0403_AnsonLF_Monitoring_April2022_FID1741290_20220718

DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Jett Environmental Consulting, PLLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Steve Jett
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Chambers Development of North 375 Dozer Drive April 11,12,14,15 and 19,
Carolina, Inc. - Anson Waste Polkton, NC 28135 04-03 .1600 2022
Management Facility
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Steve Jett Owner [phone]
Facility Representative Name (Print) /jd /, Title (Area Code) Telephone Number
Signature
07/18/2022 Affix NC Licensed/ Professional Geologist Seal
Date
Jett Environmental Consulting, PLLC, 18 Lexington Oaks Court, Foristell, MO 63348
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

Groundwater
Statistical Analysis Report
First Semi -Annual 2022
Sampling Event
Anson Waste Management Facility
Chambers Development of NC, Inc.
Polkton, North Carolina
July 2022
Prepared by:
\*0JETT
ENVIRONMENTAL
C D N S U L T! N G
18 Lexington Oaks Court 314-496-4654
Foristel% MO 63348 www.jettenviro.com

TABLE OF CONTENTS
1.0 INTRODUCTION.............................................................................1
2.0 SITE BACKGROUND AND MONITORING NETWORK................1
3.0 SITE HYDROGEOLOGY................................................................2
4.0 DATA EVALUATION......................................................................3
5.0 STATISTICAL PROCEDURES.......................................................4
5.1 Outlier Analysis...........................................................................4
5.2 Intra-Well Prediction Intervals....................................................5
5.3 Statistical Results Summary.......................................................5
6.0 CONCLUSIONS............................................................................5
TABLES
Table 1
Groundwater Monitoring Program
Table 2
Groundwater Analytical Data
Table 3
Surface Water Analytical Data
Table 4
Underdrain Analytical Data
Table 5
Enhanced Liner System (ELS) Analytical Data
Table 6
Leachate Analytical Data
APPENDICES
Appendix A Potentiometric Surface Maps &
Surface Water Sampling Location Map
Appendix B Statistical Evaluations
Appendix C Laboratory Analytical Reports & Field Sampling Forms

Groundwater Statistical Analysis Report
Anson Waste Management Facility, North Carolina 1
1.0 INTRODUCTION
On behalf of Chambers Development of North Carolina, Inc. - Anson Waste Management Facility, Jett
Environmental Consulting statistically evaluated the First Semi -Annual 2022 groundwater data. Sampling
was performed by S&ME and analytical testing was performed by Environmental Conservation
Laboratories, Inc. and Eurofins. The statistical analysis software package utilized, Sanitasll' follows a
documented decision logic that incorporates the following applicable document: USEPA "Statistical
Analysis of Groundwater Monitoring Data at RCRA Facilities, Unified Guidance" (March 2009).
2.0 SITE BACKGROUND AND MONITORING NETWORK
Per the site's Statistical Analysis Plan dated July 2001 by Herst & Associates, Inc. and in compliance with
North Carolina Department of Environmental Quality (NCDEQ) Solid Waste Management Regulations,
Section .1600 "Requirements for Municipal Solid Waste Landfill Facilities," Jett Environmental Consulting
statistically evaluated parameters from the First Semi -Annual 2022 event using intra-well prediction interval
analysis. Prediction intervals are considered a powerful tool for groundwater statistical analysis, when
feasible, due to their inherent low false negative and false positive rates utilizing confirmatory resampling,
if necessary.
As part of the Phase 3 construction, Civil & Environmental Consultants, Inc. (CEC) oversaw the installation
of three additional wells (MW-10S, MW-11S, and MW-12S) in September 2018. CEC submitted an
Updated Water Quality Monitoring Plan (WQMP) on December 17, 2018. The Updated WQMP outlined
sampling of the three new wells in addition to three existing wells that were not part of the formal
groundwater program (MW-13S, MW-14D, and MW-15D). Wells MW-13S, MW-14D, and MW-15D were
previously installed during the Phase 5 Preliminary Design Hydrogeologic Investigation in May 2017. In an
April 9, 2019 Phase 3 Baseline Groundwater Monitoring Report by CEC, data from four initial baseline
sampling events (October 2018, November 2018, December 2018, and January 2019) was submitted to
NCDEQ.
Phase 3 wells MW-12S, MW-13S, and MW-14D were replaced by wells MW-12R, MW-13R, and MW-14R
in September 2020 to account for the location of Phases 4/5. Wells MW-12R, MW-13R, and MW-14R were
sampled for the first time in October 2020. Wells MW-12R, MW-13R and MW-14R completed the four initial
baseline sampling events during the First Semi -Annual 2022 event. Therefore, statistical evaluation at MW-
12R, MW-13R, and MW-14R can be initiated during the Second Semi -Annual 2022 event.
Background is defined as samples collected from each well from October 2000 through the January 2019
event. Background will generally be reviewed every two to three years to determine if more recent data
can be added to the background pool of data. For the newer wells, background consists of the first four
sampling events. The parameters subject to statistical evaluation during detection monitoring are noted in
NCDEQ Section .1633 as constituents listed in Appendix I of 40 CFR Part 258 "Appendix I Constituents for
Detection Monitoring". Table 1 lists the site's groundwater monitoring wells, their representative hydraulic
position, and zone monitored. Each well was sampled during the First Semi -Annual 2022 event.
Per September 28, 2012 NCDEQ correspondence, approval was granted to sample the Shallow zone wells
on a semi-annual basis, with the groundwater elevations monitored in Deep zone wells (MW-3D, MW-4D,
MW-5D, and MW-8D) on a semi-annual basis. The approval was under the condition that a groundwater
sample be collected from a Deep zone well if its accompanying Shallow zone well did not contain enough
water to yield a sample. Each of the Shallow zone wells (MW-3S, MW-4S, MW-5S, and MW-8S) was able
to be sampled during the First Semi -Annual 2022 event.
In a May 29, 2018 memorandum, NCDEQ requested groundwater and surface water samples be analyzed
for 1,4-dioxane. In correspondence dated January 2, 2020, NCDEQ provided the following revisions to the
site's 1,4-dioxane monitoring requirements:

Groundwater Statistical Analysis Report
Anson Waste Management Facility, North Carolina 2
(1) analyze for 1,4-dioxane in groundwater samples from the downgradient compliance monitoring
wells and in all underdrain samples (UD-1, UD-2, & UD-3) semi-annually every other year starting
with the 1st semi-annual monitoring event in 2020 (i.e., April/October 2020, April/October 2022,
April/October 2024, etc.). The facility can optionally include the background well MW-2S, but this
is not required by the Section;
(2) discontinue monitoring for 1,4-dioxane in stream surface water samples (BG-1, BG-2, SG-3, and
SG-4); and
(3) continue to collect and analyze leachate and Enhanced Liner System (ELS) sump samples for 1,4-
dioxane during semi-annual sample events.
In addition to groundwater monitoring, the site has a surface water monitoring network consisting of the
following points:
Upstream Downstream
Pinch Gut Creek Upstream (BG-1) Brown Creek Downstream (SG-3)
Brown Creek Upstream (BG-2) Pinch Gut Creek Downstream (SG-4)
The four surface water sampling points are sampled semi-annually for the 40 CFR Part 258 Appendix I list
in conjunction with the groundwater monitoring wells. Each of the surface water points was able to be
sampled during the First Semi -Annual 2022 event. Appendix A provides a map of the surface water
sampling point locations.
During permitting of Phase 2, a sampling station (SG-5) was added at the outlet of an underdrain built below
Phase 2B (this point was renamed UD-1 as part of the latest Water Quality Monitoring Plan). Two additional
underdrain sampling stations were added during Summer 2016: Underdrain Combo 1 E/2A (this point was
renamed UD-2 as part of the latest Water Quality Monitoring Plan) and Underdrain 2C-North (this point was
renamed UD-3 as part of the latest Water Quality Monitoring Plan). UD-1, UD-2, and UD-3 are to be
sampled semi-annually (contingent on flow availability) for the 40 CFR Part 258 Appendix I list. Each of
the underdrain points was able to be sampled during the First Semi -Annual 2022 event, except UD-3 which
was dry. The potentiometric surface maps in Appendix A display the locations of the underdrain sampling
locations.
A leachate sample is also collected semi-annually for analysis in accordance with the facility's permit. The
leachate sample is analyzed for the 40 CFR Part 258 Appendix I list, biochemical oxygen demand, chemical
oxygen demand, nitrate as N, pH, phosphorous, specific conductance, and sulfate. A leachate sample was
able to be collected during the First Semi -Annual 2022 event.
According to the latest Water Quality Monitoring Plan, two ELS sumps (#5 and #7) are to be sampled if
liquids are present. The ELS sumps are sampled semi-annually for the 40 CFR Part 258 Appendix I list.
ELS sumps #5 and #7 were able to be sampled during the First Semi -Annual 2022 event.
3.0 SITE HYDROGEOLOGY
The following site hydrogeology summary was taken from a document titled Baseline Sampling Report,
Anson Waste Management Facility, dated June 2001 by Almes & Associates, Inc.
The site is located in the Piedmont Physiographic province within the Triassic -age Wadesboro basin. In
general, the lithology of the site is composed of saprolitic soils and partially weathered rocks grouped
together as "overburden" and competent bedrock. Three rock types comprise the bedrock at the site;
Triassic sediments of the Wadesboro basin (Chatham Group), bedded argillites of the Carolina Slate belt
(Floyd Church Formation), and diabase units in two north-west trending features (dikes). The three bedrock
types and overburden appear to have similar hydraulic characteristics and behave as equivalent to a single
porous granular media. As a result, the direction of groundwater flow should be largely controlled by site
topography.

Groundwater Statistical Analysis Report
Anson Waste Management Facility, North Carolina 3
The groundwater monitoring system at the site has been designed to monitor groundwater within both the
overburden and the bedrock. Those monitoring wells designated with an "S"-suffix are screened within the
overburden to monitor the shallow groundwater and those wells designated with a "D"-suffix are deeper
wells screened within the bedrock. Based on data obtained during previous hydrogeologic investigations
at that site, it was determined that the geologic units were in communication, the groundwater flow pattern
appears to be controlled by topography, and the subsurface may be represented as a porous granular
media. The location and completed intervals for monitoring wells MW-1 D and MW-6D were selected
specifically to collect background and downgradient water quality data, respectively, from the diabase dikes
at the site.
Well clusters at the site are located based on former drainage features, and monitor the upper saprolite
aquifer and the upper bedrock aquifer: MW-2S, MW-3S, MW-3D, MW-4S, MW-4D, MW-5S, MW-5D, MW-
8S, and MW-8D. The following wells are also located to focus on drainage features that align with the
regional joint pattern visible in the topography: MW-9, MW-10S, MW-11 S, MW-16S, MW-17S, MW-18S,
MW-19S and MW-20S. These wells do not exceed "auger refusal" depth, therefore they remain in the
shallow saprolite aquifer. Wells MW-1 D, MW-2D, MW-12R, MW-13R, MW-14R, and MW-15D are installed
in the upper bedrock aquifer due to a shallow top -of -bedrock depth and not encountering groundwater
within the upper saprolite region, necessitating installing within the deeper upper bedrock aquifer.
Appendix A provides potentiometric surface maps and groundwater flow calculations for the Shallow zone
and Deep zone utilizing groundwater level data from the First Semi -Annual 2022 event. Groundwater flow
direction for the First Semi -Annual 2022 event was to the north in the Shallow zone and to the north /
northeast in the Deep zone. Groundwater flow rate for the First Semi -Annual 2022 event was estimated to
range from 73 feet/year in the Shallow zone to 109.5 feet/year in the Deep zone.
4.0 DATA EVALUATION
Appendix C contains a copy of the laboratory analytical reports and field log sheets for the First Semi -
Annual 2022 event for the groundwater, surface water, underdrain, leachate, and ELS sump samples.
Groundwater
The analytical results for the First Semi -Annual 2022 event for the groundwater samples are summarized
on Table 2. No volatile organic compounds (VOCs) were detected at or above the laboratory method
reporting limits (MRLs) in the groundwater samples. As shown on Table 2, a few NC Appendix I inorganic
constituents were detected in samples from one or more wells at concentrations above their respective
MRLs, consistent with past events. Of the detections, only the following Appendix I constituents were
detected above an MRL and NC 2L standard in the groundwater monitoring wells during the First Semi -
Annual 2022 sampling event: total arsenic at MW-12R; total barium at MW-8S and MW-9; total beryllium at
MW-2D; and total cobalt at MW-2D and MW-15D. Therefore, total barium at MW-8S and MW-9; total
beryllium at MW-2D; and total cobalt at MW-21D and MW-15D were statistically evaluated to determine if
concentrations statistically exceed background (see Section 5.2). Well MW-12R is in the process of
collecting background data and will not have sufficient number of data points for statistical analysis until the
Second Semi -Annual 2022 event.
Surface Water
The analytical results for the First Semi -Annual 2022 event for the surface water samples are summarized
on Table 3. Each of the surface water points was able to be sampled during the First Semi -Annual 2022
event. During the First Semi -Annual 2022 event no Appendix I inorganic constituents or VOCs were
reported at quantified levels above an NC 2B Surface Water Standard.

Groundwater Statistical Analysis Report
Anson Waste Manaaement Facilitv. North Carolina 4
Underdrain
The analytical results for the First Semi -Annual 2022 event for the underdrain samples are summarized on
Table 4. Each of the underdrain points was able to be sampled during the First Semi -Annual 2022 event,
except LID-3 which was dry. During the First Semi -Annual 2022 event, no Appendix I VOCs were detected
in underdrain samples at quantified concentrations above their respective MRLs.
Enhanced Liner Svstem
According to the latest Water Quality Monitoring Plan (WQMP), an evaluation is to be made semi-annually
of the volume of free liquid removed from the ELS sumps. The results of the evaluation and the VOC
analysis of the ELS sump liquids are to be included in the semi-annual groundwater report. The analytical
results for the First Semi -Annual 2022 event for the ELS sump samples are summarized on Table 5.
According to site personnel, liquids were present at ELS sump #5 and #7 during the last six-month
monitoring period. Samples were collected from ELS sumps #5 and #7 during the First Semi -Annual 2022
event for the required VOCs. Liquids that are present in ELS sumps #5 and #7 are pumped to the leachate
collection/disposal system and managed as leachate. According to the field forms, ELS Sump #5 is labeled
as "Sump 313" and ELS Sump #7 is labeled as "Sump 4B."
As shown on Table 5, VOCs were detected in the ELS sump sample, consistent with previous events.
Total metals are also sampled at the ELS sump to supplement the VOC analyses (see Table 5). According
to the site, from November 2021 through April 2022, the total volume of liquids measured in ELS sumps #5
and #7 was 2,330 gallons and 3,465 gallons, respectively.
Leachate
During the First Semi -Annual 2022 event, a sample was collected from the leachate collection system. The
leachate sample results are summarized on Table 6.
5.0 STATISTICAL PROCEDURES
The following Appendix I constituents were confirmed detected above the MRL and an NC 2L Standard
during the First Semi -Annual 2022 sampling event: total arsenic at MW-12R; total barium at MW-8S and
MW-9; total beryllium at MW-2D; and total cobalt at MW-2D and MW-15D. With the exception of MW-12R
(see Section 4.0), statistical analyses (i.e., intra-well prediction limits) were performed to establish
background concentrations and determine if the NC 2L value -to -value exceedance exhibited a statistically
significant increase.
Per 15A NCAC 02L .0202(b)(1), for the NC 2L Standards, only detections of a substance at or above the
laboratory practical quantitation limit (PQL) can constitute a violation of the standard. Therefore, estimated
values below the PQL are not considered a violation of a NC 2L Rule standard. Hence, statistical
evaluations were not performed for estimated values for this Report.
5.1 Outlier Analysis
The background data were evaluated for the presence of statistical outliers. Methodologies for determining
a statistical outlier are defined in the USEPA Unified Guidance. Any statistical outliers that were determined
were removed from the background data set prior to performing prediction interval statistical analysis.
According to the Unified Guidance, data that are not normally or log -normally distributed are not
recommended for evaluation of outliers. In cases where the data were not normally or log -normally
distributed, outliers were not removed from the data set. Background outliers flagged for removal are
identified on the statistical plots provided in Appendix B.

Groundwater Statistical Analysis Report
Anson Waste Manaaement Facilitv. North Carolina 5
5.2 Intra-Well Prediction Intervals
The prediction interval is a statistical method used to compare a single observation to a group of
observations. The prediction interval is calculated to include observations from the same population with a
specified confidence. In groundwater monitoring, a prediction interval approach may be used to make
comparisons between background and compliance data. The interval is developed to contain all future
observations, within a certain probability. For the Anson Waste Management site, intra-well prediction
intervals have been developed based on a 99% confidence that future observations will fall within the range.
If any future observation exceeds the prediction interval, this is considered statistically significant evidence
that the observation is not representative of the background group.
During parametric prediction interval analysis, the mean and the standard deviation are calculated for the
raw or transformed background data. The number of comparison observations, K, is defined to be included
in the interval. If less than 15% of the background observations are nondetects, the nondetects are replaced
with one half of the reporting limit prior to performing the analysis. If more than 15% but less than 50% of
the background data are below the reporting limit, the data's sample mean and standard deviation are
adjusted according to the Kaplan -Meier method. However, when the background data are not transformed -
normal or contain greater than 50% observations below the reporting limit, SanitasT' automatically
constructs a non -parametric prediction interval. During non -parametric analysis, the highest value from the
background data is used to set the upper limit of the prediction interval.
Prediction interval summary tables are presented in Appendix B. Included in Appendix B are time series
plots for each of the inorganic parameters reported for groundwater this event.
5.3 Statistical Results Summary
For the First Semi -Annual 2022 event, total barium at MW-9 and total cobalt at MW-2D and MW-15D
exhibited statistical exceedances. Review of the field sampling forms indicates that MW-9 was sampled
with a bailer due to sediment buildup resulting in an inoperable bladder pump. Field turbidity measurements
ranged from 38.17 to 188 NTU during purging and the sample was collected with a field turbidity of 188
NTU.
Dissolved metals samples were also collected at well MW-2D, MW-8S, MW-9, MW-12R, and MW-15D,
during the First Semi -Annual 2022 event. The dissolved barium result at MW-9 (551 ug/L) was below the
NC 2L Standard. The dissolved cobalt result at MW-21D (<10.0 ug/L) and MW-15D (7.16 J ug/L) did not
exhibit quantified detections above the NC 2L Standard. The lower dissolved barium/cobalt concentrations
confirmed that suspended solids had an influence on total (unfiltered) concentrations, causing artificially
higher results that were not representative of the water quality.
6.0 CONCLUSIONS
The following Appendix I constituents were confirmed detected above the laboratory MRL and NC 2L
Standards during the First Semi -Annual 2022 sampling event: total arsenic at MW-12R; total barium at
MW-8S and MW-9; total beryllium at MW-2D; and total cobalt at MW-2D and MW-15D.
For the First Semi -Annual 2022 event, total barium at MW-9 and total cobalt at MW-2D and MW-15D
exhibited statistical exceedances. Review of the field sampling forms indicates that MW-9 was sampled
with a bailer due to sediment buildup resulting in an inoperable bladder pump. Field turbidity measurements
ranged from 38.17 to 188 NTU during purging and the sample was collected with a field turbidity of 188
NTU.
Dissolved metals samples were also collected at well MW-2D, MW-8S, MW-9, MW-12R, and MW-15D,
during the First Semi -Annual 2022 event. The dissolved barium result at MW-9 (551 ug/L) was below the
NC 2L Standard. The dissolved cobalt result at MW-21D (<10.0 ug/L) and MW-15D (7.16 J ug/L) did not
exhibit quantified detections above the NC 2L Standard. The lower dissolved barium/cobalt concentrations

Groundwater Statistical Analysis Report
Anson Waste Management Facility, North Carolina 6
confirmed that suspended solids had an influence on total (unfiltered) concentrations, causing artificially
higher results that were not representative of the water quality.
No VOCs were detected at or above the laboratory MRLs in the groundwater or underdrain samples at
quantified concentrations above their respective MRLs.
During the First Semi -Annual 2022 event, no Appendix I inorganic constituents or VOCs were reported at
quantified levels above an NC 2B Surface Water Standard.
The site will continue monitoring in accordance with the requirements for Detection Monitoring as outlined
in Title 15A NCAC 13B .1633. The next semi-annual event is tentatively scheduled for October 2022.

TABLES

TABLE 1
GROUNDWATER MONITORING PROGRAM
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
ZONE
UPGRADIENT WELLS
DOWNGRADIENT WELLS
Shallow
MW-2S
MW-3S, MW-4S, MW-5S, MW-8S,
MW-9, MW-10S, MW-11 S
MW-3D, MW-4D, MW-5D, MW-8D, MW-12R,
Deep
MW-1 D, MW-2D
MW-13R, MW-14R, MW-15D
Note. Deep Zone wells MW-3D, MW-4D, MW-5D, and MW-8D are only required to be sampled if the adjacent
Shallow Zone well (i.e. MW-3S, MW-4S, MW-5S, or MW-8S) is dry during a respective event.

TABLE 2
GROUNDWATER ANALYTICAL DATA
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
Constituent
Units
MDL
MRL
NC 2L Std
SHALLOW ZONE
MW-2S MW-3S MW-4S MW-5S MW-8S MW-9 MW-10S MW-11S
DEEP ZONE
MW-1D MW-2D MW-12R MW-13R MW-14R MW-15D
Antimony Total
u /L
0.740
2.00
1
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
Arsenic Total
u /L
7.60
10.0
10
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
11.3 <10.0
<10.0
<10.0
<10.0
Barium Total
u /L
1.10
10.0
700
120
37.8
176
79.8
2220 1920
739 551
581
693
125
239
189
230
8.89 J
17.1
Beryllium Total
u /L
0.160
1.00
4
2.04
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
4.98 0.583 J
<1.00
<1.00
<1.00
<1.00
Cadmium Total
u /L
1 0.360
1 1.00
2
1 <1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
<1.00
Chromium Total
u /L
1.40
10.0
10
1.76 J
<10.0
1 5.97 J
<10.0
1 3.38 J
2.05 J
<10.0
<10.0
<10.0
1 1.68 J
<10.0
I <10.0
2.78 J
1.94 J
Cobalt Total
u /L
1.40
10.0
1
5.61 J
3.18 J
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
16.0 <10.0
<10.0
<10.0
1.67 J
12.5 7.16 J
Copper Total
u /L
1.60
10.0
1,000
5.36 J
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
7.24 J
4.37 J
<10.0
<10.0
8.35 J
Lead Total
u /L
3.10
10.0
15
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
4.13 J
<10.0
<10.0
3.46 J
Nickel Total
u /L
2.20
10.0
100
8.79 J
2.77 J
5.60 J
3.21
4.04 J
<10.0
<10.0
<10.0
7.26 J
11.5
<10.0
<10.0
4.10 J
22.8
Selenium Total
u /L
1.82
2.00
20
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
Silver Total
u /L
1.90
10.0
20
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
Thallium Total
u /L
0.220
2.00
2
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
<2.00
Vanadium Total
u /L
1.40
10.0
7
<10.0
<10.0
<10.0
<10.0
<10.0
2.59 J
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
Zinc Total
ug/L
4.40
10.0
1000
8.91 J
<10.0
12.2
<10.0
7.87 J
<10.0
<10.0
<10.0
<10.0
11.1
5.8 J
<10.0
<10.0
29.0
Field Dissolved Oxygen
m /L
NA
NA
NE
5.32
1.64
1.74
2.11
3.83
6.34
2.14
0.89
2.24
2.05
2.1
0.25
7.07
3.13
Field pH
SU
NA
NA
NE
4.79
5.72
5.91
5.98
6.22
7.31
7.03
7.03
6.71
6.15
6.4
6.93
6.33
5.85
Field Specific Conductance
uS/cm
NA
NA
NE
256.9
368.2
169.4
249.9
601
964.0
1740
674.0
329.9
316.9
114.3
232.8
137.8
107.2
Field Temperature
°C
NA
NA
NE
17.1
19.9
17.6
19.9
17.4
18.2
18.0
19.9
16.7
17.6
18.9
17.7
16.2
21.6
Field Turbidity
NTU
NA
NA
NE
4.91
8.52
27.18
6.95
17.40
188
4.06
9.78
5.2
20.78
13.71
9.49
372
38.45
NE: Denotes a NC 2L Standard is not established.
J: Denotes Sample result above the MDL but below the MRL; estimated value; value may not be accurate.
MDL: Denotes Laboratory Method Detection Limit.
MRL: Denotes Laboratory Method Reporting Limit.
Denotes a concentration at or above an MRL is also above the 2L Standard:
Denotes a concentration is above a 2L Standard, but below the MRL:
Field data are last recorded measurement during purging.
Samplers inadvertently labeled MW-9 as MW-9S, MW-12R as MW-12S, MW-13R as GMW-13, and MW-14R as GMW-14. Identification above has been adjusted accordingly.
MW-15D was also analyzed for dissolved cobalt, with dissolved metal results listed to the right of the total metal results.
MW-12R was also analyzed for dissolved arsenic, with dissolved metal results listed to the right of the total metal results.
MW-9 was also analyzed for dissolved barium, with dissolved metal results listed to the right of the total metal results.
MW-2D was also analyzed for dissolved beryllium, with dissolved metal results listed to the right of the total metal results.
MW-8S was also analyzed for dissolved barium, with dissolved metal results listed to the right of the total metal results.

TABLE 3
SURFACE WATER ANALYTICAL DATA
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
Constituent
Units
NC 2B
Standard
MDL
MRL
BG-1
BG-2
SG-3
SG-4
Antimony Total
ug/L
640
0.74
2
<2.00
<2.00
<2.00
<2.00
Arsenic Total
ug/L
10
7.6
10
<10.0
<10.0
<10.0
<10.0
Barium Total
ug/L
21,000
1.1
10
44.7
28.6
32.2
45.3
Beryllium Total
ug/L
6.5
0.16
1
<1.00
<1.00
<1.00
<1.00
Cadmium Total
ug/L
NE
0.36
1
<1.00
<1.00
<1.00
<1.00
Chromium Total
ug/L
NE
1.4
10
1.46 J
2.27 J
<10.0
1.63 J
Cobalt Total
ug/L
4
1.4
10
1.52 J
4.06 J
2.32 J
2.12 J
Copper Total
ug/L
NE
1.6
10
1.78 J
2.35 J
3.43 J
2.13 J
Lead Total
ug/L
NE
3.1
10
<10.0
4.47 J
<10.0
<10.0
Nickel Total
ug/L
NE
2.2
10
<10.0
2.31 J
<10.0
<10.0
Selenium Total
ug/L
5
1.82
2
<2.00
<2.00
<2.00
<2.00
Silver Total
ug/L
0.06
1.9
10
<10.0
<10.0
<10.0
<10.0
Thallium Total
ug/L
0.47
0.22
2
<2.00
<2.00
<2.00
<2.00
Vanadium Total
ug/L
NE
1.4
10
1.86 J
2.59 J
2.38 J
2.62 J
Zinc Total
ug/L
NE
4.4
10
<10.0
<10.0
4.40 J
<10.0
Field Dissolved Oxygen
mg/L
NE
NA
NA
4.49
4.40
5.28
4.44
Field pH
SU
NE
NA
NA
7.22
7.59
8.64
7.66
Field Specific Conductance
us/cm
NE
NA
NA
74.4
63.7
109.7
90.0
Field Temperature
°C
NE
NA
NA
17.4
18.8
17.2
17.9
Field Turbidity
NTU
NE
NA
NA
26.76
1 21.59
1 21.50
23.71
No VOCs were detected above an MRL during this event.
NE: Denotes a NC 2B Standard is not established.
J: Denotes Sample result above the MDL but below the MRL; estimated value; value may not be accurate.
MDL: Denotes Laboratory Method Detection Limit.
MRL: Denotes Laboratory Method Reporting Limit.
NA: Denotes Not Applicable.
Denotes a concentration at or above an MRL is also above the 2B Standard:
Denotes a concentration is above a 2B Standard, but below the MRL:

TABLE 4
UNDERDRAIN ANALYTICAL DATA
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
Constituent
Units
MDL
MRL
UD-1
UD-2
UD-3
Antimony Total
ug/L
0.740
2.00
<2.00
<2.00
NS
Arsenic Total
ug/L
7.60
10.0
<10.0
<10.0
NS
Barium Total
ug/L
1.10
10.0
27.9
64.1
NS
Beryllium Total
ug/L
0.160
1.00
<1.00
<1.00
NS
Cadmium Total
ug/L
0.360
1.00
<1.00
<1.00
NS
Chromium Total
ug/L
1.40
10.0
2.02 J
<10.0
NS
Cobalt Total
ug/L
1.40
10.0
94.1
5.53 J
NS
Copper Total
ug/L
1.60
10.0
<10.0
<10.0
NS
Lead Total
ug/L
3.10
10.0
<10.0
<10.0
NS
Nickel Total
ug/L
2.20
10.0
4.40 J
4.33 J
NS
Selenium Total
ug/L
1.82
2.00
<2.00
<2.00
NS
Silver Total
ug/L
1.90
10.0
<10.0
<10.0
NS
Thallium Total
ug/L
0.220
2.00
<2.00
<2.00
NS
Vanadium Total
ug/L
1.40
10.0
<10.0
<10.0
NS
Zinc Total
ug/L
4.40
10.0
<10.0
<10.0
NS
Field Dissolved Oxygen
mg/L
NA
NA
2.92
4.46
NS
Field pH
SU
NA
NA
5.93
6.03
NS
Field Specific Conductance
us/cm
NA
NA
273.6
85.2
NS
Field Temperature
°C
NA
NA
25.3
23.9
NS
Field Turbidity
NTU
NA
NA
8.10
5.10
NS
No VOCs were detected above an MRL during this event.
J: Denotes Sample result above the MDL but below the MRL; estimated value; value may not be accurate.
MDL: Denotes Laboratory Method Detection Limit.
MRL: Denotes Laboratory Method Reporting Limit.
NS: Not Sampled, point dry this event.
NA: Denotes Not Applicable.

TABLE 5
ENHANCED LINER SYSTEM (ELS) ANALYTICAL DATA
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
Constituent
UNITS
MDL
MRL
ELS #5
ELS #7
Antimony
mg/L
0.00052
0.005
0.00141
0.00343
Arsenic
mg/L
0.00086
0.003
0.0192
0.0422
Barium
mg/L
0.00089
0.005
0.629
2.55
Beryllium
mg/L
0.0002
0.0005
0.00029
<0.000500
Cadmium
mg/L
0.000078
0.0005
<0.000500
0.00024
Chromium
m /L
0.00160
0.00500
0.00508 J
0.0428
Cobalt
mg/L
0.000120
0.000500
0.00998
0.039
Copper
m /L
0.00170
0.00500
0.032
0.218
Lead
m /L
0.000980
0.00250
0.00089
0.00712
Mercury
u /L
0.0800
0.200
<0.200
<0.200
Nickel
mg/L
0.0018
0.005
0.034
0.462
Selenium
mg/L
0.0012
0.0025
0.00124
0.00305
Silver
mg/L
0.00039
0.001
<0.00100
<0.00100
Thallium
mg/L
0.00026
0.001
<0.00100
<0.00100
Vanadium
mg/L
0.0018
0.01
0.00579
0.0219
Zinc
mg/L
0.01
0.02
0.16
0.0916
pH field
SU
NA
NA
6.72
6.35
Specific Conductance field
US/cm
NA
NA
3999+
3999+
1,2-Dichloroethane
u /L
0.25
1.00
<1.00
0.682 J
1,2-Dichloropropane
u /L
0.22
1.00
0.324 J
<1.00
1,4-Dichlorobenzene
u /L
0.310
1.00
9.68
3.98
1,4-dioxane
u /L
3.00
10.0
249
791
Benzene
u /L
0.270
1.00
11.7
9.28
Chlorobenzene
u /L
0.150
1.00
<1.00
2.22
Eth (benzene
u /L
0.200
1.00
59.8
32.3
Methyl ethyl ketone
u /L
6.4
10.0
<10.0
66.7
Methyl isobut I ketone
u /L
2.70
10.0
<10.0
13.8
Styrene
u /L
0.270
1.00
0.909 J
<1.00
Toluene
u /L
0.250
1.00
23.6
2.57
Vinyl chloride
u /L
0.400
1.00
1.45
0.523 J
X lene total
u /L
0.230
1.00
93.2
15.7
Only the VOCs detected are included on this table.
J: Denotes Sample result above the MDL but below the MRL; estimated value.
MDL: Denotes Laboratory Method Detection Limit.
MRL: Denotes Laboratory Method Reporting Limit.
NA: Denotes Not Applicable.

TABLE 6
LEACHATE ANALYTICAL DATA
FIRST SEMI-ANNUAL 2022 EVENT
ANSON WASTE MANAGEMENT FACILITY
Constituent
UNITS
MDL
MRL
I Leachate
Ammonia
mg/L
0.500
1.25
370
Antimony, Total
mg/L
0.000500
0.00500
0.0466
Arsenic, Total
mg/L
0.00150
0.00300
0.249
Barium, Total
mg/L
0.000610
0.00500
1.59
Beryllium, Total
mg/L
0.000170
0.000500
0.000290 J
Biological Oxygen Demand
mg/L
0
2.00
708
Cadmium, Total
mg/L
0.000150
0.000500
0.000340 J
Chemical Oxygen Demand
mg/L
5.00
10.0
4180
Chromium, Total
m /L
0.00160
0.00500
0.512
Cobalt, Total
mg/L
0.000120
0.000500
0.0567
Copper, Total
m /L
0.00170
0.00500
0.0847
Cyanide
mg/L
0.00250
0.0100
0.0217
Kjeldahl Nitrogen as N
mg/L
1.00
2.00
884
Lead, Total
m /L
0.000980
0.00250
0.006600
Mercury, Total
m /L
0.0000800
0.000200
<0.000200
Nickel, Total
mg/L
0.00190
0.00500
0.447
Nitrate as N
m /L
0.0100
0.0500
0.188
Oil & Grease
mg/L
1.4
5.2
11.4
Phenolics, Total Recoverable
mg/L
0.0250
0.0500
2.09
Selenium, Total
mg/L
0.00100
0.00250
0.006
Silver, Total
mg/L
0.000100
0.00100
<0.00100
Sulfate
mg/L
2.00
5.00
2840
Thallium, Total
m /L
0.000490
0.00100
<0.00100
Total Phosphorus
m /L
0.0410
0.100
8.71
Total Suspended Solids
m /L
0
50.0
69.0
Vanadium, Total
m /L
0.00530
0.0100
0.440
Zinc, Total
m /L
0.00960
0.0200
0.0911
1,4-dioxane
u /L
1.5
5
159
Methyl butyl ketone
u /L
3.2
10
4.48
Methyl isobutyl ketone
u /L
2.7
10
19.8
Acetone
u /L
37
100
2890
Eth (benzene
u /L
0.2
1
1.75
Methyl ethyl ketone
u /L
64
100
1940
1,4-Dichlorobenzene
u /L
0.31
1
0.481 J
Toluene
u /L
0.25
1
5.49
X lene total
u /L
0.23
1
4.69
pH field
SU
NA
NA
1.33
Specific Conductance field
US/cm
NA
NA
481
Only the VOCs detected are included on this table.
J: Denotes Sample result above the MDL but below the MRL; estimated value.
H: Sample was prepped or analyzed beyond specified holding time.
MDL: Denotes Laboratory Method Detection Limit.
MRL: Denotes Laboratory Method Reporting Limit.
NA: Denotes Not Applicable.

APPENDICES
APPENDIX A
POTENTIOMETRIC SURFACE MAPS
SURFACE WATER SAMPLING LOCATION MAP

00,
00,
0MW-11S I
250.32
[ j ...
MW-10S
' I � 250.55
MW-16S \ a e I
NM^"" �o `
PROPERTY
/ o BOUNDARY �-
MW-17S `
ONM LID-2 JD-3 I
MO-9
259.17 PINCH GUT
LID-1 CREEK
MENT
MW-18S B SIN NO.
oNM
OMW-19S
NM SEDIMENT
o I " BASIN NO. 1
O O 2B°
MW 205� ' e e
NM_
♦ ' o ` 100 200 300 600 `
♦ ` C� MScale in Feet `
W-SS
♦ 295.0o Mw_43 , Q Graphic Scale: finch = 300 feet `
288.51 ��VJJ
7 LEGEND
v� 9O MW-3S Groundwater Monitoring Well
' 289.78 Groundwater Elevation (fmsl)
a o ( —280— Potentiometric Surface
Contour (fmsl)
Mw � 0.011 Hydraulic Gradient &
MW-3s 9Groundwater Flow Direction
28
Mw-2s uD-z 0 Underdrain Sampling Location
305.30
` R Note2: Water levels collected by an April 11- 2022.
\ I NoteFebruary Date of Aerial Topography February 27, 2016, by Independent Mapping Consultants. Basemap derived from
SEDIMENT •° site layout and cell boundaries provided by ESP Associates, P.A. and Civil Design Solutions, Inc.
BASIN NO. 4 � ANC ARE
J ETT Shallow zone First Semi -Annual 2022
18 Lexington Oaks Court ,
Forist1 M0 -4654 Potentiometric Surface Map
ENVIRONMEN IAL www.j ttenv o4rom
C 0 N S u L T I N S Anson Waste Management Facility, Polkton, North Carolina

0245 30R '
' MW-14R
243.11
R 025152
\. 250 \
I
zso /
MW-15D
319.80 S
1 `. ,0
' 2eo 1
1� PROPERTY
BOUNDARY `
UD-2 JD-3
PINCH GUT
UD-1 CREEK
C,
B SIN N NO. A
a
0
o
SEDIMENT `
o C� - - 1 BASIN NO. 1
O G `
o °
MW 5D o
�276.00 0 0
o
o 100 200 300 600
t9550 ` Scale in Feet
Graphic Scale: 1 inch = 300 feet
LEGEND
. _ e MW-31D Groundwater Monitoring Well
0� 0 / f
MW-1D �—/ 288.63
zsosa• � Groundwater Elevation (fmsl)
a —280— Potentiometric Surface i
_ Contour (fmsl)
` ♦ moo MW-3D i = 0.014 Hydraulic Gradient &
288.63 Groundwater Flow Direction
sssD UD-2 • Underdrain Sampling Location
♦ ♦ Skiot No Water levels collected by 5&ME on April 11-1%2022.
\2\ fl Note2: Date of Aerial Topography February 27, 2016, by Independent Mapping Consultants. Basemap derived from
SEDIMENT site layout and cell boundaries provided by ESP Associates, P.A. and Civil Design Solutions, Inc.
L ARE
J ETT Dee zone First Semi -Annual 2022
18 Lexington Oaks Court p ,
Foris 314-40-4654 Potentiometric Surface Map
314-496-4654
C OYN S U L T I N G www.jettenviro.com Anson Waste Management Facility, Polkton, North Carolina

m
A
r . 1SG-3 °sY
1 �\ A
BG-2
I GUT
EAR
\ \ � �p � / •• NORTH
MINNGIRATI£ IN, \
\ BINDING
0 250 500 1000 2000
\ N " Scale in Feet
Graphic Scale: 1 inch = 1000 feet
TEMPDRIRY / \ \ lA4M %UMMT
991MENT tRAPS
LEGEND
\ � erimiin
BG-1 Surface Water Monitoring Point
�SE�OIMENT MAP BG-1 IN el: Date of Aerial Topography February 27, 2016, by Independent Mapping Consultants. Basemap derived from site
layout and cell boundaries provided by ESP Associates, P.A. and Civil Design Solutions, Inc.
JETT
ENVIRONMEN IAL
C 0 N S U L T I N G
18 Lexington Oaks Court Surface Water Sampling Location Map
Foristell, MO 63348
314Anson Waste Management Facility, Polkton, North Carolina
www.jettenviro.com nvlro.

Groundwater Elevation Summary Table
Anson Waste Management Facility
Well
Top of PVC Casing
Elevation (fmsl)'
Depth to Water
(ft)2
Groundwater
fmsl
Elevation ( )
Shallow Wells
MW-2S
318.00
12.70
305.30
MW-3S
295.87
6.09
289.78
MW-4S
294.29
5.78
288.51
MW-5S
282.15
6.01
276.14
MW-8S
311.85
16.85
295.00
MW-9
274.58
15.41
259.17
MW-10S
264.76
14.21
250.55
MW-11 S
258.68
8.36
250.32
MW-16S
279.12
NM
NM
MW-17S
278.92
NM
NM
MW-18S
277.20
NM
NM
MW-19S
294.68
NM
NM
MW-20S
286.00
NM
NM
Deep Wells
MW-1 D
309.69
19.15
290.54
MW-2D
317.74
15.75
301.99
MW-3D
295.60
6.97
288.63
MW-4D
294.16
9.14
285.02
MW-5D
281.94
5.94
276.00
MW-8D
311.61
16.11
295.50
MW-12R
261.06
9.54
251.52
MW-13R
278.01
32.71
245.30
MW-14R
282.12
39.01
243.11
MW-15D
332.90
13.10
319.80
Note 1: Wells MW-1 through MW-9 Top of PVC Casing Elevations from Table 1 of
the Baseline Sampling Report dated June 2001 by Almes & Associates, Inc.,
with the exception of MW-9, which was provided by Lawrence Associates in email
correspondence dated December 22, 2011. Wells MW-10S through MW-15D
Top of PVC Casing Elevations from Table 1 of the Phase 3 Baseline Groundwater
Monitoring Report dated April 9, 2019 by Civil & Environmental Consultants, Inc. (CEC).
Wells MW-16S through MW-20S Top of PVC Casing Elevations from Table 1 of
the Design Hydrogeological Investigation Report for the Phase 5 Expansion Area
dated March 13, 2018 by CEC. Wells MW-12R, MW-13R, and MW-14R Top of PVC
Casing Elevations provided by Lawrence Associates in email correspondence dated
October 8, 2020.
Note 2: Depth to water measurements collected by S&ME on April 11-19, 2022.
Note 3: According to S&ME, wells MW-16S, MW-17S, MW-18S, MW-19S, and MW-20S were
inaccessible and not measured.

Groundwater Flow Velocity Calculations
Anson Waste Management Facility
First Semi -Annual 2022 Event
Shallow Zone Velocity
V = [(k)(i)]/(n)
V = [(4.8x10-4 cm/sec)(0.016 ft/ft]/O.11
V = 7.Ox10-1 cm/sec
V = 0.20 ft/day
V = 73 ft/yr
Deep Zone Velocity
V = [(k)(i)]/(n)
V = [(5.2x10-4 cm/sec)(0.037 ft/ft]/O.18
V = 1.07x10-4 cm/sec
V = 0.30 ft/day
V = 109.5 ft/yr
Hydraulic conductivity and effective porosity values from the following document: Design
Hydrogeologic Report, Phase 2 Expansion, Anson Waste Management Facility. Dated
February 2008 by ESP Associates, P.A. & David Garrett & Associates.
Conversion factor: ft/day = 2,835 x cm/sec.
Shallow Zone
Gradient (i) is from the average gradient at site using the potentiometric surface map from Point A to
Point B.
Gradient (i) = Change in Groundwater Elevation along Flow Path
is From Point A (300 contour) to Point B (260 contour) = 40 ft / 2529 ft = 0.016 ft/ft
Deep Zone
Gradient (i) is from the average gradient at site using the potentiometric surface map from Point A to
Point B.
Gradient (i) = Change in Groundwater Elevation along Flow Path
West -Northwest is From Point A (310 contour) to Point B (250 contour) = 60 ft / 1019 ft = 0.059 ft/ft
South -Northwest is From Point A (300 contour) to Point B (250 contour) = 50 ft / 3546 ft = 0.014 ft/ft
Average is (0.059 ft/ft + 0.014 ft/ft) / 2 = 0.037 ft/ft

APPENDIX B
STATISTICAL EVALUATIONS

Prediction Limit
Anson County LF
Client: Waste Connections
Data: AnsonCounty
Printed 6/15/2022, 11:13 AM
Constituent
Well
Uooer Lim. Lower Lim. Date Observ.
Sic.
Ba N
Ba Mean
Std. Day. %NDs ND Adi.
Transform Atha
Method
Barium Total (mg/L)
MW-8S
2.6 n/a
4/15/2022 2.22
No
40
n/a
n/a 0 n/a
n/a
04001159
NP Intra (normality) 1 of 2
Barium Total (mg/L)
MW-9
0.64 n/a
4/14/2022 0.739
Yes
17
-0.5938
0.08497 0 None
In(x)
0.00438
Param Intra 1 of 2
Beryllium Total (mg/L)
MW-2D
0.0055 n/a
4/15/2022 0.00498
No
27
n/a
n/a 29.63 n/a
n/a
0.002502
NP Intra (normality) 1 of 2
Cobalt Total (mg/L)
MW-2D
0.0084 n/a
4/15/2022 0.016
Yes
27
0.00004308000016M.22
Kaplan -Meier xA2
0.00438
Param Intra 1 of 2
Cobalt Total (mg/L)
MW-15D
0.0050 n/a
4/11/2022 0.0125
Yes
4
n/a
n/a 100 n/a
n/a
0.06138
NP Intra (NDs) 1 of 2

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Within Limit
3
2.4
J 1.8
0)
E
1.2
0 4-
11 /1 /00
Prediction Limit
Intrawell Non -parametric
2/15/05 6/1 /09 9/15/13 12/30/17 4/15/22
■ MW-8S background
♦ MW-8S compliance
Limit = 2.6
Non -parametric test used in lieu of parametric prediction limit because the Shapiro Wilk normality test showed the data
to be non -normal at the 0.01 alpha level. Limit is highest of 40 background values. Well -constituent pair annual alpha
= 0.002316. Individual comparison alpha = 0.001159 (1 of 2). Distribution was found to be non -normal after removal
of suspect values, so outliers could not be identified.
Constituent: Barium Total Analysis Run 6/15/2022 11:10 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Exceeds Limit
1.M
0.48
E
0.32
0.16
0 4-
7/19/11
Prediction Limit
Intrawell Parametric
9/10/13 11 /3/15 12/27/17 2/19/20 4/14/22
■ MW-9 background
♦ MW-9 compliance
Limit = 0.64
Background Data Summary (based on natural log transformation): Mean=-0.5938, Std. Dev.=0.08497, n=17.
Normality test: Shapiro Wilk @alpha = 0.05, calculated = 0.989, critical = 0.892. Kappa = 1.743 (c=3, w=4, 1 of 2,
event alpha = 0.05132). Report alpha = 0.00438. Dixon's outlier test was performed on the background data. One
background outlier was removed: 0.967 (10/20/2016).
Constituent: Barium Total Analysis Run 6/15/2022 11:10 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
Within Limit
0.006
0.0048
0.0036
0)
E
0.0024
0.0012
0
10/31 /00
Prediction Limit
Intrawell Non -parametric
2/14/05 5/31 /09 9/14/13 12/29/17 4/15/22
■ MW-21D background
♦ MW-21D compliance
Limit = 0.0055
Non -parametric test used in lieu of parametric prediction limit because the Shapiro Wilk normality test showed the data
to be non -normal at the 0.01 alpha level. Limit is highest of 27 background values. 29.63% NDs. Well -constituent
pair annual alpha = 0.004998. Individual comparison alpha = 0.002502 (1 of 2). Distribution was found to be non -
normal after removal of suspect values, so outliers could not be identified.
Constituent: Beryllium Total Analysis Run 6/15/2022 11:10 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
Exceeds Limit
0.02
M1
0.012
E
MOO A;
0 !
10/31 /00
Prediction Limit
Intrawell Parametric
2/14/05 5/31 /09 9/14/13 12/29/17 4/15/22
■ MW-2D background
♦ MW-2D compliance
Limit = 0.0084
Background Data Summary (based on square transformation) (after Kaplan -Meier Adjustment): Mean=0.00004309,
Std. Dev.=0.00001692, n=27, 22.22% NDs. Normality test: Shapiro Wilk @alpha = 0.01, calculated = 0.9078, critical
= 0.894. Kappa = 1.633 (c=3, w=4, 1 of 2, event alpha = 0.05132). Report alpha = 0.00438. EPA 1989 outlier
screening was performed on the background data (to establish suspected outliers for Dixon's/Rosner's). No
background outliers were found.
Constituent: Cobalt Total Analysis Run 6/15/2022 11:10 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
Exceeds Limit
0.02
0.016
0.012
E
0.008
0.004
0
10/9/18
Prediction Limit
Intrawell Non -parametric
6/22/19 3/4/20 11 /15/20 7/29/21 4/11 /22
■ MW-15D background
♦ MW-15D compliance
Limit = 0.0050
Non -parametric test used in lieu of parametric prediction limit because censored data exceeded 50%. All background
values (n = 4) were censored; limit is most recent reporting limit. Well -constituent pair annual alpha = 0.119.
Individual comparison alpha = 0.06138 (1 of 2). Distribution was found to be non -normal after removal of suspect
values, so outliers could not be identified.
Constituent: Cobalt Total Analysis Run 6/15/2022 11:10 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

TIME SERIES PLOTS

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.06
0.048
0.036
J
E
0.024
0.012
0 !
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Antimony Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.08
0.064
0.048
J
E
0.032
0.016
0 !
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Arsenic Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
4
3.2
2.4
J
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1.6
0.8 —
0 P
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Barium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.05
0.04
0.03
J
E
0.02
0.01
0 1:—
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Beryllium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.06
0.048
0.036
J
E
0.024
0.012
0
10/30/00
Time Series
A 11 � 11 11�1� 11
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11 1 AL.4"
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2/14/05 6/1 /09 9/16/13 1 /1 /18
4/19/22
Constituent: Cadmium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
J
CM
E
0.5
I
0.4
I
0.3
0.2
0.1
Time Series
a
0
10/30/00
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Chromium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦ MW-10S
♦ MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
J
E
0.2
0.16
0.12
0.08
0.04
0`
Time Series
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4.,7♦
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-T
10/30/00 2/14/05 6/1 /09 9/16/13 1 /1 /18
Constituent: Cobalt Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
2
1.6
1.2
J
E
0.8
0.4
0 �k
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Copper Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.3
0.24
0.18
J
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E
0.12
0.06
0 +,* ,Y
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Lead Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
J
0
E
0.7
0.56
0.42
0.28 1
0.14
0
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Nickel Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
Time Series
0.02
0.016
0.012
J
E
0.008
0.004
0
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11S
10/30/00 2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Selenium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
3
2.4
1.8
J
E
1.2
0.6
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18
4/19/22
Constituent: Silver Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦ MW-10S
♦ MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.03
0.024
0.018
J
E
0.012
0.006
0 !
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Thallium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.6
0.48
0.36
J
E
0.24
0.12
0 ! �,j,
10/30/00
Time Series
2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Vanadium Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-2S (bg)
MW-3S
MW-4S
MW-5S
MW-8S
MW-9
MW-10S
MW-11 S

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.8
0.64
0.48
J
E
0.32
0.16
Time Series
,., t
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2/14/05 6/1 /09 9/16/13 1 /1 /18 4/19/22
Constituent: Zinc Total Analysis Run 6/15/2022 11:20 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
•
MW-2S (bg)
♦
MW-3S
■
MW-4S
♦
MW-5S
♦
MW-8S
♦
MW-9
♦
MW-10S
♦
MW-11S

Sanitas'" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.007
0.0056
0.0042
J
E
0.0028
0.0014
0
10/30/00
Time Series
vvP�
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♦
MW-1 D (bg)
■
MW-2D (bg)
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♦
MW-4D
MW-5D
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MW-15D
♦
MW-12R
■
I
MW-13R
MW-14R
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Antimony Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.03
0.024
0.018
J
E
0.012
0.006
Time Series
„
Ir
10/30/00
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Arsenic Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
♦
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
1
0.8
0.6
J
E
0.4
0.2
0 !
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Barium Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-1 D (bg)
MW-2D (bg)
MW-3D
MW-4D
MW-5D
Mid-8D
MW-15D
MW-12R
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.006
0.0048
0.0036
J
E
of !
0.0012
0
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Beryllium Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-1 D (bg)
MW-2D (bg)
MVW-
MW-4D
MW-5D
ivi vv-cw
MW-15D
MW-12R
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.003
0.0024
0.0018
J
E
0.0012
0.0006
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Cadmium Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
♦
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.01
0.008
0.006
J
E
0.004
0.002
0
10/30/00
Time Series
I
U
r1
U
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Chromium Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
MVW-
♦
MW-4D
MW-5D
A
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.02
0.016
0.012
J
E
0.008
0.004
Time Series
I�
v w
0
10/30/00
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Cobalt Total Analysis Run 6/15/2022 11:27 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.4
0.32
0.24
J
E
0.16
0.08
0q, -, V-:=
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Copper Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-1 D (bg)
MW-2D (bg)
MW•
MW-4D
MW-5D
Mid-8D
MW-15D
MW-12R
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.02
0.016
0.012
J
E
0.008
0.004
Time Series
10/30/00
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Lead Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
♦
MW-3D
♦
MW-4D
MW-5D
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.2
0.16
0.12
J
E
0.08
0.04
0 !
10/30/00
Time Series
I
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Nickel Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-1 D (bg)
MW-2D (bg)
MW•
MW-4D
MW-5D
Mid-8D
MW-15D
MW-12R
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
Time Series
0.01
0.008
0.006
J
I
0.004
I
0.002
4
0
10/30/00 2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Selenium Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
♦
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
3
2.4
1.8
J
E
1.2
0.6
0 'TTII
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Silver Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
MW-1 D (bg)
MW-2D (bg)
MW-3D
MW-4D
MW-5D
Mid-8D
MW-15D
MW-12R
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.02
0.016
0.012
J
E
0.008
0.004
0 !
10/30/00
Time Series
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Thallium Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
♦
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.03
0.024
0.018
J
E
0.012
I
0.006
1
0
10/30/00
Time Series
1`7 ran, 1
♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
♦
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
MW-14R
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Vanadium Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

Sanitas" v.9.6.34 Software licensed to Jett Environmental Consulting. UG
Hollow symbols indicate censored values.
0.04
0.032
0.024
J
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0.016
0.008
0
10/30/00
Time Series
1
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♦
MW-1 D (bg)
■
MW-2D (bg)
MW•
♦
MW-4D
MW-5D
Mid-8D
MW-15D
♦
MW-12R
■
MW-13R
F
MW-14R
2/13/05 5/30/09 9/14/13 12/29/17 4/15/22
Constituent: Zinc Total Analysis Run 6/15/2022 11:28 AM
Anson County LF Client: Waste Connections Data: AnsonCounty

APPENDIX C
LABORATORY ANALYTICAL REPORTS
FIELD SAMPLING FORMS

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-214585-1
Client Project/Site: Anson Landfill Liner Sumpa
r:
S&ME, Inc.
Attn Accounts Payable
644 Eastern Star Rd
Kingsport, Tennessee 37663
Attn: Lindsey Harris
r
Authorized for release by.
51512022 8:14:39 PM
Noel Savoie, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
LCS and/or LCSD is outside acceptance limits, low biased.
*+ LCS and/or LCSD is outside acceptance limits, high biased.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Abbreviation These commonly used abbreviations may or may not be present in this report.
n Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 680-214585-1
Eurofins Savannah
Page 2 of 28 5/5/2022

Sample Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Lab Sample ID Client Sample ID
680-214585-1 ELS Sump 3b 4/26/22
680-214585-2 ELS Sump 4b 4/26/22
Matrix
Water
Water
Collected Received
04/26/2210:35 04/27/2210:15
04/26/2210:50 04/27/2210:15
Job ID: 680-214585-1
Page 3 of 28
Eurofins Savannah
5/5/2022

Case Narrative
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Job ID: 680-214585-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-214585-1
Comments
No additional comments.
Job ID: 680-214585-1
Receipt
The samples were received on 4/27/2022 10:15 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 3.60 C.
GC/MS VOA
Method 8260D SIM: The following sample(s) was collected in a properly preserved vial; however, the pH was outside the required criteria
when verified by the laboratory. The sample was analyzed within the 7-day holding time specified for unpreserved samples: ELS Sump
4b 4/26/22 (680-214585-2).
Method 8260D SIM: The following samples were diluted to bring the concentration of target analytes within the calibration range: ELS
Sump 3b 4/26/22 (680-214585-1) and ELS Sump 4b 4/26/22 (680-214585-2). Elevated reporting limits (RLs) are provided.
Method 8260D: The laboratory control sample (LCS) for analytical batch 680-718616 recovered outside control limits for the following
analyte: 2-Hexanone. 2-Hexanone has been identified as a poor performing analyte when analyzed using this method; therefore,
re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method 8260D: The laboratory control sample/laboratory control sample duplicate (LCS/LCSD) for analytical batch 680-718616 recovered
outside control limits for the following analyte: Chloromethane. This analyte was biased high in the LCS/LCSD and were not detected in
the associated samples; therefore, the data have been reported.
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 680-718616.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 7470A: The following samples for metals were received unpreserved and were preserved upon receipt to the laboratory: ELS
Sump 3b 4/26/22 (680-214585-1) and ELS Sump 4b 4/26/22 (680-214585-2). Regulatory documents require a 24-hour waiting period
from the time of the addition of the acid preservative to the time of digestion.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 28 5/5/2022

Client Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Client Sample ID: ELS Sump 3b 4/26/22
Date Collected: 04/26/22 10:35
Date Received: 04/27/22 10:15
Method: 8260D SIM - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
1,4-Dioxane
249
Surrogate
%Recovery Qualifier
Dibromofluoromethane
100
Toluene-d8 (Surr)
88
4-Bromofluorobenzene
95
Method: 8260D -Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
Acetone
<3.70
Acrylonitrile
<5.50
Benzene
11.7
Bromochloromethane
<0.340
Bromodichloromethane
<0.250
Bromoform
<0.590
Bromomethane
<3.70
2-Butanone (MEK)
<6.40
Carbon disulfide
<0.430
Carbon tetrachloride
<0.300
Chlorobenzene
<0.150
Chlorodibromomethane
<0.390
Chloroethane
<4.60
Chloroform
<0.270
Chloromethane
<0.540
cis-1,2-Dichloroethene
<0.250
cis-1,3-Dichloropropene
<0.260
1,2-Dibromo-3-Chloropropane
<1.80
1,2-Dibromoethane (EDB)
<0.330
Dibromomethane
<0.340
1,2-Dichlorobenzene
<0.310
1,4-Dichlorobenzene
9.68
1,1-Dichloroethane
<0.330
1,2-Dichloroethane
<0.250
1,1-Dichloroethene
<0.330
1,2-Dichloropropane
0.324 J
Ethylbenzene
59.8
2-Hexanone
<3.20
lodomethane
<3.90
Methylene Chloride
<3.20
4-Methyl-2-pentanone (MIBK)
<2.70
Styrene
0.909 J
1,1,1,2-Tetrachloroethane
<0.360
1,1,2,2-Tetrachloroethane
<0.400
Tetrachloroethene
<0.350
Toluene
23.6
trans-1,4-Dichloro-2-butene
<1.25
trans-1,2-Dichloroethene
<0.340
trans-1,3-Dichloropropene
<0.230
1,1,1-Trichloroethane
<0.210
1,1,2-Trichloroethane
<0.320
F
Job ID: 680-214585-1
Lab Sample ID: 680-214585-1
Matrix: Water
RL
MDL
Unit
D Prepared
Analyzed
10.0
3.00
ug/L
05/03/2219:10
Limits
Prepared
Analyzed
50 - 150
05/03/22 19:10
50 - 150
05103122 19:10
50 - 150
05103122 19:10
RL
MDL
Unit
D Prepared
Analyzed
10.0
3.70
ug/L
05/02/2218:42
20.0
5.50
ug/L
05/01/22 17:24
1.00
0.270
ug/L
05/01/22 17:24
1.00
0.340
ug/L
05/01/22 17:24
1.00
0.250
ug/L
05/01/22 17:24
1.00
0.590
ug/L
05/01/22 17:24
5.00
3.70
ug/L
05/01/22 17:24
10.0
6.40
ug/L
05/01/22 17:24
2.00
0.430
ug/L
05/01/22 17:24
1.00
0.300
ug/L
05/01/22 17:24
1.00
0.150
ug/L
05/01/22 17:24
1.00
0.390
ug/L
05/01/22 17:24
5.00
4.60
ug/L
05/01/22 17:24
1.00
0.270
ug/L
05/01/22 17:24
1.00
0.540
ug/L
05/01/22 17:24
1.00
0.250
ug/L
05/01/22 17:24
1.00
0.260
ug/L
05/01/22 17:24
5.00
1.80
ug/L
05/01/22 17:24
1.00
0.330
ug/L
05/01/22 17:24
1.00
0.340
ug/L
05/01/22 17:24
1.00
0.310
ug/L
05/01/22 17:24
1.00
0.310
ug/L
05/01/22 17:24
1.00
0.330
ug/L
05/01/22 17:24
1.00
0.250
ug/L
05/01/22 17:24
1.00
0.330
ug/L
05/01/22 17:24
1.00
0.220
ug/L
05/01/22 17:24
1.00
0.200
ug/L
05/01/22 17:24
10.0
3.20
ug/L
05/01/22 17:24
10.0
3.90
ug/L
05/01/22 17:24
5.00
3.20
ug/L
05/01/22 17:24
10.0
2.70
ug/L
05/01/22 17:24
1.00
0.270
ug/L
05/01/22 17:24
1.00
0.360
ug/L
05/01/22 17:24
1.00
0.400
ug/L
05/01/22 17:24
0.500
0.350
ug/L
05/01/22 17:24
1.00
0.250
ug/L
05/01/22 17:24
2.00
1.25
ug/L
05/01/22 17:24
1.00
0.340
ug/L
05/01/22 17:24
1.00
0.230
ug/L
05/01/22 17:24
1.00
0.210
ug/L
05/01/22 17:24
1.00
0.320
ug/L
05/01/22 17:24
Page 5 of 28
Eurofins Savannah
5/5/2022

Client Sample Results
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Client Sample ID: ELS Sump 3b
4/26/22
Lab Sample ID: 680-214585-1
Date Collected: 04/26/22 10:35
Matrix: Water
Date Received: 04/27/22 10:15
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Trichloroethene
<0.200
1.00
0.200
ug/L
-
05/01/2217:24
1
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/01/2217:24
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/01/2217:24
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/01/22 17:24
1
Vinyl chloride
1.45
1.00
0.400
ug/L
05/01/22 17:24
1
Xylenes, Total
93.2
1.00
0.230
ug/L
05/01/22 17:24
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
102
70 - 130
05101122 17.24
1
4-Bromofluorobenzene (Surr)
101
70 - 130
05/02/22 18:42
1
Dibromofluoromethane (Surr)
106
70 - 130
05101122 17:24
1
Dibromofluoromethane (Surr)
108
70 - 130
05102122 18:42
1
1,2-Dichloroethane-d4 (Surr)
97
60- 124
05101122 17:24
1
1,2-Dichloroethane-d4 (Surr)
106
60- 124
05102122 18:42
1
Toluene-d8 (Surr)
109
70 - 130
05101122 17:24
1
Toluene-d8 (Surr)
105
70 - 130
05/02/22 18:42
1
Method: 6020B - Metals (ICP/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Antimony
0.00141 J
0.00500
0.000520
mg/L
05/02/2214:01
05/03/2216:38
1
Arsenic
0.0192
0.00300
0.000860
mg/L
05/02/2214:01
05/03/2216:38
1
Barium
0.629
0.00500
0.000890
mg/L
05/02/2214:01
05/03/2216:38
1
Beryllium
0.000290 J
0.000500
0.000200
mg/L
05/02/2214:01
05/03/2216:38
1
Cadmium
<0.0000780
0.000500
0.0000780
mg/L
05/02/2214:01
05/03/2216:38
1
Chromium
0.00508
0.00500
0.00260
mg/L
05/02/2214:01
05/03/2216:38
1
Cobalt
0.00998
0.000500
0.000220
mg/L
05/02/2214:01
05/03/2216:38
1
Copper
0.0320
0.00500
0.000900
mg/L
05/02/2214:01
05/03/2216:38
1
Lead
0.000890 J
0.00250
0.000340
mg/L
05/02/2214:01
05/03/2216:38
1
Nickel
0.0340
0.00500
0.00180
mg/L
05/02/2214:01
05/03/2216:38
1
Selenium
0.00124 J
0.00250
0.00120
mg/L
05/02/2214:01
05/03/2216:38
1
Silver
<0.000390
0.00100
0.000390
mg/L
05/02/2214:01
05/03/2216:38
1
Thallium
<0.000260
0.00100
0.000260
mg/L
05/02/2214:01
05/0312216:38
1
Vanadium
0.00579 J
0.0100
0.00180
mg/L
05/02/2214:01
05/0312216:38
1
Zinc
0.160
0.0200
0.0100
mg/L
05/02/2214:01
05/0312216:38
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
<0.0800
0.200
0.0800
ug/L
05/02/2214:18
05/03/2211:43
1
Client Sample ID: ELS Sump 4b
4/26/22
Lab Sample ID: 680-214585-2
Date Collected: 04/26/22 10:50
Matrix: Water
Date Received: 04/27/22 10:15
Method: 8260D SIM - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
1,4-Dioxane
791
50.0
15.0
ug/L
05/0312218:45
50
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dfl Fac
Dibromofluoromethane
103
50 - 150
05103122 18:45
50
Toluene-d8 (Surr)
88
50 - 150
05/03/22 18:45
50
4-Bromofluorobenzene
94
50 - 150
05/03/22 18:45
50
Eurofins Savannah
Page 6 of 28 5/5/2022

Client Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Client Sample ID: ELS Sump 4b 4/26/22
Date Collected: 04/26/22 10:50
Date Received: 04/27/22 10:15
Method: 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
Acetone
<3.70
Acrylonitrile
<5.50
Benzene
9.28
Bromochloromethane
<0.340
Bromodichloromethane
<0.250
Bromoform
<0.590
Bromomethane
<3.70
2-Butanone (MEK)
66.7
Carbon disulfide
<0.430
Carbon tetrachloride
<0.300
Chlorobenzene
2.22
Chlorodibromomethane
<0.390
Chloroethane
<4.60
Chloroform
<0.270
Chloromethane
<0.540
cis-1,2-Dichloroethene
<0.250
cis-1,3-Dichloropropene
<0.260
1,2-Dibromo-3-Chloropropane
<1.80
1,2-Dibromoethane (EDB)
<0.330
Dibromomethane
<0.340
1,2-Dichlorobenzene
<0.310
1,4-Dichlorobenzene
3.98
1,1-Dichloroethane
<0.330
1,2-Dichloroethane
0.682 J
1,1-Dichloroethene
<0.330
1,2-Dichloropropane
<0.220
Ethylbenzene
32.3
2-Hexanone
<3.20
lodomethane
<3.90
Methylene Chloride
<3.20
4-Methyl-2-pentanone (MIBK)
13.8
Styrene
<0.270
1,1,1,2-Tetrachloroethane
<0.360
1,1,2,2-Tetrachloroethane
<0.400
Tetrachloroethene
<0.350
Toluene
2.57
trans-1,4-Dichloro-2-butene
<1.25
trans-1,2-Dichloroethene
<0.340
trans-1,3-Dichloropropene
<0.230
1,1,1-Trichloroethane
<0.210
1,1,2-Trichloroethane
<0.320
Trichloroethene
<0.200
Trichlorofluoromethane
<0.330
1,2,3-Trichloropropane
<0.480
Vinyl acetate
<0.690
Vinyl chloride
0.523 J
Xylenes, Total
15.7
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 101
Job ID: 680-214585-1
Lab Sample ID: 680-214585-2
Matrix: Water
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
10.0
3.70
ug/L
05/02/2219:05
1
20.0
5.50
ug/L
05/01/2217:44
1
1.00
0.270
ug/L
05/01/2217:44
1
1.00
0.340
ug/L
05/01/2217:44
1
1.00
0.250
ug/L
05/01/2217:44
1
1.00
0.590
ug/L
05/01/2217:44
1
5.00
3.70
ug/L
05/01/2217:44
1
10.0
6.40
ug/L
05/01/2217:44
1
2.00
0.430
ug/L
05/01/2217:44
1
1.00
0.300
ug/L
05/01/2217:44
1
1.00
0.150
ug/L
05/01/2217:44
1
1.00
0.390
ug/L
05/01/2217:44
1
5.00
4.60
ug/L
05/01/2217:44
1
1.00
0.270
ug/L
05/01/2217:44
1
1.00
0.540
ug/L
05/01/2217:44
1
1.00
0.250
ug/L
05/01/2217:44
1
1.00
0.260
ug/L
05/01/2217:44
1
5.00
1.80
ug/L
05/01/2217:44
1
1.00
0.330
ug/L
05/01/22 17:44
1
1.00
0.340
ug/L
05/01/22 17:44
1
1.00
0.310
ug/L
05/01/22 17:44
1
1.00
0.310
ug/L
05/01/2217:44
1
1.00
0.330
ug/L
05/01/2217:44
1
1.00
0.250
ug/L
05/01/2217:44
1
1.00
0.330
ug/L
05/01/2217:44
1
1.00
0.220
ug/L
05/01/2217:44
1
1.00
0.200
ug/L
05/01/2217:44
1
10.0
3.20
ug/L
05/01/2217:44
1
10.0
3.90
ug/L
05/01/2217:44
1
5.00
3.20
ug/L
05/01/2217:44
1
10.0
2.70
ug/L
05/01/2217:44
1
1.00
0.270
ug/L
05/01/2217:44
1
1.00
0.360
ug/L
05/01/2217:44
1
1.00
0.400
ug/L
05/0112217:44
1
0.500
0.350
ug/L
05/0112217:44
1
1.00
0.250
ug/L
05/01/2217:44
1
2.00
1.25
ug/L
05/01/2217:44
1
1.00
0.340
ug/L
05/01/2217:44
1
1.00
0.230
ug/L
05/01/2217:44
1
1.00
0.210
ug/L
05/01/2217:44
1
1.00
0.320
ug/L
05/01/2217:44
1
1.00
0.200
ug/L
05/01/2217:44
1
1.00
0.330
ug/L
05/01/2217:44
1
1.00
0.480
ug/L
05/01/2217:44
1
2.00
0.690
ug/L
05/01/2217:44
1
1.00
0.400
ug/L
05/01/2217:44
1
1.00
0.230
ug/L
05/01/2217:44
1
Limits
Prepared Analyzed
DU Fac
70 - 130
05101122 17:44
1
Eurofins Savannah
Page 7 of 28 5/5/2022

Client Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Job ID: 680-214585-1
Client Sample ID: ELS Sump 4b 4/26/22 Lab Sample ID: 680-214585-2
Date Collected: 04/26/22 10:50 Matrix: Water
Date Received: 04/27/22 10:15
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
102
70 - 130
Dibromofluoromethane (Surr)
102
70 - 130
Dibromofluoromethane (Surr)
110
70 - 130
1,2-Dichloroethane-d4 (Surr)
94
60- 124
1,2-Dichloroethane-d4 (Surr)
104
60- 124
Toluene-d8 (Surr)
109
70 - 130
Toluene-d8 (Surr)
106
70 - 130
Method: 6020E - Metals (ICP/MS)
Analyte
Result Qualifier
RL
Antimony
0.00343 J
0.00500
Arsenic
0.0422
0.00300
Barium
2.55
0.00500
Beryllium
<0.000200
0.000500
Cadmium
0.000240 J
0.000500
Chromium
0.0428
0.00500
Cobalt
0.0390
0.000500
Copper
0.218
0.00500
Lead
0.00712
0.00250
Nickel
0.462
0.00500
Selenium
0.00305
0.00250
Silver
<0.000390
0.00100
Thallium
<0.000260
0.00100
Vanadium
0.0219
0.0100
Zinc
0.0916
0.0200
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
Mercury
<0.0800
0.200
Prepared
Analyzed
Dil Fac
05102122 19:05
1
05101122 17:44
1
05102122 19:05
1
05101122 17:44
1
05102122 19:05
1
05101122 17:44
1
05102122 19:05
1
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.000520
mg/L
05/02/2214:01
05/03/2216:41
1
0.000860
mg/L
05/02/2214:01
05/03/2216:41
1
0.000890
mg/L
05/02/2214:01
05/03/2216:41
1
0.000200
mg/L
05/02/2214:01
05/03/2216:41
1
0.0000780
mg/L
05/02/2214:01
05/03/2216:41
1
0.00260
mg/L
05/02/2214:01
05/03/2216:41
1
0.000220
mg/L
05102/2214:01
05/03/2216:41
1
0.000900
mg/L
05102/2214:01
05/03/2216:41
1
0.000340
mg/L
05102/2214:01
05103/2216:41
1
0.00180
mg/L
05/02/2214:01
05/03/2216:41
1
0.00120
mg/L
05/02/2214:01
05/03/2216:41
1
0.000390
mg/L
05/02/2214:01
05/03/2216:41
1
0.000260
mg/L
05/02/2214:01
05/03/2216:41
1
0.00180
mg/L
05/02/2214:01
05/03/2216:41
1
0.0100
mg/L
05/02/2214:01
05/03/2216:41
1
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.0800
ug/L
05/02/2214:18
05/03/2211:45
1
Eurofins Savannah
Page 8 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS
Job ID: 680-214585-1
FLab Sample ID: MB 680-718541/9
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
<3.70
10.0
3.70
ug/L
05/01/22 13:37
1
Acrylonitrile
<5.50
20.0
5.50
ug/L
05/01/22 13:37
1
Benzene
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
Bromochloromethane
<0.340
1.00
0.340
ug/L
05/0112213:37
1
Bromodichloromethane
<0.250
1.00
0.250
ug/L
05/0112213:37
1
Bromoform
<0.590
1.00
0.590
ug/L
05/0112213:37
1
Bromomethane
<3.70
5.00
3.70
ug/L
05/01/22 13:37
1
2-Butanone (MEK)
<6.40
10.0
6.40
ug/L
05/01/22 13:37
1
Carbon disulfide
<0.430
2.00
0.430
ug/L
05/01/22 13:37
1
Carbon tetrachloride
<0.300
1.00
0.300
ug/L
05/01/22 13:37
1
Chlorobenzene
<0.150
1.00
0.150
ug/L
05/01/22 13:37
1
Chlorodibromomethane
<0.390
1.00
0.390
ug/L
05/01/22 13:37
1
Chloroethane
<4.60
5.00
4.60
ug/L
05/01/22 13:37
1
Chloroform
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
Chloromethane
<0.540
1.00
0.540
ug/L
05/01/22 13:37
1
cis-1,2-Dichloroethene
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
cis-1,3-Dichloropropene
<0.260
1.00
0.260
ug/L
05/01/22 13:37
1
1,2-Dibromo-3-Chloropropane
<1.80
5.00
1.80
ug/L
05/01/22 13:37
1
1,2-Dibromoethane (EDB)
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
Dibromomethane
<0.340
1.00
0.340
ug/L
05/0112213:37
1
1,2-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/01/22 13:37
1
1,4-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/01/22 13:37
1
1,1-Dichloroethane
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,2-Dichloroethane
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
1,1-Dichloroethene
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,2-Dichloropropane
<0.220
1.00
0.220
ug/L
05/01/22 13:37
1
Ethylbenzene
<0.200
1.00
0.200
ug/L
05/01/22 13:37
1
2-Hexanone
<3.20
10.0
3.20
ug/L
05/01/22 13:37
1
lodomethane
<3.90
10.0
3.90
ug/L
05/01/22 13:37
1
Methylene Chloride
<3.20
5.00
3.20
ug/L
05/01/22 13:37
1
4-Methyl-2-pentanone (MIBK)
<2.70
10.0
2.70
ug/L
05/01/22 13:37
1
Styrene
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
1,1,1,2-Tetrachloroethane
<0.360
1.00
0.360
ug/L
05/01/22 13:37
1
1,1,2,2-Tetrachloroethane
<0.400
1.00
0.400
ug/L
05/0112213:37
1
Tetrachloroethene
<0.350
0.500
0.350
ug/L
05/0112213:37
1
Toluene
<0.250
1.00
0.250
ug/L
05/0112213:37
1
trans-1,4-Dichloro-2-butene
<1.25
2.00
1.25
ug/L
05/01/22 13:37
1
trans-1,2-Dichloroethene
<0.340
1.00
0.340
ug/L
05/01/22 13:37
1
trans-1,3-Dichloropropene
<0.230
1.00
0.230
ug/L
05/01/22 13:37
1
1,1,1-Trichloroethane
<0.210
1.00
0.210
ug/L
05/01/22 13:37
1
1,1,2-Trichloroethane
<0.320
1.00
0.320
ug/L
05/01/22 13:37
1
Trichloroethene
<0.200
1.00
0.200
ug/L
05/01/22 13:37
1
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/01/22 13:37
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/01/22 13:37
1
Vinyl chloride
<0.400
1.00
0.400
ug/L
05/01/22 13:37
1
Xylenes, Total
<0.230
1.00
0.230
ug/L
05/01/22 13:37
1
Eurofins Savannah
Page 9 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Job ID: 680-214585-1
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 680-718541/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed Dil Fa
4-Bromofluorobenzene (Surr)
103
70 - 130
05101122 13:37 1 •
Dibromofluoromethane (Surr)
101
70 - 130
05101122 13:37 1
1,2-Dichloroethane-d4 (Surr)
90
60- 124
05101122 13:37 1
Toluene-d8 (Surr)
110
70 - 130
05101122 13:37 1
Lab Sample ID: LCS 680-718541/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec
Limits
Acetone
250
204.1
ug/L
82
67 - 120
Acrylonitrile
500
457.7
ug/L
92
70 - 130
Benzene
50.0
47.74
ug/L
95
70 - 130
Bromochloromethane
50.0
48.72
ug/L
97
70 - 130
Bromodichloromethane
50.0
48.32
ug/L
97
70 - 130
Bromoform
50.0
50.81
ug/L
102
69 - 129
Bromomethane
50.0
51.64
ug/L
103
28 - 192
2-Butanone (MEK)
250
217.7
ug/L
87
69 - 120
Carbon disulfide
50.0
40.77
ug/L
82
70 - 130
Carbon tetrachloride
50.0
46.76
ug/L
94
70 - 130
Chlorobenzene
50.0
51.39
ug/L
103
70 - 130
Chlorodibromomethane
50.0
49.42
ug/L
99
70 - 130
Chloroethane
50.0
54.47
ug/L
109
31 - 213
Chloroform
50.0
47.53
ug/L
95
70 - 130
Chloromethane
50.0
41.61
ug/L
83
59 - 127
cis-1,2-Dichloroethene
50.0
47.34
ug/L
95
70 - 130
cis- 1,3-Dichloropropene
50.0
51.87
ug/L
104
70 - 130
1,2-Dibromo-3-Chloropropane
50.0
50.69
ug/L
101
70 - 130
1,2-Dibromoethane (EDB)
50.0
51.48
ug/L
103
70 - 130
Dibromomethane
50.0
48.79
ug/L
98
70 - 130
1,2-Dichlorobenzene
50.0
52.37
ug/L
105
70 - 130
1,4-Dichlorobenzene
50.0
51.62
ug/L
103
70 - 130
1,1-Dichloroethane
50.0
45.36
ug/L
91
70-130
1,2-Dichloroethane
50.0
49.55
ug/L
99
70 - 130
1,1-Dichloroethene
50.0
42.92
ug/L
86
70-130
1,2-Dichloropropane
50.0
49.82
ug/L
100
70 - 130
Ethylbenzene
50.0
51.38
ug/L
103
70 - 130
2-Hexanone
250
235.3
ug/L
94
70 - 130
lodomethane
50.0
42.62
ug/L
85
52 - 129
Methylene Chloride
50.0
43.05
ug/L
86
70 - 130
4-Methyl-2-pentanone (MIBK)
250
248.7
ug/L
99
68 - 120
Styrene
50.0
51.96
ug/L
104
70 - 130
1,1,1,2-Tetrachloroethane
50.0
53.54
ug/L
107
70-130
1,1,2,2-Tetrachloroethane
50.0
48.69
ug/L
97
70-130
Tetrachloroethene
50.0
51.54
ug/L
103
70 - 130
Toluene
50.0
49.96
ug/L
100
70 - 130
trans- 1,4-Dichloro-2-butene
50.0
46.46
ug/L
93
67-120
trans- 1,2-Dichloroethene
50.0
43.05
ug/L
86
70 - 130
Eurofins Savannah
Page 10 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc. Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 680-718541/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
trans- 1,3-Dichloropropene
50.0
53.53
ug/L
107
70 - 130
1,1,1-Trichloroethane
50.0
43.22
ug/L
86
70-130
1,1,2-Trichloroethane
50.0
50.50
ug/L
101
70-130
Trichloroethene
50.0
50.31
ug/L
101
70 - 130
Trichlorofluoromethane
50.0
52.74
ug/L
105
63 - 142
1,2,3-Trichloropropane
50.0
51.05
ug/L
102
70 - 130
Vinyl acetate
100
103.0
ug/L
103
67 - 135
Vinyl chloride
50.0
43.49
ug/L
87
66 - 129
Xylenes, Total
100
99.61
ug/L
100
70 - 130
LCS LCS
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
97
70 - 130
Dibromofluoromethane (Surr)
98
70 - 130
1,2-Dichloroethane-d4 (Surr)
99
60 - 124
Toluene-d8 (Surr)
104
70 - 130
Lab Sample ID: LCSD 680-718541/5
Client Sample ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCSD
LCSD
%Rec
RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
250
210.7
ug/L
84
67 - 120
3
30
Acrylonitrile
500
465.7
ug/L
93
70 - 130
2
30
Benzene
50.0
48.34
ug/L
97
70 - 130
1
30
Bromochloromethane
50.0
49.04
ug/L
98
70 - 130
1
30
Bromodichloromethane
50.0
49.37
ug/L
99
70 - 130
2
30
Bromoform
50.0
51.33
ug/L
103
69 - 129
1
30
Bromomethane
50.0
54.04
ug/L
108
28 - 192
5
30
2-Butanone (MEK)
250
227.9
ug/L
91
69 - 120
5
30
Carbon disulfide
50.0
41.59
ug/L
83
70 - 130
2
30
Carbon tetrachloride
50.0
48.08
ug/L
96
70 - 130
3
30
Chlorobenzene
50.0
51.95
ug/L
104
70 - 130
1
30
Chlorodibromomethane
50.0
49.83
ug/L
100
70 - 130
1
30
Chloroethane
50.0
56.92
ug/L
114
31 - 213
4
30
Chloroform
50.0
48.25
ug/L
97
70 - 130
2
30
Chloromethane
50.0
42.76
ug/L
86
59 - 127
3
30
cis-1,2-Dichloroethene
50.0
47.81
ug/L
96
70 - 130
1
30
cis- 1,3-Dichloropropene
50.0
52.79
ug/L
106
70 - 130
2
20
1,2-Dibromo-3-Chloropropane
50.0
52.10
ug/L
104
70 - 130
3
30
1,2-Dibromoethane (EDB)
50.0
52.20
ug/L
104
70 - 130
1
30
Dibromomethane
50.0
48.95
ug/L
98
70 - 130
0
30
1,2-Dichlorobenzene
50.0
52.76
ug/L
106
70 - 130
1
30
1,4-Dichlorobenzene
50.0
52.04
ug/L
104
70 - 130
1
30
1,1-Dichloroethane
50.0
45.88
ug/L
92
70-130
1
30
1,2-Dichloroethane
50.0
50.61
ug/L
101
70 - 130
2
50
1,1-Dichloroethene
50.0
44.05
ug/L
88
70-130
3
20
1,2-Dichloropropane
50.0
50.42
ug/L
101
70 - 130
1
20
Ethylbenzene
50.0
52.26
ug/L
105
70 - 130
2
20
0
Eurofins Savannah
Page 11 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Job ID: 680-214585-1
Lab Sample ID: LCSD 680-718541/5
Client Sample ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCSD LCSD
%Rec
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
2-Hexanone
250
242.1
ug/L
97
70 - 130
3
20
lodomethane
50.0
42.75
ug/L
86
52 - 129
0
30
Methylene Chloride
50.0
43.77
ug/L
88
70 - 130
2
30
4-Methyl-2-pentanone (MIBK)
250
253.7
ug/L
101
68 - 120
2
30
Styrene
50.0
53.20
ug/L
106
70 - 130
2
30
1,1,1,2-Tetrachloroethane
50.0
54.67
ug/L
109
70-130
2
30
1,1,2,2-Tetrachloroethane
50.0
49.16
ug/L
98
70-130
1
30
Tetrachloroethene
50.0
53.10
ug/L
106
70 - 130
3
30
Toluene
50.0
50.70
ug/L
101
70 - 130
1
30
trans-1,4-Dichloro-2-butene
50.0
47.54
ug/L
95
67 - 120
2
30
trans-1,2-Dichloroethene
50.0
43.51
ug/L
87
70 - 130
1
30
trans-1,3-Dichloropropene
50.0
53.89
ug/L
108
70 - 130
1
30
1,1,1-Trichloroethane
50.0
44.15
ug/L
88
70-130
2
30
1,1,2-Trichloroethane
50.0
51.24
ug/L
102
70-130
1
30
Trichloroethene
50.0
51.59
ug/L
103
70 - 130
3
30
Trichlorofluoromethane
50.0
53.06
ug/L
106
63 - 142
1
30
1,2,3-Trichloropropane
50.0
52.54
ug/L
105
70 - 130
3
30
Vinyl acetate
100
105.9
ug/L
106
67 - 135
3
30
Vinyl chloride
50.0
44.24
ug/L
88
66 - 129
2
30
Xylenes, Total
100
101.0
ug/L
101
70 - 130
1
30
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 70 - 130
Dibromofluoromethane (Surr) 99 70 - 130
1,2-Dichloroethane-d4 (Surr) 100 60- 124
Toluene-d8 (Surr) 106 70 - 130
rLab Sample ID: MB 680-718616/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718616
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Acetone
<3.70
10.0
3.70
ug/L
05/02/22 13:32 1
Acrylonitrile
<5.50
20.0
5.50
ug/L
05/02/22 13:32 1
Benzene
<0.270
1.00
0.270
ug/L
05/02/22 13:32 1
Bromochloromethane
<0.340
1.00
0.340
ug/L
05/02/22 13:32 1
Bromodichloromethane
<0.250
1.00
0.250
ug/L
05/02/22 13:32 1
Bromoform
<0.590
1.00
0.590
ug/L
05/02/22 13:32 1
Bromomethane
<3.70
5.00
3.70
ug/L
05/02/22 13:32 1
2-Butanone (MEK)
<6.40
10.0
6.40
ug/L
05/02/22 13:32 1
Carbon disulfide
<0.430
2.00
0.430
ug/L
05/02/22 13:32 1
Carbon tetrachloride
<0.300
1.00
0.300
ug/L
05/02/22 13:32 1
Chlorobenzene
<0.150
1.00
0.150
ug/L
05/02/22 13:32 1
Chlorodibromomethane
<0.390
1.00
0.390
ug/L
05/02/22 13:32 1
Chloroethane
<4.60
5.00
4.60
ug/L
05/02/22 13:32 1
Chloroform
<0.270
1.00
0.270
ug/L
05/02/22 13:32 1
Chloromethane
<0.540
1.00
0.540
ug/L
05/02/22 13:32 1
cis-1,2-Dichloroethene
<0.250
1.00
0.250
ug/L
05/02/22 13:32 1
Eurofins Savannah
Page 12 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Job ID: 680-214585-1
Lab Sample ID: MB 680-718616/9
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718616
MB MB
Analyte
Result Qualifier
RL
MDL
unit
D Prepared Analyzed
Dil Fac
cis-1,3-Dichloropropene
<0.260
1.00
0.260
ug/L
05/02/22 13:32
1
1,2-Dibromo-3-Chloropropane
<1.80
5.00
1.80
ug/L
05/02/22 13:32
1
1,2-Dibromoethane (EDB)
<0.330
1.00
0.330
ug/L
05/02/22 13:32
1
Dibromomethane
<0.340
1.00
0.340
ug/L
05/02/22 13:32
1
1,2-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/02/22 13:32
1
1,4-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/02/22 13:32
1
1,1-Dichloroethane
<0.330
1.00
0.330
ug/L
05/02/22 13:32
1
1,2-Dichloroethane
<0.250
1.00
0.250
ug/L
05/02/22 13:32
1
1,1-Dichloroethene
<0.330
1.00
0.330
ug/L
05/0212213:32
1
1,2-Dichloropropane
<0.220
1.00
0.220
ug/L
05/0212213:32
1
Ethylbenzene
<0.200
1.00
0.200
ug/L
05/0212213:32
1
2-Hexanone
<3.20
10.0
3.20
ug/L
05/02/22 13:32
1
lodomethane
<3.90
10.0
3.90
ug/L
05/02/22 13:32
1
Methylene Chloride
<3.20
5.00
3.20
ug/L
05/02/22 13:32
1
4-Methyl-2-pentanone (MIBK)
<2.70
10.0
2.70
ug/L
05/02/22 13:32
1
Styrene
<0.270
1.00
0.270
ug/L
05/02/22 13:32
1
1,1,1,2-Tetrachloroethane
<0.360
1.00
0.360
ug/L
05/02/22 13:32
1
1,1,2,2-Tetrachloroethane
<0.400
1.00
0.400
ug/L
05/02/22 13:32
1
Tetrachloroethene
<0.350
0.500
0.350
ug/L
05/02/22 13:32
1
Toluene
<0.250
1.00
0.250
ug/L
05/02/22 13:32
1
trans-1,4-Dichloro-2-butene
<1.25
2.00
1.25
ug/L
05/02/22 13:32
1
trans-1,2-Dichloroethene
<0.340
1.00
0.340
ug/L
05/02/22 13:32
1
trans-1,3-Dichloropropene
<0.230
1.00
0.230
ug/L
05/02/22 13:32
1
1,1,1-Trichloroethane
<0.210
1.00
0.210
ug/L
05/0212213:32
1
1,1,2-Trichloroethane
<0.320
1.00
0.320
ug/L
05/0212213:32
1
Trichloroethene
<0.200
1.00
0.200
ug/L
05/0212213:32
1
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/02/22 13:32
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/02/22 13:32
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/02/22 13:32
1
Vinyl chloride
<0.400
1.00
0.400
ug/L
05/02/22 13:32
1
Xylenes, Total
<0.230
1.00
0.230
ug/L
05/02/22 13:32
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dfl Fac
4-Bromofluorobenzene (Surr)
96
70 - 130
05102122 13:32 1
Dibromofluoromethane (Surr)
121
70 - 130
05102122 13:32 1
1,2-Dichloroethane-d4 (Surr)
110
60- 124
05102122 13:32 1
Toluene-d8 (Surr)
104
70 - 130
05/02/22 13:32 1
Lab Sample ID: LCS 680-718616/4
Client Sample
ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718616
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
213.6
ug/L
85
67 -120
Acrylonitrile
500
436.0
ug/L
87
70 - 130
Benzene
50.0
46.27
ug/L
93
70 - 130
Bromochloromethane
50.0
48.09
ug/L
96
70 - 130
Bromodichloromethane
50.0
45.58
ug/L
91
70 - 130
Eurofins Savannah
Page 13 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc. Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 680-718616/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 718616
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Bromoform
50.0
42.69
ug/L
85
69 - 129
Bromomethane
50.0
56.62
ug/L
113
28 - 192
2-Butanone (MEK)
250
197.8
ug/L
79
69 - 120
Carbon disulfide
50.0
54.43
ug/L
109
70 - 130
Carbon tetrachloride
50.0
42.44
ug/L
85
70 - 130
Chlorobenzene
50.0
45.80
ug/L
92
70 - 130
Chlorodibromomethane
50.0
39.94
ug/L
80
70 - 130
Chloroethane
50.0
56.05
ug/L
112
31 - 213
Chloroform
50.0
47.90
ug/L
96
70 - 130
Chloromethane
50.0
73.41 .+
ug/L
147
59 - 127
cis-1,2-Dichloroethene
50.0
46.69
ug/L
93
70 - 130
cis- 1,3-Dichloropropene
50.0
42.50
ug/L
85
70 - 130
1,2-Dibromo-3-Chloropropane
50.0
38.91
ug/L
78
70 - 130
1,2-Dibromoethane (EDB)
50.0
39.41
ug/L
79
70 - 130
Dibromomethane
50.0
44.30
ug/L
89
70 - 130
1,2-Dichlorobenzene
50.0
47.96
ug/L
96
70 - 130
1,4-Dichlorobenzene
50.0
46.56
ug/L
93
70 - 130
1,1-Dichloroethane
50.0
49.71
ug/L
99
70-130
1,2-Dichloroethane
50.0
47.63
ug/L
95
70 - 130
1,1-Dichloroethene
50.0
48.01
ug/L
96
70-130
1,2-Dichloropropane
50.0
45.80
ug/L
92
70 - 130
Ethylbenzene
50.0
45.62
ug/L
91
70 - 130
2-Hexanone
250
173.7 `-
ug/L
69
70 - 130
lodomethane
50.0
48.23
ug/L
96
52 - 129
Methylene Chloride
50.0
42.64
ug/L
85
70 - 130
4-Methyl-2-pentanone (MIBK)
250
184.8
ug/L
74
68 - 120
Styrene
50.0
44.05
ug/L
88
70 - 130
1,1,1,2-Tetrachloroethane
50.0
47.06
ug/L
94
70-130
1,1,2,2-Tetrachloroethane
50.0
51.05
ug/L
102
70-130
Tetrachloroethene
50.0
40.11
ug/L
80
70 - 130
Toluene
50.0
41.34
ug/L
83
70 - 130
trans- 1,4-Dichloro-2-butene
50.0
36.78
ug/L
74
67-120
trans- 1,2-Dichloroethene
50.0
50.91
ug/L
102
70 - 130
trans- 1,3-Dichloropropene
50.0
41.04
ug/L
82
70 - 130
1,1,1-Trichloroethane
50.0
39.52
ug/L
79
70-130
1,1,2-Trichloroethane
50.0
42.21
ug/L
84
70-130
Trichloroethene
50.0
42.42
ug/L
85
70 - 130
Trichlorofluoromethane
50.0
64.05
ug/L
128
63 - 142
1,2,3-Trichloropropane
50.0
46.26
ug/L
93
70 - 130
Vinyl acetate
100
97.91
ug/L
98
67 - 135
Vinyl chloride
50.0
51.18
ug/L
102
66 - 129
Xylenes, Total
100
90.27
ug/L
90
70 - 130
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
104
70 - 130
Dibromofluoromethane (Surr)
104
70 - 130
1,2-Dichloroethane-d4 (Surr)
96
60 - 124
Toluene-d8 (Surr)
104
70 - 130
0
Eurofins Savannah
Page 14 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Job ID: 680-214585-1
Lab Sample ID: LCSD 680-718616/5
Client Sample ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718616
Spike
LCSD LCSD
°/Rec
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
250
217.3
ug/L
87
67 - 120
2
30
Acrylonitrile
500
438.8
ug/L
88
70 - 130
1
30
Benzene
50.0
46.70
ug/L
93
70 - 130
1
30
Bromochloromethane
50.0
47.48
ug/L
95
70 - 130
1
30
Bromodichloromethane
50.0
45.81
ug/L
92
70 - 130
1
30
Bromoform
50.0
43.02
ug/L
86
69 - 129
1
30
Bromomethane
50.0
52.35
ug/L
105
28 - 192
8
30
2-Butanone (MEK)
250
201.6
ug/L
81
69 - 120
2
30
Carbon disulfide
50.0
53.30
ug/L
107
70 - 130
2
30
Carbon tetrachloride
50.0
42.95
ug/L
86
70 - 130
1
30
Chlorobenzene
50.0
45.94
ug/L
92
70 - 130
0
30
Chlorodibromomethane
50.0
41.29
ug/L
83
70 - 130
3
30
Chloroethane
50.0
51.11
ug/L
102
31 - 213
9
30
Chloroform
50.0
47.86
ug/L
96
70 - 130
0
30
Chloromethane
50.0
77.98 *+
ug/L
156
59 - 127
6
30
cis-1,2-Dichloroethene
50.0
47.04
ug/L
94
70 - 130
1
30
cis-1,3-Dichloropropene
50.0
42.73
ug/L
85
70 - 130
1
20
1,2-Dibromo-3-Chloropropane
50.0
39.02
ug/L
78
70 - 130
0
30
1,2-Dibromoethane (EDB)
50.0
41.16
ug/L
82
70 - 130
4
30
Dibromomethane
50.0
45.19
ug/L
90
70 - 130
2
30
1,2-Dichlorobenzene
50.0
47.95
ug/L
96
70 - 130
0
30
1,4-Dichlorobenzene
50.0
46.39
ug/L
93
70 - 130
0
30
1,1-Dichloroethane
50.0
49.73
ug/L
99
70-130
0
30
1,2-Dichloroethane
50.0
47.00
ug/L
94
70 - 130
1
50
1,1-Dichloroethene
50.0
51.58
ug/L
103
70-130
7
20
1,2-Dichloropropane
50.0
46.94
ug/L
94
70 - 130
2
20
Ethylbenzene
50.0
45.90
ug/L
92
70 - 130
1
20
2-Hexanone
250
182.5
ug/L
73
70 - 130
5
20
lodomethane
50.0
48.35
ug/L
97
52 - 129
0
30
Methylene Chloride
50.0
42.77
ug/L
86
70 - 130
0
30
4-Methyl-2-pentanone (MIBK)
250
193.6
ug/L
77
68 - 120
5
30
Styrene
50.0
44.71
ug/L
89
70 - 130
1
30
1,1,1,2-Tetrachloroethane
50.0
47.03
ug/L
94
70-130
0
30
1,1,2,2-Tetrachloroethane
50.0
51.73
ug/L
103
70-130
1
30
Tetrachloroethene
50.0
41.33
ug/L
83
70 - 130
3
30
Toluene
50.0
42.40
ug/L
85
70 - 130
3
30
trans-1,4-Dichloro-2-butene
50.0
36.53
ug/L
73
67 - 120
1
30
trans-1,2-Dichloroethene
50.0
51.56
ug/L
103
70 - 130
1
30
trans-1,3-Dichloropropene
50.0
41.50
ug/L
83
70 - 130
1
30
1,1,1-Trichloroethane
50.0
41.15
ug/L
82
70-130
4
30
1,1,2-Trichloroethane
50.0
42.92
ug/L
86
70-130
2
30
Trichloroethene
50.0
43.66
ug/L
87
70 - 130
3
30
Trichlorofluoromethane
50.0
48.52
ug/L
97
63 - 142
28
30
1,2,3-Trichloropropane
50.0
47.35
ug/L
95
70 - 130
2
30
Vinyl acetate
100
80.36
ug/L
80
67 - 135
20
30
Vinyl chloride
50.0
53.58
ug/L
107
66 - 129
5
30
Xylenes, Total
100
91.13
ug/L
91
70 - 130
1
30
Eurofins Savannah
Page 15 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCSD 680-71861615
Matrix: Water
Analysis Batch: 718616
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 105
70 - 130
Dibromofluoromethane (Surr) 104
70 - 130
1,2-Dichloroethane-d4 (Surr) 97
60 - 124
Toluene-d8 (Surr) 104
70 - 130
F
Job ID: 680-214585-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
0
Method: 8260D SIM - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 400-576242/4
Client Sample ID: Method Blank C
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 576242
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
1,4-Dioxane
<0.300
1.00
0.300 ug/L
05/03/2217:55 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Dibromofluoromethane
102
50 - 150
05103122 17:55 1
Toluene-d8 (Surr)
88
50 - 150
05103122 17:55 1
4-Bromofluorobenzene
94
50 - 150
05103122 17:55 1
Lab Sample ID: LCS 400-576242/1002
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 576242
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier Unit
D %Rec Limits
1,4-Dioxane
10.0
10.48 ug/L
105 50 - 150
LCS LCS
Surrogate
%Recovery Qualifier
Limits
Dibromofluoromethane
101
50 - 150
Toluene-d8 (Surr)
91
50 - 150
4-Bromofluorobenzene
94
50 - 150
Lab Sample ID: 680-214585-1 MS
Client Sample ID: ELS Sump 3b 4/26/22
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 576242
Sample Sample
Spike
MS MS
%Rec
Analyte
Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
1,4-Dioxane
249
100
333.5 ug/L
85 50 - 150
MS MS
Surrogate
%Recovery Qualifier
Limits
Dibromofluoromethane
101
50 - 150
Toluene-d8 (Surr)
90
50 - 150
4-Bromofluorobenzene
94
50 - 150
Page 16 of 28
Eurofins Savannah
5/5/2022

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Method: 8260D SIM - Volatile Organic Compounds (GUMS)
(Continued)
Lab Sample ID: 680-214585-1 MSD
Client Sample ID: ELS Sump 3b 4/26/22
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 576242
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
1,4-Dioxane
249
100
374.1
ug/L
126
50 - 150 11 50
MSD MSD
Surrogate %Recovery Qualifier
Limits
Dibromofluoromethane
101
50 - 150
Toluene-d8 (Surr)
91
50 - 150
4-Bromofluorobenzene
95
50 - 150
Method: 6020B - Metals (ICP/MS)
Lab Sample ID: MB 680-718741/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718995
Prep Batch: 718741
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Antimony
<0.000520
0.00500
0.000520
mg/L
05/02/2214:01
05/03/2216:07 1
Arsenic
<0.000860
0.00300
0.000860
mg/L
05/02/2214:01
05/03/2216:07 1
Barium
<0.000890
0.00500
0.000890
mg/L
05/02/2214:01
05/03/2216:07 1
Beryllium
<0.000200
0.000500
0.000200
mg/L
05/02/2214:01
05/03/2216:07 1
Cadmium
<0.0000780
0.000500
0.0000780
mg/L
05/02/2214:01
05/03/2216:07 1
Chromium
<0.00260
0.00500
0.00260
mg/L
05/02/2214:01
05/03/2216:07 1
Cobalt
<0.000220
0.000500
0.000220
mg/L
05/02/2214:01
05/03/2216:07 1
Copper
<0.000900
0.00500
0.000900
mg/L
05/02/2214:01
05/03/2216:07 1
Lead
<0.000340
0.00250
0.000340
mg/L
05/02/2214:01
05/03/2216:07 1
Nickel
<0.00180
0.00500
0.00180
mg/L
05102/2214:01
05103/2216:07 1
Selenium
<0.00120
0.00250
0.00120
mg/L
05102/2214:01
05103/2216:07 1
Silver
<0.000390
0.00100
0.000390
mg/L
05102/2214:01
05103/2216:07 1
Thallium
<0.000260
0.00100
0.000260
mg/L
05/02/2214:01
05/03/2216:07 1
Vanadium
<0.00180
0.0100
0.00180
mg/L
05/02/2214:01
05/03/2216:07 1
Zinc
<0.0100
0.0200
0.0100
mg/L
05/02/2214:01
05/03/2216:07 1
Lab Sample ID: LCS 680-718741/2-A
Client Sample
ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718995
Prep Batch: 718741
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Antimony
0.0500
0.04957
mg/L
99
80 - 120
Arsenic
0.100
0.1002
mg/L
100
80 - 120
Barium
0.100
0.09854
mg/L
99
80 - 120
Beryllium
0.0500
0.04909
mg/L
98
80 - 120
Cadmium
0.0500
0.05042
mg/L
101
80 - 120
Chromium
0.100
0.1030
mg/L
103
80 - 120
Cobalt
0.0500
0.05227
mg/L
105
80 - 120
Copper
0.0991
0.1087
mg/L
110
80 - 120
Lead
0.505
0.4960
mg/L
98
80 - 120
Nickel
0.0990
0.1055
mg/L
107
80 - 120
Selenium
0.100
0.09475
mg/L
95
80 - 120
Silver
0.0500
0.05043
mg/L
101
80 - 120
Thallium
0.0400
0.03902
mg/L
98
80 - 120
Vanadium
0.0998
0.09934
mg/L
100
80 - 120
Eurofins Savannah
Page 17 of 28 5/5/2022

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Method: 6020B - Metals (ICP/MS) (Continued)
Lab Sample ID: LCS 680-718741/2-A
Matrix: Water
Analysis Batch: 718995
Analyte
Zinc
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 680-718743/1-A
Matrix: Water
Analysis Batch: 718940
Analyte
Mercury
Lab Sample ID: LCS 680-718743/2-A
Matrix: Water
Analysis Batch: 718940
Analyte
Mercury
Spike LCS LCS
Added Result Qualifier Unit
0.100 0.09993 mg/L
MB MB
Result Qualifier RL MDL Unit
<0.0800 0.200 0.0800 ug/L
Spike LCS LCS
Added Result Qualifier Unit
2.50 2.378 ug/L
F
Job ID: 680-214585-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718741
%Rec
D %Rec Limits
100 80 - 120
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718743
D Prepared Analyzed oil Fac
05/02/2214:18 05/03/2211:10 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718743
%Rec
D %Rec Limits
95 80 -120
Page 18 of 28
Eurofins Savannah
5/5/2022

QC Association Summary
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill
Liner Sumpa
GC/MS VOA
Analysis Batch: 576242
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
8260D SIM
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
8260D SIM
MB 400-576242/4
Method Blank
Total/NA
Water
8260D SIM
LCS 400-576242/1002
Lab Control Sample
Total/NA
Water
8260D SIM
680-214585-1 MS
ELS Sump 3b 4/26/22
Total/NA
Water
8260D SIM
680-214585-1 MSD
ELS Sump 3b 4/26/22
Total/NA
Water
8260D SIM
Analysis Batch: 718541
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
8260D
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
8260D
MB 680-718541/9
Method Blank
Total/NA
Water
8260D
LCS 680-718541/4
Lab Control Sample
Total/NA
Water
8260D
LCSD 680-718541/5
Lab Control Sample Dup
Total/NA
Water
8260D
Analysis Batch: 718616
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
8260D
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
8260D
MB 680-718616/9
Method Blank
Total/NA
Water
8260D
LCS 680-718616/4
Lab Control Sample
Total/NA
Water
8260D
LCSD 680-718616/5
Lab Control Sample Dup
Total/NA
Water
8260D
Metals
Prep Batch: 718741
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
3010A
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
3010A
MB 680-718741/1-A
Method Blank
Total/NA
Water
3010A
LCS 680-718741/2-A
Lab Control Sample
Total/NA
Water
3010A
Prep Batch: 718743
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
7470A
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
7470A
MB 680-718743/1-A
Method Blank
Total/NA
Water
7470A
LCS 680-718743/2-A
Lab Control Sample
Total/NA
Water
7470A
Analysis Batch: 718940
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
7470A
718743
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
7470A
718743
MB 680-718743/1-A
Method Blank
Total/NA
Water
7470A
718743
LCS 680-718743/2-A
Lab Control Sample
Total/NA
Water
7470A
718743
Analysis Batch: 718995
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214585-1
ELS Sump 3b 4/26/22
Total/NA
Water
6020B
718741
680-214585-2
ELS Sump 4b 4/26/22
Total/NA
Water
6020B
718741
MB 680-718741/1-A
Method Blank
Total/NA
Water
6020B
718741
Eurofins Savannah
Page 19 of 28 5/5/2022

QC Association Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Liner Sumpa
Metals (Continued)
Analysis Batch: 718995 (Continued)
Lab Sample ID Client Sample ID
LCS 680-718741/2-A Lab Control Sample
Job ID: 680-214585-1
Prep Type Matrix Method Prep Batch
Total/NA Water 6020B 718741
Eurofins Savannah
Page 20 of 28 5/5/2022

Lab Chronicle
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Client Sample ID: ELS Sump 3b 4/26/22
Lab Sample ID: 680-214585-1
Date Collected: 04/26/22 10:35
Matrix: Water
Date Received: 04/27/22 10:15
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
718616
05/02/22 18:42
P1C
TAL SAV
Instrument ID: CMSAB
Total/NA Analysis 8260D
1
5 mL
5 mL
718541
05/01/22 17:24
EMA
TAL SAV
Instrument ID: CMSB
Total/NA Analysis 8260D SIM
10
5 mL
5 mL
576242
05/03/22 19:10
PP1
TAL PEN
Instrument ID: Curie
Total/NA Prep 3010A
50 mL
250 mL
718741
05/02/22 14:01
JE
TAL SAV
Total/NA Analysis 6020B
1
718995
05/03/22 16:38
BWR
TAL SAV
Instrument ID: ICPMSD
Total/NA Prep 7470A
50 mL
50 mL
718743
05/02/22 14:18
JKL
TAL SAV
Total/NA Analysis 7470A
1
718940
05/03/22 11:43
JKL
TAL SAV
Instrument ID: QuickTrace2
Client Sample ID: ELS Sump 4b 4/26/22
Lab Sample ID: 680-214585-2
Date Collected: 04/26/22 10:50
Matrix: Water
Date Received: 04/27/22 10:15
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
718616
05/02/22 19:05
P1C
TAL SAV
Instrument ID: CMSAB
Total/NA Analysis 8260D
1
5 mL
5 mL
718541
05/01/22 17:44
EMA
TAL SAV
Instrument ID: CMSB
Total/NA Analysis 8260D SIM
50
5 mL
5 mL
576242
05/03/22 18:45
PP1
TAL PEN
Instrument ID: Curie
Total/NA Prep 3010A
50 mL
250 mL
718741
05/02/22 14:01
JE
TAL SAV
Total/NA Analysis 6020E
1
718995
05/03/22 16:41
BWR
TAL SAV
Instrument ID: ICPMSD
Total/NA Prep 7470A
50 mL
50 mL
718743
05/02/22 14:18
JKL
TAL SAV
Total/NA Analysis 7470A
1
718940
05/03/22 11:45
JKL
TAL SAV
Instrument ID: QuickTrace2
Laboratory References:
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
0
Page 21 of 28
Eurofins Savannah
5/5/2022

Accreditation/Certification Summary
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Laboratory: Eurofins Savannah
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
AFCEE
SAVLAB
Alabama
State
41450
06-30-22
Alaska (UST)
State
17-016
09-22-22
ANAB
Dept. of Defense ELAP
L2463
09-18-22
ANAB
ISO/IEC 17025
1-2463.01
09-22-22
California
State
2939
06-30-22
Florida
NELAP
E87052
06-30-22
Georgia
State
E87052
06-30-22
Georgia (DW)
State
803
06-30-22
Guam
State
19-007R
04-17-23
Hawaii
State
<cert No.>
06-30-22
Illinois
NELAP
200022
11-30-22
Indiana
State
C-GA-02
06-30-22
Iowa
State
353
07-01-23
Kentucky (UST)
State
NA
06-30-22
Louisiana
NELAP
02011
06-30-22
Louisiana (DW)
State
LA009
12-31-22
Maine
State
GA00006
09-25-22
Maryland
State
250
12-31-22
Massachusetts
State
M-GA006
06-30-22
Michigan
State
9925
06-30-22
Mississippi
State
<cert No.>
06-30-22
Nebraska
State
NE-OS-7-04
06-30-22
New Jersey
NELAP
GA769
06-30-22
New Mexico
State
GA00006
06-30-22
New York
NELAP
10842
04-01-23
North Carolina (DW)
State
13701
07-01-22
North Carolina (WW/SW)
State
269
12-31-22
Pennsylvania
NELAP
68-00474
06-30-22
Puerto Rico
State
GA00006
01-01-23
South Carolina _
State
98001
06-30-22
Tennessee
State
02961
06-30-22
Texas
NELAP
T1047004185-19-14
11-30-22
Texas _
TCEQ Water Supply
T104704185
06-30-22
USDA
US Federal Programs
P330-18-00313
09-03-24
Virginia
NELAP
10509
06-14-22
Washington
State
C805
06-10-22
Wisconsin
State
999819810
08-31-22
Wyoming
State
8TMS-L
06-30-22
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Alabama
State
40150
06-30-22
ANAB
ISO/IEC 17025
L2471
02-23-23
Arkansas DEQ
State
88-0689
09-01-22
California
State
2510
06-30-22
Florida
NELAP
E81010
06-30-22
Georgia
State
E81010(FL)
06-30-22
Eurofins Savannah
Page 22 of 28
5/5/2022

Accreditation/Certification Summary
Client: S&ME, Inc.
Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Laboratory: Eurofins Pensacola (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications
are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Illinois
NELAP
200041
10-09-22
Kansas
NELAP
E-10253
10-31-22
Kentucky (UST)
State
53
06-30-22
Kentucky (WW)
State
KY98030
12-31-22
Louisiana
NELAP
30976
06-30-22
Louisiana (DW)
State
LA017
12-31-22
Maryland
State
233
09-30-22
Massachusetts
State
M-FL094
06-30-22
Michigan
State
9912
06-30-22
North Carolina (WW/SW)
State
314
12-31-22
Oklahoma
NELAP
9810
08-31-22
Pennsylvania
NELAP
68-00467
01-31-23
South Carolina
State
96026
06-30-22
Tennessee
State
TN02907
06-30-22
Texas
NELAP
T104704286
09-30-22
US Fish & Wildlife
US Federal Programs
058448
07-31-22
USDA
US Federal Programs
P330-21-00056
05-17-24
Virginia
NELAP
460166
06-14-22
West Virginia DEP
State
136
05-31-22
Eurofins Savannah
Page 23 of 28 5/5/2022

Method Summary C
Client: S&ME, Inc. Job ID: 680-214585-1
Project/Site: Anson Landfill Liner Sumpa
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
TAL SAV
8260D SIM
Volatile Organic Compounds (GC/MS)
SW846
TAL PEN
6020B
Metals (ICP/MS)
SW846
TAL SAV
7470A
Mercury (CVAA)
SW846
TAL SAV
3010A
Preparation, Total Metals
SW846
TAL SAV
5030B
Purge and Trap
SW846
TAL SAV
5030C
Purge and Trap
SW846
TAL PEN
7470A
Preparation, Mercury
SW846
TAL SAV
Protocol References: C
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References: m
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 24 of 28 5/5/2022

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Page 26 of 28
5/5/2022

Login Sample Receipt Checklist
Client: S&ME, Inc.
Login Number: 214585
List Number: 1
Creator: Sims, Robert D
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Job Number: 680-214585-1
List Source: Eurofins Savannah
L
Eurofins Savannah
Page 27 of 28 5/5/2022

Client: S&ME, Inc.
Login Number: 214585
List Number: 2
Creator: Whitley, Adrian
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
N/A
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
2.6°C IR8
Job Number: 680-214585-1
List Source: Eurofins Pensacola
List Creation: 04/28/22 02:22 PM
Eurofins Savannah
Page 28 of 28 5/5/2022

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, May 4, 2022
S&ME, Inc. (SM011)
Attn: Lindsey Harris
644 Eastern Star Road
Kingsport, TN 37663
RE: Laboratory Results for
Project Number: 4140-15-007, Project Name/Desc: Anson LF - Leachate
ENCO Workorder(s): CF04528
Dear Lindsey Harris,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, April 27, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 9

PROJECT NARRATIVE
Date:
04May2022
Client:
S&ME, Inc. (SM011)
Project:
Anson LF - Leachate
Lab ID:
CF04528
Overview
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Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
No Comments
Quality Control Remarks
No Comments
Other Comments
2mL H2SO4 added to sample container 01 A and sample pH did not adjusted to correct method limits.
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Shahla Vakili
Project Manager
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 of 9

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-Leachate Lab ID: CF04528-01 Sampled: 04/26/22 09:35 Received: 04/27/22 10:00
Parameter Preparation Hold Date/Time(s)
EPA 351.2 Same 05/24/22
Prep Date/Time(s) Analysis Date/Time(s)
05/02/22 10:35 05/03/22 13:18
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 9

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SAMPLE DETECTION SUMMARY
Client ID: 0401-Leachate Lab ID: CF04528-01
Analvte Results Flag MDL PQL Units Method Notes
Total Kjeldahl Nitrogen 850 D 26 48 mg/L EPA 351.2
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 9

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ANALYTICAL RESULTS
Description: 0401-Leachate Lab Sample ID:CF04528-01 Received: 04/27/22 10:00
Matrix: Waste Sampled:04/26/22 09:35 Work Order: CF04528
Project: Anson LF - Leachate Sampled By: SKYLER SCHMEL
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes
Total Kjeldahl Nitrogen^ 850 D mg/L 100 26 48 2EO2014 EPA 351.2 05/03/22 13:18 MSE
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) of 9

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2EO2O14 - Same
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Blank (2E02014-BLK1) Prepared: 05/02/2022 10:35 Analyzed: 05/03/2022 13:04
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (2E02014-BS1) Prepared: 05/02/2022 10:35 Analyzed: 05/03/2022 13:06
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 99 90-110
Matrix Spike (2E02014-MS3)
Prepared: 05/02/2022 10:35 Analyzed: 05/03/2022 13:09
Source: CF04439-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
5.2
0.48
mg/L
7.20 0.79 62 90-110
QM-07
Matrix Spike (2E02014-MS2)
Prepared: 05/02/2022 10:35 Analyzed: 05/03/2022 13:14
Source: CFOSIOS-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.9
0.48
mg/L
7.20 0.83 56 90-110
QM-07
Matrix Spike Dup (2E02014-MSD1)
Prepared: 05/02/2022 10:35 Analyzed: 05/03/2022 13:11
Source: CF04439-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
3.5
0.48
mg/L
7.20 0.79 38 90-110 39
10
QM-07,
QM-11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 of 9

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 9

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Page 8 of f

Sample Preservation Verification
ENCO Cary
EI�ICC'
Work Order: CF04528
Client: S&MF, Inc. (SM011)
Lagged In: 27-Apr-22 11:02
Preservation Check Performed By:
CF04528-01
Project: Anson LF - Leachate
Project #: 4140-15-007
Logged By: Samantha
`LHyatt
Date/Time: `--t 1Z-3
Cont
Type
Pres (pH)
Requirement
pH Checked !
In Control
PH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250mLP+H2SO4
<2
Y 7 N i NA
Y 1, N/ NAtr
Reaclent Name fD
1
2
pH Strip ID: C
Rea ent Name ID
3
4
Reagent Name ID
5
6
C:IELMNTIPrintlwko_PreservationCheck.rpt Page 9 of 9

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, April 26, 2022
S&ME, Inc. (SM011)
Attn: Lindsey Harris
644 Eastern Star Road
Kingsport, TN 37663
RE: Laboratory Results for
Project Number: 4140-15-007, Project Name/Desc: Anson LF SW
ENCO Workorder(s): CF04529
Dear Lindsey Harris,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, April 15, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 29

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-BG1
Lab ID: CF04529-01
Sampled: 04/13/22 15:00
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:31
EPA 6020E
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 11:48
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 03:43
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 16:30
04/19/22 22:53
Client ID: 0401-BG2
Lab ID: CF04529-02
Sampled: 04/13/22 12:00
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:33
EPA 6020E
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 13:31
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 04:09
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 16:30
04/19/22 23:20
Client ID: 0401-SG3
Lab ID: CF04529-03
Sampled: 04/13/22 10:45
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:36
EPA 6020B
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 13:35
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 04:35
EPA 8260D
EPA 5030B_MS
04/27/22
04/19/22 16:30
04/19/22 23:48
Client ID: 0401-SG4
Lab ID: CF04529-04
Sampled: 04/13/22 13:50
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:38
EPA 6020B
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 13:41
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 05:00
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 16:30
04/20/22 00:15
Client ID: 0401-UD1
Lab ID: CF04529-05
Sampled: 04/14/22 11:10
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/11/22
04/25/22 15:12
04/26/22 10:41
EPA 6020B
EPA 3005A
10/11/22
04/18/22 02:07
04/21/22 13:45
EPA 8260D
EPA 5030B_MIS
04/28/22
04/19/22 12:59
04/20/22 05:26
EPA 8260D
EPA 503013_MS
04/28/22
04/21/22 19:08
04/22/22 10:10
Client ID: 0401-UD2
Lab ID: CF04529-06
Sampled: 04/14/22 11:35
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/11/22
04/25/22 15:12
04/26/22 10:43
EPA 6020E
EPA 3005A
10/11/22
04/18/22 02:07
04/21/22 13:50
EPA 8260D
EPA 503013_MS
04/28/22
04/19/22 12:59
04/20/22 05:52
EPA 8260D
EPA 503013_MS
04/28/22
04/21/22 19:08
04/22/22 10:38
Client ID: 0401-TRIPBLANK
Lab ID: CF04529-07
Sampled: 04/13/22 10:45
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
04/27/22
04/19/22 19:47
04/20/22 09:26
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 29

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SAMPLE DETECTION SUMMARY
Client ID: 0401-BG1
Lab ID: CF04529-01
Analvte
Results Flag MDL
PQL
Units
Method Notes
Barium - Total
44.7 1.10
10.0
ug/L
EPA 6010D
Chromium - Total
1.46 J 1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.52 J 1.40
10.0
ug/L
EPA 6010D
Copper - Total
1.78 J 1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
1.86 J 1.40
10.0
uq/L
EPA 6010D
Client ID: 0401-BG2
Lab ID:
CF04529-02
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
28.6
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.27
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
4.06
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.35
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
4.47
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.31
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
2.59
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 0401-SG3
Lab ID:
CF04529-03
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
32.2
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
2.32
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
3.43
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
2.38
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
4.40
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-SG4
Lab ID:
CF04529-04
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
45.3
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
1.63
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
2.12
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
2.13
J
1.60
10.0
ug/L
EPA 6010D
Vanadium - Total
2.62
J
1.40
10.0
uq/L
EPA 6010D
I Client ID: 0401-UD1 Lab ID: CF04529-05
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
27.9
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.02
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
94.1
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
4.40
1
2.20
10.0
ug/L
EPA 6010D
Client ID: 0401-UD2
Lab ID:
CF04529-06
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
64.1
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
5.53
1
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
4.33
1
2.20
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 29

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ANALYTICAL RESULTS
Description: 0401-BG1 Lab Sample ID:CF04529-01 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 15:00 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/19/22 22:53
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/19/22 22:53
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/19/22 22:53
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/19/22 22:53
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 4 Of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-13G1 Lab Sample ID:CF04529-01 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 15:00 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/19/22 22:53 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/19/22 22:53 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
52
1
50.0
105 %
53-136
2D19028
EPA 8260D
04119122 22:53
RKY
Dibromofluoromethane
49
1
50.0
97 %
67-129
2D19028
EPA 8260D
04119122 22:53
RKY
Toluene-c48
54
1
50.0
108 %
59-134
2D19028
EPA 8260D
04119122 22:53
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 11:48
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Barium [7440-39-3]^
44.7
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:31
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:31
JDH
Chromium [7440-47-3]^
1.46
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Cobalt[7440-48-4]^
1.52
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Copper[7440-50-8]^
1.78
J
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 11:48
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 11:48
JDH
Vanadium [7440-62-2]^
1.86
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:31
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 03:43
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.7
1
5.00
94 %
75-125
2D19038
EPA 8260D
04120122 03:43
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) Of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-BG2 Lab Sample ID:CF04529-02 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 12:00 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/19/22 23:20
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/19/22 23:20
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/19/22 23:20
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/19/22 23:20
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 6 Of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-13G2 Lab Sample ID:CF04529-02 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 12:00 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/19/22 23:20 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/19/22 23:20 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
47
1
50.0
94 %
53-136
2D19028
EPA 8260D
04119122 23:20
RKY
Dibromofluoromethane
52
1
50.0
103 %
67-129
2D19028
EPA 8260D
04119122 23:20
RKY
Toluene-c48
55
1
50.0
110 %
59-134
2D19028
EPA 8260D
04119122 23:20
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:31
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Barium [7440-39-3]^
28.6
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:33
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:33
JDH
Chromium [7440-47-3]^
2.27
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Cobalt[7440-48-4]^
4.06
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Copper[7440-50-8]^
2.35
J
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Lead [7439-92-1]^
4.47
J
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Nickel[7440-02-O]^
2.31
J
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:31
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:31
JDH
Vanadium [7440-62-2]^
2.59
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:33
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 04:09
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
99 %
75-125
2D19038
EPA 8260D
04120122 04:09
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-SG3 Lab Sample ID:CF04529-03 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 10:45 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/19/22 23:48
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/19/22 23:48
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/19/22 23:48
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/19/22 23:48
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 8 Of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-SG3 Lab Sample ID:CF04529-03 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 10:45 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/19/22 23:48 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/19/22 23:48 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
2D19028
EPA 8260D
04119122 23:48
RKY
Dibromofluoromethane
50
1
50.0
100 %
67-129
2D19028
EPA 8260D
04119122 23:48
RKY
Toluene-c48
52
1
50.0
104 %
59-134
2D19028
EPA 8260D
04119122 23:48
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:35
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Barium [7440-39-3]^
32.2
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:36
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:36
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Cobalt[7440-48-4]^
2.32
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Copper[7440-50-8]^
3.43
J
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:35
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:35
JDH
Vanadium [7440-62-2]^
2.38
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Zinc[7440-66-6]^
4.40
J
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:36
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 04:35
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D19038
EPA 8260D
04120122 0425
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-SG4 Lab Sample ID:CF04529-04 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 13:50 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/20/22
00:15
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/20/22
00:15
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/20/22
00:15
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/20/22
00:15
RKY QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
F Page 10 Of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-SG4 Lab Sample ID:CF04529-04 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/13/22 13:50 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/20/22 00:15 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/20/22 00:15 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
2D19028
EPA 8260D
04120122 00:15
RKY
Dibromofluoromethane
50
1
50.0
100 %
67-129
2D19028
EPA 8260D
04120122 00:15
RKY
Toluene-c48
51
1
50.0
102 %
59-134
2D19028
EPA 8260D
04120122 00:15
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:41
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Barium [7440-39-3]^
45.3
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:38
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:38
JDH
Chromium [7440-47-3]^
1.63
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Cobalt[7440-48-4]^
2.12
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Copper[7440-50-8]^
2.13
J
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:41
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:41
JDH
Vanadium [7440-62-2]^
2.62
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:38
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 05:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.9
1
5.00
97 %
75-125
2D19038
EPA 8260D
04120122 05:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-UD1 Lab Sample ID:CF04529-05 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/14/22 11:10 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D21036
EPA 8260D
04/22/22 10:10
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D21036
EPA 8260D
04/22/22 10:10
RKY
Benzene [71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Chlorobenzene [108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D21036
EPA 8260D
04/22/22 10:10
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 12 Of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-UD1 Lab Sample ID:CF04529-05 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/14/22 11:10 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D21036 EPA 8260D 04/22/22 10:10 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D21036 EPA 8260D 04/22/22 10:10 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
52
1
50.0
104 %
53-136
2D21036
EPA 8260D
04122122 10:10
RKY
Dibromofluoromethane
48
1
50.0
95 %
67-129
2D21036
EPA 8260D
0412212210:10
RKY
Toluene-c48
53
1
50.0
106 %
59-134
2D21036
EPA 8260D
0412212210:10
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:45
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Barium [7440-39-3]^
27.9
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:41
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:41
JDH
Chromium [7440-47-3]^
2.02
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Cobalt[7440-48-4]^
94.1
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Nickel[7440-02-O]^
4.40
J
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:45
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:45
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:41
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 05:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.8
1
5.00
96 %
75-125
2D19038
EPA 8260D
04120122 05:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-UD2 Lab Sample ID:CF04529-06 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/14/22 11:35 Work Order: CF04529
Project: Anson LF SW Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D21036
EPA 8260D
04/22/22 10:38
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D21036
EPA 8260D
04/22/22 10:38
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D21036
EPA 8260D
04/22/22 10:38
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 14 of 29

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-UD2 Lab Sample ID:CF04529-06 Received: 04/15/22 10:30
Matrix: Surface Water Sampled:04/14/22 11:35 Work Order: CF04529
Project: Anson LF SW Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D21036 EPA 8260D 04/22/22 10:38 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D21036 EPA 8260D 04/22/22 10:38 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2D21036
EPA 8260D
04122122 10:38
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2D21036
EPA 8260D
0412212210:38
RKY
Toluene-c48
54
1
50.0
108 %
59-134
2D21036
EPA 8260D
041221221038
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:50
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Barium [7440-39-3]^
64.1
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:43
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:43
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Cobalt[7440-48-4]^
5.53
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Nickel[7440-02-O]^
4.33
J
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:50
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:50
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:43
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 05:52
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D19038
EPA 8260D
04120122 05:52
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 of 29

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-TRIPBLANK Lab Sample ID: CF04529-07 Received: 04/15/22 10:30
Matrix: Water Sampled:04/13/22 10:45 Work Order: CF04529
Project: Anson LF SW Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19031
EPA 8260D
04/20/22 09:26
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19031
EPA 8260D
04/20/22 09:26
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19031
EPA 8260D
04/20/22 09:26
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 16 Of 29

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ANALYTICAL RESULTS
Description: 0401-TRIPBLANK Lab Sample ID:CF04529-07 Received: 04/15/22 10:30
Matrix: Water Sampled:04/13/22 10:45 Work Order: CF04529
Project: Anson LF SW Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19031 EPA 8260D 04/20/22 09:26 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19031 EPA 8260D 04/20/22 09:26 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
49
1
50.0
99 %
53-136
2D19031
EPA 8260D
04120122 09:26
RKY
Dibromofluoromethane
52
1
50.0
103 %
67-129
2D19031
EPA 8260D
04120122 09:26
RKY
Toluene-d8
54
1
50.0
107 %
59-134
2D19031
EPA 8260D
04120122 09:26
RKY
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2DI902B - EPA 5030B MS
Blank (2D39028-BLK1) Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 20:07
Analvte
Result
Flaq
POL
Units
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 Of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D2902B - EPA 5030B MS - Continued
Blank (2D39028-BLK1) Continued Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 20:07
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
50
u91L
50.0 99 53-136
Dibromofluoromethane
53
u91L
50.0 107 67-129
Toluene-d8
59
u91L
50.0 118 59-134
LCS (2D19028-BSI)
Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 18:16
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
96
75-133
Benzene
18
1.0
ug/L
20.0
88
80-134
Chlorobenzene
18
1.0
ug/L
20.0
88
80-120
Toluene
18
1.0
ug/L
20.0
91
71-120
Trichloroethene
18
1.0
ug/L
20.0
91
74-120
4-Bromofluorobenzene
48
u91L
50.0
96
53-136
Dibromofluoromethane
50
u91L
50.0
101
67-129
Toluene-d8
51
u91L
50.0
102
59-134
Matrix Spike (2D19028-MS1)
Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 18:44
Source: CF05306-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
94
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
95
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
95
74-120
4-Bromofluorobenzene
49
u91L
50.0
98
53-136
Dibromofluoromethane
47
u91L
50.0
95
67-129
Toluene-d8
55
u91L
50.0
109
59-134
Matrix Spike Dup (21319028-MSD1)
Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 19:12
Source: CF05306-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
95
75-133
1
20
Benzene
20
1.0
ug/L
20.0
0.15 U
99
80-134
3
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
98
80-120
3
16
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
6
17
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
86
74-120
10
22
4-Bromofluorobenzene 48 u91L 50.0 95 53-136
Dibromofluoromethane 49 u91L 50.0 99 67-129
Toluene-d8 54 u91L 50.0 108 59-134
Batch 2D19031 - EPA 5030B MS
Blank (2D39031-BLK3) Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L
1,1,1-Trichloroethane 0.12 U 1.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D29031 - EPA 5030B MS - Continued
Blank (2D39031-BLK1) Continued Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:58
Analvte
Result
Flaq
POL
Units
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
4-Bromofluorobenzene 47 u91L 50.0 95 53-136
Dibromofluoromethane 48 u91L 50.0 97 67-129
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 20 of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D29031 - EPA 5030B MS - Continued
Blank (2D39031-BLK1) Continued Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 54 u91L 50.0 107 59-134
LCS (21319031-BS1) Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 07:08
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
94
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
94
80-120
Toluene
18
1.0
ug/L
20.0
92
71-120
Trichloroethene
17
1.0
ug/L
20.0
87
74-120
4-Bromofluorobenzene
49
u91L
50.0
97
53-136
Dibromofluoromethane
49
u91L
50.0
96
67-129
Toluene-d8
53
u91L
50.0
107
59-134
Matrix Spike (21319031-MS1)
Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 07:36
Source: CF05306-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
0.21 U
83
75-133
Benzene
17
1.0
ug/L
20.0
0.15 U
87
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
90
80-120
Toluene
17
1.0
ug/L
20.0
0.14 U
86
71-120
Trichloroethene
15
1.0
ug/L
20.0
0.15 U
75
74-120
4-Bromofluorobenzene
49
u91L
50.0
99
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
52
u91L
50.0
104
59-134
Matrix Spike Dup (21319031-MS131)
Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:03
Source: CF05306-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
97
75-133
15
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
20
17
QM-11
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
106
80-120
16
16
Toluene
20
1.0
ug/L
20.0
0.14 U
99
71-120
14
17
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
33
22
QM-11
4-Bromofluorobenzene 51 u91L 50.0 101 53-136
Dibromofluoromethane 47 u91L 50.0 94 67-129
Toluene-& 54 u91L 50.0 109 59-134
Batch 2D21036 - EPA 5030B MS
Blank (2D21036-BLK3) Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:56
Spike Source %REC
Analvte
Result
Flaq
POL
Units Level Result %REC Limits
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full
Page 21 of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D21036 - EPA 5030B MS - Continued
Blank (2D21036-BLK1) Continued Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:56
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 49 u91L 50.0 97 53-136
Dibromofluoromethane 50 u91L 50.0 100 67-129
Toluene-d8 52 u91L 50.0 104 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 29

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D21036 - EPA 5030B MS - Continued
LCS (2D21036-BSI) Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 05:06
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
91
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
97
80-120
Toluene
18
1.0
ug/L
20.0
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
97
74-120
4-Bromofluorobenzene
53
u91L
50.0
105
53-136
Dibromofluoromethane
50
u91L
50.0
99
67-129
Toluene-d8
55
u91L
50.0
109
59-134
Matrix Spike (2D23036-MS1)
Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 05:33
Source: CF05306-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
91
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
97
80-120
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
93
74-120
4-Bromofluorobenzene
51
u91L
50.0
101
53-136
Dibromofluoromethane
51
u91L
50.0
102
67-129
Toluene-d8
51
u91L
50.0
102
59-134
Matrix Spike Dup (2D23036-MSD1)
Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:01
Source: CF05306-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
99
75-133
8
20
Benzene
19
1.0
ug/L
20.0
0.15 U
97
80-134
1
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
102
80-120
5
16
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
5
17
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
4
22
4-Bromofluorobenzene 51 u91L 50.0 101 53-136
Dibromofluoromethane 48 u91L 50.0 97 67-129
Toluene-d8 54 u91L 50.0 108 59-134
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D18002 - EPA 3005A
Blank (2D38002-BLK1) Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:39
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2D18002-BSI)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 29

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D28002 - EPA 3005A - Continued
LCS (2D18002-BSI) Continued Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:43
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
21.1
1.00
ug/L
20.0 106 80-120
Selenium
21.3
1.00
ug/L
20.0 106 80-120
Thallium
19.8
1.00
ug/L
20.0 99 80-120
Matrix Spike (2D18002-MS3)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:52
Source: CF04529-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
42.2
2.00
ug/L
40.0 0.740 U 105 75-125
Selenium
41.6
2.00
ug/L
40.0 1.82 U 104 75-125
Thallium
39.8
2.00
ug/L
40.0 0.220 U 100 75-125
Matrix Spike Dup (2D18002-MSD1)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:56
Source: CF04529-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
43.6
2.00
ug/L
40.0 0.740 U 109 75-125 3
20
Selenium
41.9
2.00
ug/L
40.0 1.82 U 105 75-125 0.7
20
Thallium
39.5
2.00
ug/L
40.0 0.220 U 99 75-125 0.9
20
Post Spike (2D18002-PS1)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 12:35
Source: CF04529-01
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
21.1
1.00
ug/L
20.0 0.0493 105 75-125
Selenium
19.6
1.00
ug/L
20.0 -0.167 98 75-125
Thallium
19.4
1.00
ug/L
20.0 0.00656 97 75-125
Batch 1D22018 - EPA 3005A
Blank (2D22018-BLK1)
Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 09:45
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2D22018-BSI)
Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 09:52
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Arsenic 204 10.0 ug/L 200 102 80-120
Barium 209 10.0 ug/L 200 104 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 Of 29

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D22018 - EPA 3005A - Continued
LCS (2D22018-BSI) Continued Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 09:52
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Beryllium
20.3
1.00
ug/L
20.0
101
80-120
Cadmium
20.2
1.00
ug/L
20.0
101
80-120
Chromium
203
10.0
ug/L
200
101
80-120
Cobalt
206
10.0
ug/L
200
103
80-120
Copper
203
10.0
ug/L
200
101
80-120
Lead
202
10.0
ug/L
200
101
80-120
Nickel
202
10.0
ug/L
200
101
80-120
Silver
203
10.0
ug/L
200
102
80-120
Vanadium
201
10.0
ug/L
200
101
80-120
Zinc
209
10.0
ug/L
200
104
80-120
Matrix Spike (2D22018-MS3)
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 09:55
Source: CF04526-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
208
10.0
ug/L
200
7.60 U
104
75-125
Barium
427
10.0
ug/L
200
230
99
75-125
Beryllium
20.6
1.00
ug/L
20.0
0.160 U
103
75-125
Cadmium
19.8
1.00
ug/L
20.0
0.360 U
99
75-125
Chromium
203
10.0
ug/L
200
1.40 U
102
75-125
Cobalt
202
10.0
ug/L
200
1.40 U
101
75-125
Copper
198
10.0
ug/L
200
1.60 U
99
75-125
Lead
201
10.0
ug/L
200
3.10 U
101
75-125
Nickel
200
10.0
ug/L
200
2.20 U
100
75-125
Silver
204
10.0
ug/L
200
1.90 U
102
75-125
Vanadium
202
10.0
ug/L
200
1.40 U
101
75-125
Zinc
209
10.0
ug/L
200
4.40 U
104
75-125
Matrix Spike Dup (21322018-MS131)
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 09:58
Source: CF04526-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
213
10.0
ug/L
200
7.60 U
107
75-125
2
20
Barium
437
10.0
ug/L
200
230
103
75-125
2
20
Beryllium
20.8
1.00
ug/L
20.0
0.160 U
104
75-125
1
20
Cadmium
20.2
1.00
ug/L
20.0
0.360 U
101
75-125
2
20
Chromium
207
10.0
ug/L
200
1.40 U
104
75-125
2
20
Cobalt
208
10.0
ug/L
200
1.40 U
104
75-125
3
20
Copper
201
10.0
ug/L
200
1.60 U
101
75-125
2
20
Lead
206
10.0
ug/L
200
3.10 U
103
75-125
2
20
Nickel
203
10.0
ug/L
200
2.20 U
102
75-125
2
20
Silver
206
10.0
ug/L
200
1.90 U
103
75-125
1
20
Vanadium
205
10.0
ug/L
200
1.40 U
102
75-125
2
20
Zinc
214
10.0
ug/L
200
4.40 U
107
75-125
2
20
Post Spike (2D22018-PS1)
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 10:00
Source: CF04526-05
Spike
Source %REC
RPD
Analvte Result Flaq POL Units
Level
Result %REC Limits
RPD Limit Notes
Arsenic 0.213 0.0100 mg/L
0.200
0.00662 103 80-120
Barium 0.434 0.0100 mg/L
0.200
0.230 102 80-120
FINAL This report relates only to the sample as received by the
laboratory, and
may only be reproduced in full.
Page 25 Of 29

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D2201B - EPA 3005A - Continued
Post Spike (21322018-13SI) Continued
Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 10:00
Source: CF04526-OS
Spike
Source
%REC RPD
Analvte Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Beryllium 0.0210
0.00100
mg/L
0.0200
3.39E-6
105
80-120
Cadmium 0.0206
0.00100
mg/L
0.0200
-0.000214
103
80-120
Chromium 0.207
0.0100
mg/L
0.200
0.00119
103
80-120
Cobalt 0.210
0.0100
mg/L
0.200
0.000999
104
80-120
Copper 0.202
0.0100
mg/L
0.200
-0.00108
101
80-120
Lead 0.209
0.0100
mg/L
0.200
0.000591
104
80-120
Nickel 0.205
0.0100
mg/L
0.200
0.00144
102
80-120
Silver 0.212
0.0100
mg/L
0.200
7.75E-5
106
80-120
Vanadium 0.205
0.0100
mg/L
0.200
-0.000793
103
80-120
Zinc 0.216
0.0100
mg/L
0.200
0.00437
106
80-120
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2D2903B -EPA 5030B MS
Blank (2D39038-BLK1)
Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 22:59
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-d8 4.8 u91L 5.00 96 75-125
LCS (21319038-BSI) Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 21:17
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dioxane
23
2.0
ug/L
25.0
94
80-133
Toluene-d8
5.1
u91L
5.00
103
75-125
Matrix Spike (2D19038-MS1)
Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 21:42
Source: AF03107-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dioxane
23
2.0
ug/L
25.0
0.80 U
90
80-133
Toluene-c48 4.9 u91L 5.00 97 75-125
Matrix Spike Dup (21319038-MS131) Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 22:08
Source: AF03107-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 22 2.0 ug/L 25.0 0.80 U 89 80-133 2 19
Toluene-d8 4.8 u91L 5.00 97 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 Of 29

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www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 of 29

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29

Sample Preservation Verification
ENCO Cary
ENCO
Work Order: CF04529
Client: S&ME, Inc. (SM011)
Logged In: 15-Apr-22 11:47
Preservation Check Performed By.
CF04529-01
Project:
Anson LF SW
Project #.
4140-15-007
Logged By:
Rachel Ann o`nis
Date/Time: i
Cont
Type
Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted Date me
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y / N ! NA
Y (N) NA
CF04529-02
Cont
T e
yP
Pres (pH)
Requirement
pH Checked i
in Control
Date/Time
pH Adjusted Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2
Y / N / NA
TY (N NA
CF04529-03
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N/ NA
Y N NA
C F04529-04
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comment,-
A
250mLP+HNO3
<2
Y N / NA
Y NA
C F04529 -05
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
LnatelTime
pH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y) N / NA
1' 1 `N ) NA
CF04529-06
Cont
Type
ties (pH)
Requirement
pH Checked 1
In Control
pH Adjusted Date/Tim
Adjusted
Reagent Used/Comments
A
25QmLP+HNO3
<2
YY IN NA
Y N NA
Reaclent Name Fp
1
2
pH strip IDPH Strips C2A0640
Rea ent Name ID
3
4
Reagent Name IG
5
6
CaeimntlPrin[\WKo_rreservaTionuneCK.rpt I Page 29 of 29

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-214576-1
Client Project/Site: Anson Landfill Leachate POTW
Revision: 3
Fir-
S&ME, Inc.
Attn Accounts Payable
644 Eastern Star Rd
Kingsport, Tennessee 37663
Attn: Lindsey Harris
Authorized for release by:
6/3/2022 4:13:05 PM
Noel Savoie, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
A Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
MIL Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 680-214576-1
Eurofins Savannah
Page 2 of 38 6/3/2022 (Rev. 3)

Client: S&ME, Inc. Sample Summary Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Lab Sample ID Client Sample ID Matrix Collected Received
680-214576-1 Leachate Water 04/26/22 09:35 04/27/22 10:15
Page 3 of 38 Eurq)BOPY 3)

Case Narrative
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Job ID: 680-214576-1
Laboratory: Eurofins Savannah
Narrative
Job ID: 680-214576-1
0
Job Narrative
680-214576-1
Comments
No additional comments.
Revision
The report being provided is a revision of the original report sent on 5/16/2022. The report (revision 2) is being revised due to: client
requested the lab run pH on an unpreserved sample.
The report (revision 3) is being revised due to provide results for Nitrate -Nitrite that were not reported originally.
Receipt
The sample was received on 4/27/2022 10:15 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 4.21 C.
Receipt Exceptions
Container arrived marked for 420.1 analysis. Analysis not selected on COC
Logged per COC.
GC/MS VOA
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 680-718624.
Method 8260D SIM: The following sample was diluted to bring the concentration of target analytes within the calibration range: Leachate
(680-214576-1). Elevated reporting limits (RLs) are provided.
Method 8260D SIM: The following sample was collected in a properly preserved vial; however, the pH was outside the required criteria
when verified by the laboratory. The sample was analyzed within the 7-day holding time specified for unpreserved samples: Leachate
(680-214576-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
HPLC/IC
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
Method 7470A: The following samples for metals were received unpreserved and were preserved upon receipt to the laboratory: Leachate
(680-214576-1). Regulatory documents require a 24-hour waiting period from the time of the addition of the acid preservative to the time
of digestion.
Method 7470A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 680-718823. A LCS/LCSD was performed instead.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method 353.2: The reference method requires samples to be preserved to a pH of <2. The following sample(s) was received with
insufficient preservation at a pH of: 7. The sample(s) was preserved to the appropriate pH in the laboratory.
Method 901213: Sample tested positive for nitrate/nitrite prior to analysis: Leachate (680-214576-1)
Method SM 5220D: COD results may be biased high due to chloride interference for the following sample: Leachate (680-214576-1).
Methods 1664A, 1664B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 680-718993.
Eurofins Savannah
Page 4 of 38 6/3/2022 (Rev. 3)

Case Narrative
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Job ID: 680-214576-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
Job ID: 680-214576-1
0
Method 1664B: The reference method requires samples to be preserved to a pH of <2. The following sample was received with
insufficient preservation at a pH of 6: Leachate (680-214576-1). The sample(s) was preserved to the appropriate pH in the laboratory
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 5 of 38 6/3/2022 (Rev. 3)

Client Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Client Sample ID: Leachate
Lab Sample ID: 680-214576-1
Date Collected: 04/26/22 09:35
Matrix:
Water
Date Received: 04/27/22 10:15
Method: 8260D SIM - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,4-Dioxane
159
5.00
1.50
ug/L
05/03/2219:35
5
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
Dibromofluoromethane
102
50 - 150
05/03/22 19:35
5
Toluene-d8 (Surr)
90
50 - 150
05103122 19:35
5
4-Bromofluorobenzene
95
50 - 150
05103122 19:35
5
Method: 8260D - Volatile Organic
Compounds by GC/MS
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.360
1.00
0.360
ug/L
05/01/22 17:05
1
1,1,1-Trichloroethane
<0.210
1.00
0.210
ug/L
05/01/22 17:05
1
1,1,2,2-Tetrachloroethane
<0.400
1.00
0.400
ug/L
05/01/22 17:05
1
1,1,2-Trichloroethane
<0.320
1.00
0.320
ug/L
05/01/22 17:05
1
1,1-Dichloroethane
<0.330
1.00
0.330
ug/L
05/01/22 17:05
1
1,1-Dichloroethene
<0.330
1.00
0.330
ug/L
05/01/22 17:05
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/01/22 17:05
1
1,2-Dibromo-3-Chloropropane
<1.80
5.00
1.80
ug/L
05/01/22 17:05
1
1,2-Dibromoethane (EDB)
<0.330
1.00
0.330
ug/L
05/01/22 17:05
1
1,2-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/01/22 17:05
1
1,2-Dichloroethane
<0.250
1.00
0.250
ug/L
05/01/22 17:05
1
1,2-Dichloropropane
<0.220
1.00
0.220
ug/L
05/01/22 17:05
1
1,4-Dichlorobenzene
0.481 J
1.00
0.310
ug/L
05/01/22 17:05
1
2-Hexanone
4.48 J
10.0
3.20
ug/L
05/01/22 17:05
1
4-Methyl-2-pentanone (MIBK)
19.8
10.0
2.70
ug/L
05/01/22 17:05
1
Acrylonitrile
<5.50
20.0
5.50
ug/L
05/01/22 17:05
1
Benzene
<0.270
1.00
0.270
ug/L
05/01/22 17:05
1
Bromochloromethane
<0.340
1.00
0.340
ug/L
05/01/22 17:05
1
Bromodichloromethane
<0.250
1.00
0.250
ug/L
05/01/22 17:05
1
Bromoform
<0.590
1.00
0.590
ug/L
05/01/22 17:05
1
Bromomethane
<3.70
5.00
3.70
ug/L
05/01/22 17:05
1
Carbon disulfide
<0.430
2.00
0.430
ug/L
05/01/22 17:05
1
Carbon tetrachloride
<0.300
1.00
0.300
ug/L
05/01/22 17:05
1
Chlorobenzene
<0.150
1.00
0.150
ug/L
05/01/22 17:05
1
Chlorodibromomethane
<0.390
1.00
0.390
ug/L
05/01/22 17:05
1
Chloroethane
<4.60
5.00
4.60
ug/L
05/01/22 17:05
1
Chloroform
<0.270
1.00
0.270
ug/L
05/01/22 17:05
1
Chloromethane
<0.540
1.00
0.540
ug/L
05/01/22 17:05
1
cis-1,2-Dichloroethene
<0.250
1.00
0.250
ug/L
05/01/22 17:05
1
cis-1,3-Dichloropropene
<0.260
1.00
0.260
ug/L
05/01/22 17:05
1
Dibromomethane
<0.340
1.00
0.340
ug/L
05/01/22 17:05
1
Ethylbenzene
1.75
1.00
0.200
ug/L
05/01/22 17:05
1
lodomethane
<3.90
10.0
3.90
ug/L
05/01/22 17:05
1
Methylene Chloride
<3.20
5.00
3.20
ug/L
05/01/22 17:05
1
Styrene
<0.270
1.00
0.270
ug/L
05/01/22 17:05
1
Tetrachloroethene
<0.350
0.500
0.350
ug/L
05/01/22 17:05
1
Toluene
5.49
1.00
0.250
ug/L
05/01/22 17:05
1
trans-1,2-Dichloroethene
<0.340
1.00
0.340
ug/L
05/01/22 17:05
1
trans- 1,3-Dichloropropene
<0.230
1.00
0.230
ug/L
05/01/22 17:05
1
trans-1,4-Dichloro-2-butene
<1.25
2.00
1.25
ug/L
05/01/22 17:05
1
Trichloroethene
<0.200
1.00
0.200
ug/L
05/01/22 17:05
1
Eurofins Savannah
Page 6 of 38 6/3/2022 (Rev. 3)

Client Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Job ID: 680-214576-1
Client Sample ID: Leachate Lab Sample ID: 680-214576-1
Date Collected: 04/26/22 09:35 Matrix: Water
Date Received: 04/27/22 10:15
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/01/22 17:05
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/01/22 17:05
1
Vinyl chloride
<0.400
1.00
0.400
ug/L
05/01/22 17:05
1
Xylenes, Total
4.69
1.00
0.230
ug/L
05/01/22 17:05
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
95
60- 124
05101122 17:05
1
4-Bromofluorobenzene (Surr)
100
70 - 130
05101122 17:05
1
Dibromofluoromethane (Surr)
101
70 - 130
05101122 17:05
1
Toluene-d8 (Surr)
109
70 - 130
05101122 17:05
1
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
2-Butanone (MEK)
1940
100
64.0
ug/L
05/02/22 20:30
10
Acetone
2890
100
37.0
ug/L
05/02/22 20:30
10
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
103
60- 124
05102122 20:30
10
4-Bromofluorobenzene (Surr)
119
70 - 130
05102122 20:30
10
Dibromofluoromethane (Surr)
101
70 - 130
05102122 20:30
10
Toluene-d8 (Surr)
101
70 - 130
05102122 20:30
10
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
2840
25.0
10.0
mg/L
05/04/2213:01
25
Method: 6020B - Metals (ICP/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Antimony
0.0466
0.00500
0.000520
mg/L
04/29/2211:53
05/02/2214:52
1
Arsenic
0.249
0.00300
0.000860
mg/L
04/29/2211:53
05/02/2214:52
1
Barium
1.59
0.00500
0.000890
mg/L
04/29/2211:53
05/02/2214:52
1
Beryllium
0.000290
J
0.000500
0.000200
mg/L
04/29/2211:53
05/02/2214:52
1
Cadmium
0.000340
J
0.000500
0.0000780
mg/L
04/29/2211:53
05/02/2214:52
1
Chromium
0.512
0.00500
0.00260
mg/L
04/29/2211:53
05/02/2214:52
1
Cobalt
0.0567
0.000500
0.000220
mg/L
04/29/2211:53
05/02/2214:52
1
Copper
0.0847
0.00500
0.000900
mg/L
04/29/2211:53
05/02/2214:52
1
Lead
0.00660
0.00250
0.000340
mg/L
04/29/2211:53
05/02/2214:52
1
Nickel
0.447
0.00500
0.00180
mg/L
04/29/2211:53
05/02/2214:52
1
Selenium
0.00600
0.00250
0.00120
mg/L
04/29/2211:53
05/02/2214:52
1
Silver
<0.000390
0.00100
0.000390
mg/L
04/29/2211:53
05/02/2214:52
1
Thallium
<0.000260
0.00100
0.000260
mg/L
04/29/2211:53
05/02/2214:52
1
Vanadium
0.440
0.0100
0.00180
mg/L
04/29/2211:53
05/02/2214:52
1
Zinc
0.0911
0.0200
0.0100
mg/L
04/29/2211:53
05/02/2214:52
1
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
<0.0000800
0.000200
0.0000800
mg/L
05/03/22 08:39
05/03/22 14:43
1
General Chemistry
Analyte
Result
Qualifier
NONE
NONE
Unit
D
Prepared
Analyzed
Dil Fac
pH
8.5
HF
Su
05/18/2210:00
1
Eurofins Savannah
Page 7 of 38 6/3/2022 (Rev. 3)

Client Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Job ID: 680-214576-1
Client Sample ID: Leachate Lab Sample ID: 680-214576-1
Date Collected: 04/26/22 09:35 Matrix: Water
Date Received: 04/27/22 10:15
Analyte
Result Qualifier
Oil & Grease
11.4
Kjeldahl Nitrogen as N
884
Nitrate Nitrite as N
0.188
Phosphorus, Total
8.71
Cyanide, Total
0.0217
Ammonia
370
Phenolics, Total Recoverable
2.09
Chemical Oxygen Demand
4180
Analyte
Result Qualifier
Biochemical Oxygen Demand
708
Total Suspended Solids
69.0
Method: Field Sampling - Field Sampling
Analyte
Result Qualifier
Field pH
1.33
Field Temperature
27.4
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
4.9
1.4
mg/L
05/04/22 07:14
05/04/22 09:55
1
200
100
mg/L
04/28/22 13:22
04/30/22 09:10
100
0.0500
0.0100
mg/L
05/03/2211:21
1
1.00
0.410
mg/L
04/28/2213:22
04/29/2213:21
1
0.0100
0.00250
mg/L
04/28/2210:57
04/28/2219:57
1
50.0
20.0
mg/L
04/28/22 09:26
04/28/22 14:07
200
0.250
0.125
mg/L
05/02/2211:53
05/02/2217:03
5
1000
500
mg/L
04/29/2214:48
100
RL
RL
Unit
D Prepared
Analyzed
Dil Fac
2.00
2.00
mg/L
04/27/2213:38
1
12.5
12.5
mg/L
04/28/2216:19
1
NONE
NONE
Unit
D Prepared
Analyzed
Dil Fac
su
04/26/22 09:35
1
Degrees C
04/26/22 09:35
1
Eurofins Savannah
Page 8 of 38 6/3/2022 (Rev. 3)

Volatile Organic Compounds by GC/MS
8260D
M, pica . -
1,1,1,2-Tetrachloroethane
630-20-6
1,1,1-Trichloroethane
71-55-6
1,1,2,2-Tetrachloroethane
79-34-5
1,1,2-Trichloroethane
79-00-5
1,1-Dichloroethane
75-34-3
1,1-Dichloroethene
75-35-4
1,2,3-Trichloropropane
96-18-4
1,2-Dibromo-3-Chloro ro ane
96-12-8
1,2-Dibromoethane (EDB)
106-934
1,2-Dichlorobenzene
95-50-1
1,2-Dichloroethane
107-06-2
1,2-Dichloropropane
78-87-5
1,4-Dichlorobenzene
106-46-7
2-Butanone (MEK)
78-93-3
2-Hexanone
591-78-6
4-Meth I-2- entanone MIBK
108-10-1
Acetone
67-64-1
Acrylonitrile
107-13-1
Benzene
71-43-2
Bromochloromethane
74-97-5
Bromodichloromethane
75-27-4
Bromoform
75-25-2
Bromomethane
74-83-9
Carbon disulfide
75-15-0
Carbon tetrachloride
56-23-5
Chlorobenzene
108-90-7
Chlorodibromomethane
124-48-1
Chloroethane
75-00-3
Chloroform
67-66-3
Chloromethane
74-87-3
cis-1,2-Dichloroethene
156-59-2
cis-1,3-Dichloropropene
10061-01-5
Dibromomethane
74-95-3
Ethylbenzene
100-41-4
lodomethane
74-88-4
Methylene Chloride
75-09-2
Styrene
100-42-5
Tetrachloroethene
127-18-4
Toluene
108-88-3
trans-1,2-Dichloroethene
156-60-5
trans-1,3-Dichloro ro ene
10061-02-6
trans-1,4-Dichloro-2-butene
110-57-6
Trichloroethene
79-01-6
Trichlorofluoromethane
75-69-4
Vinyl acetate
108-05-4
Vinyl chloride
75-01-4
Xylenes, Total
1330-20-7
1,2-Dichloroethane-d4 Surr
17060-07-0
4-Bromofluorobenzene (Surr)
460-00-4
Dibromofluoromethane (Surr)
1868-53-7
Toluene-d8 Surr
2037-26-5
Metals ICP/MS
6020B
Antimony
7440-36-0
Arsenic
7440-38-2
Barium
7440-39-3
Beryllium
7440-41-7
Cadmium
7440-43-9
Chromium
7440-47-3
Cobalt
744048-4
Copper
7440-50-8
Lead
7439-92-1
Nickel
7440-02-0
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
Page 9 of 38 6/3/2022 (Rev. 3)

17439-97-6
Mercury CVAA
7470A
iMercury
BOD, 5-Day
15210B
I Biochemical Oxygen Demand
STL00311
COD
15220D
lChemical Oxygen Demand
ISTL00070
Nitrogen, Nitrate -Nitrite
1353.2_Pres
INitrate Nitrite as N
ISTLOO217
Nitrogen, Ammonia
1350.1
jAmmonia
7664-41-7
C anide, Total andor Amenable
19012B
lCyanide, Total
57-12-5
Phenolics, Total Recoverable
1420.1
1 Phenolics, Total Recoverable
ISTLOO166
Phosphorus, Total
1365.4
1 Phosphorus, Total
7723-14-0
Anions, Ion Chromatography
1300_ORGFM_28D
ISulfate
14808-79-8
Nitrogen, Total Kieldahl
1351.2
1 Kieldahl Nitrogen as N
ISTLOO296
HEM and SGT-HEM
11664B
1011 & Grease
ISTLOO181
Solids, Total Suspended (TSS)
12540D
I Total Suspended Solids
ISTLOO161
Volatile Organic Compounds (GC/MS)
8260D_SIM
1,4-Dioxane
123-91-1
Fluorobenzene
462-06-6
Chlorobenzene-d5
3114-55-4
1,4-Dichlorobenzene-d4
3855-82-1
Dibromofluoromethane
1868-53-7
Toluene-d8 (Surr)
2037-26-5
4-Bromofluorobenzene
460-00-4
Page 10 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds by GUMS
Lab Sample ID: MB 680-718541/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.360
1.00
0.360
ug/L
05/01/22 13:37
1
1,1,1-Trichloroethane
<0.210
1.00
0.210
ug/L
05/01/22 13:37
1
1,1,2,2-Tetrachloroethane
<0.400
1.00
0.400
ug/L
05/01/22 13:37
1
1,1,2-Trichloroethane
<0.320
1.00
0.320
ug/L
05/01/22 13:37
1
1,1-Dichloroethane
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,1-Dichloroethene
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/01/22 13:37
1
1,2-Dibromo-3-Chloropropane
<1.80
5.00
1.80
ug/L
05/01/22 13:37
1
1,2-Dibromoethane (EDB)
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
1,2-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/01/22 13:37
1
1,2-Dichloroethane
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
1,2-Dichloropropane
<0.220
1.00
0.220
ug/L
05/01/22 13:37
1
1,4-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/01/22 13:37
1
2-Butanone (MEK)
<6.40
10.0
6.40
ug/L
05/01/22 13:37
1
2-Hexanone
<3.20
10.0
3.20
ug/L
05/01/22 13:37
1
4-Methyl-2-pentanone (MIBK)
<2.70
10.0
2.70
ug/L
05/01/22 13:37
1
Acetone
<3.70
10.0
3.70
ug/L
05/01/22 13:37
1
Acrylonitrile
<5.50
20.0
5.50
ug/L
05/01/22 13:37
1
Benzene
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
Bromochloromethane
<0.340
1.00
0.340
ug/L
05/01/22 13:37
1
Bromodichloromethane
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
Bromoform
<0.590
1.00
0.590
ug/L
05/01/22 13:37
1
Bromomethane
<3.70
5.00
3.70
ug/L
05/01/22 13:37
1
Carbon disulfide
<0.430
2.00
0.430
ug/L
05/01/22 13:37
1
Carbon tetrachloride
<0.300
1.00
0.300
ug/L
05/01/22 13:37
1
Chlorobenzene
<0.150
1.00
0.150
ug/L
05/01/22 13:37
1
Chlorodibromomethane
<0.390
1.00
0.390
ug/L
05/01/22 13:37
1
Chloroethane
<4.60
5.00
4.60
ug/L
05/01/22 13:37
1
Chloroform
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
Chloromethane
<0.540
1.00
0.540
ug/L
05/01/22 13:37
1
cis-1,2-Dichloroethene
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
cis-1,3-Dichloropropene
<0.260
1.00
0.260
ug/L
05/01/22 13:37
1
Dibromomethane
<0.340
1.00
0.340
ug/L
05/01/22 13:37
1
Ethylbenzene
<0.200
1.00
0.200
ug/L
05/01/22 13:37
1
lodomethane
<3.90
10.0
3.90
ug/L
05/01/22 13:37
1
Methylene Chloride
<3.20
5.00
3.20
ug/L
05/01/22 13:37
1
Styrene
<0.270
1.00
0.270
ug/L
05/01/22 13:37
1
Tetrachloroethene
<0.350
0.500
0.350
ug/L
05/01/22 13:37
1
Toluene
<0.250
1.00
0.250
ug/L
05/01/22 13:37
1
trans- 1,2-Dichloroethene
<0.340
1.00
0.340
ug/L
05/01/22 13:37
1
trans- 1,3-Dichloropropene
<0.230
1.00
0.230
ug/L
05/01/22 13:37
1
trans- 1,4-Dichloro-2-butene
<1.25
2.00
1.25
ug/L
05/01/22 13:37
1
Trichloroethene
<0.200
1.00
0.200
ug/L
05/01/22 13:37
1
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/01/22 13:37
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/01/22 13:37
1
Vinyl chloride
<0.400
1.00
0.400
ug/L
05/01/22 13:37
1
Xylenes, Total
<0.230
1.00
0.230
ug/L
05/01/22 13:37
1
0
Eurofins Savannah
Page 11 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 680-718541/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 90
60- 124
05101122 13:37 1 •
4-Bromofluorobenzene (Surr) 103
70 - 130
05101122 13:37 1
Dibromofluoromethane (Surr) 101
70 - 130
05101122 13:37 1
Toluene-d8 (Surr) 110
70 - 130
05101122 13:37 1
Lab Sample ID: LCS 680-718541/4
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
53.54
ug/L
107
70-130
1,1,1-Trichloroethane
50.0
43.22
ug/L
86
70-130
1,1,2,2-Tetrachloroethane
50.0
48.69
ug/L
97
70-130
1,1,2-Trichloroethane
50.0
50.50
ug/L
101
70-130
1,1-Dichloroethane
50.0
45.36
ug/L
91
70-130
1,1-Dichloroethene
50.0
42.92
ug/L
86
70-130
1,2,3-Trichloropropane
50.0
51.05
ug/L
102
70-130
1,2-Dibromo-3-Chloropropane
50.0
50.69
ug/L
101
70 -130
1,2-Dibromoethane (EDB)
50.0
51.48
ug/L
103
70 -130
1,2-Dichlorobenzene
50.0
52.37
ug/L
105
70 -130
1,2-Dichloroethane
50.0
49.55
ug/L
99
70 -130
1,2-Dichloropropane
50.0
49.82
ug/L
100
70 -130
1,4-Dichlorobenzene
50.0
51.62
ug/L
103
70 -130
2-Butanone (MEK)
250
217.7
ug/L
87
69 -120
2-Hexanone
250
235.3
ug/L
94
70 -130
4-Methyl-2-pentanone (MIBK)
250
248.7
ug/L
99
68-120
Acetone
250
204.1
ug/L
82
67-120
Acrylonitrile
500
457.7
ug/L
92
70 -130
Benzene
50.0
47.74
ug/L
95
70-130
Bromochloromethane
50.0
48.72
ug/L
97
70 -130
Bromodichloromethane
50.0
48.32
ug/L
97
70 -130
Bromoform
50.0
50.81
ug/L
102
69 -129
Bromomethane
50.0
51.64
ug/L
103
28 -192
Carbon disulfide
50.0
40.77
ug/L
82
70 -130
Carbon tetrachloride
50.0
46.76
ug/L
94
70 -130
Chlorobenzene
50.0
51.39
ug/L
103
70 -130
Chlorodibromomethane
50.0
49.42
ug/L
99
70 -130
Chloroethane
50.0
54.47
ug/L
109
31 - 213
Chloroform
50.0
47.53
ug/L
95
70 -130
Chloromethane
50.0
41.61
ug/L
83
59 -127
cis-1,2-Dichloroethene
50.0
47.34
ug/L
95
70 -130
cis-1,3-Dichloropropene
50.0
51.87
ug/L
104
70 -130
Dibromomethane
50.0
48.79
ug/L
98
70 -130
Ethylbenzene
50.0
51.38
ug/L
103
70 -130
lodomethane
50.0
42.62
ug/L
85
52 -129
Methylene Chloride
50.0
43.05
ug/L
86
70 -130
Styrene
50.0
51.96
ug/L
104
70 -130
Tetrachloroethene
50.0
51.54
ug/L
103
70 -130
Eurofins Savannah
Page 12 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID:
680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds
by GUMS (Continued)
Lab Sample ID: LCS 680-718541/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
Toluene
50.0
49.96
ug/L
100
70 -130
•
trans- 1,2-Dichloroethene
50.0
43.05
ug/L
86
70-130
trans- 1,3-Dichloropropene
50.0
53.53
ug/L
107
70-130
trans- 1,4-Dichloro-2-butene
50.0
46.46
ug/L
93
67-120
Trichloroethene
50.0
50.31
ug/L
101
70 -130
Trichlorofluoromethane
50.0
52.74
ug/L
105
63 -142
Vinyl acetate
100
103.0
ug/L
103
67 -135
Vinyl chloride
50.0
43.49
ug/L
87
66 -129
Xylenes, Total
100
99.61
ug/L
100
70 -130
LCS LCS
Surrogate %Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 99
60- 124
4-Bromofluorobenzene (Surr) 97
70 - 130
Dibromofluoromethane (Surr) 98
70 - 130
Toluene-d8 (Surr) 104
70 - 130
Lab Sample ID: LCSD 680-718541/5
Client Sample
ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCSD
LCSD
%Rec
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
1,1,1,2-Tetrachloroethane
50.0
54.67
ug/L
109
70-130
2
30
1,1,1-Trichloroethane
50.0
44.15
ug/L
88
70-130
2
30
1,1,2,2-Tetrachloroethane
50.0
49.16
ug/L
98
70-130
1
30
1,1,2-Trichloroethane
50.0
51.24
ug/L
102
70-130
1
30
1,1-Dichloroethane
50.0
45.88
ug/L
92
70-130
1
30
1,1-Dichloroethene
50.0
44.05
ug/L
88
70-130
3
20
1,2,3-Trichloropropane
50.0
52.54
ug/L
105
70-130
3
30
1,2-Dibromo-3-Chloropropane
50.0
52.10
ug/L
104
70-130
3
30
1,2-Dibromoethane(EDB)
50.0
52.20
ug/L
104
70-130
1
30
1,2-Dichlorobenzene
50.0
52.76
ug/L
106
70 -130
1
30
1,2-Dichloroethane
50.0
50.61
ug/L
101
70 -130
2
50
1,2-Dichloropropane
50.0
50.42
ug/L
101
70 -130
1
20
1,4-Dichlorobenzene
50.0
52.04
ug/L
104
70 -130
1
30
2-Butanone (MEK)
250
227.9
ug/L
91
69 -120
5
30
2-Hexanone
250
242.1
ug/L
97
70 -130
3
20
4-Methyl-2-pentanone (MIBK)
250
253.7
ug/L
101
68-120
2
30
Acetone
250
210.7
ug/L
84
67-120
3
30
Acrylonitrile
500
465.7
ug/L
93
70 -130
2
30
Benzene
50.0
48.34
ug/L
97
70 -130
1
30
Bromochloromethane
50.0
49.04
ug/L
98
70 -130
1
30
Bromodichloromethane
50.0
49.37
ug/L
99
70 -130
2
30
Bromoform
50.0
51.33
ug/L
103
69 -129
1
30
Bromomethane
50.0
54.04
ug/L
108
28 -192
5
30
Carbon disulfide
50.0
41.59
ug/L
83
70 -130
2
30
Carbon tetrachloride
50.0
48.08
ug/L
96
70 -130
3
30
Chlorobenzene
50.0
51.95
ug/L
104
70 -130
1
30
Chlorodibromomethane
50.0
49.83
ug/L
100
70 -130
1
30
Eurofins Savannah
Page 13 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate
POTW
Method: 8260D - Volatile
Organic Compounds by GUMS (Continued)
Lab Sample ID: LCSD 680-718541/5
Client Sample ID: Lab Control Sample
Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718541
Spike
LCSD LCSD
%Rec
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD
Limit
Chloroethane
50.0
56.92
ug/L
114
31 - 213 4
30
•
Chloroform
50.0
48.25
ug/L
97
70 -130 2
30
Chloromethane
50.0
42.76
ug/L
86
59 -127 3
30
cis-1,2-Dichloroethene
50.0
47.81
ug/L
96
70 -130 1
30
cis-1,3-Dichloropropene
50.0
52.79
ug/L
106
70 -130 2
20
Dibromomethane
50.0
48.95
ug/L
98
70 -130 0
30
Ethylbenzene
50.0
52.26
ug/L
105
70 -130 2
20
lodomethane
50.0
42.75
ug/L
86
52 -129 0
30
Methylene Chloride
50.0
43.77
ug/L
88
70 -130 2
30
Styrene
50.0
53.20
ug/L
106
70 -130 2
30
Tetrachloroethene
50.0
53.10
ug/L
106
70 -130 3
30
Toluene
50.0
50.70
ug/L
101
70 -130 1
30
trans- 1,2-Dichloroethene
50.0
43.51
ug/L
87
70-130 1
30
trans- 1,3-Dichloropropene
50.0
53.89
ug/L
108
70-130 1
30
trans- 1,4-Dichloro-2-butene
50.0
47.54
ug/L
95
67-120 2
30
Trichloroethene
50.0
51.59
ug/L
103
70 -130 3
30
Trichlorofluoromethane
50.0
53.06
ug/L
106
63 -142 1
30
Vinyl acetate
100
105.9
ug/L
106
67 -135 3
30
Vinyl chloride
50.0
44.24
ug/L
88
66 -129 2
30
Xylenes, Total
100
101.0
ug/L
101
70 -130 1
30
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
100
60- 124
4-Bromofluorobenzene (Surr)
98
70 - 130
Dibromofluoromethane (Surr)
99
70 - 130
Toluene-d8 (Surr)
106
70 - 130
Lab Sample ID: MB 680-718624/10
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718624
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.360
1.00
0.360
ug/L
05/02/22 14:01
1
1,1,1-Trichloroethane
<0.210
1.00
0.210
ug/L
05/02/22 14:01
1
1,1,2,2-Tetrachloroethane
<0.400
1.00
0.400
ug/L
05/02/22 14:01
1
1,1,2-Trichloroethane
<0.320
1.00
0.320
ug/L
05/02/22 14:01
1
1,1-Dichloroethane
<0.330
1.00
0.330
ug/L
05/02/22 14:01
1
1,1-Dichloroethene
<0.330
1.00
0.330
ug/L
05/02/22 14:01
1
1,2,3-Trichloropropane
<0.480
1.00
0.480
ug/L
05/02/22 14:01
1
1,2-Dibromo-3-Chloropropane
<1.80
5.00
1.80
ug/L
05/02/22 14:01
1
1,2-Dibromoethane (EDB)
<0.330
1.00
0.330
ug/L
05/02/22 14:01
1
1,2-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/02/22 14:01
1
1,2-Dichloroethane
<0.250
1.00
0.250
ug/L
05/02/22 14:01
1
1,2-Dichloropropane
<0.220
1.00
0.220
ug/L
05/02/22 14:01
1
1,4-Dichlorobenzene
<0.310
1.00
0.310
ug/L
05/02/22 14:01
1
2-Butanone (MEK)
<6.40
10.0
6.40
ug/L
05/02/22 14:01
1
2-Hexanone
<3.20
10.0
3.20
ug/L
05/02/22 14:01
1
4-Methyl-2-pentanone (MIBK)
<2.70
10.0
2.70
ug/L
05/02/22 14:01
1
Eurofins Savannah
Page 14 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic
Compounds by GUMS (Continued)
Lab Sample ID: MB 680-718624/10
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718624
MB
MB
Analyte
Result
Qualifier RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Acetone
<3.70
10.0
3.70
ug/L
05/02/22 14:01
1
Acrylonitrile
<5.50
20.0
5.50
ug/L
05/02/22 14:01
1
Benzene
<0.270
1.00
0.270
ug/L
05/02/22 14:01
1
Bromochloromethane
<0.340
1.00
0.340
ug/L
05/02/22 14:01
1
Bromodichloromethane
<0.250
1.00
0.250
ug/L
05/02/22 14:01
1
Bromoform
<0.590
1.00
0.590
ug/L
05/02/22 14:01
1
Bromomethane
<3.70
5.00
3.70
ug/L
05/02/22 14:01
1
Carbon disulfide
<0.430
2.00
0.430
ug/L
05/02/22 14:01
1
Carbon tetrachloride
<0.300
1.00
0.300
ug/L
05/02/22 14:01
1
Chlorobenzene
<0.150
1.00
0.150
ug/L
05/02/22 14:01
1
Chlorodibromomethane
<0.390
1.00
0.390
ug/L
05/02/22 14:01
1
Chloroethane
<4.60
5.00
4.60
ug/L
05/02/22 14:01
1
Chloroform
<0.270
1.00
0.270
ug/L
05/02/22 14:01
1
Chloromethane
<0.540
1.00
0.540
ug/L
05/02/22 14:01
1
cis-1,2-Dichloroethene
<0.250
1.00
0.250
ug/L
05/02/22 14:01
1
cis-1,3-Dichloropropene
<0.260
1.00
0.260
ug/L
05/02/22 14:01
1
Dibromomethane
<0.340
1.00
0.340
ug/L
05/02/22 14:01
1
Ethylbenzene
<0.200
1.00
0.200
ug/L
05/02/22 14:01
1
lodomethane
<3.90
10.0
3.90
ug/L
05/02/22 14:01
1
Methylene Chloride
<3.20
5.00
3.20
ug/L
05/02/22 14:01
1
Styrene
<0.270
1.00
0.270
ug/L
05/02/22 14:01
1
Tetrachloroethene
<0.350
0.500
0.350
ug/L
05/02/22 14:01
1
Toluene
<0.250
1.00
0.250
ug/L
05/02/22 14:01
1
trans- 1,2-Dichloroethene
<0.340
1.00
0.340
ug/L
05/02/22 14:01
1
trans- 1,3-Dichloropropene
<0.230
1.00
0.230
ug/L
05/02/22 14:01
1
trans- 1,4-Dichloro-2-butene
<1.25
2.00
1.25
ug/L
05/02/22 14:01
1
Trichloroethene
<0.200
1.00
0.200
ug/L
05/02/22 14:01
1
Trichlorofluoromethane
<0.330
1.00
0.330
ug/L
05/02/22 14:01
1
Vinyl acetate
<0.690
2.00
0.690
ug/L
05/02/22 14:01
1
Vinyl chloride
<0.400
1.00
0.400
ug/L
05/02/22 14:01
1
Xylenes, Total
<0.230
1.00
0.230
ug/L
05/02/22 14:01
1
MB
MB
Surrogate %Recovery
Qualifier Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
104
60- 124
05102122 14:01
1
4-Bromofluorobenzene (Surr)
113
70 - 130
05102122 14:01
1
Dibromofluoromethane (Surr)
102
70 - 130
05102122 14:01
1
Toluene-d8 (Surr)
101
70 - 130
05102122 14:01
1
Lab Sample ID: LCS 680-718624/5
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718624
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
51.71
ug/L 103
70-130
1,1,1-Trichloroethane
50.0
53.14
ug/L 106
70-130
1,1,2,2-Tetrachloroethane
50.0
53.03
ug/L 106
70-130
1,1,2-Trichloroethane
50.0
50.90
ug/L 102
70-130
1,1-Dichloroethane
50.0
50.83
ug/L 102
70-130
Eurofins Savannah
Page 15 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 680-718624/5
Matrix: Water
Analysis Batch: 718624
Job ID: 680-214576-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
50.0
51.04
ug/L
102
70-130
1,2,3-Trichloropropane
50.0
54.11
ug/L
108
70-130
1,2-Dibromo-3-Chloropropane
50.0
52.92
ug/L
106
70-130
1,2-Dibromoethane(EDB)
50.0
52.05
ug/L
104
70-130
1,2-Dichlorobenzene
50.0
54.44
ug/L
109
70 -130
1,2-Dichloroethane
50.0
50.85
ug/L
102
70 -130
1,2-Dichloropropane
50.0
52.77
ug/L
106
70 -130
1,4-Dichlorobenzene
50.0
51.23
ug/L
102
70 -130
2-Butanone (MEK)
250
224.3
ug/L
90
69 -120
2-Hexanone
250
246.0
ug/L
98
70-130
4-Methyl-2-pentanone (MIBK)
250
242.6
ug/L
97
68-120
Acetone
250
230.6
ug/L
92
67-120
Acrylonitrile
500
470.0
ug/L
94
70 -130
Benzene
50.0
50.62
ug/L
101
70-130
Bromochloromethane
50.0
50.10
ug/L
100
70 -130
Bromodichloromethane
50.0
55.27
ug/L
111
70 -130
Bromoform
50.0
52.88
ug/L
106
69 -129
Bromomethane
50.0
50.73
ug/L
101
28 -192
Carbon disulfide
50.0
52.26
ug/L
105
70 -130
Carbon tetrachloride
50.0
53.96
ug/L
108
70 -130
Chlorobenzene
50.0
49.92
ug/L
100
70 -130
Chlorodibromomethane
50.0
53.91
ug/L
108
70 -130
Chloroethane
50.0
47.07
ug/L
94
31 - 213
Chloroform
50.0
52.13
ug/L
104
70 -130
Chloromethane
50.0
54.62
ug/L
109
59 -127
cis-1,2-Dichloroethene
50.0
52.19
ug/L
104
70 -130
cis-1,3-Dichloropropene
50.0
54.01
ug/L
108
70 -130
Dibromomethane
50.0
50.92
ug/L
102
70 -130
Ethylbenzene
50.0
52.31
ug/L
105
70 -130
lodomethane
50.0
48.73
ug/L
97
52 -129
Methylene Chloride
50.0
48.11
ug/L
96
70 -130
Styrene
50.0
52.22
ug/L
104
70 -130
Tetrachloroethene
50.0
47.63
ug/L
95
70 -130
Toluene
50.0
51.51
ug/L
103
70 -130
trans- 1,2-Dichloroethene
50.0
50.21
ug/L
100
70-130
trans- 1,3-Dichloropropene
50.0
55.27
ug/L
111
70-130
trans- 1,4-Dichloro-2-butene
50.0
55.43
ug/L
111
67-120
Trichloroethene
50.0
49.62
ug/L
99
70 -130
Trichlorofluoromethane
50.0
53.82
ug/L
108
63 -142
Vinyl acetate
100
108.1
ug/L
108
67 -135
Vinyl chloride
50.0
54.86
ug/L
110
66 -129
Xylenes, Total
100
101.6
ug/L
102
70 -130
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1, 2-Dichloroethane-d4 (Surr)
99
60 -124
4-Bromofluorobenzene (Surr)
110
70 -130
Dibromofluoromethane (Surr)
102
70 -130
Toluene-d8 (Surr)
100
70 - 130
0
Eurofins Savannah
Page 16 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID:
680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCSD 680-718624/6
Client Sample
ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718624
Spike
LCSD
LCSD
%Rec
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
1,1,1,2-Tetrachloroethane
50.0
51.24
ug/L
102
70-130
1
30
1,1,1-Trichloroethane
50.0
53.40
ug/L
107
70-130
0
30
1,1,2,2-Tetrachloroethane
50.0
52.80
ug/L
106
70-130
0
30
1,1,2-Trichloroethane
50.0
52.05
ug/L
104
70-130
2
30
1,1-Dichloroethane
50.0
50.64
ug/L
101
70-130
0
30
1,1-Dichloroethene
50.0
50.74
ug/L
101
70-130
1
20
1,2,3-Trichloropropane
50.0
53.24
ug/L
106
70-130
2
30
1,2-Dibromo-3-Chloropropane
50.0
53.34
ug/L
107
70-130
1
30
1,2-Dibromoethane(EDB)
50.0
52.10
ug/L
104
70-130
0
30
1,2-Dichlorobenzene
50.0
54.87
ug/L
110
70 -130
1
30
1,2-Dichloroethane
50.0
47.46
ug/L
95
70 -130
7
50
1,2-Dichloropropane
50.0
52.47
ug/L
105
70 -130
1
20
1,4-Dichlorobenzene
50.0
53.11
ug/L
106
70 -130
4
30
2-Butanone (MEK)
250
210.4
ug/L
84
69 -120
6
30
2-Hexanone
250
243.9
ug/L
98
70-130
1
20
4-Methyl-2-pentanone (MIBK)
250
241.7
ug/L
97
68-120
0
30
Acetone
250
220.4
ug/L
88
67 -120
4
30
Acrylonitrile
500
453.6
ug/L
91
70 -130
4
30
Benzene
50.0
50.62
ug/L
101
70 -130
0
30
Bromochloromethane
50.0
49.45
ug/L
99
70 -130
1
30
Bromodichloromethane
50.0
54.78
ug/L
110
70 -130
1
30
Bromoform
50.0
54.18
ug/L
108
69 -129
2
30
Bromomethane
50.0
52.63
ug/L
105
28 -192
4
30
Carbon disulfide
50.0
52.72
ug/L
105
70 -130
1
30
Carbon tetrachloride
50.0
53.94
ug/L
108
70 -130
0
30
Chlorobenzene
50.0
49.41
ug/L
99
70 -130
1
30
Chlorodibromomethane
50.0
53.79
ug/L
108
70 -130
0
30
Chloroethane
50.0
49.13
ug/L
98
31 - 213
4
30
Chloroform
50.0
51.97
ug/L
104
70 -130
0
30
Chloromethane
50.0
54.48
ug/L
109
59 -127
0
30
cis-1,2-Dichloroethene
50.0
51.63
ug/L
103
70 -130
1
30
cis-1,3-Dichloropropene
50.0
52.89
ug/L
106
70 -130
2
20
Dibromomethane
50.0
50.13
ug/L
100
70 -130
2
30
Ethylbenzene
50.0
51.83
ug/L
104
70 -130
1
20
lodomethane
50.0
51.39
ug/L
103
52 -129
5
30
Methylene Chloride
50.0
48.28
ug/L
97
70 -130
0
30
Styrene
50.0
53.25
ug/L
107
70 -130
2
30
Tetrachloroethene
50.0
48.25
ug/L
97
70 -130
1
30
Toluene
50.0
50.86
ug/L
102
70 -130
1
30
trans- 1,2-Dichloroethene
50.0
50.03
ug/L
100
70-130
0
30
trans- 1,3-Dichloropropene
50.0
54.33
ug/L
109
70-130
2
30
trans- 1,4-Dichloro-2-butene
50.0
54.99
ug/L
110
67-120
1
30
Trichloroethene
50.0
49.64
ug/L
99
70 -130
0
30
Trichlorofluoromethane
50.0
52.87
ug/L
106
63 -142
2
30
Vinyl acetate
100
97.07
ug/L
97
67 -135
11
30
Vinyl chloride
50.0
54.83
ug/L
110
66 -129
0
30
Xylenes, Total
100
101.2
ug/L
101
70 -130
0
30
Eurofins Savannah
Page 17 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCSD 680-718624/6
Matrix: Water
Analysis Batch: 718624
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
98
60-124
4-Bromofluorobenzene (Surr)
109
70 - 130
Dibromofluoromethane (Surr)
102
70 - 130
Toluene-d8 (Surr)
102
70- 130
Method: 8260D SIM - Volatile Organic Compounds (GC/MS)
Job ID: 680-214576-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Lab Sample ID: MB 400-576242/4
Matrix: Water
Analysis Batch: 576242
MB MB
Analyte Result Qualifier RL MDL Unit D
1,4-Dioxane <0.300 1.00 0.300 ug/L
MB MB
Surrogate %Recovery Qualifier Limits
Dibromofluoromethane 102 50 - 150
Toluene-d8 (Surr) 88 50 - 150
4-Bromofluorobenzene 94 50 - 150
- E
Client Sample ID: Method Blank F
Prep Type: Total/NA
Prepared Analyzed
Dil Fac
05/03/22 17:55
1
Prepared Analyzed
DU Fac
05103122 17.55
1
05103122 17.55
1
05103122 17.55
1
Lab Sample ID: LCS 400-576242/1002 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 576242
Spike
LCS LCS
Analyte
Added
Result Qualifier Unit
1,4-Dioxane
10.0
10.48 ug/L
LCS LCS
Surrogate %Recovery Qualifier
Limits
Dibromofluoromethane
101
50 -150
Toluene-d8 (Surr)
91
50 - 150
4-Bromofluorobenzene
94
50 - 150
Method: 300.0 - Anions, Ion Chromatography
Lab Sample ID: MB 680-719080/2
Matrix: Water
Analysis Batch: 719080
MB MB
Analyte
Result Qualifier
RL MDL Unit D
Sulfate
<0.400
1.00 0.400 mg/L
%Rec
D %Rec Limits
105 50-150
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
05/04/22 10:27 1
Lab Sample ID: LCS 680-719080/3 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 719080
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfate 10.0 9.445 mg/L 94 90 -110
Eurofins Savannah
Page 18 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Method: 300.0 - Anions, Ion Chromatography (Continued)
Lab Sample ID: LCSD 680-719080/4
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 719080
Spike
LCSD LCSD
%Rec RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Sulfate
10.0
9.697
mg/L
97
90 -110 3 15 Y
Method: 6020B - Metals (ICP/MS)
Lab Sample ID: MB 680-718369/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718842
Prep Batch: 718369
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Antimony <0.000520
0.00500
0.000520
mg/L
04/29/2211:53
05/02/2214:34 1
Arsenic <0.000860
0.00300
0.000860
mg/L
04/29/2211:53
05/02/2214:34 1
Barium <0.000890
0.00500
0.000890
mg/L
04/29/2211:53
05/02/2214:34 1
Beryllium <0.000200
0.000500
0.000200
mg/L
04/29/2211:53
05/02/2214:34 1
Cadmium <0.0000780
0.000500
0.0000780
mg/L
04/29/2211:53
05/02/2214:34 1
Chromium <0.00260
0.00500
0.00260
mg/L
04/29/2211:53
05/02/2214:34 1
Cobalt <0.000220
0.000500
0.000220
mg/L
04/29/2211:53
05/02/2214:34 1
Copper <0.000900
0.00500
0.000900
mg/L
04/29/2211:53
05/02/2214:34 1
Lead <0.000340
0.00250
0.000340
mg/L
04/29/2211:53
05/02/2214:34 1
Nickel <0.00180
0.00500
0.00180
mg/L
04/29/2211:53
05/02/2214:34 1
Selenium <0.00120
0.00250
0.00120
mg/L
04/29/2211:53
05/02/2214:34 1
Silver <0.000390
0.00100
0.000390
mg/L
04/29/2211:53
05/02/2214:34 1
Thallium <0.000260
0.00100
0.000260
mg/L
04/29/2211:53
05/02/2214:34 1
Vanadium <0.00180
0.0100
0.00180
mg/L
04/29/2211:53
05/02/2214:34 1
Zinc <0.0100
0.0200
0.0100
mg/L
04/29/2211:53
05/02/2214:34 1
Lab Sample ID: LCS 680-718369/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718842
Prep Batch: 718369
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Antimony
0.0500
0.05042
mg/L
101
80 -120
Arsenic
0.100
0.1010
mg/L
101
80 -120
Barium
0.100
0.09744
mg/L
97
80-120
Beryllium
0.0500
0.05208
mg/L
104
80 -120
Cadmium
0.0500
0.05067
mg/L
101
80 -120
Chromium
0.100
0.1024
mg/L
102
80 -120
Cobalt
0.0500
0.05295
mg/L
106
80 -120
Copper
0.0991
0.1085
mg/L
109
80 -120
Lead
0.505
0.5046
mg/L
100
80 -120
Nickel
0.0990
0.1060
mg/L
107
80 -120
Selenium
0.100
0.09742
mg/L
97
80 -120
Silver
0.0500
0.05173
mg/L
103
80 -120
Thallium
0.0400
0.03929
mg/L
98
80-120
Vanadium
0.0998
0.1010
mg/L
101
80 -120
Zinc
0.100
0.1003
mg/L
100
80 -120
Eurofins Savannah
Page 19 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 680-718823/1-A
Matrix: Water
Analysis Batch: 718940
MB MB
Analyte Result Qualifier
Mercury <0.0000800
Lab Sample ID: LCS 680-718823/2-A
Matrix: Water
Analysis Batch: 718940
Analyte
Mercury
Lab Sample ID: LCSD 680-718823/3-A
Matrix: Water
Analysis Batch: 718940
Analyte
Mercury
Method: 1664B - HEM and SGT-HEM
Job ID: 680-214576-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718823
RL MDL Unit D Prepared Analyzed Dil Fac
0.000200 0.0000800 mg/L 05/03/22 08:39 05/03/22 14:30 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718823
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
0.00250 0.002461 mg/L 98 80 -120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 718823
Spike LCSD LCSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.00250 0.002475 mg/L 99 80 -120 1 20
Lab Sample ID: MB 680-718993/1-A
Matrix: Water
Analysis Batch: 719044
MB
MB
Analyte Result
Qualifier
Oil & Grease <1.4
Lab Sample ID: LCS 680-718993/2-A
Matrix: Water
Analysis Batch: 719044
Spike
Added
�Analyte
Oil & Grease
40.0
Lab Sample ID: LCSD 680-718993/3-A
Matrix: Water
Analysis Batch: 719044
Spike
Analyte
Added
Oil & Grease
40.0
Method: 351.2_ASP - Total Kjedahl Nitrogen
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718993
RL MDL Unit D Prepared Analyzed Dil Fac
5.0 1.4 mg/L 05/04/22 07:14 05/04/22 09:55 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718993
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
38.40 mg/L 96 78 -114
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 718993
LCSD LCSD %Rec RPD
Result Qualifier Unit D %Rec Limits RPD Limit
38.40 mg/L 96 78 -114 0 18
Lab Sample ID: MB 680-718222/13-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 718487 Prep Batch: 718222
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Kjeldahl Nitrogen as N <0.100 0.200 0.100 mg/L 04/28/22 13:22 04/29/22 13:36 1
Eurofins Savannah
Page 20 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
F
Job ID: 680-214576-1
Method: 351.2 ASP - Total Kjedahl Nitrogen (Continued)
Lab Sample ID: LCS 680-718222/14-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 718487 Prep Batch: 718222
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
LKjeldahl Nitrogen as N 2.00 1.834 mg/L 92 75-125
Method: 353.2 - Nitrogen, Nitrate -Nitrite
Lab Sample ID: MB 680-718891/14
Matrix: Water
Analysis Batch: 718891
MB MB
Analyte Result Qualifier RL
Nitrate Nitrite as N <0.0100 0.0500
FLab Sample ID: LCS 680-718891/17
Matrix: Water
Analysis Batch: 718891
Spike
Analyte Added
Nitrate Nitrite as N 1.00
Client Sample ID: Method Blank
Prep Type: Total/NA
F
MDL Unit D Prepared Analyzed Dil Fac
0.0100 mg/L 05/03/2211:10 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
Result Qualifier Unit
0.9930 mg/L
%Rec
D %Rec Limits
99 90-110
Method: 365.4 - Total Phosphorus
FLab Sample ID: MB 680-718222/13-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718489
Prep Batch: 718222
MB
MB
Analyte Result
Qualifier RL MDL Unit
D Prepared Analyzed Dil Fac
Phosphorus, Total <0.0410
0.100 0.0410 mg/L
04/28/22 13:22 04/29/22 12:47 1
Lab Sample ID: LCS 680-718222/14-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718489
Prep Batch: 718222
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier
Unit D %Rec Limits
Phosphorus, Total
2.00 2.102
mg/L 105 90-110
Method: 4500 H+ B-2011 - pH
Lab Sample ID: LCS 680-721403/3
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 721403
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier
Unit D %Rec Limits
7.01 7.1
SU 101 63-158
LpH
Method: 5210B ASP - CBOD
FLab Sample ID: USB 680-717941/4
Matrix: Water
Analysis Batch: 717941
USB USB
Analyte Result Qualifier
Biochemical Oxygen Demand <2.00
Client Sample ID: Method Blank
Prep Type: Total/NA
RL RL Unit D Prepared Analyzed Dil Fac
2.00 2.00 mg/L 04/27/2212:42 1
Eurofins Savannah
Page 21 of 38 6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Method: 521013 ASP - CBOD
Lab Sample ID: LCS 680-717941/5
Matrix: Water
Analysis Batch: 717941
Analyte
Biochemical Oxygen Demand
Lab Sample ID: LCSD 680-717941/6
Matrix: Water
Analysis Batch: 717941
Analyte
Biochemical Oxygen Demand
Job ID: 680-214576-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
LCS
Result
LCS
Qualifier Unit
D %Rec
%Rec
Limits
198
189.2
mg/L
96
85 - 115
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec RPD
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
198
183.2
mg/L
93
85 -115 3 30
Method: 9012B - Cyanide, Total andor Amenable
Lab Sample ID: MB 680-718193/12-A
Matrix: Water
Analysis Batch: 718286
MB MB
Analyte Result Qualifier RL
Cyanide, Total <0.00250 0.0100
FLab Sample ID: LCS 680-718193/13-A
Matrix: Water
Analysis Batch: 718286
Analyte
Cyanide, Total
Method: EPA 350.1 -Ammonia
Lab Sample ID: MB 680-718139/1-A
Matrix: Water
Analysis Batch: 718234
MB MB
Analyte Result Qualifier
Ammonia <0.100
Lab Sample ID: LCS 680-718139/3-A
Matrix: Water
Analysis Batch: 718234
Analyte
Ammonia
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718193
MDL Unit D Prepared Analyzed Dil Fac
0.00250 mg/L 04/28/2210:56 04/28/2219:41 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718193
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
0.0500 0.04633 mg/L 93 85 -115
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718139
RL MDL Unit D Prepared Analyzed Dil Fac
0.250 0.100 mg/L 04/28/22 09:26 04/28/22 12:09 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 718139
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
1.00 0.9209 mg/L 92 90 -1 00
Method: EPA 420.1 - Phenolics, Total Recoverable
Lab Sample ID: MB 680-718701/1-A
Matrix: Water
Analysis Batch: 718772
MB MB
Analyte Result Qualifier RL
[Phenolics, Total Recoverable <0.0250 0.0500
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 718701
MDL Unit D Prepared Analyzed Dil Fac
0.0250 mg/L 05/02/2211:53 05/02/2216:35 1
Page 22 of 38
Eurofins Savannah
6/3/2022 (Rev. 3)

QC Sample Results
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
F
Job ID: 680-214576-1
Method: EPA 420.1 - Phenolics, Total Recoverable (Continued)
Lab Sample ID: LCS 680-718701/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 718772 Prep Batch: 718701
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Phenolics, Total Recoverable 0.100 0.1113 mg/L 111 75-125
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-718256/1
Matrix: Water
Analysis Batch: 718256
MB MB
Analyte Result Qualifier RL RL Unit
Total Suspended Solids <2.50 2.50 2.50 mg/L
Lab Sample ID: LCS 680-718256/2
Matrix: Water
Analysis Batch: 718256
Client Sample ID: Method Blank
Prep Type: Total/NA
F
D Prepared Analyzed Dil Fac
04/28/22 16:19 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Total Suspended Solids
951
786.0
mg/L
83 80 -120
FLab Sample ID: LCSD 680-718256/3
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718256
Spike
LCSD
LCSD
%Rec RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Total Suspended Solids
951
830.0
mg/L
87 60- 220 5 25
Method: SM 5220D - COD
Lab Sample ID: MB 680-718419/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718419
MB
MB
Analyte Result
Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Chemical Oxygen Demand <5.00
10.0
5.00 mg/L
04/29/22 14:48 1
Lab Sample ID: LCS 680-718419/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 718419
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Chemical Oxygen Demand
50.0
46.10
mg/L
92 90-110
Eurofins Savannah
Page 23 of 38 6/3/2022 (Rev. 3)

QC Association Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
GC/MS VOA
Analysis Batch: 576242
Lab Sample ID
Client Sample ID
680-214576-1
Leachate
MB 400-576242/4
Method Blank
LCS 400-576242/1002
Lab Control Sample
Analysis Batch: 718541
Lab Sample ID
Client Sample ID
680-214576-1
Leachate
MB 680-718541/9
Method Blank
LCS 680-718541/4
Lab Control Sample
LCSD 680-718541/5
Lab Control Sample Dup
Analysis Batch: 718624
Lab Sample ID
Client Sample ID
680-214576-1 - DL
Leachate
MB 680-718624/10
Method Blank
LCS 680-718624/5
Lab Control Sample
LCSD 680-718624/6
Lab Control Sample Dup
HPLC/IC
Analysis Batch: 719080
Lab Sample ID
Client Sample ID
680-214576-1
Leachate
MB 680-719080/2
Method Blank
LCS 680-719080/3
Lab Control Sample
LCSD 680-719080/4
Lab Control Sample Dup
Metals
Prep Batch: 718369
Job ID: 680-214576-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8260D SIM
Total/NA
Water
8260D SIM
Total/NA Water 8260D SIM
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8260D
Total/NA
Water
8260D
Total/NA
Water
8260D
Total/NA
Water
8260D
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8260D
Total/NA
Water
8260D
Total/NA
Water
8260D
Total/NA
Water
8260D
Prep Type
Matrix
Method
Total/NA
Water
300.0
Total/NA
Water
300.0
Total/NA
Water
300.0
Total/NA
Water
300.0
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-214576-1
Leachate
Total/NA
Water
3010A
MB 680-718369/1-A
Method Blank
Total/NA
Water
3010A
LCS 680-718369/2-A
Lab Control Sample
Total/NA
Water
3010A
Prep Batch: 718823
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-214576-1
Leachate
Total/NA
Water
7470A
MB 680-718823/1-A
Method Blank
Total/NA
Water
7470A
LCS 680-718823/2-A
Lab Control Sample
Total/NA
Water
7470A
LCSD 680-718823/3-A
Lab Control Sample Dup
Total/NA
Water
7470A
Analysis Batch: 718842
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
6020B
718369
MB 680-718369/1-A
Method Blank
Total/NA
Water
6020B
718369
LCS 680-718369/2-A
Lab Control Sample
Total/NA
Water
6020B
718369
Analysis Batch: 718940
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
7470A
718823
MB 680-718823/1-A
Method Blank
Total/NA
Water
7470A
718823
Page 24 of 38
Eurofins Savannah
6/3/2022 (Rev. 3)

QC Association Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Metals (Continued)
Analysis Batch: 718940 (Continued)
Lab Sample ID Client Sample ID
LCS 680-718823/2-A Lab Control Sample
LCSD 680-718823/3-A Lab Control Sample Dup
General Chem
Prep Type Matrix
Total/NA Water
Total/NA Water
Job ID: 680-214576-1
Method Prep Batch
7470A 718823
7470A 718823
Analysis Batch: 717941
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
5210B ASP
USB 680-717941/4
Method Blank
Total/NA
Water
5210B_ASP
LCS 680-717941/5
Lab Control Sample
Total/NA
Water
5210B_ASP
LCSD 680-717941/6
Lab Control Sample Dup
Total/NA
Water
5210B_ASP
Prep Batch: 718139
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
Distill/Ammonia
MB 680-718139/1-A
Method Blank
Total/NA
Water
Distill/Ammonia
LCS 680-718139/3-A
Lab Control Sample
Total/NA
Water
Distill/Ammonia
Prep Batch: 718193
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
9012B
MB 680-718193/12-A
Method Blank
Total/NA
Water
9012B
LCS 680-718193/13-A
Lab Control Sample
Total/NA
Water
9012B
Prep Batch: 718222
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
Digestion
MB 680-718222/13-A
Method Blank
Total/NA
Water
Digestion
LCS 680-718222/14-A
Lab Control Sample
Total/NA
Water
Digestion
Analysis Batch: 718234
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
EPA 350.1
718139
MB 680-718139/1-A
Method Blank
Total/NA
Water
EPA 350.1
718139
LCS 680-718139/3-A
Lab Control Sample
Total/NA
Water
EPA 350.1
718139
Analysis Batch: 718256
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
SM 2540D
MB 680-718256/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-718256/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-718256/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 718286
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
9012B
718193
MB 680-718193/12-A
Method Blank
Total/NA
Water
9012B
718193
LCS 680-718193/13-A
Lab Control Sample
Total/NA
Water
9012B
718193
Page 25 of 38
Eurofins Savannah
6/3/2022 (Rev. 3)

QC Association Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
General Chemistry
Analysis Batch: 718419
Job ID: 680-214576-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
SM 5220D
MB 680-718419/3
Method Blank
Total/NA
Water
SM 5220D
LCS 680-718419/4
Lab Control Sample
Total/NA
Water
SM 5220D
Analysis Batch: 718487
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
351.2_ASP
718222
MB 680-718222/13-A
Method Blank
Total/NA
Water
351.2_ASP
718222
LCS 680-718222/14-A
Lab Control Sample
Total/NA
Water
351.2_ASP
718222
Analysis Batch: 718489
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
365.4
718222
MB 680-718222/13-A
Method Blank
Total/NA
Water
365.4
718222
LCS 680-718222/14-A
Lab Control Sample
Total/NA
Water
365.4
718222
Prep Batch: 718701
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
Distill/Phenol
MB 680-718701/1-A
Method Blank
Total/NA
Water
Distill/Phenol
LCS 680-718701/2-A
Lab Control Sample
Total/NA
Water
Distill/Phenol
Analysis Batch: 718772
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
EPA 420.1
718701
MB 680-718701/1-A
Method Blank
Total/NA
Water
EPA420.1
718701
LCS 680-718701/2-A
Lab Control Sample
Total/NA
Water
EPA420.1
718701
Analysis Batch: 718891
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
353.2
MB 680-718891/14
Method Blank
Total/NA
Water
353.2
LCS 680-718891/17
Lab Control Sample
Total/NA
Water
353.2
Prep Batch: 718993
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
1664B
MB 680-718993/1-A
Method Blank
Total/NA
Water
1664B
LCS 680-718993/2-A
Lab Control Sample
Total/NA
Water
1664B
LCSD 680-718993/3-A
Lab Control Sample Dup
Total/NA
Water
1664B
Analysis Batch: 719044
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
1664B
718993
MB 680-718993/1-A
Method Blank
Total/NA
Water
1664B
718993
LCS 680-718993/2-A
Lab Control Sample
Total/NA
Water
1664B
718993
LCSD 680-718993/3-A
Lab Control Sample Dup
Total/NA
Water
1664B
718993
Analysis Batch: 721403
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-214576-1
Leachate
Total/NA
Water
4500 H+ B-2011
Eurofins Savannah
Page 26 of 38 6/3/2022 (Rev. 3)

QC Association Summary C
Client: S&ME, Inc. Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
General Chemistry (Continued)
Analysis Batch: 721403 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
LCS 680-721403/3 Lab Control Sample Total/NA Water 4500 H+ B-2011
Field Service / Mobile Lab
Analysis Batch: 718080
Lab Sample ID Client Sample ID
680-214576-1 Leachate
Prep Type Matrix Method Prep Batch
Total/NA Water Field Sampling 9
F
F
Page 27 of 38
Eurofins Savannah
6/3/2022 (Rev. 3)

Lab Chronicle
Client: S&ME, Inc.
Job ID:
680-214576-1
Project/Site: Anson Landfill Leachate POTW
Client Sample
ID: Leachate
Lab
Sample ID: 680-214576-1
Date Collected: 04/26/22
09:35
Matrix: Water
Date Received: 04/27/22 10:15
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA
Analysis 8260D
1
5 mL
5 mL
718541
05/01/22 17:05
EMA
TAL SAV
Instrument ID: CMSB
Total/NA
Analysis 8260D DL
10
5 mL
5 mL
718624
05/02/22 20:30
P1 C
TAL SAV
Instrument ID: CMSU
Total/NA
Analysis 8260D SIM
5
5 mL
5 mL
576242
05/03/22 19:35
PP1
TAL PEN
Instrument ID: Curie
•
Total/NA
Analysis 300.0
25
5 mL
5 mL
719080
05/04/22 13:01
OK
TAL SAV
Instrument ID: CICK
Total/NA
Prep 3010A
50 mL
250 mL
718369
04/29/22 11:53
JE
TAL SAV
Total/NA
Analysis 6020B
1
718842
05/02/22 14:52
BWR
TAL SAV
Instrument ID: ICPMSD
Total/NA
Prep 7470A
50 mL
50 mL
718823
05/03/22 08:39
JKL
TAL SAV
Total/NA
Analysis 7470A
1
718940
05/03/22 14:43
JKL
TAL SAV
Instrument ID: QuickTrace2
Total/NA
Prep 1664B
508 mL
500 mL
718993
05/04/22 07:14
JAS
TAL SAV
Total/NA
Analysis 1664B
1
719044
05/04/22 09:55
JAS
TAL SAV
Instrument ID: NoEquip
Total/NA
Prep Digestion
2 mL
20 mL
718222
04/28/22 13:22
SM
TAL SAV
Total/NA
Analysis 351.2_ASP
100
718487
04/30/22 09:10
NVF
TAL SAV
Instrument ID: SEAL 2
Total/NA
Analysis 353.2
1
2 mL
2 mL
718891
05/03/22 11:21
MB
TAL SAV
Instrument ID: LACHAT2
Total/NA
Prep Digestion
2 mL
20 mL
718222
04/28/22 13:22
SM
TAL SAV
Total/NA
Analysis 365.4
1
718489
04/29/22 13:21
NVF
TAL SAV
Instrument ID: SEAL 2
Total/NA
Analysis 4500 H+ B-2011
1
721403
05/18/22 10:00
DR
TAL SAV
Instrument ID: MANTECH 2
Total/NA
Analysis 521 OB_ASP
1
717941
04/27/22 13:38
OLB
TAL SAV
Instrument ID: BOD 2
Total/NA
Prep 9012B
6 mL
6 mL
718193
04/28/22 10:57
NVF
TAL SAV
Total/NA
Analysis 9012B
1
718286
04/28/22 19:57
NVF
TAL SAV
Instrument ID: KONELAB4
Total/NA
Prep Distill/Ammonia
6 mL
6 mL
718139
04/28/22 09:26
DR
TAL SAV
Total/NA
Analysis EPA 350.1
200
2 mL
2 mL
718234
04/28/22 14:07
DR
TAL SAV
Instrument ID: KONELAB1
Total/NA
Prep Distill/Phenol
6 mL
6 mL
718701
05/02/22 11:53
SM
TAL SAV
Total/NA
Analysis EPA 420.1
5
6 mL
6 mL
718772
05/02/22 17:03
SM
TAL SAV
Instrument ID: KONELA133
Total/NA
Analysis SM 2540D
1
200 mL
1000 mL
718256
04/28/22 16:19
PG
TAL SAV
Instrument ID: NOEQUIP
Total/NA
Analysis SM 5220D
100
2 mL
2 mL
718419
04/29/22 14:48
ALG
TAL SAV
Instrument ID: SPC7
Total/NA
Analysis Field Sampling
1
718080
04/26/22 09:35
TIC
TAL SAV
Instrument ID: NOEQUIP
Eurofins Savannah
Page 28 of 38 6/3/2022 (Rev. 3)

Lab Chronicle
Client: S&ME, Inc. Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Laboratory References:
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
0
Eurofins Savannah
Page 29 of 38 6/3/2022 (Rev. 3)

Accreditation/Certification Summary
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Laboratory: Eurofins Savannah
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
AFCEE
SAVLAB
Alabama State
41450
06-30-22
Alaska (UST) State
17-016
09-22-22
ANAB Dept. of Defense ELAP
L2463
09-18-22
ANAB ISO/IEC 17025
L2463.01
09-22-22
Arkansas DEQ State
19-015-0
02-01-23
California State
2939
06-30-22
Florida NELAP
E87052
06-30-22
Georgia State
E87052
06-30-22
Georgia (DW) State
803
06-30-22
Guam State
19-007R
04-17-23
Hawaii State
<cert No.>
06-30-22
Illinois NELAP
200022
11-30-22
Indiana State
C-GA-02
06-30-22
Iowa State
353
07-01-23
Kentucky (UST) State
NA
06-30-22
Louisiana NELAP
30690
06-30-22
Louisiana (DW) State
LA009
12-31-22
Maine State
GA00006
09-25-22
Maryland State
250
12-31-22
Massachusetts State
M-GA006
06-30-22
Michigan State
9925
06-30-22
Mississippi State
<cert No.>
06-30-22
Nebraska State
NE-OS-7-04
06-30-22
New Jersey NELAP
GA769
06-30-22
New Mexico State
GA00006
06-30-22
New York NELAP
10842
04-01-23
North Carolina (DW) State
13701
07-01-22
North Carolina (WW/SW) State
269
12-31-22
Pennsylvania NELAP
68-00474
06-30-22
Puerto Rico State
GA00006
01-01-23
South Carolina State
98001
06-30-22
Tennessee State
TN02961
06-30-22
Texas NELAP
T1047004185-19-14
11-30-22
Texas TCEQ Water Supply
T104704185
06-30-22
USDA US Federal Programs
P330-18-00313
09-03-24
Virginia NELAP
460161
06-14-22
Washington State
C805
06-10-22
Wisconsin State
999819810
08-31-22
Wyoming State
8TMS-L
06-30-22
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
Alabama State
40150
06-30-22
ANAB ISO/IEC 17025
L2471
02-23-23
Arkansas DEQ State
88-0689
09-01-22
California State
2510
06-30-22
Florida NELAP
E81010
06-30-22
Eurofins Savannah
Page 30 of 38 6/3/2022 (Rev. 3)

Accreditation/Certification Summary
Client: S&ME, Inc.
Job ID: 680-214576-1
Project/Site: Anson Landfill Leachate POTW
Laboratory: Eurofins Pensacola (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
Georgia State
E81010(FL)
06-30-22
Illinois NELAP
200041
10-09-22
Kansas NELAP
E-10253
10-31-22
Kentucky (UST) State
53
06-30-22
Kentucky (WW) State
KY98030
12-31-22
Louisiana NELAP
30976
06-30-22
Louisiana (DW) State
LA017
12-31-22
Maryland State
233
09-30-22
Massachusetts State
M-FLO94
06-30-22
Michigan State
9912
06-30-22
North Carolina (WW/SW) State
314
12-31-22
Oklahoma NELAP
9810
08-31-22
Pennsylvania NELAP
68-00467
01-31-23
South Carolina State
96026
06-30-22
Tennessee State
TN02907
06-30-22
Texas NELAP
T104704286
09-30-22
US Fish & Wildlife US Federal Programs
058448
07-31-22
USDA US Federal Programs
P330-21-00056
05-17-24
Virginia NELAP
460166
06-14-22
West Virginia DEP State
136
05-31-22
Eurofins Savannah
Page 31 of 38 6/3/2022 (Rev. 3)

Method Summary
Client: S&ME, Inc.
Project/Site: Anson Landfill Leachate POTW
Job ID: 680-214576-1
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
TAL SAV
8260D SIM
Volatile Organic Compounds (GC/MS)
SW846
TAL PEN
300.0
Anions, Ion Chromatography
MCAWW
TAL SAV
6020B
Metals (ICP/MS)
SW846
TAL SAV
7470A
Mercury (CVAA)
SW846
TAL SAV
1664B
HEM and SGT-HEM
1664B
TAL SAV
351.2_ASP
Total Kjedahl Nitrogen
EPA
TAL SAV
353.2
Nitrogen, Nitrate -Nitrite
MCAWW
TAL SAV
365.4
Total Phosphorus
EPA
TAL SAV
4500 H+ B-2011
pH
SM
TAL SAV
521OB_ASP
CBOD
SM
TAL SAV
9012B
Cyanide, Total andorAmenable
SW846
TAL SAV
EPA 350.1
Ammonia
EPA
TAL SAV
EPA 420.1
Phenolics, Total Recoverable
EPA
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
SM 5220D
COD
SM
TAL SAV
Field Sampling
Field Sampling
EPA
TAL SAV
1664B
HEM and SGT-HEM (Aqueous)
1664B
TAL SAV
3010A
Preparation, Total Metals
SW846
TAL SAV
5030B
Purge and Trap
SW846
TAL SAV
5030C
Purge and Trap
SW846
TAL PEN
7470A
Preparation, Mercury
SW846
TAL SAV
9012B
Cyanide, Total and/orAmenable, Distillation
SW846
TAL SAV
Digestion
Digestion, Hot Block
MCAWW
TAL SAV
Distill/Ammonia
Distillation, Ammonia
None
TAL SAV
Distill/Phenol
Distillation, Phenolics
None
TAL SAV
Protocol References:
1664B = EPA-821-98-002
EPA= US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
None = None
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 32 of 38 6/3/2022 (Rev. 3)

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Page 35 of 38 6/3/2022 (Rev. 3)

ANSON WASTE MANAGEMENT FACILITY
ANSON COUNTY, NORTH CAROLINA
LEACHATE SAMPLING LOG
S&ME PROJECT:
DATE:
PERSONNEL:
4140-15-007
4/26/2022
Skyler Schmal
***Add temp & pH to C of C
LEACHATE SAMPLE
Field Readings
pH
1.33
Conductivity (mS/sec)
481
Temperature (°C)
27.4
Sample Time:
9:3 5
Page 36 of 38 6/3/2022 (Rev. 3)

Login Sample Receipt Checklist
Client: S&ME, Inc.
Job Number: 680-214576-1
Login Number: 214576
List Number: 1
Creator: Sims, Robert D
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 37 of 38 6/3/2022 (Rev. 3)

Client: S&ME, Inc.
Login Number: 214576
List Number: 2
Creator: Whitley, Adrian
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
N/A
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
2.6°C IR8
Job Number: 680-214576-1
List Source: Eurofins Pensacola
List Creation: 04/28/22 02:22 PM
Eurofins Savannah
Page 38 of 38 6/3/2022 (Rev. 3)

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, May 23, 2022
S&ME, Inc. (SM011)
Attn: Lindsey Harris
644 Eastern Star Road
Kingsport, TN 37663
RE: Laboratory Results for
Project Number: 4140-15-007, Project Name/Desc: Anson LF - Dissolved metals
ENCO Workorder(s): CF04527
Dear Lindsey Harris,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, April 15, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-MW9S
Lab ID: CF04527-01
Sampled: 04/14/22 10:35
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/11/22
05/16/22 05:24
05/20/22 12:09
Client ID: 0401-MW12S
Lab ID: CF04527-04
Sampled: 04/11/22 11:53
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/08/22
05/16/22 05:24
05/20/22 12:11
Client ID: 0401-MW15D
Lab ID: CF04527-07
Sampled: 04/11/22 13:47
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/08/22
05/16/22 05:24
05/20/22 12:14
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 8

(� �Eo
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 0401-MW9S Lab ID: CF04527-01
Analvte Results Flag MDL PQL Units Method Notes
Barium - Dissolved 551 1.10 10.0 uq/L EPA 6010D
I Client ID: 0401-MW15D Lab ID: CF04527-07
Analvte
Cobalt - Dissolved
Results Flag MDL PQL Units
7.16 1 1.40 10.0 ug/L
Method Notes
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW9S Lab Sample ID:CF04527-01 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/14/22 10:35 Work Order: CF04527
Project: Anson LF - Dissolved metals Sampled By: CLIENT
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units LF MDL P L Batch Method Analyzed Ay Notes
Barium [7440-39-3]^ 551 ug/L 1 1.10 10.0 2E16007 EPA 6010D 05/20/22 12:09 JDH
Description: 0401-MW12S Lab Sample ID:CF04527-04 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 11:53 Work Order: CF04527
Project: Anson LF - Dissolved metals Sampled By: CLIENT
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Arsenic [7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 2E16007 EPA 6010D 05/20/22 12:11 JDH
Description: 0401-MW15D Lab Sample ID:CF04527-07 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 13:47 Work Order: CF04527
Project: Anson LF - Dissolved metals Sampled By: CLIENT
(Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units LF MDL P L Batch Method Analyzed By Notes
Cobalt[7440-48-4]^ 7.16 J ug/L 1 1.40 10.0 2E16007 EPA 6010D 05/20/22 12:14 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 of 8

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 2E16007 - EPA 3005A
Blank (2E36007-BLK1)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 11:19
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Blank (2E36007-BLK2)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 11:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
LCS (2E16007-BS1)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 11:26
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
210
10.0
ug/L
200 105 80-120
Barium
216
10.0
ug/L
200 108 80-120
Cobalt
215
10.0
ug/L
200 108 80-120
Matrix Spike (2E16007-MS1)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 11:59
Source: CF06100-05
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
217
10.0
ug/L
200 7.60 U 108 75-125
Barium
223
10.0
ug/L
200 5.64 109 75-125
Cobalt
220
10.0
ug/L
200 1.40 U 110 75-125
Matrix Spike Dup (2E16007-MSDS)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 12:01
Source: CF06100-05
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
221
10.0
ug/L
200 7.60 U 110 75-125 2
20
Barium
227
10.0
ug/L
200 5.64 111 75-125 2
20
Cobalt
223
10.0
ug/L
200 1.40 U 112 75-125 2
20
Post Spike (2E36007-13SI)
Prepared: 05/16/2022 05:24 Analyzed: 05/20/2022 12:04
Source: CF06100-05
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.230
0.0100
mg/L
0.200
-0.00243
115
80-120
Barium
0.232
0.0100
mg/L
0.200
0.00564
113
80-120
Cobalt
0.228
0.0100
mg/L
0.200
0.000768
114
80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) Of

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 of 8

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ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, June 10, 2022
S&ME, Inc. (SM011)
Attn: Lindsey Harris
644 Eastern Star Road
Kingsport, TN 37663
RE: Laboratory Results for
Project Number: 4140-15-007, Project Name/Desc: Anson LF - Dissolved metals
ENCO Workorder(s): CF05791
Dear Lindsey Harris,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, April 26, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 9

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-MW2D Lab ID: CF05791-03 Sampled: 04/15/22 10:30 Received: 04/26/22 10:00
Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 6010D EPA 3005A 10/12/22
06/05/22 22:31 06/07/22 09:50
Client ID: 0401-MWBS Lab ID: CF05791-07 Sampled: 04/15/22 12:25 Received: 04/26/22 10:00
Parameter Preparation Hold Date/Time(s) Preo Date/Time(s) Analysis Date/Time(s)
EPA 6010D EPA 3005A 10/12/22
06/08/22 00:22 06/10/22 09:27
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 9

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SAMPLE DETECTION SUMMARY
Client ID: 0401-MW2D Lab ID: CF05791-03
Analvte Results Flag MDL PQL Units Method Notes
Beryllium - Dissolved 0.583 1 0.160 1.00 uq/L EPA 6010D LG-01
Client ID: 0401-MWBS Lab ID: CF05791-07
Analvte Results Flag MDL PQL Units Method Notes
Barium - Dissolved 1920 1.10 10.0 ug/L EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 9

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ANALYTICAL RESULTS
Description: 0401-MW2D Lab Sample ID:CF05791-03 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 10:30 Work Order: CF05791
Project: Anson LF - Dissolved metals Sampled By: Kelsey Vassallo
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units LF MDL POLL Batch Method Analyzed Ay Notes
Beryllium [7440-41-7]^ 0.583 J ug/L 1 0.160 1.00 2FO5002 EPA 6010D 06/07/22 09:50 JDH LG-01
Cobalt[7440-48-41^ 1.40 U ug/L 1 1.40 10.0 2FO5002 EPA 6010D 06/07/22 09:50 JDH LG-01
Description: 0401-MW8S Lab Sample ID:CF05791-07 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 12:25 Work Order: CF05791
Project: Anson LF - Dissolved metals Sampled By: Kelsey Vassallo
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes
Barium [7440-39-3]^ 1920 ug/L 1 1.10 10.0 2FO5004 EPA 6010D 06/10/22 09:27 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 of 9

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 2FO5002 - EPA 3005A
Blank (2F05002-BLKI)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 09:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
0.160
U
1.00
ug/L
Cobalt
1.40
U
10.0
ug/L
Blank (21`05002-BLK2)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 09:47
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
0.160
U
1.00
ug/L
Cobalt
1.40
U
10.0
ug/L
LCS (2F05002-BS1)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 09:53
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
22.1
1.00
ug/L
20.0 111 80-120
Cobalt
220
10.0
ug/L
200 110 80-120
Matrix Spike (21`05002-MS3)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 09:57
Source: CF05791-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
23.0
1.00
ug/L
20.0 0.583 112 75-125
Cobalt
219
10.0
ug/L
200 1.40 U 109 75-125
Matrix Spike Dup (21`05002-MSD3)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 09:59
Source: CF05791-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
22.3
1.00
ug/L
20.0 0.583 108 75-125 3
20
Cobalt
217
10.0
ug/L
200 1.40 U 108 75-125 0.9
20
Post Spike (2F05002-PS3)
Prepared: 06/05/2022 22:31 Analyzed: 06/07/2022 10:02
Source: CF05791-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Beryllium
0.0229
0.00100
mg/L
0.0200 0.000583 112 80-120
Cobalt
0.219
0.0100
mg/L
0.200-0.000210 109 80-120
Batch 2FO5004 - EPA 3005A
Blank (2F05004-BLKI) Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 09:20
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Barium 1.10 U 10.0 ug/L
Blank (2F05004-BLK2) Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 09:23
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Barium 1.10 U 10.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) Of 9

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 2F05004 - EPA 3005A - Continued
LCS (2F05004-BSI) Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 09:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Barium
214
10.0
ug/L
200 107 80-120
Matrix Spike (2F05004-MS3)
Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 09:34
Source: CF05791-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Barium
2070
10.0
ug/L
200 1920 76 75-125
Matrix Spike Dup (21`05004-MS133)
Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 10:16
Source: CF05791-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Barium
2180
10.0
ug/L
200 1920 128 75-125 5
20
QM-07
Post Spike (2F05004-PS3)
Prepared: 06/08/2022 00:22 Analyzed: 06/10/2022 09:39
Source: CF05791-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Barium
2.07
0.0100
mg/L
0.200 1.92 74 80-120
QM-08
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 9

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
LG-01 Sample filtered in laboratory.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 9

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ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, May 6, 2022
S&ME, Inc. (SM011)
Attn: Lindsey Harris
644 Eastern Star Road
Kingsport, TN 37663
RE: Laboratory Results for
Project Number: 4140-15-007, Project Name/Desc: Anson LF
ENCO Workorder(s): CF04526,CF05798
Dear Lindsey Harris,
Enclosed is a copy of your laboratory report for test samples received by our laboratory
between Friday, April 15, 2022 and Tuesday, April 26, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 69

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-MW9S
Lab ID: CF04526-01
Sampled: 04/14/22 10:35
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/11/22
04/19/22 08:01
04/22/22 09:38
EPA 6020E
EPA 3005A
10/11/22
04/18/22 02:07
04/21/22 12:48
EPA 8260D
EPA 503013_MS
04/28/22
04/19/22 12:59
04/19/22 23:51
EPA 8260D
EPA 503013_MS
04/28/22
04/21/22 19:08
04/22/22 09:42
Client ID: 0401-MW10S
Lab ID: CF04526-02
Sampled: 04/11/22 10:50
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/08/22
04/19/22 08:01
04/22/22 09:40
EPA 6020E
EPA 3005A
10/08/22
04/18/22 02:07
04/21/22 12:52
EPA 8260D
EPA 503013_MS
04/25/22
04/18/22 14:00
04/18/22 20:04
EPA 8260D
EPA 503013_MS
04/25/22
04/19/22 12:59
04/20/22 00:17
Client ID: 0401-MW11S
Lab ID: CF04526-03
Sampled: 04/12/22 14:05
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/09/22
04/20/22 01:23
04/20/22 14:56
EPA 6020B
EPA 3005A
10/09/22
04/18/22 02:07
04/21/22 12:56
EPA 8260D
EPA 503013_MS
04/26/22
04/19/22 12:59
04/20/22 00:42
EPA 8260D
EPA 5030B_MS
04/26/22
04/19/22 16:30
04/19/22 21:58
Client ID: 0401-MW12S
Lab ID: CF04526-04
Sampled: 04/11/22 11:53
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/08/22
04/20/22 01:23
04/20/22 15:17
EPA 6020B
EPA 3005A
10/08/22
04/18/22 02:07
04/21/22 13:00
EPA 8260D
EPA 503013_MS
04/25/22
04/18/22 14:00
04/18/22 20:32
EPA 8260D
EPA 503013_MS
04/25/22
04/19/22 12:59
04/20/22 01:08
Client ID: 0401-MW13S
Lab ID: CF04526-05
Sampled: 04/12/22 12:40
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/09/22
04/25/22 15:12
04/26/22 09:49
EPA 6020B
EPA 3005A
10/09/22
04/18/22 02:07
04/21/22 13:05
EPA 8260D
EPA 5030B_MIS
04/26/22
04/19/22 12:59
04/20/22 01:34
EPA 8260D
EPA 503013_MS
04/26/22
04/19/22 16:30
04/19/22 22:25
Client ID: 0401-MW14D
Lab ID: CF04526-06
Sampled: 04/13/22 09:55
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:09
EPA 6020E
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 13:09
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 02:00
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 19:47
04/20/22 15:56
Client ID: 0401-MW15D
Lab ID: CF04526-07
Sampled: 04/11/22 13:47
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/08/22
04/25/22 15:12
04/26/22 10:20
EPA 6020E
EPA 3005A
10/08/22
04/18/22 02:07
04/21/22 13:13
EPA 8260D
EPA 503013_MS
04/25/22
04/18/22 14:00
04/18/22 20:59
EPA 8260D
EPA 503013_MS
04/25/22
04/19/22 12:59
04/20/22 02:26
Client ID: 0401-Field Blank
Lab ID: CF04526-08
Sampled: 04/13/22 09:00
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/10/22
04/25/22 15:12
04/26/22 10:28
EPA 6020E
EPA 3005A
10/10/22
04/18/22 02:07
04/21/22 13:27
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 12:59
04/20/22 02:51
EPA 8260D
EPA 503013_MS
04/27/22
04/19/22 19:47
04/20/22 09:54
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 69

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-TripBlank
Lab ID: CF04526-09
Sampled: 04/11/22 10:50
Received: 04/15/22 10:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
04/25/22
04/18/22 14:00
04/18/22 18:13
EPA 8260D
EPA 503013_MS
04/25/22
04/19/22 12:59
04/20/22 03:17
Client ID: 0401-MWlD
Lab ID: CF05798-01
Sampled: 04/15/22 11:30
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
04/29/22 05:18
05/03/22 10:54
EPA 6020E
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 09:23
EPA 8260D
EPA 503013_MS
04/29/22
04/26/22 16:30
04/26/22 20:49
EPA 8260D
EPA 5030B_MS
04/29/22
04/27/22 12:43
04/27/22 13:32
Client ID: 0401-MW2S
Lab ID: CF05798-02
Sampled: 04/15/22 10:00
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
04/29/22 05:18
05/03/22 10:57
EPA 6020B
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 10:44
EPA 8260D
EPA 503013_MS
04/29/22
04/26/22 16:30
04/26/22 21:16
EPA 8260D
EPA 503013_MS
04/29/22
04/27/22 12:43
04/27/22 13:58
Client ID: 0401-MW2D
Lab ID: CF05798-03
Sampled: 04/15/22 10:30
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
05/02/22 01:24
05/03/22 13:40
EPA 6020B
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 10:57
EPA 8260D
EPA 5030B_MIS
04/29/22
04/26/22 16:30
04/26/22 21:44
EPA 8260D
EPA 503013_MS
04/29/22
04/27/22 12:43
04/27/22 14:24
Client ID: 0401-MW3S
Lab ID: CF05798-04
Sampled: 04/19/22 10:10
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/16/22
05/02/22 01:24
05/03/22 13:43
EPA 6020E
EPA 3005A
10/16/22
05/02/22 01:30
05/05/22 11:02
EPA 8260D
EPA 503013_MS
05/03/22
04/26/22 16:30
04/26/22 22:12
EPA 8260D
EPA 503013_MS
05/03/22
04/27/22 12:43
04/27/22 14:50
Client ID: 0401-MW4S
Lab ID: CF05798-05
Sampled: 04/15/22 14:00
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
05/02/22 01:24
05/03/22 13:50
EPA 6020E
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 11:06
EPA 8260D
EPA 503013_MS
04/29/22
04/26/22 16:30
04/26/22 22:39
EPA 8260D
EPA 503013_MS
04/29/22
04/27/22 12:43
04/27/22 15:15
Client ID: 0401-MWSS
Lab ID: CF05798-06
Sampled: 04/19/22 10:40
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/16/22
05/02/22 01:24
05/03/22 13:53
EPA 6020E
EPA 3005A
10/16/22
05/02/22 01:30
05/05/22 11:10
EPA 8260D
EPA 503013_MS
O5/03/22
04/26/22 16:30
04/26/22 23:07
EPA 8260D
EPA 503013_MS
05/03/22
04/27/22 12:43
04/27/22 15:41
Client ID: 0401-MW8S
Lab ID: CF05798-07
Sampled: 04/15/22 12:25
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
05/02/22 01:24
05/03/22 13:56
EPA 6020B
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 11:14
EPA 8260D
EPA 5030B_MS
04/29/22
04/26/22 16:30
04/26/22 23:35
EPA 8260D
EPA 5030B_MS
04/29/22
04/27/22 12:43
04/27/22 16:07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 69

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 0401-Field Duplicate
Lab ID: CF05798-08
Sampled: 04/15/22 00:00
Received: 04/26/22 10:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
10/12/22
05/02/22 01:24
05/03/22 13:58
EPA 6020E
EPA 3005A
10/12/22
05/02/22 01:30
05/05/22 11:19
EPA 8260D
EPA 503013_MS
04/29/22
04/26/22 16:30
04/27/22 00:02
EPA 8260D
EPA 503013_MS
04/29/22
04/27/22 12:43
04/27/22 16:33
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 69

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SAMPLE DETECTION SUMMARY
Client ID: 0401-MW9S
Lab ID:
CF04526-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
739
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.05
J
1.40
10.0
ug/L
EPA 6010D
Vanadium - Total
2.59
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 0401-MW10S
Lab ID:
CF04526-02
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
581
1.10
10.0
uq/L
EPA 6010D
I Client ID: 0401-MW11S Lab ID: CF04526-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
693
1.10
10.0
ug/L
EPA 6010D
Client ID: 0401-MW12S
Lab ID:
CF04526-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Arsenic - Total
11.3
7.60
10.0
ug/L
EPA 6010D
Barium - Total
189
1.10
10.0
ug/L
EPA 6010D
Copper - Total
4.37
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
4.13
J
3.10
10.0
ug/L
EPA 6010D
Zinc - Total
5.80
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-MW13S
Lab ID:
CF04526-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
230
1.10
10.0
ug/L
EPA 6010D
Client ID: 0401-MW14D
Lab ID:
CF04526-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
8.89
J
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.78
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.67
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
4.10
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 0401-MW15D
Lab ID:
CF04526-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
17.1
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
1.94
1
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
12.5
1.40
10.0
ug/L
EPA 6010D
Copper - Total
8.35
J
1.60
10.0
ug/L
EPA 6010D
Lead - Total
3.46
1
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
22.8
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
29.0
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-MW1D
Lab ID:
CF05798-01
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
125
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
7.26
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 0401-MW2S
Lab ID:
CF05798-02
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
120
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
2.04
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.76
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
5.61
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
5.36
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
8.79
J
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
8.91
J
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) Of 69

(� �Eo
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: 0401-MW2D
Lab ID:
CF05798-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
239
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
4.98
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.68
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
16.0
1.40
10.0
ug/L
EPA 6010D
Copper - Total
7.24
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
11.5
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
11.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-MW3S
Lab ID:
CF05798-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
37.8
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
3.18
1
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
2.77
1
2.20
10.0
ug/L
EPA 6010D
Client ID: 0401-MW4S
Lab ID:
CF05798-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
176
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
5.97
1
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
5.60
1
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
12.2
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-MWSS
Lab ID:
CF05798-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
79.8
1.10
10.0
ug/L
EPA 6010D
Nickel - Total
3.21
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 0401-MW8S
Lab ID:
CF05798-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
2220
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
3.38
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
4.04
J
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
7.87
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 0401-Field Duplicate
Lab ID:
CF05798-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
240
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
5.45
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
18.7
1.40
10.0
ug/L
EPA 6010D
Copper - Total
8.59
J
1.60
10.0
ug/L
EPA 6010D
Nickel - Total
13.2
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
13.3
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 69

0Nk"q09
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ANALYTICAL RESULTS
Description: 0401-MW9S Lab Sample ID:CF04526-01 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/14/22 10:35 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D21036
EPA 8260D
04/22/22 09:42
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D21036
EPA 8260D
04/22/22 09:42
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D21036
EPA 8260D
04/22/22 09:42
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 7 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW9S Lab Sample ID:CF04526-01 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/14/22 10:35 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D21036 EPA 8260D 04/22/22 09:42 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D21036 EPA 8260D 04/22/22 09:42 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
109 %
53-136
2D21036
EPA 8260D
04122122 09:42
RKY
Dibromofluoromethane
46
1
50.0
92 %
67-129
2D21036
EPA 8260D
04122122 09:42
RKY
Toluene-d8
55
1
50.0
110 %
59-134
2D21036
EPA 8260D
04122122 09:42
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 12:48
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Barium [7440-39-3]^
739
ug/L
1
1.10
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D19006
EPA 6010D
04/22/22 09:38
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D19006
EPA 6010D
04/22/22 09:38
JDH
Chromium [7440-47-3]^
2.05
J
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 12:48
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 12:48
JDH
Vanadium [7440-62-2]^
2.59
J
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D19006
EPA 6010D
04/22/22 09:38
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/19/22 23:51
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D19038
EPA 8260D
04119122 23:51
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW10S Lab Sample ID:CF04526-02 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 10:50 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D18032
EPA 8260D
04/18/22 20:04
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D18032
EPA 8260D
04/18/22 20:04
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D18032
EPA 8260D
04/18/22 20:04
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D18032
EPA 8260D
04/18/22 20:04
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 9 Of 69

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ANALYTICAL RESULTS
Description: 0401-MW10S Lab Sample ID:CF04526-02 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 10:50 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D18032 EPA 8260D 04/18/22 20:04 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D18032 EPA 8260D 04/18/22 20:04 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
97 %
53-136
2D18032
EPA 8260D
04116122 20:04
RKY
Dibromofluoromethane
51
1
50.0
102 %
67-129
2D18032
EPA 8260D
04116122 20:04
RKY
Toluene-d8
52
1
50.0
104 %
59-134
2D18032
EPA 8260D
04116122 20:04
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 12:52
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Barium [7440-39-3]^
581
ug/L
1
1.10
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D19006
EPA 6010D
04/22/22 09:40
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D19006
EPA 6010D
04/22/22 09:40
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 12:52
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 12:52
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D19006
EPA 6010D
04/22/22 09:40
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 00:17
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D19038
EPA 8260D
04120122 00:17
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW11S Lab Sample ID:CF04526-03 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/12/22 14:05 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/19/22 21:58
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/19/22 21:58
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/19/22 21:58
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/19/22 21:58
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 11 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW11S Lab Sample ID:CF04526-03 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/12/22 14:05 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/19/22 21:58 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/19/22 21:58 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
47
1
50.0
94 %
53-136
2D19028
EPA 8260D
04119122 21:58
RKY
Dibromofluoromethane
50
1
50.0
100 %
67-129
2D19028
EPA 8260D
04119122 21:58
RKY
Toluene-d8
56
1
50.0
111 %
59-134
2D19028
EPA 8260D
04119122 21:58
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 12:56
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Barium [7440-39-3]^
693
ug/L
1
1.10
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D20001
EPA 6010D
04/20/22 14:56
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D20001
EPA 6010D
04/20/22 14:56
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 12:56
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 12:56
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D20001
EPA 6010D
04/20/22 14:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 00:42
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.8
1
5.00
96 %
75-125
2D19038
EPA 8260D
04120122 00:42
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW12S Lab Sample ID:CF04526-04 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 11:53 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D18032
EPA 8260D
04/18/22 20:32
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D18032
EPA 8260D
04/18/22 20:32
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D18032
EPA 8260D
04/18/22 20:32
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D18032
EPA 8260D
04/18/22 20:32
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 13 of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW12S Lab Sample ID:CF04526-04 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 11:53 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D18032 EPA 8260D 04/18/22 20:32 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D18032 EPA 8260D 04/18/22 20:32 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
97 %
53-136
2D18032
EPA 8260D
04116122 20:32
RKY
Dibromofluoromethane
52
1
50.0
103 %
67-129
2D18032
EPA 8260D
04116122 20:32
RKY
Toluene-d8
52
1
50.0
105 %
59-134
2D18032
EPA 8260D
04116122 20:32
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:00
JDH
Arsenic[7440-38-2]^
11.3
ug/L
1
7.60
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Barium [7440-39-3]^
189
ug/L
1
1.10
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D20001
EPA 6010D
04/20/22 15:17
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D20001
EPA 6010D
04/20/22 15:17
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Copper[7440-50-8]^
4.37
J
ug/L
1
1.60
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Lead [7439-92-1]^
4.13
J
ug/L
1
3.10
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:00
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:00
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Zinc[7440-66-6]^
5.80
J
ug/L
1
4.40
10.0
2D20001
EPA 6010D
04/20/22 15:17
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 01:08
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D19038
EPA 8260D
04120122 01:08
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW13S Lab Sample ID:CF04526-05 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/12/22 12:40 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY QV-01
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19028
EPA 8260D
04/19/22 22:25
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19028
EPA 8260D
04/19/22 22:25
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19028
EPA 8260D
04/19/22 22:25
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19028
EPA 8260D
04/19/22 22:25
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 15 Of 69

(� �Eo
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ANALYTICAL RESULTS
Description: 0401-MW13S Lab Sample ID:CF04526-05 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/12/22 12:40 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19028 EPA 8260D 04/19/22 22:25 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19028 EPA 8260D 04/19/22 22:25 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
2D19028
EPA 8260D
04119122 22:25
RKY
Dibromofluoromethane
52
1
50.0
105 %
67-129
2D19028
EPA 8260D
04119122 22:25
RKY
Toluene-d8
53
1
50.0
107 %
59-134
2D19028
EPA 8260D
04119122 22:25
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:05
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Barium [7440-39-3]^
230
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 09:49
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 09:49
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:05
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:05
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 09:49
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 01:34
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.6
1
5.00
93 %
75-125
2D19038
EPA 8260D
04120122 01:34
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW14D Lab Sample ID:CF04526-06 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/13/22 09:55 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19031
EPA 8260D
04/20/22 15:56
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19031
EPA 8260D
04/20/22 15:56
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19031
EPA 8260D
04/20/22 15:56
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 17 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW14D Lab Sample ID:CF04526-06 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/13/22 09:55 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19031 EPA 8260D 04/20/22 15:56 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19031 EPA 8260D 04/20/22 15:56 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
47
1
50.0
95 %
53-136
2D19031
EPA 8260D
0412012215:56
RKY
Dibromofluoromethane
52
1
50.0
105 %
67-129
2D19031
EPA 8260D
0412012215:56
RKY
Toluene-d8
55
1
50.0
110 %
59-134
2D19031
EPA 8260D
0412012215:56
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:09
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Barium [7440-39-3]^
8.89
J
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:09
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:09
JDH
Chromium [7440-47-3]^
2.78
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Cobalt[7440-48-4]^
1.67
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Nickel[7440-02-O]^
4.10
J
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:09
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:09
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:09
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 02:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.8
1
5.00
97 %
75-125
2D19038
EPA 8260D
04120122 02:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW15D Lab Sample ID:CF04526-07 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 13:47 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D18032
EPA 8260D
04/18/22 20:59
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D18032
EPA 8260D
04/18/22 20:59
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D18032
EPA 8260D
04/18/22 20:59
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D18032
EPA 8260D
04/18/22 20:59
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 19 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW15D Lab Sample ID:CF04526-07 Received: 04/15/22 10:30
Matrix: Ground Water Sampled:04/11/22 13:47 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D18032 EPA 8260D 04/18/22 20:59 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D18032 EPA 8260D 04/18/22 20:59 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
47
1
50.0
94 %
53-136
2D18032
EPA 8260D
04116122 20:59
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
2D18032
EPA 8260D
04116122 20:59
RKY
Toluene-d8
54
1
50.0
109 %
59-134
2D18032
EPA 8260D
04116122 20:59
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:13
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Barium [7440-39-3]^
17.1
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:20
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:20
JDH
Chromium [7440-47-3]^
1.94
J
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Cobalt[7440-48-4]^
12.5
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Copper[7440-50-8]^
8.35
J
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Lead [7439-92-1]^
3.46
J
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Nickel[7440-02-O]^
22.8
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:13
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:13
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Zinc[7440-66-6]^
29.0
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:20
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 02:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.8
1
5.00
96 %
75-125
2D19038
EPA 8260D
04120122 02:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-Field Blank Lab Sample ID:CF04526-08 Received: 04/15/22 10:30
Matrix: Water Sampled:04/13/22 09:00 Work Order: CF04526
Project: Anson LF Sampled By:SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D19031
EPA 8260D
04/20/22 09:54
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D19031
EPA 8260D
04/20/22 09:54
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D19031
EPA 8260D
04/20/22 09:54
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
I Page 21 of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-FieldBlank Lab Sample ID:CF04526-08 Received: 04/15/22 10:30
Matrix: Water Sampled:04/13/22 09:00 Work Order: CF04526
Project: Anson LF Sampled By: SKYLER SCHMEL
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D19031 EPA 8260D 04/20/22 09:54 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D19031 EPA 8260D 04/20/22 09:54 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
2D19031
EPA 8260D
04120122 09:54
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
2D19031
EPA 8260D
04120122 09:54
RKY
Toluene-d8
54
1
50.0
108 %
59-134
2D19031
EPA 8260D
04120122 09:54
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2D18002
EPA 6020B
04/21/22 13:27
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Barium [7440-39-3]^
1.10
u
ug/L
1
1.10
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D22018
EPA 6010D
04/26/22 10:28
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D22018
EPA 6010D
04/26/22 10:28
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Nickel[7440-02-0]^
2.20
u
ug/L
1
2.20
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2D18002
EPA 6020B
04/21/22 13:27
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2D18002
EPA 6020B
04/21/22 13:27
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2D22018
EPA 6010D
04/26/22 10:28
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D19038
EPA 8260D
04/20/22 02:51
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
4.8
1
5.00
97 %
75-125
2D19038
EPA 8260D
04120122 02:51
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-Trip Blank Lab Sample ID: CF04526-09 Received: 04/15/22 10:30
Matrix: Water Sampled:04/11/22 10:50 Work Order: CF04526
Project: Anson LF Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D18032
EPA 8260D
04/18/22
18:13
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D18032
EPA 8260D
04/18/22
18:13
RKY
Benzene [71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Chlorobenzene [108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D18032
EPA 8260D
04/18/22
18:13
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D18032
EPA 8260D
04/18/22
18:13
RKY QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
F Page 23 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-TripBlank Lab Sample ID:CF04526-09 Received: 04/15/22 10:30
Matrix: Water Sampled:04/11/22 10:50 Work Order: CF04526
Project: Anson LF Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D18032 EPA 8260D 04/18/22 18:13 RKY
Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D18032 EPA 8260D 04/18/22 18:13 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
50
1
50.0
100 %
53-136
2D18032
EPA 8260D
04116122 18:13
RKY
Dibromofluoromethane
53
1
50.0
105 %
67-129
2D18032
EPA 8260D
0411612218:13
RKY
Toluene-d8
54
1
50.0
107 %
59-134
2D18032
EPA 8260D
0411612218:13
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2D19038
EPA 8260D
04/20/22 03:17
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy Notes
Toluene-d8
4.7
1
5.00
94 %
75-125
2D19038
EPA 8260D
04120122 03:17
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 Of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MWlD Lab Sample ID:CF05798-01 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 11:30 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 20:49
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 20:49
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 20:49
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 20:49
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 25 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MWlD Lab Sample ID:CF05798-01 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 11:30 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 20:49 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 20:49 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
2D26024
EPA 8260D
04126122 20:49
RKY
Dibromofluoromethane
49
1
50.0
99 %
67-129
2D26024
EPA 6260D
04126122 20:49
RKY
Toluene-d8
53
1
50.0
106 %
59-134
2D26024
EPA 6260D
04126122 20:49
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 09:23
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Barium [7440-39-3]^
125
ug/L
1
1.10
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2D29004
EPA 6010D
05/03/22 10:54
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D29004
EPA 6010D
05/03/22 10:54
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Nickel[7440-02-O]^
7.26
J
ug/L
1
2.20
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 09:23
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 09:23
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Zinc [7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2D29004
EPA 6010D
05/03/22 10:54
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 13:32
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.9
1
5.00
97 %
75-125
2D27041
EPA 8260D
041271221322
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW2S Lab Sample ID:CF05798-02 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 10:00 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 21:16
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 21:16
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 21:16
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 21:16
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 27 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW2S Lab Sample ID:CF05798-02 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 10:00 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 21:16 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 21:16 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
50
1
50.0
99 %
53-136
2D26024
EPA 8260D
04126122 21:16
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
2D26024
EPA 8260D
04126122 21:16
RKY
Toluene-d8
55
1
50.0
111 %
59-134
2D26024
EPA 8260D
04126122 21:16
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 10:44
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Barium [7440-39-3]^
120
ug/L
1
1.10
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Beryllium [7440-41-7]^
2.04
ug/L
1
0.160
1.00
2D29004
EPA 6010D
05/03/22 10:57
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2D29004
EPA 6010D
05/03/22 10:57
JDH
Chromium [7440-47-3]^
1.76
J
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Cobalt[7440-48-4]^
5.61
J
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Copper[7440-50-8]^
5.36
J
ug/L
1
1.60
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Nickel[7440-02-O]^
8.79
J
ug/L
1
2.20
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 10:44
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 10:44
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Zinc[7440-66-6]^
8.91
J
ug/L
1
4.40
10.0
2D29004
EPA 6010D
05/03/22 10:57
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 13:58
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
&
Notes
Toluene-d8
4.9
1
5.00
97 %
75-125
2D27041
EPA 8260D
0412712213:58
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW2D Lab Sample ID:CF05798-03 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 10:30 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 21:44
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 21:44
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 21:44
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 21:44
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 29 Of 69

(� �Eo
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ANALYTICAL RESULTS
Description: 0401-MW2D Lab Sample ID:CF05798-03 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 10:30 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 21:44 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 21:44 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
99 %
53-136
2D26024
EPA 8260D
04126122 21:44
RKY
Dibromofluoromethane
52
1
50.0
104 %
67-129
2D26024
EPA 8260D
04126122 21:44
RKY
Toluene-d8
54
1
50.0
108 %
59-134
2D26024
EPA 8260D
04126122 21:44
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 10:57
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Barium [7440-39-3]^
239
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Beryllium [7440-41-7]^
4.98
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Chromium [7440-47-3]^
1.68
J
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Cobalt[7440-48-4]^
16.0
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Copper[7440-50-8]^
7.24
J
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Nickel[7440-02-O]^
11.5
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 10:57
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 10:57
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Zinc[7440-66-6]^
11.1
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:40
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 14:24
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.6
1
5.00
93 %
75-125
2D27041
EPA 8260D
0412712214:24
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW3S Lab Sample ID:CF05798-04 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/19/22 10:10 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22
22:12
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22
22:12
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22
22:12
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22
22:12
RKY QV-01
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 31 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW3S Lab Sample ID:CF05798-04 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/19/22 10:10 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 22:12 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 22:12 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
52
1
50.0
104 %
53-136
2D26024
EPA 8260D
04126122 22:12
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
2D26024
EPA 8260D
04126122 22:12
RKY
Toluene-d8
56
1
50.0
112 %
59-134
2D26024
EPA 8260D
04126122 22:12
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 11:02
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Barium [7440-39-3]^
37.8
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Cobalt[7440-48-4]^
3.18
J
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Nickel[7440-02-O]^
2.77
J
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 11:02
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 11:02
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:43
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 14:50
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2D27041
EPA 8260D
0412712214:50
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW4S Lab Sample ID:CF05798-05 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 14:00 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 22:39
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 22:39
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 22:39
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 22:39
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 33 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW4S Lab Sample ID:CF05798-05 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 14:00 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 22:39 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 22:39 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
98 %
53-136
2D26024
EPA 8260D
04126122 22:39
RKY
Dibromofluoromethane
49
1
50.0
98 %
67-129
2D26024
EPA 6260D
04126122 22:39
RKY
Toluene-d8
53
1
50.0
107 %
59-134
2D26024
EPA 6260D
04126122 22:39
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 11:06
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Barium [7440-39-3]^
176
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Chromium [7440-47-3]^
5.97
J
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Nickel[7440-02-O]^
5.60
J
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 11:06
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 11:06
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Zinc[7440-66-6]^
12.2
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:50
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 15:15
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.6
1
5.00
92 %
75-125
2D27041
EPA 8260D
0412712215:15
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW5S Lab Sample ID:CF05798-06 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/19/22 10:40 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 23:07
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 23:07
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 23:07
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 23:07
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 35 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW5S Lab Sample ID:CF05798-06 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/19/22 10:40 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 23:07 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 23:07 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
49
1
50.0
98 %
53-136
2D26024
EPA 8260D
04126122 23:07
RKY
Dibromofluoromethane
50
1
50.0
100 %
67-129
2D26024
EPA 8260D
04126122 23:07
RKY
Toluene-d8
54
1
50.0
107 %
59-134
2D26024
EPA 8260D
04126122 23:07
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 11:10
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Barium [7440-39-3]^
79.8
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Nickel[7440-02-O]^
3.21
J
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 11:10
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 11:10
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Zinc[7440-66-6]^
4.40
u
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:53
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 15:41
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.8
1
5.00
97 %
75-125
2D27041
EPA 8260D
0412712215:41
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 of 69

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW8S Lab Sample ID:CF05798-07 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 12:25 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
21)26024
EPA 8260D
04/26/22 23:35
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
21)26024
EPA 8260D
04/26/22 23:35
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
21)26024
EPA 8260D
04/26/22 23:35
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
21)26024
EPA 8260D
04/26/22 23:35
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
F Page 37 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-MW8S Lab Sample ID:CF05798-07 Received: 04/26/22 10:00
Matrix: Ground Water Sampled:04/15/22 12:25 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/26/22 23:35 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/26/22 23:35 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
48
1
50.0
96 %
53-136
2D26024
EPA 8260D
04126122 23:35
RKY
Dibromofluoromethane
54
1
50.0
107 %
67-129
2D26024
EPA 8260D
04126122 23:35
RKY
Toluene-d8
54
1
50.0
108 %
59-134
2D26024
EPA 8260D
04126122 2335
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 11:14
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Barium [7440-39-3]^
2220
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Beryllium [7440-41-7]^
0.160
u
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Chromium [7440-47-3]^
3.38
J
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Cobalt[7440-48-4]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Copper[7440-50-8]^
1.60
u
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Nickel[7440-02-O]^
4.04
J
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 11:14
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 11:14
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Zinc[7440-66-6]^
7.87
J
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:56
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 16:07
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.6
1
5.00
93 %
75-125
2D27041
EPA 8260D
0412712216:07
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 of 69

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-Field Duplicate Lab Sample ID:CF05798-08 Received: 04/26/22 10:00
Matrix: Water Sampled:04/15/22 00:00 Work Order: CF05798
Project: Anson LF Sampled By:CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2D26024
EPA 8260D
04/27/22 00:02
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2D26024
EPA 8260D
04/27/22 00:02
RKY QV-01
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY QV-01
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY QV-01
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
U
ug/L
1
0.70
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Trichloroethene [79-01-6]^
0.15
U
ug/L
1
0.15
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Trichlorofluoromethane [75-69-4]^
0.24
U
ug/L
1
0.24
1.0
2D26024
EPA 8260D
04/27/22 00:02
RKY
Vinyl acetate [108-05-4]A
0.95
U
ug/L
1
0.95
5.0
2D26024
EPA 8260D
04/27/22 00:02
RKY QV-01
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
r Page 39 Of 69

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 0401-FieldDuplicate Lab Sample ID:CF05798-08 Received: 04/26/22 10:00
Matrix: Water Sampled:04/15/22 00:00 Work Order: CF05798
Project: Anson LF Sampled By: CLIENT
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2D26024 EPA 8260D 04/27/22 00:02 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2D26024 EPA 8260D 04/27/22 00:02 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
46
1
50.0
92 %
53-136
2D26024
EPA 8260D
04127122 00:02
RKY
Dibromofluoromethane
53
1
50.0
106 %
67-129
2D26024
EPA 8260D
04127122 00:02
RKY
Toluene-d8
52
1
50.0
104 %
59-134
2D26024
EPA 8260D
04127122 00:02
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
u
ug/L
2
0.740
2.00
2EO2002
EPA 6020B
05/05/22 11:19
JDH
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Barium [7440-39-3]^
240
ug/L
1
1.10
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Beryllium [7440-41-7]^
5.45
ug/L
1
0.160
1.00
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360
1.00
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Cobalt[7440-48-4]^
18.7
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Copper[7440-50-8]^
8.59
J
ug/L
1
1.60
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Nickel[7440-02-O]^
13.2
ug/L
1
2.20
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Selenium [7782-49-2]^
1.82
u
ug/L
2
1.82
2.00
2EO2002
EPA 6020B
05/05/22 11:19
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Thallium [7440-28-0]^
0.220
u
ug/L
2
0.220
2.00
2EO2002
EPA 6020B
05/05/22 11:19
JDH
Vanadium [7440-62-2]^
1.40
u
ug/L
1
1.40
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Zinc[7440-66-6]^
13.3
ug/L
1
4.40
10.0
2EO2001
EPA 6010D
05/03/22 13:58
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
u
ug/L
1
0.80
2.0
2D27041
EPA 8260D
04/27/22 16:33
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
Toluene-d8
4.8
1
5.00
96 %
75-125
2D27041
EPA 8260D
041271221633
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 of 69

(� �Eo
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2DI8032 - EPA 5030B MS
Blank (2D38032-BLK1) Prepared: 04/18/2022 14:00 Analyzed: 04/18/2022 17:46
Analvte
Result
Flaq
POL
Units
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D28032 - EPA 5030B MS - Continued
Blank (2D38032-BLK1) Continued Prepared: 04/18/2022 14:00 Analyzed: 04/18/2022 17:46
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
48
u91L
50.0 96 53-136
Dibromofluoromethane
51
u91L
50.0 101 67-129
Toluene-d8
52
u91L
50.0 105 59-134
LCS (2D18032-BSI)
Prepared: 04/18/2022 14:00 Analyzed: 04/18/2022 15:55
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
90
75-133
Benzene
18
1.0
ug/L
20.0
88
80-134
Chlorobenzene
18
1.0
ug/L
20.0
88
80-120
Toluene
17
1.0
ug/L
20.0
87
71-120
Trichloroethene
17
1.0
ug/L
20.0
85
74-120
4-Bromofluorobenzene
45
u91L
50.0
90
53-136
Dibromofluoromethane
47
u91L
50.0
93
67-129
Toluene-d8
52
u91L
50.0
105
59-134
Matrix Spike (21318032-1VIS1)
Prepared: 04/18/2022 14:00 Analyzed: 04/18/2022 16:22
Source: CF05306-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
99
75-133
Benzene
20
1.0
ug/L
20.0
0.15 U
99
80-134
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
99
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
93
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
94
74-120
4-Bromofluorobenzene
46
u91L
50.0
93
53-136
Dibromofluoromethane
51
u91L
50.0
101
67-129
Toluene-d8
52
u91L
50.0
105
59-134
Matrix Spike Dup (2D18032-MSD1)
Prepared: 04/18/2022 14:00 Analyzed: 04/18/2022 16:50
Source: CF05306-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
93
75-133
6
20
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
6
17
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
97
80-120
2
16
Toluene
18
1.0
ug/L
20.0
0.14 U
91
71-120
2
17
Trichloroethene
18
1.0
ug/L
20.0
0.15 U
90
74-120
5
22
4-Bromofluorobenzene 48 u91L 50.0 96 53-136
Dibromofluoromethane 49 u91L 50.0 98 67-129
Toluene-d8 52 u91L 50.0 104 59-134
Batch 2D19028 - EPA 5030B MS
Blank (2D39028-BLK3) Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 20:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L
1,1,1-Trichloroethane 0.12 U 1.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D2902B - EPA 5030B MS - Continued
Blank (2D39028-BLK1) Continued Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 20:07
Analvte
Result
Flaq
POL
Units
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC
Level Result %REC Limits
RPD
RPD Limit Notes
4-Bromofluorobenzene 50 u91L 50.0 99 53-136
Dibromofluoromethane 53 u91L 50.0 107 67-129
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D2902B - EPA 5030B MS - Continued
Blank (2D39028-BLK1) Continued Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 20:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 59 u91L 50.0 118 59-134
LCS (21319028-BS1) Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 18:16
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
96
75-133
Benzene
18
1.0
ug/L
20.0
88
80-134
Chlorobenzene
18
1.0
ug/L
20.0
88
80-120
Toluene
18
1.0
ug/L
20.0
91
71-120
Trichloroethene
18
1.0
ug/L
20.0
91
74-120
4-Bromofluorobenzene
48
u91L
50.0
96
53-136
Dibromofluoromethane
50
u91L
50.0
101
67-129
Toluene-d8
51
u91L
50.0
102
59-134
Matrix Spike (21319028-MS1)
Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 18:44
Source: CF05306-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
94
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
95
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
95
74-120
4-Bromofluorobenzene
49
u91L
50.0
98
53-136
Dibromofluoromethane
47
u91L
50.0
95
67-129
Toluene-d8
55
u91L
50.0
109
59-134
Matrix Spike Dup (21319028-MS131)
Prepared: 04/19/2022 16:30 Analyzed: 04/19/2022 19:12
Source: CF05306-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
95
75-133
1
20
Benzene
20
1.0
ug/L
20.0
0.15 U
99
80-134
3
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
98
80-120
3
16
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
6
17
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
86
74-120
10
22
4-Bromofluorobenzene 48 u91L 50.0 95 53-136
Dibromofluoromethane 49 u91L 50.0 99 67-129
Toluene-& 54 u91L 50.0 108 59-134
Batch 2D19031 - EPA 5030B MS
Blank (2D39031-BLK3) Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:58
Spike Source %REC
Analvte
Result
Flaq
POL
Units Level Result %REC Limits
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full
Page 44 of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D29031 - EPA 5030B MS - Continued
Blank (2D39031-BLK1) Continued Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:58
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 47 u91L 50.0 95 53-136
Dibromofluoromethane 46 u91L 50.0 97 67-129
Toluene-d8 54 u91L 50.0 107 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D29031 - EPA 5030B MS - Continued
LCS (211319031-BSI) Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 07:08
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
94
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
94
80-120
Toluene
18
1.0
ug/L
20.0
92
71-120
Trichloroethene
17
1.0
ug/L
20.0
87
74-120
4-Bromofluorobenzene
49
u91L
50.0
97
53-136
Dibromofluoromethane
49
u91L
50.0
98
67-129
Toluene-d8
53
u91L
50.0
107
59-134
Matrix Spike (2D19031-MS1)
Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 07:36
Source: CF05306-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
0.21 U
83
75-133
Benzene
17
1.0
ug/L
20.0
0.15 U
87
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
90
80-120
Toluene
17
1.0
ug/L
20.0
0.14 U
86
71-120
Trichloroethene
15
1.0
ug/L
20.0
0.15 U
75
74-120
4-Bromofluorobenzene
49
u91L
50.0
99
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
52
u91L
50.0
104
59-134
Matrix Spike Dup (2D19031-MSD1)
Prepared: 04/19/2022 19:47 Analyzed: 04/20/2022 08:03
Source: CF05306-06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
97
75-133
15
20
Benzene
21
1.0
ug/L
20.0
0.15 U
107
80-134
20
17
QM-11
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
106
80-120
16
16
Toluene
20
1.0
ug/L
20.0
0.14 U
99
71-120
14
17
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
105
74-120
33
22
QM-11
4-Bromofluorobenzene 51 u91L 50.0 101 53-136
Dibromofluoromethane 47 u91L 50.0 94 67-129
Toluene-d8 54 u91L 50.0 109 59-134
Batch 2D21036 - EPA 5030B MS
Blank (2D21036-BLK3) Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:56
Spike Source %REC
Analvte
Result
Flaq
POL
Units Level Result %REC Limits
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D21036 - EPA 5030B MS - Continued
Blank (2D21036-BLK1) Continued Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:56
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
49
ug/L
50.0
97
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
52
u91L
50.0
104
59-134
LCS (21323036-BSI)
Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 05:06
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
91
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D21036 - EPA 5030B MS - Continued
LCS (2D21036-BSI) Continued Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 05:06
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Chlorobenzene
19
1.0
ug/L
20.0 97 80-120
Toluene
18
1.0
ug/L
20.0 92 71-120
Trichloroethene
19
1.0
ug/L
20.0 97 74-120
4-Bromofluorobenzene
53
u91L
50.0 105 53-136
Dibromofluoromethane
50
u91L
50.0 99 67-129
Toluene-d8
55
u91L
50.0 109 59-134
Matrix Spike (2D23036-MS1)
Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 05:33
Source: CF05306-03
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
91
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
97
80-120
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
93
74-120
4-Bromofluorobenzene
51
u91L
50.0
101
53-136
Dibromofluoromethane
51
u91L
50.0
102
67-129
Toluene-d8
51
u91L
50.0
102
59-134
Matrix Spike Dup (21323036-MS131)
Prepared: 04/21/2022 19:08 Analyzed: 04/22/2022 06:01
Source: CF05306-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
99
75-133
8
20
Benzene
19
1.0
ug/L
20.0
0.15 U
97
80-134
1
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
102
80-120
5
16
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
5
17
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
4
22
4-Bromofluorobenzene 51 u91L 50.0 101 53-136
Dibromofluoromethane 48 u91L 50.0 97 67-129
Toluene-d8 54 u91L 50.0 108 59-134
Batch 2D26024 - EPA 5030B MS
Blank (2D26024-BLK3) Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 20:21
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dich loroethane
1,1-Dichloroethene
1, 2, 3-Trich I o rop ropa ne
1,2-Di bromo-3-ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.17
U
1.0
ug/L
0.12
U
1.0
ug/L
0.28
U
1.0
ug/L
0.14
U
1.0
ug/L
0.13
U
1.0
ug/L
0.21
U
1.0
ug/L
0.23
U
1.0
ug/L
0.48
U
1.0
ug/L
0.66
U
1.0
ug/L
0.19
U
1.0
ug/L
0.21
U
1.0
ug/L
0.10
U
1.0
ug/L
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 48 of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D26024 - EPA 5030B MS - Continued
Blank (2D26024-BLK1) Continued Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 20:21
Analvte
Result
Flaq
POL
Units
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 47
u91L
50.0 95 53-136
Dibromofluoromethane 52
u91L
50.0 105 67-129
Toluene-d8 56
u91L
50.0 112 59-134
LCS (21326024-BSI)
Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 18:30
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
90
75-133
Benzene
19
1.0
ug/L
20.0
94
80-134
Chlorobenzene
20
1.0
ug/L
20.0
98
80-120
Toluene
18
1.0
ug/L
20.0
92
71-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2D26024 - EPA 5030B MS - Continued
LCS (2D26024-BSI) Continued Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 18:30
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Trichloroethene
19
1.0
ug/L
20.0
95
74-120
4-Bromofluorobenzene
49
u91L
50.0
97
53-136
Dibromofluoromethane
50
u91L
50.0
100
67-129
Toluene-d8
53
u91L
50.0
106
59-134
Matrix Spike (2D26024-MS1)
Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 18:58
Source: CF05306-04
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
100
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
96
80-134
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
99
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
94
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
4-Bromofluorobenzene
50
u91L
50.0
100
53-136
Dibromofluoromethane
49
u91L
50.0
98
67-129
Toluene-d8
54
u91L
50.0
107
59-134
Matrix Spike Dup (21326024-MS131)
Prepared: 04/26/2022 16:30 Analyzed: 04/26/2022 19:25
Source: CF05306-04
Spike
Source
%REC
RPD
Analvte
Result Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
102
75-133
2
20
Benzene
20
1.0
ug/L
20.0
0.15 U
101
80-134
5
17
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
100
80-120
2
16
Toluene
18
1.0
ug/L
20.0
0.14 U
89
71-120
6
17
Trichloroethene
18
1.0
ug/L
20.0
0.15 U
88
74-120
10
22
4-Bromofluorobenzene 54 u91L 50.0 108 53-136
Dibromofluoromethane 54 u91L 50.0 108 67-129
Toluene-d8 54 u91L 50.0 109 59-134
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2DIS002 - EPA 3005A
Blank (2D38002-BLK3) Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:39
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (21318002-BSI)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:43
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Antimony
21.1
1.00
ug/L
20.0
106
80-120
Selenium
21.3
1.00
ug/L
20.0
106
80-120
Thallium
19.8
1.00
ug/L
20.0
99
80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2DIS002 - EPA 3005A - Continued
Matrix Spike (2D18002-MS3)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:52
Source: CF04529-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
42.2
2.00
ug/L
40.0 0.740 U 105 75-125
Selenium
41.6
2.00
ug/L
40.0 1.82 U 104 75-125
Thallium
39.8
2.00
ug/L
40.0 0.220 U 100 75-125
Matrix Spike Dup (2D18002-MSD1)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 11:56
Source: CF04529-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
43.6
2.00
ug/L
40.0 0.740 U 109 75-125 3
20
Selenium
41.9
2.00
ug/L
40.0 1.82 U 105 75-125 0.7
20
Thallium
39.5
2.00
ug/L
40.0 0.220 U 99 75-125 0.9
20
Post Spike (2D18002-PS1)
Prepared: 04/18/2022 02:07 Analyzed: 04/21/2022 12:35
Source: CF04529-01
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
21.1
1.00
ug/L
20.0 0.0493 105 75-125
Selenium
19.6
1.00
ug/L
20.0 -0.167 98 75-125
Thallium
19.4
1.00
ug/L
20.0 0.00656 97 75-125
Batch 2D19006 - EPA 3005A
Blank (2D39006-BLK1)
Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 08:59
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
Blank (2D19006-BLK2)
Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 09:05
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2DI9006 - EPA 3005A - Continued
Blank (2D39006-BLK2) Continued Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 09:05
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2D19006-BSI)
Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 09:11
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
207
10.0
ug/L
200
104 80-120
Barium
205
10.0
ug/L
200
103 80-120
Beryllium
20.4
1.00
ug/L
20.0
102 80-120
Cadmium
20.7
1.00
ug/L
20.0
103 80-120
Chromium
205
10.0
ug/L
200
102 80-120
Cobalt
208
10.0
ug/L
200
104 80-120
Copper
203
10.0
ug/L
200
101 80-120
Lead
205
10.0
ug/L
200
102 80-120
Nickel
204
10.0
ug/L
200
102 80-120
Silver
202
10.0
ug/L
200
101 80-120
Vanadium
202
10.0
ug/L
200
101 80-120
Zinc
208
10.0
ug/L
200
104 80-120
Matrix Spike (2D19006-MS3)
Prepared:
04/19/2022
08:01 Analyzed: 04/22/2022 09:14
Source: CF04852-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
198
10.0
ug/L
200
7.60 U
99 75-125
Barium
264
10.0
ug/L
200
63.3
100 75-125
Beryllium
19.3
1.00
ug/L
20.0
0.160 U
96 75-125
Cadmium
20.9
1.00
ug/L
20.0
0.584
101 75-125
Chromium
197
10.0
ug/L
200
1.40 U
98 75-125
Cobalt
199
10.0
ug/L
200
1.40 U
100 75-125
Copper
192
10.0
ug/L
200
1.60 U
96 75-125
Lead
203
10.0
ug/L
200
3.10 U
102 75-125
Nickel
204
10.0
ug/L
200
2.20 U
102 75-125
Silver
200
10.0
ug/L
200
1.90 U
100 75-125
Vanadium
203
10.0
ug/L
200
3.64
99 75-125
Zinc
208
10.0
ug/L
200
4.40 U
104 75-125
Matrix Spike Dup (2D19006-MSD1)
Prepared:
04/19/2022
08:01 Analyzed: 04/22/2022 09:17
Source: CF04852-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
192
10.0
ug/L
200
7.60 U
96
75-125
3
20
Barium
263
10.0
ug/L
200
63.3
100
75-125
0.5
20
Beryllium
19.0
1.00
ug/L
20.0
0.160 U
95
75-125
1
20
Cadmium
20.8
1.00
ug/L
20.0
0.584
101
75-125
0.5
20
Chromium
195
10.0
ug/L
200
1.40 U
98
75-125
0.9
20
Cobalt
198
10.0
ug/L
200
1.40 U
99
75-125
0.4
20
Copper
191
10.0
ug/L
200
1.60 U
95
75-125
0.7
20
Lead
200
10.0
ug/L
200
3.10 U
100
75-125
2
20
Nickel
203
10.0
ug/L
200
2.20 U
102
75-125
0.3
20
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be
reproduced in
full.
Page 52 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2DI9006 - EPA 3005A - Continued
Matrix Spike Dup (2D19006-MSD1) Continued
Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 09:17
Source: CF04852-03
Spike Source %REC
RPD
Analvte Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Silver 197
10.0
ug/L
200 1.90 U 98 75-125 1
20
Vanadium 201
10.0
ug/L
200 3.64 99 75-125 0.9
20
Zinc 208
10.0
ug/L
200 4.40 U 104 75-125 0.4
20
Post Spike (2D19006-PS1)
Prepared: 04/19/2022 08:01 Analyzed: 04/22/2022 09:19
Source: CF04852-03
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.204
0.0100
mg/L
0.200
-0.00138
102
80-120
Barium
0.268
0.0100
mg/L
0.200
0.0633
103
80-120
Beryllium
0.0199
0.00100
mg/L
0.0200
-0.000595
100
80-120
Cadmium
0.0214
0.00100
mg/L
0.0200
0.000584
104
80-120
Chromium
0.204
0.0100
mg/L
0.200
-0.000483
102
80-120
Cobalt
0.205
0.0100
mg/L
0.200
0.000674
102
80-120
Copper
0.198
0.0100
mg/L
0.200
-0.00402
99
80-120
Lead
0.210
0.0100
mg/L
0.200
0.00163
104
80-120
Nickel
0.211
0.0100
mg/L
0.200
0.000665
105
80-120
Silver
0.211
0.0100
mg/L
0.200
-0.00129
106
80-120
Vanadium
0.208
0.0100
mg/L
0.200
0.00364
102
80-120
Zinc
0.216
0.0100
mg/L
0.200
0.00257
107
80-120
Batch 1D20001 - EPA 3005A
Blank (2D20001-BLK1)
Prepared:
04/20/2022
01:23 Analyzed: 04/20/2022 14:53
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2D20001-BSI)
Prepared: 04/20/2022 01:23 Analyzed: 04/20/2022 14:59
Spike
Source
%REC
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits
Arsenic
205
10.0
ug/L
200
102
80-120
Barium
203
10.0
ug/L
200
102
80-120
Beryllium
20.3
1.00
ug/L
20.0
102
80-120
Cadmium
20.4
1.00
ug/L
20.0
102
80-120
Chromium
202
10.0
ug/L
200
101
80-120
Cobalt
207
10.0
ug/L
200
103
80-120
Copper
200
10.0
ug/L
200
100
80-120
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 53 of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D20001 - EPA 3005A - Continued
LCS (2D20001-BSI) Continued Prepared: 04/20/2022 01:23 Analyzed: 04/20/2022 14:59
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Lead
205
10.0
ug/L
200
102
80-120
Nickel
202
10.0
ug/L
200
101
80-120
Silver
200
10.0
ug/L
200
100
80-120
Vanadium
198
10.0
ug/L
200
99
80-120
Zinc
206
10.0
ug/L
200
103
80-120
Matrix Spike (2D20001-MS3)
Prepared:
04/20/2022
01:23 Analyzed: 04/20/2022 15:01
Source: CF04526-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
199
10.0
ug/L
200
7.60 U
100
75-125
Barium
860
10.0
ug/L
200
693
83
75-125
Beryllium
20.4
1.00
ug/L
20.0
0.160 U
102
75-125
Cadmium
19.0
1.00
ug/L
20.0
0.360 U
95
75-125
Chromium
201
10.0
ug/L
200
1.40 U
101
75-125
Cobalt
199
10.0
ug/L
200
1.40 U
99
75-125
Copper
190
10.0
ug/L
200
1.60 U
95
75-125
Lead
197
10.0
ug/L
200
3.10 U
99
75-125
Nickel
201
10.0
ug/L
200
2.20 U
101
75-125
Silver
200
10.0
ug/L
200
1.90 U
100
75-125
Vanadium
197
10.0
ug/L
200
1.40 U
99
75-125
Zinc
205
10.0
ug/L
200
4.40 U
103
75-125
Matrix Spike Dup (21320001-MS131)
Prepared:
04/20/2022
01:23 Analyzed: 04/20/2022 15:04
Source: CF04526-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
203
10.0
ug/L
200
7.60 U
102
75-125
2
20
Barium
870
10.0
ug/L
200
693
89
75-125
1
20
Beryllium
20.2
1.00
ug/L
20.0
0.160 U
101
75-125
0.7
20
Cadmium
18.8
1.00
ug/L
20.0
0.360 U
94
75-125
0.8
20
Chromium
199
10.0
ug/L
200
1.40 U
100
75-125
1
20
Cobalt
197
10.0
ug/L
200
1.40 U
99
75-125
0.9
20
Copper
188
10.0
ug/L
200
1.60 U
94
75-125
0.9
20
Lead
197
10.0
ug/L
200
3.10 U
99
75-125
0.08
20
Nickel
199
10.0
ug/L
200
2.20 U
100
75-125
0.9
20
Silver
197
10.0
ug/L
200
1.90 U
99
75-125
1
20
Vanadium
195
10.0
ug/L
200
1.40 U
97
75-125
1
20
Zinc
205
10.0
ug/L
200
4.40 U
102
75-125
0.3
20
Post Spike (2D20001-PS1)
Prepared:
04/20/2022
01:23 Analyzed: 04/20/2022 15:07
Source: CF04526-03
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD Limit Notes
Arsenic
0.197
0.0100
mg/L
0.200
-0.00817
98
80-120
Barium
0.881
0.0100
mg/L
0.200
0.693
94
80-120
Beryllium
0.0206
0.00100
mg/L
0.0200
-4.32E-6
103
80-120
Cadmium
0.0190
0.00100
mg/L
0.0200
-0.000801
95
80-120
Chromium
0.202
0.0100
mg/L
0.200
0.000892
101
80-120
Cobalt
0.198
0.0100
mg/L
0.200
-0.000631
99
80-120
Copper
0.191
0.0100
mg/L
0.200
-0.00610
95
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and may only be
reproduced in
full.
Page 54 of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D20001 - EPA 3005A - Continued
Post Spike (21320001-13SI) Continued
Prepared: 04/20/2022 01:23 Analyzed: 04/20/2022 15:07
Source: CF04526-03
Spike
Source
%REC RPD
Analvte Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Lead 0.197
0.0100
mg/L
0.200
-0.00313
99
80-120
Nickel 0.201
0.0100
mg/L
0.200
-0.00172
100
80-120
Silver 0.205
0.0100
mg/L
0.200
-5.48E-5
103
80-120
Vanadium 0.197
0.0100
mg/L
0.200
-0.00315
99
80-120
Zinc 0.208
0.0100
mg/L
0.200
0.00111
103
80-120
Batch 2D22018 - EPA 3005A
Blank (2D22018-BLK3)
Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 09:45
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2D22018-BSI)
Prepared: 04/25/2022 15:12 Analyzed: 04/26/2022 09:52
Spike
Source %REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC Limits RPD Limit Notes
Arsenic
204
10.0
ug/L
200
102 80-120
Barium
209
10.0
ug/L
200
104 80-120
Beryllium
20.3
1.00
ug/L
20.0
101 80-120
Cadmium
20.2
1.00
ug/L
20.0
101 80-120
Chromium
203
10.0
ug/L
200
101 80-120
Cobalt
206
10.0
ug/L
200
103 80-120
Copper
203
10.0
ug/L
200
101 80-120
Lead
202
10.0
ug/L
200
101 80-120
Nickel
202
10.0
ug/L
200
101 80-120
Silver
203
10.0
ug/L
200
102 80-120
Vanadium
201
10.0
ug/L
200
101 80-120
Zinc
209
10.0
ug/L
200
104 80-120
Matrix Spike (2D22018-MS3)
Prepared:
04/25/2022 15:12 Analyzed: 04/26/2022 09:55
Source: CF04526-05
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
208
10.0
ug/L
200
7.60 U
104
75-125
Barium
427
10.0
ug/L
200
230
99
75-125
Beryllium
20.6
1.00
ug/L
20.0
0.160 U
103
75-125
Cadmium
19.8
1.00
ug/L
20.0
0.360 U
99
75-125
Chromium
203
10.0
ug/L
200
1.40 U
102
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D2201B - EPA 3005A - Continued
Matrix Spike (2D22018-MS3) Continued
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 09:55
Source: CF04526-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Cobalt
202
10.0
ug/L
200
1.40 U
101 75-125
Copper
198
10.0
ug/L
200
1.60 U
99 75-125
Lead
201
10.0
ug/L
200
3.10 U
101 75-125
Nickel
200
10.0
ug/L
200
2.20 U
100 75-125
Silver
204
10.0
ug/L
200
1.90 U
102 75-125
Vanadium
202
10.0
ug/L
200
1.40 U
101 75-125
Zinc
209
10.0
ug/L
200
4.40 U
104 75-125
Matrix Spike Dup (2D22018-MSD1)
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 09:58
Source: CF04526-05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
213
10.0
ug/L
200
7.60 U
107 75-125 2
20
Barium
437
10.0
ug/L
200
230
103 75-125 2
20
Beryllium
20.8
1.00
ug/L
20.0
0.160 U
104 75-125 1
20
Cadmium
20.2
1.00
ug/L
20.0
0.360 U
101 75-125 2
20
Chromium
207
10.0
ug/L
200
1.40 U
104 75-125 2
20
Cobalt
208
10.0
ug/L
200
1.40 U
104 75-125 3
20
Copper
201
10.0
ug/L
200
1.60 U
101 75-125 2
20
Lead
206
10.0
ug/L
200
3.10 U
103 75-125 2
20
Nickel
203
10.0
ug/L
200
2.20 U
102 75-125 2
20
Silver
206
10.0
ug/L
200
1.90 U
103 75-125 1
20
Vanadium
205
10.0
ug/L
200
1.40 U
102 75-125 2
20
Zinc
214
10.0
ug/L
200
4.40 U
107 75-125 2
20
Post Spike (2D22018-PS1)
Prepared:
04/25/2022
15:12 Analyzed: 04/26/2022 10:00
Source: CF04526-05
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.213
0.0100
mg/L
0.200
0.00662
103
80-120
Barium
0.434
0.0100
mg/L
0.200
0.230
102
80-120
Beryllium
0.0210
0.00100
mg/L
0.0200
3.39E-6
105
80-120
Cadmium
0.0206
0.00100
mg/L
0.0200
-0.000214
103
80-120
Chromium
0.207
0.0100
mg/L
0.200
0.00119
103
80-120
Cobalt
0.210
0.0100
mg/L
0.200
0.000999
104
80-120
Copper
0.202
0.0100
mg/L
0.200
-0.00108
101
80-120
Lead
0.209
0.0100
mg/L
0.200
0.000591
104
80-120
Nickel
0.205
0.0100
mg/L
0.200
0.00144
102
80-120
Silver
0.212
0.0100
mg/L
0.200
7.75E-5
106
80-120
Vanadium
0.205
0.0100
mg/L
0.200
-0.000793
103
80-120
Zinc
0.216
0.0100
mg/L
0.200
0.00437
106
80-120
Batch 2D29004 - EPA 3005A
Blank (2D29004-BLK3)
Prepared: 04/29/2022 05:18 Analyzed: 05/03/2022 09:30
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 56 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D29004 - EPA 3005A - Continued
Blank (2D29004-BLK1) Continued
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:30
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
Blank (2D29004-BLK2)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:34
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2D29004-BSI)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:39
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
205
10.0
ug/L
200
102 80-120
Barium
204
10.0
ug/L
200
102 80-120
Beryllium
20.4
1.00
ug/L
20.0
102 80-120
Cadmium
20.7
1.00
ug/L
20.0
103 80-120
Chromium
203
10.0
ug/L
200
102 80-120
Cobalt
209
10.0
ug/L
200
105 80-120
Copper
204
10.0
ug/L
200
102 80-120
Lead
206
10.0
ug/L
200
103 80-120
Nickel
204
10.0
ug/L
200
102 80-120
Silver
205
10.0
ug/L
200
102 80-120
Vanadium
201
10.0
ug/L
200
100 80-120
Zinc
206
10.0
ug/L
200
103 80-120
Matrix Spike (2D29004-MS1)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:42
Source: CF04294-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD Limit Notes
Arsenic
200
10.0
ug/L
200
7.60 U
100
75-125
Barium
245
10.0
ug/L
200
43.8
100
75-125
Beryllium
20.8
1.00
ug/L
20.0
0.300
103
75-125
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be
reproduced in
full.
Page 57 of 69

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D29004 - EPA 3005A - Continued
Matrix Spike (2D29004-MS3) Continued
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:42
Source: CF04294-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Cadmium
20.5
1.00
ug/L
20.0
0.360 U
102 75-125
Chromium
204
10.0
ug/L
200
1.60
101 75-125
Cobalt
206
10.0
ug/L
200
1.40 U
103 75-125
Copper
205
10.0
ug/L
200
4.92
100 75-125
Lead
207
10.0
ug/L
200
3.10 U
103 75-125
Nickel
202
10.0
ug/L
200
2.20 U
101 75-125
Silver
205
10.0
ug/L
200
1.90 U
102 75-125
Vanadium
201
10.0
ug/L
200
1.40 U
100 75-125
Zinc
500
10.0
ug/L
200
304
98 75-125
Matrix Spike (2D29004-MS2)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:55
Source: CF04294-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
204
10.0
ug/L
200
7.60 U
102 75-125
Barium
239
10.0
ug/L
200
40.5
99 75-125
Beryllium
20.5
1.00
ug/L
20.0
0.160 U
102 75-125
Cadmium
19.9
1.00
ug/L
20.0
0.360 U
99 75-125
Chromium
200
10.0
ug/L
200
1.40 U
100 75-125
Cobalt
203
10.0
ug/L
200
1.40 U
102 75-125
Copper
200
10.0
ug/L
200
1.60 U
100 75-125
Lead
202
10.0
ug/L
200
3.10 U
101 75-125
Nickel
197
10.0
ug/L
200
2.20 U
99 75-125
Silver
203
10.0
ug/L
200
1.90 U
101 75-125
Vanadium
197
10.0
ug/L
200
1.40 U
99 75-125
Zinc
219
10.0
ug/L
200
16.5
101 75-125
Matrix Spike Dup (2D29004-MSD1)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:44
Source: CF04294-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
200
10.0
ug/L
200
7.60 U
100 75-125 0.2
20
Barium
243
10.0
ug/L
200
43.8
100 75-125 0.6
20
Beryllium
20.8
1.00
ug/L
20.0
0.300
102 75-125 0.2
20
Cadmium
20.4
1.00
ug/L
20.0
0.360 U
102 75-125 0.08
20
Chromium
203
10.0
ug/L
200
1.60
101 75-125 0.8
20
Cobalt
205
10.0
ug/L
200
1.40 U
102 75-125 0.8
20
Copper
204
10.0
ug/L
200
4.92
100 75-125 0.7
20
Lead
205
10.0
ug/L
200
3.10 U
102 75-125 1
20
Nickel
201
10.0
ug/L
200
2.20 U
100 75-125 0.5
20
Silver
204
10.0
ug/L
200
1.90 U
102 75-125 0.5
20
Vanadium
199
10.0
ug/L
200
1.40 U
99 75-125 0.8
20
Zinc
499
10.0
ug/L
200
304
98 75-125 0.2
20
Post Spike (2D29004-PS1)
Prepared:
04/29/2022
05:18 Analyzed: 05/03/2022 09:47
Source: CF04294-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD Limit Notes
Arsenic
0.205
0.0100
mg/L
0.200
-0.00310
103
80-120
Barium
0.249
0.0100
mg/L
0.200
0.0438
103
80-120
Beryllium
0.0214
0.00100
mg/L
0.0200
0.000300
106
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be
reproduced in
full.
Page 58 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2D29004 - EPA 3005A - Continued
Post Spike (2D29004-PS1) Continued
Prepared: 04/29/2022 05:18 Analyzed: 05/03/2022 09:47
Source: CF04294-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Cadmium
0.0208
0.00100
mg/L
0.0200
9.75E-6
104
80-120
Chromium
0.209
0.0100
mg/L
0.200
0.00160
104
80-120
Cobalt
0.211
0.0100
mg/L
0.200
0.000842
105
80-120
Copper
0.212
0.0100
mg/L
0.200
0.00492
103
80-120
Lead
0.208
0.0100
mg/L
0.200
0.00194
103
80-120
Nickel
0.206
0.0100
mg/L
0.200
0.000250
103
80-120
Silver
0.209
0.0100
mg/L
0.200
0.000463
104
80-120
Vanadium
0.205
0.0100
mg/L
0.200
-0.000492
103
80-120
Zinc
0.503
0.0100
mg/L
0.200
0.304
100
80-120
Batch 2EO2001 - EPA 3005A
Blank (2E02001-BLK1)
Prepared: 05/02/2022 01:24 Analyzed: 05/03/2022 10:59
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2E02001-BSI)
Prepared: 05/02/2022 01:24 Analyzed: 05/03/2022 11:35
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
202
10.0
ug/L
200
101
80-120
Barium
201
10.0
ug/L
200
101
80-120
Beryllium
20.2
1.00
ug/L
20.0
101
80-120
Cadmium
20.3
1.00
ug/L
20.0
101
80-120
Chromium
200
10.0
ug/L
200
100
80-120
Cobalt
206
10.0
ug/L
200
103
80-120
Copper
202
10.0
ug/L
200
101
80-120
Lead
203
10.0
ug/L
200
102
80-120
Nickel
201
10.0
ug/L
200
101
80-120
Silver
202
10.0
ug/L
200
101
80-120
Vanadium
197
10.0
ug/L
200
99
80-120
Zinc
203
10.0
ug/L
200
101
80-120
Matrix Spike (2E02001-MS3)
Prepared:
05/02/2022
01:24 Analyzed: 05/03/2022 11:37
Source: CF05211-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
201
10.0
ug/L
200
7.60 U
101
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 Of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2E02001 - EPA 3005A - Continued
Matrix Spike (2E02001-MS3) Continued
Prepared:
05/02/2022
01:24 Analyzed: 05/03/2022 11:37
Source: CF05211-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Barium
208
10.0
ug/L
200
6.36
101 75-125
Beryllium
20.4
1.00
ug/L
20.0
0.160 U
102 75-125
Cadmium
20.4
1.00
ug/L
20.0
0.360 U
102 75-125
Chromium
202
10.0
ug/L
200
1.40 U
101 75-125
Cobalt
207
10.0
ug/L
200
1.40 U
104 75-125
Copper
202
10.0
ug/L
200
1.60 U
101 75-125
Lead
203
10.0
ug/L
200
3.10 U
102 75-125
Nickel
200
10.0
ug/L
200
2.20 U
100 75-125
Silver
203
10.0
ug/L
200
1.90 U
102 75-125
Vanadium
198
10.0
ug/L
200
1.40 U
99 75-125
Zinc
202
10.0
ug/L
200
4.40 U
101 75-125
Matrix Spike Dup (2E02001-MSD1)
Prepared:
05/02/2022
01:24 Analyzed: 05/03/2022 11:40
Source: CF05211-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
201
10.0
ug/L
200
7.60 U
100 75-125 0.3
20
Barium
205
10.0
ug/L
200
6.36
99 75-125 2
20
Beryllium
20.0
1.00
ug/L
20.0
0.160 U
100 75-125 2
20
Cadmium
19.9
1.00
ug/L
20.0
0.360 U
99 75-125 3
20
Chromium
199
10.0
ug/L
200
1.40 U
99 75-125 2
20
Cobalt
202
10.0
ug/L
200
1.40 U
101 75-125 2
20
Copper
199
10.0
ug/L
200
1.60 U
100 75-125 1
20
Lead
198
10.0
ug/L
200
3.10 U
99 75-125 3
20
Nickel
198
10.0
ug/L
200
2.20 U
99 75-125 1
20
Silver
200
10.0
ug/L
200
1.90 U
100 75-125 2
20
Vanadium
196
10.0
ug/L
200
1.40 U
98 75-125 1
20
Zinc
199
10.0
ug/L
200
4.40 U
99 75-125 2
20
Post Spike (2E02001-PSI)
Prepared:
05/02/2022
01:24 Analyzed: 05/03/2022 11:43
Source: CF05211-01
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.206
0.0100
mg/L
0.200
-0.00181
103
80-120
Barium
0.216
0.0100
mg/L
0.200
0.00636
105
80-120
Beryllium
0.0210
0.00100
mg/L
0.0200
-1.06E-5
105
80-120
Cadmium
0.0209
0.00100
mg/L
0.0200
0.000175
104
80-120
Chromium
0.210
0.0100
mg/L
0.200
-2.09E-5
105
80-120
Cobalt
0.214
0.0100
mg/L
0.200
0.000870
107
80-120
Copper
0.211
0.0100
mg/L
0.200
0.00103
105
80-120
Lead
0.210
0.0100
mg/L
0.200
-0.00370
105
80-120
Nickel
0.208
0.0100
mg/L
0.200
0.000363
104
80-120
Silver
0.211
0.0100
mg/L
0.200
0.000812
105
80-120
Vanadium
0.206
0.0100
mg/L
0.200
0.000142
103
80-120
Zinc
0.209
0.0100
mg/L
0.200
0.00102
104
80-120
Batch 2E02002 - EPA 3005A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 of 69

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2EO2002 - EPA 3005A - Continued
Blank (2E02002-BLK1)
Prepared: 05/02/2022 01:30 Analyzed: 05/05/2022 09:13
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2E02002-BSI)
Prepared: 05/02/2022 01:30 Analyzed: 05/05/2022 09:18
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Antimony
20.4
1.00
ug/L
20.0
102
80-120
Selenium
20.0
1.00
ug/L
20.0
100
80-120
Thallium
20.7
1.00
ug/L
20.0
104
80-120
Matrix Spike (2E02002-MS3)
Prepared: 05/02/2022 01:30 Analyzed: 05/05/2022 09:27
Source: CF05798-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Antimony
42.8
2.00
ug/L
40.0
0.740 U
107
75-125
Selenium
39.3
2.00
ug/L
40.0
1.82 U
98
75-125
Thallium
40.1
2.00
ug/L
40.0
0.220 U
100
75-125
Matrix Spike Dup (2E02002-MSDS)
Prepared: 05/02/2022 01:30 Analyzed: 05/05/2022 09:32
Source: CF05798-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Antimony
42.1
2.00
ug/L
40.0
0.740 U
105
75-125 2
20
Selenium
39.5
2.00
ug/L
40.0
1.82 U
99
75-125 0.4
20
Thallium
40.4
2.00
ug/L
40.0
0.220 U
101
75-125 0.6
20
Post Spike (2E02002-PS1)
Prepared: 05/02/2022 01:30 Analyzed: 05/05/2022 09:36
Source: CF05798-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Antimony
21.3
1.00
ug/L
20.0
0.00397
106
75-125
Selenium
20.6
1.00
ug/L
20.0
0.0530
103
75-125
Thallium
20.3
1.00
ug/L
20.0
0.0220
101
75-125
Volatile Organic Compounds by GCMS SIM Isotope Dilution
- Quality Control
Batch 2D19038 - EPA 5030E MS
Blank (2D39038-BLK3) Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 22:59
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 0.80 U 2.0 ug/L
Toluene-& 4.8 u91L 5.00 96 75-125
LCS (2D19038-BSI) Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 21:17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 23 2.0 ug/L 25.0 94 80-133
Toluene-& 5.1 u91L 5.00 103 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 Of 69

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2D2903B - EPA 5030B MS - Continued
Matrix Spike (21)19038-MS3)
Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 21:42
Source: CF04526-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
23
2.0
ug/L
25.0
0.80 U
90 80-133
Toluene-d8
4.9
u91L
5.00
97 75-125
Matrix Spike Dup (21319038-MS131)
Prepared: 04/19/2022 12:59 Analyzed: 04/19/2022 22:08
Source: CF04526-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
22
2.0
ug/L
25.0
0.80 U
89 80-133 2
19
Toluene-d8
4.8
u91L
5.00
97 75-125
Batch 2D27041 - EPA 5030E MS
Blank (2D27041-BLK3)
Prepared: 04/27/2022 00:00 Analyzed: 04/27/2022 12:57
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dioxane
0.80 U
2.0
ug/L
Toluene-d8
4.8
u91L
5.00 96 75-125
LCS (2D27041-BS1)
Prepared: 04/27/2022 00:00 Analyzed: 04/27/2022 12:32
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
24
2.0
ug/L
25.0 96 80-133
Toluene-d8
4.9
u91L
5.00 98 75-125
Matrix Spike (2D27041-MS1)
Prepared: 04/27/2022 00:00 Analyzed: 04/27/2022 21:16
Source: CF05798-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
1,4-Dioxane
24
2.0
ug/L
25.0 0.80 U 95 80-133
Toluene-d8
5.0
u91L
5.00 99 75-125
Matrix Spike Dup (21327041-MS131)
Prepared: 04/27/2022 00:00 Analyzed: 04/27/2022 21:41
Source: CF05798-01
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
1,4-Dioxane
24 2.0
ug/L
25.0 0.80 U 94 80-133 1 19
Toluene-d8
4.8
u91L
5.00 96 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 62 Of 69

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QI-02 Internal standard outside acceptance limits. Samples results are considered estimated.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 of 69

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Sample Preservation Verification
ENCO Cary
ENCC
Work Order: CF04526 Project: Anson LF
Client: S&ME, Inc. (SM011) Project #: 4140-15-007
Lagged In: 15-Apr-22 10:46 Logged By: Samantha L tatt Preservation Check Performed By: „ Date/Time: 1 2Z 100 W
CF04526-01
Cant
Type
.
Pres (pH)
Requirement
pH Checked /
-fn Control
Datef ime
pl Ad usted Adjusted
;--�,
Reagent Used/Comments
A
250mLP+HNO3
<2
Y /, N/ NA
Y N P NA
CF04526-02
Cont
Type,
yp
Pres (pH)
pH Checked I
-°In
DatelTime
pH Adjusted
Reagent Used/Comments
Requirement
Control
Adiusted
A
250mLP+HNO3
<2
Y N / NA
Y /N I,NA
CF04526-03
Cont
Type
yp
Pres (pH)
Requirement
pH Checked /
-fri Control
DatefT-ime
pH Adjusted Adjusted
Reagent UsedlComments
A
250mLP+HNO3
<2
Y ) N / NA
YIN !, NA
C F04526-04
Cant
Type
Pres (pH)
pH Checked f
j k'n, Control
Date/Time
pH Adjusted
Adjusted
Reagent Used/CommentsRequirement
A
250mLP+HNO3
<2
Y/ N I NA
Y 1 N ,1 NA
j
CF04526-05
Cont
Type
-
Pres (pH)
Requirement
pH Chocked/
in Control
Date/Time
PH Adjusted
Adjusted
Reagent UsedlComments
A
250mLP+HNO3
<2
Y I N/ NA
Y II(N J NA
CF04526-06 '
Cont
Type
Yp
Pres (pH)
pH Checked /
DaterFtme
PH Adjusted Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
(Y l N/ NA
Y I N 1 NA
CF04526-07
Cont
T e
Pres (pH)
Requirement
pH Checked i
l Controj
Date/TimeYP
pH AdjustedDate/TimeReagent
Used/Comments
A
250mLP+HNO3
<2
Y )N / NA
I Y / N` NA
CF04526-08
Cont
T e
YR
Pres (pH)
Requirement
pH Checked /
In, Control
Date/Time
PH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y 1+ N / NA
Y / ,t ! NA
Rea ent Name ID
1
2
pH Strip ID:
Reagent Name ID
3
4
Reactent Name ID
5
6 -
C:IELMNT1Printlwko_PreservationCheck, rpt I Page 66 of 69

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Sample Preservation Verification
ENCO Cary19 C� 1C.
CCMJ=
`.
Work Order CF05798 Project: Anson LF
Client: SME, Inc. (SM011) Project #: 4140-15-007
Logged In: 26-Apr-22 12:54 Logged By: Rachel Ann oni h
Preservation Check Performed By: _ Date/Time:
CF05798-01
Cant
Type
Pres (PH)
Requirement
PH Checked/
In Control
Dateliime
PH Adjusted Adjusted
Reagent Used/Comments
A
250mLP+HNO3
1 2
Y N/ NA
I Y I N i NA
CF05798-02
Cont
Type
Pres (pH)
Requirement
pH Checked/
In Control
1 I)H Adjusted Date/Time
Adjusted
Reagent Used/comments
A
250mLP+HNO3
<2
Y'11 N / NA
I Y N NA
CFO.5798-03
Cont
Type
Pres (PH)
Requirement
pH Checked I
In Control
PH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y / N / NA
Y !` N ,1 NA
C F05798-04
Cont
Type
Pres (pH)
pH Checked 1
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adjusted
A
25OmLP+HNO3 .
=2
Y 1 N / NA
Y N` / NA
CF05798-05
Cont
Type
Pres (pH)
Requirement
pH Checked !
in Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y J N I NA
Y 1(N NA
CF05798-06
Cont
Type
Pres (pH)
Requirement 1--.,In
pH Checked 1
Contras
Date/Time
pH Adjusted Adjusted
I
Reagent Used/Comments
A
250mLP+HNO3
<2
Y)I N l NA
I Y l NA •
CF05798-07
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
PH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
91 N/ NA
Y N l NA
CF05798-08
Conk
Type
Pres (PH)
Requirement
PH Checked /
e In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 1
Y I N I NA
Y N I NA
Rea ent Name !D
1
•2
pH Strip ID:
PH Strips C2AO640
Reagent Name ID
3
4
Reagent Name ID
51 .7T7
6
C:IelmntlPrii ...... _ .---'YMOU11L,rreUK.rpt
Page 69 of 69

ANSON COUNTY LANDFILL
WATER LEVELS ONLY - See Low Flow Forms for Purge/Sample Information for Monitoring Wells Sampled in April 2022
S&ME Project No. 4140-15-007
ID AS SHOWN ON MAP:
DEPTH TO WATER (TOC):
DEPTH TO WATER (BGS):
CASING
HEIGHT/STICK UP
(FT.):
TOTAL DEPTH OF WELL
(BGS).
DATE WATER
LEVEL
MEASURED:
MW-1 D
19.15
--
--
--
4/15/2022
MW-2S
12.70
--
--
--
4/15/2022
MW-2D
15.75
--
--
--
4/15/2022
MW-3S
6.09
--
--
--
4/19/2022
MW-3D
6.97
--
--
--
4/19/2022
MW-4S
5.78
--
--
--
4/15/2022
MW-4D
9.14
--
--
--
4/15/2022
MW-5S
6.01
--
--
--
4/19/2022
MW-5D
5.94
--
--
--
4/19/2022
MW-8S
16.85
--
--
--
4/15/2022
MW-8D
16.11
--
--
--
4/15/2022
MW-9S
15.41
--
--
--
4/14/2022
MW-10S
14.21
--
--
--
4/11/2022
MW-11 S
8.36
--
--
--
4/12/2022
GMW-12
9.54
--
--
55.09
4/11/2022
GMW-13
32.71
28.45
4.26
61.46
4/12/2022
GMW-14
39.01
35.04
3.97
51.97
4/12/2022
MW-15D
13.10
9.30
3.80
41.50
4/11/2022
*NOTE - MAP USED FOR FIELD SAMPLING WAS FIGURE #2 EXISTING GROUNDWATER WELL LOCATIONS FROM PHASE 3 BASELINE GW MONITORING REPORT (4-9-19)
No well tag on MW-3S, MW-5S

ANSON WASTE MANAGEMENT FACILITY
ANSON COUNTY, NORTH CAROLINA
SUMP SAMPLING LOG
S&ME PROJECT:
DATE:
PERSONNEL:
4140-15-007
4/26/2022
Skyler Schmal
SUMP #5 (Labelled at landfill as SUMP 3B)
Specific
Conductivity
Notes
Sample Time:
pH
(mS/sec)
10:35
6.72
3999+
Second #3 Sump/313
SUMP #7 (Labelled at landfill as SUMP 4B)
Specific
Conductivity
Notes
Sample Time:
pH
(mS/sec)
10:50
6.35
3999+
Second #4 Sump/413

ANSON WASTE MANAGEMENT FACILITY
ANSON COUNTY, NORTH CAROLINA
LEACHATE SAMPLING LOG
S&ME PROJECT: 4140-15-007
DATE:
PERSONNEL:
4/26/2022
Skyler Schmal
***Add temp & pH to C of C
LEACHATE SAMPLE
Field Readings
pH
1.33
Conductivity (mS/sec)
481
Temperature (°C)
27.4
Sample Time: 9:35

ANSON WASTE MANAGEMENT FACILITY
ANSON COUNTY, NORTH CAROLINA
SURFACE WATER SAMPLING LOG
S&ME Project No: 4140-15-007
PERSONNEL: J. Tavouga, K. Vassallo & S. Schmal
SURFACE WATER/UNDERDRAIN SAMPLE INFORMATION
Location
Sample Date
Sample Time
pH
Specific
Conductivity
(LIS/cm)
ORP (mV)
Temperature
(oC)
Turbidity
(ntu)
DO
(mg/L)
Comments
BG-1
Pinch Gut Creek Background
4/13/2022
15:00
7.22
74.4
105.7
17.4
26.76
4.49
SG-4
Pinch Gut Creek Downgradient
4/13/2022
13:50
7.66
90.0
98.4
17.9
23.71
4.44
BG-2
Brown Creek Background
4/13/2022
12:00
7.59
63.7
119.0
18.8
21.59
4.40
SG-3
Brown Creek Downgradient
4/13/2022
10:45
8.64
109.7
91.3
17.2
21.50
5.28
UD-1
Phase 26 Cell Outlet
4/14/2022
11:10
5.93
273.6
95.1
25.3
8.10
2.92
Former SG-5, close to MW-9 and sediment pond
UD-2
Smaller HOPE pipe
4/14/2022
11:35
6.03
85.2
185.2
23.9
5.10
4A6
Former UD 1E/2A - smaller diameter HDPE pipe
UD-3
Larger HDPE Pipe
NO FLOW AT TIME OF SAMPLING
Former UD 2C North - larger diameter HDPE i e

Project Name: Anson County Landfill I s
Project Location: 375 Dozer Drive, Polkton, INC s�
Project Number:
4140-15-007 Purge Date:
April 15, 2022
Source Well:
MW-1D Purge Time:
27 Minutes
Locked?:
Yes Sample Date:
April 15, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
11:30
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 11:27 0.7 100 19.59 16.7 6.71 329.9 2.24 97.2 5.2 End of Purging
Sample Method: Bladder Pump Sample Start Time: 11:30 Sample End Time: 11:35
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/15/2022
Notes: To convert ORP to Eh, add 205 mV to CRP.
Measuring Point:
Top of Casing
Depth to Water:
19.15
ft-TOC
Total Well Depth:
45.50
ft-TOC
Height of Water Column:
26.35
feet
Screen Length: 10 feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
4.3
Gal
3 *Well Volume
12.90
Gal
5 *Well Volume
21.50
Gal
Purge Method:
Bladder Pump
Start Time:
11:00
End Time:
11:27
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
0.7
Gallons
Dedicated bladder pump. Screen on well tag
Final Volume Purge Rate:
100
mL/mi
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
11:00
0.0
---
---
---
---
---
---
---
---
Start Purging
11:03
0.1
100
19.59
16.6
6.76
338.0
4.52
124.9
6.42
11:06
0.2
100
19.66
16.8
6.72
332.1
3.57
126.8
5.32
11:11
0.3
100
19.59
16.8
6.71
329.5
2.95
127.1
4.82
11:17
0.4
100
19.59
16.8
6.71
329.4
2.23
115.4
4.48
11:22
0.6
100
19.59
16.7
6.71
329.6
2.21
103.8
5.15
11:27
0.7
100
19.59
16.7
6.71
329.9
2.24
97.2
5.16
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

!11!1 =
F�m III IIII! I ITAR1111111011,11:1141
Project Name: Anson County Landfill
�r
Project Location: 375 Dozer Drive, Polkton, INC I
Project Number:
4140-15-007 Purge Date:
April 15, 2022
Source Well:
MW-2S Purge Time:
20 Minutes
Locked?:
Yes Sample Date:
April 15, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
10:00
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 09:55 0.8 150 16.00 17.1 4.79 256.9 5.32 283.7 4.91 End of Purging
Sample Method: Bladder Pump Sample Start Time: 10:00 Sample End Time: 10:05
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/14/2022
Notes: To convert CRP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
12.70
ft-TOC
Total Well Depth:
31.80
ft-TOC
Height of Water Column:
19.10
feet
Screen Length: 15 feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
3.1
Gal
3 *Well Volume
9.35
Gal
5 *Well Volume
15.58
Gal
Purge Method:
Bladder Pump
Start Time:
9:35
End Time:
9:55
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
0.8
Gallons
Dedicated bladder pump. Screen on well tag
Final Volume Purge Rate:
150
mL/mi
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
09:35
0.0
---
---
---
---
---
---
---
---
Start Purging
09:40
0.2
150
13.49
16.4
5.10
260.0
4.44
259.0
6.78
09:45
0.4
150
14.76
17.0
4.60
255.6
3.25
302.4
9.23
09:50
0.6
150
15.38
16.9
4.60
256.3
3.29
296.0
6.73
09:55
0.8
150
16.00
17.1
4.79
256.9
5.32
283.7
4.91
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
1,4-Dioxane 8260
3
250mL P
HCI
Form Revision Date: 2/12/18 16:00

s
• • • •'
Project Name: Anson County Landfill I
Project Location: 375 Dozer Drive, Polkton, NC
Project Number:
4140-15-007 Purge Date:
April 15, 2022
Source Well:
MW-2D Purge Time:
15 Minutes
Locked?:
Yes Sample Date:
April 15, 2022
Sampled By:
K. Vassallo & S. Schmal Sample Time:
10:30
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 10:25 0.4 100 17.05 17.6 6.15 316.9 2.05 78.8 20.78 End of Purging
Sample Method: Bladder Pump Sample Start Time: 10:30 Sample End Time: 10:35
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/15/2022
11
Notes: To convert ORP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
15.75
ft-TOC
Total Well Depth:
35.50
ft-TOC
Height of Water Column:
19.75
feet
Screen Length: 10 feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
3.2
Gal
3 *Well Volume
9.67
Gal
5 *Well Volume
16.11
Gal
Purge Method:
Bladder Pump
Start Time:
10:10
End Time:
10:25
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
0.4
Gallons
Dedicated bladder pump. Screen on well tag
Final Volume Purge Rate:
100
mL/mi
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
10:10
0.0
---
---
---
---
---
---
---
---
Start Purging
10:15
0.1
100
16.30
17.2
6.24
321.9
5.27
128.0
7.72
10:20
0.3
100
16.71
17.5
5.99
351.4
3.71
85.5
16.71
10:25
0.4
100
17.05
17.6
6.15
316.9
2.05
78.8
20.78
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

Project Name: Anson County Landfill I s
Project Location: 375 Dozer Drive, Polkton, INC s�
Project Number:
4140-15-007 Purge Date:
April 19, 2022
Source Well:
MW-3S Purge Time:
30 Minutes
Locked?:
Yes Sample Date:
April 19, 2022
Sampled By:
J. Tayouga & S. Schmal Sample Time:
10:10
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 10:00 1.6 200 8.19 19.9 5.72 368.2 1.64 322.2 8.52 End of Purging
Sample Method: Bladder Pump Sample Start Time: 10:10 Sample End Time: 10:10
Analytical Data
Name Signature Date
(1) Jasmine Tayouga 4/19/2022
Notes: To convert CRP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
6.09
ft-TOC
Total Well Depth:
20.50
ft-TOC
Height of Water Column:
14.41
feet
Screen Length: - feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
2.4
Gal
3 *Well Volume
7.05
Gal
5 *Well Volume
11.76
Gal
Purge Method:
Bladder Pump
Start Time:
9:30
End Time:
10:00
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
1.6
Gallons
Dedicated bladder pump. No well tag. MW-
DTW (TOC): 6.97'.
Final Volume Purge Rate:
200
mL/mifl3D
Well Purged Dry?:
No
(Yes/N
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
09:30
0.0
---
---
---
---
---
---
---
---
Start Purging
09:35
0.3
200
6.47
19.7
5.71
339.0
4.24
148.2
47.50
09:40
0.5
200
7.68
19.5
5.78
342.0
1.97
179.0
29.5
09:45
0.8
200
7.87
20.0
5.72
356.4
1.84
254.1
15.30
09:50
1.1
200
8.01
20.0
5.71
359.8
1.76
302.4
10.01
09:55
1.3
200
8.12
20.0
5.72
360.0
1.68
315.9
9.87
10:00
1.6
200
8.19
19.9
5.72
368.2
1.64
322.2
8.52
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

Project Name: Anson County Landfill I r
Project Location: 375 Dozer Drive, Polkton, NC
Project Number:
4140-15-007 Purge Date:
April 15, 2022
Source Well:
MW-4S Purge Time:
23 Minutes
Locked?:
Yes Sample Date:
April 15, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
13:35
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 13:58 1.1 200 10.59 17.6 5.91 169.4 1.74 167.8 27.18 End of Purging
Sample Method: Bladder Pump Sample Start Time: 13:35 Sample End Time: 13:45
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/15/2022
Notes:
Measuring Point:
Top of Casing
Depth to Water:
5.78
ft-TOC
Total Well Depth:
27.50
ft-TOC
Height of Water Column:
21.72
feet
Screen Length: - feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
3.5
Gal
3 *Well Volume
10.63
Gal
5 *Well Volume
17.72
Gal
Purge Method:
Bladder Pump
Start Time:
13:35
End Time:
13:58
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
1.1
Gallons
Dedicated bladder pump. No well tag. MW-
DTW (TOC): 9.14'.
Final Volume Purge Rate:
200
mL/mifl4l)
Well Purged Dry?:
No
(Yes/N
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
13:35
0.0
---
---
---
---
---
---
---
Start Purging
13:40
0.3
200
5.64
20.0
5.97
173.E
2.05
167.5
9.80
13:45
0.5
200
6.60
20.6
5.92
171.1
1.97
173.1
4.89
13:50
0.7
150
8.60
21.4
5.92
170.0
1.86
175.4
4.75
13:58
1.1
200
10.59
17.6
5.91
169.4
1.74
167.8
27.18
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

F�m
Project Name: Anson County Landfill
�r
Project Location: 375 Dozer Drive, Polkton, INC I s�
Project Number:
4140-15-007 Purge Date:
April 19, 2022
Source Well:
MW-5S Purge Time:
18 Minutes
Locked?:
Yes Sample Date:
April 19, 2022
Sampled By:
J. Tayouga & S. Schmal Sample Time:
10:40
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 10:35 1.0 200 6.84 19.9 5.98 249.9 2.11 142.8 6.95 End of Purging
Sample Method: Bladder Pump Sample Start Time: 10:40 Sample End Time: 10:45
Analytical Data
Name Signature Date
i
(1) Jasmine Tayouga 4/19/2022
Notes:
Measuring Point:
Top of Casing
Depth to Water:
6.01
ft-TO
Total Well Depth:
33.35
ft-TOC
Height of Water Column:
27.34
feet
Screen Length: - feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
4.5
Gal
3 *Well Volume
13.38
Gal
5 *Well Volume
22.31
Gal
Purge Method:
Bladder Pump
Start Time:
10:17
End Time:
10:35
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
1.0
Gallons
Dedicated bladder pump. No well tag. MW-
DTW (TOC): 5.94'.
Final Volume Purge Rate:
200
mL/miflSD
Well Purged Dry?:
No
(Yes/N
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
10:17
0.0
---
---
---
---
---
---
---
---
Start Purging
10:20
0.2
200
6.22
20.2
6.17
257.5
2.18
129.2
8.65
10:25
0.4
200
6.47
20.0
6.01
252.1
2.14
130.8
8.44
10:30
0.7
200
6.61
20.1
5.94
251.6
2.19
135.5
7.14
10:35
1.0
200
6.84
19.9
5.98
249.9
2.11
142.8
6.95
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

• • •• 111ITAR1111111011,11:1141�►
Project Name: Anson County Landfill I r
Project Location: 375 Dozer Drive, Polkton, NC
Project Number:
4140-15-007 Purge Date:
April 15, 2022
Source Well:
MW-8S Purge Time:
20 Minutes
Locked?:
Yes Sample Date:
April 15, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
12:25
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals z 5 minutes and purge volumes ? 1 flow -through cell volume)
Final: 12:25 0.8 150 21.60 17.4 6.22 601 3.83 103.2 17.40 End of Purging
Sample Method: Bladder Pump Sample Start Time: 12:25 Sample End Time: 12:30
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/15/2022
Notes: To convert CRP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
16.85
ft-TOC
Total Well Depth:
28.70
ft-TOC
Height of Water Column:
11.85
feet
Screen Length: - feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
1.9
Gal
3 *Well Volume
5.80
Gal
5 *Well Volume
9.67
Gal
Purge Method:
Bladder Pump
Start Time:
12:05
End Time:
12:25
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
0.8
Gallons
Dedicated bladder pump. No well tag. MW-
BID flush mount DTW (TOC): 16.11'. Field
Du licate collected.
Final Volume Purge Rate:
150
mL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(p5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
12:05
0.0
---
---
---
---
---
---
---
Start Purging
12:07
0.1
150
16.85
17.4
6.3
657
4.2
51
10.1
12:15
0.4
150
19.65
17.4
6.29
649.0
4.02
78.3
7.54
12:20
0.6
150
20.85
17.4
6.24
622.0
3.84
94.8
17.4
12:25
0.8
150
21.60
17.4
6.22
601.0
3.83
103.2
17.4
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

r
F�m
Project Name: Anson County Landfill 3
Project Location: 375 Dozer Drive, Polkton, INC I
Project Number:
4140-15-007 Purge Date:
April 14, 2022
Source Well:
MW-9S Purge Time:
8 Minutes
Locked?:
Yes Sample Date:
April 14, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
10:35
Weather:
Overcast Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ 1 flow-throughcellvolume)
Final: 10:31 1.0 18.2 7.31 964.0 6.34 76.5 188 End of Purging
Sample Method: Bailer Sample Start Time: 10:35 Sample End Time: 10:40
Analytical Data
Name Signature Date
(1) Kelsey Vassallo U 4/14/2022
Notes: To convert ORP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
15.41
ft-TOC
Total Well Depth:
45.28
ft-TO
Height of Water Column:
29.87
feet
Screen Length: 15 feet Stickup:
-
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
4.9
Gal
3 *Well Volume
14.62
Gal
5 *Well Volume
24.37
Gal
Purge Method:
Start Time:
10:23
End Time:
10:31
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
1.0
Gallons
Dedicated bladder pump filled with sediment.
Used bailer to purge and sample.
Final Volume Purge Rate:
-
MIL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(m5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
10:23
0.0
---
---
---
---
---
---
---
---
Start Purging
10:25
1.0
---
---
17.8
7.53
954.0
7.60
79.0
38.17
10:29
#VALUE!
---
---
18.1
7.45
956.0
7.01
75.9
34.57
10:31
#VALUE!
---
---
18.2
7.31
964.0
6.34
76.5
187.7
End Purging
Sampled with bailer -bladder pump no longer works due to sediment buildup at the
bottom of the well
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs 8260
3
40mL VOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

S L
Project Name: Anson County Landfill ;a
Project Location: 375 Dozer Drive, Polkton, INC
Project Number:
4140-15-007 Purge Date:
April 11, 2022
Source Well:
MW-10S Purge Time:
23 Minutes
Locked?:
Yes Sample Date:
April 11, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
10:50
Weatherl
Sunny Air Temp:
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ 1 flow-throughcellvolume)
Final: 10:45 1.2 200 17.65 18.0 7.03 1740 2.14 408.1 4.06 End of Purging
Sample Method: Peristaltic Pump Sample Start Time: 10:50 Sample End Time: 10:55
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/11/2022
Notes: To convert CRP to Eh, add 205 mV to CRP.
Measuring Point:
Top of Casing
Depth to Water:
14.21
ft-TOC
Total Well Depth:
36.00
ft-TO
Height of Water Column:
21.79
feet
Screen Length: 10 feet Stickup:
4.01
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
3.6
Gal
3 *Well Volume
10.67
Gal
5 *Well Volume
17.78
Gal
Purge Method:
Peristaltic Pump
Start Time:
10:22
End Time:
10:45
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
1.2
Gallons
Peristaltic pump used due to blockage at 14'
bgs. Screen on well tag 26-36 ft bgs.
Final Volume Purge Rate:
200
MIL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mi./min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(m5/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
10:22
0.0
---
---
---
---
---
---
---
---
Start Purging
10:25
0.2
200
14.98
17.4
7.05
1751
2.62
331.6
5.54
10:30
0.4
200
16.25
17.5
7.03
1746
2.52
398.4
4.40
10:35
0.7
200
16.75
17.7
7.03
1745
2.29
382.3
5.02
10:40
1.0
200
17.19
17.7
7.03
1743
2.23
376.6
5.10
10:45
1.2
200
17.65
18.0
7.03
1740
2.14
408.1
4.06
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

!
F�A
Project Name: Anson County Landfills !
Project Location: 375 Dozer Drive, Polkton, NC I !
Project Number: 4140-15-007 Purge Date: April 12, 2022
Source Well:
MW-11S
Purge Time:
44 Minutes
Locked?:
Yes
Sample Date:
April 12, 2022
Sampled By:
SJT/SRS
Sample Time:
14:05
Weather:
Sunny
Air Temp:
Water Level & Well Data
Measuring Point:
Top of Casing
Well Volume
Well Diameter 2 inch
Water Volume 7.0 Gal
3 Well Volume 20.88 Gal
5 Well Volume 34.79 Gal
Time: 13:16 End Time: 14:00
(If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi
Pump Intake Depth from Top of Casing: ft-TOC
Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL
DTW-TOC at 25 % Drawdown of WC Above Pump: ft-TOC Comments:
Final Volume Purged: 2.1 Gallons No dedicated pump -used peristaltic due to
Final Volume Purge Rate: 180 mL/min access issues. Screen on well tag 28-38 ft bgs.
Well Purged Dry?: No (Yes/No)
Volume Depth to Dissolved
Time Purged Flow Rate Water Temp Oxygen Spec. Cond. pH ORP* Turbidity Comment
(gal) (mUmin) (ft) (°C) (mg/L) (p5/cm) (s.u.) (mV) (NTU)
13:16 0.0 --- --- --- --- --- --- --- --- Start Purging
13:18 0.1 180 9.20 19.8 6.93 702.0 7.06 19.7 25.9
13:23 0.3 180 9.52 19.3 1.90 699.0 7.03 12.0 28.5
13:33 0.8 180 9.80 19.8 0.64 698.0 7.04 -0.7 29.7
13:43 1.3 180 9.84 19.3 0.63 692.0 7.03 -10.5 19.7
13:52 1.7 180 9.92 19.6 0.64 680.0 7.03 -25.5 15.9
14:00 2.1 180 9.83 19.9 0.9 674 7.0 -30 9.78 End Purging
14:00 2.1 180 9.83 19.9 0.89 674.0 7.03 -29.8 9.78 End of Purging
Method QTy Container Preservative Method City Container Preservative
VOCs8260 3 40mLVOAs HCl
1,4-Dioxane 8260 3 40mL VOAs HCl
Metals 6010 (Total) 1 250mL P HNO3
Metals 6010 (Dissolved) 1 250mL P Unpreserved
Form Revision Date: 2/12/18 16:00
Time: 13:16 End Time: 14:00
(If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi
Pump Intake Depth from Top of Casing: ft-TOC
Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL
DTW-TOC at 25 % Drawdown of WC Above Pump: ft-TOC Comments:
Final Volume Purged: 2.1 Gallons No dedicated pump -used peristaltic due to
Final Volume Purge Rate: 180 mL/min access issues. Screen on well tag 28-38 ft bgs.
Well Purged Dry?: No (Yes/No)
Volume Depth to Dissolved
Time Purged Flow Rate Water Temp Oxygen Spec. Cond. pH ORP* Turbidity Comment
(gal) (mUmin) (ft) (°C) (mg/L) (p5/cm) (s.u.) (mV) (NTU)
13:16 0.0 --- --- --- --- --- --- --- --- Start Purging
13:18 0.1 180 9.20 19.8 6.93 702.0 7.06 19.7 25.9
13:23 0.3 180 9.52 19.3 1.90 699.0 7.03 12.0 28.5
13:33 0.8 180 9.80 19.8 0.64 698.0 7.04 -0.7 29.7
13:43 1.3 180 9.84 19.3 0.63 692.0 7.03 -10.5 19.7
13:52 1.7 180 9.92 19.6 0.64 680.0 7.03 -25.5 15.9
14:00 2.1 180 9.83 19.9 0.9 674 7.0 -30 9.78 End Purging
14:00 2.1 180 9.83 19.9 0.89 674.0 7.03 -29.8 9.78 End of Purging
Method QTy Container Preservative Method City Container Preservative
VOCs8260 3 40mLVOAs HCl
1,4-Dioxane 8260 3 40mL VOAs HCl
Metals 6010 (Total) 1 250mL P HNO3
Metals 6010 (Dissolved) 1 250mL P Unpreserved
Form Revision Date: 2/12/18 16:00
Volume Depth to Dissolved
Time Purged Flow Rate Water Temp Oxygen Spec. Cond. pH ORP* Turbidity Comment
(gal) (mUmin) (ft) (°C) (mg/L) (p5/cm) (s.u.) (mV) (NTU)
13:16 0.0 --- --- --- --- --- --- --- --- Start Purging
13:18 0.1 180 9.20 19.8 6.93 702.0 7.06 19.7 25.9
13:23 0.3 180 9.52 19.3 1.90 699.0 7.03 12.0 28.5
13:33 0.8 180 9.80 19.8 0.64 698.0 7.04 -0.7 29.7
13:43 1.3 180 9.84 19.3 0.63 692.0 7.03 -10.5 19.7
13:52 1.7 180 9.92 19.6 0.64 680.0 7.03 -25.5 15.9
14:00 2.1 180 9.83 19.9 0.9 674 7.0 -30 9.78 End Purging
14:00 2.1 180 9.83 19.9 0.89 674.0 7.03 -29.8 9.78 End of Purging
Method QTy Container Preservative Method City Container Preservative
VOCs8260 3 40mLVOAs HCl
1,4-Dioxane 8260 3 40mL VOAs HCl
Metals 6010 (Total) 1 250mL P HNO3
Metals 6010 (Dissolved) 1 250mL P Unpreserved
Form Revision Date: 2/12/18 16:00
Method QTy Container Preservative Method City Container Preservative
VOCs8260 3 40mLVOAs HCl
1,4-Dioxane 8260 3 40mL VOAs HCl
Metals 6010 (Total) 1 250mL P HNO3
Metals 6010 (Dissolved) 1 250mL P Unpreserved
Form Revision Date: 2/12/18 16:00
Form Revision Date: 2/12/18 16:00

r
F�m
Project Name: Anson County Landfill 3
Project Location: 375 Dozer Drive, Polkton, INC I
Project Number:
4140-15-007 Purge Date:
April 11, 2022
Source Well:
MW-12R Purge Time:
29 Minutes
Locked?:
Yes Sample Date:
April 11, 2022
Sampled By:
K. Vassallo & S. Schmal Sample Time:
11:53
Weather:
Sunny Air Temp:
-
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ 1 flow-throughcellvolume)
Final: 11:49 1.9 250 12.71 18.9 6.4 114.3 2.1 -88.1 13.71 End of Purging
Sample Method: Submersible Pump Sample Start Time: 11:53 Sample End Time: 11:58
Analytical Data
Name Signature Date
(1) Kelsey Vassallo U 4/11/2022
Notes: To convert CRP to Eh, add 205 mV to CRP.
Measuring Point:
Top of Casing
Depth to Water:
9.54
ft-TOC
Total Well Depth:
55.09
ft-TO
Height of Water Column:
45.55
feet
Screen Length: 10 feet Stickup:
4.09
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
7.4
Gal
3 *Well Volume
22.30
Gal
5 *Well Volume
37.17
Gal
Purge Method:
Submersible Pump
Start Time:
11:20
End Time:
11:49
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
46.0
ft-TOC
Water Column Above Pump Intake:
36.46
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
18.66
ft-TOC
Comments:
Final Volume Purged:
1.9
Gallons
Replacement well for MW-125. Screened
interval on tag 41.0' - 51.0'. Developed on
10/19/20.
Final Volume Purge Rate:
250
MIL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mi./min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cond.
(pS/cm)
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
11:20
0.0
---
---
---
---
---
---
---
---
Start Purging
11:24
0.3
250
11.03
18.6
6.84
106.6
2.06
77.4
41.18
11:29
0.6
250
11.50
18.6
6.63
105.9
2.02
40.9
19.35
11:34
0.9
250
11.87
18.7
6.57
106.5
2.03
18.3
12.15
11:39
1.3
250
12.14
18.7
6.40
111.0
2.04
-70.3
12.38
11:44
1.6
250
12.44
18.8
6.36
112.8
2.04
-84.4
12.57
11:49
1.9
250
12.71
18.9
6.35
114.3
2.06
-88.1
13.71
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs 8260
3
40mL VOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

Project Name:
Project Location:
Project Number:
Anson County Landfill
375 Dozer Drive, Polkton, NC
4140-15-007
Purge Date:
'W
9
qmh._ ._
April 12, 2022
Source Well:
GMW-13
Purge Time:
96 Minutes
Locked?:
Yes
Sample Date:
April 12, 2022
Sampled By:
SJT/SRS
Sample Time:
12:40
Weather:
Sunny
Air Temp:
Water Level & Well Data
Measuring Point:
Top of Casing
Well Volume
Depth to Water:
32.71
ft-TOC
Well Diameter
2
inch
Total Well Depth:
61.46
ft-TOC
Water Volume
4.7
Gal
Height of Water Column:
28.75
feet
3 * Well Volume
14.07
Gal
Screen Length: 10 1 feet I Stickup:
4.26
ft-GRD
5 * Well Volume
23.46
Gal
Well Purging Information
Purge Method:
Submersible Pump
Start Time:
11:03
End Time:
12:39
(If Used) Bladder Pump Control Settings:
On (sec): I
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
55.0
ft-TOC
Water Column Above Pump Intake:
22.29
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
38.28
ft-TOC
Comments:
Final Volume Purged:
1 4.9
Gallons
Replacement well for MW-135. We'll tag
bottom of screen 57.7
Final Volume Purge Rate:
200
mL/min
Well Purged Dry?:
(Yes/No)
Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume)
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
CC)
Dissolved
Oxygen
(mg/L)
Spec. Cond.
(PS/cm)
pH
(s.u.)
ORP*
(mV)
Turbidity
(NTU)
Comment
11:03
0.0
---
---
---
---
---
---
---
---
Start Purging
11:05
0.1
200
32.99
17.5
4.02
298.0
7.34
-110.1
381.3
11:10
0.4
200
32.92
19.0
0.67
289.6
7.23
-97.7
490.8
11:20
0.9
200
33.29
18.3
0.43
263.4
7.12
-75.1
248.7
11:30
1.4
200
33.31
19.0
0.47
253.0
7.05
-61.2
176
11:40
2.0
200
33.27
20.0
0.42
248.8
7.01
-50.9
128.6
11:55
2.7
200
33.44
18.7
0.46
246.0
6.99
-45.0
85.23
12:05
3.3
200
33.87
18.1
0.36
239.4
6.96
-39.3
59.53
12:15
3.8
200
34.71
17.7
0.26
234.2
6.93
-33.5
27.91
12:25
4.3
200
35.01
17.8
0.26
233.6
6.93
-33.8
17.17
12:35
4.9
200
35.17
17.7
0.25
232.8
6.93
-34.7
17.09
End Purging
12:39
9.49
Final Turbidity
Final: 12:39 1 4.9 1 200 1 35.17 1 17.7 1 0.25 1 232.8 1 6.93 1 -34.7 1 9.49 1 End of Purging
Sample Method: 1 Submersible Pump Sample Start Time: 12:40 Sample End Time: 12:40
Analytical Data
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs 8260
3
40mL VOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Name Signature Date
f
(1) Jasmine Tayouga 4/12/2022
Notes: To convert ORP to Eh, add 205 mV to ORP.
Form Revision Date: 2/12/18 16:00

Project Name: Anson County Landfill !
Project Location: 375 Dozer Drive, Polkton, NC
Project Number: 4140-15-007
Purge Date:
April 12, 2022
Source Well: GMW-14
Purge Time:
18 Minutes
Locked?: Yes
Sample Date:
April 13, 2022
Sampled By: SJT/SRS
Sample Time:
9:55
Weather: Sunny
Air Temp:
Water Level & Well Data
Well Purging Information
Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume)
Final: 10:06 0.0 #N/A #N/A 16.2 7.07 137.8 6.33 82.5 372 End of Purging
Sample Method: Bailer Sample Start Time: 09:55 Sample End Time: 09:55
Analytical Data
Name Signature Date
(1) Jasmine Tayouga l NNaw 4/12/2022
Notes: Drop sampled with bailer
Measuring Point:
Top of Casing
Depth to Water:
39.01
ft-TOC
Total Well Depth:
51.97
ft-TOC
Height of Water Column:
12.96
feet
Screen Length: 15 feet Stickup:
3.97
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
2.1
Gal
3 *Well Volume
6.34
Gal
5 *Well Volume
10.57
Gal
Purge Method:
Submersible Pump
Start Time:
9:48
End Time:
10:06
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
ft-TOC
Water Column Above Pump Intake:
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
ft-TOC
Comments:
Final Volume Purged:
0.0
Gallons
Replacement well for MW-14D.
Final Volume Purge Rate:
#N/A
mL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mL/min)
Depth to
Water
(ft)
Temp
CC)
Dissolved
Oxygen
(mg/L)
Spec. Cond.
(PS/cm)
pH
(s.u.)
ORP*
(mV)
Turbidity
(NTU)
Comment
09:48
0.0
---
---
--
---
---
---
---
---
Start Purging
09:50
-
-
16.5
8.84
148.9
6.62
161.4
19.32
09:55
-
-
16.2
7.48
132.9
6.46
138.0
121.60
10:00
-
-
16.2
9.05
134.3
6.34
99.3
198.10
10:06
-
-
-
16.2
7.07
137.8
6.33
82.5
371.90
End Purging
Purged on 4/12. Drop sampled on 4/13 with bailer. Turbidity at time of sample 7.88 ntu.
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs 8260
3
40mL VOAs
HCI
1,4-Dioxane 8260
3
40mL VOAs
HCI
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00

Project Name: Anson County Landfill
Project Location: 375 Dozer Drive, Polkton, INC
Project Number:
4140-15-007 Purge Date:
April 11, 2022
Source Well:
MW-15D Purge Time:
55 Minutes
Locked?:
No Sample Date:
April 11, 2022
Sampled By:
S. Schmal & K. Vassallo Sample Time:
13:47
Weather:
Sunny Air Temp:
Water Level & Well Data
We Purging Information
Field Parameters (Taken at time intervals >_ 5 minutes an purge volumes >_ 1 flow-throughcellvolume)
Final: 13:45 2.9 200 34.36 21.6 5.85 107.2 3.13 155.3 38.45 End of Purging
Sample Method: Submersible Pump Sample Start Time: 13:47 Sample End Time: 13:52
Analytical Data
Name Signature Date
(1) Kelsey Vassallo 4/11/2022
Notes: To convert ORP to Eh, add 205 mV to ORP.
Measuring Point:
Top of Casing
Depth to Water:
13.10
ft-TOC
Total Well Depth:
41.50
ft-TO
Height of Water Column:
28.40
feet
Screen Length: 10 feet Stickup:
3.8
ft-GRD
Well Volume
Well Diameter
2
inch
Water Volume
4.6
Gal
3 *Well Volume
13.90
Gal
5 *Well Volume
23.17
Gal
Purge Method:
Submersible Pump
Start Time:
12:50
End Time:
13:45
(If Used) Bladder Pump Control Settings:
On (sec):
Off (sec):
Pressure:
psi
Pump Intake Depth from Top of Casing:
40.0
ft-TOC
Water Column Above Pump Intake:
26.90
feet
Flow Through Cell Vol: 200 mL
DTW-TOC at 25% Drawdown of WC Above Pump:
19.83
ft-TOC
Comments:
Final Volume Purged:
2.9
Gallons
No dedicated pump -used monsoon with
control box. Screen on well tag 31.5-41.5 ft
b s.
Final Volume Purge Rate:
200
MIL/min
Well Purged Dry?:
No
(Yes/No)
Time
Volume
Purged
(gal)
Flow Rate
(mi./min)
Depth to
Water
(ft)
Temp
(°C)
pH
(s.u.)
Spec. Cord.
(II
Dissolved
Oxygen
(mg/L)
ORP*
(mV)
Turbidity
(NTU)
Comment
12:50
0.0
---
---
---
---
---
---
---
---
Start Purging
12:54
0.2
200
31.87
19.9
6.17
89.4
5.61
62.6
60.88
13:00
0.5
200
32.69
20.0
5.91
88.8
4.30
165.2
100.30
13:05
0.8
200
33.10
20.5
5.90
88.6
4.09
163.4
74.35
13:10
1.1
200
33.39
20.9
5.88
91.5
3.76
156.9
48.55
13:15
1.3
200
33.61
20.8
5.87
94.3
3.79
156.9
42.82
13:20
1.6
200
33.70
21.3
5.87
97.3
3.41
154.0
42.88
13:25
1.8
200
33.88
21.4
5.86
99.8
3.59
156.2
41.60
13:30
2.1
200
34.02
21.4
5.86
101.6
3.39
155.1
38.59
13:35
2.4
200
34.16
21.3
5.86
103.1
3.35
153.9
39.81
13:40
2.6
200
34.27
21.7
5.85
105.7
3.27
154.9
39.80
13:45
2.9
200
34.36
21.6
5.85
107.2
3.13
155.3
38.45
End Purging
Method
Qty
Container
Preservative
Method
Qty
Container
Preservative
VOCs8260
3
40mLVOAs
HCl
1,4-Dioxane 8260
3
40mL VOAs
HCl
Metals 6010 (Total)
1
250mL P
HNO3
Metals 6010 (Dissolved)
1
250mL P
Unpreserved
Form Revision Date: 2/12/18 16:00