3612_DukeAllen_RABLF_Mar2022_LeachateReport_FID1693753_20220704

�> DUKE
ENERGY
July 2, 2022
Ms. Sarah Moutos
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
1646 Mail Service Center
Raleigh, NC 27699-1646
526 South Church Street
Charlotte, NC 28202
Mailing Address:
PO Box 1006
Mail Code EC13K
Charlotte, NC 28201-1006
704 382 7171
Subject: Semi-annual Leachate Sampling Results — March 2022 Event
Duke Energy Carolinas, LLC
Allen Steam Station
Retired Ash Basin Ash Landfill, Phase I, Cells 1 and 2, Permit #36-12
Dear Ms. Moutos:
In accordance with the current landfill Operations Plan, Duke Energy is providing the results of semi-
annual leachate sampling for the Allen Steam Station (Allen or Station) Retired Ash Basin (RAB) Ash
Landfill located in Gaston County, North Carolina.
On March 7, 2022, leachate samples were collected from the leachate collection system at sample ports
for Cell 1 and Cell 2 as depicted on Figure 1.
For the March 2022 leachate sampling event, total dissolved solids (TDS) exceeded the laboratory
method residue limit on the samples collected from Cell 1 and Cell 2 on March 7, 2022. The original TDS
analysis was conducted on the last day prior to expiration of the allowable holding time; therefore, the
leachate samples for TDS from Cell 1 and Cell 2 were recollected on March 17, 2022
Samples were collected by Duke Energy personnel. A summary of sampling results can be found in
Table 1. Laboratory analytical and field forms are provided as Attachments 1 and 2, respectively. The
parameters tested are not bound by state groundwater or surface water standards.
The Allen RAB Ash Landfill leachate is sampled semi-annually during March and September. The next
landfill leachate sampling event will occur during September 2022 with documentation to follow.
If you have any questions or concerns, please contact me at 704-382-7171 or at
Courtney.Murphy(aDduke-energy.com.
Sincerely, dwkilwokol
Courtney W. Murphy, P.G.
Environmental Services
Cc (via email): Mr. Jeff Flanagan — Allen Steam Station
Mr. Scott Harris — Allen Steam Station
Mr. Randy Gantt — Allen Steam Station
Ms. Erica Tuchbaum — Duke Energy Corporation
Ms. Kimberlee Witt — Duke Energy Corporation
Page 1 of 1

DENR USE ONLY [:]Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No } Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management- Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(1).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Duke Energy Carolinas, LLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Cnnrtnav W Murnhv PC Phone: l7041 3A9-7171
E-mail: (nurtnPv MurnhvMduka-anarnv rnm
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Retired Ash Basin (RAB) Ash Original- March 7, 2022
Landfill 253 Plant Allen Rd. 36-12 .0500 TDS Resample- March 17,
Duke Energy Belmont, NC 28012 2022
Allen Steam Station
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Methane gas monitoring data
Groundwater monitoring data from private water supply wells ❑ Corrective action data (specify)
X Leachate monitoring data ❑
Surface water monitoring data Other(specify)
Notification attached?
e No. No groundwater or surface water standards were exceeded.
Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 213 surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Courtney W. Murphy, P.G. Lead Environmental Specialist [phone]
Facility Representative Name (Print) Title (Area Code) Telephone Number
Courtney W. Murphy,�.G. Digitally signed by Courtney W. Murphy, P.G. 7I212022 Affix NC Licensed! Professions[ Geologist Seal
YDate:2022.07.041633:52-04'00'
Signature Date
Duke Energy Corporation, Mail Code EC13K, P.O. Box 1006, Charlotte, NC 28201-1006
Facility Representative Address
#F-0566
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 612009
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Notes:
Table 1- Leachate Analytical Data
Allen Steam Station
Retired Ash Basin (RAB) Ash Landfill (Permit No. 36-12)
Constituent
Analytical Result
(µg/L unless otherwise noted)
March 7, 2022
Cell 1
Cell 2
Antimony
0.104 U
0.104 U
Arsenic
18.4
53.7
Barium
28
34
Beryllium
1.68
2.12
Boron
62,200
166,000
Cadmium
5.89
0.937 J
Chloride
92 mg/L
150 mg/L
Chromium
1 U
1 U
Cobalt
1,060
1,270
Copper
0.131 mg/L
0.048 mg/L
Fluoride
0.35 J mg/L
0.87 J mg/L
Iron
30
26
Lead
1.08
0.507 J
Manganese
13,000
14,700
Mercury
0.02 J
0.02 J
Nickel
528
79
Nitrate (as N)
70 mg-N/L
30 mg-N/L
pH
4.28 S.U.
4.17 S.U.
pH*
4.15 S.U.
4.35 S.U.
Selenium
28.9
153
Silver
0.035 U
0.054 J
Sulfate
3,800 mg/L
2,900 mg/L
Temperature ('C)
21.0 °C
21.0 °C
Temperature (°C)*
18.0 °C
19.0 °C
TDS
5,860 mg/L
5,040 mg/L
TDS*
4,550 mg/L
4,100mg/L
Thallium
6.53
1.07
Vanadium
0.405
0.114 U
Zinc
0.535 mg/L
0.122 mg/L
µg/L = micrograms per liter
mg/L = milligrams per liter
mg-N/L = milligrams of Nitrogen per liter
S.U. = standard units
.0 = degrees Celcius
* For the March 2022 leachate sampling event, TDS exceeded the laboratory method residue limit on
the samples collected from Cell 1 and Cell 2 on March 7, 2022. The original TDS analysis was conducted
on the last day prior to expiration of the allowable holding time; therefore, the leachate samples for
TDS from Cell 1 and Cell 2 were recollected on March 17, 2022. pH and temperature were measured
and recorded again for the March 17, 2022 resample of TDS.

Attachment 1
Allen Retired Ash Basin (RAB) Ash Landfill
Semi -Annual Monitoring Event
Leachate Analytical Results

DUE Analytical Laboratory Page 1 of 16
ENERGY
Y
Order Number:
Project Name:
Task Code:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J22020330
ALLEN - GW LEACHATE
LCS
C Murphy, R Gantt,D O Brien, B Moeller, J Stowe
Allen Steam Station
253 Plant Allen Road
Belmont, NC 28012
Peggy Kendall
Phone: [phone]
" Date:
Pegg'-yfCendall
Note: The TDS samples were recollected and will report under job order J22030358.
3/25/2022
QC Note: LCS-Cell 1 Hg MS/MSD recoveries were outside the QC limits. The blank and LCS were within the control limits. The
sample result was <0.05 ug/L.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 2 of 16
Sample ID
Plant/Station
Collection
Date and Time
Collected By
Sample Description
2022003886
ALLEN
07-Mar-22 11:50 AM
Connor Zahora
ALN LCS-CELL1
2022003887
ALLEN
07-Mar-22 12:00 PM
Connor Zahora
ALN LCS-CELL2
2022003888
ALLEN
07-Mar-22 12:10 PM
Connor Zahora
ALN FB-20220307-1210
3 Total Samples

Page 3 of 16
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals❑ Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
d❑ Job Summary Report
J❑ Sample Identification
❑ Technical Validation of Data Package
d❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑ Chain of Custody
❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 3/25/2022

Certificate of Laboratory Analysis Page 4 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Site: ALN LCS-CELL1 Sample #: 2022003886
Collection Date: 03/07/2022 11:50 AM Loc code: ALN LCS-CELL1 Matrix: GW RCRA
Analyte
Result
Units Qualifiers
RDL
MDL
DF
Method
Analysis Date/Time
Analyst
INORGANIC IONS BY IC - Q22030124
Chloride
92
mg/L
5
0.0154
50
EPA 9056A
03/08/2022 08:20
BGN9034
Fluoride
0.35 J
mg/L
5
0.0479
50
EPA 9056A
03/08/2022 08:20
BGN9034
Nitrate
310
mg/L
5
0.0209
50
EPA 9056A
03/08/2022 08:20
BGN9034
Nitrate as N
70
mg-N/L
1.15
0.002
50
EPA 9056A
03/08/2022 08:20
BGN9034
Sulfate
3800
mg/L
100
0.0428
1000
EPA 9056A
03/08/2022 08:20
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q22030207
Mercury (Hg)
0.02 J
ug/L M
0.05
0.01
1
EPA 7470A
03/10/2022 13:28
JAA5429
TOTAL RECOVERABLE METALS BY ICP - Q22030228
Barium (Ba)
0.028
mg/L
0.005
0.002
1
SW 6010D
03/16/2022 13:52
DMFRANC
Boron (B)
62.2
mg/L
5
0.005
100
SW 6010D
03/16/2022 13:52
DMFRANC
Chromium (Cr)
0.001 U
mg/L
0.005
0.001
1
SW 6010D
03/16/2022 13:52
DMFRANC
Copper (Cu)
0.131
mg/L
0.005
0.001
1
SW 6010D
03/16/2022 13:52
DMFRANC
Iron (Fe)
0.030
mg/L
0.01
0.004
1
SW 6010D
03/16/2022 13:52
DMFRANC
Manganese (Mn)
13.0
mg/L
0.005
0.001
1
SW 6010D
03/16/2022 13:52
DMFRANC
Nickel (Ni)
0.528
mg/L
0.005
0.001
1
SW 6010D
03/16/2022 13:52
DMFRANC
Zinc (Zn)
0.535
mg/L
0.005
0.004
1
SW 6010D
03/16/2022 13:52
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q22030237
Antimony (Sb)
0.104 U
ug/L
1
0.104
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Arsenic (As)
18.4
ug/L
1
0.111
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Beryllium (Be)
1.68
ug/L
1
0.249
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Cadmium (Cd)
5.89
ug/L
1
0.032
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Cobalt (Co)
1060
ug/L
20
0.077
20
SW 6020B
03/15/2022 18:58
CWSPEN3
Lead (Pb)
1.08
ug/L
1
0.037
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Selenium (Se)
28.9
ug/L
1
0.193
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Silver (Ag)
0.035 U
ug/L
1
0.035
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Thallium (TI) Low Level
6.53
ug/L
0.2
0.041
1
SW 6020B
03/15/2022 18:58
CWSPEN3
Vanadium (V) Low Level
0.405
ug/L
0.3
0.114
1
SW 6020B
03/15/2022 18:58
CWSPEN3
TOTAL DISSOLVED SOLIDS - Q22030217
TDS
5860
mg/L H1
125
25
1
SM2540C
03/15/202213:00
Ghutchi

Certificate of Laboratory Analysis Page 5 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Site: ALN LCS-CELL2 Sample #: 2022003887
Collection Date: 03/07/2022 12:00 PM Loc code: ALN LCS-CELL2 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF
INORGANIC IONS BY IC - Q22030124
Chloride
150
mg/L
Fluoride
0.87 J
mg/L
Nitrate
130
mg/L
Nitrate as N
30
mg-N/L
Sulfate
2900
mg/L
MERCURY (COLD VAPOR) IN WATER - Q22030207
Mercury (Hg)
0.02 J
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q22030228
Barium (Ba)
0.034
mg/L
Boron (B)
166
mg/L
Chromium (Cr)
0.001 U
mg/L
Copper (Cu)
0.048
mg/L
Iron (Fe)
0.026
mg/L
Manganese (Mn)
14.7
mg/L
Nickel (Ni)
0.079
mg/L
Zinc (Zn)
0.122
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
- Q22030237
Antimony (Sb)
0.104 U
ug/L
Arsenic (As)
53.7
ug/L
Beryllium (Be)
2.12
ug/L
Cadmium (Cd)
0.937 J
ug/L
Cobalt (Co)
1270
ug/L
Lead (Pb)
0.507 J
ug/L
Selenium (Se)
153
ug/L
Silver (Ag)
0.054 J
ug/L
Thallium (TI) Low Level
1.07
ug/L
Vanadium (V) Low Level
0.114 U
ug/L
TOTAL DISSOLVED SOLIDS - Q22030217
TDS
5040
mg/L H1
Method Analysis Date/Time Analyst
5
0.0154
50
EPA 9056A
03/08/2022 08:35
BGN9034
5
0.0479
50
EPA 9056A
03/08/2022 08:35
BGN9034
5
0.0209
50
EPA 9056A
03/08/2022 08:35
BGN9034
1.15
0.002
50
EPA 9056A
03/08/2022 08:35
BGN9034
100
0.0428
1000
EPA 9056A
03/08/2022 08:35
BGN9034
0.05
0.01
1
EPA 7470A
03/10/2022 13:34
JAA5429
0.005
0.002
1
SW 6010D
03/16/2022 13:57
DMFRANC
5
0.005
100
SW 6010D
03/16/2022 13:57
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 13:57
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 13:57
DMFRANC
0.01
0.004
1
SW 6010D
03/16/2022 13:57
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 13:57
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 13:57
DMFRANC
0.005
0.004
1
SW 6010D
03/16/2022 13:57
DMFRANC
1
0.104
1
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.111
1
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.249
1
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.032
1
SW 6020B
03/16/2022 17:26
CWSPEN3
20
0.077
20
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.037
1
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.193
1
SW 6020B
03/16/2022 17:26
CWSPEN3
1
0.035
1
SW 6020B
03/16/2022 17:26
CWSPEN3
0.2
0.041
1
SW 6020B
03/16/2022 17:26
CWSPEN3
0.3
0.114
1
SW 6020B
03/16/2022 17:26
CWSPEN3
125
25
1
SM2540C
03/15/202213:00
Ghutchi

Certificate of Laboratory Analysis Page 6 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Site: ALN FB-20220307-1210 Field Blank Sample #: 2022003888
Collection Date: 03/07/2022 12:10 PM Loc code: ALN FB Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF
INORGANIC IONS BY IC - Q22030124
Chloride 0.0154 U mg/L
Fluoride 0.0479 U mg/L
Nitrate 0.04 J mg/L
Nitrate as N 0.01 J mg-N/L
Sulfate 0.0428 U mg/L
MERCURY (COLD VAPOR) IN WATER - Q22030207
Mercury (Hg) 0.01 J ug/L
TOTAL RECOVERABLE METALS BY ICP - Q22030228
Barium (Ba)
0.002 U
mg/L
Boron (B)
0.006 J
mg/L
Chromium (Cr)
0.001 U
mg/L
Copper (Cu)
0.003 J
mg/L
Iron (Fe)
0.004 U
mg/L
Manganese (Mn)
0.001 U
mg/L
Nickel (Ni)
0.001 U
mg/L
Zinc (Zn)
0.004 U
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS - Q22030237
Antimony (Sb)
0.104 U
ug/L
Arsenic (As)
0.124 J
ug/L
Beryllium (Be)
0.249 U
ug/L
Cadmium (Cd)
0.032 U
ug/L
Cobalt (Co)
0.077 U
ug/L
Lead (Pb)
0.037 U
ug/L
Selenium (Se)
0.406 J
ug/L
Silver (Ag)
0.035 U
ug/L
Thallium (TI) Low Level
0.068 J
ug/L
Vanadium (V) Low Level
0.114 U
ug/L
Method Analysis Date/Time Analyst
0.1
0.0154
1
EPA 9056A
03/08/2022 08:06
BGN9034
0.1
0.0479
1
EPA 9056A
03/08/2022 08:06
BGN9034
0.1
0.0209
1
EPA 9056A
03/08/2022 08:06
BGN9034
0.023
0.002
1
EPA 9056A
03/08/2022 08:06
BGN9034
0.1
0.0428
1
EPA 9056A
03/08/2022 08:06
BGN9034
0.05
0.01
1
EPA 7470A
03/10/2022 13:36
JAA5429
0.005
0.002
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.05
0.005
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.01
0.004
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.005
0.001
1
SW 6010D
03/16/2022 14:02
DMFRANC
0.005
0.004
1
SW 6010D
03/16/2022 14:02
DMFRANC
1
0.104
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.111
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.249
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.032
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.077
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.037
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.193
1
SW 6020B
03/16/2022 17:09
CWSPEN3
1
0.035
1
SW 6020B
03/16/2022 17:09
CWSPEN3
0.2
0.041
1
SW 6020B
03/16/2022 17:09
CWSPEN3
0.3
0.114
1
SW 6020B
03/16/2022 17:09
CWSPEN3

Certificate of Laboratory Analysis Page 7 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Qualifiers:
H1 Sample Analysis performed past the recommended holding time. The results should be considered as estimated values.
J Analyte detected above the MDL, but below the RL. Analyte concentration should be considered an estimate.
M Matrix Spike and/or Matrix Spike Duplicate recovery was outside of the control limits. The associated Laboratory Control
Spike (LCS) recovery was acceptable.
N1: The TDS samples were analyzed within the method recommended holding time of 7-days; however,the results
exceeded the method residue limit. The samples were reanalyzed outside of the holding time and were reported with
qualified results.

Certificate of Laboratory Analysis Page 8 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030124 Dionex INORGANIC IONS BY IC
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Chloride
0
0
mg/L
1
0.0154
0.1
< MDL
Fluoride
0
0
mg/L
1
0.0479
0.1
< MDL
Nitrate
0
0
mg/L
1
0.0209
0.1
< MDL
Sulfate
0.002
0.002
mg/L
1
0.0428
0.1
< MDL
LCS # 1
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
Chloride
1.98
1.98
mg/L
1
0.0154
2
99
90
110
Fluoride
2.02
2.02
mg/L
1
0.0479
2
101
90
110
Nitrate
2.04
2.04
mg/L
1
0.0209
2
102
90
110
Sulfate
1.9
1.9
mg/L
1
0.0428
2
95
90
110
MS # 1
Parent Sample:
J22030125 -- 2022005890
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
Qualifier
Chloride
3.56
3.56
mg/L
1
0.0154
2
99.2
80
120
Fluoride
1.96
1.96
mg/L
1
0.0479
2
97.4
80
120
Nitrate
5.39
5.39
mg/L
1
0.0209
2
100
80
120
Sulfate
3.03
3.03
mg/L
1
0.0428
2
103
80
120
MSD # 1
Parent Sample:
J22030125 -- 2022005890
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
RPD
Qualifier
Chloride
3.56
3.56
mg/L
1
0.0154
2
99.3
80
120
0.101
Fluoride
1.96
1.96
mg/L
1
0.0479
2
97.5
80
120
0.154
Nitrate
5.38
5.38
mg/L
1
0.0209
2
100
80
120
0.349
Sulfate
3.03
3.03
mg/L
1
0.0428
2
103
80
120
0

Certificate of Laboratory Analysis Page 9 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030207 HG 7470 MERCURY (COLD VAPOR) IN WATER
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
0.01
0.01
ug/L
1
0.01
0.05
= MDL
Blank # 2
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
0.002
0.002
ug/L
1
0.01
0.05
< MDL
Blank # 3
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
0.003
0.003
ug/L
1
0.01
0.05
< MDL
Blank # 4
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
0.009
0.009
ug/L
1
0.01
0.05
< MDL
MDL—Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
Mercury (Hg)
0.006
0.006
ug/L
1
0.01
0.05
< MDL
LCS # 1
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery LCL UCL
Qualifier
Mercury (Hg)
1.87
1.87
ug/L
1
0.01
2
93.3 85 115
LCS # 2
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
1.87
1.87
ug/L
1
0.01
2
93.5
85 115
MDL_Spike # 1
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.051
0.051
ug/L
1
0.01
0.05
102
MS # 1
Parent Sample:
J22020330 -- 2022003886
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.284
0.284
ug/L
1
0.01
1
26.2
75 125
M
MSD # 1
Parent Sample:
J22020330 -- 2022003886
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL RPD
Qualifier
Mercury (Hg)
0.278
0.278
ug/L
1
0.01
1
25.6
75 125 2.32
M
MS # 2
Parent Sample:
J22030086 -- 2022005662
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL UCL
Qualifier
Mercury (Hg)
0.786
0.786
ug/L
1
0.01
1
77.4
75 125

Certificate of Laboratory Analysis Page 10 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030207 HG 7470 MERCURY (COLD VAPOR) IN WATER
MSD # 2
Parent Sample:
J22030086
-- 2022005662
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL RPD
Qualifier
Mercury (Hg)
0.797
0.797
ug/L
1
0.01
1
78.5
75
125 1.41
MS # 3
Parent Sample:
J22030086
-- 2022005672
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
Mercury (Hg)
0.613
0.613
ug/L
1
0.01
1
61.3
75
125
M
MSD # 3
Parent Sample:
J22030086
-- 2022005672
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL RPD
Qualifier
Mercury (Hg)
0.577
0.577
ug/L
1
0.01
1
57.7
75
125 6.05
M
Qualifiers:
M Matrix Spike and/or Matrix Spike Duplicate recovery was outside of the control limits. The associated
Laboratory Control Spike (LCS) recovery was acceptable.

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030228 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Barium (Ba)
-0.000151
-0.000151
mg/L
1
0.002
0.005
< MDL
Boron (B)
-0.000416
-0.000416
mg/L
1
0.005
0.05
< MDL
Chromium (Cr)
-0.000973
-0.000973
mg/L
1
0.001
0.005
< MDL
Copper (Cu)
-0.000232
-0.000232
mg/L
1
0.001
0.005
< MDL
Iron (Fe)
-0.000833
-0.000833
mg/L
1
0.004
0.01
< MDL
Manganese (Mn)
-0.000183
-0.000183
mg/L
1
0.001
0.005
< MDL
Nickel (Ni)
-0.000314
-0.000314
mg/L
1
0.001
0.005
< MDL
Zinc (Zn)
-0.000801
-0.000801
mg/L
1
0.004
0.005
< MDL
LCS # 1
Page 11 of 16
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Barium (Ba)
5.09
5.09
mg/L
1
0.002
5
102
80
120
Boron (B)
5.01
5.01
mg/L
1
0.005
5
100
80
120
Chromium (Cr)
5.05
5.05
mg/L
1
0.001
5
101
80
120
Copper (Cu)
5.02
5.02
mg/L
1
0.001
5
100
80
120
Iron (Fe)
5.04
5.04
mg/L
1
0.004
5
101
80
120
Manganese (Mn)
4.99
4.99
mg/L
1
0.001
5
99.9
80
120
Nickel (Ni)
5.14
5.14
mg/L
1
0.001
5
103
80
120
Zinc (Zn)
5.16
5.16
mg/L
1
0.004
5
103
80
120
MS # 1
Parent Sample:
J22030086
-- 2022005675
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Barium (Ba)
5.18
5.18
mg/L
1
0.002
5
102
75
125
Boron (B)
5.74
5.74
mg/L
1
0.005
5
101
75
125
Chromium (Cr)
5
5
mg/L
1
0.001
5
100
75
125
Copper (Cu)
5
5
mg/L
1
0.001
5
99.9
75
125
Iron (Fe)
5.1
5.1
mg/L
1
0.004
5
101
75
125
Manganese (Mn)
5.1
5.1
mg/L
1
0.001
5
99.4
75
125
Nickel (Ni)
5.04
5.04
mg/L
1
0.001
5
101
75
125
Zinc (Zn)
5.07
5.07
mg/L
1
0.004
5
101
75
125
MSD # 1
Parent Sample:
J22030086
-- 2022005675
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
RPD
Barium (Ba)
5.14
5.14
mg/L
1
0.002
5
101
75
125
0.62
Boron (B)
5.68
5.68
mg/L
1
0.005
5
99.6
75
125
0.963
Chromium (Cr)
4.97
4.97
mg/L
1
0.001
5
99.4
75
125
0.722
Copper (Cu)
4.97
4.97
mg/L
1
0.001
5
99.4
75
125
0.501
Iron (Fe)
5.06
5.06
mg/L
1
0.004
5
99.7
75
125
0.826
Manganese (Mn)
5.05
5.05
mg/L
1
0.001
5
98.5
75
125
0.886
Nickel (Ni)
5.02
5.02
mg/L
1
0.001
5
100
75
125
0.457
Qualifier
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 12 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030228 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
MSD # 1 Parent Sample: J22030086 -- 2022005675
Parameter Measured Final Units Dil MDL Spike % Recovery LCL UCL RPD Qualifier
Zinc (Zn) 5.03 5.03 mg/L 1 0.004 5 100 75 125 0.852

Certificate of Laboratory Analysis Page 13 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030237 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
Parameter
Measured
Final
Units
Dil
MDL
RDL
Relative Concentration
Antimony (Sb)
-0.039
-0.039
ug/L
1
0.104
1
< MDL
Arsenic (As)
-0.009
-0.009
ug/L
1
0.111
1
< MDL
Beryllium (Be)
-0.02
-0.02
ug/L
1
0.249
1
< MDL
Cadmium (Cd)
-0.017
-0.017
ug/L
1
0.032
1
< MDL
Cobalt (Co)
-0.023
-0.023
ug/L
1
0.077
1
< MDL
Lead (Pb)
-0.017
-0.017
ug/L
1
0.037
1
< MDL
Selenium (Se)
-0.063
-0.063
ug/L
1
0.193
1
< MDL
Silver (Ag)
-0.004
-0.004
ug/L
1
0.035
1
< MDL
Thallium (TI) Low Level
0.004
0.004
ug/L
1
0.041
0.2
< MDL
Vanadium (V) Low Level
-0.009
-0.009
ug/L
1
0.114
0.3
< MDL
LCS # 1
Parameter
Measured
Final
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
Antimony (Sb)
49.3
49.3
ug/L
1
0.104
50
98.6
80
120
Arsenic (As)
50.6
50.6
ug/L
1
0.111
50
101
80
120
Beryllium (Be)
51.6
51.6
ug/L
1
0.249
50
103
80
120
Cadmium (Cd)
51.3
51.3
ug/L
1
0.032
50
103
80
120
Cobalt (Co)
50.7
50.7
ug/L
1
0.077
50
101
80
120
Lead (Pb)
52
52
ug/L
1
0.037
50
104
80
120
Selenium (Se)
49
49
ug/L
1
0.193
50
98
80
120
Silver (Ag)
51.7
51.7
ug/L
1
0.035
50
103
80
120
Thallium (TI) Low Level
50.6
50.6
ug/L
1
0.041
50
101
80
120
Vanadium (V) Low Level
50.6
50.6
ug/L
1
0.114
50
101
80
120
MS # 1
Parent Sample:
J22030086 -- 2022005676
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Antimony (Sb)
51.4
51.4
ug/L
1
0.104
50
102
75
125
Arsenic (As)
49.7
49.7
ug/L
1
0.111
50
99.2
75
125
Beryllium (Be)
52.2
52.2
ug/L
1
0.249
50
104
75
125
Cadmium (Cd)
50.6
50.6
ug/L
1
0.032
50
101
75
125
Cobalt (Co)
48.7
48.7
ug/L
1
0.077
50
96.9
75
125
Lead (Pb)
51.3
51.3
ug/L
1
0.037
50
103
75
125
Selenium (Se)
47.4
47.4
ug/L
1
0.193
50
94.7
75
125
Silver (Ag)
50.7
50.7
ug/L
1
0.035
50
101
75
125
Thallium (TI) Low Level
50.1
50.1
ug/L
1
0.041
50
100
75
125
Vanadium (V) Low Level
52.2
52.2
ug/L
1
0.114
50
103
75
125
MSD # 1
Parent Sample:
J22030086 -- 2022005676
Parameter
Measured
Final
Units
Dil
MDL
Spike
% Recovery
LCL
UCL RPD
Antimony (Sb)
51.7
51.7
ug/L
1
0.104
50
102
75
125 0.564
Qualifier
Qualifier
Qualifier
Qualifier

Certificate of Laboratory Analysis Page 14 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030237 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
MSD # 1
Parameter
Measured
Final
Units
Dil
MDL
Arsenic (As)
49.1
49.1
ug/L
1
0.111
Beryllium (Be)
52.4
52.4
ug/L
1
0.249
Cadmium (Cd)
50.3
50.3
ug/L
1
0.032
Cobalt (Co)
48.7
48.7
ug/L
1
0.077
Lead (Pb)
51
51
ug/L
1
0.037
Selenium (Se)
48.4
48.4
ug/L
1
0.193
Silver (Ag)
49.9
49.9
ug/L
1
0.035
Thallium (TI) Low Level
49.8
49.8
ug/L
1
0.041
Vanadium (V) Low Level
52.4
52.4
ug/L
1
0.114
Parent Sample:
J22030086 -- 2022005676
Spike
% Recovery
LCL
UCL
RPD
50
98
75
125
1.2
50
105
75
125
0.388
50
101
75
125
0.68
50
96.9
75
125
0.0227
50
102
75
125
0.683
50
96.8
75
125
2.15
50
99.8
75
125
1.56
50
99.5
75
125
0.521
50
104
75
125
0.408
Qualifier

Certificate of Laboratory Analysis Page 15 of 16
This report shall not be reproduced, except in full.
Order # J22020330
Level II QC Summary
Q22030217 TDS TOTAL DISSOLVED SOLIDS
Blank # 1
Blank # 2
Parameter Measured Final
TDS 1
Parameter Measured Final
TDS 1
Duplicate # 1
Parameter Measured Final
TDS 387
Duplicate # 2
Parameter Measured Final
TDS 362
LCS # 1
LCS # 2
Parameter Measured Final
TDS 102
Parameter Measured Final
TDS 96
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
mg/L
1
25
25
< MDL
Units
Dil
MDL
RDL
Relative Concentration
Qualifier
mg/L
1
25
25
< MDL
Parent Sample:
J22020072 -- 2022002817
Units
Dil
MDL
RPD
Qualifier
mg/L
1
25
1.79
Parent Sample:
J22030217 -- 2022006388
Units
Dil
MDL
RPD
Qualifier
mg/L
1
25
0.832
Units
Dil
MDL
Spike
% Recovery
LCL
UCL
Qualifier
mg/L
1
25
100
102
90
110
Units
Dil
MDL
S ike
% Recovery
LCL
UCL
Qualifier
mg/L
1
25
100
96
90
110

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
DUKE Duke Energy Analytical Laboratory i
* Mall Cod. MG03A3IB•Ila1-7405) i
Analytical LaboratoryUse Onlyi
rclt: IV VI IV
NC Page 1_
J22020330
Matrix WATER
Hunbr.vme, C. 2ao75
ENERGY Pirry,,
iOrder#
s.mPl..o,gln,e„eFr x_ i _1_of
sue_ DISTRIBUTION
!Lopped By Date 8 Ti­I
I
5-
pa) e7s-sz4s I�
ORIGINAL to LAB, COPY to CLIENT
SAMPLE PROGRAM i
Project Name PLANT ALLEN- LEACHATE Phone No:
Ground Water_X_ NPDES_
Drinking Water_ UST_
Vendor
COLLECTION SYSTEM (PERMIT# 36-
i
`
RCRA Waste
121
.Cooler TemP.l41...................................
.........................................
Client COURTNEY MURPHY, RANDY GANTT, BRYAN :PO#
MOELLER, DEE OBRIEN, JOSH STOWE Filtration (0.45 um)
b
Unfiltered
11
Filtered
Operating Unit: AS00 Process:BENVWS Account: i I Preservative
ICE
ICE
..............................................................
Project: Activity to: Facility ID:ALN _.._.._.._._ Container Volume (mL)
300
Soo
500
..r.�
Program I EOuiS Task Code: ALN LCS Sub-ProgramlTask Code:
Container Type
HDPE
PET
PET
rc�
METALS - ICP TRM
a
(SW6010D): Ba,B, Cr,
EPA
Customer to complete all appropriate non -shaded areas. a
Cu, Fe, Mn, Ni, Zn (8)
9056A:
Sample Description or ID
Hg (7470A) (1), IMS
Cl, F,
TDS
U
I SAMPLE ID i Collection Information
TRM (SW6020B): Sb,
NO3-N,
at
d.
NUMBER
As, Be, Cd, Co, Pb, Se,
SO4
u a
Ag, TI(LL), V(LL) (10)
c
Date Time Printed Name Signature D o
12
2022003886
ALN LCS-CELL?
_7,ZZ
I I Sv
CowAll a, ZAtibttA
i
x
1
1
1
3
2022003887 !
ALN LCS-CELL2
qymt
I Lod
CWAVDIL ZAHO0.A
x
1
1
1
3
2022003888 !
ALN_FB-1Q%2DS07-12tt7
-7 7!L
t Zto
Co%mg - ZA140CA
(�
X
1
t
O
1&
r�
0
0
0
0
i I
i
0
0
0
I I
0
I i
0
0
i
0
'
i-�
0
i i
0
I i
0
'
TOTAL # CONTAINERS
0
0
0
3
3
3
0
0
0
0
0
0
9
Customer to sign & date below
Relinquished By Date/Time
S 7-Z2_ 14W
Accepted B DatelTime
�
y
i
Requested Turnaround
Total 9
� 2
S
Relinquished By Date/Time
Accepted By: Date/Time
a
c
a o
21 Days
Relinquished By Date/Time
Accepted By: Date/Time
E
m
>= 9
14 Days
Seat/Locked By Date/Time
Sealed/Lock Opened By Date/Time
°a m
'7 Days
— m
Comments
Use indicated or comparable methods; NC SWS EDD format required. EQUIS EDD required.
d
E
3
Other
0
' Add. Cost Will Apply
U

DUE Analytical Laboratory Page 1 of
ENERGY
Y
Order Number:
Project Name:
Task Code:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J22030358
ALLEN - GW LEACHATE
LCS
C Murphy, R Gantt,D O Brien, B Moeller, J Stowe
Allen Steam Station
253 Plant Allen Road
Belmont, NC 28012
Peggy Kendall
Pegg- y Kendall
Phone: [phone]
Date:
Note: This is the TDS re -sample for the initial sampling event 3-7-2022 (Job Order J22020330)
Data Flags & Calculations:
3/25/2022
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time Collected By
2022007180 ALLEN 17-Mar-22 9:55 AM Connor Zahora
2022007181 ALLEN 17-Mar-22 10:05 AM Connor Zahora
2022007182 ALLEN 17-Mar-22 10:15 AM Connor Zahora
3 Total Samples
Sample Description
ALN LCS-CELL1
ALN LCS-CELL2
ALN FB-20220317-1015
Page 2 of 8

Page 3 of 8
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals❑ Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
d❑ Job Summary Report
J❑ Sample Identification
❑ Technical Validation of Data Package
d❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑ Chain of Custody
❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 3/25/2022

Certificate of Laboratory Analysis Page 4 of 8
This report shall not be reproduced, except in full.
Order # J22030358
Site: ALN LCS-CELL1 Sample #: 2022007180
Collection Date: 03/17/2022 09:55 AM Loc code: ALN LCS-CELL1 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
TOTAL DISSOLVED SOLIDS - Q22030343
TDS 4550 mg/L 250 25 1 SM2540C 03/22/202211:38 Ebatian

Certificate of Laboratory Analysis Page 5 of 8
This report shall not be reproduced, except in full.
Order # J22030358
Site: ALN LCS-CELL2 Sample #: 2022007181
Collection Date: 03/17/2022 10:05 AM Loc code: ALN LCS-CELL2 Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
TOTAL DISSOLVED SOLIDS - Q22030343
TDS 4100 mg/L 250 25 1 SM2540C 03/22/202211:39 Ebatian

Certificate of Laboratory Analysis Page 6 of 8
This report shall not be reproduced, except in full.
Order # J22030358
Site: ALN FB-20220317-1015 Field Blank Sample #: 2022007182
Collection Date: 03/17/2022 10:15 AM Loc code: ALN QA Matrix: GW RCRA
Analyte Result Units Qualifiers RDL MDL DF Method Analysis Date/Time Analyst
TOTAL DISSOLVED SOLIDS - Q22030343
TDS 25 U mg/L 25 25 1 SM2540C 03/17/2022 12:43 Ebatian

Certificate of Laboratory Analysis Page 7 of 8
This report shall not be reproduced, except in full.
Order # J22030358
Level II QC Summary
Q22030343 TDS TOTAL DISSOLVED SOLIDS
Blank # 1
LCS # 1
Parameter Measured Final
TDS 15 15
Parameter Measured Final
TDS 104 104
LCSD # 1
Parameter Measured Final
TDS 102 102
LCS # 2
LCS # 3
Parameter Measured Final
TDS 100 100
Parameter Measured Final
TDS 102 102
Units Dil MDL RDL Relative Concentration
mg/L 1 25 25 < MDL
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 25 100 104 90 110
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 25 100 102
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 25 100 100 90 110
Units Dil MDL Spike % Recovery LCL UCL
mg/L 1 25 100 102 90 110
Qualifier
Qualifier
RPD Qualifier
1.94
Qualifier
Qualifier

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
Duke Energy Analytical Laboratory i
i
i Analytical Laboratory Use Only - - -
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - i Page 8 of 8
! Order # J22030358
Matrix WATER
�! M.II GOEa 9 Hag (BuildingFerry Rd 74e5)
•� DUKE
n.e.r. Ferry as
srm*r 0r� r— Scc x_ i Page _1_ of 1_
ENERGY una2e
Nunter-ill., N.C. 29078
i DISTRIBUTION
Logged By
>
`D,ab TI •
(704) 87sa24s i
ORIGINAL to LAB, COPY to CLIENT
t_._-_-_-_._-_-_-_--•--_-_-_-_-_--- -_,_,-,_,_• Fe.;Pa�nes00a-_._-_._-_-_j
SAMPLE PROGRAM
Project Name PLANT ALLEN- LEACHATE Plwa. No:
COLLECTION SYSTEM (PERMIT# 36-
Ground Water _X_ NPDES_
Ddnking Water_ UST_
!Vendor
€
i
RCRA Waste
'.�
._.._.._. _.
-Cooler Temp-ICj.
_.._. _.._.._.._.._.._.-
.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._.._
ClientCOURTNEY MURPHY, RANDY GANTT, BRYAN •Poe
e MOELLER, DEE OBRIEN, JOSH STOWE I ! Filtration (0.45 um)
b
Unfiltered
b
Filtered
Operating Unit: A300 Process:BENVWS Account: Preservative
.m.m.
Ice
L...........................................................................
Project: Activity ID: Facility ID:ALN Container Volume (mL)
500
Program I EQuiS Task Code: ALN LCS I Sub-ProgramlTask Coda: Container Type
PET
o:
Customer to complete all appropriate non -shaded areas.
c
Sample Description or ID
TDS
0
' SAMPLE ID ! Collection Information
d
a
! NUMBER ! e i
o
Date Time Printed Name Signature ci o`
9
r—�
2022007180
ALN_LCS-CELL1
3•17-ZI
00;
fmwoq ZAHO"
I X
t
is 2022007181 ;
ALN LCS-CELL2
11-ZZ
1005
*o& Ho*4
X
1
2022007182
ALN_FB
17- 'L
IOts
LpNNOlt +► ar-iO.
X
0
o
0
;
o
'
0
0
i
o
i
0
0
o
i
0
0
0
0
0
!
i 1
TOTAL a CONTAINERS
0
1 0
0
0
0
3
0
0
0
0
0
0
3
Relinquished By
DatelTime
Accepted By:
Date/Time
Requested Turnaround
p
a ����
�� ICJ
a
Relinquished By DateMme
Accepted By: Date/Time
w
� c
d �
a
21 Days
Relinquished By Date/Time
Accepted By: DateMme
E
14 Days
c
m
r a
Seal/Locked By Date/Time
Sealed/Lock Opened By Daternme
C.
'7 Days
E m
'— 61
-O
0
Comments
E
Other
Use indicated or comparable methods; NC SWS EDD format required. EQUIS EDD required.
o
Add. Cost Will Apply
U
Total

Attachment 2
Allen Retired Ash Basin (RAB) Ash Landfill
Semi -Annual Monitoring Event
Leachate Field Forms

❑CAMA [—]CCR[�;:]Landfill ❑NPDES ❑ DGWFASW ❑LRB ❑ SPECIAL STUDY.
Site: 44-7 Well/SW ID: LCS -GEC 1
Date: 3- 742
❑GROUNDWATER SAMPLE [:]SURFACE WATER SAMPLE ❑LEACHATE SAMPLE ❑WLO ❑ WELL DEVELOPMENT
FIELD STAFF: Qt—
COMPANY: ❑ DUKE ENERGY
❑ OTHER:
WEATHER: ❑SUNNY Q PARTLY CLOUDY ❑ OVERCAST ❑ RAIN [] SNOW AIR TEMP: �6 -F
FIELD METER TYPE/ SERIAL #:
TURBIDIMETER TYPE/ SERIAL #:
START PURGE TIME: TINS SAMPLE COLLECTION TIME: 146
PUMPITUBING INTAKE DEPTH: — (�) DEPTH TO WATER: r (ft) MULT FACTOR*: 0.163 [-(radius/12)2'3.14'7.48]
WELL DIAMETER: ' (in) HEIGHT OF WC: (ft) WELL VOLUME: (gal)
WELL DEPTH: (ft) TOTAL VOLUME PURGED: (gal)
TYPE OF PUMP:
Bladder
Peristaltic
12 Volt
Grundfos
Other ( )
PURGE METHOD:
/
SAMPLING METHOD:
PUMP SETTING:
P
R
0
Low Flow Sampling Stabilization Criteria
• pH t 0.1 standard unit
• Specific Conductance t 5% in pS/cm
• DO t 0.2 mg/l.
• Turbidity less than 10 NTUs
TIME
WATER
LEVEL
FLOW
RATE
VOLUME
REMOVED
TEMPERATURE
DO
SPECIFIC
CONDUCTANCE
pH
ORP
TURBIDITY
(FT)
(x.xx)
(mUmin)
(x)
(gallons OR mL)
(x.xx)
(°C)
(x)
(mg/L)
(x.xx)
(PS/CM)
W
(su)
(x.xx)
(mv)
(x)
(NTU)
(x.x)
(017
—
N `(w
—
Z 1
5-cr7
KIo7
Lt. Z1
47,1
17.1
11 TV
_
—
Zt
5, 1
Its S
W, o
PLEASE REFER TO THE BACK OF THIS SHEET IF THE CHART ABOVE IS FULL
IS REDEVELOPMENT NEEDED (>10 NTUS)? ❑ YES[,-] NO WERE ALL SAMPLES ON ICE WITHIN 15 MINUTES? RYES ❑ NO
IS A TURBIDITY METER DUPLICATE REQUIRED? ❑YES 0 NO IS THE LOCATION FIELD VEHICLE ACCESSIBLE? ❑'YES ❑ NO
IS THE TURBIDITY METER DUPLICATE TAKEN, WITHIN 15%? ❑ YES ❑ NO DUPLICATE 1 (NTU) DUPLICATE 2 (NTU)
FINAL SAMPLE OBSERVATIONS: �r,
DETECTED ODOR pQ0�r H2S Petroleum Earthy Musty Undetermined
ODOR STRENGTH t
Minor Strong
ADDITIONAL NOTES: APPEARANCE r Cloudy Turbid Red/Iron Film on Surface Sheen l"- Floc
WELL TAG
PROTECTIVE CASING
LOCK
DUST CAP
CONCRETE PAD
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
Version 1.0 Revised 12/17/2018 RDP

F-]CAMA ECCRaLandfill [:]NPDES ❑ DGW❑ASW ❑LRB ❑ SPECIAL STUDY.
FIELD SAMPLING LOG
Site: /Veen Well/SW ID: LCS-6FU Z
aGROUNDWATER SAMPLE
FIELD STAFF: CI
COMPANY: 0 DUKE ENERGY
❑ OTHER:
a
Date: 3- 7-21
]SURFACE WATER SAMPLE ❑LEACHATE SAMPLE WLO 0WELL DEVELOPMENT
WEATHER: ❑SUNNY QPARTLYCLOUDY ❑OVERCAST ❑RAIN ❑SNOW AIRTEMP:_6"F
FIELD METER TYPE/ SERIAL #: 743SZ4
TURBIDIMETER TYPE/ SERIAL M 33711
START PURGE TIME: 1/S7 SAMPLE COLLECTION TIME: IZZO
PUMP/TUBING INTAKE DEPTH:
(ft) DEPTH TO WATER: (ft) MULT FACTOR *: 0.163 I*(radius/12)2*3.14*7.481
WELL DIAMETER: (in) HEIGHT OF WC: (ft) WELL VOLUME: (gal)
WELL DEPTH: / (ft) TOTAL VOLUME PURGED: l (gal)
TYPE OF PUMP: Bladder Peristaltic 12 Volt Grundfos Other ( )
PURGE METHOD:
SAMPLING METHOD:
p R D
PUMP SETTING:
Low Flow Sampling Stabilization Criteria
(ps) (sec) (sec)
PH t 0.1 standard unit
• Specific Conductance f 5% In pS/cm
• DO t 0.2 mg/1
• Turbidity less than 10 NTUs
FLOW
RATE
m min)
(x)
VOLUME
REMOVED
(gallons OR ML)
(x.xx)
TEMPERATURE
(*C)
(x)
DO
(mg/L)
(x.xx)
3•i8
SPECIFIC
CONDUCTANCE
(NS/cm)
(x)
Rog7
P H
(su)
(x.xx)
KZg
ORP
(mv)
(x)
Diu
TURBIDITY
(NTU)
(x.x)
6.S
TIME
WATER
LEVEL
(FT)
(x.xx)
TU=
o A rrL Inc Tuic cuFt=T
IF THE
CHART
ABOVE IS FULL
IS REDEVELOPMENT NEEDED (>10 NTUS)? ❑ YES F ,NO ^v` WERE ALL SAMPLES ON ICE WITHIN 15 MINUTES? DYES ❑ NO
IS A TURBIDITY METER DUPLICATE REQUIRED? ❑YES 0 NO IS THE LOCATION FIELD VEHICLE ACCESSIBLE? ©YES ❑ NO
IS THE TURBIDITY METER DUPLICATE TAKEN, WITHIN 15%? ❑ YES NO DUPLICATE 1 (NTU) DUPLICATE 2 (NTU)
FINAL SAMPLE OBSERVATIONS:
DETECTED ODOR N e H2S Petroleum Earthy Musty Undetermined
ODOR STRENGTH a Minor Strong
ADDITIONAL NOTES: APPEARANCE Cl r Cloudy Turbid Red/Iron Film on Surface Sheen Fi s Floc
WELL TAG PROTECTIVE CASING LOCK DUST CAP CONCRETE PAD
GOOD I BAD I NONE I GOOD I BAD I NONE I GOOD I BAD I NONE GOOD BAD NONE GOOD BAD NONE
---/I I I J
Version 1.0 Revised 12/17/2018 RDP

❑LAMA F-]CCRF—,]Landfill ❑NPDES ❑ DGW❑ASW ❑LRB ❑ SPECIAL STUDY IceS!tMir-
FIELD SAMPLING LOG CAKE
o ENERGNY
Site: Allen Well/SW ID: LcS- c6v. 1 Date: 3-o--n
GROUNDWATER SAMPLE ❑SURFACE WATER SAMPLE ❑ LEACHATE SAMPLE ❑ WLO [:]WELL DEVELOPMENT
FIELD STAFF: OL
COMPANY: DUKE ENERGY
❑ OTHER:
WEATHER: []SUNNY DPARTLYCLOUDY ❑OVERCAST [-]RAIN EISNOW AIR TEMP: " °F
FIELD METER TYPE/ SERIAL #:635774
TURBIDIMETER TYPE/ SERIAL #: 331A
START PURGE TIME: SAMPLE COLLECTION TIME: ��SS
PUMPITUBING INTAKE DEPTH: (ft) DEPTH TO WATER: - (ft) MULT FACTOR * 0.163 [-(radius112)2'3.147.48]
WELL DIAMETER: (in) HEIGHT OF WC: (ft) WELL VOLUME: (gal)
WELL DEPTH: (ft) TOTAL VOLUME PURGED: 0.25 (gal)
TYPE OF PUMP:
Bladder
Peristaltic
12 Volt
Grundfos
Other ( )
PURGE METHOD:
SAMPLING METHOD:
PUMP SETTING:
P
R
D
cPSo (Sec) (Se,) Low Flow Sampling Stabilization Criteria
• pH f 0.1 standard unit
• Speck Conductance t 5% in pS/cm
DO t 0.2 mg/t
• Turbidity less than 10 NTUs
TIME
WATER
LEVEL
FLOW
RATE
VOLUME
REMOVED
TEMPERATURE
DO
SPECIFIC
CONDUCTANCE
pH
ORP
TURBIDITY
(FT)
(x.xx)
(mL/min)
W
(gallons OR mL)
(x.xx)
(*C)
W
(mg/L)
(x.xx)
(PS/CM)
W
(su)
(x.xx)
(mv)
W
(NTU)
(x.x)
p9$1.
-
- 40u
0.6
tv
H2OD
4815
q.15
656.3
!.V
of
-
N411M
M 0.73
18
2•1110
4$67
Y. 15
6&7
PLEASE REFER TO THE BACK OF THIS SHEET IF THE CHART ABOVE IS FULL
IS REDEVELOPMENT NEEDED (>10 NTUS)? ❑ YES F-1 NO WERE ALL SAMPLES ON ICE WITHIN 15 MINUTES? 2YES ❑ NO
IS A TURBIDITY METER DUPLICATE REQUIRED? ❑YES R NO IS THE LOCATION FIELD VEHICLE ACCESSIBLE? EYES ❑ NO
IS THE TURBIDITY METER DUPLICATE TAKEN, WITHIN 15%? ❑ YES ❑ NO DUPLICATE 1 (NTU) DUPLICATE 2 (NTU)
FINAL SAMPLE OBSERVATIONS:
DETECTED ODOR t9e H2S Petroleum Earthy Musty Undetermined
ODOR STRENGTH Oe Minor Strong
ADDITIONAL NOTES: APPEARANCE Or Cloudy Turbid Red/Iron Film on Surface Sheen Fines Floc
WELL TAG
PROTECTIVE CASING
LOCK
DUST CAP
CONCRETE PAD
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
i
Version 1.0 Revised 12/17/2018 RDP

F]CAMA F—]CCRFLandfiill [—]NPDES ❑ DGW❑ASW FJLRB ❑ SPECIAL STUDY flePv i4
FIELD SAMPLING LOG IS)DUKE
ENERGY
Site: 411m Well/SW ID: -vs -(,ELL 2 Date: 3 •o•22
IEl GROUNDWATER SAMPLE ❑SURFACE WATER SAMPLE ❑ LEACHATE SAMPLE ❑ WLO [:]WELL DEVELOPMENT
FIELD STAFF: 6177.
COMPANY: Q DUKE ENERGY
❑ OTHER:
WEATHER: []SUNNY ZPARTLYCLOUDY []OVERCAST ❑RAIN ❑SNOW AIRTEMP: SZ "F
FIELD METER TYPE/ SERIAL #: ?635Z4
TURBIDIMETER TYPE/ SERIAL #: 31IR
START PURGE TIME: rboo SAMPLE COLLECTION TIME: /005
PUMP/TUBING INTAKE DEPTH: (ft) DEPTH TO WATER: (ft) MULT FACTOR'°: 0.163 [•(radius/12)2.3.14.7.48]
WELL DIAMETER: (in) HEIGHT OF WC: (ft) WELL VOLUME: (gal)
WELL DEPTH: (ft) TOTAL VOLUME PURGED: d.Zv (gal)
TYPE OF PUMP:
Bladder
Peristaltic
12 Volt
Grundfos
Other ( )
PURGE METHOD:
SAMPLING METHOD:
PUMP SETTING:
a
R
o
(psi) (sec) (sec) Low Flow Sampling Stabilization Criteria
• pH f 0.1 standard unit
• Specific Conductance t 5% in pS/cm
• DO t 0.2 mg/t
• Turbidity less than 10 NTUs
WATER
LEVEL
FLOW
RATE
VOLUME
REMOVED
TEMPERATURE
DO
SPECIFIC
CONDUCTANCE
pH
ORP
TURBIDITY
TIME
(FT)
(x.xx)
(mUmin)
(x)
(gallons OR mL)
(x.xx)
VC)
(x)
(mg/L)
(x.xx)
(PS/cm)
W
(su)
(x.xx)
(mv)
(x)
(NTU)
(x.x)
toot
—
^' *
p.to
tq
4.57
N06*7
K.3-
541
(-Z
too 3
r
ti 2�
o•?.o
(q
2.70
417 Z
q. 3S
557
0.4
PLEASE REFER TO THE BACK OF THIS SHEET IF THE CHART ABOVE 15 FULL
IS REDEVELOPMENT NEEDED (>10 NTUS)?
❑ YES ©
NO WERE ALL SAMPLES ON ICE WITHIN 15 MINUTES? ❑/ YES ❑ NO
IS A TURBIDITY METER DUPLICATE REQUIRED?
RYES i❑
NO IS THE LOCATION FIELD VEHICLE ACCESSIBLE? /❑YES ❑ NO
IS THE TURBIDITY METER DUPLICATE TAKEN, WITHIN 15%?
❑ YES ❑ NO DUPLICATE 1 (NTU) DUPLICATE 2 (NTU)
FINAL SAMPLE OBSERVATIONS:
DETECTED ODOR
l'.:y`
H2S Petroleum Earthy Musty Undetermined
ODOR STRENGTH
Carp e
Minor Strong
ADDITIONAL NOTES: APPEARANCE
Or
Cloudy Turbid Red/Iron Film on Surface Sheen Fines Floc
WELL TAG
PROTECTIVE CASING
LOCK
DUST CAP
CONCRETE PAD
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
GOOD
BAD
NONE
r
i
r
/
l
Version 1.0 Revised 12/17/2018 RDP