0302_AlleghanyCoLandfill_Monitoring_combined_FID1740661_20220726

July 29, 2022
NC DEQ
Division of Waste Management - Solid Waste Section
ATTN: Mr. Perry Sugg, PG (Permitting Hydrogeologist)
1646 Mail Service Center
Raleigh, North Carolina 2769-1646
RE: Semi -Annual Assessment/Detection Monitoring Report
Alleghany County Closed MSW Landfill
Permit # 0302-MSWL-1981
Sparta, North Carolina
Mr. Sugg,
ARM
Geothermal, Eroronmeraal,
& Well Trilling
Attached is the Environmental Monitoring Reporting Form and Monitoring Report for the above referenced
facility. The entire report is provided in pdf for your review. Review of the current analytical results for
Appendix I Volatiles indicate all of the monitoring wells and stream samples to be compliant for all
hydrocarbon compounds tested with the exception of low level non -compliant vinyl chloride found at 0303T-
MW3. Vanadium exceeding 2L IMAC standards was found at 0303T-MW1, 0303T-MW3, and slightly turbid
stream samples 0303T-ST1 and 0303T-ST2. Cobalt exceeding 2L IMAC standards was found at 0303T-MW2
and 0303T-MW3. Barium exceeding MCL was found at 0303T-MW3. All other monitoring wells and stream
samples revealed compliant metals compounds tested.
In a continued evaluation of the low level vinyl chloride contamination present at 0303T-MW3, it appears that
the contaminant is stable within a localized area and does not appear to be a threat to human health or the
environment. 0303T-MW3 is considered an upgradient background well and is immediately bordered to the
north by mountainside. Sparse residential activity is present to the northwest at greater than 500' with no
legitimate identifiable source for the contaminant. At this point, it is undetermined as to the source of the vinyl
chloride for there have been no historical reported spills or other known incidents in this specific location.
Residuals from PVC (poly vinyl chloride) well materials could possibly be a contributive source. The well will
continue to be closely monitored and in the event contaminant concentrations significantly increase or begin
to appear within down gradient wells, additional hydrogeological analyses or assessment could become
necessary.
Historical methane monitoring at the site revealed the monitoring wells to contain low level methane readings
ranging from 0 to 120 ppm. During this event, all monitoring wells revealed no measurable methane levels
and LEL readings were consistent at 0%. No detectable methane levels were found at the scale house or
tipping scale area and low level methane ranging from 0 to 30 ppm was found at the recycle center. The
methane well, located in the central portion of the landfill, revealed methane concentrations ranging from 40
to 1,020 ppm and a %LEL between 0% and 10%. Methane % volume was calculated at 0.102%.
It is recommended that the groundwater/surface water monitoring program continue on a semi-annual
schedule. Methane monitoring for all five monitoring wells, the on -site methane well, and enclosed structures
will continue on a quarterly basis. If you have any questions please do not hesitate to call Jim Corvette, PG
or Joe Zuncich at [phone].
Sincerely,
5J01_S91 L. Zuncic
Project Manager, CWD, Environmental Geologist
cc. Alleghany County, ATTN: Mr. Mike James, County Manager, P.O. Box 366, Sparta, North
Carolina 28675
Applied Keoource Management, P C.
F 0. Box 882, 257 Transfer Station (load, Hampstead, NC 26445 910.270.2919 Fax [phone]

i 6ENR USE ONLY: ❑Pa_per Report [:]Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
i-'NC DENR I IEnvironmental Monitoring
Division of Waste Management -Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 26 surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Applied Resource Management, P.C.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Joseph L. Zuncich
E-mail, [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Alleghany County Landfill 431 Osborne Road 0302- 0500 Jun
Sparta, NC 28675 MSWLF-1981 a 16, 2022
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑X
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
❑ Assessment Monitoring
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
❑ Corrective Action
Notification attached?
No. No groundwater or surface water standards were exceeded.
RX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
James L. Corvette, P.G. President
FGili entative Name (Print) Title
Signature
P.O. Box 882, 257 Transfer Station Rd., Hampstead, NC 28443
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
910 270-2919
(Area Code) Telephone Number ,`lillf
Utj Affix NC Lice 2o.%s
plogist Seal
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COFioex4
Revised 6/2009

y
ASSESSMENT/DETECTION MONITORING REPORT
FOR THE
ALLEGHANY COUNTY MUNICIPAL
SOLID WASTE LANDFILL (CLOSED)
SPARTA, NORTH CAROLINA
Permit #:
Land Use:
Prop. Owner:
Site Operator:
Date:
Nat. ofRe/ease:
Coordinates:
0302-MSWLF-1981
Municipal Solid Waste L-- -Jr.
Alleghany County
348 South Main Street
Sparta, North Carolina 2
[phone]
Alleghany County
348 South Main Street
Sparta, North Carolina 2
[phone]
July 11, 2022
Suspected hydrocarbon leachate discharge from
landfill disposal
Latitude(North): 36" 29' 26" N
Longitude(West): 81 " 08' 58" W
Prepared By: Applied Resource Management, PC
257 Transfer Station Road
P. O. Box 882
Hampstead, North Carolina 28443
[phone]
Fax [phone]
r��

TABLE OF CONTENTS
Page
1.0 SUMMARY OF SAMPLING RESULTS 1
1.1 Summary of Analytical Results ................................ 1
1.2 Proximity of the Plume to the Nearest Receptor ................... 4
1.3 Description of Current Plume Size ............................. 5
1.4 Groundwater Flow Direction .................................. 6
1.5 Predictive Rate of Contaminant Transport ....................... 6
2.0 CONCLUSIONS AND RECOMMENDATIONS
3.0 REFERENCES
TABLES
TABLE 1 SEMI-ANNUAL MONITORING WELL, METHANE
SCREENING, AND STREAM SAMPLING DATA SUMMARY
TABLE 2 QUARTERLY METHANE MONITORING DATA SUMMARY
TABLE 3A HISTORICAL GROUNDWATER SAMPLE RESULTS
SUMMARY (APPENDIX 1 VOCs)
TABLE 36 HISTORICAL GROUNDWATER SAMPLE RESULTS
SUMMARY (APPENDIX 1 METALS)
FIGURES
FIGURE 1 SITE MAP WITH MONITORING WELL AND STREAM
SAMPLE LOCATIONS
FIGURE 2 SITE MAP WITH DOMESTIC WELL LOCATIONS
FIGURE 3 HISTORICAL VINYL CHLORIDE CONCENTRATIONS
FIGURE 4 GROUNDWATER TABLE CONTOURS AS OF 6/16/22
APPENDICES
APPENDIX A LABORATORY REPORT
APPENDIX B NCDWM-SOLID WASTE SECTION LANDFILL GAS
MONITORING DATA FORMS FOR 2022
APPENDIX C LANDFILL EDD
h

ASSESSMENT/DETECTION MONITORING REPORT
FOR THE
ALLEGHANY COUNTY MUNICIPAL
SOLID WASTE LANDFILL (CLOSED)
SPARTA, NORTH CAROLINA
PERMIT # 0302-MSWLF-1981
PREPARED FOR:
ALLEGHANY COUNTY
SPARTA, NORTH CAROLINA
J U LY 11, 2022
1.0 SUMMARY OF SAMPLING RESULTS
1.1 Summary of Analytical Results
(Refer to Tables 1, 2, 3, and Appendices A and B)
As summarized on the referenced tables, numerous semi-annual
groundwater sampling and quarterly methane monitoring events have been
conducted at the site. Due to the accumulation of analytical data over
several years, the summary has been revised to include the previous three
years of data. This event included the sampling of the five monitoring wells
(0303T-MW 1 through 0303T-MW5), and two stream samples (0303T-ST1
and 0303T-ST2). Also, methane monitoring was conducted on -site at
designated locations. Figure 1 is a Site Map With Monitoring Well And
Stream Sample Locations. Review of the current analytical results for
Appendix I Volatiles indicate that all monitoring wells and surface water
stream samples were found to be compliant for all hydrocarbon compounds
tested with the exception of low level non -compliant vinyl chloride in 0303T-
MW3 at an estimated 0.67 ppb. The up hydraulic gradient well 0303T-
MW3, has historically contained low level non -compliant vinyl chloride and
has also revealed non detect levels. It should be noted that due to
consecutive compliant 1,4-Dioxane concentrations for all sampling locations,
this analysis was previously removed from the sampling program.
Appendix I metals barium, cobalt, and vanadium were found during this
event at low level non -compliant concentrations. Vanadium exceeding 2L
MAC standards was found at 0303T-MW 1 (estimated 0.00043 ppm, 0303T-
MW3 (estimated 0.00048 ppm), stream samples 0303T-ST1 (0.0011 ppm)
and 0303T-ST2 (estimated 0.00084 ppm). Cobalt exceeding 2L IMAC
standards was found at 0303T-MW2 at 0.01041 ppm and 0303T-MW3 at
0.0137 ppm. Barium exceeding MCL was found at 0303T-MW3 at 2.030

July 11, 2022
ppm. All other monitoring wells and surface water stream samples were
found to be compliant for all Appendix I Volatiles and Appendix I Metals.
Historical results have revealed 0303T-MW1 to contain fluctuating low
compliant and non -compliant vinyl chloride and benzene concentrations.
Benzene concentrations at 0303T-MW 1 have ranged from below laboratory
quantitation limits to 5.02 ppb. Since the June 2011 monitoring event, both
the benzene and vinyl chloride concentrations have been found to be none
detected. 0303T-MW2 has historically revealed non -compliant methylene
chloride concentrations ranging from 5.0 to 17.1 ppb. This event revealed
none detected, and methylene chloride has been found to be none detected
since June of 2016. 0303T-MW3 has historically shown low level non-
compliant vinyl chloride concentrations and none detectable levels. This
event and previous event revealed a low level non -compliant concentrations
from 1.3 ppb to an estimated 0.67 ppb. Up gradient well, 0303T-MW4 has
revealed all compliant concentrations for this event. All compounds have
been compliant since December of 2014, with the exception of a non-
compliant 2-Hexanone concentration of 55.4 ppb in the December 2015
monitoring event. Concentrations of 2-Hexanone have been complaint or
none detected since the June 2016 event, and remain compliant for this
event. The down gradient well, 0303T-MW5, located between 0303T-MW1
and Vile Creek, has consistently revealed all target compounds to be
compliant, with the exception of the low level non -complaint chloromethane
concentration at 6.8 ppb in the December 2016 event; however, this event
and the last several results revealed none detected. All other monitoring
wells and stream samples collected during this event and previous events
were found to be compliant for Appendix I Volatiles.
Domestic water supply wells identified on Figure 2 were initially sampled in
2008 and all five were found to be compliant. The closest cross hydraulic
gradient well, well#5 was sampled in December, 2012, and was found to
remain compliant. The on -site Water Supply Well #1 was sampled during
the November 30, 2017 event and analyzed for Appendix I Volatiles only. All
compound concentrations were found to be none detected.
Methane monitoring was conducted during this event at all five monitoring
wells, the on -site methane well, and the enclosed structures identified as the
scale house, the recycling center, and the tipping scale area. Non detect
methane concentrations were recorded for all monitoring well locations (see
Table 1). Historically, low level methane readings have been periodically
found in the monitoring wells ranging from 0 to 120 ppm. %LEL and
%volume CH4 readings forthe monitoring wells were consistent at 0% during
this event. No detectable methane levels were found at the scale house or
tipping scale area and low level methane renging from 0 to 30 ppm was
found at the recycling/storage center. The methane well, located in the
central portion of the landfill, revealed methane concentrations ranging from
E

July 11, 2022
40 to 1,020 ppm, a % LEL between 0% and 10%, and a % CH4 volume
calculated at 0.102%.
Results of Well Gauging
A Semi -Annual Monitoring Well Data Summary is presented in Table 1.
Depth to the groundwater table, as measured on 6/16/22, ranged from 4.96
to 33.44 feet.
Sampling Methods and Results
(Refer to Tables 2, 3A, 3B, 3C and Appendix A and B)
As part of this monitoring event, five monitoring wells, 0303T-MW 1 through
0303T-MW5 were purged of at least three well volumes of groundwater, field
measured for parameters pH, temperature, conductivity, turbidity, and
sampled. Field measurements are included in Table 1. All groundwater
samples collected revealed low turbidity at <5NTUs. Stream samples were
found to be slightly turbid ranging from 8.85 to 12.2 NTUs. pH readings were
found ranging from 6.23 units at 0303T-MW2 to 5.36 units at 0303T-MW4.
Temperatures ranged from 68 F to 69.98 F. All of the monitoring well
groundwater samples and stream samples were analyzed by Pace Analytical
Services, LLC for Appendix I Volatiles and Appendix I Metals per NC Landfill
parameters. 1,4-Dioxane analysis was previously omitted due to consecutive
compliant concentrations for all samples collected. The laboratory results
are enclosed as Appendix A.
Appendix I VOCs Results
This event revealed all five monitoring wells (0303T-MW1 through 0303T-
MW5), and two stream samples (0303T-ST1 and 0303T-ST2) to be
compliant for all Appendix I volatile organic compounds with the exception
of an estimated low level non -compliant vinyl chloride concentration (0.67
ppb) found in 0303T-MW3. A Historical Groundwater Sample Results
Summary (Appendix I VOCs) is provided in Table 3A.
Appendix I Metals Results
Appendix I metals barium, cobalt, and vanadium were found during this
event at low level non -compliant concentrations. Vanadium exceeding 2L
IMAC standards was found at 0303T-MW 1 (estimated 0.00043 ppm, 0303T-
MW3 (estimated 0.00048 ppm), stream samples 0303T-ST1 (0.0011 ppm)
and 0303T-ST2 (estimated 0.00084 ppm). Cobalt exceeding 2L IMAC
standards was found at 0303T-MW2 at 0.01041 ppm and 0303T-MW3 at
0.0137 ppm. Barium exceeding MCL was found at 0303T-MW3 at 2.030
ppm. Monitoring well and stream samples were found to be compliant during
c

July 11, 2022
this event. A Historical Groundwater Sample Results Summary (Appendix
Metals) is provided in Table 3B.
Methane Monitoring Results
Methane monitoring was conducted at the site utilizing an RKI Instruments
Gas Tracer. No measurable methane concentrations were detected in any
of the monitoring wells during this event. Historically, the monitoring wells
were found to contain low level methane readings ranging from 0 to 120
ppm. LEL and CH4 volume readings were consistent at 0%. The methane
well, located in the central portion of the landfill, revealed methane
concentrations ranging from 40 to 1,020 ppm, with a %LEL between 0% and
10%. CH4 by volume was measured at 0.102%. In addition, methane
monitoring was conducted inside the enclosed structures identified as the
scale house, the recycling center/storage area, and the tipping scale area.
No measurable methane levels were detected at these locations with the
exception of a low level methane reading at the recycle center ranging from
0 to 30 ppm. A Quarterly Methane Monitoring Data Summary is provided in
Table 2, and a NCDWM-Solid Waste Section Landfill Gas Monitoring Data
Form is provided in Appendix B.
1.2 Proximity of the Plume to the Nearest Receptor
(Refer to Figure 2)
Sensitive receptors of contamination, as defined by the NCDEQ "include
groundwater supply wells and subsurface building structures, as well as any
potential for adverse impact to humans, plants, or animals." Five surrounding
water supply wells were identified in 2008 by Alleghany County personnel,
located within a 500 foot buffer of the former landfill. Figure 2 is a site map
that includes the domestic well locations. A summary of surrounding water
wells are as follows:
WELL
OWNER/
WELL
MUNICIPAL
MUNICIPAL
APPROXIMATE
#
ADDRESS
TYPE/
WATER
WATER
DISTANCE FROM
USE
AVAILABLE
CONNECTION
SOURCE AREA OF
RELEASE (ft.)
1
Alleghany Co.
Drinking
NO
NO
<200'
P.O. Box 366
&
Sparta, NC 28675
Irrigation
2
Marry Perry
Drinking
NO
NO
490'
501 Osborne Rd.
&
Sparta, NC 28675
Irrigation
3
Mary & Rick Perry
Drinking
NO
NO
420'
464 Osborne Rd.
&
Sparta, NC 28675
Irrigation
4
Billy Dale Alley
Drinking
NO
NO
420'
264 Osborne Rd.
&
Sparta, NC 28675
Irrigation
4

July 11, 2022
5
Edwin & Laura
Drinking
NO
NO
400'
Bloodworth
&
231 Osborne Rd.
Irrigation
Sparta, NC 28675
(Inactive)
The five surrounding domestic water supply wells were initially sampled in
July 2008 and revealed all hydrocarbon concentrations to be compliant. Due
to the continued low level vinyl chloride concentrations found at 0303T-MW3,
the closest cross hydraulic gradient water supply well, Well #5, was included
in the December, 2012 monitoring event and sampled for Appendix I VOCs
and Metals. All compounds were found to be compliant. Since that time,
Well #5 has remained inactive due to property abandonment. The on -site
water supply well, Well #1 was sampled in late November, 2017 and was
found to remain compliant. An updated water supply well survey was
conducted during a previous event. Wells 1-4 appear to still be in use. Well
#5 is on an abandoned property and its building structure is uninhabitable.
1.3 Description of Current Plume Size
Historical results have shown varying low level hydrocarbon concentrations
of benzene and vinyl chloride exceeding NCAC T:15A 02L Groundwater
Standards at monitoring well 0303T-MW1 and 0303T-MW3. Also, 0303T-
MW2 has revealed low level methylene chloride and 1,1 dichloroethane
concentrations during several previous events above the State action limit.
This event revealed all groundwater and surface water samples to be
compliant for all Appendix 1 Vocs with the exception of 0303T-MW3 which
contained estimated vinyl chloride at 0.67 ppm. The Appendix 1 metals
barium, cobalt, and vanadium were found at low level non -compliant
concentrations. Vanadium exceeding 2L IMAC standards was found at
0303T-MW 1 ,0303T-MW3, and stream samples 0303T-ST1 and 0303T-ST2.
Cobalt exceeding 2L IMAC standards was found at 0303T-MW2 and 0303T-
MW3. Barium exceeding MCL was found at 0303T-MW3.
0303T-MW3 Evaluation
The contaminant vinyl chloride has been present at times within the surficial
groundwater aquifer monitoring well 0303T-MW3. In review of historical data
dating back to 2008 and as shown on Figure 3, vinyl chloride was below
quantitation limits during the 7/2/2008 sampling event. Starting 12/18/2008
through 12/14/12, non -compliant vinyl chloride concentrations ranging from
estimated 0.320 ppb to 1.56 ppb were found to be present within the well.
For the following year from 6/19/13 to 6/12/14, no vinyl chloride
concentrations were detected. Since that period up to present, the vinyl
chloride concentrations have been found from none detected to 1.3 ppb.
This event revealed a continued non -compliant vinyl chloride estimated
concentration decreasing to 0.67 ppb. It appears that the contaminant is
stable within a localized area and does not appear to be a threat to human
health or the environment. 0303T-MW3 is considered an upgradient
0

July 11, 2022
background well and is immediately bordered to the north by mountainside.
Sparse residential activity is present to the northwest at greater than 500'
with no legitimate identifiable source for the contaminant.
At this point, it remains undetermined as to the source of the vinyl chloride
for there have been no historical reported spills or other known incidents in
this location. It is theorized that the contaminant could possibly be
associated with residuals from PVC (polyvinyl chloride) well materials.
1.4 Groundwater Flow Direction
(Refer to Figure 4)
As presented on Figure 4, groundwater flow appears consistent with
historical data and remains toward the southeast under the site.
1.5 Predictive Rate of Contaminant Transport
As shown on Figure 4, an overall groundwater flow toward the southeast
was identified within the area of investigation. A hydraulic gradient (dh/dl) of
4.1 % was calculated between 0303T-MW2 and 0303T-MW4. No slug
testing or other hydrogeological testing has been conducted as of this date.
In the event contaminant concentrations significantly increase or begin to
appearwithin down gradient wells, additional hydrogeological analyses could
become necessary.
2.0 CONCLUSIONS AND RECOMMENDATIONS
Review of historical results have shown fluctuating low level volatile hydrocarbon
compounds meeting and exceeding the NCAC T:15A 02L Groundwater Standards
at monitoring wells 0303T-MW1 through 0303T-MW5. Review of the current
analytical results for Appendix I Volatiles indicate all of the monitoring wells and
stream samples to be compliant for all hydrocarbon compounds tested with the
exception of low level non -compliant vinyl chloride found at 0303T-MW-3.
Vanadium exceeding 2L IMAC standards was found at 0303T-MW1, 0303T-MW3,
and slightly turbid stream samples 0303T-ST1 and 0303T-ST2. Cobalt exceeding
2L IMAC standards was found at 0303T-MW2 and 0303T-MW3. Barium exceeding
MCL was found at 0303T-MW3. All other monitoring wells and stream samples
revealed compliant metals compounds tested.
In a continued evaluation of the low level vinyl chloride contamination present at
0303T-MW3, it appears that the contaminant is stable within a localized area and
does not appear to be a threat to human health or the environment. 0303T-MW3
is considered an upgradient background well and is immediately bordered to the
north by mountainside. Sparse residential activity is present to the northwest at
greater than 500' with no legitimate identifiable source for the contaminant. At this
point, it is undetermined as to the source of the vinyl chloride for there have been
9

July 11, 2022
no historical reported spills or other known incidents in this specific location.
Residuals from PVC (poly vinyl chloride) well materials could possibly be a
contributive source. The well will continue to be closely monitored and in the event
contaminant concentrations significantly increase or begin to appear within down
gradient wells, additional hydrogeological analyses or assessment could become
necessary.
Historical methane monitoring at the site revealed the monitoring wells to contain
low level methane readings ranging from 0 to 120 ppm.
During this event, no measurable methane concentrations were detected at any of
the monitoring wells. No detectable methane levels were found at the scale house
or tipping scale area and low level methane ranging from 0 to 30 ppm was found at
the recycling center. The methane well, located in the central portion of the landfill,
revealed methane concentrations ranging from 40 to 1,020 ppm and a %LEL
between 0% and 10%. Methane % volume was calculated at 0.102%.
It is recommended thatthe groundwater/surface water monitoring program continue
on a semi-annual schedule. Methane monitoring for all five monitoring wells, the
on -site methane well, and enclosed structures will continue on a quarterly basis.
7

July 11, 2022
3.0 REFERENCES
North Carolina Department of Environment and Natural Resources, NC Solid Waste
Program. Requirements For Municipal Solid Waste Landfill Facilities (MSWLFs).
North Carolina Department of Environmental and Natural Resources, March 2007.
Ground Water Section Guidelines forthe Investigation and Remediation of Soil and
Ground Water.
North Carolina Department of Environment and Natural Resources, Waste
Management - Constituent List Last Updated 11/15/18.

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>N U E N
0) U E
CD
0 0
0 M
0 CD
E E
N M >,
C CO w.
II co cn '0
L Q
� ) if

TABLE 2
2022 QUARTERLY METHANE MONITORING
DATA SUMMARY
ALLEGHANY COUNTY
0302-MSWLF-1981
SAMPLE LOCATION/
SAMPLED BY
DATE
WELL
DEPTH
IN FEET
METHANE GAS
%LEU %VOLUME
METHANE GAS
PPM
0303T-MW1
3/31/2022
36
0/ 0
10 ppm stabilized
0303T-MW2
3/31/2022
29
0/ 0
0 ppm stabilized
0303T-MW3
3/31/2022
51
0/ 0
0 ppm stabilized
0303T-MW4
3/31/2022
42
0/ 0
0 ppm stabilized
0303T-MW5
3/31/2022
19
0/ 0
0 ppm stabilized
METHANE WELL
3/31/2022
Approx 160
0-30/a/ 0.038%
30-380 ppm
SCALE HOUSE
3/31/2022
NA
0/ 0
0 ppm stabilized
RECYCLING CENTER
3/31/2022
NA
0/ 0
0 ppm stabilized
TIPPING SCALE
3/31/2022
NA
0/ 0
0 ppm stabilized
0303T-MW1
6/16/2022
36
0/ 0
0 ppm stabilized
0303T-MW2
6/16/2022
29
0/ 0
0 ppm stabilized
0303T-MW3
6/16/2022
51
0/ 0
0 ppm stabilized
0303T-MW4
6/16/2022
42
0/ 0
0 ppm stabilized
0303T-MW5
6/16/2022
19
0/ 0
0 ppm stabilized
METHANE WELL
6/16/2022
Approx 160
0-10°/d 0.10%
40-1,020
SCALE HOUSE
6/16/2022
NA
0/ 0
0 ppm stabilized
RECYCLING CENTER
6/16/2022
NA
0/ 0
0 ppm stabilzed
TIPPING SCALE
6/16/2022
NA
0/ 0
0 ppm stabilized
LEL = Lower explosive limit
PPM = Parts per million
NA = Not applicable
Monitoring conducted with RKI Gas Tracer

TABLE 3A (PAGE 1 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
2L
MCL
I 0303T-MW1
DATE SAMPLED
1 6/19/19
12/18/19
1 6/2/20
12/3/20
1 6/30121
12/21/21
1 6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
ND
ND
ND
ND
ND
ND
ND
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
350`
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
4-METHYL-2-PENTANONE
NE
NE
ND
ND
ND
ND
ND
ND
ND
TETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
TRICH LOROFLOU ROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
TRICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
ND
ND I
ND I
ND I
ND
ND ND
Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste
Groundwater Protection Standard (GWP).
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
= Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 2 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L STD.
MCL
0303T-MW2
DATE SAMPLED
6/19/19
12/18/19
6/2/20
12/3/20
6/30/21
12/21/21
6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
0.94 J
0.31 J
ND
ND
0.82 J
ND
0.83 J
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
70
80
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
0.78 J
0.87 J
0.50 J
ND
ND
1.0
1,1-DICHLOROETHANE
6
NE
3.9
3.3
3.4
2.9
2.8
2.7
2.8
1,1-DICHLOROETHENE
350
7
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROETHANE
0.4
5
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
4.0
2.2
4.0
1.6
3.9
2.1
4.2
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
TETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
TRICHLOROFLOUROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
TRICHLOROETHENE
3
5
0.80 J
0.57 J
0.49 J
0.50 J
0.57 J
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
Varies
ND
ND
ND
ND
ND
ND
ND
Snarled areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
(GWP) Standard.
ug/L = parts per billion
NE = not established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 3 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L STD.
MCL
0303T-MW3
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
6/30/21
12/21/22
1 6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
0.42 J
0.71 J
ND
0.98 J
0.76 J
0.73 J
0.46 J
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
1.3
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
350
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
4.6
8.3
3.6
11.0
9.2
9.9
5.8
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
TETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
TRICHLOROFLOUROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
TRICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
0.98 J
ND
1.1
1.1
1.3
0.67 J
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
ND I
ND
ND
ND ND ND
ND
Jnaaea areas represent Concentrations exceeaing the NUAt; U21- Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
ug/L = parts per billion
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP Standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 4 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L STD.
MCL
0303T-MW4
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
1 6/30/21
12/21/21
1 6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
ND
ND
ND
ND
ND
ND
ND
2-BUTANONE
4,000
NE
ND
ND
ND
ND
ND
ND
ND
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
70
80
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
350
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
2-HEXANONE
NE
NE
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND j
ND
ND
TETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
TRICHLORO FLOUROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
TRICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
ND ND I
ND
ND ND
ND ND
Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
ug/L = parts per billion
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP Standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 5 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L STD.
MCL
0303T-MW5
DATE SAMPLED
6/19/19
1 12/18/19
1 6/2/20
1 12/3/20
1 6/30/21
12/21/21
6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
ND
ND
ND
ND
ND
ND
ND
2-BUTANONE
4,000
NE
ND
ND
ND
ND
ND
ND
ND
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
70
80
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
7/350'
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROPROPANE
0.6
NE
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
5
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
2-HEXANONE
NE
NE
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
TETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
TRICHLOROFLOU ROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
TRICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
ND I
ND I
ND
ND I
ND I
ND
ND
anaueu areas represent concentrations exceeding the NUAU U"LL uroundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
ug/L = parts per billion
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP Standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 6 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
MCL
0303T-ST1
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
6/30/21
12/21/21
1 6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
ND
ND
ND
ND
ND
ND
ND
-BUTANONE
4,000
NE
ND
ND
ND
ND
ND
ND
ND
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
70
80
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
350
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
ETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
RICHLOROFLOUROM ETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
RICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND I
ND
ND
ND
ND
ND
ND
ALL OTHER COMPOUNDS
Varies
ND I
ND
ND ND ND
ND
ND
5naded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
ug/L = parts per billion
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP Standard
MCL = Maximum Contaminant Limit

TABLE 3A (PAGE 7 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I VOCs)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
MCL
0303T-ST2
DATE SAMPLED
6/19/19
12/18/19
6/2/20
1 12/3/20
1 6130/21
12/21/21
6/16/22
APPENDIX I VOLATILES/ 8260 MSV LOW LEVEL LANDFILL (CONCENTRATIONS IN ug/L)
ACETONE
6,000
NE
ND
ND
ND
ND
ND
ND
ND
BENZENE
1
5
ND
ND
ND
ND
ND
ND
ND
-BUTANONE
4,000
NE
ND
ND
ND
ND
ND
ND
ND
CARBON DISULFIDE
700
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROBENZENE
50
100
ND
ND
ND
ND
ND
ND
ND
CHLOROETHANE
3,000
NE
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
70
80
ND
ND
ND
ND
ND
ND
ND
CHLOROMETHANE
3
NE
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROBENZENE
20
600
ND
ND
ND
ND
ND
ND
ND
1,4-DICHLOROBENZENE
6
75
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHANE
6
NE
ND
ND
ND
ND
ND
ND
ND
1,1-DICHLOROETHENE
350
7
ND
ND
ND
ND
ND
ND
ND
CIS-1,2-DICHLOROETHENE
70
70
ND
ND
ND
ND
ND
ND
ND
1,2-DICHLOROPROPANE
0.6
5
ND
ND
ND
ND
ND
ND
ND
1,4-DIOXANE
3
NE
ND
NA
NA
NA
NA
NA
NA
ETHYLBENZENE
600
700
ND
ND
ND
ND
ND
ND
ND
METHYLENE CHLORIDE
5
5
ND
ND
ND
ND
ND
ND
ND
ETRACHLOROETHENE
0.7
5
ND
ND
ND
ND
ND
ND
ND
1,1,1-TRICHLOROETHANE
200
200
ND
ND
ND
ND
ND
ND
ND
RICHLOROFLOUROMETHANE
2,000
NE
ND
ND
ND
ND
ND
ND
ND
TOLUENE
600
1,000
ND
ND
ND
ND
ND
ND
ND
RICHLOROETHENE
3
5
ND
ND
ND
ND
ND
ND
ND
VINYL CHLORIDE
0.03
2
ND
ND
ND
ND
ND
ND
ND
TOTAL XYLENE
500
10,000
ND
ND
ND
ND
ND
ND
ND
,JALL OTHER COMPOUNDS
Varies
ND ND I
ND I ND
ND
ND
ND
Shaded areas represent concentrations exceeding the NGAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
ug/L = parts per billion
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed
Groundwater Protection Compliance Standards updated October 15, 2018
Note: Compounds listed are not established (NE) as per DEQ Calculated GWP Standard
MCL = Maximum Contaminant Limit

TABLE 3B (PAGE 1 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
IMAC
MCL
STOP
0303T-MW1
DATE SAMPLED
6/19/19
12/18/19
6/2/20
1 12/3/20
6/30/21
12/21/21
1 6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
NE
0.010
NE
ND
ND
ND
ND
ND
ND
0.00022J
BARIUM
0.7
NE
2.0
NE
0.0261
0.0220
0.0264
0.0233
0.0655
0.0279
0.0176
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
ND
CADMIUM
0.002
NE
0.005
NE
ND
0.00060J
ND
ND
0.0013
ND
0.0000891
CHROMIUM
0.010
NE
0.100
NE
ND
0.0010J
ND
ND
ND
ND
0.00075J
COBALT
NE
0.001
NE
NE
ND
ND
ND
ND
ND
ND
0.00014J
COPPER
1.0
NE
1.3
NE
0.0021
0.0034J
ND
ND
ND
ND
0.0025
LEAD
0.015
NE
0.015
NE
ND
ND
ND
ND
ND
ND
0.00079J
MERCURY
0.001
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
NICKEL
0.10
NE
NE
NE
0.0016
0.0025J
ND
ND
0.0037J
ND
0.0013
SELENIUM
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
0.00022J
SILVER
0.020
NE
NE
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
ND
VANADIUM
NE
0.0003
NE
NE
ND
ND
ND
ND
ND
ND
I
0.00043J
ZINC
1.0
NE
NE
NE
ND
ND
ND
ND
ND
ND
0.0027J
anaaea areas represent concentrations exceeding the NUAU 02L groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 3B (PAGE 2 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
IMAC
MCL
STOP
0303T-MW2
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
12/3/20
6/30/21
12/21/21
6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
NE
0.010
NE
ND
ND
0.0066J
ND
ND
ND
0.000097J
BARIUM
0.7
NE
2.0
NE
0.0623
0.0563
0.0776
0.0680
0.0888
0.0786
0.0977
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
ND
CADMIUM
0.002
NE
0.005
NE
ND
ND
ND
ND
ND
ND
ND
CHROMIUM
0.010
NE
0.100
NE
ND
ND
ND
ND
ND
ND
ND
COBALT
NE
0.001
NE
NE
0.0140
ND
0.0047J
ND
0.0126
ND
0.01041
COPPER
1.0
NE
1.3
NE
ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE
ND
ND
ND
ND
ND
ND
0.00024J
MERCURY
0.001
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
NICKEL
0.10
NE
NE
NE
0.0030 J
ND
ND
ND
ND
ND
0.0024
SELENIUM
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
ND
SILVER
0.020
NE
NE
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
0.000060J
VANADIUM
NE
0.0003
NE
I NE I
ND
ND
ND
ND
ND
ND
ND
ZINC
1 1.0 1
NE
I NE I
NE 10.0084
J
ND
0.0118
ND
0.0120
ND 1
0.0149
Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 313 (PAGE 3 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
IMAC
MCL
STD. TO
0303T-MW3
DATE SAMPLED 6/19/19
12/18/19
6/2/20
1 12/3/20
1 6/30/21
1 12/21/21
1 6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
NE
0.010
NE 0.0090 J
ND
0.0064J
0.0056 J
0.0079J
ND
0.0025
BARIUM
0.7
NE
2.0
NE 1.970
2.220
1.560
0.336
1.290
0.512
2.030
BERYLLIUM
NE
0.004
0.004
NE 0.0023
0.0026J
0.0010
ND
0.0017
ND
0.0017
CADMIUM
0.002
NE
0.005
NE 0.0023
ND
0.0051
0.0139
0.0009J
0.0232
0.0020
CHROMIUM
0.010
NE
0.100
NE ND
ND
ND
ND
ND
ND
0.00087J
COBALT
NE
0.001
NE
NE 0.0147
0.0222J
0.0076
ND
0.0112
ND
0.0137
COPPER
1.0
NE
1.3
NE ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE 0.0021 J
0.0090J
ND
ND
ND
ND
0.00031J
MERCURY
0.001
NE
0.002
NE ND
ND
ND
ND
ND
ND
0.00016J
NICKEL
0.10
NE
NE
NE 0.0052
0.0085J
0.0052
0.0106
0.0051
0.0138
0.0040
SELENIUM
0.020
NE
0.050
NE ND
ND
ND
ND
ND
ND
0.0011J
SILVER
0.020
NE
NE
NE ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE ND
ND
ND
ND
ND
ND
0.00017J
VANADIUM
NE
0.0003
NE
NE ND
ND
ND
ND
ND
I ND
0.00048J
ZINC
1.0
NE
NE
NE 0.0449
0.0651
0.0544
0.100
0.107
1 0.445
1 0.0562
Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 3B (PAGE 4 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
[MAC
MCL
STOP
0303T-MW4
DATE SAMPLED 6/19/19
12/18/19
6/2/20
1 12/3/20
1 6/30/21
1 12/21/21
1 6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
NE
0.010
NE
ND
ND
ND
ND
0.0056J
ND
ND
BARIUM
0.7
NE
2.0
NE
0.176
0.172
0.120
0.133
0.155
0.181
0.160
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
0.00015
CADMIUM
0.002
NE
0.005
NE
ND
0.00043J
ND
ND
ND
ND
0.000088J
CHROMIUM
0.010
NE
0.100
NE
ND
ND
ND
ND
ND
ND
ND
COBALT
NE
0.001
NE
NE
ND
ND
ND
ND
ND
ND
0.00067J
COPPER
1.0
NE
1.3
NE
ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE
ND
0.0026J
ND
ND
ND
ND
0.00017J
MERCURY
0.001
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
NICKEL
0.10
NE
NE
NE
ND
ND
ND
ND
ND
ND
0.00061J
SELENIUM
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
0.000079,11
SILVER
0.020
NE
NE
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
ND
VANADIUM
NE
0.0003
NE
NE
ND
ND
ND
ND
ND
ND
ND
ZINC
1.0
NE
NE
NE
ND
ND
ND
ND
ND
ND
ND
Snarled areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 3B (PAGE 5 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
2L
IMAC
MCL
GWP
STD.
0303T-MW5
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
1 6/30/21
12/21/21
6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
NE
0.010
NE
ND
ND
ND
ND
ND
ND
0.000098J
BARIUM
0.7
NE
2.0
NE
0.0196
0.0212
0.0202
0.0202
0.0184
0.0200
0.0185
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
0.00012
CADMIUM
0.002
NE
0.005
NE
ND
0.00042J
ND
ND
ND
ND
ND
CHROMIUM
0.010
NE
0.100
NE
ND
ND
ND
ND
ND
ND
0.00051J
COBALT
NE
0.001
NE
NE
ND
ND
ND
ND
ND
ND
0.00087J
COPPER
1.0
NE
1.3
NE
ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE
0.0019 J
ND
ND
ND
ND
ND
ND
NICKEL
0.10
NE
NE
NE
0.0013 J
ND
ND
ND
ND
ND
0.00061J
MERCURY
0.001
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
SELENIUM
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
0.00011J
SILVER
0.020
NE
NE
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
ND
VANADIUM
NE
0.0003
NE
NE
ND
ND
ND
ND
Na
ND
ND
ZINC
1.0
NE
NE
NE 1
0.0164
ND
ND
ND
0.121
ND
0.0113 11
5naded areas represent concentrations exceeding the NGAC: 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 3B (PAGE 6 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
IMAC
MCL
STOP
0303T-ST1
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
1 6/30/21
12/21/21
6/16122
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ARSENIC
0.010
1 NE
0.010
NE
ND
ND
ND
ND
ND
ND
0.00010J
BARIUM
0.7
NE
2.0
NE
0.0353
0.0367
0.0289
0.0336
0.0369
0.0343
0.0421
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
ND
CADMIUM
0.002
NE
0.005
NE
ND
ND
ND
ND
ND
ND
ND
CHROMIUM
0.010
NE
0.100
NE
ND
ND
ND
ND
ND
ND
0.00056J
COBALT
NE
0.001
NE
NE
ND
ND
ND
ND
ND
ND
0.00057J
COPPER
1.0
NE
1.3
NE
ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE
ND
0.00191
ND
ND
ND
ND
0.00027J
NICKEL
0.10
NE
NE
NE
0.0015 J
0.0011J
ND
ND
ND
ND
0.0012
MERCURY
0.001
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
SELENIUM
0.020 1
NE
0.002
NE
ND
ND
ND
ND
ND
ND
0.000073J
SILVER
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
ND
VANADIUM
NE
0.0003
NE
NE
0.0020 J
ND
ND
ND
ND
ND
ZINC
1.0
NE
NE
NE
ND
ND
ND
ND
ND
ND
P0.0011
ND
Shaded areas represent
concentrations exceeding the
NCAC 02L Groundwater
Standards
nr Snliri
Waste ('rni
indwntar
Prntnrtinn
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

TABLE 3B (PAGE 7 OF 7)
HISTORICAL GROUNDWATER SAMPLE RESULTS SUMMARY
(APPENDIX I METALS)
ALLEGHANY COUNTY LANDFILL
SPARTA, NORTH CAROLINA
ANALYTE
NCAC
02L
STD.
IMAC
MCL
STWDP
0303T-ST2
DATE SAMPLED
6/19/19
12/18/19
1 6/2/20
1 12/3/20
6/30/21
12/21/21
6/16/22
APPENDIX I METALS (CONCENTRATIONS IN mg/L)
ANTIMONY
NE
NE
NE
0.001
ND
ND
0.0034 J
ND
ND
ND
ND
ARSENIC
0.010
NE
0.010
NE
ND
ND
0.0075J
ND
ND
ND
0.000094J
BARIUM
0.7
NE
2.0
NE
0.0211
0.0136
0.0352
0.0144
0.0169
0.0132
0.0154
BERYLLIUM
NE
0.004
0.004
NE
ND
ND
ND
ND
ND
ND
ND
CADMIUM
0.002
NE
0.005
NE
ND
ND
ND
ND
ND
ND
ND
CHROMIUM
0.010
NE
0.100
NE
ND
ND
ND
ND
ND
ND
0.00071J
COBALT
NE
0.001
NE
NE
ND
ND
ND
ND
ND
ND
0.00060J
COPPER
1.0
NE
1.3
NE
ND
ND
ND
ND
ND
ND
ND
LEAD
0.015
NE
0.015
NE
ND
ND
ND
ND
ND
ND
0.00039J
NICKEL
0.10
NE
NE
NE
0.0016 J
ND
ND
ND
ND
ND
0.00094J
SELENIUM
0.020
NE
0.002
NE
ND
ND
ND
ND
ND
ND
ND
SILVER
0.020
NE
0.050
NE
ND
ND
ND
ND
ND
ND
ND
THALLIUM
NE
0.0002
0.002
NE
ND
ND
ND
ND
ND
ND
ND
VANADIUM
NE
0.0003
NE
NE
0.0020 J
ND
0.0050
ND
ND
ND
0.00084J
ZINC
1.0
NE
NE
NE
0.0040 J
ND
ND
ND
ND
ND
ND
Shaded areas represent concentrations exceeding the NCAC 02L Groundwater Standards or Solid Waste Groundwater Protection
Standard (GWP).
2L IMAC = Interim Maximum Allowable Concentration MCL = Maximum Contaminant Level
Groundwater Protection Compliance Standards updated October 15, 2018
mg/L = parts per million
NE = Not Established
J = Estimated Concentration
ND = None Detected
NA = Not Analyzed

FIGURES

Fi,
te ; : � - qp W.3 1
�..
►, ^' Scale House 0303T-MW4
Rd Storage Center
Former Landfill
' Methane -
_ _ Monitoring WellZ�II
Former Landfill V r
• 0303T-MW2 A.
ru ti
TI
0303T-MW5
I 0303T-ST2
Vile Creek. ��►
LEGEND
9 Monitoring Well
E) Methane Well N
• Stream Sampling locations
Adapted from the Alleghany County
GIS On -Line Website Aerial Dated 2014.
TITLE: SITE MAP WITH MONITORING WELL FIGURE:
Applied Resource AND STREAM SAMPLE LOCATIONS
Management, P C. JOB: SCALE: DATE: DRAWN BY:
Hampstead, NC2aaa3 9625 Approx:
- �nn� 1/6/17 KLC/EFC

LO
N
m C.0
O m
3
0
CU
El
�;

wM
ZZ/9L/9 0-1LZ/LZ/ZL O
LL
LZ/OE/9
� J m
O p OZ/E2 L
z
O OZ/Z/9 0 W J
N I I m-0 0
C\l0 v (I 6L/6L2L �, p
O += I 6 L/6 L/9 0 J Z
+� _� ` (n = O
N
J 8L/E2L E U w 't
in
}� Q ti
SL/b4/9 N Z I p
Z
b u/o£nL � o � v
LULZ/9 v U Z -�
bi Ro U)
I 9L/L/ZL z° 00 < Q
c~n U)
9L/Z/9 =
—polo ! 9 UL L2 L Llj N
'p 6 V J (p
"= I SL/SL/9 N O
J I c
bL/8L2L C)
I �
I0 VL2L/9 d
!' E UWU cu
V
I- I U)
p EL/6L/9 v
v a ZUK/U
M cu i� U
0O � ZL/lZ/9 Z3 q
., 00 (o +1'
a U) LL/9L/ZL
L
0 LL/EL/9 _
O N 3'. 0) 4)
'0 O L/ZZ2 L
O :)O Q
+� LO OL/6/9
C) .�
-� 04 60/ZZ2 L -p Q Q Q
o L- Q a� a
Q602/9 : (D N 00
V H, 0 0 0 0
J Z 80/82l cp N 0 C)
p O O :2 2
V 802/L
L C) d co N J a O
I/fin uoilealuaouoo apiaolyC) lAuin m z

16
`'0303T-MW3�
rm 0°; (3,051.75)
aje House %�
so � 0303T-N
kIn1pping sale 3 043.4
F `
Afrea !�^
Rd�le/Storage Center
w - �-
000
(3,040.00) Former Landfi
L
�.
!A.
030.00 ■ =00 Oo"
lb
R►
ZFormer Landfill 0100- 0303T-MW2
sow (3,018.81)
(3,020.00) " �■
R0303� �.
LEGEND
6 Monitoring Well
(3,051.75) Groundwater Elevation In Feet AMSL N
Contour Interval = 10'
Hydraulic Flow Direction
Adapted from the Alleghany County GIS On -Line Website Aerial Dated 2014.
TITLE. GROUNDWATER TABLE CONTOURS FIGURE:
Applied Resource AS OF 6/16/22
Management, P C. JOB: SCALE: JDATE: DRAWN BY: ..
Hampstead, NC2e443 9625 1 Approx. ' 7/14/22 JLZ

APPENDIX A

..Analytical'
www.pacalabs.oaa
June 24, 2022
Joe Zuncich
ARM'S Waterworks
PO Box 882
Hampstead, NC 28443
RE: Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Dear Joe Zuncich:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network.
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
aAAa
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. LLC
Page 1 of 36

aceAnalytical
wmpacal&63.c0o
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersviile, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification M 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #. E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36

aceAnalytical
www.pacelabs.com
Project.
Pace Project No
ALLEGHANY COUNTY LANDFILL
92610715
Lab ID
Sample ID
92610715001
0303T-MW1
92610715002
0303T-MW2
92610715003
0303T-MW3
92610715004
0303T-MW4
92610715005
0303T-MW5
92610715006
0303T-ST1
92610715007
0303T-ST2
92610715008
TRIP BLANK
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water
06/16/2214:37
06/17/2213:32
Water
06/16/2211:42
06/17/2213:32
Water
06/16/2216:42
06/17/2213:32
Water
06/16/2215:52
06/17/2213:32
Water
06/16/2213:27
06/17/2213:32
Water
06/16/2212:45
06/17/2213:32
Water
06/16/2213:47
06/17/2213:32
Water
06/16/22 00:00
06/17/22 13:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36

aceAnalytical
www.paeNabs.carrr
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Lab ID Sample ID
92610715001 0303T-MW1
92610715002 0303T-MW2
92610716003 0303T-MW3
92610715004 0303T-MW4
92610715005 0303T-MW5
92610715006 0303T-ST1
92610716007 0303T-ST2
92610715008 TRIP BLANK
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
SAMPLE ANALYTE COUNT
Method
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 200.8 Rev 5.4
EPA 245.1 Rev 3.0 1994
EPA 8260D
EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts Reported Laboratory
D1361
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
CRW, DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
CRW, DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
DBB1
15
PASI-A
NMP
1
PASI-A
CL
53
PASI-C
CL
53
PASI-C
Page 4 of 36

aceAnalytical s
www.pacolabs.com
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW1 Lab ID: 92610715001 Collected: 06/16/22 14:37 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 22:45
7440-36-0
Arsenic
/ 0.22.1
�17f0
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 22:45
7440-38-2
Barium
17.6
ug/L
1.0
0.21
1
06/21/22 12:15
06/21/22 22:45
7440-39-3
Beryllium
NO
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 22:45
7440-41-7
Cadmium 000031 0.089J
ug/L
0.20
0,060
1
06/21/22 12:15
06/21/22 22:45
7440-43-9
Chromium
0.75J
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 22:45
7440-47-3
Cobalt
0.14J
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 22:45
7440-48-4
Copper
2.5
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 22:45
7440-50-8
Lead
0.79J
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 22:45
7439-92-1
Nickel
1.3
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 22:45
7440-02-0
Selenium
0.22J
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 22:45
7782-49-2
Silver
ND
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 22:45
7440-22-4
Thallium
NO
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 22:45
7440-28-0
Vanadium
0.43J
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 22:45
7440-62-2
Zinc
2.7.11
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 22:45
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services - Asheville
Mercury
NO
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:09
7439-97-6
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/22/22 07:56
67-64-1
Acrylonitrile
NO
ug/L
10.0
1.8
1
06/22/22 07:56
107-13-1
Benzene
NO
ug/L
1.0
0.34
1
06/22/22 07:56
71-43-2
Bromochloromethane
NO
ug/L
1.0
0.47
1
06/22/22 07:56
74-97-5
Bromodichloromethane
NO
ug/L
1.0
0.31
1
06/22/22 07:56
75-27-4
Bromoform
NO
ug/L
1.0
0.34
1
06/22/22 07:56
75-25-2
Bromomethane
NO
ug/L
2.0
1.7
1
06/22/22 07:56
74-83-9
Carbon disulfide
ND
ug/L
2.0
0.36
1
06/22/22 07:56
75-15-0
Carbon tetrachloride
NO
ug/L
1.0
0.33
1
06/22/22 07:56
56-23-5
Chlorobenzene
NO
ug/L
1.0
0.28
1
06/22/22 07:56
108-90-7
Chloroethane
NO
ug/L
1.0
0.65
1
06/22/22 07:56
75-00-3
Chloroform
NO
ug/L
1.0
0.43
1
06/22/22 07:56
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
06/22/22 07:56
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/22/22 07:56
96-12-8
Dibromochloromethane
NO
ug/L
1.0
0.36
1
06/22/22 07:56
124-48-1
1,2-Dibromoethane(EDB)
NO
ug/L
1.0
0.27
1
06/22/22 07:56
106-93-4
Dibromomethane
NO
ug/L
1.0
0.39
1
06/22/22 07:56
74-95-3
1,2-Dichlorobenzene
NO
ug/L
1.0
0.34
1
06/22/22 07:56
95-50-1
1,4-Dichlorobenzene
NO
ug/L
1.0
0.33
1
06/22/22 07:56
106-46-7
trans-1,4-Dichloro-2-butene
NO
ug/L
1.0
0.56
1
06/22/22 07:56
110-57-6
1,1-Dichloroethane
NO
ug/L
1.0
0.37
1
06/22/22 07:56
75-34-3
1,2-Dichloroethane
NO
ug/L
1.0
0.32
1
06/22/22 07:56
107-06-2
1,1-Dichloroethene
NO
ug/L
1.0
0.35
1
06/22/22 07:56
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services LLC Page 5 of 36

aceAnalj cal"
WW.puN863XM
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW1 Lab ID: 92610715001 Collected: 06/16/22 14:37 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No Qual
8260D MSV Low Level
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometh a ne
1,2,3-Trichloropropane
1,1,2-Trichlorotrifluoroethane
1,2,3-Trimethylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/24/2022 09:29 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/22/22 07:56
156-59-2
ND
ug/L
1.0
0.40
1
06/22/22 07:56
156-60-5
ND
ug/L
1.0
0.36
1
06/22/22 07:56
78-87-5
ND
ug/L
1.0
0.36
1
06/22/22 07:56
10061-01-5
ND
ug/L
1.0
0.36
1
06/22/22 07:56
10061-02-6
ND
ug/L
1.0
0.30
1
06/22/22 07:56
100-41-4
ND
ug/L
5.0
0.48
1
06/22/22 07:56
591-78-6
ND
ug/L
20.0
9.7
1
06/22/22 07:56
74-88-4
ND
ug/L
5.0
2.0
1
06/22/22 07:56
75-09-2
ND
ug/L
5.0
2.7
1
06/22/22 07:56
108-10-1
ND
ug/L
1.0
0.29
1
06/22/22 07:56
100-42-5
ND
ug/L
1.0
0.31
1
06/22/22 07:56
630-20-6
ND
ug/L
1.0
0.22
1
06/22/22 07:56
79-34-5
ND
ug/L
1.0
0.29
1
06/22/22 07:56
127-18-4
ND
ug/L
1.0
0.48
1
06/22/22 07:56
108-88-3
_ ND
ug/L
1.0
0.33
1
06/22/22 07:56
71-55-6
ND
ug/L
1.0
0.32
1
06/22/22 07:56
79-00-5
ND
ug/L
1.0
0.38
1
06/22/22 07:56
79-01-6
ND
ug/L
1.0
0.30
1
06/22/22 07:56
75-69-4
ND
ug/L
1.0
0.26
1
06/22/22 07:56
96-18-4
ND
ug/L
1.0
0.32
1
06/22/22 07:56
76-13-1
ND
ug/L
1.0
0.33
1
06/22/22 07:56
526-73-8
ND
ug/L
1.0
0.50
1
06/22/22 07:56
95-63-6
ND
ug/L
1.0
0.33
1
06/22/22 07:56
108-67-8
ND
ug/L
2.0
1.3
1
06/22/22 07:56
108-05-4
ND
ug/L
1.0
0.39
1
06/22/22 07:56
75-01-4
ND
ug/L
1.0
0.34
1
06/22/22 07:56
1330-20-7
100
%
70-130
1
06/22/22 07:56
460-00-4
111
%
70-130
1
06/22/22 07:56
17060-07-0
100
%
70-130
1
06/22/22 07:56
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 6 of 36

acMnalytical
www.pacelabs.eam
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW2 Lab ID: 92610716002 Collected: 06/16/22 11:42 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 22:49
7440-36-0
Arsenic
0.097J
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 22:49
7440-38-2
Barium
97.7
ug/L
1.0
0.21
1
06/21/22 12:15
06/21/22 22:49
7440-39-3
Beryllium
ND
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 22:49
7440-41-7
Cadmium
ND
ug/L
0.20
0.060
1
06/21/22 12:15
06/21/22 22:49
7440-43-9
Chromium
ND
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 22:49
7440-47-3
Cobalt
10.1
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 22:49
7440-48-4
Copper
ND
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 22:49
7440-50-8
Lead
0.24.1
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 22:49
7439-92-1
Nickel
2.4
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 22:49
7440-02-0
Selenium
ND
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 22:49
7782-49-2
Silver
ND
ug/L
0.40
0,070
1
06/21/22 12:15
06/21/22 22:49
7440-22-4
Thallium
0.060J
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 22:49
7440-28-0
Vanadium
ND
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 22:49
7440-62-2
Zinc
14.9
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 22:49
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:15
7439-97-6
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/21/22 23:19
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/21/22 23:19
107-13-1
Benzene
0.83J
ug/L
1.0
0.34
1
06/21/22 23:19
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/21/22 23:19
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/21/22 23:19
75-274
Bromoform
ND
ug/L
1.0
0.34
1
06/21/22 23:19
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/21/22 23:19
74-83-9
Carbon disulfide
ND
ug/L
2.0
0.36
1
06/21/22 23:19
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/21/22 23:19
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/21/22 23:19
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/21/22 23:19
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
06/21/22 23:19
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/21/22 23:19
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/21/22 23:19
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/21/22 23:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/21/22 23:19
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/21/22 23:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/21/22 23:19
95-50-1
1,4-Dichlorobenzene
1.0
ug/L
1.0
0.33
1
06/21/22 23:19
106-46-7
trans- 1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/21/22 23:19
110-57-6
1,1-Dichloroethane
2.8
ug/L
1.0
0.37
1
06/21/22 23:19
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/21/22 23:19
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/21/22 23:19
75-35-4
REPORT OF LABORATORY ANALYSIS
IK,v1
v1
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services LLC Page 7 of 36

aceAnalytical e
wwepacelahs.cws
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW2
Lab ID:
92610715002
Collected:
06/16/22 11:42
Received: 06/17/22 13-32 Matrix. Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis- 1,2-Dichloroethene
4.2
ug/L
1.0
0.38
1
06/21/22 23:19
156-59-2
trans- 1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/21/22 23:19
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
06/21/22 23:19
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/21/22 23:19
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/21/22 23:19
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/21/22 23:19
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/21/22 23:19
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/21/22 23:19
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/21/22 23:19
75-09-2
4-Methyl-2-pentanone (MIRK)
ND
ug/L
5.0
2.7
1
06/21/22 23:19
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/21/22 23:19
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0,31
1
06/21/22 23:19
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/21/22 23:19
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/21/22 23:19
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/21/22 23:19
108-88-3
1, 1, 1 -Trichloroethane
ND
ug/L
1.0
0.33
1
06/21/22 23:19
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/21/22 23:19
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/21/22 23:19
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/21/22 23:19
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/21/22 23:19
96-18-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
0.32
1
06/21/22 23:19
76-13-1
1,2,3-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/21/22 23:19
526-73-8
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/21/22 23:19
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/21/22 23:19
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/21/22 23:19
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/21/22 23:19
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/21/22 23:19
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/21/22 23:19
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
06/21/22 23:19
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
06/21/22 23:19
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 8 of 36

aceAnalytical
wwr.pacelabs.com
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW3 Lab ID: 92610716003 Collected: 06/16/22 16:42 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 22:53
7440-36-0
Arsenic
2.5
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 22:53
7440-38-2
Barium
2030
ug/L
20.0
4.3
20
06/21/22 12:15
06/22/22 22:00
7440-39-3
Beryllium
1.7
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 22:53
7440-41-7
Cadmium
2.0
ug/L
0.20
0.060
1
06/21/22 12:15
06/21/22 22:53
7440-43-9
Chromium
0.87J
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 22:53
7440-47-3
Cobalt
13.7
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 22:53
7440-48-4
Copper
NO
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 22:53
7440-50-8
Lead
0.31J
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 22:53
7439-92-1
Nickel
4.0
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 22:53
7440-02-0
Selenium
11.11.1
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 22:53
7782-49-2
Silver
ND
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 22:53
7440-22-4
Thallium
0.17.1
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 22:53
7440-28-0
Vanadium
0.48.1
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 22:53
7440-62-2
Zinc
66.2
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 22:53
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
0.116.1
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:17
7439-97-6
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
NO
ug/L
25.0
5.1
1
06/21/22 23:37
67-64-1
Acrylonitrile
NO
ug/L
10.0
1.8
1
06/21/22 23:37
107-13-1
Benzene
0.46.1
ug/L
1.0
0.34
1
06/21/22 23:37
71-43-2
Bromochloromethane
NO
ug/L
1.0
0.47
1
06/21/22 23:37
74-97-5
Bromodichloromethane
NO
ug/L
1.0
0.31
1
06/21/22 23:37
75-27-4
Bromoform
NO
ug/L
1.0
0.34
1
06/21/22 23:37
75-25-2
Bromomethane
NO
ug/L
2.0
1.7
1
06/21/22 23:37
74-83-9
Carbon disulfide
NO
ug/L
2.0
0.36
1
06/21/22 23:37
75-15-0
Carbon tetrachloride
NO
ug/L
1.0
0.33
1
06/21/22 23:37
56-23-5
Chlorobenzene
NO
ug/L
1.0
0.28
1
06/21/22 23:37
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/21/22 23:37
75-00-3
Chloroform
NO
ug/L
1.0
0.43
1
06/21/22 23:37
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
06/21/22 23:37
74-87-3
1,2-Dibromo-3-chloropropane
NO
ug/L
2.0
0.34
1
06/21/22 23:37
96-12-8
Dibromochloromethane
NO
ug/L
1.0
0.36
1
06/21/22 23:37
124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
1.0
0.27
1
06/21/22 23:37
106-93-4
Dibromomethane
NO
ug/L
1.0
0.39
1
06/21/22 23:37
74-95-3
1,2-Dichlorobe nzene
NO
ug/L
1.0
0.34
1
06/21/22 23:37
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/21/22 23:37
106-46-7
trans-1,4-Dichloro-2-butene
NO
ug/L
1.0
0.56
1
06/21/22 23:37
110-57-6
1,1-Dichloroethane
NO
ug/L
1.0
0.37
1
06/21/22 23:37
75-34-3
1,2-Dichloroethane
NO
ug/L
1.0
0.32
1
06/21/22 23:37
107-06-2
1,1-Dichloroethene
NO
ug/L
1.0
0.35
1
06/21/22 23:37
75-35-4
REPORT OF LABORATORY ANALYSIS
IK,v1
v1
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 9 of 36

a ce Analytical
WWW.pacde63.c0m
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW3 Lab ID: 92610715003 Collected: 06/16/22 16:42 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
cis-1,2-Dichloroethene
5.8
ug/L
1.0
0.38
1
06/21/22 23:37
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/21/22 23 37
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
06/21/22 23:37
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/21/22 23:37
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/21/2223.37
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/21/22 23:37
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/21/22 23:37
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/21/22 23:37
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/21/22 23:37
75-09-2
4-Methyl-2-pentanone (MIRK)
ND
ug/L
5.0
2.7
1
06/21/22 23:37
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/21/22 23:37
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/21/22 23:37
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/21/22 23:37
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/21/22 23:37
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/21/22 23:37
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/21/22 23:37
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/21/22 23:37
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/21/22 23:37
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/21/22 23:37
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/21/22 23:37
96-18-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
0.32
1
06/21/22 23:37
76-13-1
1,2,3-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/21/22 23:37
526-73-8
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/21/22 23:37
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0,33
1
06/21/22 23:37
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/21/22 23:37
108-05-4
Vinyl chloride
0.67J
ug/L
1.0
0.39
1
06/21/22 23:37
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/21/22 23:37
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/21/22 23:37
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
06/21/22 23:37
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
06/21/22 23:37
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services LLC
Page 10 of 36

aceAnalytical
www.pcaiab3.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville. NC 28078
[phone]
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Sample: 0303T-MW4 Lab ID: 92610715004 Collected: 06/16/22 15:52 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 22:56
7440-36-0
Arsenic
ND
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 22:56
7440-38-2
Barium
160
ug/L
5.0
1.1
5
06/21/22 12:15
06/22/22 22:04
7440-39-3
Beryllium
0.15
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 22:56
7440-41-7
Cadmium
0.088J
ug/L
0.20
0.060
1
06/21/22 12:15
06/21/22 22:56
7440-43-9
Chromium
ND
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 22:56
7440-47-3
Cobalt
0.67.1
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 22:56
7440-48-4
Copper
ND
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 22:56
7440-50-8
Lead
0.17J
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 22:56
7439-92-1
Nickel
0.611
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 22:56
7440-02-0
Selenium
0.079J
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 22:56
7782-49-2
Silver
ND
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 22:56
7440-22-4
Thallium
ND
ug/L
0.47
0,050
1
06/21/22 12:15
06/21/22 22:56
7440-28-0
Vanadium
ND
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 22:56
7440-62-2
Zinc
ND
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 22:56
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND
. ug/L
0.20
0.12
1
06/21/22 14:14
06/22/22 10:19
7439-97-6
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/22/22 08:15
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/22/22 08 15
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/22/22 08:15
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/22/22 08:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/22/22 08:15
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/22/22 08:15
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/22/22 08:15
74-83-9
Carbon disulfide
ND
ug/L
2.0
0.36
1
06/22/22 08:15
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/22/22 08:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/22/22 08:15
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/22/22 08:15
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
06/22/22 08:15
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/22/22 08:15
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/22/22 08:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/22/22 08:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/22/22 08:15
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/22/22 08:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/22/22 08:15
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:15
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/22/22 08:15
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/22/22 08:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/22/22 08:15
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services. LLC Page 11 of 36

aceAnaljftal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Sample: 0303T-MW4 Lab ID: 92610715004 Collected: 06/16/22 15.52 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
cis-1,2-Dichloroethene
NO
ug/L
1.0
0.38
1
06/22/22 08:15
156-59-2
trans- 1,2-Dichloroethene
NO
ug/L
1.0
0.40
1
06/22/22 08:15
156-60-5
1,2-Dichloropropane
NO
ug/L
1.0
0.36
1
06/22/22 08:15
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
1.0
0.36
1
06/22/22 08:15
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
1.0
0.36
1
06/22/22 08:15
10061-02-6
Ethylbenzene
NO
ug/L
1.0
0.30
1
06/22/22 08:15
100-41-4
2-Hexanone
NO
ug/L
5.0
0.48
1
06/22/22 08:15
591-78-6
lodomethane
NO
ug/L
20.0
9.7
1
06/22/22 08,15
74-88-4
Methylene Chloride
NO
ug/L
5.0
2.0
1
06/22/22 08:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/22/22 08:15
108-10-1
Styrene
NO
ug/L
1.0
0.29
1
06/22/22 08:15
100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
1.0
0.31
1
06/22/22 08:15
630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
1.0
0.22
1
06/22/22 08:15
79-34-5
Tetrachloroethene
NO
ug/L
1.0
0.29
1
06/22/22 08:15
127-18-4
Toluene
NO
ug/L
1.0
0.48
1
06/22/22 08:15
108-88-3
1,1,1-Trichloroethane
NO
ug/L
1.0
0.33
1
06/22/22 08:15
71-55-6
1,1,2-Trichloroethane
NO
ug/L
1.0
0.32
1
06/22/22 08:15
79-00-5
Trichloroethene
NO
ug/L
1.0
0.38
1
06/22/22 08:15
79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
0.30
1
06/22/22 08:15
75-69-4
1,2,3-Trichloropropane
NO
ug/L
1.0
0.26
1
06/22/22 08:15
96-18-4
1,1,2-Trichlorotrifluoroethane
NO
ug/L
1.0
0.32
1
06/22/22 08:15
76-13-1
1,2,3-Trimethylbenzene
NO
ug/L
1.0
0.33
1
06/22/22 08:15
526-73-8
1,2,4-Trimethylbenzene
NO
ug/L
1.0
0.50
1
06/22/22 08:15
95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
1.0
0.33
1
06/22/22 08:15
108-67-8
Vinyl acetate
NO
ug/L
2.0
1.3
1
06/22/22 08:15
108-054
Vinyl chloride
NO
ug/L
1.0
0.39
1
06/22/22 08:15
75-01-4
Xylene (Total)
NO
ug/L
1.0
0.34
1
06/22/22 08:15
1330-20-7
Surrogates
4-Bromofluorobe nzene (S)
101
%
70-130
1
06/22/22 08:15
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
06/22/22 08:15
17060-07-0
Toluene-d8(S)
101
%
70-130
1
06/22/22 08:15
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC
Page 12 of 36

aceAnalytical
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ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-MW5 Lab ID: 92610715005 Collected: 06/16/22 13:27 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 23:07
7440-36-0
Arsenic
0.0981
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 23:07
7440-38-2
Barium
18.6
ug/L
1.0
0.21
1
06/21/22 12:15
06/21/22 23:07
7440-39-3
Beryllium
0.12
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 23:07
7440-41-7
Cadmium
NO
ug/L
0.20
0.060
1
06/21/22 12:15
06/21/22 23:07
7440-43-9
Chromium
0.511
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 23:07
7440-47-3
Cobalt
0.87.1
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 23:07
7440-48-4
Copper _
ND
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 23:07
7440-50-8
Lead
NO
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 23:07
7439-92-1
Nickel
0.611.1
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 23:07
7440-02-0
Selenium
0.11J
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 23:07
7782-49-2
Silver
NO
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 23:07
7440-22-4
Thallium
ND
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 23:07
7440-28-0
Vanadium
ND
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 23:07
7440-62-2
Zinc
11.3
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 23:07
7440-66-6
245.1 Mercury
Analytical Method: EPA
245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:21
7439-97-6
8260D MSV Low Level
Analytical Method: EPA
8260D
Pace Analytical Services - Charlotte
Acetone
NO
ug/L
25.0
5.1
1
06/22/22 08:33
67-64-1
Acrylonitrile
NO
ug/L
10.0
1.8
1
06/22/22 08.33
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/22/22 08:33
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/22/22 08:33
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/22/22 08:33
75-27-4
Bromoform
NO
ug/L
1.0
0.34
1
06/22/22 08:33
75-25-2
Bromomethane
NO
ug/L
2.0
1.7
1
06/22/22 08:33
74-83-9
Carbon disulfide
NO
ug/L
2.0
0.36
1
06/22/22 08:33
75-15-0
Carbon tetrachloride
NO
ug/L
1.0
0.33
1
06/22/22 08:33
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/22/22 08:33
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/22/22 08:33
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
06/22/22 08:33
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
06/22/22 08:33
74-87-3
1,2-Dibromo-3-chloropropane
NO
ug/L
2.0
0.34
1
06/22/22 08:33
96-12-8
Dibromochloromethane
NO
ug/L
1.0
0.36
1
06/22/22 08:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/22/22 08:33
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/22/22 08:33
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/22/22 08:33
95-50-1
1,4-Dichlorobenzene
NO
ug/L
1.0
0.33
1
06/22/22 08:33
106-46-7
trans-1,4-Dichloro-2-butene
NO
ug/L
1.0
0.56
1
06/22/22 08:33
110-57-6
1,1-Dichloroethane
NO
ug/L
1.0
0.37
1
06/22/22 08:33
75-34-3
1,2-Dichloroethane
NO
ug/L
1.0
0.32
1
06/22/22 08:33
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/22/22 08:33
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services. I.I.C. Page 13 of 36

(���a'neAnalj&cale
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project. ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Sample: 0303T-MW5
Lab ID:
92610715005
Collected:
06/16/22 13:27
Received: 06/17/22 13:32 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis- 1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/22/22 08:33
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/22/22 08:33
156-60-5
1,2-DicWoropropane
ND
ug/L
1.0
0.36
1
06/22/22 08:33
78-87-5
cis- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/22/22 08:33
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/22/22 08:33
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/22/22 08:33
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/22/22 08:33
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/22/22 08 33
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/22/22 08:33
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/22/22 08:33
108-10-1
Styrene
NO
ug/L
1.0
0.29
1
06/22/22 08:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/22/22 08:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/22/22 08:33
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/22/22 08:33
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/22/22 08:33
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/22/22 08:33
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:33
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/22/22 08:33
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/22/22 08:33
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/22/22 08:33
96-18-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:33
76-13-1
1,2,3-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:33
526-73-8
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/22/22 08:33
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:33
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/22/22 08:33
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/22/22 08:33
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/22/22 08:33
1330-20-7
Surrogates
4-Bromofluorobenzene(S)
100
%
70-130
1
06/22/22 08:33
460-00-4
1,2-Dichloroethane-d4 (S)
114
%
70-130
1
06/22/22 08:33
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
06/22/22 08:33
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full
without the written consent of Pace Analytical Services, LLC
Page 14 of 36

aceAnalytical
www.pacolobs.com
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-ST1 Lab ID: 92610715006 Collected: 06/16/22 12:45 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 23:11
7440-36-0-
Arsenic
0.10.1
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 23:11
7440-38-2
Barium
42.1
ug/L
1.0
0.21
1
06/21/22 12:15
06/21/22 23:11
7440-39-3
Beryllium
ND
ug/L
0.10
0.050
1
06/21/22 12:15
06/21/22 23:11
7440-41-7
Cadmium
ND
ug/L
0.20
0.060
1
06/21/22 12:15
06/21/22 23:11
7440-43-9
Chromium
0.56J
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 23:11
7440-47-3
Cobalt
0.57.1
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 23:11
7440-48-4
Copper
ND
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 23:11
7440-50-8
Lead
0.27J
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 23:11
7439-92-1
Nickel
1.2
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 23:11
7440-02-0
Selenium
0.073J
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 23:11
7782-49-2
Silver
ND
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 23:11
7440-22-4
Thallium
ND
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 23:11
7440-28-0
Vanadium
1.1
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 23:11
7440-62-2
Zinc
ND
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 23:11
7440-66-6
245.1 Mercury
Analytical Method: EPA
245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
-
Pace Analytical Services - Asheville
Mercury
ND
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:27
7439-97-6
8260D MSV Low Level
Analytical Method: EPA
8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/22/22 08:51
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/22/22 08:51
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/22/22 08:51
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/22/22 08:51
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/22/22 08:51
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/22/22 08:51
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/22/22 08:51
74-83-9
Carbon disulfide
ND
ug/L
2.0
0.36
1
06/22/22 08:51
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/22/22 08:51
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/22/22 08:51
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/22/22 08:51
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
06/22/22 08:51
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/22/22 08:51
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/22/22 08:51
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/22/22 08:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/22/22 08:51
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/22/22 08:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/22/22 08:51
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:51
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/22/22 08:51
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/22/22 08:51
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:51
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/22/22 08 51
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 15 of 36

aceAnalytical
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ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-ST1
Parameters
Lab ID:
Results
92610715006
Units
Collected:
Report
Limit
06/16/22 12.45
MDL OF
Received, 06/17/22 13:32 Matrix- Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis- 1,2-Dichloroethene
NO
ug/L
1.0
0.38
1
06/22/22 08:51
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
1.0
0.40
1
06/22/22 08:51
156-60-5
1,2-Dichloropropane
NO
ug/L
1.0
0.36
1
06/22/22 08:51
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
1.0
0,36
1
06/22/22 08:51
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/22/22 08:51
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/22/22 08:51
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/22/22 08:51
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/22/22 08:51
74-88-4
Methylene Chloride
NO
ug/L
5.0
2.0
1
06/22/22 08:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/22/22 08:51
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/22/22 08:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/22/22 08:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/22/22 08:51
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/22/22 08:51
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/22/22 08:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/22/22 08:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:51
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/22/22 08:51
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/22/22 08:51
75-69-4
1,2,3-Trichloropropane
NO
ug/L
1.0
0.26
1
06/22/22 08:51
96-18-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
0.32
1
06/22/22 08:51
76-13-1
1,2,3-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:51
526-73-8
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/22/22 08:51
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/22/22 08:51
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/22/22 08:51
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/22/22 08:51
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/22/22 08:51
1330-20-7
Surrogates
4-Bromofluorobenzene(S)
100
%
70-130
1
06/22/22 08:51
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
06/22/22 08:51
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
06/22/22 08:51
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 16 of 36

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ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 0303T-ST2 Lab ID: 92610715007 Collected: 06/16/22 13:47 Received: 06/17/22 13:32 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Antimony
ND
ug/L
1.0
0.20
1
06/21/22 12:15
06/21/22 23:15
7440-36-0
Arsenic
0.094J
ug/L
1.0
0.087
1
06/21/22 12:15
06/21/22 23:15
7440-38-2
Barium
16.4
ug/L
1.0
0.21
1
06/21/22 12:15
06/21/22 23:15
7440-39-3
Beryllium
ND
ug/L
0.10
0,050
1
06/21/22 12:15
06/21/22 23:15
7440-41-7
Cadmium
ND
ug/L
0.20
0,060
1
06/21/22 12:15
06/21/22 23:15
7440-43-9
Chromium
0.71J
ug/L
1.0
0.50
1
06/21/22 12:15
06/21/22 23:15
7440-47-3
Cobalt
0.601
ug/L
1.0
0.050
1
06/21/22 12:15
06/21/22 23:15
7440-48-4
Copper
ND
ug/L
2.0
1.1
1
06/21/22 12:15
06/21/22 23:15
7440-50-8
Lead
0.39.1
ug/L
1.0
0.077
1
06/21/22 12:15
06/21/22 23:15
7439-92-1
Nickel
0.94J
ug/L
1.0
0.42
1
06/21/22 12:15
06/21/22 23:15
7440-02-0
Selenium
ND
ug/L
2.0
0.072
1
06/21/22 12:15
06/21/22 23:15
7782-49-2
Silver
ND
ug/L
0.40
0.070
1
06/21/22 12:15
06/21/22 23:15
7440-22-4
Thallium
ND
ug/L
0.47
0.050
1
06/21/22 12:15
06/21/22 23:15
7440-28-0
Vanadium
0.84.1
ug/L
1.0
0.25
1
06/21/22 12:15
06/21/22 23:15
7440-62-2
Zinc
ND
ug/L
10.0
2.7
1
06/21/22 12:15
06/21/22 23:15
7440-66-6
245.1 Mercury
Analytical
Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND
ug/L
0.20
0.12
1
06/21/2214:14
06/22/2210:30
7439-97-6
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/22/22 09:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/22/22 09 10
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/22/22 09:10
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/22/22 09:10
74-97-5
Bromodichloromethane
NO
ug/L
1.0
0.31
1
06/22/22 09:10
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/22/22 09:10
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/22/22 09:10
74-83-9
Carbon disulfide
ND
ug/L
2.0
0.36
1
06/22/22 09:10
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/22/22 09:10
56-23-5
Chlorobenzene
NO
ug/L
1.0
0.28
1
06/22/22 09:10
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/22/22 09:10
75-00-3
Chloroform
ND
ug/L
1.0
0.43
1
06/22/22 09:10
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/22/22 09:10
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/22/22 09:10
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/22/22 09:10
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/22/22 09:10
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/22/22 09:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/22/22 09:10
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/22/22 09:10
106-46-7
trans- 1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/22/22 09:10
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/22/22 09:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 09:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/22/22 09:10
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/24/2022 09.29 AM without the written consent of Pace Analytical Services, LLC Page 17 of 36

aceAnalytkal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Sample: 0303T-ST2
Lab ID:
92610715007
Collected:
06/16/22 13:47
Received. 06/17/22 13:32 Matrix Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/22/22 09:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/22/22 09:10
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.36
1
06/22/22 09:10
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/22/22 09:10
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/22/22 09:10
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/22/22 09:10
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/22/22 09:10
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/22/22 09:10
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/22/22 09:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/22/22 09:10
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/22/22 09:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/22/22 09:10
630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
1.0
0.22
1
06/22/22 09:10
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/22/22 09:10
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/22/22 09:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/22/22 09:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/22/22 09:10
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/22/22 09:10
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/22/22 09:10
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/22/22 09:10
96-18-4
1,1,2-Trichlorotrifluoroethane
NO
ug/L
1.0
0.32
1
06/22/22 09:10
76-13-1
1,2,3-Trimethylbenzene
NO
ug/L
1.0
0.33
1
06/22/22 09:10
526-73-8
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/22/22 09:10
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/22/22 09:10
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/22/22 09:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/22/22 09:10
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/22/22 09:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
06/22/22 09:10
460-00-4
1,2-Dichloroethane-d4 (S)
114
%
70-130
1
06/22/22 09:10
17060-07-0
Toluene-d8(S)
102
%
70-130
1
06/22/22 09:10
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 18 of 36

Pace Analytical Services, LLC
® 9800 KinceyAve Suite loo
aceMalXical Huntersville, NC 28078
www.pacolgbs.com
[phone]
ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Sample: TRIP BLANK Lab ID: 92610715008 Collected: 06/16/22 00:00 Received: 06/17/22 13.32 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
NO
ug/L
25.0
5.1
1
06/21/22 22:42
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/21/22 22:42
107-13-1
Benzene
NO
ug/L
1.0
0.34
1
06/21/22 22.42
7143-2
Bromochloromethane
NO
ug/L
1.0
0.47
1
06/21/22 22:42
74-97-5
Bromodichloromethane
NO
ug/L
1.0
0.31
1
06/21/2222.42
75-27-4
Bromoform
NO
ug/L
1.0
0.34
1
06/21/22 22:42
75-25-2
Bromomethane
NO
ug/L
2.0
1.7
1
06/21/22 22:42
74-83-9
Carbon disulfide
NO
ug/L
2.0
0.36
1
06/21/22 22:42
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/21/22 22:42
56-23-5
Chlorobenzene
NO
ug/L
1.0
0.28
1
06/21/22 22:42
108-90-7
Chloroethane
NO
ug/L
1.0
0.65
1
06/21/22 22:42
75-00-3
Chloroform
NO
ug/L
1.0
0.43
1
06/21/22 22:42
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
06/21/22 22:42
74-87-3
1,2-Dibromo-3-chloropropane
NO
ug/L
2.0
0.34
1
06/21/22 22:42
96-12-8
Dibromochloromethane
NO
ug/L
1.0
0.36
1
06/21/22 22:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/21/22 22:42
106-93-4
Dibromomethane
NO
ug/L
1.0
0.39
1
06/21/22 22:42
74-95-3
1,2-Dichlorobenzene
NO
ug/L
1.0
0.34
1
06/21/22 22:42
95-50-1
1,4-Dichlorobenzene
NO
ug/L
1.0
0.33
1
06/21/22 22:42
106-46-7
trans-1,4-Dichloro-2-butene
NO
ug/L
1.0
0.56
1
06/21/22 22:42
110-57-6
1,1-Dichloroethane
NO
ug/L
1.0
0.37
1
06/21/22 22:42
75-34-3
1,2-Dichloroethane
NO
ug/L
1.0
0.32
1
06/21/22 22:42
107-06-2
1,1-Dichloroethene
NO
ug/L
1.0
0.35
1
06/21/22 22:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/21/22 22:42
156-59-2
trans- 1,2-Dichloroethene
NO
ug/L
1.0
0.40
1
06/21/22 22:42
156-60-5
1,2-Dichloropropane
NO
ug/L
1.0
0.36
1
06/21/22 22:42
78-87-5
cis- 1,3-Dichloropropene
NO
ug/L
1.0
0.36
1
06/21/22 22:42
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
1.0
0.36
1
06/21/22 22:42
10061-02-6
Ethylbenzene
NO
ug/L
1.0
0.30
1
06/21/22 22:42
10041-4
2-Hexanone
NO
ug/L
5.0
0.48
1
06/21/22 22:42
591-78-6
lodomethane
NO
ug/L
20.0
9.7
1
06/21/22 22:42
74-88-4
Methylene Chloride
NO
ug/L
5.0
2.0
1
06/21/22 22:42
75-09-2
4-Methyl-2-pentanone (MIRK)
NO
ug/L
5.0
2.7
1
06/21/22 22:42
108-10-1
Styrene
NO
ug/L
1.0
0.29
1
06/21/22 22:42
100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
1.0
0.31
1
06/21/22 22:42
630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
1.0
0.22
1
06/21/22 22:42
79-34-5
Tetrachloroethene
NO
ug/L
1.0
0.29
1
06/21/22 22:42
127-18-4
Toluene
NO
ug/L
1.0
0.48
1
06/21/22 22:42
108-88-3
1,1,1-Trichloroethane
NO
ug/L
1.0
0.33
1
06/21/22 22:42
71-55-6
1,1,2-Trichloroethane
NO
ug/L
1.0
0.32
1
06/21/22 22:42
79-00-5
Trichloroethene
NO
ug/L
1.0
0.38
1
06/21/22 22:42
79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
0.30
1
06/21/22 22:42
75-69-4
1,2,3-Trichloropropane
NO
ug/L
1.0
0.26
1
06/21/22 22:42
96-18-4
1,1,2-Trichlorotrifluoroethane
NO
ug/L
1.0
0.32
1
06/21/22 22:42
76-13-1
1,2,3-Trimethylbenzene
NO
ug/L
1.0
0.33
1
06/21/22 22:42
526-73-8
REPORT OF LABORATORY ANALYSIS
IK,v1
v1
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Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 19 of 36

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ANALYTICAL RESULTS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: TRIP BLANK
Parameters
Lab ID:
Results
92610715008
Units
Collected:
Report
Limit
06/16/22 00:00
MDL DF
Received 06/17/22 13.32 Matrix Water
Prepared Analyzed CAS No Qual
8260D MSV Low Level
Analytical
Method: EPA 8260D
Pace Analytical Services
- Charlotte
1,2,4-Trimethylbenzene
ND
ug/L
1.0
0.50
1
06/21/22 22:42
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
1.0
0.33
1
06/21/22 22:42
108-67-8
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/21/22 22:42
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/21/22 22:42
75-01-4
Xylene (Total)
NO
ug/L
1.0
0.34
1
06/21/22 22:42
1330-20-7
Surrogates
4-Bromofluorobenzene(S)
95
%
70-130
1
06/21/22 22:42
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130•
1
06/21/22 22:42
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
06/21/22 22:42
2037-26-5
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 705892 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610715001, 92610715002, 92610715003, 92610715004, 92610715005, 92610715006, 92610715007
METHOD BLANK: 3682826 Matrix: Water
Associated Lab Samples: 92610715001, 92610715002, 92610715003, 92610715004, 92610715005, 92610715006, 92610715007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury ug/L ND 0.20 0.12 06/22/2210:05
LABORATORY CONTROL SAMPLE: 3682827
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 97 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3682828 3682829
MS MSD
92610715001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.5 97 98 70-130 1 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project- ALLEGHANY COUNTY LANDFILL
Pace Project No. 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 705841 Analysis Method: EPA 200.8 Rev 5.4
QC Batch Method: EPA 200.8 Rev 5.4 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92610715001, 92610715002, 92610715003, 92610715004, 92610715005, 92610715006, 92610715007
METHOD BLANK: 3682568 Matrix: Water
Associated Lab Samples: 92610715001, 92610715002, 92610715003, 92610715004, 92610715005, 92610715006. 92610715007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
1.0
0.20
06/21/22 21:58
Arsenic
ug/L
ND
1.0
0.087
06/21/22 21:58
Barium
ug/L
ND
1.0
0.21
06/21/22 21:58
Beryllium
ug/L
ND
0.10
0.050
06/21/22 21:58
Cadmium
ug/L
ND
0.20
0.060
06/21/22 21:58
Chromium
ug/L
ND
1.0
0,50
06/21/22 21:58
Cobalt
ug/L
ND
1.0
0.050
06/21/22 21:58
Copper
ug/L
ND
2.0
1.1
06/21/22 21:58
Lead
ug/L
ND
1.0
0.077
06/21/22 21:58
Nickel
ug/L
ND
1.0
0.42
06/21/22 21:58
Selenium
ug/L
ND
2.0
0.072
06/21/22 21:58
Silver
ug/L
ND
0.40
0.070
06/21/22 21:58
Thallium
ug/L
ND
0.47
0.050
06/21/22 21:58
Vanadium
ug/L
ND
1.0
0.25
06/21/22 21:58
Zinc
ug/L
ND
10.0
2.7
06/21/22 21:58
LABORATORY CONTROL SAMPLE:
3682569
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Antimony
ug/L
50
50.6
101
85-115
Arsenic
ug/L
50
51.1
102
85-115
Barium
ug/L
50
52.3
105
85-115
Beryllium
ug/L
50
50.9
102
85-115
Cadmium
ug/L
50
50.7
101
85-115
Chromium
ug/L
50
53.0
106
85-115
Cobalt
ug/L
50
52.6
105
85-115
Copper
ug/L
50
52.2
104
85-115
Lead
ug/L
50
50.5
101
85-115
Nickel
ug/L
50
52.2
104
85-115
Selenium
ug/L
50
50.8
102
85-115
Silver
ug/L
25
25.5
102
85-115
Thallium
ug/L
25
25.2
101
85-115
Vanadium
ug/L
50
51.5
103
85-115
Zinc
ug/L
50
52.4
105
85-115
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services LLC Page 22 of 36

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QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3682570
3682571
MS
MSD
92609164001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
50
50
50.0
50.6
99
100
70-130
1
20
Arsenic
ug/L
ND
50
50
51.3
51.2
101
101
70-130
0
20
Barium
ug/L
63.4
50
50
114
115
102
103
70-130
1
20
Beryllium
ug/L
ND
50
50
50.5
51.0
101
102
70-130
1
20
Cadmium
ug/L
0.00026
50
50
50.1
50.6
100
101
70-130
1
20
mg/L
Chromium
ug/L
0.038
50
50
89.0
90.2
101
103
70-130
1
20
mg/L
Cobalt
ug/L
ND
50
50
51.1
51.7
102
103
70-130
1
20
Copper
ug/L
0.0077
50
50
58.2
58.7
101
102
70-130
1
20
mg/L
Lead
ug/L
ND
50
50
50.5
51.2
100
101
70-130
1
20
Nickel
ug/L
0.014
50
50
64.2
66.4
100
104
70-130
3
20
mg/L
Selenium
ug/L
ND
50
50
51.4
51.8
100
100
70-130
1
20
Silver
ug/L
ND
25
25
24.9
25.3
100
101
70-130
2
20
Thallium
ug/L
ND
25
25
24.9
25.2
100
101
70-130
1
20
Vanadium
ug/L
ND
50
50
51.2
51.1
102
102
70-130
0
20
Zinc
ug/L
0.040
50
50
91.0
91.0
103
103
70-130
0
20
mg/L
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 3682572
3682573
MS
MSD
92610715004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
50
50
47.8
51.8
96
104
70-130
8
20
Arsenic
ug/L
ND
50
50
48.7
52.5
97
105
70-130
7
20
Barium
ug/L
160
50
50
208
213
95
106
70-130
3
20
Beryllium
ug/L
0.15
50
50
48.5
53.5
97
107
70-130
10
20
Cadmium
ug/L
0.088J
50
50
48.0
51.8
96
103
70-130
8
20
Chromium
ug/L
ND
50
50
49.4
52.8
98
105
70-130
7
20
Cobalt
ug/L
0.67.1
50
50
49.1
52.4
97
103
70-130
6
20
Copper
ug/L
ND
50
50
48.6
51.7
97
103
70-130
6
20
Lead
ug/L
0.17J
50
50
48.0
51.5
96
103
70-130
7
20
Nickel
ug/L
0.61J
50
50
48.6
52.1
96
103
70-130
7
20
Selenium
ug/L
0.079J
50
50
48.2
52.3
96
105
70-130
8
20
Silver
ug/L
ND
25
25
23.7
25.8
95
103
70-130
9
20
Thallium
ug/L
ND
25
25
24.1
25.8
96
103
70-130
7
20
Vanadium
ug/L
ND
50
50
48.5
52.2
97
104
70-130
7
20
Zinc
ug/L
ND
50
50
52.3
54.7
100
105
70-130
5
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services LLC
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QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
QC Batch: 706000 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92610715001, 92610715004, 92610715005, 92610715006, 92610715007
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 3683525 Matrix: Water
Associated Lab Samples: 92610715001, 92610715004, 92610715005, 92610715006, 92610715007
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/22/22 03:58
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/22/22 03:58
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/22/22 03:58
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/22/22 03:58
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
0.32
06/22/22 03:58
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/22/22 03:58
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/22/22 03:58
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/22/22 03:58
1,2,3-Trimethylbenzene
ug/L
ND
1.0
0.33
06/22/22 03:58
1,2,4-Trimethylbenzene
ug/L
ND
1.0
0.50
06/22/22 03:58
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/22/22 03:58
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/22/22 03:58
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/22/22 03:58
1,2-Dichloroethane
ug/c
ND
1.0
0.32
06/22/22 03:58
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/22/22 03:58
1,3,5-Trimethylbenzene
ug/L
ND
1.0
0,33
06/22/22 03:58
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/22/22 03:58
2-Hexanone
ug/L
ND
5.0
0.48
06/22/22 03:58
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/22/22 03:58
Acetone
ug/L
ND
25.0
5.1
06/22/22 03:58
Acrylonitrile
ug/L
ND
10.0
1.8
06/22/22 03:58
Benzene
ug/L
ND
1.0
0.34
06/22/22 03:58
Bromochloromethane
ug/L
ND
1.0
0.47
06/22/22 03:58
Bromodichloromethane
ug/L
ND
1.0
0.31
06/22/22 03:58
Bromoform
ug/L
ND
1.0
0.34
06/22/22 03:58
Bromomethane
ug/L
ND
2.0
1.7
06/22/22 03:58 v2
Carbon disulfide
ug/L
ND
2.0
0.36
06/22/22 03:58
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/22/22 03:58
Chlorobenzene
ug/L
ND
1.0
0.28
06/22/22 03:58
Chloroethane
ug/L
ND
1.0
0.65
06/22/22 03:58
Chloroform
ug/L
ND
1.0
0.43
06/22/22 03:58
Chloromethane
ug/L
ND
1.0
0.54
06/22/22 03:58
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/22/22 03:58
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/22/22 03:58
Dibromochloromethane
ug/L
ND
1.0
0,36
06/22/22 03:58
Dibromomethane
ug/L
ND
1.0
0.39
06/22/22 03:58
Ethylbenzene
ug/L
ND
1.0
0.30
06/22/22 03:58
lodomethane
ug/L
ND
20.0
9.7
06/22/22 03:58
Methylene Chloride
ug/L
ND
5.0
2.0
06/22/22 03:58
Styrene
ug/L
ND
1.0
0.29
06/22/22 03:58
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 24 of 36

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QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.. 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 3683525 Matrix: Water
Associated Lab Samples: 92610715001, 92610715004, 92610715005, 92610715006, 92610715007
Blank Reporting
Parameter Units Result Limit MDL
Analyzed Qualifiers
Tetrachloroethene
ug/L
ND
1.0
0.29
06/22/22 03:58
Toluene
ug/L
ND
1.0
0.48
06/22/22 03:58
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/22/22 03:58
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/22/22 03:58
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/22/22 03:58
Trichloroethene
ug/L
ND
1.0
0.38
06/22/22 03:58
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/22/22 03:58
Vinyl acetate
ug/L
ND
2.0
1.3
06/22/22 03:58
Vinyl chloride
ug/L
ND
1.0
0.39
06/22/22 03:58
Xylene (Total)
ug/L
ND
1.0
0.34
06/22/22 03:58
1,2-Dichloroethane-d4 (S)
%
113
70-130
06/22/22 03:58
4-Bromofluorobenzene (S)
%
102
70-130
06/22/22 03:58
Toluene-d8 (S)
%
100
70-130
06/22/22 03:58
LABORATORY CONTROL SAMPLE:
Parameter
3683526
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.2
100
70-130
1,1,1-Trichloroethane
ug/L
50
52.4
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.4
97
70-130
1,1,2-Trichloroethane
ug/L
50
50.2
100
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
52.3
105
70-130
1,1-Dichloroethane
ug/L
50
53.8
108
70-130
1,1-Dichloroethene
ug/L
50
54.5
109
70-132
1,2,3-Trichloropropane
ug/L
50
47.6
95
70-130
1,2,3-Trimethylbenzene
ug/L
50
48.5
97
70-130
1,2,4-Trimethylbenzene
ug/L
50
49.4
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
45.6
91
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.4
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.4
97
70-130
1,2-Dichloroethane
ug/L
50
53.3
107
70-130
1,2-Dichloropropane
ug/L
50
52.5
105
70-130
1,3,5-Trimethylbenzene
ug/L
50
49.8
100
70-130
1,4-Dichlorobenzene
ug/L
50
46.8
94
70-130
2-Hexanone
ug/L
100
103
103
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
102
102
70-144
Acrylonitrile
ug/L
250
280
112
70-130
Benzene
ug/L
50
48.1
96
70-130
Bromochloromethane
ug/L
50
53.8
108
70-130
Bromodichloromethane
ug/L
50
51.4
103
70-130
Bromoform
ug/L
50
50.3
101
70-131
Bromomethane
ug/L
50
41.5
83
30-177 v3
Carbon disulfide
ug/L
50
53.9
108
70-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 25 of 36

Pace Analytical Services, LLC
aceMalXical 9800 Kincey Ave Suite 1 o0
Huntersville, NC 28078
ttrwr.pateNobs.caa [phone]
QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
LABORATORY CONTROL SAMPLE:
Parameter
3683526
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Carbon tetrachloride
ug/L
50
48.7
97
70-130
Chlorobenzene
ug/L
50
48.5
97
70-130
Chloroethane
ug/L
50
48.9
98
46-131
Chloroform
ug/L
50
53.4
107
70-130
Chloromethane
ug/L
50
53.7
107
49-130
cis-1,2-Dichloroethene
ug/L
50
54.7
109
70-130
cis-1,3-Dichloropropene
ug/L
50
52.2
104
70-130
Dibromochloromethane
ug/L
50
50.4
101
70-130
Dibromomethane
ug/L
50
48.2
96
70-130
Ethylbenzene
ug/L
50
49.0
98
70-130
lodomethane
ug/L
100
122
122
47-140
Methylene Chloride
ug/L
50
50.3
101
68-130
Styrene
ug/L
50
48.4
97
70-130
Tetrachloroethene
ug/L
50
45.2
90
70-130
Toluene
ug/L
50
46.6
93
70-130
trans-1,2-Dichloroethene
ug/L
50
55.5
111
70-130
trans-1,3-Dichloropropene
ug/L
50
52.7
105
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
49.5
99
25-200
Trichloroethene
ug/L
50
47.9
96
70-130
Trichlorofluoromethane
ug/L
50
46.9
94
61-130
Vinyl acetate
ug/L
100
118
118
70-140
Vinyl chloride
ug/L
50
57.1
114
59-142
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
114
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3683527
3683528
MS
MSD
92610715001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
NO
20
20
23.6
22.3
118
112
70-135
5
30
1,1,1-Trichloroethane
ug/L
NO
20
20
25.7
24.2
128
121
70-148
6
30
1,1,2,2-Tetrachloroethane
ug/L
NO
20
20
23.1
22.1
116
111
70-131
4
30
1,1,2-Trichloroethane
ug/L
ND
20
20
23.2
21.8
116
109
70-136
6
30
1,1,2-
ug/L
NO
20
20
26.6
25.2
133
126
70-154
5
30
Trich to rotriflu oroetha ne
1,1-Dichloroethane
ug/L
NO
20
20
26.2
24.8
131
124
70-147
6
30
1,1-Dichloroethene
ug/L
NO
20
20
26.9
25.6
134
128
70-158
5
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.8
21.8
114
109
67-137
5
30
1,2,3-Trimethylbenzene
ug/L
NO
20
20
23.4
22.7
117
114
70-133
3
30
1,2,4-Trimethylbenzene
ug/L
NO
20
20
23.7
23.2
118
116
70-134
2
30
1,2-Dibromo-3-
ug/L
NO
20
20
21.4
21.4
107
107
69-136
0
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
NO
20
20
23.7
22.5
118
113
70-137
5
30
1,2-Dichlorobenzene
ug/L
NO
20
20
22.7
22.7
114
114
70-133
0
30
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC
Page 26 of 36

aceAna1j cal
[e-mail]
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3683527
3683528
MS
MSD
92610715001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,2-Dichloroethane
ug/L
ND
20
20
25.1
23.6
125
118
67-138
6
30
1,2-Dichloropropane
ug/L
ND
20
20
25.1
237
125
119
70-138
5
30
1,3,5-Trimethylbenzene
ug/L
ND
20
20
24.0
23.7
120
118
70-138
1
30
1,4-Dichlorobenzene
ug/L
ND
20
20
22.6
22.0
113
110
70-133
3
30
2-Hexanone
ug/L
ND
40
40
49.8
48.3
125
121
67-139
3
30
•4-Methyl-2-pentanone
ug/L
ND
40
40
46.3
45.3
116
113
67-136
2
30
(MIBK)
Acetone
ug/L
ND
40
40
47.4
45.7
119
114
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
132
126
132
126
68-140
5
30
Benzene
ug/L
ND
20
20
23.7
22.5
118
113
67-150
5
30
Bromochloromethane
ug/L
ND
20
20
24.8
23.4
124
117
70-146
6
30
Bromodichloromethane
ug/L
ND
20
20
23.8
22.7
119
113
70-138
5
30
Bromoform
ug/L
ND
20
20
22.4
21.1
112
106
57-138
6
30
Bromomethane
ug/L
ND
20
20
19.8
18.8
99
94
10-200
5
30 v3
Carbon disulfide
ug/L
ND
20
20
26.3
25.1
131
125
70-152
5
30
Carbon tetrachloride
ug/L
ND
20
20
23.8
22.7
119
114
70-147
5
30
Chlorobenzene
ug/L
ND
20
20
23.7
22.4
118
112
70-137
6
30
Chloroethane
ug/L
ND
20
20
27.8
26.2
139
131
51-166
6
30
Chloroform
ug/L
ND
20
20
25.5
24.7
127
123
70-144
3
30
Chloromethane
ug/L
ND
20
20
26.9
25.7
135
128
24-161
5
30 v3
cis-1,2-Dichloroethene
ug/L
ND
20
20
26.2
24.8
131
124
67-148
5
30
cis-1,3-Dicbloropropene
ug/L
ND
20
20
23,9
22.6
120
113
70-142
5
30
Dibromochloromethane
ug/L
ND
20
20
23.2
21.7
116
108
68-138
7
30
Dibromomethane
ug/L
ND
20
20
21.7
20.7
109
103
70-134
5
30
Ethylbenzene
ug/L
ND
20
20
24.2
23.1
121
115
68-143
5
30
lodomethane
ug/L
ND
40
40
51.5
47.1
129
118
20-161
9
30
Methylene Chloride
ug/L
ND
20
20
23.2
22.0
116
110
64-148
5
30
Styrene
ug/L
ND
20
20
22.7
21.5
114
108
70-136
5
30
Tetrachloroethene
ug/L
ND
20
20
22.2
21.2
111
106
70-139
5
30
Toluene
ug/L
ND
20
20
22.2
21.5
111
108
47-157
3
30
trans- 1,2-Dichloroethene
ug/L
ND
20
20
27.0
25.7
135
128
70-149
5
30
trans- 1,3-Dichloropropene
ug/L
ND
20
20
24.1
23.0
120
115
70-138
5
30
trans- 1,4-Dichloro-2-butene
ug/L
ND
20
20
23.2
22.5
116
113
31-145
3
30
Trichloroethene
ug/L
ND
20
20
23.6
22.5
118
112
70-149
5
30
Trichlorofluoromethane
ug/L
ND
20
20
24.2
22.6
121
113
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
52.5
49.7
131
124
48-156
6
30
Vinyl chloride
ug/L
ND
20
20
28.4
26.6
142
133
55-172
7
30
Xylene (Total)
ug/L
ND
60
60
72.8
69.3
121
115
66-145
5
30
1,2-Dichloroethane-d4(S)
%
108
109
70-130
4-Bromofluorobenzene(S)
%
105
103
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 27 of 36

aceAnalj cal
WM.Pacelabs.com
QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
QC Batch: 706022 Analysis Method:
QC Batch Method: EPA 8260D Analysis Description:
Laboratory:
Associated Lab Samples: 92610715002, 92610715003, 92610715008
EPA 8260D
8260D MSV Low Level
Pace Analytical Services - Charlotte
METHOD BLANK: 3683660
Matrix: Water
Associated Lab Samples: 92610715002,
92610715003,
92610715008
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/21/22 15:18
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/21/22 15:18
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/21/22 15:18
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/21/22 15:18
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
0.32
06/21/22 15:18
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/21/22 15:18
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/21/22 15:18
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/21/22 15:18
1,2,3-Trimethylbenzene
ug/L
ND
1.0
0.33
06/21/22 15:18
1,2,4-Trimethylbenzene
ug/L
ND
1.0
0.50
06/21/22 15:18
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/21/22 15:18
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/21/22 15:18
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/21/22 15:18
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/21/22 15:18
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/21/22 15:18
1,3,5-Trimethylbenzene
ug/L
ND
1.0
0.33
06/21/22 15:18
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/21/22 15:18
2-Hexanone
ug/L
ND
5.0
0.48
06/21/22 15:18
4-Methyl-2-pentanone (MIRK)
ug/L
ND
5.0
2.7
06/21/22 15:18
Acetone
ug/L
ND
25.0
5.1
06/21/22 15:18
Acrylonitrile
ug/L
ND
10.0
1.8
06/21/22 15:18
Benzene
ug/L
ND
1.0
0.34
06/21/22 15:18
Bromochloromethane
ug/L
ND
1.0
0.47
06/21/22 15:18
Bromodichloromethane
ug/L
ND
1.0
0.31
06/21/22 15:18
Bromoform
ug/L
ND
1.0
0.34
06/21/22 15:18
Bromomethane
ug/L
ND
2.0
1.7
06/21/22 15:18
Carbon disulfide
ug/L
ND
2.0
0.36
06/21/22 15:18
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/21/22 15:18
Chlorobenzene
ug/L
ND
1.0
0.28
06/21/22 15:18
Chloroethane
ug/L
ND
1.0
0.65
06/21/22 15:18
Chloroform
ug/L
ND
1.0
0.43
06/21/22 15:18
Chloromethane
ug/L
ND
1.0
0.54
06/21/22 15:18
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/21/22 15:18
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/21/22 15:18
Dibromochloromethane
ug/L
ND
1.0
0.36
06/21/22 15:18
Dibromomethane
ug/L
ND
1.0
0.39
06/21/22 15:18
Ethylbenzene
ug/L
ND
1.0
0.30
06/21/22 15:18
lodomethane
ug/L
ND
20.0
9.7
06/21/22 15:18
Methylene Chloride
ug/L
ND
5.0
2.0
06/21/22 15:18
Styrene
ug/L
ND
1.0
0.29
06/21/22 15:18
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
IK,v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 28 of 36

aceAnalytical
www.pacolmbs.com
QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No. 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 3683660
Matrix: Water
Associated Lab Samples
92610715002, 92610715003, 92610715008
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Tetrachloroethene
ug/L
ND
1.0
0.29
06/21/22 15:18
Toluene
ug/L
ND
1.0
0.48
06/21/22 15:18
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/21/22 15:18
trans-1.3-Dichloropropene
ug/L
ND
1.0
0.36
06/21/22 15:18
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/21/22 15:18 v1
Trichloroethene
ug/L
ND
1.0
0.38
06/21/22 15:18
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/21/22 15:18
Vinyl acetate
ug/L
ND
2.0
1.3
06/21/22 15:18
Vinyl chloride
ug/L
ND
1.0
0.39
06/21/22 15:18
Xylene (Total)
ug/L
ND
1.0
0.34
06/21/22 15:18
1,2-Dichloroethane-d4 (S)
%
101
70-130
06/21/22 15:18
4-Bromofluorobenzene (S)
%
97
70-130
06/21/22 15:18
Toluene-d8 (S)
%
96
70-130
06/21/22 15:18
LABORATORY CONTROL SAMPLE: 3683661
Qualifiers
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
48.6
97
70-130
1,1,1-Trichloroethane
ug/L
50
47.7
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.0
94
70-130
1,1,2-Trichloroethane
ug/L
q0
45.0
90
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
50.4
101
70-130
1,1-Dichloroethane
ug/L
50
46.4
93
70-130
1,1-Dichloroethene
ug/L
50
49.7
99
70-132
1,2,3-Trichloropropane
ug/L
50
47.3
95
70-130
1,2,3-Trimethylbenzene
ug/L
50
49.5
99
70-130
1,2,4-Trimethylbenzene
ug/L
50
50.5
101
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53A
106
70-132
1,2-Dibromoethane (EDB)
ug/L
50
47.2
94
70-130
1,2-Dichlorobenzene
ug/L
50
47.6
95
70-130
1,2-Dichloroethane
ug/L
50
46.4
93
70-130
1,2-Dichloropropane
ug/L
50
48.9
98
70-130
1,3,5-Trimethylbenzene
ug/L
50
49.7
99
70-130
1,4-Dichlorobenzene
ug/L
50
48.9
98
70-130
2-Hexanone
ug/L
100
109
109
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.3
97
70-130
Acetone
ug/L
100
100
100
70-144
Acrylonitrile
ug/L
250
250
100
70-130
Benzene
ug/L
50
45.8
92
70-130
Bromochloromethane
ug/L
50
45.0
90
70-130
Bromodichloromethane
ug/L
50
49.4
99
70-130
Bromoform
ug/L
50
65.4
131
70-131 IK.v1
Bromomethane
ug/L
50
53.7
107
30-177
Carbon disulfide
ug/L
50
49.9
100
70-133
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services LLC Page 29 of 36

aceAnalytical
www.pacelabs.etxa
QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
LABORATORY CONTROL SAMPLE:
Parameter
3683661
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Carbon tetrachloride
ug/L
50
48.4
97
70-130
Chlorobenzene
ug/L
50
48.4
97
70-130
Chloroethane
ug/L
50
52.2
104
46-131
Chloroform
ug/L
50
47.2
94
70-130
Chloromethane
ug/L
50
48.0
96
49-130
cis- 1,2-Dichloroethene
ug/L
50
47.1
94
70-130
cis-1,3-Dichloropropene
ug/L
50
53.5
107
70-130
Dibromochloromethane
ug/L
50
53.4
107
70-130
Dibromomethane
ug/L
50
48.8
98
70-130
Ethylbenzene
ug/L
50
47.8
96
70-130
lodomethane
ug/L
100
107
107
47-140
Methylene Chloride
ug/L
50
47.4
95
68-130
Styrene
ug/L
50
50.5
101
70-130
Tetrachloroethene
ug/L
50
44.3
89
70-130
Toluene
ug/L
50
44.6
89
70-130
trans-1,2-Dichloroethene
ug/L
50
49.0
98
70-130
trans-1,3-Dichloropropene
ug/L
50
49.5
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
65.5
131
25-200 v1
Trichloroethene
ug/L
50
47.1
94
70-130
Trichlorofluoromethane
ug/L
50
47.7
95
61-130
Vinyl acetate
ug/L
100
104
104
70-140
Vinyl chloride
ug/L
50
47.2
94
59-142
Xylene (Total)
ug/L
150
145
97
70-130
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8(S)
%
97
70-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3683662
MS
92610715002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3683663
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.9
21.9
115
110
70-135
5
30
1,1,1-Trichloroethane
ug/L
ND
20
20
23.4
22.8
117
114
70-148
2
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
21.0
113
105
70-131
7
30
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
20.0
104
100
70-136
4
30
1,1,2-
ug/L
ND
20
20
25.9
24.4
130
122
70-154
6
30
Trich lorotriflu oroethane
1,1-Dichloroethane
ug/L
2.8
20
20
25.1
23.6
112
104
70-147
6
30
1,1-Dichloroethene
ug/L
ND
20
20
24.5
24.1
122
120
70-158
2
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.4
20.9
112
104
67-137
7
30
1,2,3-Trimethylbenzene
ug/L
ND
20
20
23.2
22.4
116
112
70-133
4
30
1,2,4-Trimethylbenzene
ug/L
ND
20
20
23.5
22.8
118
114
70-134
3
30
1,2-Dibromo-3-
ug/L
ND
20
20
23.8
21.5
119
108
69-136
10
30
chloropropane
1,2-Dibromoethane (EDB) ug/L ND 20 20 22.5 21.2 113 106 70-137 6 30
1,2-Dichlorobenzene ug/L ND 20 20 22.1 21.6 111 108 70-133 2 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 30 of 36

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QUALITY CONTROL DATA
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3683662
MS
92610715002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3683663
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,2-Dichloroethane
ug/L
ND
20
20
22.3
21.6
112
108
67-138
3
30
1,2-Dichloropropane
ug/L
ND
20
20
23.2
22.5
116
113
70-138
3
30
1,3,5-Trimethylbenzene
ug/L
ND
20
20
23.6
22.7
118
113
70-138
4
30
1,4-Dichlorobenzene
ug/L
1.0
20
20
23.1
23.4
111
112
70-133
1
30
2-Hexanone
ug/L
ND
40
40
53.2
47.6
133
119
67-139
11
30
4-Methyl-2-pentanone
ug/L
ND
40
40
45.9
43.6
115
109
67-136
5
30
(MIBK)
Acetone
ug/L
ND
40
40
48.7
44.5
122
111
55-159
9
30
Acrylonitrile
ug/L
ND
100
100
118
110
118
110
68-140
7
30
Benzene
ug/L
0.83J
20
20
23.1
222
111
107
67-150
4
30
Bromochloromethane
ug/L
ND
20
20
23.1
22.1
115
111
70-146
4
30
Bromodichloromethane
ug/L
ND
20
20
22.2
21.6
111
108
70-138
3
30
Bromoform
ug/L
ND
20
20
24.0
22.2
120
111
57-138
8
30 IK
Bromomethane
ug/L
ND
20
20
26.6
26.1
133
131
10-200
2
30 v3
Carbon disulfide
ug/L
ND
20
20
23.5
21.1
118
105
70-152
11
30
Carbon tetrachloride
ug/L
ND
20
20
23.9
23.1
120
115
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
23.7
22.5
117
111
70-137
5
30
Chloroethane
ug/L
ND
20
20
26.9
25.9
131
127
51-166
4
30 v3
Chloroform
ug/L
ND
20
20
20.9
20.5
104
103
70-144
2
30
Chloromethane
ug/L
ND
20
20
25.3
24.3
127
121
24-161
4
30 v3
cis-1,2-Dichloroethene
ug/L
4.2
20
20
26.8
26.8
113
113
67-148
0
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.7
22.9
119
114
70-142
4
30
Dibromochloromethane
ug/L
ND
20
20
22.8
21.5
114
107
68-138
6
30
Dibromomethane
ug/L
ND
20
20
23.2
21.7
116
109
70-134
7
30
Ethylbenzene
ug/L
ND
20
20
23.8
22.5
119
113
68-143
6
30
lodomethane
ug/L
ND
40
40
42.8
41.5
107
104
20-161
3
30
Methylene Chloride
ug/L
ND
20
20
20.5
19.3
103
97
64-148
6
30
Styrene
ug/L
ND
20
20
24.0
22.4
120
112
70-136
7
30
Tetrachloroethene
ug/L
ND
20
20
23.1
21.2
115
106
70-139
9
30
Toluene
ug/L
ND
20
20
21.5
21.0
108
105
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.1
23.6
121
118
70-149
2
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.8
22.0
114
110
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.6
19.8
113
99
31-145
13
30
Trichloroethene
ug/L
ND
20
20
23.5
23.0
118
115
70-149
2
30
Trichlorofluoromethane
ug/L
ND
20
20
23.3
22.9
116
115
61-154
2
30
Vinyl acetate
ug/L
ND
40
40
47.4
45.4
119
113
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
25.6
24.4
128
122
55-172
5
30 v3
Xylene (Total)
ug/L
ND
60
60
70.9
67.2
118
112
66-145
5
30
1,2-Dichloroethane-d4 (S)
%
98
101
70-130
4-Bromofluorobenzene (S)
%
99
98
70-130
Toluene-d8 (S)
%
98
100
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 31 of 36

aceAnalytical
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QUALIFIERS
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.. 92610715
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2022 09:29 AM without the written consent of Pace Analytical Services, LLC Page 32 of 36

acoAnaljftal
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: ALLEGHANY COUNTY LANDFILL
Pace Project No.: 92610715
Pace Analytical Services, LLC
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92610715001
0303T-MW1
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610715002
0303T-MW2
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5A
706039
92610715003
0303T-MW3
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610716004
0303T-MW4
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610716005
0303T-MW5
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610716006
0303T-ST1
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610715007
0303T-ST2
EPA 200.8 Rev 5.4
705841
EPA 200.8 Rev 5.4
706039
92610715001
0303T-MW1
EPA 245.1 Rev 3.0 1994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715002
0303T-MW2
EPA 245.1 Rev 3.0 1994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715003 •
0303T-MW3
EPA 245.1 Rev 3.0 1994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715004
0303T-MW4
EPA 245.1 Rev 3.0 t994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715006
0303T-MW5
EPA 245.1 Rev 3.0 1994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715006
0303T-ST1
EPA 245.1 Rev 3.0 1994
705892
EPA 245.1 Rev 3.0 1994
706139
92610715007
0303T-ST2
EPA 245.1 Rev 3.0 1994
705892
EPA 245 1 Rev 3.0 1994
706139
92610715001
0303T-MW1
EPA 8260D
706000
92610715002
0303T-MW2
EPA 8260D
706022
92610715003
0303T-MW3
EPA 8260D
706022
92610715004
0303T-MW4
EPA 8260D
706000
92610716005
0303T-MW5
EPA 8260D
706000
926107115006
0303T-ST1
EPA 8260D -
706000
92610715007
0303T-ST2
EPA 8260D
706000
92610715008 TRIP BLANK EPA 8260D 706022
Date: 06/24/2022 09:29 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC
Page 33 of 36

Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood[] Huntersville [I Raleigh❑ Mechanicsvillen Atlantaf-I Kornar«,111.1-1
Client Name: WN : 92.610715
Project fE;
❑Courier: Fed E. ❑UPS ❑LISPS ❑Client II I II' I I II I I (I I'lll �II
Commercial Eli a e []Other:
92610715
Custody Sea[ Present? QYes ONo Seals intact? []Yes ❑No
Packing Material; ❑Bubble Wrap .}Bubble Bags ❑None [2 Other
Thermometer: _
❑ IRGun to:
Date/Initials Person Examining Contents:_ /—�_
Biological Tissue ozen? " I ( Z Z
[]Yes []No ILINIA
----� Type of Ice: 0Wet ❑Blue []tone
Correction Factor:
Cooler Temp: ` Add/Subtract (°C) Tempshould be above freezing to 61C
Cooler Temp Corrected ('C): ) QSamples out of temp criteria. Samples on ice, cooling process
Regulated Soil has begun
USDA Re
g (Q N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA NY ciSC
Did sanples originate from a foreign source (internationally,
(check maps)? []Yes []No includng Hawaii and Puerto Rico)? []Yes I-INo
Chain of Custody Present?
6es
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes•
C]No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
Ore
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
D1Yes -1�
QYes
[]No
❑No
❑N/A
❑N/A
6.
Containers Intact?
[(Yes
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
&.
Sample Labels Match COC7
es
ENO
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix;
Headspace in VOA Vials (>5-6mm)? ❑Y u o ❑N/A 10.
Trip Blank Present? es QNo ❑N/A 11.
Trip Blank Custody Seals Present? EleY s ❑No ❑N/A
COMMENTS/SAMPLE D15CREP
Field Data Required? ❑Yes ❑No
'r-' '11' C• AA eoc��lr
J i1 1- r 19i1 T i Y fr'1
. unru:�rsY�nur ��
Lot ID of splittontainers:
-- - F —
Person contartari- DateMme
Project Manager SCURF Review:
ProjgC;;�anagetSRERetiiew: _—_`..--- -_--
Qualtrax ID. 69614
Date:
n»tom•
Page 1 of 2 Page 34 of 36

Effective Date: 05/121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and Project WO� ; 92;61 �715
within the acceptance range for preservation samples.
Exceptions: VOAsoliform, TDC,DILand_Grease, DRO/8015 (water} DOC, Mfg PM: BY Due Date: 06/24/22
"Bottom half of box is to list number of bottles CLIENT: 92—ARM WATER
***Check all unpreserved Nitrates for chlorine
#
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PH Adjustment Log for Preserved Samples
sample 1D Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative tot ff
adjusted added
+ ••-+ .+ ++u �N.u.�r dut�Uuy +.ui ii+ �Jit)ittil .U111j�i+ul,0.'"VIel, .1 u,pi sent to the North Carolina UNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2
Page 35 of 36

O
A
r 1
; m
TEMP in C
Received on
Ice
(YIN)
us y
Sealed
Cooler
Y/N
Samples
Intact
(YIN)
i
a
I- I- 1--,!- 1- 1- IA fw 1- 1 ITEM #
O 3 (�
a 0 D
S ..- O
N a
V W Son ••�
rr.om
W n�.
xINS
a
1
MATRIX CODE (see valid codes to left)
SAMPLE TYPE (G=GRAB C=C01.1P)
O
.D1
m �
D
A 0
m 0
r
In
D In
m
z
o
M
m
SAMPLE TEMP AT COLLECTION
# OF CONTAR.ERS
Unpreserved
HZSO4
HNO3
m
HCI In
m
NaOH m
Na2S203 m
Methanol
Other
Analyses Test YIN
App I VOC
App I Metals
Trip BI AP,r
Residual Chorine (YIN)
w
a mm a
� N �
O a
O 8, � N � .TDI 7
m N n A� OCb
r.6J
P 8 w N
3 S
� N �
c c
3
n o
n rp
�i
3
m
d
c
�v nM;arnEi
u W o G 7
m
° Q. m
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n
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x ,
N C
c m
� S �
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c o
r
m
n 3
0
m
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m I
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(A I
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m 3 ? 9 - C
3 e 03 w to in
2,.PPPg m ? �nm��
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Gv
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m p
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RL0D
C pl
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Im � Z
c y
a n �
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m `w (D
i = c
3 ra
g a to
N pp
v
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Page 36 of 36

APPENDIX B

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1 As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Facility Name:
Alleghany County Landfill Permit Number: 0302-MSWLF-1981
Sampling Date: 03/31 /22 NC Landfill Rule (.0500 or.1600): .0500
Sample Collector Name & Position: Joe Zuncich, Project Manager
Gas Meter Type & Serial Number: Gas Tracer 246030184RN Gas Meter Calibration Date: 1/28/2022
Field Calibration Date &Time: 3-31-2022/ 1537
Field Calibration Gas Type (1515 or35150): 35/50 Field Calibration Gas Canister Expiration Date: 5/19/2024
Gas Meter Pump Rate:
0.5 LPM
Ambient Air Temperature: 62 Barometric Pressure (in. or mm Hg): 29.51 Weather Conditions: Overcast, light rain
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CH4 (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (H2S) gas monitoring may be required for Construction & Demolition Landfills (CDLFs). See individual
permit conditions and/or Facility LFG monitoring plan.
Location or
LFG Well ID
S ample
Tube
Purge
Time of
Day
Time
Pumped
(sec)
Initial
�o LEL
Stabilized
%LEL
% CH4
(volume)
% 02
(volume)
% CO2
(volume)
% H2S*
(volume)
NOTES
0303T-MW1
Yes
1707
120
0
0
0
20.9
-
NA
10 ppm stabilized
0303T-MW2
Yes
1646
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW2
Yes
1542
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW4
Yes
1717
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW5
Yes
1658
120
0
0
0
20.9
-
NA
0 ppm stabilized
Recycle center
Yes
1602
120
0
0
0
20.9
-
NA
0 ppm stabilized
Tipping scale
Yes
1608
120
0
0
0
20.9
-
NA
0 ppm stabilized
Scale House
Yes
1556
120
0
0
0
20.9
-
NA
0 ppm stabilized
Methane well
Yes
1621
120
0 - 3%
0 - 3%
0.038%
20.6
-
NA
30 - 380 ppm stabilized
NOTE: 1f needed, attach additional data forms to include additional LFG monitoring data locations for the facility
ACTION LEN ELS: Methane: _1.25% by volume (inside structures) AND _>5% by volume (at facility boundary)
Hydrogen Sulfide: >1% by volume (inside structures) AND =4% by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. 1 am aware that there are significant penalties for making any false statement, representation,
or certification including the possibility of a fine and imprisonment.
Joseph L. Zuncich
SIGNATURE
Project Manager
TITLE
Revised - February 4, 2020

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by arty person upon request (NC General Statute 132-6).
Facili Name: Alleghany County Landfill Permit Number: 0302-MSWLF-1981
h'
6/16/22
Sampling Date: NC Landfill Rule (.0500 or.1600):
Sample Collector Name & Position: Joe Zuncich, Project Manager
.0500
Gas Meter Type & Serial Number: Gas Tracer 246030184RN Gas Meter Calibration Date: 1/28/2022
Field Calibration Date &Time: 6-16-2022/ 1059
Field Calibration Gas Type (15 15 or 35 'S0): 35/50 Field Calibration Gas Canister Expiration Date: 5/19/2024
Gas Meter Pump Rate:
0.5 LPM
Ambient Air Temperature: 85 Barometric Pressure (in. or min Hg): 30.07 Weather Conditions: Mostly sunny
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CHI (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (112S) gas monitoring may be required for Construction & Demolition Landfills (CDLFs), See individual
permit conditions and or Facility LFG monitoring plan
Location or
LFG Well ID
Sample
Tube
Purge
Time of
Day
Time
Pumped
(sec)
Initial
% LEL
Stabilized
% LEL
°o CH4
(volume)
00 02
(volume)
°o CO2
(volume)
°o H2S*
(volume)
NOTES
0303T-MW1
Yes
1402
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW2
Yes
1121
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-M
Yes
1609
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW4
Yes
1522
120
0
0
0
20.9
-
NA
0 ppm stabilized
0303T-MW5
Yes
1308
120
0
0
0
20.9
-
NA
0 ppm stabilized
Recycle cent
ir Yes
1653
120
0
0
0
20.9
-
NA
-30. Oppm stabilized
Tipping scale
Yes
1704
120
0
0
0
20.9
-
NA
0 ppm stabilized
Scale House
Yes
1106
120
0
0
0
20.9
-
NA
0 ppm stabilized
Methane well
Yes
1710
120
0 -10%
0 - 10%
0.102%
20.2
-
NA
40 - 1.020 ppm stabilized
NOTE: 1f needed, attach additional data forms to include additional LFG monitoring data locations for the facdtty
ACTION LEVELS: Methane: >1.25% by volume (inside structures) AND >5% by volume (at facility boundary)
Hydrogen Sulfide: >1% by volume (inside structures) AND >4% by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. I am aware that there are significant penalties for making any false statement, representation,
or certification including the possibility of a fine and imprisonment.
2 Project Manager
SIGNATU TITLE
Revised — February 4, 2020

APPENDIX C

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C C C C— — C—— C C — C C C C—— C C —— C — C C C C C— C— C— C C
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