6002_Mecklenburg_HolbrooksRoad_MSWLF_Sept2022GW_FID1740117_20221011

[�7ENR USE ONLY []Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
' 'NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Holbrooks Road Landfill 15401 Holbrooks Road 60-02 .0500 September 14-15, 2022
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells El
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. Project Manager
Facility Pe�prc entativelbme (Print) Title
10/11 /2022
Signature — �� Date
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
980-314-3855
(Area Code) Telephone Number
Affix NC Licensed/ PGQfessional Geologist Seal
Revised 6/2009

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MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
October 11, 2022
Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Holbrooks Road Landfill Permit 60-02
Semi-annual WQ Monitoring
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Holbrooks Road Landfill September 14-15, 2022 in accordance with the approved sample
and analysis plan dated March 27, 2003. This report details the results of that monitoring
event. Laboratory analytical data, field -measured data table of values exceeding 2L
standards is contained on the electronic data deliverable submittal.
Samples were collected from fifteen (15) monitoring wells (HRW-7, HRW-8, HRW-9R,
HRW-10, HRW-11 R, HRW-12, HRW-13, HRW-14, HRW-15, HRW-16, HRW-17,
HRW- 18. HRW-19, HRW-20 and HRW-21) and three (3) surface -water sampling
locations (HRSW-2, HRSW-3 and HRSW-4). Samples were analyzed for metals and
volatile organic compounds ("VOCs") listed in Appendix I of 40 CFR Part
258.54 "Detection monitoring program". Samples were also analyzed for 1,4-Dioxane as
required as of July 1, 2018. Field measurements of temperature, pH, and specific
conductivity were made at each sampling location using a calibrated instrument.
Additionally, measurements of dissolved oxygen were made at each surface -water
sampling location.
The electronic data deliverable package containing the monitoring data is labeled to
reflect the units used for reporting. Surface water standards listed are the water quality
standards established for freshwater classification for aquatic life as outlined in 15A
NCAC 213 "Classification and Water Quality Standards Applicable to Surface Waters of
North Carolina". Groundwater standards listed are the standards outlined in 15A NCAC
2L "Classification of Water Quality Standards applicable to the Groundwaters of North
Carolina". If the sample is reported in parts per billion, then the standard is also reported
in parts per billion.
PEOPLE -PRIDE - PROGRESS - PARTNERSHIP
2145 Suttle Ave - Charlotte, North Carolina 28208 - [phone] Fax [phone]
www.wipeoutwaste.com

Page 2
Surface -water samples:
Barium was detected in all 3 stream sampling locations. The following table summarizes
the metals detections for the surface water sampling locations.
Sample Location
Barium ug/1
HRSW-2 upstream
45.6
HRSW-4 mid -stream
43.3
HRSW-3 downstream
45.4
No VOCs were detected in any of the samples collected from the three surface -water
sampling locations (HRSW-2, HRSW-4 and HRSW-3). All field -measured parameters
were within the established regulatory limits. The following table summarizes field -
measured parameters for surface water samples.
Sample Location
Temp.
°C
pH
S.U.
Specific Conductivity
ms/cm
Dissolved Oxygen
mg/l
HRSW-2 upstream
17.9
7.0
0.245
8.08
HRSW-4 mid -stream
17.8
7.1
0.231
8.27
HRSW-3 downstream
17.3
6.9
0.257
8.20
Groundwater samples:
Vanadium, cobalt, lead, chromium and nickel were detected in various wells above the 21
standard. The following table summarizes metals detection for groundwater samples.
Well ID
As
ug/l
Ba
ug/l
Be
ug/l
Cd
ug/l
Cr
ug/1
Co
ug/l
Cu
ug/1
Pb
ug/1
Ni
ug/1
Se
ug/l
Vn
ug/1
Zn
ug/1
HRW-7
-----
101
-----
-----
-----
-----
-----
-----
-----
-----
-----
31.1
HRW-8
-----
127
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-9R
-----
461
-----
-----
-----
-----
31.3
24.5
-----
-----
23.4
-----
HRW-10
-----
164
-----
14.7
-----
-----
-----
-----
-----
HRW-11R
-----
419
-----
40.7
----
-----
129
-----
-----
-----
HRW-12
-----
866
-----
-----
-----
58.4
86.3
-----
177
-----
-----
-----
HRW-13
------
104
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-14
----
37.6
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-15
-----
153
-----
-----
12.0
-----
101
28.7
-----
-----
72.9
45.0
HRW-16
-----
101
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-17
-----
50.6
----
------
------
-----
-----
-----
-----
-----
-----
-----
HRW-18
-----
315
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-19
-----
93.3
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-20
-----
121
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-21
-----
63.5
-----
-----
-----
-----
-----
----
-----
-----
-----
-----
2L Std.
10
700
4
2
10
1
1,000
15
100
20
0.3
1,000
Note: Results shown in bold exceed the 2L standard.

Page 3
VOCs were detected in eight monitoring wells; HRW-7, HRW-9R, HRW-10, HRW-11R,
HRW-12, HRW-16, HRW-18 and HRW-20. The following table summarizes VOC
detections.
Well ID
Volatile Constituent
Concentration
2L Standard
u /1)
u /1
HRW-7
Cis-1,2-Dichloroethene
1.3
70
HRW-9R
Chlorobenzene
2.9
50
Chloroethane
1.4
3 000
1,2-Dichlorobenzene
5.8
20
1,4-Dichlorobenzene
8.0
6
1,1-Dichloroethane
28.6
6
1,2-Dichloroethane
2.1
0.4
cis-1,2-Dichloroethane
68.6
70
trans-1,2-Dichloroethene
1.0
100
1,2-Dichloropropane
2.7
0.6
Vinyl Chloride
6.6
0.03
1,4-Dioxane
10.6
3
HRW-10
Chloroethane
1.1
3000
1,4-Dioxane
5.9
3
HRW-11R
Chlorobenzene
14.4
50
Chloroethane
1.1
3000
1,4-Dichlorobenzene
3.1
6
1,4-Dioxane
182
3
HRW-12
Chlorobenzene
8.3
50
Chloroethane
1.6
3000
1,4-Dichlorobenzene
2.6
6
1,1-Dichloroethane
7.1
6
1,4-Dioxane
133
3
HRW-16
1,4-Dioxane
2.5
3
Benzene
1.9
1
HRW-18
Chlorobenzene
7.3
50
Chloroethane
3.4
3000
1,1-Dichloroethane
26.4
6
cis-1,2-Dichloroethane
1.6
70
1,2-Dichloropropane
3.1
0.6
1,4-Dichlorobenzene
7.0
6
1,4-Dioxane
15.7
3
Vinyl Chloride
9.3
0.03
HRW-20
Chloroethane
1.0
3000
1,1-Dichloroethane
9.3
6
cis-1,2-Dichloroethane
1.2
70
Note: Results shown in bold exceed the 2L standard.

Page 4
Measurements of pH were more acidic than the 21, standard range of 6.5 to 8.5 standard
units at all monitoring wells. Field- measured parameters for groundwater samples are
summarized in the following table.
Sample Location
Temp. °C
PH
Specific Conductivity ms/cm
HRW-7
19.3
5.9
0.2758
HRW-8
16.1
6.4
0.502
HRW-9R
14.9
6.3
1.228
HRW-10
17.7
6.2
0.816
HRW-11 R
17.2
6.2
2.500
HRW-12
15.8
6.3
2.248
HRW-13
17.2
5.6
0.357
HRW-14
16.0
6.1
0.241
HRW-15
15.7
6.0
0.263
HRW-16
17.8
5.3
0.120
HRW-17
16.0
6.4
0.212
HRW-18
17.4
6.3
1.467
HRW-19
16.5
6.2
0.367
HRW-20
15.9
5.9
0.409
HRW-21
16.6
6.2
0.501
Note: Results shown in bold are outside of the 2L standard range of 6.5 - 8.5 S.U.
Please call me at [phone] if you have any questions regarding this report.
O0000 Sincerely,
r Amber R. Grzymski, P.G. �._.
Project Manager
Solid Waste Services

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-••—••- STREAM LOCATION (SEE REFERENCE 1)
APPROXIMATE POTENTIOMETRIC SURFACE CONTOUR (SPRING 2014)
GROUNDWATER DIVIDE
® MONITORING WELL (SEE REFERENCE 1)
DIRECTION OF GROUNDWATER FLOW
REFERENCES
1. PROPERTY LINES, MONITORING WELLS, STREAM AND WATER BODY
LOCATIONS, AND STRUCTURE LOCATIONS FROM MECKLENBURG
COUNTY GIS DEPARTMENT. EXISTING TOPOGRAPHY FROM NCDOT
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 27, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625613
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92625613001
6002-HRW7
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625613002
6002-HRW18
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625613003
6002-HRW19
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625613004
6002-HRW20
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625613005
6002-HRW21
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625613006
TRIP BLANK
EPA 8260D
GAW
52
PASI-C
PASI-C = Pace Analytical
Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW7 Lab ID: 92625613001 Collected: 09/14/22 10:35 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 18:25
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:25
7440-41-7
Barium
101
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:25
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:25
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:25
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:25
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:25
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:25
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:25
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 18:25
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:25
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 18:25
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:25
7440-62-2
Zinc
31.1
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:25
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:25
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/22/22 18:15
09/25/22 01:28
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 11:51
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 11:51
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 11:51
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 11:51
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 11:51
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 11:51
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 11:51
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 11:51
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 11:51
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 11:51
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 11:51
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 11:51
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 11:51
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 11:51
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 11:51
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 11:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 11:51
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 11:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:51
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:51
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 11:51
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:51
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:51
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW7 Lab ID: 92625613001 Collected: 09/14/22 10:35 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:51
75-35-4
cis-1,2-Dichloroethene
1.3
ug/L
1.0
1
09/15/22 11:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:51
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:51
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:51
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 11:51
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 11:51
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 11:51
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 11:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 11:51
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 11:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:51
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 11:51
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 11:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:51
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 11:51
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 11:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 11:51
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 11:51
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 11:51
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 11:51
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 11:51
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 11:51
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
09/15/22 11:51
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
09/15/22 11:51
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
09/15/22 11:51
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/14/22 17:16
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
09/14/22 17:16
17060-07-0
Toluene-d8 (S)
92
%
70-130
1
09/14/22 17:16
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW18 Lab ID: 92625613002 Collected: 09/14/22 10:30 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 18:44
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:44
7440-41-7
Barium
315
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:44
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:44
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:44
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:44
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:44
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:44
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:44
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 18:44
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:44
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 18:44
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:44
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:44
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:44
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/22/22 18:15
09/25/22 01:34
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 14:56
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 14:56
107-13-1
Benzene
1.9
ug/L
1.0
1
09/15/22 14:56
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 14:56
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 14:56
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 14:56
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 14:56
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 14:56
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 14:56
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 14:56
56-23-5
Chlorobenzene
7.3
ug/L
1.0
1
09/15/22 14:56
108-90-7
Chloroethane
3.4
ug/L
1.0
1
09/15/22 14:56
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 14:56
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 14:56
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 14:56
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 14:56
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 14:56
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 14:56
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 14:56
95-50-1
1,4-Dichlorobenzene
7.0
ug/L
1.0
1
09/15/22 14:56
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 14:56
110-57-6
1,1-Dichloroethane
26.4
ug/L
1.0
1
09/15/22 14:56
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 14:56
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW18 Lab ID: 92625613002 Collected: 09/14/22 10:30 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 14:56
75-35-4
cis-1,2-Dichloroethene
1.6
ug/L
1.0
1
09/15/22 14:56
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 14:56
156-60-5
1,2-Dichloropropene
3.1
ug/L
1.0
1
09/15/22 14:56
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 14:56
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 14:56
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 14:56
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 14:56
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 14:56
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 14:56
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 14:56
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 14:56
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 14:56
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 14:56
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 14:56
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 14:56
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 14:56
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 14:56
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 14:56
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 14:56
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 14:56
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 14:56
108-05-4
Vinyl chloride
9.3
ug/L
1.0
1
09/15/22 14:56
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 14:56
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 14:56
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 14:56
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
09/15/22 14:56
460-00-4
1,2-Dichloroethane-d4 (S)
119
%
70-130
1
09/15/22 14:56
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 14:56
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
15.7
ug/L
2.0
1
09/14/22 17:35
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
09/14/22 17:35
17060-07-0
Toluene-d8 (S)
93
%
70-130
1
09/14/22 17:35
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW19 Lab ID: 92625613003 Collected: 09/14/22 09:25 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 18:49
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:49
7440-41-7
Barium
93.3
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:49
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:49
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:49
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:49
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:49
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:49
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:49
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 18:49
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:49
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 18:49
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:49
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:49
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:49
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2217:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 15:14
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 15:14
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 15:14
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 15:14
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 15:14
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 15:14
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 15:14
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 15:14
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 15:14
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 15:14
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 15:14
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 15:14
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 15:14
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 15:14
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 15:14
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 15:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 15:14
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 15:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:14
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:14
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 15:14
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 15:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 15:14
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW19 Lab ID: 92625613003 Collected: 09/14/22 09:25 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 15:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 15:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 15:14
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 15:14
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 15:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 15:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 15:14
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 15:14
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 15:14
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 15:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 15:14
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 15:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 15:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 15:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 15:14
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 15:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 15:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 15:14
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 15:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 15:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 15:14
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 15:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 15:14
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 15:14
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 15:14
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 15:14
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
09/15/22 15:14
460-00-4
1,2-Dichloroethane-d4 (S)
117
%
70-130
1
09/15/22 15:14
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/15/22 15:14
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/14/22 17:54
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
09/14/22 17:54
17060-07-0
Toluene-d8 (S)
93
%
70-130
1
09/14/22 17:54
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW20 Lab ID: 92625613004 Collected: 09/14/22 09:50 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 18:54
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:54
7440-41-7
Barium
121
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:54
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:54
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:54
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:54
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:54
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:54
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:54
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 18:54
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:54
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 18:54
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:54
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:54
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:54
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:16
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 15:33
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 15:33
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 15:33
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 15:33
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 15:33
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 15:33
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 15:33
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 15:33
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 15:33
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 15:33
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 15:33
108-90-7
Chloroethane
1.0
ug/L
1.0
1
09/15/22 15:33
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 15:33
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 15:33
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 15:33
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 15:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 15:33
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 15:33
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:33
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:33
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 15:33
110-57-6
1,1-Dichloroethane
9.3
ug/L
1.0
1
09/15/22 15:33
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 15:33
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW20 Lab ID: 92625613004 Collected: 09/14/22 09:50 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/27/2022 02:09 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99
%
115
%
103
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
93 %
93 %
1.0
1
09/15/22 15:33
75-35-4
1.0
1
09/15/22 15:33
156-59-2
1.0
1
09/15/22 15:33
156-60-5
1.0
1
09/15/22 15:33
78-87-5
1.0
1
09/15/22 15:33
10061-01-5
1.0
1
09/15/22 15:33
10061-02-6
1.0
1
09/15/22 15:33
100-41-4
5.0
1
09/15/22 15:33
591-78-6
20.0
1
09/15/22 15:33
74-88-4
5.0
1
09/15/22 15:33
75-09-2
5.0
1
09/15/22 15:33
108-10-1
1.0
1
09/15/22 15:33
100-42-5
1.0
1
09/15/22 15:33
630-20-6
1.0
1
09/15/22 15:33
79-34-5
1.0
1
09/15/22 15:33
127-18-4
1.0
1
09/15/22 15:33
108-88-3
1.0
1
09/15/22 15:33
71-55-6
1.0
1
09/15/22 15:33
79-00-5
1.0
1
09/15/22 15:33
79-01-6
1.0
1
09/15/22 15:33
75-69-4
1.0
1
09/15/22 15:33
96-18-4
2.0
1
09/15/22 15:33
108-05-4
1.0
1
09/15/22 15:33
75-01-4
1.0
1
09/15/22 15:33
1330-20-7
2.0
1
09/15/22 15:33
179601-23-1
1.0
1
09/15/22 15:33
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/15/22 15:33 460-00-4
09/15/22 15:33 17060-07-0
09/15/22 15:33 2037-26-5
09/14/22 18:13 17060-07-0
09/14/2218:13 2037-26-5
Page 11 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW21 Lab ID: 92625613005 Collected: 09/14/22 08:55 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 18:58
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:58
7440-41-7
Barium
63.5
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:58
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:58
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:58
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:58
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:58
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 18:58
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:58
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 18:58
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:58
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 18:58
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:58
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 18:58
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 18:58
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:22
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 15:51
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 15:51
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 15:51
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 15:51
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 15:51
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 15:51
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 15:51
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 15:51
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 15:51
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 15:51
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 15:51
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 15:51
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 15:51
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 15:51
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 15:51
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 15:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 15:51
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 15:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:51
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 15:51
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 15:51
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 15:51
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 15:51
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: 6002-HRW21 Lab ID: 92625613005 Collected: 09/14/22 08:55 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/27/2022 02:09 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
116
%
103
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
95 %
93 %
1.0
1
09/15/22 15:51
75-35-4
1.0
1
09/15/22 15:51
156-59-2
1.0
1
09/15/22 15:51
156-60-5
1.0
1
09/15/22 15:51
78-87-5
1.0
1
09/15/22 15:51
10061-01-5
1.0
1
09/15/22 15:51
10061-02-6
1.0
1
09/15/22 15:51
100-41-4
5.0
1
09/15/22 15:51
591-78-6
20.0
1
09/15/22 15:51
74-88-4
5.0
1
09/15/22 15:51
75-09-2
5.0
1
09/15/22 15:51
108-10-1
1.0
1
09/15/22 15:51
100-42-5
1.0
1
09/15/22 15:51
630-20-6
1.0
1
09/15/22 15:51
79-34-5
1.0
1
09/15/22 15:51
127-18-4
1.0
1
09/15/22 15:51
108-88-3
1.0
1
09/15/22 15:51
71-55-6
1.0
1
09/15/22 15:51
79-00-5
1.0
1
09/15/22 15:51
79-01-6
1.0
1
09/15/22 15:51
75-69-4
1.0
1
09/15/22 15:51
96-18-4
2.0
1
09/15/22 15:51
108-05-4
1.0
1
09/15/22 15:51
75-01-4
1.0
1
09/15/22 15:51
1330-20-7
2.0
1
09/15/22 15:51
179601-23-1
1.0
1
09/15/22 15:51
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/15/22 15:51 460-00-4
09/15/22 15:51 17060-07-0
09/15/22 15:51 2037-26-5
1e11-71C!f JIAE 3EWMf aS4Qi
09/14/22 18:32 17060-07-0
09/14/2218:32 2037-26-5
Page 13 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: TRIP BLANK Lab ID: 92625613006 Collected: 09/14/22 08:31 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 11:14
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 11:14
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 11:14
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 11:14
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 11:14
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 11:14
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 11:14
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 11:14
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 11:14
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 11:14
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 11:14
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 11:14
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 11:14
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 11:14
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 11:14
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 11:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 11:14
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 11:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:14
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:14
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 11:14
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:14
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:14
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:14
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 11:14
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 11:14
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 11:14
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 11:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 11:14
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 11:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 11:14
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 11:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:14
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 11:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 11:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 11:14
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 11:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 11:14
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 30

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[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
Sample: TRIP BLANK
Parameters
Lab ID: 92625613006 Collected: 09/14/22 08:31
Results Units Report Limit DF
Received: 09/14/22 13:05 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/15/22 11:14
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/15/22 11:14
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/15/22 11:14
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
09/15/22 11:14
460-00-4
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
09/15/22 11:14
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
09/15/22 11:14
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
QC Batch: 725626 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005
METHOD BLANK: 3780263 Matrix: Water
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
50.0
09/26/2218:15
Arsenic
ug/L
ND
30.0
09/26/2218:15
Barium
ug/L
ND
10.0
09/26/2218:15
Beryllium
ug/L
ND
10.0
09/26/2218:15
Cadmium
ug/L
ND
10.0
09/26/2218:15
Chromium
ug/L
ND
10.0
09/26/2218:15
Cobalt
ug/L
ND
40.0
09/26/2218:15
Copper
ug/L
ND
20.0
09/26/2218:15
Lead
ug/L
ND
20.0
09/26/2218:15
Nickel
ug/L
ND
20.0
09/26/2218:15
Selenium
ug/L
ND
40.0
09/26/2218:15
Silver
ug/L
ND
10.0
09/26/2218:15
Thallium
ug/L
ND
200
09/26/2218:15
Vanadium
ug/L
ND
20.0
09/26/2218:15
Zinc
ug/L
ND
20.0
09/26/2218:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3780264
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
960
96
80-120
Arsenic
ug/L
1000
983
98
80-120
Barium
ug/L
1000
985
98
80-120
Beryllium
ug/L
1000
1010
101
80-120
Cadmium
ug/L
1000
996
100
80-120
Chromium
ug/L
1000
1020
102
80-120
Cobalt
ug/L
1000
991
99
80-120
Copper
ug/L
1000
1010
101
80-120
Lead
ug/L
1000
988
99
80-120
Nickel
ug/L
1000
976
98
80-120
Selenium
ug/L
1000
996
100
80-120
Silver
ug/L
1000
986
99
80-120
Thallium
ug/L
1000
950
95
80-120
Vanadium
ug/L
1000
1070
107
80-120
Zinc
ug/L
1000
994
99
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625613
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3780265
3780266
MS
MSD
92625613001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Arsenic
ug/L
ND
1000
1000
1050
1040
105
104
75-125
1
Barium
ug/L
101
1000
1000
1150
1150
105
105
75-125
0
Beryllium
ug/L
ND
1000
1000
1060
1060
106
106
75-125
1
Cadmium
ug/L
ND
1000
1000
1060
1070
106
107
75-125
1
Chromium
ug/L
ND
1000
1000
1060
1060
105
105
75-125
0
Cobalt
ug/L
ND
1000
1000
1030
1030
103
103
75-125
1
Copper
ug/L
ND
1000
1000
1080
1080
107
107
75-125
0
Lead
ug/L
ND
1000
1000
1030
1040
103
103
75-125
0
Nickel
ug/L
ND
1000
1000
1020
1010
102
101
75-125
1
Selenium
ug/L
ND
1000
1000
1040
1040
104
103
75-125
1
Silver
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Thallium
ug/L
ND
1000
1000
996
989
99
99
75-125
1
Vanadium
ug/L
ND
1000
1000
1130
1130
112
112
75-125
0
Zinc
ug/L
31.1
1000
1000
1070
1070
104
104
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
QC Batch: 725173 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92625613001, 92625613002
METHOD BLANK: 3778107
Matrix:
Water
Associated Lab Samples: 92625613001, 92625613002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
09/24/22 23:52
LABORATORY CONTROL SAMPLE:
3778108
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
93.5
93 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3778109 3778110
MS MSD
92625280001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 93.0 93.4 93 93 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
QC Batch: 725298 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92625613003, 92625613004, 92625613005
METHOD BLANK: 3778817
Matrix:
Water
Associated Lab Samples: 92625613003, 92625613004, 92625613005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
09/26/2217:40
LABORATORY CONTROL SAMPLE:
3778818
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
99.9
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3778819 3778820
MS MSD
92625613003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 101 102 100 102 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
QC Batch: 723470 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005, 92625613006
METHOD BLANK: 3769532 Matrix: Water
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005, 92625613006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,1-Trichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,2-Trichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1-Dichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
1,2,3-Trichloropropane
ug/L
ND
1.0
09/15/22 09:05
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
09/15/22 09:05
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichlorobenzene
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloropropane
ug/L
ND
1.0
09/15/22 09:05
1,4-Dichlorobenzene
ug/L
ND
1.0
09/15/22 09:05
2-Butanone (MEK)
ug/L
ND
5.0
09/15/22 09:05
2-Hexanone
ug/L
ND
5.0
09/15/22 09:05
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/15/22 09:05
Acetone
ug/L
ND
25.0
09/15/22 09:05
Acrylonitrile
ug/L
ND
10.0
09/15/22 09:05
Benzene
ug/L
ND
1.0
09/15/22 09:05
Bromochloromethane
ug/L
ND
1.0
09/15/22 09:05
Bromodichloromethane
ug/L
ND
1.0
09/15/22 09:05
Bromoform
ug/L
ND
1.0
09/15/22 09:05
Bromomethane
ug/L
ND
2.0
09/15/22 09:05
Carbon disulfide
ug/L
ND
2.0
09/15/22 09:05
Carbon tetrachloride
ug/L
ND
1.0
09/15/22 09:05
Chlorobenzene
ug/L
ND
1.0
09/15/22 09:05
Chloroethane
ug/L
ND
1.0
09/15/22 09:05
Chloroform
ug/L
ND
1.0
09/15/22 09:05
Chloromethane
ug/L
ND
1.0
09/15/22 09:05
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/15/22 09:05
Dibromochloromethane
ug/L
ND
1.0
09/15/22 09:05
Dibromomethane
ug/L
ND
1.0
09/15/22 09:05
Ethylbenzene
ug/L
ND
1.0
09/15/22 09:05
lodomethane
ug/L
ND
20.0
09/15/22 09:05
m&p-Xylene
ug/L
ND
2.0
09/15/22 09:05
Methylene Chloride
ug/L
ND
5.0
09/15/22 09:05
o-Xylene
ug/L
ND
1.0
09/15/22 09:05
Styrene
ug/L
ND
1.0
09/15/22 09:05
Tetrachloroethene
ug/L
ND
1.0
09/15/22 09:05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
METHOD BLANK: 3769532 Matrix: Water
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005, 92625613006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/15/22 09:05
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/15/22 09:05
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/15/22 09:05
Trichloroethene
ug/L
ND
1.0
09/15/22 09:05
Trichlorofluoromethane
ug/L
ND
1.0
09/15/22 09:05
Vinyl acetate
ug/L
ND
2.0
09/15/22 09:05
Vinyl chloride
ug/L
ND
1.0
09/15/22 09:05
Xylene (Total)
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloroethane-d4 (S)
%
109
70-130
09/15/22 09:05
4-Bromofluorobenzene (S)
%
98
70-130
09/15/22 09:05
Toluene-d8 (S)
%
101
70-130
09/15/22 09:05
LABORATORY CONTROL SAMPLE:
Parameter
3769533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.0
98
70-130
1,1,1-Trichloroethane
ug/L
50
44.5
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.5
101
70-130
1,1,2-Trichloroethane
ug/L
50
47.0
94
70-130
1,1-Dichloroethane
ug/L
50
44.5
89
70-130
1,1-Dichloroethene
ug/L
50
45.3
91
70-130
1,2,3-Trichloropropane
ug/L
50
49.3
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.2
100
70-131
1,2-Dibromoethane (EDB)
ug/L
50
48.3
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.3
101
70-130
1,2-Dichloroethane
ug/L
50
45.6
91
70-130
1,2-Dichloropropane
ug/L
50
45.9
92
70-130
1,4-Dichlorobenzene
ug/L
50
49.7
99
70-130
2-Butanone (MEK)
ug/L
100
84.9
85
70-134
2-Hexanone
ug/L
100
98.0
98
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.8
94
70-130
Acetone
ug/L
100
90.6
91
70-133
Acrylonitrile
ug/L
250
231
92
70-130
Benzene
ug/L
50
44.1
88
70-130
Bromochloromethane
ug/L
50
47.1
94
70-130
Bromodichloromethane
ug/L
50
46.8
94
70-130
Bromoform
ug/L
50
47.7
95
70-130
Bromomethane
ug/L
50
45.2
90
45-151
Carbon disulfide
ug/L
50
47.0
94
70-130
Carbon tetrachloride
ug/L
50
44.8
90
70-130
Chlorobenzene
ug/L
50
49.0
98
70-130
Chloroethane
ug/L
50
57.7
115
39-152
Chloroform
ug/L
50
45.2
90
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 30

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
LABORATORY CONTROL SAMPLE:
Parameter
3769533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
50
48.2
96
58-130
cis-1,2-Dichloroethene
ug/L
50
45.2
90
70-130
cis-1,3-Dichloropropene
ug/L
50
49.8
100
70-130
Dibromochloromethane
ug/L
50
46.5
93
70-130
Dibromomethane
ug/L
50
46.3
93
70-130
Ethylbenzene
ug/L
50
49.0
98
70-130
lodomethane
ug/L
100
97.8
98
53-141
m&p-Xylene
ug/L
100
100
100
70-130
Methylene Chloride
ug/L
50
41.6
83
66-130
o-Xylene
ug/L
50
50.2
100
70-130
Styrene
ug/L
50
51.7
103
70-130
Tetrachloroethene
ug/L
50
44.7
89
70-130
Toluene
ug/L
50
46.8
94
70-130
trans-1,2-Dichloroethene
ug/L
50
45.0
90
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.1
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
51.8
104
57-185
Trichloroethene
ug/L
50
47.5
95
70-130
Trichlorofluoromethane
ug/L
50
43.3
87
62-130
Vinyl acetate
ug/L
100
90.1
90
70-144
Vinyl chloride
ug/L
50
50.2
100
62-130
Xylene (Total)
ug/L
150
150
100
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
3769534
Units
92625613001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.9
109
70-141
1,1,1-Trichloroethane
ug/L
ND
20
23.0
115
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
22.8
114
69-142
1,1,2-Trichloroethane
ug/L
ND
20
21.7
109
70-138
1,1-Dichloroethane
ug/L
ND
20
23.2
116
70-150
1,1-Dichloroethene
ug/L
ND
20
24.0
120
70-156
1,2,3-Trichloropropane
ug/L
ND
20
22.5
112
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20.5
102
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.7
108
70-138
1,2-Dichlorobenzene
ug/L
ND
20
22.4
112
70-141
1,2-Dichloroethane
ug/L
ND
20
23.7
119
69-143
1,2-Dichloropropane
ug/L
ND
20
22.1
111
68-156
1,4-Dichlorobenzene
ug/L
ND
20
21.7
109
70-142
2-Butanone (MEK)
ug/L
ND
40
45.3
113
60-157
2-Hexanone
ug/L
ND
40
46.3
116
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
43.9
110
70-141
Acetone
ug/L
ND
40
46.5
116
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
MATRIX SPIKE SAMPLE:
Parameter
3769534
Units
92625613001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
107
107
69-147
Benzene
ug/L
ND
20
21.9
109
70-142
Bromochloromethane
ug/L
ND
20
22.0
110
70-146
Bromodichloromethane
ug/L
ND
20
22.0
110
70-139
Bromoform
ug/L
ND
20
17.5
88
64-140
Bromomethane
ug/L
ND
20
22.4
112
28-192
Carbon disulfide
ug/L
ND
20
23.0
115
70-151
Carbon tetrachloride
ug/L
ND
20
22.2
111
70-148
Chlorobenzene
ug/L
ND
20
22.3
112
70-141
Chloroethane
ug/L
ND
20
32.4
162
58-191
Chloroform
ug/L
ND
20
21.3
107
70-148
Chloromethane
ug/L
ND
20
24.3
121
43-162
cis-1,2-Dichloroethene
ug/L
1.3
20
24.7
117
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
20.5
102
70-139
Dibromochloromethane
ug/L
ND
20
19.6
98
70-144
Dibromomethane
ug/L
ND
20
20.2
101
70-139
Ethylbenzene
ug/L
ND
20
23.0
115
70-143
lodomethane
ug/L
ND
40
35.4
88
35-171
m&p-Xylene
ug/L
ND
40
46.2
116
70-144
Methylene Chloride
ug/L
ND
20
21.6
108
62-149
o-Xylene
ug/L
ND
20
22.2
111
70-145
Styrene
ug/L
ND
20
22.6
113
70-143
Tetrachloroethene
ug/L
ND
20
19.5
97
70-145
Toluene
ug/L
ND
20
21.9
110
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
23.5
117
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
19.9
99
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
15.7
78
51-159
Trichloroethene
ug/L
ND
20
22.3
107
62-146
Trichlorofluoromethane
ug/L
ND
20
22.8
114
63-153
Vinyl acetate
ug/L
ND
40
42.5
106
61-162
Vinyl chloride
ug/L
ND
20
24.2
121
61-163
Xylene (Total)
ug/L
ND
60
68.5
114
70-143
1,2-Dichloroethane-d4 (S)
%
107
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 3769535
Parameter
Units
92625615001
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
SAMPLE DUPLICATE: 3769535
Parameter
Units
92625615001
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
.82J
Chloroethane
ug/L
1.1
1.1
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
110
114
4-Bromofluorobenzene (S)
%
99
95
Toluene-d8 (S)
%
101
101
RPD Qualifiers
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
QC Batch: 723329 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92625613001, 92625613002, 92625613003, 92625613004, 92625613005
METHOD BLANK: 3768916
Matrix:
Water
Associated Lab Samples:
92625613001, 92625613002, 92625613003, 92625613004, 92625613005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/14/22 16:56
1,2-Dichloroethane-d4 (S)
%
93
70-130
09/14/22 16:56
Toluene-d8 (S)
%
92
70-130
09/14/22 16:56
LABORATORY CONTROL SAMPLE: 3768917
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 17.8 89 70-130
1,2-Dichloroethane-d4 (S) % 92 70-130
Toluene-d8 (S) % 92 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3768918
3768919
MS
MSD
92625613001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.3
19.2 96
96
63-136 1
1,2-Dichloroethane-d4 (S)
%
97
96
70-130
Toluene-d8(S)
%
94
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625613
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625613
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92625613001
6002-HRW7
EPA 3010A
725626
EPA6010D
725796
92625613002
6002-HRW18
EPA 3010A
725626
EPA6010D
725796
92625613003
6002-HRW19
EPA 3010A
725626
EPA6010D
725796
92625613004
6002-HRW20
EPA 3010A
725626
EPA6010D
725796
92625613005
6002-HRW21
EPA 3010A
725626
EPA6010D
725796
92625613001
6002-HRW7
EPA 3005A
725173
EPA 6020B
725366
92625613002
6002-HRW18
EPA 3005A
725173
EPA 6020B
725366
92625613003
6002-HRW19
EPA 3005A
725298
EPA 6020B
725536
92625613004
6002-HRW20
EPA 3005A
725298
EPA 6020B
725536
92625613005
6002-HRW21
EPA 3005A
725298
EPA 6020B
725536
92625613001
6002-HRW7
EPA 8260D
723470
92625613002
6002-HRW18
EPA 8260D
723470
92625613003
6002-HRW19
EPA 8260D
723470
92625613004
6002-HRW20
EPA 8260D
723470
92625613005
6002-HRW21
EPA 8260D
723470
92625613006
TRIP BLANK
EPA 8260D
723470
92625613001
6002-HRW7
EPA 8260D Mod.
723329
92625613002
6002-HRW18
EPA 8260D Mod.
723329
92625613003
6002-HRW19
EPA 8260D Mod.
723329
92625613004
6002-HRW20
EPA 8260D Mod.
723329
92625613005
6002-HRW21
EPA 8260D Mod.
723329
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 30

r�aG'e ,-vvWv vV I TaIIIVIC LVIIUILIVII %J[JVr' lI rEk t:1 JL
— - Effective Date: 0511212ti 05tr2j2622 - - ---- -
Laboratory receiving samples: r —�
cheve�� Eden__ Greenwood -I ---I EitintPr,CVt1l0 [7 ---
curler•
❑ Commercial
Cuqtn
-Client. Name: �O ■ 9'�6 -
Project #
13
���1�1�'nht_�rrtl ('r
UPS
[]Other:
_uatinLvnmain rerson cxmnin n&6onren[S:
Packing Material: ❑Bubble Wrap ❑Bubble Bags - - -- -- —
g []None ❑ Other Biological Tissu ro:en? '
Thermometer: ❑Yes []No . N/A
lIRGurtID: n v Type of ice: CZW.t ❑Blue Done
�I!! Correction Factor:
Cooler Temp: — Add/Subtract (°C) U Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected j°�: liasbegun
USDA Regulated Sail ( M N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally,
(check maosl?f1Yes f1Nn
.._._....w .._.__..-..-.--- —.......,.y..._ y..v
Comments/Discrepancy:
Chain of Custody Present?
©
[]No❑N/A
1.
Sam pies Arrived within Hold Time?
' 'Yes
❑ o
[I N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
JZffj.
❑NIA
3.
Rush Turn Around Time Requested?
Des
No
❑N/A
4.
Sufficient Volume?
[Wgs
❑Na
❑N/A
5.
Correct Containers Used?
s
❑No
[--]N/A
6.
-Pace Containers Used?
Y s
❑No
❑N/A
Containers intact?
Yes
❑Na
❑N A
1.
Dissolved analysis: Samples Field Filtered?
❑Y s
❑No
N/A
S.
Sample Labels Match COC?
Ves
[]No
©N/A
9.
-includes Date/Time/ID/Analysis Matrix:
ON�
Headspace In VOA Vials (>S-Smm)?
❑ es
E2/No
❑NJA
10.
Trip Stank Present?
JJYes
❑No
[]NIA
11.
Trip Blank Custody Seals Present?
Dyes
2 No
❑N/A
d
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOWTION
Person contacted: — - — -- - bate/Time:
Project Manager SCURF Review:
Rr0i4Ct managar srtr
Date;
Field Data Required?
Qualtrax ID: 69614 Page 1 of 2 Page 28 of 30

Race
---- —• • --" •'—'-, ---- ry _--I I Et.11G 4VE I U I IIVEI 1-'lJVll J%t:l%;IJJL
Effective Date: 05/121202205/12/2022
`Check mark top half of Box if pH and/or dechlorination is verified and
to Ithln the acceptance range for preservation samples.
Exceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, Etflg
*"Bottom half of Box is to list number of bottles
-'*Check all unpreserved Nitrates for chlorine
W01t : 926266113
Project f pM • M14$ Dus_.pate:-49/28/22-
CLIENT: 92—MECK CO
z
ctl
d
z
N
u
M
a
£�
ry
Iv
a
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Qualtrax ID: 69614 Page 2 of 2 Page 29 of 30

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Page 30 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 27, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625615
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92625615001
6002-HRW10
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625615002
6002-HRW11R
EPA 601OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625615003
6002-HRW12
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625615004
6002-HRW13
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625615005
6002-HRW17
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
GAW
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92625615006
TRIP BLANK
EPA 8260D
GAW
52
PASI-C
PASI-C = Pace Analytical
Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW10 Lab ID: 92625615001 Collected: 09/14/22 12:10 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:13
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:13
7440-41-7
Barium
164
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:13
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:13
7440-43-9
Chromium
14.7
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:13
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:13
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:13
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:13
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:13
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:13
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:13
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:13
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:13
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:13
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:13
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:28
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 12:09
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 12:09
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 12:09
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 12:09
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 12:09
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 12:09
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 12:09
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 12:09
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 12:09
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 12:09
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 12:09
108-90-7
Chloroethane
1.1
ug/L
1.0
1
09/15/22 12:09
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 12:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 12:09
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 12:09
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 12:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 12:09
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 12:09
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 12:09
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 12:09
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 12:09
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 12:09
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 12:09
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW10 Lab ID: 92625615001 Collected: 09/14/22 12:10 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:09
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:09
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:09
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 12:09
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 12:09
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 12:09
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 12:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 12:09
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 12:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 12:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 12:09
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 12:09
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 12:09
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 12:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 12:09
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 12:09
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 12:09
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 12:09
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 12:09
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 12:09
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 12:09
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 12:09
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 12:09
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/15/22 12:09
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70-130
1
09/15/22 12:09
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 12:09
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
5.9
ug/L
2.0
1
09/14/22 18:51
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
09/14/22 18:51
17060-07-0
Toluene-d8 (S)
92
%
70-130
1
09/14/22 18:51
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW11R Lab ID: 92625615002 Collected: 09/14/22 11:00 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:17
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:17
7440-41-7
Barium
419
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:17
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:17
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:17
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:17
7440-50-8
Nickel
129
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:17
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:17
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:17
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:17
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:17
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:17
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:17
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:17
7440-66-6
Cobalt
40.7
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:17
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:34
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 12:46
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 12:46
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 12:46
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 12:46
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 12:46
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 12:46
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 12:46
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 12:46
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 12:46
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 12:46
56-23-5
Chlorobenzene
14.4
ug/L
1.0
1
09/15/22 12:46
108-90-7
Chloroethane
1.1
ug/L
1.0
1
09/15/22 12:46
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 12:46
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 12:46
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 12:46
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 12:46
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 12:46
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 12:46
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 12:46
95-50-1
1,4-Dichlorobenzene
3.1
ug/L
1.0
1
09/15/22 12:46
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 12:46
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 12:46
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 12:46
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW11R Lab ID: 92625615002 Collected: 09/14/22 11:00 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:46
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:46
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 12:46
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:46
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 12:46
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 12:46
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 12:46
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 12:46
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 12:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 12:46
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 12:46
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 12:46
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 12:46
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 12:46
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 12:46
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 12:46
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 12:46
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 12:46
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 12:46
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 12:46
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 12:46
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 12:46
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 12:46
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 12:46
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 12:46
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
09/15/22 12:46
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
09/15/22 12:46
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 12:46
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
182
ug/L
5.0
2.5
09/15/22 21:42
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
70-130
2.5
09/15/22 21:42
17060-07-0
Toluene-d8 (S)
91
%
70-130
2.5
09/15/22 21:42
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW12 Lab ID: 92625615003 Collected: 09/14/22 11:15 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:22
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:22
7440-41-7
Barium
866
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:22
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:22
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:22
7440-47-3
Copper
86.3
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:22
7440-50-8
Nickel
177
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:22
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:22
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:22
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:22
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:22
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:22
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:22
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:22
7440-66-6
Cobalt
58.4
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:22
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 16:09
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 16:09
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 16:09
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 16:09
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 16:09
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 16:09
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 16:09
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 16:09
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 16:09
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 16:09
56-23-5
Chlorobenzene
8.3
ug/L
1.0
1
09/15/22 16:09
108-90-7
Chloroethane
1.6
ug/L
1.0
1
09/15/22 16:09
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 16:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 16:09
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 16:09
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 16:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 16:09
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 16:09
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 16:09
95-50-1
1,4-Dichlorobenzene
2.6
ug/L
1.0
1
09/15/22 16:09
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 16:09
110-57-6
1,1-Dichloroethane
7.1
ug/L
1.0
1
09/15/22 16:09
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 16:09
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW12 Lab ID: 92625615003 Collected: 09/14/22 11:15 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 16:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 16:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 16:09
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 16:09
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 16:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 16:09
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 16:09
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 16:09
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 16:09
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 16:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 16:09
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 16:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 16:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 16:09
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 16:09
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 16:09
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 16:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 16:09
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 16:09
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 16:09
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 16:09
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 16:09
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 16:09
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/15/22 16:09
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/15/22 16:09
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/15/22 16:09
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
09/15/22 16:09
460-00-4
1,2-Dichloroethane-d4 (S)
116
%
70-130
1
09/15/22 16:09
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 16:09
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
133
ug/L
4.0
2
09/15/22 22:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95
%
70-130
2
09/15/22 22:01
17060-07-0
Toluene-d8 (S)
91
%
70-130
2
09/15/22 22:01
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW13 Lab ID: 92625615004 Collected: 09/14/22 11:30 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:27
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:27
7440-41-7
Barium
104
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:27
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:27
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:27
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:27
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:27
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:27
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:27
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:27
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:27
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:27
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:27
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:27
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:27
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2218:58
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 13:05
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 13:05
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 13:05
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 13:05
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 13:05
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 13:05
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 13:05
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 13:05
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 13:05
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 13:05
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 13:05
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 13:05
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 13:05
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 13:05
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 13:05
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 13:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 13:05
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 13:05
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 13:05
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 13:05
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 13:05
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 13:05
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 13:05
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW13 Lab ID: 92625615004 Collected: 09/14/22 11:30 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/27/2022 02:09 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
117
%
100
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
95 %
93 %
1.0
1
09/15/22 13:05
75-35-4
1.0
1
09/15/22 13:05
156-59-2
1.0
1
09/15/22 13:05
156-60-5
1.0
1
09/15/22 13:05
78-87-5
1.0
1
09/15/22 13:05
10061-01-5
1.0
1
09/15/22 13:05
10061-02-6
1.0
1
09/15/22 13:05
100-41-4
5.0
1
09/15/22 13:05
591-78-6
20.0
1
09/15/22 13:05
74-88-4
5.0
1
09/15/22 13:05
75-09-2
5.0
1
09/15/22 13:05
108-10-1
1.0
1
09/15/22 13:05
100-42-5
1.0
1
09/15/22 13:05
630-20-6
1.0
1
09/15/22 13:05
79-34-5
1.0
1
09/15/22 13:05
127-18-4
1.0
1
09/15/22 13:05
108-88-3
1.0
1
09/15/22 13:05
71-55-6
1.0
1
09/15/22 13:05
79-00-5
1.0
1
09/15/22 13:05
79-01-6
1.0
1
09/15/22 13:05
75-69-4
1.0
1
09/15/22 13:05
96-18-4
2.0
1
09/15/22 13:05
108-05-4
1.0
1
09/15/22 13:05
75-01-4
1.0
1
09/15/22 13:05
1330-20-7
2.0
1
09/15/22 13:05
179601-23-1
1.0
1
09/15/22 13:05
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/15/22 13:05 460-00-4
09/15/22 13:05 17060-07-0
09/15/22 13:05 2037-26-5
1I11-71C!f A, F11911mileas*SQi
09/14/22 19:30 17060-07-0
09/14/2219:30 2037-26-5
Page 11 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW17 Lab ID: 92625615005 Collected: 09/14/22 11:45 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:32
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:32
7440-41-7
Barium
50.6
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:32
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:32
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:32
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:32
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:32
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:32
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:32
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:32
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:32
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:32
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:32
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:32
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:32
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/2214:15
09/26/2219:04
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 16:28
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 16:28
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 16:28
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 16:28
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 16:28
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 16:28
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 16:28
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 16:28
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 16:28
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 16:28
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 16:28
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 16:28
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 16:28
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 16:28
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 16:28
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 16:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 16:28
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 16:28
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 16:28
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 16:28
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 16:28
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 16:28
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 16:28
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: 6002-HRW17 Lab ID: 92625615005 Collected: 09/14/22 11:45 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/27/2022 02:09 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97
%
119
%
103
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
95 %
93 %
1.0
1
09/15/22 16:28
75-35-4
1.0
1
09/15/22 16:28
156-59-2
1.0
1
09/15/22 16:28
156-60-5
1.0
1
09/15/22 16:28
78-87-5
1.0
1
09/15/22 16:28
10061-01-5
1.0
1
09/15/22 16:28
10061-02-6
1.0
1
09/15/22 16:28
100-41-4
5.0
1
09/15/22 16:28
591-78-6
20.0
1
09/15/22 16:28
74-88-4
5.0
1
09/15/22 16:28
75-09-2
5.0
1
09/15/22 16:28
108-10-1
1.0
1
09/15/22 16:28
100-42-5
1.0
1
09/15/22 16:28
630-20-6
1.0
1
09/15/22 16:28
79-34-5
1.0
1
09/15/22 16:28
127-18-4
1.0
1
09/15/22 16:28
108-88-3
1.0
1
09/15/22 16:28
71-55-6
1.0
1
09/15/22 16:28
79-00-5
1.0
1
09/15/22 16:28
79-01-6
1.0
1
09/15/22 16:28
75-69-4
1.0
1
09/15/22 16:28
96-18-4
2.0
1
09/15/22 16:28
108-05-4
1.0
1
09/15/22 16:28
75-01-4
1.0
1
09/15/22 16:28
1330-20-7
2.0
1
09/15/22 16:28
179601-23-1
1.0
1
09/15/22 16:28
95-47-6
70-130 1
70-130 1
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/15/22 16:28 460-00-4
09/15/22 16:28 17060-07-0
09/15/22 16:28 2037-26-5
09/14/22 20:08 17060-07-0
09/14/22 20:08 2037-26-5
Page 13 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: TRIP BLANK Lab ID: 92625615006 Collected: 09/14/22 08:40 Received: 09/14/22 13:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/15/22 11:32
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/15/22 11:32
107-13-1
Benzene
ND
ug/L
1.0
1
09/15/22 11:32
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/15/22 11:32
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/15/22 11:32
75-27-4
Bromoform
ND
ug/L
1.0
1
09/15/22 11:32
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/15/22 11:32
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/15/22 11:32
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/15/22 11:32
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/15/22 11:32
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/15/22 11:32
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/15/22 11:32
75-00-3
Chloroform
ND
ug/L
1.0
1
09/15/22 11:32
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/15/22 11:32
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/15/22 11:32
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/15/22 11:32
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/15/22 11:32
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/15/22 11:32
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:32
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/15/22 11:32
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/15/22 11:32
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:32
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/15/22 11:32
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:32
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:32
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/15/22 11:32
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:32
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:32
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/15/22 11:32
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/15/22 11:32
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/15/22 11:32
591-78-6
lodomethane
ND
ug/L
20.0
1
09/15/22 11:32
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/15/22 11:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/15/22 11:32
108-10-1
Styrene
ND
ug/L
1.0
1
09/15/22 11:32
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:32
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/15/22 11:32
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/15/22 11:32
127-18-4
Toluene
ND
ug/L
1.0
1
09/15/22 11:32
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:32
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/15/22 11:32
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/15/22 11:32
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/15/22 11:32
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/15/22 11:32
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/15/22 11:32
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/15/22 11:32
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
Sample: TRIP BLANK
Parameters
Lab ID: 92625615006 Collected: 09/14/22 08:40
Results Units Report Limit DF
Received: 09/14/22 13:05 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/15/22 11:32
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/15/22 11:32
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/15/22 11:32
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
09/15/22 11:32
460-00-4
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
09/15/22 11:32
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
09/15/22 11:32
2037-26-5
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
QC Batch: 725626 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005
METHOD BLANK: 3780263 Matrix: Water
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
50.0
09/26/2218:15
Arsenic
ug/L
ND
30.0
09/26/2218:15
Barium
ug/L
ND
10.0
09/26/2218:15
Beryllium
ug/L
ND
10.0
09/26/2218:15
Cadmium
ug/L
ND
10.0
09/26/2218:15
Chromium
ug/L
ND
10.0
09/26/2218:15
Cobalt
ug/L
ND
40.0
09/26/2218:15
Copper
ug/L
ND
20.0
09/26/2218:15
Lead
ug/L
ND
20.0
09/26/2218:15
Nickel
ug/L
ND
20.0
09/26/2218:15
Selenium
ug/L
ND
40.0
09/26/2218:15
Silver
ug/L
ND
10.0
09/26/2218:15
Thallium
ug/L
ND
200
09/26/2218:15
Vanadium
ug/L
ND
20.0
09/26/2218:15
Zinc
ug/L
ND
20.0
09/26/2218:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3780264
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
960
96
80-120
Arsenic
ug/L
1000
983
98
80-120
Barium
ug/L
1000
985
98
80-120
Beryllium
ug/L
1000
1010
101
80-120
Cadmium
ug/L
1000
996
100
80-120
Chromium
ug/L
1000
1020
102
80-120
Cobalt
ug/L
1000
991
99
80-120
Copper
ug/L
1000
1010
101
80-120
Lead
ug/L
1000
988
99
80-120
Nickel
ug/L
1000
976
98
80-120
Selenium
ug/L
1000
996
100
80-120
Silver
ug/L
1000
986
99
80-120
Thallium
ug/L
1000
950
95
80-120
Vanadium
ug/L
1000
1070
107
80-120
Zinc
ug/L
1000
994
99
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625615
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3780265
3780266
MS
MSD
92625613001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Arsenic
ug/L
ND
1000
1000
1050
1040
105
104
75-125
1
Barium
ug/L
101
1000
1000
1150
1150
105
105
75-125
0
Beryllium
ug/L
ND
1000
1000
1060
1060
106
106
75-125
1
Cadmium
ug/L
ND
1000
1000
1060
1070
106
107
75-125
1
Chromium
ug/L
ND
1000
1000
1060
1060
105
105
75-125
0
Cobalt
ug/L
ND
1000
1000
1030
1030
103
103
75-125
1
Copper
ug/L
ND
1000
1000
1080
1080
107
107
75-125
0
Lead
ug/L
ND
1000
1000
1030
1040
103
103
75-125
0
Nickel
ug/L
ND
1000
1000
1020
1010
102
101
75-125
1
Selenium
ug/L
ND
1000
1000
1040
1040
104
103
75-125
1
Silver
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Thallium
ug/L
ND
1000
1000
996
989
99
99
75-125
1
Vanadium
ug/L
ND
1000
1000
1130
1130
112
112
75-125
0
Zinc
ug/L
31.1
1000
1000
1070
1070
104
104
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
QC Batch: 725298 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005
METHOD BLANK: 3778817
Matrix:
Water
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
09/26/2217:40
LABORATORY CONTROL SAMPLE:
3778818
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
99.9
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3778819 3778820
MS MSD
92625613003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 101 102 100 102 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
QC Batch: 723470 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005, 92625615006
METHOD BLANK: 3769532 Matrix: Water
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005, 92625615006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,1-Trichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1,2-Trichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1-Dichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,1-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
1,2,3-Trichloropropane
ug/L
ND
1.0
09/15/22 09:05
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
09/15/22 09:05
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichlorobenzene
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloroethane
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloropropane
ug/L
ND
1.0
09/15/22 09:05
1,4-Dichlorobenzene
ug/L
ND
1.0
09/15/22 09:05
2-Butanone (MEK)
ug/L
ND
5.0
09/15/22 09:05
2-Hexanone
ug/L
ND
5.0
09/15/22 09:05
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/15/22 09:05
Acetone
ug/L
ND
25.0
09/15/22 09:05
Acrylonitrile
ug/L
ND
10.0
09/15/22 09:05
Benzene
ug/L
ND
1.0
09/15/22 09:05
Bromochloromethane
ug/L
ND
1.0
09/15/22 09:05
Bromodichloromethane
ug/L
ND
1.0
09/15/22 09:05
Bromoform
ug/L
ND
1.0
09/15/22 09:05
Bromomethane
ug/L
ND
2.0
09/15/22 09:05
Carbon disulfide
ug/L
ND
2.0
09/15/22 09:05
Carbon tetrachloride
ug/L
ND
1.0
09/15/22 09:05
Chlorobenzene
ug/L
ND
1.0
09/15/22 09:05
Chloroethane
ug/L
ND
1.0
09/15/22 09:05
Chloroform
ug/L
ND
1.0
09/15/22 09:05
Chloromethane
ug/L
ND
1.0
09/15/22 09:05
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/15/22 09:05
Dibromochloromethane
ug/L
ND
1.0
09/15/22 09:05
Dibromomethane
ug/L
ND
1.0
09/15/22 09:05
Ethylbenzene
ug/L
ND
1.0
09/15/22 09:05
lodomethane
ug/L
ND
20.0
09/15/22 09:05
m&p-Xylene
ug/L
ND
2.0
09/15/22 09:05
Methylene Chloride
ug/L
ND
5.0
09/15/22 09:05
o-Xylene
ug/L
ND
1.0
09/15/22 09:05
Styrene
ug/L
ND
1.0
09/15/22 09:05
Tetrachloroethene
ug/L
ND
1.0
09/15/22 09:05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
METHOD BLANK: 3769532 Matrix: Water
Associated Lab Samples: 92625615001, 92625615002, 92625615003, 92625615004, 92625615005, 92625615006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/15/22 09:05
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/15/22 09:05
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/15/22 09:05
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/15/22 09:05
Trichloroethene
ug/L
ND
1.0
09/15/22 09:05
Trichlorofluoromethane
ug/L
ND
1.0
09/15/22 09:05
Vinyl acetate
ug/L
ND
2.0
09/15/22 09:05
Vinyl chloride
ug/L
ND
1.0
09/15/22 09:05
Xylene (Total)
ug/L
ND
1.0
09/15/22 09:05
1,2-Dichloroethane-d4 (S)
%
109
70-130
09/15/22 09:05
4-Bromofluorobenzene (S)
%
98
70-130
09/15/22 09:05
Toluene-d8 (S)
%
101
70-130
09/15/22 09:05
LABORATORY CONTROL SAMPLE:
Parameter
3769533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.0
98
70-130
1,1,1-Trichloroethane
ug/L
50
44.5
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.5
101
70-130
1,1,2-Trichloroethane
ug/L
50
47.0
94
70-130
1,1-Dichloroethane
ug/L
50
44.5
89
70-130
1,1-Dichloroethene
ug/L
50
45.3
91
70-130
1,2,3-Trichloropropane
ug/L
50
49.3
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.2
100
70-131
1,2-Dibromoethane (EDB)
ug/L
50
48.3
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.3
101
70-130
1,2-Dichloroethane
ug/L
50
45.6
91
70-130
1,2-Dichloropropane
ug/L
50
45.9
92
70-130
1,4-Dichlorobenzene
ug/L
50
49.7
99
70-130
2-Butanone (MEK)
ug/L
100
84.9
85
70-134
2-Hexanone
ug/L
100
98.0
98
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.8
94
70-130
Acetone
ug/L
100
90.6
91
70-133
Acrylonitrile
ug/L
250
231
92
70-130
Benzene
ug/L
50
44.1
88
70-130
Bromochloromethane
ug/L
50
47.1
94
70-130
Bromodichloromethane
ug/L
50
46.8
94
70-130
Bromoform
ug/L
50
47.7
95
70-130
Bromomethane
ug/L
50
45.2
90
45-151
Carbon disulfide
ug/L
50
47.0
94
70-130
Carbon tetrachloride
ug/L
50
44.8
90
70-130
Chlorobenzene
ug/L
50
49.0
98
70-130
Chloroethane
ug/L
50
57.7
115
39-152
Chloroform
ug/L
50
45.2
90
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 30

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
LABORATORY CONTROL SAMPLE:
Parameter
3769533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
50
48.2
96
58-130
cis-1,2-Dichloroethene
ug/L
50
45.2
90
70-130
cis-1,3-Dichloropropene
ug/L
50
49.8
100
70-130
Dibromochloromethane
ug/L
50
46.5
93
70-130
Dibromomethane
ug/L
50
46.3
93
70-130
Ethylbenzene
ug/L
50
49.0
98
70-130
lodomethane
ug/L
100
97.8
98
53-141
m&p-Xylene
ug/L
100
100
100
70-130
Methylene Chloride
ug/L
50
41.6
83
66-130
o-Xylene
ug/L
50
50.2
100
70-130
Styrene
ug/L
50
51.7
103
70-130
Tetrachloroethene
ug/L
50
44.7
89
70-130
Toluene
ug/L
50
46.8
94
70-130
trans-1,2-Dichloroethene
ug/L
50
45.0
90
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.1
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
51.8
104
57-185
Trichloroethene
ug/L
50
47.5
95
70-130
Trichlorofluoromethane
ug/L
50
43.3
87
62-130
Vinyl acetate
ug/L
100
90.1
90
70-144
Vinyl chloride
ug/L
50
50.2
100
62-130
Xylene (Total)
ug/L
150
150
100
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
3769534
Units
92625613001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.9
109
70-141
1,1,1-Trichloroethane
ug/L
ND
20
23.0
115
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
22.8
114
69-142
1,1,2-Trichloroethane
ug/L
ND
20
21.7
109
70-138
1,1-Dichloroethane
ug/L
ND
20
23.2
116
70-150
1,1-Dichloroethene
ug/L
ND
20
24.0
120
70-156
1,2,3-Trichloropropane
ug/L
ND
20
22.5
112
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20.5
102
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.7
108
70-138
1,2-Dichlorobenzene
ug/L
ND
20
22.4
112
70-141
1,2-Dichloroethane
ug/L
ND
20
23.7
119
69-143
1,2-Dichloropropane
ug/L
ND
20
22.1
111
68-156
1,4-Dichlorobenzene
ug/L
ND
20
21.7
109
70-142
2-Butanone (MEK)
ug/L
ND
40
45.3
113
60-157
2-Hexanone
ug/L
ND
40
46.3
116
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
43.9
110
70-141
Acetone
ug/L
ND
40
46.5
116
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
MATRIX SPIKE SAMPLE:
Parameter
3769534
Units
92625613001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
107
107
69-147
Benzene
ug/L
ND
20
21.9
109
70-142
Bromochloromethane
ug/L
ND
20
22.0
110
70-146
Bromodichloromethane
ug/L
ND
20
22.0
110
70-139
Bromoform
ug/L
ND
20
17.5
88
64-140
Bromomethane
ug/L
ND
20
22.4
112
28-192
Carbon disulfide
ug/L
ND
20
23.0
115
70-151
Carbon tetrachloride
ug/L
ND
20
22.2
111
70-148
Chlorobenzene
ug/L
ND
20
22.3
112
70-141
Chloroethane
ug/L
ND
20
32.4
162
58-191
Chloroform
ug/L
ND
20
21.3
107
70-148
Chloromethane
ug/L
ND
20
24.3
121
43-162
cis-1,2-Dichloroethene
ug/L
1.3
20
24.7
117
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
20.5
102
70-139
Dibromochloromethane
ug/L
ND
20
19.6
98
70-144
Dibromomethane
ug/L
ND
20
20.2
101
70-139
Ethylbenzene
ug/L
ND
20
23.0
115
70-143
lodomethane
ug/L
ND
40
35.4
88
35-171
m&p-Xylene
ug/L
ND
40
46.2
116
70-144
Methylene Chloride
ug/L
ND
20
21.6
108
62-149
o-Xylene
ug/L
ND
20
22.2
111
70-145
Styrene
ug/L
ND
20
22.6
113
70-143
Tetrachloroethene
ug/L
ND
20
19.5
97
70-145
Toluene
ug/L
ND
20
21.9
110
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
23.5
117
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
19.9
99
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
15.7
78
51-159
Trichloroethene
ug/L
ND
20
22.3
107
62-146
Trichlorofluoromethane
ug/L
ND
20
22.8
114
63-153
Vinyl acetate
ug/L
ND
40
42.5
106
61-162
Vinyl chloride
ug/L
ND
20
24.2
121
61-163
Xylene (Total)
ug/L
ND
60
68.5
114
70-143
1,2-Dichloroethane-d4 (S)
%
107
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 3769535
Parameter
Units
92625615001
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
SAMPLE DUPLICATE: 3769535
Parameter
Units
92625615001
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
.82J
Chloroethane
ug/L
1.1
1.1
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
110
114
4-Bromofluorobenzene (S)
%
99
95
Toluene-d8 (S)
%
101
101
RPD Qualifiers
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
QC Batch: 723329 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92625615001, 92625615004, 92625615005
METHOD BLANK: 3768916
Matrix:
Water
Associated Lab Samples:
92625615001, 92625615004, 92625615005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/14/22 16:56
1,2-Dichloroethane-d4 (S)
%
93
70-130
09/14/22 16:56
Toluene-d8 (S)
%
92
70-130
09/14/22 16:56
LABORATORY CONTROL SAMPLE: 3768917
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 17.8 89 70-130
1,2-Dichloroethane-d4 (S) % 92 70-130
Toluene-d8 (S) % 92 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3768918
3768919
MS
MSD
92625613001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.3
19.2 96
96
63-136 1
1,2-Dichloroethane-d4 (S)
%
97
96
70-130
Toluene-d8(S)
%
94
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
QC Batch: 723674 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92625615002, 92625615003
METHOD BLANK: 3770822
Associated Lab Samples: 92625615002, 92625615003
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit
Analyzed
ND 2.0
09/15/2214:59
94 70-130
09/15/2214:59
94 70-130
09/15/2214:59
Qualifiers
LABORATORY CONTROL SAMPLE: 3770823
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 70-130
1,2-Dichloroethane-d4 (S) % 94 70-130
Toluene-d8 (S) % 93 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3770824
3770825
MS
MSD
92625809034 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 703 200
200
850
854 73
75
63-136 0
1,2-Dichloroethane-d4 (S)
%
94
95
70-130
Toluene-d8(S)
%
91
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 6002 HOLBROOKS RD LANDFILL
Pace Project No.: 92625615
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2022 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92625615
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92625615001
6002-HRW10
EPA 3010A
725626
EPA6010D
725796
92625615002
6002-HRW11 R
EPA 3010A
725626
EPA6010D
725796
92625615003
6002-HRW12
EPA 3010A
725626
EPA6010D
725796
92625615004
6002-HRW13
EPA 3010A
725626
EPA6010D
725796
92625615005
6002-HRW17
EPA 3010A
725626
EPA6010D
725796
92625615001
6002-HRW10
EPA3005A
725298
EPA6020B
725536
92625615002
6002-HRW11 R
EPA 3005A
725298
EPA 6020B
725536
92625615003
6002-HRW12
EPA3005A
725298
EPA6020B
725536
92625615004
6002-HRW13
EPA3005A
725298
EPA6020B
725536
92625615005
6002-HRW17
EPA3005A
725298
EPA6020B
725536
92625615001
6002-HRW10
EPA 8260D
723470
92625615002
6002-HRW11R
EPA 8260D
723470
92625615003
6002-HRW12
EPA 8260D
723470
92625615004
6002-HRW13
EPA 8260D
723470
92625615005
6002-HRW17
EPA 8260D
723470
92625615006
TRIP BLANK
EPA 8260D
723470
92625615001
6002-HRW10
EPA 8260D Mod.
723329
92625615002
6002-HRW11R
EPA 8260D Mod.
723674
92625615003
6002-HRW12
EPA 8260D Mod.
723674
92625615004
6002-HRW13
EPA 8260D Mod.
723329
92625615005
6002-HRW17
EPA 8260D Mod.
723329
Date: 09/27/2022 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 30

[ice
: �4i:Se.YU SIhY14
L-EfflectivcDatey05/�tWM�02Q22-- -
Laboratory receiving Samples:
- nehasellla n Eden❑ Ceeeed-Huirefsviile - t
• Cllent-Narne: __ - - - -
WO## 9262561 --
ourrer: ElFed EX lent
❑ Commercial ❑Pace ❑Other:
926251315
.
Date Initials Person ExaminingCorgents: r -- - .
-
Packing Mater a : _JQBubble Wrap su le Bags ❑Nona. Q. Other Biological Tissue frozen?
Ther❑Yes [-]No 14N/A
momeer: _—_ _ __ ,._. --
IR
Gun
Type of Ice: �j[Jwet OBlue Done
Correction Factor: "�
Cooler Temp: Add/Subtract 1°C) Temp should be above freezing to 6*C
[]Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('Q: 5 - has begun
USDA Regulated Soil (VN/A, water sample)
Did samples originate Mu arantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (intgna}ionally,
icheck maosI? MYes I )i a including Hawaiian Puerto Rico}? 7Yes I Mo
Comments/Discrepancy-
Chain of Custody Present?
Yes
❑N❑
❑N/A
1.
Samples Arrived within Hold Time?
. Yes
[]No
[]N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
JXNo
❑N/A
4.
Sufficient Volume?
Yes
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
No
[]No
[]N/A
❑N/A
6.
Containers intact?
es
[:]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered? []Yes
No
❑N/A
S,
Sample. Labels Match COC?
-includes Date/Time/ID/Analysis
1 Yes
Matrix: V
❑N❑
[I N/A
9.
Headspace in VOA Vials (>5-6rnm)?
QYes
❑No
❑N/A
SD.
Trip Blank Present?
Trip Blank Custody Seals Present?
Ryes
[]Yes
-E]kNo
J-
No
❑N/A
❑N/A
11.
�
COMMENTS/SAMPLE DISCREPANCY
CtfENT NOTIFICATION/RESOCUVON
Person contacted:
Project Manager SCURF Review:
—-.R. ..,_cnrn....:......
Lot ID Of Split Containers:
Date/Time:
Date:
Field Data Required? []Yes ❑No
Qualtrax ID: 69614 Page 1 of 2 Page 28 of 30

- 013
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- Effective -Date: 0-5H21202205-[12/20tz - - - -
*Check mark to half of box it H and/or dechlorination is verified -_and �� �`'6256 15
R P / _. - _. ---- - Project # �---
�witftlrti#heacceRtant erQati�rsae>tfsl s. I PM: iMWB Due .Rate,.-.09/28/22
Exceptions: VOA, Ca form, TOC, Oif and Grease, DRO/8015 {water] DOC, LLHg CLIENT: 92-MECK CID
"Bottom half of box is to list number of bottles l -
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_..pH -Adjustment Log for Preserved -Samples -
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #t
_ ..
,uufe. rv1-vtlt2ve( were Fs a usscrepancy affecting North Larouna corn pilance samptes, a copy of this form well nesent to the North Carolina 0ENR Certification Office (i.e.
Outof hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID. 69614 Page 2 of 2
Page 29 of 30

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Page 30 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 28, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
6002- HOLBROOKS RD LANDIFLL
92626011
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92626011001
6002-HRW8
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626011002
6002-HRW9R
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626011003
6002-HRW14
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626011004
6002-HRW15
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626011005
6002-HRW16
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626011006
TRIP BLANK
EPA 8260D
CL
52
PASI-C
PASI-C = Pace Analytical
Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW8 Lab ID: 92626011001 Collected: 09/15/22 12:00 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:42
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:42
7440-41-7
Barium
127
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:42
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:42
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:42
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:42
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:42
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:42
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:42
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:42
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:42
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:42
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:42
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:42
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:42
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 21:44
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/19/22 23:28
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/19/22 23:28
107-13-1
Benzene
ND
ug/L
1.0
1
09/19/22 23:28
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/19/22 23:28
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/19/22 23:28
75-27-4
Bromoform
ND
ug/L
1.0
1
09/19/22 23:28
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/19/22 23:28
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/19/22 23:28
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/19/22 23:28
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/19/22 23:28
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/19/22 23:28
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/19/22 23:28
75-00-3
Chloroform
ND
ug/L
1.0
1
09/19/22 23:28
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/19/22 23:28
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/19/22 23:28
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/19/22 23:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/19/22 23:28
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/19/22 23:28
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 23:28
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 23:28
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/19/22 23:28
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/19/22 23:28
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/19/22 23:28
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW8 Lab ID: 92626011001 Collected: 09/15/22 12:00 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:28
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:28
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:28
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/19/22 23:28
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/19/22 23:28
591-78-6
lodomethane
ND
ug/L
20.0
1
09/19/22 23:28
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/19/22 23:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/19/22 23:28
108-10-1
Styrene
ND
ug/L
1.0
1
09/19/22 23:28
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 23:28
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 23:28
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/19/22 23:28
127-18-4
Toluene
ND
ug/L
1.0
1
09/19/22 23:28
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/19/22 23:28
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/19/22 23:28
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/19/22 23:28
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/19/22 23:28
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/19/22 23:28
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/19/22 23:28
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/19/22 23:28
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/19/22 23:28
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/19/22 23:28
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/19/22 23:28
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/19/22 23:28
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
09/19/22 23:28
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
09/19/22 23:28
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/15/22 23:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
09/15/22 23:37
17060-07-0
Toluene-d8 (S)
91
%
70-130
1
09/15/22 23:37
2037-26-5
Date: 09/28/2022 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW9R Lab ID: 92626011002 Collected: 09/15/22 11:15 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:46
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:46
7440-41-7
Barium
461
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:46
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:46
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:46
7440-47-3
Copper
31.3
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:46
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:46
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:46
7440-22-4
Lead
24.5
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:46
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:46
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:46
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:46
7440-28-0
Vanadium
23.4
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:46
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:46
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:46
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:08
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 01:35
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 01:35
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 01:35
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 01:35
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 01:35
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 01:35
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 01:35
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 01:35
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 01:35
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 01:35
56-23-5
Chlorobenzene
2.9
ug/L
1.0
1
09/20/22 01:35
108-90-7
Chloroethane
1.4
ug/L
1.0
1
09/20/22 01:35
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 01:35
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 01:35
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 01:35
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 01:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 01:35
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 01:35
74-95-3
1,2-Dichlorobenzene
5.8
ug/L
1.0
1
09/20/22 01:35
95-50-1
1,4-Dichlorobenzene
8.0
ug/L
1.0
1
09/20/22 01:35
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 01:35
110-57-6
1,1-Dichloroethane
28.6
ug/L
1.0
1
09/20/22 01:35
75-34-3
1,2-Dichloroethane
2.1
ug/L
1.0
1
09/20/22 01:35
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW9R Lab ID: 92626011002 Collected: 09/15/22 11:15 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/20/22 01:35
75-35-4
cis-1,2-Dichloroethene
68.6
ug/L
1.0
1
09/20/22 01:35
156-59-2
trans-1,2-Dichloroethene
1.1
ug/L
1.0
1
09/20/22 01:35
156-60-5
1,2-Dichloropropene
2.7
ug/L
1.0
1
09/20/22 01:35
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 01:35
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 01:35
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/20/22 01:35
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/20/22 01:35
591-78-6
lodomethane
ND
ug/L
20.0
1
09/20/22 01:35
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/20/22 01:35
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/20/22 01:35
108-10-1
Styrene
ND
ug/L
1.0
1
09/20/22 01:35
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 01:35
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 01:35
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/20/22 01:35
127-18-4
Toluene
ND
ug/L
1.0
1
09/20/22 01:35
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/20/22 01:35
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/20/22 01:35
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/20/22 01:35
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/20/22 01:35
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/20/22 01:35
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/20/22 01:35
108-05-4
Vinyl chloride
6.6
ug/L
1.0
1
09/20/22 01:35
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/20/22 01:35
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/20/22 01:35
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/20/22 01:35
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
09/20/22 01:35
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/20/22 01:35
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/20/22 01:35
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
10.6
ug/L
2.0
1
09/15/22 23:56
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
09/15/22 23:56
17060-07-0
Toluene-d8 (S)
89
%
70-130
1
09/15/22 23:56
2037-26-5
Date: 09/28/2022 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW14 Lab ID: 92626011003 Collected: 09/15/22 10:15 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:51
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:51
7440-41-7
Barium
37.6
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:51
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:51
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:51
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:51
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:51
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:51
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:51
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:51
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:51
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:51
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:51
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:51
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:51
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:14
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/19/22 23:46
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/19/22 23:46
107-13-1
Benzene
ND
ug/L
1.0
1
09/19/22 23:46
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/19/22 23:46
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/19/22 23:46
75-27-4
Bromoform
ND
ug/L
1.0
1
09/19/22 23:46
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/19/22 23:46
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/19/22 23:46
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/19/22 23:46
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/19/22 23:46
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/19/22 23:46
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/19/22 23:46
75-00-3
Chloroform
ND
ug/L
1.0
1
09/19/22 23:46
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/19/22 23:46
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/19/22 23:46
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/19/22 23:46
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/19/22 23:46
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/19/22 23:46
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 23:46
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 23:46
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/19/22 23:46
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/19/22 23:46
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/19/22 23:46
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW14 Lab ID: 92626011003 Collected: 09/15/22 10:15 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:46
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:46
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 23:46
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:46
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 23:46
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/19/22 23:46
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/19/22 23:46
591-78-6
lodomethane
ND
ug/L
20.0
1
09/19/22 23:46
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/19/22 23:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/19/22 23:46
108-10-1
Styrene
ND
ug/L
1.0
1
09/19/22 23:46
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 23:46
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 23:46
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/19/22 23:46
127-18-4
Toluene
ND
ug/L
1.0
1
09/19/22 23:46
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/19/22 23:46
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/19/22 23:46
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/19/22 23:46
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/19/22 23:46
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/19/22 23:46
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/19/22 23:46
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/19/22 23:46
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/19/22 23:46
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/19/22 23:46
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/19/22 23:46
95-47-6
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
09/19/22 23:46
460-00-4
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
09/19/22 23:46
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
09/19/22 23:46
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/16/22 00:34
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
09/16/22 00:34
17060-07-0
Toluene-d8 (S)
91
%
70-130
1
09/16/22 00:34
2037-26-5
Date: 09/28/2022 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW15 Lab ID: 92626011004 Collected: 09/15/22 10:30 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 19:56
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:56
7440-41-7
Barium
153
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:56
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:56
7440-43-9
Chromium
12.0
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:56
7440-47-3
Copper
101
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:56
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:56
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 19:56
7440-22-4
Lead
28.7
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:56
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 19:56
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:56
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 19:56
7440-28-0
Vanadium
72.9
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:56
7440-62-2
Zinc
45.0
ug/L
20.0
1
09/26/22 09:25
09/26/22 19:56
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 19:56
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:20
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 00:05
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 00:05
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 00:05
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 00:05
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 00:05
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 00:05
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 00:05
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 00:05
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 00:05
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 00:05
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/20/22 00:05
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/20/22 00:05
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 00:05
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 00:05
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 00:05
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 00:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 00:05
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 00:05
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:05
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:05
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 00:05
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:05
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:05
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW15 Lab ID: 92626011004 Collected: 09/15/22 10:30 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/28/2022 03:41 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
95
%
102
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
106 %
102 %
1.0
1
09/20/22 00:05
75-35-4
1.0
1
09/20/22 00:05
156-59-2
1.0
1
09/20/22 00:05
156-60-5
1.0
1
09/20/22 00:05
78-87-5
1.0
1
09/20/22 00:05
10061-01-5
1.0
1
09/20/22 00:05
10061-02-6
1.0
1
09/20/22 00:05
100-41-4
5.0
1
09/20/22 00:05
591-78-6
20.0
1
09/20/22 00:05
74-88-4
5.0
1
09/20/22 00:05
75-09-2
5.0
1
09/20/22 00:05
108-10-1
1.0
1
09/20/22 00:05
100-42-5
1.0
1
09/20/22 00:05
630-20-6
1.0
1
09/20/22 00:05
79-34-5
1.0
1
09/20/22 00:05
127-18-4
1.0
1
09/20/22 00:05
108-88-3
1.0
1
09/20/22 00:05
71-55-6
1.0
1
09/20/22 00:05
79-00-5
1.0
1
09/20/22 00:05
79-01-6
1.0
1
09/20/22 00:05
75-69-4
1.0
1
09/20/22 00:05
96-18-4
2.0
1
09/20/22 00:05
108-05-4
1.0
1
09/20/22 00:05
75-01-4
1.0
1
09/20/22 00:05
1330-20-7
2.0
1
09/20/22 00:05
179601-23-1
1.0
1
09/20/22 00:05
95-47-6
70-130 1
70-130 1
70-130 1
01)
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/20/22 00:05 460-00-4
09/20/22 00:05 17060-07-0
09/20/22 00:05 2037-26-5
09/15/22 23:18 17060-07-0
09/15/22 23:18 2037-26-5
Page 11 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW16 Lab ID: 92626011005 Collected: 09/15/22 10:50 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 20:10
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:10
7440-41-7
Barium
101
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:10
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:10
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:10
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:10
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:10
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:10
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:10
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 20:10
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:10
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 20:10
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:10
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:10
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:10
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:26
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 00:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 00:23
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 00:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 00:23
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 00:23
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 00:23
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 00:23
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 00:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 00:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 00:23
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/20/22 00:23
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/20/22 00:23
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 00:23
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 00:23
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 00:23
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 00:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 00:23
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 00:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:23
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 00:23
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:23
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 30

leAnalyiical
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: 6002-HRW16 Lab ID: 92626011005 Collected: 09/15/22 10:50 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/28/2022 03:41 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96
%
96
%
100
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
2.5 ug/L
94 %
91 %
1.0
1
09/20/22 00:23
75-35-4
1.0
1
09/20/22 00:23
156-59-2
1.0
1
09/20/22 00:23
156-60-5
1.0
1
09/20/22 00:23
78-87-5
1.0
1
09/20/22 00:23
10061-01-5
1.0
1
09/20/22 00:23
10061-02-6
1.0
1
09/20/22 00:23
100-41-4
5.0
1
09/20/22 00:23
591-78-6
20.0
1
09/20/22 00:23
74-88-4
5.0
1
09/20/22 00:23
75-09-2
5.0
1
09/20/22 00:23
108-10-1
1.0
1
09/20/22 00:23
100-42-5
1.0
1
09/20/22 00:23
630-20-6
1.0
1
09/20/22 00:23
79-34-5
1.0
1
09/20/22 00:23
127-18-4
1.0
1
09/20/22 00:23
108-88-3
1.0
1
09/20/22 00:23
71-55-6
1.0
1
09/20/22 00:23
79-00-5
1.0
1
09/20/22 00:23
79-01-6
1.0
1
09/20/22 00:23
75-69-4
1.0
1
09/20/22 00:23
96-18-4
2.0
1
09/20/22 00:23
108-05-4
1.0
1
09/20/22 00:23
75-01-4
1.0
1
09/20/22 00:23
1330-20-7
2.0
1
09/20/22 00:23
179601-23-1
1.0
1
09/20/22 00:23
95-47-6
70-130 1
70-130 1
70-130 1
01)
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/20/22 00:23 460-00-4
09/20/22 00:23 17060-07-0
09/20/22 00:23 2037-26-5
[ek7f[:7f���eIelfiF'><if��c?�;SQiI
09/16/22 00:15 17060-07-0
09/16/22 00:15 2037-26-5
Page 13 of 30

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: TRIP BLANK Lab ID: 92626011006 Collected: 09/15/22 08:20 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/19/22 18:01
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/19/22 18:01
107-13-1
Benzene
ND
ug/L
1.0
1
09/19/22 18:01
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/19/22 18:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/19/22 18:01
75-27-4
Bromoform
ND
ug/L
1.0
1
09/19/22 18:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/19/22 18:01
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/19/22 18:01
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/19/22 18:01
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/19/22 18:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/19/22 18:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/19/22 18:01
75-00-3
Chloroform
ND
ug/L
1.0
1
09/19/22 18:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/19/22 18:01
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/19/22 18:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/19/22 18:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/19/22 18:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/19/22 18:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 18:01
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 18:01
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/19/22 18:01
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/19/22 18:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/19/22 18:01
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:01
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:01
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:01
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/19/22 18:01
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/19/22 18:01
591-78-6
lodomethane
ND
ug/L
20.0
1
09/19/22 18:01
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/19/22 18:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/19/22 18:01
108-10-1
Styrene
ND
ug/L
1.0
1
09/19/22 18:01
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 18:01
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 18:01
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/19/22 18:01
127-18-4
Toluene
ND
ug/L
1.0
1
09/19/22 18:01
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/19/22 18:01
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/19/22 18:01
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/19/22 18:01
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/19/22 18:01
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/19/22 18:01
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/19/22 18:01
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/19/22 18:01
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
Sample: TRIP BLANK
Parameters
Lab ID: 92626011006 Collected: 09/15/22 08:20
Results Units Report Limit DF
Received: 09/15/22 16:05 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/19/22 18:01
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/19/22 18:01
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/19/22 18:01
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
09/19/22 18:01
460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
09/19/22 18:01
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
09/19/22 18:01
2037-26-5
Date: 09/28/2022 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 30

leAnalyiical
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
QC Batch: 725626 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005
METHOD BLANK: 3780263 Matrix: Water
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
50.0
09/26/2218:15
Arsenic
ug/L
ND
30.0
09/26/2218:15
Barium
ug/L
ND
10.0
09/26/2218:15
Beryllium
ug/L
ND
10.0
09/26/2218:15
Cadmium
ug/L
ND
10.0
09/26/2218:15
Chromium
ug/L
ND
10.0
09/26/2218:15
Cobalt
ug/L
ND
40.0
09/26/2218:15
Copper
ug/L
ND
20.0
09/26/2218:15
Lead
ug/L
ND
20.0
09/26/2218:15
Nickel
ug/L
ND
20.0
09/26/2218:15
Selenium
ug/L
ND
40.0
09/26/2218:15
Silver
ug/L
ND
10.0
09/26/2218:15
Thallium
ug/L
ND
200
09/26/2218:15
Vanadium
ug/L
ND
20.0
09/26/2218:15
Zinc
ug/L
ND
20.0
09/26/2218:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3780264
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
960
96
80-120
Arsenic
ug/L
1000
983
98
80-120
Barium
ug/L
1000
985
98
80-120
Beryllium
ug/L
1000
1010
101
80-120
Cadmium
ug/L
1000
996
100
80-120
Chromium
ug/L
1000
1020
102
80-120
Cobalt
ug/L
1000
991
99
80-120
Copper
ug/L
1000
1010
101
80-120
Lead
ug/L
1000
988
99
80-120
Nickel
ug/L
1000
976
98
80-120
Selenium
ug/L
1000
996
100
80-120
Silver
ug/L
1000
986
99
80-120
Thallium
ug/L
1000
950
95
80-120
Vanadium
ug/L
1000
1070
107
80-120
Zinc
ug/L
1000
994
99
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
6002- HOLBROOKS RD LANDIFLL
92626011
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3780265
3780266
MS
MSD
92625613001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Arsenic
ug/L
ND
1000
1000
1050
1040
105
104
75-125
1
Barium
ug/L
101
1000
1000
1150
1150
105
105
75-125
0
Beryllium
ug/L
ND
1000
1000
1060
1060
106
106
75-125
1
Cadmium
ug/L
ND
1000
1000
1060
1070
106
107
75-125
1
Chromium
ug/L
ND
1000
1000
1060
1060
105
105
75-125
0
Cobalt
ug/L
ND
1000
1000
1030
1030
103
103
75-125
1
Copper
ug/L
ND
1000
1000
1080
1080
107
107
75-125
0
Lead
ug/L
ND
1000
1000
1030
1040
103
103
75-125
0
Nickel
ug/L
ND
1000
1000
1020
1010
102
101
75-125
1
Selenium
ug/L
ND
1000
1000
1040
1040
104
103
75-125
1
Silver
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Thallium
ug/L
ND
1000
1000
996
989
99
99
75-125
1
Vanadium
ug/L
ND
1000
1000
1130
1130
112
112
75-125
0
Zinc
ug/L
31.1
1000
1000
1070
1070
104
104
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
QC Batch: 725456 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005
METHOD BLANK: 3779489
Matrix:
Water
Associated Lab Samples: 92626011001, 92626011002,
92626011003, 92626011004, 92626011005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
09/27/22 21:32
LABORATORY CONTROL SAMPLE:
3779490
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
96.0
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3779491 3779492
MS MSD
92626011001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 92.8 93.6 93 93 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
QC Batch: 723786 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005, 92626011006
METHOD BLANK: 3771336 Matrix: Water
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005, 92626011006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,1-Trichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,2-Trichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1-Dichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
1,2,3-Trichloropropane
ug/L
ND
1.0
09/19/22 17:43
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
09/19/22 17:43
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichlorobenzene
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloropropane
ug/L
ND
1.0
09/19/22 17:43
1,4-Dichlorobenzene
ug/L
ND
1.0
09/19/22 17:43
2-Butanone (MEK)
ug/L
ND
5.0
09/19/22 17:43
2-Hexanone
ug/L
ND
5.0
09/19/22 17:43
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/19/22 17:43
Acetone
ug/L
ND
25.0
09/19/22 17:43
Acrylonitrile
ug/L
ND
10.0
09/19/22 17:43
Benzene
ug/L
ND
1.0
09/19/22 17:43
Bromochloromethane
ug/L
ND
1.0
09/19/22 17:43
Bromodichloromethane
ug/L
ND
1.0
09/19/22 17:43
Bromoform
ug/L
ND
1.0
09/19/22 17:43
Bromomethane
ug/L
ND
2.0
09/19/22 17:43
Carbon disulfide
ug/L
ND
2.0
09/19/22 17:43
Carbon tetrachloride
ug/L
ND
1.0
09/19/22 17:43
Chlorobenzene
ug/L
ND
1.0
09/19/22 17:43
Chloroethane
ug/L
ND
1.0
09/19/22 17:43
Chloroform
ug/L
ND
1.0
09/19/22 17:43
Chloromethane
ug/L
ND
1.0
09/19/22 17:43
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/19/22 17:43
Dibromochloromethane
ug/L
ND
1.0
09/19/22 17:43
Dibromomethane
ug/L
ND
1.0
09/19/22 17:43
Ethylbenzene
ug/L
ND
1.0
09/19/22 17:43
lodomethane
ug/L
ND
20.0
09/19/22 17:43
m&p-Xylene
ug/L
ND
2.0
09/19/22 17:43
Methylene Chloride
ug/L
ND
5.0
09/19/22 17:43
o-Xylene
ug/L
ND
1.0
09/19/22 17:43
Styrene
ug/L
ND
1.0
09/19/22 17:43
Tetrachloroethene
ug/L
ND
1.0
09/19/22 17:43
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
METHOD BLANK: 3771336 Matrix: Water
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011004, 92626011005, 92626011006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
09/19/22 17:43
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/19/22 17:43
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/19/22 17:43
Trichloroethene
ug/L
ND
1.0
09/19/22 17:43
Trichlorofluoromethane
ug/L
ND
1.0
09/19/22 17:43
Vinyl acetate
ug/L
ND
2.0
09/19/22 17:43
Vinyl chloride
ug/L
ND
1.0
09/19/22 17:43
Xylene (Total)
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloroethane-d4 (S)
%
99
70-130
09/19/22 17:43
4-Bromofluorobenzene (S)
%
98
70-130
09/19/22 17:43
Toluene-d8 (S)
%
103
70-130
09/19/22 17:43
LABORATORY CONTROL SAMPLE:
Parameter
3771337
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.0
96
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
44.8
90
70-130
1,1,2-Trichloroethane
ug/L
50
47.6
95
70-130
1,1-Dichloroethane
ug/L
50
47.7
95
70-130
1,1-Dichloroethene
ug/L
50
50.7
101
70-130
1,2,3-Trichloropropane
ug/L
50
44.2
88
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
47.0
94
70-131
1,2-Dibromoethane (EDB)
ug/L
50
48.2
96
70-130
1,2-Dichlorobenzene
ug/L
50
45.7
91
70-130
1,2-Dichloroethane
ug/L
50
46.5
93
70-130
1,2-Dichloropropane
ug/L
50
46.2
92
70-130
1,4-Dichlorobenzene
ug/L
50
44.0
88
70-130
2-Butanone (MEK)
ug/L
100
86.8
87
70-134
2-Hexanone
ug/L
100
91.4
91
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
92.4
92
70-130
Acetone
ug/L
100
87.1
87
70-133
Acrylonitrile
ug/L
250
232
93
70-130
Benzene
ug/L
50
46.7
93
70-130
Bromochloromethane
ug/L
50
47.6
95
70-130
Bromodichloromethane
ug/L
50
45.5
91
70-130
Bromoform
ug/L
50
49.2
98
70-130
Bromomethane
ug/L
50
47.6
95
45-151
Carbon disulfide
ug/L
50
53.7
107
70-130
Carbon tetrachloride
ug/L
50
51.9
104
70-130
Chlorobenzene
ug/L
50
46.6
93
70-130
Chloroethane
ug/L
50
52.0
104
39-152
Chloroform
ug/L
50
47.5
95
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 30

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
LABORATORY CONTROL SAMPLE:
Parameter
3771337
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
50
48.2
96
58-130
cis-1,2-Dichloroethene
ug/L
50
47.0
94
70-130
cis-1,3-Dichloropropene
ug/L
50
49.1
98
70-130
Dibromochloromethane
ug/L
50
47.0
94
70-130
Dibromomethane
ug/L
50
51.3
103
70-130
Ethylbenzene
ug/L
50
46.7
93
70-130
lodomethane
ug/L
100
111
111
53-141
m&p-Xylene
ug/L
100
92.1
92
70-130
Methylene Chloride
ug/L
50
47.4
95
66-130
o-Xylene
ug/L
50
46.3
93
70-130
Styrene
ug/L
50
47.4
95
70-130
Tetrachloroethene
ug/L
50
46.4
93
70-130
Toluene
ug/L
50
46.2
92
70-130
trans-1,2-Dichloroethene
ug/L
50
49.3
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.0
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
45.9
92
57-185
Trichloroethene
ug/L
50
49.4
99
70-130
Trichlorofluoromethane
ug/L
50
46.1
92
62-130
Vinyl acetate
ug/L
100
98.1
98
70-144
Vinyl chloride
ug/L
50
48.0
96
62-130
Xylene (Total)
ug/L
150
138
92
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
3771338
Units
92626011001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
22.3
112
70-141
1,1,1-Trichloroethane
ug/L
ND
20
25.6
128
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
21.1
105
69-142
1,1,2-Trichloroethane
ug/L
ND
20
22.8
114
70-138
1,1-Dichloroethane
ug/L
ND
20
23.9
118
70-150
1,1-Dichloroethene
ug/L
ND
20
27.2
136
70-156
1,2,3-Trichloropropane
ug/L
ND
20
21.0
105
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.8
109
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
22.8
114
70-138
1,2-Dichlorobenzene
ug/L
ND
20
21.9
110
70-141
1,2-Dichloroethane
ug/L
ND
20
21.8
109
69-143
1,2-Dichloropropane
ug/L
ND
20
23.3
117
68-156
1,4-Dichlorobenzene
ug/L
ND
20
21.4
107
70-142
2-Butanone (MEK)
ug/L
ND
40
45.5
114
60-157
2-Hexanone
ug/L
ND
40
43.5
109
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
45.4
114
70-141
Acetone
ug/L
ND
40
42.9
107
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
MATRIX SPIKE SAMPLE:
Parameter
3771338
Units
92626011001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
111
111
69-147
Benzene
ug/L
ND
20
23.3
116
70-142
Bromochloromethane
ug/L
ND
20
23.5
117
70-146
Bromodichloromethane
ug/L
ND
20
22.3
111
70-139
Bromoform
ug/L
ND
20
22.0
110
64-140
Bromomethane
ug/L
ND
20
26.1
131
28-192
Carbon disulfide
ug/L
ND
20
26.3
132
70-151
Carbon tetrachloride
ug/L
ND
20
25.4
127
70-148
Chlorobenzene
ug/L
ND
20
22.3
111
70-141
Chloroethane
ug/L
ND
20
28.4
142
58-191
Chloroform
ug/L
ND
20
23.9
120
70-148
Chloromethane
ug/L
ND
20
24.6
123
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
24.1
119
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
22.2
111
70-139
Dibromochloromethane
ug/L
ND
20
21.2
106
70-144
Dibromomethane
ug/L
ND
20
23.8
119
70-139
Ethylbenzene
ug/L
ND
20
22.5
113
70-143
lodomethane
ug/L
ND
40
47.2
118
35-171
m&p-Xylene
ug/L
ND
40
44.0
110
70-144
Methylene Chloride
ug/L
ND
20
24.1
121
62-149
o-Xylene
ug/L
ND
20
21.7
108
70-145
Styrene
ug/L
ND
20
22.1
110
70-143
Tetrachloroethene
ug/L
ND
20
22.7
113
70-145
Toluene
ug/L
ND
20
23.2
116
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
26.1
130
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
22.5
112
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
17.8
89
51-159
Trichloroethene
ug/L
ND
20
25.4
127
62-146
Trichlorofluoromethane
ug/L
ND
20
27.3
136
63-153
Vinyl acetate
ug/L
ND
40
46.9
117
61-162
Vinyl chloride
ug/L
ND
20
24.3
121
61-163
Xylene (Total)
ug/L
ND
60
65.6
109
70-143
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
93
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 3771339
Parameter
Units
92626011003
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
SAMPLE DUPLICATE: 3771339
Parameter
Units
92626011003
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
.61J
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
91
92
4-Bromofluorobenzene (S)
%
94
95
Toluene-d8 (S)
%
102
98
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
QC Batch: 723674 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92626011001, 92626011002, 92626011003, 92626011005
METHOD BLANK: 3770822
Matrix:
Water
Associated Lab Samples:
92626011001, 92626011002,
92626011003, 92626011005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/15/22 14:59
1,2-Dichloroethane-d4 (S)
%
94
70-130
09/15/22 14:59
Toluene-d8 (S)
%
94
70-130
09/15/22 14:59
LABORATORY CONTROL SAMPLE: 3770823
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 70-130
1,2-Dichloroethane-d4 (S) % 94 70-130
Toluene-d8 (S) % 93 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3770824
3770825
MS
MSD
92625809034 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 703 200
200
850
854 73
75
63-136 0
1,2-Dichloroethane-d4 (S)
%
94
95
70-130
Toluene-d8(S)
%
91
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
QC Batch: 723675 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92626011004
METHOD BLANK: 3770826
Matrix:
Water
Associated Lab Samples: 92626011004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/15/22 15:02
1,2-Dichloroethane-d4 (S)
%
97
70-130
09/15/22 15:02
Toluene-d8 (S)
%
102
70-130
09/15/22 15:02
LABORATORY CONTROL SAMPLE: 3770827
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.3 91 70-130
1,2-Dichloroethane-d4 (S) % 100 70-130
Toluene-d8 (S) % 106 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3770828
3770829
MS
MSD
92625809043 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 341 100
100
441
420 100
79
63-136 5
1,2-Dichloroethane-d4 (S)
%
93
95
70-130
Toluene-d8(S)
%
91
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 30

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 6002- HOLBROOKS RD LANDIFLL
Pace Project No.: 92626011
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 30

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
6002- HOLBROOKS RD LANDFILL
Pace Project No.:
92626011
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92626011001
6002-HRW8
EPA 3010A
725626
EPA 601OD
725796
92626011002
6002-HRW9R
EPA 3010A
725626
EPA 601OD
725796
92626011003
6002-HRW14
EPA 3010A
725626
EPA 601OD
725796
92626011004
6002-HRW15
EPA 3010A
725626
EPA 601OD
725796
92626011005
6002-HRW16
EPA 3010A
725626
EPA 601OD
725796
92626011001
6002-HRW8
EPA 3005A
725456
EPA 6020B
725610
92626011002
6002-HRW9R
EPA 3005A
725456
EPA 6020B
725610
92626011003
6002-HRW14
EPA 3005A
725456
EPA 6020B
725610
92626011004
6002-HRW15
EPA 3005A
725456
EPA 6020B
725610
92626011005
6002-HRW16
EPA 3005A
725456
EPA 6020B
725610
92626011001
6002-HRW8
EPA 8260D
723786
92626011002
6002-HRW9R
EPA 8260D
723786
92626011003
6002-HRW14
EPA 8260D
723786
92626011004
6002-HRW15
EPA 8260D
723786
92626011005
6002-HRW16
EPA 8260D
723786
92626011006
TRIP BLANK
EPA 8260D
723786
92626011001
6002-HRW8
EPA 8260D Mod.
723674
92626011002
6002-HRW9R
EPA 8260D Mod.
723674
92626011003
6002-HRW14
EPA 8260D Mod.
723674
92626011004
6002-HRW15
EPA 8260D Mod.
723675
92626011005
6002-HRW16
EPA 8260D Mod.
723674
Date: 09/28/2022 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 30

� --vace
— -Effective-Date-0511-2f2i nOFY/12/2022---.-.--
Laboratory receiving samples:
-- Asheville M--. -Eden[Q—Greenwoa - Huntenville-P
Courier:
❑ Commercial
Client Nance:
red Ex LJUPS
Pace
❑Other.
—Rafe` h --MedraiMcsville ants nersvilt -_
Project #; W0 # • 92626011
nt II I l i l llll11111111111
92626011
Date Initials Person fxaminfnggrit�gt5;
p Bags- ❑None Q Other Biological Tissu F en?
Packing Material: — --- - ubble ultra Bubble
Thermometers ❑Yes ❑No S/A
IR Gun ID: — Type of ice: AllUet� ❑Blue — — -----
❑None
� Correction factor:
Cooler Temp: L 1 Add/subtract (°C) { 0Temp should be above freezing to 5°C
—�
Cooler Temp Corrected
L 7i t j []samples out of temp criteria. Samples on ice, cooling process
(° �- l
USDA Regulated Soil (l N/A, water sample) 5as6egvn
//
Did samples originate in a qulrantine zone within the United States: CA. NY, or SC Did samoles arieinntP frnm n fnrainn
(check maps)? VYes L�,JN6
including Hawaii and Puerto Ricai? [:]Yes. ffNo
Comments/Discrepancy-
Chain of Custody Present?
QYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
ElYes
[]No
❑N/A
2.
Short Hald Time Analysis (<72 hr.)?
Des
1940
❑N/A
3.
Rush Turn Around Time Requested?
Des
E94o
❑N/A
4.
Sufficient Volume?
�5es
❑No
[I N/A
5.
Correct Containers Used?
Y
❑No
❑N/A
6.
-Pace Containers Used?
��
�ld�'es
❑No
❑N/A
Containers [ntact?
Wes
[]No
❑N/A
7,
Dissolved ana€Ysis: Samples Field Filtered?
[]Yes
`BNo
❑N/A
8.
Sample Labels Match COC?
•\( Yes
[]No
❑N/A
9.
\JV 1
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VaA Vials (s5-6mm)?
(:]YesNa
r
N/A'
Trip Blank Present?
u4s
o01
fSJ�A
11.
Trip Blank Custody Seals Present?
❑yes
�fa
❑N/A
3
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: i7ate/Time:
Project Manager SCURF Review: Date:
P,n€art AA;;na.or ,Pr P—;,.....
Helo Data Required? VYes LJNo
O
Z�
Qualtrax ID: 69614 Page 1 of 2 Page 28 of 30

pace
Effective -Date, 05112/2a329S-f12-[2022
*Check mark top half of box if pH and/or dechlorination_ is verified and
with4n-the acceptance range for presm3tion samTfts. -- --
Exceptions: VOA, Coliform, TOC, Olt and Grease, ORO/8015 {water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project # IA� 92' 6� --
PM. MI4B Due Date: 09/29/22
CLIENT: 92—MECK CO
..
N
N
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--
- - -- --pN Adjustment Log for -Preserved Samples_
Sample Id
Type of Preservative
— -
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 9
�I-. 4V 1µ;1JCV G[ MICIC 0 d UI]LI Cold ftly d1leLLIII6 NW 111 Ldl Ulllld OJIIlrilldl 1L� 4011 IJJM7 , d WJJ'/ VI 11l ll;Ul III W]" UN $en[ to use North Carolina t]t NK t.ertificahon Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax R- 69614 Page 2 of 2
Page 29 of 30

D
m
m
m
TEMP In C
Received an
Ice
(YIN)
usti a y-
Sealed
Cooler
(YIN)
samnl—
ntact
(YIN)
o i. 1. 11 rn . IA
f
j ITEM #
�o�Eo��m�❑�
o u c W Y f p
o G
�ap�oN� a
�00
m
�E MATRIX COLE (see valid codes la left)
SAMPLE TYPE (G=GRAB C-COMP)
Y►
�,
�i
a
m
X0
Cn
O
n
>fy
n
a rM 1`6 No
°
�
m
z
m
°
�
O
m
SAMPLE TEMP AT COLLECTION
N OF CONTAINERS
Unpreserved
H25D4
�
HND3
N
HCI
n
R1
m
NaOH
Na252D3
�
N
Methanol
Other
Analyses Test
Y/N
6010I6020
VDC 8260
VCC 8260 SJIM (1.4-Oioxan
Trip BLANK
Residual Chlorine (YIN)
m a m0 a n 23 m
o w S a n
N G l4 �
a
b 3 �z N n �
N
N K
m a n
N
a x
w 3 p fp D
N �
c rn 3
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Page 30 of 30

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 28, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 25

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92626013001 6002-HRSW2
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626013002 6002-HRSW3
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626013003 6002-HRSW4
EPA 601 OD
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92626013004 TRIP BLANK
EPA 8260D
CL
52
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW2 Lab ID: 92626013001 Collected: 09/15/22 10:00 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 20:15
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:15
7440-41-7
Barium
45.6
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:15
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:15
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:15
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:15
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:15
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:15
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:15
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 20:15
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:15
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 20:15
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:15
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:15
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:15
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:44
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 00:41
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 00:41
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 00:41
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 00:41
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 00:41
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 00:41
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 00:41
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 00:41
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 00:41
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 00:41
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/20/22 00:41
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/20/22 00:41
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 00:41
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 00:41
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 00:41
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 00:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 00:41
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 00:41
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:41
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:41
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 00:41
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:41
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:41
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW2 Lab ID: 92626013001 Collected: 09/15/22 10:00 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:41
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:41
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:41
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/20/22 00:41
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/20/22 00:41
591-78-6
lodomethane
ND
ug/L
20.0
1
09/20/22 00:41
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/20/22 00:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/20/22 00:41
108-10-1
Styrene
ND
ug/L
1.0
1
09/20/22 00:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 00:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 00:41
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/20/22 00:41
127-18-4
Toluene
ND
ug/L
1.0
1
09/20/22 00:41
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/20/22 00:41
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/20/22 00:41
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/20/22 00:41
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/20/22 00:41
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/20/22 00:41
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/20/22 00:41
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/20/22 00:41
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/20/22 00:41
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/20/22 00:41
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/20/22 00:41
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
09/20/22 00:41
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/20/22 00:41
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
09/20/22 00:41
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/15/22 23:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
09/15/22 23:37
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 23:37
2037-26-5
Date: 09/28/2022 03:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW3 Lab ID: 92626013002 Collected: 09/15/22 08:50 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 20:20
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:20
7440-41-7
Barium
45.4
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:20
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:20
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:20
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:20
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:20
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:20
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:20
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 20:20
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:20
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 20:20
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:20
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:20
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:20
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:50
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 00:59
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 00:59
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 00:59
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 00:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 00:59
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 00:59
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 00:59
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 00:59
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 00:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 00:59
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/20/22 00:59
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/20/22 00:59
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 00:59
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 00:59
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 00:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 00:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 00:59
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 00:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:59
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 00:59
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 00:59
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/20/22 00:59
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW3 Lab ID: 92626013002 Collected: 09/15/22 08:50 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 00:59
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:59
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 00:59
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/20/22 00:59
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/20/22 00:59
591-78-6
lodomethane
ND
ug/L
20.0
1
09/20/22 00:59
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/20/22 00:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/20/22 00:59
108-10-1
Styrene
ND
ug/L
1.0
1
09/20/22 00:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 00:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 00:59
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/20/22 00:59
127-18-4
Toluene
ND
ug/L
1.0
1
09/20/22 00:59
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/20/22 00:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/20/22 00:59
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/20/22 00:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/20/22 00:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/20/22 00:59
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/20/22 00:59
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/20/22 00:59
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/20/22 00:59
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/20/22 00:59
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/20/22 00:59
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
09/20/22 00:59
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
09/20/22 00:59
17060-07-0
Toluene-d8(S)
100
%
70-130
1
09/20/22 00:59
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/15/22 23:57
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
09/15/22 23:57
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/15/22 23:57
2037-26-5
Date: 09/28/2022 03:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW4 Lab ID: 92626013003 Collected: 09/15/22 09:30 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
09/26/22 09:25
09/26/22 20:24
7440-38-2
Beryllium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:24
7440-41-7
Barium
43.3
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:24
7440-39-3
Cadmium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:24
7440-43-9
Chromium
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:24
7440-47-3
Copper
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:24
7440-50-8
Nickel
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:24
7440-02-0
Silver
ND
ug/L
10.0
1
09/26/22 09:25
09/26/22 20:24
7440-22-4
Lead
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:24
7439-92-1
Antimony
ND
ug/L
50.0
1
09/26/22 09:25
09/26/22 20:24
7440-36-0
Selenium
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:24
7782-49-2
Thallium
ND
ug/L
200
1
09/26/22 09:25
09/26/22 20:24
7440-28-0
Vanadium
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:24
7440-62-2
Zinc
ND
ug/L
20.0
1
09/26/22 09:25
09/26/22 20:24
7440-66-6
Cobalt
ND
ug/L
40.0
1
09/26/22 09:25
09/26/22 20:24
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
09/23/22 18:00
09/27/22 22:55
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/20/22 01:17
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/20/22 01:17
107-13-1
Benzene
ND
ug/L
1.0
1
09/20/22 01:17
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/20/22 01:17
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/20/22 01:17
75-27-4
Bromoform
ND
ug/L
1.0
1
09/20/22 01:17
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/20/22 01:17
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/20/22 01:17
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/20/22 01:17
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/20/22 01:17
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/20/22 01:17
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/20/22 01:17
75-00-3
Chloroform
ND
ug/L
1.0
1
09/20/22 01:17
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/20/22 01:17
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/20/22 01:17
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/20/22 01:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/20/22 01:17
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/20/22 01:17
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 01:17
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/20/22 01:17
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/20/22 01:17
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/20/22 01:17
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/20/22 01:17
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: 6002-HRSW4 Lab ID: 92626013003 Collected: 09/15/22 09:30 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
09/20/22 01:17
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 01:17
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/20/22 01:17
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/20/22 01:17
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 01:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/20/22 01:17
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/20/22 01:17
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/20/22 01:17
591-78-6
lodomethane
ND
ug/L
20.0
1
09/20/22 01:17
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/20/22 01:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/20/22 01:17
108-10-1
Styrene
ND
ug/L
1.0
1
09/20/22 01:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 01:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/20/22 01:17
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/20/22 01:17
127-18-4
Toluene
ND
ug/L
1.0
1
09/20/22 01:17
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/20/22 01:17
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/20/22 01:17
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/20/22 01:17
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/20/22 01:17
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/20/22 01:17
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/20/22 01:17
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/20/22 01:17
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
09/20/22 01:17
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
09/20/22 01:17
179601-23-1
o-Xylene
ND
ug/L
1.0
1
09/20/22 01:17
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
09/20/22 01:17
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
09/20/22 01:17
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
09/20/22 01:17
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
09/16/22 00:16
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
09/16/22 00:16
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
09/16/22 00:16
2037-26-5
Date: 09/28/2022 03:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: TRIP BLANK Lab ID: 92626013004 Collected: 09/15/22 08:25 Received: 09/15/22 16:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
09/19/22 18:19
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
09/19/22 18:19
107-13-1
Benzene
ND
ug/L
1.0
1
09/19/22 18:19
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
09/19/22 18:19
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/19/22 18:19
75-27-4
Bromoform
ND
ug/L
1.0
1
09/19/22 18:19
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/19/22 18:19
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
09/19/22 18:19
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
09/19/22 18:19
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
09/19/22 18:19
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/19/22 18:19
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/19/22 18:19
75-00-3
Chloroform
ND
ug/L
1.0
1
09/19/22 18:19
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/19/22 18:19
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
09/19/22 18:19
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/19/22 18:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/19/22 18:19
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/19/22 18:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 18:19
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/19/22 18:19
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
09/19/22 18:19
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
09/19/22 18:19
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
09/19/22 18:19
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
09/19/22 18:19
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:19
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:19
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
09/19/22 18:19
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
09/19/22 18:19
100-41-4
2-Hexanone
ND
ug/L
5.0
1
09/19/22 18:19
591-78-6
lodomethane
ND
ug/L
20.0
1
09/19/22 18:19
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
09/19/22 18:19
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
09/19/22 18:19
108-10-1
Styrene
ND
ug/L
1.0
1
09/19/22 18:19
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 18:19
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
09/19/22 18:19
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
09/19/22 18:19
127-18-4
Toluene
ND
ug/L
1.0
1
09/19/22 18:19
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
09/19/22 18:19
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
09/19/22 18:19
79-00-5
Trichloroethene
ND
ug/L
1.0
1
09/19/22 18:19
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
09/19/22 18:19
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
09/19/22 18:19
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
09/19/22 18:19
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
09/19/22 18:19
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
Sample: TRIP BLANK
Parameters
Lab ID: 92626013004 Collected: 09/15/22 08:25
Results Units Report Limit DF
Received: 09/15/22 16:05 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
09/19/22 18:19
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
09/19/22 18:19
179601-23-1
o-Xylene
ND ug/L
1.0
1
09/19/22 18:19
95-47-6
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
09/19/22 18:19
460-00-4
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
09/19/22 18:19
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
09/19/22 18:19
2037-26-5
Date: 09/28/2022 03:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
QC Batch: 725626 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92626013001, 92626013002, 92626013003
METHOD BLANK: 3780263 Matrix: Water
Associated Lab Samples: 92626013001, 92626013002, 92626013003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
50.0
09/26/2218:15
30.0
09/26/2218:15
10.0
09/26/2218:15
10.0
09/26/2218:15
10.0
09/26/2218:15
10.0
09/26/2218:15
40.0
09/26/2218:15
20.0
09/26/2218:15
20.0
09/26/2218:15
20.0
09/26/2218:15
40.0
09/26/2218:15
10.0
09/26/2218:15
200
09/26/2218:15
20.0
09/26/2218:15
20.0
09/26/2218:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3780264
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
960
96
80-120
Arsenic
ug/L
1000
983
98
80-120
Barium
ug/L
1000
985
98
80-120
Beryllium
ug/L
1000
1010
101
80-120
Cadmium
ug/L
1000
996
100
80-120
Chromium
ug/L
1000
1020
102
80-120
Cobalt
ug/L
1000
991
99
80-120
Copper
ug/L
1000
1010
101
80-120
Lead
ug/L
1000
988
99
80-120
Nickel
ug/L
1000
976
98
80-120
Selenium
ug/L
1000
996
100
80-120
Silver
ug/L
1000
986
99
80-120
Thallium
ug/L
1000
950
95
80-120
Vanadium
ug/L
1000
1070
107
80-120
Zinc
ug/L
1000
994
99
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDIFLL
92626013
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3780265
3780266
MS
MSD
92625613001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Arsenic
ug/L
ND
1000
1000
1050
1040
105
104
75-125
1
Barium
ug/L
101
1000
1000
1150
1150
105
105
75-125
0
Beryllium
ug/L
ND
1000
1000
1060
1060
106
106
75-125
1
Cadmium
ug/L
ND
1000
1000
1060
1070
106
107
75-125
1
Chromium
ug/L
ND
1000
1000
1060
1060
105
105
75-125
0
Cobalt
ug/L
ND
1000
1000
1030
1030
103
103
75-125
1
Copper
ug/L
ND
1000
1000
1080
1080
107
107
75-125
0
Lead
ug/L
ND
1000
1000
1030
1040
103
103
75-125
0
Nickel
ug/L
ND
1000
1000
1020
1010
102
101
75-125
1
Selenium
ug/L
ND
1000
1000
1040
1040
104
103
75-125
1
Silver
ug/L
ND
1000
1000
1030
1030
103
103
75-125
0
Thallium
ug/L
ND
1000
1000
996
989
99
99
75-125
1
Vanadium
ug/L
ND
1000
1000
1130
1130
112
112
75-125
0
Zinc
ug/L
31.1
1000
1000
1070
1070
104
104
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
QC Batch: 725456 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92626013001, 92626013002, 92626013003
METHOD BLANK: 3779489
Matrix:
Water
Associated Lab Samples: 92626013001, 92626013002, 92626013003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
09/27/22 21:32
LABORATORY CONTROL SAMPLE:
3779490
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
96.0
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3779491 3779492
MS MSD
92626011001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 92.8 93.6 93 93 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
QC Batch: 723786 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92626013001, 92626013002, 92626013003, 92626013004
METHOD BLANK: 3771336 Matrix: Water
Associated Lab Samples: 92626013001, 92626013002, 92626013003, 92626013004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,1-Trichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1,2-Trichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1-Dichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,1-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
1,2,3-Trichloropropane
ug/L
ND
1.0
09/19/22 17:43
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
09/19/22 17:43
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichlorobenzene
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloroethane
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloropropane
ug/L
ND
1.0
09/19/22 17:43
1,4-Dichlorobenzene
ug/L
ND
1.0
09/19/22 17:43
2-Butanone (MEK)
ug/L
ND
5.0
09/19/22 17:43
2-Hexanone
ug/L
ND
5.0
09/19/22 17:43
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/19/22 17:43
Acetone
ug/L
ND
25.0
09/19/22 17:43
Acrylonitrile
ug/L
ND
10.0
09/19/22 17:43
Benzene
ug/L
ND
1.0
09/19/22 17:43
Bromochloromethane
ug/L
ND
1.0
09/19/22 17:43
Bromodichloromethane
ug/L
ND
1.0
09/19/22 17:43
Bromoform
ug/L
ND
1.0
09/19/22 17:43
Bromomethane
ug/L
ND
2.0
09/19/22 17:43
Carbon disulfide
ug/L
ND
2.0
09/19/22 17:43
Carbon tetrachloride
ug/L
ND
1.0
09/19/22 17:43
Chlorobenzene
ug/L
ND
1.0
09/19/22 17:43
Chloroethane
ug/L
ND
1.0
09/19/22 17:43
Chloroform
ug/L
ND
1.0
09/19/22 17:43
Chloromethane
ug/L
ND
1.0
09/19/22 17:43
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/19/22 17:43
Dibromochloromethane
ug/L
ND
1.0
09/19/22 17:43
Dibromomethane
ug/L
ND
1.0
09/19/22 17:43
Ethylbenzene
ug/L
ND
1.0
09/19/22 17:43
lodomethane
ug/L
ND
20.0
09/19/22 17:43
m&p-Xylene
ug/L
ND
2.0
09/19/22 17:43
Methylene Chloride
ug/L
ND
5.0
09/19/22 17:43
o-Xylene
ug/L
ND
1.0
09/19/22 17:43
Styrene
ug/L
ND
1.0
09/19/22 17:43
Tetrachloroethene
ug/L
ND
1.0
09/19/22 17:43
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
METHOD BLANK: 3771336 Matrix: Water
Associated Lab Samples: 92626013001, 92626013002, 92626013003, 92626013004
Blank Reporting
Parameter Units Result Limit
Analyzed
Toluene
ug/L
ND
1.0
09/19/22 17:43
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/19/22 17:43
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/19/22 17:43
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
09/19/22 17:43
Trichloroethene
ug/L
ND
1.0
09/19/22 17:43
Trichlorofluoromethane
ug/L
ND
1.0
09/19/22 17:43
Vinyl acetate
ug/L
ND
2.0
09/19/22 17:43
Vinyl chloride
ug/L
ND
1.0
09/19/22 17:43
Xylene (Total)
ug/L
ND
1.0
09/19/22 17:43
1,2-Dichloroethane-d4 (S)
%
99
70-130
09/19/22 17:43
4-Bromofluorobenzene (S)
%
98
70-130
09/19/22 17:43
Toluene-d8 (S)
%
103
70-130
09/19/22 17:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3771337
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.0
96
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
44.8
90
70-130
1,1,2-Trichloroethane
ug/L
50
47.6
95
70-130
1,1-Dichloroethane
ug/L
50
47.7
95
70-130
1,1-Dichloroethene
ug/L
50
50.7
101
70-130
1,2,3-Trichloropropane
ug/L
50
44.2
88
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
47.0
94
70-131
1,2-Dibromoethane (EDB)
ug/L
50
48.2
96
70-130
1,2-Dichlorobenzene
ug/L
50
45.7
91
70-130
1,2-Dichloroethane
ug/L
50
46.5
93
70-130
1,2-Dichloropropane
ug/L
50
46.2
92
70-130
1,4-Dichlorobenzene
ug/L
50
44.0
88
70-130
2-Butanone (MEK)
ug/L
100
86.8
87
70-134
2-Hexanone
ug/L
100
91.4
91
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
92.4
92
70-130
Acetone
ug/L
100
87.1
87
70-133
Acrylonitrile
ug/L
250
232
93
70-130
Benzene
ug/L
50
46.7
93
70-130
Bromochloromethane
ug/L
50
47.6
95
70-130
Bromodichloromethane
ug/L
50
45.5
91
70-130
Bromoform
ug/L
50
49.2
98
70-130
Bromomethane
ug/L
50
47.6
95
45-151
Carbon disulfide
ug/L
50
53.7
107
70-130
Carbon tetrachloride
ug/L
50
51.9
104
70-130
Chlorobenzene
ug/L
50
46.6
93
70-130
Chloroethane
ug/L
50
52.0
104
39-152
Chloroform
ug/L
50
47.5
95
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 25

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
LABORATORY CONTROL SAMPLE:
Parameter
3771337
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
50
48.2
96
58-130
cis-1,2-Dichloroethene
ug/L
50
47.0
94
70-130
cis-1,3-Dichloropropene
ug/L
50
49.1
98
70-130
Dibromochloromethane
ug/L
50
47.0
94
70-130
Dibromomethane
ug/L
50
51.3
103
70-130
Ethylbenzene
ug/L
50
46.7
93
70-130
lodomethane
ug/L
100
111
111
53-141
m&p-Xylene
ug/L
100
92.1
92
70-130
Methylene Chloride
ug/L
50
47.4
95
66-130
o-Xylene
ug/L
50
46.3
93
70-130
Styrene
ug/L
50
47.4
95
70-130
Tetrachloroethene
ug/L
50
46.4
93
70-130
Toluene
ug/L
50
46.2
92
70-130
trans-1,2-Dichloroethene
ug/L
50
49.3
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.0
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
45.9
92
57-185
Trichloroethene
ug/L
50
49.4
99
70-130
Trichlorofluoromethane
ug/L
50
46.1
92
62-130
Vinyl acetate
ug/L
100
98.1
98
70-144
Vinyl chloride
ug/L
50
48.0
96
62-130
Xylene (Total)
ug/L
150
138
92
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
3771338
Units
92626011001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
22.3
112
70-141
1,1,1-Trichloroethane
ug/L
ND
20
25.6
128
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
21.1
105
69-142
1,1,2-Trichloroethane
ug/L
ND
20
22.8
114
70-138
1,1-Dichloroethane
ug/L
ND
20
23.9
118
70-150
1,1-Dichloroethene
ug/L
ND
20
27.2
136
70-156
1,2,3-Trichloropropane
ug/L
ND
20
21.0
105
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.8
109
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
22.8
114
70-138
1,2-Dichlorobenzene
ug/L
ND
20
21.9
110
70-141
1,2-Dichloroethane
ug/L
ND
20
21.8
109
69-143
1,2-Dichloropropane
ug/L
ND
20
23.3
117
68-156
1,4-Dichlorobenzene
ug/L
ND
20
21.4
107
70-142
2-Butanone (MEK)
ug/L
ND
40
45.5
114
60-157
2-Hexanone
ug/L
ND
40
43.5
109
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
45.4
114
70-141
Acetone
ug/L
ND
40
42.9
107
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 25

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
MATRIX SPIKE SAMPLE:
Parameter
3771338
Units
92626011001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
111
111
69-147
Benzene
ug/L
ND
20
23.3
116
70-142
Bromochloromethane
ug/L
ND
20
23.5
117
70-146
Bromodichloromethane
ug/L
ND
20
22.3
111
70-139
Bromoform
ug/L
ND
20
22.0
110
64-140
Bromomethane
ug/L
ND
20
26.1
131
28-192
Carbon disulfide
ug/L
ND
20
26.3
132
70-151
Carbon tetrachloride
ug/L
ND
20
25.4
127
70-148
Chlorobenzene
ug/L
ND
20
22.3
111
70-141
Chloroethane
ug/L
ND
20
28.4
142
58-191
Chloroform
ug/L
ND
20
23.9
120
70-148
Chloromethane
ug/L
ND
20
24.6
123
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
24.1
119
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
22.2
111
70-139
Dibromochloromethane
ug/L
ND
20
21.2
106
70-144
Dibromomethane
ug/L
ND
20
23.8
119
70-139
Ethylbenzene
ug/L
ND
20
22.5
113
70-143
lodomethane
ug/L
ND
40
47.2
118
35-171
m&p-Xylene
ug/L
ND
40
44.0
110
70-144
Methylene Chloride
ug/L
ND
20
24.1
121
62-149
o-Xylene
ug/L
ND
20
21.7
108
70-145
Styrene
ug/L
ND
20
22.1
110
70-143
Tetrachloroethene
ug/L
ND
20
22.7
113
70-145
Toluene
ug/L
ND
20
23.2
116
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
26.1
130
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
22.5
112
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
17.8
89
51-159
Trichloroethene
ug/L
ND
20
25.4
127
62-146
Trichlorofluoromethane
ug/L
ND
20
27.3
136
63-153
Vinyl acetate
ug/L
ND
40
46.9
117
61-162
Vinyl chloride
ug/L
ND
20
24.3
121
61-163
Xylene (Total)
ug/L
ND
60
65.6
109
70-143
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
93
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 3771339
Parameter
Units
92626011003
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
SAMPLE DUPLICATE: 3771339
Parameter
Units
92626011003
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
.61J
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
91
92
4-Bromofluorobenzene (S)
%
94
95
Toluene-d8 (S)
%
102
98
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/28/2022 03:40 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
QC Batch: 723675 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92626013001, 92626013002, 92626013003
METHOD BLANK: 3770826
Matrix:
Water
Associated Lab Samples:
92626013001, 92626013002, 92626013003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
09/15/22 15:02
1,2-Dichloroethane-d4 (S)
%
97
70-130
09/15/22 15:02
Toluene-d8 (S)
%
102
70-130
09/15/22 15:02
LABORATORY CONTROL SAMPLE: 3770827
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.3 91 70-130
1,2-Dichloroethane-d4 (S) % 100 70-130
Toluene-d8 (S) % 106 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3770828
3770829
MS
MSD
92625809043 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 341 100
100
441
420 100
79
63-136 5
1,2-Dichloroethane-d4 (S)
%
93
95
70-130
Toluene-d8(S)
%
91
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 6002 HOLBROOKS RD LANDIFLL
Pace Project No.: 92626013
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
6002 HOLBROOKS RD LANDFILL
92626013
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92626013001
6002-HRSW2
EPA 3010A
725626
EPA 6010D
725796
92626013002
6002-HRSW3
EPA 3010A
725626
EPA 6010D
725796
92626013003
6002-HRSW4
EPA 3010A
725626
EPA 6010D
725796
92626013001
6002-HRSW2
EPA 3005A
725456
EPA 6020B
725610
92626013002
6002-HRSW3
EPA 3005A
725456
EPA 6020B
725610
92626013003
6002-HRSW4
EPA 3005A
725456
EPA 6020B
725610
92626013001
6002-HRSW2
EPA 8260D
723786
92626013002
6002-HRSW3
EPA 8260D
723786
92626013003
6002-HRSW4
EPA 8260D
723786
92626013004
TRIP BLANK
EPA 8260D
723786
92626013001
6002-HRSW2
EPA 8260D Mod.
723675
92626013002
6002-HRSW3
EPA 8260D Mod.
723675
92626013003
6002-HRSW4
EPA 8260D Mod.
723675
Date: 09/28/2022 03:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 25

-pace
s fx�}r-U.Sf:�:Fz
Laboratory receiving samples:
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Client Name:
nwrc[
r[ ra lc6[ra n, ,ruleI MU01ILd mr-myrsmupei----- ---
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Courier: =
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❑ Commercial
❑Pace
❑other:
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Date Initials Person Exalnin€ngf:nntents,
P'ackirtg Material -
bhre'Wrap
❑Bubble Bags []None Q
Other
Biological Tissue Frozen?
Thermometer:
— --
[]Yes [f No ❑N/A
EJKGun IU: I v ka I Type of Ice: et ❑slue ❑hone
%rectionFactor:
Cooler Temp: --J , ind/Stabtbtract (°C) O Temp should be above freezing to 5°C
L l []Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C U . has begun
USDA Regulated Soil ( Q1A, wat "sample)
Did samples originate in a qua ntine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (€Wationally,
(check maos)? MYes N.M -- r,.._-
Comments/Discrepancy:
Chain of Custody Present?
a
❑No
❑N/A
1,
Samples Arrived within Hold Time?
es
ON,
❑N/A
2.
Short bold Time Arralys€s (<72 hr.)?
❑Yes
Na
[I N/A
3.
Rush Turn Around Time Requested?
❑Yes
a
❑N/A
4.
Sufficient Volume?
Yes
El No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
\Erfes
"Ig�es
❑No
[:]No
[]N/A
❑N/A
6.
Containers Intact?
es
❑No
❑N/A
3.
Dissolver! analysis: Samples Field Filtered?
❑Yes
o
❑N/A
S.
Sample Labels Match C©C?
-includes Date/Time/ID/Analysis Matrix:
es
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑yet
o
[]N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
es
❑Yes
[]No
❑N/A
❑N/A
11.
t
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Persori contacted: �- - -- -� Date/Time:
Project Manager SCURF Review:
¢roiPet N1;;0;4uRr SAF Rwui�...•
Date:
Field Data Required? ❑Yes []No
Qualtrax ID: 69614 Page 1 of 2 Page 23 of 25

' Vace
412;ii:jj IUM
-Effective Date: 05/12/202-205/12/2022
*Check mark top half of box if pH and/or dech[orina#ion is verified and Project # WOlt • 9L,V�1 3 _
wit-hirt-the-accePtarrcerange orpreservatfe>�t ptcss- — - ----- PM: MWB Due Date: 09/29/22
Exceptlons: VOA, Cvli€arm, TOC, Oil and Grease, DRO/8015 (waterl DOC, LLHg CLIENT : 92-MECK CO
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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— pH Adjustment Log for Preserved- Samples --
Sample ID
Type of Preservative
---
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
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added
Lot 4
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.. •...— — ... I— a ����� c�.uray uue�aius rvw,i� wiui�uu wniyuuu�.: �euiTsu, a �uNY UI LIII� 1Vi i WIII UBSent to the North Carolina OENR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 24 of 25

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Page 25 of 25