MO-28833_48049_CA_SAR_20200224_Soil Assessment Report

February 24, 2020
Consulting Engineers
GEQSCIENCE
GROUP
North Carolina Department of Environmental Quality
Division of Waste Management
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Attention: Underground Storage Tank Section
Reference: Soil Remediation Report
Sedgefteld Shopping Center - 2807 South Boulevard
Charlotte, North Carolina
Geoscience Project No. CH 14.00 t TEV
Incident No. PENDING
This Soil Remediation Report summarizes the removal of petroleum impacted soils following the
closure of an underground storage tanks (UST) that was formerly used to store heating oil for the
businesses located at 2807 South Boulevard.
Site Name:
Sedgefield Shopping Center - 2807
South Boulevard
UST Owner/Operator:
Unknown
Consultant:
Geoscience Group, Inc.
500 Clanton Road, Suite K
Charlotte, North Carolina 28217
[phone]
Site Location:
2807 South Boulevard
Charlotte, North Carolina 28209
Property Owner:
Marsh Properties, LLC
2401 Park Road
Charlotte, North Carolina 28203
Laboratory:
Waypoint Analytical
449 Springbrook Lane
Charlotte, North Carolina 28224
[phone]
Date Discovered: November 25, 2019 Latitude/Longitude: 35.199130°/-80.866825"
Quantity of Release: Unknown Cause of Release: Tank Corrosion
Source of Release: UST-1 System Contents/Size: Heating Oil, 550-gal.
1, Thomq+►+l'CHT ;,� a Professional Engineer for Geoscience Group, Inc., do certify that the
in �c _ �, f�&is report is correct and accurate to the best of my knowledge.
North Cafifta=e"t'ise No. 035050
Geoscience Group, Inc. is licensed to practice engineering in North Carolina. The certification
number of the company is F-0585.
Enclosures
P:I...BNVa014i017 — SedgefieldliJSTlSedgefick RemedRpt.doc
500 Clanton Road Charlotte, North Carolina Telephone Facsimile NC License
Suite K 28217 704.525.2003 704.525.2051 F-0585

Geoscience Project No. CH14.0017.EV
February 24, 2020
Page 2
SITE HIS TOR YAND CHARACTERIZATION
The subject property is a 1.313± acre tract located along the eastern side of South Boulevard
between Elmhurst and Marsh Roads in Charlotte, North Carolina. The site consists of
Mecklenburg County Tax Parcel ID No. 14704201. Until its recent demolition, the property
had been occupied by a single -story multi -tenant retail building since at least 1945. The
footprint of the former building is shown on Figure No. CHI4.017-A in Appendix II.
The installation and usage dates for the former storage tank (UST-1) are not known. As shown
on the Site Layout, Figure No. CH14.017-A, the former tank was located adjacent to the back
exterior wall of the building. No other USTs have been encountered on Parcel No. 14704201,
and no other USTs are known to have been used at the site. Tables B-1 and B-2 in Appendix
I summarize the UST-1 information.
Based on review of the 1985 Geologic Map of North Carolina, the subject site is located within
the Charlotte Belt of the Piedmont Physiographic Province. This Province is generally
characterized by igneous intrusive and metamorphic bedrock that is Devonian to Ordovician
in age. The intrusive rock is typically overlain with a layer of soil and weathered rock, ranging
in thickness from 0 to 150 feet. Bedrock within the Charlotte Belt consists primarily of the
diorite -granite complex, with the granite appearing to be the predominant component of the
complex. According to the Geologic Map, the subject site is underlain with granitic rock.
According to the 1967 (Photorevised in 1988) "Charlotte East, North Carolina" United States
Geological Survey (USGS) 7.5-minute quadrangle map, the subject site is located between
approximately 738 and 740 feet above mean sea level (MSL). The ground surface across the
project site generally slopes downward toward the west. The low elevation of 738 feet MSL is
located along the western property boundary and the high elevation of 740 feet MSL is located
on the eastern and southern portions of the subject site.
INITIAL INVESTIGATION
Geoscience was on site on November 14, 2019 to monitor the excavation of a test pit in an
area behind the building where a geophysical survey of the back parking lot had identified an
anomaly. That test pit uncovered the top of UST-1. Observation through a hole in the top of
the tank indicated that UST-1 was partially full of fluid that appeared to be mostly water.
While the test pit was open, one (1) soil sample (S-1) was collected from a hand auger boring
advanced adjacent to the northwestern end of the tank. The approximate location of the soil
sample is depicted on Figure No. CH14.017-13 in Appendix II. The sample was placed in
laboratory -provided containers, packed on ice, and transported in a cooler under appropriate
chain -of -custody procedures to Prism Laboratories, Inc. (Prism) of Charlotte, North Carolina
for chemical analyses. Soil sample S-1 was analyzed for Gasoline -Range Organics (TPH-
GRO), Diesel -Range Organics (TPH-DRO), and volatile organic compounds by EPA Method
8260.

Geoscience Project No. CH14.0017.EV
February 24, 2020
Page 3
As shown on Table B-3 in Appendix II, TPH-DRO was detected in sample S-1 at a
concentration of 380 mg/kg. This concentration exceeds the 100 mg/kg action level
established by NCDEQ for TPH-DRO. In addition, acetone, bromomethane, and methyl ethyl
ketone were detected in the sample, but at concentrations below applicable remediation
standards. A copy of the Prism laboratory report is included in Appendix IV.
Based on the results obtained from sample S-1, it was apparent that there had been a release
from the UST system. Geoscience recommended that UST-1 be closed by removal.
CLOSURE PROCEDURES
Geoscience returned to the site on January 23, 2020 to monitor the permanent closure of
UST-1. EVO Corporation (EVO) was contracted to remove the tank and excavate
contaminated soils encountered beneath the UST. Prior to excavation, a vacuum truck was
used to remove residual fluids from the tank. Approximately 350 gallons of water mixed with
fuel oil was recovered from UST-1. The fluid removed from UST-1 was transported to EVO's
facility for proper disposal. A copy of the Certificate of Disposal for the fluid is included in
Appendix V for your review.
The clean overburden on top of the tank was removed and stockpiled on -site. The tank was
then removed from the ground (Photograph 1 in Appendix III). The exterior of UST-1
exhibited obvious corrosion through holes. The tank was subsequently transported to EVO's
facility for proper disposal. A copy of the Tank Disposal Certificate is included in Appendix
V. UST-1 was approximately was approximately 72 inches long and 48 inches in diameter
for an estimated capacity of 550 gallons
CLOSURE INVESTIGATION
Following removal of the tank, the soils beneath the UST was examined for indications of
petroleum release. Although soils beneath the tank exhibited a petroleum odor, no staining of
the soils was noted beneath the tank. Furthermore, no free product was encountered in the
tank basin.
A soil sample (identified as S-1 in the laboratory report, but referred to as S-IA in this report
to prevent confusion with the November 2019 soil sample) was collected approximately 1 foot
beneath the bottom of the southeastern end of UST-1. The approximate location of the soil
sample is depicted on Figure No. CH14.017-13 in Appendix II. The sample was placed in
laboratory -provided containers, packed on ice, and transported in a cooler under appropriate
chain -of -custody procedures to Waypoint Analytical (Waypoint) of Charlotte, North Carolina
for chemical analyses. Soil sample S-IA was analyzed for TPH-GRO and TPH-DRO.
As summarized in Table B-3 in Appendix I, neither TPH-GRO nor TPH-DRO were detected
in sample S-IA

Geoscience Project No. CH14.0017.EV
February 24, 2020
Page 4
SOIL REMEDIATION
The UST-1 tank basin was over -excavated laterally and vertically in an effort to remediate the
impacted soils that had been identified by the November 2019 sampling event. The final
excavation measured approximately twelve (12) feet long, ten (10) feet wide, and nine (9) feet
deep. The extent of the excavation was determined by screening the excavated soils with a
photo -ionization detector.
The excavated soils were loaded directly onto trucks and transported to EVO's facility for
proper disposal. A total of 14.29 tons of impacted soil were hauled off -site for treatment.
Copies of the manifests and Certificate of Disposal for the impacted soil are included in
Appendix V for your review.
Upon completion of the soil removal, confirmatory soil samples (S-2 through S-6) were
obtained from the bottom and sidewalls of the UST-1 excavation. The soil samples were
submitted to Waypoint under appropriate chain -of -custody for chemical analyses using EPA
Method 8260 (volatile organics), EPA Method 8270 (semi -volatile organics), and MADEP
VPH/EPH (aliphatic and aromatic hydrocarbons). The excavation was subsequently
backfilled with the clean overburden and clean soil from an off -site location.
The analytical results of the confirmatory soil samples are summarized in Table B-3 in
Appendix I. As indicated on the table, C9-C22 aromatic and C9-C 18 aliphatic hydrocarbons
were detected in sample S-2 (bottom) at concentrations exceeding their respective
"residential" maximum soil contaminant concentrations (MSCCs). In addition,
1-methylnaphthalene, 2-methylnaphthalene, and naphthalene exceeded their respective "soil
to groundwater" MSCCs in sample S-2. Although several other petroleum compounds were
detected in samples S-2, S-4, and S-5, no other exceedances of applicable cleanup standards
were encountered in the confirmation samples. A copy of the laboratory test report is included
in Appendix IV.
POTENTIAL RECEPTORS
Geoscience conducted a walking survey of the area within 500 feet of UST-l. No potential
receptors were noted. Specifically, no water supply wells were noted within 500 feet of the
release area. The nearest surface water is Dairy Branch (creek), located approximately
1,000 feet northeast of the release area.
CONCLUSIONS
Geoscience has observed and documented the closure of an underground storage tank (UST-
1) formerly located at 2807 South Boulevard in Charlotte, North Carolina. The tank was
previously used to store heating oil and was approximately 550 gallons in capacity. The
installation and usage dates of the tanks are not known. Soil sampling conducted following
removal of the UST confirmed that the soils immediately beneath UST-1 have been impacted
by a release of petroleum.

Geoscience Project No. CH14.0017.EV
February 24, 2020
Page 5
In an effort to remediate the release, approximately 14.29 tons of petroleum impacted soil was
excavated from the former tank basin and disposed of properly. Upon removal of these soils,
a total of five (5) confirmation samples collected from within the resulting excavation were
submitted for laboratory analysis. Soil sample S-2, from the bottom of the excavation,
exhibited exceedances of both the "soil to groundwater" and "residential" cleanup standards.
However, none of the detected compounds were present at concentrations exceeding
"industrial/commercial" MSCCs.
Given that no potential receptors were observed within 150 feet of the release area, Geoscience
concludes that the release can be classified as "Low Risk" and closed without conducting
further cleanup. However, recordation of an appropriate "Notice of Residual Petroleum"
would be required to obtain a "No Further Action" determination. Geoscience anticipates that
the "Notice of Residual Petroleum" would restrict redevelopment of the site for residential
purposes and disallow use of groundwater at the property. The residential land use restriction
could be avoided by remediating the remaining soils that exceed residential MSCCs.

APPENDIX I
Tables:
Table B-1: Site History - UST/AST System and Other Release Information
Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party Information
Table B-3: Summary of Soil Sampling Results

Table B-1: Site History - UST/AST System and Other Release Information
Revision February 18, 2020 Incident Pending Incident Name: Sedgefield Shopping Center - 2807 South
Date: Number: Boulevard
UST ID
Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Piping/Pumps
Installation
Date
Status of
UST
Was Release
Associated
with System
UST-1
Heating Oil
Heating Oil
550
Steel
72" Long
48" Diam.
small diameter
copper line
Unknown
Removed
Yes
AST ID
Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Piping/Pumps
Installation
Date
Status of
UST
Was Release
Associated
with System
N/A
Incident
Material
Date of
Description of Release
Number
Released
Release
Petroleum impacted soils were discovered beneath heating oil UST during site assessment. Release
Pending
Heating Oil
Unknown
apparently due to corrosion of tank. Total amount released and date of initial release are unknown. No
free product encountered. DRO as high as 380 mg/kg. encountered beneath UST-1.

Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party
Information
Revision February 18, 2020 Incident Pending Incident Sedgefield Shopping Center -
Date: Number: Name: 2807 South Boulevard
UST ID
Number:
UST-1
Facility
Number:
N/A
Name of Owner
Dates of Operation
Marsh Properties, LLC
Unknown
Street Address
2401 Park Road
City
State
Zip Code
TelephoneNumber
Charlotte
NC
28224
704-602-2062
Name of Operator
Dates of Operation
Unknown
Unknown
Street Address
2807 South Boulevard
City
State
Zip Code
TelephoneNumber
Charlotte
NC
28209
Unknown
Incident Number
Pending
Name of Other Responsible Party
Dates of Releases
N/A
unknown
Street Address
City
State
Zip Code
TelephoneNumber

Table B-3: Summary Of Soil Sampling Results
Revision Date:2/ 18/20 Incident Name/Number: Sedgefield Shopping Center - 2807 South Boulevard - Incident Number Pending
Date Collected
11/14/2019
1/23/2020
1/23/2020
1/23/2020
1/23/2020
1/23/2020
1/23/2020
U
U
e
�
.y�.
0
U
U
c
U
`
o
U
Source Area
UST Basin
Bottom
UST Basin
Bottom
Excavation
Bottom
Excavation
Sidewall
Excavation
Sidewall
Excavation
Sidewall
Excavation
Sidewall
Sample Depth (ft BGS)
7.5
7.5
9
8
8
8
8
Incident Phase
Investigation
Closure
Closure
Closure
Closure
Closure
Closure
Sample ID
S-1
S-IA
S-2
S-3
S-4
S-5
S-6
Analytical Method
Contaminant of Concern
TPH (mg/kg)
DRO
380
<3.1
N.A.
N.A.
N.A.
N.A.
N.A.
N/A
N/A
N/A
GRO
<2.2
<2.3
N.A.
N.A.
N.A.
N.A.
N.A.
N/A
N/A
N/A
/
VPH EPH (mg/kg)
C9-C22 Aromatics
N.A.
N.A.
902
<12.9
<12.5
<10.8
<10.5
31
469
12,264
C5-C8 Aliphatics
N.A.
N.A.
<5.4
<6.1
<5.4
<1.8
<1.8
68
939
24,528
C9-C18 Aliphatics
N.A.
N.A.
2,060
<4.6
<4.3
1.8 J
<2.6
540
1,500
40,000
C 19-C36 Aliphatics
N.A.
N.A.
470
<6.4
<6.3
<6.1
<5.9
N/A
31,000
810,000
8260 (mg/kg)
1,2,4-Trimethylbenzene
<0.00059
N.A.
0.21
<0.00077
<0.00094
<0.00071
<0.00071
8.5
782
20,440
1,3,5-Trimethylbenzene
<0.00070
N.A.
0.019
<0.00092
<0.0011
<0.00084
<0.00084
8.3
782
20,440
4-Isopropyltoluene
<0.0014
N.A.
0.026
<0.0018
<0.0022
<0.0017
<0.0017
0.12
100
4,000
Acetone
0.16
N.A.
0.21
<0.0019
0.038
<0.0017
<0.0017
24
14,000
360,000
Bromomethane
0.0054 J
N.A.
<0.0040
<0.0036
<0.0044
<0.0033
<0.0033
0.4
22
570
Ethylbenzene
<0.00083
N.A.
0.0081
<0.0011
<0.0013
<0.0010
<0.0010
4.9
1,560
40,000
Isopropylbenzene
<0.00064
N.A.
0.016
<0.00085
<0.0010
<0.00078
<0.00078
1.7
1,564
40,880
m,p-Xylenes
<0.0014
N.A.
0.029
<0.0019
<0.0023
<0.0017
<0.0017
4.6
3,129
81,760
Methyl Ethyl Ketone
0.022
N.A.
0.037
<0.0017
<0.0021
<0.0016
<0.0016
16
9,385
245,280
Naphthalene
<0.00056
N.A.
0.055
<0.00074
<0.00090
<0.00067
<0.00067
0.16
313
8,176
n-Butylbenzene
<0.00052
N.A.
0.034
<0.00068
<0.00083
<0.00062
<0.00062
4.3
626
16,350
n-Propylbenzene
<0.00080
N.A.
0.035
<0.0011
<0.0013
<0.00097
<0.00097
1.7
626
16,350
o-Xylene
<0.00059
N.A.
0.015
<0.00078
<0.00095
<0.00071
<0.00071
4.6
3,129
81,760
sec-Butylbenzene
<0.00060
N.A.
0.031
<0.00079
<0.00096
<0.00072
<0.00072
3.3
626
16,350
tert-Butylbenzene
<0.00066
N.A.
0.0051 J
<0.00087
<0.0011
<0.00087
<0.00079
3.4
626
16,350
Xylenes - total
<0.0020
N.A.
0.045
<0.0026
<0.0032
<0.0024
<0.0024
4.6
3,129
81,760
8270 (mg/kg)
1-Methylnaphthalene
N.A.
N.A.
6.0
<0.16
<0.16
<0.16
<0.14
0.004
20
100
2-Methylnaphthalene
N.A.
N.A.
8.2
<0.019
<0.019
<0.019
<0.018
3.6
63
1,635
Acenaphthene
N.A.
N.A.
1.0
<0.023
<0.023
<0.022
<0.021
8.2
940
24,000
Naphthalene
N.A.
N.A.
0.58 J
<0.021
<0.021
<0.021
<0.020
0.16
313
8,176
Phenanthrene
N.A.
N.A.
6.7
<0.011
<0.011
<0.011
<<0.010
56
469
12,264
Notes: N.A. - Not Analyzed
N/A - Not Applicable
BRL - Below Reporting Limit
- Exceeds TPH Action Level (100 mg/kg - DRO; 50 mg/kg - GRO)
- Exceeds Soil To Groundwater MSCC
- Exceeds Residential MSCC
- Exceeds Industrial/Commercial MSCC

APPENDIX II
Figures:
Figure No. CH14.017-A - Site Layout
Figure No. CH14.017-B - Sample Location Diagram

04 t
SITE
`COP
J
► f:� t� .
Charlott
f Former Chan°
Building
,f n
S A}�
T
r

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.:.:..............................................
Former Building
(2807 South Boulevard) ::. ::::::::::
:: ::::
.........................
.S-6'
�® S-1 •.
S-3
S-5 ®,
,S-4
Z.�
Approximate
Extent of
Excavation
SIT.
I GEOSCIENCE GROUP, INC. I
CHARLOTTE, NORTH CAROLMA
SCALE: 1" z 10' 1APPROVED BY:
DRAWN BY: Mecklenburg Co.
N DATE: January 28, 2020 ` -" ` REVISED: ANP
SEDGEFIELD SHOPPING CENTER PHASE 36
CHARLOTTE, NORTH CAROLINA
FIGURE NUMBER:
SAMPLE LOCATION DIAGRAM CH14.017-11

APPENDIX III
Site Photographs

RAW
IR
�or q
r7r

APPENDIX IV
Laboratory Reports

Case Narrative
P R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Geoscience Group
Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: Sedgefield
Lab Submittal Date: 11/14/2019
Prism Work Order: 9110276
11 /25/19 10:30
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a'J
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash
VP Laboratory Services
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13

IP�R I S M Full -Service Analytical Environmental Solutions
-_LABORATORIES, ING
Sample Receipt Summary
11 /25/2019
Prism Work Order: 9110276
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
S-1 9110276-01 Solid 11/14/19 14:54 11/14/19 15:22
Samples were received in good condition at 5.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

Full -Service Analytical &Environmental
Summary of Detections
/PRISM
Solutions
11/25/2019
eO�T�R
Prism Work Order: 9110276
Prism ID
Client ID
Parameter
Method Result Units
9110276-01
S-1
Diesel Range Organics
`8015C 380 mg/kg dry
9110276-01
S-1
Acetone
8260D 0.16 mg/kg dry
9110276-01
S-1
Bromomethane
8260D 0.0054 J mg/kg dry
9110276-01
S-1
Methyl Ethyl Ketone (2-Butanone)
8260D 0.022 mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

PRISM Laboratory Report
/ Full -Service Analytical &
Environmental Solutions 11/25/2019
LA60RATORIES, ING.
Geoscience Group Project: Sedgefield Client Sample ID: S-1
Attn: Tom Hassett Prism Sample ID: 9110276-01
500-K Clanton Rd. Prism Work Order: 9110276
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 11/14/19 14:54
Time Submitted: 11/14/19 15:22
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Diesel Range Organics by GC/FID
Diesel Range Organics
380
mg/kg dry
110
36
10
*8015C
11/20/19 11:32
ZRC
P9K0322
Surrogate
Recovery Control Limits
o-Terphenyl
67 %
31-123
Gasoline Range Organics by GC/FID
Gasoline Range Organics
BRL
mg/kg dry
8.1
2.2
50
*8015C
11/18/19 13:09
TBL
P91<0286
Surrogate
Recovery Control Limits
a,a,a-Trifluorotoluene
118 %
50-137
General Chemistry Parameters
% Solids
66.0
% by
0.100
0.100
1
*SM2540 G
11/19/19 9:57
EDV
P9K0327
Weight
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00068
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0055
0.00081
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00040
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0055
0.00060
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1-Dichloroethane
BRL
mg/kg dry
0.0055
0.0010
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260D
11/21/19 22:06
JLB
P91<0392
1,1-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00085
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00079
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0055
0.00063
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00053
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00059
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2-Dibromoethane
BRL
mg/kg dry
0.0055
0.00050
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00062
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2-Dichloroethane
BRL
mg/kg dry
0.0055
0.00066
1
8260D
11/21/19 22:06
JLB
P91<0392
1,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00083
1
8260D
11/21/19 22:06
JLB
P91<0392
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00070
1
8260D
11/21/19 22:06
JLB
P91<0392
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00069
1
8260D
11/21/19 22:06
JLB
P91<0392
1,3-Dichloropropane
BRL
mg/kg dry
0.0055
0.00046
1
8260D
11/21/19 22:06
JLB
P91<0392
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00070
1
8260D
11/21/19 22:06
JLB
P91<0392
2,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00069
1
8260D
11/21/19 22:06
JLB
P91<0392
2-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00074
1
8260D
11/21/19 22:06
JLB
P91<0392
4-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00063
1
8260D
11/21/19 22:06
JLB
P91<0392
4-Isopropyltoluene
BRL
mg/kg dry
0.0055
0.0014
1
8260D
11/21/19 22:06
JLB
P91<0392
Acetone
0.16
mg/kg dry
0.022
0.0014
1
8260D
11/21/19 22:06
JLB
P9K0392
Benzene
BRL
mg/kg dry
0.0055
0.00086
1
8260D
11/21/19 22:06
JLB
P91<0392
Bromobenzene
BRL
mg/kg dry
0.0055
0.00077
1
8260D
11/21/19 22:06
JLB
P91<0392
Bromochloromethane
BRL
mg/kg dry
0.0055
0.00091
1
8260D
11/21/19 22:06
JLB
P91<0392
Bromodichloromethane
BRL
mg/kg dry
0.0055
0.00053
1
8260D
11/21/19 22:06
JLB
P91<0392
Bromoform
BRL
mg/kg dry
0.0055
0.00043
1
8260D
11/21/19 22:06
JLB
P91<0392
Bromomethane 0.0054
J
mg/kg dry
0.011
0.0027
1
8260D
11/21/19 22:06
JLB
P91K0392
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 13

PRISM Laboratory Report
/ Full -Service Analytical &
Environmental Solutions 11/25/2019
LA60RATORIES, ING.
Geoscience Group Project: Sedgefield Client Sample ID: S-1
Attn: Tom Hassett Prism Sample ID: 9110276-01
500-K Clanton Rd. Prism Work Order: 9110276
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 11/14/19 14:54
Time Submitted: 11/14/19 15:22
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Carbon Tetrachloride
BRL
mg/kg dry
0.0055
0.0011
1
8260D
11/21/19 22:06
JLB
P91<0392
Chlorobenzene
BRL
mg/kg dry
0.0055
0.00086
1
8260D
11/21/19 22:06
JLB
P91<0392
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
11/21/19 22:06
JLB
P9K0392
Chloroform
BRL
mg/kg dry
0.0055
0.00068
1
8260D
11/21/19 22:06
JLB
P9K0392
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
11/21/19 22:06
JLB
P9K0392
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.00087
1
8260D
11/21/19 22:06
JLB
P9K0392
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00055
1
8260D
11/21/19 22:06
JLB
P9K0392
Dibromochloromethane
BRL
mg/kg dry
0.0055
0.00037
1
8260D
11/21/19 22:06
JLB
P9K0392
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
11/21/19 22:06
JLB
P91<0392
Ethylbenzene
BRL
mg/kg dry
0.0055
0.00083
1
8260D
11/21/19 22:06
JLB
P91<0392
Isopropyl Ether
BRL
mg/kg dry
0.0055
0.00081
1
8260D
11/21/19 22:06
JLB
P91<0392
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0055
0.00064
1
8260D
11/21/19 22:06
JLB
P91<0392
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0014
1
8260D
11/21/19 22:06
JLB
P91<0392
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00038
1
8260D
11/21/19 22:06
JLB
P91<0392
Methyl Ethyl Ketone (2-Butanone)
0.022
mg/kg dry
0.022
0.0013
1
8260D
11/21/19 22:06
JLB
P9K0392
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00045
1
8260D
11/21/19 22:06
JLB
P91<0392
Methylene Chloride
BRL
mg/kg dry
0.0055
0.00090
1
8260D
11/21/19 22:06
JLB
P91<0392
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0055
0.00078
1
8260D
11/21/19 22:06
JLB
P91<0392
Naphthalene
BRL
mg/kg dry
0.011
0.00056
1
8260D
11/21/19 22:06
JLB
P9K0392
n-Butylbenzene
BRL
mg/kg dry
0.0055
0.00052
1
8260D
11/21/19 22:06
JLB
P9K0392
n-Propylbenzene
BRL
mg/kg dry
0.0055
0.00080
1
8260D
11/21/19 22:06
JLB
P9K0392
o-Xylene
BRL
mg/kg dry
0.0055
0.00059
1
8260D
11/21/19 22:06
JLB
P9K0392
sec-Butylbenzene
BRL
mg/kg dry
0.0055
0.00060
1
8260D
11/21/19 22:06
JLB
P9K0392
Styrene
BRL
mg/kg dry
0.0055
0.00054
1
8260D
11/21/19 22:06
JLB
P9K0392
tert-Butylbenzene
BRL
mg/kg dry
0.0055
0.00066
1
8260D
11/21/19 22:06
JLB
P91<0392
Tetrachloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260D
11/21/19 22:06
JLB
P91<0392
Toluene
BRL
mg/kg dry
0.0055
0.00088
1
8260D
11/21/19 22:06
JLB
P91<0392
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0011
1
8260D
11/21/19 22:06
JLB
P91<0392
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00047
1
8260D
11/21/19 22:06
JLB
P91<0392
Trichloroethylene
BRL
mg/kg dry
0.0055
0.0011
1
8260D
11/21/19 22:06
JLB
P91<0392
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
11/21/19 22:06
JLB
P9K0392
Vinyl acetate
BRL
mg/kg dry
0.011
0.00060
1
8260D
11/21/19 22:06
JLB
P9K0392
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
11/21/19 22:06
JLB
P9K0392
Xylenes, total
BRL
mg/kg dry
0.017
0.0020
1
8260D
11/21/19 22:06
JLB
P9K0392
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
104 %
70-130
Dibromofluoromethane
109 %
84-123
Toluene-d8
99 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

�► E
P R I S M Service Analytical
Environmental Solutions
LABORATORIES, I -
Level II QC Report
11/25/19
Geoscience Group Project: Sedgefield Prism Work Order: 9110276
Attn: Tom Hassett Time Submitted: 11/14/2019 3:22:OOPM
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911<0392 - 5035
Blank (P9K0392-BLK1)
Prepared &Analyzed: 11/21/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13

Level II QC Report
Ape I S n n Full -Service Analytical 11 /25/19
' V' Environmental Solutionss
�W'LA 0O 0RIE& ING
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Sedgefield
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9KO392 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110276
Time Submitted: 11/14/2019 3:22:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9K0392-BLK1)
Prepared &Analyzed: 11/21/19
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
51.8
ug/L
50.00
104
70-130
Surrogate: Dibromofluoromethane
50.8
ug/L
50.00
102
84-123
Surrogate: Toluene-d8
50.0
ug/L
50.00
100
76-129
LCS (P9KO392-BS1)
Prepared &Analyzed: 11/21/19
1,1,1,2-Tetrachloroethane
0.0431
0.0050
mg/kg wet
0.05000
86
72-115
1,1,1-Trichloroethane
0.0438
0.0050
mg/kg wet
0.05000
88
67-131
1,1,2,2-Tetrachloroethane
0.0411
0.0050
mg/kg wet
0.05000
82
56-126
1,1,2-Trichloroethane
0.0420
0.0050
mg/kg wet
0.05000
84
70-133
1,1-Dichloroethane
0.0432
0.0050
mg/kg wet
0.05000
86
74-127
1,1-Dichloroethylene
0.0413
0.0050
mg/kg wet
0.05000
83
67-149
1, 1 -Dichloropropylene
0.0452
0.0050
mg/kg wet
0.05000
90
71-130
1,2,3-Trichlorobenzene
0.0421
0.010
mg/kg wet
0.05000
84
68-130
1,2,3-Trichloropropane
0.0418
0.0050
mg/kg wet
0.05000
84
60-137
1,2,4-Trichlorobenzene
0.0430
0.010
mg/kg wet
0.05000
86
66-125
1,2,4-Trimethylbenzene
0.0434
0.0050
mg/kg wet
0.05000
87
69-129
1,2-Dibromoethane
0.0421
0.0050
mg/kg wet
0.05000
84
70-132
1,2-Dichlorobenzene
0.0415
0.0050
mg/kg wet
0.05000
83
72-123
1,2-Dichloroethane
0.0389
0.0050
mg/kg wet
0.05000
78
68-128
1,2-Dichloropropane
0.0427
0.0050
mg/kg wet
0.05000
85
73-130
1,3,5-Trimethylbenzene
0.0435
0.0050
mg/kg wet
0.05000
87
69-128
1,3-Dichlorobenzene
0.0419
0.0050
mg/kg wet
0.05000
84
71-120
1,3-Dichloropropane
0.0431
0.0050
mg/kg wet
0.05000
86
75-124
1,4-Dichlorobenzene
0.0409
0.0050
mg/kg wet
0.05000
82
71-123
2,2-Dichloropropane
0.0458
0.0050
mg/kg wet
0.05000
92
50-142
2-Chlorotoluene
0.0421
0.0050
mg/kg wet
0.05000
84
67-124
4-Chlorotoluene
0.0421
0.0050
mg/kg wet
0.05000
84
71-126
4-Isopropyltoluene
0.0451
0.0050
mg/kg wet
0.05000
90
68-129
Acetone
0.0770
0.020
mg/kg wet
0.1000
77
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 13

Level II QC Report
Ape I S n n Full -Service Analytical 11 /25/19
' V' Environmental Solutionss
�W'LA 0O 0RIE& ING
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Sedgefield
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9KO392 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110276
Time Submitted: 11/14/2019 3:22:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9K0392-BS1)
Prepared &Analyzed: 11/21/19
Benzene
0.0419
0.0050
mg/kg wet
0.05000
84
74-127
Bromobenzene
0.0420
0.0050
mg/kg wet
0.05000
84
73-125
Bromochloromethane
0.0411
0.0050
mg/kg wet
0.05000
82
72-134
Bromodichloromethane
0.0427
0.0050
mg/kg wet
0.05000
85
75-122
Bromoform
0.0449
0.0050
mg/kg wet
0.05000
90
66-135
Bromomethane
0.0415
0.010
mg/kg wet
0.05000
83
20-180
Carbon Tetrachloride
0.0437
0.0050
mg/kg wet
0.05000
87
64-143
Chlorobenzene
0.0416
0.0050
mg/kg wet
0.05000
83
74-118
Chloroethane
0.0433
0.010
mg/kg wet
0.05000
87
33-149
Chloroform
0.0426
0.0050
mg/kg wet
0.05000
85
73-127
Chloromethane
0.0338
0.010
mg/kg wet
0.05000
68
45-143
cis-1,2-Dichloroethylene
0.0412
0.0050
mg/kg wet
0.05000
82
76-134
cis-1,3-Dichloropropylene
0.0456
0.0050
mg/kg wet
0.05000
91
71-125
Dibromochloromethane
0.0426
0.0050
mg/kg wet
0.05000
85
73-122
Dichlorodifluoromethane
0.0329
0.010
mg/kg wet
0.05000
66
26-146
Ethylbenzene
0.0437
0.0050
mg/kg wet
0.05000
87
74-128
Isopropyl Ether
0.0423
0.0050
mg/kg wet
0.05000
85
59-159
Isopropylbenzene (Cumene)
0.0451
0.0050
mg/kg wet
0.05000
90
68-126
m,p-Xylenes
0.0884
0.010
mg/kg wet
0.1000
88
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0446
0.020
mg/kg wet
0.05000
89
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0412
0.020
mg/kg wet
0.05000
82
63-149
Methyl Isobutyl Ketone
0.0436
0.020
mg/kg wet
0.05000
87
57-162
Methylene Chloride
0.0401
0.0050
mg/kg wet
0.05000
80
74-129
Methyl-tert-Butyl Ether
0.0440
0.0050
mg/kg wet
0.05000
88
70-130
Naphthalene
0.0433
0.010
mg/kg wet
0.05000
87
57-157
n-Butylbenzene
0.0451
0.0050
mg/kg wet
0.05000
90
65-135
n-Propylbenzene
0.0433
0.0050
mg/kg wet
0.05000
87
67-130
o-Xylene
0.0438
0.0050
mg/kg wet
0.05000
88
74-126
sec-Butylbenzene
0.0447
0.0050
mg/kg wet
0.05000
89
66-131
Styrene
0.0452
0.0050
mg/kg wet
0.05000
90
77-121
tert-Butyl benzene
0.0448
0.0050
mg/kg wet
0.05000
90
67-132
Tetrachloroethylene
0.0446
0.0050
mg/kg wet
0.05000
89
68-130
Toluene
0.0428
0.0050
mg/kg wet
0.05000
86
71-129
trans- 1,2-Dichloroethylene
0.0413
0.0050
mg/kg wet
0.05000
83
73-132
trans- 1,3-Dichloropropylene
0.0452
0.0050
mg/kg wet
0.05000
90
68-123
Trichloroethylene
0.0418
0.0050
mg/kg wet
0.05000
84
75-133
Trichlorofluoromethane
0.0410
0.010
mg/kg wet
0.05000
82
44-146
Vinyl acetate
0.0468
0.010
mg/kg wet
0.05000
94
85-161
Vinyl chloride
0.0425
0.010
mg/kg wet
0.05000
85
48-147
Xylenes, total
0.132
0.015
mg/kg wet
0.1500
88
74-126
Surrogate:4-Bromofluorobenzene
49.8
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
48.9
ug/L
50.00
98
84-123
Surrogate: Toluene-d8
49.9
ug/L
50.00
100
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 13

Level II QC Report
Ape I S n n Full -Service Analytical 11 /25/19
' V' Environmental Solutionss
�W'LA 0O 0RIE& ING
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Sedgefield
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9110276
Time Submitted: 11/14/2019 3:22:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO392 - 5035
LCS Dup (P9KO392-BSD1)
Prepared &Analyzed: 11/21/19
1,1,1,2-Tetrachloroethane
0.0458
0.0050
mg/kg wet
0.05000
92
72-115
6
20
1,1,1-Trichloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
67-131
4
20
1,1,2,2-Tetrachloroethane
0.0433
0.0050
mg/kg wet
0.05000
87
56-126
5
20
1,1,2-Trichloroethane
0.0445
0.0050
mg/kg wet
0.05000
89
70-133
6
20
1,1-Dichloroethane
0.0455
0.0050
mg/kg wet
0.05000
91
74-127
5
20
1,1-Dichloroethylene
0.0430
0.0050
mg/kg wet
0.05000
86
67-149
4
20
1, 1 -Dichloropropylene
0.0470
0.0050
mg/kg wet
0.05000
94
71-130
4
20
1,2,3-Trichlorobenzene
0.0453
0.010
mg/kg wet
0.05000
91
68-130
7
20
1,2,3-Trichloropropane
0.0435
0.0050
mg/kg wet
0.05000
87
60-137
4
20
1,2,4-Trichlorobenzene
0.0456
0.010
mg/kg wet
0.05000
91
66-125
6
20
1,2,4-Trimethylbenzene
0.0459
0.0050
mg/kg wet
0.05000
92
69-129
6
20
1,2-Dibromoethane
0.0446
0.0050
mg/kg wet
0.05000
89
70-132
6
20
1,2-Dichlorobenzene
0.0445
0.0050
mg/kg wet
0.05000
89
72-123
7
20
1,2-Dichloroethane
0.0421
0.0050
mg/kg wet
0.05000
84
68-128
8
20
1,2-Dichloropropane
0.0462
0.0050
mg/kg wet
0.05000
92
73-130
8
20
1,3,5-Trimethylbenzene
0.0459
0.0050
mg/kg wet
0.05000
92
69-128
6
20
1,3-Dichlorobenzene
0.0441
0.0050
mg/kg wet
0.05000
88
71-120
5
20
1,3-Dichloropropane
0.0456
0.0050
mg/kg wet
0.05000
91
75-124
6
20
1,4-Dichlorobenzene
0.0439
0.0050
mg/kg wet
0.05000
88
71-123
7
20
2,2-Dichloropropane
0.0476
0.0050
mg/kg wet
0.05000
95
50-142
4
20
2-Chlorotoluene
0.0444
0.0050
mg/kg wet
0.05000
89
67-124
5
20
4-Chlorotoluene
0.0447
0.0050
mg/kg wet
0.05000
89
71-126
6
20
4-Isopropyltoluene
0.0468
0.0050
mg/kg wet
0.05000
94
68-129
4
20
Acetone
0.0779
0.020
mg/kg wet
0.1000
78
29-198
1
20
Benzene
0.0450
0.0050
mg/kg wet
0.05000
90
74-127
7
20
Bromobenzene
0.0448
0.0050
mg/kg wet
0.05000
90
73-125
6
20
Bromochloromethane
0.0446
0.0050
mg/kg wet
0.05000
89
72-134
8
20
Bromodichloromethane
0.0462
0.0050
mg/kg wet
0.05000
92
75-122
8
20
Bromoform
0.0475
0.0050
mg/kg wet
0.05000
95
66-135
6
20
Bromomethane
0.0443
0.010
mg/kg wet
0.05000
89
20-180
7
20
Carbon Tetrachloride
0.0458
0.0050
mg/kg wet
0.05000
92
64-143
5
20
Chlorobenzene
0.0441
0.0050
mg/kg wet
0.05000
88
74-118
6
20
Chloroethane
0.0457
0.010
mg/kg wet
0.05000
91
33-149
5
20
Chloroform
0.0455
0.0050
mg/kg wet
0.05000
91
73-127
7
20
Chloromethane
0.0354
0.010
mg/kg wet
0.05000
71
45-143
5
20
cis-1,2-Dichloroethylene
0.0439
0.0050
mg/kg wet
0.05000
88
76-134
6
20
cis-1,3-Dichloropropylene
0.0489
0.0050
mg/kg wet
0.05000
98
71-125
7
20
Dibromochloromethane
0.0458
0.0050
mg/kg wet
0.05000
92
73-122
7
20
Dichlorodifluoromethane
0.0342
0.010
mg/kg wet
0.05000
68
26-146
4
20
Ethylbenzene
0.0459
0.0050
mg/kg wet
0.05000
92
74-128
5
20
Isopropyl Ether
0.0457
0.0050
mg/kg wet
0.05000
91
59-159
8
20
Isopropylbenzene (Cumene)
0.0474
0.0050
mg/kg wet
0.05000
95
68-126
5
20
m,p-Xylenes
0.0929
0.010
mg/kg wet
0.1000
93
75-124
5
20
Methyl Butyl Ketone (2-Hexanone)
0.0438
0.020
mg/kg wet
0.05000
88
61-157
2
20
Methyl Ethyl Ketone (2-Butanone)
0.0394
0.020
mg/kg wet
0.05000
79
63-149
5
20
Methyl Isobutyl Ketone
0.0440
0.020
mg/kg wet
0.05000
88
57-162
1
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13

P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, I -
Level II QC Report
11/25/19
Geoscience Group Project: Sedgefield Prism Work Order: 9110276
Attn: Tom Hassett Time Submitted: 11/14/2019 3:22:OOPM
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO392 - 5035
LCS Dup (P9K0392-BSD1)
Prepared & Analyzed: 11/21/19
Methylene Chloride
0.0425
0.0050
mg/kg wet
0.05000
85
74-129
6
20
Methyl-tert-Butyl Ether
0.0474
0.0050
mg/kg wet
0.05000
95
70-130
7
20
Naphthalene
0.0455
0.010
mg/kg wet
0.05000
91
57-157
5
20
n-Butylbenzene
0.0469
0.0050
mg/kg wet
0.05000
94
65-135
4
20
n-Propylbenzene
0.0452
0.0050
mg/kg wet
0.05000
90
67-130
4
20
o-Xylene
0.0464
0.0050
mg/kg wet
0.05000
93
74-126
6
20
sec-Butylbenzene
0.0468
0.0050
mg/kg wet
0.05000
94
66-131
4
20
Styrene
0.0482
0.0050
mg/kg wet
0.05000
96
77-121
6
20
tert-Butylbenzene
0.0471
0.0050
mg/kg wet
0.05000
94
67-132
5
20
Tetrachloroethylene
0.0464
0.0050
mg/kg wet
0.05000
93
68-130
4
20
Toluene
0.0453
0.0050
mg/kg wet
0.05000
91
71-129
6
20
trans-1,2-Dichloroethylene
0.0435
0.0050
mg/kg wet
0.05000
87
73-132
5
20
trans- 1,3-Dichloropropylene
0.0491
0.0050
mg/kg wet
0.05000
98
68-123
8
20
Trichloroethylene
0.0442
0.0050
mg/kg wet
0.05000
88
75-133
6
20
Trichlorofluoromethane
0.0423
0.010
mg/kg wet
0.05000
85
44-146
3
20
Vinyl acetate
0.0501
0.010
mg/kg wet
0.05000
100
85-161
7
20
Vinyl chloride
0.0440
0.010
mg/kg wet
0.05000
88
48-147
4
20
Xylenes, total
0.139
0.015
mg/kg wet
0.1500
93
74-126
5
20
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
49.8
ug/L
50.00
100
84-123
Surrogate: Toluene-d8
50.0
ug/L
50.00
100
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 13

P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, I -
Level II QC Report
11/25/19
Geoscience Group Project: Sedgefield Prism Work Order: 9110276
Attn: Tom Hassett Time Submitted: 11/14/2019 3:22:OOPM
500-K Clanton Rd.
Charlotte, NC 28217
Gasoline Range Organics by GC/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - 5030B
Blank (1291<0286-BLK1)
Prepared &Analyzed: 11/18/19
Gasoline Range Organics
BRL
5.0
mg/kg wet
Surrogate: a,a,a-Trifluorotoluene
5.30
mg/kg wet
5.000 106
50-137
LCS (P9K0286-BSI)
Prepared &Analyzed: 11/18/19
Gasoline Range Organics
64.0
5.0
mg/kg wet
50.00 128
41-138
Surrogate: a,a,a-Trifluorotoluene
6.10
mg/kg wet
5.000 122
50-137
LCS Dup (P9K0286-BSD1)
Prepared & Analyzed: 11/18/19
Gasoline Range Organics
66.2
5.0
mg/kg wet
50.00 132
41-138 3 20
Surrogate: a,a,a-Trifluorotoluene
5.60
mg/kg wet
5.000 112
50-137
Matrix Spike (P9K0286-MSI)
Source: 9110276-01
Prepared &Analyzed: 11/18/19
Gasoline Range Organics
88.1
7.6
mg/kg dry
75.72 6.09 108
41-138
Surrogate: a,a,a-Trifluorotoluene
7.04
mg/kg dry
7.572 93
50-137
Matrix Spike Dup (P9K0286-MSD1)
Source: 9110276-01
Prepared & Analyzed: 11/18/19
Gasoline Range Organics
87.6
7.6
mg/kg dry
75.72 6.09 108
41-138 0.5 34
Surrogate: a,a,a-Trifluorotoluene
7.72
mg/kg dry
7.572 102
50-137
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13

Level II QC Report
P R I S M Full -Service Analytical 11/25/19
Environmental Solutions
LABORATORIES, ING.
Geoscience Group Project: Sedgefield Prism Work Order: 9110276
Attn: Tom Hassett Time Submitted: 11/14/2019 3:22:OOPM
500-K Clanton Rd.
Charlotte, NC 28217
Diesel Range Organics by GC/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO322 - 3546
Blank (P9K0322-BLK1)
Prepared: 11/18/19 Analyzed: 11/20/19
Diesel Range Organics
BRL
7.0 mg/kg wet
Surrogate: o-Terphenyl
1.07
mg/kg wet
1.333 80 31-123
LCS (P9K0322-BSI)
Prepared: 11/18/19 Analyzed: 11/20/19
Diesel Range Organics
49.5
7.0 mg/kg wet
66.40 75 46-126
Surrogate: o-Terphenyl
1.02
mg/kg wet
1.328 77 31-123
LCS Dup (P9K0322-BSD1)
Prepared: 11/18/19 Analyzed: 11/20/19
Diesel Range Organics
54.5
7.0 mg/kg wet
66.60 82 46-126 10 20
Surrogate: o-Terphenyl
1.19
mg/kg wet
1.332 89 31-123
Matrix Spike (P9K0322-MSI)
Source: 9110276-01
Prepared: 11/18/19 Analyzed: 11/20/19
Diesel Range Organics
1250
11 mg/kg dry
100.7 379 868 50-117 M
Surrogate: o-Terphenyl
9.02
mg/kg dry
2.014 448 31-123 SR
Matrix Spike Dup (P9K0322-MSD1)
Source: 9110276-01
Prepared: 11/18/19 Analyzed: 11/20/19
Diesel Range Organics
346
11 mg/kg dry
100.8 379 NR 50-117 114 24 M
Surrogate: o-Terphenyl
1.36
mg/kg dry
2.017 68 31-123
Sample Extraction
Data
Prep Method: 3546
Lab Number Batch
Initial
Final
Date/Time
9110276-01 P91<0322
30.01 g
1 mL
11/18/19 11:45
Prep Method: 5030E
Lab Number Batch
Initial
Final
Date/Time
9110276-01 P91<0286
4.66 mL
5 mL
11/18/19 8:11
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
9110276-01 P91<0327
30 g
30 g
11/18/19 15:34
Prep Method: 5035
Lab Number Batch
Initial
Final
Date/Time
9110276-01 P91<0392
6.84 g
5 mL
11/21/19 10:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 0f 13

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Page 13 of 13

Case Narrative
Waypoint.
ANALYTICAL
Geoscience Group
Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Sedgefield
Lab Submittal Date: 01/23/2020
Work Order: 0010326
2/6/20 11:44
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a'J
Angela D. Overcash
Senior Project Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash
Senior Project Manager
A Fractionation Surrogate is below range. Sample refractionated with similar results. Sample matrix suspected.
CCVL CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and
found acceptable. Result is reported but considered estimated.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Receipt Summary
Way�j;/
n
02/06/2020
poi� .
Work Order: 0010326
L
ANALYTICAL
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
S-1
0010326-01
Solid
01/23/20 0:00 01/23/20 11:54
S-2
0010326-02
Solid
01/23/20 0:00 01/23/20 11:54
S-3
0010326-03
Solid
01/23/20 0:00 01/23/20 11:54
S-4
0010326-04
Solid
01/23/20 0:00 01/23/20 11:54
S-5
0010326-05
Solid
01/23/20 0:00 01/23/20 11:54
S-6
0010326-06
Solid
01/23/20 0:00 01/23/20 11:54
Samples were received in good condition at 5.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYTICAL
Summary of Detections
02/06/2020
Work Order: 0010326
Waypoint ID
Client ID
Parameter
Method
Result
Units
0010326-02
S-2
C9-CI8 Aliphatics
MADEP EPH
1900
mg/kg dry
0010326-02
S-2
C19-C36 Aliphatics
MADEP EPH
470
mg/kg dry
0010326-02
S-2
C11-C22 Aromatics
MADEP EPH
860
mg/kg dry
0010326-02
S-2
1-Methylnaphthalene
8270E
6.0
mg/kg dry
0010326-02
S-2
2-Methylnaphthalene
8270E
8.2
mg/kg dry
0010326-02
S-2
Acenaphthene
8270E
1.0
mg/kg dry
0010326-02
S-2
Naphthalene
8270E
0.58 J
mg/kg dry
0010326-02
S-2
Phenanthrene
8270E
6.7
mg/kg dry
0010326-02
S-2
1,2,4-Trimethylbenzene
8260D
0.21
mg/kg dry
0010326-02
S-2
1,3,5-Trimethylbenzene
8260D
0.019
mg/kg dry
0010326-02
S-2
4-Isopropyltoluene
8260D
0.026
mg/kg dry
0010326-02
S-2
Acetone
8260D
0.21
mg/kg dry
0010326-02
S-2
Ethylbenzene
8260D
0.0081
mg/kg dry
0010326-02
S-2
I sopropyl benzene (Cumene)
8260D
0.016
mg/kg dry
0010326-02
S-2
m,p-Xylenes
8260D
0.029
mg/kg dry
0010326-02
S-2
Methyl Ethyl Ketone (2-Butanone)
8260D
0.037 CCVL
mg/kg dry
0010326-02
S-2
Naphthalene
8260D
0.055
mg/kg dry
0010326-02
S-2
n-Butylbenzene
8260D
0.034
mg/kg dry
0010326-02
S-2
n-Propylbenzene
8260D
0.035
mg/kg dry
0010326-02
S-2
o-Xylene
8260D
0.015
mg/kg dry
0010326-02
S-2
sec -Butyl benzene
8260D
0.031
mg/kg dry
0010326-02
S-2
tert-Butylbenzene
8260D
0.0051 J
mg/kg dry
0010326-02
S-2
Xylenes, total
8260D
0.045
mg/kg dry
0010326-02
S-2
C9-C12 Aliphatics
MADEP VPH
160
mg/kg dry
0010326-02
S-2
C9-C10 Aromatics
MADEP VPH
42
mg/kg dry
0010326-04
S-4
Acetone
8260D
0.038
mg/kg dry
0010326-05
S-5
C9-Cl8 Aliphatics
MADEP EPH
1.8 J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint.
ANALYTICAL
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Parameter
Laboratory Report
02/06/2020
Project: Sedgefield Client Sample ID: S-1A
Sample ID: 0010326-01
Work Order: 0010326
Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL
mg/kg dry
9.2 3.1
1 *8015C 1/31/20 2:35
ZRC POA0462
Surrogate
Recovery
Control Limits
o-Terphenyl
78 %
31-123
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL
mg/kg dry
8.4 2.3
50 *8015C 1/29/20 16:09
TBL POA0483
Surrogate
Recovery
Control Limits
a,a,a-Trifluorotoluene
88 %
50-137
General Chemistry Parameters
% Solids 75.5
% by
0.100 0.100
1 *SM2540 G 2/3/20 8:20
EDV POA0526
Weight
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-2
Attn: Tom Hassett Sample ID: 0010326-02
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report MDL
Limit
Dilution
Factor
Method Analysis
Date/Time
Analyst
Batch
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
1900
mg/kg dry
37 1.9
1
MADEP EPH 1/29/20 17:40
ZRC
POA0439
C19-C36 Aliphatics
470
mg/kg dry
37 6.3
1
MADEP EPH 1/29/20 17:40
ZRC
POA0439
C11-C22 Aromatics
860
mg/kg dry
37 10
1
MADEP EPH 1129/20 17:40
ZRC
POA0439
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
57 %
40-140
o-Terphenyl
72 %
40-140
2-Fluorobiphenyl
95 %
40-140
2-Bromonaphthalene
69 %
40-140
General Chemistry Parameters
% Solids
67.1
% by
0.100
0.100
1
'SM2540 G
213120 8:20
EDV
POA0526
Weight
Semivolatile Organic Compounds by GUMS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.98
0.17
1
8270E
1/31/20 13:12
JMV
POA0489
1,2-Dichlorobenzene
BRL
mg/kg dry
0.98
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
1,3-Dichlorobenzene
BRL
mg/kg dry
0.98
0.14
1
8270E
1/31/20 13:12
JMV
POA0489
1,4-Dichlorobenzene
BRL
mg/kg dry
0.49
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
1-Methyl naphthalene
6.0
mg/kg dry
0.98
0.015
1
8270E
1/31/20 13:12
JMV
POA0489
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.98
0.21
1
8270E
1/31/20 13:12
JMV
POA0489
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.98
0.24
1
8270E
1/31/20 13:12
JMV
POA0489
2,4-Dichlorophenol
BRL
mg/kg dry
0.98
0.19
1
8270E
1/31/20 13:12
JMV
POA0489
2,4-Dimethylphenol
BRL
mg/kg dry
0.49
0.20
1
8270E
1/31/20 13:12
JMV
POA0489
2,4-Dinitrophenol
BRL
mg/kg dry
2.2
0.58
1
8270E
1/31/20 13:12
JMV
POA0489
2,4-Dinitrotoluene
BRL
mg/kg dry
0.98
0.26
1
8270E
1/31/20 13:12
JMV
POA0489
2,6-Dinitrotoluene
BRL
mg/kg dry
0.98
0.25
1
8270E
1/31/20 13:12
JMV
POA0489
2-Chloronaphthalene
BRL
mg/kg dry
0.98
0.24
1
8270E
1/31/20 13:12
JMV
POA0489
2-Chlorophenol
BRL
mg/kg dry
0.98
0.19
1
8270E
1/31/20 13:12
JMV
POA0489
2-Methyl naphthalene
8.2
mg/kg dry
0.98
0.019
1
8270E
1/31/20 13:12
JMV
POA0489
2-Methylphenol
BRL
mg/kg dry
0.98
0.19
1
8270E
1/31/20 13:12
JMV
POA0489
2-Nitrophenol
BRL
mg/kg dry
0.98
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.98
0.20
1
8270E
1/31/20 13:12
JMV
POA0489
3/4-Methyl phenol
BRL
mg/kg dry
0.98
0.21
1
8270E
1/31/20 13:12
JMV
POA0489
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.2
0.54
1
8270E
1/31/20 13:12
JMV
POA0489
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.98
0.23
1
8270E
1/31/20 13:12
JMV
POA0489
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.98
0.19
1
8270E
1/31/20 13:12
JMV
POA0489
4-Chloroaniline
BRL
mg/kg dry
0.49
0.12
1
8270E
1/31/20 13:12
JMV
POA0489
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.30
1
8270E
1/31/20 13:12
JMV
POA0489
4-Nitrophenol
BRL
mg/kg dry
0.98
0.24
1
8270E
1/31/20 13:12
JMV
POA0489
Acenaphthene
1.0
mg/kg dry
0.98
0.023
1
8270E
1/31/20 13:12
JMV
POA0489
Acenaphthylene
BRL
mg/kg dry
0.98
0.019
1
8270E
1/31/20 13:12
JMV
POA0489
Anthracene
BRL
mg/kg dry
0.98
0.011
1
8270E
1/31/20 13:12
JMV
POA0489
Azobenzene
BRL
mg/kg dry
0.98
0.21
1
8270E
1/31/20 13:12
JMV
POA0489
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-2
Attn: Tom Hassett Sample ID: 0010326-02
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)anthracene
BRL
mg/kg dry
0.98
0.012
1
8270E
1/31/20 13:12
JMV
POA0489
Benzo(a)pyrene
BRL
mg/kg dry
0.98
0.0088
1
8270E
1/31/20 13:12
JMV
POA0489
Benzo(b)fluoranthene
BRL
mg/kg dry
0.98
0.0091
1
8270E
1/31/20 13:12
JMV
POA0489
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.98
0.0097
1
8270E
1/31/20 13:12
JMV
POA0489
Benzo(k)fluoranthene
BRL
mg/kg dry
0.98
0.010
1
8270E
1/31/20 13:12
JMV
POA0489
Benzoic Acid
BRL
mg/kg dry
3.0
0.82
1
8270E
1/31/20 13:12
JMV
POA0489
Benzyl alcohol
BRL
mg/kg dry
0.98
0.18
1
8270E
1/31/20 13:12
JMV
POA0489
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.98
0.19
1
8270E
1/31/20 13:12
JMV
POA0489
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.98
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.49
0.18
1
8270E
1/31/20 13:12
JMV
POA0489
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.98
0.22
1
8270E
1/31/20 13:12
JMV
POA0489
Butyl benzyl phthalate
BRL
mg/kg dry
0.49
0.17
1
8270E
1/31/20 13:12
JMV
POA0489
Chrysene
BRL
mg/kg dry
0.98
0.012
1
8270E
1/31/20 13:12
JMV
POA0489
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.98
0.028
1
8270E
1/31/20 13:12
JMV
POA0489
Dibenzofuran
BRL
mg/kg dry
0.98
0.27
1
8270E
1/31/20 13:12
JMV
POA0489
Diethyl phthalate
BRL
mg/kg dry
0.98
0.25
1
8270E
1/31/20 13:12
JMV
POA0489
Dimethyl phthalate
BRL
mg/kg dry
0.98
0.24
1
8270E
1/31/20 13:12
JMV
POA0489
Di-n-butyl phthalate
BRL
mg/kg dry
0.98
0.24
1
8270E
1/31/20 13:12
JMV
POA0489
Di-n-octyl phthalate
BRL
mg/kg dry
0.49
0.25
1
8270E
1/31/20 13:12
JMV
POA0489
Fluoranthene
BRL
mg/kg dry
0.98
0.011
1
8270E
1/31/20 13:12
JMV
POA0489
Fluorene
BRL
mg/kg dry
0.98
0.017
1
8270E
1/31/20 13:12
JMV
POA0489
Hexachlorobenzene
BRL
mg/kg dry
0.98
0.22
1
8270E
1/31/20 13:12
JMV
POA0489
Hexachlorobutadiene
BRL
mg/kg dry
0.98
0.22
1
8270E
1/31/20 13:12
JMV
POA0489
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.98
0.34
1
8270E
1/31/20 13:12
JMV
POA0489
Hexachloroethane
BRL
mg/kg dry
0.98
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.98
0.028
1
8270E
1/31/20 13:12
JMV
POA0489
Isophorone
BRL
mg/kg dry
0.98
0.21
1
8270E
1/31/20 13:12
JMV
POA0489
Naphthalene
0.58 J
mg/kg dry
0.98
0.021
1
8270E
1/31/20 13:12
JMV
POA0489
Nitrobenzene
BRL
mg/kg dry
0.49
0.21
1
8270E
1/31/20 13:12
JMV
POA0489
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.98
0.23
1
8270E
1/31/20 13:12
JMV
POA0489
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.98
0.27
1
8270E
1/31/20 13:12
JMV
POA0489
Pentachlorophenol
BRL
mg/kg dry
1.5
0.63
1
8270E
1/31/20 13:12
JMV
POA0489
Phenanthrene
6.7
mg/kg dry
0.98
0.011
1
8270E
1131/20 13:12
JMV
POA0489
Phenol
BRL
mg/kg dry
0.98
0.16
1
8270E
1/31/20 13:12
JMV
POA0489
Pyrene
BRL
mg/kg dry
0.98
0.014
1
8270E
1/31/20 13:12
JMV
POA0489
Pyridine
BRL
mg/kg dry
0.49
0.094
1
8270E
1/31/20 13:12
JMV
POA0489
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
80 %
39-132
2-Fluorobiphenyl
72 %
44-115
2-Fluorophenol
66 %
35-115
Nitrobenzene-d5
98 %
37-122
Phenol-d5
62 %
34-121
Terphenyl-d14
70 %
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-2
Attn: Tom Hassett Sample ID: 0010326-02
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0081
0.00099
1
8260D
2/3/20 22:34
TLB
POB0017
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0081
0.0012
1
8260D
2/3/20 22:34
TLB
POB0017
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0081
0.00059
1
8260D
2/3/20 22:34
TLB
POB0017
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0081
0.00088
1
8260D
2/3/20 22:34
TLB
POB0017
1,1-Dichloroethane
BRL
mg/kg dry
0.0081
0.0015
1
8260D
2/3/20 22:34
TLB
POB0017
1,1-Dichloroethylene
BRL
mg/kg dry
0.0081
0.0015
1
8260D
2/3/20 22:34
TLB
POB0017
1,1-Dichloropropylene
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.016
0.0012
1
8260D
2/3/20 22:34
TLB
POB0017
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0081
0.00092
1
8260D
2/3/20 22:34
TLB
POB0017
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.016
0.00077
1
8260D
2/3/20 22:34
TLB
POB0017
1,2,4-Trimethylbenzene
0.21
mg/kg dry
0.0081
0.00086
1
8260D
2/3/20 22:34
TLB
POB0017
1,2-Dibromoethane
BRL
mg/kg dry
0.0081
0.00073
1
8260D
2/3/20 22:34
TLB
POB0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0081
0.00091
1
8260D
2/3/20 22:34
TLB
POB0017
1,2-Dichloroethane
BRL
mg/kg dry
0.0081
0.00097
1
8260D
2/3/20 22:34
TLB
POB0017
1,2-Dichloropropane
BRL
mg/kg dry
0.0081
0.0012
1
8260D
2/3/20 22:34
TLB
POB0017
1,3,5-Trimethylbenzene
0.019
mg/kg dry
0.0081
0.0010
1
8260D
2/3/20 22:34
TLB
POB0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0081
0.0010
1
8260D
2/3/20 22:34
TLB
POB0017
1,3-Dichloropropane
BRL
mg/kg dry
0.0081
0.00068
1
8260D
2/3/20 22:34
TLB
POB0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0081
0.0010
1
8260D
2/3/20 22:34
TLB
POB0017
2,2-Dichloropropane
BRL
mg/kg dry
0.0081
0.0010
1
8260D
2/3/20 22:34
TLB
POB0017
2-Chlorotoluene
BRL
mg/kg dry
0.0081
0.0011
1
8260D
2/3/20 22:34
TLB
POB0017
4-Chlorotoluene
BRL
mg/kg dry
0.0081
0.00092
1
8260D
2/3/20 22:34
TLB
POB0017
4-Isopropyltoluene
0.026
mg/kg dry
0.0081
0.0020
1
8260D
2/3/20 22:34
TLB
POB0017
Acetone
0.21
mg/kg dry
0.032
0.0021
1
8260D
2/3/20 22:34
TLB
POB0017
Benzene
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
Bromobenzene
BRL
mg/kg dry
0.0081
0.0011
1
8260D
2/3/20 22:34
TLB
POB0017
Bromochloromethane
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
Bromodichloromethane
BRL
mg/kg dry
0.0081
0.00077
1
8260D
2/3/20 22:34
TLB
POB0017
Bromoform
BRL
mg/kg dry
0.0081
0.00063
1
8260D
2/3/20 22:34
TLB
POB0017
Bromomethane
BRL CCVL
mg/kg dry
0.016
0.0040
1
8260D
2/3/20 22:34
TLB
POB0017
Carbon Tetrachloride
BRL
mg/kg dry
0.0081
0.0016
1
8260D
2/3/20 22:34
TLB
POB0017
Chlorobenzene
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
Chloroethane
BRL
mg/kg dry
0.016
0.0015
1
8260D
2/3/20 22:34
TLB
POB0017
Chloroform
BRL
mg/kg dry
0.0081
0.00099
1
8260D
2/3/20 22:34
TLB
POB0017
Chloromethane
BRL
mg/kg dry
0.016
0.0025
1
8260D
2/3/20 22:34
TLB
POB0017
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0081
0.00080
1
8260D
2/3/20 22:34
TLB
POB0017
Dibromochloromethane
BRL
mg/kg dry
0.0081
0.00054
1
8260D
2/3/20 22:34
TLB
POB0017
Dichlorodifluoromethane
BRL
mg/kg dry
0.016
0.0023
1
8260D
2/3/20 22:34
TLB
POB0017
Ethylbenzene
0.0081
mg/kg dry
0.0081
0.0012
1
8260D
2/3/20 22:34
TLB
POB0017
Isopropyl Ether
BRL
mg/kg dry
0.0081
0.0012
1
8260D
2/3/20 22:34
TLB
POB0017
Isopropyl benzene (Cumene)
0.016
mg/kg dry
0.0081
0.00095
1
8260D
2/3/20 22:34
TLB
POB0017
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waypoint.
02/06/2020
ANALYTICAL
Geoscience Group
Project: Sedgefield
Client Sample ID: S-2
Attn: Tom Hassett
Sample ID: 0010326-02
500-K Clanton Rd.
Work Order: 0010326
Charlotte, NC 28217
Sample Matrix: Solid
Time Collected:
01/23/20 00:00
Time Submitted:
01/23/20 11:54
Parameter
Result Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
0.029
mg/kg dry
0.016
0.0021
1
8260D
2/3/20 22:34
TLB
POB0017
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.032
0.00056
1
8260D
2/3/20 22:34
TLB
POB0017
Methyl Ethyl Ketone (2-Butanone)
0.037
CCVL mg/kg dry
0.032
0.0019
1
8260D
2/3/20 22:34
TLB
POB0017
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.032
0.00066
1
8260D
2/3/20 22:34
TLB
POB0017
Methylene Chloride
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0081
0.0011
1
8260D
2/3/20 22:34
TLB
POB0017
Naphthalene
0.055
mg/kg dry
0.016
0.00082
1
8260D
2/3/20 22:34
TLB
POB0017
n-Butylbenzene
0.034
mg/kg dry
0.0081
0.00076
1
8260D
2/3/20 22:34
TLB
POB0017
n-Propylbenzene
0.035
mg/kg dry
0.0081
0.0012
1
8260D
2/3120 22:34
TLB
POB0017
o-Xylene
0.015
mg/kg dry
0.0081
0.00086
1
8260D
2/3/20 22:34
TLB
POB0017
sec-Butylbenzene
0.031
mg/kg dry
0.0081
0.00088
1
8260D
2/3/20 22:34
TLB
POB0017
Styrene
BRL
mg/kg dry
0.0081
0.00079
1
8260D
2/3/20 22:34
TLB
POB0017
tert-Butylbenzene
0.0051
J mg/kg dry
0.0081
0.00096
1
8260D
2/3/20 22:34
TLB
POB0017
Tetrachloroethylene
BRL
mg/kg dry
0.0081
0.0015
1
8260D
2/3/20 22:34
TLB
POB0017
Toluene
BRL
mg/kg dry
0.0081
0.0013
1
8260D
2/3/20 22:34
TLB
POB0017
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0081
0.0016
1
8260D
2/3/20 22:34
TLB
POB0017
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0081
0.00070
1
8260D
2/3/20 22:34
TLB
POB0017
Trichloroethylene
BRL
mg/kg dry
0.0081
0.0016
1
8260D
2/3/20 22:34
TLB
POB0017
Trichlorofluoromethane
BRL
mg/kg dry
0.016
0.0022
1
8260D
2/3/20 22:34
TLB
POB0017
Vinyl acetate
BRL
mg/kg dry
0.016
0.00088
1
8260D
2/3/20 22:34
TLB
POB0017
Vinyl chloride
BRL
mg/kg dry
0.016
0.0016
1
8260D
2/3/20 22:34
TLB
POB0017
Xylenes, total
0.045
mg/kg dry
0.024
0.0029
1
8260D
2/3/20 22:34
TLB
POB0017
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
94 %
70-130
Dibromofluoromethane
99 %
84-123
Toluene-d8
102 %
76-129
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8Aliphatics BRL mg/kg dry
27 5.4 100
MADEP VPH 1/29/20 15:53
TBL POA0482
C9-C12 Aliphatics 160 mg/kg dry
27 2.4 100
MADEP VPH 1/29/20 15:53
TBL POA0482
C9-C10 Aromatics 42 mg/kg dry
27 2.6 100
MADEP VPH 1/29/20 15:53
TBL POA0482
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
99 %
70-130
2,5-Dibromotoluene (FID)
116 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-3
Attn: Tom Hassett Sample ID: 0010326-03
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18Aliphatics
BRL
mg/kg dry
38
1.9
1
MADEP EPH
1/29/20 18:16
ZRC
POA0439
C1 9-C36 Aliphatics
BRL
mg/kg dry
38
6.4
1
MADEP EPH
1/29/20 18:16
ZRC
POA0439
C1 1 -C22 Aromatics
BRL
mg/kg dry
38
10
1
MADEP EPH
1/29/20 18:16
ZRC
POA0439
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
72 %
40-140
o-Terphenyl
77 %
40-140
2-Fluorobiphenyl
72 %
40-140
2-Bromonaphthalene
71 %
40-140
General Chemistry Parameters
% Solids
66.1
% by
0.100
0.100
1
*SM2540 G
2/3/20 8:20
EDV
POA0526
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
1.0
0.18
1
8270E
1/31/20 13:34
JMV
POA0489
1,2-Dichlorobenzene
BRL
mg/kg dry
1.0
0.16
1
8270E
1/31/20 13:34
JMV
POA0489
1,3-Dichlorobenzene
BRL
mg/kg dry
1.0
0.15
1
8270E
1/31/20 13:34
JMV
POA0489
1,4-Dichlorobenzene
BRL
mg/kg dry
0.50
0.16
1
8270E
1/31/20 13:34
JMV
POA0489
1-Methyl naphthalene
BRL
mg/kg dry
1.0
0.015
1
8270E
1/31/20 13:34
JMV
POA0489
2,4,5-Trichlorophenol
BRL
mg/kg dry
1.0
0.21
1
8270E
1/31/20 13:34
JMV
POA0489
2,4,6-Trichlorophenol
BRL
mg/kg dry
1.0
0.24
1
8270E
1/31/20 13:34
JMV
POA0489
2,4-Dichlorophenol
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
2,4-Dimethylphenol
BRL
mg/kg dry
0.50
0.21
1
8270E
1/31/20 13:34
JMV
POA0489
2,4-Dinitrophenol
BRL
mg/kg dry
2.3
0.58
1
8270E
1/31/20 13:34
JMV
POA0489
2,4-Dinitrotoluene
BRL
mg/kg dry
1.0
0.26
1
8270E
1/31/20 13:34
JMV
POA0489
2,6-Dinitrotoluene
BRL
mg/kg dry
1.0
0.26
1
8270E
1/31/20 13:34
JMV
POA0489
2-Chloronaphthalene
BRL
mg/kg dry
1.0
0.24
1
8270E
1/31/20 13:34
JMV
POA0489
2-Chlorophenol
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
2-Methyl naphthalene
BRL
mg/kg dry
1.0
0.019
1
8270E
1/31/20 13:34
JMV
POA0489
2-Methylphenol
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
2-Nitrophenol
BRL
mg/kg dry
1.0
0.17
1
8270E
1/31/20 13:34
JMV
POA0489
3,3'-Dichlorobenzidine
BRL
mg/kg dry
1.0
0.20
1
8270E
1/31/20 13:34
JMV
POA0489
3/4-Methyl phenol
BRL
mg/kg dry
1.0
0.22
1
8270E
1/31/20 13:34
JMV
POA0489
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.3
0.55
1
8270E
1/31/20 13:34
JMV
POA0489
4-Bromophenyl phenyl ether
BRL
mg/kg dry
1.0
0.23
1
8270E
1/31/20 13:34
JMV
POA0489
4-Chloro-3-methylphenol
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
4-Chloroaniline
BRL
mg/kg dry
0.50
0.12
1
8270E
1/31/20 13:34
JMV
POA0489
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.31
1
8270E
1/31/20 13:34
JMV
POA0489
4-Nitrophenol
BRL
mg/kg dry
1.0
0.25
1
8270E
1/31/20 13:34
JMV
POA0489
Acenaphthene
BRL
mg/kg dry
1.0
0.023
1
8270E
1/31/20 13:34
JMV
POA0489
Acenaphthylene
BRL
mg/kg dry
1.0
0.020
1
8270E
1/31/20 13:34
JMV
POA0489
Anthracene
BRL
mg/kg dry
1.0
0.011
1
8270E
1/31/20 13:34
JMV
POA0489
Azobenzene
BRL
mg/kg dry
1.0
0.21
1
8270E
1/31/20 13:34
JMV
POA0489
Benzo(a)anthracene
BRL
mg/kg dry
1.0
0.012
1
8270E
1/31/20 13:34
JMV
POA0489
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-3
Attn: Tom Hassett Sample ID: 0010326-03
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
1.0
0.0089
1
8270E
1/31/20 13:34
JMV
POA0489
Benzo(b)fluoranthene
BRL
mg/kg dry
1.0
0.0092
1
8270E
1/31/20 13:34
JMV
POA0489
Benzo(g,h,i)perylene
BRL
mg/kg dry
1.0
0.0098
1
8270E
1/31/20 13:34
JMV
POA0489
Benzo(k)fluoranthene
BRL
mg/kg dry
1.0
0.011
1
8270E
1/31/20 13:34
JMV
POA0489
Benzoic Acid
BRL
mg/kg dry
3.0
0.83
1
8270E
1/31/20 13:34
JMV
POA0489
Benzyl alcohol
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
1.0
0.19
1
8270E
1/31/20 13:34
JMV
POA0489
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
1.0
0.16
1
8270E
1/31/20 13:34
JMV
POA0489
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.50
0.18
1
8270E
1/31/20 13:34
JMV
POA0489
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
1.0
0.23
1
8270E
1/31/20 13:34
JMV
POA0489
Butyl benzyl phthalate
BRL
mg/kg dry
0.50
0.17
1
8270E
1/31/20 13:34
JMV
POA0489
Chrysene
BRL
mg/kg dry
1.0
0.012
1
8270E
1/31/20 13:34
JMV
POA0489
Dibenzo(a,h)anthracene
BRL
mg/kg dry
1.0
0.029
1
8270E
1/31/20 13:34
JMV
POA0489
Dibenzofuran
BRL
mg/kg dry
1.0
0.27
1
8270E
1/31/20 13:34
JMV
POA0489
Diethyl phthalate
BRL
mg/kg dry
1.0
0.26
1
8270E
1/31/20 13:34
JMV
POA0489
Dimethyl phthalate
BRL
mg/kg dry
1.0
0.24
1
8270E
1/31/20 13:34
JMV
POA0489
Di-n-butyl phthalate
BRL
mg/kg dry
1.0
0.25
1
8270E
1/31/20 13:34
JMV
POA0489
Di-n-octyl phthalate
BRL
mg/kg dry
0.50
0.26
1
8270E
1/31/20 13:34
JMV
POA0489
Fluoranthene
BRL
mg/kg dry
1.0
0.011
1
8270E
1/31/20 13:34
JMV
POA0489
Fluorene
BRL
mg/kg dry
1.0
0.017
1
8270E
1/31/20 13:34
JMV
POA0489
Hexachlorobenzene
BRL
mg/kg dry
1.0
0.22
1
8270E
1/31/20 13:34
JMV
POA0489
Hexachlorobutadiene
BRL
mg/kg dry
1.0
0.23
1
8270E
1/31/20 13:34
JMV
POA0489
Hexachlorocyclopentadiene
BRL
mg/kg dry
1.0
0.34
1
8270E
1/31/20 13:34
JMV
POA0489
Hexachloroethane
BRL
mg/kg dry
1.0
0.16
1
8270E
1/31/20 13:34
JMV
POA0489
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
1.0
0.028
1
8270E
1/31/20 13:34
JMV
POA0489
Isophorone
BRL
mg/kg dry
1.0
0.21
1
8270E
1/31/20 13:34
JMV
POA0489
Naphthalene
BRL
mg/kg dry
1.0
0.021
1
8270E
1/31/20 13:34
JMV
POA0489
Nitrobenzene
BRL
mg/kg dry
0.50
0.21
1
8270E
1/31/20 13:34
JMV
POA0489
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
1.0
0.23
1
8270E
1/31/20 13:34
JMV
POA0489
N-Nitrosodiphenylamine
BRL
mg/kg dry
1.0
0.27
1
8270E
1/31/20 13:34
JMV
POA0489
Pentachlorophenol
BRL
mg/kg dry
1.5
0.64
1
8270E
1/31/20 13:34
JMV
POA0489
Phenanthrene
BRL
mg/kg dry
1.0
0.011
1
8270E
1/31/20 13:34
JMV
POA0489
Phenol
BRL
mg/kg dry
1.0
0.16
1
8270E
1/31/20 13:34
JMV
POA0489
Pyrene
BRL
mg/kg dry
1.0
0.014
1
8270E
1/31/20 13:34
JMV
POA0489
Pyridine
BRL
mg/kg dry
0.50
0.095
1
8270E
1/31/20 13:34
JMV
POA0489
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
110 %
39-132
2-Fluorobiphenyl
91 %
44-115
2-Fluorophenol
96 %
35-115
Nitrobenzene-d5
85 %
37-122
Phenol-d5
92 %
34-121
Terphenyl-d14
103 %
54-127
Volatile Organic Compounds by GUMS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-3
Attn: Tom Hassett Sample ID: 0010326-03
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0073
0.00089
1
8260D
2/3/20 19:34
TLB
POB0017
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0073
0.00053
1
8260D
2/3/20 19:34
TLB
POB0017
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0073
0.00079
1
8260D
2/3/20 19:34
TLB
POB0017
1,1-Dichloroethane
BRL
mg/kg dry
0.0073
0.0013
1
8260D
2/3/20 19:34
TLB
POB0017
1,1-Dichloroethylene
BRL
mg/kg dry
0.0073
0.0013
1
8260D
2/3/20 19:34
TLB
POB0017
1,1-Dichloropropylene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.015
0.0010
1
8260D
2/3/20 19:34
TLB
POB0017
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0073
0.00083
1
8260D
2/3/20 19:34
TLB
POB0017
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.015
0.00070
1
8260D
2/3/20 19:34
TLB
POB0017
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0073
0.00077
1
8260D
2/3/20 19:34
TLB
POB0017
1,2-Dibromoethane
BRL
mg/kg dry
0.0073
0.00065
1
8260D
2/3/20 19:34
TLB
POB0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0073
0.00081
1
8260D
2/3/20 19:34
TLB
POB0017
1,2-Dichloroethane
BRL
mg/kg dry
0.0073
0.00087
1
8260D
2/3/20 19:34
TLB
POB0017
1,2-Dichloropropane
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0073
0.00092
1
8260D
2/3/20 19:34
TLB
POB0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0073
0.00091
1
8260D
2/3/20 19:34
TLB
POB0017
1,3-Dichloropropane
BRL
mg/kg dry
0.0073
0.00061
1
8260D
2/3/20 19:34
TLB
POB0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0073
0.00093
1
8260D
2/3/20 19:34
TLB
POB0017
2,2-Dichloropropane
BRL
mg/kg dry
0.0073
0.00091
1
8260D
2/3/20 19:34
TLB
POB0017
2-Chlorotoluene
BRL
mg/kg dry
0.0073
0.00098
1
8260D
2/3/20 19:34
TLB
POB0017
4-Chlorotoluene
BRL
mg/kg dry
0.0073
0.00083
1
8260D
2/3/20 19:34
TLB
POB0017
4-Isopropyltoluene
BRL
mg/kg dry
0.0073
0.0018
1
8260D
2/3/20 19:34
TLB
POB0017
Acetone
BRL
mg/kg dry
0.029
0.0019
1
8260D
2/3/20 19:34
TLB
POB0017
Benzene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
Bromobenzene
BRL
mg/kg dry
0.0073
0.0010
1
8260D
2/3/20 19:34
TLB
POB0017
Bromochloromethane
BRL
mg/kg dry
0.0073
0.0012
1
8260D
2/3/20 19:34
TLB
POB0017
Bromodichloromethane
BRL
mg/kg dry
0.0073
0.00069
1
8260D
2/3/20 19:34
TLB
POB0017
Bromoform
BRL
mg/kg dry
0.0073
0.00057
1
8260D
2/3/20 19:34
TLB
POB0017
Bromomethane
BRL
mg/kg dry
0.015
0.0036
1
8260D
2/3/20 19:34
TLB
POB0017
Carbon Tetrachloride
BRL
mg/kg dry
0.0073
0.0014
1
8260D
2/3/20 19:34
TLB
POB0017
Chlorobenzene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
Chloroethane
BRL
mg/kg dry
0.015
0.0014
1
8260D
2/3/20 19:34
TLB
POB0017
Chloroform
BRL
mg/kg dry
0.0073
0.00089
1
8260D
2/3/20 19:34
TLB
POB0017
Chloromethane
BRL
mg/kg dry
0.015
0.0022
1
8260D
2/3/20 19:34
TLB
POB0017
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0073
0.00072
1
8260D
2/3/20 19:34
TLB
POB0017
Dibromochloromethane
BRL
mg/kg dry
0.0073
0.00049
1
8260D
2/3/20 19:34
TLB
POB0017
Dichlorodifluoromethane
BRL
mg/kg dry
0.015
0.0021
1
8260D
2/3/20 19:34
TLB
POB0017
Ethylbenzene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
Isopropyl Ether
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0073
0.00085
1
8260D
2/3/20 19:34
TLB
POB0017
m,p-Xylenes
BRL
mg/kg dry
0.015
0.0019
1
8260D
2/3/20 19:34
TLB
POB0017
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-3
Attn: Tom Hassett Sample ID: 0010326-03
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.029
0.00051
1
8260D
2/3/20 19:34
TLB
POB0017
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.029
0.0017
1
8260D
2/3/20 19:34
TLB
POB0017
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.029
0.00060
1
8260D
2/3/20 19:34
TLB
POB0017
Methylene Chloride
BRL
mg/kg dry
0.0073
0.0012
1
8260D
2/3/20 19:34
TLB
POB0017
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0073
0.0010
1
8260D
2/3/20 19:34
TLB
POB0017
Naphthalene
BRL
mg/kg dry
0.015
0.00074
1
8260D
2/3/20 19:34
TLB
POB0017
n-Butylbenzene
BRL
mg/kg dry
0.0073
0.00068
1
8260D
2/3/20 19:34
TLB
POB0017
n-Propylbenzene
BRL
mg/kg dry
0.0073
0.0011
1
8260D
2/3/20 19:34
TLB
POB0017
o-Xylene
BRL
mg/kg dry
0.0073
0.00078
1
8260D
2/3/20 19:34
TLB
POB0017
sec-Butylbenzene
BRL
mg/kg dry
0.0073
0.00079
1
8260D
2/3/20 19:34
TLB
POB0017
Styrene
BRL
mg/kg dry
0.0073
0.00071
1
8260D
2/3/20 19:34
TLB
POB0017
tert-Butylbenzene
BRL
mg/kg dry
0.0073
0.00087
1
8260D
2/3/20 19:34
TLB
POB0017
Tetrachloroethylene
BRL
mg/kg dry
0.0073
0.0013
1
8260D
2/3/20 19:34
TLB
POB0017
Toluene
BRL
mg/kg dry
0.0073
0.0012
1
8260D
2/3/20 19:34
TLB
POB0017
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0073
0.0014
1
8260D
2/3/20 19:34
TLB
POB0017
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0073
0.00063
1
8260D
2/3/20 19:34
TLB
POB0017
Trichloroethylene
BRL
mg/kg dry
0.0073
0.0014
1
8260D
2/3/20 19:34
TLB
POB0017
Trichlorofluoromethane
BRL
mg/kg dry
0.015
0.0020
1
8260D
2/3/20 19:34
TLB
POB0017
Vinyl acetate
BRL
mg/kg dry
0.015
0.00079
1
8260D
2/3/20 19:34
TLB
POB0017
Vinyl chloride
BRL
mg/kg dry
0.015
0.0014
1
8260D
2/3/20 19:34
TLB
POB0017
Xylenes, total
BRL
mg/kg dry
0.022
0.0026
1
8260D
2/3/20 19:34
TLB
POB0017
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
98 %
84-123
Toluene-d8
97 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8Aliphatics
BRL
mg/kg dry
31
6.1
100
MADEP VPH
1/29/20 16:22
TBL
POA0482
C9-C12Aliphatics
BRL
mg/kg dry
31
2.7
100
MADEP VPH
1/29/20 16:22
TBL
POA0482
C9-C10Aromatics
BRL
mg/kg dry
31
2.9
100
MADEP VPH
1/29/20 16:22
TBL
POA0482
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
99 %
70-130
2,5-Dibromotoluene (FID)
118 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-4
Attn: Tom Hassett Sample ID: 0010326-04
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18Aliphatics
BRL
mg/kg dry
37
1.9
1
MADEP EPH
1/29/20 18:52
ZRC
POA0439
C1 9-C36 Aliphatics
BRL
mg/kg dry
37
6.3
1
MADEP EPH
1/29/20 18:52
ZRC
POA0439
C1 1 -C22 Aromatics
BRL
mg/kg dry
37
10
1
MADEP EPH
1/29/20 18:52
ZRC
POA0439
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
78 %
40-140
o-Terphenyl
80 %
40-140
2-Fluorobiphenyl
78 %
40-140
2-Bromonaphthalene
83 %
40-140
General Chemistry Parameters
% Solids
66.5
% by
0.100
0.100
1
*SM2540 G
2/3120 8:20
EDV
POA0526
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.99
0.18
1
8270E
1/31/20 13:57
JMV
POA0489
1,2-Dichlorobenzene
BRL
mg/kg dry
0.99
0.16
1
8270E
1/31/20 13:57
JMV
POA0489
1,3-Dichlorobenzene
BRL
mg/kg dry
0.99
0.15
1
8270E
1/31/20 13:57
JMV
POA0489
1,4-Dichlorobenzene
BRL
mg/kg dry
0.50
0.16
1
8270E
1/31/20 13:57
JMV
POA0489
1-Methyl naphthalene
BRL
mg/kg dry
0.99
0.015
1
8270E
1/31/20 13:57
JMV
POA0489
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.99
0.21
1
8270E
1/31/20 13:57
JMV
POA0489
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.99
0.24
1
8270E
1/31/20 13:57
JMV
POA0489
2,4-Dichlorophenol
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
2,4-Dimethylphenol
BRL
mg/kg dry
0.50
0.21
1
8270E
1/31/20 13:57
JMV
POA0489
2,4-Dinitrophenol
BRL
mg/kg dry
2.3
0.58
1
8270E
1/31/20 13:57
JMV
POA0489
2,4-Dinitrotoluene
BRL
mg/kg dry
0.99
0.26
1
8270E
1/31/20 13:57
JMV
POA0489
2,6-Dinitrotoluene
BRL
mg/kg dry
0.99
0.26
1
8270E
1/31/20 13:57
JMV
POA0489
2-Chloronaphthalene
BRL
mg/kg dry
0.99
0.24
1
8270E
1/31/20 13:57
JMV
POA0489
2-Chlorophenol
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
2-Methyl naphthalene
BRL
mg/kg dry
0.99
0.019
1
8270E
1/31/20 13:57
JMV
POA0489
2-Methylphenol
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
2-Nitrophenol
BRL
mg/kg dry
0.99
0.17
1
8270E
1/31/20 13:57
JMV
POA0489
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.99
0.20
1
8270E
1/31/20 13:57
JMV
POA0489
3/4-Methyl phenol
BRL
mg/kg dry
0.99
0.22
1
8270E
1/31/20 13:57
JMV
POA0489
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.3
0.55
1
8270E
1/31/20 13:57
JMV
POA0489
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.99
0.23
1
8270E
1/31/20 13:57
JMV
POA0489
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
4-Chloroaniline
BRL
mg/kg dry
0.50
0.12
1
8270E
1/31/20 13:57
JMV
POA0489
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.30
1
8270E
1/31/20 13:57
JMV
POA0489
4-Nitrophenol
BRL
mg/kg dry
0.99
0.25
1
8270E
1/31/20 13:57
JMV
POA0489
Acenaphthene
BRL
mg/kg dry
0.99
0.023
1
8270E
1/31/20 13:57
JMV
POA0489
Acenaphthylene
BRL
mg/kg dry
0.99
0.020
1
8270E
1/31/20 13:57
JMV
POA0489
Anthracene
BRL
mg/kg dry
0.99
0.011
1
8270E
1/31/20 13:57
JMV
POA0489
Azobenzene
BRL
mg/kg dry
0.99
0.21
1
8270E
1/31/20 13:57
JMV
POA0489
Benzo(a)anthracene
BRL
mg/kg dry
0.99
0.012
1
8270E
1/31/20 13:57
JMV
POA0489
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-4
Attn: Tom Hassett Sample ID: 0010326-04
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.99
0.0089
1
8270E
1/31/20 13:57
JMV
POA0489
Benzo(b)fluoranthene
BRL
mg/kg dry
0.99
0.0092
1
8270E
1/31/20 13:57
JMV
POA0489
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.99
0.0098
1
8270E
1/31/20 13:57
JMV
POA0489
Benzo(k)fluoranthene
BRL
mg/kg dry
0.99
0.011
1
8270E
1/31/20 13:57
JMV
POA0489
Benzoic Acid
BRL
mg/kg dry
3.0
0.82
1
8270E
1/31/20 13:57
JMV
POA0489
Benzyl alcohol
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.99
0.19
1
8270E
1/31/20 13:57
JMV
POA0489
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.99
0.16
1
8270E
1/31/20 13:57
JMV
POA0489
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.50
0.18
1
8270E
1/31/20 13:57
JMV
POA0489
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.99
0.22
1
8270E
1/31/20 13:57
JMV
POA0489
Butyl benzyl phthalate
BRL
mg/kg dry
0.50
0.17
1
8270E
1/31/20 13:57
JMV
POA0489
Chrysene
BRL
mg/kg dry
0.99
0.012
1
8270E
1/31/20 13:57
JMV
POA0489
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.99
0.029
1
8270E
1/31/20 13:57
JMV
POA0489
Dibenzofuran
BRL
mg/kg dry
0.99
0.27
1
8270E
1/31/20 13:57
JMV
POA0489
Diethyl phthalate
BRL
mg/kg dry
0.99
0.26
1
8270E
1/31/20 13:57
JMV
POA0489
Dimethyl phthalate
BRL
mg/kg dry
0.99
0.24
1
8270E
1/31/20 13:57
JMV
POA0489
Di-n-butyl phthalate
BRL
mg/kg dry
0.99
0.25
1
8270E
1/31/20 13:57
JMV
POA0489
Di-n-octyl phthalate
BRL
mg/kg dry
0.50
0.26
1
8270E
1/31/20 13:57
JMV
POA0489
Fluoranthene
BRL
mg/kg dry
0.99
0.011
1
8270E
1/31/20 13:57
JMV
POA0489
Fluorene
BRL
mg/kg dry
0.99
0.017
1
8270E
1/31/20 13:57
JMV
POA0489
Hexachlorobenzene
BRL
mg/kg dry
0.99
0.22
1
8270E
1/31/20 13:57
JMV
POA0489
Hexachlorobutadiene
BRL
mg/kg dry
0.99
0.22
1
8270E
1/31/20 13:57
JMV
POA0489
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.99
0.34
1
8270E
1/31/20 13:57
JMV
POA0489
Hexachloroethane
BRL
mg/kg dry
0.99
0.16
1
8270E
1/31/20 13:57
JMV
POA0489
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.99
0.028
1
8270E
1/31/20 13:57
JMV
POA0489
Isophorone
BRL
mg/kg dry
0.99
0.21
1
8270E
1/31/20 13:57
JMV
POA0489
Naphthalene
BRL
mg/kg dry
0.99
0.021
1
8270E
1/31/20 13:57
JMV
POA0489
Nitrobenzene
BRL
mg/kg dry
0.50
0.21
1
8270E
1/31/20 13:57
JMV
POA0489
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.99
0.23
1
8270E
1/31/20 13:57
JMV
POA0489
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.99
0.27
1
8270E
1/31/20 13:57
JMV
POA0489
Pentachlorophenol
BRL
mg/kg dry
1.5
0.63
1
8270E
1/31/20 13:57
JMV
POA0489
Phenanthrene
BRL
mg/kg dry
0.99
0.011
1
8270E
1/31/20 13:57
JMV
POA0489
Phenol
BRL
mg/kg dry
0.99
0.16
1
8270E
1/31/20 13:57
JMV
POA0489
Pyrene
BRL
mg/kg dry
0.99
0.014
1
8270E
1/31/20 13:57
JMV
POA0489
Pyridine
BRL
mg/kg dry
0.50
0.095
1
8270E
1/31/20 13:57
JMV
POA0489
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
106 %
39-132
2-Fluorobiphenyl
82 %
44-115
2-Fluorophenol
82 %
35-115
Nitrobenzene-d5
74 %
37-122
Phenol-d5
78 %
34-121
Terphenyl-d14
95 %
54-127
Volatile Organic Compounds by GUMS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-4
Attn: Tom Hassett Sample ID: 0010326-04
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0089
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0089
0.00065
1
8260D
2/3/20 20:04
TLB
POB0017
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0089
0.00096
1
8260D
2/3/20 20:04
TLB
POB0017
1,1-Dichloroethane
BRL
mg/kg dry
0.0089
0.0016
1
8260D
2/3/20 20:04
TLB
POB0017
1,1-Dichloroethylene
BRL
mg/kg dry
0.0089
0.0016
1
8260D
2/3/20 20:04
TLB
POB0017
1,1-Dichloropropylene
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.018
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0089
0.0010
1
8260D
2/3/20 20:04
TLB
POB0017
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.018
0.00085
1
8260D
2/3/20 20:04
TLB
POB0017
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0089
0.00094
1
8260D
2/3/20 20:04
TLB
POB0017
1,2-Dibromoethane
BRL
mg/kg dry
0.0089
0.00080
1
8260D
2/3/20 20:04
TLB
POB0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0089
0.00099
1
8260D
2/3/20 20:04
TLB
POB0017
1,2-Dichloroethane
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
1,2-Dichloropropane
BRL
mg/kg dry
0.0089
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
1,3-Dichloropropane
BRL
mg/kg dry
0.0089
0.00074
1
8260D
2/3/20 20:04
TLB
POB0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
2,2-Dichloropropane
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
2-Chlorotoluene
BRL
mg/kg dry
0.0089
0.0012
1
8260D
2/3/20 20:04
TLB
POB0017
4-Chlorotoluene
BRL
mg/kg dry
0.0089
0.0010
1
8260D
2/3/20 20:04
TLB
POB0017
4-Isopropyltoluene
BRL
mg/kg dry
0.0089
0.0022
1
8260D
2/3/20 20:04
TLB
POB0017
Acetone
0.038
mg/kg dry
0.036
0.0023
1
8260D
2/3/20 20:04
TLB
POB0017
Benzene
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
Bromobenzene
BRL
mg/kg dry
0.0089
0.0012
1
8260D
2/3/20 20:04
TLB
POB0017
Bromochloromethane
BRL
mg/kg dry
0.0089
0.0015
1
8260D
2/3/20 20:04
TLB
POB0017
Bromodichloromethane
BRL
mg/kg dry
0.0089
0.00084
1
8260D
2/3/20 20:04
TLB
POB0017
Bromoform
BRL
mg/kg dry
0.0089
0.00069
1
8260D
2/3/20 20:04
TLB
POB0017
Bromomethane
BRL
mg/kg dry
0.018
0.0044
1
8260D
2/3/20 20:04
TLB
POB0017
Carbon Tetrachloride
BRL
mg/kg dry
0.0089
0.0017
1
8260D
2/3/20 20:04
TLB
POB0017
Chlorobenzene
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
Chloroethane
BRL
mg/kg dry
0.018
0.0017
1
8260D
2/3/20 20:04
TLB
POB0017
Chloroform
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
Chloromethane
BRL
mg/kg dry
0.018
0.0027
1
8260D
2/3/20 20:04
TLB
POB0017
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0089
0.00088
1
8260D
2/3/20 20:04
TLB
POB0017
Dibromochloromethane
BRL
mg/kg dry
0.0089
0.00060
1
8260D
2/3/20 20:04
TLB
POB0017
Dichlorodifluoromethane
BRL
mg/kg dry
0.018
0.0025
1
8260D
2/3/20 20:04
TLB
POB0017
Ethylbenzene
BRL
mg/kg dry
0.0089
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
Isopropyl Ether
BRL
mg/kg dry
0.0089
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0089
0.0010
1
8260D
2/3/20 20:04
TLB
POB0017
m,p-Xylenes
BRL
mg/kg dry
0.018
0.0023
1
8260D
2/3/20 20:04
TLB
POB0017
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-4
Attn: Tom Hassett Sample ID: 0010326-04
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.036
0.00061
1
8260D
2/3/20 20:04
TLB
POB0017
Methyl Ethyl Ketone (2-Butanone)
BRL CCVL
mg/kg dry
0.036
0.0021
1
8260D
2/3/20 20:04
TLB
POB0017
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.036
0.00072
1
8260D
2/3/20 20:04
TLB
POB0017
Methylene Chloride
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0089
0.0012
1
8260D
2/3/20 20:04
TLB
POB0017
Naphthalene
BRL
mg/kg dry
0.018
0.00090
1
8260D
2/3/20 20:04
TLB
POB0017
n-Butylbenzene
BRL
mg/kg dry
0.0089
0.00083
1
8260D
2/3/20 20:04
TLB
POB0017
n-Propylbenzene
BRL
mg/kg dry
0.0089
0.0013
1
8260D
2/3/20 20:04
TLB
POB0017
o-Xylene
BRL
mg/kg dry
0.0089
0.00095
1
8260D
2/3/20 20:04
TLB
POB0017
sec-Butylbenzene
BRL
mg/kg dry
0.0089
0.00096
1
8260D
2/3/20 20:04
TLB
POB0017
Styrene
BRL
mg/kg dry
0.0089
0.00086
1
8260D
2/3/20 20:04
TLB
POB0017
tert-Butylbenzene
BRL
mg/kg dry
0.0089
0.0011
1
8260D
2/3/20 20:04
TLB
POB0017
Tetrachloroethylene
BRL
mg/kg dry
0.0089
0.0016
1
8260D
2/3/20 20:04
TLB
POB0017
Toluene
BRL
mg/kg dry
0.0089
0.0014
1
8260D
2/3/20 20:04
TLB
POB0017
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0089
0.0017
1
8260D
2/3/20 20:04
TLB
POB0017
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0089
0.00076
1
8260D
2/3/20 20:04
TLB
POB0017
Trichloroethylene
BRL
mg/kg dry
0.0089
0.0017
1
8260D
2/3/20 20:04
TLB
POB0017
Trichlorofluoromethane
BRL
mg/kg dry
0.018
0.0024
1
8260D
2/3/20 20:04
TLB
POB0017
Vinyl acetate
BRL
mg/kg dry
0.018
0.00096
1
8260D
2/3/20 20:04
TLB
POB0017
Vinyl chloride
BRL
mg/kg dry
0.018
0.0018
1
8260D
2/3/20 20:04
TLB
POB0017
Xylenes, total
BRL
mg/kg dry
0.027
0.0032
1
8260D
2/3/20 20:04
TLB
POB0017
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
99 %
84-123
Toluene-d8
99 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8Aliphatics
BRL
mg/kg dry
27
5.4
100
MADEP VPH
1/29/20 16:51
TBL
POA0482
C9-C12Aliphatics
BRL
mg/kg dry
27
2.4
100
MADEP VPH
1/29/20 16:51
TBL
POA0482
C9-C10Aromatics
BRL
mg/kg dry
27
2.5
100
MADEP VPH
1/29/20 16:51
TBL
POA0482
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
106 %
70-130
2,5-Dibromotoluene (FID)
125 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-5
Attn: Tom Hassett Sample ID: 0010326-05
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
1.8 J
mg/kg dry
36
1.8
1
MADEP EPH
1/30/20 23:37
ZRC
POA0439
C1 9-C36 Aliphatics
BRL
mg/kg dry
36
6.1
1
MADEP EPH
1/30/20 23:37
ZRC
POA0439
C11-C22 Aromatics
BRL
mg/kg dry
36
9.9
1
MADEP EPH
1/30/20 23:37
ZRC
POA0439
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
78 %
40-140
o-Terphenyl
79 %
40-140
2-Fluorobiphenyl
72 %
40-140
2-Bromonaphthalene
28 %
40-140
A
General Chemistry Parameters
% Solids
68.5
% by
0.100
0.100
1
*SM2540 G
2/3/20 8:20
EDV
POA0526
Weight
Semivolatile Organic Compounds by GUMS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.96
0.17
1
8270E
1/31/20 12:49
JMV
POA0489
1,2-Dichlorobenzene
BRL
mg/kg dry
0.96
0.16
1
8270E
1/31/20 12:49
JMV
POA0489
1,3-Dichlorobenzene
BRL
mg/kg dry
0.96
0.14
1
8270E
1/31/20 12:49
JMV
POA0489
1,4-Dichlorobenzene
BRL
mg/kg dry
0.48
0.15
1
8270E
1/31/20 12:49
JMV
POA0489
1-Methyl naphthalene
BRL
mg/kg dry
0.96
0.015
1
8270E
1/31/20 12:49
JMV
POA0489
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.96
0.20
1
8270E
1/31/20 12:49
JMV
POA0489
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.96
0.23
1
8270E
1/31/20 12:49
JMV
POA0489
2,4-Dichlorophenol
BRL
mg/kg dry
0.96
0.19
1
8270E
1/31/20 12:49
JMV
POA0489
2,4-Dimethylphenol
BRL
mg/kg dry
0.48
0.20
1
8270E
1/31/20 12:49
JMV
POA0489
2,4-Dinitrophenol
BRL
mg/kg dry
2.2
0.56
1
8270E
1/31/20 12:49
JMV
POA0489
2,4-Dinitrotoluene
BRL
mg/kg dry
0.96
0.26
1
8270E
1/31/20 12:49
JMV
POA0489
2,6-Dinitrotoluene
BRL
mg/kg dry
0.96
0.25
1
8270E
1/31/20 12:49
JMV
POA0489
2-Chloronaphthalene
BRL
mg/kg dry
0.96
0.23
1
8270E
1/31/20 12:49
JMV
POA0489
2-Chlorophenol
BRL
mg/kg dry
0.96
0.18
1
8270E
1/31/20 12:49
JMV
POA0489
2-Methyl naphthalene
BRL
mg/kg dry
0.96
0.019
1
8270E
1/31/20 12:49
JMV
POA0489
2-Methylphenol
BRL
mg/kg dry
0.96
0.18
1
8270E
1/31/20 12:49
JMV
POA0489
2-Nitrophenol
BRL
mg/kg dry
0.96
0.16
1
8270E
1/31/20 12:49
JMV
POA0489
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.96
0.19
1
8270E
1/31/20 12:49
JMV
POA0489
3/4-Methyl phenol
BRL
mg/kg dry
0.96
0.21
1
8270E
1/31/20 12:49
JMV
POA0489
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.2
0.53
1
8270E
1/31/20 12:49
JMV
POA0489
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.96
0.23
1
8270E
1/31/20 12:49
JMV
POA0489
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.96
0.18
1
8270E
1/31/20 12:49
JMV
POA0489
4-Chloroaniline
BRL
mg/kg dry
0.48
0.12
1
8270E
1/31/20 12:49
JMV
POA0489
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.29
1
8270E
1/31/20 12:49
JMV
POA0489
4-Nitrophenol
BRL
mg/kg dry
0.96
0.24
1
8270E
1/31/20 12:49
JMV
POA0489
Acenaphthene
BRL
mg/kg dry
0.96
0.022
1
8270E
1/31/20 12:49
JMV
POA0489
Acenaphthylene
BRL
mg/kg dry
0.96
0.019
1
8270E
1/31/20 12:49
JMV
POA0489
Anthracene
BRL
mg/kg dry
0.96
0.011
1
8270E
1/31/20 12:49
JMV
POA0489
Azobenzene
BRL
mg/kg dry
0.96
0.21
1
8270E
1/31/20 12:49
JMV
POA0489
Benzo(a)anthracene
BRL
mg/kg dry
0.96
0.012
1
8270E
1/31/20 12:49
JMV
POA0489
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-5
Attn: Tom Hassett Sample ID: 0010326-05
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.96
0.0086
1
8270E
1/31/20 12:49
JMV
POA0489
Benzo(b)fluoranthene
BRL
mg/kg dry
0.96
0.0089
1
8270E
1/31/20 12:49
JMV
POA0489
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.96
0.0095
1
8270E
1/31/20 12:49
JMV
POA0489
Benzo(k)fluoranthene
BRL
mg/kg dry
0.96
0.010
1
8270E
1/31/20 12:49
JMV
POA0489
Benzoic Acid
BRL
mg/kg dry
2.9
0.80
1
8270E
1/31/20 12:49
JMV
POA0489
Benzyl alcohol
BRL
mg/kg dry
0.96
0.18
1
8270E
1/31/20 12:49
JMV
POA0489
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.96
0.18
1
8270E
1/31/20 12:49
JMV
POA0489
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.96
0.15
1
8270E
1/31/20 12:49
JMV
POA0489
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.48
0.17
1
8270E
1/31/20 12:49
JMV
POA0489
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.96
0.22
1
8270E
1/31/20 12:49
JMV
POA0489
Butyl benzyl phthalate
BRL
mg/kg dry
0.48
0.17
1
8270E
1/31/20 12:49
JMV
POA0489
Chrysene
BRL
mg/kg dry
0.96
0.011
1
8270E
1/31/20 12:49
JMV
POA0489
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.96
0.028
1
8270E
1/31/20 12:49
JMV
POA0489
Dibenzofuran
BRL
mg/kg dry
0.96
0.26
1
8270E
1/31/20 12:49
JMV
POA0489
Diethyl phthalate
BRL
mg/kg dry
0.96
0.25
1
8270E
1/31/20 12:49
JMV
POA0489
Dimethyl phthalate
BRL
mg/kg dry
0.96
0.23
1
8270E
1/31/20 12:49
JMV
POA0489
Di-n-butyl phthalate
BRL
mg/kg dry
0.96
0.24
1
8270E
1/31/20 12:49
JMV
POA0489
Di-n-octyl phthalate
BRL
mg/kg dry
0.48
0.25
1
8270E
1/31/20 12:49
JMV
POA0489
Fluoranthene
BRL
mg/kg dry
0.96
0.011
1
8270E
1/31/20 12:49
JMV
POA0489
Fluorene
BRL
mg/kg dry
0.96
0.017
1
8270E
1/31/20 12:49
JMV
POA0489
Hexachlorobenzene
BRL
mg/kg dry
0.96
0.21
1
8270E
1/31/20 12:49
JMV
POA0489
Hexachlorobutadiene
BRL
mg/kg dry
0.96
0.22
1
8270E
1/31/20 12:49
JMV
POA0489
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.96
0.33
1
8270E
1/31/20 12:49
JMV
POA0489
Hexachloroethane
BRL
mg/kg dry
0.96
0.15
1
8270E
1/31/20 12:49
JMV
POA0489
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.96
0.027
1
8270E
1/31/20 12:49
JMV
POA0489
Isophorone
BRL
mg/kg dry
0.96
0.21
1
8270E
1/31/20 12:49
JMV
POA0489
Naphthalene
BRL
mg/kg dry
0.96
0.020
1
8270E
1/31/20 12:49
JMV
POA0489
Nitrobenzene
BRL
mg/kg dry
0.48
0.20
1
8270E
1/31/20 12:49
JMV
POA0489
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.96
0.22
1
8270E
1/31/20 12:49
JMV
POA0489
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.96
0.26
1
8270E
1/31/20 12:49
JMV
POA0489
Pentachlorophenol
BRL
mg/kg dry
1.5
0.61
1
8270E
1/31/20 12:49
JMV
POA0489
Phenanthrene
BRL
mg/kg dry
0.96
0.011
1
8270E
1/31/20 12:49
JMV
POA0489
Phenol
BRL
mg/kg dry
0.96
0.16
1
8270E
1/31/20 12:49
JMV
POA0489
Pyrene
BRL
mg/kg dry
0.96
0.014
1
8270E
1/31/20 12:49
JMV
POA0489
Pyridine
BRL
mg/kg dry
0.48
0.092
1
8270E
1/31/20 12:49
JMV
POA0489
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
106 %
39-132
2-Fluorobiphenyl
83 %
44-115
2-Fluorophenol
88 %
35-115
Nitrobenzene-d5
78 %
37-122
Phenol-d5
82 %
34-121
Terphenyl-d14
97 %
54-127
Volatile Organic Compounds by GUMS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-5
Attn: Tom Hassett Sample ID: 0010326-05
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00081
1
8260D
2/3/20 20:34
TLB
POB0017
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0067
0.00098
1
8260D
2/3/20 20:34
TLB
POB0017
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00049
1
8260D
2/3/20 20:34
TLB
POB0017
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0067
0.00072
1
8260D
2/3/20 20:34
TLB
POB0017
1,1-Dichloroethane
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 20:34
TLB
POB0017
1,1-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 20:34
TLB
POB0017
1,1-Dichloropropylene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00095
1
8260D
2/3/20 20:34
TLB
POB0017
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0067
0.00076
1
8260D
2/3/20 20:34
TLB
POB0017
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00064
1
8260D
2/3/20 20:34
TLB
POB0017
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00071
1
8260D
2/3/20 20:34
TLB
POB0017
1,2-Dibromoethane
BRL
mg/kg dry
0.0067
0.00060
1
8260D
2/3/20 20:34
TLB
POB0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00074
1
8260D
2/3/20 20:34
TLB
POB0017
1,2-Dichloroethane
BRL
mg/kg dry
0.0067
0.00079
1
8260D
2/3/20 20:34
TLB
POB0017
1,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00084
1
8260D
2/3/20 20:34
TLB
POB0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00083
1
8260D
2/3/20 20:34
TLB
POB0017
1,3-Dichloropropane
BRL
mg/kg dry
0.0067
0.00056
1
8260D
2/3/20 20:34
TLB
POB0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00084
1
8260D
2/3/20 20:34
TLB
POB0017
2,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.00083
1
8260D
2/3/20 20:34
TLB
POB0017
2-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00089
1
8260D
2/3/20 20:34
TLB
POB0017
4-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00076
1
8260D
2/3/20 20:34
TLB
POB0017
4-Isopropyltoluene
BRL
mg/kg dry
0.0067
0.0017
1
8260D
2/3/20 20:34
TLB
POB0017
Acetone
BRL
mg/kg dry
0.027
0.0017
1
8260D
2/3/20 20:34
TLB
POB0017
Benzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
Bromobenzene
BRL
mg/kg dry
0.0067
0.00092
1
8260D
2/3/20 20:34
TLB
POB0017
Bromochloromethane
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 20:34
TLB
POB0017
Bromodichloromethane
BRL
mg/kg dry
0.0067
0.00063
1
8260D
2/3/20 20:34
TLB
POB0017
Bromoform
BRL
mg/kg dry
0.0067
0.00052
1
8260D
2/3/20 20:34
TLB
POB0017
Bromomethane
BRL
mg/kg dry
0.013
0.0033
1
8260D
2/3/20 20:34
TLB
POB0017
Carbon Tetrachloride
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 20:34
TLB
POB0017
Chlorobenzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
Chloroethane
BRL
mg/kg dry
0.013
0.0013
1
8260D
2/3/20 20:34
TLB
POB0017
Chloroform
BRL
mg/kg dry
0.0067
0.00082
1
8260D
2/3/20 20:34
TLB
POB0017
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
8260D
2/3/20 20:34
TLB
POB0017
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00066
1
8260D
2/3/20 20:34
TLB
POB0017
Dibromochloromethane
BRL
mg/kg dry
0.0067
0.00045
1
8260D
2/3/20 20:34
TLB
POB0017
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0019
1
8260D
2/3/20 20:34
TLB
POB0017
Ethylbenzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 20:34
TLB
POB0017
Isopropyl Ether
BRL
mg/kg dry
0.0067
0.00098
1
8260D
2/3/20 20:34
TLB
POB0017
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0067
0.00078
1
8260D
2/3/20 20:34
TLB
POB0017
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
8260D
2/3/20 20:34
TLB
POB0017
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-5
Attn: Tom Hassett Sample ID: 0010326-05
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.027
0.00046
1
8260D
2/3/20 20:34
TLB
POB0017
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.027
0.0016
1
8260D
2/3/20 20:34
TLB
POB0017
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.027
0.00054
1
8260D
2/3/20 20:34
TLB
POB0017
Methylene Chloride
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 20:34
TLB
POB0017
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0067
0.00093
1
8260D
2/3/20 20:34
TLB
POB0017
Naphthalene
BRL
mg/kg dry
0.013
0.00067
1
8260D
2/3/20 20:34
TLB
POB0017
n-Butylbenzene
BRL
mg/kg dry
0.0067
0.00062
1
8260D
2/3/20 20:34
TLB
POB0017
n-Propylbenzene
BRL
mg/kg dry
0.0067
0.00097
1
8260D
2/3/20 20:34
TLB
POB0017
o-Xylene
BRL
mg/kg dry
0.0067
0.00071
1
8260D
2/3/20 20:34
TLB
POB0017
sec-Butylbenzene
BRL
mg/kg dry
0.0067
0.00072
1
8260D
2/3/20 20:34
TLB
POB0017
Styrene
BRL
mg/kg dry
0.0067
0.00065
1
8260D
2/3/20 20:34
TLB
POB0017
tert-Butylbenzene
BRL
mg/kg dry
0.0067
0.00079
1
8260D
2/3/20 20:34
TLB
POB0017
Tetrachloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 20:34
TLB
POB0017
Toluene
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 20:34
TLB
POB0017
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 20:34
TLB
POB0017
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00057
1
8260D
2/3/20 20:34
TLB
POB0017
Trichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 20:34
TLB
POB0017
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0018
1
8260D
2/3/20 20:34
TLB
POB0017
Vinyl acetate
BRL
mg/kg dry
0.013
0.00072
1
8260D
2/3/20 20:34
TLB
POB0017
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
8260D
2/3/20 20:34
TLB
POB0017
Xylenes, total
BRL
mg/kg dry
0.020
0.0024
1
8260D
2/3/20 20:34
TLB
POB0017
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
70-130
Dibromofluoromethane
101 %
84-123
Toluene-d8
97 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8Aliphatics
BRL
mg/kg dry
9.1
1.8
100
MADEP VPH
1/29/20 17:20
TBL
POA0482
C9-C12Aliphatics
BRL
mg/kg dry
9.1
0.80
100
MADEP VPH
1/29/20 17:20
TBL
POA0482
C9-C10Aromatics
BRL
mg/kg dry
9.1
0.85
100
MADEP VPH
1/29/20 17:20
TBL
POA0482
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
100 %
70-130
2,5-Dibromotoluene (FID)
119 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-6
Attn: Tom Hassett Sample ID: 0010326-06
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18Aliphatics
BRL
mg/kg dry
35
1.8
1
MADEP EPH
1/29/20 20:42
ZRC
POA0439
C1 9-C36 Aliphatics
BRL
mg/kg dry
35
5.9
1
MADEP EPH
1/29/20 20:42
ZRC
POA0439
C1 1 -C22 Aromatics
BRL
mg/kg dry
35
9.6
1
MADEP EPH
1/29/20 20:42
ZRC
POA0439
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
79 %
40-140
o-Terphenyl
83 %
40-140
2-Fluorobiphenyl
77 %
40-140
2-Bromonaphthalene
78 %
40-140
General Chemistry Parameters
% Solids
71.3
% by
0.100
0.100
1
*SM2540 G
2/3/20 8:20
EDV
POA0526
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.92
0.16
1
8270E
1/31/20 14:20
JMV
POA0489
1,2-Dichlorobenzene
BRL
mg/kg dry
0.92
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
1,3-Dichlorobenzene
BRL
mg/kg dry
0.92
0.14
1
8270E
1/31/20 14:20
JMV
POA0489
1,4-Dichlorobenzene
BRL
mg/kg dry
0.46
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
1-Methyl naphthalene
BRL
mg/kg dry
0.92
0.014
1
8270E
1/31/20 14:20
JMV
POA0489
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.92
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.92
0.22
1
8270E
1/31/20 14:20
JMV
POA0489
2,4-Dichlorophenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
2,4-Dimethylphenol
BRL
mg/kg dry
0.46
0.19
1
8270E
1/31/20 14:20
JMV
POA0489
2,4-Dinitrophenol
BRL
mg/kg dry
2.1
0.54
1
8270E
1/31/20 14:20
JMV
POA0489
2,4-Dinitrotoluene
BRL
mg/kg dry
0.92
0.25
1
8270E
1/31/20 14:20
JMV
POA0489
2,6-Dinitrotoluene
BRL
mg/kg dry
0.92
0.24
1
8270E
1/31/20 14:20
JMV
POA0489
2-Chloronaphthalene
BRL
mg/kg dry
0.92
0.23
1
8270E
1/31/20 14:20
JMV
POA0489
2-Chlorophenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
2-Methyl naphthalene
BRL
mg/kg dry
0.92
0.018
1
8270E
1/31/20 14:20
JMV
POA0489
2-Methylphenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
2-Nitrophenol
BRL
mg/kg dry
0.92
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
3/4-Methyl phenol
BRL
mg/kg dry
0.92
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.1
0.51
1
8270E
1/31/20 14:20
JMV
POA0489
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.92
0.22
1
8270E
1/31/20 14:20
JMV
POA0489
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
4-Chloroaniline
BRL
mg/kg dry
0.46
0.11
1
8270E
1/31/20 14:20
JMV
POA0489
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.4
0.28
1
8270E
1/31/20 14:20
JMV
POA0489
4-Nitrophenol
BRL
mg/kg dry
0.92
0.23
1
8270E
1/31/20 14:20
JMV
POA0489
Acenaphthene
BRL
mg/kg dry
0.92
0.021
1
8270E
1/31/20 14:20
JMV
POA0489
Acenaphthylene
BRL
mg/kg dry
0.92
0.018
1
8270E
1/31/20 14:20
JMV
POA0489
Anthracene
BRL
mg/kg dry
0.92
0.010
1
8270E
1/31/20 14:20
JMV
POA0489
Azobenzene
BRL
mg/kg dry
0.92
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
Benzo(a)anthracene
BRL
mg/kg dry
0.92
0.011
1
8270E
1/31/20 14:20
JMV
POA0489
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-6
Attn: Tom Hassett Sample ID: 0010326-06
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.92
0.0083
1
8270E
1/31/20 14:20
JMV
POA0489
Benzo(b)fluoranthene
BRL
mg/kg dry
0.92
0.0085
1
8270E
1/31/20 14:20
JMV
POA0489
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.92
0.0091
1
8270E
1/31/20 14:20
JMV
POA0489
Benzo(k)fluoranthene
BRL
mg/kg dry
0.92
0.0098
1
8270E
1/31/20 14:20
JMV
POA0489
Benzoic Acid
BRL
mg/kg dry
2.8
0.77
1
8270E
1/31/20 14:20
JMV
POA0489
Benzyl alcohol
BRL
mg/kg dry
0.92
0.17
1
8270E
1/31/20 14:20
JMV
POA0489
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.92
0.18
1
8270E
1/31/20 14:20
JMV
POA0489
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.92
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.46
0.17
1
8270E
1/31/20 14:20
JMV
POA0489
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.92
0.21
1
8270E
1/31/20 14:20
JMV
POA0489
Butyl benzyl phthalate
BRL
mg/kg dry
0.46
0.16
1
8270E
1/31/20 14:20
JMV
POA0489
Chrysene
BRL
mg/kg dry
0.92
0.011
1
8270E
1/31/20 14:20
JMV
POA0489
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.92
0.027
1
8270E
1/31/20 14:20
JMV
POA0489
Dibenzofuran
BRL
mg/kg dry
0.92
0.25
1
8270E
1/31/20 14:20
JMV
POA0489
Diethyl phthalate
BRL
mg/kg dry
0.92
0.24
1
8270E
1/31/20 14:20
JMV
POA0489
Dimethyl phthalate
BRL
mg/kg dry
0.92
0.22
1
8270E
1/31/20 14:20
JMV
POA0489
Di-n-butyl phthalate
BRL
mg/kg dry
0.92
0.23
1
8270E
1/31/20 14:20
JMV
POA0489
Di-n-octyl phthalate
BRL
mg/kg dry
0.46
0.24
1
8270E
1/31/20 14:20
JMV
POA0489
Fluoranthene
BRL
mg/kg dry
0.92
0.011
1
8270E
1/31/20 14:20
JMV
POA0489
Fluorene
BRL
mg/kg dry
0.92
0.016
1
8270E
1/31/20 14:20
JMV
POA0489
Hexachlorobenzene
BRL
mg/kg dry
0.92
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
Hexachlorobutadiene
BRL
mg/kg dry
0.92
0.21
1
8270E
1/31/20 14:20
JMV
POA0489
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.92
0.32
1
8270E
1/31/20 14:20
JMV
POA0489
Hexachloroethane
BRL
mg/kg dry
0.92
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.92
0.026
1
8270E
1/31/20 14:20
JMV
POA0489
Isophorone
BRL
mg/kg dry
0.92
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
Naphthalene
BRL
mg/kg dry
0.92
0.020
1
8270E
1/31/20 14:20
JMV
POA0489
Nitrobenzene
BRL
mg/kg dry
0.46
0.20
1
8270E
1/31/20 14:20
JMV
POA0489
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.92
0.21
1
8270E
1/31/20 14:20
JMV
POA0489
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.92
0.25
1
8270E
1/31/20 14:20
JMV
POA0489
Pentachlorophenol
BRL
mg/kg dry
1.4
0.59
1
8270E
1/31/20 14:20
JMV
POA0489
Phenanthrene
BRL
mg/kg dry
0.92
0.010
1
8270E
1/31/20 14:20
JMV
POA0489
Phenol
BRL
mg/kg dry
0.92
0.15
1
8270E
1/31/20 14:20
JMV
POA0489
Pyrene
BRL
mg/kg dry
0.92
0.013
1
8270E
1/31/20 14:20
JMV
POA0489
Pyridine
BRL
mg/kg dry
0.46
0.088
1
8270E
1/31/20 14:20
JMV
POA0489
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
106 %
39-132
2-Fluorobiphenyl
86 %
44-115
2-Fluorophenol
87 %
35-115
Nitrobenzene-d5
79 %
37-122
Phenol-d5
83 %
34-121
Terphenyl-d14
95 %
54-127
Volatile Organic Compounds by GUMS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-6
Attn: Tom Hassett Sample ID: 0010326-06
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00082
1
8260D
2/3/20 21:04
TLB
POB0017
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0067
0.00098
1
8260D
2/3/20 21:04
TLB
POB0017
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00049
1
8260D
2/3/20 21:04
TLB
POB0017
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0067
0.00072
1
8260D
2/3/20 21:04
TLB
POB0017
1,1-Dichloroethane
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 21:04
TLB
POB0017
1,1-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 21:04
TLB
POB0017
1,1-Dichloropropylene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00096
1
8260D
2/3/20 21:04
TLB
POB0017
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0067
0.00076
1
8260D
2/3/20 21:04
TLB
POB0017
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00064
1
8260D
2/3/20 21:04
TLB
POB0017
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00071
1
8260D
2/3/20 21:04
TLB
POB0017
1,2-Dibromoethane
BRL
mg/kg dry
0.0067
0.00060
1
8260D
2/3/20 21:04
TLB
POB0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00075
1
8260D
2/3/20 21:04
TLB
POB0017
1,2-Dichloroethane
BRL
mg/kg dry
0.0067
0.00079
1
8260D
2/3/20 21:04
TLB
POB0017
1,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00084
1
8260D
2/3/20 21:04
TLB
POB0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00083
1
8260D
2/3/20 21:04
TLB
POB0017
1,3-Dichloropropane
BRL
mg/kg dry
0.0067
0.00056
1
8260D
2/3/20 21:04
TLB
POB0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00085
1
8260D
2/3/20 21:04
TLB
POB0017
2,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.00083
1
8260D
2/3/20 21:04
TLB
POB0017
2-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00089
1
8260D
2/3/20 21:04
TLB
POB0017
4-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00076
1
8260D
2/3/20 21:04
TLB
POB0017
4-Isopropyltoluene
BRL
mg/kg dry
0.0067
0.0017
1
8260D
2/3/20 21:04
TLB
POB0017
Acetone
BRL
mg/kg dry
0.027
0.0017
1
8260D
2/3/20 21:04
TLB
POB0017
Benzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
Bromobenzene
BRL
mg/kg dry
0.0067
0.00093
1
8260D
2/3/20 21:04
TLB
POB0017
Bromochloromethane
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 21:04
TLB
POB0017
Bromodichloromethane
BRL
mg/kg dry
0.0067
0.00063
1
8260D
2/3/20 21:04
TLB
POB0017
Bromoform
BRL
mg/kg dry
0.0067
0.00052
1
8260D
2/3/20 21:04
TLB
POB0017
Bromomethane
BRL
mg/kg dry
0.013
0.0033
1
8260D
2/3/20 21:04
TLB
POB0017
Carbon Tetrachloride
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 21:04
TLB
POB0017
Chlorobenzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
Chloroethane
BRL
mg/kg dry
0.013
0.0013
1
8260D
2/3/20 21:04
TLB
POB0017
Chloroform
BRL
mg/kg dry
0.0067
0.00082
1
8260D
2/3/20 21:04
TLB
POB0017
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
8260D
2/3/20 21:04
TLB
POB0017
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00066
1
8260D
2/3/20 21:04
TLB
POB0017
Dibromochloromethane
BRL
mg/kg dry
0.0067
0.00045
1
8260D
2/3/20 21:04
TLB
POB0017
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0019
1
8260D
2/3/20 21:04
TLB
POB0017
Ethylbenzene
BRL
mg/kg dry
0.0067
0.0010
1
8260D
2/3/20 21:04
TLB
POB0017
Isopropyl Ether
BRL
mg/kg dry
0.0067
0.00098
1
8260D
2/3/20 21:04
TLB
POB0017
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0067
0.00078
1
8260D
2/3/20 21:04
TLB
POB0017
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
8260D
2/3/20 21:04
TLB
POB0017
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• � 02/06/2020
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield Client Sample ID: S-6
Attn: Tom Hassett Sample ID: 0010326-06
500-K Clanton Rd. Work Order: 0010326
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 01/23/20 00:00
Time Submitted: 01/23/20 11:54
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.027
0.00046
1
8260D
2/3/20 21:04
TLB
POB0017
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.027
0.0016
1
8260D
2/3/20 21:04
TLB
POB0017
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.027
0.00054
1
8260D
2/3/20 21:04
TLB
POB0017
Methylene Chloride
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 21:04
TLB
POB0017
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0067
0.00094
1
8260D
2/3/20 21:04
TLB
POB0017
Naphthalene
BRL
mg/kg dry
0.013
0.00067
1
8260D
2/3/20 21:04
TLB
POB0017
n-Butylbenzene
BRL
mg/kg dry
0.0067
0.00062
1
8260D
2/3/20 21:04
TLB
POB0017
n-Propylbenzene
BRL
mg/kg dry
0.0067
0.00097
1
8260D
2/3/20 21:04
TLB
POB0017
o-Xylene
BRL
mg/kg dry
0.0067
0.00071
1
8260D
2/3/20 21:04
TLB
POB0017
sec-Butylbenzene
BRL
mg/kg dry
0.0067
0.00072
1
8260D
2/3/20 21:04
TLB
POB0017
Styrene
BRL
mg/kg dry
0.0067
0.00065
1
8260D
2/3/20 21:04
TLB
POB0017
tert-Butylbenzene
BRL
mg/kg dry
0.0067
0.00079
1
8260D
2/3/20 21:04
TLB
POB0017
Tetrachloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
8260D
2/3/20 21:04
TLB
POB0017
Toluene
BRL
mg/kg dry
0.0067
0.0011
1
8260D
2/3/20 21:04
TLB
POB0017
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 21:04
TLB
POB0017
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00057
1
8260D
2/3/20 21:04
TLB
POB0017
Trichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
8260D
2/3/20 21:04
TLB
POB0017
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0018
1
8260D
2/3/20 21:04
TLB
POB0017
Vinyl acetate
BRL
mg/kg dry
0.013
0.00072
1
8260D
2/3/20 21:04
TLB
POB0017
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
8260D
2/3/20 21:04
TLB
POB0017
Xylenes, total
BRL
mg/kg dry
0.020
0.0024
1
8260D
2/3/20 21:04
TLB
POB0017
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
100 %
84-123
Toluene-d8
98 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8Aliphatics
BRL
mg/kg dry
9.3
1.8
100
MADEP VPH
1/29/20 17:50
TBL
POA0482
C9-C12Aliphatics
BRL
mg/kg dry
9.3
0.82
100
MADEP VPH
1/29/20 17:50
TBL
POA0482
C9-C10Aromatics
BRL
mg/kg dry
9.3
0.88
100
MADEP VPH
1/29/20 17:50
TBL
POA0482
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
101 %
70-130
2,5-Dibromotoluene (FID)
120 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

0
Waypoint.
ANALYTICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POB0017 - 5035
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (120130017-1311-K1)
Prepared & Analyzed: 02/03/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POB0017 - 5035
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POB0017-BLK1)
Prepared & Analyzed: 02/03/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
0.000520
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00 100 70-130
Surrogate: Dibromofluoromethane
49.4
ug/L
50.00 99 84-123
Surrogate: Toluene-d8
49.2
ug/L
50.00 98 76-129
LCS (POB0017-BSI)
Prepared &Analyzed: 02/03/20
1,1,1,2-Tetrachloroethane
0.0478
0.0050
mg/kg wet
0.05000
96
72-115
1,1,1-Trichloroethane
0.0443
0.0050
mg/kg wet
0.05000
89
67-131
1,1,2,2-Tetrachloroethane
0.0435
0.0050
mg/kg wet
0.05000
87
56-126
1,1,2-Trichloroethane
0.0452
0.0050
mg/kg wet
0.05000
90
70-133
1,1-Dichloroethane
0.0454
0.0050
mg/kg wet
0.05000
91
74-127
1,1-Dichloroethylene
0.0425
0.0050
mg/kg wet
0.05000
85
67-149
1, 1 -Dichloropropylene
0.0444
0.0050
mg/kg wet
0.05000
89
71-130
1,2,3-Trichlorobenzene
0.0480
0.010
mg/kg wet
0.05000
96
68-130
1,2,3-Trichloropropane
0.0462
0.0050
mg/kg wet
0.05000
92
60-137
1,2,4-Trichlorobenzene
0.0484
0.010
mg/kg wet
0.05000
97
66-125
1,2,4-Trimethylbenzene
0.0465
0.0050
mg/kg wet
0.05000
93
69-129
1,2-Dibromoethane
0.0454
0.0050
mg/kg wet
0.05000
91
70-132
1,2-Dichlorobenzene
0.0464
0.0050
mg/kg wet
0.05000
93
72-123
1,2-Dichloroethane
0.0424
0.0050
mg/kg wet
0.05000
85
68-128
1,2-Dichloropropane
0.0445
0.0050
mg/kg wet
0.05000
89
73-130
1,3,5-Trimethylbenzene
0.0551
0.0050
mg/kg wet
0.05000
110
69-128
1,3-Dichlorobenzene
0.0464
0.0050
mg/kg wet
0.05000
93
71-120
1,3-Dichloropropane
0.0447
0.0050
mg/kg wet
0.05000
89
75-124
1,4-Dichlorobenzene
0.0464
0.0050
mg/kg wet
0.05000
93
71-123
2,2-Dichloropropane
0.0446
0.0050
mg/kg wet
0.05000
89
50-142
2-Chlorotoluene
0.0463
0.0050
mg/kg wet
0.05000
93
67-124
4-Chlorotoluene
0.0463
0.0050
mg/kg wet
0.05000
93
71-126
4-Isopropyltoluene
0.0469
0.0050
mg/kg wet
0.05000
94
68-129
Acetone
0.0754
0.020
mg/kg wet
0.1000
75
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POB0017 - 5035
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POB0017-BS1)
Prepared &Analyzed: 02/03/20
Benzene
0.0448
0.0050
mg/kg wet
0.05000
90
74-127
Bromobenzene
0.0460
0.0050
mg/kg wet
0.05000
92
73-125
Bromochloromethane
0.0444
0.0050
mg/kg wet
0.05000
89
72-134
Bromodichloromethane
0.0448
0.0050
mg/kg wet
0.05000
90
75-122
Bromoform
0.0472
0.0050
mg/kg wet
0.05000
94
66-135
Bromomethane
0.0436
0.010
mg/kg wet
0.05000
87
20-180
Carbon Tetrachloride
0.0435
0.0050
mg/kg wet
0.05000
87
64-143
Chlorobenzene
0.0453
0.0050
mg/kg wet
0.05000
91
74-118
Chloroethane
0.0531
0.010
mg/kg wet
0.05000
106
33-149
Chloroform
0.0451
0.0050
mg/kg wet
0.05000
90
73-127
Chloromethane
0.0379
0.010
mg/kg wet
0.05000
76
45-143
cis-1,2-Dichloroethylene
0.0432
0.0050
mg/kg wet
0.05000
86
76-134
cis-1,3-Dichloropropylene
0.0451
0.0050
mg/kg wet
0.05000
90
71-125
Dibromochloromethane
0.0461
0.0050
mg/kg wet
0.05000
92
73-122
Dichlorodifluoromethane
0.0382
0.010
mg/kg wet
0.05000
76
26-146
Ethylbenzene
0.0456
0.0050
mg/kg wet
0.05000
91
74-128
Isopropyl Ether
0.0424
0.0050
mg/kg wet
0.05000
85
59-159
Isopropylbenzene (Cumene)
0.0474
0.0050
mg/kg wet
0.05000
95
68-126
m,p-Xylenes
0.0920
0.010
mg/kg wet
0.1000
92
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0442
0.020
mg/kg wet
0.05000
88
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0367
0.020
mg/kg wet
0.05000
73
63-149
Methyl Isobutyl Ketone
0.0422
0.020
mg/kg wet
0.05000
84
57-162
Methylene Chloride
0.0418
0.0050
mg/kg wet
0.05000
84
74-129
Methyl-tert-Butyl Ether
0.0447
0.0050
mg/kg wet
0.05000
89
70-130
Naphthalene
0.0457
0.010
mg/kg wet
0.05000
91
57-157
n-Butylbenzene
0.0472
0.0050
mg/kg wet
0.05000
94
65-135
n-Propylbenzene
0.0459
0.0050
mg/kg wet
0.05000
92
67-130
o-Xylene
0.0450
0.0050
mg/kg wet
0.05000
90
74-126
sec-Butylbenzene
0.0460
0.0050
mg/kg wet
0.05000
92
66-131
Styrene
0.0462
0.0050
mg/kg wet
0.05000
92
77-121
tert-Butyl benzene
0.0459
0.0050
mg/kg wet
0.05000
92
67-132
Tetrachloroethylene
0.0464
0.0050
mg/kg wet
0.05000
93
68-130
Toluene
0.0453
0.0050
mg/kg wet
0.05000
91
71-129
trans- 1,2-Dichloroethylene
0.0428
0.0050
mg/kg wet
0.05000
86
73-132
trans- 1,3-Dichloropropylene
0.0455
0.0050
mg/kg wet
0.05000
91
68-123
Trichloroethylene
0.0464
0.0050
mg/kg wet
0.05000
93
75-133
Trichlorofluoromethane
0.0456
0.010
mg/kg wet
0.05000
91
44-146
Vinyl acetate
0.0363
0.010
mg/kg wet
0.05000
73
85-161
Vinyl chloride
0.0443
0.010
mg/kg wet
0.05000
89
48-147
Xylenes, total
0.137
0.015
mg/kg wet
0.1500
91
74-126
Surrogate:4-Bromofluorobenzene
50.0
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
49.1
ug/L
50.00
98
84-123
Surrogate: Toluene-d8
49.9
ug/L
50.00
100
76-129
L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POB0017 - 5035
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (POB0017-MS1)
Source: 0010326-03
Prepared & Analyzed: 02/03/20
1,1,1,2-Tetrachloroethane
0.0471
0.0076
mg/kg dry
0.07564
BRL
62
60-120
1,1,1-Trichloroethane
0.0518
0.0076
mg/kg dry
0.07564
BRL
69
52-139
1,1,2,2-Tetrachloroethane
0.0404
0.0076
mg/kg dry
0.07564
BRL
53
39-135
1,1,2-Trichloroethane
0.0433
0.0076
mg/kg dry
0.07564
BRL
57
44-140
1,1-Dichloroethane
0.0511
0.0076
mg/kg dry
0.07564
BRL
68
59-137
1,1-Dichloroethylene
0.0520
0.0076
mg/kg dry
0.07564
BRL
69
54-162
1, 1 -Dichloropropylene
0.0533
0.0076
mg/kg dry
0.07564
BRL
70
55-137
1,2,3-Trichlorobenzene
0.0451
0.015
mg/kg dry
0.07564
BRL
60
34-120
1,2,3-Trichloropropane
0.0412
0.0076
mg/kg dry
0.07564
BRL
54
45-139
1,2,4-Trichlorobenzene
0.0449
0.015
mg/kg dry
0.07564
BRL
59
35-116
1,2,4-Trimethylbenzene
0.0494
0.0076
mg/kg dry
0.07564
BRL
65
38-142
1,2-Dibromoethane
0.0421
0.0076
mg/kg dry
0.07564
BRL
56
49-132
1,2-Dichlorobenzene
0.0457
0.0076
mg/kg dry
0.07564
BRL
60
42-130
1,2-Dichloroethane
0.0429
0.0076
mg/kg dry
0.07564
BRL
57
51-131
1,2-Dichloropropane
0.0477
0.0076
mg/kg dry
0.07564
BRL
63
55-138
1,3,5-Trimethylbenzene
0.0602
0.0076
mg/kg dry
0.07564
BRL
80
44-140
1,3-Dichlorobenzene
0.0467
0.0076
mg/kg dry
0.07564
BRL
62
41-129
1,3-Dichloropropane
0.0431
0.0076
mg/kg dry
0.07564
BRL
57
53-129
1,4-Dichlorobenzene
0.0460
0.0076
mg/kg dry
0.07564
BRL
61
44-134
2,2-Dichloropropane
0.0520
0.0076
mg/kg dry
0.07564
BRL
69
30-147
2-Chlorotoluene
0.0481
0.0076
mg/kg dry
0.07564
BRL
64
46-132
4-Chlorotoluene
0.0481
0.0076
mg/kg dry
0.07564
BRL
64
44-135
4-Isopropyltoluene
0.0503
0.0076
mg/kg dry
0.07564
BRL
66
32-144
Acetone
0.0646
0.030
mg/kg dry
0.1513
BRL
43
34-143
Benzene
0.0497
0.0076
mg/kg dry
0.07564
BRL
66
60-135
Bromobenzene
0.0466
0.0076
mg/kg dry
0.07564
BRL
62
45-135
Bromochloromethane
0.0454
0.0076
mg/kg dry
0.07564
BRL
60
55-136
Bromodichloromethane
0.0462
0.0076
mg/kg dry
0.07564
BRL
61
55-127
Bromoform
0.0405
0.0076
mg/kg dry
0.07564
BRL
54
40-136
Bromomethane
0.0428
0.015
mg/kg dry
0.07564
BRL
57
30-137
Carbon Tetrachloride
0.0513
0.0076
mg/kg dry
0.07564
BRL
68
48-153
Chlorobenzene
0.0472
0.0076
mg/kg dry
0.07564
BRL
62
57-125
Chloroethane
0.0677
0.015
mg/kg dry
0.07564
BRL
90
16-177
Chloroform
0.0492
0.0076
mg/kg dry
0.07564
BRL
65
56-137
Chloromethane
0.0478
0.015
mg/kg dry
0.07564
BRL
63
40-145
cis-1,2-Dichloroethylene
0.0478
0.0076
mg/kg dry
0.07564
BRL
63
58-140
cis-1,3-Dichloropropylene
0.0455
0.0076
mg/kg dry
0.07564
BRL
60
42-135
Dibromochloromethane
0.0432
0.0076
mg/kg dry
0.07564
BRL
57
49-127
Dichlorodifluoromethane
0.0470
0.015
mg/kg dry
0.07564
BRL
62
25-151
Ethylbenzene
0.0495
0.0076
mg/kg dry
0.07564
BRL
65
44-144
Isopropyl Ether
0.0444
0.0076
mg/kg dry
0.07564
BRL
59
51-155
Isopropylbenzene (Cumene)
0.0518
0.0076
mg/kg dry
0.07564
BRL
68
41-140
m,p-Xylenes
0.0996
0.015
mg/kg dry
0.1513
BRL
66
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0350
0.030
mg/kg dry
0.07564
BRL
46
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0305
0.030
mg/kg dry
0.07564
BRL
40
24-160
Methyl Isobutyl Ketone
0.0367
0.030
mg/kg dry
0.07564
BRL
49
25-163
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

�
Level II QC Report
�
Waypoint.
2/6/20
ANALYTICAL
Geoscience Group
Project: Sedgefield
Work Order: 0010326
Attn: Tom Hassett
Time Submitted:
1/23/2020 11:54:OOAM
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Reporting
Spike
Source
%REC RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits RPD Limit Notes
Batch POB0017 - 5035
Matrix Spike (POB0017-MS1)
Source: 0010326-03
Prepared & Analyzed: 02/03/20
Methylene Chloride
0.0463
0.0076
mg/kg dry
0.07564
BRL
61
53-144
Methyl-tert-Butyl Ether
0.0436
0.0076
mg/kg dry
0.07564
BRL
58
49-135
Naphthalene
0.0430
0.015
mg/kg dry
0.07564
BRL
57
32-127
n-Butylbenzene
0.0506
0.0076
mg/kg dry
0.07564
BRL
67
23-148
n-Propylbenzene
0.0501
0.0076
mg/kg dry
0.07564
BRL
66
35-144
o-Xylene
0.0480
0.0076
mg/kg dry
0.07564
BRL
63
43-143
sec-Butylbenzene
0.0506
0.0076
mg/kg dry
0.07564
BRL
67
34-144
Styrene
0.0472
0.0076
mg/kg dry
0.07564
BRL
62
42-132
tert-Butyl benzene
0.0504
0.0076
mg/kg dry
0.07564
BRL
67
36-150
Tetrachloroethylene
0.0535
0.0076
mg/kg dry
0.07564
BRL
71
47-142
Toluene
0.0500
0.0076
mg/kg dry
0.07564
BRL
66
57-135
trans- 1,2-Dichloroethylene
0.0498
0.0076
mg/kg dry
0.07564
BRL
66
58-141
trans- 1,3-Dichloropropylene
0.0442
0.0076
mg/kg dry
0.07564
BRL
58
41-124
Trichloroethylene
0.0503
0.0076
mg/kg dry
0.07564
BRL
67
38-164
Trichlorofluoromethane
0.0567
0.015
mg/kg dry
0.07564
BRL
75
30-157
Vinyl acetate
0.0362
0.015
mg/kg dry
0.07564
BRL
48
61-154 M
Vinyl chloride
0.0572
0.015
mg/kg dry
0.07564
BRL
76
40-156
Xylenes, total
0.148
0.023
mg/kg dry
0.2269
BRL
65
36-148
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
50.0
ug/L
50.00
100
84-123
Surrogate: Toluene-d8
49.2
ug/L
50.00
98
76-129
Matrix Spike Dup (POB0017-MSD1)
Source: 0010326-03
Prepared & Analyzed: 02/03/20
1,1,1,2-Tetrachloroethane
0.0430
0.0076
mg/kg dry
0.07564
BRL
57
60-120
9
15 M
1,1,1-Trichloroethane
0.0451
0.0076
mg/kg dry
0.07564
BRL
60
52-139
14
21
1,1,2,2-Tetrachloroethane
0.0374
0.0076
mg/kg dry
0.07564
BRL
49
39-135
8
22
1,1,2-Trichloroethane
0.0404
0.0076
mg/kg dry
0.07564
BRL
53
44-140
7
21
1,1-Dichloroethane
0.0444
0.0076
mg/kg dry
0.07564
BRL
59
59-137
14
21
1,1-Dichloroethylene
0.0454
0.0076
mg/kg dry
0.07564
BRL
60
54-162
14
22
1, 1 -Dichloropropylene
0.0455
0.0076
mg/kg dry
0.07564
BRL
60
55-137
16
19
1,2,3-Trichlorobenzene
0.0408
0.015
mg/kg dry
0.07564
BRL
54
34-120
10
41
1,2,3-Trichloropropane
0.0375
0.0076
mg/kg dry
0.07564
BRL
50
45-139
9
25
1,2,4-Trichlorobenzene
0.0405
0.015
mg/kg dry
0.07564
BRL
54
35-116
10
62
1,2,4-Trimethylbenzene
0.0426
0.0076
mg/kg dry
0.07564
BRL
56
38-142
15
24
1,2-Dibromoethane
0.0395
0.0076
mg/kg dry
0.07564
BRL
52
49-132
6
15
1,2-Dichlorobenzene
0.0408
0.0076
mg/kg dry
0.07564
BRL
54
42-130
11
21
1,2-Dichloroethane
0.0391
0.0076
mg/kg dry
0.07564
BRL
52
51-131
9
13
1,2-Dichloropropane
0.0416
0.0076
mg/kg dry
0.07564
BRL
55
55-138
14
16
1,3,5-Trimethylbenzene
0.0525
0.0076
mg/kg dry
0.07564
BRL
69
44-140
14
29
1,3-Dichlorobenzene
0.0408
0.0076
mg/kg dry
0.07564
BRL
54
41-129
13
24
1,3-Dichloropropane
0.0395
0.0076
mg/kg dry
0.07564
BRL
52
53-129
9
15 M
1,4-Dichlorobenzene
0.0410
0.0076
mg/kg dry
0.07564
BRL
54
44-134
11
21
2,2-Dichloropropane
0.0453
0.0076
mg/kg dry
0.07564
BRL
60
30-147
14
20
2-Chlorotoluene
0.0420
0.0076
mg/kg dry
0.07564
BRL
56
46-132
14
29
4-Chlorotoluene
0.0420
0.0076
mg/kg dry
0.07564
BRL
56
44-135
14
23
4-Isopropyltoluene
0.0434
0.0076
mg/kg dry
0.07564
BRL
57
32-144
15
22
Acetone
0.0602
0.030
mg/kg dry
0.1513
BRL
40
34-143
7
49 M
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POB0017 - 5035
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POB0017-MSD1)
Source: 0010326-03
Prepared & Analyzed: 02/03/20
Benzene
0.0440
0.0076
mg/kg dry
0.07564
BRL
58
60-135
12
20
Bromobenzene
0.0414
0.0076
mg/kg dry
0.07564
BRL
55
45-135
12
25
Bromochloromethane
0.0416
0.0076
mg/kg dry
0.07564
BRL
55
55-136
9
18
Bromodichloromethane
0.0407
0.0076
mg/kg dry
0.07564
BRL
54
55-127
13
17
Bromoform
0.0391
0.0076
mg/kg dry
0.07564
BRL
52
40-136
3
35
Bromomethane
0.0396
0.015
mg/kg dry
0.07564
BRL
52
30-137
8
30
Carbon Tetrachloride
0.0433
0.0076
mg/kg dry
0.07564
BRL
57
48-153
17
23
Chlorobenzene
0.0420
0.0076
mg/kg dry
0.07564
BRL
56
57-125
12
14
Chloroethane
0.0595
0.015
mg/kg dry
0.07564
BRL
79
16-177
13
47
Chloroform
0.0439
0.0076
mg/kg dry
0.07564
BRL
58
56-137
12
18
Chloromethane
0.0423
0.015
mg/kg dry
0.07564
BRL
56
40-145
12
26
cis-1,2-Dichloroethylene
0.0426
0.0076
mg/kg dry
0.07564
BRL
56
58-140
12
28
cis-1,3-Dichloropropylene
0.0410
0.0076
mg/kg dry
0.07564
BRL
54
42-135
11
32
Dibromochloromethane
0.0400
0.0076
mg/kg dry
0.07564
BRL
53
49-127
8
24
Dichlorodifluoromethane
0.0407
0.015
mg/kg dry
0.07564
BRL
54
25-151
14
37
Ethylbenzene
0.0435
0.0076
mg/kg dry
0.07564
BRL
58
44-144
13
19
Isopropyl Ether
0.0398
0.0076
mg/kg dry
0.07564
BRL
53
51-155
11
13
Isopropylbenzene (Cumene)
0.0451
0.0076
mg/kg dry
0.07564
BRL
60
41-140
14
27
m,p-Xylenes
0.0879
0.015
mg/kg dry
0.1513
BRL
58
36-148
13
20
Methyl Butyl Ketone (2-Hexanone)
0.0343
0.030
mg/kg dry
0.07564
BRL
45
30-147
2
42
Methyl Ethyl Ketone (2-Butanone)
0.0291
0.030
mg/kg dry
0.07564
BRL
38
24-160
5
42
Methyl Isobutyl Ketone
0.0350
0.030
mg/kg dry
0.07564
BRL
46
25-163
5
44
Methylene Chloride
0.0413
0.0076
mg/kg dry
0.07564
BRL
55
53-144
11
14
Methyl-tert-Butyl Ether
0.0403
0.0076
mg/kg dry
0.07564
BRL
53
49-135
8
22
Naphthalene
0.0394
0.015
mg/kg dry
0.07564
BRL
52
32-127
9
44
n-Butylbenzene
0.0435
0.0076
mg/kg dry
0.07564
BRL
58
23-148
15
39
n-Propylbenzene
0.0430
0.0076
mg/kg dry
0.07564
BRL
57
35-144
15
27
o-Xylene
0.0424
0.0076
mg/kg dry
0.07564
BRL
56
43-143
12
17
sec-Butylbenzene
0.0439
0.0076
mg/kg dry
0.07564
BRL
58
34-144
14
28
Styrene
0.0423
0.0076
mg/kg dry
0.07564
BRL
56
42-132
11
28
tert-Butyl benzene
0.0438
0.0076
mg/kg dry
0.07564
BRL
58
36-150
14
29
Tetrachloroethylene
0.0459
0.0076
mg/kg dry
0.07564
BRL
61
47-142
15
26
Toluene
0.0431
0.0076
mg/kg dry
0.07564
BRL
57
57-135
15
22
trans- 1,2-Dichloroethylene
0.0437
0.0076
mg/kg dry
0.07564
BRL
58
58-141
13
18
trans- 1,3-Dichloropropylene
0.0402
0.0076
mg/kg dry
0.07564
BRL
53
41-124
10
20
Trichloroethylene
0.0433
0.0076
mg/kg dry
0.07564
BRL
57
38-164
15
18
Trichlorofluoromethane
0.0489
0.015
mg/kg dry
0.07564
BRL
65
30-157
15
27
Vinyl acetate
0.0312
0.015
mg/kg dry
0.07564
BRL
41
61-154
15
35
Vinyl chloride
0.0482
0.015
mg/kg dry
0.07564
BRL
64
40-156
17
35
Xylenes, total
0.130
0.023
mg/kg dry
0.2269
BRL
57
36-148
12
20
Surrogate:4-Bromofluorobenzene
49.5
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
50.2
ug/L
50.00
100
84-123
Surrogate: Toluene-d8
49.1
ug/L
50.00
98
76-129
A]
in
M
M
M
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0489 - 3546
Blank (POA0489-BLK1)
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyl naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl naphthalene
2-Methylphenol
2-Nitrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
2.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
Prepared:01/29/20 Analyzed: 01/31/20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0489 - 3546
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0489-BLK1)
Prepared: 01/29/20 Analyzed: 01/31/20
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
4.01
mg/kg wet
3.333
120
39-132
Surrogate: 2-Fluorobiphenyl
1.62
mg/kg wet
1.667
97
44-115
Surrogate: 2-Fluorophenol
3.39
mg/kg wet
3.333
102
35-115
Surrogate: Nitrobenzene-d5
1.48
mg/kg wet
1.667
89
37-122
Surrogate: Phenol-d5
3.27
mg/kg wet
3.333
98
34-121
Surrogate: Terphenyl-04
1.85
mg/kg wet
1.667
111
54-127
LCS (POA0489-BS1)
Prepared: 01/29/20 Analyzed: 01/31/20
1,2,4-Trichlorobenzene
1.32
0.66
mg/kg wet
1.667
79
34-118
1,2-Dichlorobenzene
1.32
0.66
mg/kg wet
1.667
79
33-117
1,3-Dichlorobenzene
1.31
0.66
mg/kg wet
1.667
78
30-115
1,4-Dichlorobenzene
1.29
0.33
mg/kg wet
1.667
77
31-115
1-Methyl naphthalene
1.46
0.66
mg/kg wet
1.667
87
40-119
2,4,5-Trichlorophenol
1.63
0.66
mg/kg wet
1.667
98
62-124
2,4,6-Trichlorophenol
1.67
0.66
mg/kg wet
1.667
100
39-126
2,4-Dichlorophenol
1.40
0.66
mg/kg wet
1.667
84
40-122
2,4-Dimethylphenol
1.61
0.33
mg/kg wet
1.667
97
30-127
2,4-Dinitrophenol
1.45
1.5
mg/kg wet
1.667
87
27-129 J
2,4-Dinitrotoluene
1.69
0.66
mg/kg wet
1.667
101
48-126
2,6-Dinitrotoluene
1.65
0.66
mg/kg wet
1.667
99
46-124
2-Chloronaphthalene
1.48
0.66
mg/kg wet
1.667
89
41-114
2-Chlorophenol
1.50
0.66
mg/kg wet
1.667
90
34-121
2-Methyl naphthalene
1.37
0.66
mg/kg wet
1.667
82
38-122
2-Methylphenol
1.55
0.66
mg/kg wet
1.667
93
32-122
2-Nitrophenol
1.37
0.66
mg/kg wet
1.667
82
36-123
3,3'-Dichlorobenzidine
1.60
0.66
mg/kg wet
1.667
96
22-121
3/4-Methyl phenol
1.41
0.66
mg/kg wet
1.667
85
34-119
4,6-Dinitro-2-methylphenol
1.72
1.5
mg/kg wet
1.667
104
29-132
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0489 - 3546
LCS (POA0489-BSI)
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,hJ)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B i s(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a, h )anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate: 2, 4, 6-Tribromophenol
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Prepared:01/29/20 Analyzed: 01/31/20
1.61
0.66
mg/kg wet
1.667
97
46-124
1.48
0.66
mg/kg wet
1.667
89
45-122
1.15
0.33
mg/kg wet
1.667
69
17-106
1.52
1.0
mg/kg wet
1.667
91
45-121
1.84
0.66
mg/kg wet
1.667
ill
30-132
1.57
0.66
mg/kg wet
1.667
94
40-123
1.66
0.66
mg/kg wet
1.667
99
32-132
1.64
0.66
mg/kg wet
1.667
99
47-123
1.62
0.66
mg/kg wet
1.667
97
39-125
1.69
0.66
mg/kg wet
1.667
102
49-126
1.91
0.66
mg/kg wet
1.667
115
45-129
1.77
0.66
mg/kg wet
1.667
106
45-132
1.86
0.66
mg/kg wet
1.667
112
43-134
1.87
0.66
mg/kg wet
1.667
112
47-132
1.15
2.0
mg/kg wet
1.667
69
10-83
1.48
0.66
mg/kg wet
1.667
89
29-122
1.26
0.66
mg/kg wet
1.667
76
36-121
1.15
0.66
mg/kg wet
1.667
69
31-120
1.19
0.33
mg/kg wet
1.667
71
33-131
1.80
0.66
mg/kg wet
1.667
108
51-133
1.70
0.33
mg/kg wet
1.667
102
48-132
1.75
0.66
mg/kg wet
1.667
105
50-124
1.31
0.66
mg/kg wet
1.667
79
45-134
1.52
0.66
mg/kg wet
1.667
91
44-120
1.54
0.66
mg/kg wet
1.667
92
50-124
1.50
0.66
mg/kg wet
1.667
90
48-124
1.70
0.66
mg/kg wet
1.667
102
51-128
1.86
0.33
mg/kg wet
1.667
112
45-140
1.66
0.66
mg/kg wet
1.667
100
50-127
1.57
0.66
mg/kg wet
1.667
94
43-125
1.56
0.66
mg/kg wet
1.667
94
45-122
1.39
0.66
mg/kg wet
1.667
83
32-123
1.47
0.66
mg/kg wet
1.667
88
32-117
1.25
0.66
mg/kg wet
1.667
75
28-117
2.11
0.66
mg/kg wet
1.667
126
45-133
1.07
0.66
mg/kg wet
1.667
64
30-122
1.30
0.66
mg/kg wet
1.667
78
35-123
1.16
0.33
mg/kg wet
1.667
69
34-122
1.46
0.66
mg/kg wet
1.667
88
36-120
1.98
0.66
mg/kg wet
1.667
119
38-127
1.63
1.0
mg/kg wet
1.667
98
25-133
1.62
0.66
mg/kg wet
1.667
97
50-121
1.48
0.66
mg/kg wet
1.667
89
34-121
1.84
0.66
mg/kg wet
1.667
110
47-127
0.782
0.33
mg/kg wet
1.667
47
10-60
3.52
mg/kg wet
3.333
106
39-132
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0489 - 3546
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POA0489-BS1)
Prepared: 01/29/20 Analyzed: 01/31/20
Surrogate: 2-Fluorobiphenyl
1.46
mg/kg wet
1.667
88
44-115
Surrogate: 2-Fluorophenol
3.08
mg/kg wet
3.333
92
35-115
Surrogate: Nitrobenzene-d5
1.25
mg/kg wet
1.667
75
37-122
Surrogate: Phenol-d5
2.89
mg/kg wet
3.333
87
34-121
Surrogate: Terphenyl-04
1.68
mg/kg wet
1.667
101
54-127
Matrix Spike (POA0489-MS1)
Source: 0010326-05
Prepared: 01/29/20 Analyzed: 01/31/20
1,2,4-Trichlorobenzene
1.96
0.96
mg/kg dry
2.432
BRL
81
34-118
1,2-Dichlorobenzene
2.06
0.96
mg/kg dry
2.432
BRL
85
33-117
1,3-Dichlorobenzene
2.02
0.96
mg/kg dry
2.432
BRL
83
30-115
1,4-Dichlorobenzene
2.01
0.48
mg/kg dry
2.432
BRL
83
31-115
1-Methyl naphthalene
2.17
0.96
mg/kg dry
2.432
BRL
89
40-119
2,4,5-Trichlorophenol
2.60
0.96
mg/kg dry
2.432
BRL
107
45-121
2,4,6-Trichlorophenol
2.53
0.96
mg/kg dry
2.432
BRL
104
39-126
2,4-Dichlorophenol
2.15
0.96
mg/kg dry
2.432
BRL
88
40-122
2,4-Dimethylphenol
2.24
0.48
mg/kg dry
2.432
BRL
92
30-127
2,4-Dinitrophenol
2.53
2.2
mg/kg dry
2.432
BRL
104
27-129
2,4-Dinitrotoluene
2.64
0.96
mg/kg dry
2.432
BRL
109
48-126
2,6-Dinitrotoluene
2.59
0.96
mg/kg dry
2.432
BRL
107
46-124
2-Chloronaphthalene
2.32
0.96
mg/kg dry
2.432
BRL
95
41-114
2-Chlorophenol
2.27
0.96
mg/kg dry
2.432
BRL
93
34-121
2-Methyl naphthalene
2.05
0.96
mg/kg dry
2.432
BRL
84
38-122
2-Methylphenol
2.36
0.96
mg/kg dry
2.432
BRL
97
32-122
2-Nitrophenol
2.02
0.96
mg/kg dry
2.432
BRL
83
36-123
3,3'-Dichlorobenzidine
2.02
0.96
mg/kg dry
2.432
BRL
83
22-121
3/4-Methyl phenol
2.15
0.96
mg/kg dry
2.432
BRL
88
34-119
4,6-Dinitro-2-methylphenol
2.80
2.2
mg/kg dry
2.432
BRL
115
29-132
4-Bromophenyl phenyl ether
2.40
0.96
mg/kg dry
2.432
BRL
99
46-124
4-Chloro-3-methylphenol
2.25
0.96
mg/kg dry
2.432
BRL
92
45-122
4-Chloroaniline
1.64
0.48
mg/kg dry
2.432
BRL
67
17-106
4-Chlorophenyl phenyl ether
2.36
1.5
mg/kg dry
2.432
BRL
97
45-121
4-Nitrophenol
3.14
0.96
mg/kg dry
2.432
BRL
129
30-132
Acenaphthene
2.38
0.96
mg/kg dry
2.432
BRL
98
40-123
Acenaphthylene
2.60
0.96
mg/kg dry
2.432
BRL
107
32-132
Anthracene
2.54
0.96
mg/kg dry
2.432
BRL
104
47-123
Azobenzene
2.49
0.96
mg/kg dry
2.432
BRL
102
39-125
Benzo(a)anthracene
2.60
0.96
mg/kg dry
2.432
BRL
107
49-126
Benzo(a)pyrene
2.86
0.96
mg/kg dry
2.432
BRL
118
45-129
Benzo(b)fluoranthene
2.88
0.96
mg/kg dry
2.432
BRL
119
45-132
Benzo(g,h,i)perylene
2.87
0.96
mg/kg dry
2.432
BRL
118
43-134
Benzo(k)fluoranthene
2.70
0.96
mg/kg dry
2.432
BRL
111
47-132
Benzoic Acid
2.38
2.9
mg/kg dry
2.432
BRL
98
10-83 M, J
Benzyl alcohol
2.21
0.96
mg/kg dry
2.432
BRL
91
29-122
bis(2-Chloroethoxy)methane
1.89
0.96
mg/kg dry
2.432
BRL
78
36-121
Bis(2-Chloroethyl)ether
2.11
0.96
mg/kg dry
2.432
BRL
87
31-120
Bis(2-chloroisopropyl)ether
1.81
0.48
mg/kg dry
2.432
BRL
74
33-131
Bis(2-Ethylhexyl)phthalate
2.72
0.96
mg/kg dry
2.432
BRL
112
51-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0489 - 3546
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (POA0489-MS1)
Source: 0010326-05
Prepared: 01/29/20 Analyzed: 01/31/20
Butyl benzyl phthalate
2.66
0.48
mg/kg dry
2.432
BRL
109
48-132
Chrysene
2.80
0.96
mg/kg dry
2.432
BRL
115
50-124
Dibenzo(a,h)anthracene
3.07
0.96
mg/kg dry
2.432
BRL
126
45-134
Dibenzofuran
2.39
0.96
mg/kg dry
2.432
BRL
98
44-120
Diethyl phthalate
2.41
0.96
mg/kg dry
2.432
BRL
99
50-124
Dimethyl phthalate
2.33
0.96
mg/kg dry
2.432
BRL
96
48-124
Di-n-butyl phthalate
2.60
0.96
mg/kg dry
2.432
BRL
107
51-128
Di-n-octyl phthalate
2.85
0.48
mg/kg dry
2.432
BRL
117
45-140
Fluoranthene
2.53
0.96
mg/kg dry
2.432
BRL
104
50-127
Fluorene
2.49
0.96
mg/kg dry
2.432
BRL
102
43-125
Hexachlorobenzene
2.37
0.96
mg/kg dry
2.432
BRL
97
45-122
Hexachlorobutadiene
2.05
0.96
mg/kg dry
2.432
BRL
84
32-123
Hexachlorocyclopentadiene
2.41
0.96
mg/kg dry
2.432
BRL
99
32-117
Hexachloroethane
1.96
0.96
mg/kg dry
2.432
BRL
80
28-117
Indeno(1,2,3-cd)pyrene
2.76
0.96
mg/kg dry
2.432
BRL
114
45-133
Isophorone
1.62
0.96
mg/kg dry
2.432
BRL
66
30-122
Naphthalene
1.96
0.96
mg/kg dry
2.432
BRL
81
35-123
Nitrobenzene
1.73
0.48
mg/kg dry
2.432
BRL
71
34-122
N-Nitroso-di-n-propylamine
2.22
0.96
mg/kg dry
2.432
BRL
91
36-120
N-Nitrosodiphenylamine
2.89
0.96
mg/kg dry
2.432
BRL
119
38-127
Pentachlorophenol
2.73
1.5
mg/kg dry
2.432
BRL
112
25-133
Phenanthrene
2.47
0.96
mg/kg dry
2.432
BRL
102
50-121
Phenol
2.18
0.96
mg/kg dry
2.432
BRL
90
34-121
Pyrene
2.81
0.96
mg/kg dry
2.432
BRL
115
47-127
Pyridine
0.564
0.48
mg/kg dry
2.432
BRL
23
20-150
Surrogate: 2,4,6-Trlbromophenol
5.45
mg/kg dry
4.864
112
39-132
Surrogate: 2-Fluorobiphenyl
2.21
mg/kg dry
2.432
91
44-115
Surrogate: 2-Fluorophenol
4.48
mg/kg dry
4.864
92
35-115
Surrogate: Nitrobenzene-d5
1.79
mg/kg dry
2.432
74
37-122
Surrogate: Phenol-d5
4.29
mg/kg dry
4.864
88
34-121
Surrogate: Terphenyl-d14
2.54
mg/kg dry
2.432
104
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0489 - 3546
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POA0489-MSD1)
Source: 0010326-05
Prepared: 01/29/20 Analyzed: 01/31/20
1,2,4-Trichlorobenzene
1.73
0.96
mg/kg dry
2.430
BRL
71
34-118
13
20
1,2-Dichlorobenzene
1.72
0.96
mg/kg dry
2.430
BRL
71
33-117
18
20
1,3-Dichlorobenzene
1.68
0.96
mg/kg dry
2.430
BRL
69
30-115
18
20
1,4-Dichlorobenzene
1.66
0.48
mg/kg dry
2.430
BRL
68
31-115
19
20
1-Methyl naphthalene
1.89
0.96
mg/kg dry
2.430
BRL
78
40-119
14
20
2,4,5-Trichlorophenol
2.24
0.96
mg/kg dry
2.430
BRL
92
45-121
15
35
2,4,6-Trichlorophenol
2.29
0.96
mg/kg dry
2.430
BRL
94
39-126
10
20
2,4-Dichlorophenol
1.86
0.96
mg/kg dry
2.430
BRL
77
40-122
14
20
2,4-Dimethylphenol
2.04
0.48
mg/kg dry
2.430
BRL
84
30-127
9
20
2,4-Dinitrophenol
2.18
2.2
mg/kg dry
2.430
BRL
90
27-129
15
20
2,4-Dinitrotoluene
2.32
0.96
mg/kg dry
2.430
BRL
95
48-126
13
20
2,6-Dinitrotoluene
2.23
0.96
mg/kg dry
2.430
BRL
92
46-124
15
20
2-Chloronaphthalene
1.99
0.96
mg/kg dry
2.430
BRL
82
41-114
15
20
2-Chlorophenol
1.90
0.96
mg/kg dry
2.430
BRL
78
34-121
18
20
2-Methyl naphthalene
1.78
0.96
mg/kg dry
2.430
BRL
73
38-122
14
20
2-Methylphenol
2.00
0.96
mg/kg dry
2.430
BRL
82
32-122
17
20
2-Nitrophenol
1.81
0.96
mg/kg dry
2.430
BRL
74
36-123
11
20
3,3'-Dichlorobenzidine
2.08
0.96
mg/kg dry
2.430
BRL
86
22-121
3
20
3/4-Methyl phenol
1.81
0.96
mg/kg dry
2.430
BRL
74
34-119
17
20
4,6-Dinitro-2-methylphenol
2.44
2.2
mg/kg dry
2.430
BRL
100
29-132
14
20
4-Bromophenyl phenyl ether
2.13
0.96
mg/kg dry
2.430
BRL
88
46-124
12
20
4-Chloro-3-methylphenol
1.93
0.96
mg/kg dry
2.430
BRL
79
45-122
15
20
4-Chloroaniline
1.42
0.48
mg/kg dry
2.430
BRL
58
17-106
15
20
4-Chlorophenyl phenyl ether
2.05
1.5
mg/kg dry
2.430
BRL
84
45-121
14
20
4-Nitrophenol
2.71
0.96
mg/kg dry
2.430
BRL
111
30-132
15
20
Acenaphthene
2.14
0.96
mg/kg dry
2.430
BRL
88
40-123
11
20
Acenaphthylene
2.24
0.96
mg/kg dry
2.430
BRL
92
32-132
15
20
Anthracene
2.27
0.96
mg/kg dry
2.430
BRL
94
47-123
11
20
Azobenzene
2.17
0.96
mg/kg dry
2.430
BRL
89
39-125
14
20
Benzo(a)anthracene
2.33
0.96
mg/kg dry
2.430
BRL
96
49-126
11
20
Benzo(a)pyrene
2.55
0.96
mg/kg dry
2.430
BRL
105
45-129
12
20
Benzo(b)fluoranthene
2.44
0.96
mg/kg dry
2.430
BRL
101
45-132
17
20
Benzo(g,h,i)perylene
2.52
0.96
mg/kg dry
2.430
BRL
104
43-134
13
20
Benzo(k)fluoranthene
2.50
0.96
mg/kg dry
2.430
BRL
103
47-132
8
20
Benzoic Acid
2.10
2.9
mg/kg dry
2.430
BRL
87
10-83
12
20
Benzyl alcohol
1.91
0.96
mg/kg dry
2.430
BRL
78
29-122
15
20
bis(2-Chloroethoxy)methane
1.68
0.96
mg/kg dry
2.430
BRL
69
36-121
12
20
Bis(2-Chloroethyl)ether
1.81
0.96
mg/kg dry
2.430
BRL
74
31-120
15
20
Bis(2-chloroisopropyl)ether
1.55
0.48
mg/kg dry
2.430
BRL
64
33-131
15
20
Bis(2-Ethylhexyl)phthalate
2.47
0.96
mg/kg dry
2.430
BRL
102
51-133
10
20
Butyl benzyl phthalate
2.35
0.48
mg/kg dry
2.430
BRL
97
48-132
12
20
Chrysene
2.39
0.96
mg/kg dry
2.430
BRL
98
50-124
16
20
Dibenzo(a,h)anthracene
1.61
0.96
mg/kg dry
2.430
BRL
66
45-134
62
20
Dibenzofuran
2.07
0.96
mg/kg dry
2.430
BRL
85
44-120
14
20
Diethyl phthalate
2.09
0.96
mg/kg dry
2.430
BRL
86
50-124
14
20
Dimethyl phthalate
2.06
0.96
mg/kg dry
2.430
BRL
85
48-124
12
20
J
M,J
u
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0489 - 3546
Matrix Spike Dup (POA0489-M
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-N itrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate: 2, 4, 6-Tribromophenol
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluoro ph enol
Surrogate: Nitrobenzene-d5
Surrogate: Phenol-d5
Surrogate: Terphenyl-04
Source:0010326-05
Prepared:01/29/20 Analyzed: 01/31/20
2.29
0.96
mg/kg dry
2.430
BRL
94
51-128
2.53
0.48
mg/kg dry
2.430
BRL
104
45-140
2.26
0.96
mg/kg dry
2.430
BRL
93
50-127
2.16
0.96
mg/kg dry
2.430
BRL
89
43-125
2.12
0.96
mg/kg dry
2.430
BRL
87
45-122
1.78
0.96
mg/kg dry
2.430
BRL
73
32-123
2.06
0.96
mg/kg dry
2.430
BRL
85
32-117
1.61
0.96
mg/kg dry
2.430
BRL
66
28-117
2.78
0.96
mg/kg dry
2.430
BRL
114
45-133
1.43
0.96
mg/kg dry
2.430
BRL
59
30-122
1.69
0.96
mg/kg dry
2.430
BRL
70
35-123
1.52
0.48
mg/kg dry
2.430
BRL
62
34-122
1.87
0.96
mg/kg dry
2.430
BRL
77
36-120
2.62
0.96
mg/kg dry
2.430
BRL
108
38-127
2.41
1.5
mg/kg dry
2.430
BRL
99
25-133
2.22
0.96
mg/kg dry
2.430
BRL
91
50-121
1.85
0.96
mg/kg dry
2.430
BRL
76
34-121
2.49
0.96
mg/kg dry
2.430
BRL
103
47-127
0.490
0.48
mg/kg dry
2.430
BRL
20
20-150
4.80
mg/kg dry
4.861
99
39-132
1.92
mg/kg dry
2.430
79
44-115
3.82
mg/kg dry
4.861
79
35-115
1.61
mg/kg dry
2.430
66
37-122
3.64
mg/kg dry
4.861
75
34-121
2.24
mg/kg dry
2.430
92
54-127
12 20
12 20
12 20
14 20
11 20
14 20
16 20
19 20
0.5 20
12 20
15 20
13 20
17 20
10 20
12 20
11 20
17 20
12 20
14 60
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Analyte
Batch POA0482 - MADEP VPH (S
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0482-BLK1)
Prepared & Analyzed: 01/29/20
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-C12 Aliphatics
BRL
5.0
mg/kg wet
C9-C10 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
9740
ug/L
10000 97
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11700
ug/L
10000 117
70-130
LCS (POA0482-BS1)
Prepared &Analyzed: 01/29/20
C5-C8Aliphatics
39.4
5.0
mg/kg wet
32.00 123
70-130
C9-C10 Aromatics
9.79
5.0
mg/kg wet
10.67 92
70-130
C9-Cl2 Aliphatic
37.4
5.0
mg/kg wet
32.00 117
70-130
Surrogate: 2,5-Dibromotoluene (PID)
9580
ug/L
10000 96
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11400
ug/L
10000 114
70-130
LCS Dup (POA0482-BSD1)
Prepared &Analyzed: 01/29/20
C5-C8 Aliphatics
40.3
5.0
mg/kg wet
32.00 126
70-130 2 50
C9-C10 Aromatics
9.97
5.0
mg/kg wet
10.67 93
70-130 2 50
C9-Cl2 Aliphatic
37.0
5.0
mg/kg wet
32.00 116
70-130 1 50
Surrogate: 2,5-Dibromotoluene (PID)
9740
ug/L
10000 97
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11600
ug/L
10000 116
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Gasoline Range Organics by GC/FID - Quality Control
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0483 - 5030B Soil
Blank (POA0483-BLK1)
Prepared &Analyzed: 01/29/20
Gasoline Range Organics
BRL
5.0 mg/kg wet
Surrogate: a,a,a-Trifluorotoluene
5.00
mg/kg wet
5.000 100
50-137
LCS (POA0483-BS1)
Prepared &Analyzed: 01/29/20
Gasoline Range Organics
52.9
5.0 mg/kg wet
50.00 106
41-138
Surrogate: a,a,a-Trifluorotoluene
4.85
mg/kg wet
5.000 97
50-137
Matrix Spike (POA0483-MS1)
Source: 0010326-01
Prepared & Analyzed: 01/29/20
Gasoline Range Organics
68.5
6.6 mg/kg dry
66.23 3.44 98
41-138
Surrogate: a,a,a-Trifluorotoluene
4.70
mg/kg dry
6.623 71
50-137
Matrix Spike Dup (POA0483-MSD1)
Source: 0010326-01
Prepared: 01/29/20 Analyzed: 01/30/20
Gasoline Range Organics
61.1
6.6 mg/kg dry
66.23 3.44 87
41-138 11 34
Surrogate: a,a,a-Trifluorotoluene
4.50
mg/kg dry
6.623 68
50-137
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Analyte
Batch POA0439 - 3546
Reporting
Result Limit Units
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0439-BLK1)
Prepared: 01/27/20 Analyzed: 01/29/20
C9-Cl8 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C11-C22 Aromatics
BRL
25
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.33
mg/kg wet
2.000
66
40-140
Surrogate: o-Terphenyl
1.32
mg/kg wet
2.000
66
40-140
Surrogate: 2-Fluorobiphenyl
2.61
mg/kg wet
4.000
65
40-140
Surrogate: 2-Bromonaphthalene
2.78
mg/kg wet
4.000
69
40-140
LCS (POA0439-BS1)
Prepared: 01/27/20
Analyzed: 01/29/20
C9-C18 Aliphatics
32.0
25
mg/kg wet
60.00
53
40-140
C19-C36 Aliphatics
59.2
25
mg/kg wet
80.00
74
40-140
C11-C22 Aromatics
125
25
mg/kg wet
170.0
74
40-140
Surrogate: 1-Chlorooctadecane
1.32
mg/kg wet
2.000
66
40-140
Surrogate: o-Terphenyl
1.43
mg/kg wet
2.000
72
40-140
Surrogate: 2-Fluorobiphenyl
3.04
mg/kg wet
4.000
76
40-140
Surrogate: 2-Bromonaphthalene
3.19
mg/kg wet
4.000
80
40-140
Matrix Spike (POA0439-MS1)
Source: 0010326-02
Prepared: 01/27/20
Analyzed: 01/29/20
C9-C18Aliphatics
2140
37
mg/kg dry
88.59 1860
318
40-140 MI
C19-C36 Aliphatics
609
37
mg/kg dry
118.1 474
115
40-140
C11-C22Aromatics
1160
37
mg/kg dry
251.0 860
118
40-140
Surrogate: 1-Chlorooctadecane
1.93
mg/kg dry
2.953
65
40-140
Surrogate: o-Terphenyl
2.20
mg/kg dry
2.953
75
40-140
Surrogate: 2-Fluorobiphenyl
5.59
mg/kg dry
5.906
95
40-140
Surrogate: 2-Bromonaphthalene
3.61
mg/kg dry
5.906
61
40-140
Matrix Spike Dup (POA0439-MSD1)
Source: 0010326-02
Prepared: 01/27/20
Analyzed: 01/29/20
C9-C18Aliphatics
2000
37
mg/kg dry
89.12 1860
159
40-140 7 50 MI
C19-C36 Aliphatics
596
37
mg/kg dry
118.8 474
103
40-140 2 50
C11-C22Aromatics
972
37
mg/kg dry
252.5 860
44
40-140 17 50
Surrogate: 1-Chlorooctadecane
1.88
mg/kg dry
2.971
63
40-140
Surrogate: o-Terphenyl
2.05
mg/kg dry
2.971
69
40-140
Surrogate: 2-Fluorobiphenyl
5.34
mg/kg dry
5.941
90
40-140
Surrogate: 2-Bromonaphthalene
3.75
mg/kg dry
5.941
63
40-140
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group Project: Sedgefield
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Diesel Range Organics by GC/FID - Quality Control
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0462 - 3546
Blank (POA0462-BLK1)
Prepared: 01/28/20 Analyzed: 01/30/20
Diesel Range Organics
BRL
7.0 mg/kg wet
Surrogate: o-Terphenyl
0.882
mg/kg wet
1.333 66 31-123
LCS (POA0462-BS1)
Prepared: 01/28/20 Analyzed: 01/30/20
Diesel Range Organics
55.1
7.0 mg/kg wet
66.58 83 46-126
Surrogate: o-Terphenyl
0.934
mg/kg wet
1.332 70 31-123
Matrix Spike (POA0462-MS1)
Source: 0010326-01
Prepared: 01/28/20 Analyzed: 01/30/20
Diesel Range Organics
78.3
9.2 mg/kg dry
87.77 5.79 83 50-117
Surrogate: o-Terphenyl
1.36
mg/kg dry
1.755 78 31-123
Matrix Spike Dup (POA0462-MSD1)
Source: 0010326-01
Prepared: 01/28/20 Analyzed: 01/30/20
Diesel Range Organics
94.5
9.3 mg/kg dry
88.15 5.79 101 50-117 19 24
Surrogate: o-Terphenyl
1.51
mg/kg dry
1.763 86 31-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint..
ANALYQ)
TICAL
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
General Chemistry Parameters - Quality Control
Analyte
Project: Sedgefield
Level II QC Report
2/6/20
Work Order: 0010326
Time Submitted: 1/23/2020 11:54:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0526 - Solids, Dry Weight
Duplicate (POA0526-DUP1) Source: 0010326-06 Prepared: 01/31/20 Analyzed: 02/03/20
% Solids 71.8 0.100 % by Weight 71.3 0.7 20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
0010326-01
POA0462
30.15 g
1 mL
01/28/20 17:37
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
0010326-02
POA0439
10 g
2 mL
01/27/20 16:05
0010326-03
POA0439
10.02 g
2 mL
01/27/20 16:05
0010326-04
POA0439
10.05 g
2 mL
01/27/20 16:05
0010326-05
POA0439
10.08 g
2 mL
01/27/20 16:05
0010326-06
POA0439
10.01 g
2 mL
01/27/20 16:05
Prep Method: 5030E Soil
Lab Number
Batch
Initial
Final
Date/Time
0010326-01
POA0483
3.95 g
5 mL
01/29/20 12:39
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DatelTime
0010326-01
POA0526
30 g
30 g
01 /31 /20 8:15
0010326-02
POA0526
30 g
30 g
01 /31 /20 8:15
0010326-03
POA0526
30 g
30 g
01 /31 /20 8:15
0010326-04
POA0526
30 g
30 g
01 /31 /20 8:15
0010326-05
POA0526
30 g
30 g
01 /31 /20 8:15
0010326-06
POA0526
30 g
30 g
01 /31 /20 8:15
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
0010326-02
POA0489
30 g
1 mL
01/29/20 16:00
0010326-03
POA0489
30.05 g
1 mL
01/29/20 16:00
0010326-04
POA0489
29.98 g
1 mL
01/29/20 16:00
0010326-05
POA0489
30.03 g
1 mL
01/29/20 16:00
0010326-06
POA0489
30.04 g
1 mL
01/29/20 16:00
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
0010326-02
POB0017
4.59 g
5 mL
02/03/20 12:27
0010326-03
POB0017
5.18 g
5 mL
02/03/20 12:27
0010326-04
POB0017
4.23 g
5 mL
02/03/20 12:27
0010326-05
POB0017
5.48 g
5 mL
02/03/20 12:27
0010326-06
POB0017
5.25 g
5 mL
02/03/20 12:27
Prep Method: MADEP VPH
(S)
Lab Number
Batch
Initial
Final
Daterrime
0010326-02
POA0482
4.12 g
16 mL
01/29/20 14:04
0010326-03
POA0482
3.67 g
16 mL
01/29/20 14:04
0010326-04
POA0482
4.16 g
16 mL
01/29/20 14:04
0010326-05
POA0482
4.02 g
5.33 mL
01/29/20 14:04
0010326-06
POA0482
3.76 g
5.33 mL
01/29/20 14:04
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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APPENDIX V
Disposal Documents

rev a
CORPORATION
1703 Mvpmve Street
Winston-Salem, NO 27107
ph 336-725-5844
fax [phone]
TANK DISPOSAL CERTIFICATE
Tank Owner: Marsh Realty Co.
Site Address: 12.17 South Boulevard
Charlotte, NC
Description of Tanks:
Tank Size of Tank Contents
Number
1 550 Gallons #2 Fuel Oil
Transporter: Evo Corporation
EC Project #: 012039
Disposal Certification:
Evo Corporation does hereby certify that the above named storage tank was
transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem; NC for
proper disposal and recycling.

vo
CORPORATION
17031/atrave Street
Winston-Salem, NC 27107
Ph 336-725-5844
fax [phone]
CERTIFICATE OF DISPOSAL
Eva Corporation does hereby certify that 350 gallons of non -hazardous
contaminated water received on .1/23/2020 from:
Generator: Marsh Realty Co.
Originating at: 1217 South Boulevard
Charlotte, NC
EC Waste ID #: 012039
has been disposed of by Eva Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Eva Corporation

Iwo .
CORPORATION
1703 Vargrave Street
Winston-Salem, NO 27107
ph 336-725-5844
fax [phone]
CERTIFICATE OF DISPOSAL
Evo Corporation does hereby certify that 14.29 tons of non -hazardous
contaminated material received on 1/23/20220 from:
Generator: Marsh Realty Co.
Originating at: 1217 South Boulevard
Charlotte, NC
EC Waste ID #: 012039
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
j �' Lj
Signature
Thomas W. Hammett
CEO
Evo Corporation

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorpnet
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No.
GENERATOR INFORMATION
Marsh Realty Company 704-602-2062
Generator: Phone:
Site Address: 121 ? South Boulle"-` ar
City/State: . Chaxlott:e NC 28209 Contact: Jaiuirl MeLawha-rin
MATERIAL DESCRIPTION 1 QUANTITY 1 WEIGHT
Gross Weight (Ibs):
Empty Weight (lbs):
Net Weight (lbs):
Quantity'�j
Material:
Contaminant: #2 Fuel Cit
Tons Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter: Byo Corporation
Truck. #: 't C)
Phone: [phone]
Contact: ,nV__ iiwrit►r
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and 1 hereby receive this material for
delivery to the facility designate.
Driver
FACILITY INFORMAT[ON
.Ebro Corporation
Winston-Salem. C 27107
012039
Evo Project*
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and�or disposal in a manner that has been authorized by the State of North Carolina.
S
Date: J — 13
Evo Corporation, 2008
nvoice Pink/Carrier

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorpnet
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 09653
GENERATOR INFORMATION
Mars. Realty Company 70 -602- 062
Generator: Phone:
Site Address: 1217. South B. ou evard
City/State: Char .otLe_ NC 28209 Contact:
Gross Weight (lbs):
Empty Weight (Ibs):
Net Weight (lbs):
MATERIAL DESCRIPTION 1 QUANTITY 1 WEIGHT
-- 3 Ike
Quantity [1-1 ` J_[T
Material:
Contaminant: #2 Fuel Chi.
(9s Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter: Eyo Corporation Phone:
Truck #:
E R1
Contact: TonV Disbeir
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and 1 hereby receive this material for
delivery to the facility designate.
Driver Si nature: I 0-�' 'Inn/ k'1/ Date:
FACILITY INFORMATION
Eve Corp oration
%stoat. -Salem C 27107
Evo Project #:
Phone:
Contact:
xwq-INT41
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment andlor i)osal in a maker that has been authorized by the State of North Carolina..
Facilitv Signature:
Date: 1 1 W312A
Eva Corporation, 2008

Foss Recycling Winston Salem
3459 'Thomasville Road
Winston-Salem, NC 27147
Phone : [phone]
DISBER TONY
EVO TRUCKING
WINSTON SALLM NC
CATCH WEIGHTS
q.61103q
J�
SCALE TICKET
IN�NImePAGE
�II���I
Ticket No.
15778589 Scale: 88
In
23 San 2020 2:09 pm
out
; 23 San 2020
Supplier-##
DISO40
Plate No.
EVO
Vehicle
WHITE SEMI.216
Served By
rganzales
621500 LBS $0.00
Net --- $0.00
Total $0.00
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2020
RUBEN GON
- �� 42941
rnrVALsa j1ILt_SS SIGNED
Mission: Excellence in Recycling

Beverly, Trudy
From: Beverly, Trudy
Sent: Wednesday, September 29, 2021 1:54 PM
To: Tom Hassett
Subject: RE: [External] [Not Virus Scanned] Heating oil UST - 2807 South Boulevard
Hey Tom,
Documentation received. No need to send a paper nor a cd. I will let you know if I have questions.
Have a great day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.B everlyL&ncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-prosram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-maps
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hit 2s://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.aov/nedeci/Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
htips:Hfiles.nc. gov/ncdeq/\Vaste%2OManagement/D WMiUST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Tom Hassett[mailto:[e-mail]]
Sent: Wednesday, September 29, 2021 1:43 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] [Not Virus Scanned] Heating oil UST - 2807 South Boulevard
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
-iis message contains an attachment that was NOT virus scanned and could be
ou are receiving a file from an unknown source, please forward the email as an
attachment to
Trudy,
or contact the DIT Service Desk at 919-754-60

We were finalizing a Phase I ESA for a property in Charlotte and I did not see the site on the LUST database. We
previously monitored the removal of a heating oil tank (associated with a former boiler), but the closure documentation
apparently never made it to DEQ.
Therefore, I am attaching a UST-61 form and the closure report as our client has asked us to get the incident
resolved. Would you need me to send paper copies and CDs by mail?
We left soils in place that exceed residential, but not industrial/commercial, MSCCs. However we found no receptors
that would elevate the Risk category, so believe that the incident can be closed. We are putting together a NORR for the
owner and will forward that when signed.
Thank you,
Tom
Thomas C. Hassett, P.E.
Senior Engineer
GEOSCIENCE GROUP, INC.
500-K Clanton Road
Charlotte, NC 28217
[phone] - Office
[phone] - Fax
[phone] - Mobile