6001_Mecklenburg_Harrisburg_MSWLF_June22GW_FID1691375_20220630

DENR USE ONLY: I I ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No
NC DENR
Division of Waste Management - Solid Waste
Doc/Event #:
Environmental Monitoring
Reaortina Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
General Statute 132-1, As such, these documents are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g, naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Harrisburg Road Landfill 7817 Harrisburg Road, Charlotte 60-01 .0500 June 6-7 & 21, 2022
Environmental Status: (Check all that apply)
Initial/Background Monitoring QX Detection Monitoring Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Q
Groundwater monitoring data from private water supply wells El
Leachate monitoring data ❑
Surface water monitorina data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. 1 am aware that th
levels;ere
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G.
Facility
Signature
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
Title
Manager
NC PE Firm License Number (if applicable effective May 1, 2009)
980-314-3855
(Area Code) Telephone Number
6 30-2022 Affix NC Licensed/
Date
Geologist Seal
Revised 6/2009

MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
June 3 0, 2022
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report June 2022
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill June 6 and June 7,2022 in accordance with the approved
revised sample and analysis plan dated May 11, 2004. Samples were collected from
eleven monitoring wells (HBW-12A, HBW-12B, HBW-14, HBW-14B, HBW-14C,
HB W4 4D, HB W4 7B, HBW-20, HBW-21, HBW-22 and background well HBW-28)
and three surface -water sampling locations (HB2006, HB2008 and, HB2010). Laboratory
analytical data, field -measured data, and a table of results exceeding water quality
standards along with a preliminary explanation of the cause and significance are included
on the electronic data deliverable (EDD) submittal.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 2B "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
PEOPLE • PRIDE • PROGRESS •PARTNERSHIP
2145 Suttle Ave •Charlotte, NC 28208-5237 • [phone] •FAX [phone]
www.wipeoutwaste9 com

Page 2
Surface -water samples:
Barium was detected in HB 2006, HB 2008 and HB 2010 at 30.8 ppb, 22.5 ppb and 41.9
ppb, respectively. No other analytes were detected in the surface water samples. Field -
measured parameters for surface -water samples were within the range of established
standards and are summarized in the table below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
Oxygen
HB2006
18.5° C
7.6
0.267 ms/cm
8.03 mg/l
HB2008
18.50 C
7.8
0.281 ms/cm
8.48 mg/l
HB2010
17.90 C
7.7
0.284 ms/cm
8.41 mg/l
Groundwater samples:
Multiple metals were detected above 2L standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/1
Be
ug/1
Cd
ug/l
Cr
ug/l
Co
ug/1
Cu
ug/l
Ni
ug/l
Pb
ug/1
Th
ug/l
Vn
ug/l
Zn
ug/1
HBW 12A
42.0
-----
-----
-----
-----
27.4
-----
28.5
------
41.6
------
HB W 12B
67.7
-----
-----
-----
-----
42.0
-----
35.6
------
73.1
-----
HBW 14
90.8
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW 14B
22.1
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW14C46.9
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW14D55.4
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW17B63.2
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HBW-20
30.0
-----
-----
-----
-----
32.8
-----
24A
------
SU
31.6
HBW-21
15.6
-----
-----
-----
-----
-----
-----
23.7
------
-----
-----
HBW-22
50.1
-----
-----
25.2
-----
-----
-----
-----
-----
-----
-----
HBW-28*
42.7
-----
-----
-----
-----
41.1
-----
-----
------
-----
-----
2L Std, ug/1
700
4
2.0
10
1
1,000
100
15
0.2
7
1,000
Note: Bolded results exceed 2L Standard, *Background Well
The following ten volatile organic compounds ("VOCs") were detected in the sample
collected from well HBW-17B0
VOC
Sam le Result u /1
2L Standard u /1
Benzene
10.4
1
Tetrachloroeth lene
31.4
0.7
Trichloroeth lene
26.0
2.8
1,4-Dichlorobenzene
1.2
6
1,1-Dichloroethane
7.5
6
1,2-Dichloro ro ane
10.2
0.6
cis4,2 Dichloroethene
150
70
trans-1,2-Dichloroethene
1.6
100
X lens total
12.6
500
Vinyl Chloride
2A
0.03
Note: Bolded results exceed 2L Standard

The pH was measured to be more acidic than the standard in the samples collected from
HBW 12A, HBW 12B, HBW 14C, HBW 14D, HBW 17B, HB W20, HB W21, HB W22 and
background monitoring well HBW-28. Field -measured parameters for groundwater
samples are summarized in the following table:
Location
Tem erature
Pn
Conductivi
HBW12A
15.3 °C
6.0
0.394 ms/cm
HBW 12B
15.2 °C
6.0
0.383 ms/cm
HBW14
14.9 °C
6.6
0.217 ms/cm
HBW14B
15.3 °C
6.6
0.243 ms/cm
HBW14C
15.0 °C
6.4
0.221 ms/cm
HBW 14D
15.40C
6.3
0.206 ms/cm
HBW17B
17.1 °C
4.8
0.062 ms/cm
HBW-20
16.0 °C
61
0.149 ms/cm
HBW-21
16.2 °C
690
0.201 ms/cm
HBW-22
18.2 °C
5.6
0.074 ms/cm
*HBW-28
17.3 °C
5.4
0.039 ms/cm
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
Sincerely,
Amber R. Grzymski, P.G.
Project Manager
LUESA Solid Waste Services

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Landfill Gas Monitoring Data Form
Facility Name: Harrisburg Road Landfill
Permit Number: 60-01
Date of Sampling: 6/21/2022 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: David E. Coleman. Environmental Specialist
Type and Serial Number of Gas Meter: Gem 5000 #G507530
Calibration Date of Gas Meter: 4/1/2022 Date and Time of Field Calibration: 6/21/2022 12:40
Type of Field Calibration Gas (15/15 or 35/50): 35/50
Expiration Date of Field Calibration Gas Canister: January 2025
Pump Rate of Gas Meter: 120 Seconds Ambient Air Temperature: 85 Degrees
Barometric Pressure: 29.42 General Weather Conditions: Sunny, Winds SE4
Sam le ID
Time
% LEL
% CH4
% CO2
% 02
Comments
MP-1
13:24
>100
59.3
40.1
0
Methane Extraction System
MP-2
13:19
>100
54.1
28.0
2.9
Methane Extraction System
MP-3
13:13
0
0
0.1
18.8
Methane Extraction System
MP4
13:09
>100
1998
12.2
13.0
Methane Extraction System
MP-5
14:20
0
0
2.8
17.6
MP-6
14:27
0
0
4.5
15.6
MP-7
14:34
0
0
5.1
16.0
MP-8
14:40
0
0
6.8
14.5
MP-9A
14:46
0
0
1.4
19.4
MP-913
14:52
0
0
4.1
16.5
MP-11
12:50
>100
8.9
8.0
13.3
MP42
12:57
0
0
9.0
13.0
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
Joe
3NATURE
TITLE

60-01 Harrisbura Rd Landfill Methane Wells
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 14, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on June 06, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 39

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HARRISBURG RD LF PERM 60-01
92608158
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92608158001
6001-HBW28
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158002
6001-HBW20
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158003
6001-HBW14
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158004
6001-HBW14B
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158005
6001-HBW14C
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158006
6001-HBW14D
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
NSCQ
52
PASI-C
92608158007
6001-HB2006
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
92608158008
6001-HB2008
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
92608158009
6001-HB2010
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
92608158010
HB2006
EPA 8260D
NSCQ
52
PASI-C
92608158011
HB2008
EPA 8260D
NSCQ
52
PASI-C
92608158012
HB2010
EPA 8260D
NSCQ
52
PASI-C
92608158013
TRIP BLANK
EPA 8260D
NSCQ
52
PASI-C
PASI-C = Pace Analytical
Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW28 Lab ID: 92608158001 Collected: 06/06/22 10:00 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2216:53
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:53
7440-41-7
Barium
42.7
ug/L
10.0
1
06/08/2211:39
06/08/2216:53
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:53
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:53
7440-47-3
Copper
41.1
ug/L
20.0
1
06/08/2211:39
06/08/2216:53
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2216:53
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:53
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2216:53
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2216:53
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2216:53
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2216:53
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2216:53
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2216:53
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2216:53
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 21:59
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 08:40
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 08:40
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 08:40
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 08:40
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 08:40
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 08:40
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 08:40
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 08:40
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 08:40
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 08:40
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 08:40
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 08:40
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 08:40
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 08:40
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 08:40
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 08:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 08:40
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 08:40
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:40
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:40
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 08:40
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:40
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:40
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW28 Lab ID: 92608158001 Collected: 06/06/22 10:00 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:40
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:40
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:40
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 08:40
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 08:40
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 08:40
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 08:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 08:40
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 08:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:40
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 08:40
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 08:40
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:40
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:40
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 08:40
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 08:40
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 08:40
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 08:40
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 08:40
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/08/22 08:40
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/08/22 08:40
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/08/22 08:40
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/08/22 08:40
460-00-4
1,2-Dichloroethane-d4 (S)
114
%
70-130
1
06/08/22 08:40
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
06/08/22 08:40
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW20 Lab ID: 92608158002 Collected: 06/06/22 10:35 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2216:57
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:57
7440-41-7
Barium
30.0
ug/L
10.0
1
06/08/2211:39
06/08/2216:57
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:57
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:57
7440-47-3
Copper
32.8
ug/L
20.0
1
06/08/2211:39
06/08/2216:57
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2216:57
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2216:57
7440-22-4
Lead
24.4
ug/L
20.0
1
06/08/2211:39
06/08/2216:57
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2216:57
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2216:57
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2216:57
7440-28-0
Vanadium
50.8
ug/L
20.0
1
06/08/2211:39
06/08/2216:57
7440-62-2
Zinc
31.6
ug/L
20.0
1
06/08/2211:39
06/08/2216:57
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2216:57
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 22:05
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 08:59
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 08:59
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 08:59
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 08:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 08:59
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 08:59
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 08:59
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 08:59
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 08:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 08:59
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 08:59
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 08:59
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 08:59
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 08:59
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 08:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 08:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 08:59
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 08:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:59
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:59
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 08:59
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:59
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW20 Lab ID: 92608158002 Collected: 06/06/22 10:35 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:59
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:59
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:59
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 08:59
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 08:59
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 08:59
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 08:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 08:59
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 08:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:59
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 08:59
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 08:59
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:59
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 08:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 08:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 08:59
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 08:59
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 08:59
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/08/22 08:59
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/08/22 08:59
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/08/22 08:59
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/08/22 08:59
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
06/08/22 08:59
17060-07-0
Toluene-d8(S)
99
%
70-130
1
06/08/22 08:59
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14 Lab ID: 92608158003 Collected: 06/06/22 11:45 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:02
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:02
7440-41-7
Barium
90.8
ug/L
10.0
1
06/08/2211:39
06/08/2217:02
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:02
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:02
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:02
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:02
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:02
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:02
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:02
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:02
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:02
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:02
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:02
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:02
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 22:11
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 09:17
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 09:17
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 09:17
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 09:17
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 09:17
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 09:17
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 09:17
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 09:17
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 09:17
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 09:17
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 09:17
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 09:17
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 09:17
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 09:17
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 09:17
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 09:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 09:17
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 09:17
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:17
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:17
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 09:17
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 09:17
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 09:17
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14 Lab ID: 92608158003 Collected: 06/06/22 11:45 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 09:17
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 09:17
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 09:17
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 09:17
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 09:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 09:17
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 09:17
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 09:17
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 09:17
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 09:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 09:17
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 09:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 09:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 09:17
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 09:17
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 09:17
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 09:17
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 09:17
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 09:17
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 09:17
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 09:17
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 09:17
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 09:17
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/08/22 09:17
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/08/22 09:17
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/08/22 09:17
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
06/08/22 09:17
460-00-4
1,2-Dichloroethane-d4 (S)
113
%
70-130
1
06/08/22 09:17
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
06/08/22 09:17
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14B Lab ID: 92608158004 Collected: 06/06/22 11:30 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:07
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:07
7440-41-7
Barium
22.1
ug/L
10.0
1
06/08/2211:39
06/08/2217:07
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:07
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:07
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:07
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:07
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:07
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:07
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:07
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:07
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:07
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:07
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:07
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:07
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 22:47
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 09:36
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 09:36
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 09:36
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 09:36
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 09:36
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 09:36
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 09:36
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 09:36
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 09:36
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 09:36
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 09:36
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 09:36
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 09:36
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 09:36
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 09:36
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 09:36
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 09:36
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 09:36
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:36
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:36
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 09:36
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 09:36
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 09:36
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14B Lab ID: 92608158004 Collected: 06/06/22 11:30 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/14/2022 02:28 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
112
%
114
%
90
%
1.0
1
06/08/22 09:36
75-35-4
1.0
1
06/08/22 09:36
156-59-2
1.0
1
06/08/22 09:36
156-60-5
1.0
1
06/08/22 09:36
78-87-5
1.0
1
06/08/22 09:36
10061-01-5
1.0
1
06/08/22 09:36
10061-02-6
1.0
1
06/08/22 09:36
100-41-4
5.0
1
06/08/22 09:36
591-78-6
20.0
1
06/08/22 09:36
74-88-4
5.0
1
06/08/22 09:36
75-09-2
5.0
1
06/08/22 09:36
108-10-1
1.0
1
06/08/22 09:36
100-42-5
1.0
1
06/08/22 09:36
630-20-6
1.0
1
06/08/22 09:36
79-34-5
1.0
1
06/08/22 09:36
127-18-4
1.0
1
06/08/22 09:36
108-88-3
1.0
1
06/08/22 09:36
71-55-6
1.0
1
06/08/22 09:36
79-00-5
1.0
1
06/08/22 09:36
79-01-6
1.0
1
06/08/22 09:36
75-69-4
1.0
1
06/08/22 09:36
96-18-4
2.0
1
06/08/22 09:36
108-05-4
1.0
1
06/08/22 09:36
75-01-4
1.0
1
06/08/22 09:36
1330-20-7
2.0
1
06/08/22 09:36
179601-23-1
1.0
1
06/08/22 09:36
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/08/22 09:36 460-00-4
06/08/22 09:36 17060-07-0
06/08/22 09:36 2037-26-5
Page 11 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14C Lab ID: 92608158005 Collected: 06/06/22 11:20 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:12
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:12
7440-41-7
Barium
46.9
ug/L
10.0
1
06/08/2211:39
06/08/2217:12
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:12
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:12
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:12
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:12
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:12
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:12
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:12
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:12
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:12
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:12
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:12
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:12
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 22:53
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 09:54
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 09:54
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 09:54
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 09:54
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 09:54
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 09:54
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 09:54
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 09:54
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 09:54
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 09:54
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 09:54
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 09:54
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 09:54
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 09:54
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 09:54
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 09:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 09:54
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 09:54
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:54
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 09:54
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 09:54
110-57-6
1,1-Dichloroethane
1.1
ug/L
1.0
1
06/08/22 09:54
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 09:54
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14C Lab ID: 92608158005 Collected: 06/06/22 11:20 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/14/2022 02:28 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
113
%
99
%
1.0
1
06/08/22 09:54
75-35-4
1.0
1
06/08/22 09:54
156-59-2
1.0
1
06/08/22 09:54
156-60-5
1.0
1
06/08/22 09:54
78-87-5
1.0
1
06/08/22 09:54
10061-01-5
1.0
1
06/08/22 09:54
10061-02-6
1.0
1
06/08/22 09:54
100-41-4
5.0
1
06/08/22 09:54
591-78-6
20.0
1
06/08/22 09:54
74-88-4
5.0
1
06/08/22 09:54
75-09-2
5.0
1
06/08/22 09:54
108-10-1
1.0
1
06/08/22 09:54
100-42-5
1.0
1
06/08/22 09:54
630-20-6
1.0
1
06/08/22 09:54
79-34-5
1.0
1
06/08/22 09:54
127-18-4
1.0
1
06/08/22 09:54
108-88-3
1.0
1
06/08/22 09:54
71-55-6
1.0
1
06/08/22 09:54
79-00-5
1.0
1
06/08/22 09:54
79-01-6
1.0
1
06/08/22 09:54
75-69-4
1.0
1
06/08/22 09:54
96-18-4
2.0
1
06/08/22 09:54
108-05-4
1.0
1
06/08/22 09:54
75-01-4
1.0
1
06/08/22 09:54
1330-20-7
2.0
1
06/08/22 09:54
179601-23-1
1.0
1
06/08/22 09:54
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/08/22 09:54 460-00-4
06/08/22 09:54 17060-07-0
06/08/22 09:54 2037-26-5
Page 13 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14D Lab ID: 92608158006 Collected: 06/06/22 11:10 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:16
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:16
7440-41-7
Barium
55.4
ug/L
10.0
1
06/08/2211:39
06/08/2217:16
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:16
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:16
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:16
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:16
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:16
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:16
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:16
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:16
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:16
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:16
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:16
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:16
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 22:59
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 10:13
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 10:13
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 10:13
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 10:13
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 10:13
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 10:13
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 10:13
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 10:13
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 10:13
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 10:13
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 10:13
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 10:13
75-00-3
Chloroform
ND
ug/L
1.0
1
06/08/22 10:13
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 10:13
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 10:13
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 10:13
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 10:13
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 10:13
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:13
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:13
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 10:13
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:13
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:13
107-06-2
REPORT OF LABORATORY ANALYSIS
v1
L1,v1
v1
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HBW14D Lab ID: 92608158006 Collected: 06/06/22 11:10 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/14/2022 02:28 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
109
%
113
%
100
%
1.0
1
06/08/22 10:13
75-35-4
1.0
1
06/08/22 10:13
156-59-2
1.0
1
06/08/22 10:13
156-60-5
1.0
1
06/08/22 10:13
78-87-5
1.0
1
06/08/22 10:13
10061-01-5
1.0
1
06/08/22 10:13
10061-02-6
1.0
1
06/08/22 10:13
100-41-4
5.0
1
06/08/22 10:13
591-78-6
20.0
1
06/08/22 10:13
74-88-4
5.0
1
06/08/22 10:13
75-09-2
5.0
1
06/08/22 10:13
108-10-1
1.0
1
06/08/22 10:13
100-42-5
1.0
1
06/08/22 10:13
630-20-6
1.0
1
06/08/22 10:13
79-34-5
1.0
1
06/08/22 10:13
127-18-4
1.0
1
06/08/22 10:13
108-88-3
1.0
1
06/08/22 10:13
71-55-6
1.0
1
06/08/22 10:13
79-00-5
1.0
1
06/08/22 10:13
79-01-6
1.0
1
06/08/22 10:13
75-69-4
1.0
1
06/08/22 10:13
96-18-4
2.0
1
06/08/22 10:13
108-05-4
1.0
1
06/08/22 10:13
75-01-4
1.0
1
06/08/22 10:13
1330-20-7
2.0
1
06/08/22 10:13
179601-23-1
1.0
1
06/08/22 10:13
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/08/22 10:13 460-00-4
06/08/22 10:13 17060-07-0
06/08/22 10:13 2037-26-5
Page 15 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HB2006 Lab ID: 92608158007 Collected: 06/06/22 12:45 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:42
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:42
7440-41-7
Barium
30.8
ug/L
10.0
1
06/08/2211:39
06/08/2217:42
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:42
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:42
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:42
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:42
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:42
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:42
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:42
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:42
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:42
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:42
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:42
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:42
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services
- Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:05
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HB2008 Lab ID: 92608158008 Collected: 06/06/22 13:05 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:47
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:47
7440-41-7
Barium
22.5
ug/L
10.0
1
06/08/2211:39
06/08/2217:47
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:47
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:47
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:47
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:47
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:47
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:47
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:47
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:47
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:47
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:47
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:47
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:47
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services
- Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:11
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: 6001-HB2010 Lab ID: 92608158009 Collected: 06/06/22 12:00 Received: 06/06/22 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/08/2211:39
06/08/2217:52
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:52
7440-41-7
Barium
41.9
ug/L
10.0
1
06/08/2211:39
06/08/2217:52
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:52
7440-43-9
Chromium
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:52
7440-47-3
Copper
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:52
7440-50-8
Nickel
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:52
7440-02-0
Silver
ND
ug/L
10.0
1
06/08/2211:39
06/08/2217:52
7440-22-4
Lead
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:52
7439-92-1
Antimony
ND
ug/L
50.0
1
06/08/2211:39
06/08/2217:52
7440-36-0
Selenium
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:52
7782-49-2
Thallium
ND
ug/L
200
1
06/08/2211:39
06/08/2217:52
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:52
7440-62-2
Zinc
ND
ug/L
20.0
1
06/08/2211:39
06/08/2217:52
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/08/2211:39
06/08/2217:52
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services
- Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:17
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2006
Lab ID: 92608158010
Collected:
06/06/22
12:45
Received: 06/06/22 14:35 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 10:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 10:31
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 10:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 10:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 10:31
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 10:31
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 10:31
74-83-9 v1
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 10:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 10:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 10:31
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 10:31
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 10:31
75-00-3 L1,v1
Chloroform
ND
ug/L
1.0
1
06/08/22 10:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 10:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 10:31
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 10:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 10:31
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 10:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 10:31
110-57-6 v1
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:31
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:31
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:31
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:31
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:31
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 10:31
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 10:31
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 10:31
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 10:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 10:31
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 10:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 10:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 10:31
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 10:31
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 10:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 10:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 10:31
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 10:31
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 10:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 10:31
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 10:31
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 10:31
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2006
Parameters
Lab ID: 92608158010 Collected: 06/06/22 12:45
Results Units Report Limit DF
Received: 06/06/22 14:35 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/08/22 10:31
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/08/22 10:31
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/08/22 10:31
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
06/08/22 10:31
460-00-4
1,2-Dichloroethane-d4 (S)
114 %
70-130
1
06/08/22 10:31
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
06/08/22 10:31
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2008
Lab ID: 92608158011
Collected:
06/06/22
13:05
Received: 06/06/22 14:35 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 10:49
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 10:49
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 10:49
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 10:49
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 10:49
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 10:49
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 10:49
74-83-9 v1
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 10:49
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 10:49
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 10:49
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 10:49
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 10:49
75-00-3 L1,v1
Chloroform
ND
ug/L
1.0
1
06/08/22 10:49
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 10:49
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 10:49
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 10:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 10:49
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 10:49
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:49
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 10:49
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 10:49
110-57-6 v1
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:49
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 10:49
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:49
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 10:49
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:49
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 10:49
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 10:49
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 10:49
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 10:49
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 10:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 10:49
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 10:49
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 10:49
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 10:49
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 10:49
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 10:49
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 10:49
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 10:49
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 10:49
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 10:49
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 10:49
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 10:49
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 10:49
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2008
Parameters
Lab ID: 92608158011 Collected: 06/06/22 13:05
Results Units Report Limit DF
Received: 06/06/22 14:35 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/08/22 10:49
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/08/22 10:49
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/08/22 10:49
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
06/08/22 10:49
460-00-4
1,2-Dichloroethane-d4 (S)
114 %
70-130
1
06/08/22 10:49
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
06/08/22 10:49
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2010
Lab ID: 92608158012
Collected:
06/06/22
12:00
Received: 06/06/22 14:35 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 11:26
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 11:26
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 11:26
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 11:26
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 11:26
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 11:26
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 11:26
74-83-9 v1
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 11:26
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 11:26
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 11:26
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 11:26
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 11:26
75-00-3 L1,v1
Chloroform
ND
ug/L
1.0
1
06/08/22 11:26
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 11:26
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 11:26
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 11:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 11:26
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 11:26
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 11:26
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 11:26
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 11:26
110-57-6 v1
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 11:26
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 11:26
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 11:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 11:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 11:26
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 11:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 11:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 11:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 11:26
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 11:26
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 11:26
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 11:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 11:26
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 11:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 11:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 11:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 11:26
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 11:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 11:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 11:26
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 11:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 11:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 11:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 11:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 11:26
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: HB2010
Parameters
Lab ID: 92608158012 Collected: 06/06/22 12:00
Results Units Report Limit DF
Received: 06/06/22 14:35 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/08/22 11:26
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/08/22 11:26
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/08/22 11:26
95-47-6
Surrogates
4-Bromofluorobenzene (S)
118 %
70-130
1
06/08/22 11:26
460-00-4
1,2-Dichloroethane-d4 (S)
114 %
70-130
1
06/08/22 11:26
17060-07-0
Toluene-d8(S)
99 %
70-130
1
06/08/22 11:26
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: TRIP BLANK
Lab ID: 92608158013
Collected:
06/06/22
00:00
Received: 06/06/22 14:35 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/08/22 08:22
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/08/22 08:22
107-13-1
Benzene
ND
ug/L
1.0
1
06/08/22 08:22
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/08/22 08:22
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/08/22 08:22
75-27-4
Bromoform
ND
ug/L
1.0
1
06/08/22 08:22
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/08/22 08:22
74-83-9 v1
2-Butanone (MEK)
ND
ug/L
5.0
1
06/08/22 08:22
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/08/22 08:22
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/08/22 08:22
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/08/22 08:22
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/08/22 08:22
75-00-3 L1,v1
Chloroform
ND
ug/L
1.0
1
06/08/22 08:22
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/08/22 08:22
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/08/22 08:22
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/08/22 08:22
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/08/22 08:22
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/08/22 08:22
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:22
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/08/22 08:22
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/08/22 08:22
110-57-6 v1
1,1-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:22
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/08/22 08:22
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:22
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:22
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/08/22 08:22
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:22
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:22
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/08/22 08:22
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/08/22 08:22
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/08/22 08:22
591-78-6
lodomethane
ND
ug/L
20.0
1
06/08/22 08:22
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
06/08/22 08:22
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/08/22 08:22
108-10-1
Styrene
ND
ug/L
1.0
1
06/08/22 08:22
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:22
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/08/22 08:22
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/08/22 08:22
127-18-4
Toluene
ND
ug/L
1.0
1
06/08/22 08:22
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:22
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/08/22 08:22
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/08/22 08:22
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/08/22 08:22
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/08/22 08:22
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/08/22 08:22
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/08/22 08:22
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Sample: TRIP BLANK
Parameters
Lab ID: 92608158013 Collected: 06/06/22 00:00
Results Units Report Limit DF
Received: 06/06/22 14:35 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/08/22 08:22
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/08/22 08:22
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/08/22 08:22
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
06/08/22 08:22
460-00-4
1,2-Dichloroethane-d4 (S)
115 %
70-130
1
06/08/22 08:22
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
06/08/22 08:22
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
QC Batch: 702999 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158007,
92608158008,92608158009
METHOD BLANK: 3668561 Matrix: Water
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158007,
92608158008,92608158009
Parameter
Blank
Units Result
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Vanadium
ug/L
Zinc
ug/L
Reporting
Limit
Analyzed Qualifiers
ND
50.0
06/08/22 15:11
ND
30.0
06/08/22 15:11
ND
10.0
06/08/22 15:11
ND
10.0
06/08/22 15:11
ND
10.0
06/08/22 15:11
ND
10.0
06/08/22 15:11
ND
40.0
06/08/22 15:11
ND
20.0
06/08/22 15:11
ND
20.0
06/08/22 15:11
ND
20.0
06/08/22 15:11
ND
40.0
06/08/22 15:11
ND
10.0
06/08/22 15:11
ND
200
06/08/22 15:11
ND
20.0
06/08/22 15:11
ND
20.0
06/08/22 15:11
LABORATORY CONTROL SAMPLE:
Parameter
3668562
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
1070
107
80-120
Arsenic
ug/L
1000
1090
109
80-120
Barium
ug/L
1000
1010
101
80-120
Beryllium
ug/L
1000
1060
106
80-120
Cadmium
ug/L
1000
1080
108
80-120
Chromium
ug/L
1000
1060
106
80-120
Cobalt
ug/L
1000
1100
110
80-120
Copper
ug/L
1000
1080
108
80-120
Lead
ug/L
1000
1080
108
80-120
Nickel
ug/L
1000
1100
110
80-120
Selenium
ug/L
1000
1050
105
80-120
Silver
ug/L
1000
1020
102
80-120
Thallium
ug/L
1000
1060
106
80-120
Vanadium
ug/L
1000
1140
114
80-120
Zinc
ug/L
1000
1080
108
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LF PERM 60-01
92608158
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3668563
3668564
MS
MSD
92602813001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1030
1080
103
108
75-125
5
Arsenic
ug/L
ND
1000
1000
1050
1090
105
109
75-125
4
Barium
ug/L
48.0
1000
1000
1060
1120
101
107
75-125
6
Beryllium
ug/L
ND
1000
1000
1030
1080
103
108
75-125
5
Cadmium
ug/L
ND
1000
1000
1040
1090
104
109
75-125
5
Chromium
ug/L
ND
1000
1000
1020
1080
102
108
75-125
5
Cobalt
ug/L
ND
1000
1000
1050
1100
105
110
75-125
4
Copper
ug/L
ND
1000
1000
1040
1090
104
109
75-125
5
Lead
ug/L
ND
1000
1000
1040
1080
103
108
75-125
4
Nickel
ug/L
ND
1000
1000
1050
1090
105
109
75-125
4
Selenium
ug/L
ND
1000
1000
1020
1060
102
106
75-125
4
Silver
ug/L
ND
1000
1000
988
1040
99
104
75-125
5
Thallium
ug/L
ND
1000
1000
1030
1060
103
106
75-125
4
Vanadium
ug/L
ND
1000
1000
1100
1160
110
116
75-125
5
Zinc
ug/L
12.OJ
1000
1000
1040
1090
103
108
75-125
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
QC Batch: 703049 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158007,
92608158008,92608158009
METHOD BLANK: 3668809 Matrix: Water
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158007,
92608158008,92608158009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Thallium ug/L ND 1.0 06/09/22 21:35
LABORATORY CONTROL SAMPLE: 3668810
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 100 107 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3669048 3669049
MS MSD
92608158003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 107 106 107 106 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
QC Batch: 702873 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158010,
92608158011,92608158012,92608158013
METHOD BLANK: 3668233 Matrix: Water
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158010,
92608158011,92608158012,92608158013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/08/22 07:27
1,1,1-Trichloroethane
ug/L
ND
1.0
06/08/22 07:27
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/08/22 07:27
1,1,2-Trichloroethane
ug/L
ND
1.0
06/08/22 07:27
1,1-Dichloroethane
ug/L
ND
1.0
06/08/22 07:27
1,1-Dichloroethene
ug/L
ND
1.0
06/08/22 07:27
1,2,3-Trichloropropane
ug/L
ND
1.0
06/08/22 07:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/08/22 07:27
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/08/22 07:27
1,2-Dichlorobenzene
ug/L
ND
1.0
06/08/22 07:27
1,2-Dichloroethane
ug/L
ND
1.0
06/08/22 07:27
1,2-Dichloropropane
ug/L
ND
1.0
06/08/22 07:27
1,4-Dichlorobenzene
ug/L
ND
1.0
06/08/22 07:27
2-Butanone (MEK)
ug/L
ND
5.0
06/08/22 07:27
2-Hexanone
ug/L
ND
5.0
06/08/22 07:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/08/22 07:27
Acetone
ug/L
ND
25.0
06/08/22 07:27
Acrylonitrile
ug/L
ND
10.0
06/08/22 07:27
Benzene
ug/L
ND
1.0
06/08/22 07:27
Bromochloromethane
ug/L
ND
1.0
06/08/22 07:27
Bromodichloromethane
ug/L
ND
1.0
06/08/22 07:27
Bromoform
ug/L
ND
1.0
06/08/22 07:27
Bromomethane
ug/L
ND
2.0
06/08/22 07:27
Carbon disulfide
ug/L
ND
2.0
06/08/22 07:27
Carbon tetrachloride
ug/L
ND
1.0
06/08/22 07:27
Chlorobenzene
ug/L
ND
1.0
06/08/22 07:27
Chloroethane
ug/L
ND
1.0
06/08/22 07:27
Chloroform
ug/L
ND
1.0
06/08/22 07:27
Chloromethane
ug/L
ND
1.0
06/08/22 07:27
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/08/22 07:27
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/08/22 07:27
Dibromochloromethane
ug/L
ND
1.0
06/08/22 07:27
Dibromomethane
ug/L
ND
1.0
06/08/22 07:27
Ethylbenzene
ug/L
ND
1.0
06/08/22 07:27
lodomethane
ug/L
ND
20.0
06/08/22 07:27
m&p-Xylene
ug/L
ND
2.0
06/08/22 07:27
Methylene Chloride
ug/L
ND
5.0
06/08/22 07:27
o-Xylene
ug/L
ND
1.0
06/08/22 07:27
Styrene
ug/L
ND
1.0
06/08/22 07:27
v1
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
METHOD BLANK: 3668233 Matrix: Water
Associated Lab Samples: 92608158001, 92608158002, 92608158003, 92608158004, 92608158005, 92608158006, 92608158010,
92608158011,92608158012,92608158013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Tetrachloroethene
ug/L
ND
1.0
06/08/22 07:27
Toluene
ug/L
ND
1.0
06/08/22 07:27
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/08/22 07:27
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/08/22 07:27
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/08/22 07:27 v1
Trichloroethene
ug/L
ND
1.0
06/08/22 07:27
Trichlorofluoromethane
ug/L
ND
1.0
06/08/22 07:27
Vinyl acetate
ug/L
ND
2.0
06/08/22 07:27
Vinyl chloride
ug/L
ND
1.0
06/08/22 07:27
Xylene (Total)
ug/L
ND
1.0
06/08/22 07:27
1,2-Dichloroethane-d4 (S)
%
115
70-130
06/08/22 07:27
4-Bromofluorobenzene (S)
%
98
70-130
06/08/22 07:27
Toluene-d8 (S)
%
99
70-130
06/08/22 07:27
LABORATORY CONTROL SAMPLE:
Parameter
3668234
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,1-Trichloroethane
ug/L
50
51.3
103
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
54.4
109
70-130
1,1,2-Trichloroethane
ug/L
50
51.3
103
70-130
1,1-Dichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethene
ug/L
50
57.5
115
70-132
1,2,3-Trichloropropane
ug/L
50
53.2
106
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.8
104
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
70-130
1,2-Dichlorobenzene
ug/L
50
54.0
108
70-130
1,2-Dichloroethane
ug/L
50
52.6
105
70-130
1,2-Dichloropropane
ug/L
50
52.7
105
70-130
1,4-Dichlorobenzene
ug/L
50
53.9
108
70-130
2-Butanone (MEK)
ug/L
100
110
110
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
110
110
70-130
Acetone
ug/L
100
112
112
70-144
Acrylonitrile
ug/L
250
260
104
70-130
Benzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
49.2
98
70-130
Bromodichloromethane
ug/L
50
50.7
101
70-130
Bromoform
ug/L
50
48.1
96
70-131
Bromomethane
ug/L
50
64.7
129
30-177 v1
Carbon disulfide
ug/L
50
53.5
107
70-133
Carbon tetrachloride
ug/L
50
49.0
98
70-130
Chlorobenzene
ug/L
50
53.3
107
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 39

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
LABORATORY CONTROL SAMPLE:
Parameter
3668234
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloroethane
ug/L
50
67.1
Chloroform
ug/L
50
51.5
Chloromethane
ug/L
50
60.6
cis-1,2-Dichloroethene
ug/L
50
52.2
cis-1,3-Dichloropropene
ug/L
50
51.0
Dibromochloromethane
ug/L
50
49.7
Dibromomethane
ug/L
50
50.7
Ethylbenzene
ug/L
50
52.6
lodomethane
ug/L
100
119
m&p-Xylene
ug/L
100
107
Methylene Chloride
ug/L
50
54.9
o-Xylene
ug/L
50
51.9
Styrene
ug/L
50
52.1
Tetrachloroethene
ug/L
50
50.0
Toluene
ug/L
50
50.6
trans-1,2-Dichloroethene
ug/L
50
54.3
trans- 1,3-Dichloropropene
ug/L
50
52.0
trans-1,4-Dichloro-2-butene
ug/L
50
60.3
Trichloroethene
ug/L
50
52.0
Trichlorofluoromethane
ug/L
50
57.9
Vinyl acetate
ug/L
100
105
Vinyl chloride
ug/L
50
58.4
Xylene (Total)
ug/L
150
159
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
134
46-131 L1,v1
103
70-130
121
49-130
104
70-130
102
70-130
99
70-130
101
70-130
105
70-130
119
47-140
107
70-130
110
68-130
104
70-130
104
70-130
100
70-130
101
70-130
109
70-130
104
70-130
121
25-200 v1
104
70-130
116
61-130
105
70-140
117
59-142
106
70-130
104
70-130
98
70-130
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3668235
MS
92608158012 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3668236
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.6
23.7
113
118
70-135
4
1,1,1-Trichloroethane
ug/L
ND
20
20
22.2
23.6
111
118
70-148
6
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.3
23.8
116
119
70-131
2
1,1,2-Trichloroethane
ug/L
ND
20
20
21.2
22.2
106
111
70-136
4
1,1-Dichloroethane
ug/L
ND
20
20
22.4
23.4
112
117
70-147
4
1,1-Dichloroethene
ug/L
ND
20
20
25.9
27.6
130
138
70-158
6
1,2,3-Trichloropropane
ug/L
ND
20
20
23.2
23.8
116
119
67-137
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
19.1
21.8
96
109
69-136
13
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
23.2
113
116
70-137
3
1,2-Dichlorobenzene
ug/L
ND
20
20
20.6
23.9
103
119
70-133
15
1,2-Dichloroethane
ug/L
ND
20
20
22.6
23.6
113
118
67-138
4
1,2-Dichloropropane
ug/L
ND
20
20
22.2
23.6
111
118
70-138
6
1,4-Dichlorobenzene
ug/L
ND
20
20
22.8
24.1
114
121
70-133
6
2-Butanone (MEK)
ug/L
ND
40
40
51.0
52.6
127
132
61-147
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3668235
3668236
MS
MSD
92608158012
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
2-Hexanone
ug/L
ND
40
40
48.9
51.5
122
129
67-139
5
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
45.6
48.6
114
122
67-136
6
Acetone
ug/L
ND
40
40
46.7
50.0
117
125
55-159
7
Acrylonitrile
ug/L
ND
100
100
111
117
111
117
68-140
5
Benzene
ug/L
ND
20
20
21.5
22.5
108
113
67-150
5
Bromochloromethane
ug/L
ND
20
20
21.8
22.5
109
112
70-146
3
Bromodichloromethane
ug/L
ND
20
20
21.4
22.5
107
113
70-138
5
Bromoform
ug/L
ND
20
20
19.1
20.0
95
100
57-138
5
Bromomethane
ug/L
ND
20
20
28.4
29.6
142
148
10-200
4 v1
Carbon disulfide
ug/L
ND
20
20
23.7
24.9
119
124
70-152
5
Carbon tetrachloride
ug/L
ND
20
20
21.8
23.2
109
116
70-147
6
Chlorobenzene
ug/L
ND
20
20
23.2
23.9
116
119
70-137
3
Chloroethane
ug/L
ND
20
20
31.5
32.8
157
164
51-166
4
Chloroform
ug/L
ND
20
20
22.8
23.2
114
116
70-144
2
Chloromethane
ug/L
ND
20
20
27.5
28.4
137
142
24-161
3
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.4
23.7
112
118
67-148
5
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.0
22.1
105
111
70-142
5
Dibromochloromethane
ug/L
ND
20
20
20.6
21.4
103
107
68-138
4
Dibromomethane
ug/L
ND
20
20
21.1
22.7
105
113
70-134
7
Ethylbenzene
ug/L
ND
20
20
23.3
24.0
117
120
68-143
3
lodomethane
ug/L
ND
40
40
50.7
53.5
127
134
20-161
5
m&p-Xylene
ug/L
ND
40
40
47.2
48.4
118
121
53-157
3
Methylene Chloride
ug/L
ND
20
20
22.8
23.5
114
117
64-148
3
o-Xylene
ug/L
ND
20
20
22.7
23.3
114
116
68-143
3
Styrene
ug/L
ND
20
20
22.7
23.6
113
118
70-136
4
Tetrachloroethene
ug/L
ND
20
20
22.2
23.1
111
115
70-139
4
Toluene
ug/L
ND
20
20
21.6
22.8
108
114
47-157
5
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.8
25.2
119
126
70-149
5
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.0
22.3
105
112
70-138
6
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.2
24.0
111
120
31-145
8 v1
Trichloroethene
ug/L
ND
20
20
22.2
23.3
111
116
70-149
5
Trichlorofluoromethane
ug/L
ND
20
20
26.4
27.6
132
138
61-154
4
Vinyl acetate
ug/L
ND
40
40
41.0
43.2
103
108
48-156
5
Vinyl chloride
ug/L
ND
20
20
26.3
27.9
131
140
55-172
6
Xylene (Total)
ug/L
ND
60
60
69.9
71.7
116
120
66-145
3
1,2-Dichloroethane-d4 (S)
%
109
108
70-130
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8(S)
%
100
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 39

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: HARRISBURG RD LF PERM 60-01
Pace Project No.: 92608158
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92608158001
6001-HBW28
EPA 3010A
702999
EPA6010D
703108
92608158002
6001-HBW20
EPA 3010A
702999
EPA6010D
703108
92608158003
6001-HBW14
EPA 3010A
702999
EPA6010D
703108
92608158004
6001-HBW14B
EPA 3010A
702999
EPA6010D
703108
92608158005
6001-HBW14C
EPA 3010A
702999
EPA6010D
703108
92608158006
6001-HBW14D
EPA 3010A
702999
EPA6010D
703108
92608158007
6001-HB2006
EPA 3010A
702999
EPA6010D
703108
92608158008
6001-HB2008
EPA 3010A
702999
EPA6010D
703108
92608158009
6001-HB2010
EPA 3010A
702999
EPA6010D
703108
92608158001
6001-HBW28
EPA3005A
703049
EPA6020B
703172
92608158002
6001-HBW20
EPA3005A
703049
EPA6020B
703172
92608158003
6001-HBW14
EPA3005A
703049
EPA6020B
703172
92608158004
6001-HBW14B
EPA3005A
703049
EPA6020B
703172
92608158005
6001-HBW14C
EPA3005A
703049
EPA6020B
703172
92608158006
6001-HBW14D
EPA3005A
703049
EPA6020B
703172
92608158007
6001-HB2006
EPA3005A
703049
EPA6020B
703172
92608158008
6001-HB2008
EPA3005A
703049
EPA6020B
703172
92608158009
6001-HB2010
EPA3005A
703049
EPA6020B
703172
92608158001
6001-HBW28
EPA 8260D
702873
92608158002
6001-HBW20
EPA 8260D
702873
92608158003
6001-HBW14
EPA 8260D
702873
92608158004
6001-HBW14B
EPA 8260D
702873
92608158005
6001-HBW14C
EPA 8260D
702873
92608158006
6001-HBW14D
EPA 8260D
702873
92608158010
HB2006
EPA 8260D
702873
92608158011
HB2008
EPA 8260D
702873
92608158012
HB2010
EPA 8260D
702873
92608158013
TRIP BLANK
EPA 8260D
702873
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 39

r "Liu
Effective Date: 051121202205/12/2022
Laboratory receiving Samples:
Asheville ❑ Eden❑ Greenwood ❑. Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition Client Name; ject t WQ • 96Q8158
Upon Pro
Courier: ❑iced"Ex Duot ❑usp5 7client
❑ Commercial ❑Pace []Other: jj I I
926Dun
Custudy Sea[ Present? ❑Yes No Seals Intact? []Yes D No
Packing Material: ❑Hubble Wrap ❑Bubble Sags []None ❑ Other
Thermome r
VJ IR Gum ID: (`J� Type of ice: fW11t
`1 Correction Factor:
Cooler Temp: rAdd/Subtract (°C) ')
Cooler Temp Corrected ('C): L
USDA Regulated Soil (❑ N/AkNo
water sample)
Did samples originate inarantine zone within the United States; CA, NY, or SC
(check maml? FlYes
taste/fnitialsPerson EMaminfngGontents-2 ` `'_ [ .Z2-
❑Blue ❑fftne
Biological Tissue ozen?.
[]Yes❑No [/A
Temp should be above freezing to 67C
05arnples out of temp criteria, Samples on ice, cooling process
has begun
Did s;rnp les originate from a foreign saurce (inter tionafly,
incln ite Hawah and Puerto Rim]? MYpc NU
Comments/Discre p ancyt
Chain of Custody Present?
dyes
[]No
[IN/A
1.
5amples Arrived within. Hold Time?
es
[]No
[]N/A
2.
Short Holdl'TiineAnalysis (c72 hr.)?
❑Yes-
N
❑NIA
3.
Rush Turn Around Time Requested?
Dyes
524
❑NIA
4.
Sufficient Volume?
Yes
CjNo
❑NIA
5.
Correct ContainersUsed?
-Pace Containers Used?
❑yes
❑ii
❑Na
❑No.
❑N/A
F-1N/A
6.
Containers Intact?
es
[IN.
0IYJA
7.
Dissolveda na[ysis; Samples Field Filtered?
❑Y s
❑Nta:
N/A"
a..
Sample. Labels Match COC?
-Inciudes DateMme/ID/Analysis Matrfv
Yes
❑No
❑N/A
9.
Headspace in VOA Vials(>5-6mm)?
INS
EIN..
❑NJA
ia.
Trip Blank Present?
Trip Blank Custody Seals present?
es
Des
❑NZP.
❑N/A.
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spR containers:
CLIENT NOTIFICATiONJRFSOLLITiON
Person contacted:
Project Manager SCURF Review:
--2.r912[i�rianager.SFiERauie+rr: � __.�_ � _
Date/'Time:.
Date:
Field Data Required? ❑Yes ❑No
Qualtrax ID: 69614
Page 1 of 2
Page 36 of 39

Effective bate: 05R212022051-1212022.
' 9L'6Q8t.s8
*Check mark tap half of boss if pH andjordechlorknatkon Is verified' and praieet 4 Wo •
within the acceptance range for presefva an samples. PM : M14B Due Date, 06/20/22
€xce+Ltimn;�UflPk:folifor+vrTO.0 OffandGtease o�0 $t 5.water2QC.
CLIENT: 92-MECK CO
*tors hatf of iron-is.fa list-noatiaer of bottles
***Check all unpreserved Nitrates for chtdrine
K,
N
ti
T
4
4
5
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a
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can
m
NNN
N
N
TL.
N
N
\N
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y
Y\4
X
N\.
L\
N\Nr:.5
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X
N
N.
N\N
1
_
Ik
J
X/\
tV
12
I
N
-
12
p€i Adiustment tog for Preserved Samples
Sample 10 Type-OfRresemaite-preservation adjusted. _ Time preser aafa Amount, a€ftservaVtve Lot' #
added
^f;^,".a"`�.:....r�, �: .-,.a;a '.: g.��a o_2 •.�'l 3:FoZh rg ,7, aT! is co n,i �� i rn+:uiii no 4°`L
Crut of holdi incn.rrect p reservative; OUt of tempt incarrect:containers.
WOF"11 cafoiIna DEN
Qualtrax tD- 69614
Page 2 of'2
Page 37 of 39

;j
U
m
(") y
C7
;] rA
s
s
s
,D
co
N
Im
Cn
A
w
N
s
ITEM #
N
A �
0
0
0
0
0
0
z
n
m
N
Z
Go
2
m
i
m
S
m
S
m
S
m
w O
O
oa
m
a�
N
o A
m
n
A
A
A
A
ni
O
ni
4
a m N
f°
N
(n
m
o
}
T ^�>
N
y
N 7
O
i
c m 1
F
c
D
»
m
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m
o
x
o
m
V•
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•
W O D O N L o n O-
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y opg ❑N vg gno
n
�
y
�
_
�• o
m
�?
w
m
o
a
a m
O
v
m
'o
i
MATRIX CODE (see valid codes to fefl)
Z:E
#
3
m,
C
2
SAI.SPLE TYPE (G=GRAB C=CpP.SP)
`
y'
S
d
m'
Gi
R
O
NiO
m
m
D
uyr
rn
A
^
m
O
r
n
z
_
4
rrl
:0
_
$
m
c
m
a
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m
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3
i
m
I'd
m
m
m
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0z
ZO
O
Cti
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y
r
N
N
❑
�
o
v
v
r
tj
�
r•
Q
m
r
Gt
Sn
-¢i
m
SAMPLE TEUP AT COLLECTION
A
p
S2]
m
m
0
aa. 0
4 OF CONTAINERS
-
-
m
a
y
m
Unpreserved
v
o
m
o
O
m
H2SO4
c,
#
../
HNO3
d
m
L
m
v
o
HCI
cn
in
NaOH
nr
n
Ns2S203
mm
3
m
Methanol
Olher
m
K
Analyses Test
YIN
a
x
x
x
x
x
x
Metals- 0010/6020
s
X
I'd
x
N
„
c
G.
�
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M
a
A
a
n
IN
t
�
❑
y
y
T
liz
R
m
Q.
a
m
d
-
TEMP in C
to
1° to
q
Residual Chlorine (YIN)»'
n
m
o
E
y
Received on
tiA
Ice
��
y
y
(YIN)
m
O
uslcY
Sealed
z
Cooler
YIN
f
0
z
`�
l
\
P. Inlacl
�'
(YIN)
Ll
0
3
Page 38 of 39

0
n a;
m
N
c
ep
m
-i
m
en
A
w
to
ITEM #
3
'•'
c,
m
m
o
H w
N
o
]
a
..
3
2
2
2
a+
0
rn
0
rn
o
Z
n
n
O
O
O
O
M
O
Cv
Q
x
m
=
@
x
m
d 0
3
m c
�.
0
0
(+•
3
UI
cn
y
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z
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x
c
3
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)
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p
n
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a m
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H
O
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MATRIX CODE (see valid codes to left}
1
-1
-i
-1
So
#
SAMPLE TYPE (G=GRAB C=COMP)
ma-
N
m
O
�p
c
3
m
N
n
r
D
r
rn
N
g
m
0
a
z
?
m
n
z
m
C
v
m
c
m
w
D
m
r"
mm
c
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0
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z
o
a
=
t
CN
N
,y
�.1
N
3
4i
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.
m
r-
Z
4 f
m
13
V1
v
SAMPLE TEMP AT COLLECTION
c
m
a
m
a a
n
on D
m
# OF CONTAINERS
F
W
rt
rt
p N
'o
Unpreserved
4r�
ytt,�,
m
3
ro
o
o n
tfs
K
`r a
H2804
#
m
z
w
HNO3
-0
m
m
w
d
m
o
HCI
in
{a
NaOH
m
w
l�
666{�
n
Na2S203
m
d
m
Methanol
{�
Other
Analyses Test
YIN
r
\
m
5
a
Cep
x
x
x
Metals-fi01D76020
o
H
x
x
x
VOC's
v
m
i
s
1O
3
A
U`
A
]
u
N
�
\
m
m
%
1
�
<_
Z
m
IN
IN
TEMI in C
-C
Residual Chlorine (Y/N)
y
am
r.,
E
m
r
o
u
Reccit-cd on
_
�,�
Ice
r
i
/`�U
n
y
(YIN)
m
\
z
Sealed
Gooler
O
YIN
?
Samples
Intact
(YIN)
w
( n
n 0 n
m =r
n v.Zn
ID O O
m
n n #
o Q
Er Ic C
m
to J
� w
ID r-
CD� n
m ❑
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Z
c D y
nID
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N 0
N .t 0
CY N ii
n
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C CD
or m 7
a CL �•h
0 0
l!
Gi C
a 57
a
2,
6
n
Page 39 of 39

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 14, 2022
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92608280001 6001-HBW21
EPA 6010D
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92608280002 6001-HBW22
EPA 6010D
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
92608280003 6001-HBW12B
EPA 6010D
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92608280004 6001-HBW17B
EPA 6010D
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
CL
52
PASI-C
92608280005 6001-HBW12A
EPA 6010D
KH
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92608280006 TRIP BLANK
EPA 8260D
SAS
52
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW21 Lab ID: 92608280001 Collected: 06/07/22 09:35 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/09/22 12:26
06/09/22 20:38
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:38
7440-41-7
Barium
15.6
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:38
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:38
7440-43-9
Chromium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:38
7440-47-3
Copper
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:38
7440-50-8
Nickel
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:38
7440-02-0
Silver
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:38
7440-22-4
Lead
23.7
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:38
7439-92-1
Antimony
ND
ug/L
50.0
1
06/09/22 12:26
06/09/22 20:38
7440-36-0
Selenium
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 20:38
7782-49-2
Thallium
ND
ug/L
200
1
06/09/22 12:26
06/09/22 20:38
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:38
7440-62-2
Zinc
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:38
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 20:38
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:23
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 14:08
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 14:08
107-13-1
Benzene
ND
ug/L
1.0
1
06/09/22 14:08
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 14:08
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 14:08
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 14:08
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 14:08
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 14:08
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 14:08
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 14:08
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 14:08
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 14:08
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 14:08
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 14:08
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 14:08
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 14:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 14:08
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 14:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:08
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:08
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 14:08
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:08
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:08
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW21
Lab ID: 92608280001 Collected:
06/07/22
09:35
Received: 06/07/22 12:21 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:08
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:08
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:08
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/09/22 14:08
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/09/22 14:08
591-78-6
lodomethane
ND
ug/L
20.0
1
06/09/22 14:08
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
06/09/22 14:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/09/22 14:08
108-10-1
Styrene
ND
ug/L
1.0
1
06/09/22 14:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 14:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 14:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/09/22 14:08
127-18-4
Toluene
ND
ug/L
1.0
1
06/09/22 14:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/09/22 14:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/09/22 14:08
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/09/22 14:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/09/22 14:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/09/22 14:08
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/09/22 14:08
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/09/22 14:08
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/09/22 14:08
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/09/22 14:08
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/09/22 14:08
95-47-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
06/09/22 14:08
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
06/09/22 14:08
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
06/09/22 14:08
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW22 Lab ID: 92608280002 Collected: 06/07/22 09:15 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/09/22 12:26
06/09/22 20:57
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:57
7440-41-7
Barium
50.1
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:57
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:57
7440-43-9
Chromium
25.2
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:57
7440-47-3
Copper
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:57
7440-50-8
Nickel
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:57
7440-02-0
Silver
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 20:57
7440-22-4
Lead
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:57
7439-92-1
Antimony
ND
ug/L
50.0
1
06/09/22 12:26
06/09/22 20:57
7440-36-0
Selenium
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 20:57
7782-49-2
Thallium
ND
ug/L
200
1
06/09/22 12:26
06/09/22 20:57
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:57
7440-62-2
Zinc
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 20:57
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 20:57
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:29
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 15:59
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 15:59
107-13-1
Benzene
ND
ug/L
1.0
1
06/09/22 15:59
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 15:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 15:59
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 15:59
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 15:59
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 15:59
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 15:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 15:59
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 15:59
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 15:59
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 15:59
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 15:59
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 15:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 15:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 15:59
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 15:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 15:59
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 15:59
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 15:59
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/09/22 15:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 15:59
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW22
Lab ID: 92608280002 Collected:
06/07/22
09:15
Received: 06/07/22 12:21 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/09/22 15:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 15:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 15:59
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/09/22 15:59
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 15:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 15:59
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/09/22 15:59
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/09/22 15:59
591-78-6
lodomethane
ND
ug/L
20.0
1
06/09/22 15:59
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
06/09/22 15:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/09/22 15:59
108-10-1
Styrene
ND
ug/L
1.0
1
06/09/22 15:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 15:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 15:59
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/09/22 15:59
127-18-4
Toluene
ND
ug/L
1.0
1
06/09/22 15:59
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/09/22 15:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/09/22 15:59
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/09/22 15:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/09/22 15:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/09/22 15:59
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/09/22 15:59
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/09/22 15:59
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/09/22 15:59
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/09/22 15:59
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/09/22 15:59
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
06/09/22 15:59
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
06/09/22 15:59
17060-07-0
Toluene-d8(S)
103
%
70-130
1
06/09/22 15:59
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW12B Lab ID: 92608280003 Collected: 06/07/22 10:00 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/09/22 12:26
06/09/22 21:02
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:02
7440-41-7
Barium
67.7
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:02
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:02
7440-43-9
Chromium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:02
7440-47-3
Copper
42.0
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:02
7440-50-8
Nickel
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:02
7440-02-0
Silver
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:02
7440-22-4
Lead
35.6
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:02
7439-92-1
Antimony
ND
ug/L
50.0
1
06/09/22 12:26
06/09/22 21:02
7440-36-0
Selenium
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:02
7782-49-2
Thallium
ND
ug/L
200
1
06/09/22 12:26
06/09/22 21:02
7440-28-0
Vanadium
73.1
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:02
7440-62-2
Zinc
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:02
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:02
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:35
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 14:26
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 14:26
107-13-1
Benzene
ND
ug/L
1.0
1
06/09/22 14:26
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 14:26
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 14:26
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 14:26
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 14:26
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 14:26
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 14:26
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 14:26
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 14:26
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 14:26
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 14:26
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 14:26
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 14:26
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 14:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 14:26
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 14:26
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:26
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:26
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 14:26
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:26
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:26
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW12B
Lab ID: 92608280003 Collected:
06/07/22
10:00
Received: 06/07/22 12:21 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 14:26
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 14:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/09/22 14:26
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/09/22 14:26
591-78-6
lodomethane
ND
ug/L
20.0
1
06/09/22 14:26
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
06/09/22 14:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/09/22 14:26
108-10-1
Styrene
ND
ug/L
1.0
1
06/09/22 14:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 14:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 14:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/09/22 14:26
127-18-4
Toluene
ND
ug/L
1.0
1
06/09/22 14:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/09/22 14:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/09/22 14:26
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/09/22 14:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/09/22 14:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/09/22 14:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/09/22 14:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/09/22 14:26
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/09/22 14:26
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/09/22 14:26
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/09/22 14:26
95-47-6
Surrogates
4-Bromofluorobenzene (S)
105
%
70-130
1
06/09/22 14:26
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
06/09/22 14:26
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
06/09/22 14:26
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW17B Lab ID: 92608280004 Collected: 06/07/22 10:25 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/09/22 12:26
06/09/22 21:06
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:06
7440-41-7
Barium
63.2
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:06
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:06
7440-43-9
Chromium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:06
7440-47-3
Copper
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:06
7440-50-8
Nickel
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:06
7440-02-0
Silver
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:06
7440-22-4
Lead
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:06
7439-92-1
Antimony
ND
ug/L
50.0
1
06/09/22 12:26
06/09/22 21:06
7440-36-0
Selenium
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:06
7782-49-2
Thallium
ND
ug/L
200
1
06/09/22 12:26
06/09/22 21:06
7440-28-0
Vanadium
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:06
7440-62-2
Zinc
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:06
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:06
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:41
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 18:28
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 18:28
107-13-1
Benzene
10.4
ug/L
1.0
1
06/09/22 18:28
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 18:28
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 18:28
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 18:28
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 18:28
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 18:28
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 18:28
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 18:28
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 18:28
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 18:28
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 18:28
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 18:28
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 18:28
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 18:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 18:28
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 18:28
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 18:28
95-50-1
1,4-Dichlorobenzene
1.2
ug/L
1.0
1
06/09/22 18:28
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 18:28
110-57-6
1,1-Dichloroethane
7.5
ug/L
1.0
1
06/09/22 18:28
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 18:28
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW17B Lab ID: 92608280004 Collected: 06/07/22 10:25 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/14/2022 02:28 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
150
ug/L
1.6
ug/L
10.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
31.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
26.0
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
2.4
ug/L
12.6
ug/L
ND
ug/L
12.6
ug/L
102
%
101
%
101
%
1.0
1
06/09/22 18:28
75-35-4
1.0
1
06/09/22 18:28
156-59-2
1.0
1
06/09/22 18:28
156-60-5
1.0
1
06/09/22 18:28
78-87-5
1.0
1
06/09/22 18:28
10061-01-5
1.0
1
06/09/22 18:28
10061-02-6
1.0
1
06/09/22 18:28
100-41-4
5.0
1
06/09/22 18:28
591-78-6
20.0
1
06/09/22 18:28
74-88-4 v2
5.0
1
06/09/22 18:28
75-09-2
5.0
1
06/09/22 18:28
108-10-1
1.0
1
06/09/22 18:28
100-42-5
1.0
1
06/09/22 18:28
630-20-6
1.0
1
06/09/22 18:28
79-34-5
1.0
1
06/09/22 18:28
127-18-4
1.0
1
06/09/22 18:28
108-88-3
1.0
1
06/09/22 18:28
71-55-6
1.0
1
06/09/22 18:28
79-00-5
1.0
1
06/09/22 18:28
79-01-6
1.0
1
06/09/22 18:28
75-69-4
1.0
1
06/09/22 18:28
96-18-4
2.0
1
06/09/22 18:28
108-05-4
1.0
1
06/09/22 18:28
75-01-4
1.0
1
06/09/22 18:28
1330-20-7
2.0
1
06/09/22 18:28
179601-23-1
1.0
1
06/09/22 18:28
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/09/22 18:28 460-00-4
06/09/22 18:28 17060-07-0
06/09/22 18:28 2037-26-5
Page 11 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW12A Lab ID: 92608280005 Collected: 06/07/22 09:50 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
06/09/22 12:26
06/09/22 21:11
7440-38-2
Beryllium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:11
7440-41-7
Barium
42.0
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:11
7440-39-3
Cadmium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:11
7440-43-9
Chromium
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:11
7440-47-3
Copper
27.4
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:11
7440-50-8
Nickel
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:11
7440-02-0
Silver
ND
ug/L
10.0
1
06/09/22 12:26
06/09/22 21:11
7440-22-4
Lead
28.5
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:11
7439-92-1
Antimony
ND
ug/L
50.0
1
06/09/22 12:26
06/09/22 21:11
7440-36-0
Selenium
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:11
7782-49-2
Thallium
ND
ug/L
200
1
06/09/22 12:26
06/09/22 21:11
7440-28-0
Vanadium
41.6
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:11
7440-62-2
Zinc
ND
ug/L
20.0
1
06/09/22 12:26
06/09/22 21:11
7440-66-6
Cobalt
ND
ug/L
40.0
1
06/09/22 12:26
06/09/22 21:11
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
06/08/22 14:42
06/09/22 23:58
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 14:45
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 14:45
107-13-1
Benzene
ND
ug/L
1.0
1
06/09/22 14:45
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 14:45
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 14:45
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 14:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 14:45
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 14:45
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 14:45
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 14:45
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 14:45
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 14:45
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 14:45
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 14:45
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 14:45
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 14:45
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 14:45
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 14:45
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:45
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 14:45
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 14:45
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:45
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 14:45
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 27

leAnalyiical
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: 6001-HBW12A Lab ID: 92608280005 Collected: 06/07/22 09:50 Received: 06/07/22 12:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/14/2022 02:28 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
103
%
107
%
102
%
1.0
1
06/09/22 14:45
75-35-4
1.0
1
06/09/22 14:45
156-59-2
1.0
1
06/09/22 14:45
156-60-5
1.0
1
06/09/22 14:45
78-87-5
1.0
1
06/09/22 14:45
10061-01-5
1.0
1
06/09/22 14:45
10061-02-6
1.0
1
06/09/22 14:45
100-41-4
5.0
1
06/09/22 14:45
591-78-6
20.0
1
06/09/22 14:45
74-88-4 v2
5.0
1
06/09/22 14:45
75-09-2
5.0
1
06/09/22 14:45
108-10-1
1.0
1
06/09/22 14:45
100-42-5
1.0
1
06/09/22 14:45
630-20-6
1.0
1
06/09/22 14:45
79-34-5
1.0
1
06/09/22 14:45
127-18-4
1.0
1
06/09/22 14:45
108-88-3
1.0
1
06/09/22 14:45
71-55-6
1.0
1
06/09/22 14:45
79-00-5
1.0
1
06/09/22 14:45
79-01-6
1.0
1
06/09/22 14:45
75-69-4
1.0
1
06/09/22 14:45
96-18-4
2.0
1
06/09/22 14:45
108-05-4
1.0
1
06/09/22 14:45
75-01-4
1.0
1
06/09/22 14:45
1330-20-7
2.0
1
06/09/22 14:45
179601-23-1
1.0
1
06/09/22 14:45
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/09/22 14:45 460-00-4
06/09/22 14:45 17060-07-0
06/09/22 14:45 2037-26-5
Page 13 of 27

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[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: TRIP BLANK
Lab ID: 92608280006 Collected:
06/07/22
09:05
Received: 06/07/22 12:21 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
06/09/22 12:53
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
06/09/22 12:53
107-13-1
Benzene
ND
ug/L
1.0
1
06/09/22 12:53
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
06/09/22 12:53
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/09/22 12:53
75-27-4
Bromoform
ND
ug/L
1.0
1
06/09/22 12:53
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/09/22 12:53
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
06/09/22 12:53
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
06/09/22 12:53
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
06/09/22 12:53
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
06/09/22 12:53
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/09/22 12:53
75-00-3
Chloroform
ND
ug/L
1.0
1
06/09/22 12:53
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/09/22 12:53
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
06/09/22 12:53
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/09/22 12:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/09/22 12:53
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/09/22 12:53
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 12:53
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/09/22 12:53
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
06/09/22 12:53
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
06/09/22 12:53
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/09/22 12:53
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/09/22 12:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 12:53
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/09/22 12:53
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
06/09/22 12:53
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 12:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/09/22 12:53
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/09/22 12:53
100-41-4
2-Hexanone
ND
ug/L
5.0
1
06/09/22 12:53
591-78-6
lodomethane
ND
ug/L
20.0
1
06/09/22 12:53
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
06/09/22 12:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/09/22 12:53
108-10-1
Styrene
ND
ug/L
1.0
1
06/09/22 12:53
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 12:53
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/09/22 12:53
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/09/22 12:53
127-18-4
Toluene
ND
ug/L
1.0
1
06/09/22 12:53
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/09/22 12:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/09/22 12:53
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/09/22 12:53
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/09/22 12:53
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/09/22 12:53
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/09/22 12:53
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
06/09/22 12:53
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Sample: TRIP BLANK
Parameters
Lab ID: 92608280006 Collected: 06/07/22 09:05
Results Units Report Limit DF
Received: 06/07/22 12:21 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
06/09/22 12:53
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
06/09/22 12:53
179601-23-1
o-Xylene
ND ug/L
1.0
1
06/09/22 12:53
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103 %
70-130
1
06/09/22 12:53
460-00-4
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
06/09/22 12:53
17060-07-0
Toluene-d8(S)
103 %
70-130
1
06/09/22 12:53
2037-26-5
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
QC Batch: 703340 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005
METHOD BLANK: 3670317 Matrix: Water
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
50.0
06/09/2218:53
Arsenic
ug/L
ND
30.0
06/09/2218:53
Barium
ug/L
ND
10.0
06/09/2218:53
Beryllium
ug/L
ND
10.0
06/09/2218:53
Cadmium
ug/L
ND
10.0
06/09/2218:53
Chromium
ug/L
ND
10.0
06/09/2218:53
Cobalt
ug/L
ND
40.0
06/09/2218:53
Copper
ug/L
ND
20.0
06/09/2218:53
Lead
ug/L
ND
20.0
06/09/2218:53
Nickel
ug/L
ND
20.0
06/09/2218:53
Selenium
ug/L
ND
40.0
06/09/2218:53
Silver
ug/L
ND
10.0
06/09/2218:53
Thallium
ug/L
ND
200
06/09/2218:53
Vanadium
ug/L
ND
20.0
06/09/2218:53
Zinc
ug/L
ND
20.0
06/09/2218:53
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3670318
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
1060
106
80-120
Arsenic
ug/L
1000
1080
108
80-120
Barium
ug/L
1000
1050
105
80-120
Beryllium
ug/L
1000
1050
105
80-120
Cadmium
ug/L
1000
1070
107
80-120
Chromium
ug/L
1000
1060
106
80-120
Cobalt
ug/L
1000
1070
107
80-120
Copper
ug/L
1000
1080
108
80-120
Lead
ug/L
1000
1050
105
80-120
Nickel
ug/L
1000
1070
107
80-120
Selenium
ug/L
1000
1050
105
80-120
Silver
ug/L
1000
1020
102
80-120
Thallium
ug/L
1000
1030
103
80-120
Vanadium
ug/L
1000
1140
114
80-120
Zinc
ug/L
1000
1060
106
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 27

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDILL
92608280
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3670477
3670478
MS
MSD
92608280001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1060
1080
106
108
75-125
2
Arsenic
ug/L
ND
1000
1000
1060
1090
106
109
75-125
2
Barium
ug/L
15.6
1000
1000
1080
1100
106
108
75-125
2
Beryllium
ug/L
ND
1000
1000
1050
1080
105
108
75-125
3
Cadmium
ug/L
ND
1000
1000
1070
1080
107
108
75-125
2
Chromium
ug/L
ND
1000
1000
1060
1100
105
109
75-125
4
Cobalt
ug/L
ND
1000
1000
1060
1080
106
108
75-125
2
Copper
ug/L
ND
1000
1000
1100
1140
109
112
75-125
3
Lead
ug/L
23.7
1000
1000
1060
1080
104
106
75-125
2
Nickel
ug/L
ND
1000
1000
1060
1080
106
108
75-125
2
Selenium
ug/L
ND
1000
1000
1060
1090
106
109
75-125
3
Silver
ug/L
ND
1000
1000
1000
1030
100
103
75-125
2
Thallium
ug/L
ND
1000
1000
1040
1060
104
106
75-125
2
Vanadium
ug/L
ND
1000
1000
1150
1180
113
116
75-125
3
Zinc
ug/L
ND
1000
1000
1050
1070
104
107
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
QC Batch: 703049 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005
METHOD BLANK: 3668809
Matrix:
Water
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
06/09/22 21:35
LABORATORY CONTROL SAMPLE:
3668810
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
107
107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3669048 3669049
MS MSD
92608158003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 100 100 107 106 107 106 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
QC Batch: 703327 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005, 92608280006
METHOD BLANK: 3670221 Matrix: Water
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005, 92608280006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/09/22 12:16
1,1,1-Trichloroethane
ug/L
ND
1.0
06/09/22 12:16
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/09/22 12:16
1,1,2-Trichloroethane
ug/L
ND
1.0
06/09/22 12:16
1,1-Dichloroethane
ug/L
ND
1.0
06/09/22 12:16
1,1-Dichloroethene
ug/L
ND
1.0
06/09/22 12:16
1,2,3-Trichloropropane
ug/L
ND
1.0
06/09/22 12:16
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
06/09/22 12:16
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/09/22 12:16
1,2-Dichlorobenzene
ug/L
ND
1.0
06/09/22 12:16
1,2-Dichloroethane
ug/L
ND
1.0
06/09/22 12:16
1,2-Dichloropropane
ug/L
ND
1.0
06/09/22 12:16
1,4-Dichlorobenzene
ug/L
ND
1.0
06/09/22 12:16
2-Butanone (MEK)
ug/L
ND
5.0
06/09/22 12:16
2-Hexanone
ug/L
ND
5.0
06/09/22 12:16
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/09/22 12:16
Acetone
ug/L
ND
25.0
06/09/22 12:16
Acrylonitrile
ug/L
ND
10.0
06/09/22 12:16
Benzene
ug/L
ND
1.0
06/09/22 12:16
Bromochloromethane
ug/L
ND
1.0
06/09/22 12:16
Bromodichloromethane
ug/L
ND
1.0
06/09/22 12:16
Bromoform
ug/L
ND
1.0
06/09/22 12:16
Bromomethane
ug/L
ND
2.0
06/09/22 12:16
Carbon disulfide
ug/L
ND
2.0
06/09/22 12:16
Carbon tetrachloride
ug/L
ND
1.0
06/09/22 12:16
Chlorobenzene
ug/L
ND
1.0
06/09/22 12:16
Chloroethane
ug/L
ND
1.0
06/09/22 12:16
Chloroform
ug/L
ND
1.0
06/09/22 12:16
Chloromethane
ug/L
ND
1.0
06/09/22 12:16
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/09/22 12:16
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/09/22 12:16
Dibromochloromethane
ug/L
ND
1.0
06/09/22 12:16
Dibromomethane
ug/L
ND
1.0
06/09/22 12:16
Ethylbenzene
ug/L
ND
1.0
06/09/22 12:16
lodomethane
ug/L
ND
20.0
06/09/22 12:16
m&p-Xylene
ug/L
ND
2.0
06/09/22 12:16
Methylene Chloride
ug/L
ND
5.0
06/09/22 12:16
o-Xylene
ug/L
ND
1.0
06/09/22 12:16
Styrene
ug/L
ND
1.0
06/09/22 12:16
Tetrachloroethene
ug/L
ND
1.0
06/09/22 12:16
v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 27

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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
METHOD BLANK: 3670221 Matrix: Water
Associated Lab Samples: 92608280001, 92608280002, 92608280003, 92608280004, 92608280005, 92608280006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
06/09/22 12:16
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/09/22 12:16
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/09/22 12:16
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
06/09/22 12:16
Trichloroethene
ug/L
ND
1.0
06/09/22 12:16
Trichlorofluoromethane
ug/L
ND
1.0
06/09/22 12:16
Vinyl acetate
ug/L
ND
2.0
06/09/22 12:16
Vinyl chloride
ug/L
ND
1.0
06/09/22 12:16
Xylene (Total)
ug/L
ND
1.0
06/09/22 12:16
1,2-Dichloroethane-d4 (S)
%
108
70-130
06/09/22 12:16
4-Bromofluorobenzene (S)
%
103
70-130
06/09/22 12:16
Toluene-d8 (S)
%
104
70-130
06/09/22 12:16
LABORATORY CONTROL SAMPLE:
Parameter
3670222
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,1-Trichloroethane
ug/L
50
51.1
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.9
98
70-130
1,1,2-Trichloroethane
ug/L
50
48.3
97
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
53.1
106
70-132
1,2,3-Trichloropropane
ug/L
50
48.9
98
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
43.5
87
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.6
101
70-130
1,2-Dichlorobenzene
ug/L
50
49.5
99
70-130
1,2-Dichloroethane
ug/L
50
47.0
94
70-130
1,2-Dichloropropane
ug/L
50
48.2
96
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
113
113
70-133
2-Hexanone
ug/L
100
103
103
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
100
100
70-130
Acetone
ug/L
100
97.8
98
70-144
Acrylonitrile
ug/L
250
262
105
70-130
Benzene
ug/L
50
47.5
95
70-130
Bromochloromethane
ug/L
50
41.5
83
70-130
Bromodichloromethane
ug/L
50
43.6
87
70-130
Bromoform
ug/L
50
49.1
98
70-131
Bromomethane
ug/L
50
41.4
83
30-177 v3
Carbon disulfide
ug/L
50
50.9
102
70-133
Carbon tetrachloride
ug/L
50
48.3
97
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
57.8
116
46-131
Chloroform
ug/L
50
49.0
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 27

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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
LABORATORY CONTROL SAMPLE:
Parameter
3670222
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
56.0
cis-1,2-Dichloroethene
ug/L
50
49.9
cis-1,3-Dichloropropene
ug/L
50
45.9
Dibromochloromethane
ug/L
50
49.7
Dibromomethane
ug/L
50
41.6
Ethylbenzene
ug/L
50
50.8
lodomethane
ug/L
100
57.4
m&p-Xylene
ug/L
100
99.3
Methylene Chloride
ug/L
50
44.5
o-Xylene
ug/L
50
47.8
Styrene
ug/L
50
49.6
Tetrachloroethene
ug/L
50
49.5
Toluene
ug/L
50
45.9
trans-1,2-Dichloroethene
ug/L
50
50.4
trans- 1,3-Dichloropropene
ug/L
50
46.2
trans-1,4-Dichloro-2-butene
ug/L
50
56.7
Trichloroethene
ug/L
50
47.0
Trichlorofluoromethane
ug/L
50
47.4
Vinyl acetate
ug/L
100
121
Vinyl chloride
ug/L
50
60.7
Xylene (Total)
ug/L
150
147
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
112
49-130
100
70-130
92
70-130
99
70-130
83
70-130
102
70-130
57
47-140 v3
99
70-130
89
68-130
96
70-130
99
70-130
99
70-130
92
70-130
101
70-130
92
70-130
113
25-200
94
70-130
95
61-130
121
70-140
121
59-142
98
70-130
101
70-130
102
70-130
95
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3670223
MS
92608455004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3670224
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
16.0
17.3
80
87
70-135
8
1,1,1-Trichloroethane
ug/L
ND
20
20
18.4
21.3
92
106
70-148
14
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
15.3
16.8
76
84
70-131
10
1,1,2-Trichloroethane
ug/L
ND
20
20
16.2
18.4
81
92
70-136
13
1,1-Dichloroethane
ug/L
ND
20
20
18.6
21.3
93
106
70-147
13
1,1-Dichloroethene
ug/L
ND
20
20
19.2
22.1
96
111
70-158
14
1,2,3-Trichloropropane
ug/L
ND
20
20
15.6
15.2
78
76
67-137
2
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
13.2
15.6
66
78
69-136
17 M1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
15.3
17.0
77
85
70-137
10
1,2-Dichlorobenzene
ug/L
ND
20
20
16.7
18.8
83
94
70-133
12
1,2-Dichloroethane
ug/L
ND
20
20
17.1
19.8
86
99
67-138
15
1,2-Dichloropropane
ug/L
ND
20
20
17.5
19.2
88
96
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
18.4
20.3
82
92
70-133
10
2-Butanone (MEK)
ug/L
ND
40
40
31.4
37.7
79
94
61-147
18
2-Hexanone
ug/L
ND
40
40
28.3
32.0
71
80
67-139
12
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
28.8
32.7
72
82
67-136
13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3670223
MS
92608455004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3670224
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
31.1
37.1
78
93
55-159
18
Acrylonitrile
ug/L
ND
100
100
85.5
95.3
85
95
68-140
11
Benzene
ug/L
4.9
20
20
22.8
25.0
89
100
67-150
9
Bromochloromethane
ug/L
ND
20
20
18.9
20.4
95
102
70-146
8
Bromodichloromethane
ug/L
ND
20
20
17.4
19.5
87
97
70-138
11
Bromoform
ug/L
ND
20
20
14.4
15.7
72
79
57-138
9
Bromomethane
ug/L
ND
20
20
10.3
14.7
51
74
10-200
36 R1
Carbon disulfide
ug/L
ND
20
20
19.0
20.6
95
103
70-152
8
Carbon tetrachloride
ug/L
ND
20
20
19.0
20.5
95
102
70-147
7
Chlorobenzene
ug/L
ND
20
20
17.3
19.0
85
93
70-137
9
Chloroethane
ug/L
ND
20
20
21.1
24.5
105
123
51-166
15
Chloroform
ug/L
ND
20
20
17.5
19.6
87
98
70-144
11
Chloromethane
ug/L
ND
20
20
17.9
20.0
90
100
24-161
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.5
21.3
92
102
67-148
9
cis-1,3-Dichloropropene
ug/L
ND
20
20
15.9
18.2
80
91
70-142
14
Dibromochloromethane
ug/L
ND
20
20
15.3
16.9
77
85
68-138
10
Dibromomethane
ug/L
ND
20
20
17.5
19.8
88
99
70-134
12
Ethylbenzene
ug/L
ND
20
20
18.2
19.4
87
93
68-143
6
lodomethane
ug/L
ND
40
40
36.2
44.3
90
111
20-161
20
m&p-Xylene
ug/L
2.4
40
40
37.5
40.4
88
95
53-157
7
Methylene Chloride
ug/L
ND
20
20
14.4
16.8
72
84
64-148
16 IK
o-Xylene
ug/L
4.6
20
20
21.9
23.8
87
96
68-143
8
Styrene
ug/L
ND
20
20
17.1
18.9
85
94
70-136
10
Tetrachloroethene
ug/L
ND
20
20
16.3
18.0
81
90
70-139
10
Toluene
ug/L
2.4
20
20
19.9
21.6
87
96
47-157
8
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.4
21.3
97
106
70-149
9
trans- 1,3-Dichloropropene
ug/L
ND
20
20
15.5
18.4
78
92
70-138
17
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
13.0
14.4
65
72
31-145
10
Trichloroethene
ug/L
ND
20
20
18.6
19.9
93
100
70-149
7
Trichlorofluoromethane
ug/L
ND
20
20
18.4
20.5
92
103
61-154
11
Vinyl acetate
ug/L
ND
40
40
31.5
35.8
79
90
48-156
13
Vinyl chloride
ug/L
2.4
20
20
22.1
24.2
99
109
55-172
9
Xylene (Total)
ug/L
7.0
60
60
59.4
64.2
87
95
66-145
8
1,2-Dichloroethane-d4 (S)
%
104
102
70-130
4-Bromofluorobenzene (S)
%
100
99
70-130
Toluene-d8(S)
%
101
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/14/2022 02:28 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 27

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: HARRISBURG RD LANDILL
Pace Project No.: 92608280
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92608280001
6001-HBW21
EPA 3010A
703340
EPA6010D
703436
92608280002
6001-HBW22
EPA 3010A
703340
EPA6010D
703436
92608280003
6001-HBW12B
EPA 3010A
703340
EPA6010D
703436
92608280004
6001-HBW17B
EPA 3010A
703340
EPA6010D
703436
92608280005
6001-HBW12A
EPA 3010A
703340
EPA6010D
703436
92608280001
6001-HBW21
EPA3005A
703049
EPA6020B
703172
92608280002
6001-HBW22
EPA3005A
703049
EPA6020B
703172
92608280003
6001-HBW12B
EPA3005A
703049
EPA6020B
703172
92608280004
6001-HBW17B
EPA3005A
703049
EPA6020B
703172
92608280005
6001-HBW12A
EPA3005A
703049
EPA6020B
703172
92608280001
6001-HBW21
EPA 8260D
703327
92608280002
6001-HBW22
EPA 8260D
703327
92608280003
6001-HBW12B
EPA 8260D
703327
92608280004
6001-HBW17B
EPA 8260D
703327
92608280005
6001-HBW12A
EPA 8260D
703327
92608280006
TRIP BLANK
EPA 8260D
703327
Date: 06/14/2022 02:28 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 24 of 27

�L. I ICte. CNv t-t•QNt I'1UNI-UUU3 vUl sample Condition Upon Receipt
;- -ace
. I . • ii
Effective Date: 05112/202205/12/2022
Laboratory receiving samples:
Asheville ❑
Eden❑ Greenwood
❑ Huntersville d
Raleigh[] Mechanicsville❑ Atlanta❑ Kernersville❑
Sample
Client Name:
p.0
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Al,
Courier:
El Commercial
Fed Ex
❑Pace
UPS LISPS
❑Other.
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Custody Seal Present? ❑Yes do
Seals Intact? ❑Yes
VN092608�280
Date/Initials Person Examining Contents: r __
Packing Material:
❑Bubble Wrap
EfBBubble Bags ❑None
❑ Other Biological Tissue oxen? C -I(Z2-
Thermome r:
nYes RNo I Y1NIA
IR Gun ID:
4 Type of ice: Vel ❑Blue
Correction Factor:
Cooler Temp: Z i Add/Subtract (°C)
Cooler Temp Corrected ( 9 `
USDA Regulated Soil ( L%dNIA, water sample) }
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maps)? I—IYes MNO
Chain of Custody Present?
es
❑No
❑N/A
1.
Samples Arrived within Hold Time?
es
Elo
N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
Des
a
❑N/A
4.
Sufficient Volume?
dyes
❑No
[]N/A
5.
Correct Containers Used?
es
❑No
❑N/A
6.
-Pace Containers Used?
Yes
❑No
❑N/A
Containers Intact?
Yes
❑No
❑N
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[-]No
GkA
F9.
Sample Labels Match COC?
es
❑No
❑N/A
❑None
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Ricol? [:]Yes ❑No
Comments/Discreoancv:
-Includes Date/Time/ID/Analysis Matrix: M
Headspace in VOA Vials (>5-6mm)? E:Iyv No ❑N/A 10.
Trip Blank Present? 6Xes ❑No ❑N/A 11,
Trip Blank Custody Seals Present? ❑Yes WZ. ❑N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: bate/Time:
Project Manager SCURF Review: Date:
Project Manager SRF RN411N141' Ca'tr.
Qualtrax ID; 69614 Page 1 of 2 Page 25 of 27

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Page 26 of 27

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