MO-28888_48094_CA_IAR_20211101_Initial Abatement Report

20 Day Report and Initial Abatement Report
West Sugar Creek LLC
2422 West Sugar Creek
Charlotte NC
(Former Players Sporting Goods)
Contacts:
Owner: West Sugar Creek LLC 2131 Ayrsley Town Blvd, Charlotte NC Andy Hinson (704 ) 975-
5758
Closure Contractor; RPI, Mike Holcomb, PO Box 519 Cornelius, NC [phone]
Consultant; Philip Thompson PG., 2411 Lawyers Road West, Indian Trail NC 28079 (704) 882-
2788
Laboratory; Laboratory; SGS 4405 Vinland Road, Orlando Fl. 32811 NC 1D # 573 (704) 919-
1533,
UST release discovered October 7,2019
Quantity of release: Unknown
Source of release: Heating Oil UST
Type of release: 42 Heating Oil (Diesel Fuel)
Gasoline
Size and contents of UST:
1.550-ballon Heating Oil
2. 550-gallon Heating Oil
Quantity of soil excavated, 10 Tons
Minimal soil excavated. One TPH sample at fill port, One risk based sample at 7' below grade.
One Risk based Water Sample
Longitude and Latitude of the Site.
35.26985`N - 80.797954 W
Philip Thompson PG

Philip R. Thompson P.G.
4"d Ewwzee smiew
2411.da"e w Rmd Ved 7nstd -&& 2g079 (704) 592- 27,F8
Ms Trudy Beverly
NCDENR Mooresville Regional Office
610 East Center Avenue
Mooresville NC 28115
Re. Twenty Day Report and Initial Abatement, including Excavation and Soil Remediation
for the West Sugar Creek LLC (former Players Sporting Goods), 2422 West Sugar Creek
Road, Charlotte NC.
Dear Ms. Beverly
I respectfully submit for your review and comment, this report summarizing the Soil Excavation
and Remediation for two 550-Gallon Non -Regulated, Non -Registered Gasoline Underground
Storage Tanks at the former Players Sporting Goods, 2422 West Sugar Creek Road, Charlotte
NC.
Contacts.
Owner: West Sugar Creek LLC 2131 Ayrsley Town Blvd, Charlotte NC Andy Hinson (704 ) 975-
5758
Closure Contractor; RPI, Mike Holcomb, PO Box 519 Cornelius, NC [phone]
Consultant; Philip Thompson PG., 2411 Lawyers Road West, Indian Trail NC 28079 (704) 882-
2788
Laboratory; Laboratory; SGS 4405 Vinland Road, Orlando Fl. 32811 NC ID # 573 (704) 919-
1533,
Tank
Installation
Size in
Tank
Last Contents
Previous
No.
Date
Gallons
Dimensions
Contents
I
Unknown
550
4' by 5.5'
Heating Oil
Heating Oil
2
Unknown
550
4' by 5.5'
Heating Oil
Heating Oil
Site History
The UST's at the site was utilized for heating the commercial building at the site. The location of
the site is indicated on a excerpt of the 7.5 minute USGS map for Derita NC and is presented as
Figure 1. An Excerpt from the Mecklenburg County Polaris site indicating the property boundaries
is attached as Figure 2.

There is notice on contaminated property the site due to a Dry Cleaning facility located nearby. The
dry cleaning investigation found no contamination of the property, the notice was put in place due to
the proximity of the site..
Remediation Activities
On October 7, 2019, RPI and TGES initiated the excavation activities at the site. A soil sample was
collected at the 6" below grade near the fill port confirming spillage from the UST. During the UST
removal an additional UST was encountered. Neither Soil staining or odors were encountered in
the excavation. Approximately 10 yards, (14.5) Tons) of soil was excavated. The location of the
USTs and sample CS-1 is indicated on Figure 3. Please note the UST were predominantly located
on the right of way of Hunter Blvd.
The excavation was 8' by 6' by 7' deep. Sample CS-1 was collected at 7' below grade at the base
of the excavation.
The Confirmation samples was delivered to SGS Laboratories and analyzed by EPA Methods 8260,
8270, VPH and EPH. The results of the soil sampling are summarized on Table 1. The analytical
data associated with the sampling events is presented in Appendix A, along with the Chain of
Custodies.
Receptors
The Site is served by public water, TGES found no wells with 150 feet of the source.
Results and Recommendations
The sampling data indicate the soil has been exceeded soil to groundwater for three constituents.
Benzene was detected at .0099 mg/kg, Soil to Groundwater for Benzene is .0056 mg/kg.
Naphthalene was detected at .822J mg/kg, Soil to Groundwater for Naphthalene .2 mg/kg.
MADEP VPH/EPH was detected at 33 mg/kg ,. Soil to Groundwater for MADEP VPH/EPH is 31
mg/kg. All constituents are less than residential standards.
There are no wells with 150 feet of the UST. Since the site is already under a Notice of
Contamination for Dry Cleaning Fluid. TGES recommends the site be closed with a NORP for soil
and groundwater.
Please call me at 704 882-2788 if you have any questions or require any additional information.
Philip R. Thompson P.G_

Geologist
Attachments

Table 2.. Soil Analytical Data
Hison Property Sugar Creek Road
Charlotte
Date Collected
1O/712O19
CS-1
S. to G.
Residential
Industrial
SPA Method 8260
7'
Benzene
D_O099
0.0056
18
164
Toluene
0.31
4.3
1200
32000
Ethylbenzene
0.0635
4.9
1660
40000
Xylenes
0 702
4A
3129
8476O
N- Butyl -Benzene
0,0335
4.3
.626
16350
Sec Butyl -Benzene
0.0136
3.3
626
16350
Tert Butyl -Benzene
ND
3.4
626
•16350
isopropyl -benzene-
0.0133
1.7
1564
4O880
naphthalene
0.148
0.2
1.5.7
27
1,2,4 Trimelhylbenzene
1.23
0.2
5.5
27
1,3,5 Trinnathylbenzene
0.151
8.3
782
20440
MTBE
NO
0.091
350
31100
1PE
N D
0.37
155
4058
EPA Method 8270
Phenanthrene,
NO
56
469
12264
1-methyl-naphthalene
0.223
0.004
20
100
2-methyl-naphthalene
0.423
3.6
63
1635
naphthalene
J2.2i
0.16
313
8176
Flourene
ND
47
620
113001O
Pyrene
NO
270
469
12264
Flouranthene
NO
330
625
9930
Benzo anthrocene
NC
0.17
6.6
32
Benzo Pyrene
NO
0.058
O.66
3.2
Benzo (K) Flourathene
NO
5.8
66
327
Benzo (8) Flourathene
NO
0.6
6.6
32
MADEP VPH
C-5 to C-8 4.19 68 939 24528
C-9 to C-16 79 640 -1500 3600O
C-19 to C-36 23 Immobile
C-9 to C 22 33 31 469 12264
VPH acid EPH results in micrograms per liter
Numbers in Blue exceed soil to groundwaler
Numbers in l3olrr Pad exceed residential standards

Figures

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Figure 1. Site Location Map Thompson Geologic
2422 West Sugar Creek Road 2411 Lawyers Road West
Charlotte NC IndianTrail NC 28079

Polaris 3 G Map — Mecklenburg County, North Carolina
Figure 2. 2422 West Sugar Creek

Appendix B
Hazardous Waste Manifests

Appendix A
Soil Analytical .Data

Appendix C
Tank Disposal Certificate

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SGS,
Orlando, FL
The results set forth herein are provided by SGS North America Inc. e-Hardeopy 2.0
Atttattuated Report
Technical Report for
Thompson Geological
Hinson Property; N Sugur Creek, Charlotte, NC
SGS Job Number: FA68803
Sampling Date: 10/07/19
Report to:
Thompson Geological
�2411 Lawyers Rd W
Indian Trail, NC 28079
[e-mail]
JATTN: Phil Thompson
Total number of pages in report: 1 9
RQ
Test results contained within this data package meet the requirements Caitlin Brice, M..S
of the National Environmental Laboratory Accreditation Program General Manager
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(S73), NI(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. - 4405 Vineland Road - Suite C-15 - Orlando, FL 32811 - tot; 407-425-6700 - fax: [phone]
SGS is the sale authority fcrr authorizing edits or modifications to ihis documen€. Please shirt's your ideas about
Unauthorized modification of this report is strictly prohibited_ Iruw we can sen'e you bolter at: ISCIS
12evicw standard teens ai: LHS.US.CuSta€uirCare ii, sgs.txt€n
I of 49
FAW03

Sections:
Table of Contents
-1-
Section1: Sample Summary .......................................................................•----•-•....................
3
Section2 Case Narrative/Conformance Summary..............................................................
4
...............
Section4: Sample Results........................................................................................................
8
4.1: FA68803-1: CONFIRMATION SAMPLE SUGAR CREEK ......................................
9
4.2: FA68803-2: CS-1 7'......................................................................................................
10
Section° —I. ;........................................................................................................
17
51: Chain. of Custody..........................••-•.........................................--•.................................
18
SectionC�: QC Data Summaries .....................................................................
0
6.1: Method Blank Summary................................................................................................
21
6.2: Blank Spike Summary..............................................................................................•----
24
6.3: Blank Spike/Blank Spike Duplicate Summary..............................................................
26
6.4-. Matrix Spike/Matrix Spike Duplicate Summary...........................................................
27
Section 7: MS Semi-volatiles - QC Data Summaries............................................................
30
7.1: Method Blank Summary ................................................................................................
31
7.2: Blank Spike Summary ...................................................................................................
33
7.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................
35
Section 8: GC Volatiles - QC Data Summaries.....................................................................
37
8.1: Method Blank Summary ................................................................................................
38
8.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
39
8.3: Matrix Spike Summary .................................................•
8.4: Duplicate Summary .......................................................................................................
41
Section 9: GC/LC Semi-volatiles - QC Data Summaries.....................................................
42
9.1: Method Blank Summary ................................................................................................
43
9.2: Blank Spike Summary .....................•--............................-----..........................................
45
9.3: Blank Spike/Blank Spike Duplicate Summary..............................................................
46
9.4: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
48
9.5: Duplicate Summary.......................................................................................................
49
-uS1 2 of 49
FAMOZ

SGS North America Inc.
Sample Summary
Thompson Geological
Hinson Property; N Sugar Creek, Charlotte, NC Job No: FA68803
;ample
Collected
Matrix
Client
dumber
Date Time By
Received Code Type
Sample 1D
This report contains results reported as ND = Not detected. The following applies:
Organics ND — Not detected above the MDL
FA68803-1 10/07/19 10.00 PT 10/09/19 SO Soil CONFIRMATION SAMPLE SUGAR
CREEK
FA68803-2 10/07/19 10:30 PT 10/09/19 SO Soil CS-1 7'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
E rr

SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: Thompson Geological Job No: FA69903
Site: Hinson Property; N Sugar Creek, Charlotte, NC
Report Date 10/16/2019 7:35:53
2 Samples were collected on 10107/2019 and were received at SGS North America Inc - Orlando on 10/09/2019 properly preserved, at 1.9
Deg. C and intact. These Samples received an SGS Orlando job number of FA68803. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section. Except as noted below, all method specified calibrations
and quality control performance criteria were met for this job. For more information, please refer to QC summary pages_
MS Volatiles By Method SW846 82601)
Matrix: SO Batch ID: V213517
All samples were analyzed within the recommended method holding time.
Sample(s) FA68836-4MS, FA68836-4MSD were used as the QC samples .indicated.
All method blanks for this batch meet method specific criteria.
Blank Spike Recovery(s) for Chloroethane, Ethyl Alcohol are outside control limits.
Matrix SpikeRecovery(s) for 1,1,1-Trichloroethane, 1,1,2,2-Tetrachloroethane, 1,I,2-Trichloroethane, 1,I-Dichloroethylene,
112,3-Trichlorobenzene, 1,2,3-Trichloropropane, 1,2,4-Trichlorobenzene, 1,2-Dibromoethane, 1,2-Dieblorobenzene,
1,3-➢ichlorobenzene, 1,3-Dichloropropane, 1,4-Dichlorobenzene, 2,2-Dichloropropane, 2-Butanone (MEK), 2-Hexamone,
4-Methyl-2-pentanone (MIBK), Acetone, Bromobenzene, Bromoform, Carbon Tetrachloride, Chloroeflme,
Dibromochloromethane, Ethyl Alcohol, Methyl Bromide, Naphthalene, p-Isopropyltoluene, Styrene, trans-1,3-Dichlompropene,
Trichlorofluoromethane, Vinyl Acetate, Vinyl Chloride are outside control limits. Probable cause is due to matrix intcrference.
Matrix Spike Duplicate Recov"s) for 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,2-Dichlorobenzene,
1,3-Dicblorobenzene, 1,4-Dichlorobenzene, Acetone, Bromobenzene, Bromoform, Ethyl Alcohol, Naphthalene, p-Chlorotoluene,
p-Isopropyltoluene, Styrene, Vinyl Acetate are outside control limits. Probable cause is due to matrix interference.
RPD(s) for MSD for 1,2,3-Trichloropropane, 2,2-Dichlompropane, 2-Butanone (MEK), 2-Hexanoue, 4-Methyl-2-pentanone
(MIBK), Acetone, Chloroethane, Dichlorodifluoromethane, Ethyl Alcohol, Methyl Chloride, Naphthalene,
Trichlorofluoromethanc, Vinyl Chloride are outside control limits for sample FA68836-4MSD. Probable cause is due to sample
non -homogeneity.
FA68803-2: Results reported from Bisulfate preserved sample_
FA68803-2 for Chloroethane: Associated 1CV and BS outside control limits high, however sample ND. Associated CCV outside
of control limits high, sample was ND.
FA68803-2 for Bromodichloromethane: Initial calibration response factors not 8260D compliant.
FA68803-2 for Methylene Chloride: Associated CCV outside of control limits high, sample was ND.
FA68803-2 for Ethyl Alcohol: Associated BS recovery outside control lints, high. Associated CCV outside of control limits
high.
Matrix: SO Batch ID: VF3220
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria,
VF3220-ES: No sample available for MS/MSD.
VF3220-BSD: No sample available for MS/MSD.
MS Semi-volatiles By Method SW846 8270E
Matrix: SO
Batch ID. OP77248
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) FA68836-1MS, FA68836-IMSD were used as the QC samples indicated.
GC Volatiles By Method MADEP VPH REV 1.1
Matrix: SO Batch ID: GUU1519
All samples were analyzed within the recommended method holding time.
Sample(s) FA68803-2DUP, FA68803-2MS were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
I A-
SGS
4 of 49
FA6a80$

Matrix Spike Recovery(s) for C9- C10 Aromatics, C9- C10 Aromatics (Unadj.), C9- C12 Aliphatics (Unadj.) are outside control
limits. Probable cause is due to matrix interference.
RPD(s) for Duplicate for C9- C12 Aliphatics are outside control limits for sample FA68803-2DUP_ Probable cause is due to
sample non -homogeneity.
GC/LC Semi-volatiles By Method MADEP EPH REV 1.1
Matrix: SO Batch ID: OP77224
All samples were extracted within the recommended method holding time_
All samples were analyzed within the recommended method holding time.
Sarple(s) FA68805-IDUP were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
FA68803-2: Dilution required prior to fractionation due to matrix.
GC/LC Semi-volatiles By Method SW846 8015C
Matrix: SO Batch ID: OP77283
All samples were extracted within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
Sample(s) FA68803-1MS, FA68803-1MSD were used as the QC samples indicated.
All method blanks for this batch meet method specific criteria.
Matrix Spike Recovery(s) for TPH (C10-C28) are outside control limits. Outside control limits due to high level in sample
relative to spike amount.
Matrix Spike Duplicate Recovery(s) for TPH (C 10-C28) are outside control limits. Probable cause is due to matrix interference.
General Chemistry By Method SM19 2540G
Matrix: SO Batch 11): GN83297
Sample(s) FA68812-t7DUP were used as the QC samples for Solids, Percent.
Matrix: SO Batch ID: GN83306
Sample(s) FA68803-IDUP were used as the QC samples for Solids, Percent.
SGS Orlando certifies that this report meets the project requirements for analytical data produced for the samples as received at SGS
Orlando and as stated on the COC. SGS Orlando certifies that the data meets the Data Quality Objectives for precision, accuracy and
completeness as specified in the SGS Orlando Quality Manual except as noted above_ This report is to be used in its entirety.
SGS Orlando is not responsible for any assumptions of data quality if partial data packages are used.
Narrative prepared by:
Ariel Hartney, Client Services (Signature on File)
bs
5 of 49
b
FAU803

Summary of Hits Page 1 of 2
Job Number; FA68803
Account: Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Collected: 10/07/ 19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68803-1 CONFIRMATION SAMPLE SUGAR CREEK
TPH (C10-C28) 532 56 28 mg/kg SW846 8015C
FA68803-2 CS-17'
Acetone a
134 J
250
130
ug/kg
SW846 8260D
Benzene b
9.9
6.4
1.6
ug/kg
SW846 8260D
2-Butanone (MEK) b
17.9 J
32
9.3
ug/kg
SW846 8260D
n-Butylbenzene b
33.5
6.4
1.3
ug/kg
SW846 8260D
sec-Butylbenzene b
13.6
6.4
1.3
ug/kg
SW846 8260D
1,2-Dibromoethane b
1.4 J
6.4
1.3
ug/kg
SW846 8260D
1,2-Dichloroethane b
1.9 J
6.4
1.3
ug/kg
SW846 8260D
Ethyl Alcohol °
178 J
510
95
ug/kg
SW846 8260D
Ethylbenzene b
63.5
6.4
1.3
ug/kg
SW846 9260D
Isopropylbenzcne b
13.3
6.4
1.3
ug/kg
SW846 8260D
p-Isopropyltoluene b
6.5
6.4
1.3
ug/kg
SW846 8260D
Naphthalene b
148
6.4
2.5
ug/kg
SW846 8260D
n-Propylbenzene b
58.8
6.4
1.3
ug/kg
SW846 8260D
Toluene b
108
25
13
ug/kg
SW846 8260D
1,2,4-Trimethylbenzene
1230
430
86
ug/kg
SW846 8260D
1,3,5-Trimethylbenzene b
151
6.4
1.3
ug/kg
SW846 8260D
m,p-Xylene b
257
13
1.4
ug/kg
SW846 8260D
o-Xylene b
146
6.4
1.3
ug/kg
SW846 8260D
Xylene (total) b
403
19
2.7
ug/kg
SW846 9260D
bis(2-Ethylhexyl)phthalate
62.9 J
380
38
ug/kg
SW846 8270E
1-Methylnaphthalene
223
190
19
ug/kg
SW846 8270E
2-Methylnaphthalene
427
190
19
ug/kg
SW846 8270E
Naphthalene
270
190
19
ug/kg
SW846 8270E
Ethylbenzene
210
180
88
ug/kg
MADEP VPH REV 1.1
Naphthalene
946
440
260
ug/kg
MADEP VPH REV 1.1
Toluene
310
180
88
ug/kg
MADEP VPH REV 1.1
m,p-Xylene
702
350
180
ug/kg
MADEP VPH REV 1.1
o-Xylene
496
180
88
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)
4190 J
8800
3100
ug/kg
MADEP VPH REV 1.1
C9- C12 Aliphatics (Unadj.)
7920 J
8800
3100
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)
10000
8800
3100
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics
3880 J
8800
3100
ug/kg
MADEP VPH REV 1.1
C9- C12 Aliphatics
6520 J
8800
3100
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics
10000
8800
3100
ug/kg
MADEP VPH REV 1.1
Acenaphthylene d
1190
1100
560
ug/kg
MADEP EPH REV 1.1
Naphthalene d
822 J
1100
560
ug/kg
MADEP EPH REV 1.1
CII-C22 Aromatics (Unadj.) d
47300 J
56000
22000
ug/kg
MADEP EPH REV 1.1
C11-C22 Aromatics d
44800 J
56000
22000
ug/kg
MADEP EPH REV 1.1
C19-C36 AIiphatics d
23000 J
56000
14000
ug/kg
MADEP EPH REV 1.1
G of !&9
NJ
FAM03

Summary of Hits Page 2 of 2
Job Number: FA68803
Account: Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Collected: 10/07/19
Lab Sample lD Client Sample ID Result/
Analyte Qual RL MDL Units Method
(a) Results reported from Bisulfate preserved sample_ Associated CCV outside of control limits high.
(b) Results reported from Bisulfate preserved sample.
(c) Results reported from Bisulfate preserved sample. Associated BS recovery outside control limits, high.
Associated CCV outside of control limits high.
(d) Dilution required prior to fractionation due to matrix.
7ot49

SGS
Orlando, FL
Sample Results
Report of Analysis
Section 4
a
SG$ of 49
FA68803

SGS North America Inc.
Report of Analysis
Client Sample ID: CONFIRMATION SAMPLE SUGAR CREEK
Lab Sample ID: FA68803-1 Date Sampled: 10/07/19
Matrix: SO - Soil Date Received: 10/09/19
Method: SW846 8015C SW846 3546 Percent Solids: 89.1
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of I
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WW22509.D 10 10/16/19 11:30 SJL 10/15/19 08:49 OP77283 GWW926
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No. Compound
TPH (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result RL MDL Units Q
532 56 28 mg/kg
Run# 1 Run# 2 Limits
83% 56-1.22%
ND — Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E mm Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

SGS North America Inc.
Report of Analysis
Client Sample ID: CS-1 7'
Lab Sample ID: FA68803-2 Date Sampled: I0/07/ 19
Matrix: SO - Soil Date Received: 10/09/19
Method: SW846 8260D Percent Solids: 88.1
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page I of 3
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Faun #1 a 21313564.D
1
10/10/19 14:51
SP
n/a
n/a
V2B517
Run #2 F0092037.1)
1
10/10/19 14:53
SP
n/a
n/a
VF3220
Initial Weight Final Volume Methanol Aliquot
Run #1 4.46 g 5.0 ml
Run #2 3.57 g 5.0 ml 100 ul
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
134
250
130
ug/kg
71-43-2
Benzene
9.9
6.4
1.6
ug/kg
108-86-1
Bromobenzene
ND
6.4
1.3
ug/kg
74-97-5
Bromochloromethane
ND
6.4
1.9
ug/kg
75-27-4
Bromodichloromethane c
ND
6.4
1.3
ug/kg
75-25-2
Bromoform
ND
6.4
1.3
ug/kg
78-93-3
2-Butanone (MBK)
17.9
32
9.3
ug/kg
104-51-8
n-Butylbenzene
33.5
6.4
1.3
ug/kg
135-98-8
sec-Butylbenzene
13.6
6.4
1.3
ug/kg
98-06-6
tert-Butylbenzene
ND
6.4
1.3
ug/kg
56-23-5
Carbon Tetrachloride
ND
6.4
1.3
ug/kg
108-90-7
Cblorobenzene
ND
6.4
1.3
ug/kg
75-00-3
Chloroethane d
ND
6.4
2.5
ug/kg
67-66-3
Chloroform
ND
6.4
1.7
ug/kg
95-49-8
o-Chlorotoluene
ND
6.4
1.3
ug/kg
106-43-4
p-Chlorotoluene
ND
6.4
1.3
ug/kg
124-48-1
Dibromochloromethane
ND
6.4
1.3
ug/kg
106-93-4
1,2-Dibrumoethanc
1.4
6.4
1.3
ug/kg
75-71-8
Dichlorodifluoromethane
ND
6.4
2.5
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
6.4
1.3
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
6A
1.3
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
6.4
1.5
ug/kg
75-34-3
1,1-Dichloroethane
ND
6A
2.3
ug/kg
107-06-2
1,2-Dichloroethane
19
6.4
1.3
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
6.4
1.3
ug/kg
156-59-2
cis- 1,2 -Dichloroethylene
ND
6.4
1.8
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
6.4
1.3
ug/kg
78-87-5
1,2-Diehloropropane
ND
6.4
1.3
ug/kg
142-28-9
1,3-Dichloropropane
ND
6.4
1.3
ug/kg
594-20-7
2,2-Dichloropropane
ND
6.4
1.3
ug/kg
563-58-6
1,1-Dichloropropene
ND
6.4
1.3
ug/kg
10061-01-5
cis-1,3-Dichloropropene
ND
6.4
1.3
ug/kg
1]
J
J
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyze found in associated method blank
E _ Indicates value exceeds calibration range N - Indicates presumptive evidence of a compound
10of49
FA68803

SGS North America Inc.
Report of Analysis
Client Sample ID: CS-1 7'
Lab Sample ID: FA68803-2 Date Sampled: 10/07/19
Matrix: SO - Soil Date Received: 10/09/19
Method: SW846 8260D Percent Solids: 88.1
Project: Hinson Property; N Sugar Creek, Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans-1,3-Dichloropropene
ND
6.4
1.3
ug/kg
108-20-3
Di -Isopropyl Ether
ND
6.4
3.0
ug/kg
64-17-5
Ethyl Alcohol e
178
510
95
ug/kg J
10041-4
Ethylbenzene
63.5
6.4
I.3
ug/kg
591-78-6
2-Hexanone
ND
32
9.5
ug/kg
98-82-8
Isopropylbenzene
13.3
6.4
1.3
ug/kg
99-87-6
p-lsopropyltoluene
6.5
6.4
L3
ug/kg
74-93-9
Methyl Bromide
ND
6.4
2.5
ug/kg
74-87-3
Methyl Chloride
ND
6.4
2.5
ug/kg
75-09-2
Methylene Chloride
ND
25
14
ug/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
32
9.5
ug/kg
1634.04-4
Methyl Tert Butyl Ether
ND
6.4
1.3
ug/kg
91-20-3
Naphthalene
148
6.4
2.5
ug/kg
103-65-1
n-Propylbenzene
58.8
6.4
1.3
ug/kg
100-42-5
Styrene
ND
6.4
1.3
ug/kg
630-20-6
1,1,1,2-Tetrachloroethane
ND
6.4
1.3
ug/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
6.4
1.3
ug/kg
127-18-4
Tetrachloroethylene
ND
6.4
1.6
ug/kg
108-88-3
Toluene
108
25
13
ug/kg
87-61-6
1,2,3-Trichlorobenzene
ND
6.4
1.9
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
6.4
1.3
ug/kg
71-55-6
1,1,1-Triehloroethane
ND
6.4
1.3
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
6.4
1.3
ug/kg
79-01-6
Trichloroethylene
ND
6.4
1.3
ug/kg
75-69-4
Trichlorofluoromethane
ND
6.4
2.5
ug/kg
96-18-4
1,2,3-Trichloropropane
ND
6.4
1.6
ug/kg
95-63-6
1,2,4-Trimethylbenzene
12309
430
86
ug/kg
108-67-8
1,3,5-Trimethylbenzene
151
6.4
1.3
ug/kg
108-054
Vinyl Acetate
ND
32
21
ug/kg
75-014
Vinyl Chloride
ND
6.4
1.3
ug/kg
m,p-Xylene
257
13
1.4
ug/kg
95-47-6
o-Xylene
146
6.4
1.3
ug/kg
1330-20-7
Xylene (total)
403
19
2.7
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
116%
99%
72-135%
2037-26-5
Toluene-138
103%
101%
75-126%
460-00-4
4-Bromofluorobenzene
99%
96%
7I-133%
Page 2 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS99 of 49
FA68BO3

SGS North America Inc.
Report of Analysis
Client Sample ID: CS-1 7'
Lab Sample ID: FA68803-2 Date Sampled: 10/07/19
Matrix: SO - Soil Date Received: 10/09/19
Method: SW846 8260D Percent Solids: 88.1
Project: Hinson Property, N Sugar Creek, Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
Page 3 of 3
(a) Results reported from Bisulfate preserved sample.
(b) Associated CCV outside of control limits high.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated 1CV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND-
(e) Associated BS recovery outside control limits, high_ Associated CCV outside of control limits high.
(1) Associated CCV outside of control limits high, sample was ND.
(g) Result is from Run# 2
ND — Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N — Indicates presumptive evidence of a compound
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SGS
Orlando, FL
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 5
SGS17 of 49
FA68303

SGS North America Inc - Orlando fAWbOl
_qn-0 Chain of Custody SGS-ORLANDOJOB#: PAGE oF.
V TM4m�5-6%0 FAx 407-42M707
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FA68803: Chain of Custody
Page 1 of 2
t3T
18 of 49
—S—GST
FA1i8803

SGS Sample Receipt Summary
Job Number_ FA68803 Client THOMPSON PROPERTY Project: HINSON PROPERTY
Date I Time Received: 10I9/2019 9:00:00 AM Delivery Method.- FX Airbill 96'.
Therm 10. IR 1;
Therm CF: 1;
# of Coolers: 1
Cooler Temps (Raw Measured) °Cr Cooler
1: (0.9);
Cooler Temps (Corrected)'C: Cooler
1: (1.9);
Cooler information
_Y _or
d_
sanuLofarM.arSID
X .or
N
NIA
1. Custody Seals Present
®
❑
1_ Sample labels present on betties
®
❑
2. Custody Seals Intact
®
❑
2. Samples preserved properly
R
❑
3. Temp criteria achieved
©
❑
3. Sufficient volumelcontainers recvd for analysis:
id
❑
4. Cooler temp verification
IR Gin
4. Condition of sample
Intact
5. Cooler media
Ice 38
5. Sample recvd within HT
6. DateslrimesllDs on COC match Sample Label
Trio Blank Information
Y or
N NIA
7. VOCs have headspace
❑
❑
1. Trip Blank present! cooler
=
❑
8. Bottles received for unspecified tests
❑
0
2. Trip Blank listed on COC
_
d ❑
9. Compositing instructions dear
❑
or
S NIA
10. Voa Soil Kits/Jars received past 48hrs?
�
0
❑y
3. Type Of TB Received
]
_i
11. % Solids Jar received?
❑
❑
12. Residual Chlorine Present?
El
0
he
Misc. ln uil on
Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: 1 Number of Lab Filtered Metals:
Test Strip Lot its: pH 0-3 230315 _ pH 10-12 219813A_ _ Other: (Specify)
Residual Chlorine Test Strip Lot #:
Comments — -
sewer
Rev. base u5124177 Technician: PETERH Cate: 1019/20199.00:00AM Reviewer: Date:
FA68803: Chain of Custodv
Page 2 of 2
SG819
of 49
FAG3W3

SGS
Orlando, FL
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 6
1�
-SG - zo of 49
FA66803

Method Blank Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of 2
Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch
V213517-MB 2B13560.D 1 10/10/19 SP n/a n/a V213517
The QC reported here applies to the following samples:
FA68803-2
CAS No. Compound
Method: SW846 8260D
Result RL MDL Units Q
67-64-1
Acetone
ND
200
100
ug/kg
71-43-2
Benzene
ND
5.0
1.2
ug/kg
108-86-1
Bromobenzene
ND
5.0
1.0
ug/kg
74-97-5
Bromochloromethane
ND
5.0
1.5
ug/kg
75-27-4
Bromodichioromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.0
ug/kg
78-93-3
2-Butanone (MEK)
ND
25
7.3
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
135-98-8
sec-Butylbenzene
ND
5.0
1.0
ug/kg
98-06-6
tert-Butylbenzene
ND
5.0
1.0
ug/kg
56-23-5
Carbon Tetrachloride
ND
5.0
1.0
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.0
ug/kg
67-66-3
Chloroform
ND
5.0
I.3
ug/kg
95-49-8
o-Chlorotoluene
ND
5.0
1.0
ug/kg
106-43-4
p-Chlorotoluene
ND
5.0
1.0
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodilluoromethane
ND
5.0
2.0
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
5.0
1.0
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
5.0
1.2
ug/kg
75-34-3
1,1-Dichloroethane
ND
5.0
1.8
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1,1-Dichloroethylene
ND
5.0
1.0
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
5.0
1.4
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
5.0
1.0
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.0
ug/kg
142-28-9
1,3-Dichloropropane
ND
5.0
1.0
ug/kg
594-20-7
2,2-Dichloropropane
ND
5.0
1.0
ug/kg
563-58-6
1,1-Dichloropropene
ND
5.0
1.0
ug/kg
10061-01-5 cis- 1, 3-Dichloropropene
ND
5.0
1.0
ug/kg
10061-02-6 trans-1,3-Dichloropropene
ND
5.0
1.0
ug/kg
108-20-3
Di -Isopropyl Ether
ND
5.0
2.3
ug/kg
64-17-5
Ethyl Alcohol
ND
400
75
ug/kg
100-414
Ethylbenzene
ND
5.0
1.0
ug/kg
01
SG21 of 49
FAZU803

Method Blank Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 2 of 2
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-MB 2B13560.1) 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
CAS No. Compound Result RL MDL Units Q
591-78-6
2-Hexanone
7.6
25
7.5
ug/kg 7
98-82-8
Isopropylbenzene
ND
5.0
1.0
ug/kg
99-87-6
p-Isopropyltoluene
ND
5.0
1.0
ug/kg
74-83-9
Methyl Bromide
ND
5.0
2.0
ug/kg
74-87-3
Methyl Chloride
ND
5.0
2.0
ug/kg
75-09-2
Methylene Chloride
ND
20
11
ug/kg
108-10-1
4-Methyl-2-pentanone (MIRK) ND
25
7.5
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.0
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propytbenzene
ND
5.0
t.0
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
1.0
ug/kg
127-18-4
Tetrachloroetbylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
20
10
ug/kg
87-61-6
1,2,3-Trichlorobenzene
ND
5.0
1.4
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
t.0
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
5.0
L.0
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.0
ug/kg
79-01-6
Trichioroethylene
ND
5.0
1.0
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
2.0
ug/kg
96-18-4
1,2,3-Trichloropropane
ND
5.0
1.3
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-05-4
Vinyl Acetate
ND
25
16
ug/kg
75-014
Vinyl Chloride
ND
5.0
1.0
ug/kg
m,p-Xylene
ND
I0
1.1
ug/kg
95-47-6
o-Xylene
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.1
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
97%
75-1.24%
17060-07-0
1,2-Dichloroethane-D4
113%
72-135%
2037-26-5
Toluene-D8
101%
75-126%
460-00-4
4-Bromofluorobenzene
92%
71-133%
Gzz of 49
FA68803

Method Blank Summary
Job Number: FA68803
Account., TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of 1
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3220-MB F0092034.D 1 10/10/19 SP n/a n/a VF3220
The QC reported here applies to the following samples:
FA68803-2
CAS No. Compound
95-63-6 1,2,4-Trimethylben7ene
CAS No, Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1,2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-$romolluorobenzene
Method: SW846 8260D
Result
RL MDL Units Q
ND
5.0 1.0 ug/kg
Limits
100%
75-124%
97%
72-135%
101%
75-126%
99%
71-133%
C
-SW
23 of 49
FA66803

Blank Spike Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V2B517-BS
2B13561.1)
1
10/10/19
SP
n/a
n/a
V2B517
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
CAS No. Compound
Spike BSP BSP
uglkg ug/kg % Limits
67-64-1
Acetone
250
360
144
61-152
71-43-2
Benzene
50
52.9
106
76-126
108-86-1
Bromobenzenc
50
48.9
98
76-122
74-97-5
Bromochloromethane
50
50.5
101
77-120
75-27-4
Bromodichloromethane
50
54.4
109
74-130
75-25-2
Broinoform
50
53.2
106
76-127
78-93-3
2-Butanone (MEK)
250
315
126
75-137
104-51-8
n-Butylbenzene
50
54.7
109
71-128
135-98-8
sec-Butylbenzene
50
52.2
104
79-135
98-06-6
tert-Butylbenzer►e
50
50.7
101
77-133
56-23-5
Carbon Tetrachloride
50
58.2
116
78-133
108-90-7
Chlorobenzene
50
53.1
106
81-129
75-00-3
Chloroethane
50
69.9
140*
68-133
67-66-3
Chloroform
50
57.7
115
72-123
95-49-8
o-Chlorotoiuene
50
53.3
107
77-129
10643-4
p-Chlorotoluene
50
52.0
104
80-134
124-48-1
Dibromochloromethane
50
52.6
105
76-127
106-934
1,2-Dibrornoethane
50
50.8
102
77-126
75-71-8
Dichlorodifluoromethane
50
46.5
93
68-168
95-50-1
1,2-Dichlorobenzene
50
49.5
99
80-129
541-73-1
1,3-Dichlorobenzene
50
50.5
101
81-129
10646-7
1,4-Dichlorobenzene
50
51.0
102
76-130
75-34-3
1,1-Dichloroethane
50
59A
118
73-125
107-06-2
1,2-Dicbloroethane
50
57.1
114
74-128
75-354
1, 1 -Dichloroethylene
50
59.1
118
81-136
156-59-2
cis-1,2-Dichloroethylene
50
54.5
109
74-126
156-60-5
trans-1,2-Dichloroethylene
50
57.8
116
70-127
78-87-5
1,2-Dichloropropane
50
52.5
105
74-125
142-28-9
1,3-Dichloropropane
50
49.6
99
76-122
594-20-7
2,2-Dichloropropane
50
65.4
131
77-133
563-58-6
I,1-Dichloropropene
50
55.9
112
75-130
10061-01-5 cis- 1, 3-Dichloropropene
50
48.3
97
80-123
10061-02-6 trans- 1, 3-Dichloropropene
50
54.0
108
75-131
108-20-3
Di -isopropyl Ether
50
549
110
75-122
64-17-5
Ethyl Alcohol
1000
1620
162*
53-154
10041-4
Ethylbenzene
50
55.6
ill
77-123
* = Outside of Control Limits.
SGS24 of 49
FA68803

Blank Spike Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 2 of 2
le File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
17-BS 21313561.1) 1 10/10/19 SP n/a nla V213517
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
591-78-6
2-Hexanone
250
270
108
72-133
98-82-8
Isopropylbenzene
50
56.5
113
80-136
99-87-6
p-Isopropyltoluene
50
522
104
77-131
74-83-9
Methyl Bromide
50
57.8
116
65-139
74-87-3
Methyl Chloride
50
54.7
109
71-144
75-09-2
Methylene Chloride
50
63.0
126
74-137
108-10-1
4-Methyl-2-pentanone (MIBK) 250
280
112
76-132
1634-04-4
Methyl Tert Butyl Ether
50
47.1
94
77-120
91-20-3
Naphthalene
50
49.6
99
79-129
103-65-1
n-Propylbenzene
50
52.3
105
80-135
100-42-5
Styrene
50
51.4
103
78-125
630-20-6
1,1,1,2-Tetrachloroethane
50
55.2
110
78-126
79-34-5
1,1,2,2-Tetrachloroethane
50
54.5
109
71-126
127-18-4
Tetrachloroethylene
50
52.1
104
79-130
108-88-3
Toluene
50
51.5
103
76-124
87-61-6
1,2,3-Trichlorobenzene
50
47.2
94
77-128
120-82-1
1,2,4-Trichlorobenzene
50
47.4
95
78-130
71-55-6
1, 1, 1 -Triebloroethane
50
57.5
115
70-129
79-00-5
1,1,2-Triehloroethane
SO
51.2
102
74-124
79-01-6
Trichloroethylene
50
53.4
107
75-128
75-694
Trichloroftuoromethane
50
63.1
126
73-145
96-18-4
1,2,3-Trichloropropane
50
52.1
104
74-127
108-67-8
1,3,5-Trimethylbenzene
50
52.I
104
73-122
108-054
Vinyl Acetate
250
278
111
48-164
75-01-4
Vinyl Chloride
50
56.0
112
76-141
m,p-Xylene
100
ill
Ill
80-128
95-47-6
o-Xylene
50
54.2
108
80-132
1330-20-7
Xylene (total)
150
165
110
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
108%
72-135%
2037-26-5
Toluene-138
100%
75-126%
460-004
4-13romofluorobenzene
89%
71-133%
* = Outside of Control Limits.
SG 7
25 of 49
FAS8803

Blank Spike/Blank Spike Duplicate Summary Page I of I
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3220-BS a F0092032.D 1 10/10/19 SP n/a n/a VF3220
VF3220-BSD a F0092033.1) 1 10/10/19 SP n/a n/a VF3220
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
Spike BSP BSP BSD BSD Limits
CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD
95-63-6 1,2,4-Trimethylbenzene 50 51.6 103 52.7 105 2 74-123/30
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1, 2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
(a) No sample available for MS/MSD
* = Outside of Control Limits.
BSP
BSD
Limits
103%
100%
75-124%
102%
103%
72-135%
100%
103%
75-126%
101%
102%
71-I33%

Matrix Spike/Matrix Spike Duplicate Summary Page I of 3
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample
File Ill DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA688364MS a
2B13583.1) 1
10/10/19
SP
n/a
n/a
V2B517
FA68836-4MSD a
2BI3584.D 1
10/10/19
SP
n/a
n/a
V213517
FA68836-4 b
2BI3569_D 1
10/10/19
SP
n/a
n/a
V213517
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
FA688364
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
67-64-1
Acetone
522
303
326
-65*
300
461
-20*
34*
61-152/27
7143-2
Benzene
ND
60.6
63.7
105
59.9
61.4
102
4
76-126/26
108-86-1
Bromobenzene
ND
60.6
42.7
70*
59.9
44.7
75*
5
76-122/32
74-97-5
Bromochloromethane
ND
60.6
47.1
78
59.9
54.5
91
15
77-120/24
75-274
Bromodiehloromethane
ND
60.6
56.8
94
59.9
60.8
101
7
74-130/25
75-25-2
Bromoform
ND
60.6
35.8
59*
59.9
45.1
75*
23
76-127/26
78-93-3
2-Butanone (MEK)
ND
303
203
67*
300
324
108
46*
75-137/25
104-51-8
n-Butylbenzene
ND
60.6
56.0
92
59.9
52.8
88
6
71-128/35
135-98-8
sec-Butylbenzene
ND
60.6
60.3
99
59.9
57.8
96
4
79-135/34
98-06-6
tert-Butylbenzene
ND
60.6
57.0
94
59.9
59.4
99
4
77-133/34
56-23-5
Carbon Tetrachloride
ND
60.6
86.5
143*
59.9
68.0
114
24
78-133/29
108-90-7
Chlorobenzene
ND
60.6
55.5
92
59.9
54.3
91
2
81-129/29
75-00-3
Chloroethane
ND
60.6
125
206*
59.9
68.2
114
59*
68-133/29
67-66-3
Chloroform
ND
60.6
65.7
108
59.9
67.8
113
3
72-123/26
95-49-8
o-Chlorotoluene
ND
60.6
54.4
90
59.9
53.4
89
2
77-129/33
106-43-4
p-Chlorotoluene
ND
60.6
49.6
82
59.9
47.6
79*
4
80-I34/33
124-48-1
Dibronaochloromethane
ND
60.6
43.2
71*
59.9
54.0
90
22
76-127/27
106-93-4
1,2-Dibromoethane
ND
60.6
38.2
63*
59.9
48.8
81
24
77-126/26
75-71-8
Dichlorodifluoromethane
ND
60.6
73.2
121
59.9
52.7
88
33*
68-168/29
95-50-1
1,2-Dieblorobenzene
ND
60.6
34.1
56*
59.9
37.4
62*
9
80-129/32
541-73-1
1,3-Dichlorobenzene
ND
60.6
39.3
65*
59.9
40.6
68*
3
81-129/33
I06-46-7
1,4-Dichlorobenzene
ND
60.6
38.9
64*
59.9
40.3
67*
4
76-130/32
75-34-3
I,I-Dichloroethane
ND
60.6
71.5
118
59.9
70.4
118
2
73-125/27
107-06-2
1,2-Dichioroethane
ND
60.6
51.1
84
59.9
62.7
105
20
74-128/23
75-35-4
1,1-Dichloroethylene
ND
60.6
90.0
148*
59.9
71.4
119
23
81-136/28
156-59-2
cis-1,2-Dichloroethylene
ND
60.6
60.7
100
59.9
62.7
105
3
74-126/26
156-60-5
trans-1,2-Dichtoroethylene
ND
60.6
74.3
123
59.9
67.6
113
9
70-127/27
78-87-5
1,2-Dichloropropane
ND
60.6
60.2
99
59.9
59.3
99
2
74-125/25
142-29-9
1,3-Dichloropropane
ND
60.6
41.5
68*
59.9
51.9
87
22
76-122/26
594-20-7
2,2-Dichloropropane
ND
60.6
99.5
164*
599
72.0
120
32*
77-133/28
563-58-6
I,I-Dichloropropene
ND
60.6
67.4
111
59.9
669
112
1
75-130/28
10061-01-5 cis-1,3-Dichloropropene
ND
60.6
48.4
80
59.9
50.9
85
5
80-123/26
1006I-02-6 trans- 1, 3-Dichloropropene
ND
60.6
44.4
73*
59.9
55.4
92
22
75-131/28
108-20-3
Di -Isopropyl Ether
ND
60.6
74.2
122
59.9
67.2
112
10
75-122/25
64-17-5
Ethyl Alcohol
ND
1210
12700
1047*
1200
6490
542*
65*
53-154/42
100-41-4
Ethylbenzene
ND
60.6
66.3
109
59.9
61.9
103
7
77-123/31
* = Outside of Control Limits.
'27 of a9
11631 ,Z

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA68803
Page 2 of 3
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By
FA68836-4MS a 21313583.13 1 10/10/19 SP
FA68836-4MSD a 2B13584.D 1 10/10/19 SP
FA688364 b 2313569.D 1 10/10/19 SP
Prep Date
n/a
n/a
n/a
Prep Batch
n/a
n/a
n/a
Analytical Batch
V2B517
V213517
V213517
The QC reported here applies to the following samples: Method: SW846 8260D
FA68803-2
FA68836-4
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
591-78-6
2-Hexanone
ND
303
134
44*
300
223
74
50*
72-133/26
98-82-8
Isopropylbenzene
ND
60.6
67.3
111
59.9
63.6
106
6
80-136/32
99-87-6
p-Isopropyltoluene
16.1
60.6
57.8
69*
59.9
54.6
64*
6
77-131/34
74-83-9
Methyl Bromide
ND
60.6
86.6
143*
59.9
63.9
107
30
65-139/31
74-87-3
Methyl Chloride
ND
60.6
79.8
132
59.9
60.0
100
28*
71-144/27
75-09-2
Methylene Chloride
ND
60.6
81.2
134
59.9
78.5
131
3
74-137/28
108-10-1
4-Methyl-2-pentanone (MIBK) ND
303
176
58*
300
303
101
53*
76-132/26
1634-04-4
Methyl Tert Butyl Ether
ND
60.6
52.1
86
59.9
54.3
91
4
77-120/24
91-20-3
Naphthalene
ND
60.6
14.0
23*
599
20.5
34*
38*
79-129/33
103-65-1
n-Propyibenzene
ND
60.6
60.3
99
59.9
56.7
95
6
80-135/33
100-42-5
Styrene
ND
60.6
43.9
72*
59.9
40.5
68*
8
78-125/30
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
60.6
56.8
94
59.9
62.2
104
9
78-126/27
79-34-5
1,1,2,2-Tetrachloroethane
ND
60.6
36.4
60*
59.9
48.9
81
29
71-126/30
127-18-4
Tetrachloroethylene
ND
60.6
61.0
lot
59.9
61.9
103
1
79-130/31
108-88-3
Toluene
ND
60.6
57.7
95
59.9
60.7
101
5
76-124/30
87-61-6
1,2,3-Trichlorobenzene
ND
60.6
16.4
27*
59.9
22.0
37*
29
77-128/35
120-82-1
1,2,4-Trichlorobenzene
ND
60.6
20.1
33*
59.9
25.3
42*
23
78-130/34
71-55-6
1, 1, 1 -Trichloroethane
ND
60.6
86.1
142*
59.9
67.2
112
25
70-129/27
79-00-5
1,1,2-Trichloroethane
ND
60.6
42.3
70*
59.9
53.9
90
24
74-124/28
79-01-6
Trichloroethylene
ND
60.6
63.8
105
59.9
62.6
104
2
75-128/27
75-694
Trichlorofluoromethane
ND
60.6
107
176*
59.9
74.9
125
35*
73-145/31
96-18-4
1,2,3-Tricbtoropropane
ND
60.6
33.8
56*
599
46.3
77
31*
74-127/27
108-67-8
1,3,5-Trimethylbenzene
ND
60.6
55.9
92
59.9
54.8
91
2
73-122/33
108-05-4
Vinyl Acetate
ND
303
85.1
28*
300
117
39*
32
48-164/37
75-01-4
Vinyl Chloride
ND
60.6
92.8
153*
59.9
64.1
107
37*
76-141/27
m,p-Xyiene
ND
t21
130
107
120
122
102
6
80-128/30
95-47-6
o-Xylene
ND
60.6
60.2
99
59.9
58.7
98
3
80-132/30
1330-20-7
Xylene (total)
ND
182
191
105
180
180
100
6
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA68836-4
Limits
1868-53-7
Dibromofluoromethane
95%
103%
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
94%
111%
114%
72-135%
2037-26-5
Toluene-138
96%
105%
lot%
75-126%
460-004
4-Bromofluorobenzene
87%
89%
94%
71-133%
* = Outside of Control Limits.
5b
YX
K"

Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number: FA68803
Account: TGNCIT Thompson. Geological
Project: Hinson Property; N Sugar Creels, Charlotte, NC
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA68836-4MS a
2B13583.1) 1
10/10/19
SP
n/a
n/a
V2B517
FA688364MSD a
2813584.D 1
10/10/19
SP
n/a
nla
V2B517
FA68836_4 e
2B13569_D 1
10/10/19
SP
n/a
n/a
V213517
The QC reported here applies to the following samples:
FA68803-2
Method: SW846 8260D
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Internal standard response outside control limits. Confirmed
by MS/MSD.
* — Outside of Control Limits.
SG$-
29 of 49
FAGES03

SGS
Orlando, FL
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Bunk Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 7
33 o 49

Method Blank Summary
Job Number; FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page I of 2
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-MB 91006761.D 1 10/15/19 MV 10/11/19 OP77248 S91250
The QC reported here applies to the following samples:
FA68803-2
CAS No. Compound
Method: SW846 8270E
Result RL MDL, Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
170
19
ug/kg
95-57-8
2-Chlorophenol
ND
170
20
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
19
ug/kg
105-67-9
2,4-Dituethylphenol
ND
170
44
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
20
ug/kg
3&4-Methylphenol
ND
170
27
ug/kg
88-75-5
2-NitrophenoI
ND
170
18
ug/kg
100-02-7
4-Nitrophenol
ND
830
170
ug/kg
87-86-5
Pentachlorophenol
ND
830
170
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
19
ug/kg
83-32-9
Acenaphthene
ND
170
18
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
19
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
20
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
18
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
22
ug/kg
100-51-6
Benzyl Alcohol
ND
170
17
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
10647-8
4-Chloroaniline
ND
170
42
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
17
ug/kg
I1144-4
bis(2-Chloroethyl)ether
ND
170
19
ug/kg
108-60-1
2,2'-Oxybis(I-chloropropane)
ND
170
21
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
17
ug/kg
7005-72-3
4-Chloropheuylphenylether
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
21
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
170
17
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
170
18
ug/kg
FA68803

Method Blank Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By
OP77248-MB 9I00676 L D 1 10/ 15/ 19 MV
The QC reported here applies to the following samples:
FA68803-2
CAS No. Compound
Page 2 of 2
Prep Date Prep Batch Analytical Batch
10/11/19 OP77248 S91250
Method: SW846 8270E
Result RL MDL Units Q
106-46-7
1,4-Dichlorobenzene
ND
170
22
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
40
ug/kg
84-66-2
Diethyl Phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl Phthalate
ND
170
33
ug/kg
117-84-0
Di-n-octyl Phthalate
ND
170
33
ug/kg
84-74-2
Di-n-butyl Phthalate
ND
330
67
ug/kg
122-66-7
1,2-Diphenylhydrazine
ND
170
17
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
17
ug/kg
86-73-7
Fluorene
ND
170
18
ug/kg
118-74-1
Hexachlorobenzene
ND
170
17
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
17
ug/kg
77-474
Hexachlorocyclopentadiene
ND
170
33
ug/kg
67-72-1
Hexachloroethane
ND
170
20
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
20
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
90-12-0
1-Methylnaphthalene
ND
170
17
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
17
ug/kg
91-20-3
Naphthalene
ND
170
I7
ug/kg
98-95-3
Nitrobenzene
ND
170
17
ug/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
170
17
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
18
ug/kg
85-01-8
Phenanthrene
ND
170
17
ug/kg
129-00-0
Pyrene
ND
170
19
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
170
20
ug/kg
CAS No. Surrogate Recoveries Limits
367-12-4
2-Fluorophenol
72%
40-102%
4I65-62-2
Phenol-d5
76%
41-100%
118-79-6
2,4,6-TribromophenoI
79%
42-108%
4165-60-0
Nitrobenzene-6
72%
40-105%
321-60-8
2-Fluorobiphenyl
77%
43-107%
1718-51-0
Terphenyl-d14
77%
45-119%
- 32 of
„L.53�*--

Blank Spike Summary
.lob Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page I of 2
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-BS 91006760.D I 10/15/19 MV 10/11/19 OP77248 S91250
The QC reported here applies to the following samples:
FA68803-2
Spike
BSP
BSP
CAS No.
Compound
ug/kg
uglkg
%
Limits
65-85-0
Benzoic Acid
3330
2580
77
36-118
59-50-7
4-Chtoro-3-methyl Phenol
1670
1400
84
52-108
95-57-8
2-Chtorophenot
1670
1340
80
48-104
120-83-2
2,4-Dichlorophenol
1670
1450
87
51-105
105-67-9
2,4-Dimethylphenol
1670
1300
78
43-96
51-29-5
2,4-Dinitrophenol
3330
2530
76
40-1I9
534-52-1
4,6-Dinitro-o-cresol
3330
3000
90
64-121
95-48-7
2-Methylphenol
1670
1190
71
46-107
3&4-Methylphenol
3330
2400
72
44-111
88-75-5
2-Nitrophenot
1670
1390
83
49-104
100-02-7
4-Nitrophenot
3330
2590
78
56-116
87-86-5
Pentachlorophenol
3330
2560
77
61-114
108-95-2
Phenol
1670
1310
79
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1550
93
56-109
83-32-9
Acenaphthene
1670
1330
80
56-109
208-96-8
Acenaphthytene
1670
1420
85
56-106
120-12-7
Authracene
1670
1310
79
61-110
56-55-3
Benzo(a)anthracene
1670
1470
88
66-111
50-32-8
Benzo(a)pyrene
1670
1340
80
59-104
205-99-2
Benzo(b)fluoranthene
1670
1440
86
67-113
191-24-2
Benzo(g,h,i)perylene
1670
1370
82
67-113
207-08-9
Benzo(k)fluoranthene
1670
1420
85
67-114
100-51-6
Benzyl Alcohol
1670
1170
70
53-108
101-55-3
4-Bromophenyl phenyl ether
1670
1520
91
62-110
85-68-7
Butyl benzyl phthalate
1670
1490
89
65-113
106-47-8
4-Chloroaniline
1670
1130
68
30-115
111-91-1
bis(2-Chloroethoxy)methane
1670
1430
86
48-105
111-44-4
bis(2-Chloroethyl)ether
1670
1220
73
46-103
108-60-1
2,2'-Oxybis(I-chloropropane)
1670
1160
70
40-110
91-58-7
2-Chloronaphthalene
1670
1360
82
53-106
7005-72-3
4-Chlorophenyl phenyl ether
1670
1450
87
58-106
2I8-01-9
Chrysene
1670
1460
88
65-112
53-70-3
Dibenzo(a,h)anthracene
1670
1380
83
68-I15
132-64-9
Dibenzofuran
1670
1400
84
57-108
95-50-1
1,2-Dichlorobenzene
1670
1190
71
44-102
541-73-1
1,3-Dichlorobenzene
1670
1160
70
42-100
* = Outside of Control Limits.
Method: SW946 8270E
33 of 6,,9
FA.CH03

Blank Spike Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 2 of 2
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-BS 9I006760.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:
FA68803-2
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
106-46-7
1,4-Dichlorobenzene
1670
1170
70
40-106
91-94-1
3,3'-Dichlorobenzidine
1670
1280
77
36-114
84-66-2
Diethyl Phthalate
1670
1430
86
61-109
131-11-3
Dimethyl Phthalate
1670
1430
86
59-108
117-84-0
Di-n-octyl Phthalate
1670
1500
90
64-119
84-74-2
Di-n-butyl Phthalate
1670
1390
83
63-108
122-66-7
1,2-Diphenylhydrazine
1670
1420
85
58-112
117-81-7
bis(2-Ethylhexyi)phthalate
1670
1510
91
64-115
206-44-0
Fluoranthene
1670
1320
79
60-108
86-73-7
Fluorene
1670
1380
83
58-109
118-74-1
Hexachlorobenzene
1670
1380
83
59-111
87-68-3
Hexachlorobutadiene
1670
1240
74
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1220
73
49-110
67-72-1
Hexachloroethane
1670
1160
70
40-105
193-39-5
Indcno(1,2,3-cd)pyrenc
1670
1350
81
66-116
78-59-1
Isophorone
1670
1210
73
42-89
90-12-0
1-Methylnaphthalene
1670
1250
75
49-106
91-57-6
2-Methylnaphthalene
1670
1170
70
47-106
91-20-3
Naphthalene
1670
1250
75
44-104
98-95-3
Nitrobenzene
1670
1270
76
43-108
621-64-7
N-Nitrosodi-n-propylamine
1670
1190
71
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1370
82
62-110
85-01-8
Phenanthrene
1670
1330
80
63-111
129-00-0
Pyrene
1670
1460
88
65-115
120-82-1
I,2,4-Trichlorobenzene
1670
1270
76
45-100
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
72%
40-102%
4165-62-2
Phenol-d5
77%
4I-100%
118-79-6
2,4,6-Tribromophenol
81%
42-108%
4165-60-0
Nitrobenzene-d5
72%
40-105%
321-60-8
2-Fluorobiphenyl
77%
43-107%
1718-51-0
Terphenyl-d14
77%
45-119%
* — Outside of Control Limits.
Method: SW846 8270E
..,6f16s

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property, N Sugar Creek, Charlotte, NC
Page 1 of 2
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP77248-MS
9I006765.1) 1
10/15/19
MV
10/11/19
OP77248
S91250
OP77248-MSD
9I006766.D 1
10/15/19
MV
10/11/19
OP77248
S91250
FA68836-I
9I006764,D 1
10/15/19
MV
10/11/19
OP77248
S91250
The QC reported here applies to the following samples:
Method: SW846 8270E
FA68803-2
y
w
i
FA68836-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
uglkg
uglkg
%
ug/kg
ug/kg
%
RPD
RecIRPD
65-85-0
Benzoic Acid
ND
3770
2820
75
3720
2640
71
7
36-118/41
59-50-7
4-Chloro-3-methyl Phenol
ND
1880
1530
81
1860
1460
79
5
52-108/21
95-57-8
2-Chlorophenol
ND
1890
1400
74
1860
1370
74
2
48-104/26
120-83-2
2,4-Dichlorophenol
ND
1880
1570
83
1860
1490
80
5
51-105/27
105-67-9
2,4-Dimethylphenol
ND
1880
1440
76
1860
1360
73
6
43-96/23
51-29-5
2,4-Dinitrophenol
ND
3770
2770
74
3720
2630
71
5
40-I19/32
534-52-1
4,6-Dinitro-o-cresol
ND
3770
3360
89
3720
3200
86
5
64-121/29
95-48-7
2-Methylphenol
ND
1880
1300
69
1860
1250
67
4
46-107/24
3&4-Methylphenol
ND
3770
2570
68
3720
2490
67
3
44-111/24
88-75-5
2-Nitrophenol
ND
1880
1460
78
1860
1400
75
4
49-104/27
100-02-7
4-Nitrophenol
ND
3770
2930
78
3720
2800
75
5
56-116/23
87-86-5
Pentachlorophenol
ND
3770
3110
83
3720
2950
79
5
61-114/23
108-95-2
Phenol
ND
1880
1370
73
1860
1330
72
3
45-110/24
88-06-2
2,4,6-Trichlorophenol
ND
1880
1680
89
1860
1610
87
4
56-I09/25
83-32-9
Acenaphthene
ND
1880
1470
78
1860
1370
74
7
56-109/23
208-96-8
Acenaphthylene
ND
1880
1520
81
1860
1440
77
5
56-106/23
120-12-7
Anthracene
ND
1890
1500
80
1860
1400
75
7
61-110121
56-55-3
Benzo(a)anthracene
ND
1880
1680
89
1860
1610
87
4
66-111/23
50-32-8
Benzo(a)pyrene
ND
1880
1530
81
1860
1470
79
4
59-104/23
205-99-2
Renzo(b)fluoranthene
ND
1880
1630
87
1860
1560
84
4
67-113/24
191-24-2
Benzo(g,h,i)perylenc
ND
1880
1510
80
1860
1460
79
3
67-113/21
207-08-9
Benzo(k)fluoranthene
ND
1880
1580
84
1860
1520
82
4
67-114/22
100-51-6
Benzyl Alcohol
ND
1880
1240
66
1860
1220
66
2
53-108/24
101-55-3
4-Bromophenyl phenyl ether
ND
1880
1700
90
1860
1590
86
7
62-11.0/21
85-68-7
Butyl benzyl phthalate
ND
1880
1660
88
1860
1600
86
4
65-113/20
106-47-8
4-Chloroaniline
ND
1880
1210
64
1860
1180
63
3
30-115/30
111-91-1
bis(2-Chloroethoxy)methane
ND
1880
1480
79
1860
1400
75
6
48-105/24
111-44-4
bis(2-Chloroethyl)ether
ND
1880
1240
66
1860
1210
65
2
46-103/27
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
1880
1170
62
1860
1150
62
2
40-110/25
91-58-7
2-Chloronaphthalene
ND
1880
1470
78
1860
1400
75
5
53-106/23
7005-72-3
4-Chlorophenyt phenyl ether
ND
1880
1600
85
1860
1480
80
8
58-106/21
218-01-9
Chrysene
ND
1880
1620
86
1860
1600
86
1
65-112/25
53-70-3
Dibenzo(a,h)anthracene
ND
1880
1510
80
1860
1480
80
2
68-115/23
I32-64-9
Dibenzofiran
ND
1880
1520
81
1860
1440
77
5
57-108/22
95-50-1
1,2-Dichlorobenzene
ND
1880
1240
66
1960
1210
65
2
44-102/28
541-73-1
1,3-Dichlorobenzene
ND
1880
1200
64
1860
1180
63
2
42-100/30
* = Outside of Control Limits.
��AI— 35 of 49
FA66&63

Matrix Spike/Matrix Spike Duplicate Summary
Page 2
Job Number:
FA69803
of 2
Account:
TGNCIT Thompson Geological
Project:
Hinson Property; N Sugar Creek, Charlotte, NC
Sample
File 1D DF Analyzed By
Prep Date
Prep Batch
Analytical Batch
OP77248-MS
91006765.D 1 10/15/19 MV
10/11/19
OP77248
S91250
OP77248-MSD
91006766.1) 1 10/15/19 MV
10/11/19
OP77248
S9I250
FA68836-1
9I006764.D 1 10/15/19 MV
10/11/19
OP77248
S9I250
The QC reported here applies to the following samples:
Method: SW946 8270E
FA68803-2
--I
w
FA68836-1
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
uglkg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
106-46-7
1,4-Dichlorobenzene
ND
1890
1200
64
1860
1180
63
2
40-106/29
91-94-1
3,3'-Dichlorobenzidine
ND
1880
1440
76
1860
1460
79
1
36-114/28
84-66-2
Diethyl Phthalate
ND
1880
1580
84
1860
1490
80
7
61-109/20
131-I1-3
Dimethyl Phthalate
ND
1880
1600
85
1860
1490
80
7
59-108/20
117-84-0
Di-n-octyl Phthalate
ND
1880
1710
91
1860
1630
88
5
64-119/21
84-74-2
Di-n-butyl Phthalate
ND
1880
1590
84
1860
1510
81
5
63-108/19
122-66-7
1,2-Diphenylhydrazine
ND
1880
1580
84
1860
1480
80
7
58-112/22
117-81-7
bis(2-Ethylhexyl)phthalate
81.8 J
1880
1740
88
1860
1690
87
3
64-115/23
206-44-0
Fluoranthene
ND
1880
1510
80
1860
1420
76
6
60-108/25
86-73-7
Fluorene
ND
1880
1540
82
1860
1440
77
7
58-109/21
118-74-1
Hexachlorobenzene
ND
1880
1580
84
1860
1490
80
6
59-111121
87-68-3
Hexachlorobutadiene
ND
1880
1300
69
1860
1240
67
5
41-108/27
77-47-4
Hexachlorocyclopentadiene
ND
1880
1310
70
1860
1230
66
6
49-I10/31
67-72-1
Hexachloroethane
ND
1890
1170
62
1860
1150
62
2
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
ND
1880
t500
80
1860
1470
79
2
66-116/22
78-59-1
Isophorone
ND
1980
1310
70
1860
1240
67
5
42-89/22
90-12-0
I-Methylnaphthalene
ND
1880
1350
72
1860
1260
68
7
49406/26
91-57-6
2-Methy1naphthalene
ND
1880
1270
67
1860
1210
65
5
47-106/27
91-20-3
Naphthalene
ND
1980
1320
70
1860
1260
68
5
44-104/27
98-95-3
Nitrobenzene
ND
1880
1320
70
1860
1260
68
5
43-108/25
621-64-7
N-Nitrosodi-n-propylamine
ND
1880
1260
67
1960
1210
65
4
48-108127
86-30-6
N-Nitrosodiphenylamine
ND
1880
1530
81
1860
1460
79
5
62-110/21
85-01-8
Phenanthrene
ND
1880
1520
81
1860
1440
77
5
63-111/22
129-00-0
Pyrene
ND
1880
1640
87
1860
1590
86
3
65-115/25
I20-82-1
1,2,4-Trichlorobenzene
ND
1880
1360
72
1860
1300
70
5
45-100/26
CAS No.
Surrogate Recoveries
MS
MSD
FA68836-1
Limits
367-12-4
2-Fluorophenol
66%
66%
64%
40-102%
4165-62-2
Phenol-d5
71%
70%
67%
4I-100%
118-79-6
2,4,6-Tribromophenol
82%
78%
74%
42-108%
4165-60-0
Nitrobenzene-0
67%
66%
63%
40-105%
321-60-8
2-Fluorobiphenyt
75%
72%
69%
43-107%
1718-51-0
Terphenyl-d14
76%
75%
711/1.
45-il9%
* = Outside of Control Limits.

.. SGS
Orlando, FL
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix. Spike and Duplicate Summaries
Section 8
a

Method Blank Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By
GUU1519-MB UU029239.1) 1 10/11/19 SH
The QC reported here applies to the following samples:
FA68803-2
Page 1 of I
Prep Date Prep Batch Analytical Batch
n/a n/a GUU 1519
Method: MADEP VPH REV 1.1
CAS No.
Compound
Result
RL
MDL
Units Q
71-43-2
Benzene
ND
51
51
ug/kg
100-41-4
Ethylbenzene
ND
100
51
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
100
51
ug/kg
91-20-3
Naphthalene
ND
260
150
ug/kg
108-88-3
Toluene
ND
100
51
ug/kg
m,p-Xylene
ND
200
100
ug/kg
95-47-6
o-Xylene
ND
I00
51
ug/kg
C5- C8 Aliphatics (Unadj)
ND
5100
1800
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
5100
1800
ug/kg
C9- C10 Aromatics (Unadj.)
ND
5100
1800
ug/kg
CS- C8 Aliphatics
ND
5100
1800
ug/kg
C9- C12 Aliphatics
ND
5100
1800
ug/kg
C9- C10 Aromatics
ND
5100
1800
ug/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
BFB
100%
70-130%
460-00-4
BFB
95%
70-130%
90
-- - 33 of 4.9

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson. Property; N Sugar Creek, Charlotte, NC
Page 1 of 1
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUU1519-BS
UU029237.1) 1
10/11/19
SH
n/a
n/a
GUU1519
GUU15l9-BSD
UU029238.1) 1
10/11/19
SH
n/a
n/a
GUU1519
The QC reported here applies to the following samples:
FA68803-2
Method: MADEP VPH REV 1.1
Spike
ESP
BSP
BSD
BSD
Limits N
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/R.PD L
71-43-2
Benzene
4160
4090
98
4080
98
0
70430/25 •°
100-41-4
Ethylbenzene
4160
4120
99
4090
98
1
70-130/25
1634-04-4
Methyl Tort Butyl Ether
4160
4150
100
4140
99
0
70-130/25
91-20-3
Naphthalene
4160
3860
93
3810
92
1
70-130/25
108-98-3
Toluene
4160
4070
98
4060
98
0
70-130/25
m,p-Xylene
8320
8100
97
8000
96
1
70-130/25
95-47-6
o-Xylene
4160
4100
99
4070
98
1
70-130/25
C5- C8 Aliphaties (Unadj.)
12500
13700
110
13700
110
0
70-130/25
C9- C12 Aliphatics (Unadj.)
8320
8280
99
8720
105
5
70-130/25
C9- C 10 Aromatics (Unadj.)
4160
4170
100
4070
98
2
70-130/25
C9- C10 Aromatics
4160
4170
100
4070
98
2
70-130/25
CAS No.
Surrogate Recoveries
ESP
BSD
Limits
460-004
BFB
103%
95%
70-130%
460-004
BFB
101%
93%
70-130%
* — Outside of Control Limits.
- 30 of 4G
:aU&eos

Matrix Spike Summary Page i of 1
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68803-2MS UU029246.D 1 10/11/19 SH n/a n/a GUU1519
FA68803-2 UU029241.D 1 10/11/19 SH n/a n/a GUU1519
The QC reported here applies to the following samples:
Method: MADEP VPH REV 1.1
FA68803-2
FA68803-2
Spike
MS
MS
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
Limits
71-43-2
Benzene
ND
7150
7020
98
70-130
100-41-4
Ethyibenzene
210
7150
7290
99
70-130
1634-04-4
Methyl `Pert Butyl Ether
ND
7150
7250
101
70-130
91-20-3
Naphthalene
946
7150
7700
94
70-130
108-88-3
Toluene
310
7150
7300
98
70-130
m,p-Xylene
702
14300
14700
98
70-130
95-47-6
o-Xylene
496
7150
7570
99
70-130
C5- C8 Aliphaties (Unadj.)
4190 J
42900
50200
107
70-130
C9- C12 Aliphaties (Unadj.)
7920 J
35700
56700
136*
70-130
C9- C10 Aromatics (Unadj.)
10000
21400
21200
52*
70-130
C9- C10 Aromatics
10000
21400
21200
52*
70-130
CAS No.
Surrogate Recoveries
MS
FA68803-2 Limits
460-00-4
BFB
123%
127%
70-130%
460-00-4
BFB
121%
120%
70-130%
* — Outside of Control Limits.
w
40of4�)
i��n8843

Duplicate Summary Page I of I
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68803-21)UP UU029245.13 1 10/11/19 SH n/a nla GUU1519
FA68803-2 UU029241.D 1 10/11/19 SH nla nla GUU1519
The QC reported here applies to the following samples:
Method: MADEP VPH REV 1.1
FA68803-2
FA68803-2
DUP
®°
CAS No.
Compound
ug/kg Q
uglkg
Q
RPD
Limits —�
71-43-2
Benzene
ND
ND
ne
50 • •
100-41-4
Etbylbenzene
210
230
9
50
1634-04-4
Methyl Tert Butyl Ether
ND
ND
nc
50
91-20-3
Naphthalene
946
1060
11
50
108-88-3
Toluene
310
319
3
50
m,p-Xylene
702
731
4
50
95-47-6
o-Xylene
496
637
25
50
C5- C8 Aliphatics (Unadj_)
4190 J
4270
J
2
50
C9- C12 Aliphatics (Unadj.)
7920 J
4840
J
48
50
C9- C10 Aromatics (Unadj.)
10000
10600
6
50
C5- C8 Aliphatics
3880 J
3950
J
2
50
C9- C12 Aliphatics
6520 J
3240
J
67*
50
C9- C10 Aromatics
10000
10600
6
50
CAS No.
Surrogate Recoveries
DUP
FA68803-2
Limits
460-00-4
BFB
131%*
127%
70-130%
460-00-4
BFB
128%
120%
70-130%
* = Outside of Control Limits.

SGS
Orlando, FL
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 9
a
42 c, 6 49

Method Blank Summary Page I of I
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77224-MB NN026620.1) 1 10/11/19 RS 10/10/19 OP77224 GNN1306
The QC reported here applies to the following samples:
Method: MADEP EPH REV 1.1
FA68803-2
CAS No.
Compound
Result
RL
MDL
Units Q
83-32-9
Acenaphthene
ND
200
100
ug/kg
208-96-8
Acenaphthylene
ND
200
100
ug/kg
120-12-7
Anthracene
ND
200
100
ug/kg
56-55-3
Benzo(a)anthracene
ND
200
100
ug/kg
50-32-8
Benzo(a)pyrene
ND
200
100
ug/kg
205-99-2
Benzo(b)tluoranthene
ND
200
I00
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
200
100
ug/kg
207-08-9
Benzo(k)tluoranthene
ND
200
100
ug/kg
218-01-9
Chrysene
ND
200
100
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
200
100
ug/kg
206-44-0
Fluoranthene
ND
200
100
ug/kg
86-73-7
Fluorene
ND
200
100
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
200
100
ug/kg
91-57-6
2-Methytnaphthalene
ND
200
100
ug/kg
91-20-3
Naphthalene
ND
200
100
ug/kg
85-01-8
Phenanthrene
ND
200
100
ug/kg
129-00-0
Pyrene
ND
200
100
ug/kg
CI I-C22 Aromatics (Unadj)
ND
10000
4000
ug/kg
C11-C22 Aromatics
ND
10000
4000
ug/kg
C9-C18 Aliphatics
3820
10000
2500
ug/kg J
C19-06 Aliphatics
ND
10000
2500
ug/kg
CAS No. Surrogate Recoveries
3396-33-2
1-Chlorooctadecane
580-13-2
2-Bromonaphthalene
84-15-1
o-Terphenyl
321-60-8
2-Fluorobiphenyl
Limits
60% 40-140"%
76% 40-140%
70% 40-140%
73% 40-140%
a: 43 of 49
'•kt �v�?Lx.
F.A68BG3

Method Blank Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By
OP77283-MB WW22496.1) 1 10/15/19 SJL
The QC reported here applies to the following samples:
FA68803-1
CAS No. Compound Result RL
TPH (C10-C28) ND 5.0
Page 1 of 1
Prep Date Prep Batch Analytical Batch
10/15/19 OP77283 GWW925
Method: SW846 8015C
MDL Units Q
2.5 mg/kg
CAS No. Surrogate Recoveries Limits
84-15-1 o-Terphenyl 58% 56-122%
SGS 44 of 49
FA698oa

Blank Spike Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of I
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77283-BS WW22495.D 1 10/15/19 S1L 10/15/19 OP77283 GWW925
The QC reported here applies to the following samples:
FA68803-1
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
* = Outside of Control Limits.
Method: SW846 8015C
Spike BSP BSP
mg/kg mg/kg % Limits
50 33.6 67 62-116
BSP Limits $e
71% 56-122%
45 of 49
SG
FFA68803

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP77224-BS
NN026697.D
2
10/15/19
NJ
10/10/19
OP77224
GNN1309
OP77224-BSD
NN026698.1)
2
10/15/19
NJ
10/10/19
OP77224
GNN1309
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA68803-2
Spike
BSP
BSP
BSD
BSD
Limits
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
83-32-9
Acenaphthene
5000
3000
60
3350
67
11
40-140/30
208-96-8
Acenaphthylene
5000
2690
54
3020
60
12
40-140/30
120-12-7
Anthracene
5000
3160
63
3530
71
11
40-140/30
56-55-3
Benzo(a)anthracene
5000
3180
64
3570
71
12
40-140/30
50-32-8
Benzo(a)pyrene
5000
3110
62
3470
69
11
40-140/30
205-99-2
Benzo(b)fluoranthene
5000
3180
64
3560
71
11
40-I40/30
191-24-2
Benzo(g,h,i)perylene
5000
2990
60
3330
67
11
40-140/30
207-08-9
Benzo(k)fluoranthene
5000
3250
65
3640
73
11
40-I40/30
218-01-9
Chrysene
5000
3250
65
3640
73
11
40-I40130
53-70-3
Dibenzo(a,h)anthracene
5000
3380
68
3770
75
Il
40-140/30
206-44-0
Fluoranthene
5000
3200
64
3580
72
11
40-140/30
86-73-7
Fluorene
5000
2980
60
3320
66
11
40-140/30
193-39-5
lndeno(1,2,3-cd)pyrene
5000
3000
60
3370
67
12
40-140130
91-57-6
2-Methylnaphthalene
5000
2430
49
2730
55
12
40-140/30
91-20-3
Naphthalene
5000
2500
50
2800
56
11
40-140/30
85-01-8
Phenanthrene
5000
3050
61
3410
68
it
40-140/30
129-00-0
Pyrene
5000
3240
65
3620
72
11
40-140/30
CI I-C22 Aromatics (Unadj.)
85000
60200
71
65900
78
9
40-140/30
Ci I-C22 Aromatics
85000
8570
10*
8180
10*
5
50-150/30 a
C9-C18 Aliphatics
30000
20200
67
17800
59
13
40-140/30
C19-C36 Aliphatics
40000
22500
56
25200
63
11
40-140/30
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
3386-33-2
1-Chlorooctadecane
53%
59%
40-140%
590-13-2
2-13rumonaphthalene
63%
77%
40-140%
84-15-1
o-Terphenyl
65%
71%
40-140%
321-60-8
2-Fluorobiphenyl
65%
75%
40-140%
Sample
Compound
Col #1
Col #2
Breakthrough
Limit
OP77224-BS
2-Methylnaphthalene
2430
ND
0.0%
5.0
OP77224-BS
Naphthalene
2500
ND
0.0%
5.0
OP77224-BSD
2-Methylnaphthalene
2730
ND
0.0%
5.0
OP77224-BSD
Naphthalene
2800
ND
0.0%
5.0
* = Outside of Control Limits.
FA632 0 11

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF Analyzed By
OP77224-BS NN026697.1) 2 10/15/19 NJ
OP77224-BSD NN026698.D 2 10/15/19 NJ
The QC reported here applies to the following samples:
FA68803-2
(a) Advisory control limits.
* = Outside of Control Limits.
Page 2 of 2
Prep Date Prep Batch Analytical Batch
10/10/19 OP77224 GNN1309
10/10/19 OP77224 GNN1309
Method: MADEP EPH REV 1.1
47 of 49
FAfi8863

Matrix Spike/Matrix Spike Duplicate Summary
Page
.lob Number:
FA68803
1 of I
Account:
TGNCIT Thompson Geological
Project:
Hinson Property; N Sugar Creek, Charlotte, NC
Sample
File ID DF Analyzed By
Prep Date
Prep Batch
Analytical Batch
OP77283-MS
WW22510.D 10 10/16/19 SJL
10/15/19
OP77283
GWW926
OP77283-MSD
WW22511.D 10 10/16/19 SJL
10/15/19
OP77293
GWW926
FA68803-1
WW22509.D 10 10/16/I9 SJL
10/15/19
OP77283
GWW926
The QC reported here applies to the following samples: Method: SW846 8015C
FA68803-1
FA68803-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound mg/kg Q mglkg mg/kg % mg/kg mg/kg % RPD Rec/RPD
TPH (CIO-C28) 532 55.8 539 13* a 55.3 430 -184* 3 22 62-116/35
CAS No. Surrogate Recoveries MS MSD FA68803-1 Limits
84-15-1 o-Terphenyl 81% 82% 83% 56-122%
(a) Outside control Iimits due to high level in sample relative to spike amount.
* — Outside of Control Limits.
— � 48 of 49
FAM03

Duplicate Summary
Job Number: FA68803
Account: TGNCIT Thompson Geological
Project: Hinson Property; N Sugar Creek, Charlotte, NC
Sample File ID DF
OP77224-DUP NN026631.D 200
FA68805-13 NN026632,1) 200
Analyzed By Prep Date
10/12/19 RS 10/10/19
10/12/19 RS 10/10/19
Page I of I
Prep Batch Analytical Batch
OP77224 GNN1307
OP77224 GNN 1307
The QC reported here applies to the following samples: Method: MADBP I PH REV 1.1
FA68803-2
FA68805-1 DUP
CAS No. Compound ug/kg Q ug/kg Q RPD Limits
83-32-9
Acenaphthene
45000 U
ND
nc
30 b
208-96-8
Acenaphthylene
45000 U
ND
nc
30 b
120-12-7
Anthracene
45000 U
ND
nc
30 b
56-55-3
Benzo(a)anthracene
45000 U
ND
ne
30 b
50-32-8
Benzo(a)pyrene
45000 U
ND
nc
30 b
205-99-2
Benzo(b)fluoranthene
45000 U
ND
nc
30 b
191-24-2
Benzo(g,h,i)perylcne
45000 U
ND
ne
30 b
207-08-9
Benzo(k)fluoranthene
45000 U
ND
ne
30 b
218-01-9
Chrysene
45000 U
ND
ne
30 b
53-70-3
Dibenzo(a,b)anthracene
45000 U
ND
ne
30 b
206-44-0
Fluoranthene
45000 U
ND
nc
30 b
86-73-7
Fluorene
45000 U
ND
nc
30 b
193-39-5
Indeno(1,2,3-cd)pyrene
45000 U
ND
ne
30 b
91-57-6
2-Methylnaphthalene
45000 U
ND
nc
30 b
91-20-3
Naphthalene
45000 U
ND
ne
30 b
85-01-8
Phenanthrene
45000 U
ND
ne
30 b
129-00-0
Pyrene
45000 U
ND
ne
30 b
CI1-C22 Aromatics (Unadj.)
1400000 1
1280000 J
9
30 b
CI 1-C22 Aromatics
1400000 I
1280000 J
9
30 b
C9-CI8 Aliphatics
5240000 V
5440000
4
30 b
C19-C36 Aliphatics
1530000 1
1580000 J
3
30 b
CAS No.
Surrogate Recoveries
DUP
FA68805-1
Limits
3386-33-2
1-Chlorooctadecane
0%* c
0%* c
40-140%
580-13-2
2-Bromonaphthalene
0%* c
0%* c
40-140%
84-15-1
o-Terphenyl
0%* c
0%* c
40-140%
321-60-8
2-Fluorobiphenyl
0%* °
0%* e
40-140%
(a) Dilution required prior to fractionation due to matrix.
(b) Advisory control limits.
(c) Outside control limits due to dilution.
* = Outside of Control Limits.
sG49 of 49
FABB803

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, November 1, 2021 3:05 PM
To: Philip Thompson
Subject: RE: [External] 2422 West Sugar Creek
Received. I'll let you know when it's ready.
Trudy
Trudy Beverly, L.G.
F Hydrogeologist, Division of Waste Management
cc�.�DEQNorth Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
ht_pt s://deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htt2s://deg.nc.gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedea/Waste%2OMana2ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeg/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Philip Thompson [mailto:[e-mail]]
Sent: Monday, November 1, 2021 1:17 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] 2422 West Sugar Creek
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Attached is the IA for 2422 West Sugar Creek. The monitor well has been closed. The USTs were actually in
the Right of way not on the property (I Don't know if that makes any difference). I am sending you a NORP
this week, If Ron can sign it and get it out, that would be appreciated. We are try to get the property closed and
sold.