Alamac_Lumberton_Annual_GW_Monitoring

%S.I.tions-IES
Industrial & Environmental Services
1101 Nowell Rd.
Raleigh, NC 27607
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TRANSMITTAL
To: Lisa Taber From: M. Tony Lieberman
Fax: Pages Report
Phone: [phone] Date: January 28, 2011
2010 Annual Groundwater Monitoring Mark Cabral, Alamac American
Re: Report CC: Sean Boyles, FRO
Alamac American Knits, LLC File
Lumberton, NC
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Dear Lisa:
Enclosed please find the 2010 Annual Groundwater Monitoring Report submitted on behalf of Alamac American
Knits in Lumberton, NC. This is the fifth report submitted in accordance with the Brownfields Agreement signed
February 24, 2006. If you have any comments or questions, please contact me.
• Signature:
• Date: January 28, 2011

2010 ANNUAL GROUNDWATER
MONITORING REPORT
ALAMAC AMERICAN KNITS LLC
1885 ALAMAC ROAD
LUMBERTON, ROBESON COUNTY,
NORTH CAROLINA 28359
BROWNFIELDS PROJECT NO. 06001-02-78
GROUNDWATER INCIDENT No. 18926
Latitude N 341 35.2751
Longitude W 791 00.3231
Prepared for:
Alamac American Knits LLC
1885 Alamac Road (P.O. Box 1347)
Lumberton, North Carolina 28359
Prepared by:
Solutions-IES, Inc.
1101 Nowell Road
Raleigh, NC 27607
Phone: [phone]; Fax [phone]
www.solutions-ies.com
Solutions-IES Project No. 1000.02A3.AAKL
January 2011
Sean Jarvah
Environmental Specialist
M. Tony Lieberman
Senior Environmental Manager

TABLE OF CONTENTS
SECTION
PAGE
1.0
INTRODUCTION............................................................................................................... 1
2.0
BACKGROUND..................................................................................................................1
3.0
GROUNDWATER RECOVERY SYSTEM OPERATION & MAINTENANCE ....... 2
3.1 HYDRAULIC PERFORMANCE...........................................................................................2
3.2 VOLATILE ORGANIC COMPOUND REMOVAL AND DISPOSAL................................2
4.0
ENVIRONMENTAL MONITORING.............................................................................. 3
4.1 SOURCE AREA GROUNDWATER.....................................................................................3
4.2 RESIDENTIAL WATER SUPPLY WELL............................................................................4
5.0
CONCLUSIONS..................................................................................................................4
6.0
REFERENCES.................................................................................................................... 6
TABLES
Table 3-1 Operational Data Summary for Groundwater Recovery Wells
Table 3-2 Historical Summary of Volatile Organic Compounds in Groundwater from Recovery
Wells
Table 3-3 Historical Summary of Volatile Organic Compounds in On -Site Wastewater Treatment
Plant Effluent
Table 4-1 Historical Summary of Selected Bio-geochemical Parameters in Groundwater
FIGURES
Figure 1
Site Location
Figure 2
Facility Layout and Groundwater Sampling Locations
Figure 3
Chlorinated Ethene Concentrations in RW-1
Figure 4
Chlorinated Ethene Concentrations in RW-2
Figure 5
Chlorinated Ethene Concentrations in RW-3
APPENDICES
Appendix A Laboratory Analytical Reports
Appendix B Field Notes
T:\Project FilesWlamac\1000.02A3.AAK\Monitoring Reports\December 2010 Mon Rpt\Annual Report Draft-2010.doc
ii

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
1.0 INTRODUCTION
This 2010 Annual Groundwater Monitoring Report has been prepared by Solutions-IES, Inc. for the
North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste
Management (DWM), Brownfields Program, on behalf of Alamac American Knits LLC (Alamac),
Lumberton, North Carolina. This is the fifth annual report prepared in accordance with the Brownfields
Agreement (BFA) entered into by the NCDENR and Alamac on February 24, 2006.
2.0 BACKGROUND
The Alamac facility is located in Lumberton, Robeson County, North Carolina (Figure 1). A current
facility layout with groundwater sampling locations is shown in Figure 2. Until the December 2006
Groundwater Monitoring Report, previous reports were prepared in accordance with the Water Quality
Monitoring Plan (WQMP) originally submitted to the NCDENR, Division of Water Quality (DWQ),
Aquifer Protection Section (APS; formerly the Groundwater Protection Section), Fayetteville Regional
Office (FRO), approved on August 16, 1999 and modified January 29, 2001. Based on the requirements
of the WQMP, quarterly sampling and semi-annual reporting were maintained through the first quarter of
2004. On June 7, 2004, quarterly sampling was reduced to annual sampling and reporting. Sampling and
reporting proceeded under these guidelines until the approval of the Brownfields Agreement in February
2006.
This 2010 Annual Groundwater Monitoring Report includes the monitoring activities during the annual
groundwater sampling event completed November 2, 2010. On September 18, 2008, Ms. Lisa Taber of
the Brownfields Program agreed to further reduce the number of wells being sampled by eliminating the
requirement to collect samples from source area wells MW-1, MW-I I and MW-15, downgradient well
MW-23, and offsite well MW-19 (Figure 2). This report documents the sampling and analysis of the
three recovery wells (RW-1, RW-2 and RW-3) and one offsite residential water supply well at 2237
Alamac Rd. which comprise the remaining monitoring program.

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
3.0 GROUNDWATER RECOVERY SYSTEM OPERATION & MAINTENANCE
3.1 HYDRAULIC PERFORMANCE
Except for the pump for RW-2 being down for two days in May, the groundwater recovery system
operated without interruption during 2010. Alamac plant personnel periodically inspected the three
recovery wells that comprise the groundwater extraction system and recorded system performance
measurements including the pumping rate and the cumulative volume of groundwater recovered from
each well. Historical and current operational data through December 31, 2010 are presented in Table 3-1.
Extraction flow rates during 2010 were recorded in two ways: (1) from instantaneous flow rate readings
taken off meters assigned to each recovery well, and (2) by dividing the totalizer flow meter reading for
each well by the number of days (converted to minutes) of operation (i.e., average annual flow rate). As
shown in Table 3-1, during the 2010 reporting period covered by this report, the average flow rate for
RW-1 was 1.53 gallons per minute (gpm); the average flow rate in extraction well RW-2 was calculated
to be 1.40 gpm; and the average flow rate from extraction well RW-3 was 8.46 gpm. From startup in
1999 through December 31, 2010, approximately 61.6 million gallons of groundwater have been
extracted, discharged and treated in the on -site wastewater treatment plant (WWTP). That is an increase
of 5.7 million gallons from last year. Both the instantaneous and average annual recovery rates at each
well in 2010 are similar to those recorded in preceding years indicating consistent and continued
operation throughout the reporting period.
3.2 VOLATILE ORGANIC COMPOUND REMOVAL AND DISPOSAL
A summary of the historical VOC data including the November 2010 samples collected from the three
recovery wells is provided in Table 3-2. The laboratory analytical report for the November 2, 2010
sampling event is provided in Appendix A.
To estimate the mass of volatile organic compounds (VOCs) removed from the groundwater via the
recovery system, the volume of water extracted from each well was multiplied by the concentration of
total VOCs in the recovered groundwater from that well. During the 2010 reporting period from
December 31, 2009, through the sampling date of November 2, 2010, approximately 175 lbs (80 kg) of
VOCs were removed from the groundwater. Individually, since pumping began, RW-1 has collected and
2

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
discharged 378 lbs (172 kg); RW-2 has collected and discharged 1,103 lbs (500 kg); and RW-3 has
extracted and discharged 1,262 lbs (572 kg) of VOCs. Altogether since pumping began, a conservative
estimate of approximately 2,743 lbs (1,244 kg) of VOCs have been removed from the treatment area via
the recovery well network.
The groundwater recovered from the three recovery wells is discharged directly to the on -site WWTP.
Alamac operates this WWTP under an NPDES permit and monitors the effluent quality at the outfall in
accordance with the permit. Although no sampling of the outfall was required by the WQMP or is
currently required under the Brownfields Agreement, effluent samples from the WWTP have been
monitored since 1999. Alamac provided Solutions-IES with the wastewater analyses on samples
collected on March 2, June 8, September 14, and December 14, 2010. No tetrachloroethene (PCE),
trichloroethene (TCE), cis-1,2-dichloroethene (cis-1,2-DCE) or vinyl chloride (VC) were detected in the
WWTP effluent (Table 3-3). Copies of the WWTP effluent analytical reports for the reporting period are
provided in Appendix A.
4.0 ENVIRONMENTAL MONITORING
4.1 SOURCE AREA GROUNDWATER
The groundwater sampling protocol for the November 2010 sampling event included sampling the three
recovery wells (RW-1, RW-2 and RW-3) for VOCs and bio-geochemical parameters' and the water
supply well located at 2237 Alamac Road for VOCs. Samples from recovery wells RW-1, RW-2 and
RW-3 were collected directly from sampling ports located on the former treatment system pad.
Temperature, pH, specific conductivity, oxidation-reduction potential (ORP) and dissolved oxygen (DO)
were measured in the field (see Field Notes in Appendix B). The samples were collected in laboratory -
supplied glassware, packaged and shipped under chain -of -custody control to Prism Laboratories, Inc. in
Charlotte, NC. Samples were analyzed for VOCs by Method 8260B.
The summary of historical groundwater bio-geochemical parameter data shown in Table 4-1 indicates
that there is little change in the pH, conductivity and DO parameters compared to 2009; the ORP values
' Bio-geochemical parameter analysis includes field measurements of temperature, pH, conductivity, oxidation-
reduction potential (ORP) and dissolved oxygen (DO).

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
have continued to drop since 2007. A summary of the historical VOC data, including the November 2010
samples, is provided in Table 3-2. Graphs depicting the historical concentrations of PCE, TCE, cis-1,2-
DCE, VC and total VOCs in RW-1, RW-2 and RW-3 are provided in Figures 3, 4, and 5, respectively.
The 15A NCAC 2L.0202 Groundwater Standards (NC 2L Standards) were updated in January 2010. 1,1-
DCA changed from 70 µg/L to 6 µg/L and vinyl chloride changed from 0.015 µg/L to 0.03 µg/L. These
changes had little effect on the reporting criteria required for Alamac. In RW-1, there has been little
change to the concentrations of the target chlorinated ethenes over time, with concentrations being
significantly over the NC 2L Standards. RW-2 has shown decreasing levels of cis-1,2-DCE, while levels
of the other target constituents have remained relatively unchanged and above NC 2L Standards. In RW-
3, there is evidence that most of the PCE and TCE have been removed though TCE concentrations still
remain above the NC 2 Standard of 3.0 µg/L. Concentrations of cis-1,2-DCE and vinyl chloride have
changed little since last reporting period and still remain well above the 2L Standards.
4.2 RESIDENTIAL WATER SUPPLY WELL
The residential water supply well located at 2237 Alamac Road (State Route 2289) was sampled on
November 2, 2010. The spigot closest to the well house was opened and water was allowed to flow for
approximately 20 minutes. The property owner stated she only uses the water for her garden and she is
connected to a municipal water source. After the bio-geochemical parameters were measured and
recorded in the field book, a water sample was collected directly into laboratory -supplied glassware. The
sample was submitted to Prism Laboratories under chain -of custody procedures for analysis of VOCs by
EPA Method 8260.
No VOCs were detected above the laboratory method detection limits. The data are summarized in Table
3-2 and Table 4-1. The laboratory report is included in Appendix A. The VOC data were transmitted
separately via email to Ms. Lisa Taber of the Brownfields Program on January 7, 2011.
5.0 CONCLUSIONS
The groundwater recovery and discharge system is the only remediation approach that is still active in the
source area. It continues to effectively capture and remove contamination from the aquifer. Reductions
in concentrations do appear to be continually occurring, particularly in the vicinity of RW-2, likely a
result of the combination of limited in situ bioactivity and physical extraction by pumping.
4

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
Concentrations of chlorinated solvents appear to have changed little in RW-3, as seen in Figure 5 of the
report. RW-1 continues to effectively extract VOCs, but concentrations do not appear to be decreasing as
consistently seen in RW-2. Based on the volume of groundwater extracted and the concentrations
measured in the recovered water over time, it has been estimated that the recovery system has removed
approximately 2,743 lbs (1,244 kg) of VOCs since its installation in November 1999. Combined with the
removal of an estimated initial 732 lbs (332 kg) of VOCs via the other remediation activities that were
implemented (Ref. 2), the total amount of VOCs physically removed from the site now is calculated to be
approximately 3,475 lbs (1,576 kg).

2010 Annual Groundwater Monitoring Report Solutions-IES Project No. 1000.02A3.AAKL
Alamac American Knits LLC, Lumberton, NC January 20, 2011
6.0 REFERENCES
1. Proposed Remedial Action Report, S&ME, Inc., April 1999.
2. Report of Excavation and Disposal of PCE-Contaminated Soil, Soil Solutions, Inc., April 1999.
3. Water Quality Monitoring Plan, S&ME, Inc., July 1999.
4. Injection Well Permit Application, S&ME, Inc., September 29, 1999.
5. Groundwater Monitoring Report, S&ME, Inc., March 28, 2000.
6. Groundwater Monitoring Report, S&ME, Inc., September 5, 2000.
7. Groundwater Monitoring Report, S&ME, Inc., February 2, 2001.
8. Evaluation Report for Injection of Liquid Soybean Oil, S&ME, Inc., March 21, 2001.
9. Groundwater Monitoring Report, Solutions-IES, June 2001.
10. Groundwater Monitoring Report, Solutions-IES, December 2001
11. Groundwater Monitoring Report, Solutions-IES, June 2002
12. Groundwater Monitoring Report, Solutions-IES, December 2002
13. Groundwater Monitoring Report, Solutions-IES, June 2003
14. Groundwater Monitoring Report, Solutions-IES, December 2003
15. Groundwater Monitoring Report, Solutions-IES, December 2004
16. Groundwater Monitoring Report, Solutions-IES, December 2005
17. Groundwater Monitoring Report, Solutions-IES, December 2006
18. Groundwater Monitoring Report, Solutions-IES, December 2007
19. Brownfields Agreement between NCDENR and Alamac American Knits, LLC, February 24, 2006
20. Groundwater Monitoring Report, Solutions-IES, December 2008
21. Groundwater Monitoring Report, Solutions-IES, December 2009
0

TABLES

TABLE 3-1
OPERATIONAL DATA SUMMARY
FOR GROUNDWATER RECOVERY WELLS
ALAMAC AMERICAN KNITS
LUMBERTON, NORTH CAROLINA
Date
Days of
Operation
Recovery Well Data
Flow Rates
m
Cumulative Volume al
RW-1
RW-2
RW-3
Total from all
RWs
RW-1
RW-2
RW-3
Total from
all RWs
11/8/1999
0
5.14
4.59
10.31
20.0
583
728
1,584
2,895
12/29/1999
51
1.89
3.30
12.77
18.0
111,166
158,258
793,114
1,062,538
8/24/2000
290
1.61
1.30
11.57
14.5
442,666
409,627
4,979,515
5,831,808
12/31/2001
784
1.59
1.14
8.65
11.4
1,381,075
752,965
11,047,359
13,181,399
12/30/02
1148
1.97
1.31
8.15
11.4
2,094,174
1,188,524
15,490,630
18,773,328
12/29/O3
1512
2.68
0.68
7.76
11.1
3,074,928
1,591,610
19:527,601
24,194,139
11/01/04
1820
2.66
0.55
7.68
10.9
3,865,038
1,928,465
22,797,606
28,591,109
12/01/05
2215
2.25
1.O1
7.60
10.9
4,834,285
2,390,003
27,092,242
34,316,530
. Instantaneous
Flow
0.92
Rate Reading
7.63
(gpm) - 2005
10.9
Avg.
1.70
Flow Rate (gpm)
0.82
for year 2005
7.57
10.1
O1/O1/06
2246
2.26
1.13
7.65
11.0
4,906,556
2,428,642
27,432,044
34,767,242
02/01/06
2277
2.14
0.77
7.51
10.4
4,976,734
2,469,077
27,769,328
35,215,139
03/01/06
2305
2.24
0.89
7.66
10.8
5,039,501
2,504,908
28,071,261
35,615,670
04/01/06
2336
2.12
0.96
7.31
10.4
5,109,765
2,544,739
28,404,594
36,059,098
05/01/06
2366
2.04
0.92
7.44
10.4
1 5,173,575
2,583,622
28,725,059
36,482,256
06/01/06
2397
2.01
0.81
7.54
10.4
5,239,225
2,623,007
29,058,935
36,921,167
07/01/06
2427
2.03
0.77
7.53
10.3
5,301,167
2,657,337
29,385,817
37,344,321
08/01/06
2458
2.00
1.15
7.29
10.4
5,364,078
2,704,834
29,706,813
37,775,725
09/01/06
2489
1.90
1.24
7.83
11.0
5,427,190
2,756,752
30,039,212
38,223,154
10/01/06
2519
1.84
1.30
6.84
10.0
5,486,630
2,810,648
N 59,269
38,656,547
11/01/06
2550
1.80
1.35
6.95
10.1
5,544,423
2,869,432
3Q,654,815
39,068,670
12/O1/06
2580
1.79
1.43
4.47
7.7
5,601,019
1 2,930,821
30,964,147
39,495,987
Avg. Instantaneous Flow Rate Reading (gpm) - 2006
Avg. Flow Rate (gpm)
for year 2006
2.01
1.06
7.17
10.24
1.46
L01
7.36
9.83
O1/01/07
2611
170
1.24
7.48
10.4
5,656,490
2,993,572
31,296,714
39,946,776
02/O1/07
2642
197
1.79
7.45
11.2
5,710,307
3,056,307
31,631,715
40,398,329
03/O1/07
2670
195
1.51
7.75
11.2
5,764,398
3,122,557
31,952,676
40,839,631
04/O1/07
2701
2.18
1.42
7.82
11.4
5,820,482
3,182,525
32,292,556
41,295,563
05/01/07
2731
2.11
1.33
7.72
11.2
5,876,996
3,242,042
32,617,275
41,736,313
06/01/07
2762
196
1.31
8.21
11.5
5,936,332
3,301,030
32,971,841
42,209,203
07/01/07
2792
225
1.26
7.67
11.2
5,998,552
3,358,354
33,320,050
42,676,956
08/01/07
2823
333
1.37
6.53
11.2
6,061,356
3,415,969
33,675,880
43,153,205
09/01/07
2854
324
1.19
8.60
13.0
6,118,403
3,473,983
33,991,754
43,584,140
10/01/07
2884
2.86
1.50
7.47
11.8
6,156,864
3,537,236
34,301,745
43,995,845
11/01/07
2915
1,15
1.31
7.92
10.4
6,189,583
3,596,820
34,647,851
44,434,254
12/O1/07
2945
1,44
1.33
8.09
10.9
6,226,814
3,656,987
34,991,546
44,875,347
Avg. Instantaneous
Flow
Rate Reading
(gpm) - 2007
Avg.
Flow Rate (gpm)
for year 2007
2.18
1.38
7.73
11.28
1.19
1.38
7.66
10.23
O1/01/08
2976
1,35
1.31
8.21
10.9
6,273,407
3,711,140
35,355,359
45,339,906
02/01/08
3007
1.04
1.29
8.09
10.4
6,315,604
3,768,421
35,721,621
45,805,646
03/01/08
3036
1.06
1.52
8.40
11.0
6,347,156
3,832,245
36,065,183
46,244,584
04/01/08
3067
1.14
1.49
8.21
10.8
6,386,099
3,894,496
36,427,110
46,707,705
05/01/08
3097
1.61
1.20
8.03
10.8
6,429,563
3,954,158
36,781,739
47,165,460
06/01/08
3128
1.30
1.16
8.03
10.5
6,473,286
3,996,678
37,141,152
47,611,116
07/01/08
3158
1.38
1 1.21
7.85
10.4
6,515,123
4,046,569
37,482,315
48,044,007
08/01/08
3189
1.37
1.35
8.34
11.1
6,557,474
410,420
37,844,761
44,812,655
09/01/08
3220
1.58
1.41
8.04
11.0
6,598,577
4,157,110
38,198,263
48,953,950
10/O1/08
3250
1.67
1.29
8.18
11.1
6,647,701
4,215,247
38,549,475
49,412,423
11/O1/08
3281
1.37
1.33
7.37
10.1
6,696,147
4,275,071
38,907,703
49,878,921
Avg. Instantaneous Flow Rate Reading
(gpm) - 2008
Avg. Flow Rate (gpm)
for year 2008
1.35
1.32
8.07
10.74
0.97
1.28
8.09
10.34
O1/O1/09
3342
1.26
1.67
8.31
11.2
6,780,442
4,415,221
39,619,425
50,815,088
02/O1/09
3373
1.12
0.04 *
8.09
9.2
6,817,519
39,987,306
4,462,479
51,267,304
03/01/09
3401
1.45
1.45
7.99
10.9
6,858,717
4,469,689
40,307,995
51,636,401
04/01/09
3432
1.69
1.34
8.21
11.2
6,906,810
4,531,274
40,675,204
52,113,288
05/01/09
3462
1.59
1.44
7.90
10.9
6,960,590
4,596,433
41,021,973
52,578,996
06/01/09
3493
1.60
1.50
8.20
11.3
7,012,912
4,658,947
41,384,503
53,056,362
07/01/09
3523
1.52
1 1.44
8.37
11.3
7,060,195
4,720,380
41,734,467
53,515,042
08/01/09
3554
1.46
1.40
8.65
11.5
7,108,916
4,785,146
42,120,638
54,014,700
09/O1/09
3181
1.41
1.35
8.24
11.0
7,154,835
4,847,456
42,484,264
54,486,555
10/Ol/09
3615
1.47
1.43
9.35
12.3
7,198,509
4,908,096
42,846,434
54,953,039
11/01/09
3646
1.47
1.46
8.19
ILI
7,246,374
4,973,650
43,232,861
55,452,885
12/01/09
3676
1.47
1.46
8.50
11.4
7,293,768
5,036,556
43,575,328
55,905,652
Avg. Instantaneous Flow Rate Reading
(gpm) - 2009
Avg. Flow Rate (gpm)
for year 2009
1.46
1.45
8.33
11.09
1.24
1.57
9.65
12.46
01/01/10
3707
1.45
1.40
8.60
11.5
7,342,062
5,100,890
43,955,425
56,398,377
02/O1/10
3738
1.37
1.47
8.51
11.4
7,388,086
5,165,365
44,334,467
56,887,918
03/01/10
3766
1.71
1.99
8.92
12.6
1 7,425,792
5,225,243
44,661,950
57,312,985
04/01/10
3797
1.43
1.33
8.31
11.1
7,464,876
5,287,751
45,042,637
57,795,264
05/01/10
3827
1.52
1.29
7.45
10.3
7,508,624
5,345,077
45,400,963
58,254,664
06/01/10
3858
1.55
1.33
8.50
11.4
7,559,139
5,392,209
45,742,796
58,694,144
07/01/10
3888
1.60
1.43
8.37
11.4
7,608,764
5,450,720
46,103,208
59,162,692
08/01/10
3919
1.32
1.37
8.41
11.1
7,656,330
5,510,839
46,467,111
59,634,280
09/01/10
1 3950
1 1.71
1.27
9.61
12.6
7,702,429
5,568,519
46,852,245
60,123,193
10/O1/10
3980
1.64
1.30
7.55
10.5
7,734,455
5,623,672
47,246,402
60,624,529
11/01/10
4011
1.55
1.32
9.23
12.1
7,806,155
5,682,554
47,632,579
61,121,288
12/01/10
4041
1.23
1.26
8.00
10.5
,,10
5,733,056
47,986,685
61,563, 751
Avg. Instantaneous Flow Rate Reading (up.) _ 27�.
Avg. Flow Rate (gpm)
foryear 2010
1.53 1 1.40 8.46 1 11.44
1.24 1 1.57
19.83
12.63
Kw-L was down L> anys in rwmary Loov. i, iow rate is averaged for tnai
month.
Page 1 of 1

TABLE 3-2
HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER FROM RECOVERY WELLS
ALAMAC AMERICAN KNITS
LUMBERTON, NORTH CAROLINA
Well ID
Sample Date
Days
after
Startup
Tetrachloroethene
(u /L)
Trichloroethene
(u /L)
1,1,1-
Trichloroethane
(u /L)
1,1,2-
Trichloroethane
(u /L)
1,1-
Dichloroethane
(u /L)
1,1-
Dichloroethene
(a �
cis-1,2-
Dichloroethene
OWL)
trans-1,2-
Dichloroethene
(u /L)
Vinyl
Chloride
(u /L)
Toluene
(u /L)
Naphthalene
(ug/L)
Other VOCs
(u /L)
TOTAL
VOCs
OWL)
15A NCAC 2L Standards
0.70
3.0
200
Not listed
70
6*
100
0.03**
1,000
21
Compound Specific
RW-1
11/03/99
-5
15
170
<5
<5
32
2,000
32
200
<5
15
Benzene (8.0)
2,479
10/24/00
351
360
1,300
<5
<5
17
<5
4,800
66
200
26
160
Benzene (12)
6,945
11/14/01
737
200
840
8.3
<5
14
6.7
3,200
12
70
<5
83
BRL
4,434
11/13/02
1101
210
820
16
<5
7.3
6.4
3,800
15
130
<5
47
1,2-Dichloropropane (61)
5,113
11/3/03
1456
180
750
<5
<5
<5
7.8
4,000
11
130
<5
26
BRL
5105
11/O1/04
1820
270
800
<5
<5
<5
8.3
4,200
37
170
<5
<5
BRL
5485
10/25/05
2178
380
790
<5
<5
<5
11
3,700
21
160
<5
31
BRL
5,093
11/28/06
2577
560
1,100
<10
<10
<10
<10
4,600
8.7 J
180
<10
<10
BRL
6,449
10/25/07
2908
470
1,400
<10
<10
5.1 J
5.2 J
3,100
19 J
200
<10
<10
BRL
5,199
11/06/08
3286
600
860
<10
<10
7.2 J
10
5,200
32
180
<10
<10
BRL
6,889
10/30/09
3644
460
960
<10
<10
6.7 J
8.6 J
5,500
34
200
<10
9.6 J
BRL
7,179
11/02/10
4012
470
1,100
<100
<100
<100
<100
5,600
<100
120 J
<100
<100
BRL
7,290
RW-2
11/03/99
-5
8,200
7,700
<5
<5
22
120
31,000
430
29700
96
660
Benzene (61), Ethylbenzene (22),
Xylenes (57),
1,2-Dichlorobenzene (7.3)
51,020
10/24/00
351
1,200
3,900
<5
<5
16
30,000
410
2,700
45
140
1,2-DiBenzene (8.5) (5.9),
Benzene (8.5)
38,480
11/14/01
737
1,200
19800
<50
<50
<50
<50
17,000
83
740
<50
90
BRL
20,913
11/13/02
1101
290
830
<50
<50
<50
<50
34,000
160
2,200
<50
83
1,2-Dichloropropane (98);
1,1-Dichloropropee (130)
37,791
11/3/03
1456
320
29500
<50
<50
<50
<50
25,000
73
19300
<50
<50
BRL
29,193
11/O1/04
1820
630
49800
<50
<50
<50
55
22,000
160
19100
<50
<50
Benzene (8.0)
28,698
10/25/05
2178
93
300
<50
<50
<50
<50
21,000
130
29200
<50
<50
BRL
23,723
11/28/06
2577
<100
170 J
<100
<100
<100
<100
19,000
<200
19700
<100
<100
BRL
20,870
10/25/07
2908
140
470
<100
<100
<100
<100
18,000
110 J
29000
<100
<100
BRL
20,720
11/06/08
3286
280
1,500
<100
<100
<100
<100
16,000
11
920
<100
<100
BRL
18,810
10/30/09
3644
190
830
<100
<100
<100
<100
14,000
88 J
1,200
<100
<100
BRL
16,308
11/02/10
4012
150
660
<100
<100
<100
<100
13,000
84 J
830
<100
<100
BRL
14,724
RW-3
11/03/99
-5
110
68
<5
<5
8.5
<5
330
<5
<10
<5
<25
BRL
517
10/24/00
351
<5
19
<5
<5
6.1
6.7
6,500
67
1100
8.5
26
BRL
7,733
11/14/01
737
<5
6.8
6.7
<5
<5
<5
2,000
8.8
320
<5
14
BRL
2,356
11/13/02
1101
<50
<50
<50
<50
<50
<50
2,800
<50
610
<50
<50
BRL
3,410
11/03/03
1456
1 <5
8.8
<5
<5
<5
<5
3,100
8.7
350
1 <5
6.8
BRL
3,474
11/O1/04
1820
<5
15.0
<5
<5
<5
<5
2,700
16
330
<5
<5
BRL
3,061
10/25/05
2178
<5
6.2
<5
<5
<5
<5
1,700
7.6
250
<5
<5
BRL
1,964
11/28/06
2577
<10
<20
<10
<20
<10
<10
1,800
<20
290
<10
<10
BRL
2,090
10/25/07
2908
<10
5.6 J
<10
<10
<10
<10
960
5.3 J
140
<10
<10
BRL
1,111
11/06/08
3286
<10
15 J
<10
<10
<10
<10
1,600
12 J
240
<10
<10
BRL
1,867
10/30/09
3644
<10
8.0 J
<10
<10
<10
<10
1,100
5.3 J
140
<10
<10
BRL
1,253
11/02/10
4012
<10
12 J
<10
<10
<10
<10
1,300
8.9 J
150
<10
<10
BRL
1,471
11/28/06
2577
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<2.0
<1.0
<1.0
BRL
0
10/25/07
2908
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<2.0
<1.0
<1.0
BRL
0
2237
Alamac
11/06/08
3286
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<2.0
<1.0
<1.0
BRL
0
Road
10/30/09
3644
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<2.0
<1.0
<1.0
Bromoform (2.5),
Chlorodibromomethane (0.57 J)
3.07
11/02/10
4012
<1.0
1 <2.0
1 <1.0
<1.0
<1.0
<1.0
<1.0
1 <2.0
<2.0
<1.0
<1.0
BRL
0
NS - Not Sampled
BRL - Below Reporting Limit
Shaded cells represent concentrations exceeding the 15A NCAC 2L Standard
Values in bold represent concetrations exceeding the detection limit.
J - Estimated value between the Reporting Limit and the Method Detection Limit.
Days after startup indicate number of days groundwater recovery system has been in operation since system was started on November 8, 1999..
N/A = Not Applicable
* = NC 2L Standard changed in Jan 2010 from 70 µg/L to 6 µg/L.
**= NC 2L Standard changed in Jan 2010 from 0.015 µg/L to 0.03 µg/L.
Startup date 11/8/1999
Page 1 of 1 Table 3-2

TABLE 3-3
HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN ON -SITE WASTEWATER
TREATMENT PLANT EFFLUENT
ALAMAC AMERICAN KNITS
LUMBERTON, NORTH CAROLINA
cis-1,2-
WWTP
Sample
Tetrachloroethene
Trichloroethene
Vinyl Chloride
Dichloroethene
Effluent
Date
(1192)
(µg/L)
(1192)
(1192)
1999
11/09/99
<5
<5
<5
<5
2000
04/13/00
<5
<5
<5
<10
2001
09/04/01
<5
<5
<5
<10
2002
11/05/02
<5
<5
<5
<10
2003
12/01/03
<5
<5
<5
<10
2004
12/07/04
<5
<5
0.8
<10
2005
10/04/05
<0.01
<0.01
<0.01
<0.01
2006
12/11/06
<1.0
<1.0
<1.0
<2.0
03713707
<1.0
<1.0
<1.0
<2.0
c
06/05/07
<5.0
<5.0
<5.0
<10
N
09/11/07
<1.0
<1.0
<1.0
<2.0
12/04/07
<5.0
<5.0
<5.0
<10.0
03 04 08
<5.0
<5.0
<5.0
<10.0
00
0
0
06/03/08
<5.0
<5.0
<5.0
<10.0
09/16/08
<2.0
<1.0
<1.0
<2.0
03/10/09
<1.0
<1.0
<1.0
<2.0
06/09/09
<1.0
<1.0
<1.0
<2.0
0
N
09/15/09
<1.0
<1.0
<1.0
<2.0
12/15/09
<1.0
<1.0
<1.0
<2.0
03/02/10
<1.0
<1.0
<1.0
<2.0
0
06/08/10
<1.0
<1.0
<1.0
<2.0
N
09/14/10
<1.0
<1.0
<1.0
<2.0
12/14/10
<1.0
<1.0
<1.0
<2.0
1. All samples were collected by Alamac as part of their monthly NPDES permit monitoring.
2. Monthly data for 1999 through 2004 included in prior Groundwater Monitoring Reports.
3. Bold indicates value exceeded laboratory method detection limit.
Page 1 of 1 Table 3-3

TABLE 4-1
HISTORICAL SUMMARY OF SELECTED BIO-GEOCHEMICAL PARAMETERS IN GROUNDWATER
ALAMAC AMERICAN KNITS
LUMBERTON, NORTH CAROLINA
Well ID
Sampling
Date
Days after
Startup
pH
SU
DO
(m )
ORP
(mv)
Conductivity
(AS/cm)
RECOVERY WELLS
RW-1
11/03/99
-5
5.8
0.40
5
NA
10/24/00
351
NA
0.23
NA
NA
11/14/O1
737
6.7
1.21
<-100
203
11/13/02
1101
5.7
1.30
-56
230
11/03/03
1456
5.9
1.19
25
134
11/01/04
1820
5.5
1.14
18
108
10/25/05
2178
5.0
1.10
-5
212
11/28/06
2577
5.4
1.51
-178
91
10/25/07
2908
5.5
3.32
53
117
11/06/08
3286
4.9
4.96
38
129
10/30/09
3644
5.8
5.18
13
96
11/02/10
4012
5.0
5.11
-36
171
RW-2
11/03/99
-5
5.2
0.26
0
NA
10/24/00
351
NA
0.78
NA
NA
11/14/O1
737
6.4
1.40
-60
343
11/13/02
1101
5.6
1.26
-42
330
11/03/03
1456
5.8
1.23
20
346
11/01/04
1820
5.3
1.23
0.2
355
10/25/05
2178
5.4
1.48
-74.0
265
11/28/06
2577
5.8
1.78
-199
207
10/25/07
2908
5.3
5.73
39
237
11/06/08
3286
5.1
2.15
38
194
10/30/09
3644
6.0
6.32
-16
222
11/02/10
4012
1 5.5
6.20
-67
254
RW-3
11/03/99
-5
5.2
5.22
40
NA
10/24/00
351
NA
1.98
NA
NA
11/14/O1
737
6.6
1.71
-82
125
11/13/02
1101
5.5
1.27
-43
120
11/03/03
1456
5.6
1.26
52
96
11/01/04
1820
5.5
1.10
-1
118
10/25/05
2178
5.3
2.41
42
120
11/28/06
2577
5.6
2.62
-197
91
10/25/07
2908
5.4
3.24
34
105
11/06/08
10/30/09
11/02/10
3286
5.5
6.0
5.6
4.73
5.08
5.20
68
38
-40
118
110
119
3644
4012
2237 Alamac Rd
11/28/06
6.0
0.16
-137
82
10/25/07
5.7
0.52
109
107
11/06/08
5.5
3.93
157
105
10/30/2009
5.6
1.85
118
119
11/2/2010
5.2
4.04
28
98
NA - Not analyzed
Days after startup indicate number of days groundwater recovery system has been in operation since system
was started on November 8, 1999.
SU - Standard Units
mg/L = Milligrams per liter
mV = Millivolts
µS/cm - MicroSiemens per centimeter
Page 1 of 1

FIGURES

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FIGURE:
In d'uR iall & E.nviro1)1nc•>J 4 servilms
ALAMAC AMERICAN KNITS LLC
1
1101 NOWELL ROAD
LUMBERTON, NORTH CAROLINA
RALEIGH, NORTH CAROLINA 27609
TEL.: [phone] FAX.: [phone]

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Figure 3. Chlorinated Ethene Concentrations in RW-1
12000
10000
8000
0
6000
a�
r. 4000
0
U
2000
Q
-5 495 995 1495 1995 2495 2995 3495 3995 4495
Days Since Startup
PCE f TCE � cis- 1,2-DCE VC )K Total VOCs

50,000
1-1
It 40,000
30,000
20,000
0
U 10,000
Figure 4. Chlorinated Ethene Concentrations in RW-2
-5 495
995 1,495 1,995 2,495 2,995 3,495 3,995 4,495
Days Since Startup
t PCE f TCE f cis-1,2-DCE VC --*--Total VOCs

Figure 5. Chlorinated Ethene Concentrations in RW-3
10,000 -
9,000
8,000
7,000
=L 6,000
5,000
4,000
3,000
2,000
1,000
0,
-5 495 995 1,495 1,995 2,495 2,995 3,495 3,995 4,495
Days Since Startup
PCE f TCE f cis-1,2-DCE VC --*—Total VOCs

APPENDIX A
LABORATORY ANALYTICAL REPORTS

Case Narrative
PRI S M Full -Service Analytical &
JI I Environmental Solutions
LABORATORIES, INC.
Solutions-IES, Inc.
Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Project: Alamac
Lab Submittal Date: 11/03/2010
Prism Work Order: 0110138
11 /17/2010
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a-,--.1
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 18

Sample Receipt Summary
&GIE R I IS M
Full -Service Analytical R
Environmental Solutions
11/17/2010
LABORATORIES, INC.
Prism Work Order:
0110138
Client Sample ID
Lab Sample ID Matrix
Date Sampled
Date Received
RW-1
0110138-01 Water
11/02/10
11/03/10
RW-2
0110138-02 Water
11/02/10
11/03/10
RW-3
0110138-03 Water
11/02/10
11/03/10
2237
0110138-04 Water
11/02/10
11/03/10
TRIP BLANK
0110138-05 Water
11/02/10
11/03/10
Samples received in good condition at 3.1 degrees C unless otherwise noted.
Summary
of Detections
R I S M
Full -Service Analytical &
�P
Environmental Solutions
11/17/2010
LABORATORIES, INa
Prism Work Order:
0110138
Prism ID Client ID
Parameter
Method
Result
Units
0110138-01 RW-1
cis- 1,2-Dichloroethylene
8260E
5600
ug/L
0110138-01 RW-1
Tetrachloroethylene
8260B
470
ug/L
0110138-01 RW-1
Trichloroethylene
8260B
1100
ug/L
0110138-01 RW-1
Vinyl chloride
8260E
120 .1
ug/L
0110138-02 RW-2
cis- 1,2-Dichloroethylene
8260E
13000
ug/L
0110138-02 RW-2
Tetrachloroethylene
8260E
150
ug/L
0110138-02 RW-2
trans- 1,2-Dichloroethylene
8260E
84 1
ug/L
0110138-02 RW-2
Trichloroethylene
8260E
660
ug/L
0110138-02 RW-2
Vinyl chloride
8260B
830
ug/L
0110138-03 RW-3
cis- 1,2-Dichloroethylene
8260B
1300
ug/L
0110138-03 RW-3
trans- 1,2-Dichloroethylene
8260B
8.9 J
ug/L
0110138-03 RW-3
Trichloroethylene
8260E
12 .1
ug/L
0110138-03 RW-3
Vinyl chloride
8260E
150
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 18

PRISM Fun -Service Analytical &
Laboratory Report
Environmental Solutions 11/17/2010
&
I LABORATORIES, INC.
Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-1
Attn: Sean K. Jarvah Prism Sample ID: 0110138-01
1101 Nowell Road Prism Work Order: 0110138
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:02
Time Submitted: 11/03/10 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
BRL
ug/L
100
15
100
8260B
11/9/10 13:58
LMW
POK0222
1,1,1-Trichloroethane
BRL
ug/L
100
6.3
100
8260B
11/9/10 13:58
LMW
POK0222
1,1,2,2-Tetrachloroethane
BRL
ug/L
100
7.1
100
8260B
11/9/10 13:58
LMW
POK0222
1,1,2-Trichloroethane
BRL
ug/L
100
17
100
8260B
11/9/10 13:58
LMW
POK0222
1,1-Dichloroethane
BRL
ug/L
100
9.6
100
8260B
11/9/10 13:58
LMW
POK0222
1,1-Dichloroethylene
BRL
ug/L
100
7.8
100
8260E
11/9/10 13:58
LMW
POK0222
1,1-Dichloropropylene
BRL
ug/L
100
6.1
100
8260E
11/9/10 13:58
LMW
POK0222
1,2,3-Trichlorobenzene
BRL
ug/L
200
20
100
8260E
11/9/10 13:58
LMW
POK0222
1,2,3-Trichloropropane
BRL
ug/L
100
8.1
100
8260B
11/9/10 13:58
LMW
POK0222
1,2,4-Trichlorobenzene
BRL
ug/L
100
10
100
8260E
11/9/10 13:58
LMW
POK0222
1,2,4-Trimethyl benzene
BRL
ug/L
100
4.8
100
8260E
11/9/10 13:58
LMW
POK0222
1,2-Dibromo-3-chloropropane
BRL
ug/L
200
59
100
8260E
11/9/10 13:58
LMW
POK0222
1,2-Dibromoethane
BRL
ug/L
100
14
100
8260B
11/9/10 13:58
LMW
POK0222
1,2-Dichlorobenzene
BRL
ug/L
100
7.6
100
8260B
11/9/10 13:58
LMW
POK0222
1,2-Dichloroethane
BRL
ug/L
100
14
100
8260B
11/9/10 13:58
LMW
POK0222
1,2-Dichloropropane
BRL
ug/L
100
13
100
8260B
11/9/10 13:58
LMW
POK0222
1,3,5-Trimethyl benzene
BRL
ug/L
100
5.7
100
8260B
11/9/10 13:58
LMW
POK0222
1,3-Dichlorobenzene
BRL
ug/L
100
7.4
100
8260E
11/9/10 13:58
LMW
POK0222
1,3-Dichloropropane
BRL
ug/L
100
11
100
8260E
11/9/10 13:58
LMW
POK0222
1,4-Dichlorobenzene
BRL
ug/L
100
6.8
100
8260E
11/9/10 13:58
LMW
POK0222
2,2-Dichloropropane
BRL
ug/L
200
11
100
8260B
11/9/10 13:58
LMW
POK0222
2-Chloroethyl Vinyl Ether
BRL
ug/L
200
22
100
8260E
11/9/10 13:58
LMW
POK0222
2-Chlorotoluene
BRL
ug/L
100
3.8
100
8260E
11/9/10 13:58
LMW
POK0222
4-Chlorotoluene
BRL
ug/L
100
5.3
100
8260E
11/9/10 13:58
LMW
POK0222
4-Isopropyltoluene
BRL
ug/L
100
6.5
100
8260B
11/9/10 13:58
LMW
POK0222
Acetone
BRL
ug/L
1000
62
100
8260B
11/9/10 13:58
LMW
POK0222
Acrolein
BRL
ug/L
10000
110
100
8260B
11/9/10 13:58
LMW
POK0222
Acrylonitrile
BRL
ug/L
10000
86
100
8260B
11/9/10 13:58
LMW
POK0222
Benzene
BRL
ug/L
100
7.2
100
8260B
11/9/10 13:58
LMW
POK0222
Bromobenzene
BRL
ug/L
100
6.4
100
8260E
11/9/10 13:58
LMW
POK0222
Bromochloromethane
BRL
ug/L
100
13
100
8260E
11/9/10 13:58
LMW
POK0222
Bromodichloromethane
BRL
ug/L
100
6.2
100
8260E
11/9/10 13:58
LMW
POK0222
Bromoform
BRL
ug/L
100
27
100
8260B
11/9/10 13:58
LMW
POK0222
Bromomethane
BRL
ug/L
300
47
100
8260E
11/9/10 13:58
LMW
POK0222
Carbon disulfide
BRL
ug/L
500
140
100
8260E
11/9/10 13:58
LMW
POK0222
Carbon Tetrachloride
BRL
ug/L
200
12
100
8260E
11/9/10 13:58
LMW
POK0222
Chlorobenzene
BRL
ug/L
100
6.1
100
8260B
11/9/10 13:58
LMW
POK0222
Chloroethane
BRL
ug/L
500
13
100
8260B
11/9/10 13:58
LMW
POK0222
Chloroform
BRL
ug/L
100
8.9
100
8260B
11/9/10 13:58
LMW
POK0222
Chloromethane
BRL
ug/L
200
11
100
8260B
11/9/10 13:58
LMW
POK0222
cis-1,2-Dichloroethylene
5600
ug/L
100
7.6
100
8260B
1119/10 13:58
LMW
POK0222
cis-1,3-Dichloropropylene
BRL
ug/L
100
10
100
8260B
11/9/10 13:58
LMW
POK0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-1
Attn: Sean K. Jarvah Prism Sample ID: 0110138-01
1101 Nowell Road Prism Work Order: 0110138
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:02
Time Submitted: 11/03/10 15:40
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dibromochloromethane
BRL
ug/L
100
30
100
8260E
11/9/10 13:58
LMW
POK0222
Dibromomethane
BRL
ug/L
100
13
100
8260E
11/9/10 13:58
LMW
POK0222
Dichlorodifluoromethane
BRL
ug/L
200
11
100
8260E
11/9/10 13:58
LMW
POK0222
Ethylbenzene
BRL
ug/L
100
6.7
100
8260B
11/9/10 13:58
LMW
POK0222
Hexachlorobutadiene
BRL
ug/L
200
36
100
8260E
11/9/10 13:58
LMW
POK0222
Isopropyl Ether
BRL
ug/L
100
4.3
100
8260E
11/9/10 13:58
LMW
POK0222
Isopropylbenzene (Cumene)
BRL
ug/L
100
7.2
100
8260E
11/9/10 13:58
LMW
POK0222
m,p-Xylenes
BRL
ug/L
200
8.1
100
8260B
11/9/10 13:58
LMW
POK0222
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
500
19
100
8260B
11/9/10 13:58
LMW
POK0222
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
500
90
100
8260B
11/9/10 13:58
LMW
POK0222
Methyl Isobutyl Ketone
BRL
ug/L
500
12
100
8260B
11/9/10 13:58
LMW
POK0222
Methylene Chloride
BRL
ug/L
200
44
100
8260B
11/9/10 13:58
LMW
POK0222
Methyl-tert-Butyl Ether
BRL
ug/L
100
7.0
100
8260E
11/9/10 13:58
LMW
POK0222
Naphthalene
BRL
ug/L
100
9.8
100
8260E
11/9/10 13:58
LMW
POK0222
n-Butylbenzene
BRL
ug/L
100
11
100
8260E
11/9/10 13:58
LMW
POK0222
n-Propylbenzene
BRL
ug/L
100
6.0
100
8260B
11/9/10 13:58
LMW
POK0222
o-Xylene
BRL
ug/L
100
4.6
100
8260E
11/9/10 13:58
LMW
POK0222
sec-Butylbenzene
BRL
ug/L
100
8.7
100
8260E
11/9/10 13:58
LMW
POK0222
Styrene
BRL
ug/L
100
4.7
100
8260E
11/9/10 13:58
LMW
POK0222
tert-Butylbenzene
BRL
ug/L
100
8.0
100
8260B
11/9/10 13:58
LMW
POK0222
Tetrachloroethylene
470
ug/L
100
6.9
100
8260B
11/9/10 13:58
LMW
POK0222
Toluene
BRL
ug/L
100
4.2
100
8260E
11/9/10 13:58
LMW
POK0222
trans-1,2-Dichloroethylene
BRL
ug/L
200
12
100
8260E
11/9/10 13:58
LMW
POK0222
trans-1,3-Dichloropropylene
BRL
ug/L
100
4.3
100
8260B
11/9/10 13:58
LMW
POK0222
Trichloroethylene
1100
ug/L
200
5.4
100
8260B
11/9/10 13:58
LMW
POK0222
Trichlorofluoromethane
BRL
ug/L
200
8.8
100
8260E
11/9/10 13:58
LMW
POK0222
Vinyl acetate
BRL
ug/L
2000
10
100
8260E
11/9/10 13:58
LMW
POK0222
Vinyl chloride
120 J
ug/L
200
16
100
8260B
11/9/10 13:58
LMW
POK0222
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
94 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc.
Project: Alamac Client Sample ID: RW-2
Attn: Sean K. Jarvah
Prism Sample ID: 0110138-02
1101 Nowell Road
Prism Work Order: 0110138
Raleigh, NC 27607
Sample Matrix: Water Time Collected: 11/02/10 11:04
Time Submitted: 11/03/10 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/L
100
15
100
8260B
11/9/10 10:54
LMW
POK0222
1,1,1-Trichloroethane
BRL
ug/L
100
6.3
100
8260B
11/9/10 10:54
LMW
POK0222
1,1,2,2-Tetrachloroethane
BRL
ug/L
100
7.1
100
8260E
11/9/10 10:54
LMW
POK0222
1,1,2-Trichloroethane
BRL
ug/L
100
17
100
8260E
11/9/10 10:54
LMW
POK0222
1,1-Dichloroethane
BRL
ug/L
100
9.6
100
8260E
11/9/10 10:54
LMW
POK0222
1,1-Dichloroethylene
BRL
ug/L
100
7.8
100
8260E
11/9/10 10:54
LMW
POK0222
1,1-Dichloropropylene
BRL
ug/L
100
6.1
100
8260E
11/9/10 10:54
LMW
POK0222
1,2,3-Trichlorobenzene
BRL
ug/L
200
20
100
8260E
11/9/10 10:54
LMW
POK0222
1,2,3-Trichloropropane
BRL
ug/L
100
8.1
100
8260B
11/9/10 10:54
LMW
POK0222
1,2,4-Trichlorobenzene
BRL
ug/L
100
10
100
8260B
11/9/10 10:54
LMW
POK0222
1,2,4-Trimethyl benzene
BRL
ug/L
100
4.8
100
8260B
11/9/10 10:54
LMW
POK0222
1,2-Dibromo-3-chloropropane
BRL
ug/L
200
59
100
8260B
11/9/10 10:54
LMW
POK0222
1,2-Dibromoethane
BRL
ug/L
100
14
100
8260B
11/9/10 10:54
LMW
POK0222
1,2-Dichlorobenzene
BRL
ug/L
100
7.6
100
8260B
11/9/10 10:54
LMW
POK0222
1,2-Dichloroethane
BRL
ug/L
100
14
100
8260E
11/9/10 10:54
LMW
POK0222
1,2-Dichloropropane
BRL
ug/L
100
13
100
8260E
11/9/10 10:54
LMW
POK0222
1,3,5-Trimethyl benzene
BRL
ug/L
100
5.7
100
8260E
11/9/10 10:54
LMW
POK0222
1,3-Dichlorobenzene
BRL
ug/L
100
7.4
100
8260E
11/9/10 10:54
LMW
POK0222
1,3-Dichloropropane
BRL
ug/L
100
11
100
8260E
11/9/10 10:54
LMW
POK0222
1,4-Dichlorobenzene
BRL
ug/L
100
6.8
100
8260E
11/9/10 10:54
LMW
POK0222
2,2-Dichloropropane
BRL
ug/L
200
11
100
8260B
11/9/10 10:54
LMW
POK0222
2-Chloroethyl Vinyl Ether
BRL
ug/L
200
22
100
8260B
11/9/10 10:54
LMW
POK0222
2-Chlorotoluene
BRL
ug/L
100
3.8
100
8260B
11/9/10 10:54
LMW
POK0222
4-Chlorotoluene
BRL
ug/L
100
5.3
100
8260B
11/9/10 10:54
LMW
POK0222
4-Isopropyltoluene
BRL
ug/L
100
6.5
100
8260B
11/9/10 10:54
LMW
POK0222
Acetone
BRL
ug/L
1000
62
100
8260B
11/9/10 10:54
LMW
POK0222
Acrolein
BRL
ug/L
10000
110
100
8260E
11/9/10 10:54
LMW
POK0222
Acrylonitrile
BRL
ug/L
10000
86
100
8260E
11/9/10 10:54
LMW
POK0222
Benzene
BRL
ug/L
100
7.2
100
8260E
11/9/10 10:54
LMW
POK0222
Bromobenzene
BRL
ug/L
100
6.4
100
8260E
11/9/10 10:54
LMW
POK0222
Bromochloromethane
BRL
ug/L
100
13
100
8260E
11/9/10 10:54
LMW
POK0222
Bromodichloromethane
BRL
ug/L
100
6.2
100
8260E
11/9/10 10:54
LMW
POK0222
Bromoform
BRL
ug/L
100
27
100
8260B
11/9/10 10:54
LMW
POK0222
Bromomethane
BRL
ug/L
300
47
100
8260B
11/9/10 10:54
LMW
POK0222
Carbon disulfide
BRL
ug/L
500
140
100
8260B
11/9/10 10:54
LMW
POK0222
Carbon Tetrachloride
BRL
ug/L
200
12
100
8260B
11/9/10 10:54
LMW
POK0222
Chlorobenzene
BRL
ug/L
100
6.1
100
8260B
11/9/10 10:54
LMW
POK0222
Chloroethane
BRL
ug/L
500
13
100
8260B
11/9/10 10:54
LMW
POK0222
Chloroform
BRL
ug/L
100
8.9
100
8260E
11/9/10 10:54
LMW
POK0222
Chloromethane
BRL
ug/L
200
11
100
8260E
11/9/10 10:54
LMW
POK0222
cis-1,2-Dichloroethylene 13000
ug/L
1000
76
1000
8260B
11/9/10 14:24
LMW
POK0222
cis-1,3-Dichloropropylene
BRL
ug/L
100
10
100
8260B
11/9/10 10:54
LMW
POK0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-2
Attn: Sean K. Jarvah Prism Sample ID: 0110138-02
1101 Nowell Road Prism Work Order: 0110138
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:04
Time Submitted: 11/03/10 15:40
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dibromochloromethane
BRL
ug/L
100
30
100
8260E
11/9/10 10:54
LMW
POK0222
Dibromomethane
BRL
ug/L
100
13
100
8260E
11/9/10 10:54
LMW
POK0222
Dichlorodifluoromethane
BRL
ug/L
200
11
100
8260E
11/9/10 10:54
LMW
POK0222
Ethylbenzene
BRL
ug/L
100
6.7
100
8260B
11/9/10 10:54
LMW
POK0222
Hexachlorobutadiene
BRL
ug/L
200
36
100
8260E
11/9/10 10:54
LMW
POK0222
Isopropyl Ether
BRL
ug/L
100
4.3
100
8260E
11/9/10 10:54
LMW
POK0222
Isopropylbenzene (Cumene)
BRL
ug/L
100
7.2
100
8260E
11/9/10 10:54
LMW
POK0222
m,p-Xylenes
BRL
ug/L
200
8.1
100
8260B
11/9/10 10:54
LMW
POK0222
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
500
19
100
8260B
11/9/10 10:54
LMW
POK0222
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
500
90
100
8260B
11/9/10 10:54
LMW
POK0222
Methyl Isobutyl Ketone
BRL
ug/L
500
12
100
8260B
11/9/10 10:54
LMW
POK0222
Methylene Chloride
BRL
ug/L
200
44
100
8260B
11/9/10 10:54
LMW
POK0222
Methyl-tert-Butyl Ether
BRL
ug/L
100
7.0
100
8260E
11/9/10 10:54
LMW
POK0222
Naphthalene
BRL
ug/L
100
9.8
100
8260E
11/9/10 10:54
LMW
POK0222
n-Butylbenzene
BRL
ug/L
100
11
100
8260E
11/9/10 10:54
LMW
POK0222
n-Propylbenzene
BRL
ug/L
100
6.0
100
8260B
11/9/10 10:54
LMW
POK0222
o-Xylene
BRL
ug/L
100
4.6
100
8260E
11/9/10 10:54
LMW
POK0222
sec-Butylbenzene
BRL
ug/L
100
8.7
100
8260E
11/9/10 10:54
LMW
POK0222
Styrene
BRL
ug/L
100
4.7
100
8260E
11/9/10 10:54
LMW
POK0222
tert-Butylbenzene
BRL
ug/L
100
8.0
100
8260B
11/9/10 10:54
LMW
POK0222
Tetrachloroethylene
150
ug/L
100
6.9
100
8260B
11/9/10 10:54
LMW
POK0222
Toluene
BRL
ug/L
100
4.2
100
8260E
11/9/10 10:54
LMW
POK0222
trans-1,2-Dichloroethylene
84 J
ug/L
200
12
100
8260E
11/9/10 10:54
LMW
POK0222
trans-1,3-Dichloropropylene
BRL
ug/L
100
4.3
100
8260B
11/9/10 10:54
LMW
POK0222
Trichloroethylene
660
ug/L
200
5.4
100
8260B
11/9/10 10:54
LMW
POK0222
Trichlorofluoromethane
BRL
ug/L
200
8.8
100
8260E
11/9/10 10:54
LMW
POK0222
Vinyl acetate
BRL
ug/L
2000
10
100
8260E
11/9/10 10:54
LMW
POK0222
Vinyl chloride
830
ug/L
200
16
100
8260B
11/9/10 10:54
LMW
POK0222
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
107 %
75-129
Toluene-d8
94 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc.
Project: Alamac Client Sample ID: RW-3
Attn: Sean K. Jarvah
Prism Sample ID: 0110138-03
1101 Nowell Road
Prism Work Order: 0110138
Raleigh, NC 27607
Sample Matrix: Water Time Collected: 11/02/10 11:06
Time Submitted: 11/03/10 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/L
10
1.5
10
8260B
11/9/10 10:28
LMW
POK0222
1,1,1-Trichloroethane
BRL
ug/L
10
0.63
10
8260B
11/9/10 10:28
LMW
POK0222
1,1,2,2-Tetrachloroethane
BRL
ug/L
10
0.71
10
8260B
11/9/10 10:28
LMW
POK0222
1,1,2-Trichloroethane
BRL
ug/L
10
1.7
10
8260B
11/9/10 10:28
LMW
POK0222
1,1-Dichloroethane
BRL
ug/L
10
0.96
10
8260B
11/9/10 10:28
LMW
POK0222
1,1-Dichloroethylene
BRL
ug/L
10
0.78
10
8260B
11/9/10 10:28
LMW
POK0222
1,1-Dichloropropylene
BRL
ug/L
10
0.61
10
8260B
11/9/10 10:28
LMW
POK0222
1,2,3-Trichlorobenzene
BRL
ug/L
20
2.0
10
8260B
11/9/10 10:28
LMW
POK0222
1,2,3-Trichloropropane
BRL
ug/L
10
0.81
10
8260B
11/9/10 10:28
LMW
POK0222
1,2,4-Trichlorobenzene
BRL
ug/L
10
1.0
10
8260B
11/9/10 10:28
LMW
POK0222
1,2,4-Trimethyl benzene
BRL
ug/L
10
0.48
10
8260B
11/9/10 10:28
LMW
POK0222
1,2-Dibromo-3-chloropropane
BRL
ug/L
20
5.9
10
8260B
11/9/10 10:28
LMW
POK0222
1,2-Dibromoethane
BRL
ug/L
10
1.4
10
8260B
11/9/10 10:28
LMW
POK0222
1,2-Dichlorobenzene
BRL
ug/L
10
0.76
10
8260B
11/9/10 10:28
LMW
POK0222
1,2-Dichloroethane
BRL
ug/L
10
1.4
10
8260B
11/9/10 10:28
LMW
POK0222
1,2-Dichloropropane
BRL
ug/L
10
1.3
10
8260B
11/9/10 10:28
LMW
POK0222
1,3,5-Trimethyl benzene
BRL
ug/L
10
0.57
10
8260B
11/9/10 10:28
LMW
POK0222
1,3-Dichlorobenzene
BRL
ug/L
10
0.74
10
8260B
11/9/10 10:28
LMW
POK0222
1,3-Dichloropropane
BRL
ug/L
10
1.1
10
8260B
11/9/10 10:28
LMW
POK0222
1,4-Dichlorobenzene
BRL
ug/L
10
0.68
10
8260B
11/9/10 10:28
LMW
POK0222
2,2-Dichloropropane
BRL
ug/L
20
1.1
10
8260B
11/9/10 10:28
LMW
POK0222
2-Chloroethyl Vinyl Ether
BRL
ug/L
20
2.2
10
8260B
11/9/10 10:28
LMW
POK0222
2-Chlorotoluene
BRL
ug/L
10
0.38
10
8260B
11/9/10 10:28
LMW
POK0222
4-Chlorotoluene
BRL
ug/L
10
0.53
10
8260B
11/9/10 10:28
LMW
POK0222
4-Isopropyltoluene
BRL
ug/L
10
0.65
10
8260B
11/9/10 10:28
LMW
POK0222
Acetone
BRL
ug/L
100
6.2
10
8260B
11/9/10 10:28
LMW
POK0222
Acrolein
BRL
ug/L
1000
11
10
8260E
11/9/10 10:28
LMW
POK0222
Acrylonitrile
BRL
ug/L
1000
8.6
10
8260E
11/9/10 10:28
LMW
POK0222
Benzene
BRL
ug/L
10
0.72
10
8260B
11/9/10 10:28
LMW
POK0222
Bromobenzene
BRL
ug/L
10
0.64
10
8260B
11/9/10 10:28
LMW
POK0222
Bromochloromethane
BRL
ug/L
10
1.3
10
8260B
11/9/10 10:28
LMW
POK0222
Bromodichloromethane
BRL
ug/L
10
0.62
10
8260B
11/9/10 10:28
LMW
POK0222
Bromoform
BRL
ug/L
10
2.7
10
8260B
11/9/10 10:28
LMW
POK0222
Bromomethane
BRL
ug/L
30
4.7
10
8260B
11/9/10 10:28
LMW
POK0222
Carbon disulfide
BRL
ug/L
50
14
10
8260B
11/9/10 10:28
LMW
POK0222
Carbon Tetrachloride
BRL
ug/L
20
1.2
10
8260B
11/9/10 10:28
LMW
POK0222
Chlorobenzene
BRL
ug/L
10
0.61
10
8260B
11/9/10 10:28
LMW
POK0222
Chloroethane
BRL
ug/L
50
1.3
10
8260B
11/9/10 10:28
LMW
POK0222
Chloroform
BRL
ug/L
10
0.89
10
8260B
11/9/10 10:28
LMW
POK0222
Chloromethane
BRL
ug/L
20
1.1
10
8260B
11/9/10 10:28
LMW
POK0222
cis-1,2-Dichloroethylene
1300
ug/L
100
7.6
100
8260B
11/9/10 7:48
LMW
POK0222
cis-1,3-Dichloropropylene
BRL
ug/L
10
1.0
10
8260B
11/9/10 10:28
LMW
POK0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc.
Project: Alamac Client Sample ID: RW-3
Attn: Sean K. Jarvah
Prism Sample ID: 0110138-03
1101 Nowell Road
Prism Work Order: 0110138
Raleigh, NC 27607
Sample Matrix: Water Time Collected: 11/02/10 11:06
Time Submitted: 11/03/10 15:40
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dibromochloromethane
BRL
ug/L
10
3.0
10
8260B
11/9/10 10:28
LMW
POK0222
Dibromomethane
BRL
ug/L
10
1.3
10
8260B
11/9/10 10:28
LMW
POK0222
Dichlorodifluoromethane
BRL
ug/L
20
1.1
10
8260B
11/9/10 10:28
LMW
POK0222
Ethylbenzene
BRL
ug/L
10
0.67
10
8260B
11/9/10 10:28
LMW
POK0222
Hexachlorobutadiene
BRL
ug/L
20
3.6
10
8260B
11/9/10 10:28
LMW
POK0222
Isopropyl Ether
BRL
ug/L
10
0.43
10
8260B
11/9/10 10:28
LMW
POK0222
Isopropylbenzene (Cumene)
BRL
ug/L
10
0.72
10
8260B
11/9/10 10:28
LMW
POK0222
m,p-Xylenes
BRL
ug/L
20
0.81
10
8260B
11/9/10 10:28
LMW
POK0222
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
50
1.9
10
8260B
11/9/10 10:28
LMW
POK0222
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
50
9.0
10
8260B
11/9/10 10:28
LMW
POK0222
Methyl Isobutyl Ketone
BRL
ug/L
50
1.2
10
8260B
11/9/10 10:28
LMW
POK0222
Methylene Chloride
BRL
ug/L
20
4.4
10
8260B
11/9/10 10:28
LMW
POK0222
Methyl-tert-Butyl Ether
BRL
ug/L
10
0.70
10
8260B
11/9/10 10:28
LMW
POK0222
Naphthalene
BRL
ug/L
10
0.98
10
8260B
11/9/10 10:28
LMW
POK0222
n-Butylbenzene
BRL
ug/L
10
1.1
10
8260B
11/9/10 10:28
LMW
POK0222
n-Propylbenzene
BRL
ug/L
10
0.60
10
8260B
11/9/10 10:28
LMW
POK0222
o-Xylene
BRL
ug/L
10
0.46
10
8260B
11/9/10 10:28
LMW
POK0222
sec-Butylbenzene
BRL
ug/L
10
0.87
10
8260B
11/9/10 10:28
LMW
POK0222
Styrene
BRL
ug/L
10
0.47
10
8260B
11/9/10 10:28
LMW
POK0222
tert-Butylbenzene
BRL
ug/L
10
0.80
10
8260B
11/9/10 10:28
LMW
POK0222
Tetrachloroethylene
BRL
ug/L
10
0.69
10
8260B
11/9/10 10:28
LMW
POK0222
Toluene
BRL
ug/L
10
0.42
10
8260B
11/9/10 10:28
LMW
POK0222
trans-1,2-Dichloroethylene
8.9 J
ug/L
20
1.2
10
8260B
1119/10 10:28
LMW
POK0222
trans-1,3-Dichloropropylene
BRL
ug/L
10
0.43
10
8260B
11/9/10 10:28
LMW
POK0222
Trichloroethylene
12 J
ug/L
20
0.54
10
8260B
11/9/10 10:28
LMW
POK0222
Trichlorofluoromethane
BRL
ug/L
20
0.88
10
8260B
11/9/10 10:28
LMW
POK0222
Vinyl acetate
BRL
ug/L
200
1.0
10
8260E
11/9/10 10:28
LMW
POK0222
Vinyl chloride
150
ug/L
20
1.6
10
8260B
11/9/10 10:28
LMW
POK0222
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
80-124
Dibromofluoromethane
106 %
75-129
Toluene-d8
94 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc. Project: Alamac Client Sample ID: 2237
Attn: Sean K. Jarvah Prism Sample ID: 0110138-04
1101 Nowell Road Prism Work Order: 0110138
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35
Time Submitted: 11/03/10 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/L
1.0
0.15
1
8260B
11/11/10 18:09
LMW
POK0338
1,1,1-Trichloroethane
BRL
ug/L
1.0
0.063
1
8260B
11/11/10 18:09
LMW
POK0338
1,1,2,2-Tetrachloroethane
BRL
ug/L
1.0
0.071
1
8260B
11/11/10 18:09
LMW
POK0338
1,1,2-Trichloroethane
BRL
ug/L
1.0
0.17
1
8260B
11/11/10 18:09
LMW
POK0338
1,1-Dichloroethane
BRL
ug/L
1.0
0.096
1
8260B
11/11/10 18:09
LMW
POK0338
1,1-Dichloroethylene
BRL
ug/L
1.0
0.078
1
8260B
11/11/10 18:09
LMW
POK0338
1,1-Dichloropropylene
BRL
ug/L
1.0
0.061
1
8260B
11/11/10 18:09
LMW
POK0338
1,2,3-Trichlorobenzene
BRL
ug/L
2.0
0.20
1
8260B
11/11/10 18:09
LMW
POK0338
1,2,3-Trichloropropane
BRL
ug/L
1.0
0.081
1
8260B
11/11/10 18:09
LMW
POK0338
1,2,4-Trichlorobenzene
BRL
ug/L
1.0
0.10
1
8260B
11/11/10 18:09
LMW
POK0338
1,2,4-Trimethyl benzene
BRL
ug/L
1.0
0.048
1
8260B
11/11/10 18:09
LMW
POK0338
1,2-Dibromo-3-chloropropane
BRL
ug/L
2.0
0.59
1
8260B
11/11/10 18:09
LMW
POK0338
1,2-Dibromoethane
BRL
ug/L
1.0
0.14
1
8260B
11/11/10 18:09
LMW
POK0338
1,2-Dichlorobenzene
BRL
ug/L
1.0
0.076
1
8260B
11/11/10 18:09
LMW
POK0338
1,2-Dichloroethane
BRL
ug/L
1.0
0.14
1
8260B
11/11/10 18:09
LMW
POK0338
1,2-Dichloropropane
BRL
ug/L
1.0
0.13
1
8260B
11/11/10 18:09
LMW
POK0338
1,3,5-Trimethyl benzene
BRL
ug/L
1.0
0.057
1
8260B
11/11/10 18:09
LMW
POK0338
1,3-Dichlorobenzene
BRL
ug/L
1.0
0.074
1
8260B
11/11/10 18:09
LMW
POK0338
1,3-Dichloropropane
BRL
ug/L
1.0
0.11
1
8260B
11/11/10 18:09
LMW
POK0338
1,4-Dichlorobenzene
BRL
ug/L
1.0
0.068
1
8260B
11/11/10 18:09
LMW
POK0338
2,2-Dichloropropane
BRL
ug/L
2.0
0.11
1
8260B
11/11/10 18:09
LMW
POK0338
2-Chloroethyl Vinyl Ether
BRL
ug/L
2.0
0.22
1
8260B
11/11/10 18:09
LMW
POK0338
2-Chlorotoluene
BRL
ug/L
1.0
0.038
1
8260B
11/11/10 18:09
LMW
POK0338
4-Chlorotoluene
BRL
ug/L
1.0
0.053
1
8260B
11/11/10 18:09
LMW
POK0338
4-Isopropyltoluene
BRL
ug/L
1.0
0.065
1
8260B
11/11/10 18:09
LMW
POK0338
Acetone
BRL
ug/L
10
0.62
1
8260B
11/11/10 18:09
LMW
POK0338
Acrolein
BRL
ug/L
100
1.1
1
8260E
11/11/10 18:09
LMW
POK0338
Acrylonitrile
BRL
ug/L
100
0.86
1
8260B
11/11/10 18:09
LMW
POK0338
Benzene
BRL
ug/L
1.0
0.072
1
8260B
11/11/10 18:09
LMW
POK0338
Bromobenzene
BRL
ug/L
1.0
0.064
1
8260B
11/11/10 18:09
LMW
POK0338
Bromochloromethane
BRL
ug/L
1.0
0.13
1
8260B
11/11/10 18:09
LMW
POK0338
Bromodichloromethane
BRL
ug/L
1.0
0.062
1
8260B
11/11/10 18:09
LMW
POK0338
Bromoform
BRL
ug/L
1.0
0.27
1
8260B
11/11/10 18:09
LMW
POK0338
Bromomethane
BRL
ug/L
3.0
0.47
1
8260B
11/11/10 18:09
LMW
POK0338
Carbon disulfide
BRL
ug/L
5.0
1.4
1
8260B
11/11/10 18:09
LMW
POK0338
Carbon Tetrachloride
BRL
ug/L
2.0
0.12
1
8260B
11/11/10 18:09
LMW
POK0338
Chlorobenzene
BRL
ug/L
1.0
0.061
1
8260B
11/11/10 18:09
LMW
POK0338
Chloroethane
BRL
ug/L
5.0
0.13
1
8260B
11/11/10 18:09
LMW
POK0338
Chloroform
BRL
ug/L
1.0
0.089
1
8260B
11/11/10 18:09
LMW
POK0338
Chloromethane
BRL
ug/L
2.0
0.11
1
8260B
11/11/10 18:09
LMW
POK0338
cis-1,2-Dichloroethylene
BRL
ug/L
1.0
0.076
1
8260B
11/11/10 18:09
LMW
POK0338
cis-1,3-Dichloropropylene
BRL
ug/L
1.0
0.10
1
8260B
11/11/10 18:09
LMW
POK0338
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc. Project: Alamac Client Sample ID: 2237
Attn: Sean K. Jarvah Prism Sample ID: 0110138-04
1101 Nowell Road Prism Work Order: 0110138
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35
Time Submitted: 11/03/10 15:40
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Dibromochloromethane
BRL
ug/L
1.0
0.30
1
8260B
11/11/10 18:09
LMW
POK0338
Dibromomethane
BRL
ug/L
1.0
0.13
1
8260B
11/11/10 18:09
LMW
POK0338
Dichlorodifluoromethane
BRL
ug/L
2.0
0.11
1
8260B
11/11/10 18:09
LMW
POK0338
Ethylbenzene
BRL
ug/L
1.0
0.067
1
8260B
11/11/10 18:09
LMW
POK0338
Hexachlorobutadiene
BRL
ug/L
2.0
0.36
1
8260B
11/11/10 18:09
LMW
POK0338
Isopropyl Ether
BRL
ug/L
1.0
0.043
1
8260B
11/11/10 18:09
LMW
POK0338
Isopropylbenzene (Cumene)
BRL
ug/L
1.0
0.072
1
8260B
11/11/10 18:09
LMW
POK0338
m,p-Xylenes
BRL
ug/L
2.0
0.081
1
8260B
11/11/10 18:09
LMW
POK0338
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
5.0
0.19
1
8260B
11/11/10 18:09
LMW
POK0338
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
5.0
0.90
1
8260B
11/11/10 18:09
LMW
POK0338
Methyl Isobutyl Ketone
BRL
ug/L
5.0
0.12
1
8260B
11/11/10 18:09
LMW
POK0338
Methylene Chloride
BRL
ug/L
2.0
0.44
1
8260B
11/11/10 18:09
LMW
POK0338
Methyl-tert-Butyl Ether
BRL
ug/L
1.0
0.070
1
8260B
11/11/10 18:09
LMW
POK0338
Naphthalene
BRL
ug/L
1.0
0.098
1
8260B
11/11/10 18:09
LMW
POK0338
n-Butylbenzene
BRL
ug/L
1.0
0.11
1
8260B
11/11/10 18:09
LMW
POK0338
n-Propylbenzene
BRL
ug/L
1.0
0.060
1
8260B
11/11/10 18:09
LMW
POK0338
o-Xylene
BRL
ug/L
1.0
0.046
1
8260B
11/11/10 18:09
LMW
POK0338
sec-Butylbenzene
BRL
ug/L
1.0
0.087
1
8260B
11/11/10 18:09
LMW
POK0338
Styrene
BRL
ug/L
1.0
0.047
1
8260B
11/11/10 18:09
LMW
POK0338
tert-Butylbenzene
BRL
ug/L
1.0
0.080
1
8260B
11/11/10 18:09
LMW
POK0338
Tetrachloroethylene
BRL
ug/L
1.0
0.069
1
8260B
11/11/10 18:09
LMW
POK0338
Toluene
BRL
ug/L
1.0
0.042
1
8260B
11/11/10 18:09
LMW
POK0338
trans-1,2-Dichloroethylene
BRL
ug/L
2.0
0.12
1
8260B
11/11/10 18:09
LMW
POK0338
trans-1,3-Dichloropropylene
BRL
ug/L
1.0
0.043
1
8260B
11/11/10 18:09
LMW
POK0338
Trichloroethylene
BRL
ug/L
2.0
0.054
1
8260B
11/11/10 18:09
LMW
POK0338
Trichlorofluoromethane
BRL
ug/L
2.0
0.088
1
8260B
11/11/10 18:09
LMW
POK0338
Vinyl acetate
BRL
ug/L
20
0.10
1
8260B
11/11/10 18:09
LMW
POK0338
Vinyl chloride
BRL
ug/L
2.0
0.16
1
8260B
11/11/10 18:09
LMW
POK0338
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
99 % 80-124
Dibromofluoromethane
105 %
75-129
Toluene-d8
89 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc.
Project: Alamac Client Sample ID: TRIP BLANK
Attn: Sean K. Jarvah
Prism Sample ID: 0110138-05
1101 Nowell Road
Prism Work Order: 0110138
Raleigh, NC 27607
Sample Matrix: Water Time Collected: 11/02/10 11:35
Time Submitted: 11/03/10 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/L
1.0
0.15
1
8260B
11/9/10
4:15
LMW
POK0222
1,1,1-Trichloroethane
BRL
ug/L
1.0
0.063
1
8260B
11/9/10
4:15
LMW
POK0222
1,1,2,2-Tetrachloroethane
BRL
ug/L
1.0
0.071
1
8260B
11/9/10
4:15
LMW
POK0222
1,1,2-Trichloroethane
BRL
ug/L
1.0
0.17
1
8260B
11/9/10
4:15
LMW
POK0222
1,1-Dichloroethane
BRL
ug/L
1.0
0.096
1
8260B
11/9/10
4:15
LMW
POK0222
1,1-Dichloroethylene
BRL
ug/L
1.0
0.078
1
8260B
11/9/10
4:15
LMW
POK0222
1,1-Dichloropropylene
BRL
ug/L
1.0
0.061
1
8260B
11/9/10
4:15
LMW
POK0222
1,2,3-Trichlorobenzene
BRL
ug/L
2.0
0.20
1
8260B
11/9/10
4:15
LMW
POK0222
1,2,3-Trichloropropane
BRL
ug/L
1.0
0.081
1
8260B
11/9/10
4:15
LMW
POK0222
1,2,4-Trichlorobenzene
BRL
ug/L
1.0
0.10
1
8260B
11/9/10
4:15
LMW
POK0222
1,2,4-Trimethyl benzene
BRL
ug/L
1.0
0.048
1
8260B
11/9/10
4:15
LMW
POK0222
1,2-Dibromo-3-chloropropane
BRL
ug/L
2.0
0.59
1
8260B
11/9/10
4:15
LMW
POK0222
1,2-Dibromoethane
BRL
ug/L
1.0
0.14
1
8260B
11/9/10
4:15
LMW
POK0222
1,2-Dichlorobenzene
BRL
ug/L
1.0
0.076
1
8260B
11/9/10
4:15
LMW
POK0222
1,2-Dichloroethane
BRL
ug/L
1.0
0.14
1
8260B
11/9/10
4:15
LMW
POK0222
1,2-Dichloropropane
BRL
ug/L
1.0
0.13
1
8260B
11/9/10
4:15
LMW
POK0222
1,3,5-Trimethyl benzene
BRL
ug/L
1.0
0.057
1
8260B
11/9/10
4:15
LMW
POK0222
1,3-Dichlorobenzene
BRL
ug/L
1.0
0.074
1
8260B
11/9/10
4:15
LMW
POK0222
1,3-Dichloropropane
BRL
ug/L
1.0
0.11
1
8260B
11/9/10
4:15
LMW
POK0222
1,4-Dichlorobenzene
BRL
ug/L
1.0
0.068
1
8260B
11/9/10
4:15
LMW
POK0222
2,2-Dichloropropane
BRL
ug/L
2.0
0.11
1
8260B
11/9/10
4:15
LMW
POK0222
2-Chloroethyl Vinyl Ether
BRL
ug/L
2.0
0.22
1
8260B
11/9/10
4:15
LMW
POK0222
2-Chlorotoluene
BRL
ug/L
1.0
0.038
1
8260B
11/9/10
4:15
LMW
POK0222
4-Chlorotoluene
BRL
ug/L
1.0
0.053
1
8260B
11/9/10
4:15
LMW
POK0222
4-Isopropyltoluene
BRL
ug/L
1.0
0.065
1
8260B
11/9/10
4:15
LMW
POK0222
Acetone
BRL
ug/L
10
0.62
1
8260B
11/9/10
4:15
LMW
POK0222
Acrolein
BRL
ug/L
100
1.1
1
8260E
11/9/10
4:15
LMW
POK0222
Acrylonitrile
BRL
ug/L
100
0.86
1
8260B
11/9/10
4:15
LMW
POK0222
Benzene
BRL
ug/L
1.0
0.072
1
8260B
11/9/10
4:15
LMW
POK0222
Bromobenzene
BRL
ug/L
1.0
0.064
1
8260B
11/9/10
4:15
LMW
POK0222
Bromochloromethane
BRL
ug/L
1.0
0.13
1
8260B
11/9/10
4:15
LMW
POK0222
Bromodichloromethane
BRL
ug/L
1.0
0.062
1
8260B
11/9/10
4:15
LMW
POK0222
Bromoform
BRL
ug/L
1.0
0.27
1
8260B
11/9/10
4:15
LMW
POK0222
Bromomethane
BRL
ug/L
3.0
0.47
1
8260B
11/9/10
4:15
LMW
POK0222
Carbon disulfide
BRL
ug/L
5.0
1.4
1
8260B
11/9/10
4:15
LMW
POK0222
Carbon Tetrachloride
BRL
ug/L
2.0
0.12
1
8260B
11/9/10
4:15
LMW
POK0222
Chlorobenzene
BRL
ug/L
1.0
0.061
1
8260B
11/9/10
4:15
LMW
POK0222
Chloroethane
BRL
ug/L
5.0
0.13
1
8260B
11/9/10
4:15
LMW
POK0222
Chloroform
BRL
ug/L
1.0
0.089
1
8260B
11/9/10
4:15
LMW
POK0222
Chloromethane
BRL
ug/L
2.0
0.11
1
8260B
11/9/10
4:15
LMW
POK0222
cis-1,2-Dichloroethylene
BRL
ug/L
1.0
0.076
1
8260B
11/9/10
4:15
LMW
POK0222
cis-1,3-Dichloropropylene
BRL
ug/L
1.0
0.10
1
8260B
11/9/10
4:15
LMW
POK0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/17/2010
LABORATORIES INC.
Solutions-IES, Inc.
Project: Alamac Client Sample ID: TRIP BLANK
Attn: Sean K. Jarvah
Prism Sample ID: 0110138-05
1101 Nowell Road
Prism Work Order: 0110138
Raleigh, NC 27607
Sample Matrix: Water Time Collected: 11/02/10 11:35
Time Submitted: 11/03/10 15:40
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Dibromochloromethane
BRL
ug/L
1.0
0.30
1
8260B
11/9/10
4:15
LMW
POK0222
Dibromomethane
BRL
ug/L
1.0
0.13
1
8260B
11/9/10
4:15
LMW
POK0222
Dichlorodifluoromethane
BRL
ug/L
2.0
0.11
1
8260B
11/9/10
4:15
LMW
POK0222
Ethylbenzene
BRL
ug/L
1.0
0.067
1
8260B
11/9/10
4:15
LMW
POK0222
Hexachlorobutadiene
BRL
ug/L
2.0
0.36
1
8260B
11/9/10
4:15
LMW
POK0222
Isopropyl Ether
BRL
ug/L
1.0
0.043
1
8260B
11/9/10
4:15
LMW
POK0222
Isopropylbenzene (Cumene)
BRL
ug/L
1.0
0.072
1
8260B
11/9/10
4:15
LMW
POK0222
m,p-Xylenes
BRL
ug/L
2.0
0.081
1
8260B
11/9/10
4:15
LMW
POK0222
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
5.0
0.19
1
8260B
11/9/10
4:15
LMW
POK0222
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
5.0
0.90
1
8260B
11/9/10
4:15
LMW
POK0222
Methyl Isobutyl Ketone
BRL
ug/L
5.0
0.12
1
8260B
11/9/10
4:15
LMW
POK0222
Methylene Chloride
BRL
ug/L
2.0
0.44
1
8260B
11/9/10
4:15
LMW
POK0222
Methyl-tert-Butyl Ether
BRL
ug/L
1.0
0.070
1
8260B
11/9/10
4:15
LMW
POK0222
Naphthalene
BRL
ug/L
1.0
0.098
1
8260B
11/9/10
4:15
LMW
POK0222
n-Butylbenzene
BRL
ug/L
1.0
0.11
1
8260B
11/9/10
4:15
LMW
POK0222
n-Propylbenzene
BRL
ug/L
1.0
0.060
1
8260B
11/9/10
4:15
LMW
POK0222
o-Xylene
BRL
ug/L
1.0
0.046
1
8260B
11/9/10
4:15
LMW
POK0222
sec-Butylbenzene
BRL
ug/L
1.0
0.087
1
8260B
11/9/10
4:15
LMW
POK0222
Styrene
BRL
ug/L
1.0
0.047
1
8260B
11/9/10
4:15
LMW
POK0222
tert-Butylbenzene
BRL
ug/L
1.0
0.080
1
8260B
11/9/10
4:15
LMW
POK0222
Tetrachloroethylene
BRL
ug/L
1.0
0.069
1
8260B
11/9/10
4:15
LMW
POK0222
Toluene
BRL
ug/L
1.0
0.042
1
8260B
11/9/10
4:15
LMW
POK0222
trans-1,2-Dichloroethylene
BRL
ug/L
2.0
0.12
1
8260B
11/9/10
4:15
LMW
POK0222
trans-1,3-Dichloropropylene
BRL
ug/L
1.0
0.043
1
8260B
11/9/10
4:15
LMW
POK0222
Trichloroethylene
BRL
ug/L
2.0
0.054
1
8260B
11/9/10
4:15
LMW
POK0222
Trichlorofluoromethane
BRL
ug/L
2.0
0.088
1
8260B
11/9/10
4:15
LMW
POK0222
Vinyl acetate
BRL
ug/L
20
0.10
1
8260B
11/9/10
4:15
LMW
POK0222
Vinyl chloride
BRL
ug/L
2.0
0.16
1
8260B
11/9/10
4:15
LMW
POK0222
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
80-124
Dibromofluoromethane
103 %
75-129
Toluene-d8
96 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 12 of 18

,ot P R I IS M EService Analytical s
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
11/17/10
Solutions-IES, Inc. Project: Alamac
Attn: Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 0110138
Time Submitted: 11/3/10 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POK0222 - 5030B
Blank (POK0222-BLK1)
Prepared: 11/08/10 Analyzed: 11/09/10
1,1,1,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,1-Trichloroethane
BRL
1.0
ug/L
1,1,2,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,2-Trichloroethane
BRL
1.0
ug/L
1,1-Dichloroethane
BRL
1.0
ug/L
1,1-Dichloroethylene
BRL
1.0
ug/L
1,1-Dichloropropylene
BRL
1.0
ug/L
1,2,3-Trichlorobenzene
BRL
2.0
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2,4-Trimethyl benzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
1.0
ug/L
1,2-Dichlorobenzene
BRL
1.0
ug/L
1,2-Dichloroethane
BRL
1.0
ug/L
1,2-Dichloropropane
BRL
1.0
ug/L
1,3,5-Trimethyl benzene
BRL
1.0
ug/L
1,3-Dichlorobenzene
BRL
1.0
ug/L
1,3-Dichloropropane
BRL
1.0
ug/L
1,4-Dichlorobenzene
BRL
1.0
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
2-Chloroethyl Vinyl Ether
BRL
2.0
ug/L
2-Chlorotoluene
BRL
1.0
ug/L
4-Chlorotoluene
BRL
1.0
ug/L
4-Isopropyltoluene
BRL
1.0
ug/L
Acetone
BRL
10
ug/L
Acrolein
BRL
100
ug/L
Acrylonitrile
BRL
100
ug/L
Benzene
BRL
1.0
ug/L
Bromobenzene
BRL
1.0
ug/L
Bromochloromethane
BRL
1.0
ug/L
Bromodichloromethane
BRL
1.0
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
3.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
1.0
ug/L
Chloroethane
BRL
5.0
ug/L
Chloroform
BRL
1.0
ug/L
Chloromethane
BRL
2.0
ug/L
cis-1,2-Dichloroethylene
BRL
1.0
ug/L
cis-1,3-Dichloropropylene
BRL
1.0
ug/L
Dibromochloromethane
BRL
1.0
ug/L
Dibromomethane
BRL
1.0
ug/L
Dichlorodifluoromethane
BRL
2.0
ug/L
Ethylbenzene
BRL
1.0
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 13 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Solutions-IES, Inc. Project: Alamac
Attn: Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
11/17/10
Prism Work Order: 0110138
Time Submitted: 11/3/10 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POK0222 - 5030B
Blank (POK0222-BLK1)
Prepared: 11/08/10 Analyzed: 11/09/10
Hexachlorobutadiene
BRL
2.0
ug/L
Isopropyl Ether
BRL
1.0
ug/L
Isopropylbenzene (Cumene)
BRL
1.0
ug/L
m,p-Xylenes
BRL
2.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
2.0
ug/L
Methyl-tert-Butyl Ether
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
n-Butylbenzene
BRL
1.0
ug/L
n-Propylbenzene
BRL
1.0
ug/L
o-Xylene
BRL
1.0
ug/L
sec-Butylbenzene
BRL
1.0
ug/L
Styrene
BRL
1.0
ug/L
tert-Butylbenzene
BRL
1.0
ug/L
Tetrachloroethylene
BRL
1.0
ug/L
Toluene
BRL
1.0
ug/L
trans-1,2-Dichloroethylene
BRL
2.0
ug/L
trans-1,3-Dichloropropylene
BRL
1.0
ug/L
Trichloroethylene
BRL
2.0
ug/L
Trichlorofluoromethane
BRL
2.0
ug/L
Vinyl acetate
BRL
20
ug/L
Vinyl chloride
BRL
2.0
ug/L
Surrogate:4-Bromofluorobenzene
24.7
ug/L
25.0 99 80-124
Surrogate: Dibromofluoromethane
26.1
ug/L
25.0 105 75-129
Surrogate: Toluene-d8
23.5
ug/L
25.0 94 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 14 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/17/10
Solutions-IES, Inc. Project: Alamac
Attn: Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 0110138
Time Submitted: 11/3/10 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POK0222 - 5030B
LCS (POK0222-BSI)
Prepared: 11/08/10 Analyzed: 11/09/10
1,1-Dichloroethylene
59.3
1.0
ug/L
50.0
119
70-154
Benzene
51.7
1.0
ug/L
50.0
103
77-128
Chlorobenzene
50.8
1.0
ug/L
50.0
102
78-119
Toluene
52.6
1.0
ug/L
50.0
105
76-131
Trichloroethylene
55.6
2.0
ug/L
50.0
ill
77-133
Surrogate:4-Bromofluorobenzene
25.9
ug/L
25.0
103
80-124
Surrogate: Dibromofluoromethane
24.7
ug/L
25.0
99
75-129
Surrogate: Toluene-d8
24.1
ug/L
25.0
96
77-123
LCS Dup (POK0222-BSD1)
Prepared: 11/08/10 Analyzed: 11/09/10
1,1-Dichloroethylene
54.6
1.0
ug/L
50.0
109
70-154
8
200
Benzene
49.1
1.0
ug/L
50.0
98
77-128
5
200
Chlorobenzene
48.0
1.0
ug/L
50.0
96
78-119
6
200
Toluene
49.2
1.0
ug/L
50.0
98
76-131
7
200
Trichloroethylene
51.8
2.0
ug/L
50.0
104
77-133
7
200
Surrogate:4-Bromofluorobenzene
26.1
ug/L
25.0
104
80-124
Surrogate: Dibromofluoromethane
24.4
ug/L
25.0
98
75-129
Surrogate: Toluene-d8
24.2
ug/L
25.0
97
77-123
Batch POK0338 - 5030B
Blank (POK0338-BLK1)
Prepared & Analyzed: 11 /11 /10
1,1,1,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,1-Trichloroethane
BRL
1.0
ug/L
1,1,2,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,2-Trichloroethane
BRL
1.0
ug/L
1,1-Dichloroethane
BRL
1.0
ug/L
1,1-Dichloroethylene
BRL
1.0
ug/L
1,1-Dichloropropylene
BRL
1.0
ug/L
1,2,3-Trichlorobenzene
BRL
2.0
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2,4-Trimethyl benzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
1.0
ug/L
1,2-Dichlorobenzene
BRL
1.0
ug/L
1,2-Dichloroethane
BRL
1.0
ug/L
1,2-Dichloropropane
BRL
1.0
ug/L
1,3,5-Trimethyl benzene
BRL
1.0
ug/L
1,3-Dichlorobenzene
BRL
1.0
ug/L
1,3-Dichloropropane
BRL
1.0
ug/L
1,4-Dichlorobenzene
BRL
1.0
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
2-Chloroethyl Vinyl Ether
BRL
2.0
ug/L
2-Chlorotoluene
BRL
1.0
ug/L
4-Chlorotoluene
BRL
1.0
ug/L
4-Isopropyltoluene
BRL
1.0
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 15 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/17/10
Solutions-IES, Inc. Project: Alamac
Attn: Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 0110138
Time Submitted: 11/3/10 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POK0338 - 5030B
Blank (POK0338-BLK1)
Prepared & Analyzed: 11 /11 /10
Acetone
BRL
10
ug/L
Acrolein
BRL
100
ug/L
Acrylonitrile
BRL
100
ug/L
Benzene
BRL
1.0
ug/L
Bromobenzene
BRL
1.0
ug/L
Bromochloromethane
BRL
1.0
ug/L
Bromodichloromethane
BRL
1.0
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
3.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
1.0
ug/L
Chloroethane
BRL
5.0
ug/L
Chloroform
BRL
1.0
ug/L
Chloromethane
BRL
2.0
ug/L
cis-1,2-Dichloroethylene
BRL
1.0
ug/L
cis-1,3-Dichloropropylene
BRL
1.0
ug/L
Dibromochloromethane
BRL
1.0
ug/L
Dibromomethane
BRL
1.0
ug/L
Dichlorodifluoromethane
BRL
2.0
ug/L
Ethylbenzene
BRL
1.0
ug/L
Hexachlorobutadiene
BRL
2.0
ug/L
Isopropyl Ether
BRL
1.0
ug/L
Isopropylbenzene (Cumene)
BRL
1.0
ug/L
m,p-Xylenes
BRL
2.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
2.0
ug/L
Methyl-tert-Butyl Ether
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
n-Butylbenzene
BRL
1.0
ug/L
n-Propylbenzene
BRL
1.0
ug/L
o-Xylene
BRL
1.0
ug/L
sec-Butylbenzene
BRL
1.0
ug/L
Styrene
BRL
1.0
ug/L
tert-Butylbenzene
BRL
1.0
ug/L
Tetrachloroethylene
BRL
1.0
ug/L
Toluene
BRL
1.0
ug/L
trans-1,2-Dichloroethylene
BRL
2.0
ug/L
trans-1,3-Dichloropropylene
BRL
1.0
ug/L
Trichloroethylene
BRL
2.0
ug/L
Trichlorofluoromethane
BRL
2.0
ug/L
Vinyl acetate
BRL
20
ug/L
Vinyl chloride
BRL
2.0
ug/L
Surrogate:4-Bromofluorobenzene
25.1
ug/L 25.0 100 80-124
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 16 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Solutions-IES, Inc. Project: Alamac
Attn: Sean K. Jarvah
1101 Nowell Road
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
11/17/10
Prism Work Order: 0110138
Time Submitted: 11/3/10 3:4O:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POK0338 - 5030B
Blank (POK0338-BLK1)
Prepared & Analyzed: 11 /11 /10
Surrogate: Dibromofluoromethane
26.1
ug/L
25.0 104
75-129
Surrogate: Toluene-d8
22.4
ug/L
25.0 89
77-123
LCS (POK0338-BSI)
Prepared & Analyzed: 11 /11 /10
1,1-Dichloroethylene
57.2
1.0
ug/L
50.0 114
70-154
Benzene
50.2
1.0
ug/L
50.0 100
77-128
Chlorobenzene
46.0
1.0
ug/L
50.0 92
78-119
Toluene
49.8
1.0
ug/L
50.0 100
76-131
Trichloroethylene
51.8
2.0
ug/L
50.0 104
77-133
Surrogate:4-Bromofluorobenzene
25.0
ug/L
25.0 100
80-124
Surrogate: Dibromofluoromethane
24.6
ug/L
25.0 99
75-129
Surrogate: Toluene-d8
22.9
ug/L
25.0 92
77-123
LCS Dup (POK0338-BSD1)
Prepared & Analyzed: 11 /11 /10
1,1-Dichloroethylene
57.5
1.0
ug/L
50.0 115
70-154
0.5
200
Benzene
51.2
1.0
ug/L
50.0 102
77-128
2
200
Chlorobenzene
46.4
1.0
ug/L
50.0 93
78-119
0.9
200
Toluene
51.1
1.0
ug/L
50.0 102
76-131
3
200
Trichloroethylene
52.9
2.0
ug/L
50.0 106
77-133
2
200
Surrogate:4-Bromofluorobenzene
24.9
ug/L
25.0 99
80-124
Surrogate: Dibromofluoromethane
25.6
ug/L
25.0 102
75-129
Surrogate: Toluene-d8
23.0
ug/L
25.0 92
77-123
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch
Initial
Final
Date
0110138-01
POK0222
10
mL
10 mL
11/08/10
0110138-02
POK0222
10
mL
10 mL
11/08/10
0110138-02
POK0222
10
mL
10 mL
11/08/10
0110138-03
POK0222
10
mL
10 mL
11/08/10
0110138-03
POK0222
10
mL
10 mL
11/08/10
0110138-04
POK0338
10
mL
10 mL
11/11/10
0110138-05
POK0222
10
mL
10 mL
11/08/10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 17 of 18

CHAIN OF CUSTODY RECORD
PAGE --/ OF —/— QUOTE # TO ENSURE PROPER BILLING:
Project Name: 19 ,1 6 MA C-
Short Hold Analysis: (Yes) " UST Project: (Yes)
lam
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or OC Requirements
Invoice To: ��v ''j ALA," Ayo ^ , e t
Address:
Phone: 'I )11- 3' I.S-) QW2. Fax (Yes) I"o "— Purchase Order No./Billing Reference A mt- ©R A 3
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Addres5$:y cyr-l.G4al .❑
Requested Due Date Q 1 Day ❑ 2 Days 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC�
EDD Type: " Excel— Other "Working
,_PDF� Days" ❑ 6-9 Days ❑ Standard 10 days
Sc— OTHER N/A
Site Location Name: Samples received after 15:00 will be processed next business day.
X-
Site Location Physical Address: U,"l, 00-o n . A) L Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
NO
Sample Iced Upon Collection: YES_)(
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
�
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
LAB
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
(��fl REMARKS
ID NO.
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
ML
RNN-3
o�
o
VQ3
I3�
d
O
Af
7
Sampler' Signatur Sampled By (Print Name)L A4 Affiliation »J
Uponquishi , his Chain o tody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
.re
submftt in wrl in to the Prist oject Manager. There will be charges f r any changes after analyses have been initialized.
Relinquis ey: (i na re) Received 8 nature) Date Military/Hours Additional Comments: Sfte Arrnral Ttme
lSs I �� 10
Re q ed By: i ature) Receive ? t $tte Departure Time
Field Tech Fee
Relinquishe B ecew La ratori Date _
-hod of -pmenCO S S BE TAPED SHUT WITH CUSTODY SEALS OR T SPOR TION TO THE LABORATORY. 'Log- Group No.
SAMPLES OT�CEPTEDD VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORAT RY.❑
Fed Ex ❑ UPS ❑ Hand-deliveredervice ❑ Other
NPDES: UST: GR UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
O NC ❑ SC ❑ NC ❑ SC )(NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SCI ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ q Page 18 of 18
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (ZerO:Head Space)

® Microbac Laboratories, Inc.
Page I of 2
FAYETTEVILLE DIVISION
STATE CERT ID.
2592 HOPE MILLS ROAD
FAYETTEVILLE, NC 28306
NC 411
[phone] FAX [phone]
NC 437714
R. W. SANDERS, VICE PRESIDENT
USDA 43787
http://www.microbac.com E-Mail: [e-mail]
CI-IEMISIKY ' MCKUt91ULUCiY ' NUUIJ NAPhl Y • CUNSUMERYKUUUCIS
WA'IER • AIR • WASTES • MOOD • PHARMACEL) HCALS • NUTRACEUTICALS
CERTIF/CA%E OF ANALYST'S
Alamac American Knits - Lumb
Mr. Cleve Collins
Post Office Box 1347
Lumberton, NC 28359
Permit No. NC0004618
Sampler: Collins
Date Reported:
03/26/2010
Date Received:
03/02/2010
Order Number:
1003-00054
Invoice No.:
72210
Customer 9:
W003
Sample Date:
Sample Time:
0:00
S.ubect: Effluent samples - Quarterly
SNIP 'rest Method Result Date Time Tech
041. 1w�84,?�13�, COI':�pOfiEfiP.: i
CHROMIUM SM 3111 B 0.0021 mg/L 03/17/2010 5:59 RAS
002ffliieri�,
COPPER
SM 3111 B
<0.050 mg/L
03/16/2010
16:18
TDA
MERCURY, LOW
EPA 1631E
3.13 ng/L
03/10/2010
10:47
CHI
PHENOL
EPA 420.1
0.006 mg/L
03/23/2010
0:00
ECI
SULFIDE
SM 4500 S2 D
<0.1 rng/L
03/08/2010
16:00
DCR
[VOLATILES]
EPA 624
0:00
1,2-cis-DICHLOROEi"HYLENE
EPA 624
<1.0 pg/L
03/11/2010
16:14
CHI
PERCHLOROEI-HYLENE
EPA 624
<1.0 ug/L
03/11/2010
16:14
CHI
TRICHLOROEiHYLENE
EPA 624
<1.0 ug/L
03/11/2010
16:14
CHI
VINYL CHLORIDE
EPA 624
<2.0 pg/L
03/11/2010
16:14
CHI
ZINC
SM 3111 B
0.034 ITig/L
03/16/2010
10:42
TDA
ooffilunt Grab (Qupiica�e)
MERCURY, LOW EPA 1631E 3.40 ng/L 03/10/2010 10:49 CHI
0C4 Tr ii, ��it'1if
MERCURY, LOW EPA 1.631E <0.500 ng/L 03/10/2010 10:52 CHI
TECI I I1\I1TIA1S: CHI-Microbac, Chicagoland; PIT-Microbac, Pittsburgh; CMP-Microbac, Camp Hill; BAP/AJF-Microbac, Greensboro;
All other initials are Microbac, Fayetteville except as noted.
LAB CODES: N/D = Noae Detected N/F = None Found < = Less than > = Greater than Est. = Estimated
MEMBER
The data and other information contained on this, and other accompanying documents, represent only the saniple(s) analyzed and is rendered upon the
condition that it is not to be reproduced wholly or in part for advertising or other purposes without written approval from the laboratory. W
USDA-EPA-NIDSH testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

Fayetteville Division
2592 Hope Mills Rd 8-B Wendy Court
Fayetteville, NC 28306 Greensboro, NC 27409
910.864,1920 Phone [phone] Phone
910.864,8774 Fax [phone] Fax
Certificate of Analysis
Alamac American Knits - Lumb
Mr. Cleve Collins Project: Effluent Samples - Qtrly Date Reported: June 24, 2010
Post Office Box 1347 Date Received: ,hme 08, 2010
Lumberton NC, 28359 Sampled By: Cleve Collins Date Sampled: ,Tune O8, 2010
Effluent, Composite
1006276-01
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: Microbac - Fayetteville Division
Chromium
—0.003
mg/L
6/28/10 9:23
RAS
SM 20th Ed. 3113 .B
I
Effluent, Grab
1006276-02
Analyte
Result
Unit
Analysis Date/Tine
Analyst
Method
Qualifier
Analyzed by: Microbac - Chicagoland Division
cis-1,2-Dichloroethene
<0.0010
mg/L
BR
EPA 624
Tetrachloroetliene
<0.0010
mg/L
BR
EPA 624
Trichloroethene
<0.0010
mg/L
BR
EPA 624
Vinyl chloride
<0.0020
mg/L
BR
EPA 624
Mercury, Low -Level
3.26
ng/L
6/16/10 16:37
RPL
EPA 1631E
Analyzed by: Microbac - Fayetteville Division
Copper,—
—<0.0500
mg/L
6/13/10 12:17
TDA
SM 20th Ed. 3111 B
Phenolics, Total Recoverable
_<0.0100
mg/L,
6/24/10 12:00
AJF
EPA 420.1
Sulfide, Total--
<1.00
mg/L
6/15/10 8:25
AJF
SM 20th Ed. 4500-S, F,
Zinc
0.0330
mg/L
7/21/10 14:52
RAS
SM 20th Ed, 3111 B
Effluent
- Duplicate, Grab
1006276-03
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: ficrobac - chicagoland Division
Mercury, Low -Level
3.2
ng/L
6/16/10 16:39
RPL
EPA 1631.E
Trip Blank
1006276-04
Analyte
Result
Unit
Analysis Date/Tine
Analyst
Method
Qualifier
Analyzed by: Microbac - Chicagoland Division
Mercury. Low -Level
<.05
ng/L
6/16/10 16:42
RPL
EPA 1631E
State Certifications: Respectfully Submitted
NCDNR #11,#693 �y
NCDOH #37714, #37795 X. �`
USDA #3787 R. W. sanders, VP/Muiaging Director
Tharlk you for your business. We inrile porn;feedGnck on urn' lcreT q%service !o you. Please comae! rGe iPTlmmgin¢Director, Ran Sanders a1910-S6a-I910. Jnrnes Nokes. Precidenl. N
,jnakes a)rrricroLnaannr or' I'rer-or Bgpce. CEO, at ibopcern!ruicroLaaconr ivah any conuuenls orsu,-�,eslions.
Page 1 of 2

Fayetteville Division
2592 Hope Mills Rd 8-B Wendy Court
Fayetteville, NC 28306 Greensboro, NC 27409
910.864.1920 Phone [phone] Phone
910.864.8774 Fax [phone] Fax
Certificate of Analysis
Alamac American Knits - Lumb
Mr. Cleve Collins Project: Effluent Samples - Qtrly, Pt. 1 Date Reported: October 11, , 20 1C
Post Office Box 1347 Date Received: September 14
Lumberton NC, 28359 Sampled By: Cleve Collins Date Sampled: September 14, 201C
Effluent, Composite
1009230-01
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: Microbac - Fayetteville Division
Chromium
0.002
mg/L
9/28/10 12:08
RAS
SM 20th Ed. 3113 B
Effluent, Grab
1009230-02
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: ECI
Phenolics, Total Recoverable
<0.004
mg/L
9/21/10 0:00
ECI
EPA 420.1
Sulfide, Total
0.08
mg/L
9/16/10 0:00
ECI
SM 20th Ed. 4500-S, D
Analyzed by: Microbac - Fayetteville Division
Copper
<0.0500
mg/L
9/22/10 14:17
TDA
SM 20th Ed. 3111 B
Zinc
0.0100
mg/L
9/22/10 10:37
TDA
SM 20th Ed. 3111 B
Analyzed by: Microbac Laboratories, Inc.
- Chicagoland
cis-1,2-Dichloroethene
<0.0010
mg/L
9/23/10 15:41
JLN
EPA 624 Rev 7/95
U
Tetrachloroethene
<0.0010
mg/L
9/23/10 15:41
JLN
EPA 624 Rev 7/95
U
Trichloroethene
<0.0010
mg/L
9/23/10 15:41
JLN
EPA 624 Rev 7/95
U
Vinyl chloride
<0.0020
mg/L
9/23/10 15:41
JLN
EPA 624 Rev 7/95
U
Qualifier Definitions
U Analyte included in the analysis, but not detected
State Certifications: Respectfully Submitted
NCDNR #11, #693
NCDOH #37714, #37795�
USDA #3787 R. W. Sanders, VP/Managing Director
Thank you for your business. We invite your feedback on our level ofservice to you. Please contact the VP/Managing Director, Ron Sanders at 910-864-1920, James Nokes, President, of
[e-mail] or Trevor Boyce, CGO, at [e-mail] with any comments or suggestions.
Page 1 of 1

3
Fayetteville Division
25921-1opc Mills Rd
Pa.yetteville, NC. 28306
910,864,1920 Phone
910,564.8774.Fax
Certificate of Analysis
Ala nac American Knits - crumb T:)wo Reported: December 31, 2010
Mr, Cleve Collins Project; WW Snmples - Qtrly
Date Received: DCCCmber 14, 2610
Past of -rice Box 134 7
Lu}nbcrton NC, 28359 Sampled fly: Cleve Collins Dnt4 Sampl4il; Dcaemher 14, 2010
E ffluenL Grab
1012312-01
Annlyte Result
t.)nit
Analysis Date/Time
Analyst
Method.
Qualifier
Analyzed by: Microbac . Fayetteville Division
Copper 0.0560
mg/L
12/20/10 10:03
RAS
SM 20th Ed. 3111 B
Zinc 0.0240
mg/L
12/28/10 14:23
RAS
SM 20th Ed. 3111 B
Analyzed by: Mlcma ac Laboratories, Inc. - chicagoland
cis-1,2-Dichloroethene <0.0010
mg/1'
12/20/10 16:10
JLN
1 PA 624 Rev 7/95
t,J
Tet►-aehioroethene <0.0010
mg/L
12/20/10 16:10
JLN
EPA 624 Rev 7/95
U
Trichloroethene <0.0010
mg/L
12/20/10 16:10
11.,N
FPA. 624 Rev 7/95
U
Vinyl chloride <0.0020
mg/l,
12/20/10 16:10
JLN
EPA 624 Rev 7/95
U
llJMuent, Coils DOSite
1012312-02
Ea.iyte Result
1Jitit
Analysis Date/Time
Analyst
Method
QualiCer
Analyzed by: Mltrabac - Fayetteville Division
Chromium 0.002
mg/L
12/28/10 11:22
RAS
$M 20th Ed. 3113 B
QuAlificr Definitions
Ana.lyte incluciccl in the ;inalysi:3, but ri«t detected
Stye certifications; Respectfully Submitted
NCDNR #11
NCDOW 037714
USDA #3787 R, W, Sanders, VP/Managing Director
ThinK you for your business. We fnrllc ymrr./cr:dhoclr rnt Ut[r level nj,SRYV(Cu tr) }wrr. Plcrrve enrriaer rfre. ITrI {anaP,ln.> 1�rrecYor, 12n r Srnrdera al 910•Rf,4.��?0, .lrrnrarc Nr)k�s, !'YestcJrnfr, ur
/rrnkcs( nrira r,Gcrc.c rn or Trevor Ggrcv, C O, at rhnpr_r.�7m/ rr)har.ennr rr dla arry cvnrrrrerare nr srrggedlnrra.
Pagc t of ]

APPENDIX B
FIELD NOTES