4
NE
NE
NE
Hexachlorocyclopentadi
1,3-Cyclopentadiene,1,2,3,4,5,5-
77-47-4
ene
hexachloro-
NE
NE
50
50
67-72-1
Hexachloroethane
Ethane, hexachloro-
NE
NE
NE
2.5
1888-71-7
Hexachloropropene
1-Propene, 1,1,2,3,3,3-hexachloro
NE
NE
NE
NE
193-39-5
Indeno(1,2,3-cd)pyrene
Indeno[1,2,3-cd]pyrene
0.05
NE
NE
NE
78-83-1
Isobutyl alcohol
1-Propanol, 2-methyl-
NE
NE
NE
NE
1,4,5,8-
Dimethanonaphthalene,1,2,3,4,1
0,10-hexachloro-1,4,4a,5,8,8a
465-73-6
Isodrin
hexahydro-(1a,4a,4a' ,5' ,8' ,8a' )-
NE
NE
NE
NE
2-Cyclohexen-l-one,3,5,5-
78-59-1
Isophorone
trimethyl-
40
NE
NE
NE
120-58-1
Isosafrole
1,3-Benzodioxole, 5-(1-propenyl)-
NE
NE
NE
NE
1,3,4-Metheno-2H-cyclobuta-
[cd]pentalen-2-one,
1,1a,3,3a,4,5,5,5a,5b,6-
143-50-0
Kepone
decachlorooctahydro-
NE
NE
NE
NE
m-Cresol; 3-
108-39-4
Methylphenol
Phenol, 3-methyl-
400
NE
NE
NE
m-Dichlorobenzene; 1,3
541-73-1
Dichlorobenzene
Benzene, 1,3-dichloro-
200
NE
NE
NE
99-65-0
m-Dinitrobenzene
Benzene, 1,3-dinitro-
NE
NE
NE
NE
7439-97-6
Mercury
Mercury
1
NE
2
NE
126-98-7
Methacrylonitrile
2-Propenenitrile, 2-methyl-
NE
NE
NE
NE
1,2,Ethanediamine, N,N-dimethyl-
91-80-5
Methapyrilene
N'-2-pyridinyl-N'-( 2-
NE
NE
NE
NE
Benzene, 1,1'-
(2,2,2,trichloroethylidene)bis [4-
72-43-5
Methoxychlor
methoxy-
40
NE
NE
NE
2-Propenoic acid, 2-methyl-,
80-62-6
Methyl methacrylate
methyl ester
25
NE
NE
NE
Methyl
66-27-3
methanesulfonate
Methanesulfonic acid,methyl ester
NE
NE
NE
NE
Methyl parathion;
Phosphorothioic acid,0,0-
298-00-0
Parathion methyl
dimethyl
NE
NE
NE
NE
m-Nitroaniline; 3-
99-09-2
Nitroaniline
Benzenamine, 3-nitro-
NE
NE
NE
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
2L Std.
IMAC
MCL
Calculated
CAS
(pg/L)
GWP Std
Number
Name
Other Names
91-20-3
Naphthalene
Naphthalene
6
NE
NE
NE
98-95-3
Nitrobenzene
Benzene, nitro-
NE
NE
NE
NE
55-18-5
N-Nitrosodiethylamine
Ethanamine, N-ethyl-N-nitroso-
NE
NE
NE
NE
62-75-9
Nitrosodimethylamine
Methanamine, N-methyl-N-nitroso
0.0007
NE
NE
NE
N-Nitrosodi-n-
924-16-3
butylamine
1-Butanamine, N-butyl-N-nitroso-
NE
NE
NE
NE
86-30-6
N-Nitrosodiphenylamine
Benzenamine, N-nitroso-N-phenyl-
NE
NE
NE
NE
N-
N itrosod i propyla m i ne;
N-Nitroso-N-
dipropylamine; Di-n-
1-Propanamine, N-nitroso-N-
621-64-7
propylnitrosamine
propyl-
NE
NE
NE
NE
N-
Nitrosomethylethalamin
10595-95-6
e
Ethanamine, N-methyl-N-nitroso-
NE
NE
NE
NE
100-75-4
N-Nitrosopiperidine
Piperidine, 1-nitroso-
NE
NE
NE
NE
930-55-2
N-Nitrosopyrrolidine
Pyrrolidine, 1-nitroso-
NE
NE
NE
NE
0,0,0-Triethyl
Phosphorothioic acid,0,0,0-
126-68-1
phosphorothioate
triethyl ester
NE
NE
NE
NE
0,0-Diethyl 0-2-
pyrazinyl
phosphorothioate;
Phosphorothioic acid,0,0-diethyl
297-97-2
Thionazin
0-pyrazinyl ester
NE
NE
NE
NE
o-Cresol; 2-
95-48-7
Methylphenol
Phenol, 2-methyl-
400
NE
NE
NE
o-Nitroaniline; 2-
88-74-4
Nitroaniline
Benzenamine, 2-nitro-
NE
NE
NE
NE
o-Nitrophenol; 2-
88-75-5
Nitrophenol
Phenol, 2-nitro-
NE
NE
NE
NE
95-53-4
o-Toluidine
Benzenamine, 2-methyl-
NE
NE
NE
NE
p-
(Dimethylamino)azoben
Benzenamine, N,N-dimethyl-4-
60-11-7
zene
(phenylazo)-
NE
NE
NE
NE
Phosphorothioic acid,0,0-diethyl-
56-38-2
Parathion
0-(4-nitrophenyl) ester
NE
NE
NE
NE
106-47-8
p-Chloroaniline
Benzenamine, 4-chloro-
NE
NE
NE
NE
p-Chloro-m-cresol; 4-
59-50-7
Chloro-3-methylphenol
Phenol, 4-chloro-3-methyl -
NE
NE
NE
NE
p-Cresol; 4-
106-44-5
Methylphenol
Phenol, 4-methyl-
40
NE
NE
NE
608-93-5
Pentachlorobenzene
Benzene, pentachloro-
NE
NE
NE
NE
Pentachloronitrobenzen
82-68-8
e
Benzene, pentachloronitro-
NE
NE
NE
NE
87-86-5
Pentachlorophenol
Phenol, pentachloro-
0.3
NE
1
NE

Table 7. Appendix II Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
IMAC
2L Std.
MCL
Calculated
CAS
(pg/L)
GWP Std
Number
Name
Other Names
62-44-2
Phenacetin
Acetamide, N-(4-ethoxyphenyl)
NE
NE
NE
NE
85-01-8
Phenanthrene
Phenanthrene
200
NE
NE
NE
108-95-2
Phenol
Phenol
30
NE
NE
NE
Phosphorodithioic acid,0,0-diethyl
298-02-2
Phorate
S-[(ethylthio)methyl ]ester
1
NE
NE
NE
p-Nitroaniline; 4-
100-01-6
Nitroaniline
Benzenamine, 4-nitro-
NE
NE
NE
NE
p-Nitrophenol; 4-
100-02-7
Nitrophenol
Phenol, 4-nitro-
NE
NE
NE
NE
Polychlorinated
biphenyls; PCBs
1,1'-Biphenyl,chloro derivatives
1336-36-3
1016/1242
Method 1016/1242
NE
0.09
0.5
NE
106-50-3
p-Phenylenediamine
1,4-Benzenediamine
NE
NE
NE
NE
Benzamide, 3,5-dichloro-N-(1,1-
23950-58-5
Pronamide
dimethyl-2-propynyl)-
NE
NE
NE
NE
Propionitrile; Ethyl
107-12-0
cyanide
Propanenitrile
NE
NE
NE
NE
129-00-0
Pyrene
Pyrene
200
NE
NE
NE
94-59-7
Safrole
1,3-Benzodioxole, 5-(2-propenyl)-
NE
NE
NE
NE
Propanoic acid, 2-(2,4,5-
93-72-1
Silvex; 2,4,5-TP
trichlorophenoxy)-
50
NE
NE
NE
18496-25-8
Sulfide
Sulfide
NE
NE
NE
NE
99-35-4
sym-Trinitrobenzene
Benzene, 1,3,5-trinitro-
NE
NE
NE
NE
7440-31-5
Tin
Tin
2000
NE
NE
NE
8001-35-2
Toxaphene
Toxaphene
0.03
NE
3
NE
All units are in micrograms per liter (pg/L)
2L STD = 15A NCAC 2L groundwater standard
'Applicable Groundwater Protection Standard is the lower of the listed standards.

Table 8. List of Compounds Detected during the July 2022 Sampling Event (7/19-20/2022)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(Ng/L)
MDL
I (Ng/L)
INC 2L or 28
Std* (Ng/L)
IMAC
(N9/L)
MCL
(Ng/L)
III a Groundwater Samples
7/20/2022
1,4-Dioxane
7.0
0.80
3
-
-
7/20/2022
Acetone
35
10
6000
-
-
MW6R
7/20/2022
Barium Total
2010
1.10
700
-
2000
7/20/2022
Copper Total
2.2
1.60
1000
-
1300
7/20/2022
Zinc Total
14.4
4.4
1000
-
-
7/20/2022
Barium Total
104
1.10
700
-
2000
PO4
7/20/2022
Beryllium Total
0.2093
0.160
4
-
4
7/20/2022
Zinc Total
10.5
4.40
1000
-
-
7/19/2022
Barium Total
150
1.10
700
-
2000
7/19/2022
Beryllium Total
2.78
0.160
4
-
4
7/19/2022
Cobalt Total
5.983
1.40
1
-
-
7/19/2022
Copper Total
6.073
1.60
1000
-
1300
P11R
7/19/2022
Lead Total
7.583
3.10
15
-
15
7/19/2022
Nickel Total
4.771
2.20
100
-
-
7/19/2022
Vanadium Total
10.9
1.40
7
-
-
7/19/2022
Zinc Total
110
4.40
1000
-
-
7/20/2022
1,4-Dioxane
1.63
0.80
3
-
-
7/20/2022
Barium Total
71.5
1.10
700
-
2000
P12
7/20/2022
Beryllium Total
1.78
0.160
4
-
4
7/20/2022
Zinc Total
9.093
4.40
1000
-
-
7/19/2022
1,4-Dioxane
83 D
4.0
3
-
-
7/19/2022
2-Butanone
7.6
1.3
4000
-
-
7/19/2022
Acetone
34
10
6000
-
-
7/20/2022
Barium Total
1090
1.10
700
-
2000
7/19/2022
Benzene
3.0
0.15
1
-
5
P16R
7/19/2022
Chlorobenzene
1.8
0.17
50
-
100
7/20/2022
Chromium Total
2.493
1.40
10
-
100
7/20/2022
Cobalt Total
2.673
1.40
1
-
-
7/20/2022
Nickel Total
10.6
2.20
100
-
-
7/19/2022
Toluene
0.543
0.14
600
-
1000
7/20/2022
Vanadium Total
4.751
1.40
1 7
-
-
7/20/2022
1,4-Dioxane
3.9
0.80
3
-
-
7/20/2022
Barium Total
227
1.10
700
-
2000
7/20/2022
Beryllium Total
1.83
0.160
4
-
4
7/20/2022
Chlorobenzene
1.9
0.17
50
-
100
P17
7/20/2022
Chromium Total
2.921
1.40
10
-
100
7/20/2022
Cobalt Total
1.403
1.40
1
-
-
7/20/2022
Nickel Total
2.263
2.20
100
-
-
7/20/2022
Vanadium Total
3.61 J
1.40
7
-
-
7/20/2022
Zinc Total
5.82 J
4.40
1000
-
-

Table 8. List of Compounds Detected during the July 2022 Sampling Event (7/19-20/2022)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(N9/L)
MDL
(N9/L)
INC 2L or 213
Std* 9/L)
IMAC
(pg/L)
MCL
(pg/L)
7/20/2022
1,1-Dichloroethane
4.1
0.13
6
-
-
7/20/2022
cis- 1,2-Dich loroethene
2.4
0.15
70
-
70
7/20/2022
1,4-Dichlorobenzene
6.3
0.19
6
-
75
7/20/2022
1,4-Dioxane
160 D
4.0
3
-
-
7/20/2022
Barium Total
1970
1.10
700
-
2000
7/20/2022
Benzene
4.2
0.15
1
-
5
7/20/2022
Beryllium Total
14.4
0.160
4
-
4
7/20/2022
Chlorobenzene
17
0.17
50
-
100
7/20/2022
Cobalt Total
18.3
1.40
1
-
-
P19
7/20/2022
Eth (benzene
1.6
0.13
600
-
700
7/20/2022
Lead Total
5.353
3.10
15
-
15
7/20/2022
Mercury Total
1.06
0.150
1
-
2
7/20/2022
Naphthalene
1.5
0.11
6
-
-
7/20/2022
Nickel Total
26.1
2.20
100
-
-
7/20/2022
Selenium Total
1.843
1.82
20
-
50
7/20/2022
Toluene
0.513
0.14
600
-
1000
7/20/2022
Vinyl Chloride
0.753
0.32
0.03
-
2
7/20/2022
Zinc Total
107
4.40
1000
-
-
7/19/2022
1,1-Dichloroethane
0.513
0.13
6
-
-
7/19/2022
1,4-Dichlorobenzene
3.8
0.19
6
-
75
7/19/2022
1,4-Dioxane
79 D
4.0
3
-
-
7/20/2022
Barium Total
842
1.10
700
-
2000
7/20/2022
Beryllium Total
0.9573
0.160
4
-
4
7/19/2022
Benzene
2.2
0.15
1
-
5
P2OR
7/20/2022
Cobalt Total
2.843
1.40
1
-
-
7/19/2022
Chlorobenzene
1.6
0.17
50
-
100
7/19/2022
Diethyl phthalate
3.43
2.4
6000
-
-
7/19/2022
Naphthalene
1.5
0.11
6
-
-
7/20/2022
Nickel Total
8.563
2.20
100
-
-
7/19/2022
o-Xylene
1.1
0.065
-
-
-
7/19/2022
X lenes Total
1.11
0.45
500
-
10000
7/20/2022
1,4-Dioxane
0.873
0.80
3
-
-
7/20/2022
Barium Total
99.7
1.10
700
-
2000
7/20/2022
Beryllium Total
7.96
0.160
4
-
4
7/20/2022
Cadmium Total
0.8191
0.360
2
-
5
P2OD
7/20/2022
Chromium Total
9.931
1.40
10
-
100
7/20/2022
Cobalt Total
2.403
1.40
1
-
-
7/20/2022
Lead Total
4.821
3.10
15
-
15
7/20/2022
Toluene
1.9
0.14
600
-
1000
7/20/2022
Vanadium Total
9.793
1.40
7
-
-
7 20/2022
Zinc Total
17.9
4.40
1000
-
-
7/19/2022
1,4-Dioxane
0.843
0.80
3
-
-
7/20/2022
Barium Total
34.6
1.10
700
-
2000
7/20/2022
Beryllium Total
0.7213
0.160
4
-
4
P28
7/20/2022
Chromium Total
1.793
1.400
10
-
100
7/20/2022
Cobalt Total
1.823
1.400
1
-
-
7/20/2022
Vanadium Total
2.92 J
2.20
7
-
7/20/2022
Zinc Total
13.1
4.40
1000
-
-
7/19/2022
1,4-Dichlorobenzene
1.9
0.19
6
-
75
7/19/2022
1,4-Dioxane
140 D
4.0
3
-
-
7/20/2022
Barium Total
370
1.10
700
-
2000
P29
7/19/2022
Benzene Total
2.0
0.15
1
-
5
7/19/2022
Chlorobenzene
13
0.17
50
-
100
7/19/2022
Naphthalene
1.6
0.11
6
-
-
7/20/2022
Vanadium Total
1 9.163
1 1.40
1 7
1 -
I-
PZ1
1 7/20/2022
1,4-Dioxane
1 1.13
1 0.8
1 3
1 -
I-

Table 8. List of Compounds Detected during the July 2022 Sampling Event (7/19-20/2022)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or 2B
Std* (Ng/L)
IMAC
(Ng/L)
MCL
F(pg/L)
Surface Water Samples
7/20/2022
Barium Total
35.9
1.10
21,000+
-
2000
7/20/2022
Chloroform
5.2
0.18
2000
-
2000
SWi
7/20/2022
Cobalt Total
2.38 J
1.40
4
-
-
7/20/2022
Toluene
jZinc Total
0.70 J
6.96 J
0.14
4.40
11
36.5
-
520
7/20/2022
-
5000'
SW2
7/20/2022
Barium Total
71
2.33 J
1.10
1.40
21,000+
-
2000
7/20/2022
IChromium Total
23.81-
-
-
7/20/2022
Cobalt Total
2.57 J
1.40
4
-
-
QA/QC Samp/es
7/20/2022
Carbon Disulfide
170
1.5
700
-
-
EB
7/20/2022
N-Nitrosodiethylamine
5.1 J
2.1
-
-
-
7/20/2022
Toluene
1.3
0.14
600
-
1000
7/20/2022
Zinc Total
8.54 J
4.4
1000
-
-
7/20/2022
1,4-Dioxane
1.2 J
0.8
3
-
-
7/20/2022
Barium Total
448
1.1
700
-
2000
FB
7/20/2022
Carbon Disulfide
3.43
1.5
700
-
-
7/20/2022
Cobalt Total
1.43 J
1.4
1
-
-
7/20/2022
Nickel Total
10.2
2.2
100
-
-
7/20/2022
Zinc Total
80.2
4.4
1000
-
-
TB
7/19/2022
1 Methylene Chloride
0.59 J
0.23
5
1 -
5
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
I = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 213 standards are listed for
surface water sampling locations (SW1 and SW2).
Value represents an EPA action level.
#Value represents an EPA secondary Maximum Contaminant Level.
+NC In -Stream Target Value for Surface Waters.
"Hardness -dependent metal standard calculated assuming an in -stream hardness of 25 mg/L of CaCO3.
Concentrations highlighted in yellow were detected above the 2L (or 26) standards.
Concentrations highlighted in orange were detected above the IMAC.
Concentrations highlighted in blue were detected above the EPA MCL.

APPENDIX A
CORRESPONDENCE FROM THE
NC DIVISION OF WASTE MANAGEMENT

Waste Management
ENVIRONMENTAL QUALITY
March 16, 2017
Sent Via Email — iohn.demary@pittcountync.�ov
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for Assessment of Benzene Contamination Migration
Pitt County MSW Landfill (Northern and Southern)
Pitt County
Solid Waste Permit Number 74-01
DIN 27529
Dear Mr. Demary:
ROY COOPER
Governor
MICHAEL S. REGAN
secretar4
MICHAEL SCOTT
Director
The NC Solid Waste Section has completed a review of the Proposal for Assessment of Benzene
Contamination Migration dated March 15, 2017 (DIN 27528) submitted on your behalf by Groundwater
Management Associates, Inc. (GMA) for the closed Pitt County MSW Landfill, NC Solid Waste Permit
Number 7401. During the January 2017 semiannual water quality monitoring event benzene was
detected at concentrations exceeding the NC 2L Groundwater Standards in two groundwater monitoring
wells.
Based upon the groundwater exceedances, Pitt County is requesting to collect two pore water samples
from the beneath the southern boundary ditch and analyze for Appendix I constituents. The proposed
sampling locations are located downgradient of groundwater monitoring well P20R and will be sampled
during the July 2017 semiannual water quality monitoring event.
As a result, the Proposal for Assessment of Benzene Contamination Migration is approved as described. If
you have any questions, please feel free to contact me by email at [e-mail] or
by phone at 828.296.4706. Thank you for your continued cooperation with this matter.
Sincerely,
L)4—
Jaclynne Drummond
Compliance Hydrogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
State of North Carolina 1 Environmental Quality I Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa, NC 28778
828 296 4500

cc sent via email: Tim Corley, Pitt County Engineer
Jason Watkins, Field Operations Branch Head
Drew Hammonds, Eastern District Supervisor
Ray Williams, Environmental Senior Specialist
Elizabeth Werner, Permitting Hydrogeologist
Emma Shipley, GMA
Steve Campbell, GMA
Stetrni Nurtl+Cur ill mo I [mici.tlllnmmalQuollty I WmleManeprmem
AnixwllleRr�fu iAlllfhrr I AlM1ltU4 il1�jtlMaY tit I %w:vmw%(xL NC 1NI16
iU1117W+ a`�C10

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
June 26, 2019
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County Municipal Solid
Waste Landfill
Closed and Unlined Pitt County MSW Landfill Northern and Southern Units
Pitt County
Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974
FID 1323161
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Proposal for 1,4-Dioxane Assessment
and Pilot Study at the Pitt County Municipal Solid Waste Landfill dated June 21, 2019 (FID 1323159)
and submitted on your behalf by Groundwater Management Associates, Inc. for the closed and unlined
Pitt County Landfill, Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974.
To address the 1,4-Dioxane being detected within the groundwater at the landfill, Pitt County is
proposing to:
1) Delineate the vertical and horizontal extent of 1,4-Dioxane by installing two additional groundwater
monitoring wells (Type II and Type III) and six surface water gauges;
2) Initiate a one-year pilot study to determine the effectiveness of cap upgrades and repairs to see if
they have limited the infiltration of rainwater into the soil cap, and if they have reduced leachate
volumes and concentrations. Geophysical testing of the Southern Unit only will also be conducted to
evaluate landfill cap integrity. The County will repair any areas identified by the geophysical testing
and will inspect surface water drainage structures on the mound to ensure that they are operating as
designed. Once repairs are made, geophysical testing will be repeated to document hydrologic
benefits from cap repairs and to determine if the repairs have significantly reduced rainfall infiltration;
and
3) Install two instream piezometers approximately 1.5 feet below the ditch bottom at the locations of
the currently collected porewater samples. The instream piezometers will be used to collect
representative groundwater samples, measure groundwater levels, and determine any discharge
relationships at repeatable locations just below the stream bed.
Based upon a review of the Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County
Municipal Solid Waste Landfill, the Section approves the activities as described. If you have any
questions or concerns regarding this letter, please feel free to contact me by phone at 828.296.4706
or by email at [e-mail]. Thank you for your continued cooperation with this
matter.
a E Qom_
North Carolina Department oFEnvlronmental Quality I Division of Waste Management
Asheville Regional Office 12090 U.S. Highway 70 1Swan nanoa, North Carolina 28778
828,296.4500

Sincerely,
L;�4' rc�—�
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County Engineer
Ed Mussler, SWS Chief
Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Sherri Stanley, SWS Permitting Branch Head
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
Dr. Richard Spruill, GMA
Jay Holley, GMA
North Camtlna Geparnorni of Envlron*neidal Quality I NvIs1on of Wasic Managrrnent
Asheville Regional Office 1 20,90 U.S. Hlghway 70 1 Swannanoa, North Carolina 28778
82&29h_4500

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
July 2, 2020
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Request for Reduced Sampling Frequency of Appendix 11 Constituents
Closed and Unlined Pitt County MSW Landfill Southern Unit
Pitt County
Solid Waste Permit Number 7401-MSWLF-1974
FID 1417776
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Request for Reduced Sampling
Frequency of Appendix II Constituents dated July 1, 2020 (FID 1417773) and submitted on your behalf
by Groundwater Management Associates, Inc. for the closed and unlined Pitt County Landfill Southern
Unit, Solid Waste Permit Number 7401-MSWLF-1974.
In accordance with 15A NCAC 13B .1634 a request was provided to the Section to modify the
groundwater monitoring frequency for the full set of Appendix II constituents because no Appendix II
constituents have been detected since 2014. Pitt County is requesting to sample for Appendix II
constituents on a biennial basis with the next scheduled Appendix II sampling event occurring during
July 2022. The County will continue to sample for Appendix I parameters and for 1,4-dioxane on a
semi-annual basis.
Based upon a review of the Request for Reduced Sampling Frequency of Appendix 11 Constituents, the
Section approves the request as written at this time. If you have any questions or concerns regarding
this response letter, please feel free to contact me by phone at 828.296.4706 or by email at
[e-mail].
Sincerely,
1
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County
a E Qom_
North Carolina Department oFEnvlronmental Quality I Division of Waste Management
Asheville Regional Office 12090 U.S. Highway 70 1Swan nanoa, North Carolina 28778
828,296.4500

Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
North Carull na Deparl ment of Ernlronmmtal Quality I iNvision of Mstc Ktamgemenr
Asheville Reylvnal Uffloe 1 2090 U.S. Hlghx y 70 1 Sw mmn.a, North Cwoftmk 28775
M-064900

APPENDIX B
SAMPLING RECORDS

GMA #25101- Pitt County Landfill — Sample Collection Field Sheet Date: -7- to 2 Z
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
0
ty
ZZ
Sample ID:
MW6R
Field Team Members:
C ]S t FAQ
Field Staff Initials
Duties (check all that apply)
❑ Notes
0"Water Level
Z Field Parameters
eSample Collection
❑ Other
❑ Notes
❑ Water Level
❑ Field Parameters
❑ Sample Collection
❑ Other
Sampling For:
0- Appendix I
D-�'Appendix II
0-lDelayed Metals?
Sample Type:
E1 Monitoring Well
❑ Surface
Water ❑
Temporary Piezometer
Collection Method; Gl,�PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.79 ft Diameter: 2 in Screen interval: 7.0 - 17.0 ftBLS
Water Level
Water Le►rel: ft Water Level Date: T-'k -- L time: �7
Water Column M ft 3 Well Volume gal Zz - .- a
Purge Parameters continue on grid below, if necessa
Bads
pH
(S.U.$)
Sp, Cond.
(PS/CM)
DRP
(mvolts)
DO
(mg/1)
Temp
COO(NTU)
Turbidity
7
Dry'
Comments- Purge Volume
(gal)
Is' Bail
(� `tip
Z "`I Z
-j Z.i
�`� �
�L�.0
Z:.`L
2nd Well
Volume
�� ��
SVIO
y2t,L\
z>X>1
31d Well
Volume
6,—L,L
2Nk4 :
^-�
L 1,
2v-,
Sample Collection Date/Time: 2 -2Z V,
Delayed Metals Collection Date/Time: t-`L� 2Z 15=� Turbidity during Metals Collection:
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCI
❑
8260D SIM ID
1 4-dioxane
VOAs
3
HCl
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
Z;\GMAv5iXX-Prrr COUNM25101 - LANDFILL�METHOaS & BLANK WELL SAMPLING r-ORMS�WELL SAMPLING F0RM_BA1L1NG-20220124,DDU

GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Date; _1r -VZ
11
Sample ID:
Field Team Members:
C_�s i COS
Field Staff Initials Duties (check all that apply)
❑ Notes 0 Water Level 2rField Parameters ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: l" Appendix I C Appendix II ❑ Delayed Metals?
Sample Type: C?-­Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: 01PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Iv-3-2- Well
Stickup (ft): 13W ft Diameter: 2
Water Level: ` ft Water Level Date: Z
I I.C�6
Water Column ,ft 3 Well Volume
Al-2a\
in Screen interval: 40tr!50-0 ft 6L5
Water Level
time: -fit tj tZ
gal
Pure Parameters continue on a0d below, if necessary)
Bails
pH
(S.U.$)
Sp, Cond.
(µS/cm}
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
?
Dry'
Comments- Purge Volume
(gal)
2nd Well
Volume
L\'V;
��C�u1
40. j
'� t
n,ox
lc�c"
3'd Weli
Volume
LX,k L.11
Lk
Jj, k
` t,-1
Sample Collection Date/Time: =i •2z Z'L-- 1V" ;-O
Delayed Metals Collection Date/Time: Turbidity during Metals Collection:
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCl
❑
8260D SIM I❑
14-dioxane
VOAs
3
HCl
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r1h = 0,4856745 * h *Use Teflon bailers for delayed metals
2:jGMAO110f-P1TT COUVM25101 - LANDFILL�ME HODS & BLANK WELL SAMPLING FORMS\WELL SAMPLING FORM_BMLING_20220124.00CK

.7
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date: I-i`t•22._
All wells 2" in diameter, Use r = 0.083 feet App II collected every other July starting in 2022.
Sample ID: P11R Field Team Members: CSS � b%
Field Staff Initials Duties (check all that apply)
❑ Notes Dilater Level T5 Field Parameters 2--ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: 2"—Appendix I B�__Appendix II ❑ Delayed Metals?
Sample Type: I- Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: 0 PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.74 ft Diameter:
Water Level: —CA L � ft Water Level Date: -Z_
Water Column lc .-7L� ft 3 Well Volume
2 in Screen interval: 13.0 - 16.0 ft BLS
Water Level
time: 1« aQ
gal -2 i � �,
Purge Parameters continue on greid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
VQ
Turbidity
(NTU)
?
Dry'
Comments- Purge Volume
(gal)
i Bail
12.-7
2nd Well
Volume
-00\
r1�.'a
'I, 5
��3
1ti.'�
�:�L\
3rd Well
Volume
Sample Collection Date/Time: 4v
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
❑ All samples preserved
El All samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container T
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCI
❑
8260D 5IM ID
1 4-dioxane
VCAs
3
HCl
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
nla
3 Vols (in gallons) = 70.5 rZh = 0.4856745 * h *Use Teflon bailers for delayed metals
Z:�GMQ5=-PrrT COUNTY\25101 - LANDFILLjMETHOD5 & BLANK WELL SAMPLING FORMS�WELLSAMPLING FORM_BAILING 20220124.DOCX

GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet Date: 1 - 2,0-Z`--
All wells 2" in diameter. Use r = 0.083 feet App H collected every other July starting in 2022.
Sample ID: P12 Field Team Members:
Field Staff Initials Duties (check all that apply)
❑ Notes El -Water Level Z-Field Parameters I71-S-ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ET-- Appendix I ❑Appendix II ❑ Delayed Metals?
Sample Type: I] ---Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: I1�-PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth +
Stickup (ft):
Well
ft Diameter: `
Water Level: � , 1-7 ft Water Level Date: T i`\ Z
Water Column -74-k ft 3 Well Volume
20.91
2 in Screen interval: 10.5 -17.5 ft BLS
Water Level
time: ic,
gal 33%.I
Purge Parameters continue on grid below, if necessary)
Bails
pH
Sp. Cond.
DRP
DO
Temp
Turbidity
D ry'a
Comments- Purge Volume
(S,U,$)
(PS/cm)
(molts)
(mg/1)
(°C)
(NTU)
(gal)
1st Bail
r�
_
5L�.1
2-7•A
2nd Well
Volume
S_3
Cck.l
3 7.-7
3ro Well
Volume
Sample Collection Date/Time:
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
El All samples preserved
El All samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Loh Anal pis
Container T
No. of Containers
Preservation
❑
$260D A I
VOAs
3
HCl
❑
826OD SIM ID
1 4-dioxane
VOAs
3
HCl
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
11- Ammer
2
n/a
3 Vols (in gallons) = 70.5 rah = 0.4856745 * h *Use Teflon bailers for delayed metals
2:\GMAV51XX-Parr COUN'V'Y125101 - LANDFILL\METHODS & BLANK WELL SAMPLING FORMSIWELL SAMPLING FORM_ BAILING_20220124.DOCX

GMA #25101- Pitt County Landfill — Sample Collection Field Sheet Date: I-ti°1rZZ
All wells 2" in diameter. Use r = 0,083 feet App II collected every other ]uly starting in 2022.
�L,
i5
Sample ID: P16R
Field Team Members: c7n I f�6y�-
Field Staff Initials Duties (check all that apply)
❑ Notes Water Level D- Field Parameters C]'§'a mple Collection ❑ Other
❑ Notes ❑ Water Level ElField Parameters ElSample Collection ❑ Other
f
Sampling For: © Appendix I Appendix II Delayed Metals?
Sample Type: ❑ Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 17.14 ft Diameter: 2
Water Level: c�.-7� ft Water Level Date: 'I -l`t-? Z
Water Column ~7- a 3 ft 3 Well Volume
in Screen interval: 11.0 - 14.0 ft BLS
Water Level
time:
gal i5 �,. ��
Purge Parameters continue on grHd below, if necessa
Bails
pH
(S.U.$)
Sp. Cond.
(PS/CM)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
D ry"a
Comments- Purge Volume
(gal)
1st Bait
(�.
2q
^ ILI.�
�-1."3
23 A
Lk. t 6
2ndWell Volume
Volume
G 6 b
S isT
^
3.3s-
2L - o
�� LIA i �
3'd We
Volume
-
Sample Collection Date/Time:
`1'-1c1-27- 2fI�
Delayed Metals Collection Date/Time: -1-2c 2.7_ 0'-c.=)
Turbidity during Metals Collection: _Lta 7
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on ice/cooler
Lab Anal is
Container 7 e
No. of Containers
Preservation
❑
8250D A I
VOAs
3
HCf
❑
8260D SIM ID
VOAs
3
HCI
;
Notes/ Maps etc.
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
I:04Al25M-PITT COUNTY\25101 - LAN DFILL\M ETHODS & BLANK WELL SAMPLING FORMSjWELL SAMPLING FORM-BAIIING�-20220124DOCX

17.
lS�
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date:
All wells 2" in diameter. Use r = 0.083 feet App H collected every other July starting in 2022.
Sample ID: P17 Field Team Members: Cn ", C6
Field Staff Initials Duties (check all that apply)
❑ Notes 2-Water Level f'Field Parameters Er -Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: Q--�Appendix I Er Appendix 11 ❑ Delayed Metals?
Sample Type: O�-­Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑PVC Bailer ❑ Teflon Sailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 15.08 ft Diameter:
Water Level: 5 .. ft Water Level Date: 1-
Water Column a ft 3 Well Volume
2 in Screen interval: 8.0 -11.0 ft BLS
Water Level
-2 time: -7
gal 1'�s�
Purge Parameters continue on grid below, if necessary)
Baits
pH
(S.U.$)
Sp. Cond.
(i,S/cm)
DRP
(mvoits)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
Dry?
ry'
Comments- Purge Volume
(gal)
1st Bail
2:.L,
lk.S ;
2,1-7
2"a Weil
Volume
S. 1-7
-7
1 `s
3'd Well
Volume
Sample Collection Date/Time: I 12D I 1-2.
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
El All samples preserved
El All samples placed on ice/cooler
Notes/Maps etc.:
tq•.3Y
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
825OD A I
VOAs
3
HCI
❑
825OD SIM ID
1 4-dioxane
VOAs
3
HCI
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
I Amber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h *Use Teflon hailers for delayed metals
Z:\GMAV51>5(-PITT COUNM25101 - LAN DFILLW EMODS & BLANK WELL SAMPLING FORMSjWELL SAMPLING FORM BAILING 20220I24AOCK

t5
GMA #25101 - Pitt County Landfill -- Sample Collection Field Sheet Date:-7-20•2�
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Sample ID: P19
Field Team Members:
Field Staff Initials Duties (check all that apply)
❑ Notes J:;]-VVater Level a --Field Parameters O sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: if- Appendix I C3— Appendix II ❑ Delayed Metals?
Sample Type: LY Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: L�PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 18.4 ft Diameter: 2 in Screen interval: 9.0 -13.0 ft BLS
Water Level
Water Level: ft Water Level Date: -z Z time:
Water Column 'i: l Lj ft 3 Well Volume gal 2 �--
Pur a Parameters continue on rid below if necessa
Bails
pH
(S.LI.$)
Sp. Cond.
(µS/cm)
ORP
{molts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTu)
7
Dry"
Comments- Purge Volume
(gal)
15t Bail
`'�.S`'�
j -v\
3�. L
�,z
2`5•�
ti,2
2"d Wei I
Volume
��ct�
2�-`�
-, .
7 ►�,
'2l.'Z
3"d Well
Volume
nn
Sample Collection Date/Time:-
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCI
❑
8260D SIM ID
i 4-dioxane
VOAs
3
HCI
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
n/a
= 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
Z:�GMA01)0(-PITT COUNTY\25101 - LANDFILL\METHODS & BLANK WELL SAMPLING FORMS\WELL SAMPLING FORM_$AILING ZOZZOI24.00"

1
6's
k*Z
GMA #25101- Pitt County Landfill — Sample Collection Field Sheet Date: -7 C� -?-L
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Sample ID: P20D Field Team Members: C-$S t WA
Field Staff Initials Duties (check all that apply)
❑ Notes ❑-Water Level C'Field Parameters ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: 9�— Appendix I 13— Appendix II ❑ Delayed Metals?
Sample Type: iT Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer ❑ Teflon Bailer Ci• Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 63.02 ft Diameter: 2 in Screen interval: 50.0 - 60.0 ft BLS
Water Level
Water Level: 11,til� ft Water Level Date: -Z*Z time: li s
Water Column S l. u L ft 3 Well Volume gal I �-- Z �, 1
Pure Parameters continue on grid below, if necessary)
Balls
pH
(S.U.$)
Sp. Cond.
(µS/cm)
DRP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(HTU)
D rY"a
Comments- Purge Volume
(gal)
ZA Ball
..
2"a Wei I
Volume
j 1
3rd Well
Volume
y�
D��
►. r
�.��
� •�
61-3
LS .
Sample Collection Date/Time: 1- 2:,11 C1= LO
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
El All samples preserved
❑ All samples placed on ice/cooler ❑ 8260p SIM ID
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container T
No. of Containers
Preservation
El
8260� A I
VOAs
3
HCl
14•dioxane
VOAs
3
HCI
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
2,\GMA�25ixx-Prrr couNTY12s101 - LAN0FILLftTKODS & BLANK WELL SAMPLING FORMSNWELL SAMPLING FORM -MU NG 20nO121.00C 4

GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date: -1 -
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
125�
',Z
Sample ID: P20R
Field Team Members: C, b1� t 1jw
Field Staff Initials Duties (check all that apply)
❑ Notes E-Water Level 2-Field Parameters 215ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: 2� Appendix I Ir Appendix II Er' --Delayed Metals?
Sample Type: [ Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: 2r�PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth +
Stickup (ft):
Well
33.51 ft Diameter:
Water Level: j-z ft Water Level Date:
Water Column 21. z6 ft 3 Well Volume
-7 -15.2 Z-
2 in Screen interval: 10.0 - 30.0 ft BLS
Water Level
time:
gal L�Z "�- A
Purge Parameters continue on grid below, if necessary)
Bails
PH
Sp. Cond.
ORP
DO
Temp
Turbidity
Dry?
Comments- Purge Volume
(S.U.$)
OAS/cm)
(mvolts)
(mg/1)
(OC)
(NTU)
(gal)
1st Bail
5 .c�C7
��6 i.-�
�-�
2'L ,
2"d Well-12
Volume
3"d Well
Volume
6 i6
-Z2g16
n
-Z5-o
Sample Collection Date/Time: _ -1`_� _ _ 16 to
Delayed Metals Collection Date/Time: -7-2-- 7 L 11''j Turbidity during Metals Collection:
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCi
0
8260D SIM ID
14-diaxane
VOAs
3
HCI
❑
App I Metals
250 m L Plastic
1
H NO3
❑
App R Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h *Use Teflon bailers for delayed metals
2:LGMA�251XX-PrTT COUWM25101 - LANDFILL�METHODS & BLANK WELL SAMPLING FORMS�WELL SAMPLING FORNLBAILING 20220124,AOQL

GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date: All wells wells 2" in diameter. Use r = 0,083 feet App II collected every other July starting in 2022.
1
1-16
.12
Sample ID: P28
Field Team Members: d
Field Staff Initials Duties (check all that apply)
❑ Notes [KrW- ater Level ❑-field Parameters 2-Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: D� Appendix I D3 Appendix II I�Delayed Metals?
Sample Type: Er— Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: 0-- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 10.94 ft Diameter: 2
Water Level: L-1-5 ft Water Level Date: -7-rk--2
Water Column L i`'1 ft 3 Well Volume
in Screen interval: 3.5 - 8.0 ft BLS
Water Level
time:
gal IZ
Purge Parameters continue on rid below,! necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µS1cm)
URP
(mvolts)
DU
(mg/1)
Temp
(°C)
Turbidity
(NTU)
?
Dry'
Comments- Purge Volume
(gal)
1A Bail
2"a Well
Volume
�i✓
3"d Well
Volume
.2p
6� a
17-.3'
Sample Collection Date/Time: —1 • VA-2�X E S '•2-
Delayed Metals Collection Date/Time: W Turbidity during Metals Collection: I-S6
Laboratory Analysis & Containers:
❑ All samples preserved
❑ All samples placed on icelcooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCI
❑
8260D SIM ID
14-dioxane
VOAs
3
HCI
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayer! metals
Z:\GMAWM-PiTT COUNTYV5101 - LANOFILL�MMODS & "K WELL SAMPLING FORMS�WELL SAMPLING FORM_MLING_20220IZ4.DM

GMA #25101 - Pitt County Landfill -- Sample Collection Field Sheet Date:
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Sample ID: P29
Field Team Members: CS-S NVtk
Field Staff initials Duties (checy all that apply)
El Notes Water Level Field Parameters Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: Appendix I ® Appendix II e�' Delayed Metals?
Sample Type: ®-- Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: IrPVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 14.96 ft Diameter: 2
Water Level: to ft Water Level Date:
Water Column �.9b h 3 Well Volume
in Screen interval: 7.0 - 12.0 ft BLS
Water Level
time: 6V-' )0
gal t 3
Purge Parameters continue on rid below if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
?
Dry'
Comments- Purge Volume
(gal)
1n Bail
L\.3
2nd Well
Volum
3"d Well
Sample Collection Date/Time: - ►°I Z2 'k=50 c ,,,
Delayed Metals Collection Date/Time: %ZL% Turbidity during Metals Collection: k 4•
Laboratory Analysis & Containers:
fl All samples preserved
dAll samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
a
8260D AppI
VOAs
3
HCi
8260D SIM ID
1 4-dioxane
VOAs
3
HCl
4�5
App I Metals
250 mL Plasbc
1
HNO3
�3
App II Pesticides
IL Amber
2
n/a
3 Vois (in gallons) = 70.5 rzh = 0A856745 * h
*Use Teflon bailers for delayed metals
Z:NGMA�25IXX-PUT COUNM5101 - LANDFIL LIMETHODS & RLANY. WELL SAMPLING FORMSIMLL SAMPUNG FORM_6A111NG-20220124.DDCK

Pitt County Landfill July Monitoring Event Field Sheet year; Collected By:
r•
Total Well
Q
Depth
Depth
Height of
Field Parameters
Date/Time
c
(including
to
Water
3 Well
Well
Specific
Water Purging
°
stickup) (ft
water
Column
Volumes
Gallons Bailed
Temp Conductance DO Turbidity
level completion/ Metals
Well
,`.°
BLS)
tftj
(h) (ft)
(gallons)
extracted Dry?
Baits pH (00 (µs) (mg/L) (ntu)
collected Velatfiles Sampling Sampling
Notes
y
+
5W1
All App 11,1,4-
N/A
N/A p ,�r
L Lk
q _
Ica•
dioxane
SW2
AI! App II, l,a-
N/A
NIA
(ta
'�;
�r7^C3
)
i7
dioxane
l
P21
App 11 8260D,
1,4-diN/A
3.4
1
J
L�r
/A
ind Vol:V
3rd Vol-
1st Ball:
�y."{
��.�
U �] \
V .4�
�` i
tr►:y�
� { �,Ij �Z
and Vol-
•
PZ2
App II 82600,
1,4.dioxane
3.4
�•Z 1
N/A
�Y
3rd Val:
1-�•3
FB
All App I1,1,4-
N/A
N/A
N/A
dioxane
t 5
ES
All App ll, 1,4-
N/A
N/A
N/A
dioxane
Lo ; ?56
Collect surface water Samples Facing upstream. Collect from point of confluence for 5W2.
EB: Pour lab DI water into bailer and over gloves and rope into ss pitcher then into sample containers.
FB: Use lab DI water to fill sample containers directly. Collect on -site preferably near the dirt road within the landfill to evaluate For possible field contaminants from road dust.
3 Well Volumes (in gallons) = 70.5 r2h = 0.4856745 * h All wells 2 inch diameter. Use r = 0.083 feet One 3-foot bailer = 0.27 gal GMA
Page 1ofI

APPENDIX C
LABORATORY REPORT AND CHAIN -OF -CUSTODY
FORMS FOR WATER SAMPLES

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, August 4, 2022
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill
ENCO Workorder(s): CF10299
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, July 21, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 1 46

(� �Eo
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1304
Lab ID: CF10299-01
Sampled: 07/20/22 13:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:18
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
14:48
EPA 7470A
EPA 245.1
08/17/22
07/22/22
16:58
07/26/22
03:10
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
13:49
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
13:49
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
14:08
EPA 8260D
EPA 5030B_MIS
08/03/22
07/27/22
14:23
07/29/22
13:11
EPA 8270E
EPA 3510C MS
07/27/22
09/04/22
07/26/22
22:04
07/28/22
14:57
EPA 9014
Same
08/03/22
07/29/22
09:52
08/01/22
10:07
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1204
Lab ID: CF10299-01RE1
Sampled: 07/20/22 13:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
14:24
Client ID: 7401-MW6R
Lab ID: CF10299-02
Sampled: 07/20/22 11:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
14:02
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
14:02
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
14:33
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22
14:23
07/29/22
13:40
EPA 8270E
EPA 3510C—MS
07/27/22
09/04/22
07/26/22
22:04
07/28/22
15:27
EPA 9014
Same
08/03/22
07/29/22
09:52
08/01/22
10:08
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-MW6R
Lab ID: CF10299-02RE1
Sampled: 07/20/22 11:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/03/22
07/28/22
10:10
07/28/22
18:42
Client ID: 7401-P11R
Lab ID: CF10299-03
Sampled: 07/19/22 14:50
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/15/23
07/22/22
14:11
08/01/22
12:25
EPA 6020E
EPA 3005A
01/15/23
07/22/22
14:15
07/28/22
14:52
EPA 7470A
EPA 245.1
08/16/22
07/22/22
16:58
07/26/22
03:12
EPA 8081E
EPA 3510C
07/26/22
09/04/22
07/26/22
09:34
07/27/22
14:15
EPA 8082A
EPA 3510C
07/19/23
09/04/22
07/26/22
09:43
07/27/22
14:15
EPA 8151A
EPA 3510C
07/26/22
09/03/22
07/25/22
11:45
07/28/22
14:59
EPA 8260D
EPA 503013_MS
08/02/22
07/27/22
14:14
07/28/22
00:20
EPA 8270E
EPA 3510C MS
07/26/22
09/03/22
07/25/22
07:57
07/25/22
14:24
EPA 9014
Same
08/02/22
07/27/22
09:51
07/28/22
10:44
SM 4500S2 D-2011
NO PREP
07/26/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-P11R
Lab ID: CF10299-03RE1
Sampled: 07/19/22 14:50
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/02/22
07/28/22
10:10
07/28/22
17:50
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 146

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1332
Lab ID: CF10299-04
Sampled: 07/20/22 14:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:41
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
14:56
EPA 7470A
EPA 245.1
08/17/22
07/22/22
16:58
07/26/22
03:14
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
14:29
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
14:29
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
15:24
EPA 8260D
EPA 5030B_MIS
08/03/22
07/27/22
14:23
07/29/22
14:09
EPA 8270E
EPA 3510C MS
07/27/22
09/04/22
07/26/22
22:04
07/28/22
15:57
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
10:46
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1212
Lab ID: CF10299-04RE1
Sampled: 07/20/22 14:00
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
14:50
Client ID: 7401-P16R
Lab ID: CF10299-05
Sampled: 07/19/22 14:15
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8081E
EPA 3510C
07/26/22
09/04/22
07/26/22
09:34
07/27/22
14:42
EPA 8082A
EPA 3510C
07/19/23
09/04/22
07/26/22
09:43
07/27/22
14:42
EPA 8151A
EPA 3510C
07/26/22
09/03/22
07/25/22
11:45
07/28/22
15:49
EPA 8260D
EPA 503013_MS
08/02/22
07/27/22
14:14
07/28/22
00:48
EPA 8270E
EPA 3510C—MS
07/26/22
09/03/22
07/25/22
07:57
07/25/22
14:54
EPA 9014
Same
08/02/22
07/27/22
09:51
07/28/22
10:48
SM 4500S2 D-2011
NO PREP
07/26/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-131611
Lab ID: CF10299-05RE1
Sampled: 07/19/22 14:15
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/02/22
07/28/22
10:10
07/28/22
19:08
Client ID: 7401-131611-M
Lab ID: CF10299-06
Sampled: 07/20/22 12:03
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:43
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
15:00
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
02:38
Client ID: 7401-1217
Lab ID: CF10299-07
Sampled: 07/20/22 14:38
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:46
EPA 6020B
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
15:05
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:04
EPA 8081B
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
15:08
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
15:08
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
16:14
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22
14:23
07/29/22
14:38
EPA 8270E
EPA 3510C MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
15:24
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
10:50
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1317
Lab ID: CF10299-07RE1
Sampled: 07/20/22 14:38
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
18:16
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 146

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1339
Lab ID: CF10299-08
Sampled: 07/20/22 14:47
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:48
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
15:09
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:06
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
15:22
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
15:22
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
16:39
EPA 8260D
EPA 5030B_MIS
08/03/22
07/27/22
14:23
07/29/22
15:07
EPA 8270E
EPA 3510C MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
15:53
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
10:51
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1219
Lab ID: CF10299-08RE1
Sampled: 07/20/22 14:47
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
19:33
Client ID: 7401-P20R
Lab ID: CF10299-09
Sampled: 07/19/22 16:10
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8081E
EPA 3510C
07/26/22
09/04/22
07/26/22
09:34
07/27/22
15:35
EPA 8082A
EPA 3510C
07/19/23
09/04/22
07/26/22
09:43
07/27/22
15:35
EPA 8151A
EPA 3510C
07/26/22
09/03/22
07/25/22
11:45
07/28/22
17:04
EPA 8260D
EPA 503013_MS
08/02/22
07/27/22
14:14
07/28/22
01:17
EPA 8270E
EPA 3510C—MS
07/26/22
09/03/22
07/25/22
07:57
07/25/22
16:23
EPA 9014
Same
08/02/22
07/27/22
09:51
07/28/22
10:57
SM 4500S2 D-2011
NO PREP
07/26/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1320R
Lab ID: CF10299-09RE2
Sampled: 07/19/22 16:10
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/02/22
07/29/22
11:52
07/29/22
15:14
Client ID: 7401-P20R-M
Lab ID: CF10299-10
Sampled: 07/20/22 11:47
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
11:50
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
15:13
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:16
Client ID: 7401-P20D
Lab ID: CF10299-11
Sampled: 07/20/22 09:10
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
12:32
EPA 6020B
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
15:22
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:11
EPA 8081B
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
15:48
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
15:48
EPA 8151A
EPA 3510C
07/27/22
09/03/22
07/25/22
11:45
07/28/22
17:29
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22
14:23
07/29/22
15:36
EPA 8270E
EPA 3510C MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
16:53
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
10:58
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-1320D
Lab ID: CF10299-11RE1
Sampled: 07/20/22 09:10
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6020E
EPA 3005A
01/16/23
07/22/22
14:15
07/28/22
16:06
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
15:16
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 1 46

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1328
Lab ID: CF10299-12
Sampled: 07/19/22 15:25
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8081B
EPA 3510C
07/26/22 09/04/22
07/26/22 09:34
07/27/22 16:01
EPA 8082A
EPA 3510C
07/19/23 09/04/22
07/26/22 09:43
07/27/22 16:01
EPA 8151A
EPA 3510C
07/26/22 09/03/22
07/25/22 11:45
07/28/22 17:54
EPA 8260D
EPA 503013_MS
08/02/22
07/27/22 14:14
07/28/22 01:46
EPA 8270E
EPA 3510C MS
07/26/22 09/03/22
07/25/22 07:57
07/25/22 17:22
EPA 9014
Same
08/02/22
07/27/22 09:51
07/28/22 11:00
SM 4500S2 D-2011
NO PREP
07/26/22
07/26/22 08:10
07/26/22 08:23
Client ID: 7401-P28
Lab ID: CF10299-12RE1
Sampled: 07/19/22 15:25
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 8260D
EPA 503013_MS
08/02/22
07/28/22 10:10
07/28/22 15:41
Client ID: 7401-P28-M
Lab ID: CF10299-13
Sampled: 07/20/22 11:55
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22 14:11
08/01/22 12:35
EPA 6020B
EPA 3005A
01/16/23
07/22/22 14:15
07/28/22 15:50
EPA 7470A
EPA 245.1
08/17/22
07/27/22 04:23
07/29/22 03:19
Client ID: 7401-1329
Lab ID: CF10299-14
Sampled: 07/19/22 09:50
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8081B
EPA 3510C
07/26/22 09/04/22
07/26/22 09:34
07/27/22 16:15
EPA 8082A
EPA 3510C
07/19/23 09/04/22
07/26/22 09:43
07/27/22 16:15
EPA 8151A
EPA 3510C
07/26/22 09/03/22
07/25/22 11:45
07/28/22 18:19
EPA 8260D
EPA 503013_MS
08/02/22
07/27/22 14:14
07/28/22 02:14
EPA 9014
Same
08/02/22
07/27/22 09:51
07/28/22 11:01
SM 4500S2 D-2011
NO PREP
07/26/22
07/26/22 08:10
07/26/22 08:23
Client ID: 7401-1329
Lab ID: CF10299-14RE1
Sampled: 07/19/22 09:50
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
08/02/22
07/28/22 10:10
07/28/22 19:59
EPA 8270E
EPA 3510C MS
07/26/22 09/03/22
07/25/22 07:57
07/26/22 17:13
Client ID: 7401-P29-M
Lab ID: CF10299-15
Sampled: 07/20/22 12:11
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6010D
EPA 3005A
01/16/23
07/22/22 14:11
08/01/22 12:37
EPA 6020B
EPA 3005A
01/16/23
07/22/22 14:15
07/28/22 15:54
EPA 7470A
EPA 245.1
08/17/22
07/27/22 04:23
07/29/22 03:22
Client ID: 7401-PZ1
Lab ID: CF10299-16
Sampled: 07/20/22 15:20
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22 14:23
07/29/22 16:05
Client ID: 7401-PZ3
Lab ID: CF10299-16RE1
Sampled: 07/20/22 15:20
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22 10:10
07/28/22 16:33
Client ID: 7401-PZ2
Lab ID: CF10299-17
Sampled: 07/20/22 15:00
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/03/22
07/27/22 14:23
07/29/22 16:34
Client ID: 7401-PZ2
Lab ID: CF10299-17RE1
Sampled: 07/20/22 15:00
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22 10:10
07/28/22 16:59
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 146

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-SW3
Lab ID: CF10299-18
Sampled: 07/20/22 16:25
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
12:39
EPA 6020E
EPA 3005A
01/16/23
07/25/22
05:39
08/01/22
11:40
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:24
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
16:28
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
16:28
EPA 8151A
EPA 3510C
07/27/22
09/05/22
07/27/22
07:45
08/02/22
22:41
EPA 8270E
EPA 3510C MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
18:22
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
11:03
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-SW1
Lab ID: CF10299-18RE1
Sampled: 07/20/22 16:25
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
16:07
EPA 8260D
EPA 503013_MS
08/03/22
08/01/22
19:22
08/02/22
02:54
Client ID: 7401-SW2
Lab ID: CF10299-19
Sampled: 07/20/22 15:50
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
12:42
EPA 6020B
EPA 3005A
01/16/23
07/25/22
05:39
08/01/22
11:45
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:32
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
16:41
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
16:41
EPA 8151A
EPA 3510C
07/27/22
09/05/22
07/27/22
07:45
08/02/22
23:06
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22
14:23
07/29/22
17:32
EPA 8270E
EPA 3510C MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
18:51
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
11:05
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-SW2
Lab ID: CF10299-19RE1
Sampled: 07/20/22 15:50
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
17:25
Client ID: 7401-EB
Lab ID: CF10299-20
Sampled: 07/20/22 10:30
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22
14:11
08/01/22
12:44
EPA 6020E
EPA 3005A
01/16/23
07/25/22
05:39
08/01/22
11:49
EPA 7470A
EPA 245.1
08/17/22
07/27/22
04:23
07/29/22
03:34
EPA 8081E
EPA 3510C
07/27/22
09/04/22
07/26/22
09:34
07/27/22
16:54
EPA 8082A
EPA 3510C
07/20/23
09/04/22
07/26/22
09:43
07/27/22
16:54
EPA 8151A
EPA 3510C
07/27/22
09/05/22
07/27/22
07:45
08/02/22
23:32
EPA 8260D
EPA 503013_MS
08/03/22
07/27/22
14:23
07/29/22
10:19
EPA 8270E
EPA 3510C—MS
07/27/22
09/03/22
07/25/22
07:57
07/25/22
19:21
EPA 9014
Same
08/03/22
07/27/22
09:51
07/28/22
11:06
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22
08:10
07/26/22
08:23
Client ID: 7401-EB
Lab ID: CF10299-20RE1
Sampled: 07/20/22 10:30
Received: 07/21/22
10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22
10:10
07/28/22
13:07
EPA 8260D
EPA 503013_MS
08/03/22
08/01/22
19:22
08/02/22
01:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 146

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-FB
Lab ID: CF10299-21
Sampled: 07/20/22 15:20
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22 14:11
08/01/22 12:46
EPA 6020E
EPA 3005A
01/16/23
07/25/22 05:39
08/01/22 11:53
EPA 7470A
EPA 245.1
08/17/22
07/27/22 04:23
07/29/22 03:37
EPA 8081E
EPA 3510C
07/27/22 09/04/22
07/26/22 09:34
07/27/22 17:07
EPA 8082A
EPA 3510C
07/20/23 09/04/22
07/26/22 09:43
07/27/22 17:07
EPA 8151A
EPA 3510C
07/27/22 09/05/22
07/27/22 07:45
08/02/22 23:57
EPA 8270E
EPA 3510C MS
07/27/22 09/03/22
07/25/22 07:57
07/25/22 19:50
EPA 9014
Same
08/03/22
07/22/22 10:04
07/25/22 09:54
SM 4500S2 D-2011
NO PREP
07/27/22
07/26/22 08:10
07/26/22 08:23
Client ID: 7401-FB
Lab ID: CF10299-21RE1
Sampled: 07/20/22 15:20
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
08/03/22
07/28/22 10:10
07/28/22 13:33
EPA 8260D
EPA 503013_MS
08/03/22
08/01/22 19:22
08/02/22 01:56
Client ID: 7401-TB
Lab ID: CF10299-22
Sampled: 07/19/22 09:50
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
08/02/22
07/27/22 14:14
07/27/22 21:56
Client ID: 7401-MW6R-M
Lab ID: CF10299-23
Sampled: 07/20/22 15:30
Received: 07/21/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
01/16/23
07/22/22 14:11
08/01/22 12:49
EPA 6020B
EPA 3005A
01/16/23
07/25/22 05:39
08/01/22 11:57
EPA 7470A
EPA 245.1
08/17/22
07/27/22 04:23
07/29/22 03:39
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 1 4G

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SAMPLE DETECTION SUMMARY
Client ID: 7401-PO4
Lab ID:
CF10299-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
104
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.209
J
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
10.5
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-MW6R
Lab ID:
CF10299-02
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Acetone
35
10
20
uq/L
EPA 8260D
I Client ID: 7401-MW6R Lab ID: CF10299-02RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
7.0
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-P11R
Lab ID:
CF10299-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
150
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
2.78
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
5.98
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
6.07
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
7.58
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
4.77
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
10.9
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
110
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1312
Lab ID:
CF10299-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
71.5
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.78
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
9.09
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1312
Lab ID:
CF10299-04RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.6
J
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-11316R
Lab ID:
CF10299-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
2-Butanone
7.6
1.3
5.0
ug/L
EPA 8260D
Acetone
34
10
20
ug/L
EPA 8260D
Benzene
3.0
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
1.8
0.17
1.0
ug/L
EPA 8260D
Toluene
0.54
J
0.14
1.0
ug/L
EPA 8260D
Client ID: 7401-P16R
Lab ID:
CF10299-05RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
83
D
4.0
10
ug/L
EPA 8260D
Client ID: 7401-1316R-M
Lab ID:
CF10299-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1090
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.49
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
2.67
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
10.6
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
4.75
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1317
Lab ID:
CF10299-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
227
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.83
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
1.9
0.17
1.0
ug/L
EPA 8260D
Chromium - Total
2.92
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.40
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
2.26
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
3.61
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
5.82
J
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 146

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SAMPLE DETECTION SUMMARY
Client ID: 7401-P17 Lab ID: CF10299-07RE1
Analvte Results Flag MDL Q Units Method Notes
1,4-Dioxane 3.9 0.80 2.0 uq/L EPA 8260D
I Client ID: 7401-P19 Lab ID: CF10299-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,1-Dichloroethane
4.1
0.13
1.0
ug/L
EPA 8260D
1,4-Dichlorobenzene
6.3
0.19
1.0
ug/L
EPA 8260D
Barium - Total
1970
1.10
10.0
ug/L
EPA 6010D
Benzene
4.2
0.15
1.0
ug/L
EPA 8260D
Beryllium - Total
14.4
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
17
0.17
1.0
ug/L
EPA 8260D
cis-1,2-Dichloroethene
2.4
0.15
1.0
ug/L
EPA 8260D
Cobalt - Total
18.3
1.40
10.0
ug/L
EPA 6010D
Ethylbenzene
1.6
0.13
1.0
ug/L
EPA 8260D
Lead - Total
5.35
J
3.10
10.0
ug/L
EPA 6010D
Mercury - Total
1.06
0.150
0.200
ug/L
EPA 7470A
Naphthalene
1.5
0.11
1.0
ug/L
EPA 8260D
Nickel- Total
26.1
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
1.84
J
1.82
2.00
ug/L
EPA 6020E
Toluene
0.51
J
0.14
1.0
ug/L
EPA 8260D
Vinyl chloride
0.75
J
0.32
1.0
ug/L
EPA 8260D
Zinc - Total
107
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P19
Lab ID:
CF10299-08RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
160
D
4.0
10
ug/L
EPA 8260D
Client ID: 7401-P20R
Lab ID:
CF10299-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,1-Dichloroethane
0.51
J
0.13
1.0
ug/L
EPA 8260D
1,4-Dichlorobenzene
3.8
0.19
1.0
ug/L
EPA 8260D
Benzene
2.2
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
1.6
0.17
1.0
ug/L
EPA 8260D
Diethyl phthalate
3.4
J
2.4
10
ug/L
EPA 8270E
Naphthalene
1.5
0.11
1.0
ug/L
EPA 8260D
o-Xylene
1.1
0.065
1.0
ug/L
EPA 8260D
Xylenes (Total)
1.1
1
0.45
3.0
ug/L
EPA 8260D
Client ID: 7401-P20R
Lab ID:
CF30299-09RE2
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
79
D
4.0
10
ug/L
EPA 8260D
Client ID: 7401-P20R-M
Lab ID:
CF10299-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
842
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.957
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.84
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
8.56
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-P20D
Lab ID:
CF10299-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
99.7
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
7.96
0.160
1.00
ug/L
EPA 6010D
Cadmium - Total
0.819
J
0.360
1.00
ug/L
EPA 6010D
Chromium - Total
9.93
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
2.40
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
4.82
J
3.10
10.0
ug/L
EPA 6010D
Toluene
1.9
0.14
1.0
ug/L
EPA 8260D
Vanadium - Total
9.79
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
17.9
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P20D
Lab ID:
CF10299-11RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
0.87
J
0.80
2.0
ug/L
EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 146

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SAMPLE DETECTION SUMMARY
Client ID: 7401-P28 Lab ID: CF10299-12RE1
Analvte Results Flag MDL PQL Units Method Notes
1,4-Dioxane 0.84 J 0.80 2.0 uq/L EPA 8260D
I Client ID: 7401-P28-M Lab ID: CF10299-13
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
34.6
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.721
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.79
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.82
J
1.40
10.0
ug/L
EPA 6010D
Vanadium - Total
2.92
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
13.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P29
Lab ID:
CF10299-14
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
1,4-Dichlorobenzene
1.9
0.19
1.0
ug/L
EPA 8260D
Benzene
2.0
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
13
0.17
1.0
ug/L
EPA 8260D
Naphthalene 1.6 0.11 1.0 ug/L EPA 8260D
Client ID: 7401-P29 Lab ID: CF10299-14RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
140
D
4.0
10
ug/L
EPA 8260D
Client ID: 7401-P29-M
Lab ID:
CF10299-15
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
370
1.10
10.0
ug/L
EPA 6010D
Vanadium - Total
9.16
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-PZ1
Lab ID:
CF10299-16RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.1
J
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-SW1
Lab ID:
CF10299-18
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
35.9
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
6.96
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW3
Lab ID:
CF10299-18RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Chloroform
5.2
0.18
1.0
ug/L
EPA 8260D
Toluene
0.70
J
0.14
1.0
ug/L
EPA 8260D
Client ID: 7401-SW2
Lab ID:
CF10299-19
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
71.0
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.33
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
2.57
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-EB
Lab ID:
CF10299-20
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
N-Nitrosodiethylamine
5.1
J
2.1
10
ug/L
EPA 8270E
Toluene
1.3
0.14
1.0
ug/L
EPA 8260D
Zinc - Total
8.54
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-EB
Lab ID:
CF10299-20RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Carbon disulfide
170
1.5
5.0
uq/L
EPA 8260D
Client ID: 7401-FB
Lab ID:
CF10299-21
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Barium - Total
448
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
1.43
J 1.40
10.0
ug/L
EPA 6010D
Nickel - Total
10.2
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
80.2
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 of 46

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www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 7401-FB
Lab ID:
CF10299-21RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.2
J
0.80
2.0
ug/L
EPA 8260D
Carbon disulfide
3.4
J
1.5
5.0
ug/L
EPA 8260D
Client ID: 7401-TB
Lab ID:
CF10299-22
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Methylene chloride
0.59
J
0.23
1.0
ug/L
EPA 8260D
0-01
Client ID: 7401-MW6R-M
Lab ID:
CF10299-23
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
2010
1.10
10.0
ug/L
EPA 6010D
Copper - Total
2.20
J
1.60
10.0
ug/L
EPA 6010D
Zinc - Total
14.4
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 146

0Nk"q09
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ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 13:11
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 13:11
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 13:11
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 13:11
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 12 Of 146

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www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 13:11
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 13:11
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 13:11
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 13:11
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
58
1
50.0
115 %
53-136
2G27031
EPA 8260D
07129122 13:11
RKY
Dibromofluoromethane
66
1
50.0
132 %
67-129
2G27031
EPA 8260D
0712912213:11
RKY QS-03
Toluene-d8
57
1
50.0
114 %
59-134
2G27031
EPA 6260D
0712912213:11
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G26033
EPA 8270E
07/28/22 14:57
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
2-Methylnaphthalene [91-57-6]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
2-Methylphenol[95-48-7]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
2-Naphthylamine[91-59-8]A
3.0
u
ug/L
1
3.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
2-Nitroaniline [88-74-4]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
2-Nitrophenol[88-75-5]A
1.1
u
ug/L
1
1.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
3,3'-Dimethylbenzidine [119-93-71A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
3-Methylcholanthrene [56-49-5]A
1.3
u
ug/L
1
1.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
3-Nitroaniline [99-09-2]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Aminobiphenyl[92-67-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Chloroaniline [106-47-8]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Nitroaniline [100-01-6]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
4-Nitrophenol[100-02-7]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
5-Nitro-o-toluidine [99-55-8]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
7,12-Dimethylbenz(a)anthracene
1.4
u
ug/L
1
1.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
[57-97-6]A
a,a-Dimethylphenethylamine [122-09-8]A
3.5
U
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Acetophenone [98-86-2]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Anthracene[120-12-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzo(a)anthracene [56-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzo(a)pyrene [50-32-8]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzo(g,h,i)perylene[191-24-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzo(k)fluoranthene[207-08-9]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Benzyl alcohol [100-51-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
u
ug/L
1
1.9
5.0
2G26033
EPA
8270E
07/28/22
14:57
DFM
Butylbenzylphthalate [85-68-7]A
3.8
u
ug/L
1
3.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Chlorobenzilate [510-15-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Chrysene [218-01-9]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Diallate [2303-16-4]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Dibenzofuran [132-64-9]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Diethylphthalate [84-66-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Dimethoate [60-51-5]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Disulfoton [298-04-4]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified anaiyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Notes
Ethyl methanesulfonate [62-50-0]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Famphur[52-85-7]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Fluoranthene[206-44-0]A
3.1
u
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Fluorene [86-73-7]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Hexachlorobenzene[118-74-1]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Hexachlorobutadiene [87-68-3]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Hexachloroethane [67-72-1]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Hexachloropropene[1888-71-7]A
6.8
u
ug/L
1
6.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Isodrin [465-73-6]A
1.5
u
ug/L
1
1.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Isophorone[78-59-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Isosafrole [120-58-1]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Kepone[143-50-0]A
7.2
u
ug/L
1
7.2
20
2G26033
EPA
8270E
07/28/22
14:57
DFM
Methapyrilene [91-80-5]A
4.8
u
ug/L
1
4.8
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Methyl Methanesulfonate [66-27-3]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Methyl parathion [298-00-0]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Nitrobenzene [98-95-3]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitrosodiethylamine [55-18-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitrosodi-n-butylamine [924-16-3]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
[86-30-6/122-39-4]A
N-Nitrosomethylethylamine [10595-95-6]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitrosopiperidine [100-75-4]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
N-Nitrosopyrrolidine [930-55-2]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
[126-68-1]A
o-Toluidine [95-53-4]A
1.6
u
ug/L
1
1.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Parathion [56-38-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
p-Dimethylaminoazobenzene [60-11-7]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Pentachlorobenzene [608-93-5]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Pentachloronitrobenzene [82-68-8]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Phenacetin [62-44-2]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Phenanthrene [85-01-8]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Phenol[108-95-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Phorate[298-02-2]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Pronamide [23950-58-5]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Pyrene [129-00-0]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Safrole [94-59-7]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Thionazin [297-97-2]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
14:57
DFM
Surrogates
Resu/ts
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed By Notes
2,4,6-Tribromophenol
77
1
100
77 %
10-179
2G26033
EPA 8270E
0712812214:57 DFM
2-Fluorobiphenyl
39
1
50.0
77 %
10-149
2G26033
EPA 8270E
0712812214:57 DFM
2-Fluorophenol
50
1
100
50 %
10-110
2G26033
EPA 8270E
0712812214:57 DFM
Nitrobenzene-d5
38
1
50.0
77 %
10-149
2G26033
EPA 8270E
0712812214:57 DFM
FINAL
This report relates only
to the
sample as received
by the laboratory, and may only
be reproduced in full.
I Page 15 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
41
1
100
41 %
10-88
2G26033
EPA 8270E
07126122 14:57
DFM
Terphenyl-d14
35
1
50.0
70 %
10-188
2G26033
EPA 8270E
0712812214:57
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 13:49
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 13:49
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 13:49
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.56
1
1.00
56 %
10-139
2G26009
EPA 8081E
0712712213:49
LSK
Decachlorobiphenyl
0.53
1
1.00
53 %
10-122
2G26009
EPA 8081E
0712712213:49
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 13:49
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.52
1
1.00
52 %
10-128
2G26010
EPA 80824
0712712213:49
L5K
Decachlorobiphenyl
0.59
1
1.00
59 %
10-129
2G26010
EPA 80824
0712712213:49
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PO4 Lab Sample ID:CF10299-01 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 13:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G22028
EPA 7470A
07/26/22 03:10
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 14:48
MAM
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Barium [7440-39-3]^
104
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Beryllium [7440-41-7]^
0.209
J
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:18
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:18
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 14:48
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 14:48
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Zinc[7440-66-6]^
10.5
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:18
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G29021
EPA 9014
08/01/22 10:07
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte KAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 14:24
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
3.8
1
5.00
75 %
75-125
2G26006
EPA 8260D
0712812214:24
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 14:08
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 14:08
FCV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 14:08
FCV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 14:08
FCV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 14:08
FCV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2,4-DC4A
2.0
1
2.00
100 %
37-134
2G25024
EPA 8151A
0712612214:08
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Acetone [67-64-1]A
3S
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 13:40
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 13:40
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 13:40
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 13:40
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 18 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 13:40
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 13:40
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 13:40
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 13:40
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
60
1
50.0
120 %
53-136
2G27031
EPA 8260D
07129122 13:40
RKY
Dibromofluoromethane
64
1
50.0
129 %
67-129
2G27031
EPA 8260D
0712912213:40
RKY
Toluene-d8
58
1
50.0
116 %
59-134
2G27031
EPA 6260D
0712912213:40
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G26033
EPA 8270E
07/28/22 15:27
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
2-Methylnaphthalene [91-57-6]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
2-Methylphenol[95-48-7]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
2-Naphthylamine[91-59-8]A
3.0
u
ug/L
1
3.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
2-Nitroaniline [88-74-4]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
2-Nitrophenol[88-75-5]A
1.1
u
ug/L
1
1.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
3,3'-Dimethylbenzidine [119-93-71A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
3-Methylcholanthrene [56-49-5]A
1.3
u
ug/L
1
1.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
3-Nitroaniline [99-09-2]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Aminobiphenyl[92-67-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Chloroaniline [106-47-8]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Nitroaniline [100-01-6]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
4-Nitrophenol[100-02-7]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
5-Nitro-o-toluidine [99-55-8]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
7,12-Dimethylbenz(a)anthracene
1.4
u
ug/L
1
1.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
[57-97-6]A
a,a-Dimethylphenethylamine [122-09-8]A
3.5
U
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Acetophenone [98-86-2]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Anthracene[120-12-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzo(a)anthracene [56-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzo(a)pyrene [50-32-8]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzo(g,h,i)perylene[191-24-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzo(k)fluoranthene[207-08-9]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Benzyl alcohol [100-51-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
u
ug/L
1
1.9
5.0
2G26033
EPA
8270E
07/28/22
15:27
DFM
Butylbenzylphthalate [85-68-7]A
3.8
u
ug/L
1
3.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Chlorobenzilate [510-15-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Chrysene [218-01-9]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Diallate [2303-16-4]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Dibenzofuran [132-64-9]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Diethylphthalate [84-66-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Dimethoate [60-51-5]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Disulfoton [298-04-4]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified anaiyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Notes
Ethyl methanesulfonate [62-50-0]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Famphur[52-85-7]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Fluoranthene[206-44-0]A
3.1
u
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Fluorene [86-73-7]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Hexachlorobenzene[118-74-1]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Hexachlorobutadiene [87-68-3]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Hexachloroethane [67-72-1]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Hexachloropropene[1888-71-7]A
6.8
u
ug/L
1
6.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Isodrin [465-73-6]A
1.5
u
ug/L
1
1.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Isophorone[78-59-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Isosafrole [120-58-1]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Kepone[143-50-0]A
7.2
u
ug/L
1
7.2
20
2G26033
EPA
8270E
07/28/22
15:27
DFM
Methapyrilene [91-80-5]A
4.8
u
ug/L
1
4.8
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Methyl Methanesulfonate [66-27-3]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Methyl parathion [298-00-0]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Nitrobenzene [98-95-3]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitrosodiethylamine [55-18-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitrosodi-n-butylamine [924-16-3]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
[86-30-6/122-39-4]A
N-Nitrosomethylethylamine [10595-95-6]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitrosopiperidine [100-75-4]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
N-Nitrosopyrrolidine [930-55-2]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
[126-68-1]A
o-Toluidine [95-53-4]A
1.6
u
ug/L
1
1.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Parathion [56-38-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
p-Dimethylaminoazobenzene [60-11-7]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Pentachlorobenzene [608-93-5]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Pentachloronitrobenzene [82-68-8]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Phenacetin [62-44-2]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Phenanthrene [85-01-8]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Phenol[108-95-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Phorate[298-02-2]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Pronamide [23950-58-5]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Pyrene [129-00-0]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Safrole [94-59-7]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Thionazin [297-97-2]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:27
DFM
Surrogates
Resu/ts
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vied ffy Notes
2,4,6-Tribromophenol
86
1
100
86 %
10-179
2G26033
EPA 8270E
0712812215:27 DFM
2-Fluorobiphenyl
34
1
50.0
68 %
10-149
2G26033
EPA 8270E
0712812215:27 DFM
2-Fluorophenol
46
1
100
46 %
10-110
2G26033
EPA 8270E
0712812215:27 DFM
Nitrobenzene-d5
35
1
50.0
70 %
10-149
2G26033
EPA 8270E
0712812215:27 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 21 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
46
1
100
46 %
10-88
2G26033
EPA 8270E
0712612215:27
DFM
Terphenyl-d14
28
1
50.0
57 %
10-188
2G26033
EPA 8270E
0712812215:27
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 14:02
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:02
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 14:02
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.86
1
1.00
86 %
10-139
2G26009
EPA 8081E
0712712214:02
LSK
Decachlorobiphenyl
0.69
1
1.00
69 %
10-122
2G26009
EPA 8081E
0712712214:02
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 14:02
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.52
1
1.00
52 %
10-128
2G26010
EPA 80824
0712712214:02
L5K
Decachlorobiphenyl
0.51
1
1.00
51 %
10-129
2G26010
EPA 80824
0712712214:02
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF10299-02 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Cyanide (total) [57-12-5]^ 0.0049
U
mg/L
1
0.0049
0.010
2G29021
EPA 9014
08/01/22 10:08
MSE
Sulfide [18496-25-8]^ 0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^ 7.0
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 18:42
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-d8
4.7
1
5.00
94 %
75-125
2G26006
EPA 8260D
0712612218:42
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
u
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 14:33
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
u
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 14:33
FCV
2,4-D [94-75-7]^
0.27
u
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 14:33
FCV
Dinoseb [88-85-7]^
0.32
u
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 14:33
FCV
Pentachlorophenol [87-86-5]^
0.19
u
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 14:33
FCV
Surrogates
Results
DF
Snike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
2,4-DC4A
2,2
1
2,00
110 %
37-134
2G25024
EPA 8151A
071281221433
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P11R Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27028
EPA 8260D
07/28/22 00:20
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 00:20
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27028
EPA 8260D
07/28/22 00:20
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27028
EPA 8260D
07/28/22 00:20
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 24 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/28/22 00:20
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/28/22 00:20
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 00:20
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/28/22 00:20
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
58
1
50.0
116 %
53-136
2G27026
EPA 8260D
07126122 00:20
RKY
Dibromofluoromethane
62
1
50.0
124 %
67-129
2G27026
EPA 8260D
07126122 00:20
RKY
Toluene-d8
56
1
50.0
112 %
59-134
2G27026
EPA 6260D
07128122 00:20
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P11R Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 14:24
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:24
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 26 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22 14:24
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:24
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
88
1
100
88 %
10-179
2G25005
EPA 8270E
0712512214:24 DFM
2-Fluorobiphenyl
40
1
50.0
81 %
10-149
2G25005
EPA 8270E
0712512214:24 DFM
2-Fluorophenol
61
1
100
61 %
10-110
2G25005
EPA 8270E
0712512214:24 DFM
Nitrobenzene-d5
41
1
50.0
81 %
10-149
2G25005
EPA 8270E
0712512214:24 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 27 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
50
1
100
50 %
10-88
2G25005
EPA 8270E
0712512214:24
DFM
Terphenyl-d14
41
1
50.0
82 %
10-188
2G25005
EPA 8270E
0712512214:24
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
4,4'-DDE [72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 14:15
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:15
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 14:15
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
2,4,5,6-TCMX
0.56
1
1.00
56 %
10-139
2G26009
EPA 8081E
0712712214:15
LSK
Decachlorobiphenyl
0.72
1
1.00
72 %
10-122
2G26009
EPA 8081E
0712712214:15
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 14:15
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.50
1
1.00
50 %
10-128
2G26010
EPA 80824
0712712214:15
L5K
Decachlorobiphenyl
0.77
1
1.00
77 %
10-129
2G26010
EPA 80824
0712712214:15
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CF10299-03 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G22028
EPA 7470A
07/26/22 03:12
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 14:52
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Barium [7440-39-3]^
150
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Beryllium [7440-41-7]^
2.78
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:25
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:25
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Cobalt[7440-48-4]^
5.98
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Copper[7440-50-8]^
6.07
J
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Lead [7439-92-1]^
7.58
J
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Nickel[7440-02-O]^
4.77
J
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 14:52
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 14:52
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Vanadium [7440-62-2]^
10.9
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Zinc[7440-66-6]^
110
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:25
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:44
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 17:50
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.4
1
5.00
88 %
75-125
2G26006
EPA 8260D
0712612217:50
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 14:59
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 14:59
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 14:59
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 14:59
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 14:59
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2,4-DC4A
23
1
200
117 %
37-134
2G25024
EPA 8151A
0712612214:59
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-1312 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 14:09
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 14:09
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 14:09
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 14:09
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 30 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 14:09
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 14:09
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 14:09
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 14:09
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
58
1
50.0
116 %
53-136
2G27031
EPA 8260D
07129122 14:09
RKY
Dibromofluoromethane
65
1
50.0
129 %
67-129
2G27031
EPA 8260D
0712912214:09
RKY
Toluene-d8
55
1
50.0
111 %
59-134
2G27031
EPA 6260D
0712912214:09
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G26033
EPA 8270E
07/28/22 15:57
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
2-Methylnaphthalene [91-57-6]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
2-Methylphenol[95-48-7]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
2-Naphthylamine[91-59-8]A
3.0
u
ug/L
1
3.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
2-Nitroaniline [88-74-4]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
2-Nitrophenol[88-75-5]A
1.1
u
ug/L
1
1.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
3,3'-Dimethylbenzidine [119-93-71A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
3-Methylcholanthrene [56-49-5]A
1.3
u
ug/L
1
1.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
3-Nitroaniline [99-09-2]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Aminobiphenyl[92-67-1]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Chloroaniline [106-47-8]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Nitroaniline [100-01-6]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
4-Nitrophenol[100-02-7]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
5-Nitro-o-toluidine [99-55-8]A
3.2
u
ug/L
1
3.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
7,12-Dimethylbenz(a)anthracene
1.4
u
ug/L
1
1.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
[57-97-6]A
a,a-Dimethylphenethylamine [122-09-8]A
3.5
U
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Acetophenone [98-86-2]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Anthracene[120-12-7]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzo(a)anthracene [56-55-3]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzo(a)pyrene [50-32-8]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzo(g,h,i)perylene[191-24-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzo(k)fluoranthene[207-08-9]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Benzyl alcohol [100-51-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
u
ug/L
1
1.9
5.0
2G26033
EPA
8270E
07/28/22
15:57
DFM
Butylbenzylphthalate [85-68-7]A
3.8
u
ug/L
1
3.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Chlorobenzilate [510-15-6]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Chrysene [218-01-9]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Diallate [2303-16-4]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Dibenzofuran [132-64-9]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Diethylphthalate [84-66-2]A
2.4
u
ug/L
1
2.4
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Dimethoate [60-51-5]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Disulfoton [298-04-4]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified anaiyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Notes
Ethyl methanesulfonate [62-50-0]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Famphur[52-85-7]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Fluoranthene[206-44-0]A
3.1
u
ug/L
1
3.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Fluorene [86-73-7]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Hexachlorobenzene[118-74-1]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Hexachlorobutadiene [87-68-3]A
2.8
u
ug/L
1
2.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Hexachloroethane [67-72-1]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Hexachloropropene[1888-71-7]A
6.8
u
ug/L
1
6.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Isodrin [465-73-6]A
1.5
u
ug/L
1
1.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Isophorone[78-59-1]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Isosafrole [120-58-1]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Kepone[143-50-0]A
7.2
u
ug/L
1
7.2
20
2G26033
EPA
8270E
07/28/22
15:57
DFM
Methapyrilene [91-80-5]A
4.8
u
ug/L
1
4.8
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Methyl Methanesulfonate [66-27-3]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Methyl parathion [298-00-0]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Nitrobenzene [98-95-3]A
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitrosodiethylamine [55-18-5]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitrosodi-n-butylamine [924-16-3]A
2.0
u
ug/L
1
2.0
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
[86-30-6/122-39-4]A
N-Nitrosomethylethylamine [10595-95-6]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitrosopiperidine [100-75-4]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
N-Nitrosopyrrolidine [930-55-2]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
[126-68-1]A
o-Toluidine [95-53-4]A
1.6
u
ug/L
1
1.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Parathion [56-38-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
p-Dimethylaminoazobenzene [60-11-7]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Pentachlorobenzene [608-93-5]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Pentachloronitrobenzene [82-68-8]A
1.9
u
ug/L
1
1.9
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Phenacetin [62-44-2]A
2.7
u
ug/L
1
2.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Phenanthrene [85-01-8]A
2.6
u
ug/L
1
2.6
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Phenol[108-95-2]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Phorate[298-02-2]A
2.1
u
ug/L
1
2.1
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Pronamide [23950-58-5]A
1.7
u
ug/L
1
1.7
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Pyrene [129-00-0]A
3.5
u
ug/L
1
3.5
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Safrole [94-59-7]A
2.2
u
ug/L
1
2.2
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Thionazin [297-97-2]A
2.3
u
ug/L
1
2.3
10
2G26033
EPA
8270E
07/28/22
15:57
DFM
Surrogates
Resu/ts
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vied By Notes
2,4,6-Tribromophenol
73
1
100
73 %
10-179
2G26033
EPA 8270E
0712812215:57 DFM
2-Fluorobiphenyl
35
1
50.0
70 %
10-149
2G26033
EPA 8270E
0712812215:57 DFM
2-Fluorophenol
41
1
100
41 %
10-110
2G26033
EPA 8270E
0712812215:57 DFM
Nitrobenzene-d5
32
1
50.0
65 %
10-149
2G26033
EPA 8270E
0712812215:57 DFM
FINAL
This report relates only
to the
sample as received
by the laboratory, and may only
be reproduced in full.
I Page 33 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
32
1
100
32 %
10-88
2G26033
EPA 8270E
0712612215:57
DFM
Terphenyl-d14
34
1
50.0
68 %
10-188
2G26033
EPA 8270E
0712812215:57
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 14:29
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:29
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 14:29
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.65
1
1.00
65 %
10-139
2G26009
EPA 8081E
0712712214:29
LSK
Decachlorobiphenyl
0.68
1
1.00
68 %
10-122
2G26009
EPA 8081E
0712712214:29
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 14:29
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.77
1
1.00
77 %
10-128
2G26010
EPA 80824
0712712214:29
L5K
Decachlorobiphenyl
0.76
1
1.00
76 %
10-129
2G26010
EPA 80824
0712712214:29
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF10299-04 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G22028
EPA 7470A
07/26/22 03:14
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 14:56
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Barium [7440-39-3]^
71.5
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Beryllium [7440-41-7]^
1.78
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:41
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:41
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 14:56
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 14:56
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Zinc[7440-66-6]^
9.09
J
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:41
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:46
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte KAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.6
J
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 14:50
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.2
1
5.00
84 %
75-125
2G26006
EPA 8260D
0712612214:50
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 15:24
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 15:24
FCV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 15:24
FCV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 15:24
FCV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 15:24
FCV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2,4-DC4A
2.0
1
2.00
100 %
37-134
2G25024
EPA 8151A
0712612215:24
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
2-Butanone [78-93-3]A
7.6
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Acetone [67-64-1]A
34
ug/L
1
10
20
2G27028
EPA 8260D
07/28/22 00:48
RKY
Acetonitrile [75-05-8]A
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 00:48
RKY
Acrolein [107-02-8]A
4.0
U
ug/L
1
4.0
10
2G27028
EPA 8260D
07/28/22 00:48
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2G27028
EPA 8260D
07/28/22 00:48
RKY
Benzene [71-43-2]A
3.0
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Chlorobenzene [108-90-7]A
1.8
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 36 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/28/22 00:48
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/28/22 00:48
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 00:48
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Toluene [308-88-3]^
0.54
J
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/28/22 00:48
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
62
1
50.0
125 %
53-136
2G27026
EPA 8260D
07126122 00:48
RKY
Dibromofluoromethane
58
1
50.0
115 %
67-129
2G27026
EPA 8260D
07126122 00:48
RKY
Toluene-d8
57
1
50.0
113 %
59-134
2G27026
EPA 6260D
07128122 00:48
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 14:54
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 14:54
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 38 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22 14:54
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 14:54
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
83
1
100
83 %
10-179
2G25005
EPA 8270E
0712512214:54 DFM
2-Fluorobiphenyl
40
1
50.0
79 %
10-149
2G25005
EPA 8270E
0712512214:54 DFM
2-Fluorophenol
65
1
100
65 %
10-110
2G25005
EPA 8270E
0712512214:54 DFM
Nitrobenzene-d5
41
1
50.0
82 %
10-149
2G25005
EPA 8270E
0712512214:54 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 39 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
57
1
100
57 %
10-88
2G25005
EPA 8270E
0712512214:54
DFM
Terphenyl-d14
23
1
50.0
47 %
10-188
2G25005
EPA 8270E
0712512214:54
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 14:42
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 14:42
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 14:42
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.76
1
1.00
76 %
10-139
2G26009
EPA 8081E
0712712214:42
LSK
Decachlorobiphenyl
0.75
1
1.00
75 %
10-122
2G26009
EPA 8081E
0712712214:42
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 14:42
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.83
1
1.00
83 %
10-128
2G26010
EPA 80824
0712712214:42
L5K
Decachlorobiphenyl
0.87
1
1.00
87 %
10-129
2G26010
EPA 80824
0712712214:42
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 of 46

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ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF10299-05 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 14:15 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Cyanide (total) [57-12-5]^ 0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:48
MSE
Sulfide [18496-25-8]^ 0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^ 83
D
ug/L
5
4.0
10
2G28008
EPA 8260D
07/28/22 19:08
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
2G26006
EPA 8260D
0712612219:08
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
2,4,5-T [93-76-5]^
0.28
u
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 15:49
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
u
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 15:49
FCV
2,4-D [94-75-7]^
0.27
u
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 15:49
FCV
Dinoseb [88-85-7]^
0.32
u
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 15:49
FCV
Pentachlorophenol [87-86-5]^
0.19
u
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 15:49
FCV
Surrogates
Results
DF
Snike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By
Notes
2,4-DC4A
2.9
1
2.00
146 %
37-134
2G25024
EPA 8151A
0712812215:49
FCV
Q5-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 146

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ANALYTICAL RESULTS
Description: 7401-P16R-M Lab Sample ID:CF10299-06 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 12:03 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 02:38
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:00
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Barium [7440-39-3]^
1090
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Beryllium [7440-41-7]1
0.160
u
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:43
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:43
JDH
Chromium [7440-47-3]^
2.49
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Cobalt[7440-48-4]^
2.67
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Nickel[7440-02-O]^
10.6
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:00
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:00
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Vanadium [7440-62-2]^
4.75
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:43
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 of 146

00�
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ANALYTICAL RESULTS
Description: 7401-1317 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 14:38
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 14:38
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 14:38
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 14:38
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Chlorobenzene [108-90-7]A
1.9
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 43 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 14:38
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 14:38
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 14:38
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 14:38
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
58
1
50.0
115 %
53-136
2G27031
EPA 8260D
07129122 14:38
RKY
Dibromofluoromethane
66
1
50.0
132 %
67-129
2G27031
EPA 8260D
0712912214:38
RKY QS-03
Toluene-d8
56
1
50.0
112 %
59-134
2G27031
EPA 6260D
071291221438
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Anthracene[120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 15:24
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Chlorobenzilate[510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Chrysene[218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Dibenzofuran[132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 45 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA 8270E
07/25/22 15:24
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Pyrene[129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:24
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
86
1
100
86 %
10-179
2G25005
EPA 8270E
0712512215:24 DFM
2-Fluorobiphenyl
40
1
50.0
79 %
10-149
2G25005
EPA 8270E
0712512215:24 DFM
2-Fluorophenol
60
1
100
60 %
10-110
2G25005
EPA 8270E
0712512215:24 DFM
Nitrobenzene-d5
39
1
50.0
79 %
10-149
2G25005
EPA 8270E
0712512215:24 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 46 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
53
1
100
53 %
10-88
2G25005
EPA 8270E
0712512215:24
DFM
Terphenyl-d14
38
1
50.0
76 %
10-188
2G25005
EPA 8270E
0712512215:24
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 15:08
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:08
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 15:08
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.88
1
1.00
88 %
10-139
2G26009
EPA 8081E
0712712215:08
LSK
Decachlorobiphenyl
0.86
1
1.00
86 %
10-122
2G26009
EPA 8081E
0712712215:08
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 15:08
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.74
1
1.00
74 %
10-128
2G26010
EPA 80824
0712712215:08
L5K
Decachlorobiphenyl
0.87
1
1.00
87 %
10-129
2G26010
EPA 80824
0712712215:08
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF10299-07 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:38 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:04
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:05
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Barium [7440-39-3]^
227
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Beryllium [7440-41-7]^
1.83
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:46
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:46
JDH
Chromium [7440-47-3]^
2.92
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Cobalt[7440-48-4]^
1.40
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Nickel[7440-02-O]^
2.26
J
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:05
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:05
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Vanadium [7440-62-2]^
3.61
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Zinc[7440-66-6]^
5.82
J
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:46
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:50
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
3.9
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 18:16
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.4
1
5.00
89 %
75-125
2G26006
EPA 8260D
0712612218:16
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 16:14
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 16:14
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 16:14
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 16:14
`CV
Pentachlorophenol[87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 16:14
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2,4-DC4A
1.9
1
2.00
97 %
37-134
2G25024
EPA 8151A
0712812216:14
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-1319 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1-Dichloroethane [75-34-3]^
4.1
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,1-Dichloropropene [563-58-6]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,3-Dichloropropane [142-28-9]A
0.16
U
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
1,4-Dichlorobenzene [106-46-7]^
6.3
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
2,2-Dichloropropane [594-20-7]A
0.28
U
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
3-Chloropropene[107-05-1]A
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 15:07
RKY
Acetonitrile [75-05-8]A
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 15:07
RKY
Acrolein [107-02-8]A
4.0
U
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 15:07
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 15:07
RKY
Benzene [71-43-2]^
4.2
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Chlorobenzene [108-90-7]^
17
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
cis-1,2-Dichloroethene [156-59-2]^
2.4
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Dichlorodifluoromethane [75-71-8]^
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Ethylbenzene [300-41-4]^
1.6
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 49 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 15:07
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 15:07
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Naphthalene [91-20-3]^
1.5
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 15:07
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Toluene [308-88-3]^
0.51
J
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Vinyl chloride [75-01-4]^
0.75
J
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 15:07
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
57
1
50.0
115 %
53-136
2G27031
EPA 8260D
0712912215:07
RKY
Dibromofluoromethane
60
1
50.0
119 %
67-129
2G27031
EPA 8260D
0712912215:07
RKY
Toluene-d8
56
1
50.0
112 %
59-134
2G27031
EPA 6260D
0712912215:07
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Anthracene[120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 15:53
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Chlorobenzilate[510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Chrysene[218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Dibenzofuran[132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 51 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA 8270E
07/25/22 15:53
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Pyrene[129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 15:53
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
95
1
100
95 %
10-179
2G25005
EPA 8270E
0712512215:53 DFM
2-Fluorobiphenyl
38
1
50.0
76 %
10-149
2G25005
EPA 8270E
0712512215:53 DFM
2-Fluorophenol
59
1
100
59 %
10-110
2G25005
EPA 8270E
0712512215:53 DFM
Nitrobenzene-d5
40
1
50.0
81 %
10-149
2G25005
EPA 8270E
0712512215:53 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 52 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
56
1
100
56 %
10-88
2G25005
EPA 8270E
0712512215:53
DFM
Terphenyl-d14
31
1
50.0
61 %
10-188
2G25005
EPA 8270E
0712512215:53
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 15:22
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:22
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 15:22
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.67
1
1.00
67 %
10-139
2G26009
EPA 8081E
0712712215:22
LSK
Decachlorobiphenyl
0.78
1
1.00
78 %
10-122
2G26009
EPA 8081E
0712712215:22
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 15:22
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.62
1
1.00
62 %
10-128
2G26010
EPA 80824
0712712215:22
L5K
Decachlorobiphenyl
0.81
1
1.00
81 %
10-129
2G26010
EPA 80824
0712712215:22
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF10299-08 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 14:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
1.06
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:06
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:09
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Barium [7440-39-3]^
1970
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Beryllium [7440-41-7]^
14.4
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:48
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:48
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Cobalt[7440-48-4]^
18.3
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Lead [7439-92-1]^
5.35
J
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Nickel[7440-02-O]^
26.1
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Selenium [7782-49-2]^
1.84
J
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:09
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:09
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Zinc[7440-66-6]^
107
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:48
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:51
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
160
D
ug/L
5
4.0
10
2G28008
EPA 8260D
07/28/22 19:33
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
2G26006
EPA 8260D
071261221933
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 16:39
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 16:39
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 16:39
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 16:39
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 16:39
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2,4-DC4A
2.1
1
2.00
106 %
37-134
2G25024
EPA 8151A
071261221639
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 54 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1-Dichloroethane [75-34-3]A
0.51
J
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,1-Dichloropropene [563-58-6]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,3-Dichloropropane [142-28-9]A
0.16
U
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
1,4-Dichlorobenzene [106-46-7]A
3.8
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
2,2-Dichloropropane [594-20-7]A
0.28
U
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2G27028
EPA 8260D
07/28/22 01:17
RKY
Acetonitrile [75-05-8]A
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 01:17
RKY
Acrolein [107-02-8]A
4.0
U
ug/L
1
4.0
10
2G27028
EPA 8260D
07/28/22 01:17
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2G27028
EPA 8260D
07/28/22 01:17
RKY
Benzene [71-43-2]A
2.2
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Chlorobenzene [108-90-7]A
1.6
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 55 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/28/22 01:17
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/28/22 01:17
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Naphthalene [91-20-3]^
1.5
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
o-Xylene [95-47-6]^
1.1
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 01:17
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Xylenes(Total)[1330-20-7]^
1.1
J
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/28/22 01:17
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
62
1
50.0
124 %
53-136
2G27026
EPA 8260D
07126122 01:17
RKY
Dibromofluoromethane
59
1
50.0
117 %
67-129
2G27026
EPA 8260D
07126122 01:17
RKY
Toluene-d8
57
1
50.0
114 %
59-134
2G27026
EPA 6260D
07128122 01:17
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 16:23
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 56 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA
8270E
07/25/22
16:23
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Diethylphthalate [84-66-2]^
3.4
1
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only be reproduced in full.
I Page 57 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22
16:23
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:23
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
84
1
100
84 %
10-179
2G25005
EPA 8270E
0712512216:23 DFM
2-Fluorobiphenyl
32
1
50.0
65 %
10-149
2G25005
EPA 8270E
0712512216:23 DFM
2-Fluorophenol
53
1
100
53 %
10-110
2G25005
EPA 8270E
0712512216:23 DFM
Nitrobenzene-d5
27
1
50.0
54 %
10-149
2G25005
EPA 8270E
0712512216:23 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 58 of 146

(� �Eo
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ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
48
1
100
48 %
10-88
2G25005
EPA 8270E
0712512216:23
DFM
Terphenyl-d14
32
1
50.0
65 %
10-188
2G25005
EPA 8270E
0712512216:23
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 15:35
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:35
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 15:35
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
2,4,5,6-TCMX
0.82
1
1.00
82 %
10-139
2G26009
EPA 8081E
071271221525
LSK
Decachlorobiphenyl
0.70
1
1.00
70 %
10-122
2G26009
EPA 8081E
071271221525
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 15:35
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.78
1
1.00
78 %
10-128
2G26010
EPA 80824
0712712215:35
L5K
Decachlorobiphenyl
0.83
1
1.00
83 %
10-129
2G26010
EPA 80824
0712712215:35
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 of 46

(� �Eo
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ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF10299-09 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 16:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Cyanide (total) [57-12-5]^ 0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:57
MSE
Sulfide [18496-25-8]^ 0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^ 79
D
ug/L
5
4.0
10
2G29020
EPA 8260D
07/29/22 15:14
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
4.4
1
5.00
88 %
75-125
2G29020
EPA 8260D
0712912215:14
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
2,4,5-T [93-76-5]^
0.28
u
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 17:04
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
u
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 17:04
FCV
2,4-D [94-75-7]^
0.27
u
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 17:04
FCV
Dinoseb [88-85-7]^
0.32
u
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 17:04
FCV
Pentachlorophenol [87-86-5]^
0.19
u
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 17:04
FCV
Surrogates
Results
DF
Snike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By
Notes
2, 4-DCAA
3.6
1
2,00
181 %
37-134
2G25024
EPA 8151A
0712812217:04
FCV
Q5-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R-M Lab Sample ID:CF10299-10 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:47 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:16
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:13
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Barium [7440-39-3]^
842
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Beryllium [7440-41-7]^
0.957
J
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 11:50
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 11:50
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Cobalt[7440-48-4]^
2.84
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Nickel[7440-02-O]^
8.56
J
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:13
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:13
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 11:50
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-13201) Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 15:36
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 15:36
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 15:36
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 15:36
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 62 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 15:36
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 15:36
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 15:36
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Toluene [308-88-3]^
1.9
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 15:36
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
56
1
50.0
113 %
53-136
2G27031
EPA 8260D
0712912215:36
RKY
Dibromofluoromethane
64
1
50.0
127 %
67-129
2G27031
EPA 8260D
0712912215:36
RKY
Toluene-d8
56
1
50.0
112 %
59-134
2G27031
EPA 6260D
071291221536
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 16:53
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 16:53
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 64 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22
16:53
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
16:53
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
71
1
100
71 %
10-179
2G25005
EPA 8270E
0712512216:53 DFM
2-Fluorobiphenyl
43
1
50.0
86 %
10-149
2G25005
EPA 8270E
0712512216:53 DFM
2-Fluorophenol
48
1
100
48 %
10-110
2G25005
EPA 8270E
0712512216:53 DFM
Nitrobenzene-d5
40
1
50.0
80 %
10-149
2G25005
EPA 8270E
0712512216:53 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 65 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
35
1
100
35 %
10-88
2G25005
EPA 8270E
0712512216:53
DFM
Terphenyl-d14
33
1
50.0
66 %
10-188
2G25005
EPA 8270E
0712512216:53
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 15:48
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 15:48
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 15:48
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.81
1
1.00
81 %
10-139
2G26009
EPA 8081E
0712712215:48
LSK
Decachlorobiphenyl
0.65
1
1.00
65 %
10-122
2G26009
EPA 8081E
0712712215:48
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 15:48
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.74
1
1.00
74 %
10-128
2G26010
EPA 80824
0712712215:48
L5K
Decachlorobiphenyl
0.71
1
1.00
71 %
10-129
2G26010
EPA 80824
0712712215:48
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 66 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF10299-11 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 09:10 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:11
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:22
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Barium [7440-39-3]^
99.7
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Beryllium [7440-41-7]^
7.96
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:32
JDH
Cadmium [7440-43-9]^
0.819
J
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:32
JDH
Chromium [7440-47-3]^
9.93
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Cobalt[7440-48-4]^
2.40
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Lead [7439-92-1]^
4.82
J
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:22
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Thallium [7440-28-0]^
1.10
UD
ug/L
10
1.10
10.0
2G22022
EPA 6020B
07/28/22 16:06
MAM
QI-02
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Vanadium [7440-62-2]^
9.79
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Zinc[7440-66-6]^
17.9
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:32
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 10:58
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.87
J
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 15:16
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.3
1
5.00
86 %
75-125
2G26006
EPA 8260D
0712612215:16
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 17:29
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 17:29
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 17:29
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 17:29
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 17:29
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2, 4-DCAA
1.6
1
2,00
82 %
37-134
2G25024
EPA 8151A
0712812217:29
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 67 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-1328 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27028
EPA 8260D
07/28/22 01:46
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 01:46
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27028
EPA 8260D
07/28/22 01:46
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27028
EPA 8260D
07/28/22 01:46
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 68 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/28/22 01:46
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/28/22 01:46
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 01:46
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/28/22 01:46
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
60
1
50.0
121 %
53-136
2G27026
EPA 8260D
07126122 01:46
RKY
Dibromofluoromethane
63
1
50.0
126 %
67-129
2G27026
EPA 8260D
07126122 01:46
RKY
Toluene-d8
56
1
50.0
112 %
59-134
2G27026
EPA 6260D
07128122 01:46
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 69 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 17:22
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 17:22
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 70 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22 17:22
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22 17:22
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
52
1
100
52 %
10-179
2G25005
EPA 8270E
0712512217:22 DFM
2-Fluorobiphenyl
40
1
50.0
81 %
10-149
2G25005
EPA 8270E
0712512217:22 DFM
2-Fluorophenol
37
1
100
37 %
10-110
2G25005
EPA 8270E
0712512217:22 DFM
Nitrobenzene-d5
37
1
50.0
74 %
10-149
2G25005
EPA 8270E
0712512217:22 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 71 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
29
1
100
29 %
10-88
2G25005
EPA 8270E
0712512217:22
DFM
Terphenyl-d14
28
1
50.0
55 %
10-188
2G25005
EPA 8270E
0712512217:22
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 16:01
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:01
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 16:01
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.62
1
1.00
62 %
10-139
2G26009
EPA 8081E
0712712216:01
LSK
Decachlorobiphenyl
0.68
1
1.00
68 %
10-122
2G26009
EPA 8081E
0712712216:01
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 16:01
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.66
1
1.00
66 %
10-128
2G26010
EPA 80824
0712712216:01
L5K
Decachlorobiphenyl
0.87
1
1.00
87 %
10-129
2G26010
EPA 80824
0712712216:01
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 72 of 46

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ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF10299-12 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 15:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Cyanide (total) [57-12-5]^ 0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 11:00
MSE
Sulfide [18496-25-8]^ 0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^ 0.84
J
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 15:41
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-d8
4.3
1
5.00
87 %
75-125
2G26006
EPA 8260D
0712612215:41
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
u
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 17:54
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
u
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 17:54
FCV
2,4-D [94-75-7]^
0.27
u
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 17:54
FCV
Dinoseb [88-85-7]^
0.32
u
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 17:54
FCV
Pentachlorophenol [87-86-5]^
0.19
u
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 17:54
FCV
Surrogates
Results
DF
Snike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
2, 4-DCAA
1.7
1
2,00
86 %
37-134
2G25024
EPA 8151A
0712812217:54
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 73 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28-M Lab Sample ID:CF10299-13 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 11:55 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:19
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:50
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Barium [7440-39-3]^
34.6
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Beryllium [7440-41-7]^
0.721
J
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:35
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:35
JDH
Chromium [7440-47-3]^
1.79
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Cobalt[7440-48-4]^
1.82
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:50
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:50
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Vanadium [7440-62-2]^
2.92
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
Zinc[7440-66-6]^
13.1
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:35
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 74 of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-1329 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
1,4-Dichlorobenzene [106-46-7]A
1.9
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27028
EPA 8260D
07/28/22 02:14
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 02:14
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27028
EPA 8260D
07/28/22 02:14
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27028
EPA 8260D
07/28/22 02:14
RKY
Benzene [71-43-2]A
2.0
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Chlorobenzene [108-90-7]A
13
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 75 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/28/22 02:14
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/28/22 02:14
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Naphthalene [91-20-3]^
1.6
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/28/22 02:14
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/28/22 02:14
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
63
1
50.0
126 %
53-136
2G27026
EPA 8260D
07126122 02:14
RKY
Dibromofluoromethane
59
1
50.0
117 %
67-129
2G27026
EPA 8260D
07126122 02:14
RKY
Toluene-d8
56
1
50.0
113 %
59-134
2G27026
EPA 6260D
07128122 02:14
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4-Dichlorophenol[120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4-Dinitrophenol[51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,6-Dichlorophenol[87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/26/22 17:13
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 76 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
2-Methylnaphthalene [91-57-6]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
2-Methylphenol[95-48-7]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
2-Naphthylamine [91-59-8]A
3.0
u
ug/L
1
3.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
2-Nitroaniline [88-74-4]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
2-Nitrophenol[88-75-5]A
1.1
u
ug/L
1
1.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
3,3'-Dimethylbenzidine [119-93-71A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
3-Methylcholanthrene [56-49-5]A
1.3
u
ug/L
1
1.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
3-Nitroaniline [99-09-2]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Aminobiphenyl[92-67-1]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Chloroaniline [106-47-8]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Nitroaniline [100-01-6]A
3.2
u
ug/L
1
3.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
4-Nitrophenol[100-02-7]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
5-Nitro-o-toluidine [99-55-8]A
3.2
u
ug/L
1
3.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
7,12-Dimethylbenz(a)anthracene
1.4
u
ug/L
1
1.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
[57-97-6]A
a,a-Dimethylphenethylamine [122-09-8]A
3.5
U
ug/L
1
3.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Acetophenone [98-86-2]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Anthracene[120-12-7]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzo(a)anthracene [56-55-3]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzo(a)pyrene [50-32-8]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzo(g,h,i)perylene [191-24-2]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzo(k)fluoranthene[207-08-9]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Benzyl alcohol [100-51-6]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
u
ug/L
1
1.9
5.0
2G25005
EPA
8270E
07/26/22
17:13
DFM
Butylbenzylphthalate [85-68-7]A
3.8
u
ug/L
1
3.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Chlorobenzilate [510-15-6]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM QV-01
Chrysene [218-01-9]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Diallate [2303-16-4]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Dibenzofuran [132-64-9]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Diethylphthalate [84-66-2]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Dimethoate [60-51-5]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Disulfoton [298-04-4]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 77 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified anaiyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Notes
Ethyl methanesulfonate [62-50-0]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Famphur[52-85-7]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Fluoranthene[206-44-0]A
3.1
u
ug/L
1
3.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Fluorene [86-73-7]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Hexachlorobenzene[118-74-1]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Hexachlorobutadiene [87-68-3]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Hexachloroethane [67-72-1]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Hexachloropropene [1888-71-7]A
6.8
u
ug/L
1
6.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Isodrin [465-73-6]A
1.5
u
ug/L
1
1.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Isophorone[78-59-1]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Isosafrole [120-58-1]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Kepone[143-50-0]A
7.2
u
ug/L
1
7.2
20
2G25005
EPA
8270E
07/26/22
17:13
DFM
Methapyrilene [91-80-5]A
4.8
u
ug/L
1
4.8
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Methyl Methanesulfonate [66-27-3]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Methyl parathion [298-00-0]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Nitrobenzene [98-95-3]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitrosodiethylamine [55-18-5]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitrosodi-n-butylamine [924-16-3]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
[86-30-6/122-39-4]A
N-Nitrosomethylethylamine [10595-95-6]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitrosopiperidine [100-75-4]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
N-Nitrosopyrrolidine [930-55-2]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
[126-68-1]A
o-Toluidine [95-53-4]A
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Parathion [56-38-2]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
p-Dimethylaminoazobenzene [60-11-7]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Pentachlorobenzene [608-93-5]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Pentachloronitrobenzene [82-68-8]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Phenacetin [62-44-2]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Phenanthrene [85-01-8]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Phenol[108-95-2]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Phorate [298-02-2]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Pronamide [23950-58-5]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Pyrene [129-00-0]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Safrole [94-59-7]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Thionazin [297-97-2]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/26/22
17:13
DFM
Surrogates
Resu/ts
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed By Notes
2,4,6-Tribromophenol
80
1
100
80 %
10-179
2G25005
EPA 8270E
0712612217.•13 DFM
2-Fluorobiphenyl
34
1
50.0
68 %
10-149
2G25005
EPA 8270E
0712612217:13 DFM
2-Fluorophenol
56
1
100
56 %
10-110
2G25005
EPA 8270E
0712612217:13 DFM
Nitrobenzene-d5
34
1
50.0
68 %
10-149
2G25005
EPA 8270E
0712612217:13 DFM
FINAL
This report relates only
to the
sample as received
by the laboratory, and may only
be reproduced in full.
I Page 78 Of 146

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ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
49
1
100
49 %
10-88
2G25005
EPA 8270E
0712612217:13
DFM
Terphenyl-d14
28
1
50.0
57 %
10-188
2G25005
EPA 8270E
0712612217:13
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
4,4'-DDE [72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 16:15
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:15
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 16:15
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
2,4,5,6-TCMX
0.81
1
1.00
81 %
10-139
2G26009
EPA 8081E
0712712216:15
LSK
Decachlorobiphenyl
0.77
1
1.00
77 %
10-122
2G26009
EPA 8081E
0712712216:15
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 16:15
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.65
1
1.00
65 %
10-128
2G26010
EPA 80824
0712712216:15
L5K
Decachlorobiphenyl
0.67
1
1.00
67 %
10-129
2G26010
EPA 80824
0712712216:15
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 79 of 46

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ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF10299-14 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Cyanide (total) [57-12-5]^ 0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 11:01
MSE
Sulfide [18496-25-8]^ 0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,4-Dioxane [123-91-1]^ 140
D
ug/L
5
4.0
10
2G28008
EPA 8260D
07/28/22 19:59
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
4.5
1
5.00
90 %
75-125
2G26006
EPA 8260D
0712612219:59
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
2,4,5-T [93-76-5]^
0.28
u
ug/L
1
0.28 0.50
2G25024
EPA 8151A
07/28/22 18:19
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
u
ug/L
1
0.44 0.50
2G25024
EPA 8151A
07/28/22 18:19
FCV
2,4-D [94-75-7]^
0.27
u
ug/L
1
0.27 0.50
2G25024
EPA 8151A
07/28/22 18:19
FCV
Dinoseb [88-85-7]^
0.32
u
ug/L
1
0.32 0.50
2G25024
EPA 8151A
07/28/22 18:19
FCV
Pentachlorophenol[87-86-5]^
0.19
u
ug/L
1
0.19 0.50
2G25024
EPA 8151A
07/28/22 18:19
FCV
Surrogates
Results
DF
Suike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4-DC4A
5.0
1
2.00
248 %
37-134
2G25024
EPA 8151A
0712612218:19
FCV
Q5-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 80 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29-M Lab Sample ID:CF10299-15 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 12:11 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:22
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G22022
EPA 6020B
07/28/22 15:54
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Barium [7440-39-3]^
370
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:37
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:37
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G22022
EPA 6020B
07/28/22 15:54
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G22022
EPA 6020B
07/28/22 15:54
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Vanadium [7440-62-2]^
9.16
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:37
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 81 of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CF10299-16 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 16:05
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 16:05
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 16:05
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 16:05
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 82 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CF10299-16 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 16:05
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 16:05
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 16:05
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 16:05
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
56
1
50.0
113 %
53-136
2G27031
EPA 8260D
0712912216:05
RKY
Dibromofluoromethane
67
1
50.0
134 %
67-129
2G27031
EPA 8260D
0712912216:05
RKY
QS-03
Toluene-d8
57
1
50.0
114 %
59-134
2G27031
EPA 6260D
0712912216:05
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.1
J
ug/L
1
0.80 2.0
2G28008
EPA 8260D
07/28/22 16:33
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.5
1
5.00
90 %
75-125
2G28008
EPA 8260D
071281221633
JMW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 83 Of 146

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CF10299-17 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 15:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 16:34
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 16:34
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 16:34
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 16:34
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 84 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CF10299-17 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 15:00 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 16:34
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 16:34
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 16:34
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 16:34
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
57
1
50.0
114 %
53-136
2G27031
EPA 8260D
0712912216:34
RKY
Dibromofluoromethane
66
1
50.0
131 %
67-129
2G27031
EPA 8260D
0712912216:34
RKY
QS-03
Toluene-d8
58
1
50.0
115 %
59-134
2G27031
EPA 6260D
071291221634
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2G28008
EPA 8260D
07/28/22 16:59
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.4
1
5.00
89 %
75-125
2G28008
EPA 8260D
0712812216:59
JMW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 85 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,1-Dichloropropene [563-58-6]A
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
U
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,3-Dichloropropane [142-28-9]A
0.16
U
ug/L
1
0.16
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
2,2-Dichloropropane [594-20-7]A
0.28
U
ug/L
1
0.28
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
3-Chloropropene[107-05-1]A
0.11
U
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2HO1045
EPA 8260D
08/02/22 02:54
RKY QV-01
Acetonitrile [75-05-8]A
5.0
U
ug/L
1
5.0
10
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Acrolein [107-02-8]A
4.0
U
ug/L
1
4.0
10
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Chloroform [67-66-3]A
5.2
ug/L
1
0.18
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 86 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2HO1045
EPA 8260D
08/02/22 02:54
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2HO1045
EPA 8260D
08/02/22 02:54
RKY
QV-01
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Toluene [308-88-3]^
0.70
J
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2HO1045
EPA 8260D
08/02/22 02:54
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
59
1
60.0
98 %
53-136
2HO1045
EPA 6260D
08102122 02:54
RKY
Dibromofluoromethane
74
1
60.0
123 %
67-129
2HO1045
EPA 6260D
08102122 02:54
RKY
Toluene-c48
58
1
60.0
97 %
59-134
2HO1045
EPA 6260D
08102122 02:54
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 87 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 18:22
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:22
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 88 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22
18:22
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:22
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
84
1
100
84 %
10-179
2G25005
EPA 8270E
0712512218:22 DFM
2-Fluorobiphenyl
42
1
50.0
83 %
10-149
2G25005
EPA 8270E
0712512218:22 DFM
2-Fluorophenol
68
1
100
68 %
10-110
2G25005
EPA 8270E
0712512218:22 DFM
Nitrobenzene-d5
39
1
50.0
78 %
10-149
2G25005
EPA 8270E
0712512218:22 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 89 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
59
1
100
59 %
10-88
2G25005
EPA 8270E
0712512218:22
DFM
Terphenyl-d14
38
1
50.0
77 %
10-188
2G25005
EPA 8270E
0712512218:22
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 16:28
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:28
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 16:28
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.90
1
1.00
90 %
10-139
2G26009
EPA 8081E
0712712216:28
LSK
Decachlorobiphenyl
0.57
1
1.00
57 %
10-122
2G26009
EPA 8081E
0712712216:28
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 16:28
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.66
1
1.00
66 %
10-128
2G26010
EPA 80824
0712712216:28
L5K
Decachlorobiphenyl
0.50
1
1.00
50 %
10-129
2G26010
EPA 80824
0712712216:28
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 90 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SWI Lab Sample ID:CF10299-18 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 16:25 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:24
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G25003
EPA 6020B
08/01/22 11:40
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Barium [7440-39-3]^
35.9
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:39
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:39
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Cobalt[7440-48-4]^
2.38
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G25003
EPA 6020B
08/01/22 11:40
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G25003
EPA 6020B
08/01/22 11:40
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Zinc[7440-66-6]^
6.96
J
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:39
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 11:03
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 16:07
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.5
1
5.00
90 %
75-125
2G26006
EPA 8260D
0712612216:07
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G27005
EPA 8151A
08/02/22 22:41
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G27005
EPA 8151A
08/02/22 22:41
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G27005
EPA 8151A
08/02/22 22:41
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G27005
EPA 8151A
08/02/22 22:41
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G27005
EPA 8151A
08/02/22 22:41
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2, 4-DCAA
2.1
1
2.00
103 %
37-134
2G27005
EPA 8151A
08102122 22:41
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 91 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 17:32
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 17:32
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 17:32
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 17:32
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Carbon disulfide [75-15-0]A
1.5
u
ug/L
1
1.5
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Chloroprene [126-99-8]A
0.64
U
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
U
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Ethyl Methacrylate [97-63-2]A
0.38
U
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 92 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 17:32
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 17:32
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 17:32
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 17:32
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
57
1
50.0
115 %
53-136
2G27031
EPA 8260D
071291221732
RKY
Dibromofluoromethane
66
1
50.0
132 %
67-129
2G27031
EPA 8260D
071291221732
RKY QS-03
Toluene-c48
57
1
50.0
113 %
59-134
2G27031
EPA 6260D
071291221732
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 18:51
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 93 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
2-Methylnaphthalene [91-57-6]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
2-Methylphenol[95-48-7]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
2-Naphthylamine[91-59-8]A
3.0
u
ug/L
1
3.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
2-Nitroaniline [88-74-4]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
2-Nitrophenol[88-75-5]A
1.1
u
ug/L
1
1.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
3,3'-Dimethylbenzidine [119-93-71A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
3-Methylcholanthrene [56-49-5]A
1.3
u
ug/L
1
1.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
3-Nitroaniline [99-09-2]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Aminobiphenyl[92-67-1]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Chloroaniline [106-47-8]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Nitroaniline [100-01-6]A
3.2
u
ug/L
1
3.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
4-Nitrophenol[100-02-7]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
5-Nitro-o-toluidine [99-55-8]A
3.2
u
ug/L
1
3.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
7,12-Dimethylbenz(a)anthracene
1.4
u
ug/L
1
1.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
[57-97-6]A
a,a-Dimethylphenethylamine [122-09-8]A
3.5
U
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Acetophenone [98-86-2]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Anthracene[120-12-7]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Benzo(a)anthracene [56-55-3]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Benzo(a)pyrene [50-32-8]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Benzo(g,h,i)perylene[191-24-2]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM QV-01
Benzo(k)fluoranthene[207-08-9]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Benzyl alcohol [100-51-6]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
u
ug/L
1
1.9
5.0
2G25005
EPA
8270E
07/25/22
18:51
DFM
Butylbenzylphthalate [85-68-7]A
3.8
u
ug/L
1
3.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Chlorobenzilate [510-15-6]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Chrysene [218-01-9]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Diallate [2303-16-4]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Dibenzofuran [132-64-9]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Diethylphthalate [84-66-2]A
2.4
u
ug/L
1
2.4
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Dimethoate [60-51-5]A
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Disulfoton [298-04-4]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 94 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified anaiyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Notes
Ethyl methanesulfonate [62-50-0]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Famphur[52-85-7]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Fluoranthene[206-44-0]A
3.1
u
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Fluorene [86-73-7]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Hexachlorobenzene[118-74-1]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Hexachlorobutadiene [87-68-3]A
2.8
u
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Hexachloroethane [67-72-1]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Hexachloropropene[1888-71-7]A
6.8
u
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Isodrin [465-73-6]A
1.5
u
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Isophorone[78-59-1]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Isosafrole [120-58-1]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Kepone[143-50-0]A
7.2
u
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22
18:51
DFM
Methapyrilene [91-80-5]A
4.8
u
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Methyl Methanesulfonate [66-27-3]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Methyl parathion [298-00-0]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Nitrobenzene [98-95-3]A
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitrosodiethylamine [55-18-5]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitrosodi-n-butylamine [924-16-3]A
2.0
u
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
[86-30-6/122-39-4]A
N-Nitrosomethylethylamine [10595-95-6]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitrosopiperidine [100-75-4]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
N-Nitrosopyrrolidine [930-55-2]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
[126-68-1]A
o-Toluidine [95-53-4]A
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Parathion [56-38-2]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
p-Dimethylaminoazobenzene [60-11-7]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Pentachlorobenzene [608-93-5]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Pentachloronitrobenzene [82-68-8]A
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Phenacetin [62-44-2]A
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Phenanthrene [85-01-8]A
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Phenol[108-95-2]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Phorate[298-02-2]A
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Pronamide [23950-58-5]A
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Pyrene [129-00-0]A
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Safrole [94-59-7]A
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Thionazin [297-97-2]A
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
18:51
DFM
Surrogates
Resu/ts
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed ffy Notes
2,4,6-Tribromophenol
83
1
100
83 %
10-179
2G25005
EPA 8270E
0712512218:51 DFM
2-Fluorobiphenyl
40
1
50.0
80 %
10-149
2G25005
EPA 8270E
0712512218:51 DFM
2-Fluorophenol
64
1
100
64 %
10-110
2G25005
EPA 8270E
0712512218:51 DFM
Nitrobenzene-d5
38
1
50.0
76 %
10-149
2G25005
EPA 8270E
0712512218:51 DFM
FINAL
This report relates only
to the
sample as received
by the laboratory, and may only
be reproduced in full.
I Page 95 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
54
1
100
54 %
10-88
2G25005
EPA 8270E
0712512218:51
DFM
Terphenyl-d14
37
1
50.0
73 %
10-188
2G25005
EPA 8270E
0712512218:51
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 16:41
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 16:41
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 16:41
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,6-TCMX
0.96
1
1.00
96 %
10-139
2G26009
EPA 8081E
0712712216:41
LSK
Decachlorobiphenyl
0.71
1
1.00
71 %
10-122
2G26009
EPA 8081E
0712712216:41
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 16:41
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.83
1
1.00
83 %
10-128
2G26010
EPA 80824
0712712216:41
L5K
Decachlorobiphenyl
0.74
1
1.00
74 %
10-129
2G26010
EPA 80824
0712712216:41
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 96 of 46

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF10299-19 Received: 07/21/22 10:00
Matrix: Surface Water Sampled:07/20/22 15:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:32
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G25003
EPA 6020B
08/01/22 11:45
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Barium [7440-39-3]^
71.0
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:42
JDH
Chromium [7440-47-3]^
2.33
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Cobalt[7440-48-4]^
2.57
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G25003
EPA 6020B
08/01/22 11:45
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G25003
EPA 6020B
08/01/22 11:45
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:42
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 11:05
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 17:25
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.4
1
5.00
88 %
75-125
2G26006
EPA 8260D
0712612217:25
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G27005
EPA 8151A
08/02/22 23:06
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G27005
EPA 8151A
08/02/22 23:06
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G27005
EPA 8151A
08/02/22 23:06
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G27005
EPA 8151A
08/02/22 23:06
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G27005
EPA 8151A
08/02/22 23:06
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2, 4-DCAA
2.0
1
2.00
102 %
37-134
2G27005
EPA 8151A
08102122 23:06
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 97 Of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2G27031
EPA 8260D
07/29/22 10:19
RKY
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 10:19
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2G27031
EPA 8260D
07/29/22 10:19
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2G27031
EPA 8260D
07/29/22 10:19
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Carbon disulfide [75-15-0]A
170
ug/L
1
1.5
5.0
2HO1045
EPA 8260D
08/02/22 01:28
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Chloroprene [126-99-8]A
0.64
u
ug/L
1
0.64
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
u
ug/L
1
0.20
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Ethyl Methacrylate [97-63-2]A
0.38
u
ug/L
1
0.38
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Hexachlorobutadiene [87-68-3]A
0.22
u
ug/L
1
0.22
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 98 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27031
EPA 8260D
07/29/22 10:19
RKY QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27031
EPA 8260D
07/29/22 10:19
RKY
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27031
EPA 8260D
07/29/22 10:19
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Toluene [308-88-3]^
1.3
ug/L
1
0.14
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Xylenes(Total)[1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27031
EPA 8260D
07/29/22 10:19
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
60
1
50.0
120 %
53-136
2G27031
EPA 8260D
0712912210:19
RKY
4-Bromofluorobenzene
58
1
60.0
97 %
53-136
2HO1045
EPA 8260D
08102122 01:28
RKY
Dibromofluoromethane
64
1
50.0
127 %
67-129
2G27031
EPA 8260D
0712912210:19
RKY
Dibromofluoromethane
74
1
60.0
123 %
67-129
2HO1045
EPA 8260D
08102122 01:28
RKY
Toluene-c48
56
1
50.0
112 %
59-134
2G27031
EPA 8260D
0712912210:19
RKY
Toluene-d8
59
1
60.0
98 %
59-134
2HO1045
EPA 6260D
08102122 01:28
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1 10
2G25005
EPA 8270E
07/25/22 19:21
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 99 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2-Chloronaphthalene[91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
3-Nitroaniline [99-09-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
4-Nitrophenol[100-02-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
7,12-Di methyl benz(a)anth racene
1.4
U
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 19:21
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pagel 00 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Hexachloropropene [1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA 8270E
07/25/22 19:21
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitrosodiethylamine [55-18-5]^
5.1
J
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
u
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:21
DFM
Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes
2,4,6-Tribromophenol 83 1 100 83 % 10-179 2G25005 EPA 8270E 0712512219:21 DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 101 of 146

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ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2-Fluorobiphenyl
33
1
50.0
66 %
10-149
2G25005
EPA 8270E
0712512219:21
DFM
2-Fluorophenol
57
1
100
57 %
10-110
2G25005
EPA 8270E
0712512219:21
DFM
Nitrobenzene-d5
35
1
50.0
70 %
10-149
2G25005
EPA 8270E
0712512219:21
DFM
Phenol-d5
48
1
100
48 %
10-88
2G25005
EPA 8270E
0712512219:21
DFM
Terphenyl-di4
23
1
50.0
45 %
10-I88
2G25005
EPA 8270E
0712512219:21
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37 0.50
2G26009
EPA 8081B
07/27/22 16:54
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048 0.050
2G26009
EPA 8081B
07/27/22 16:54
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28 1.0
2G26009
EPA 8081B
07/27/22 16:54
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
2,4,5,E-TCMX
0.46
1
1.00
46 %
10-139
2G26009
EPA 8081E
0712712216:54
LSK
Decachlorobiphenyl
0.55
1
1.00
55 %
10-122
2G26009
EPA 8081E
0712712216:54
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47 0.50
2G26010
EPA 8082A
07/27/22 16:54
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.45
1
1.00
45 %
10-126
2G26010
EPA 8062A
0712712216:54
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 102 of 146

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ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Decachloroblphenyl
0.54
1
1.00
54 %
10-129
2G26010
EPA 6062A
0712712216:54
L5K
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Mercury[7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:34
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G25003
EPA 6020B
08/01/22 11:49
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:44
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:44
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G25003
EPA 6020B
08/01/22 11:49
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G25003
EPA 6020B
08/01/22 11:49
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Zinc[7440-66-6]^
8.54
J
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:44
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G27014
EPA 9014
07/28/22 11:06
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 iM 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 13:07
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
2G28008
EPA 8260D
0712812213:07
JMW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 103 of 146

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ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF10299-20 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 10:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl
Results
Fla"
Units
DF
MDL
P(—L
Batch
Method
Analyzed
By Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28
0.50
2G27005
EPA 8151A
08/02/22 23:32
FCV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44
0.50
2G27005
EPA 8151A
08/02/22 23:32
FCV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27
0.50
2G27005
EPA 8151A
08/02/22 23:32
FCV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32
0.50
2G27005
EPA 8151A
08/02/22 23:32
FCV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19
0.50
2G27005
EPA 8151A
08/02/22 23:32
FCV
Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes
2, 4-DCAA 1.8 1 2.00 90 % 37-134 2G27005 EPA 8151A 08102122 2332 FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 104 of 46

0Nk"q09
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ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1-Dichloroethane [75-34-3]A
0.13
u
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1-Dichloroethene [75-35-4]A
0.21
u
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,1-Dichloropropene [563-58-6]A
0.15
u
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
u
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
u
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
u
ug/L
1
0.48
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2-Dibromoethane [106-93-4]A
0.66
u
ug/L
1
0.66
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
u
ug/L
1
0.19
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2-Dichloroethane [107-06-2]A
0.21
u
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,2-Dichloropropane [78-87-5]A
0.10
u
ug/L
1
0.10
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
u
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,3-Dichloropropane [142-28-9]A
0.16
u
ug/L
1
0.16
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
u
ug/L
1
0.19
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
2,2-Dichloropropane [594-20-7]A
0.28
u
ug/L
1
0.28
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
3-Chloropropene[107-05-1]A
0.11
u
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
u
ug/L
1
1.1
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Acetone [67-64-1]A
10
u
ug/L
1
10
20
2HO1045
EPA 8260D
08/02/22 01:56
RKY QV-01
Acetonitrile [75-05-8]A
5.0
u
ug/L
1
5.0
10
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Acrolein [107-02-8]A
4.0
u
ug/L
1
4.0
10
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Acrylonitrile [107-13-1]A
3.5
u
ug/L
1
3.5
10
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Bromodichloromethane [75-27-4]A
0.17
u
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Bromoform [75-25-2]A
0.22
u
ug/L
1
0.22
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Bromomethane [74-83-9]A
0.14
u
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Carbon disulfide [75-15-0]A
3.4
J
ug/L
1
1.5
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Carbon tetrachloride [56-23-5]A
0.17
u
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Chlorobenzene[108-90-7]A
0.17
u
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Chloroethane [75-00-3]A
0.23
u
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Chloroform [67-66-3]A
0.18
u
ug/L
1
0.18
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Chloromethane [74-87-3]A
0.13
u
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Chloroprene [126-99-8]A
0.64
u
ug/L
1
0.64
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
u
ug/L
1
0.20
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Ethyl Methacrylate [97-63-2]A
0.38
u
ug/L
1
0.38
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Hexachlorobutadiene [87-68-3]A
0.22
u
ug/L
1
0.22
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 105 Of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2HO1045
EPA 8260D
08/02/22 01:56
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2HO1045
EPA 8260D
08/02/22 01:56
RKY
QV-01
Methyl Methacrylate [80-62-6]^
0.51
U
ug/L
1
0.51
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2HO1045
EPA 8260D
08/02/22 01:56
RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
59
1
60.0
98 %
53-136
2HO1045
EPA 6260D
08102122 01:56
RKY
Dibromofluoromethane
73
1
60.0
121 %
67-129
2HO1045
EPA 6260D
08102122 01:56
RKY
Toluene-d8
59
1
60.0
99 %
59-134
2HO1045
EPA 6260D
08102122 01:56
RKY
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4,5-Tetrachlorobenzene [95-94-3]^
3.4
U
ug/L
1
3.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
1,3,5-Trinitrobenzene [99-35-4]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
1,3-Dinitrobenzene [99-65-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
1,4-Naphthoquinone [130-15-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
1,4-Phenylenediamine [106-50-3]^
4.0
U
ug/L
1
4.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
1-Naphthylamine [134-32-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,3,4,6-Tetrachlorophenol[58-90-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4-Dichlorophenol [120-83-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4-Dinitrophenol [51-28-5]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,6-Dichlorophenol [87-65-0]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Acetylaminofluorene [53-96-3]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Chloronaphthalene [91-58-7]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Chlorophenol[95-57-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
U
ug/L
1
3.3
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 106 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
By Notes
2- Methyl naphthalene [91-57-6]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Methylphenol[95-48-7]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Naphthylamine [91-59-8]^
3.0
U
ug/L
1
3.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Nitroaniline [88-74-4]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
2-Nitrophenol[88-75-5]^
1.1
U
ug/L
1
1.1
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
3,3'-Dichlorobenzidine [91-94-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
3,3'-Dimethylbenzidine [119-93-7]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
3-Methylcholanthrene [56-49-5]^
1.3
U
ug/L
1
1.3
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
3-Nitroaniline [99-09-2]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Aminobiphenyl[92-67-1]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Bromophenyl-phenylether[101-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Chloro-3-methylphenol[59-50-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Chloroaniline [106-47-8]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Nitroaniline [100-01-6]^
3.2
U
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
4-Nitrophenol[100-02-7]^
2.8
u
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
5-Nitro-o-toluidine [99-55-8]^
3.2
u
ug/L
1
3.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
7,12-Di methyl benz(a)anth racene
1.4
u
ug/L
1
1.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
[57-97-6]^
a,a-Dimethylphenethylamine [122-09-8]^
3.5
U
ug/L
1
3.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Acenaphthene[83-32-9]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Acenaphthylene[208-96-8]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Acetophenone[98-86-2]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Anthracene [120-12-7]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Benzo(a)anthracene [56-55-3]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Benzo(a)pyrene [50-32-8]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Benzo(b)fluoranthene [205-99-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Benzo(g,h,i)perylene [191-24-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Benzylalcohol [100-51-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Bis(2-chloroethyl)ether[111-44-4]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
1.9
U
ug/L
1
1.9
5.0
2G25005
EPA 8270E
07/25/22 19:50
DFM
Butyl benzylphtha late [85-68-7]^
3.8
U
ug/L
1
3.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Chlorobenzilate [510-15-6]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Chrysene [218-01-9]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Diallate [2303-16-4]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Dibenzo(a,h)anthracene [53-70-3]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Dibenzofuran [132-64-9]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Diethylphtha late [84-66-2]^
2.4
U
ug/L
1
2.4
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Dimethoate [60-51-5]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Dimethylphtha late [131-11-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Di-n-butylphthalate [84-74-2]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Di-n-octylphthalate [117-84-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
Disulfoton [298-04-4]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA 8270E
07/25/22 19:50
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 107 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL
P(-L
Batch
Method
Analyzed
By Notes
Ethyl methanesulfonate [62-50-0]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Famphur[52-85-7]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Fluoranthene [206-44-0]^
3.1
U
ug/L
1
3.1
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Fluorene [86-73-7]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Hexachlorobenzene[118-74-1]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Hexachlorobutadiene [87-68-3]^
2.8
U
ug/L
1
2.8
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Hexachlorocyclopentadiene [77-47-4]^
2.7
U
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Hexachloroethane [67-72-1]^
2.6
U
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Hexachloropropene[1888-71-7]^
6.8
U
ug/L
1
6.8
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Isodrin [465-73-6]^
1.5
U
ug/L
1
1.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Isophorone [78-59-1]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Isosafrole [120-58-1]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Kepone[143-50-0]^
7.2
U
ug/L
1
7.2
20
2G25005
EPA
8270E
07/25/22
19:50
DFM
Methapyrilene [91-80-5]^
4.8
U
ug/L
1
4.8
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Methyl Methanesulfonate [66-27-3]^
2.2
U
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Methyl parathion [298-00-0]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Nitrobenzene [98-95-3]^
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitrosodiethylamine [55-18-5]^
2.1
U
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitrosodimethylamine [62-75-9]^
1.9
U
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitrosodi-n-butylamine [924-16-3]^
2.0
U
ug/L
1
2.0
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
2.3
U
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
[86-30-6/122-39-4]^
N-Nitrosomethylethylamine [10595-95-6]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitrosopiperidine [100-75-4]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
N-Nitrosopyrrolidine [930-55-2]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
0,0,0-Triethylphosphorothioate
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
[126-68-1]^
o-Toluidine [95-53-4]^
1.6
u
ug/L
1
1.6
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Parathion [56-38-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
p-Dimethylaminoazobenzene [60-11-7]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Pentachlorobenzene [608-93-5]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Pentachloronitrobenzene [82-68-8]^
1.9
u
ug/L
1
1.9
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Phenacetin [62-44-2]^
2.7
u
ug/L
1
2.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Phenanthrene[85-01-8]^
2.6
u
ug/L
1
2.6
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Phenol[108-95-2]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Phorate [298-02-2]^
2.1
u
ug/L
1
2.1
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Pronamide[23950-58-5]^
1.7
u
ug/L
1
1.7
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Pyrene [129-00-0]^
3.5
u
ug/L
1
3.5
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Safrole [94-59-7]^
2.2
u
ug/L
1
2.2
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Thionazin [297-97-2]^
2.3
u
ug/L
1
2.3
10
2G25005
EPA
8270E
07/25/22
19:50
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed ffy Notes
2,4,6-Tribromophenol
81
1
100
81 %
10-179
2G25005
EPA 8270E
0712512219:50 DFM
2-Fluorobiphenyl
36
1
50.0
72 %
10-149
2G25005
EPA 8270E
0712512219:50 DFM
2-Fluorophenol
60
1
100
60 %
10-110
2G25005
EPA 8270E
0712512219:50 DFM
Nitrobenzene-d5
37
1
50.0
74 %
10-149
2G25005
EPA 8270E
0712512219:50 DFM
FINAL
This report relates only
to the
sample as received by the laboratory, and may only
be reproduced in full.
I Page 108 of 146

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Phenol-d5
50
1
100
50 %
10-88
2G25005
EPA 8270E
0712512219:50
DFM
Terphenyl-d14
39
1
50.0
78 %
10-188
2G25005
EPA 8270E
0712512219:50
DFM
Organochlorine Pesticides by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
gy
Notes
4,4'-DDD [72-54-8]^
0.044
U
ug/L
1
0.044
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
4,4'-DDE[72-55-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
4,4'-DDT [50-29-3]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Aldrin [309-00-2]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
alpha-BHC [319-84-6]^
0.036
U
ug/L
1
0.036
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
beta-BHC [319-85-7]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Chlordane (tech) [12789-03-6]^
0.37
U
ug/L
1
0.37
0.50
2G26009
EPA 8081B
07/27/22 17:07
LSK
Chlordane -alpha [5103-71-9]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Chlordane -gamma [5103-74-2]^
0.042
U
ug/L
1
0.042
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
delta-BHC [319-86-8]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Dieldrin [60-57-1]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Endosulfan I[959-98-8]^
0.045
U
ug/L
1
0.045
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Endosulfan II[33213-65-9]^
0.038
U
ug/L
1
0.038
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Endosulfan sulfate [1031-07-8]^
0.032
U
ug/L
1
0.032
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Endrin [72-20-8]^
0.041
U
ug/L
1
0.041
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Endrin aldehyde [7421-93-4]^
0.049
U
ug/L
1
0.049
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
gamma-BHC [58-89-9]^
0.034
U
ug/L
1
0.034
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Heptachlor[76-44-8]^
0.047
U
ug/L
1
0.047
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Heptachlor epoxide [1024-57-3]^
0.037
U
ug/L
1
0.037
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Methoxychlor[72-43-5]^
0.048
U
ug/L
1
0.048
0.050
2G26009
EPA 8081B
07/27/22 17:07
LSK
Toxaphene[8001-35-2]^
0.28
U
ug/L
1
0.28
1.0
2G26009
EPA 8081B
07/27/22 17:07
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
2,4,5,6-TCMX
0.81
1
1.00
81 %
10-139
2G26009
EPA 8081E
0712712217:07
LSK
Decachlorobiphenyl
0.77
1
1.00
77 %
10-122
2G26009
EPA 8081E
0712712217:07
LSK
Polychlorinated Biphenyls by GC
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
PCB-1016/1242 [12674-11-2/53469-21-9]^
0.48
U
ug/L
1
0.48
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
PCB-1221[11104-28-2]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
PCB-1232[11141-16-5]^
0.50
U
ug/L
1
0.50
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
PCB-1248[12672-29-6]^
0.45
U
ug/L
1
0.45
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
PCB-1254[11097-69-1]^
0.43
U
ug/L
1
0.43
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
PCB-1260[11096-82-5]^
0.47
U
ug/L
1
0.47
0.50
2G26010
EPA 8082A
07/27/22 17:07
LSK
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,5,E-TCMX
0.80
1
1.00
80 %
10-128
2G26010
EPA 80824
0712712217:07
L5K
Decachlorobiphenyl
0.91
1
1.00
91 %
10-129
2G26010
EPA 80824
0712712217:07
L5K
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 109 of 4G

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF10299-21 Received: 07/21/22 10:00
Matrix: Water Sampled:07/20/22 15:20 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:37
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G25003
EPA 6020B
08/01/22 11:53
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Barium [7440-39-3]^
448
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:46
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:46
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Cobalt[7440-48-4]^
1.43
J
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Nickel[7440-02-O]^
10.2
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G25003
EPA 6020B
08/01/22 11:53
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G25003
EPA 6020B
08/01/22 11:53
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Zinc[7440-66-6]^
80.2
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:46
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
By
Notes
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.010
2G22008
EPA 9014
07/25/22 09:54
MSE
Sulfide [18496-25-8]^
0.010
U
mg/L
1
0.010
0.10
2G26004 >M 4500S2 D-2011
07/26/22 08:23
JOC
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
J
ug/L
1
0.80
2.0
2G28008
EPA 8260D
07/28/22 13:33
JMW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-c48
4.4
1
5.00
89 %
75-125
2G26006
EPA 8260D
071261221333
JMW
Chlorinated Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
2,4,5-T [93-76-5]^
0.28
U
ug/L
1
0.28 0.50
2G27005
EPA 8151A
08/02/22 23:57
`CV
2,4,5-TP (Silvex) [93-72-1]^
0.44
U
ug/L
1
0.44 0.50
2G27005
EPA 8151A
08/02/22 23:57
`CV
2,4-D [94-75-7]^
0.27
U
ug/L
1
0.27 0.50
2G27005
EPA 8151A
08/02/22 23:57
`CV
Dinoseb [88-85-7]^
0.32
U
ug/L
1
0.32 0.50
2G27005
EPA 8151A
08/02/22 23:57
`CV
Pentachlorophenol [87-86-5]^
0.19
U
ug/L
1
0.19 0.50
2G27005
EPA 8151A
08/02/22 23:57
`CV
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
2, 4-DCAA
1.7
1
2.00
84 %
37-134
2G27005
EPA 8151A
08102122 23:57
FCV
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 110 of 146

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TB Lab Sample ID:CF10299-22 Received: 07/21/22 10:00
Matrix: Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,1-Dichloropropene [563-58-6]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2,4-Trichlorobenzene [120-82-1]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,3-Dichlorobenzene [541-73-1]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,3-Dichloropropane [142-28-9]A
0.16
U
ug/L
1
0.16
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
2,2-Dichloropropane [594-20-7]A
0.28
U
ug/L
1
0.28
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY QV-01
3-Chloropropene[107-05-1]A
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2G27028
EPA 8260D
07/27/22 21:56
RKY
Acetonitrile [75-05-8]A
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/27/22 21:56
RKY
Acrolein [107-02-8]A
4.0
U
ug/L
1
4.0
10
2G27028
EPA 8260D
07/27/22 21:56
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2G27028
EPA 8260D
07/27/22 21:56
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Chloroprene [126-99-8]A
0.64
u
ug/L
1
0.64
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
u
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
u
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Dibromochloromethane [124-48-1]A
0.17
u
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Dibromomethane [74-95-3]A
0.27
u
ug/L
1
0.27
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Dichlorodifluoromethane [75-71-8]A
0.20
u
ug/L
1
0.20
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Ethyl Methacrylate [97-63-2]A
0.38
u
ug/L
1
0.38
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Ethylbenzene[100-41-4]A
0.13
u
ug/L
1
0.13
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Hexachlorobutadiene [87-68-3]A
0.22
u
ug/L
1
0.22
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Iodomethane [74-88-4]A
1.7
u
ug/L
1
1.7
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
I Page 111 Of 146

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ANALYTICAL RESULTS
Description: 7401-TB Lab Sample ID:CF10299-22 Received: 07/21/22 10:00
Matrix: Water Sampled:07/19/22 09:50 Work Order: CF10299
Project: Pitt County Landfill Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte I'CAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
Isobutyl alcohol [78-83-1]^
11
U
ug/L
1
11
50
2G27028
EPA 8260D
07/27/22 21:56
RKY
QL-02
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Methacrylonitrile [126-98-7]^
4.9
U
ug/L
1
4.9
10
2G27028
EPA 8260D
07/27/22 21:56
RKY
Methyl Methacrylate [80-62-61^
0.51
U
ug/L
1
0.51
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Methylene chloride [75-09-2]A
0.59
J
ug/L
1
0.23
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
0-01
Naphthalene[91-20-3]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
o-Xylene [95-47-6]^
0.065
U
ug/L
1
0.065
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Propionitrile [107-12-0]^
5.0
U
ug/L
1
5.0
10
2G27028
EPA 8260D
07/27/22 21:56
RKY
Styrene[100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
QV-01
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
U
ug/L
1
0.70
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
QV-01
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Vinyl acetate [108-05-4]^
0.95
U
ug/L
1
0.95
5.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Vinyl chloride [75-01-4]^
0.32
U
ug/L
1
0.32
1.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Xylenes (Total) [1330-20-7]^
0.45
U
ug/L
1
0.45
3.0
2G27028
EPA 8260D
07/27/22 21:56
RKY
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analured
By Notes
4-8romofluorobenzene
59
1
50.0
118 %
53-136
2G27028
EPA 8260D
07127122 21:56
RKY
Dibromofluoromethane
58
1
50.0
117 %
67-129
2G27028
EPA 8260D
07127122 21:56
RKY
Toluene-&
54
1
50.0
108 %
59-134
2G27028
EPA 8260D
07127122 21:56
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 2 Of 146

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ANALYTICAL RESULTS
Description: 7401-MW6R-M Lab Sample ID:CF10299-23 Received: 07/21/22 10:00
Matrix: Ground Water Sampled:07/20/22 15:30 Work Order: CF10299
Project: Pitt County Landfill Sampled By: Emma Shipley
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.150
U
ug/L
1
0.150
0.200
2G27005
EPA 7470A
07/29/22 03:39
CPH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
EDLL
Batch
Method
Analyzed
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2G25003
EPA 6020B
08/01/22 11:57
MAM
Arsenic [7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Barium [7440-39-3]^
2010
ug/L
1
1.10
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2G22020
EPA 6010D
08/01/22 12:49
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2G22020
EPA 6010D
08/01/22 12:49
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Copper[7440-50-8]^
2.20
J
ug/L
1
1.60
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2G25003
EPA 6020B
08/01/22 11:57
MAM
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2G25003
EPA 6020B
08/01/22 11:57
MAM
Tin[7440-31-5]^
2.90
U
ug/L
1
2.90
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
Zinc[7440-66-6]^
14.4
ug/L
1
4.40
10.0
2G22020
EPA 6010D
08/01/22 12:49
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 3 of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2627028 - EPA 50308 MS
Blank (2G27028-BLK3) Prepared: 07/27/2022 14:14 Analyzed: 07/27/2022 20:59
Analvte
Result
Flaq
POL
Units
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
3-Chloropropene
0.11
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acetonitrile
5.0
U
10
ug/L
Acrolein
4.0
U
10
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
Chloroprene
0.64
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethyl Methacrylate
0.38
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
Isobutyl alcohol
11
U
50
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pagel 14 Of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2627028 - EPA 50308 MS - Continued
Blank (2G27028-BLK3) Continued Prepared: 07/27/2022 14:14 Analyzed: 07/27/2022 20:59
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
Methacrylonitrile
4.9
U
10
ug/L
Methyl Methacrylate
0.51
U
1.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Propionitrile
5.0
U
10
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
61
ug/L
50.0
122
53-136
Dibromofluoromethane
58
u9/L
50.0
116
67-129
Toluene-d8
53
u9/L
50.0
106
59-134
LCS (2G27028-BS1)
Prepared: 07/27/2022 14:14 Analyzed: 07/27/2022 19:04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
103
75-133
Benzene
20
1.0
ug/L
20.0
100
80-134
Chlorobenzene
21
1.0
ug/L
20.0
104
80-120
Toluene
24
1.0
ug/L
20.0
118
71-120
Trichloroethene
19
1.0
ug/L
20.0
95
74-120
4-Bromofluorobenzene
61
ug/L
50.0
122
53-136
Dibromofluoromethane
52
u9/L
50.0
104
67-129
Toluene-d8
54
ug/L
50.0
108
59-134
Matrix Spike (2G27028-MS1)
Prepared: 07/27/2022 14:14 Analyzed: 07/27/2022 19:33
Source: CF11059-07
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
105
75-133
Benzene
21
1.0
ug/L
20.0
0.15 U
104
80-134
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
105
80-120
Toluene
24
1.0
ug/L
20.0
0.14 U
119
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
96
74-120
4-Bromofluorobenzene
62
u9/L
50.0
123
53-136
Dibromofluoromethane
52
u9/L
50.0
105
67-129
Toluene-d8
53
u9/L
50.0
106
59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 5 Of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2627028 - EPA 50308 MS - Continued
Matrix Spike Dup (2G27028-MSD1) Prepared: 07/27/2022 14:14 Analyzed: 07/27/2022 20:02
Source: CF11059-07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
103
75-133
2
20
Benzene
20
1.0
ug/L
20.0
0.15 U
102
80-134
3
17
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
106
80-120
0.5
16
Toluene
24
1.0
ug/L
20.0
0.14 U
121
71-120
2
17 QM-07
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
96
74-120
0.2
22
4-Bromofluorobenzene 62 u91L 50.0 123 53-136
Dibromofluoromethane 51 u91L 50.0 102 67-129
Toluene-d8 54 u91L 50.0 108 59-134
Batch 2G27031 - EPA 5030B MS
Blank (2G27031-BLK3) Prepared: 07/27/2022 14:23 Analyzed: 07/29/2022 08:52
Analvte
Result
Flaq
POL
Units
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
3-Chloropropene
0.11
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acetonitrile
5.0
U
10
ug/L
Acrolein
4.0
U
10
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 116 Of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2627031 - EPA 50308 MS - Continued
Blank (2G27031-BLK3) Continued Prepared: 07/27/2022 14:23 Analyzed: 07/29/2022 08:52
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
Chloroprene
0.64
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethyl Methacrylate
0.38
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
Isobutyl alcohol
11
U
50
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methacrylonitrile
4.9
U
10
ug/L
Methyl Methacrylate
0.51
U
1.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Propionitrile
5.0
U
10
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
61
u91L
50.0
122
53-136
Dibromofluoromethane
58
u91L
50.0
116
67-129
Toluene-d8
55
u91L
50.0
109
59-134
LCS (2G27031-BS1)
Prepared: 07/27/2022 14:23 Analyzed: 07/29/2022 06:57
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
98
75-133
Benzene
20
1.0
ug/L
20.0
98
80-134
Chlorobenzene
20
1.0
ug/L
20.0
99
80-120
Toluene
22
1.0
ug/L
20.0
112
71-120
Trichloroethene
19
1.0
ug/L
20.0
97
74-120
4-Bromofluorobenzene
61
u91L
50.0
123
53-136
Dibromofluoromethane
52
u91L
50.0
104
67-129
Toluene-d8
53
u91L
50.0
106
59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 7 Of 46

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2627031 - EPA 50308 MS - Continued
Matrix Spike (2G27031-MSS) Prepared: 07/27/2022 14:23 Analyzed: 07/29/2022 07:26
Source: CF11059-08
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
104
75-133
Benzene
20
1.0
ug/L
20.0
0.15 U
102
80-134
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
104
80-120
Toluene
24
1.0
ug/L
20.0
0.14 U
121
71-120 QM-07
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
103
74-120
4-Bromofluorobenzene
60
u91L
50.0
121
53-136
Dibromofluoromethane
52
u91L
50.0
104
67-129
Toluene-d8
52
u91L
50.0
105
59-134
Matrix Spike Dup (2G27031-MSD1)
Prepared: 07/27/2022 14:23 Analyzed: 07/29/2022 07:55
Source: CF11059-08
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
101
75-133
3
20
Benzene
20
1.0
ug/L
20.0
0.15 U
101
80-134
1
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
99
80-120
5
16
Toluene
23
1.0
ug/L
20.0
0.14 U
115
71-120
5
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
100
74-120
3
22
4-Bromofluorobenzene 60 u91L 50.0 121 53-136
Dibromofluoromethane 51 u91L 50.0 102 67-129
Toluene-d8 54 u91L 50.0 108 59-134
Batch 2HO1045 - EPA 5030B MS
Blank (2H03045-BLK1) Prepared: 08/01/2022 19:22 Analyzed: 08/02/2022 00:02
Analvte
Result
Flaq
POL
Units
1, 1, 1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
3-Chloropropene
0.11
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 8 Of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2HO1045 - EPA 50305 MS - Continued
Blank (2111-103045-BLKI) Continued Prepared: 08/01/2022 19:22 Analyzed: 08/02/2022 00:02
Analvte
Result
Flaq
POL
Units
Acetone
10
U
20
ug/L
Acetonitrile
5.0
U
10
ug/L
Acrolein
4.0
U
10
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
Chloroprene
0.64
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethyl Methacrylate
0.38
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
Isobutyl alcohol
11
U
50
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methacrylonitrile
4.9
U
10
ug/L
Methyl Methacrylate
0.51
U
1.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Propionitrile
5.0
U
10
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 60 u91L 60.0 99 53-136
Dibromofluoromethane 68 u91L 60.0 113 67-129
Toluene-d8 57 u91L 60.0 94 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 1 9 of 46

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2HO1045 - EPA 50305 MS - Continued
LCS (2H01045-BSI) Prepared: 08/01/2022 19:22 Analyzed: 08/01/2022 22:07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
98
75-133
Benzene
20
1.0
ug/L
20.0
102
80-134
Chlorobenzene
20
1.0
ug/L
20.0
99
80-120
Toluene
22
1.0
ug/L
20.0
112
71-120
Trichloroethene
19
1.0
ug/L
20.0
94
74-120
4-Bromofluorobenzene
60
u91L
60.0
100
53-136
Dibromofluoromethane
57
u91L
60.0
95
67-129
Toluene-d8
55
u91L
60.0
91
59-134
Matrix Spike (2H03045-MS1)
Prepared: 08/01/2022 19:22 Analyzed: 08/01/2022 22:35
Source: CF11059-11
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
104
75-133
Benzene
22
1.0
ug/L
20.0
0.15 U
108
80-134
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
104
80-120
Toluene
24
1.0
ug/L
20.0
0.14 U
119
71-120
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
100
74-120
4-Bromofluorobenzene
59
u91L
60.0
96
53-136
Dibromofluoromethane
56
u91L
60.0
94
67-129
Toluene-d8
55
u91L
60.0
91
59-134
Matrix Spike Dup (2H03045-MSD1)
Prepared: 08/01/2022 19:22 Analyzed: 08/01/2022 23:04
Source: CF11059-11
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
93
75-133
11
20
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
14
17
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
93
80-120
11
16
Toluene
21
1.0
ug/L
20.0
0.14 U
104
71-120
13
17
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
86
74-120
14
22
4-Bromofluorobenzene 60 u91L 60.0 101 53-136
Dibromofluoromethane 57 u91L 60.0 95 67-129
Toluene-d8 55 u91L 60.0 92 59-134
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2G25005 -EPA 351OC MS
Blank (2G25005-BLK3) Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 11:56
Analvte
Result
Flaq
POL
Units
1,2,4,5-Tetrachlorobenzene
3.4
U
10
ug/L
1,3,5-Trinitrobenzene
3.0
U
10
ug/L
1,3-Dinitrobenzene
2.5
U
10
ug/L
1,4-Naphthoquinone
2.5
U
10
ug/L
1,4-Phenylenediamine
4.0
U
10
ug/L
1-Naphthylamine
2.2
U
10
ug/L
2,3,4,6-TetrachIorophen o1
2.4
U
10
ug/L
2,4,5-Trichlorophenol
2.5
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 120 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2625005 - EPA 3510C MS - Continued
Blank (2G25005-BLK3) Continued Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 11:56
Analvte
Result
Flaq
POL
Units
2,4,6-Trichlorophenol
2.6
U
10
ug/L
2,4-Dichlorophenol
2.6
U
10
ug/L
2,4-Dimethyl phenol
2.3
U
10
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-Dinitrotoluene
2.6
U
10
ug/L
2,6-Dichlorophenol
2.0
U
10
ug/L
2,6-Dinitrotoluene
2.5
U
10
ug/L
2-Acetylaminofluorene
3.1
U
10
ug/L
2-Chloronaphthalene
2.8
U
10
ug/L
2-Chlorophenol
2.2
U
10
ug/L
2-Methyl-4,6-dinitrophenol
3.3
U
10
ug/L
2- Methyl naphthalene
2.8
U
10
ug/L
2-Methylphenol
2.0
U
10
ug/L
2-Naphthylamine
3.0
U
10
ug/L
2-Nitroaniline
2.5
U
10
ug/L
2-Nitrophenol
1.1
U
10
ug/L
3 & 4-Methylphenol
2.1
U
10
ug/L
3,3'-Dichlorobenzidine
3.5
U
10
ug/L
3,3'-Dimethylbenzidine
2.2
U
10
ug/L
3-Methylcholanthrene
1.3
U
10
ug/L
3-Nitroaniline
2.6
U
10
ug/L
4-Aminobiphenyl
3.5
U
10
ug/L
4-Bromophenyl-phenylether
2.4
U
10
ug/L
4-Chloro-3-methylphenol
2.4
U
10
ug/L
4-Chloroaniline
2.0
U
10
ug/L
4-Chlorophenyl-phenylether
2.6
U
10
ug/L
4-Nitroaniline
3.2
U
10
ug/L
4-Nitrophenol
2.8
U
10
ug/L
5-Nitro-o-toludine
3.2
U
10
ug/L
7,12-Di methyl benz(a)anth racene
1.4
U
10
ug/L
a,a-Dimethylphenethylamine
3.5
U
10
ug/L
Acenaphthene
2.7
U
10
ug/L
Acenaphthylene
2.6
U
10
ug/L
Acetophenone
2.0
U
10
ug/L
Anthracene
2.4
U
10
ug/L
Benzo(a)anthracene
2.4
U
10
ug/L
Benzo(a)pyrene
2.2
U
10
ug/L
Benzo(b)fluoranthene
2.8
U
10
ug/L
Benzo(g,h,i)perylene
2.4
U
10
ug/L
Benzo(k)fluoranthene
2.4
U
10
ug/L
Benzyl alcohol
2.4
U
10
ug/L
Bis(2-chloroethoxy)methane
2.4
U
10
ug/L
Bis(2-chloroethyl)ether
2.6
U
10
ug/L
Bis(2-chloroisopropyl)ether
2.5
U
10
ug/L
Bis(2-ethylhexyl)phthalate
1.9
U
5.0
ug/L
Butyl benzylphtha late
3.8
U
10
ug/L
Chlorobenzilate
2.4
U
10
ug/L
Chrysene
2.2
U
10
ug/L
Diallate
1.9
U
10
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 121 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2625005 - EPA 3510C MS - Continued
Blank (2G25005-BLK3) Continued Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 11:56
Analvte
Result
Flaq
POL
Units
Dibenzo(a,h)anthracene
2.3
U
10
ug/L
Dibenzofuran
2.6
U
10
ug/L
Diethylphtha late
2.4
U
10
ug/L
Dimethoate
2.3
U
10
ug/L
Dimethylphthalate
2.5
U
10
ug/L
Di-n-butylphthalate
2.8
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
Disulfoton
2.0
U
10
ug/L
Ethyl methanesulfonate
2.2
U
10
ug/L
Famphur
2.7
U
10
ug/L
Fluoranthene
3.1
U
10
ug/L
Fluorene
2.5
U
10
ug/L
Hexachlorobenzene
2.3
U
10
ug/L
Hexachlorobutadiene
2.8
U
10
ug/L
Hexachlorocyclopentadiene
2.7
U
10
ug/L
Hexachloroethane
2.6
U
10
ug/L
Hexachloropropene
6.8
U
10
ug/L
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isodrin
1.5
U
10
ug/L
Isophorone
2.5
U
10
ug/L
Isosafrole
2.2
U
10
ug/L
Kepone
7.2
U
20
ug/L
Methapyrilene
4.8
U
10
ug/L
Methyl Methanesulfonate
2.2
U
10
ug/L
Methyl parathion
2.5
U
10
ug/L
Nitrobenzene
2.5
U
10
ug/L
N-Nitrosodiethylamine
2.1
U
10
ug/L
N-Nitrosodimethylamine
1.9
U
10
ug/L
N-Nitrosodi-n-butylamine
2.0
U
10
ug/L
N-Nitroso-di-n-propylamine
2.3
U
10
ug/L
N-nitrosodiphenylamine/Diphenylamine
2.5
U
10
ug/L
N-Nitrosomethylethylamine
1.9
U
10
ug/L
N-Nitrosopiperidine
2.1
U
10
ug/L
N-Nitrosopyrrolidine
1.9
U
10
ug/L
O,O,O-Triethyl phosphorothioate
2.2
U
10
ug/L
o-Toluidine
1.6
U
10
ug/L
Parathion
1.7
U
10
ug/L
p-Dimethylaminoazobenzene
2.6
U
10
ug/L
Pentachlorobenzene
2.7
U
10
ug/L
Pentachloronitrobenzene
1.9
U
10
ug/L
Phenacetin
2.7
U
10
ug/L
Phenanthrene
2.6
U
10
ug/L
Phenol
1.7
U
10
ug/L
Phorate
2.1
U
10
ug/L
Pronamide
1.7
U
10
ug/L
Pyrene
3.5
U
10
ug/L
Safrole
2.2
U
10
ug/L
Thionazin
2.3
U
10
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
2,4,6-Tribromophenol 75 u91L 100 75 10-179
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 122 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2625005 - EPA 3510C MS - Continued
Blank (2G25005-BLK3) Continued Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 11:56
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
2-Fluorobiphenyl
41
u91L
50.0 63 10-149
2-Fluorophenol
70
u91L
100 70 10-110
Nitrobenzene-d5
41
u91L
50.0 82 10-149
Phenohd5
61
u91L
100 61 10-88
Terphenyl-d14
39
u91L
50.0 77 10-188
LCS (2G25005-BSI)
Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 12:25
Spike
Source
%REC RPD
Analvte
Result Flao
POL
Units
Level
Result %REC
Limits RPD Limit Notes
2-Chlorophenol
42
10
ug/L
50.0
84
40-109
4-Chloro-3-methylphenol
45
10
ug/L
50.0
89
58-121
4-Nitrophenol
33
10
ug/L
50.0
67
33-105
Acenaphthene
47
10
ug/L
50.0
95
39-125
N-Nitroso-di-n-propylamine
44
10
ug/L
50.0
87
48-126
Phenol
35
10
ug/L
50.0
71
19-78
Pyrene
46
10
ug/L
50.0
91
44-137
2,4,6-Tribromophenol
98
u91L
100 98 10-179
2-Fluorobiphenyl
43
u91L
50.0 67 10-149
2-Fluorophenol
73
u91L
100 73 10-110
Nitrobenzene-d5
42
u91L
50.0 84 10-149
Phenohd5
63
u91L
100 63 10-88
Terphenyl-d14
41
u91L
50.0 82 10-188
Matrix Spike (2G25005-MS3)
Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 12:55
Source: CF10789-09
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
2-Chlorophenol
38
10
ug/L
50.0
2.2 U
76
40-109
4-Chloro-3-methylphenol
44
10
ug/L
50.0
2.4 U
88
58-121
4-Nitrophenol
27
10
ug/L
50.0
2.8 U
54
33-105
Acenaphthene
49
10
ug/L
50.0
2.7 U
98
39-125
N-Nitroso-di-n-propylamine
48
10
ug/L
50.0
2.3 U
96
48-126
Phenol
22
10
ug/L
50.0
1.7 U
45
19-78
Pyrene
46
10
ug/L
50.0
3.5 U
92
44-137
2,4,6-Tribromophenol
97
u91L
100
97
10-179
2-Fluorobiphenyl
44
u91L
50.0
88
10-149
2-Fluorophenol
53
u91L
100
53
10-110
Nitrobenzene-d5
45
u91L
50.0
90
10-149
Phenol-d5
43
u91L
100
43
10-88
Terphenyl-d14
38
u91L
50.0
76
10-188
Matrix Spike Dup (2G25005-MSD1)
Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 13:25
Source: CF10789-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
2-Chlorophenol
40
10
ug/L
50.0
2.2 U
79
40-109
4
22
4-Chloro-3-methylphenol
42
10
ug/L
50.0
2.4 U
84
58-121
4
22
4-Nitrophenol
31
10
ug/L
50.0
2.8 U
63
33-105
15
27
Acenaphthene
44
10
ug/L
50.0
2.7 U
89
39-125
9
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 123 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2625005 - EPA 3510C MS - Continued
Matrix Spike Dup (2G25005-MSD1) Continued Prepared: 07/25/2022 07:57 Analyzed: 07/25/2022 13:25
Source: CF10789-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
N-Nitroso-di-n-propylamine
40
10
ug/L
50.0
2.3 U
81
48-126
17
23
Phenol
33
10
ug/L
50.0
1.7 U
66
19-78
37
18 QM-11
Pyrene
43
10
ug/L
50.0
3.5 U
87
44-137
6
24
2,4,6-Tribromophenol
100
u91L
100
102
10-179
2-Fluorobiphenyl
42
u91L
50.0
63
10-149
2-Fluorophenol
71
u91L
100
71
10-110
Nitrobenzene-d5
42
u91L
50.0
84
10-149
Phenohd5
60
u91L
100
60
10-88
Terphenyl-d14
39
u91L
50.0
78
10-188
Batch 2G26033 - EPA 3510C MS
Blank (2G26033-BLK3)
Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 11:59
Analvte
1, 2,4, 5-Tetrach I o robenzen e
1,3, 5-Trin itrobenzene
1,3-Dinitrobenzene
1,4-Naphthoquinone
1,4-Phenylened iami ne
1-Naphthylamine
2,3,4,6-Tetrach lorophenol
2,4, 5-Trichlorophenol
2,4, 6-Trich t o rop hen o f
2,4-Dichlorophenol
2,4-Di methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dichlorophenol
2,6-Dinitrotoluene
2-Acetyla m i nofl u o rene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl-4,6-din itrophenol
2- Methyl naphthalene
2-Methylphenol
2-Naphthylamine
2-Nitroaniline
2-Nitrophenol
3 & 4-Methylphenol
3,3'-Dich lorobenzidi ne
3,3'-Dimethyl benzidi ne
3-Methylcholanthrene
3-Nitroaniline
4-Aminobiphenyl
4- B romop heny I-p he nyl ethe r
4-Ch I oro-3-methyl p h en o f
4-Chloroaniline
4-Ch I oroph enyl-phenyl ether
FINAL
Result
Flaq
POL
Units
3.4
U
10
ug/L
3.0
U
10
ug/L
2.5
U
10
ug/L
2.5
U
10
ug/L
4.0
U
10
ug/L
2.2
U
10
ug/L
2.4
U
10
ug/L
2.5
U
10
ug/L
2.6
U
10
ug/L
2.6
U
10
ug/L
2.3
U
10
ug/L
2.6
U
10
ug/L
2.6
U
10
ug/L
2.0
U
10
ug/L
2.5
U
10
ug/L
3.1
U
10
ug/L
2.8
U
10
ug/L
2.2
U
10
ug/L
3.3
U
10
ug/L
2.8
U
10
ug/L
2.0
U
10
ug/L
3.0
U
10
ug/L
2.5
U
10
ug/L
1.1
U
10
ug/L
2.1
U
10
ug/L
3.5
U
10
ug/L
2.2
U
10
ug/L
1.3
U
10
ug/L
2.6
U
10
ug/L
3.5
U
10
ug/L
2.4
U
10
ug/L
2.4
U
10
ug/L
2.0
U
10
ug/L
2.6
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 124 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2626033 - EPA 3510C MS - Continued
Blank (2G26033-BLK3) Continued Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 11:59
Analvte
Result
Flaq
POL
Units
4-Nitroaniline
3.2
U
10
ug/L
4-Nitrophenol
2.8
U
10
ug/L
5-Nitro-o-toluidine
3.2
U
10
ug/L
7,12-Di methyl benz(a)anth racene
1.4
U
10
ug/L
a,a-Dimethylphenethylamine
3.5
U
10
ug/L
Acenaphthene
2.7
U
10
ug/L
Acenaphthylene
2.6
U
10
ug/L
Acetophenone
2.0
U
10
ug/L
Anthracene
2.4
U
10
ug/L
Benzo(a)anthracene
2.4
U
10
ug/L
Benzo(a)pyrene
2.2
U
10
ug/L
Benzo(b)fluoranthene
2.8
U
10
ug/L
Benzo(g,h,i)perylene
2.4
U
10
ug/L
Benzo(k)fluoranthene
2.4
U
10
ug/L
Benzyl alcohol
2.4
U
10
ug/L
Bis(2-chloroethoxy)methane
2.4
U
10
ug/L
Bis(2-chloroethyl)ether
2.6
U
10
ug/L
Bis(2-chloroisopropyl)ether
2.5
U
10
ug/L
Bis(2-ethylhexyl)phthalate
1.9
U
5.0
ug/L
Butyl benzylphtha late
3.8
U
10
ug/L
Chlorobenzilate
2.4
U
10
ug/L
Chrysene
2.2
U
10
ug/L
Diallate
1.9
U
10
ug/L
Dibenzo(a,h)anthracene
2.3
U
10
ug/L
Dibenzofuran
2.6
U
10
ug/L
Diethylphtha late
2.4
U
10
ug/L
Dimethoate
2.3
U
10
ug/L
Dimethylphthalate
2.5
U
10
ug/L
Di-n-butylphthalate
2.8
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
Disulfoton
2.0
U
10
ug/L
Ethyl methanesulfonate
2.2
U
10
ug/L
Famphur
2.7
U
10
ug/L
Fluoranthene
3.1
U
10
ug/L
Fluorene
2.5
U
10
ug/L
Hexachlorobenzene
2.3
U
10
ug/L
Hexachlorobutadiene
2.8
U
10
ug/L
Hexachlorocyclopentadiene
2.7
U
10
ug/L
Hexachloroethane
2.6
U
10
ug/L
Hexachloropropene
6.8
U
10
ug/L
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isodrin
1.5
U
10
ug/L
Isophorone
2.5
U
10
ug/L
Isosafrole
2.2
U
10
ug/L
Kepone
7.2
U
20
ug/L
Methapyrilene
4.8
U
10
ug/L
Methyl Methanesulfonate
2.2
U
10
ug/L
Methyl parathion
2.5
U
10
ug/L
Nitrobenzene
2.5
U
10
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 125 Of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2626033 - EPA 3510C MS - Continued
Blank (2G26033-BLK3) Continued Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 11:59
Analvte
Result
Flaq
POL
Units
N-Nitrosodiethylamine
2.1
U
10
ug/L
N-Nitrosodimethylamine
1.9
U
10
ug/L
N-Nitrosodi-n-butylamine
2.0
U
10
ug/L
N-Nitroso-di-n-propylamine
2.3
U
10
ug/L
N-nitrosodiphenylamine/Di phenylamine
2.5
U
10
ug/L
N-Nitrosomethylethylamine
1.9
U
10
ug/L
N-Nitrosopiperidine
2.1
U
10
ug/L
N-Nitrosopyrrolidine
1.9
U
10
ug/L
0,0,0-Triethylphosphorothioate
2.2
U
10
ug/L
o-Toluidine
1.6
U
10
ug/L
Parathion
1.7
U
10
ug/L
p-Dimethylaminoazobenzene
2.6
U
10
ug/L
Pentachlorobenzene
2.7
U
10
ug/L
Pentachloronitrobenzene
1.9
U
10
ug/L
Phenacetin
2.7
U
10
ug/L
Phenanthrene
2.6
U
10
ug/L
Phenol
1.7
U
10
ug/L
Phorate
2.1
U
10
ug/L
Pronamide
1.7
U
10
ug/L
Pyrene
3.5
U
10
ug/L
Safrole
2.2
U
10
ug/L
Thionazin
2.3
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
72
u91L
100 72 10-179
2-Fluorobiphenyl
37
u91L
50.0 73 10-149
2-Fluorophenol
59
u91L
100 59 10-110
Nitrobenzene-d5
36
u91L
50.0 72 10-149
Phenol-d5
50
u91L
100 50 10-88
TerphenyhdM
34
u91L
50.0 68 10-188
LCS (2G26033-BS1)
Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 12:29
Spike
Source
%REC
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits
2-Chorophenol
35
10
ug/L
50.0
69
40-109
4-Chloro-3-methylphenol
38
10
ug/L
50.0
76
58-121
4-Nitrophenol
19
10
ug/L
50.0
37
33-105
Acenaphthene
45
10
ug/L
50.0
89
39-125
N-Nitroso-di-n-propylamine
45
10
ug/L
50.0
90
48-126
Phenol
19
10
ug/L
50.0
39
19-78
Pyrene
44
10
ug/L
50.0
88
44-137
2,4,6-Tribromophenol
91
u91L
100
91
10-179
2-Fluorobiphenyl
44
u91L
50.0
87
10-149
2-Fluorophenol
46
u91L
100
46
10-110
Nitrobenzene-d5
43
u91L
50.0
86
10-149
Phenol-d5
34
u91L
100
34
10-88
Terphenyl-dM
41
u9/L
50.0
82
10-188
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 126 of 146

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 2626033 - EPA 3510C MS - Continued
Matrix Spike (2G26033-MSS) Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 12:58
Source: CF11059-02
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
2-Chlorophenol
35
10
ug/L
50.0
2.2 U
70
40-109
4-Chloro-3-methylphenol
38
10
ug/L
50.0
2.4 U
75
58-121
4-Nitrophenol
18
10
ug/L
50.0
2.8 U
37
33-105
Acenaphthene
45
10
ug/L
50.0
2.7 U
90
39-125
N-Nitroso-di-n-propylamine
46
10
ug/L
50.0
2.3 U
91
48-126
Phenol
18
10
ug/L
50.0
1.7 U
36
19-78
Pyrene
44
10
ug/L
50.0
3.5 U
89
44-137
2,4,6-Tribromophenol
92
u91L
100
92
10-179
2-Fluorobiphenyl
43
u91L
50.0
87
10-149
2-Fluorophenol
44
u91L
100
44
10-110
Nitrobenzene-d5
42
u91L
50.0
84
10-149
Phenol-d5
33
u91L
100
33
10-88
Terphenyhd14
43
u91L
50.0
85
10-188
Matrix Spike Dup (2G26033-MSD1)
Prepared: 07/26/2022 22:04 Analyzed: 07/28/2022 13:28
Source: CF11059-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
2-Chlorophenol
42
10
ug/L
50.0
2.2 U
84
40-109
19
22
4-Chloro-3-methylphenol
44
10
ug/L
50.0
2.4 U
88
58-121
16
22
4-Nitrophenol
30
10
ug/L
50.0
2.8 U
60
33-105
48
27 QM-11
Acenaphthene
45
10
ug/L
50.0
2.7 U
90
39-125
0.7
25
N-Nitroso-di-n-propylamine
47
10
ug/L
50.0
2.3 U
94
48-126
3
23
Phenol
30
10
ug/L
50.0
1.7 U
59
19-78
47
18 QM-11
Pyrene
46
10
ug/L
50.0
3.5 U
93
44-137
4
24
2,4,6-Tribromophenol 98
u91L
100
98
10-179
2-Fluorobiphenyl 43
u91L
50.0
86
10-149
2-Fluorophenol 70
u91L
100
70
10-110
Nitrobenzene-d5 43
u91L
50.0
85
10-149
Phenol-d5 59
u91L
100
59
10-88
Terphenyl-d14 46
u9/L
50.0
92
10-188
Organochlorine Pesticides by GC - Quality Control
Batch 2626009 - EPA 3510C
Blank (2G26009-BLKI) Prepared: 07/26/2022 09:34 Analyzed: 07/27/2022 12:10
Analvte
Result
Flaq
POL
Units
4,4'-DDD
0.044
U
0.050
ug/L
4,4'-DDE
0.048
U
0.050
ug/L
4,4'-DDT
0.049
U
0.050
ug/L
Aldrin
0.041
U
0.050
ug/L
alpha-BHC
0.036
U
0.050
ug/L
beta-BHC
0.041
U
0.050
ug/L
Chlordane (tech)
0.37
U
0.50
ug/L
Chlordane -alpha
0.048
U
0.050
ug/L
Chlordane -gamma
0.042
U
0.050
ug/L
delta-BHC
0.048
U
0.050
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 127 Of 146

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QUALITY CONTROL DATA
Organochlorine Pesticides by GC - Quality Control
Batch 2626009 - EPA 3510C - Continued
Blank (2G26009-BLK3) Continued Prepared: 07/26/2022 09:34 Analyzed: 07/27/2022 12:10
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Dieldrin
0.045
U
0.050
ug/L
Endosulfan I
0.045
U
0.050
ug/L
Endosulfan II
0.038
U
0.050
ug/L
Endosulfan sulfate
0.032
U
0.050
ug/L
Endrin
0.041
U
0.050
ug/L
Endrin aldehyde
0.049
U
0.050
ug/L
gamma-BHC
0.034
U
0.050
ug/L
Heptachlor
0.047
U
0.050
ug/L
Heptachlor epoxide
0.037
U
0.050
ug/L
Methoxychlor
0.048
U
0.050
ug/L
Toxaphene
0.28
U
1.0
ug/L
2,4,5,6-TCMX
0.74
U91L
1.00
74
10-139
Decachloroblphenyl
0.71
U91L
1.00
71
10-122
LCS (2G26009-BS1)
Prepared: 07/26/2022 09:34 Analyzed: 07/27/2022 12:23
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
4,4'-DDT
1.0
0.050
ug/L
1.00
105
37-139
Dieldrin
1.1
0.050
ug/L
1.00
107
46-132
Endrin
1.1
0.050
ug/L
1.00
106
43-133
2,4,5,E-TCMX
0.87
U91L
1.00
67
10-139
Decachlorobiphenyl
0.77
U91L
1.00
77
10-122
Matrix Spike (2G26009-MS3)
Prepared: 07/26/2022 09:34 Analyzed: 07/27/2022 12:35
Source: CF10299-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
4,4'-DDT
0.87
0.050
ug/L
1.00
0.049 U
87
37-139
Dieldrin
1.0
0.050
ug/L
1.00
0.045 U
102
46-132
Endrin
1.0
0.050
ug/L
1.00
0.041 U
103
43-133
2,4,5,6-TCMX
0.46
U91L
1.00
46
10-139
Decachlorobiphenyl
0.68
U91L
1.00
68
10-122
Matrix Spike Dup (2G26009-MSD1)
Prepared: 07/26/2022 09:34 Analyzed: 07/27/2022 12:47
Source: CF10299-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
4,4'-DDT
0.93
0.050
ug/L
1.00
0.049 U
93
37-139 7
26
Dieldrin
1.1
0.050
ug/L
1.00
0.045 U
108
46-132 6
27
Endrin
1.1
0.050
ug/L
1.00
0.041 U
109
43-133 6
26
2,4,5,E-TCMX
0.68
u9/L
1.00
68
10-139
Decachlorobiphenyl
0.82
U91L
1.00
62
10-122
Polychlorinated Biphenyls by GC - Quality Control
Batch 2G26010 - EPA 3510C
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 128 Of 146

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QUALITY CONTROL DATA
Polychlorinated Biphenyls by GC - Quality Control
Batch 2626010 - EPA 3510C - Continued
Blank (2G26010-BLK3) Prepared: 07/26/2022 09:43 Analyzed: 07/27/2022 12:59
Analvte
Result
Flaq
POL
Units
PCB-1016/1242
0.48
U
0.50
ug/L
PCB-1221
0.43
U
0.50
ug/L
PCB-1232
0.50
U
0.50
ug/L
PCB-1248
0.45
U
0.50
ug/L
PCB-1254
0.43
U
0.50
ug/L
PCB-1260
0.47
U
0.50
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,5,E-TCMX 0.60 u91L 1.00 60 10-128
Decachlorobiphenyl 0.69 u91L 1.00 69 10-129
LCS (2G26010-BS1) Prepared: 07/26/2022 09:43 Analyzed: 07/27/2022 13:11
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
PCB-1016/1242
11 0.50
ug/L
10.0 113 43-123
PCB-1260
11 0.50
ug/L
10.0 109 41-125
2,4,5,E-TCMX
0.69
u91L
1.00 69 10-128
Decachlorobiphenyl
0.73
u91L
1.00 73 10-129
Matrix Spike (2G26030-MS1)
Prepared: 07/26/2022 09:43 Analyzed: 07/27/2022 13:24
Source: CF10299-01
Spike
Source
%REC RPD
Analvte
Result Flaa Q Units
Level
Result
%REC Limits RPD Limit Notes
PCB-1016/1242
10 0.50 ug/L
10.0
0.48 U
103 43-123
PCB-1260
9.5 0.50 ug/L
10.0
0.47 U
95 41-125
2,4,5,E-TCMX
0.46
u91L
1.00
46
10-128
Decachlorobiphenyl
0.68
u91L
1.00
68
10-129
Matrix Spike Dup (2G26010-MSD1)
Prepared: 07/26/2022 09:43 Analyzed: 07/27/2022 13:36
Source: CF10299-01
Spike
Source
%REC
RPD
Analvte
Result Flaq POL
Units
Level
Result %REC
Limits RPD
Limit Notes
PCB-1016/1242
10 0.50
ug/L
10.0
0.48 U 101
43-123 2
23
PCB-1260
9.5 0.50
ug/L
10.0
0.47 U 95
41-125 0.5
31
2,4,5,E-TCMX
0.47
u91L
1.00
47
10-128
Decachlorobiphenyl
0.64
u91L
1.00
64
10-129
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 2G22028 - EPA 245.1
Blank (2G22028-BLK3)
Prepared: 07/22/2022 16:58 Analyzed: 07/26/2022 02:11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.150 U 0.200 ug/L
LCS (2G22028-BSI) Prepared: 07/22/2022 16:58 Analyzed: 07/26/2022 02:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 5.01 0.200 ug/L 5.00 100 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 129 Of 146

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 262202B - EPA 245.1 - Continued
Matrix Spike (2G22028-MSS)
Prepared: 07/22/2022 16:58 Analyzed: 07/26/2022 02:24
Source: CF08094-03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Mercury
5.05
0.200
ug/L
5.00 0.150 U 101 75-125
Matrix Spike Dup (2G22028-MSD1)
Prepared: 07/22/2022 16:58 Analyzed: 07/26/2022 02:27
Source: CF08094-03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Mercury
5.21
0.200
ug/L
5.00 0.150 U 104 75-125 3
25
Post Spike (2G22028-PSI)
Prepared: 07/22/2022 16:58 Analyzed: 07/26/2022 02:30
Source: CF08094-03
Spike Source %REC
RPD
Analvte
Result Flao
POL
Units
Level Result %REC Limits RPD
Limit Notes
Mercury
5.80
0.200
ug/L
4.76-0.00162 122 75-125
Batch 2G27005 - EPA 245.1
Blank (2G27005-BLK3) Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:33
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.150 U 0.200 ug/L
Blank (2G27005-BLK2) Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:35
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Mercury 3.00 U 4.00 ug/L
LCS (2G27005-BSI) Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:40
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.60
0.200
ug/L
5.00
112
80-120
Matrix Spike (2G27005-MS1)
Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:42
Source: CF10299-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.31
0.200
ug/L
5.00
0.150 U
86
75-125
Matrix Spike Dup (2G27005-MSD1)
Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:45
Source: CF10299-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.28
0.200
ug/L
5.00
0.150 U
86
75-125 0.6
25
Post Spike (2G27005-PSI)
Prepared: 07/27/2022 04:23 Analyzed: 07/29/2022 02:54
Source: CF10299-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.83
0.200
ug/L
4.76
0.0144
101
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods -
Quality Control
Batch 2622020 - EPA 3005A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13O Of 146

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2622020 - EPA 3005A - Continued
Blank (2G22020-BLK3) Prepared: 07/22/2022 14:11 Analyzed: 08/01/2022 11:14
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Tin
2.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2G22020-BS1)
Prepared: 07/22/2022 14:11 Analyzed: 08/01/2022 11:22
Spike
Source %REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC Limits RPD Limit Notes
Arsenic
213
10.0
ug/L
200
107 80-120
Barium
212
10.0
ug/L
200
106 80-120
Beryllium
20.5
1.00
ug/L
20.0
102 80-120
Cadmium
21.1
1.00
ug/L
20.0
105 80-120
Chromium
205
10.0
ug/L
200
102 80-120
Cobalt
210
10.0
ug/L
200
105 80-120
Copper
201
10.0
ug/L
200
100 80-120
Lead
205
10.0
ug/L
200
103 80-120
Nickel
212
10.0
ug/L
200
106 80-120
Silver
204
10.0
ug/L
200
102 80-120
Tin
206
10.0
ug/L
200
103 80-120
Vanadium
202
10.0
ug/L
200
101 80-120
Zinc
213
10.0
ug/L
200
107 80-120
Matrix Spike (2G22020-MS3)
Prepared:
07/22/2022 14:11 Analyzed: 08/01/2022 11:29
Source: CF10299-01
Spike
Source
%REC RPD
Analvte
Result Flao
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
208
10.0
ug/L
200
7.60 U
104
75-125
Barium
313
10.0
ug/L
200
104
104
75-125
Beryllium
20.5
1.00
ug/L
20.0
0.209
102
75-125
Cadmium
20.9
1.00
ug/L
20.0
0.360 U
104
75-125
Chromium
205
10.0
ug/L
200
1.40 U
103
75-125
Cobalt
210
10.0
ug/L
200
1.40 U
105
75-125
Copper
202
10.0
ug/L
200
1.60 U
101
75-125
Lead
204
10.0
ug/L
200
3.10 U
102
75-125
Nickel
212
10.0
ug/L
200
2.20 U
106
75-125
Silver
203
10.0
ug/L
200
1.90 U
101
75-125
Tin
207
10.0
ug/L
200
2.90 U
104
75-125
Vanadium
202
10.0
ug/L
200
1.40 U
101
75-125
Zinc
223
10.0
ug/L
200
10.5
106
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 131 of 146

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2622020 - EPA 3005A - Continued
Matrix Spike Dup (2G22020-MSD1)
Prepared:
07/22/2022
14:11 Analyzed: 08/01/2022 11:31
Source: CF10299-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
218
10.0
ug/L
200
7.60 U
109 75-125 5
20
Barium
318
10.0
ug/L
200
104
107 75-125 2
20
Beryllium
21.0
1.00
ug/L
20.0
0.209
104 75-125 2
20
Cadmium
21.4
1.00
ug/L
20.0
0.360 U
107 75-125 2
20
Chromium
208
10.0
ug/L
200
1.40 U
104 75-125 2
20
Cobalt
215
10.0
ug/L
200
1.40 U
107 75-125 2
20
Copper
205
10.0
ug/L
200
1.60 U
102 75-125 1
20
Lead
211
10.0
ug/L
200
3.10 U
106 75-125 4
20
Nickel
217
10.0
ug/L
200
2.20 U
109 75-125 3
20
Silver
205
10.0
ug/L
200
1.90 U
102 75-125 1
20
Tin
212
10.0
ug/L
200
2.90 U
106 75-125 2
20
Vanadium
205
10.0
ug/L
200
1.40 U
103 75-125 2
20
Zinc
229
10.0
ug/L
200
10.5
109 75-125 3
20
Post Spike (2G22020-PS1)
Prepared:
07/22/2022
14:11 Analyzed: 08/01/2022 11:34
Source: CF10299-01
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.218
0.0100
mg/L
0.200
0.00400
107
80-120
Barium
0.320
0.0100
mg/L
0.200
0.104
108
80-120
Beryllium
0.0212
0.00100
mg/L
0.0200
0.000209
105
80-120
Cadmium
0.0216
0.00100
mg/L
0.0200
0.000131
108
80-120
Chromium
0.210
0.0100
mg/L
0.200
0.00113
105
80-120
Cobalt
0.217
0.0100
mg/L
0.200
0.00125
108
80-120
Copper
0.208
0.0100
mg/L
0.200
0.000713
103
80-120
Lead
0.210
0.0100
mg/L
0.200
0.00125
104
80-120
Nickel
0.219
0.0100
mg/L
0.200
0.00142
109
80-120
Silver
0.208
0.0100
mg/L
0.200
0.000201
104
80-120
Tin
0.212
0.0100
mg/L
0.200
-0.00102
106
80-120
Vanadium
0.208
0.0100
mg/L
0.200
0.000775
103
80-120
Zinc
0.231
0.0100
mg/L
0.200
0.0105
110
80-120
Batch 2G22022 - EPA 3005A
Blank (2G22022-BLK3)
Prepared:
07/22/2022
14:15 Analyzed: 07/28/2022 13:19
Spike Source %REC RPD
Analvte
Result
Flao
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2G22022-BSI)
Prepared: 07/22/2022 14:15 Analyzed: 07/28/2022 13:23
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Antimony
21.5
1.00
ug/L
20.0
108
80-120
Selenium
18.8
1.00
ug/L
20.0
94
80-120
Thallium
21.6
1.00
ug/L
20.0
108
80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 132 Of 146

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2G22022 - EPA 3005A - Continued
Matrix Spike (2G22022-MSS)
Prepared: 07/22/2022 14:15 Analyzed: 07/28/2022 13:32
Source: CF09190-12
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
43.6
2.00
ug/L
40.0 0.740 U 109 75-125
Selenium
42.8
2.00
ug/L
40.0 1.82 U 107 75-125
Thallium
43.9
2.00
ug/L
40.0 0.220 U 110 75-125
Matrix Spike Dup (2G22022-MSD1)
Prepared: 07/22/2022 14:15 Analyzed: 07/28/2022 13:46
Source: CF09190-12
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
43.7
2.00
ug/L
40.0 0.740 U 109 75-125 0.3
20
Selenium
45.0
2.00
ug/L
40.0 1.82 U 112 75-125 5
20
Thallium
43.9
2.00
ug/L
40.0 0.220 U 110 75-125 0.05
20
Post Spike (2G22022-PSI)
Prepared: 07/22/2022 14:15 Analyzed: 07/28/2022 13:51
Source: CF09190-12
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
22.0
1.00
ug/L
20.0 0.0543 110 75-125
Selenium
21.0
1.00
ug/L
20.0-0.0363 105 75-125
Thallium
22.0
1.00
ug/L
20.0 0.0502 110 75-125
Batch 2G25003 - EPA 3005A
Blank (2G25003-BLK3)
Prepared: 07/25/2022 05:39 Analyzed: 08/01/2022 10:25
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2G25003-BS1)
Prepared: 07/25/2022 05:39 Analyzed: 08/01/2022 10:29
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
21.5
1.00
ug/L
20.0 108 80-120
Selenium
21.8
1.00
ug/L
20.0 109 80-120
Thallium
22.3
1.00
ug/L
20.0 112 80-120
Matrix Spike (2G25003-MS1)
Prepared: 07/25/2022 05:39 Analyzed: 08/01/2022 10:37
Source: CF09537-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
44.1
2.00
ug/L
40.0 0.740 U 110 75-125
Selenium
44.3
2.00
ug/L
40.0 1.82 U 111 75-125
Thallium
45.1
2.00
ug/L
40.0 0.220 U 113 75-125
Matrix Spike Dup (2G25003-MSD1)
Prepared: 07/25/2022 05:39 Analyzed: 08/01/2022 10:42
Source: CF09537-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Antimony
44.1
2.00
ug/L
40.0
0.740 U
110
75-125
0.006
20
Selenium
42.7
2.00
ug/L
40.0
1.82 U
107
75-125
4
20
Thallium
45.6
2.00
ug/L
40.0
0.220 U
114
75-125
1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 133 Of 146

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2625003 - EPA 3005A - Continued
Post Spike (2G25003-PSI)
Prepared: 07/25/2022 05:39 Analyzed: 08/01/2022 10:46
Source: CF09537-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Antimony
21.8
1.00
ug/L
20.0
0.00930
109
75-125
Selenium
22.2
1.00
ug/L
20.0
0.0312
111
75-125
Thallium
22.7
1.00
ug/L
20.0
0.00481
113
75-125
Classical Chemistry Parameters - Quality Control
Batch 2622008 - Same
Blank (2G22008-BLK3) Prepared: 07/22/2022 10:04 Analyzed: 07/25/2022 09:46
Spike Source %REC RPD
Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.010 mg/L
LCS (2G22008-BS1) Prepared: 07/22/2022 10:04 Analyzed: 07/25/2022 09:47
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.16
0.010
mg/L
0.150 106 85-115
Matrix Spike (2G22008-MS1)
Prepared: 07/22/2022 10:04 Analyzed: 07/25/2022 09:51
Source: CF03558-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.25
0.010
mg/L
0.150 0.11 94 85-115
Matrix Spike (2G22008-MS2)
Prepared: 07/22/2022 10:04 Analyzed: 07/25/2022 09:56
Source: CF10299-21
Spike Source %REC
RPD
Analvte
Result
Flao
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.14
0.010
mg/L
0.150 0.0049 U 96 85-115
Matrix Spike Dup (2G22008-MSD1)
Prepared: 07/22/2022 10:04 Analyzed: 07/25/2022 09:53
Source: CF03558-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.24
0.010
mg/L
0.150 0.11 89 85-115 3
20
Batch 2G26004 - NO PREP
Blank (2G26004-BLK3) Prepared: 07/26/2022 08:10 Analyzed: 07/26/2022 08:23
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sulfide 0.010 U 0.10 mg/L
LCS (2G26004-BSI) Prepared: 07/26/2022 08:10 Analyzed: 07/26/2022 08:23
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sulfide 0.40 0.10 mg/L 0.401 99 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 134 Of 46

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2626004 - NO PREP - Continued
Duplicate (2G26004-DUPl)
Prepared: 07/26/2022 08:10 Analyzed: 07/26/2022 08:23
Source: CF09538-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Sulfide
0.010
U
0.10
mg/L
0.010 U
25
Matrix Spike (2G26004-MS1)
Prepared: 07/26/2022 08:10 Analyzed: 07/26/2022 08:23
Source: CF09538-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Sulfide
0.40
0.10
mg/L
0.401 0.010 U 100 80-120
Matrix Spike Dup (2G26004-MSD3)
Prepared: 07/26/2022 08:10 Analyzed: 07/26/2022 08:23
Source: CF09538-01
Spike Source %REC
RPD
Analvte
Result
Flan
POL
Units
Level Result %REC Limits RPD
Limit Notes
Sulfide
0.40
0.10
mg/L
0.401 0.010 U 101 80-120 1
25
Batch 2G27014 - Same
Blank (2G27014-BLK3) Prepared: 07/27/2022 09:51 Analyzed: 07/28/2022 10:03
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.010 mg/L
LCS (2G27014-BS1) Prepared: 07/27/2022 09:51 Analyzed: 07/28/2022 10:38
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.14
0.010
mg/L
0.150 95 85-115
Matrix Spike (2G27014-MS3)
Prepared: 07/27/2022 09:51 Analyzed: 07/28/2022 10:41
Source: CF09538-01
Spike Source %REC
RPD
Analvte
Result Flan
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.13
0.010
mg/L
0.150 0.0049 U 85 85-115
Matrix Spike Dup (2G27014-MSD1)
Prepared: 07/27/2022 09:51 Analyzed: 07/28/2022 10:43
Source: CF09538-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.10
0.010
mg/L
0.150 0.0049 U 70 85-115 19
20
QM-07
Batch 2G29021 - Same
Blank (2G29021-BLK3) Prepared: 07/29/2022 09:52 Analyzed: 08/01/2022 09:53
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.010 mg/L
LCS (2G29021-BSI) Prepared: 07/29/2022 09:52 Analyzed: 08/01/2022 09:54
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.16 0.010 mg/L 0.150 106 85-115
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 135 Of 146

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2629021 - Same - Continued
Matrix Spike (2G29021-MSS)
Prepared: 07/29/2022 09:52 Analyzed: 08/01/2022 10:01
Source: CF09537-20
Analvte Result Flaq
Cyanide (total) 0.17
POL Units
0.010 mg/L
Spike Source %REC
Level Result %REC Limits RPD
0.150 0.0049 U 113 85-115
RPD
Limit Notes
Matrix Spike Dup (2G29021-MSD3)
Prepared: 07/29/2022 09:52 Analyzed: 08/01/2022 10:03
Source: CF09537-20
Analvte Result Flaa
Cyanide (total) 0.13
POL Units
0.010 mg/L
Spike Source %REC
Level Result %REC Limits RPD
0.150 0.0049 U 87 85-115 26
RPD
Limit Notes
20 QM-11
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2G26014 - EPA 5030E MS
Blank (2G26014-BLK3)
Prepared: 07/26/2022 10:07 Analyzed: 07/26/2022 12:08
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-d8 4.6 u91L 5.00 93 75-125
LCS (2G26014-BSI) Prepared: 07/26/2022 10:07 Analyzed: 07/26/2022 10:25
Spike Source %REC RPD
Analyte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 23 2.0 ug/L 25.0 91 80-133
Toluene-d8
4.6
u91L
5.00 91 75-125
Matrix Spike (2G26014-MS1)
Prepared: 07/26/2022 10:07 Analyzed: 07/26/2022 10:51
Source: CF10299-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
23
2.0
ug/L
25.0 0.80 U 90 80-133
Toluene-&
4.8
u91L
5.00 96 75-125
Matrix Spike Dup (2G26014-MSD1)
Prepared: 07/26/2022 10:07 Analyzed: 07/26/2022 11:16
Source: CF10299-01
Spike Source %REC
RPD
Analyte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
23
2.0
ug/L
25.0 0.80 U 94 80-133 4
19
Toluene-& 4.8 u91L 5.00 96 75-125
Batch 2G28008 - EPA 5030E MS
Blank (2G28008-BLK1) Prepared: 07/28/2022 07:44 Analyzed: 07/28/2022 12:24
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-& 4.5 u91L 5.00 91 75-125
LCS (2G28008-BSI) Prepared: 07/28/2022 07:44 Analyzed: 07/28/2022 10:02
Spike Source %REC RPD
Analyte Result Flao POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 136 Of 146

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2G2BOOB - EPA 5030E MS - Continued
LCS (2G28008-BS3) Continued Prepared: 07/28/2022 07:44 Analyzed: 07/28/2022 10:02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
22
2.0
ug/L
25.0 86 80-133
Toluene-d8
4.4
u91L
5.00 67 75-125
Matrix Spike (2G28008-MS1)
Prepared: 07/28/2022 07:44 Analyzed: 07/28/2022 10:39
Source: AF05576-04
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
24
2.0
ug/L
25.0 1.0 92 80-133
Toluene-d8
4.3
u91L
5.00 86 75-125
Matrix Spike Dup (2G28008-MSDI)
Prepared: 07/28/2022 07:44 Analyzed: 07/28/2022 11:05
Source: AF05576-04
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
25
2.0
ug/L
25.0 1.0 95 80-133 3
19
Toluene-d8 4.5 u91L 5.00 89 75-125
Batch 2G29020 - EPA 50308 MS
Blank (2G29020-BLK3) Prepared: 07/29/2022 00:00 Analyzed: 07/29/2022 13:57
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-d8 4.4 u91L 5.00 87 75-125
LCS (2G29020-BSI) Prepared: 07/29/2022 00:00 Analyzed: 07/29/2022 11:41
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 22 2.0 ug/L 25.0 88 80-133
Toluene-d8 4.3 u91L 5.00 85 75-125
Matrix Spike (2G29020-MS1) Prepared: 07/29/2022 00:00 Analyzed: 07/29/2022 12:14
Source: AF05576-05
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 24 2.0 ug/L 25.0 1.4 91 80-133
Toluene-d8
4.2
u91L
5.00
84
75-125
Matrix Spike Dup (2G29020-MSD1)
Prepared: 07/29/2022 00:00 Analyzed: 07/29/2022 12:40
Source: AF05576-05
Spike
Source
%REC RPD
Analvte
Result Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,4-Dioxane
24 2.0
ug/L
25.0
1.4 92
80-133 1 19
Toluene-&
4.3
u91L
5.00
86
75-125
Chlorinated Herbicides by GC - Quality Control
Batch 2625024 - EPA 3510C
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 137 Of 146

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QUALITY CONTROL DATA
Chlorinated Herbicides by GC - Quality Control
Batch 2625024 - EPA 3510C - Continued
Blank (2G25024-BLK3) Prepared: 07/25/2022 11:45 Analyzed: 07/28/2022 08:41
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
2,4,5-T
0.28
U
0.50
ug/L
2,4,5-TP (Silvex)
0.44
U
0.50
ug/L
2,4-D
0.27
U
0.50
ug/L
Dinoseb
0.32
U
0.50
ug/L
Pentachlorophenol
0.19
U
0.50
ug/L
2,4-DC,4A
2.1
u91L
2.00 107 37-134
Blank (2G25024-BLK2)
Prepared: 07/25/2022 11:45 Analyzed: 07/28/2022 09:08
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-T
0.28
U
0.50
ug/L
2,4,5-TP (Silvex)
0.44
U
0.50
ug/L
2,4-D
0.27
U
0.50
ug/L
Dinoseb
0.32
U
0.50
ug/L
Pentachlorophenol
0.19
U
0.50
ug/L
2,4-DC,4A
2.2
u91L
2.00 112 37-134
LCS (2G25024-BS3)
Prepared: 07/25/2022 11:45 Analyzed: 07/28/2022 09:33
Spike Source %REC
RPD
Analvte
Result
Flaa
CQ
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-TP (Silvex)
1.9
0.50
ug/L
2.00 97 24-135
2,4-D
1.7
0.50
ug/L
2.00 84 20-134
2, 4-DCAA
1.8
u91L
2.00 91 37-134
Matrix Spike (2G25024-MS1)
Prepared: 07/25/2022 11:45 Analyzed: 07/28/2022 09:58
Source: AF05445-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-TP (Silvex)
2.0
0.50
ug/L
2.00 0.44 U 98 24-135
2,4-D
2.3
0.50
ug/L
2.00 0.27 U 114 20-134
2, 4-DCAA
2.0
u91L
2.00 100 37-134
Matrix Spike Dup (2G25024-MSDI)
Prepared: 07/25/2022 11:45 Analyzed: 07/28/2022 10:23
Source: AF05445-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-TP (Silvex)
1.7
0.50
ug/L
2.00 0.44 U 87 24-135
19
2,4-D
2.3
0.50
ug/L
2.00 0.27 U 114 20-134 0.4
19
2,4-DC.4A
1.9
u91L
2.00 94 37-134
Batch 2627005 - EPA 3510C
Blank (2G27005-BLK3)
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 16:24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-T 0.28 U 0.50 ug/L
2,4,5-TP (Silvex) 0.44 U 0.50 ug/L
2,4-D 0.27 U 0.50 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 138 of 146

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QUALITY CONTROL DATA
Chlorinated Herbicides by GC - Quality Control
Batch 2G27005 - EPA 3510C - Continued
Blank (2G27005-BLK1) Continued
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 16:24
Spike
Source
%REC
RPD
Analvte
Resin
Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Dinoseb
0.32
U
0.50
ug/L
Pentachlorophenol
0.19
U
0.50
ug/L
2, 4-DCAA [2CJ
1.6
u91L
2.00
80
37-134
Blank (2G27005-BLK2)
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 16:49
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
2,4,5-T
1.4
U
2.5
ug/L
2,4,5-TP (Silvex)
2.2
U
2.5
ug/L
2,4-D
1.4
U
2.5
ug/L
Dinoseb
1.6
U
2.5
ug/L
Pentachlorophenol
0.95
U
2.5
ug/L
2, 4-DCAA [2C]
9.0
u9/L
10.0
90
37-134
LCS (2G27005-BSI)
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 17:14
Spike
Source
%REC
RPD
Analvte
Result
Flao
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
2,4,5-TP (Silvex)
1.4
0.50
ug/L
2.00
71
24-135
2,4-D
1.9
0.50
ug/L
2.00
96
20-134
2, 4-DCAA [2C]
2.2
u91L
2,00
111
37-134
Matrix Spike (2G27005-MS1)
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 17:39
Source: AF04821-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
2,4,5-TP (Silvex)
8.0
2.5
ug/L
10.0
2.2 U
80
24-135
2,4-D
11
2.5
ug/L
10.0
1.4 U
106
20-134
2,4-DC4A [2C]
16
u91L
10.0
158
37-134
QS-03
Matrix Spike Dup (2G27005-MSD1)
Prepared: 07/27/2022 07:45 Analyzed: 08/02/2022 18:04
Source: AF04821-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
POL
Units
Level
Result
%REC
Limits RPD
MMR
Notes
2,4,5-TP (Silvex)
6.4
2.5
ug/L
10.0
2.2 U
64
24-135 22
19
QM-11
2,4-D
8.0
2.5
ug/L
10.0
1.4 U
80
20-134 29
19
QM-11
2,4-DCAA [2C]
12
u91L
10.0
123
37-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 139 Of 46

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
1-04 Result may be biased high. Associated calibration verification standard exceeded the upper control limit.
1-05 Result may be biased low. Associated calibration verification standard did not meet the minimum control
limit.
0-01 This compound is a common laboratory contaminant.
QI-02 Internal standard outside acceptance limits. Samples results are considered estimated.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QS-03 Surrogate recovery outside acceptance limits
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14O Of 146

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U}
U

Sample Preservation Verification
ENCO Cary
Work Order: CF10299 Project Pitt County Landfill
Client: Groundwater Management Associates Inc. (GR022, Project#: [none]
Loggedin: 21-Jul-22 11.26 Logged By: Rachel Ann Y nish
Preservation Check Performed By. Date/Time: ! _LO
CF10299-01
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent UsedlComments
D
250mLA TEST)
Pest pH 5-9
Y / N I NA
Y / NA
E
250mLP+HNO3
<2
Y/ N I NA
Y /U NA
F
250mLP+Na0H
>12
/ N 1 NA
YIN 1 NA
G
250mLP+ZnAc+NaOH
>9
/ N I NA
Y I N I NA
CF10299-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
PH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
I N/ NA
Y N NA
E
250niLP+NaOH
>12
Y I N I NA
Y I N/ NA
250mLP+ZnAc+Na0H
>9
Y/ N I NA
Y 1 N 1 NA
CF10299-03
Cent
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y N/ NA
Y i N l NA
E
250mLP+HNO3
<2
Y I N I NA
Y 10 NA
F
250mLP+Na0H
>12
Y I N/ NA
Y 4LQ NA
G
25OmLP+ZnAc+NaOH
>9
Y 1 N/ NA
Y I ! NA
C F 10299-04
Cont
Type
Pres (pH)
Requirement
pH Checked/
In Control
pH Adjusted Date�rrie
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y I N/ NA
Y NA
E
250mLP+HNO3
<2
Y/ N! NA
Y N NA
F
250mLP+Na0H
>12
N! NA
Y N I NA
G
250mLP+ZnAc+NaOH
>9
:3Y/
/ N I NA
Y kq NA
CF10299-05
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y/ N r NA
Y I N NA
E
250mLP+Na0H
>12
Y 1 N ! NA
/ NA�Lila '{(
(-�lI ` >
`�
F
250mL P+ZnAc+Na0H
>9
Y / N ! NA
Y / NA
�'
Page 143 of 146
C;lelmntlPrint\wko_PreservationCheck. rpt

Sample Preservation Verification
ENCO Cary
Work Order: CF10299 Project: Pitt County Landfill
Client: Groundwater Management Associates, Inc. (GR022; Project #. [none]
Lagged In: 21-Jul-22 11:26 Logged By Rachel An^n� oni h ` l
Preservation Check Performed By: Date/Time: _I Z� Iz,& i
CF10299-06
Cont
Type Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mt P+1­11\103
r N I NA
Y '�N-�l NA
CF10299-07
Cent
Type
Pfes (p1l) pH Checked 1
Requirement In Control
H Adusted DatelTime
ptAdiusted
Reagent Used/Comments
D
250mLA {PEST)
Pest pH 5-9 Y N/ NA
Y N NA
E
250mt-P+HNO3
<2 Y N I NA
Y N NA
H
250mLP+NaOH
>12 Y/ N/ NA
Y
N NA
G
250mLP+ZnAc+NaOH
>9 YIN / NA
Y CN> NA
CF10299-08
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y / N / NA
Y N NA
E
250mLP+HNO3
<2
Y I N I NA
Y 1 N NA
F
250mLP+NaOH
>12
Y—), N / NA
YIN NA
G
250mLP+ZnAc+N@0H
>9
Y / N / NA
Y / N / NA
CF10299-09
Cont
Type
Pres (pH)
Requirement
p1-1 Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y I N I NA
Y N NA
E
250mLP+NaOH
>12
Y ! N ! NA
Y N / NA
F
250mLP+ZnAc+Na0H
9
Y N/ NA
U1 NA "] 1
f ~}
CF10299-10
W
Cont
Type
Pres (pH)
pH Checked 1
PkI Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
72
Y N/ NA
Y N I NP.
CF10299-11
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
D
250mLA (PEST)
Pest pH 5-9
Y) N / NA
Y / NA
E
250mLP+HNO3
<2
(9 N/ NA
Y I N NA
F
250mLP+NaOH
>12
Y/ N/ NA
Y I N NA
G
250mLP+ZnAc+NaOH
>9
ON/NA
Y /O NA
Page 144 of 146
C:IelmntlPrintlwko_PreservationChteck rpt

Sample Preservation Verification
ENCO Cary 9 CEOD
Work Order: CF10299 Project: Pitt County Landfill
Client Groundwater Management Associates, Inc (GR022, Project#: [nonej
Logged In 21-Jul-22 11:26 Logged By: Rachel Ann Y ni ``
Preservation Check Performed By `l L1DatelTime: ����Z CO
CF10299-12
Cont
Type
Prey (PH)
Requirement
pH Checked I
In Control
pH Adjusted Datef-Fime
Adjusted
Reagent Used/Cornments
D
250mLA (PEST)
Pest pH 5.9
4/
/ N 1 NA
Y 'N / NA
E
250mLP+NaOH
>12
N I NA
Y N I NA
1. F
250mLP+ZnAc+NaOH
>9
/ N I NA.
Y I N NA
CF10299-13
Cont
T
Pres (pH)
Requirement
pH Checked /
in Control
Date/Time
pH Adjusted Adjusted
Reagent Used/Comments
A
250rnL,P+HNO3
<2
Y/ N I NA
Y N` NA
CF10299-14
Cont
Type
(pH)
Requirement
PH Checked /
in Control
DatelTime
PH Adjusted Adjusted
Reagent Used/Comments
D
250ml-A(PEST)
Pest pH 5-9 1
Y I N/ NA
Y N I NA
E
250mLP+NaOH
>12
Y I N I NA
Y N I NA
F
250ml-P+ZnAc+NaOH
7Et
Y I N l NA
Y / / NA-7 ( 'q Op
Vr'L
C F 10299-15
d
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent UsedlComments
A
250ml- +HNO3
'2
YJ N I NA
Y/ N NA
CF10299-18
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted. Date�me
Adjusted
Reagent UsedlComments
D
250ml-A (PEST)
Pest pH 5-9
Y N/ NA
Y N NA
E
250mLP+HNO3
<2
N / NA
Y &N NA
F
250mLP+NaOH
>12
BY L/NA
Y N/ NA.G
250mLP+ZnAc+NaOH
>�
Y I N/ NA
CF10299-19
Cont
Type
Pres (pH)
pH Checked I
In Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
D
250ml-A (PEST)
Pest pH 5-9
Y N / NA
Y ((N) NA
E
250mLP+HNO3
<2
Y I N/ NA
Y N NA
F
250mLP+NaOH
>12 1Y
N/ NA
Y N/ NA
C,
250mLP+ZnAc+NaOH
>9
Y J N I NA
Y 1 I NA
Page 145 of 146
ClelmntlPrintlwko_PreservationCheck. rpt

Sample Preservation Verification I■II _ _
ENCO Cary
Work Order: CF10299 Project: Pitt County Landfill
Client: Groundwater Management Associates, Inc (GR022, Project #: [none]
Logged In 21-Jul-22 11.26 1Logged By: Rachel Ann oni h
Preservation Check Performed By. Ob Date/Time:
CF10299-20
font
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted Date(T'ime
Adjusted
Reagent Used/Comments
Cr
250mLA (PEST)
Pest pH 5 9
Y N I NA
NA
4YN
E
250mLP+HNO3
<2
Y N I NA
NA
F
250mLP+NaOH
> 12
Y I N I NA
Y N I NA
G
250mLP+ZnAc+Na0H
>9
Y N I NA
Y I N NA
CF10299-21
Cont
Type
Pres (pt-I)
Requirement
pH Checked 1
In Control
pH Adjusted Date/Time
Adjusted
Reagent iisedlComrt�ents
D
250mLA (PEST)
Pest pH 5-9
Y N I NA
Y N NA
E
25pmLP+HNO3
<2
Y N/ NA
Y N/ NA
F
250rnLP+Na0H
>12
Y ! N / NA
Y 1 / NA
G
250mLP+ZnAc+NaOH
>9
Y/ N/ NA
Y
N NA
CF10299-23
Cant
Type
Pres (pH}
Requirement
pH Checked Y
In Control
pH Adjusted DatelTlrne
Adjusted
Reagent Used/Comments
A
250mLP+1­11\103
/ N NA
Rea ent Name ID
.1 C�C12�
Reacient Name ID
3
4
Reagent Name ID
5 1
6
pH Strip ID
PH Strips C2A0640
C:IelmntlPri- ,, %vv ru_r-r eservationC heck. rpt
Page 146 of 146