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HomeMy WebLinkAboutMO-29143_48325_CA_IAR_20220308_Initial Abatement Action Reporthart'` hickman SMARTER ENVIRONMENTAL SOLUTIONS Via Email March 8, 2021 North Carolina Department of Environmental Quality UST Section 610 East Center Avenue Suite 301 Mooresville, NC 28115 Attn: Ms. Trudy Beverly Re: Heating Oil UST Removals Presbyterian Church 729 East 36th Street and 3315 North McDowell Street Charlotte, North Carolina 28205 H&H Job No. ASC-003 Dear Ms. Beverly: Hart & Hickman, PC (H&H) is providing the attached Initial Abatement Action (IAA) report in relation to three heating oil underground storage tanks (USTs) removed from the Presbyterian Church property located at 729 East 36th Street and 3315 North McDowell Street in Charlotte, North Carolina. Analytical results of closure samples indicated the presence of impacts to soil above action levels at two of the UST locations. Analytical results of confirmation samples collected following the removal of impacted soil did not indicate the presence of analyzed compounds at concentrations above Maximum Soil Contaminant Concentrations (MSCCs). As such, H&H is requesting an unrestricted use No Further Action (NFA) in relation to the former USTs. Please contact us if you have any questions or require additional information. Sincerely, Hart & Hickman, PC r Nathan O'Le ry, Project Manager 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main Initial Abatement Action Report Presbyterian Church 729 East 36th Street and 3315 North McDowell Street Charlotte, North Carolina DEQ Incident No. TBD H&H Job No. ASC-003 March 3, 2022 hart � hickman SMARTER ENVIRONMENTAL SOLUTIONS C-1269 Engineering #C-245 Geology 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main Initial Abatement Action Report A. Site Information 1. Site Identification Date of Report: March 2 2022 Facility ID: NA UST Incident Number: NA Site Name. Presbyterian Church Site Street Address: 729 East 36 Street and 3315 North McDowell Street City, Town: Charlotte Zip Code: 28205 County: Mecklenburg Description of Geographical Data Point: Former UST location Location Method: Goo le Earth Latitude: 35.2463°N Longitude:-80.8010°Vie 2. Information about Contacts Associated with the Leaking UST System UST Owner/Operator: North Charlotte Presbvterian Church Address: 1010 Vickery Drive, Charlotte, NC 28215 Tel.: Unknown Property Owner: North Charlotte Presbyterian Church Address: 1010 Vickery Drive, Charlotte, NC 28215 Tel.: Unknown Property Occupant: Vacant Address: Tel.: Consultant/Contractor: Hart & Hickman, PC Address: 2923 South Trvon Street. Suite 100, Charlotte. NC 28203 Tel.: 704 586-0007 Attn: Steve Libbe PG Analytical Laboratory: Pace Analytical State Cert. No. 12 Address: 9800 Kincey Ave. Ste 100 Huntersville NC 28078 Tel.: 704 875-9092 3. Information About Release Date Discovered: October 12. 2018 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release: Heating Oil USTs Sizes and contents of UST system: One 550- allon heating oil UST and one 1000- allon heating oil UST 4. Certification I, Stephen Libbgy, PG a Licensed Geologist at Hart & Hickman, PC, do certify that the information co Ag din this report is correct and accurate to the best of my knowledge. SEAL f 3 j31Zv •m Hart & 'icensed to practice geology/engineering in North Carolina. The certification n' wS l' of the company are C-2451C-1269. 1 Hart "ti hickman hops:,"harthick sharepotnt com/silcvlMaslerFilrs-I. Shared I rocumenWAAA-Massa NDjc05Mscenl "I Blab: Capitu'ASC-003 Church pogiIN• kc�xSrt 1AA - n3o.Jac SNAAM WRIMME ALSOWWOS B. Site History and Characterization 1. UST Owner and Operator Information: UST ID Number UST-1, UST-2, & UST-3 Facility ID Number N/A Name of Owner Dates of Ownership North Charlotte Presbyterian Church —1955-2022 Street Address 1010 Vickery Dr City State Zip Telephone Number Charlotte NC 28215 Unknown Name of Operator Dates of Operation Same as Above Unknown Street Address City State Zip Telephone Number 2 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Re oNIAA - nlo.doc SI W11 pNY1RONME l At SOLL7I % 2. UST/AST Information: Was release Approximate Description of Date UST ID Current/Last Previous Capacity Construction Status of associated Tank Associated Piping and Tank Number Contents Contents (gallons) Details UST with the Dimensions Pumps Installed UST System? UST-1 Heating Oil N/A 1,000 Steel I x 4' N/A Unknown Removed Yes UST-2 Heating Oil N/A 550 Steel 6' x 3.33' N/A Unknown Removed Yes UST-3 I Heating Oil I N/A 1 550 1 Steel 1 6' x 3.33' N/A Unknown I Removed No https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Report/IAA - njo.doc hart : hick man SMARTER ENWONMENTAL 50LUTION5 3. Non -UST spills at the site: No non -UST spills are known to have occurred at the site. 4. Description of release: During previous Phase I Environmental Site Assessment (ESA) activities conducted at the site by others in 2018, heating oil tank UST-2 was identified adjacent to the church building and heating oil tank UST-3 was identified adjacent to an on -site residential structure. Heating oil tank UST-1 located adjacent to the church school building was not identified in 2018 and was identified by H&H during a subsequent Phase I ESA in 2021. To evaluate the potential for impact from the USTs, two soil borings were advanced adjacent to UST-2 and UST-3 during the 2018 Phase I ESA. Analytical results of soil samples collected adjacent to UST-2 indicated gasoline range total petroleum hydrocarbons (TPH-GRO) and diesel range total petroleum hydrocarbons (TPH-DRO) concentrations up to 26,000 mg/kg. TPH-GRO and TPH-DRO were not detected at concentrations above the laboratory reporting limits in samples collected adjacent to UST-3. A soil sampling results summary table, sample locations map, and laboratory analytical data from the 2018 Phase I ESA are presented in Appendix A. 5. Site characteristics: The site is comprised of two parcels of land totaling approximately 1.65 acres in area, the westernmost site parcel is developed with an approximately 6,550 square foot (sq ft) church building, an approximately 2,300 sq ft single-family residence, and an approximately 4,500 sq ft school building. The easternmost parcel is currently vacant land but was most recently utilized as a community garden. A site location map is presented as Figure 1, and a site map is presented as Figure 2. The subject site is located in the Piedmont Physiographic Province of North Carolina. According to the Geologic Map of North Carolina dated 1985, the subject property lies within the Charlotte Belt. In the site area, underlying bedrock is composed of granitic rock. The land surface of the area is generally characterized as gently sloping, which may become moderately steep where intersected by streams. In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser amounts of rock fragments. Due to the range of parent rock types and their variable susceptibility to weathering, the saprolite ranges widely in color, texture, and thickness. Generally, the saprolite is thickest near interstream divides and thins toward streambeds. In profile, the saprolite normally grades from clayey soils near the land surface to highly weathered rock above competent bedrock. 4 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Re oNIAA - nlo.doc SIdAR7ER pNY1RONME l At SOLL7I % The occurrence and movement of groundwater in the Piedmont is typically within two separate but interconnected water -bearing zones. A shallow water -bearing zone occurs within the saprolite, and a deeper water -bearing zone occurs within the underlying bedrock. The site is located at an approximate elevation of 730 ft above mean sea level. Topography in the source area generally slopes to the northeast (Figure 1). Based on topography, H&H anticipates that the groundwater flow direction at the site is to the northeast toward an unnamed tributary of Little Sugar Creek located approximately 500 ft from the former UST. Visual observations during excavation activities and soil sample collection indicated that the soil surrounding UST system consisted of orange to brown silty clays (saprolite). Groundwater and bedrock were not encountered in the excavation. Municipal water is available to the site and the areas surrounding the site. A formal water supply well survey was not performed. No obvious water supply wells were observed during area reconnaissance. 6. Initial abatement actions, assessment activities, and corrective actions performed to date: Other than the 2018 soil sampling discussed above, no other known initial abatement actions, assessments, or corrective action activities have been conducted at the site. C. Site Check Report Not applicable. D. UST Closure Report following UST-12 format and Site Investigation Report for Permanent Closure or Change -in -Service of UST (UST-2 Form) 1. Preparations for closure including the steps taken to notify authorities, permits obtained and the steps taken to clean and purge the tanks: Prior to the UST closure activities, a permit authorizing the UST removal was obtained from the City of Charlotte Fire Department by EVO Environmental and Industrial Resources (EVO) of Winston-Salem, North Carolina. Prior to removal, residual fluids were removed from the USTs. The USTs were then triple -rinsed with a pressure washer and vacuum truck by EVO in accordance with Mecklenburg County requirements. Approximately 625 gallons of residual fluids and rinse water were removed from the USTs. Following removal of the residual fluids and rinse water, the USTs were purged of combustible vapors with dry -ice and subsequently tested with a combustible gas indicator to evaluate whether combustible vapors had dissipated. 5 hart hickman https://harthicksharepoinkcom/sites/MasterFiles-1/Shared Documents/AAA-Maser Projects/Ascent Real Estate Capi[al/ASC-003 Church property/RepoN1AA - nlo.doc SIdAR7ER pNY1RONME l At SOLL7I % 2. Closure procedures: Initially, soil was removed from the top and sides of the USTs with a backhoe so that the tanks could be removed from the ground. Soils encountered during the excavations were evaluated in the field for the presence of odors and staining, and for the presence of organic vapor with a photoionization detector (PID). The PID was calibrated prior to its use against an isobutylene standard. Following removal, the USTs were inspected for holes or other signs of structural damage. The USTs were single -walled and constructed of steel. The bottom surface of UST-1 and UST-2 were moderately pitted and contained several small holes. No surface pitting or holes were observed in the bottom surface of UST-3. 3. Note the amount of residual material pumped from the tank and describes the storage, sampling and disposal of the residual material and the disposal of the tank, pumps and piping: As stated above, EVO removed approximately 625 gallons of residual and rinse liquids from the USTs. The fluid was disposed by EVO at their facility in Winston-Salem, North Carolina. The disposal certificate for the residual fluid is included in Appendix B. The three USTs were transported off -site for disposal at Foss Recycling in Winston-Salem, North Carolina. The tank disposal certificate is included in Appendix C. 4. Initial response actions and initial abatement actions: Initial response and abatement actions are discussed in the following section. 5. Soil excavation and Site Investigation activities: After removal of the USTs, one closure soil sample was collected below UST-1 and one closure soil sample was collected below UST-3. Due to previous soil sampling data from 2018 which confirmed that a release had occurred from UST- 2, a closure sample was not collected below UST-2. The closure samples were analyzed for TPH-GRO by EPA Method 8015C and TPH-DRO by EPA Method 8015C. The analytical results of the closure sample collected below UST-1 indicated the presence of TPH-GRO and TPH-DRO at concentrations of 146 mg/kg and 838 mg/kg, respectively. The detected concentrations are above the DEQ action levels of 50 mg/kg and 100 mg/kg for TPH-GRO and TPH-DRO, respectively. TPH-GRO and TPH-DRO were not detected above the DEQ action levels in the soil sample collected below UST-3. Approximately 26 tons of impacted soils were excavated from the UST-1 and UST-2 basins on February 14, 2022. The excavated soil was stockpiled on plastic adjacent to the USTs and later transported to EVO's facility in Winston-Salem, North Carolina for proper disposal on February 24, 2022. A copy of the 6 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Re oNIAA - nlo.doc SIdAR7ER pNY1RONME l At SOLL7I % certificate of disposal, non -hazardous waste manifests, and certified weight tickets for the excavated soil are provided in Appendix B. The approximate dimensions of the UST-1 basin excavation were approximately 15 ft long by 8 ft wide by 8 ft deep, and the approximate dimensions of the UST-2 basin excavation were approximately 11 ft long by 7 ft wide by 7 ft deep. The approximate extents of the excavations are depicted on Figure 3. Following soil over -excavation activities, four confirmation sidewall soil samples (UST-I-SW-L, UST-I-SW-R, UST-I-SW-F, and UST-I-SW-B) were collected from the UST-1 basin excavation, and four confirmation sidewall soil samples (UST-2-SW-L, UST-2-SW-R, UST-2-SW-F, and UST-2-SW-B) were collected from the UST-2 basin excavation. In addition, confirmation base soil samples UST-1-13 and UST-2-13 were collected from the UST-1 and UST-2 excavations, respectively. In accordance with DEQ guidance, the collected post -excavation soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260B/5035A, semi-VOCs (SVOCs) by EPA Method 8270, and extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) using the Massachusetts Department of Environmental Protection (MADEP) Methods. Analytical results of the post -excavation samples from the UST basin excavations indicate the presence of trace concentrations of several VOCs and naphthalene. In addition, C9-C 18 Aliphatics and C 11-C22 Aromatics were detected at trace concentrations in confirmation soil samples UST-2-13 and UST-2-SW-R. None of the compounds were detected at concentrations above DEQ Soil -to -Groundwater, Residential, or Industrial/Commercial Maximum Soil Contaminant Concentrations (MSCCs). Soil samples were analyzed by a North Carolina certified laboratory. A chain -of - custody record was completed for samples collected and included sample description, date collected, time collected, matrix, sample container information, and analyses required. The chain -of -custody was signed by H&H prior to placement in an iced cooler for shipment to the laboratory. Prior to shipment, the cooler was closed with a seal indicating the H&H representative's signature and date such that a potential disturbance of the cooler contents could be detected by the laboratory. Soil analytical results are summarized in Table 1 and the sample locations are depicted on Figure 3. Laboratory analytical sheets are included in Appendix D. Following soil removal, the excavation was backfilled with clean imported backfill material. The imported backfill material consisted primarily of brown silty clays. 7 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Re oNIAA - nlo.doc SIdAR7ER pNY1RONME l At SOLL7I % E. Free Product Investigation and Recovery Report Not applicable. F. Groundwater and Surface Water Investigation Not applicable. G. Initial Response and Abatement Activities See Section B. H. Excavation of Contaminated Soil See Section D. I. Conclusions and Recommendations: In February 2022, two inactive 550-gallon heating oil USTs (UST-2 and UST-3) and one inactive 1,000-gallon heating oil UST (UST-1) were removed from the site. No soil impacts were identified below UST-3 based on laboratory analytical results. Approximately 26 tons of impacted soils were excavated for off -site disposal from the UST-1 and UST-2 basins. Analytical results of confirmation soil samples collected from the UST-1 and UST-2 basins do not indicate the presence of VOCs, SVOCs, VPH, or EPH at concentrations above DEQ MSCCs. Based on the results of the initial abatement action activities, H&H recommends that DEQ issue a no further action (NFA) letter for the UST incident. 8 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Re oNIAA - nlo.doc SIdAR7ER pNY1RONME l At SOLL7I % Tables qd hart hickman SMARTER ENVIRONMENTAL SOWT1ONS Table 1 Summary of Heating Oil UST Soil Sample Results Presbyterian Church 729 E. 36th Street and 3315 North McDowell Street Charlotte, North Carolina H&H Job. No. ASC-003 5030/ 3550/ Analytical Method 8015C 8015C MADEP MADEP MADEP MADEP MADEP MADEP MADEP MADEP 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8270D N U U to U U U m C m C Contaminant of Concern Q o o N N < < < _Q < (9 < N < N co N CID 00 co U O N U N N a) C c m m U 6 rn U a) c > E F U O U U U U io U m o a) c > Date Sample Incident = _ _ _ _ = Q = = o c Q Q D Sample ID Collected Source Area Depth (ft) Phase 0 0- F-- 0- > 0- > 0- w O F-- 0- w < 0- > 0 w < O 1--- a) m 1 w O E (0 z p1--- 1--- N M T X a) cn UST-1 02/14/22 UST 5 CL 146 838 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA UST-3 02/14/22 UST 5 CL 5.9 J <2.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA UST-1-13 02/14/22 UST 8 IA NA NA <5.6 <5.6 <15 BRL <15 <5.6 <15 BRL 0.0069 J 0.0060 J <0.0040 0.0177 0.0197 0.0061 J <0.0039 0.0174 J ALL BRL UST-1-SW-F 02/14/22 UST 7 IA NA NA <4.6 <4.6 <14 BRL <14 <4.6 <14 BRL <0.0038 0.0108 0.0065 J 0.0653 0.0089 J 0.0766 0.0327 0.0536 ALL BRL UST-1-SW-B 02/14/22 UST 7 IA NA NA <5.2 <5.2 <14 BRL <14 <5.2 <14 BRL <0.0055 <0.0065 <0.0047 <0.0073 <0.0039 <0.0038 <0.0047 <0.0079 ALL BRL UST-1-SW-R 02/14/22 UST 7 IA NA NA <6.7 <6.7 <14 BRL <14 <6.7 <14 BRL <0.0041 <0.0048 <0.0035 <0.0055 0.0089 J <0.0028 <0.0035 <0.0059 ALL BRL UST-1-SW-L 02/14/22 UST 7 IA NA NA <6.2 <6.2 <14 BRL <14 <6.2 <14 BRL <0.0043 <0.0051 <0.0037 <0.0057 <0.0031 <0.0030 <0.0037 <0.0062 ALL BRL UST-2-13 02/14/22 UST 7 IA NA NA <8.2 <8.2 35 35 23 <8.2 19 19 <0.0055 <0.0064 <0.0047 0.0244 <0.0039 0.0090 J <0.0046 <0.0079 ALL BRL UST-2-SW-F 02/14/22 UST 6 IA NA NA <5.1 <5.1 <14 BRL <14 <5.1 <14 BRL <0.0038 <0.0044 <0.0032 <0.0050 <0.0027 <0.0026 <0.0032 <0.0054 ALL BRL UST-2-SW-B 02/14/22 UST 6 IA NA NA <5.6 <5.6 <13 BRL <13 <5.6 <13 BRL <0.0038 <0.0045 <0.0033 <0.0050 <0.0027 <0.0026 <0.0032 <0.0055 ALL BRL UST-2-SW-R 02/14/22 UST 6 IA NA NA <4.3 <4.3 31 31 14 <4.3 19 19 <0.0038 <0.0044 <0.0032 0.0055 J <0.0027 <0.0026 <0.0032 <0.0054 ALL BRL UST-2-SW-L 02/14/22 UST 6 IA NA NA <4.7 <4.7 <14 BRL <14 <4.7 <14 BRL <0.0040 <0.0046 <0.0034 <0.0052 <0.0028 <0.0027 <0.0033 <0.0057 ALL BRL Action Level (mg/kg) 50 100 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Soil to Ground Water MSCC (mg/kg) NS NS 68 NS NS 540 NS NS NS 31 0.0072 8 1.3 0.2 5.4 6.6 6.6 6 Varies Residential MSCC (mg/kg) NS NS 625 NS NS 1,500 31,200 NS NS 469 12 60.3 1,560 5.5 1,250 156 156 3,120 Varies Industrial/Commercial MSCC (mg/kg) NS NS 9,340 NS NS 40,000 467,000 NS NS 7,000 1 59.4 297 23,300 27 18,600 1 2,330 1 2,330 1 46,700 Varies Notes: Apart from VPH and EPH, only those compounds detected are shown. Concentrations are reported in milligrams per kilogram (mg/kg). UST = Underground Storage Tank Basin; CL = Closure Sample; IA = Initial Abatement Sample; TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons; NA = Not Analyzed; NS = Not Specified; MSCC = Maximum Soil Contaminant Concentration; BRL = Below Reporting Limits; J = Estimated value between method detection limit and laboratory reporting limit. Table 1 (Page 1 of 1) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ascent Real Estate Capital/ASC-003 Church property/Report/Soil Data.xls 3/2 Hart &Hickman, pl, Appendix A 2018 Soil Assessment Data qd hart hickman SMARTER ENVIRONMENTAL SOWT1ONS Table 1: Summary of Soil Sampling Results Revision 10/2612018 Project: Forest Hill Church Parcels Project No, CH18.0129.GE Date: Analytical Method TPH (mg/kg) Contaminant of Concern ❑ 0 Sample Location Sample depth (ft) Date Collected I. HA-1 7.5 10/512018 E9.9 { 7.5 HA-2 8 10/512018 <9.9 <7.5 HA-3 $ 10/12/2018 26,000 2,300 HA-4 10 10/1212018 3,500 99 North Carolina Action limits for Total Petroleum Hydrocarbons (TPH) 100 50 LEGEND: approximate Location of SaFnpEes Uudaground Storage Tank lk s 4 GEOSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE-- 1" 25' ,APPROVED BY: DRAWN BY; Mecklenburg Co. DATE! October 18, 2018 REVISED: ANP I FOREST HILL CHURCH PARCELS I CHARLOTTE, NORTH CAROLINA SAMPLE LOCATION DIAGRAM E NUMBER: CH18.129-4 Full -Service Analytical F /'PRISMI Environmental Solutions nA Geoscience Group Tam Hassett 500-K Clanton Rd. Charlotte, NC 28217 INC. Certification No. 402 NC Drinking Water Cart No. 37735 SC Certification No. 99012 Project: Forest Hill Church Parcels Lab Submittal Date: 1010512018 Prism Work Order: 8100119 Case Narrative t Oil 8/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody, Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please calf if you have any questions relating to this analytical report. Respectfully, PRISM LABORATQR.IES, INC. Angela D. Overcash VP Laboratory Services Reviewed By Angela D. Overcesh VP Laboratory Services Data Qualifiers Key Reference: RLM Sample container suspected to have low methanol content. Results possibly biased high. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a T This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 20224-0543 Phone: 704)529-U64 -Tull Free Number: I41DW529.5364 - Fax: 700525-0409 page i of $ ZR-I S n A ErivIr nrvice Analytical s e ' V' Envl�anmentni Solutions Sample Receipt Summary 10/1812018 Prism Work Order: 8100119 Client Sample ID Lab Sample ID Matrix Daterrime Sampled DatefTime Received HA-1 6100119-01 Sand 10105/18 0.00 10/05/18 15:05 HA-2 8100119-02 Solid 10/05118 0:00 10/05/18 15:05 Samples were received In good condition at 4.1 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the wri}ten consent of Prism Laborstorles, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-DS43 Phone: 704f529-6364 - Toll Free Number: 1-0001529.6364 - Fax: 7WS25.0409 Page 2 of 8 Full- .`P,AR I S M n envir " ice Anatyutio s [V' E�vEranm�rrtsl Solutions LI5wwomwsS, C: Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Forest Hilt Church Parcels Sample Matrix: Solid Laboratory Report 1011812018 Client Sample ID: HA-1 Prism Sample ID: 8100119-01 Prism Work Order: 8100119 Time Collected: 10105118 0a:00 Time Submitted: 1010&18 15:05 Parameter Result Units Report MIL Dilution Method Analysis Analyst Batch Limit Factor datefrime II] Diesel Range Organics by GCIFID diesel Range Organics BRL mglkg dry 9.9 2.6 1 Surrogate •8015c 10/11/18 16:36 ZRC PSJ0194 Recovery Control Limits o-Terphenyl 84 % 31-123 Gasoline Range Organics by GCIFID RLM Gasoilne Range Organics BRL molt dry 7.5 1,6 50 18015C 1018N8 19:38 ANCW PeJ0103 Surrogate Recovery Control Limits s.a.a-Trifluorotoluone 148 % 50.137 SR General Chemistry Parameters %solids 70.3 %by 0,100 0.100 1 'SM2540 G 1W16M8 16:40 TJY P&J0305 Weight This report should not be reproduced, except in its entirety, without the written consent at Prism Lahoratories. Inc. 449 Springbrook Road - P.O. Box 240543 . Charlotrs, NC 28224-0543 Phone. 7WS29.6364-Toll Free Number:l-600;5x9-6364- Fax: 704152"4" Page 4 of 8 I FvliSer ice Annlylicel 8. En�lronmenf�l Boiuti�ns '-: �AKIRwTw�ame Summary of Detections 1011 B!2018 Prism Work Order: 8100119 PHam ID Client ID Parameter Method Result Lirits There were no detections reported. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643 Phone: 7641529-6364 - Toll free Number: 9-8901529-6354 -Fax, 7041525-0409 Page 3 of 8 /ri®r-i!Service Anaiyt tl %; EnYironmantal Sulutlona l•BDRATORIES 'NV Geoscienoe Group Attn: Tom Hassett 500.K Clanton Rd. Charlotte, NC 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Laboratory Report 10AW018 Client Sample I❑: HA-2 Prism Sample I❑: 8100119-02 Prism Work finder: 8100119 Time Collected: 10105/18 00:00 Time Submitted: 10/05/18 15.06 Parameter Result Units Report VIAL Dilution Method Analysis Analyst Batch Limit Factor ❑ate/Time I Diesel Range Organics by GC1FID Diesel Range Organics 13RL mglkg dry 9.9 2.6 1 'S0i5C 10111/18 17;1a ZRC P8J0194 Surrogate Recovery Control Limits o-Terphenyl St) 96 31-129 Gasoline Range Organics by GC/FlD Gasoline Range Organics 6RL mglkg dry 9.9 2.1 50 *8015C 1018f18 20;O6 ANWJ PSJ0103 Surrogate Recovery Control Limb a.a,a-Trikurotoluen e General Chemistry Parameters 134 % 50-137 % Sol Ids 70.6 %by 0.100 0.100 1 '5012540G 10119/18 16;40 TJY Pt1J0305 weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "0 Sprsngbrook Road , P.O. Box 240543 - Chariotte, NC 2822"U3 Phone: 7041529$364 -Toll Free Number. 1-8001529.6364 • Fax; 70415254409 Page 5 of 8 L"P.,pLq Full -Service Analylleal Environmental Solutions Geoscience Group Project: Forest Hill Church Parcels Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Gasoline Range Organics by GC*lD - quality Control Level II QC Report 10/18118 Prism Work Order: 8100119 Time Submitted: 1015I2018 3:05:00PM Reporting Spike Source %REG RPD Ana lyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PBJ0103 - 6035 Blank lPBJ0103-BLK1y Prepared & Analyzed: 10/08118 Gasoline Range Organics BRL 5.0 mglkg wet Surrogate' a, a, a -Tiff uornVuene 5.20 rrlglkg 5.000 104 50-137 LCS (PBJ010343S1) Prepared & Analyzed: 10108118 Gasoline Range Organics 59.7 5.0 mglkg wet 50.00 119 41-138 Surrogafe.' e,a,a-Trffuorofaluene 5.65 mg/kg 5.000 113 50-137 LCS Dup (158J0103-113SOI) Prepared & Analyzed: 10/08118 Gasoline Range Organics 64.8 6-0 mg/kg wet 50,00 130 41-139 a 20 Surrogate: a,a,a-TriRuorotoiuerre 5.45 mg/kg 5.000 109 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratodes, Irr. 449 Springbraok Road - P.Q. Box 240543 - Cha►latte, NC 28224-0543 Phone, 704f$29-6364 -Toll Free Number: 1-0401529-5364 - t=ax: 70415254MO9 Page 6 of 8 P LgF I q M I FUIP-SeryiGe Analytical & Envirenmpnral Solutions L�eES �Nc Geoscience Group Project: Forest Hill Church Parcels Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Diesel Range Organics by GCIFiD - Quality Control Level fl QC Report 10116/18 Prism Work Order: 8100119 Time Submitted: 10f512018 3:05;04PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P830194 - 3546 Blank (PU0194-BLK1) Prepared & Analyzed: 10111/18 ❑iesel Range Organics BRL 7.0 mglkg wet Svrrogafe: a-Terphenyl 7.p7 mg*g wet 1.332 81 31-123 LCS (138J0194-13S'I) _ Prepared & Analyzed:_ 1_0111118 Diesel Range Drganics 51A 7.0 mglkg wet 66.64 77 46-126 Sun-ople: o-Tsrphenyf 1.18 mglkg wet 1.333 89 31-123 LCS Dup (PaJ0194-BS01) Prepared & Analyzed. 1011 ill Diesel Range Organics 54.0 7A mg/kg wet 66.67 81 46.126 5 20 Surrogate:-7"mphenyl 1.16 rnglkg wet 1.333 87 31-121 Sample Extraction data Prep Method- 3348 Lab Number Batch Initlal Final DateMme 8100119-01 PRJ0194 30.1 g 1 mL 10J11J18 8:42 6100119-02 PBJ0194 30.07 g 1 mL 10111J18 8:42 Prep Method: 5035 L.ab Number Batch Initial Final Dekslilme 6100119-01 PBJO103 4.77 g 5 mL ioiw18 12:03 8100119-02 P8J0103 3.58 g 5 mL 1p108f18 12:03 Prep Method: Solids, Dry Weight Lab Humber Batch initial Final Dateirime 9100119-01 P8d0305 30 g 30 g 1(VI 8118 16:40 8100119-02 P8J0305 30 g 30 g 10116118 16:40 This report should not be reproduced, except in its enlirety, wlthout the written consent of Prism Laboratories, Inc. 449 Sprh►gbrook Road - P.U. Box 2405t3 - Charlotte, NC 28224-0543 Phone: 704J528-fs36d -Toll Free Number: 1-SM529.6364 - Fax: 7WS29-0409 Page 7 of 8 6 ^3 L7 Z G m m o C C U1 f H 0 co p 3 "r if1 m n e a y 0 O O-4— [n x C x 8 n r m 0 0 `[ b' °: ?; m a cn ui [] p ,c C t rri 7 7 N f fcn ❑ C ai 7 ti1 r 20 3 m -n .� ❑ n r � +1 D �' dl � a rn� w a ra T� om in m �C v no do 5' m ❑ rn �m 0 zv o •• mU m G M. am m NAM C Q} A p C min 75 y a f �r l r m m prr 1 a n� moot r~u o b X? e mw 8 T � 9 �' T M -- -•-- -- aF mm� k a rn m b M 3 a my P Q ❑ or mm H yw �m CL � m �;n m u7°,lb C O v H LL w m ?7� m �OO" m:q 0 D W y m z and x a w D cr m m S --i rn a rt'a rt�� N ❑ ❑ dz ❑� P t➢�� 3ry u� ■ yS tlF❑ 7. z � 4 m np o� d nag C m 0 7❑ Q y n� to m fn rn ❑ � � m �n n ci m � C O r m Z rn a mlic ic O A -A m Z D n a3 m W m A a P � 0 0PL jt � n , �A •a a ♦L b (Y N 0 n O cn ty d n O r'` n j G G C 7 = m r� x nos 3 m u AS D to R� tl w N S><+ Q 10 211 >rLL I o � A d n v � �• oC a is 0 c g G it fr yC C c �p m n .. M r L ;6 N Z � Cv a z m m f -�man -4 o a , p m •a a z M" 0 cl 0 O v M 402 se Narrative INC CBrti Drinking iOn Water ert ■ � :. Full -Service Analytical � INCNC ❑risking Water Cert Iva. 37735 � p12412p1 g Environmental Solutions SC GertiTrcatlon No. 99012 L a9MATOnIM INC. Geoscience Group Project: Forest Hill Church Parcels Tom Hessen 500-K Clanton Rd. Late Submittal Date. 10/12/2018 Charlotte, NC 28217 Prism Work Order: 8100259 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully. PRISM LABORATORIES, INC. Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference Reviewed By Robbi A, Jones For Angela D. Overcash President/Project Manager DO Surrogates diluted out. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not he reproduced, except in its entirety, without the written eonsent of Prism Laboratories, Inc. 449 5pringbrook Road - P.a. ISox 240543 - Chatlotte. NC 28224.0543 Phone: 704l529.6364 - Toll Free Number: 1-6001529-6364 - Fax: 7041523.0409 Page 1 of $ PRISM I Full Service al Golubo a Sample Receipt Summary Enviranm®oral Solutions 1012412018 LA6pgA;nRCa LNG Prism Work Order; 8100289 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received HA-3 8100259-01 Solid 10/12118 10:08 10/12/18 13:30 HA-4 8100259-02 Solid 10112J18 11:45 10/12/18 13:30 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road . P.O. Box 240543 - Charlotte, INC 26224-6543 Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 -Fax: 7U/625-0409 Page 2 of i3 4 Full -Service AnaEytical& ISM I Envrranmental Solutlons LAB�P�TGRILR IMr, Summary of Detections 1012412018 Prism Work Order: 8100259 Prism ID Client I❑ Parameter Method Result Units 8100259-01 HA-3 Diesel Range Organics '8i315G 26000 Mg/kg dry 81002$9-01 HA-3 Gasoline Range Organics '9Et1SC 2300 mglkg dry 8100259-02 HAA Diesel Range Organics '8015C 3500 mglkg dry 8100259-02 HA-4 Gasoline Range Organics 18aisc 99 mglkg dry This report should not be reproduced, except in its entirety, without the written consent otPrism Laboratories, Inc. 4449 8pringbrook Read - P.O. Box 240543 . Charlotte, NC 28224d1S43 Phone: 7041529.6364 - Toil Free Number: f-soW529-6364 - Fax: 704Ai2S-Wl1 Page 3 of 8 I S n � I Full-Serorce Analytical a V' I Environmental Solutions �Rn,aAcs �� Geoscience Group Attn: Tom Hassett 50D-K Clanton Rd. Charlotte, NO 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Laboratory Report 10124/2010 Client Sample ID: HA-3 Prism Sample ID: 8100259-01 Prism Work Order: 8100259 rme Collected: 10/12/18 10-08 Time Submitted: 10112I18 13:30 Parameter Result Units Report MOL Dilution Method Analysls Analyst Balch Limit Factor Dat"Mme ID Diesel Range Organics by GCIFID Diesel Range Organics 26000 rngfhg dry 1900 500 200 18615C 10M7118 9:08 IRC P8J0283 Surrogate R--ery Cdhtrol Limits o-Terphenyl 0 % 31-123 OQ Gasoline Range Organlcs by GCIFID Gasoline Range Organics 2300 m9/kg dry 93 20 Sao "8015C 10119118 9:33 ANGIJ PBJ0333 Surrogate a, a,a-Triflu orotalV en e Retavery Contrd Limits 110 % 50-137 General Chemistry Parameters % Solids 73.9 'Y by 0.100 0.100 1 `SM2S40 G 10122I18 1410 TJY P810417 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism LabDfatones, Inc_ 449 Springhroott Road - P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 7041529-5354 -Tall Free (dumber: 1-8001529-6354- Fay: 70d1525-"09 Page 4 0f 8 Laboratory Report �FR ISM I E, vir amen analytical 8 ! Environmental 801ufign3 10r2412018 '%` .AHWTpMl" iaq Geoscienee Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Client Sample ID: HA-4 Prism Sample ID: 8100259-02 Prism Work Order: 8100259 Time Cotlected: 10/12/18 11:45 Time Submitted: 1011211813:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTme Ill Diesel Range Organics by GCIFID Diesel Flange Organics 3500 mglkg dry 490 18$ 50 *$015G 10MVi8 7:50 ZRC PSJ0283 Surrogate Recovery Control Limits o-Terphenyl 0 % 3f-723 00 Gasoline Range Organics by GC1FID Gasoline Range Organics 99 myfky dry 7.9 1.7 So "8olsc 10119118 511 ANGM P$J0333 Surrogate Recovery Control Limits a,a.a-Trifluorotaluene 118 % 5D-137 General Chemistry Parameters %Solids 71.0 %by 0.100 0.100 1 '3M2540G 1012211814:30 TJY PSJ0417 Weight This report should not be reproduced, except in ita entirety, without the written consent of Prtsrn Laboratories, Inc. 449 Springbrook Road • P.O. Bum 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 • Toil Free plumber: 1$001529-4384 - Fax: 7041525-MO Page 5 of 8 �R I S h ,♦� Full -Service Analytical I V I � Environmental Sofu[fans its- h& Geosoience Group Project: Forest Hill Church Parcels Attu: Torn Hassett 500-K Clanton Rd. Charlotte. NC 28217 Gasoline Range Organics by GGlFID -{duality Control Level li QC Report 10124l18 Prism Work Order: 8100259 Time Submitted: 10/12/2018 1:30:OOPM Reporting Spike Source %REC RPD Analyse Result Urnk Units Level Result %REC Limits RP❑ Limit Notes Batch MOM - 5035 Blank (P8J0333-BLK1) Prepared BAnaWed: iOil all 8 Gasoline Range Organics RRL 5.0 rnglkg wet Surr*g'?fe: a,a,a-7nfl(forW010ene 5.05 mg*9 5.00U 101 50-137 LCS (P8J0333-051) Prepared & Analyzed: 10118/18 _ Gasoline Range organics 55.4 5.0 mglkg wet 50.00 111 41-138 Surrogate: a,a,a-Tnfiuorat0iuene 4.90 mglkg 5.000 98 50-137 l_CS Dup IMID333-MI) Prepared & Analyzed: i0/18/18 Gasoline Range Organics 81A 5.0 Mog wet 50.00 122 41-139 10 20 Surrogate: a,a,a-Trtluarotoluene &00 mglkg 5.000 100 50-137 This report should not be reproduced. except in Its entirety, without the written consent of prism Laboratories. Inc,. 448 Springhrook Rnad - P.O. Box 24OS43 - Charlotte, INC 28224.0543 Phone: 7041529-6364 - Tall Free Humber: 1.8001529-6364 - fax: 704(525-0409 Page 6of8 +� R I S i Fuu-Service AnafS'xical 8 Enviranmenx>Ri SaEu[fona ORA70o OL ING Geoscdence Group Project; Forest Hill Church Parcels Attn: Tam Hassett 5OD-K Clanton Rd. Charlotte, NC 28217 Diesel Range organics by GCIFID - Quality Control Level II QC Report 10124118 Prism Work Order: 8100259 Time Submitted: 10/12/2018 1:30:OOPM Reporting Spike Source %REC RPO Anaiyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PBJ0283 - 3546 Blank (PSJ0283-BLK1 ) Prepared a& Analyzed: 1 D116118 Dlesel Range Organics BRL 7.0 mglkg wet Surrogate: o-Terphenyl 0.929 mg/kg wet 1,333 70 31.12.3 LIDS (P8J0283-1351) _ Prepared & Analyzed: 1011-6118 Diesel Range Organics 59.1 7.0 mglkg wet 66.67 69 46.126 Surrogate: u-Terphenyl 1.24 mgft wet 1.333 93 39-123 LCS oup (P8J0253-BSDI) Prepared &Anatyze_d: 10116118 Diesel Range Organics 55.8 7.o mglkg wet 66.67 84 46-126 6 20 Surrogate. o-Terphenyl 1.08 mglkg wet 1.333 81 31-123 Sample Extraction Data Prop Method: 3546 Lab Number Batch Inkial Final Daterrinn 8100259-01 PBJ0283 30.1 g 1 mL 10118118 11:35 8100259-02 PBJ0283 30A2 g 1 mL 10116118 11:35 Prep Method: 5035 Lab Number Batch Initial Final DatalTime 81 OD259-01 POJ0333 3.62 g 5 mL 1 WI8118 10:64 81D0259-02 P8J0333 4.46 g 5 mL 10/18118 11154 Prep Method: Sands, Dry V"ht Lab Number Batch inlitlal Final Datefllme 8100269.01 P8J0417 30 g 30 9 1W2118 14:30 811DO259-02 P8J0417 30 g 30 g 10122118 14:30 This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2a224.0543 Phone: 704I529-6364 -Toll Free Number. 1.8001529.6364 - Fax: 704/525-04H Page 7 of 8 Phase I Environmental Site Assessment Forest Hill Church Parcels Charlotte, North Carolina Ceoscience Project No. CHI8.0129. GE Prepared For: Forest Hill Church elo Johnston, Allison, & Hord Attorneys 1065 East Morehead Street Charlotte, Noilh Carolina 28204 December 13, 2018 Prepared By: GECDSCENCE GROUP 500 Clanton Road, Suite K Charlotte, North Carolina 28217 Phone (704) 525-2003 Facsimile (704) 525-2051 December 13, 2018 Consulting Engineers Forest Hill Church GEQSCIENCE c/o Johnston, Allison, & Hord Attorneys GROUP 1065 East Morehead Street Charlotte, North Carolina 28204 Attention, Mr. William Berkeley Reference. Phase 1 Environmental Site Assessment Forest Hill Church Parcels Concord, North Carolina Geoscience Project No. CHI 8.0129.GE EXECUTIVE SU1MI1lfARY Geoscience Group, Inc. (Geoscience) has completed a Phase I Environmental Site Assessment (ESA) of an approximate 1.854t acre tract located along the northeastern side of East 36"' Street, immediately north of its intersection with North McDowell Street in Charlotte, North Carolina. This Phase I ESA has been performed in general accordance with the scope and limitations of ASTM Standard E 1527.13 and in compliance with Geoscience's proposal dated August 21, 2018 (Geoscience Proposal No. CH18.197P.EV). Any exceptions to, or deletions from, the ASTM E 1527-13 standard of practice are described in the INTRODUCTION section of the report. Based upon our findings, this assessment has revealed no evidence of recognized environmental conditions in association with the subject property with the exception of the following: 1) Two (2) underground storage tanks (USTs) used to stnre heating oil were observed on the subject property: UST-1 adjacent to the single-family dwelling and UST-2 adjacent to the existing church. In an attempt to determine whether releases have occurred from these USTs, Geoscience advanced a total of four (4) hand auger borings HA-1 through HA-4) adjacent to the ends of the tanks. Soil samples collected from the borings were analyzed for total petroleum hydrocarbons in the gasoline and diesel fuel ranges (TPH-GRG and TPH-DRO). Neither TPH-GRO nor TPH-DRO were detected in the samples (HA-1 and HA-2) collected adjacent to UST-1. As such, it does not appear that releases have occurred from that tank. However, the soil samples collected adjacent to UST-2 (HA-3 and HA-4) exhibited TPH-GRO and TPH-DRO concentrations exceeding Action Limits established by NCDEQ (see Table 1 in Appendix 1). Based on the sample results, it is apparent a heating oil release has occurred from UST-2. Therefore, UST-2 is considered to be a recognized environmental condition in association with the subject property. 50G Cra';ion Roan Charsore. North. Carolina Teseohone Fac rue r.'C License 5ui1e K 2821', M4 525.2003 7C•152^ 210F-DS85 Forest Hill Church Geoscience Project No. CH18.0129.GE December 13, 2018 Page 2 INTRODUCTION Purpose: This Phase I ESA was performed to identify the presence or likely presence of any hazardous substances [as defined by CERCLA 42 USC §9601(14)] or petroleum products on the property under conditions that indicate an existing release, a past release, or a material threat of a release of these products into structures on the property or into the ground, groundwater, or surface water of the property. This includes hazardous substances or petroleum substances under conditions in compliance with laws. It should be noted that the ASTM E 1527-13 standard of practice does not include an assessment of all passible conditions or circumstances that may exist at the subject site. Several anon -scope considerations that were not a part of these assessment activities included reviews for asbestos, lead based paint, wetlands, and radon, among other items not addressed by ASTM Standard E 1527--13. Based on the information provided, the Phase I ESA was performed as part of a property transaction. As such, Geoscience understands that the purpose of the assessment was, in part, to satisfy a requirement to qualify for the innocent landowner defense to CERCLA liability. In accordance with the ASTM E 1527-13 standard of practice, this Phase I ESA included a reconnaissance of the subject site and adjoining properties, interviews with persons knowledgeable about the site, and a review of historical and regulatory databases. The site reconnaissance and interviews were performed as part of the assessment to obtain information indicating the likelihood of the presence of recognized environmental conditions. Historical and regulatory sources were reviewed to help identify recognized environmental conditions in connection with the property and to develop a history with respect to site usage. Practically reviewable, publicly available information pertaining to the property was also used to prepare the Phase I ESA. This report interprets and summarizes the information obtained from interviews, document reviews, and site reconnaissance. Per ASTM E 1527-13, it is the responsibility of the User of this document to investigate the existence of environmental liens in reasonably ascertainable recorded land title records. Site Reconnaissance: The most recent site visit was performed by Geoscience on October 12, 2018. The reconnaissance consisted of observing the periphery of the property and viewing the site from accessible adjacent public thoroughfares, where possible. Interior portions of the property were systematically traversed to provide an overlapping field of view. Visual reconnaissance of adjoining properties was limited to areas and facilities that were readily observable from the subject property or from public access areas. Photographs were taken to document the features observed and environmental conditions of concern. Due to the general limitations imposed by the method of observation, the potential exists that undisclosed environmental conditions may be present beneath the areas observed. A photographic log (Photographs l through 19) of the subject site has been provided in Appendix it of this report. The approximate locations and directions of the photographs are shown on the Site Layout, Figure No. CH18.129-3, in Appendix 1. Forest Hill Church Geoscience Project No_ CHI8.0129.GE December 13, 2018 Page 3 Interviews: The persons noted in the following table were contacted to obtain information for this assessment. Documentation of our contact with the listed parties is included in Appendix V of this report. Pertinent information reported by the listed parties is discussed in the appropriate sections of the report. Name Title/Function Affiliation Date Contact Information Mr. William Client Forest Hill Church Various (704) 622-8584 Berkeley Representive Mr. Tim Charlotte Fire Hartsell Battalion Ctcief Department 14J3118 (704) 336-2461 Information Provided by User: Geoscience requested that Forest Hill Church Attorneys (the Client and User of this document) communicate any specialized knowledge or experience that is material to recognized environmental conditions in connection with the property and to identify key personnel for interview purposes. As part of that request, User and Environmental Questionnaires were submitted to the Client for completion by appropriate people. Review of the questionnaires, as completed by Mr. William Berkeley, that revealed an oil tank is located adjacent to the church. Concerns related to the tank are discussed in the Site Reconnaissance Findings section later in this report. Copies of the completed User and Environmental Questionnaires are included in Appendix V. SITE DESCRIPTION AND PHYSICAL SEWNG Location And Leval_ Description: As shown on the enclosed. Vicinity Map, Figure No. CH18.129-1, the subject site, with the physical addresses of 719 and 729 East 36'h Street and 3315 North McDowell Street, is located along the northeastern side of East 36h Street, immediately north of its intersection with McDowell Street in Charlotte, North Carolina. The site is comprised of Mecklenburg County Tax Parcel ID Nos. 09110401 and 09110402. The approximate legal boundaries of the site are shown on the Tax Line Map included in Appendix I as Figure No. CH 18.129-2. Site And Vicinity Characteristics: As depicted on the Site Layout, Figure No. CHI8.129-3, the subject property is comprised of a 1.854+ acre tract. As shown in Photographs 1 through 7 in Appendix II, an existing church, its associated school, a single-family dwelling, and their associated outbuildings currently occupy the southern portion of the subject site. The remainder of the property, as shown in Photograph 8 through 11, consists of landscaped areas and a small garden. North Alexander Street extends along the northern property boundary. The land across this roadway fiom the subject site is occupied by The Church of Jesus Christ, its associated outbuildings, Mercury Apartments and a single-family dwelling. Six (6) single-family dwellings adjoin the subject site to the east. North McDowell Road extends along the southern property boundary. Forest Hill Church Geoscience Project No. CH18.0129.GE December 13, 2018 Page 4 The land across North McDowell Road from the subject site is occupied by condominiums and two (2) single-family dwellings. East 36eh Street extends along the western properly boundary. The land across this roadway from the subject site is occupied by five (5) single- family dwellings. Topography: As part of this assessment, the 2015 County Topographic Map (Figure No. CH18.129-5), and the 1967 (Photorevised 1988) "Charlotte East, North Carolina" United States Geological Survey (USGS) 7.5-minute quadrangle map (Figure No. CH 18.129-6) were reviewed to obtain information relative to the topography of the subject site and surrounding areas. According to the contour lines of the above listed topographic maps, the subject site is located between approximately 724 and 730 feet above mean sea level (MSL). The ground surface across the project site generally slopes downward toward the northwest. The low elevation of 724 feet MSL is located on the northern property boundary and the high elevation of 730 feet MSL is located on the and southeastern portion of the site. Surficial And Bedrock Geoloy: The 1985 Geologic Map of North Carolina was reviewed as a part of this assessment to provide discretionary and non-standard physical setting source information relative to the geology in the vicinity of the subject property. A review of this map indicates that the subject site is located within the Charlotte Belt of the Piedmont Physiographic Province. This Province is generally characterized by igneous intrusive and metamorphic bedrock that is Pennian to Ordovician in age. The intrusive rock is typically overlain with a layer of soil and weathered rock, ranging in thickness from 0 to 150 feet. Bedrock within the Charlotte Belt consists primarily of the diorite -granite complex, with granite appearing to be the predominant component of the complex_ According to the geologic map of North Carolina, the regional bedrock underlying the subject property generally consists of metamorphosed quartz diorite. Surface Water And Groundwater Flow: The predominant source of groundwater in the area is the unconfined aquifer system. Water availability in the aquifer varies with location, rock type, topographic setting, and geologic structure. Recharge of the aquifer system is through the infiltration of rainwater. Surface water and groundwater flow rates and directions were not determined as part of this assessment. However, based upon review of the USGS topographic map, the infen�ed direction of groundwater flow beneath the subject property is northwestward. Based upon visual observations and the site topography, Geoscience expects that surface water at the site flows towards the northwest. Soil Conservation Service Map Review: The United States Department of Agriculture Sail Conservation Service (SCS) conducted a soil survey of Mecklenburg County, North Carolina in cooperation with the North Carolina Agricultural Experiment Station. The soil survey information reviewed for this report was issued by the SCS in September 2016 and describes the soils at the subject site as Cecil -Urban land complex with 2 to 8 percent slopes (CuB) and Helena -Urban land complex with 2 to 8 percent slopes (HuB). Forest Hill Church Geosczence Project No. CHI8.0129,GE December 13, 2018 Page 5 Utilities: Utilities provided to the subject property include: • Electricity provided by Duke Energy; Natural gas provided by Piedmont Natural Gas; • Sewage disposal provided by Charlotte Water; and Potable water provided by Charlotte Water. Environmental Liens: Per ASTM E 1527-13 it is the responsibility of the User of this document to investigate the existence of environmental liens in reasonably ascertainable recorded land title records. PROPERTY USAGE Current Uses Of The Property: As previously described, the subject site is currently occupied by a church and a single-family dwelling. Past Uses Of The Property: To the extent practically possible, past uses of the subject property were identified through historical records review, reconnaissance observation, interviews, andlor through client -provided information. Historical information sources researched during this assessment date back to 1905. A summary of the standard historical sources and data reviewed by Geoscience to identify past uses of the property are listed in the table below. Copies of representative: historical source information are provided in the applicable Appendices. Historical Data Sources Years Reviewed Data Source/PubUsher Note 1948, 1956, 1965, 1968, 1971, 1976, 1983, 1988, 1993, 1996, 1998, 2002, Mecklenburg County GIS, Aerial Photographs 2004, 2045, 2006, 2007, 2008, 2009, Google Faith and EDR 2010, 2012, 2013, 2014, 2015, 2016, 2017, and 2018 Sanborn Maps p 1911, 1929, 19M, 1953, 1958, 1962, EDR and 1963 1921, 1925, 1931, 1937, 1944, 1949, City Directories1979, 1953, 1959, 1964, 1969,1974, 1975, EDR 1984, 1989, 1991,1994, 1999, 2005, 2010, and 2014 Property Tax Listings 2018 Mecklenburg County GIS County Topographic Map 2015 Mecklenburg; County GIS U5GS Topflt;raphic Map 1942 USGS, "Charlotte, NC' 30-minute quadrangle Forest Hill Church Geoscience Project No. CHI 8.0129.GE December 13, 2018 Page 6 USGS Topographic Map 1905 and 1907 USGS, "Charlotte, NC" 15-minute quadrangle 1948, 1949, 1967, 1980, 1988, and USGS, "Charlotte East; USGS Topographic Map NC" 7.5-minute 2013 uadra le USGS Topographic Map 1949, 1972, 1996, mid 2013 USGS, "Derita, NC" 7.5- minute quadrangle Forest Hill Church, the church's school, a single-family dwelling, and their associated outbuildings currently occupy the site. Mecklenburg County tax listings indicate that the church and its school were constructed in 1929 and 1957, respectively. The single --family dwelling was reportedly constructed in 1941. These dates are consistent with our review of aerial photographs and Sanborn reaps. Our review of city directory listings revealed that prior to operating as Forest Hill Church, the church had been occupied by North Charlotte Presbyterian Church and Johnston Memorial Presbyterian Church. Further review of aerial photographs and Sanborn maps reveals a former single-family dwelling occupied the southeastern portion of the site from at least 1929 until it was demolished in 2008. The 2013 aerial photograph depicts the southeastern portion of the site being used as a garden. The remainder of the site has been vacant land since at least 1929. Current And Past Uses Of Adjoining Properties: The current and past uses of adjoining properties were identified through reconnaissance observation and records review. North: North Alexander Street extends along the northern property boundary. Our review of Sanborn maps reveals construction of this roadway occurxed sometime between 1911 and 1929. The land across North Alexander Street from the subject site is occupied by The Church of Jesus Christ, its associated outbuildings, Mercury Apartments, and a single-family dwelling. Mecklenburg Cotmty tax listings indicate the church and its outbuildings were constructed in 1979, 1969, and 1980, respectively. Mercury Apartments and the single-family dwelling were reportedly constructed in 2014 and 1926, respectively. These dates are consistent with our review of aerial photographs and Sanborn maps. Further review of aerial photographs reveals that prior to construction of the existing improvernents, the areas northwest and north of the subject site had been occupied by single-family dwellings since at least 1929. EaW: Six (6) single-family dwellings adjoin the subject site to the east. Mecklenburg County tax listings indicate the houses were constructed at various times between 1926 and 2012_ These dates are consistent with our review of aerial photographs and Sanborn maps. Prior to construction of the newer homes, those eastern adjoining lots had been occupied by previous houses since at least 1929. South: North McDowell Street extends along the southern property boundary. Our review of Sanbom maps reveals this roadway was constructed before 1929. The land across North McDowell from the subject site is occupied by condominiums and two (2) single-family dwellings. Mecklenburg County tax listings indicate the condominiums were constructed in 2010 and the single-family dwellings in 2009 and 1926, respectively. Forest Hill Church Geoscience Project No. CH18.0129.GE December 13, 2018 Page 7 These dates are consistent with our review of aerial photographs and Sanborn maps. Further review of historical sources reveals that prior to construction of the existing buildings, the land that adjoins the subject site to the south had been occupied by single-family dwellings since at least 1929. West-: East 36`h Street extends along the western property boundary. Construction of this roadway predates the 1911 Sanborn map. Our review of Sanbom maps reveals the road was named 323,d Street from at least 1929 until at least 1950 when it is renamed 36 h Street. The land across East 36"' Street fiorn the subject site is occupied by five (5) single-family dwellings_ Mecklenburg County tax listings indicate the houses were constructed between 1905 and 1940. These dates are consistent with our review of aerial photographs and Sanborn maps. REGULATORY RECORDS REV2`EW Information for the standard Federal, State and Tribal environmental record sources specified in ASTM Standard E 1527-13 § 8.2.1 was obtained through Environmental Data Resources, Inc. (EDR). Regulatory database information was reviewed to help identify evidence of recognized environmental conditions in connection with the property. The number of listed sites identified within the approximate minimum search distance (AMSD) specified in the standard environmental records database are summarized in the table on the following pages. Detailed information for sites identified within the AMSD is provided following the table along with our professional judgment about the significance, if any, of the listing. Copies of the EDR research data and a description of the databases are included in Appendix 1V of this report. Target Search Total Database Distance <'A 'A—'I4 '1-1/a 'A— 1 >1 Plotted (Miles) Federal Records NPL 1 0 a 0 ❑ NR 0 Proposed NPL 1 0 0 0 0 NR 0 Delisted NPL 1 0 0 0 0 NR 0 NPL LIENS TP NR NR NR NR NR 0 CERCLIS '/7. 0 0 1 NR NR 1 CERC-NFRAP '/2 0 0 1 NR NR 1 LIENS 2 TP NR NR NR NR NR 0. CORRACTS 1 0 0 1 1 NR 2 RCRA L G '1 0 0 NR NR NR 0 RCRA S G 'I 0 a NR NR NR 0 RCRA CES G 1 0 0 NR NR NR 0 RCRA NonGen 'I 0 1 NR NR NR 1 RCRA-TSDF '%2 0 0 1 NR NR l US ENG CONTROLS '% 0 0 0 NR NR 0 Forest Hill Church Geoscience Project No. CHI8.0129.GE December 13, 2018 Page S Search Total Database Propeerty Distance <'/e /x-'/a %-Vx %7- 1 >1 Plotted (Miles) Federal Records (Continued) US INST CONTROL % 0 0 0 NR NR 0 ERNS TP NR NR NR NR NR 0 HMIRS TP NR NR NR NR NR 0 DOT OP S TP NR NR NR NR NR 0 US CDL TP NR NR NR NR NR 0 US BROWN FIELDS '1/a 0 0 0 NR NR 0 DOD 1 0 0 0 0 NR 0 FMS 1 0 0 0 0 NR 0 LUCIS �6 0 0 0 NR NR 0 CONSENT 1 0 0 0 0 NR 0 ROD 1 0 0 0 0 NR 0 UIVITRA '!2 0 0 0 NR NR 0 ODI '/a 0 0 0 NR NR 0 MINES J 0 0 NR NR NR 0 TRI5 TP NR NR NR NR NR 0 TSCA TP NR NR NR NR NR 0 FTTS TP NR NR NR NR NR 0 HIST FTTS TP NR NR NR NR NR 0 SSTS TI' NR NR NR NR NR 0 ICIS TP NR NR NR NR NR 0 PADS TP NR NR NR NR NR 0 NITS TP NR NR NR NR NR 0 RADINFO T? NR Nit NR NR NR 0 FMS TP NR NR NR NR NR 0 ECHO TP WR NR NR NR NR 0 RAATS TP NR NR NR NR NR 0 SCRD DRYCLEANERS 0 0 0 NR NR 0 State and Local Records SHW S 1 0 0 4 12 NR 16 NC HSDS 1 0 0 I 4 NR 5 IMD 'h 2 0 16 NR NR 18 SWFILF '/. 0 1 0 NR NR 1 OLI �� 0 0 0 NR NR 0 HIST LF 'IA 0 1 0 NR NR I LUST 'fx 2 4 I5 NR NR 21 LAST % 0 0 I NR NR 1 LUST TRUST 'A 0 3 3 NR NR 6 UST V. 2 0 NR NR NR 2 AST V4 0 0 NR NR NR 0 INST CONTROL % 0 0 0 NR NR 0 SWRCY 'I2 0 0 1 NR NR I Forest Hill Church Geoscience Project No. GHI8.0129.GE December 13, 2018 Page 9 Search Total Database Propecrty Distance <''A t1/9--'/a VI—'/z '/z— 1 >1 (Miles) Plotted State and Local Records (Continued) VCP Vz 0 1 0 0 NR NR 0 DRYCLEANERS V 0 0 NR KR NR 0 BRDWNFIELDS 2 2 NR NR 4 NPDES TP NR NR NR NR NR 0 Tribal Records INDIAN RESERV 1 0 0 0 0 NR 0 INDIAN DDI '/2 0 0 0 NR NR 0 INDIAN LUST °/2 0 0 0 NR NR 0 INDIAN UST % 0 0 NR NR NR 0 INDIAN VCP 1 �/z 0 0 0 1 NR NR 0 EDR Proprietary Records Manufactmd Gas 1 0 0 0 0 NR 0 Plant EDR Historical '' 3 NR NR NR NR 3 Auto Stations EDR Historical % 2 NR NR NR NR 2 Cleaners NOTES. TP = Target Property; NR = Not Requested at this Search distance; Sites may be listed in snore than one database. Subject Property Database Findings: No listings for the subject property were discovered during the regulatory records review, Adjoining Property Database Findings: No listings for adjoining properties were discovered during the regulatory records review. Non-Adioiniag Property Database Findings: EDR reported sixty-seven (67) listings for non -adjoining sites within the AMSD. Based upon their EDR-reported locations and review of the USGS topographic map, the non -adjoining sites appear to be situated within areas that are considered to be hydraulically down gradient or cross gradient from the subject property, with inferred directions of groundwater flowing away from the subject property. Given their inferred directions of groundwater flow, distances from the subject property, and/or regulatory status, the incidents associated with the non -adjoining properties are not expected to adversely impact the subject site. As such, we do not consider these sites to be recognized environmental conditions in association with the subject property. orphan Sites: During compilation of the EDR database report, some potential risk properties may be identified which cannot be accurately mapped due to poor or inadequate address information. These properties are usually listed in the EDR report as unmappable. According to EDR, three (3) listings for unznappable (orphan) sites were identified in the database findings. At the time of our site visit, a vehicular reconnaissance of the area within Forest Hill Church Geoscience Project No. CH18.0129.GE December 13, 2018 Page 10 approximately ''/s mile of the subject property was conducted in an effort to locate orphan sites. No orphan sites were identified as being in close proximity to the subject property. Additional Environmental Record Sources: Pursuant to ASTM Standard E 1527-13, additional environmental record sources were obtained to enhance and/or supplement the standard environmental record sources. As part of this Phase I ESA, records available an the North Carolina Department of Environmental Quality (NCDEQ) website were reviewed. In addition, the Mecklenburg County Emergency Management Department was contacted to provide supplemental information and determine if any environmental conditions are known to exist or have formerly existed at the subject site and/or off -site adjoining properties. The following issues were addressed with respect to the subject site and adjoining properties: • Groundwater Quality; • Surface Water Quality; • Solid Waste; • Surface Spills; • Hazardous Waste Storage and Disposal; and • Underground Storage Tanks (USTs). Geoscience discovered no records maintained by NCDEQ pertaining to the subject site or adjoining properties. The Mecklenburg County Emergency Management Department indicated that they had no records of hazardous material responses in the vicinity of the subject site. SITE RECONNAISSANCE FINDINGS Sub ect Property Reconnaissance Findings: As mentioned previously, a reconnaissance was performed at the subject site to obtain information indicating the likelihood of recognized environmental conditions in connection with the property. A summary of uses and conditions specifically addressed and consistent with ASTM Standard E 1527-13 is provided below: • Hazardous Substances In Connection With Identified Uses: No hazardous substances were observed on the subject site. Storage Tanks: As shown in Photographs 12 and 13 in Appendix II, two (2) underground storage tanks (USTs) used to store heating oil were observed on the subject site. UST-1 adjacent to the house; and UST-2 adjacent to the church. In an effort to determine whether releases have occurred from the tanks, Geosciertce performed four (4) hand auger borings (HA-1 through HA-4) adjacent to the ends of the USTs. The approximate locations of the tanks and hand auger borings are indicatod on the Sample Location Diagram, Figure No. CH18.129 4 in Appendix I. Each boring was advanced to a depth of ten (10) feet below the ground surface, and the retrieved cuttings were screened in the field with a photoionization detector (PID). Forest Hill Church Geoscience Project No. CH18.0129.GE December 13, 2018 Page 11 Based on the PID readings, one soil sample was selected from each boring for laboratory analysis. The selected samples (HA-1 through HA-4) were placed in laboratory supplied containem, packed on ice, and submitted under appropriate chain - of -custody to Prism Laboratories to be analyzed for total petroleum hydrocarbons in the gasoline and diesel fuel ranges (TPH-GRO and TPOH-DRO). The results of the soil sample analyses are listed in Table 1 in Appendix 1. As shown, neither TPH-GRO nor TOH-DRO were detected in the samples collected adjacent to UST-1. Based on these findings in conjunction with our observation of the soils fi-om borings HA-1 and HA-2, Geoscience concludes that a release from UST-1 is not likely. As such, we do not consider UST-1 to be a recognized environmental condition in association with the subject property. The soil samples collected adjacent to UST-2 (HA-3 and HA-4) exhibited petroleum concentrations exceeding the Action Limits of 100 mglkg and 50 mg/kg established by NCDEQ for TPH-GRO and TPH-DRO, respectively. Specifically, TPH-GRO and TPH-DRO were detected in sample HA-3 at concentrations of 2,300 mg/kg and 26,000 mg/kg, respectively. The concentration in sample HA-4 were 99 mg/kg TPH-GRO and 3,500 mgfkg TPH-DRO. Based on these sample results, it is apparent a heating oil release has occurred from UST-2. Therefore, the release from UST-2 is considered to be a recognized envirorunental condition in association with the subject property. Copies of the laboratory test reports are included in Appendix V. • Polychlorinated Biphenyls_ fPCBs : During the reconnaissance, three (3) pole mounted electrical transformers were observed on the subject site. As observed, the transformers appeared to be in good condition with no evidence of leak or discharge. Based on our observations, Geoscience does not consider the on -site transformers to be recognized environmental conditions in association with the subject property. • Indications Of Solid 'Waste Disposal: As shown in Photographs 14 through 19 in Appendix II, solid wastes consisting of empty bulk totes, plastic drums, plastic, and wood were observed on the southeastern portion of the site. No evidence of improper hazardous material disposal, staining, leaks, or unusual odors were observed in the vicinity of the observed wastes. With the exception of de minimis litter, no other indications of solid waste disposal were observed on the subject property. Adioinin2 Properties Reconnaissance Findings: A summary of uses and conditions specifically addressed at adjoining properties that are consistent with ASTM Standard E 1527- 13 § 9.4.2.3 through § 9.4.4.7 and indicate the likelihood of recognized environmental conditions in connection with the subject Site is provided below: • Bazardous Substances In Connection With Identified Uses: No hazardous substances were observed on properties adjoining the subject site. Forest Hill Church Geoscience Project No. CHI 8.0129.GE December 13, 2018 Page 12 ■ Storage Tanis: No above ground or underground storage tanks were observed on properties adjoining the subject site - Polychlorinated Bi hen is (PCBs): During the reconnaissance, three (3) pole mounted electrical transformers were observed on adjoining properties. As observed, the transformers appeared to be in good condition with no evidence of leak or discharge. Based on our observations, Geoscience does not consider the off -site transformers to be recognized enviroutnental conditions in association with the subject property. • Indications Of Solid Waste Disposal: With the exception of de minimis litter, no evidence of improper solid waste disposal, staining, leaks, or unusual odors were observed on adjoining properties during our reconnaissance. FINDINGS AND CONCLUSIONS Geoscience Group, Inc. (Geoscience) has completed a Phase I Environmental Site Assessment (ESA) of an approximate 1.854± acre tract located along the northeastern side of East 361h Street, immediately north of its intersection with North McDowell Street in Charlotte, North Carolina_ This Phase l ESA has been performed in general accordance with the scope and limitations of ASTM Standard E 1527-13 and in compliance with Geoscience's proposal dated August 21, 2018 (Geoscience Proposal No. CH18.197REV). Any exceptions to, or deletions from, the ASTM E 1527-13 standard of practice are described in the INTRODUCIYON section of the report. Based upon our findings, this assessment has revealed no evidence of recognized environmental conditions in association with the subject property with the exception of the following: 1) Two (2) underground storage tanks (USTs) used to store heating oil were observed on the subject property: UST-1 adjacent to the single-family dwelling and UST-2 adjacent to the existing church. In an attempt to determine whether releases have occurred from these USTs, Geoscience advanced a total of four (4) band auger borings HA-1 through HA-4) adjacent to the ends of the tanks. Soil samples collected frorn the borings were analyzed for total petroleum hydrocarbons in the gasoline and diesel fuel ranges (TPH-GRO and TPH-DRO). Neither TPH-GRO nor TPH-DRO were detected in the samples (HA-1 and HA-2) collected adjacent to UST-1. As such, it does not appear that releases have occurred from that tank. However, the soil samples collected adjacent to UST-2 (HA-3 and HA-4) exhibited TPH-GRO and TPH-DRO concentrations exceeding Action Limits established. by NCDEQ (see Table 1 in Appendix 1). Based on the sample results, it is apparent a heating oil release has occurred from UST-2. Therefore, UST-2 is considered to be a recognized environmental condition in association with the subject property. Forest Hill Church Consulting Enginms Geoscience Project No. CHI 8.0129.GE December 13, 2018 Page 13 Much of the information provided in this summary report is based upon personal interviews and review of available documents, records, and maps held by the appropriate govenunent GE9SCIENCE and private agencies. This summary is subject to the limitations of historical GROUP documentation, availability and accuracy of pertinent records and the personal recollection of those persons contacted. RELIANCE This report is intended for the sole use of Forest Hill Church, and its lending institution for this project. This report should not be relied upon by any other parties without the express written consent of Geoscience Group, Inc. QUALIFICATIONS This report was prepared by the undersigned environmental professionals whose qualifications are included in Appendix V11 of this report. We declare that, to the best of our professional knowledge and belief, we meet the definition of Environmental Professional as defined in §312.10 of 40 CFR§ 312. We have the specific qualifications based on education, training, and experience to assess a property of the nature, history, and setting of the subject property. We have developed and performed the all appropriate inquiries in conformance with the standards and practices set forth in 40 CFR Part 312. Geoscience appreciates the opportunity to be of service to you on this project. If you have any questions regarding this report or require additional information, please contact us. Respectfully, GEOSCIENCE GROUP, INC. Ashley N. Proctor Assistant Project Manager Thomas C. Hassett, P.E. Senior Engineer Enclosures EW 201,Y129 — kr= HUU C3meb Parcels ESA_dm APPENDIX I Maps and Sketches: Figure No. CHI 8.129-1 - Vicinity Map Figure No. CHI 8.129-2 - Tax Line Map Figure No. CHI 8,129-3 - Site Layout Figure No. CH 18.129-4 — Sample Location Diagram Figure No. CHI8.129-4 - 2015 County Topographic Map Figure No. CHI 8.129-5— 1967 (Photorevised 1988) USGS Topographic Map Table 1: Summary of Soil Sampling Results GEOSCIENCE GROUP, INC. J CHARLOTTE, NORTH CAROLINA I SCALE: ]";� 210m, APPROVED BY: DRAWN BY ADC DATE; Octobci 3, 2018 1<w REVISED: ANP FOREST HILL CHURCH PARCELS I CHARLOTTE, NORTH CAROLINA VICINITY MAP RGURL NUMBER: CH18.129-1 o , 3ti �'tsaoart� � % 06830RT14 � /083087 12�� .(, o �534411A ,� titi%68 N `�OSr11[#3d3 1• �'��'•••'OS�i1U5T.�,�fj1'. � � jos ti w_ i 425) -- - - --- iMop r-------- 1A414 - g3G2 1 09i10 � 68174#07 "110408 t i (i) f r r �0911 fl d4�f / J 1 41 L -r 11,08312316~i TV �l9lifl S ti 7'6E+12 ' (45} *� 10 3 ldl� I GEOSCIENCE GROUP, INC: CHARLOTTE, NORTH CAROLINA SCALE: V � 123' APPROVED BY: DRAWN BY. Mecklenburg Co. 4i� I DATE: October 3, 2018 REVISED: ANP FOREST HILL CHURCH PARCELS CHARLOTTE, NORTH CAROLINA TAX LINE MAP E NUMBER: CH18.129-2 €t Sj( itial ehaitorrc Charlotte S� �. isirlFtifxifl {{ `�. � ti � Resiclenlial Y ti 1Y ;. SITE Residential ItcsidrteTial•: . 1.85 4+ AcRF'S T Residential ct,srtotte y�y0 , s. . ,�� � Charicttc Residential Residential . p Residential . Condominiums irnis� / y rio XdLSiflE'nt.ial r: Itesic]entit .,_� /fha joy e -1 a, LEGEND: approximate Location of SaFnpEes Uudaground Storage Tank lk s 4 GEOSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE-- 1" 25' ,APPROVED BY: DRAWN BY; Mecklenburg Co. DATE! October 18, 2018 REVISED: ANP I FOREST HILL CHURCH PARCELS I CHARLOTTE, NORTH CAROLINA SAMPLE LOCATION DIAGRAM E NUMBER: CH18.129-4 • 4 •� tt 9 K' C11 r � r � ' e SITE 5�i � • r • • a, p •.fix e .+•�i-Ll ....... r r .R � RI • Y �{ s GEGSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE: 1" 95' APPRQVFT) BY: BRAWN BY: Mecklenburg Co. �aN DATE: October 3, 20IS I �c I REVISED; ANP FOREST HILL CHURCH PARCELS CHARLOTTE, NORTH CAROLINA FIGURE IVLIIVIBER: 2015 COUNTY TOPOGRAPHIC MAP CH1BER: 5 6- ThQ GEOSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE: V z 2,000' JAPPROVED BY: , A / DRAWN BY: USGS TE: October 3, 2018 FOREST HILL CHURCH PARCELS CHARLOTTE, NORTH CAROLINA 1967 USG5 TOPOGRAPHIC MAP (PHOTOREVISED 1988) ANP E NUMBER- CH18.129-6 Table 1: Summary of Soil Sampling Results Revision 10/2612018 Project: Forest Hill Church Parcels Project No, CH18.0129.GE Date: Analytical Method TPH (mg/kg) Contaminant of Concern ❑ 0 Sample Location Sample depth (ft) Date Collected I. HA-1 7.5 10/512018 E9.9 { 7.5 HA-2 8 10/512018 <9.9 <7.5 HA-3 $ 10/12/2018 26,000 2,300 HA-4 10 10/1212018 3,500 99 North Carolina Action limits for Total Petroleum Hydrocarbons (TPH) 100 50 APPENDIX II Site Photographs 1 through 19 1) Forest Hill Church located on the on the southern portion of the subject site. 3) The existing house located on the southern -central portion of the site. site. 4) Shed located on the northern -central portion of the subject property. 5) Shed located on the eastern portion of the subject site. 6) Portable restrooms located on the eastern portion of the site. 7) Shed located on the eastern portion of the site. 8) The northern portion of the subject site as seen facing southeast from North Alexander Street. 9) The subject site as seen facing southwest from the eastern property boundary. 10) The southern portion of the subject site as seen facing northwest from North McDowell Street. 11) The western portion of the site as seen facing northeast from East 36`" Street. 12) Vent and fill pipe for an underground storage tank (UST) observed adjacent to the house on the southern -central portion of the site. 14) Drum observed on the eastern portion of the subject site. 13) Vent and fill pipe for a UST observed adjacent to the church on the southern portion of the subject property. 15) Bulk totes observed on the eastern portion of the subject site. I Lin, '. x,i�,yr' •S �r•�:1+�i}r_ _•�'yy�.,•:'ni�.' l ��* M APPENDIX III Historical Research Documentation: EDR Aerial Photo Decade Package Certified Sanborn Map Report EDR City Directory Abstract EDR Historical Topo Map Report Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 Inquiry Number: 5441860.8 October 03, 2018 6 Armstrong Road, 4th floor Shelton, CT 06484 (rEDR� Toll Free: 800.352.0050 www.edrnet.com EDR Aerial Photo Decade Package 10/03/18 I Site Name: Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 EDR Inquiry # 5441860.8 Client Name: Geoscience Group 500 Clanton Road Charlotte, NC 28217 Contact: Ashley Proctor 2ra Environmental Data Resources, Inc. (EDR) Aerial Photo Decade Package is a screening tool designed to assist environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR's professional researchers provide digitally reproduced historical aerial photographs, and when available, provide one photo perdecade. Search Results: Year Scale Details Source 2016 1 "=500' Flight Year: 2016 USDA/NAIP 2012 1 "=500' Flight Year: 2012 USDA/NAIP 2009 1 "=500' Flight Year: 2009 USDA/NAIP 2006 1 "=500' Flight Year: 2006 USDA/NAIP 1996 1 "=500' Flight Date: April 25, 1996 NCDOT 1993 1 "=500' Acquisition Date: January 28, 1993 USGS/DOQQ 1988 1 "=500' Flight Date: October 12, 1988 USDA 1983 1 "=500' Flight Date: March 03, 1983 USGS 1976 1 "=500' Flight Date: March 01, 1976 USGS 1971 1 "=500' Flight Date: March 18, 1971 USGS 1968 1 "=500' Flight Date: February 25, 1968 USDA 1965 1 "=500' Flight Date: February 22, 1965 USGS 1956 1 "=500' Flight Date: March 31, 1956 USDA 1948 1 "=500' Flight Date: May 15, 1948 USGS When delivered electronically by EDR, the aerial photo images included with this report are for ONE TIME USE ONLY. Further reproduction of these aerial photo images is prohibited without permission from EDR. For more information contact your EDR Account Executive. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 5441860 - 8 page 2 i •-4p ,,,. Vt '.�,•t � `sue �•��. _r:` J �' s•w� k.� ! ��■ ;qt � ' �-_-� � � � ,.� .. � r ..r �� ice"' � 1% ZZ I It YEAR: 2012 Aim MAW ILI 500 eEDR -- !� M •��,`�L _4 ` �77 "��F;. 74 �� ' .�4ic. �'^l' 'r' �,�'-gin e � [ 's� � l it i' �_ - y •.m r' t � .,�. r ..y �t ka ow 'i Rl 1 dour Q.pt x � �KVV_ r. _ j} � ., J � .����. .i�, _ '•� -y . fit !1 `�. ' `_�• ri Li ry • .CIS 1 �` Y, FF o7c •_ J t dL .46 �.. •�J INQUIRY #5 860.8 �, t ' ,' • ` 7 , NSb- VK� {. YEAR: 4��' �:•'�r� ��;. • ^ 4 .� � 4> • ��'- . � CeEDR �6 7� k ► I. . r IN ' u v. • >P �'Ap { �• . r T i -'000 - poor .,. ow_ . to 06 sfit �.1 1 Yl = z wr' 0400 d 4 10000, � � � 4 I ri/ 1 �r� N� � •� / ` ter, + w � - y •Al 41 1 +u► • , ry ` � � , ` � D � �� r ■ * ` I � � J � ` e ire � ;�Q f • r .z 40 eb� ' ■'' h j ... LL . NO Ila Ar �� � 1 _ `�" i • � ,fir r • r � �• � ok Alk old �= r r i r A lk 160/ �. AW r �� r sp p f ' 1 11w i rph + + y� 0 40 F + , ■ #* f i � a � ♦ram+ f i' � J `, I � � � - _ , jj� -Awl IL ��' • ti 4k .A + db } dt '■ �p mil# SL a Fir op 4��fib Ap e jr �MEMO L � - [ ffL op ■ • do .49 _ r F I�lQI! RY #: 5441860.8 ; 1 YEAR: 1976 — AIL 500, ��7' � ti. x M1 � y� .. Grp. ! .. �; � •_.,�' � aAp ilk � � � � yy. � � � � � ''..• � er�. ! . _^ . , � , � r rw fix. ���� ��� • k '� Y 10. ko • ,� �• ari .1 +7 }T■ � "f .ice �'�� �,� M �. .l Ar + ���,. - _. � -• •ram , + � �. r^t� . ONO to y _ - � r: ti. 1 '� _gym, r+/!,. ��: ;�� � • `-= _ _ '� .�Y�' y- '" -r•r„O'9 - •y� J .. %,a �l:R � w '�• � r \ ��� ., �.��•r� �y F., T;.1'� pw dot lk •,'�. `4. -:_ w - , ONO 4�K tip are � r+. ^--!'.�g+a_. t . � • sir., r« �,.• �„ - a� L � �! �'•/"� �" r�1- � + II INQUIRY #: 5441860.8� ,,�'•,¢'"� ,— _ LI 4 -, YEAR: 1965 r=•� '°. / �'`� (LL,. EDR �,�"• � � to � r F? ��� � �,,!: f bid �e - ., sA•. � rh' . R° x6 i , i a� :� � � • �. ;ram I � ' '�. � �,. Ail 99 F ,� � ` i _,7: Y ''err �i� {. w� e �• . 1i 33�� yy • �W �� �iT ..S �y Jam' 5 �i� ' � `R J>• ,,,, y� , y• � _ H � 1 lk i � ? d A`., �� ..�+ + T{J � N • yY C � � i yy���y� Y� �� r PS �'` . '. '1�G- °A. �,�'#'r � .f. �#➢I � 3e`s.. .. �. ¶ yl *{` mul IC IAWP Al 46 i4 �� - :.�' -gig!• Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 Inquiry Number: 5441860.3 October 02, 2018 6 Armstrong Road, 4th floor (rEDR� Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com Certified Sanborn® Map Report 10/02/18 Site Name: Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 EDR Inquiry # 5441860.3 Client Name: Geoscience Group 500 Clanton Road Charlotte, NC 28217 Contact: Ashley Proctor The Sanborn Library has been searched by EDR and maps covering the target property location as provided by Geoscience Group were identified for the years listed below. The Sanborn Library is the largest, most complete collection of fire insurance maps. The collection includes maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow, and others. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction of maps by the Sanborn Library LLC, the copyright holder for the collection. Results can be authenticated by visiting www.edrnet.com/sanborn. The Sanborn Library is continually enhanced with newly identified map archives. This report accesses all maps in the collection as of the day this report was generated. Certified Sanborn Results: Certification # 9006-4D7E-8BD7 Po # Project Maps Provided: 1963 1962 1958 1953 1950 1929 1911 NA Forest Hill Church Parcels Limited Permission To Make Copies Sanborn® Library search results Certification #: 9006-4D7E-8BD7 The Sanborn Library includes more than 1.2 million fire insurance maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow and others which track historical property usage in approximately 12,000 American cities and towns. Collections searched: f Library of Congress f University Publications of America f EDR Private Collection The Sanborn Library LLC Since 1866T" Geoscience Group (the client) is permitted to make up to FIVE photocopies of this Sanborn Map transmittal and each fire insurance map accompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made directly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission is conditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as leqal advice. Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 5441860 - 3 page 2 Sanborn Sheet Key This Certified Sanborn Map Report is based upon the following Sanborn Fire Insurance map sheets. 1963 Source Sheets Volume 2, Sheet 257 Volume 2, Sheet 1963 1963 1962 Source Sheets Volume 2, Sheet 257 Volume 2, Sheet 1962 1962 1958 Source Sheets Volume 2, Sheet 257 Volume 2, Sheet 1958 1958 1953 Source Sheets Volume 2, Sheet 259 Volume 2, Shee 1953 1953 5441860 - 3 page 3 Sanborn Sheet Key This Certified Sanborn Map Report is based upon the following Sanborn Fire Insurance map sheets. 1950 Source Sheets Volume 2, Sheet 259 1950 1929 Source Sheets Volume 2, Sheet 259 1929 1911 Source Sheets Volume 1, Sheet 91 1911 5441860 - 3 page 4 CEDW Certified Sanborn® Map 1963 0, y� r AL1r7�ANDES `-J_-------` 64 g r44 oy� 9 EE •� � F 1 4 "�S m 8� rii L ,l 'A10 1v'� p• X]• r p p o 'llp'0 d a O S P� � / O V a Site Name: Forest Hill Church Parcels �] Address: 729E 36TH ST City, ZIP: CHARLOTTE, 28205 Client: Geoscience Group EDR Inquiry: 5441860.3 Order Dale: 10/02/2018 CertWcation! 9006-4D7E-8BD7 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. 1 Volume 2, Sheet 259 e 6 Volume 2, Sheet 257 257 e.. � �� Ia •�' � Pq� ``e rF4 YY � PY ` ' 4 ®® sqf• �' q" jam, }.•, �da , • � 0 Feet 150 300 600 -N• 5441860 - 3 page 5 CEDW Certified Sanborn® Map 1962 r •9 t r r1 h y P �'t N AS �xp��R �F w8Q p "g�� ,� '•P' e w � S 2f 9 r m z. 4. 2E ❑ F 5, �/ s�i4 �• # c �`f ;v 9 A J �0 Site Name: Forest Hill Church Parcels ` Address: 729 E 36TH ST, City, ST, ZIP: CHARLOTTE, INC 28205 ��. �• 9 Client: Geoscie—Group EDR Inquiry: 5441860.3 Order Dale: 1018 w Certification t 9006-4D063D7E-BBD7 8 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. Volume 2, Sheet 259 V01ume 2, Sheet 257 257 259 0 Feet 150 300 600 -N• 5441860 - 3 page 6 EDR° Certified Sanborn® Map 1958 D �y PLO •!s, � a �f Site Name: Forest Hill Church Parcels Address: 729 E 36TH ST City, ST, ZIP: CHARLOTTE, INC 28205 Client: Geoscie—Group EDR Inquiry: 5441860.3 Order Dale: 10/02/2018 �p/ Certification E 9006-4D7E-8BD7 - 956 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. Volume 2, Sheet 259 Volume 2, Sheet 257 257 259 a r "!ed' L � 9 ,c I i I I 0 Feet 150 300 600 -N• 5441860 - 3 page 7 CEDW Certified Sanborn® Map 0 I WDE \� G� \\ �ti.Y ` pLS a ✓ ~Y---`------ A4EXA % ` y 5 ^� 9 .4 ' Site Name. Forest HIII Church Parcels r � n Address: 729 E 36TH ST�Ji� /{�\ City, ST, ZIP: CHARLOTTE, NC 28205 Client: Ge—ie—Group EDR Inquiry5441860.3 Ord,, Date: 10/02/2018 71 ti Certification t 90064NE-BBD7 l This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. Volume 2, Sheet 257 '- Volume 2, Sheet 259 257 259 1953 ;I I I I 0 Feet 150 300 600 -N• 5441860 - 3 page 8 CEDW Certified Sanborn® Map 1950 r'6L•3� ';- '- f F F 0 51) � _ • � x t r V .� 1 W E ^'C `�' Sidi' • N � W✓ 1 g { 92tQ � „ '�4Y Qp �'- •� Q�- /V\` mod• � � L Site Name: Forest Hill Church Parcels Address: 729 E 36TH ST City, ST, ZIP: CHARLOTTE, INC 28205 Client: Geoscience Group EDR Inquiry: 5441860.3 Order Dale: 10/02/2018 Certification E 9006-4D7E-8BD7 1 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. Volume 2, Sheet 259 p � 0II 4 a 259 Q. 0 Feet 150 300 600 I -N• 5441860 - 3 page 9 CEDW Certified Sanborn® Map 1929 ro C U �? a: f W _ � � v 31 5L' j o < v 2ci 6,, �0 s` 4 t 4` 9 4 0 a rCsg ffi r. g 5Ca �.✓ �ja ` 9 � � m s � rii m �w o `� rn �a 9 9 m � A � Site Name: Forest Hill Church Parcels ` P Address 729 E 36TH ST \ 1 l • @- City, ST, ZIP: CHARLOTTE, INC 28205 •Y CA Client: Geoscience Group '.}'-''0 EDR Inquiry: 5441860.3 Order Dale: 10/02/2018 Certification E 9006-4D7E-8BD7 C—riaht 1929 M SR f �t ,�, Y• This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection. v.. Volume 2, Sheet 259 16 ® A e ! 4 A 259 ✓' o- 0 Feet 150 300 600 I -N• 5441860 - 3 page 10 (CEDR' Certified Sanborn® Map 'k, 2, A IV Site Name: Forest Hill Church Parcels Add— 729 E 36TH ST City, ST, ZIP: CHARLOTTE, INC 28205 Client: Geowie— Group EDIR Inquiry 5441860.3 This Certified Sanborn Map combines the following sheets Outlined areas indicate map sheets within the collection. Volume 1, Sheet 91 I i I I 0 Feet 150 300 600 5441860 - 3 page 11 Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 Inquiry Number: 5441860.4 October 02, 2018 6 Armstrong Road, 4th floor (rEDR� Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com EDR Historical Topo Map Report 10/02/18 Site Name: Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 EDR Inquiry # 5441860.4 Client Name: Geoscience Group 500 Clanton Road Charlotte, NC 28217 Contact: Ashley Proctor CEDW EDR Topographic Map Library has been searched by EDR and maps covering the target property location as provided by Geoscience Group were identified for the years listed below. EDR's Historical Topo Map Report is designed to assist professionals in evaluating potential liability on a target property resulting from past activities. EDRs Historical Topo Map Report includes a search of a collection of public and private color historical topographic maps, dating back to the late 1800s. Search Results: Coordinates: P.O.# NA Latitude: 35.246331 35' 14' 47" North Project: Forest Hill Church Parcels Longitude:-80.802412 -80° 48' 9" West UTM Zone: Zone 17 North UTM X Meters: 517976.04 UTM Y Meters: 3900378.68 Elevation: 729.66' above sea level Maps Provided: 2013 1907 1996 1905 1988 1980 1967,1972 1949 1948 1942 Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 5441860 - 4 page 2 Topo Sheet Key This EDR Topo Map Report is based upon the following USGS topographic map sheets. 2013 Source Sheets Charlotte East Derita 2013 2013 7.5-minute, 24000 7.5-minute, 24000 1996 Source Sheets Derita 1996 7.5-minute, 24000 Aerial Photo Revised 1993 1988 Source Sheets Charlotte East 1988 7.5-minute, 24000 Aerial Photo Revised 1984 1980 Source Sheets Charlotte East 1980 7.5-minute, 24000 Aerial Photo Revised 1976 5441860 - 4 page 3 Topo Sheet Key This EDR Topo Map Report is based upon the following USGS topographic map sheets. 1967, 1972 Source Sheets Charlotte East 1967 7.5-minute, 24000 Aerial Photo Revised 1965 1949 Source Sheets Charlotte East 1949 7.5-minute, 24000 Aerial Photo Revised 1948 1948 Source Sheets Charlotte East 1948 7.5-minute, 24000 Aerial Photo Revised 1948 1942 Source Sheets CHARLOTTE 1942 30-minute, 125000 Derita 1972 7.5-minute, 24000 Aerial Photo Revised 1971 Derita 1948 7.5-minute, 24000 Aerial Photo Revised 1948 5441860 - 4 page 4 Topo Sheet Key This EDR Topo Map Report is based upon the following USGS topographic map sheets. 1907 Source Sheets r Charlotte 1907 15-minute, 62500 1905 Source Sheets Charlotte 1905 15-minute, 48000 5441860 - 4 page 5 (eEDW Historical Topo Map 201; SugarV Of Creek ii airta 3 x. Wood .CjrOOERELtARR.` �0 {� a } 110, R458URY AVE ASBURYAVE I.,'' o GLVRYST; _ ---...- _..... -LIB. 29 ills ,— Junction z Sugar Greek y } efl Burying Ground qg j c• 1 Ir` ` CA o g h RAL�rGN ST.29 RQ REDWOOD AVE- OWEN 2aT ` _ ti 4 m LARO. SY p� a ,y pR£ s� ewood _ 4 ff _ 4� �yF Ea:t no oair c h•4�F drT _ ,? \. .. h.CH. s ' Sr., `\ ° ''I ' •yEE'r, 9 Ake �.. ❑ 5 s - yA�� iR4j - LAW' WpQ . Lf7GH AVf 54fJp Ayf- !• ``�a �y��a � �� ��y��"sj,� ETrERf T'f ��'• � ����{ I �r� i i � � �sTyST ��C, 1�',, -_- _ ��� � ! Y Rp 5l i��gA4�L .. - ;� - -•: p4�A� o H �r BEI.MI]1VT : �- G _ .e.� -_ Ai4bARD o 'rI, � �a �'AViN ARLQTT w - Ar;_ R �. MECKLENBURG AVE o� 2 0 a . � s� N w4�P � ���y4.;• �p�'. I ,, ti r .�. - �`:��F. .f I--.� — _ _(„ @Fyr��,r� � s� q Midwood -R - 4. ' � V N This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 2013, 7.5-minute N, Derita, 2013, 7.5-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N 5441860 - 4 page 6 CEDW Historical Topo Map gc f ' Y Druid �• J� g S i k kCh04 7, �.1F$ �o • T7 rr --ty � ill � ~ �I '4 •/ $'1 ��i This report includes information from the following map sheet(s). NW N NE N, Derita, 1996, 7.5-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N 5441860 - 4 page 7 CEDW Historical Topo Map ggE �z.. � H.,•�i n k ti ,.fir,. - I'► p r.i., ,AW lx f� J i a. This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 1988, 7.5-minute t t� • �• y i � � .Il LyJ'. ., e'� 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 11 N 5441860 - 4 page 8 CEDW Historical Topo Map gg t• j r r� � g I � � ..A. � I•I l,ia If This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 1980, 7.5-minute Go� OV�S 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N 5441860 - 4 page 9 CEDW Historical Topo Map 1967. 19 f � L A A �J ■ 1 P r�O� � e ndv Juno ` o . �7J,• �� G _ N urnlrxaek is W •ce t yyt TM 5❑ f� I jGS urse • % ;y �' ram. d L _ � +�,���• ��- ' Wit a�Fo.Trn+ : ✓ :'a) ! land AM, .os7d harlRf� J, ,,per r ¢vuntry ukr �y . rH 4 i`. .lr n tiihJ 'u f'EN d Hi¢h This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 1967, 7.5-minute N, Derita, 1972, 7.5-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 11 lN• 5441860 - 4 page 10 CEDW Historical Topo Map 194� Sn • 46� ''s• GFeaLwGGd Tow it OVA �r 1 • • Q � f� r + i`J rF I t it 1 �I+ • • • • IL--__ �- it .F, jr �j •'► • Ala I�r L��i 1 '. • r • C ario#te u '��Vou Clubpiedm ram"` d • ° "� "•� ds This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 1949, 7.5-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N 5441860 - 4 page 11 CEDW Historical Topo Map 194E • b m ter Grove r • �' �� ti c - . ,AtandB ��� ii u • `@@h• ° ��o - �. June t �': , • 4�=tea Y r• JI .r • . :y. f ''� Sugar Creek o I Ch &� Jh y•• 1° ����,� �� o¢therd States ��� g4 ��S•� 'r `;;'.- _�Fairgrbunds I' Ire Jf�• `� +' ��5» +i + ,. , ..`_ � der°'•,, to !�•• • � • .IYNF.•�N = `l•�`•'- � c� 1�•`'J�' of - Ba J.t £�R •"r � l�l � Eastwood e Tcwerr = i ] a �s �7��1 �'++ ♦ � � � o'er y*`��•� ' ... WWI- � l` ••AN r 1E{tfl7Jr h This report includes information from the following map sheet(s). NW N NE TP, Charlotte East, 1948, 7.5-minute N, Derita, 1948, 7.5-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N• 5441860 - 4 page 12 s • Ojef ■iof: le t A goes ILI CEDW Historical Topo Map 190 t•�— �- f "� �0A 0 • f. r� c 4 Ole « * + If rI L _ Uri r, 4 This report includes information from the following map sheet(s). NW N NE TP, Charlotte, 1907, 15-minute E1 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N 5441860 - 4 page 14 CEDR' Historical Topo Map g( • - I � y� J r v! • This report includes information from the following map sheet(s). NW N NE TP, Charlotte, 1905, 15-minute 0 Miles 0.25 0.5 1 1.5 SITE NAME: Forest Hill Church Parcels ADDRESS: 729 E 36TH ST CHARLOTTE, NC 28205 CLIENT: Geoscience Group 1 N� 5441860 - 4 page 15 APPENDIX IV Regulatory Records Documentation: EDR Radius Map Report Forest Hill Church Parcels 729 E 36TH ST CHARLOTTE, NC 28205 Inquiry Number: 5441860.2s October 02, 2018 6 Armstrong Road, 4th floor Shelton, CT 06484 ,fc Toll Free: 800.352.0050 rEDR' www.edrnet.com FORM-LBC-CCA TABLE OF CONTENTS SECTION PAGE Executive Summary ES1 OverviewMap----------------------------------------------------------- 2 DetailMap-------------------------------------------------------------- 3 Map Findings Summary 4 MapFindings------------------------------------------------------------ 8 Orphan Summary--------------------------------------------------------- 452 Government Records Searched/Data Currency Tracking- - - - - - - - - - - - - - - - - - - - - - - - - - GR-1 GEOCHECK ADDENDUM Physical Setting Source Addendum A-1 Physical Setting Source Summary A-2 Physical Setting SSURGO Soil Map ------------------------------------------- A-6 Physical Setting Source Map------------------------------------------------ A-13 Physical Setting Source Map Findings A-15 Physical Setting Source Records Searched PSGRA Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. TC5441860.2s Page 1 EXECUTIVE SUMMARY A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR). The report was designed to assist parties seeking to meet the search requirements of EPA's Standards and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for Environmental Site Assessments (E 1527-13), the ASTM Standard Practice for Environmental Site Assessments for Forestland or Rural Property (E 2247-16), the ASTM Standard Practice for Limited Environmental Due Diligence: Transaction Screen Process (E 1528-14) or custom requirements developed for the evaluation of environmental risk associated with a parcel of real estate. TARGET PROPERTY INFORMATION ADDRESS 729 E 36TH ST CHARLOTTE, NC 28205 COORDINATES Latitude (North): Longitude (West): Universal Tranverse Mercator: UTM X (Meters): UTM Y (Meters): Elevation: 35.2463310 - 35' 14' 46.79" 80.8024120 - 80° 48' 8.68" Zone 17 517976.5 3900180.5 730 ft. above sea level USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY Target Property Map: Version Date: North Map: Version Date: AERIAL PHOTOGRAPHY IN THIS REPORT 5948285 CHARLOTTE EAST, NC 2013 5948299 DERITA, NC 2013 Portions of Photo from: 20140524, 20140603 Source: USDA TC5441860.2s EXECUTIVE SUMMARY 1 MAPPED SITES SUMMARY Target Property Address: 729 E 36TH ST CHARLOTTE, NC 28205 Click on Map ID to see full detail. MAP ID SITE NAME ADDRESS Reg SAFETY KLEEN CORP Reg GENERAL LATEX & CHEM Reg ICI - AMERICAS INC Reg DETREX CHEMICAL INDU Reg HENKEL CORP. Al COLUMBUS OIL CO (BRS 516 E 36TH A2 NORTH CHARLOTTE SERV 516 EAST 36TH STREET A3 NORTH CHARLOTTE LAUN 3306B N DAVIDSON ST 4 JOHNSTON MILL APARTM 3315 NORTH DAVIDSON A5 NORTH HIGHLANDER CEN 3220 N DAVIDSON A6 CHARLOTTE MOTOR CO 500 E 36TH A7 FIRE STATION 7 3210 N DAVIDSON ST A8 BILLS SERVICE GROC 3307 N DAVIDSON ST B9 BIO ECOLOGICAL SERVI 720 HERRIN AVE B10 BIO ECOLOGICAL SERVI 720 HERRIN AVENUE C11 VESPOINT PROPERTY 3112 NORTH DAVIDSON C12 FAT CITY SITE 3123 NORTH DAVIDSON 13 SINCLAIR REFINING CO 409 E. 35TH ST. AND 14 NEW LIFE THEOLOGICAL 3117 WHITING AVENUE 15 NODA TEXTILE 430 E. 36TH STREET 16 STEEL GARDENS 3445 SPENCER STREET 17 PAUL MCBROOM RESIDEN 3000 NORTH DAVIDSON D18 L & N TIRE SERVICE 300 E 36TH STREET D19 L & N TIRE SERVICE 300 EAST 36TH STREET E20 HIGHLAND MILLS PARK 2901 N DAVIDSON STRE E21 HIGHLAND MILLS 2901 NORTH DAVIDSON 22 INX (FORMER) FACILIT 3200 & 3210 CULLMAN D23 L & N TIRE CO. 240 E. 36TH ST. F24 TRANSMISSION SUPPLY 624 ANDERSON STREET F25 TRANSMISSION SUPPLY 642 ANDERSON STREET G26 ABERNATHY LUMBER COM 308 EAST CRAIGHEAD R G27 ABERNATHY LUMBER COM 308 E. CRAIGHEAD ROA G28 CRAIGHEAD RD. 308 E. CRAIGHEAD RD; 29 VIRGINIA MOORE TRUST 3404 RITCH AVENUE H30 TREX PROPERTIES SITE 3114 CULLMAN AVENUE H31 DETREX CHEMICAL INDU 3114 CULLMAN 132 YUASA-EXIDE DISTRIBU 3713 N. DAVIDSON ST. J33 QUICK SHOPPE # 9 3435 THE PLAZA J34 QUIK SHOPPE 9 3435 THE PLAZA DATABASE ACRONYMS RELATIVE ELEVATION NC HSDS Same NC HSDS Same NC HSDS Same NC HSDS Same NC HSDS Same EDR Hist Auto Lower NC LUST, NC UST, NC IMD Lower EDR Hist Cleaner Lower NC LUST, NC IMD Lower EDR Hist Cleaner Lower EDR Hist Auto Lower NC UST Higher EDR Hist Auto Lower RCRA NonGen / NLR Higher NC SWF/LF, NC HIST LF Higher NC LUST, NC LUST TRUST Lower NC LUST, NC LUST TRUST Lower NC BROWNFIELDS Lower NC LUST, NC LUST TRUST Higher NC BROWNFIELDS Higher NC LUST Higher NC LAST Lower NC IMD Lower NC LUST Lower NC LUST, NC BROWNFIELDS, NC IMD Lower NC IMD Lower NC SHWS Lower NC LUST, NC UST, NC IMD Lower NC IMD Higher NC LUST Higher NC LUST Lower NC UST, NC IMD Lower NC BROWNFIELDS Lower NC LUST Lower SEMS Lower SEMS-ARCHIVE, CORRACTS, RCRA-TSDF, RCRA-LQG, NC ... Lower NC SHWS Higher NC IMD Higher NC LUST, NC LUST TRUST, NC UST Higher DIST (ft. & mi.) DIRECTION 3151, 0.597, SW 3623, 0.686, WSW 4868, 0.922, West 1798, 0.341, WNW 3022, 0.572, NE 554, 0.105, NW 554, 0.105, NW 556, 0.105, NW 590, 0.112, NNW 593, 0.112, WNW 601, 0.114, NW 622, 0.118, WNW 631, 0.120, NW 692, 0.131, ENE 692, 0.131, ENE 869, 0.165, West 928, 0.176, WNW 988, 0.187, WNW 1093, 0.207, South 1134, 0.215, NW 1195, 0.226, East 1577, 0.299, WSW 1594, 0.302, NW 1594, 0.302, NW 1805, 0.342, West 1805, 0.342, West 1807, 0.342, NW 1846, 0.350, NW 1933, 0.366, ENE 1960, 0.371, ENE 2098, 0.397, NNE 2098, 0.397, NNE 2098, 0.397, NNE 2191, 0.415, NNW 2215, 0.420, WNW 2215, 0.420, WNW 2254, 0.427, NE 2264, 0.429, ESE 2264, 0.429, ESE 5441860.2s Page 2 MAPPED SITES SUMMARY Target Property Address: 729 E 36TH ST CHARLOTTE, NC 28205 Click on Map ID to see full detail. MAP ID SITE NAME ADDRESS RELATIVE DATABASE ACRONYMS ELEVATION DIST (ft. & mi.) DIRECTION 35 PHILEMON AVE SITE E CRAIGHEAD RD & PHI NC SHWS Lower 2305, 0.437, NNE K36 EXPRESS #525(E-Z SER 3400 THE PLAZA NC LUST TRUST Higher 2406, 0.456, SE K37 SAMS MART 26 3400 THE PLAZA NC LUST, NC UST, NC Financial Assurance Higher 2406, 0.456, SE K38 E-Z SERVE #525 3400 THE PLAZA NC IMD Higher 2406, 0.456, SE 139 COX, BORDERS, SHAVER 3725 N DAVIDSON STRE NC LUST, NC IMD Higher 2426, 0.459, ENE L40 PET DAIRY 3300 THE PLAZA NC LUST TRUST, NC IMD Higher 2437, 0.462, SE L41 PET DAIRY 3300 THE PLAZA NC LUST, NC UST Higher 2437, 0.462, SE M42 AMOCO #1106-GORDIES 3129 THE PLAZA NC IMD Higher 2438, 0.462, SSE M43 GORDIES AMOCO 3129 THE PLAZA NC LUST, NC UST Higher 2438, 0.462, SSE 44 CAROLINA CONSOLIDATO 400 E 33RD STREET NC SHWS, NC LUST, NC UST, NC IMD Lower 2519, 0.477, West M45 C MART 442 3109 THE PLAZA NC LUST, NC UST Higher 2519, 0.477, SSE M46 COASTAL MART #442 3109 THE PLAZA NC IMD Higher 2519, 0.477, SSE 47 SOUTHERN RESOURCES, 3826 RALEIGH ST. NC SWRCY Lower 2576, 0.488, NNE 48 AMBROSIA HOOTEN CHOC 3746 NORTH DAVIDSON NC LUST, NC IMD Higher 2615, 0.495, ENE 49 TARMAC VIRGINIA, INC 3934 RALEIGH STREET NC LUST, NC IMD Lower 2628, 0.498, NE 50 CHADBOURN GOTHAM, IN JORDAN PL & DAVIDSON NC SHWS Lower 2953, 0.559, WSW 51 MELATEX INC (FORMER 3818 NORTHMORE ST NC SHWS Higher 3009, 0.570, ENE 52 WISE RECYCLING - CHA 600 E. SUGAR CREEK R NC SHWS, NC SWRCY Higher 3249, 0.615, NE 53 GENUINE PARTS COMPAN 124 ATANDO AVENUE NC SHWS, NC VCP Lower 3330, 0.631, NW 54 KAISER FLUID TECHNOL 530 SUGAR CREEK RD E NC SHWS, NC BROWNFIELDS, NC IMD, RCRA NonGen /... Lower 3723, 0.705, NE N55 GENERAL LATEX & CHEM 2321 N. DAVIDSON ST NC SHWS Lower 3738, 0.708, WSW N56 RH BOULIGNY INC. 2320 NORTH DAVIDSON NC SHWS, NC LUST, NC LAST, NC IMD Lower 3762, 0.712, WSW 57 SAFETY KLEEN CORP 20 YADKIN AVE (2320) SEMS-ARCHIVE, CORRACTS, RCRA-TSDF, RCRA-LQG, US ... Lower 3795, 0.719, SW 058 GIBBS ELECTROPLATING 2229 N DAVIDSON NC SHWS, NC IMD Lower 4144, 0.785, WSW 59 NCDOT DIV 10 FACILIT 1119 E SUGAR CREEK R NC SHWS, NC LAST, NC IMD Higher 4197, 0.795, East 060 APPLIED RESEARCH GRO 2221 N. DAVIDSON STR NC SHWS Lower 4228, 0.801, WSW 61 DIXON QUICK COUPLING 332 ATANDO AVE NC SHWS, NC LAST, NC BROWNFIELDS, NC IMD, RCRA... Lower 4369, 0.827, NW 62 OMNISOURCE SE/ATLANT 410 ATANDO AVE NC SHWS Lower 4806, 0.910, NW 5441860.2s Page 3 EXECUTIVE SUMMARY TARGET PROPERTY SEARCH RESULTS The target property was not listed in any of the databases searched by EDR. DATABASES WITH NO MAPPED SITES No mapped sites were found in EDR's search of available ("reasonably ascertainable ") government records either on the target property or within the search radius around the target property for the following databases: STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL National Priority List Proposed NPL---------------- Proposed National Priority List Sites NPL LIENS Federal Superfund Liens Federal Delisted NPL site list Delisted NPL National Priority List Deletions Federal CERCLIS list FEDERAL FACILITY---------. Federal Facility Site Information listing Federal RCRA generators list RCRA-SQG RCRA - Small Quantity Generators RCRA-CESQG RCRA - Conditionally Exempt Small Quantity Generator Federal institutional controls / engineering controls registries LUCIS------------------------ Land Use Control Information System US ENG CONTROLS Engineering Controls Sites List US INST CONTROL Sites with Institutional Controls Federal ERNS list ERNS------------------------ Emergency Response Notification System State and tribal landfill and/or solid waste disposal site lists NC OLI Old Landfill Inventory State and tribal leaking storage tank lists INDIAN LUST Leaking Underground Storage Tanks on Indian Land State and tribal registered storage tank lists FEMA UST------------------- Underground Storage Tank Listing TC5441860.2s EXECUTIVE SUMMARY 4 EXECUTIVE SUMMARY NC AST______________________ AST Database INDIAN UST Underground Storage Tanks on Indian Land State and tribal institutional control / engineering control registries NC INST CONTROL No Further Action Sites With Land Use Restrictions Monitoring State and tribal voluntary cleanup sites INDIAN VCP------------------ Voluntary Cleanup Priority Listing ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS A Listing of Brownfields Sites Local Lists of Landfill / Solid Waste Disposal Sites INDIAN ODI Report on the Status of Open Dumps on Indian Lands DEBRIS REGION 9----------- Torres Martinez Reservation Illegal Dump Site Locations ODI Open Dump Inventory IHS OPEN DUMPS Open Dumps on Indian Land Local Lists of Hazardous waste / Contaminated Sites US HIST CDL---------------- Delisted National Clandestine Laboratory Register US CDL National Clandestine Laboratory Register Local Land Records LIENS 2 CERCLA Lien Information Records of Emergency Release Reports HMIRS_______________________ Hazardous Materials Information Reporting System NC SPILLS Spills Incident Listing NC SPILLS 90 SPILLS 90 data from FirstSearch NC SPILLS 80________________ SPILLS 80 data from FirstSearch Other Ascertainable Records FUDS Formerly Used Defense Sites DOD Department of Defense Sites SCRD DRYCLEANERS______. State Coalition for Remediation of Drycleaners Listing EPA WATCH LIST EPA WATCH LIST TSCA Toxic Substances Control Act TRIS_________________________ Toxic Chemical Release Inventory System SSTS Section 7 Tracking Systems ROD Records Of Decision RMP _________________ Risk Management Plans RAATS RCRA Administrative Action Tracking System PRP Potentially Responsible Parties PADS________________________ PCB Activity Database System TC5441860.2s EXECUTIVE SUMMARY 5 EXECUTIVE SUMMARY ICIS-------------------------- Integrated Compliance Information System FTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) MLTS------------------------ Material Licensing Tracking System COAL ASH DOE Steam -Electric Plant Operation Data COAL ASH EPA Coal Combustion Residues Surface Impoundments List PCB TRANSFORMER-------_ PCB Transformer Registration Database RADINFO Radiation Information Database HIST FTTS FIFRA/TSCA Tracking System Administrative Case Listing DOT OPS-------------------- Incident and Accident Data CONSENT Superfund (CERCLA) Consent Decrees INDIAN RESERV Indian Reservations FUSRAP--------------------- Formerly Utilized Sites Remedial Action Program UMTRA Uranium Mill Tailings Sites LEAD SMELTERS Lead Smelter Sites US AIRS--------------------- Aerometric Information Retrieval System Facility Subsystem US MINES Mines Master Index File ABANDONED MINES Abandoned Mines FINDS-----------------------. Facility Index System/Facility Registry System ECHO Enforcement & Compliance History Information UXO Unexploded Ordnance Sites DOCKET HWC--------------- Hazardous Waste Compliance Docket Listing FUELS PROGRAM EPA Fuels Program Registered Listing NC AIRS Air Quality Permit Listing NC COAL ASH--------------- Coal Ash Disposal Sites NC DRYCLEANERS Drycleaning Sites NC NPDES NPDES Facility Location Listing NC UIC----------------------. Underground Injection Wells Listing NC AOP Animal Operation Permits Listing EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP EDR Proprietary Manufactured Gas Plants EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives NC RGA HWS---------------- Recovered Government Archive State Hazardous Waste Facilities List NC RGA LF Recovered Government Archive Solid Waste Facilities List NC RGA LUST Recovered Government Archive Leaking Underground Storage Tank SURROUNDING SITES: SEARCH RESULTS Surrounding sites were identified in the following databases Elevations have been determined from the USGS Digital Elevation Model and should be evaluated on a relative (not an absolute) basis. Relative elevation information between sites of close proximity should be field verified. Sites with an elevation equal to or higher than the target property have been differentiated below from sites with an elevation lower than the target property. Page numbers and map identification numbers refer to the EDR Radius Map report where detailed data on individual sites can be reviewed. Sites listed in bold italics are in multiple databases. Unmappable (orphan) sites are not considered in the foregoing analysis. TC5441860.2s EXECUTIVE SUMMARY 6 EXECUTIVE SUMMARY STANDARD ENVIRONMENTAL RECORDS Federal CERCLIS list SEMS: SEMS (Superfund Enterprise Management System) tracks hazardous waste sites, potentially hazardous waste sites, and remedial activities performed in support of EPA's Superfund Program across the United States. The list was formerly know as CERCLIS, renamed to SEMS by the EPA in 2015. The list contains data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities, private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). This dataset also contains sites which are either proposed to or on the National Priorities List (NPL) and the sites which are in the screening and assessment phase for possible inclusion on the NPL. A review of the SEMS list, as provided by EDR, and dated 07/17/2018 has revealed that there is 1 SEMS site within approximately 0.5 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page TREX PROPERTIES SITE 3114 CULLMAN AVENUE WNW 1/4 - 1/2 (0.420 mi.) H30 52 Federal CERCLIS NFRAP site list SEMS-ARCHIVE: SEMS-ARCHIVE (Superfund Enterprise Management System Archive) tracks sites that have no further interest under the Federal Superfund Program based on available information. The list was formerly known as the CERCLIS-NFRAP, renamed to SEMS ARCHIVE by the EPA in 2015. EPA may perform a minimal level of assessment work at a site while it is archived if site conditions change and/or new information becomes available. Archived sites have been removed and archived from the inventory of SEMS sites. Archived status indicates that, to the best of EPA's knowledge, assessment at a site has been completed and that EPA has determined no further steps will be taken to list the site on the National Priorities List (NPL), unless information indicates this decision was not appropriate or other considerations require a recommendation for listing at a later time. The decision does not necessarily mean that there is no hazard associated with a given site; it only means that. based upon available information, the location is not judged to be potential NPL site. A review of the SEMS-ARCHIVE list, as provided by EDR, and dated 07/17/2018 has revealed that there is 1 SEMS-ARCHIVE site within approximately 0.5 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page DETREX CHEMICAL INDU Site ID: 0402782 EPA Id: NCD049773245 Federal RCRA CORRACTS facilities list 3114 CULLMAN WNW 114 - 112 (0.420 mi.) H31 53 CORRACTS: CORRACTS is a list of handlers with RCRA Corrective Action Activity. This report shows which nationally -defined corrective action core events have occurred for every handler that has had corrective action activity. A review of the CORRACTS list, as provided by EDR, and dated 03/01/2018 has revealed that there are 2 TC5441860.2s EXECUTIVE SUMMARY 7 EXECUTIVE SUMMARY CORRACTS sites within approximately 1 mile of the target property. Lower Elevation DETREX CHEMICAL INDU EPA ID:: NCD049773245 SAFETY KLEEN CORP EPA ID:: NCD079060059 Address RTifL�fl9��u/ 6�1 20 YADKIN AVE (2320) Federal RCRA non-CORRACTS TSD facilities list Direction / Distance Map ID Page WNW 114 - 112 (0.420 mi.) H31 53 SW 112 - 1 (0.719 mi.) 57 311 RCRA-TSDF: RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Transporters are individuals or entities that move hazardous waste from the generator offsite to a facility that can recycle, treat, store, or dispose of the waste. TSDFs treat, store, or dispose of the waste. A review of the RCRA-TSDF list, as provided by EDR, and dated 03/01/2018 has revealed that there is 1 RCRA-TSDF site within approximately 0.5 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page DETREX CHEMICAL INDU 3114 CULLMAN WNW 114 - 112 (0.420 mi.) H31 53 EPA ID:: NCD049773245 State- and tribal - equivalent NPL NC HSDS: The Hazardous Substance Disposal Sites list contains locations of uncontrolled and unregulated hazardous waste sites. The file contains sites on the national priority list as well as the state priority list. The data source is the North Carolina Center for Geographic Information and Analysis. A review of the NC HSDS list, as provided by EDR, and dated 08/09/2011 has revealed that there are 5 NC HSDS sites within approximately 1 mile of the target property. Equal/Higher Elevation Address SAFETY KLEEN CORP GENERAL LATEX & CHEM ICI - AMERICAS INC DETREX CHEMICAL INDU HENKEL CORP. State- and tribal - equivalent CERCLIS Direction / Distance Map ID Page SW 1/2 - 1 (0.597 mi.) 0 WSW 1/2 - 1 (0.686 mi.) 0 W 1/2 -1 (0.922 mi.) 0 WNW 1/4 - 1/2 (0.341 mi.) 0 NE 1/2 -1 (0.572 mi.) 0 NC SHWS: The State Hazardous Waste Sites records are the states' equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. The data come from the Department of Environment & Natural Resources' Inactive Hazardous Sites Program. A review of the NC SHWS list, as provided by EDR, and dated 05/01/2018 has revealed that there are 16 TC5441860.2s EXECUTIVE SUMMARY 8 EXECUTIVE SUMMARY NC SHWS sites within approximately 1 mile of the target property Equal/Higher Elevation Address YUASA-EXIDE DISTRIBU 3713 N. DAVIDSON ST. Facility Id: NONCD0001051 MELATEX INC (FORMER 3818 NORTHMORE ST Facility Id: NONCD0002820 WISE RECYCLING - CHA 600 E. SUGAR CREEK R Facility Id: NCD990715062 NCDOT DIV 10 FACILIT 1119 E SUGAR CREEK R Facility Id: NONCD0002179 Lower Elevation Address INX (FORMER) FACILIT Facility Id: NCD081332900 PHILEMON AVE SITE Facility Id: NONCD0003005 CAROLINA CONSOLIDATO Facility Id: NONCD0002890 CHADBOURN GOTHAM, IN Facility Id: NONCD0003012 GENUINE PARTS COMPAN Facility Id: NONCD0001764 KAISER FLUID TECHNOL Facility Id: NONCD0001946 GENERAL LATEX & CHEM Facility Id: NCD081430258 RH BOULIGNY INC. Facility Id: NONCD0002356 GIBBS ELECTROPLATING Facility Id: NONCD0001022 APPLIED RESEARCH GRO Facility Id: NCD047257472 DIXON QUICK COUPLING Facility Id: NONCD0002293 OMNISOURCE SE/ATLANT Facility Id: NONCD0001333 3200 & 3210 CULLMAN E CRAIGHEAD RD & PHI 400 E 33RD STREET JORDAN PL & DAVIDSON 124 ATANDO AVENUE 530 SUGAR CREEK RD E 2321 N. DAVIDSON ST 2320 NORTH DAVIDSON 2229 N DAVIDSON 2221 N. DAVIDSON STIR 332 ATANDO AVE 410 ATANDO AVE Direction / Distance Map ID Page NE 1/4 - 1/2 (0.427 mi.) 132 251 ENE 1/2 - 1 (0.570 mi.) 51 287 NE 112 - 1 (0.615 mi.) 52 288 E 112 - 1 (0.795 mi.) 59 441 Direction / Distance Map ID Page NW 1/4 - 1/2 (0.342 mi.) 22 38 NNE 1/4 - 1/2 (0.437 mi.) 35 255 W 114 - 112 (0.477 mi.) 44 274 WSW 1/2 - 1 (0.559 mi.) 50 287 NW 112 - 1 (0.631 mi.) 53 288 NE 112 - 1 (0.705 mi.) 54 288 WSW 1/2 - 1 (0.708 mi.) N55 305 WSW 112 - 1 (0.712 mi.) N56 305 WSW 112 - 1 (0.785 mi.) 058 439 WSW 1/2 - 1 (0.801 mi.) 060 444 NW 112 - 1 (0.827 mi.) 61 444 NW 1/2 - 1 (0.910 mi.) 62 451 State and tribal landfill and/or solid waste disposal site lists NC SWF/LF: The Solid Waste Facilities/Landfill Sites records typically contain an inventory of solid waste disposal facilities or landfills in a particular state. The data come from the Department of Environment & Natural Resources' List of Solid Waste Facility Contacts in Alpha Order. A review of the INC SWF/LF list, as provided by EDR, and dated 04/18/2018 has revealed that there is 1 TC5441860.2s EXECUTIVE SUMMARY 9 EXECUTIVE SUMMARY NC SWF/LF site within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page BIO ECOLOGICAL SERVI 720 HERRIN AVENUE ENE 118 - 114 (0.131 mi.) B10 21 Facility Status: InactiveClosed Permit Num: 60071-INCIN-1- State and tribal leaking storage tank lists NC LUST: The Leaking Underground Storage Tank Incidents Management Database contains an inventory of reported leaking underground storage tank incidents. The data come from the Department of Environment, & Natural Resources' Incidents by Address. A review of the NC LUST list, as provided by EDR, and dated 08/03/2018 has revealed that there are 21 NC LUST sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page NEW LIFE THEOLOGICAL 3117 WHITING AVENUE S 118 - 114 (0.207 mi.) 14 25 Incident Number: 40079 Current Status: File Located in Archives STEEL GARDENS 3445 SPENCER STREET E 1/8 - 1/4 (0.226 mi.) 16 27 Incident Number: 36141 Current Status: File Located in House TRANSMISSION SUPPLY 642 ANDERSON STREET ENE 1/4 - 1/2 (0.371 mi.) F25 43 Incident Phase: Closed Out Incident Number: 8826 Current Status: File Located in Archives QUIK SHOPPE 9 3435 THE PLAZA ESE 114 - 112 (0.429 mi.) J34 252 Incident Phase: Follow Up Incident Number: 8641 Current Status: File Located in House SAMS MART 26 3400 THE PLAZA SE 114 - 112 (0.456 mi.) K37 256 Incident Phase: Closed Out Incident Number: 22149 Current Status: File Located in Archives COX, BORDERS, SHAVER 3725 N DAVIDSON STRE ENE 114 - 112 (0.459 mi.) 139 260 Incident Phase: Closed Out Incident Number: 8633 Current Status: File Located in Archives PET DAIRY 3300 THE PLAZA SE 114 - 112 (0.462 mi.) L41 264 Incident Phase: Follow Up Incident Number: 5705 Current Status: File Located in House GORDIES AMOCO 3129 THE PLAZA SSE 114 - 112 (0.462 mi.) M43 268 Incident Phase: Closed Out Incident Number: 3475 Current Status: File Located in Archives C MART 442 3109 THE PLAZA SSE 114 - 112 (0.477 mi.) M45 277 Incident Phase: Response TC5441860.2s EXECUTIVE SUMMARY 10 EXECUTIVE SUMMARY Incident Number: 8792 Current Status: File Located in House AMBROSIA HOOTEN CHOC Incident Phase: Closed Out Incident Number: 27127 Current Status: File Located in Archives Lower Elevation 3746 NORTH DAVIDSON ENE 114 - 112 (0.495 mi.) 48 282 Address Direction / Distance Map ID Page NORTH CHARLOTTE SERV 516 EAST 36TH STREET NW 0 - 118 (0.105 mi.) A2 10 Incident Phase: Closed Out Incident Number: 21688 Current Status: File Located in Archives JOHNSTON MILL APARTM 3315 NORTH DAVIDSON NNW 0 - 118 (0.112 mi.) 4 14 Incident Phase: Closed Out Incident Number: 27257 Current Status: File Located in Archives VESPOINT PROPERTY 3112 NORTH DAVIDSON W 118 - 114 (0.165 mi.) C11 21 Incident Phase: Closed Out Incident Number: 40183 Current Status: File Located in Archives FAT CITY SITE 3123 NORTH DAVIDSON WNW 118 - 114 (0.176 mi.) C12 23 Incident Number: 36395 Current Status: File Located in House L & N TIRE SERVICE 300 EAST 36TH STREET NW 1/4 - 1/2 (0.302 mi.) D19 32 Incident Phase: Closed Out Incident Number: 16670 Current Status: File Located in Archives HIGHLAND MILLS PARK 2901 N DAVIDSON STRE W 114 - 112 (0.342 mi.) E20 34 Incident Phase: Closed Out Incident Number: 23762 Current Status: File Located in Archives L & N TIRE CO. 240 E. 36TH ST. NW 114 - 112 (0.350 mi.) D23 38 Incident Phase: Closed Out Incident Number: 14306 Current Status: File Located in Archives ABERNATHY LUMBER COM 308 EAST CRAIGHEAD R NNE 1/4 - 1/2 (0.397 mi.) G26 44 Incident Phase: Closed Out Incident Number: 27267 Incident Number: 36559 Current Status: File Located in Archives VIRGINIA MOORE TRUST 3404 RITCH AVENUE NNW 1/4 - 1/2 (0.415 mi.) 29 50 Incident Phase: Closed Out Incident Number: 40211 Current Status: File Located in Archives CAROLINA CONSOLIDATO 400 E 33RD STREET W 114 - 112 (0.477 mi.) 44 274 Incident Phase: Closed Out Incident Number: 13260 Current Status: File Located in Archives TARMAC VIRGINIA, INC 3934 RALEIGH STREET NE 114 - 112 (0.498 mi.) 49 284 Incident Phase: Follow Up TC5441860.2s EXECUTIVE SUMMARY 11 EXECUTIVE SUMMARY Incident Number: 8613 Current Status: File Located in House NC LAST: A listing of leaking aboveground storage tank site locations. A review of the NC LAST list, as provided by EDR, and dated 08/03/2018 has revealed that there is 1 NC LAST site within approximately 0.5 miles of the target property. Lower Elevation Address Direction / Distance Map ID PAUL MCBROOM RESIDEN 3000 NORTH DAVIDSON Incident Number: 91013 Current Status: C WSW 1/4 - 1/2 (0.299 mi.) 17 NC LUST TRUST: This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. A review of the INC LUST TRUST list, as provided by EDR, and dated 07/06/2018 has revealed that there are 6 NC LUST TRUST sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID NEW LIFE THEOLOGICAL 3117 WHITING AVENUE S 118 - 114 (0.207 mi.) 14 Site ID: 40079 QUIK SHOPPE 9 3435 THE PLAZA ESE 114 - 112 (0.429 mi.) J34 Facility Id: 0-013942 Site ID: 8641 EXPRESS #525(E-Z SER 3400 THE PLAZA SE 1/4 - 1/2 (0.456 mi.) K36 Facility Id: 0-013873 Site ID: 22149 PET DAIRY 3300 THE PLAZA SE 114 - 112 (0.462 mi.) L40 Facility Id: 0-013774 Site ID: 5705 Lower Elevation VESPO/NT PROPERTY Site ID: 40183 FAT CITY SITE Site ID: 36395 r.lr_ r_ erraa 3112 NORTH DAVIDSON 3123 NORTH DAVIDSON Direction / Distance Map ID W 118 - 114 (0.165 mi.) C11 WNW 118 - 114 (0.176 mi.) C12 State and tribal registered storage tank lists NC UST: The Underground Storage Tank database contains registered USTs. USTs are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA). The data come from the Department of Environment & Natural Resources' Petroleum Underground Storage Tank Database. A review of the NC UST list, as provided by EDR, and dated 07/27/2018 has revealed that there are 2 Page 29 Page 25 252 255 263 Page 21 23 TC5441860.2s EXECUTIVE SUMMARY 12 EXECUTIVE SUMMARY NC UST sites within approximately 0.25 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page FIRE STATION 7 3210 N DAVIDSON ST WNW 0 - 1/8 (0.118 mi.) A7 17 Tank Status: Removed Tank Status: Current Facility Id: 00-0-0000017340 Lower Elevation Address Direction / Distance Map ID Page NORTH CHARLOTTE SERV 516 EAST 36TH STREET NW 0 - 118 (0.105 mi.) A2 10 Tank Status: Removed Facility Id: 00-0-0000003325 State and tribal Brownfields sites NC BROWNFIELDS: A brownfield site is an abandoned, idled, or underused property where the threat of environmental contamination has hindered its redevelopment. All of the sites in the inventory are working toward a a brownfield agreement for cleanup and liabitliy control. A review of the INC BROWNFIELDS list, as provided by EDR, and dated 06/01/2018 has revealed that there are 4 NC BROWNFIELDS sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page NODA TEXTILE 430 E. 36TH STREET NW 1/8 - 1/4 (0.215 mi.) 15 27 Project ID: 19028-15-60 Lower Elevation SINCLAIR REFINING CO Project ID: 20019-16-60 HIGHLAND MILLS PARK Project ID: 20037-16-60 CRAIGHEAD RD. Project ID: 18015-14-60 ADDITIONAL ENVIRONMENTAL RECORDS Address Direction / Distance Map ID Page 409 E. 35TH ST. AND WNW 1/8 - 1/4 (0.187 mi.) 13 25 2901 N DAVIDSON STRE W 1/4 - 1/2 (0.342 mi.) E20 34 308 E. CRAIGHEAD RD; NNE 1/4 - 1/2 (0.397 mi.) G28 50 Local Lists of Landfill / Solid Waste Disposal Sites NC HIST LF: A listing of solid waste facilities. A review of the NC HIST LF list, as provided by EDR, and dated 11/06/2006 has revealed that there is 1 NC HIST LF site within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page BIO ECOLOGICAL SERVI 720 HERRIN AVENUE ENE 118 - 114 (0.131 mi.) B10 21 TC5441860.2s EXECUTIVE SUMMARY 13 EXECUTIVE SUMMARY Facility Status: CLOSED Facility Id: P0667 NC SWRCY: A listing of recycling center locations. A review of the NC SWRCY list, as provided by EDR, and dated 05/03/2018 has revealed that there is 1 NC SWRCY site within approximately 0.5 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page SOUTHERN RESOURCES, 3826 RALEIGH ST. NNE 1/4 - 1/2 (0.488 mi.) 47 281 Records of Emergency Release Reports NC IMD: Incident Management Database. A review of the NC IMD list, as provided by EDR, and dated 07/21/2006 has revealed that there are 18 NC IMD sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page TRANSMISSION SUPPLY 624 ANDERSON STREET ENE 1/4 - 1/2 (0.366 mi.) F24 42 Facility Id: 8826 QUICK SHOPPE # 9 3435 THE PLAZA ESE 1/4 - 1/2 (0.429 mi.) J33 251 Facility Id: 8641 E-Z SERVE #525 3400 THE PLAZA SE 1/4 - 1/2 (0.456 mi.) K38 259 Facility Id: 22149 COX, BORDERS, SHAVER 3725 N DAVIDSON SIRE ENE 114 - 112 (0.459 mi.) 139 260 Facility Id: 8633 PET DAIRY 3300 THE PLAZA SE 114 - 112 (0.462 mi.) L40 263 Facility Id: 5705 AMOCO #1106-GORDIES 3129 THE PLAZA SSE 1/4 - 1/2 (0.462 mi.) M42 267 Facility Id: 3475 COASTAL MART #442 3109 THE PLAZA SSE 1/4 - 1/2 (0.477 mi.) M46 280 Facility Id: 8792 AMBROSIA HOOTEN CHOC 3746 NORTH DAVIDSON ENE 114 - 112 (0.495 mi.) 48 282 Facility Id: 27127 Lower Elevation Address Direction / Distance Map ID Page NORTH CHARLOTTE SERV 516 EAST 36TH STREET NW 0 - 118 (0.105 mi.) A2 10 Facility Id: 21688 JOHNSTON MILL APARTM 3315 NORTH DAVIDSON NNW 0 - 118 (0.112 mi.) 4 14 Facility Id: 27257 L & N TIRE SERVICE 300 E 36TH STREET NW 1/4 - 1/2 (0.302 mi.) D18 31 Facility Id: 16670 HIGHLAND MILLS PARK 2901 N DAVIDSON STRE W 114 - 112 (0.342 mi.) E20 34 Facility Id: 23762 HIGHLAND MILLS 2901 NORTH DAVIDSON W 1/4 - 1/2 (0.342 mi.) E21 36 TC5441860.2s EXECUTIVE SUMMARY 14 Facility Id: 85764 L & N TIRE CO. Facility Id: 14306 ABERNATHY LUMBER COM Facility Id: 27267 DETREX CHEMICAL INDU Facility Id: 85654 CAROLINA CONSOLIDATO Facility Id: 13260 TARMAC VIRGINIA, INC Facility Id: 8613 Other Ascertainable Records EXECUTIVE SUMMARY 240 E. 36TH ST. NW 114 - 112 (0.350 mi.) D23 38 308 E. CRAIGHEAD ROA NNE 114 - 112 (0.397 mi.) G27 48 3114 CULLMAN WNW 114 - 112 (0.420 mi.) H31 53 400 E 33RD STREET W 114 - 112 (0.477 mi.) 44 274 3934 RALEIGH STREET NE 114 - 112 (0.498 mi.) 49 284 RCRA NonGen / NLR: RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non -Generators do not presently generate hazardous waste. A review of the RCRA NonGen / NLR list, as provided by EDR, and dated 03/01/2018 has revealed that there is 1 RCRA NonGen / NLR site within approximately 0.25 miles of the target property. Equal/Higher Elevation BIO ECOLOGICAL SERVI EPA ID:: NCD982099889 EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records Address Direction / Distance Map ID Page 720 HERRIN AVE ENE l/8 - 1/4 (0.131 mi.) B9 19 EDR Hist Auto: EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. A review of the EDR Hist Auto list, as provided by EDR, has revealed that there are 3 EDR Hist Auto sites within approximately 0.125 miles of the target property. Lower Elevation COLUMBUS OIL CO (BRS CHARLOTTE MOTOR CO BILLS SERVICE GROC Address Direction / Distance Map ID Page 516 E 36TH NW 0 - 1/8 (0.105 mi.) Al 9 500 E 36TH NW 0 - 1/8 (0.114 mi.) A6 17 3307 N DAVIDSON ST NW 0 - 1/8 (0.120 mi.) A8 19 TC5441860.2s EXECUTIVE SUMMARY 15 EXECUTIVE SUMMARY EDR Hist Cleaner: EDR has searched selected national collections of business directories and has collected listings of potential dry cleaner sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include dry cleaning establishments. The categories reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. A review of the EDR Hist Cleaner list, as provided by EDR, has revealed that there are 2 EDR Hist Cleaner sites within approximately 0.125 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page NORTH CHARLOTTE LAUN 3306E N DAVIDSON ST NW 0 - 1/8 (0.105 mi.) A3 14 NORTH HIGHLANDER CEN 3220 N DAVIDSON WNW 0 - 1/8 (0.112 mi.) A5 17 TC5441860.2s EXECUTIVE SUMMARY 16 EXECUTIVE SUMMARY Due to poor or inadequate address information, the following sites were not mapped. Count: 3 records. Site Name Database(s) J C TEETER NC SWF/LF BP STATION #24175(FORMER PLAZA ROA NC LUST TRUST VIRGINIA MOORE TRUST NC LUST TRUST TC5441860.2s EXECUTIVE SUMMARY 17 OVERVIEW MAP - 5441860.2S Target Property o 1 a 112 t 1Miles Sites at elevations higher than or equal to the target property Indian Reservations BIA Upgradient Area ♦ Sites at elevations lower than ° ° Power transmission lines Hazardous Substance the target property 100-year flood zone Disposal Sites 1 Manufactured Gas Plants 500-year flood zone National Priority List Sites Dept. Defense Sites National Wetland Inventory State Wetlands This report includes Interactive Map Layers to display and/or hide map information. The legend includes only those icons for the default map view. SITE NAME: Forest Hill Church Parcels CLIENT: Geoscience Group ADDRESS: 729 E 36TH ST CONTACT: Ashley Proctor CHARLOTTE NC 28205 INQUIRY #: 5441860.2s LAT/LONG: 35.246331 / 80.802412 DATE: October 02, 2018 4:44 pm Copyright m 2018 EDR, Inc. (c) 2015 TornTom Rel. 2015. DETAIL MAP - 5441860.2S i r - 4 *_ 1610 �13 u> eel -=r e Cl I t ' ��lllo Ml�SON CHILD OEV[I OPMCtrT. TER ? _ �.� 16 JOHNSTON YMCA SCHO�U.t n('F I'RQf RAM MCHEALTHCENTERAI u? AN5f16N YMCA \ ' CM SUCCESS RV G e - N PRINCE & PRINC H� F- AV CASE 't MANS \ \ ad AHLANQ I NIT {Ip T MON& I i N Target Property A Sites at elevations higher than or equal to the target property ♦ Sites at elevations lower than the target property 1 Manufactured Gas Plants r Sensitive Receptors National Priority List Sites Dept. Defense Sites 0 1116 1/8 1/4Miles Indian Reservations BIA Hazardous Substance Power transmission lines Disposal Sites 100-year flood zone 500-year flood zone 17 National Wetland Inventory State Wetlands This report includes Interactive Map Layers to display and/or hide map information. The legend includes only those icons for the default map view. SITE NAME: Forest Hill Church Parcels CLIENT: Geoscience Group ADDRESS: 729 E 36TH ST CONTACT: Ashley Proctor CHARLOTTE NC 28205 INQUIRY #: 5441860.2s LAT/LONG: 35.246331 / 80.802412 DATE: October 02, 2018 4:47 pm Copyright m 2018 EDR, Inc. (c) 2015 TomTom Rel. 2015. APPENDIX V User Questionnaire Environmental Questionnaire Records Of Communication Laboratory Report USER QUESTIONNAIRE Forest Hal! Church Parceh Charlotte, North Catodfiaa ntiC end Si�tsture of son ,a of ne q/ie��6 -Dgte P'eease provide an anr4wr to each question to the best of your inawledge or artuch pertlncrat info rma#on and Mant{ry a nwnberfar each atrachmen t. (I.) Are you aware of any enviro"m=tat el eanug liens against the property that are filed ; or r`CM4M Lander federal, tribal, state or local law? No ❑ Yes (Describe or attach information) Attachment No. (2.) Are you aware of any Activity and Use Limitations (AULs), such as engineering controls (egg. engineered caps, faundations, liners, treatment methods, etc, in use to prevent contamination from migrating to swTounding arms), land use restrictiarns ar institutinnAl controls (e.g. administrative measures restricting grunndwatcr use, construction, or property use) that are in place at time site and/co- have been filed or rccordc d in a registry- under federal, tribal, state or local law? XNO ❑ Yes Pescn'l)t or attach information) Attachment No. (3.) Da yov have any sntcialmz d knorwIedge or experience related to the property or nearby Pr°1artie3? For cxauxple, are you involved in tht same line of business as the can=t or former occupants of the property or an adjoining property so that you would have speeiaiized knowledge of the chemicals and processes used by this type of business? No ❑ Yes (Describe or attach int'orrnation) Anse Mont No. USER QUESTIONNAIE (Continued) Fare Hill Chump Putcels Charlotte, North Carolina K) Does the purchase price being paid for this property reasonably reflect the fair market value of the property? ❑ No Yes (Describe or attach inf'ortnetion) Attachment No. if you conclude that there is a dif eMncc, Dave you considered whether the lower purchase price is pause cantarnivation is known or believed to be present at the property? No ❑ Yes (Describe or attach infaxruation) Attachment No. (S.) Arc you aware of commonly ImoAm or reasonably ascertainable infonnatlon about the property that would help the environmental professional to identify conditions indicative of releases or threatened releases? For exauVlc., a<5 User, (a.) Do you knaw the past uses of the property? o ❑ Yes (Describe or attach inforniati m) Attachriwa No. (b) Do you know of specific chemicals that are present or once were present at the property? )�No ❑ Yes (Describe or attach infortnation) Attachment No. (c) Do you snow of spills or other them icat releases that have taken place at the propertyl XNv ❑ Yes (Describe or attach information) Attat:btr = No, (d.) Do you know of any environmental cleanups that have takers place at the property? No ❑ Yes (Describe or attach inforrrtation) Attachment No. (5.) As the User of the ESA, based on your knowledge and eaperienca related to the property an there any obvious indicators that point to the presence or likely presence of enatamirtation at floe property? io ❑ Yes (Describe or attach information) Attachmmt No. GBOSCIENCE GAMP, INC. Eavlrorun wl Questionetaire (to be completed by current property owner) Forest Hill Church Parcels, Charlotte, North Carolina 1. la for pruputy Or anp 4OiWW Property used for an industrial use? YES If Yea, please explain: NO UNKNOWN 2, T'o tbt heat of your knowledge, bm the property or =Y Ad,l ❑mk4 PgPdy been used far an iadtisttial use in the pest? YES w 0 UNKNOWN If YrM, vitae explain, 3. lathe property or say adl oiuiag pmperty used as a gasoline station, motor repair fatality, commmial printing fmdity, dry cleancrs, Photo developing laboratory, hwkyurd or landfill, or as a waste treatment; storage, disposal, processing„or recycli% facility? YES If Yes, please explain: C!� UNKNOWN d. To the best of your knowledge has the property or adjeibing property been used as a gasoline astiop, motor relish fsc"'sty, ooF*.rn=cU printing facility, dr'y cleaners, pbcto devziopitag laboratory, bmkyard ❑r landfill, or as a waste treatment, sttxsge, dispos&I, praeming, or reeycring acnity? YES t No ulvxlca If Yes, please explain; S. Ate there currently, or to the best of yvua kmowlWgc have there been previously, MY damaged or discarded mtowotiva or industrial batteries, or pesticides, paint, or othcr chor6rab its individust 0=iners of g,eatax tl= 3 gallow (19L) in volume or 50 gallons (190L) in the a egate, stared on or used at the property or at the facili t YES NO UHIICMOWN IfYes, pleaseexplain:_ __�.._... b. Are there cunentiy, or to the beg of your knowledge have there berm previously, any iaduat W drums (typically 55' gallons (208L)) ar sacks of chcnicals located an the property or at the FaaiW YES QNp j rv—NMMM+— IfYes, ply 7. Has Ell dirt been bmught onto the property that originew from a cantmai =tad site or that is of an usnIMovM origm7 YES NO l�a� If Yea, Please explaia: 8. Are there currently, or to the best of yam knowledge have there been previously. my Aug, tom, or laeaW on the property m connection with waste treatment or waste disposal? r� YES If Yea. PWM Win - Page t of 3 GEOSC1ENCE GROVP, RVC Fnvimnmrntal Questionnaire (to be completed by current property owner) Forut Hill Church Parcels, Charlotle, North Carolma P. is there cusnmay, or to the lest of yow knowledge have there have been previo nn t#�e prvpdxtyri YES NO 13PiKNOWN If Yea, please explain. 10- l8 there currently, or to the best of your knowledge have there been previously, Any registered or unr &tMW maw t ka (above or ur! otnd) located on the pmpert}ri If Yes, 11_ Are there sw-rently, or to the best of your knowledge have there bem previously, any vent pipes, fill pipes, or Acoese ways indicating a fill pipe protruding from the gmuzid an the property or adjacent to any structure located on the prop-t]7 YES No UNKNOWN Yes, please 12, Are there cumatly, or to the best of your kmwledge have there been previously, any flooring, drains, ar walls located vviffin the facility that are stained by substances caw than water or am crnining foul odors? YES _ — NO _ UNKNOWN — Yes, please explain: 13_ If the property is served by a private wail Of non-public water system, have contaminants been identified its the well or system that exceed guidelines applicable to toe water t s`tem or bass the well been designated as canes by any gavcreunerit eavitoanjM UVheaith ageXy? YES C UNKNOWN If Yes, please explain: 14. Dm the owner or occupant of the property have any lawwledge of eavitonmenUl liens or governmental notifaeaaim relating to past or MWTMI violations of eatvironmenW laws with respect to the property or any facility located an thts YES If Yes, please explain: AM t 51. 15. Hoe the owner or occupant ofthe property been iufornsed of she past or current existence of hazardous substage or petroleum products m environmental violations with respect to tkac property or any facility located on the property? YES lvo UNKNOWN if Yes, please explain:_ __.._. 16. Does the owner or occupant of the property have any knowledge of.any environmental aite assessment of the property or fatality that ittdirated the pmsenee of hazardous substances or pelroletun paaducta nu, ar ContaMination of, the ptope ny or reeommendsd fttrtber asmeamEnt ofthe pr� YES NO UNKNOWN If Yes, please explain: Page 2 of 3 GBOSCIF.NCE CROVP, nvG Enviraamentm Qus3ti0f=ire (to be vomplaed by current property cover) Forest Hill Church Parcels, Charlotte, North Carolina 17.17oes the owner of occupant of the pxoparty kao w of any Past, threatened, or pending lawsviU or admis,istrati%'V PzmcOdiugs coixeraing a relegate or threatened r+el WC pf any baxardms stti+stence or pctrokeum praducta imrolvft the PropWy by any owner or Occupant of the pro y7 YES NO� UNKNOWN If yes, Ply rxplain: is. Does the property dischuge was to wa ter on ar f to the Property Ott= than sittmn vmW into a aenitkry Sewer. System? YES NO If Ycs, please explain — y� M1—�� �lA+fKNOWAI 4 19. To the beat of your knowledge, have any hazanious mbstanae- ar petrole= praducts, uftWentified waste Ro ials, tires, automotive Or industrial bancries or any other waste materWh been dumped above grade, buried andlar burned or the property? YES, If yea, please explain: UN"OWN 20. is there a ttansformm,, capacitor, or a¢iy hydraulic equipment for which there sae any record indicating flee pntscnw ofPC'E3s7 YES If Yes, please cvlain:`--- ---(7w- 21. To die best of your knowledge, are there n the subject property? YES ',` I +lp UNKNOWN If Yes, please explain:_ — _ %twine Of Person Completing Questo—a=: TAIL: Fn-m: Address: Oi f 1 t N x represent that to the of my knowledge the above stateatettts and {sets are true wed ec►Ftrct to the best of my actual 1 awTedgc na to 'a] fasts have been suppmmed or m1hstated. hoe Osu. Page 3 of 3 CHARLOTTE FIRE DEPARTMENT Battalion Chief Tim Hartsell 500 Dalton Ave. Charlotte, NC 28206 Phone — 704-336-2461 Fax — 704-336-4204 To: Ashley Proctor Re; 719 East 36" Street, Charlotte Project: Date: 03 October 2018 Fax. Sent Via Email X A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. There are no records of any CFD response to this address involving Petroleum or other hazardous substances. A search of our records has not turned up any responses for hazardous materials at or near the above address.. Please be advised that prior to annexation in the City of Charlotte there may have been a response by the VFD that provided protection. We do not maintain any of those records. The Mecklenburg County Fire Marshalls office may be contacted for additional information. Their number is 704-336-2154 In your FOI request your reference additional information pertaining to fire code violations, permits, and underground f above ground storage tanks, and remedial actions. Please fax that request to the Fire Prevention office at 704-336-5190. Parcel or Address is listed as residing in unincorporated Mecklenburg County or one of the other municipalities. VFI3 is presently the fire department that responds to this property. As such if they handled an emergency themselves without any assistance from Emergency Management or CFD Hazmat team, we would have no record of those responses. The Mecklenburg County Fire Marshal's Office may be Contacted for additional information. Their num ber is 7Q4 336-2 154 A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. The following records were found for this property I address involving petroleum or other hazardous substances, Information related to underground and aboveground storage tanks may be requested from INC Department of Environment and Natural Resources at 704-663-1699. Sincerely Tim Hartsell Battalion Chief, Charlotte Fire Department Hazardous Materials Coordinator, Charlotte Mecklenburg Emergency Management * The property researched is by address. If the street had a former designation, that is not searched unless the previous names are proved by the requestor. CHARLOTTE FIRE DEPARTMENT Battalion Chief Tim Hartsell 500 Dalton Ave. Charlotte, NC 28206 Phone — 704-336-2461 Fax — 704-331fi-4204 To: Ashley Proctor Re: 729 East 361h Street, Charlotte Project: Date: 03 October 2018 Fax: Sent Via Email x A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. There are no records of any CFD response to this address involving Petro leum or other hazardous substances. A search of our records has not turned up any responses for hazardous materials at or near the above address. Please be advised that prior to annexation in the City of Charlotte there may have been a response by the VFD that provided protection. We do not maintain any of those records. The Mecklenburg County Fire Marshalls office may be contacted for additional information. Their number is 704-336-2154 In your FOI request your reference additional information pertaining to fire code violations, permits, and underground I above ground storage tanks, and remedial actions. Please fax that request to the Fire Prevention office at 704-336-5196. Parcel or Address is listed as residing in unincorporated Mecklenburg County or one of the other municipalities. VFD is presently the fire department that responds to this property. As such if they handled an emergency themselves without any assistance from Emergency Management or CFD Hazmat team, we would have no record of those responses. The Mecklenburg County Fire Marshal's Office may be contacted for additional information. Their number is 704-336-2154 A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. The following records were found for this property 1 address involving petroleum or other hazardous substances, Information related to underground and above ground storage tanks may be requested from NC Department of Environment and Natural Resources at 704-663-1699. Sincerely Tim Hartsell Battalion Chief, Charlotte Fire Department Hazardous Materials Coordinator, Charlotte Mecklenburg Emergency Management * The property researched is by address. if the street had a former designation, that is not searched unless the previous names are proved by the requester. CHARLOTTE FIRE DEPARTMENT Battalion Chief Tim Hartsell 13ik 500 Dalton Ave, Charlotte, NC 28206 Phone — 704-336-2461 Fax — 704-336-4204 To; Ashley Proctor Re: 3315 North McDowell Street, Charlotte Project: Date: 03 October 2018 Fax: Sent Via Email X A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. There are no records of any CFD response to this address involving petroleum or other hazardous substances. A search of our records has not turned up any responses for hazardous materials at or near the above address. Please be advised that prior to annexation in the City of Charlotte there may have been a response by the VFD that provided protection. We do not maintain any of those records. The Mecklenburg County Fire Marshalls office may be contacted for additional information. Their number is 704-336-2154 In your FCI request your reference additional information pertaining to fire code violations, permits, and underground 1 above ground storage tanks, and remedial actions. Please fax that request to the Fire Prevention office at 704-336-5190. Parcel or Address is listed as residing in unincorporated Mecklenburg County or one of the other municipalities. VFD is preseritty the fire department that responds to this property. As such if they handled an emergency themselves without any assistance from Emergency Management or CFD Hazmat team, we would have no record of those responses. The Mecklenburg County Fire Marshal's Office may be contacted for additional information. Their number is 704-336-2154 A search of our records for spills or fires involving petroleum or hazardous materials has been conducted. The following records were found for this property J address involving petroleum or other hazardous substances, Information related to underground and above ground storage tanks may be requested from NC Department of Environment and Natural Resources at 704-663-1699, Sincerely Tim Hartsell Battalion Chief, Charlotte Fire Department Hazardous Materials Coordinator, Charlotte Mecklenburg Emergency Management * i lie property researched is by address. If the street had a former designation, that is not searched unless the previous names are proved by the requestor. Full -Service Analytical F /'PRISMI Environmental Solutions nA Geoscience Group Tam Hassett 500-K Clanton Rd. Charlotte, NC 28217 INC. Certification No. 402 NC Drinking Water Cart No. 37735 SC Certification No. 99012 Project: Forest Hill Church Parcels Lab Submittal Date: 1010512018 Prism Work Order: 8100119 Case Narrative t Oil 8/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody, Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please calf if you have any questions relating to this analytical report. Respectfully, PRISM LABORATQR.IES, INC. Angela D. Overcash VP Laboratory Services Reviewed By Angela D. Overcesh VP Laboratory Services Data Qualifiers Key Reference: RLM Sample container suspected to have low methanol content. Results possibly biased high. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a T This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 20224-0543 Phone: 704)529-U64 -Tull Free Number: I41DW529.5364 - Fax: 700525-0409 page i of $ ZR-I S n A ErivIr nrvice Analytical s e ' V' Envl�anmentni Solutions Sample Receipt Summary 10/1812018 Prism Work Order: 8100119 Client Sample ID Lab Sample ID Matrix Daterrime Sampled DatefTime Received HA-1 6100119-01 Sand 10105/18 0.00 10/05/18 15:05 HA-2 8100119-02 Solid 10/05118 0:00 10/05/18 15:05 Samples were received In good condition at 4.1 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the wri}ten consent of Prism Laborstorles, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-DS43 Phone: 704f529-6364 - Toll Free Number: 1-0001529.6364 - Fax: 7WS25.0409 Page 2 of 8 Full- .`P,AR I S M n envir " ice Anatyutio s [V' E�vEranm�rrtsl Solutions LI5wwomwsS, C: Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Forest Hilt Church Parcels Sample Matrix: Solid Laboratory Report 1011812018 Client Sample ID: HA-1 Prism Sample ID: 8100119-01 Prism Work Order: 8100119 Time Collected: 10105118 0a:00 Time Submitted: 1010&18 15:05 Parameter Result Units Report MIL Dilution Method Analysis Analyst Batch Limit Factor datefrime II] Diesel Range Organics by GCIFID diesel Range Organics BRL mglkg dry 9.9 2.6 1 Surrogate •8015c 10/11/18 16:36 ZRC PSJ0194 Recovery Control Limits o-Terphenyl 84 % 31-123 Gasoline Range Organics by GCIFID RLM Gasoilne Range Organics BRL molt dry 7.5 1,6 50 18015C 1018N8 19:38 ANCW PeJ0103 Surrogate Recovery Control Limits s.a.a-Trifluorotoluone 148 % 50.137 SR General Chemistry Parameters %solids 70.3 %by 0,100 0.100 1 'SM2540 G 1W16M8 16:40 TJY P&J0305 Weight This report should not be reproduced, except in its entirety, without the written consent at Prism Lahoratories. Inc. 449 Springbrook Road - P.O. Box 240543 . Charlotrs, NC 28224-0543 Phone. 7WS29.6364-Toll Free Number:l-600;5x9-6364- Fax: 704152"4" Page 4 of 8 I FvliSer ice Annlylicel 8. En�lronmenf�l Boiuti�ns '-: �AKIRwTw�ame Summary of Detections 1011 B!2018 Prism Work Order: 8100119 PHam ID Client ID Parameter Method Result Lirits There were no detections reported. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643 Phone: 7641529-6364 - Toll free Number: 9-8901529-6354 -Fax, 7041525-0409 Page 3 of 8 /ri®r-i!Service Anaiyt tl %; EnYironmantal Sulutlona l•BDRATORIES 'NV Geoscienoe Group Attn: Tom Hassett 500.K Clanton Rd. Charlotte, NC 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Laboratory Report 10AW018 Client Sample I❑: HA-2 Prism Sample I❑: 8100119-02 Prism Work finder: 8100119 Time Collected: 10105/18 00:00 Time Submitted: 10/05/18 15.06 Parameter Result Units Report VIAL Dilution Method Analysis Analyst Batch Limit Factor ❑ate/Time I Diesel Range Organics by GC1FID Diesel Range Organics 13RL mglkg dry 9.9 2.6 1 'S0i5C 10111/18 17;1a ZRC P8J0194 Surrogate Recovery Control Limits o-Terphenyl St) 96 31-129 Gasoline Range Organics by GC/FlD Gasoline Range Organics 6RL mglkg dry 9.9 2.1 50 *8015C 1018f18 20;O6 ANWJ PSJ0103 Surrogate Recovery Control Limb a.a,a-Trikurotoluen e General Chemistry Parameters 134 % 50-137 % Sol Ids 70.6 %by 0.100 0.100 1 '5012540G 10119/18 16;40 TJY Pt1J0305 weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "0 Sprsngbrook Road , P.O. Box 240543 - Chariotte, NC 2822"U3 Phone: 7041529$364 -Toll Free Number. 1-8001529.6364 • Fax; 70415254409 Page 5 of 8 L"P.,pLq Full -Service Analylleal Environmental Solutions Geoscience Group Project: Forest Hill Church Parcels Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Gasoline Range Organics by GC*lD - quality Control Level II QC Report 10/18118 Prism Work Order: 8100119 Time Submitted: 1015I2018 3:05:00PM Reporting Spike Source %REG RPD Ana lyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PBJ0103 - 6035 Blank lPBJ0103-BLK1y Prepared & Analyzed: 10/08118 Gasoline Range Organics BRL 5.0 mglkg wet Surrogate' a, a, a -Tiff uornVuene 5.20 rrlglkg 5.000 104 50-137 LCS (PBJ010343S1) Prepared & Analyzed: 10108118 Gasoline Range Organics 59.7 5.0 mglkg wet 50.00 119 41-138 Surrogafe.' e,a,a-Trffuorofaluene 5.65 mg/kg 5.000 113 50-137 LCS Dup (158J0103-113SOI) Prepared & Analyzed: 10/08118 Gasoline Range Organics 64.8 6-0 mg/kg wet 50,00 130 41-139 a 20 Surrogate: a,a,a-TriRuorotoiuerre 5.45 mg/kg 5.000 109 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratodes, Irr. 449 Springbraok Road - P.Q. Box 240543 - Cha►latte, NC 28224-0543 Phone, 704f$29-6364 -Toll Free Number: 1-0401529-5364 - t=ax: 70415254MO9 Page 6 of 8 P LgF I q M I FUIP-SeryiGe Analytical & Envirenmpnral Solutions L�eES �Nc Geoscience Group Project: Forest Hill Church Parcels Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Diesel Range Organics by GCIFiD - Quality Control Level fl QC Report 10116/18 Prism Work Order: 8100119 Time Submitted: 10f512018 3:05;04PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P830194 - 3546 Blank (PU0194-BLK1) Prepared & Analyzed: 10111/18 ❑iesel Range Organics BRL 7.0 mglkg wet Svrrogafe: a-Terphenyl 7.p7 mg*g wet 1.332 81 31-123 LCS (138J0194-13S'I) _ Prepared & Analyzed:_ 1_0111118 Diesel Range Drganics 51A 7.0 mglkg wet 66.64 77 46-126 Sun-ople: o-Tsrphenyf 1.18 mglkg wet 1.333 89 31-123 LCS Dup (PaJ0194-BS01) Prepared & Analyzed. 1011 ill Diesel Range Organics 54.0 7A mg/kg wet 66.67 81 46.126 5 20 Surrogate:-7"mphenyl 1.16 rnglkg wet 1.333 87 31-121 Sample Extraction data Prep Method- 3348 Lab Number Batch Initlal Final DateMme 8100119-01 PRJ0194 30.1 g 1 mL 10J11J18 8:42 6100119-02 PBJ0194 30.07 g 1 mL 10111J18 8:42 Prep Method: 5035 L.ab Number Batch Initial Final Dekslilme 6100119-01 PBJO103 4.77 g 5 mL ioiw18 12:03 8100119-02 P8J0103 3.58 g 5 mL 1p108f18 12:03 Prep Method: Solids, Dry Weight Lab Humber Batch initial Final Dateirime 9100119-01 P8d0305 30 g 30 g 1(VI 8118 16:40 8100119-02 P8J0305 30 g 30 g 10116118 16:40 This report should not be reproduced, except in its enlirety, wlthout the written consent of Prism Laboratories, Inc. 449 Sprh►gbrook Road - P.U. Box 2405t3 - Charlotte, NC 28224-0543 Phone: 704J528-fs36d -Toll Free Number: 1-SM529.6364 - Fax: 7WS29-0409 Page 7 of 8 6 ^3 L7 Z G m m o C C U1 f H 0 co p 3 "r if1 m n e a y 0 O O-4— [n x C x 8 n r m 0 0 `[ b' °: ?; m a cn ui [] p ,c C t rri 7 7 N f fcn ❑ C ai 7 ti1 r 20 3 m -n .� ❑ n r � +1 D �' dl � a rn� w a ra T� om in m �C v no do 5' m ❑ rn �m 0 zv o •• mU m G M. am m NAM C Q} A p C min 75 y a f �r l r m m prr 1 a n� moot r~u o b X? e mw 8 T � 9 �' T M -- -•-- -- aF mm� k a rn m b M 3 a my P Q ❑ or mm H yw �m CL � m �;n m u7°,lb C O v H LL w m ?7� m �OO" m:q 0 D W y m z and x a w D cr m m S --i rn a rt'a rt�� N ❑ ❑ dz ❑� P t➢�� 3ry u� ■ yS tlF❑ 7. z � 4 m np o� d nag C m 0 7❑ Q y n� to m fn rn ❑ � � m �n n ci m � C O r m Z rn a mlic ic O A -A m Z D n a3 m W m A a P � 0 0PL jt � n , �A •a a ♦L b (Y N 0 n O cn ty d n O r'` n j G G C 7 = m r� x nos 3 m u AS D to R� tl w N S><+ Q 10 211 >rLL I o � A d n v � �• oC a is 0 c g G it fr yC C c �p m n .. M r L ;6 N Z � Cv a z m m f -�man -4 o a , p m •a a z M" 0 cl 0 O v M 402 se Narrative INC CBrti Drinking iOn Water ert ■ � :. Full -Service Analytical � INCNC ❑risking Water Cert Iva. 37735 � p12412p1 g Environmental Solutions SC GertiTrcatlon No. 99012 L a9MATOnIM INC. Geoscience Group Project: Forest Hill Church Parcels Tom Hessen 500-K Clanton Rd. Late Submittal Date. 10/12/2018 Charlotte, NC 28217 Prism Work Order: 8100259 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully. PRISM LABORATORIES, INC. Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference Reviewed By Robbi A, Jones For Angela D. Overcash President/Project Manager DO Surrogates diluted out. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not he reproduced, except in its entirety, without the written eonsent of Prism Laboratories, Inc. 449 5pringbrook Road - P.a. ISox 240543 - Chatlotte. NC 28224.0543 Phone: 704l529.6364 - Toll Free Number: 1-6001529-6364 - Fax: 7041523.0409 Page 1 of $ PRISM I Full Service al Golubo a Sample Receipt Summary Enviranm®oral Solutions 1012412018 LA6pgA;nRCa LNG Prism Work Order; 8100289 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received HA-3 8100259-01 Solid 10/12118 10:08 10/12/18 13:30 HA-4 8100259-02 Solid 10112J18 11:45 10/12/18 13:30 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road . P.O. Box 240543 - Charlotte, INC 26224-6543 Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 -Fax: 7U/625-0409 Page 2 of i3 4 Full -Service AnaEytical& ISM I Envrranmental Solutlons LAB�P�TGRILR IMr, Summary of Detections 1012412018 Prism Work Order: 8100259 Prism ID Client I❑ Parameter Method Result Units 8100259-01 HA-3 Diesel Range Organics '8i315G 26000 Mg/kg dry 81002$9-01 HA-3 Gasoline Range Organics '9Et1SC 2300 mglkg dry 8100259-02 HAA Diesel Range Organics '8015C 3500 mglkg dry 8100259-02 HA-4 Gasoline Range Organics 18aisc 99 mglkg dry This report should not be reproduced, except in its entirety, without the written consent otPrism Laboratories, Inc. 4449 8pringbrook Read - P.O. Box 240543 . Charlotte, NC 28224d1S43 Phone: 7041529.6364 - Toil Free Number: f-soW529-6364 - Fax: 704Ai2S-Wl1 Page 3 of 8 I S n � I Full-Serorce Analytical a V' I Environmental Solutions �Rn,aAcs �� Geoscience Group Attn: Tom Hassett 50D-K Clanton Rd. Charlotte, NO 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Laboratory Report 10124/2010 Client Sample ID: HA-3 Prism Sample ID: 8100259-01 Prism Work Order: 8100259 rme Collected: 10/12/18 10-08 Time Submitted: 10112I18 13:30 Parameter Result Units Report MOL Dilution Method Analysls Analyst Balch Limit Factor Dat"Mme ID Diesel Range Organics by GCIFID Diesel Range Organics 26000 rngfhg dry 1900 500 200 18615C 10M7118 9:08 IRC P8J0283 Surrogate R--ery Cdhtrol Limits o-Terphenyl 0 % 31-123 OQ Gasoline Range Organlcs by GCIFID Gasoline Range Organics 2300 m9/kg dry 93 20 Sao "8015C 10119118 9:33 ANGIJ PBJ0333 Surrogate a, a,a-Triflu orotalV en e Retavery Contrd Limits 110 % 50-137 General Chemistry Parameters % Solids 73.9 'Y by 0.100 0.100 1 `SM2S40 G 10122I18 1410 TJY P810417 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism LabDfatones, Inc_ 449 Springhroott Road - P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 7041529-5354 -Tall Free (dumber: 1-8001529-6354- Fay: 70d1525-"09 Page 4 0f 8 Laboratory Report �FR ISM I E, vir amen analytical 8 ! Environmental 801ufign3 10r2412018 '%` .AHWTpMl" iaq Geoscienee Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Forest Hill Church Parcels Sample Matrix: Solid Client Sample ID: HA-4 Prism Sample ID: 8100259-02 Prism Work Order: 8100259 Time Cotlected: 10/12/18 11:45 Time Submitted: 1011211813:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTme Ill Diesel Range Organics by GCIFID Diesel Flange Organics 3500 mglkg dry 490 18$ 50 *$015G 10MVi8 7:50 ZRC PSJ0283 Surrogate Recovery Control Limits o-Terphenyl 0 % 3f-723 00 Gasoline Range Organics by GC1FID Gasoline Range Organics 99 myfky dry 7.9 1.7 So "8olsc 10119118 511 ANGM P$J0333 Surrogate Recovery Control Limits a,a.a-Trifluorotaluene 118 % 5D-137 General Chemistry Parameters %Solids 71.0 %by 0.100 0.100 1 '3M2540G 1012211814:30 TJY PSJ0417 Weight This report should not be reproduced, except in ita entirety, without the written consent of Prtsrn Laboratories, Inc. 449 Springbrook Road • P.O. Bum 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 • Toil Free plumber: 1$001529-4384 - Fax: 7041525-MO Page 5 of 8 �R I S h ,♦� Full -Service Analytical I V I � Environmental Sofu[fans its- h& Geosoience Group Project: Forest Hill Church Parcels Attu: Torn Hassett 500-K Clanton Rd. Charlotte. NC 28217 Gasoline Range Organics by GGlFID -{duality Control Level li QC Report 10124l18 Prism Work Order: 8100259 Time Submitted: 10/12/2018 1:30:OOPM Reporting Spike Source %REC RPD Analyse Result Urnk Units Level Result %REC Limits RP❑ Limit Notes Batch MOM - 5035 Blank (P8J0333-BLK1) Prepared BAnaWed: iOil all 8 Gasoline Range Organics RRL 5.0 rnglkg wet Surr*g'?fe: a,a,a-7nfl(forW010ene 5.05 mg*9 5.00U 101 50-137 LCS (P8J0333-051) Prepared & Analyzed: 10118/18 _ Gasoline Range organics 55.4 5.0 mglkg wet 50.00 111 41-138 Surrogate: a,a,a-Tnfiuorat0iuene 4.90 mglkg 5.000 98 50-137 l_CS Dup IMID333-MI) Prepared & Analyzed: i0/18/18 Gasoline Range Organics 81A 5.0 Mog wet 50.00 122 41-139 10 20 Surrogate: a,a,a-Trtluarotoluene &00 mglkg 5.000 100 50-137 This report should not be reproduced. except in Its entirety, without the written consent of prism Laboratories. Inc,. 448 Springhrook Rnad - P.O. Box 24OS43 - Charlotte, INC 28224.0543 Phone: 7041529-6364 - Tall Free Humber: 1.8001529-6364 - fax: 704(525-0409 Page 6of8 +� R I S i Fuu-Service AnafS'xical 8 Enviranmenx>Ri SaEu[fona ORA70o OL ING Geoscdence Group Project; Forest Hill Church Parcels Attn: Tam Hassett 5OD-K Clanton Rd. Charlotte, NC 28217 Diesel Range organics by GCIFID - Quality Control Level II QC Report 10124118 Prism Work Order: 8100259 Time Submitted: 10/12/2018 1:30:OOPM Reporting Spike Source %REC RPO Anaiyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PBJ0283 - 3546 Blank (PSJ0283-BLK1 ) Prepared a& Analyzed: 1 D116118 Dlesel Range Organics BRL 7.0 mglkg wet Surrogate: o-Terphenyl 0.929 mg/kg wet 1,333 70 31.12.3 LIDS (P8J0283-1351) _ Prepared & Analyzed: 1011-6118 Diesel Range Organics 59.1 7.0 mglkg wet 66.67 69 46.126 Surrogate: u-Terphenyl 1.24 mgft wet 1.333 93 39-123 LCS oup (P8J0253-BSDI) Prepared &Anatyze_d: 10116118 Diesel Range Organics 55.8 7.o mglkg wet 66.67 84 46-126 6 20 Surrogate. o-Terphenyl 1.08 mglkg wet 1.333 81 31-123 Sample Extraction Data Prop Method: 3546 Lab Number Batch Inkial Final Daterrinn 8100259-01 PBJ0283 30.1 g 1 mL 10118118 11:35 8100259-02 PBJ0283 30A2 g 1 mL 10116118 11:35 Prep Method: 5035 Lab Number Batch Initial Final DatalTime 81 OD259-01 POJ0333 3.62 g 5 mL 1 WI8118 10:64 81D0259-02 P8J0333 4.46 g 5 mL 10/18118 11154 Prep Method: Sands, Dry V"ht Lab Number Batch inlitlal Final Datefllme 8100269.01 P8J0417 30 g 30 9 1W2118 14:30 811DO259-02 P8J0417 30 g 30 g 10122118 14:30 This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2a224.0543 Phone: 704I529-6364 -Toll Free Number. 1.8001529.6364 - Fax: 704/525-04H Page 7 of 8 A O x a x m v m C} 10 m n ❑ is u�(nmmI C a ❑ R $ ` rrnn m w 'o Aa p n= N Qr m G Q❑cam ��cn 7 v n� _ Q E i 'b x m " CS��3 m A = ❑ z G g ry m� a a' Wrn H w _ sass Cz 3L m At r r Q 3 O C m m .qS C7 s c 0) q9 7 O m • 2. ICrr m i i .m a m�r ?! LO co { L zo a m [n - t3r# m r � w ❑ x r r � y" x C •i fA y {Jy i ti. 7 pma Gy ^a r F C Cl s e1 m 71 1 a mQ 3i 1mh m ro YI mra� w 7 W �O z Lii m r-mil m�?in G 7a r tR a N minR77� ❑ 31 pi a Oda O � m m R S m'° 2 o o xam, Ou Q ❑ P ,. ti m m g r 0 W �° p0 ;D m G m ❑ ❑ 70 Sri r� n m °Nm n' rn a m .2 ao N 0 wee P 75 N R M.0 :3cl0 ro� N �m Cm m mn ] to oma n zm Ig rAc ��,, a ��m@ ❑ ❑� o Cm ea a7 x 4�7 p m � c 1 m _ q 'C .4 {r a < 7Z' LA O m p 0 -,m 3 p ❑ 1 ��', li 1 CA O I om w Cyr m m r�A m C Q tr` Q 7 > a y m w � H i] rm [ 3 n D 0 m Vl M A M y 3 rn I r a o a x r C] 2_ r� fp m m 7 O m o r n m a pin n en ? n f r co n�� ye q at i � O � 4 T lu 9 .d a 4 m a m w in o mm n a O � in in A a a0�i m A � � 4 m m� APPENDIX VI Qualifications of Environmental Professionals Consulting Engineea•s Ashley N. Proctor Assistant Project Manager - Charlotte, NC SPECIAL QUALIFICATIONS & EXPERIENCE RELATED TO THIS ASSIGNMENT Recent entry into the field of environmental assessments after completing Bachelor of Arts GEQSCIENCE Degree at Winthrop University. Training in basic principles of ArcGIS. Hands on experience GROUP and continuing education in environmental investigations. EDUCATION Bachelor of Arts in Environmental Studies Minor in Social Sciences Winthrop University, 2012 - 2016 SHORT COURSES Phase I and I1 Environmental Site Assessments for Commercial Real Estate ASTM - Practice E 1527-13 EXPERIENCE 2017 - Present: Assistant Project Manager Geoscience Group - Charlotte NC Perform onsite inspections and investigations, conduct field testing of soils and water, and prepare Phase I Environmental Site Assessment reports. Consulting Engineers Thomas C. Hassett, P.E. Senior Engineer - Charlotte, NC SPECIAL QUALIFICATIONS & EXPERIENCE RELATED TO THIS ASSIGNMENT Over twenty (20) years experience in a wide variety of environmental, geotechnical, and GEPSCIENCE construction materials engineering projects. Special training and experience in environmental GROUT' investigations and construction material evaluations. EDUCATION BS Studies in Mechanical Engineering McGill university, 1987 --1991 Webb Institute Of Naval Architecture, 1985 - 1986 EXPERIENCE 2014 - Present: Senior Engineer Geoscience Group - Charlotte, NC Manage site investigations, perform onsite inspections, and prepare reports for commercial and industrial. clients, Work includes environmental investigations, segmental block retaining wail design and materials testing. 20082014: Project Engineer Geoscience Group - Charlotte, NC Performed onsite inspections, managed site investigations and prepared reports for commercial and industrial clients. Work included environmental investigations, segmental block retaiztii-ig wall design, and materials testing. 1997-2008: Project Manager Geoscience Group - Charlotte, NC Conducted and directed environmental assessments, remediation projects and prepared construction materials testing reports. Short Courses Environmental Site Assessment Practices for Commercial Real Estate A5TM - Practice E 1527-13 Evaluation Of Indoor Inhalation Pathway National Environmental Health Association National Radon Proficiency Program Residential Radon Measurement 1495-1997: Laboratory Manager Geoscience Group - Charlotte, NC Conducted laboratory tests and field inspections for the selection and utilization of construction materials. 1993-1995; Engineering Technician Geoscience Group -Charlotte, NC Conducted field testing of soils, stone, concrete, asphalt, fasteners, and steel for a variety of construction projects. 1989: Laboratory Assistant Array Carps Of Engineers - Hanover, NH Evaluated simulated sea ices used for scale model testing of ship hulls. PROFESSIONAL ENGINEERING REGISTRATIONS North Carolina PROFESSIONAL CERTIFICATIONS National Environmental Health Association - Residential Radon Measurement Provider Brownfields Property Application North Carolina Brownfields Program www. n cbrownf iel d s. o ra I. PROSPECTIVE DEVELOPER (PD) INFORMATION {USE TAB KEY TO GET TO NEXT DATA ENTRY LINE — DO NOT USE THE RETURN KEY} A. PD information: Entity name Forest Hill Church Principal Officer Tom Emmrich Representative Nick Dusenbury Mailing Address 7224 Park Road Charlotte, North Carolina 28210 E-mail address nick.dusenbury@foresthill.org Phone No. 704-71 b-8700 Fax No. NIA Web site www.foresthill.org B. PD contact, person information (i.e., individual who will serve as the NQP's point of contact if different than above): Name Amy Rickers Company Johnston, Allison & Hord, P.A. Mailing Address 1065 East Morehead Street Charlotte, North Carolina 28204 E-Mail Address arickers@jahlaw_com Phone No. 704-998-2253 Fax No. 704-323-4653 C. Information reaardina all parent companies,. subsidiaries or other affiliates of i'D !attach swarate sheets) if necessary),: (Use for LLCs) Member -managed or manager -managed? Answer: NIA Cl If manager -managed, provide name of manager and percent of ownership: Name Ownership (%) Mailing Address E-Mail Address Phone No, Fax No. For all LLCs, list all members of the LLC and provide their percent of ownership: Name Ownership Mailing Address E-Mail Address Phone No. Fax No. Name Ownership (%) Mailing Address E-Mail Address Phone No. Fax No. Name Ownership Mailing Address E-Mail Address Phone No. Fax No. E Managers of manager -managed LLCs are required to execute all brownfield documents for the LLC; as to member -managed LLCs, state name of member who will sign these documents. List all parent companies, subsidiaries and other affiliates: (Use for Partnerships) N/A Check one: ❑General Partnership ❑Limited Partnership List all partners and percent of ownership: Name Ownership Mailing Address E-Mail Address Phone No. Fax No. Is this person a general or limited partner? Name Ownership {°/o} Mailing Address E-Mail Address Phone No. Fax No. Is this person a general or limited partner? List all parent companies, subsidiaries and other affiliates: C (Use for corporations other than LLCs) (If information is the same as shown in 1.A., please indicate "same as 1.A."below.) Name same as I.A. above Mailing Address E-Mail Address Phone No. Fax No. List all parent companies, subsidiaries and other affiliates: Seeds of Hope, Inc. (Use for individuals) (if individual is the same as shown in 1.A., please indicate "same as ?.A."above.) Name NIA Mailing Address E-Mail Address Phone No. Fax No. D. Does PD have or can it obtain the financial means to fully implement a brownfields agreement and assure the safe reuse of the property? (Attach supporting documentation such as letters of credit, financial statements, etc.) Answer Yes Explanation PD is a going concern with the ability and intention to utilize and develop the property to its safe and full reuse. Independent Auditor Financial Statements for year-end 2016, 2017, and 2018 are submitted with this application. E. Does PD have or can it obtain the managerial means to fully implement a brownfields agreement and assure the safe use of the property? Answer Yes Explanation The corporate structure of the organization provides the leadership to oversee the process of implementation of the Brownfields Agreement. Forest Hill Church will also work with its environmental consultant and counsel to ensure compliance and implementation of the Brownfields Agreement 7 F. Does PD have or can it obtain the technical means to fully implement a brownfields agreement and assure the safe use of the property? Answer Yes Explanation Forest Hill Church will work with its environmental consultant and its environmental counsel to ensure the Agreement is fully and properly imolemented. G. Does PD commit that it will comply (and has complied, if PD has had a prior project in the NCBP) with all applicable procedural requirements of the NCBP, including prompt payment of all statutorily required fees? Answer yes (List all NCBP project name(s) and NCBP project 1D numbers where PD or any parent company, subsidiary and other affiliate of PD has been a party to.) NIA H. Does PD currently own the property? Answer No If yes, when did PD purchase the property and from whom? (Provide name, address, telephone number and email address of the contact person for the current property owner. ) NIA If no, provide the name, address, telephone number and e-mail address of the contact person for the current property owner Johnston Memorial Presbyterian Church ffkla North Carolina Presbyterian Church c/o Molly Griffin, 1010 Vickery Drive, Charlotte, North Carolina 28215 I. If PD does not currently own the property, does PD have the property under contract to purchase? Answer Yes If yes, provide date of contract. July 31, 2018 If no, when does the PD intend to purchase the property (e.g., after the project is determined to be eligible for participation in the NCBP, after PD receives a draft BFA, after the conclusion of the brownfields process)? NIA 0 J. Describe all activities that have taken place on the property since PD or PUs parents, subsidiaries and/or other affiliates, and/or lessees or sublessees of PD, took ownership of or operated at the property (e.g., industrial, manufacturing or commercial activities, etc.). (Include a list of all regulated substances as defined at NCGS § 130A-310.31(b)(11) that have been used, stored on, or otherwise present at the property while those activities were conducted, and explain how they were used.) Forest Hill Church has been leasing the property since August 1, 2018 and has been operating on the property as a religious organization holding meetings and worship services. II. SITE INFORMATION A. Information reaardinq the proposed brownfields Property: Proposed project name 3315 McDowell Street acreage 1.887 acres County Mecklenburg street address(es) 729 East 36th Street and 3315 North McDowell Street City Charlotte zip 28205 tax ID(s) or PIN(s) 9110401 and 9110402 Past uses) Church related purposes since at least 1929 with some singly -family use, current use(s) The property is used for Church related purposes. causes)/source(s) of contamination: known Two on -site USTs used to store heating oil. One of which has been determined to have leaked suspected None B. Regulatory Agency Involvement: List the site names and all identifying numbers (ID No.) previously or currently assigned by any federal, state or local environmental regulatory agencies for the property. The ID No's may include CERCLIS numbers, RCRA generator numbers for past and present operations, UST database, Division of Water Quality's incident management database, and/or Inactive Hazardous Sites Branch inventory numbers. (In many instances, the PD will need to actively seek out this information by reading environmental site assessment reports, reviewing government files, contacting government officials, and through the use of government databases, many of which may be available over the internet.) Agency Name/lD No: NIA Agency Name/l❑ No: Agency Name/ID No: Agency Name/10 No: 0 Agency Name/l❑ No: Agency NamellD No: C. In what way(s) is the property is abandoned, idled, or underused? Property is currently used for church purposes but PD intends to expand its use into a thriving church and related use property- D. In what way(s) is the actual or possible contamination at the property a hindrance to develo ment or redevelo ment of the property (attach any supporting documentation such as letters from lending Institutions)? As a potential purchaser of the property and a nonprofit corporation, it is important that PD have any environmental issues addressed prior to possession. Without the protection afforded by the Brownfield program, the PD is unable to risk environmental liabilities associated with lingering contamination that could risk funding needed for its primary purposes. E. In what way(s) is the redevelopment of the property difficult or impossible without a brownfields agreement (attach any su000rtina documentation such as letters form lending institutions)? The possibility of environmental liability for this non-profit organization is not acceptable and the Brownfield Agreement and liability protection will resolve this issue for the PD. F. What are the planned uses of the redevelo ed brownfields property to which the PD will commit? Be as specific as specific as possible. Forest Hill intends to develop and expand the church related use of the property. G. Current tax value of brownfields property: $1,788,400.00 H. Estimated capital investment in redevelopment project: $ Approximately $4 million. I. List and describe the public benefits that will result from the property's redevelopment. Be as specific as possible. (Examples of public benefits for brownhelds projects include job creation, fax base increases, revitalization of blighted areas, preserved green space, preserved historic places, improving disadvantaged neighborhood quality -of -fife related retail shopping opportunities, affordable housing, environmental cleanup activities or set asides that have community or environmental benefits. In gauging public benefit, NGBP places great value upon fetters of support from community groups and local government that describe anticipated improvements in quality of life for neighboring communities that the project will bring about. The inclusion of such support letters with this apnlicatiorl is recommended and encouraged.) This project will update and enhance the area by providing a thriving place of worship into a developing area. The improvements to the property will further increase the tax value of the property as well. Special Note: Please describe all environment -friendly technologies and designs PD plans to utilize in its redevelopment strategy. For example, environment friendly redevelopment plans could include: Leadership in Energy and Environmental Design (LEED) Certification, green building materials; green landscaping techniques such as using drought resistant plants; energy efficient designs, materials, appliances, machinery, etc.; renewable sources of energy, and/or recycling/reuse of old building materials such as brick or wood. 10 J. Who will own the brownfields property when the Notice of Brownfields Property is filed with the register of deeds at the conclusion of the brown„fields process? (If information is the same as I.A. above, please indicate.) Name likely same as l .A above or if closing has not occurred will be with owner listed in I .H. Mailing Address E-Mail Address Phone No. Fax No. Ili. OTHER REQUIRED INFORMATION A. Brownfields Affidavit: PD must provide its certification, in the form of a signed and notarized original of the unmodified model brownfields affidavit provided by NCSP, that it did not cause or contribute to contamination at the property and that it meets all other statutory eligibility requirements. (Note: The form to use for this affidavit is attached to this application. An original hard copy of this affidavit must be filled out, signed, notarized and submitted with this application.) Is the required affidavit as described above included with this application Answer Yes B. Proposed Brownfields Agreement Form: PD must provide the completed form Proposed Brownfields Agreement. (Note: The form to use for this document is attached to this application. It must be filled out, initialed, and attached on your submittal.) Is the reciuired Proposed Brownfields Acireement, as described above included with this application? Answer Yes C. Location May: P❑ must provide a copy of the relevant portion of the 1:24,000 scale LI.S.G.S. topographic quadrangle may that shows the location of the property, clearly plotted, and that measures at least an 8 Y2 by 11 inches. (Note: these maps can be purchased through the above link, or often through retail outdoor recreation stores that can print out the relevant map. Often environmental reports have location maps that use this type of map format as the base for its location map.) Is the required location map included with this application? Answer Yes 11 D. Survey Plat: P❑ must provide a preliminary survey plat of the brownfields property with the property boundaries clearly identified, and a metes and bounds legal description that matches the property description on the plat. At this stage of the brownfields process, one or more existing survey plats from a previous property conveyance will suffice. (Before the brownfields project enters the public comment phase of the brownfields process, the PD will be required to submit a final brownfields survey plat which includes the information fisted in the brownfields survey plat guidance.) Is the recluired meliminary survey plat included with this application? Answer Yes E. Site Photoaraohs: PD must provide at least one pre -redevelopment photograph of the property, in either hard copy or electronic format, that shows existing facilities and structures. Please note that the NCBP prefers to have electronic photos instead of or in addition to hard copies. Electronic copies of photographs should be emailed to: Shirlev.Liooinsftedenr.gov with a clear indication as to which Brownfields Application they apply to. Are photographs of the orop_erty included with this application? Answer Yes Have electronic ca ies of the ohotograiphs been emailed to NCBP? Answer Yes F. Environmental Reports/Data: If it makes an affirmative eligibility determination, the NCBP will request that P❑ provide any and all existing environmental reports and data for the property on CD only. The brownfields process may be expedited if PD submits such reports/data with this application. Are any environmental reports/data being submitted with this application? Answer yes If environmental reports/data are being submitted with this application, please provide the title, date and author of each item being submitted: Phase I Environmental Site Assessment Forest Hill Church Parcels Charlotte, North Carolina Geoscience Project No. CH M0129.GE December 13, 2018 Geoscience Group IV. ADDITIONAL REQUIRED FORMS The following forms are to be filled out and submitted with the application including the Responsibility and Compliance Affidavit and the Proposed Brownfields Agreement. Submittal of the Affidavit requires signature and notarization, and the Proposed Brownfields Application requires an initial. 12 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY NORTH CAROLINA HROWNFIELDS PROGRAM IN THE 'MATTER OF: Forest Hill Church UNDER THE AUTHORITY OF ) AFFIDAVIT NORTH CAROLINA GENERAL } RE: RESPONSIBILITY STATUTES ❑ 130A-310.30, et. seq. ) AND COMPLIANCE Nick Dusenbury , being duly sworn, hereby deposes and says: 1. I am Representative of Forest Hill Church 2. [if signatory is not President, add this paragraph: "I am fully authorized to make the declarations contained herein and to legally bind Forest )-lill C`hnrch .9 3. Forest Hill Church is applying for a Brownfields Agreement with the North Carolina Department of Environmental Quality, pursuant to N.C.G.S. 0 130A, Article 9, Part 5 (Brownfields Act), in relation to the following 09110401 and 091 10402 parcel(s) in Charlotte _Mecklenburg , County, North Carolina: 729 East 36(h Street _ 3315 North McDowell Street 4. I hereby certify, under the pains and penalties of perjury and of the Brownfields Act, that Forest Hill Church , and any parent, subsidiary or other affiliate meets the eligibility requirements of N.C.G.S. ❑ 130A-310.31(b)(10), in that it has a bona fide, demonstrable desire to develop or redevelop, and did not cause or contribute to the contamination at, the parcel(s) cited in the preceding paragraph. 5. I hereby certify, under the pains and penalties of perjury and of the Brownfields Act, that Forest Hill Church meets the eligibility requirement ofN.C.G.S.❑130A- 310.32(a)(1) in that it and any parent, subsidiary or other affiliate have substantially complied with: a. the terms of any brownfields or similar agreement to which it or any parent, subsidiary or other affiliate has been a party; b. the requirements applicable to any remediation in which it or any parent, subsidiary or other affiliate has previously engaged; c. federal and state laws, regulations and rules for the protection of the environment. Affiant furtkr saith not. 5ignatafe/Mnted Name Date, Sworn to and subscribed before me this day of- OFROX SEAL ' NOn Puhlic North Carona Notary Public,;t; S _. .A i�f -1 1 ENBURC. COUNTY, NC t. My commission expires:_ MY C. nmis$On FxOres July 1. 2023 13 Preliminary Proposed Brown -fields Agreement I. Property Facts a. Property Address(es): 729 East 36th Street and 3315 North McDowell Street b. Property Seller: Johnston Memorial Presbyterian Church flkla North Charlotte Presbyterian Chi c. Property Buyer: Forest Hill Church d. Brief Property Usage History: Church related purposes since at least 1929 with some single-family use. e. The planned reuse will potentially involve the following use classification(s) (check all that apply): ❑ School/childcare/senior care ❑R Residential ❑ Commercial, retail (specify) ❑ Other commercial (specify) ❑ Office ❑ Light industrial ❑ Heavy industrial ❑ Recreational ❑ Open space ❑X Other (specify) Religious services and meeting uses I1. Contaminant Information a. The contaminant situation at the property is hest described by the following (check all that apply): ❑ Contaminants are from an on -property source(s) ❑ Contaminants are from an off -property source(s) ❑ Contaminants are from an unknown source(s) ❑ Contaminants have not yet been documented on the property 14 b. Contaminated Media Table. (If known, check appropriate boxes below) Contaminant Soil Groundwater Private Wells Vapor Intrusion Types and/or Surface Water known Suspected known Suspected known suspected known suspected o Chlorinated r Solvents 9 (list): a n i c 5 Petroleum: Two ASTs ❑ heating USTs 0 ❑i] UST, Other ❑ Other (list): i Metals n (list): 0 r 9 a n i Other (list): C 5 III. Protective Measures I am prepared to take steps necessary to make the property suitable for its planned uses while fully protecting public health and the environment. I propose that NCBP consider a brownfields agreement that will make the property suitable for the planned use(s) through the following mechanism(s) (check all that apply): ❑ Contaminant remediation to risk -based levels. 0 Engineered Controls (e.g., low permeability caps, vapor mitigation systems, etc) ❑ Land use restrictions that run with the land that will restrict or prohibit uses that are unacceptable from a risk assessment/management perspective. (Important Note: In any 15 final brownfields agreement generated by the NCBP, land use restrictions will ultimately come with the continuing obligation to submit an annual certification that the Land Use Restrictions are being complied with and remain recorded at the applicable register of deeds office. ) IV. Fees In connection with a brownfields agreement, the Act requires that the developer pay fees to offset the cost to the Department of Environmental Quality and the Department of Justice. In satisfaction of the Act, the following fees apply to a brownfields agreement that is developed for this project under the standard program, subject to negotiation of the brownfields agreement: a. A $2,000 initial fee will be due from the applicant PD when both of the following occur: 1) NCBP receives this application, the affidavit and proposed brownfields agreement, AND 2) NCBP notifies the applicant in writing that the applicant PD and the project are eligible for participation in the NCBP and continued negotiation of a brownfields agreement. b. A second fee of $6,000 will be due from the PD prior to execution of the brownfields agreement. Should the prospective developer choose to negotiate changes to the agreement that necessitate evaluation by the Department of Justice, additional fees shall apply. c. Any addendum/modifications to the BFA or NBP after they are in effect will result in an additional fee of at least $1,000. d. In the unexpected event that the environmental conditions at the property are unusually complex, such that NCBP's costs will clearly exceed the above amounts, NCBP and PD will negotiate additional fees. e. Additional fees are charged for the Ready for Reuse and Redevelopment Now programs. Vk—tViowgement Please check this box and initial in space provided to indicate your of the standard brownfields fee structure. ❑ Please check this box and initial in space provided to indicate your interest in the Redevelopment Now program and your acknowledgement of the alternate fee structure as outlined in the Redevelopment Now Fee Consent Document (under separate cover). ❑ Please check this box and initial in space provided to indicate your interest in the Ready for Reuse program. Date of Submittal: 16 Financial Statements Location Map � cis � rl� ����, �� , .. ...... j� � •: 1 V ••y •ten• • ., +•• ' � SITE a ... R . . e•• ... r � 1 ■ ; • �f ••1 k• \ � 4 i it •.J .\ •Ii `I .. w GEOSCIENCE GROUP, INC. j CHARLOTTE, NORTH CAROLINA J SCALE I'd 95' APPROVED BY: DPAWNI HY Mec;Mcnburg Co - DATE. October 3, 2018 REVISED: ANP FOREST HILL CHURCH PARCELS CHARLOTTE, NORTH CAROLINA FrUtrttE ���sEx: 2015 COUNTY TOPOGRAPHIC MAP CH1BEFt 9 5 GEOSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE: ] " = 2,000' APPROVED BY. DRAWN BY: 1iSGS DATE- October 3, 2019 REVISED, ANP 1 FOREST HILL CHURCH PARCELS CHARLOTTE, NORTH CAROLINA 1967 USGS TOPOGRAPHIC MAP rRLNUMBER (PHOTOREVISED 1988) CH18.129-6 Survey Plat pa $ Ggg iZ S:I 3I All i I ::.... ...... _......_.—.....—._.'.._T— _ •- d f' d' •SS9YOQOri Site Photographs APPENDIX X II Site Photographs i through ] 9 Q rn E m 2 -Zf �7 Environmental/Reports/Data ROY COOPER Governor MIC1 AEL S. REGAN NORTH CAROLINA Environmental Quality Secretary July 5, 2019 MICHAEL SCOTT Director Sent Via USPS and email Torn Emmrich Forest Dill Church 7224 Park Road Charlotte, NC 28210 Nick.dusenbury@foresthill.org Subject: Letter of Eligibility N. Charlotte Presbyterian Church 729 East 36' Street and 3315 North McDowell Street Charlotte, Mecklenburg County Brownfields Project Number 23039-19-060 Dear Mr. Emmrich: The North Carolina Department of Environmental Quality (DEQ) has received and reviewed your June 13, 2019 Brownfields Property Application (BPA) submitted by Forest Hill Church as a Prospective Developer seeking a Brownfields Agreement regarding the Brownfields Property. Upon review of the BPA with respect to the requirements of the Brownfields Property Reuse Act of 1997, DEQ has determined that this project is eligible for entry into the North Carolina Brownfields Program (NCBP) and for continued evaluation for a Brownfields Agreement (BFA). The next step in the BFA process will involve a detailed review of available environmental and other relevant data to determine what is currently known about contamination at the Brownfields Property, and what, if any, information gaps may exist that may require additional assessment. We are in receipt of the following documents submitted with your BPA: Report Prepared By Date Phase I ESA Geoscience Group December 13, 2018 If available, historical Brownfields Property information from the files of DEQ's Division of Waste Management will also be utilized during the evaluation process. Please forward any additional information or data you may have or can acquire for our evaluation. This should include reports from other DEQ agencies or regional offices. We will contact you regarding any additional assessment that may be necessary to establish that the Brownfields Property is or can be made suitable for the intended reuse, as required by statute. Deprb�sd�a MarcelY�l brl� North Carolina Department of Environmental Quality I Division of Waste Management 217 West Jones Street 1 1646 Mail Service Center I Raleigh, NDrth Caraltna 2709-lb46 N. Charlotte Presbyterian Church July S, 2019 Page 2 According to the BPA, the intended redevelopment for the Brownfields Property is to develop and expand the church related use of the property. Because risk management decisions may vary depending on the nature of the redevelopment, it will be important that DEQ review the locations of the various elements. Please forward any maps or drawings indicating these details, even if they are only preliminary or conceptual. Please note: pending execution of a final BFA, NCBP eligibility is provisional. The protections a BFA offers the Prospective Developer are not in effect, unless and until, the BFA is executed. If you occupy the Brownfields Property or operate or conduct activities at the Brownfields Property that result in a release of regulated substances before a BFA has been finalized for the Brownfields Property, you may be considered to have caused or contributed to contamination at the Brownfields Property. Because an entity that could be considered to have caused or contributed to contamination at the Brownfields Property cannot be a Prospective Developer under the Act, your eligibility for participation in the NCBP would be placed in jeopardy. Consult closely with your Project Manager regarding any planned site activities prior to agreement finalization. You are cautioned to conduct all such operations and activities at the Brownfields Property with great care not to cause a release of regulated substances at the Brownfields Property that could jeopardize your eligibility for participation in the NCBP. If a party other than Forest Hill Church will own the Brownfields Property at the conclusion of the brownftelds process, the final document (which gets recorded at the register of deeds' office) must be signed not only by Prospective Developer, but by that owner. Failure by the Prospective Developer to ensure, by the time the BFA negotiations are complete, the willingness to sign of any such party, and to provide DEQ the exact name, email address, telephone number, and US mail address of the party (along with the signatory/signatory's tile in the case of an entity) will delay, and could prevent, the BFA taking effect. We are excited about the potential for public benefit offered by the reuse of the N. Charlotte Presbyterian Church Site and look forward to working with you to advance this brownfields redevelopment project. If you have questions about this correspondence or require additional information, please feel free to contact the project manager Carolyn Mirinich by phone at 704-661-0330, or by e-mail at carol yn.minnich(d�ncdenr.goW. Sincerely, Bruce Nicholson Brownfields Program Manager ec: Central Files, DEQ Michael E. Scott, DEQ Carolyn Minnich, DEQ Amy Rickers, Johnston., Allison & Hord, P.A. V JQALLISON H RD Amy L. Rickers Attorney WRITER'S E-MAIL ADDRESS: arickers@jahlaw.com WRITER'S DIRECT DIAL: 704-995-2253 April 16, 2020 Bruce Nicholson Program Manager — Brownfield Program North Carolina Department of Environmental Quality Mail Service Center 1646 Raleigh, NC 27699-1646 Re: Refund of Brownfield Application Fee for BF#23039-19-060 Dear Mr. Nicholson: I am writing on behalf of my client, Forest Hill Church (the Church). The Church applied for acceptance and was deemed eligible for the Brownfield Program in 2019. Subsequent to that notification, the Church submitted its $2,000 application fee. In further review of the project the Brownfields group advised the Church it was, in fact, not eligible for the Brownfield Program and that the UST program would be a more applicable avenue for resolution of environmental concerns at the property. The Church has since been working to seek resolution in this manner. Given that the Church is a non-profit entity it is requesting that the application fee it has paid be refunded as the Brownfield Program has determined the project is no longer eligible for coverage in its program. Please deliver the refund, made out to Forest Hill Church, to: Nick Dusenbury Forest Hill Church 7224 Park Road Charlotte, NC 28210 1065 East Morehead Street, Charlotte, NC 28204 Trr MERITAS' jahlaw.corn SAW 31Meli W0L0,m0E Mr. Nicholson April 16, 2020 Page 2 Please let me know if you need any additional information in order to process this request. The Church looks forward to receiving its refund at your earliest convenience. Regards, JOHNSTON, ALLISON & HORD, P.A. Amy Rickers Cc: Carolyn Minnich, via email: carolyn.minnich@ncdenr.gov Appendix B Certificate of Disposal, Non -Hazardous Waste Manifests, and Backfill Documentation hart F hickman SMARTER ENVIRONMENTAL'GLUTIONS �.�C:) CORPORATION 1703 Vargrave Street Winston-Salam, NC 27107 ph 33&725-5844 fax 33B-725-6244 CERTIFICATE OF DISPOSAL Eva Corporation does hereby certify that 625 gallons of non -hazardous product received on 2/1412022 from: Generator: Ascent Real Estate Capital Originating at: 719 E. 36" Street Charlotte, NC EC Waste ID #: 022222 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Environmental Quality. Signature Thomas W. Hammett CEO Evo Corporation www.ewncorp net TH E NEXT LEVEL. EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 81800 s w- ae- x:.zra•^�^a:ny.f; ,-.y ,...,. �.. �.c,',.>x."x- ;. „ � ,�mr:a ''�•' - - - - ;:a '?r..: .^., .... ._ .....s.�. i._ ,-✓-...�,: i� ::.�. .. �... x'. .; .. ��- ,s:yL; ,',.p -:s;�'�vA �r3-'-�i ,c,;�s8 �irss`F ;:.;�-+v:�i�:.y:`:� z:rx, ,�� �` �q6 GENERA`TOR`[NFORiI�AT.O . . H.r � .•pis::.-p ..�.-,.. , . <.... _� ...:°-`;::,x :...� , ... , h �� N�== _ :ems �-�'w ��;i, sc.; ..s� .... .. ....:::3-..:.... A.^... u.4..... �-�:r�•:..... s.::.,+�r:..r.,t•::.: e..... S. Fxt3.''s. 3.;a,pi.spys-�YF�: ?in% rR': '^'�/''s Generator: Ascent: Beat &tzt�e Ekp Phone: Site Address: City/State: EE Contact: ataAottej ic Caci .der v.;: m.� w�n, . �:�,+.:' .F?.-:Y �. ;�ie .;,,^L�-�tw. a ... .. .. � se. -'�^ ice. �:..... � �, e ;i: e". �,� ."€a, .: r� ,: �..,>.^.•:.,..+., .n.?w-: -`ti?= %-_�.;.•'s .e.�=.F4` Ly M.. r wS F F.� Yk�"%'?r:,-. 7;._..�-k":' r<.:-3:83.^.i•h.i u .. S� o+:.! .a- s�.C. .. � � v�i .Y w .�.....qF 8. } � F.;rv-e^.� i � _ "^t a.. V s.•i �!eid � Yf�<,�Y� i . ..'u.J �� ns.F.� e x,�i K: ;•,�� .�. >t� �.� .MAY D�S:C l :TIQN��U� � a� ,�.,.�, ::�:�...,:x.r ::��.._� .. ���r�� ^ �.��!__ _ R_P� r'Q AIiTITY�J_1NE1:C Y T ..hv. .u..... ..:.-. a .... .. �.w-a...».-- .�.n..:....�.T•:+...,.:.:...,....x..,..-....k.s...�..-......i-... =: �Y.:..,...� Ffv-x - Gross Weight (Ibs): Empty Weight (lbs): Net Weight (lbs): Material: adwct Contaminant: Quantity 9�_ Tons Drums Pails Sacs Yards Other: r�.f r .......,.�.-.,.�......r�::�.......a:n^_..r..5�o- ..,,, � � ..�a::x..:.r��..ID"� ,.•".•a:t:�n:�>�.sx�ri F•��"`;�tw�� :,.;�- n.;,. Transporter: Phone: Truck #: rWIaltiolm Contact: 336- 5--5844 Tony Usher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are In proper condition for transport In commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility deAnate. Driver Signature: EVO CORPORATION 1 703 Vargrave Street Winston-Salem, NC 27107 Date: allvhz Evo Project #: (22222 Phone: 336 725-5W Contact: Tony Disher I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina, Facifi Signature:,,- Date: p9 white/Facility Canary/Invoice Goldenrod/Generator P 'Evo Corppmiion, �408 AME=.'Xf[3 CORPORATION 1703 VwUrave 5treat Motori•Salem, SEC 27107 ph 338-725-6844 tax 335-725-6244 CERTIFICATE OF DISPOSAL Evo Corporation does hereby certify that 25.86 tons of non -hazardous contaminated material received on 2/24/2022 from: Generator: Ascent Real Estate Capital Originating at: 719 E. 36th Street Charlotte, NC EC Waste ID #: 022222 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Environmental Quality. Signature Thomas W. Hammett CEO Eva Corporation www.evocorp,net T HNEXT LEVEL. EVO CORPORATION 1703 Vargrav'e Street, Winston-Salem, SIC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # {Manifest No.14161 GENERATOR INFORMATION Generator: Ascent F4%d Estate Ckpital Phone: Site Address: City/State: Contact: CWai otte, lu C act ,der (MATERIAL DESCRIPTION / QUANTITY I WEIGHT Gross Weight (lbs): _ .� Sa Empty Weight (Ibs): Net Weight (Ibs): 2, � { 700 Quantity V s (Material: Contaminant: 6ons Drums Pails Sacs Yards Other: TR�t�S��RT�R INF®RfMATlOI4i = Transporter: a rro_n Truck #: _ Q►_ _____ ,I_ Contact: 336--725-5:844 ' ny RGher As the transparter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: Date:, FACILITY INFORMATION �1 BVO CIDrPOD-ration Evo Project * -- .222 1703 Vagr;ve fleet Phone: _ Istoxi Salcm IC 27107 Contact: the carrier has delivered the materials described above to this facility, and I hereby accept this Ireatrnent and/or disposal in a manner that has been authorized by the State of North Carolina. �iture: Date: - - White/Facility Canary/invoice Pink/Carder EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Lead # Manifest No, 14162 GENERATOR INFORMATION Ascent Baal Ek�te Capital 401-935-4802 Generator: Ascent Site Address: 719 E 3151th St- City/State: chaAo w, NC Contact: Caci Jam MATERIAL DESCRIPTION f QUANTITY 1 WEIGHT ___1 Gross Weight (Ibs):�� �] Empty Weight (Ibs): Net Weight (lbs): Quantity Material: Contaminant: _a Elmatm, `(`ens Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: BVO OMPOratioa Phone: 6-725-5844- Truck #: 3 0 — 4 e7' V Contact: Ihrim- 1-%a16.as- As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for deliverer to the facility designate. Driver Signature.- Jr ®ate;,._....... FACILITY INFORMATION FerroQ)rporadon Eye Project #: 2222 1703 Vugr"e street 336.72 5-5 84-4- Phone: _ Wmeto -Salem 1U 27107 'o:ay Usher Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. F%70 CoToratimn,1008 Corporation cal Ticket . ........ ---- --- Ti lis is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, :and when properly signed and sealed shall be prima facia e►ridence of the accuracy of the weight shown as prescribed by law. Feb 24 2022�' 649 PUBLIC WEIGHMASTER Tichet : 6546 Cust. Name: EVO Truck IB: 30-698 Trailer IDS: Reweigh Fee 2.00 Quilktrip 1044 2790 Lane St Kannapal i s, NC 28083 Axle 1 211@0 1b Axle 2 a 37300 lb Axle 3 00 lb Total c 58400 lb N�A�iIY PUBLIC WEIGHMASTER LICENSE EXPIRES JUNE 30, 2022 COREYALVERSON 41656 WEIGHMASTER OR WEIGHER SIGNATURE zV(54 DIVA LESS SIGNED DRIVER IN TRUCK U SS CHECKED HERE: CERTIFICATE OF WEIGHT & MEASURE IMPRINT SEAL. HERE fI F APPLICABL.Ej FULL WEIGH T1CXET N (IF REWEIGH) CorporationScale Ticket :This Is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, `and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law. Feb 24 2022 O L Z 7-ZZ. PUBLIC WEIGHMASTER'S Ticket 6545 CERTIFICATE OF CuSt . Name: EU❑ WEIGHT & MEASURE Track I D : 30-fi98 Trailer ID: Weigh Fee: 12.50 [�uiktriA 11i344 aR� WP 2790 lane St N Hannapo 1 i s, N6 28093 PUBLIC WEIGHMASTER r ENSE EXPIRES JUNE 30, 2022 Axle ! : 19420 lb COREY ALVERSON 41656 HNIR e Axle Total 30660 lb 00 lb WEIGHMASTI 4R ILb)'n ez_ 50080 lb WEIGHER SIGNATURE INVALID UNLESS SIGNET] DRIVER IN TRUCK UNLESS CHECKED HERE: FULLWEIGH TICKET it [IF REWEIGH] R.H. 199I-L , McGIRT •� TRUCKING CO., INC. 13DO1 General Drive + Charlotte. NC 28273 Phone (7 4) 588-8527 CUSTOMER JOB NAME — 5c�' -/7, , CUSTOMER'S SIGNATURE NDT RESPONSIBLE FOR OVERWEIGHT TICKETS OR FINES. r—1 LD co U Cr)Z v c] i xz Ze Ono z �� as tam r, c1 � L w Y r Co N z Co — r w 00 O N c () U 2 �Z N lid Ll3U 0 Lin �°� m a m LU U, r H L w cr luj I a N a o a o ❑ J o 0 J "� 2 id 4 O L ~ ¢ a a fj > j D k d to Y cc w 2 OR N U Appendix C Tank Disposal Certificate hart hickman SMARTER ENVIRONMENTAL SOLUTIONS CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 _. .,. ph 335-725-5944 fax 336-725-a2" 'SANK DISPOSAL CERTIFICATE Tank Owner: Ascent Real Estate Capital Site Address: 719 E. 36th Street Charlotte, NC Description of Tanks: Tank Size of Tank Contents Number 1 1,000 Gallons 12 Fuel Oil ? 550 Gallons 42 Fuel Oil 3 550 Gallons 42 Fuel Oil Transporter: Eva Corporation EC Project M 022222 Disposal Certification: Eva Corporation does hereby certify that the above named storage tanks were transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem, NC for proper disposal and recycling. Signature Thomas W. Hammett CEO Eva Corporation ►mw evocarpmet T E NEXT LEVEL. Appendix D Laboratory Analytical Report qd hart hickman SMARTER ENVIRONMENTAL SOWT1ONS aceAnalytical WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 February 22, 2022 Nathan O'Leary Hart & Hickman 2923 S. Tryon St Charlotte, NC 28203 RE: Project: CCW-006 Pace Project No.: 92588327 Dear Nathan O'Leary: Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com 1(704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 104 accAnafyfical www, pa c ela b5-m m Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: CCW-006 Pace Project No.: 92588327 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 104 laceAnalytical" WWW.pacalahs'com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: CCW-006 Pace Project No.: 92588327 Lab ID Sample ID Matrix Date Collected Date Received 92588327001 UST-1 Solid 02/14/2214:30 02/15/2214:54 92588327002 UST-3 Solid 02/14/2214:55 02/15/2214:54 92588327003 UST-1-13 Solid 02/14/2215:25 02/15/2214:54 92588327004 UST-1-SW-F Solid 02/14/2215:15 02/15/2214:54 92588327005 UST-1-SW-13 Solid 02/14/2215:35 02/15/2214:54 92588327006 UST-1-SW-R Solid 02/14/2215:40 02/15/2214:54 92588327007 UST-1-SW-L Solid 02/14/2215:50 02/15/2214:54 92588327008 UST-2-SW-L Solid 02/14/2216:00 02/15/2214:54 92588327009 UST-2-13 Solid 02/14/2216:20 02/15/2214:54 92588327010 UST-2-SW-R Solid 02/14/2216:10 02/15/2214:54 92588327011 UST-2-SW-13 Solid 02/14/2216:30 02/15/2214:54 92588327012 UST-2-SW-F Solid 02/14/2216:40 02/15/2214:54 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 104 laceAnalytical" WWW.pacalahs'com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: CCW-006 92588327 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92588327001 UST-1 EPA 8015C AP2 2 PASI-C EPA 8015C MAD 2 PASI-C SW-846 KDF 1 PASI-C 92588327002 UST-3 EPA 8015C AP2 2 PASI-C EPA 8015C MAD 2 PASI-C SW-846 KDF 1 PASI-C 92588327003 UST-1-13 MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327004 UST-1-SW-F MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327005 UST-1-SW-13 MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327006 UST-1-SW-R MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327007 UST-1-SW-L MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327008 UST-2-SW-L MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327009 UST-2-13 MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327010 UST-2-SW-R MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 104 laceAnalytical" WWW.pacalahs'com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: CCW-006 Pace Project No.: 92588327 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SW-846 KDF 1 PASI-C 92588327011 UST-2-SW-13 MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C 92588327012 UST-2-SW-F MADEP VPH MAD 5 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D SAS 70 PASI-C SW-846 KDF 1 PASI-C PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1 Lab ID: 92588327001 Collected: 02/14/22 14:30 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015C Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Diesel Range Organics(C10- 838 mg/kg 15.4 10.9 2 02/15/22 22:51 02/16/22 17:24 C28) Surrogates n-Pentacosane (S) 55 % 32-130 2 02/15/22 22:51 02/16/22 17:24 629-99-2 Gasoline Range Organics Analytical Method: EPA 8015C Preparation Method: EPA 5030E Pace Analytical Services - Charlotte Gas Range Organics (C6-C10) 146 mg/kg 12.9 3.3 1 02/16/22 12:47 02/16/22 19:24 Surrogates 4-Bromofluorobenzene (S) 138 % 66-131 1 02/16/22 12:47 02/16/22 19:24 460-00-4 S5 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 33.9 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-3 Lab ID: 92588327002 Collected: 02/14/22 14:55 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015C Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Diesel Range Organics(C10- 5.91 mg/kg 6.3 4.5 1 02/15/22 22:51 02/16/22 16:17 C28) Surrogates n-Pentacosane (S) 57 % 32-130 1 02/15/22 22:51 02/16/22 16:17 629-99-2 Gasoline Range Organics Analytical Method: EPA 8015C Preparation Method: EPA 5030E Pace Analytical Services - Charlotte Gas Range Organics (C6-C10) ND mg/kg 8.4 2.1 1 02/17/22 14:29 02/17/22 16:40 Surrogates 4-Bromofluorobenzene (S) 82 % 66-131 1 02/17/22 14:29 02/17/22 16:40 460-00-4 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 20.2 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-13 Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 16:29 Aliphatic(C09-C12)Adjusted ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 16:29 Aromatic (C09-C10) ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 16:29 Surrogates 4-Bromofluorobenzene (FID) (S) 89 % 70-130 1 02/16/22 13:41 02/16/22 16:29 460-00-4 4-Bromofluorobenzene (PID) (S) 76 % 70-130 1 02/16/22 13:41 02/16/22 16:29 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 483 170 1 02/16/22 11:33 02/17/22 11:34 83-32-9 Acenaphthylene ND ug/kg 483 170 1 02/16/22 11:33 02/17/22 11:34 208-96-8 Aniline ND ug/kg 483 189 1 02/16/22 11:33 02/17/22 11:34 62-53-3 Anthracene ND ug/kg 483 158 1 02/16/22 11:33 02/17/22 11:34 120-12-7 Benzo(a)anthracene ND ug/kg 483 161 1 02/16/22 11:33 02/17/22 11:34 56-55-3 Benzo(a)pyrene ND ug/kg 483 167 1 02/16/22 11:33 02/17/22 11:34 50-32-8 Benzo(b)fluoranthene ND ug/kg 483 161 1 02/16/22 11:33 02/17/22 11:34 205-99-2 Benzo(g,h,i)perylene ND ug/kg 483 187 1 02/16/22 11:33 02/17/22 11:34 191-24-2 Benzo(k)fluoranthene ND ug/kg 483 170 1 02/16/22 11:33 02/17/22 11:34 207-08-9 Benzoic Acid ND ug/kg 2420 1040 1 02/16/22 11:33 02/17/22 11:34 65-85-0 Benzyl alcohol ND ug/kg 966 366 1 02/16/22 11:33 02/17/22 11:34 100-51-6 4-Bromophenylphenyl ether ND ug/kg 483 186 1 02/16/22 11:33 02/17/22 11:34 101-55-3 Butylbenzylphthalate ND ug/kg 483 204 1 02/16/22 11:33 02/17/22 11:34 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 966 340 1 02/16/22 11:33 02/17/22 11:34 59-50-7 4-Chloroaniline ND ug/kg 966 379 1 02/16/22 11:33 02/17/22 11:34 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 483 201 1 02/16/22 11:33 02/17/22 11:34 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 483 182 1 02/16/22 11:33 02/17/22 11:34 111-44-4 2-Chloronaphthalene ND ug/kg 483 192 1 02/16/22 11:33 02/17/22 11:34 91-58-7 2-Chlorophenol ND ug/kg 483 182 1 02/16/22 11:33 02/17/22 11:34 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 483 180 1 02/16/22 11:33 02/17/22 11:34 7005-72-3 Chrysene ND ug/kg 483 176 1 02/16/22 11:33 02/17/22 11:34 218-01-9 Dibenz(a,h)anthracene ND ug/kg 483 186 1 02/16/22 11:33 02/17/22 11:34 53-70-3 Dibenzofuran ND ug/kg 483 174 1 02/16/22 11:33 02/17/22 11:34 132-64-9 1,2-Dichlorobenzene ND ug/kg 483 174 1 02/16/22 11:33 02/17/22 11:34 95-50-1 1,3-Dichlorobenzene ND ug/kg 483 171 1 02/16/22 11:33 02/17/22 11:34 541-73-1 1,4-Dichlorobenzene ND ug/kg 483 185 1 02/16/22 11:33 02/17/22 11:34 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 966 327 1 02/16/22 11:33 02/17/22 11:34 91-94-1 2,4-Dichlorophenol ND ug/kg 483 189 1 02/16/22 11:33 02/17/22 11:34 120-83-2 Diethylphthalate ND ug/kg 483 177 1 02/16/22 11:33 02/17/22 11:34 84-66-2 2,4-Dimethylphenol ND ug/kg 483 201 1 02/16/22 11:33 02/17/22 11:34 105-67-9 Dimethylphthalate ND ug/kg 483 176 1 02/16/22 11:33 02/17/22 11:34 131-11-3 Di-n-butylphthalate ND ug/kg 483 163 1 02/16/22 11:33 02/17/22 11:34 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 966 451 1 02/16/22 11:33 02/17/22 11:34 534-52-1 2,4-Dinitrophenol ND ug/kg 2420 1490 1 02/16/22 11:33 02/17/22 11:34 51-28-5 2,4-Dinitrotoluene ND ug/kg 483 186 1 02/16/22 11:33 02/17/22 11:34 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-13 Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 483 177 1 02/16/22 11:33 02/17/22 11:34 606-20-2 Di-n-octylphthalate ND ug/kg 483 190 1 02/16/22 11:33 02/17/22 11:34 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 483 187 1 02/16/22 11:33 02/17/22 11:34 117-81-7 Fluoranthene ND ug/kg 483 165 1 02/16/22 11:33 02/17/22 11:34 206-44-0 Fluorene ND ug/kg 483 170 1 02/16/22 11:33 02/17/22 11:34 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 483 209 1 02/16/22 11:33 02/17/22 11:34 87-68-3 Hexachlorobenzene ND ug/kg 483 189 1 02/16/22 11:33 02/17/22 11:34 118-74-1 Hexachlorocyclopentadiene ND ug/kg 483 277 1 02/16/22 11:33 02/17/22 11:34 77-47-4 Hexachloroethane ND ug/kg 483 185 1 02/16/22 11:33 02/17/22 11:34 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 483 190 1 02/16/22 11:33 02/17/22 11:34 193-39-5 Isophorone ND ug/kg 483 215 1 02/16/22 11:33 02/17/22 11:34 78-59-1 1-Methylnaphthalene ND ug/kg 483 170 1 02/16/22 11:33 02/17/22 11:34 90-12-0 2-Methylnaphthalene ND ug/kg 483 193 1 02/16/22 11:33 02/17/22 11:34 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 483 198 1 02/16/22 11:33 02/17/22 11:34 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 483 195 1 02/16/22 11:33 02/17/22 11:34 15831-10-4 Naphthalene ND ug/kg 483 164 1 02/16/22 11:33 02/17/22 11:34 91-20-3 2-Nitroaniline ND ug/kg 2420 395 1 02/16/22 11:33 02/17/22 11:34 88-74-4 3-Nitroaniline ND ug/kg 2420 379 1 02/16/22 11:33 02/17/22 11:34 99-09-2 4-Nitroaniline ND ug/kg 966 368 1 02/16/22 11:33 02/17/22 11:34 100-01-6 Nitrobenzene ND ug/kg 483 224 1 02/16/22 11:33 02/17/22 11:34 98-95-3 2-Nitrophenol ND ug/kg 483 209 1 02/16/22 11:33 02/17/22 11:34 88-75-5 4-Nitrophenol ND ug/kg 2420 934 1 02/16/22 11:33 02/17/22 11:34 100-02-7 N-Nitrosodimethylamine ND ug/kg 483 163 1 02/16/22 11:33 02/17/22 11:34 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 483 182 1 02/16/22 11:33 02/17/22 11:34 621-64-7 N-Nitrosodiphenylamine ND ug/kg 483 171 1 02/16/22 11:33 02/17/22 11:34 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 483 230 1 02/16/22 11:33 02/17/22 11:34 108-60-1 Pentachlorophenol ND ug/kg 966 473 1 02/16/22 11:33 02/17/22 11:34 87-86-5 Phenanthrene ND ug/kg 483 158 1 02/16/22 11:33 02/17/22 11:34 85-01-8 Phenol ND ug/kg 483 215 1 02/16/22 11:33 02/17/22 11:34 108-95-2 Pyrene ND ug/kg 483 196 1 02/16/22 11:33 02/17/22 11:34 129-00-0 Pyridine ND ug/kg 483 152 1 02/16/22 11:33 02/17/22 11:34 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 483 190 1 02/16/22 11:33 02/17/22 11:34 120-82-1 2,4,5-Trichlorophenol ND ug/kg 483 221 1 02/16/22 11:33 02/17/22 11:34 95-95-4 2,4,6-Trichlorophenol ND ug/kg 483 199 1 02/16/22 11:33 02/17/22 11:34 88-06-2 Surrogates Nitrobenzene-d5 (S) 64 % 21-130 1 02/16/22 11:33 02/17/22 11:34 4165-60-0 2-Fluorobiphenyl (S) 52 % 19-130 1 02/16/22 11:33 02/17/22 11:34 321-60-8 Terphenyl-d14 (S) 46 % 15-130 1 02/16/22 11:33 02/17/22 11:34 1718-51-0 Phenol-d6 (S) 65 % 18-130 1 02/16/22 11:33 02/17/22 11:34 13127-88-3 2-Fluorophenol (S) 62 % 18-130 1 02/16/22 11:33 02/17/22 11:34 367-12-4 2,4,6-Tribromophenol (S) 63 % 18-130 1 02/16/22 11:33 02/17/22 11:34 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-B Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 233 74.7 1 02/15/22 21:19 02/17/22 17:12 67-64-1 Benzene 6.9J ug/kg 11.6 4.6 1 02/15/22 21:19 02/17/22 17:12 71-43-2 Bromobenzene ND ug/kg 11.6 3.8 1 02/15/22 21:19 02/17/22 17:12 108-86-1 Bromochloromethane ND ug/kg 11.6 3.4 1 02/15/22 21:19 02/17/22 17:12 74-97-5 Bromodichloromethane ND ug/kg 11.6 4.5 1 02/15/22 21:19 02/17/22 17:12 75-27-4 Bromoform ND ug/kg 11.6 4.1 1 02/15/22 21:19 02/17/22 17:12 75-25-2 Bromomethane ND ug/kg 23.3 18.4 1 02/15/22 21:19 02/17/22 17:12 74-83-9 2-Butanone (MEK) ND ug/kg 233 55.9 1 02/15/22 21:19 02/17/22 17:12 78-93-3 n-Butylbenzene ND ug/kg 11.6 5.5 1 02/15/22 21:19 02/17/22 17:12 104-51-8 sec-Butylbenzene ND ug/kg 11.6 5.1 1 02/15/22 21:19 02/17/22 17:12 135-98-8 tert-Butyl benzene ND ug/kg 11.6 4.1 1 02/15/22 21:19 02/17/22 17:12 98-06-6 Carbon tetrachloride ND ug/kg 11.6 4.4 1 02/15/22 21:19 02/17/22 17:12 56-23-5 Chlorobenzene ND ug/kg 11.6 2.2 1 02/15/22 21:19 02/17/22 17:12 108-90-7 Chloroethane ND ug/kg 23.3 9.0 1 02/15/22 21:19 02/17/22 17:12 75-00-3 Chloroform ND ug/kg 11.6 7.1 1 02/15/22 21:19 02/17/22 17:12 67-66-3 Chloromethane ND ug/kg 23.3 9.8 1 02/15/22 21:19 02/17/22 17:12 74-87-3 2-Chlorotoluene ND ug/kg 11.6 4.1 1 02/15/22 21:19 02/17/22 17:12 95-49-8 4-Chlorotoluene ND ug/kg 11.6 2.1 1 02/15/22 21:19 02/17/22 17:12 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 11.6 4.5 1 02/15/22 21:19 02/17/22 17:12 96-12-8 Dibromochloromethane ND ug/kg 11.6 6.5 1 02/15/22 21:19 02/17/22 17:12 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 11.6 5.1 1 02/15/22 21:19 02/17/22 17:12 106-93-4 Dibromomethane ND ug/kg 11.6 2.5 1 02/15/22 21:19 02/17/22 17:12 74-95-3 1,2-Dichlorobenzene ND ug/kg 11.6 4.2 1 02/15/22 21:19 02/17/22 17:12 95-50-1 1,3-Dichlorobenzene ND ug/kg 11.6 3.6 1 02/15/22 21:19 02/17/22 17:12 541-73-1 1,4-Dichlorobenzene ND ug/kg 11.6 3.0 1 02/15/22 21:19 02/17/22 17:12 106-46-7 Dichlorodifluoromethane ND ug/kg 23.3 5.1 1 02/15/22 21:19 02/17/22 17:12 75-71-8 1,1-Dichloroethane ND ug/kg 11.6 4.8 1 02/15/22 21:19 02/17/22 17:12 75-34-3 1,2-Dichloroethane ND ug/kg 11.6 7.7 1 02/15/22 21:19 02/17/22 17:12 107-06-2 1,1-Dichloroethene ND ug/kg 11.6 4.8 1 02/15/22 21:19 02/17/22 17:12 75-35-4 cis-1,2-Dichloroethene ND ug/kg 11.6 4.0 1 02/15/22 21:19 02/17/22 17:12 156-59-2 trans-1,2-Dichloroethene ND ug/kg 11.6 4.1 1 02/15/22 21:19 02/17/22 17:12 156-60-5 1,2-Dichloropropane ND ug/kg 11.6 3.5 1 02/15/22 21:19 02/17/22 17:12 78-87-5 1,3-Dichloropropane ND ug/kg 11.6 3.6 1 02/15/22 21:19 02/17/22 17:12 142-28-9 2,2-Dichloropropane ND ug/kg 11.6 3.8 1 02/15/22 21:19 02/17/22 17:12 594-20-7 1,1-Dichloropropene ND ug/kg 11.6 5.6 1 02/15/22 21:19 02/17/22 17:12 563-58-6 cis-1,3-Dichloropropene ND ug/kg 11.6 3.2 1 02/15/22 21:19 02/17/22 17:12 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 11.6 4.0 1 02/15/22 21:19 02/17/22 17:12 10061-02-6 Diisopropyl ether ND ug/kg 11.6 3.1 1 02/15/22 21:19 02/17/22 17:12 108-20-3 Ethylbenzene 6.OJ ug/kg 11.6 5.4 1 02/15/22 21:19 02/17/22 17:12 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 23.3 19.0 1 02/15/22 21:19 02/17/22 17:12 87-68-3 2-Hexanone ND ug/kg 116 11.2 1 02/15/22 21:19 02/17/22 17:12 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 11.6 4.0 1 02/15/22 21:19 02/17/22 17:12 98-82-8 p-Isopropyltoluene ND ug/kg 11.6 5.7 1 02/15/22 21:19 02/17/22 17:12 99-87-6 Methylene Chloride ND ug/kg 46.6 31.9 1 02/15/22 21:19 02/17/22 17:12 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 M1 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-13 Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 116 11.2 1 02/15/22 21:19 02/17/22 17:12 108-10-1 Methyl-tert-butyl ether ND ug/kg 11.6 4.4 1 02/15/22 21:19 02/17/22 17:12 1634-04-4 Naphthalene 17.7 ug/kg 11.6 6.1 1 02/15/22 21:19 02/17/22 17:12 91-20-3 n-Propylbenzene ND ug/kg 11.6 4.1 1 02/15/22 21:19 02/17/22 17:12 103-65-1 Styrene ND ug/kg 11.6 3.1 1 02/15/22 21:19 02/17/22 17:12 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 11.6 4.5 1 02/15/22 21:19 02/17/22 17:12 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 11.6 3.1 1 02/15/22 21:19 02/17/22 17:12 79-34-5 Tetrachloroethene ND ug/kg 11.6 3.7 1 02/15/22 21:19 02/17/22 17:12 127-18-4 Toluene 19.7 ug/kg 11.6 3.3 1 02/15/22 21:19 02/17/22 17:12 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 11.6 9.4 1 02/15/22 21:19 02/17/22 17:12 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 11.6 9.8 1 02/15/22 21:19 02/17/22 17:12 120-82-1 1,1,1-Trichloroethane ND ug/kg 11.6 6.1 1 02/15/22 21:19 02/17/22 17:12 71-55-6 1,1,2-Trichloroethane ND ug/kg 11.6 3.9 1 02/15/22 21:19 02/17/22 17:12 79-00-5 Trichloroethene ND ug/kg 11.6 3.0 1 02/15/22 21:19 02/17/22 17:12 79-01-6 Trichlorofluoromethane ND ug/kg 11.6 6.4 1 02/15/22 21:19 02/17/22 17:12 75-69-4 1,2,3-Trichloropropane ND ug/kg 11.6 5.9 1 02/15/22 21:19 02/17/22 17:12 96-18-4 M1 1,2,4-Trimethylbenzene 6.1J ug/kg 11.6 3.2 1 02/15/22 21:19 02/17/22 17:12 95-63-6 1,3,5-Trimethyl benzene ND ug/kg 11.6 3.9 1 02/15/22 21:19 02/17/22 17:12 108-67-8 Vinyl acetate ND ug/kg 116 8.5 1 02/15/22 21:19 02/17/22 17:12 108-05-4 Vinyl chloride ND ug/kg 23.3 5.9 1 02/15/22 21:19 02/17/22 17:12 75-01-4 v2 Xylene (Total) 17AJ ug/kg 23.3 6.6 1 02/15/22 21:19 02/17/22 17:12 1330-20-7 m&p-Xylene 11.3J ug/kg 23.3 8.0 1 02/15/22 21:19 02/17/22 17:12 179601-23-1 o-Xylene 6.2J ug/kg 11.6 5.1 1 02/15/22 21:19 02/17/22 17:12 95-47-6 Surrogates Toluene-d8 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 17:12 2037-26-5 4-Bromofluorobenzene (S) 98 % 69-134 1 02/15/22 21:19 02/17/22 17:12 460-00-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 02/15/22 21:19 02/17/22 17:12 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 30.8 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 4.6 4.6 1 02/16/22 13:41 02/16/22 16:58 Aliphatic(C09-C12)Adjusted ND mg/kg 4.6 4.6 1 02/16/22 13:41 02/16/22 16:58 Aromatic (C09-C10) ND mg/kg 4.6 4.6 1 02/16/22 13:41 02/16/22 16:58 Surrogates 4-Bromofluorobenzene (FID) (S) 95 % 70-130 1 02/16/22 13:41 02/16/22 16:58 460-00-4 4-Bromofluorobenzene (PID) (S) 81 % 70-130 1 02/16/22 13:41 02/16/22 16:58 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 453 159 1 02/16/22 11:33 02/17/22 12:01 83-32-9 Acenaphthylene ND ug/kg 453 159 1 02/16/22 11:33 02/17/22 12:01 208-96-8 Aniline ND ug/kg 453 177 1 02/16/22 11:33 02/17/22 12:01 62-53-3 Anthracene ND ug/kg 453 148 1 02/16/22 11:33 02/17/22 12:01 120-12-7 Benzo(a)anthracene ND ug/kg 453 151 1 02/16/22 11:33 02/17/22 12:01 56-55-3 Benzo(a)pyrene ND ug/kg 453 157 1 02/16/22 11:33 02/17/22 12:01 50-32-8 Benzo(b)fluoranthene ND ug/kg 453 151 1 02/16/22 11:33 02/17/22 12:01 205-99-2 Benzo(g,h,i)perylene ND ug/kg 453 176 1 02/16/22 11:33 02/17/22 12:01 191-24-2 Benzo(k)fluoranthene ND ug/kg 453 159 1 02/16/22 11:33 02/17/22 12:01 207-08-9 Benzoic Acid ND ug/kg 2270 973 1 02/16/22 11:33 02/17/22 12:01 65-85-0 Benzyl alcohol ND ug/kg 906 343 1 02/16/22 11:33 02/17/22 12:01 100-51-6 4-Bromophenylphenyl ether ND ug/kg 453 174 1 02/16/22 11:33 02/17/22 12:01 101-55-3 Butylbenzylphthalate ND ug/kg 453 191 1 02/16/22 11:33 02/17/22 12:01 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 906 319 1 02/16/22 11:33 02/17/22 12:01 59-50-7 4-Chloroaniline ND ug/kg 906 356 1 02/16/22 11:33 02/17/22 12:01 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 453 188 1 02/16/22 11:33 02/17/22 12:01 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 453 170 1 02/16/22 11:33 02/17/22 12:01 111-44-4 2-Chloronaphthalene ND ug/kg 453 180 1 02/16/22 11:33 02/17/22 12:01 91-58-7 2-Chlorophenol ND ug/kg 453 170 1 02/16/22 11:33 02/17/22 12:01 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 453 169 1 02/16/22 11:33 02/17/22 12:01 7005-72-3 Chrysene ND ug/kg 453 165 1 02/16/22 11:33 02/17/22 12:01 218-01-9 Dibenz(a,h)anthracene ND ug/kg 453 174 1 02/16/22 11:33 02/17/22 12:01 53-70-3 Dibenzofuran ND ug/kg 453 163 1 02/16/22 11:33 02/17/22 12:01 132-64-9 1,2-Dichlorobenzene ND ug/kg 453 163 1 02/16/22 11:33 02/17/22 12:01 95-50-1 1,3-Dichlorobenzene ND ug/kg 453 161 1 02/16/22 11:33 02/17/22 12:01 541-73-1 1,4-Dichlorobenzene ND ug/kg 453 173 1 02/16/22 11:33 02/17/22 12:01 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 906 306 1 02/16/22 11:33 02/17/22 12:01 91-94-1 2,4-Dichlorophenol ND ug/kg 453 177 1 02/16/22 11:33 02/17/22 12:01 120-83-2 Diethylphthalate ND ug/kg 453 166 1 02/16/22 11:33 02/17/22 12:01 84-66-2 2,4-Dimethylphenol ND ug/kg 453 188 1 02/16/22 11:33 02/17/22 12:01 105-67-9 Dimethylphthalate ND ug/kg 453 165 1 02/16/22 11:33 02/17/22 12:01 131-11-3 Di-n-butylphthalate ND ug/kg 453 152 1 02/16/22 11:33 02/17/22 12:01 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 906 423 1 02/16/22 11:33 02/17/22 12:01 534-52-1 2,4-Dinitrophenol ND ug/kg 2270 1400 1 02/16/22 11:33 02/17/22 12:01 51-28-5 2,4-Dinitrotoluene ND ug/kg 453 174 1 02/16/22 11:33 02/17/22 12:01 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 453 166 1 02/16/22 11:33 02/17/22 12:01 606-20-2 Di-n-octylphthalate ND ug/kg 453 178 1 02/16/22 11:33 02/17/22 12:01 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 453 176 1 02/16/22 11:33 02/17/22 12:01 117-81-7 Fluoranthene ND ug/kg 453 155 1 02/16/22 11:33 02/17/22 12:01 206-44-0 Fluorene ND ug/kg 453 159 1 02/16/22 11:33 02/17/22 12:01 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 453 196 1 02/16/22 11:33 02/17/22 12:01 87-68-3 Hexachlorobenzene ND ug/kg 453 177 1 02/16/22 11:33 02/17/22 12:01 118-74-1 Hexachlorocyclopentadiene ND ug/kg 453 259 1 02/16/22 11:33 02/17/22 12:01 77-47-4 Hexachloroethane ND ug/kg 453 173 1 02/16/22 11:33 02/17/22 12:01 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 453 178 1 02/16/22 11:33 02/17/22 12:01 193-39-5 Isophorone ND ug/kg 453 202 1 02/16/22 11:33 02/17/22 12:01 78-59-1 1-Methylnaphthalene ND ug/kg 453 159 1 02/16/22 11:33 02/17/22 12:01 90-12-0 2-Methylnaphthalene ND ug/kg 453 181 1 02/16/22 11:33 02/17/22 12:01 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 453 185 1 02/16/22 11:33 02/17/22 12:01 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 453 183 1 02/16/22 11:33 02/17/22 12:01 15831-10-4 Naphthalene ND ug/kg 453 154 1 02/16/22 11:33 02/17/22 12:01 91-20-3 2-Nitroaniline ND ug/kg 2270 371 1 02/16/22 11:33 02/17/22 12:01 88-74-4 3-Nitroaniline ND ug/kg 2270 356 1 02/16/22 11:33 02/17/22 12:01 99-09-2 4-Nitroaniline ND ug/kg 906 345 1 02/16/22 11:33 02/17/22 12:01 100-01-6 Nitrobenzene ND ug/kg 453 210 1 02/16/22 11:33 02/17/22 12:01 98-95-3 2-Nitrophenol ND ug/kg 453 196 1 02/16/22 11:33 02/17/22 12:01 88-75-5 4-Nitrophenol ND ug/kg 2270 876 1 02/16/22 11:33 02/17/22 12:01 100-02-7 N-Nitrosodimethylamine ND ug/kg 453 152 1 02/16/22 11:33 02/17/22 12:01 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 453 170 1 02/16/22 11:33 02/17/22 12:01 621-64-7 N-Nitrosodiphenylamine ND ug/kg 453 161 1 02/16/22 11:33 02/17/22 12:01 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 453 216 1 02/16/22 11:33 02/17/22 12:01 108-60-1 Pentachlorophenol ND ug/kg 906 443 1 02/16/22 11:33 02/17/22 12:01 87-86-5 Phenanthrene ND ug/kg 453 148 1 02/16/22 11:33 02/17/22 12:01 85-01-8 Phenol ND ug/kg 453 202 1 02/16/22 11:33 02/17/22 12:01 108-95-2 Pyrene ND ug/kg 453 184 1 02/16/22 11:33 02/17/22 12:01 129-00-0 Pyridine ND ug/kg 453 143 1 02/16/22 11:33 02/17/22 12:01 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 453 178 1 02/16/22 11:33 02/17/22 12:01 120-82-1 2,4,5-Trichlorophenol ND ug/kg 453 207 1 02/16/22 11:33 02/17/22 12:01 95-95-4 2,4,6-Trichlorophenol ND ug/kg 453 187 1 02/16/22 11:33 02/17/22 12:01 88-06-2 Surrogates Nitrobenzene-d5 (S) 64 % 21-130 1 02/16/22 11:33 02/17/22 12:01 4165-60-0 2-Fluorobiphenyl (S) 57 % 19-130 1 02/16/22 11:33 02/17/22 12:01 321-60-8 Terphenyl-d14 (S) 59 % 15-130 1 02/16/22 11:33 02/17/22 12:01 1718-51-0 Phenol-d6 (S) 64 % 18-130 1 02/16/22 11:33 02/17/22 12:01 13127-88-3 2-Fluorophenol (S) 63 % 18-130 1 02/16/22 11:33 02/17/22 12:01 367-12-4 2,4,6-Tribromophenol (S) 65 % 18-130 1 02/16/22 11:33 02/17/22 12:01 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 189 60.6 1 02/15/22 21:19 02/17/22 17:30 67-64-1 Benzene ND ug/kg 9.4 3.8 1 02/15/22 21:19 02/17/22 17:30 71-43-2 Bromobenzene ND ug/kg 9.4 3.1 1 02/15/22 21:19 02/17/22 17:30 108-86-1 Bromochloromethane ND ug/kg 9.4 2.8 1 02/15/22 21:19 02/17/22 17:30 74-97-5 Bromodichloromethane ND ug/kg 9.4 3.6 1 02/15/22 21:19 02/17/22 17:30 75-27-4 Bromoform ND ug/kg 9.4 3.3 1 02/15/22 21:19 02/17/22 17:30 75-25-2 Bromomethane ND ug/kg 18.9 14.9 1 02/15/22 21:19 02/17/22 17:30 74-83-9 2-Butanone (MEK) ND ug/kg 189 45.3 1 02/15/22 21:19 02/17/22 17:30 78-93-3 n-Butylbenzene ND ug/kg 9.4 4.5 1 02/15/22 21:19 02/17/22 17:30 104-51-8 sec-Butylbenzene ND ug/kg 9.4 4.2 1 02/15/22 21:19 02/17/22 17:30 135-98-8 tert-Butyl benzene ND ug/kg 9.4 3.4 1 02/15/22 21:19 02/17/22 17:30 98-06-6 Carbon tetrachloride ND ug/kg 9.4 3.5 1 02/15/22 21:19 02/17/22 17:30 56-23-5 Chlorobenzene ND ug/kg 9.4 1.8 1 02/15/22 21:19 02/17/22 17:30 108-90-7 Chloroethane ND ug/kg 18.9 7.3 1 02/15/22 21:19 02/17/22 17:30 75-00-3 Chloroform ND ug/kg 9.4 5.7 1 02/15/22 21:19 02/17/22 17:30 67-66-3 Chloromethane ND ug/kg 18.9 7.9 1 02/15/22 21:19 02/17/22 17:30 74-87-3 2-Chlorotoluene ND ug/kg 9.4 3.3 1 02/15/22 21:19 02/17/22 17:30 95-49-8 4-Chlorotoluene ND ug/kg 9.4 1.7 1 02/15/22 21:19 02/17/22 17:30 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 9.4 3.7 1 02/15/22 21:19 02/17/22 17:30 96-12-8 Dibromochloromethane ND ug/kg 9.4 5.3 1 02/15/22 21:19 02/17/22 17:30 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 9.4 4.2 1 02/15/22 21:19 02/17/22 17:30 106-93-4 Dibromomethane ND ug/kg 9.4 2.0 1 02/15/22 21:19 02/17/22 17:30 74-95-3 1,2-Dichlorobenzene ND ug/kg 9.4 3.4 1 02/15/22 21:19 02/17/22 17:30 95-50-1 1,3-Dichlorobenzene ND ug/kg 9.4 2.9 1 02/15/22 21:19 02/17/22 17:30 541-73-1 1,4-Dichlorobenzene ND ug/kg 9.4 2.5 1 02/15/22 21:19 02/17/22 17:30 106-46-7 Dichlorodifluoromethane ND ug/kg 18.9 4.1 1 02/15/22 21:19 02/17/22 17:30 75-71-8 1,1-Dichloroethane ND ug/kg 9.4 3.9 1 02/15/22 21:19 02/17/22 17:30 75-34-3 1,2-Dichloroethane ND ug/kg 9.4 6.2 1 02/15/22 21:19 02/17/22 17:30 107-06-2 1,1-Dichloroethene ND ug/kg 9.4 3.9 1 02/15/22 21:19 02/17/22 17:30 75-35-4 cis-1,2-Dichloroethene ND ug/kg 9.4 3.2 1 02/15/22 21:19 02/17/22 17:30 156-59-2 trans-1,2-Dichloroethene ND ug/kg 9.4 3.3 1 02/15/22 21:19 02/17/22 17:30 156-60-5 1,2-Dichloropropane ND ug/kg 9.4 2.8 1 02/15/22 21:19 02/17/22 17:30 78-87-5 1,3-Dichloropropane ND ug/kg 9.4 2.9 1 02/15/22 21:19 02/17/22 17:30 142-28-9 2,2-Dichloropropane ND ug/kg 9.4 3.1 1 02/15/22 21:19 02/17/22 17:30 594-20-7 1,1-Dichloropropene ND ug/kg 9.4 4.5 1 02/15/22 21:19 02/17/22 17:30 563-58-6 cis-1,3-Dichloropropene ND ug/kg 9.4 2.6 1 02/15/22 21:19 02/17/22 17:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 9.4 3.2 1 02/15/22 21:19 02/17/22 17:30 10061-02-6 Diisopropyl ether ND ug/kg 9.4 2.5 1 02/15/22 21:19 02/17/22 17:30 108-20-3 Ethylbenzene 10.8 ug/kg 9.4 4.4 1 02/15/22 21:19 02/17/22 17:30 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 18.9 15.4 1 02/15/22 21:19 02/17/22 17:30 87-68-3 2-Hexanone ND ug/kg 94.4 9.1 1 02/15/22 21:19 02/17/22 17:30 591-78-6 Isopropylbenzene (Cumene) 6.5J ug/kg 9.4 3.2 1 02/15/22 21:19 02/17/22 17:30 98-82-8 p-Isopropyltoluene ND ug/kg 9.4 4.6 1 02/15/22 21:19 02/17/22 17:30 99-87-6 Methylene Chloride ND ug/kg 37.8 25.9 1 02/15/22 21:19 02/17/22 17:30 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 94.4 9.1 1 02/15/22 21:19 02/17/22 17:30 108-10-1 Methyl-tert-butyl ether ND ug/kg 9.4 3.5 1 02/15/22 21:19 02/17/22 17:30 1634-04-4 Naphthalene 65.3 ug/kg 9.4 5.0 1 02/15/22 21:19 02/17/22 17:30 91-20-3 n-Propylbenzene ND ug/kg 9.4 3.4 1 02/15/22 21:19 02/17/22 17:30 103-65-1 Styrene ND ug/kg 9.4 2.5 1 02/15/22 21:19 02/17/22 17:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 9.4 3.6 1 02/15/22 21:19 02/17/22 17:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 9.4 2.5 1 02/15/22 21:19 02/17/22 17:30 79-34-5 Tetrachloroethene ND ug/kg 9.4 3.0 1 02/15/22 21:19 02/17/22 17:30 127-18-4 Toluene 8.9J ug/kg 9.4 2.7 1 02/15/22 21:19 02/17/22 17:30 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 9.4 7.6 1 02/15/22 21:19 02/17/22 17:30 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 9.4 7.9 1 02/15/22 21:19 02/17/22 17:30 120-82-1 1,1,1-Trichloroethane ND ug/kg 9.4 4.9 1 02/15/22 21:19 02/17/22 17:30 71-55-6 1,1,2-Trichloroethane ND ug/kg 9.4 3.1 1 02/15/22 21:19 02/17/22 17:30 79-00-5 Trichloroethene ND ug/kg 9.4 2.4 1 02/15/22 21:19 02/17/22 17:30 79-01-6 Trichlorofluoromethane ND ug/kg 9.4 5.2 1 02/15/22 21:19 02/17/22 17:30 75-69-4 1,2,3-Trichloropropane ND ug/kg 9.4 4.8 1 02/15/22 21:19 02/17/22 17:30 96-18-4 1,2,4-Trimethylbenzene 76.6 ug/kg 9.4 2.6 1 02/15/22 21:19 02/17/22 17:30 95-63-6 1,3,5-Trimethylbenzene 32.7 ug/kg 9.4 3.2 1 02/15/22 21:19 02/17/22 17:30 108-67-8 Vinyl acetate ND ug/kg 94.4 6.9 1 02/15/22 21:19 02/17/22 17:30 108-05-4 Vinyl chloride ND ug/kg 18.9 4.8 1 02/15/22 21:19 02/17/22 17:30 75-01-4 v2 Xylene (Total) 53.6 ug/kg 18.9 5.4 1 02/15/22 21:19 02/17/22 17:30 1330-20-7 m&p-Xylene 34.9 ug/kg 18.9 6.5 1 02/15/22 21:19 02/17/22 17:30 179601-23-1 o-Xylene 18.7 ug/kg 9.4 4.2 1 02/15/22 21:19 02/17/22 17:30 95-47-6 Surrogates Toluene-d8 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 17:30 2037-26-5 4-Bromofluorobenzene (S) 104 % 69-134 1 02/15/22 21:19 02/17/22 17:30 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 02/15/22 21:19 02/17/22 17:30 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 26.4 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-13 Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 5.2 5.2 1 02/16/22 13:41 02/16/22 17:27 Aliphatic(C09-C12)Adjusted ND mg/kg 5.2 5.2 1 02/16/22 13:41 02/16/22 17:27 Aromatic (C09-C10) ND mg/kg 5.2 5.2 1 02/16/22 13:41 02/16/22 17:27 Surrogates 4-Bromofluorobenzene (FID) (S) 95 % 70-130 1 02/16/22 13:41 02/16/22 17:27 460-00-4 4-Bromofluorobenzene (PID) (S) 81 % 70-130 1 02/16/22 13:41 02/16/22 17:27 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 478 168 1 02/16/22 11:33 02/17/22 12:28 83-32-9 Acenaphthylene ND ug/kg 478 168 1 02/16/22 11:33 02/17/22 12:28 208-96-8 Aniline ND ug/kg 478 187 1 02/16/22 11:33 02/17/22 12:28 62-53-3 Anthracene ND ug/kg 478 156 1 02/16/22 11:33 02/17/22 12:28 120-12-7 Benzo(a)anthracene ND ug/kg 478 159 1 02/16/22 11:33 02/17/22 12:28 56-55-3 Benzo(a)pyrene ND ug/kg 478 165 1 02/16/22 11:33 02/17/22 12:28 50-32-8 Benzo(b)fluoranthene ND ug/kg 478 159 1 02/16/22 11:33 02/17/22 12:28 205-99-2 Benzo(g,h,i)perylene ND ug/kg 478 185 1 02/16/22 11:33 02/17/22 12:28 191-24-2 Benzo(k)fluoranthene ND ug/kg 478 168 1 02/16/22 11:33 02/17/22 12:28 207-08-9 Benzoic Acid ND ug/kg 2390 1030 1 02/16/22 11:33 02/17/22 12:28 65-85-0 Benzyl alcohol ND ug/kg 956 362 1 02/16/22 11:33 02/17/22 12:28 100-51-6 4-Bromophenylphenyl ether ND ug/kg 478 184 1 02/16/22 11:33 02/17/22 12:28 101-55-3 Butylbenzylphthalate ND ug/kg 478 201 1 02/16/22 11:33 02/17/22 12:28 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 956 336 1 02/16/22 11:33 02/17/22 12:28 59-50-7 4-Chloroaniline ND ug/kg 956 375 1 02/16/22 11:33 02/17/22 12:28 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 478 198 1 02/16/22 11:33 02/17/22 12:28 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 478 180 1 02/16/22 11:33 02/17/22 12:28 111-44-4 2-Chloronaphthalene ND ug/kg 478 190 1 02/16/22 11:33 02/17/22 12:28 91-58-7 2-Chlorophenol ND ug/kg 478 180 1 02/16/22 11:33 02/17/22 12:28 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 478 178 1 02/16/22 11:33 02/17/22 12:28 7005-72-3 Chrysene ND ug/kg 478 174 1 02/16/22 11:33 02/17/22 12:28 218-01-9 Dibenz(a,h)anthracene ND ug/kg 478 184 1 02/16/22 11:33 02/17/22 12:28 53-70-3 Dibenzofuran ND ug/kg 478 172 1 02/16/22 11:33 02/17/22 12:28 132-64-9 1,2-Dichlorobenzene ND ug/kg 478 172 1 02/16/22 11:33 02/17/22 12:28 95-50-1 1,3-Dichlorobenzene ND ug/kg 478 169 1 02/16/22 11:33 02/17/22 12:28 541-73-1 1,4-Dichlorobenzene ND ug/kg 478 183 1 02/16/22 11:33 02/17/22 12:28 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 956 323 1 02/16/22 11:33 02/17/22 12:28 91-94-1 2,4-Dichlorophenol ND ug/kg 478 187 1 02/16/22 11:33 02/17/22 12:28 120-83-2 Diethylphthalate ND ug/kg 478 175 1 02/16/22 11:33 02/17/22 12:28 84-66-2 2,4-Dimethylphenol ND ug/kg 478 198 1 02/16/22 11:33 02/17/22 12:28 105-67-9 Dimethylphthalate ND ug/kg 478 174 1 02/16/22 11:33 02/17/22 12:28 131-11-3 Di-n-butylphthalate ND ug/kg 478 161 1 02/16/22 11:33 02/17/22 12:28 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 956 446 1 02/16/22 11:33 02/17/22 12:28 534-52-1 2,4-Dinitrophenol ND ug/kg 2390 1480 1 02/16/22 11:33 02/17/22 12:28 51-28-5 2,4-Dinitrotoluene ND ug/kg 478 184 1 02/16/22 11:33 02/17/22 12:28 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-13 Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 478 175 1 02/16/22 11:33 02/17/22 12:28 606-20-2 Di-n-octylphthalate ND ug/kg 478 188 1 02/16/22 11:33 02/17/22 12:28 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 478 185 1 02/16/22 11:33 02/17/22 12:28 117-81-7 Fluoranthene ND ug/kg 478 164 1 02/16/22 11:33 02/17/22 12:28 206-44-0 Fluorene ND ug/kg 478 168 1 02/16/22 11:33 02/17/22 12:28 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 478 207 1 02/16/22 11:33 02/17/22 12:28 87-68-3 Hexachlorobenzene ND ug/kg 478 187 1 02/16/22 11:33 02/17/22 12:28 118-74-1 Hexachlorocyclopentadiene ND ug/kg 478 274 1 02/16/22 11:33 02/17/22 12:28 77-47-4 Hexachloroethane ND ug/kg 478 183 1 02/16/22 11:33 02/17/22 12:28 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 478 188 1 02/16/22 11:33 02/17/22 12:28 193-39-5 Isophorone ND ug/kg 478 213 1 02/16/22 11:33 02/17/22 12:28 78-59-1 1-Methylnaphthalene ND ug/kg 478 168 1 02/16/22 11:33 02/17/22 12:28 90-12-0 2-Methylnaphthalene ND ug/kg 478 191 1 02/16/22 11:33 02/17/22 12:28 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 478 196 1 02/16/22 11:33 02/17/22 12:28 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 478 193 1 02/16/22 11:33 02/17/22 12:28 15831-10-4 Naphthalene ND ug/kg 478 162 1 02/16/22 11:33 02/17/22 12:28 91-20-3 2-Nitroaniline ND ug/kg 2390 391 1 02/16/22 11:33 02/17/22 12:28 88-74-4 3-Nitroaniline ND ug/kg 2390 375 1 02/16/22 11:33 02/17/22 12:28 99-09-2 4-Nitroaniline ND ug/kg 956 364 1 02/16/22 11:33 02/17/22 12:28 100-01-6 Nitrobenzene ND ug/kg 478 222 1 02/16/22 11:33 02/17/22 12:28 98-95-3 2-Nitrophenol ND ug/kg 478 207 1 02/16/22 11:33 02/17/22 12:28 88-75-5 4-Nitrophenol ND ug/kg 2390 924 1 02/16/22 11:33 02/17/22 12:28 100-02-7 N-Nitrosodimethylamine ND ug/kg 478 161 1 02/16/22 11:33 02/17/22 12:28 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 478 180 1 02/16/22 11:33 02/17/22 12:28 621-64-7 N-Nitrosodiphenylamine ND ug/kg 478 169 1 02/16/22 11:33 02/17/22 12:28 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 478 227 1 02/16/22 11:33 02/17/22 12:28 108-60-1 Pentachlorophenol ND ug/kg 956 468 1 02/16/22 11:33 02/17/22 12:28 87-86-5 Phenanthrene ND ug/kg 478 156 1 02/16/22 11:33 02/17/22 12:28 85-01-8 Phenol ND ug/kg 478 213 1 02/16/22 11:33 02/17/22 12:28 108-95-2 Pyrene ND ug/kg 478 194 1 02/16/22 11:33 02/17/22 12:28 129-00-0 Pyridine ND ug/kg 478 151 1 02/16/22 11:33 02/17/22 12:28 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 478 188 1 02/16/22 11:33 02/17/22 12:28 120-82-1 2,4,5-Trichlorophenol ND ug/kg 478 219 1 02/16/22 11:33 02/17/22 12:28 95-95-4 2,4,6-Trichlorophenol ND ug/kg 478 197 1 02/16/22 11:33 02/17/22 12:28 88-06-2 Surrogates Nitrobenzene-d5 (S) 63 % 21-130 1 02/16/22 11:33 02/17/22 12:28 4165-60-0 2-Fluorobiphenyl (S) 55 % 19-130 1 02/16/22 11:33 02/17/22 12:28 321-60-8 Terphenyl-d14 (S) 54 % 15-130 1 02/16/22 11:33 02/17/22 12:28 1718-51-0 Phenol-d6 (S) 63 % 18-130 1 02/16/22 11:33 02/17/22 12:28 13127-88-3 2-Fluorophenol (S) 61 % 18-130 1 02/16/22 11:33 02/17/22 12:28 367-12-4 2,4,6-Tribromophenol (S) 62 % 18-130 1 02/16/22 11:33 02/17/22 12:28 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-B Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 277 88.9 1 02/15/22 21:19 02/17/22 18:05 67-64-1 Benzene ND ug/kg 13.8 5.5 1 02/15/22 21:19 02/17/22 18:05 71-43-2 Bromobenzene ND ug/kg 13.8 4.5 1 02/15/22 21:19 02/17/22 18:05 108-86-1 Bromochloromethane ND ug/kg 13.8 4.1 1 02/15/22 21:19 02/17/22 18:05 74-97-5 Bromodichloromethane ND ug/kg 13.8 5.3 1 02/15/22 21:19 02/17/22 18:05 75-27-4 Bromoform ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 18:05 75-25-2 Bromomethane ND ug/kg 27.7 21.9 1 02/15/22 21:19 02/17/22 18:05 74-83-9 2-Butanone (MEK) ND ug/kg 277 66.5 1 02/15/22 21:19 02/17/22 18:05 78-93-3 n-Butylbenzene ND ug/kg 13.8 6.5 1 02/15/22 21:19 02/17/22 18:05 104-51-8 sec-Butylbenzene ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 18:05 135-98-8 tert-Butyl benzene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 18:05 98-06-6 Carbon tetrachloride ND ug/kg 13.8 5.2 1 02/15/22 21:19 02/17/22 18:05 56-23-5 Chlorobenzene ND ug/kg 13.8 2.7 1 02/15/22 21:19 02/17/22 18:05 108-90-7 Chloroethane ND ug/kg 27.7 10.7 1 02/15/22 21:19 02/17/22 18:05 75-00-3 Chloroform ND ug/kg 13.8 8.4 1 02/15/22 21:19 02/17/22 18:05 67-66-3 Chloromethane ND ug/kg 27.7 11.6 1 02/15/22 21:19 02/17/22 18:05 74-87-3 2-Chlorotoluene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 18:05 95-49-8 4-Chlorotoluene ND ug/kg 13.8 2.5 1 02/15/22 21:19 02/17/22 18:05 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 13.8 5.4 1 02/15/22 21:19 02/17/22 18:05 96-12-8 Dibromochloromethane ND ug/kg 13.8 7.8 1 02/15/22 21:19 02/17/22 18:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 18:05 106-93-4 Dibromomethane ND ug/kg 13.8 3.0 1 02/15/22 21:19 02/17/22 18:05 74-95-3 1,2-Dichlorobenzene ND ug/kg 13.8 5.0 1 02/15/22 21:19 02/17/22 18:05 95-50-1 1,3-Dichlorobenzene ND ug/kg 13.8 4.3 1 02/15/22 21:19 02/17/22 18:05 541-73-1 1,4-Dichlorobenzene ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 18:05 106-46-7 Dichlorodifluoromethane ND ug/kg 27.7 6.0 1 02/15/22 21:19 02/17/22 18:05 75-71-8 1,1-Dichloroethane ND ug/kg 13.8 5.7 1 02/15/22 21:19 02/17/22 18:05 75-34-3 1,2-Dichloroethane ND ug/kg 13.8 9.2 1 02/15/22 21:19 02/17/22 18:05 107-06-2 1,1-Dichloroethene ND ug/kg 13.8 5.7 1 02/15/22 21:19 02/17/22 18:05 75-35-4 cis-1,2-Dichloroethene ND ug/kg 13.8 4.7 1 02/15/22 21:19 02/17/22 18:05 156-59-2 trans-1,2-Dichloroethene ND ug/kg 13.8 4.8 1 02/15/22 21:19 02/17/22 18:05 156-60-5 1,2-Dichloropropane ND ug/kg 13.8 4.2 1 02/15/22 21:19 02/17/22 18:05 78-87-5 1,3-Dichloropropane ND ug/kg 13.8 4.3 1 02/15/22 21:19 02/17/22 18:05 142-28-9 2,2-Dichloropropane ND ug/kg 13.8 4.5 1 02/15/22 21:19 02/17/22 18:05 594-20-7 1,1-Dichloropropene ND ug/kg 13.8 6.6 1 02/15/22 21:19 02/17/22 18:05 563-58-6 cis-1,3-Dichloropropene ND ug/kg 13.8 3.8 1 02/15/22 21:19 02/17/22 18:05 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 13.8 4.8 1 02/15/22 21:19 02/17/22 18:05 10061-02-6 Diisopropyl ether ND ug/kg 13.8 3.7 1 02/15/22 21:19 02/17/22 18:05 108-20-3 Ethylbenzene ND ug/kg 13.8 6.5 1 02/15/22 21:19 02/17/22 18:05 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 27.7 22.7 1 02/15/22 21:19 02/17/22 18:05 87-68-3 2-Hexanone ND ug/kg 138 13.3 1 02/15/22 21:19 02/17/22 18:05 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 13.8 4.7 1 02/15/22 21:19 02/17/22 18:05 98-82-8 p-Isopropyltoluene ND ug/kg 13.8 6.8 1 02/15/22 21:19 02/17/22 18:05 99-87-6 Methylene Chloride ND ug/kg 55.4 37.9 1 02/15/22 21:19 02/17/22 18:05 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-13 Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 138 13.3 1 02/15/22 21:19 02/17/22 18:05 108-10-1 Methyl-tert-butyl ether ND ug/kg 13.8 5.2 1 02/15/22 21:19 02/17/22 18:05 1634-04-4 Naphthalene ND ug/kg 13.8 7.3 1 02/15/22 21:19 02/17/22 18:05 91-20-3 n-Propylbenzene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 18:05 103-65-1 Styrene ND ug/kg 13.8 3.7 1 02/15/22 21:19 02/17/22 18:05 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 13.8 5.3 1 02/15/22 21:19 02/17/22 18:05 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 13.8 3.7 1 02/15/22 21:19 02/17/22 18:05 79-34-5 Tetrachloroethene ND ug/kg 13.8 4.4 1 02/15/22 21:19 02/17/22 18:05 127-18-4 Toluene ND ug/kg 13.8 3.9 1 02/15/22 21:19 02/17/22 18:05 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 13.8 11.2 1 02/15/22 21:19 02/17/22 18:05 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 13.8 11.6 1 02/15/22 21:19 02/17/22 18:05 120-82-1 1,1,1-Trichloroethane ND ug/kg 13.8 7.2 1 02/15/22 21:19 02/17/22 18:05 71-55-6 1,1,2-Trichloroethane ND ug/kg 13.8 4.6 1 02/15/22 21:19 02/17/22 18:05 79-00-5 Trichloroethene ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 18:05 79-01-6 Trichlorofluoromethane ND ug/kg 13.8 7.6 1 02/15/22 21:19 02/17/22 18:05 75-69-4 1,2,3-Trichloropropane ND ug/kg 13.8 7.0 1 02/15/22 21:19 02/17/22 18:05 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 13.8 3.8 1 02/15/22 21:19 02/17/22 18:05 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 13.8 4.7 1 02/15/22 21:19 02/17/22 18:05 108-67-8 Vinyl acetate ND ug/kg 138 10.1 1 02/15/22 21:19 02/17/22 18:05 108-05-4 Vinyl chloride ND ug/kg 27.7 7.0 1 02/15/22 21:19 02/17/22 18:05 75-01-4 v2 Xylene (Total) ND ug/kg 27.7 7.9 1 02/15/22 21:19 02/17/22 18:05 1330-20-7 m&p-Xylene ND ug/kg 27.7 9.5 1 02/15/22 21:19 02/17/22 18:05 179601-23-1 o-Xylene ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 18:05 95-47-6 Surrogates Toluene-d8 (S) 100 % 70-130 1 02/15/22 21:19 02/17/22 18:05 2037-26-5 4-Bromofluorobenzene (S) 99 % 69-134 1 02/15/22 21:19 02/17/22 18:05 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 18:05 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 30.3 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 6.7 6.7 1 02/16/22 13:41 02/16/22 17:55 Aliphatic(C09-C12)Adjusted ND mg/kg 6.7 6.7 1 02/16/22 13:41 02/16/22 17:55 Aromatic (C09-C10) ND mg/kg 6.7 6.7 1 02/16/22 13:41 02/16/22 17:55 Surrogates 4-Bromofluorobenzene (FID) (S) 96 % 70-130 1 02/16/22 13:41 02/16/22 17:55 460-00-4 4-Bromofluorobenzene (PID) (S) 82 % 70-130 1 02/16/22 13:41 02/16/22 17:55 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 484 170 1 02/16/22 11:33 02/17/22 12:55 83-32-9 Acenaphthylene ND ug/kg 484 170 1 02/16/22 11:33 02/17/22 12:55 208-96-8 Aniline ND ug/kg 484 189 1 02/16/22 11:33 02/17/22 12:55 62-53-3 Anthracene ND ug/kg 484 158 1 02/16/22 11:33 02/17/22 12:55 120-12-7 Benzo(a)anthracene ND ug/kg 484 161 1 02/16/22 11:33 02/17/22 12:55 56-55-3 Benzo(a)pyrene ND ug/kg 484 167 1 02/16/22 11:33 02/17/22 12:55 50-32-8 Benzo(b)fluoranthene ND ug/kg 484 161 1 02/16/22 11:33 02/17/22 12:55 205-99-2 Benzo(g,h,i)perylene ND ug/kg 484 188 1 02/16/22 11:33 02/17/22 12:55 191-24-2 Benzo(k)fluoranthene ND ug/kg 484 170 1 02/16/22 11:33 02/17/22 12:55 207-08-9 Benzoic Acid ND ug/kg 2420 1040 1 02/16/22 11:33 02/17/22 12:55 65-85-0 Benzyl alcohol ND ug/kg 967 366 1 02/16/22 11:33 02/17/22 12:55 100-51-6 4-Bromophenylphenyl ether ND ug/kg 484 186 1 02/16/22 11:33 02/17/22 12:55 101-55-3 Butylbenzylphthalate ND ug/kg 484 204 1 02/16/22 11:33 02/17/22 12:55 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 967 340 1 02/16/22 11:33 02/17/22 12:55 59-50-7 4-Chloroaniline ND ug/kg 967 380 1 02/16/22 11:33 02/17/22 12:55 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 484 201 1 02/16/22 11:33 02/17/22 12:55 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 484 182 1 02/16/22 11:33 02/17/22 12:55 111-44-4 2-Chloronaphthalene ND ug/kg 484 192 1 02/16/22 11:33 02/17/22 12:55 91-58-7 2-Chlorophenol ND ug/kg 484 182 1 02/16/22 11:33 02/17/22 12:55 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 484 180 1 02/16/22 11:33 02/17/22 12:55 7005-72-3 Chrysene ND ug/kg 484 176 1 02/16/22 11:33 02/17/22 12:55 218-01-9 Dibenz(a,h)anthracene ND ug/kg 484 186 1 02/16/22 11:33 02/17/22 12:55 53-70-3 Dibenzofuran ND ug/kg 484 174 1 02/16/22 11:33 02/17/22 12:55 132-64-9 1,2-Dichlorobenzene ND ug/kg 484 174 1 02/16/22 11:33 02/17/22 12:55 95-50-1 1,3-Dichlorobenzene ND ug/kg 484 172 1 02/16/22 11:33 02/17/22 12:55 541-73-1 1,4-Dichlorobenzene ND ug/kg 484 185 1 02/16/22 11:33 02/17/22 12:55 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 967 327 1 02/16/22 11:33 02/17/22 12:55 91-94-1 2,4-Dichlorophenol ND ug/kg 484 189 1 02/16/22 11:33 02/17/22 12:55 120-83-2 Diethylphthalate ND ug/kg 484 177 1 02/16/22 11:33 02/17/22 12:55 84-66-2 2,4-Dimethylphenol ND ug/kg 484 201 1 02/16/22 11:33 02/17/22 12:55 105-67-9 Dimethylphthalate ND ug/kg 484 176 1 02/16/22 11:33 02/17/22 12:55 131-11-3 Di-n-butylphthalate ND ug/kg 484 163 1 02/16/22 11:33 02/17/22 12:55 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 967 451 1 02/16/22 11:33 02/17/22 12:55 534-52-1 2,4-Dinitrophenol ND ug/kg 2420 1500 1 02/16/22 11:33 02/17/22 12:55 51-28-5 2,4-Dinitrotoluene ND ug/kg 484 186 1 02/16/22 11:33 02/17/22 12:55 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 484 177 1 02/16/22 11:33 02/17/22 12:55 606-20-2 Di-n-octylphthalate ND ug/kg 484 191 1 02/16/22 11:33 02/17/22 12:55 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 484 188 1 02/16/22 11:33 02/17/22 12:55 117-81-7 Fluoranthene ND ug/kg 484 166 1 02/16/22 11:33 02/17/22 12:55 206-44-0 Fluorene ND ug/kg 484 170 1 02/16/22 11:33 02/17/22 12:55 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 484 210 1 02/16/22 11:33 02/17/22 12:55 87-68-3 Hexachlorobenzene ND ug/kg 484 189 1 02/16/22 11:33 02/17/22 12:55 118-74-1 Hexachlorocyclopentadiene ND ug/kg 484 277 1 02/16/22 11:33 02/17/22 12:55 77-47-4 Hexachloroethane ND ug/kg 484 185 1 02/16/22 11:33 02/17/22 12:55 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 484 191 1 02/16/22 11:33 02/17/22 12:55 193-39-5 Isophorone ND ug/kg 484 215 1 02/16/22 11:33 02/17/22 12:55 78-59-1 1-Methylnaphthalene ND ug/kg 484 170 1 02/16/22 11:33 02/17/22 12:55 90-12-0 2-Methylnaphthalene ND ug/kg 484 193 1 02/16/22 11:33 02/17/22 12:55 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 484 198 1 02/16/22 11:33 02/17/22 12:55 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 484 195 1 02/16/22 11:33 02/17/22 12:55 15831-10-4 Naphthalene ND ug/kg 484 164 1 02/16/22 11:33 02/17/22 12:55 91-20-3 2-Nitroaniline ND ug/kg 2420 396 1 02/16/22 11:33 02/17/22 12:55 88-74-4 3-Nitroaniline ND ug/kg 2420 380 1 02/16/22 11:33 02/17/22 12:55 99-09-2 4-Nitroaniline ND ug/kg 967 368 1 02/16/22 11:33 02/17/22 12:55 100-01-6 Nitrobenzene ND ug/kg 484 224 1 02/16/22 11:33 02/17/22 12:55 98-95-3 2-Nitrophenol ND ug/kg 484 210 1 02/16/22 11:33 02/17/22 12:55 88-75-5 4-Nitrophenol ND ug/kg 2420 935 1 02/16/22 11:33 02/17/22 12:55 100-02-7 N-Nitrosodimethylamine ND ug/kg 484 163 1 02/16/22 11:33 02/17/22 12:55 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 484 182 1 02/16/22 11:33 02/17/22 12:55 621-64-7 N-Nitrosodiphenylamine ND ug/kg 484 172 1 02/16/22 11:33 02/17/22 12:55 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 484 230 1 02/16/22 11:33 02/17/22 12:55 108-60-1 Pentachlorophenol ND ug/kg 967 473 1 02/16/22 11:33 02/17/22 12:55 87-86-5 Phenanthrene ND ug/kg 484 158 1 02/16/22 11:33 02/17/22 12:55 85-01-8 Phenol ND ug/kg 484 215 1 02/16/22 11:33 02/17/22 12:55 108-95-2 Pyrene ND ug/kg 484 196 1 02/16/22 11:33 02/17/22 12:55 129-00-0 Pyridine ND ug/kg 484 152 1 02/16/22 11:33 02/17/22 12:55 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 484 191 1 02/16/22 11:33 02/17/22 12:55 120-82-1 2,4,5-Trichlorophenol ND ug/kg 484 221 1 02/16/22 11:33 02/17/22 12:55 95-95-4 2,4,6-Trichlorophenol ND ug/kg 484 199 1 02/16/22 11:33 02/17/22 12:55 88-06-2 Surrogates Nitrobenzene-d5 (S) 62 % 21-130 1 02/16/22 11:33 02/17/22 12:55 4165-60-0 2-Fluorobiphenyl (S) 52 % 19-130 1 02/16/22 11:33 02/17/22 12:55 321-60-8 Terphenyl-d14 (S) 52 % 15-130 1 02/16/22 11:33 02/17/22 12:55 1718-51-0 Phenol-d6 (S) 61 % 18-130 1 02/16/22 11:33 02/17/22 12:55 13127-88-3 2-Fluorophenol (S) 59 % 18-130 1 02/16/22 11:33 02/17/22 12:55 367-12-4 2,4,6-Tribromophenol (S) 53 % 18-130 1 02/16/22 11:33 02/17/22 12:55 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 207 66.6 1 02/15/22 21:19 02/17/22 18:23 67-64-1 Benzene ND ug/kg 10.4 4.1 1 02/15/22 21:19 02/17/22 18:23 71-43-2 Bromobenzene ND ug/kg 10.4 3.4 1 02/15/22 21:19 02/17/22 18:23 108-86-1 Bromochloromethane ND ug/kg 10.4 3.1 1 02/15/22 21:19 02/17/22 18:23 74-97-5 Bromodichloromethane ND ug/kg 10.4 4.0 1 02/15/22 21:19 02/17/22 18:23 75-27-4 Bromoform ND ug/kg 10.4 3.7 1 02/15/22 21:19 02/17/22 18:23 75-25-2 Bromomethane ND ug/kg 20.7 16.4 1 02/15/22 21:19 02/17/22 18:23 74-83-9 2-Butanone (MEK) ND ug/kg 207 49.8 1 02/15/22 21:19 02/17/22 18:23 78-93-3 n-Butylbenzene ND ug/kg 10.4 4.9 1 02/15/22 21:19 02/17/22 18:23 104-51-8 sec-Butylbenzene ND ug/kg 10.4 4.6 1 02/15/22 21:19 02/17/22 18:23 135-98-8 tert-Butyl benzene ND ug/kg 10.4 3.7 1 02/15/22 21:19 02/17/22 18:23 98-06-6 Carbon tetrachloride ND ug/kg 10.4 3.9 1 02/15/22 21:19 02/17/22 18:23 56-23-5 Chlorobenzene ND ug/kg 10.4 2.0 1 02/15/22 21:19 02/17/22 18:23 108-90-7 Chloroethane ND ug/kg 20.7 8.0 1 02/15/22 21:19 02/17/22 18:23 75-00-3 Chloroform ND ug/kg 10.4 6.3 1 02/15/22 21:19 02/17/22 18:23 67-66-3 Chloromethane ND ug/kg 20.7 8.7 1 02/15/22 21:19 02/17/22 18:23 74-87-3 2-Chlorotoluene ND ug/kg 10.4 3.7 1 02/15/22 21:19 02/17/22 18:23 95-49-8 4-Chlorotoluene ND ug/kg 10.4 1.8 1 02/15/22 21:19 02/17/22 18:23 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 10.4 4.0 1 02/15/22 21:19 02/17/22 18:23 96-12-8 Dibromochloromethane ND ug/kg 10.4 5.8 1 02/15/22 21:19 02/17/22 18:23 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 10.4 4.6 1 02/15/22 21:19 02/17/22 18:23 106-93-4 Dibromomethane ND ug/kg 10.4 2.2 1 02/15/22 21:19 02/17/22 18:23 74-95-3 1,2-Dichlorobenzene ND ug/kg 10.4 3.7 1 02/15/22 21:19 02/17/22 18:23 95-50-1 1,3-Dichlorobenzene ND ug/kg 10.4 3.2 1 02/15/22 21:19 02/17/22 18:23 541-73-1 1,4-Dichlorobenzene ND ug/kg 10.4 2.7 1 02/15/22 21:19 02/17/22 18:23 106-46-7 Dichlorodifluoromethane ND ug/kg 20.7 4.5 1 02/15/22 21:19 02/17/22 18:23 75-71-8 1,1-Dichloroethane ND ug/kg 10.4 4.3 1 02/15/22 21:19 02/17/22 18:23 75-34-3 1,2-Dichloroethane ND ug/kg 10.4 6.9 1 02/15/22 21:19 02/17/22 18:23 107-06-2 1,1-Dichloroethene ND ug/kg 10.4 4.3 1 02/15/22 21:19 02/17/22 18:23 75-35-4 cis-1,2-Dichloroethene ND ug/kg 10.4 3.5 1 02/15/22 21:19 02/17/22 18:23 156-59-2 trans-1,2-Dichloroethene ND ug/kg 10.4 3.6 1 02/15/22 21:19 02/17/22 18:23 156-60-5 1,2-Dichloropropane ND ug/kg 10.4 3.1 1 02/15/22 21:19 02/17/22 18:23 78-87-5 1,3-Dichloropropane ND ug/kg 10.4 3.2 1 02/15/22 21:19 02/17/22 18:23 142-28-9 2,2-Dichloropropane ND ug/kg 10.4 3.4 1 02/15/22 21:19 02/17/22 18:23 594-20-7 1,1-Dichloropropene ND ug/kg 10.4 5.0 1 02/15/22 21:19 02/17/22 18:23 563-58-6 cis-1,3-Dichloropropene ND ug/kg 10.4 2.8 1 02/15/22 21:19 02/17/22 18:23 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 10.4 3.6 1 02/15/22 21:19 02/17/22 18:23 10061-02-6 Diisopropyl ether ND ug/kg 10.4 2.8 1 02/15/22 21:19 02/17/22 18:23 108-20-3 Ethylbenzene ND ug/kg 10.4 4.8 1 02/15/22 21:19 02/17/22 18:23 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 20.7 17.0 1 02/15/22 21:19 02/17/22 18:23 87-68-3 2-Hexanone ND ug/kg 104 10.0 1 02/15/22 21:19 02/17/22 18:23 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 10.4 3.5 1 02/15/22 21:19 02/17/22 18:23 98-82-8 p-Isopropyltoluene ND ug/kg 10.4 5.1 1 02/15/22 21:19 02/17/22 18:23 99-87-6 Methylene Chloride ND ug/kg 41.5 28.4 1 02/15/22 21:19 02/17/22 18:23 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 104 10.0 1 02/15/22 21:19 02/17/22 18:23 108-10-1 Methyl-tert-butyl ether ND ug/kg 10.4 3.9 1 02/15/22 21:19 02/17/22 18:23 1634-04-4 Naphthalene ND ug/kg 10.4 5.5 1 02/15/22 21:19 02/17/22 18:23 91-20-3 n-Propylbenzene ND ug/kg 10.4 3.7 1 02/15/22 21:19 02/17/22 18:23 103-65-1 Styrene ND ug/kg 10.4 2.7 1 02/15/22 21:19 02/17/22 18:23 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 10.4 4.0 1 02/15/22 21:19 02/17/22 18:23 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 10.4 2.7 1 02/15/22 21:19 02/17/22 18:23 79-34-5 Tetrachloroethene ND ug/kg 10.4 3.3 1 02/15/22 21:19 02/17/22 18:23 127-18-4 Toluene 8.9J ug/kg 10.4 2.9 1 02/15/22 21:19 02/17/22 18:23 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 10.4 8.4 1 02/15/22 21:19 02/17/22 18:23 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 10.4 8.7 1 02/15/22 21:19 02/17/22 18:23 120-82-1 1,1,1-Trichloroethane ND ug/kg 10.4 5.4 1 02/15/22 21:19 02/17/22 18:23 71-55-6 1,1,2-Trichloroethane ND ug/kg 10.4 3.4 1 02/15/22 21:19 02/17/22 18:23 79-00-5 Trichloroethene ND ug/kg 10.4 2.7 1 02/15/22 21:19 02/17/22 18:23 79-01-6 Trichlorofluoromethane ND ug/kg 10.4 5.7 1 02/15/22 21:19 02/17/22 18:23 75-69-4 1,2,3-Trichloropropane ND ug/kg 10.4 5.2 1 02/15/22 21:19 02/17/22 18:23 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 10.4 2.8 1 02/15/22 21:19 02/17/22 18:23 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 10.4 3.5 1 02/15/22 21:19 02/17/22 18:23 108-67-8 Vinyl acetate ND ug/kg 104 7.6 1 02/15/22 21:19 02/17/22 18:23 108-05-4 Vinyl chloride ND ug/kg 20.7 5.3 1 02/15/22 21:19 02/17/22 18:23 75-01-4 v2 Xylene (Total) ND ug/kg 20.7 5.9 1 02/15/22 21:19 02/17/22 18:23 1330-20-7 m&p-Xylene ND ug/kg 20.7 7.1 1 02/15/22 21:19 02/17/22 18:23 179601-23-1 o-Xylene ND ug/kg 10.4 4.6 1 02/15/22 21:19 02/17/22 18:23 95-47-6 Surrogates Toluene-d8 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 18:23 2037-26-5 4-Bromofluorobenzene (S) 98 % 69-134 1 02/15/22 21:19 02/17/22 18:23 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 02/15/22 21:19 02/17/22 18:23 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 30.9 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 6.2 6.2 1 02/16/22 13:41 02/16/22 18:24 Aliphatic(C09-C12)Adjusted ND mg/kg 6.2 6.2 1 02/16/22 13:41 02/16/22 18:24 Aromatic (C09-C10) ND mg/kg 6.2 6.2 1 02/16/22 13:41 02/16/22 18:24 Surrogates 4-Bromofluorobenzene (FID) (S) 96 % 70-130 1 02/16/22 13:41 02/16/22 18:24 460-00-4 4-Bromofluorobenzene (PID) (S) 83 % 70-130 1 02/16/22 13:41 02/16/22 18:24 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 465 164 1 02/16/22 11:33 02/17/22 13:21 83-32-9 Acenaphthylene ND ug/kg 465 164 1 02/16/22 11:33 02/17/22 13:21 208-96-8 Aniline ND ug/kg 465 182 1 02/16/22 11:33 02/17/22 13:21 62-53-3 Anthracene ND ug/kg 465 152 1 02/16/22 11:33 02/17/22 13:21 120-12-7 Benzo(a)anthracene ND ug/kg 465 155 1 02/16/22 11:33 02/17/22 13:21 56-55-3 Benzo(a)pyrene ND ug/kg 465 161 1 02/16/22 11:33 02/17/22 13:21 50-32-8 Benzo(b)fluoranthene ND ug/kg 465 155 1 02/16/22 11:33 02/17/22 13:21 205-99-2 Benzo(g,h,i)perylene ND ug/kg 465 180 1 02/16/22 11:33 02/17/22 13:21 191-24-2 Benzo(k)fluoranthene ND ug/kg 465 164 1 02/16/22 11:33 02/17/22 13:21 207-08-9 Benzoic Acid ND ug/kg 2330 999 1 02/16/22 11:33 02/17/22 13:21 65-85-0 Benzyl alcohol ND ug/kg 930 352 1 02/16/22 11:33 02/17/22 13:21 100-51-6 4-Bromophenylphenyl ether ND ug/kg 465 179 1 02/16/22 11:33 02/17/22 13:21 101-55-3 Butylbenzylphthalate ND ug/kg 465 196 1 02/16/22 11:33 02/17/22 13:21 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 930 327 1 02/16/22 11:33 02/17/22 13:21 59-50-7 4-Chloroaniline ND ug/kg 930 365 1 02/16/22 11:33 02/17/22 13:21 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 465 193 1 02/16/22 11:33 02/17/22 13:21 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 465 175 1 02/16/22 11:33 02/17/22 13:21 111-44-4 2-Chloronaphthalene ND ug/kg 465 185 1 02/16/22 11:33 02/17/22 13:21 91-58-7 2-Chlorophenol ND ug/kg 465 175 1 02/16/22 11:33 02/17/22 13:21 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 465 173 1 02/16/22 11:33 02/17/22 13:21 7005-72-3 Chrysene ND ug/kg 465 169 1 02/16/22 11:33 02/17/22 13:21 218-01-9 Dibenz(a,h)anthracene ND ug/kg 465 179 1 02/16/22 11:33 02/17/22 13:21 53-70-3 Dibenzofuran ND ug/kg 465 168 1 02/16/22 11:33 02/17/22 13:21 132-64-9 1,2-Dichlorobenzene ND ug/kg 465 168 1 02/16/22 11:33 02/17/22 13:21 95-50-1 1,3-Dichlorobenzene ND ug/kg 465 165 1 02/16/22 11:33 02/17/22 13:21 541-73-1 1,4-Dichlorobenzene ND ug/kg 465 178 1 02/16/22 11:33 02/17/22 13:21 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 930 314 1 02/16/22 11:33 02/17/22 13:21 91-94-1 2,4-Dichlorophenol ND ug/kg 465 182 1 02/16/22 11:33 02/17/22 13:21 120-83-2 Diethylphthalate ND ug/kg 465 171 1 02/16/22 11:33 02/17/22 13:21 84-66-2 2,4-Dimethylphenol ND ug/kg 465 193 1 02/16/22 11:33 02/17/22 13:21 105-67-9 Dimethylphthalate ND ug/kg 465 169 1 02/16/22 11:33 02/17/22 13:21 131-11-3 Di-n-butylphthalate ND ug/kg 465 156 1 02/16/22 11:33 02/17/22 13:21 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 930 434 1 02/16/22 11:33 02/17/22 13:21 534-52-1 2,4-Dinitrophenol ND ug/kg 2330 1440 1 02/16/22 11:33 02/17/22 13:21 51-28-5 2,4-Dinitrotoluene ND ug/kg 465 179 1 02/16/22 11:33 02/17/22 13:21 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 465 171 1 02/16/22 11:33 02/17/22 13:21 606-20-2 Di-n-octylphthalate ND ug/kg 465 183 1 02/16/22 11:33 02/17/22 13:21 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 465 180 1 02/16/22 11:33 02/17/22 13:21 117-81-7 Fluoranthene ND ug/kg 465 159 1 02/16/22 11:33 02/17/22 13:21 206-44-0 Fluorene ND ug/kg 465 164 1 02/16/22 11:33 02/17/22 13:21 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 465 202 1 02/16/22 11:33 02/17/22 13:21 87-68-3 Hexachlorobenzene ND ug/kg 465 182 1 02/16/22 11:33 02/17/22 13:21 118-74-1 Hexachlorocyclopentadiene ND ug/kg 465 266 1 02/16/22 11:33 02/17/22 13:21 77-47-4 Hexachloroethane ND ug/kg 465 178 1 02/16/22 11:33 02/17/22 13:21 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 465 183 1 02/16/22 11:33 02/17/22 13:21 193-39-5 Isophorone ND ug/kg 465 207 1 02/16/22 11:33 02/17/22 13:21 78-59-1 1-Methylnaphthalene ND ug/kg 465 164 1 02/16/22 11:33 02/17/22 13:21 90-12-0 2-Methylnaphthalene ND ug/kg 465 186 1 02/16/22 11:33 02/17/22 13:21 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 465 190 1 02/16/22 11:33 02/17/22 13:21 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 465 187 1 02/16/22 11:33 02/17/22 13:21 15831-10-4 Naphthalene ND ug/kg 465 158 1 02/16/22 11:33 02/17/22 13:21 91-20-3 2-Nitroaniline ND ug/kg 2330 381 1 02/16/22 11:33 02/17/22 13:21 88-74-4 3-Nitroaniline ND ug/kg 2330 365 1 02/16/22 11:33 02/17/22 13:21 99-09-2 4-Nitroaniline ND ug/kg 930 354 1 02/16/22 11:33 02/17/22 13:21 100-01-6 Nitrobenzene ND ug/kg 465 216 1 02/16/22 11:33 02/17/22 13:21 98-95-3 2-Nitrophenol ND ug/kg 465 202 1 02/16/22 11:33 02/17/22 13:21 88-75-5 4-Nitrophenol ND ug/kg 2330 899 1 02/16/22 11:33 02/17/22 13:21 100-02-7 N-Nitrosodimethylamine ND ug/kg 465 156 1 02/16/22 11:33 02/17/22 13:21 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 465 175 1 02/16/22 11:33 02/17/22 13:21 621-64-7 N-Nitrosodiphenylamine ND ug/kg 465 165 1 02/16/22 11:33 02/17/22 13:21 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 465 221 1 02/16/22 11:33 02/17/22 13:21 108-60-1 Pentachlorophenol ND ug/kg 930 455 1 02/16/22 11:33 02/17/22 13:21 87-86-5 Phenanthrene ND ug/kg 465 152 1 02/16/22 11:33 02/17/22 13:21 85-01-8 Phenol ND ug/kg 465 207 1 02/16/22 11:33 02/17/22 13:21 108-95-2 Pyrene ND ug/kg 465 189 1 02/16/22 11:33 02/17/22 13:21 129-00-0 Pyridine ND ug/kg 465 147 1 02/16/22 11:33 02/17/22 13:21 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 465 183 1 02/16/22 11:33 02/17/22 13:21 120-82-1 2,4,5-Trichlorophenol ND ug/kg 465 213 1 02/16/22 11:33 02/17/22 13:21 95-95-4 2,4,6-Trichlorophenol ND ug/kg 465 192 1 02/16/22 11:33 02/17/22 13:21 88-06-2 Surrogates Nitrobenzene-d5 (S) 53 % 21-130 1 02/16/22 11:33 02/17/22 13:21 4165-60-0 2-Fluorobiphenyl (S) 50 % 19-130 1 02/16/22 11:33 02/17/22 13:21 321-60-8 Terphenyl-d14 (S) 48 % 15-130 1 02/16/22 11:33 02/17/22 13:21 1718-51-0 Phenol-d6 (S) 54 % 18-130 1 02/16/22 11:33 02/17/22 13:21 13127-88-3 2-Fluorophenol (S) 52 % 18-130 1 02/16/22 11:33 02/17/22 13:21 367-12-4 2,4,6-Tribromophenol (S) 54 % 18-130 1 02/16/22 11:33 02/17/22 13:21 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 218 69.9 1 02/15/22 21:19 02/17/22 18:40 67-64-1 Benzene ND ug/kg 10.9 4.3 1 02/15/22 21:19 02/17/22 18:40 71-43-2 Bromobenzene ND ug/kg 10.9 3.5 1 02/15/22 21:19 02/17/22 18:40 108-86-1 Bromochloromethane ND ug/kg 10.9 3.2 1 02/15/22 21:19 02/17/22 18:40 74-97-5 Bromodichloromethane ND ug/kg 10.9 4.2 1 02/15/22 21:19 02/17/22 18:40 75-27-4 Bromoform ND ug/kg 10.9 3.8 1 02/15/22 21:19 02/17/22 18:40 75-25-2 Bromomethane ND ug/kg 21.8 17.2 1 02/15/22 21:19 02/17/22 18:40 74-83-9 2-Butanone (MEK) ND ug/kg 218 52.2 1 02/15/22 21:19 02/17/22 18:40 78-93-3 n-Butylbenzene ND ug/kg 10.9 5.1 1 02/15/22 21:19 02/17/22 18:40 104-51-8 sec-Butylbenzene ND ug/kg 10.9 4.8 1 02/15/22 21:19 02/17/22 18:40 135-98-8 tert-Butyl benzene ND ug/kg 10.9 3.9 1 02/15/22 21:19 02/17/22 18:40 98-06-6 Carbon tetrachloride ND ug/kg 10.9 4.1 1 02/15/22 21:19 02/17/22 18:40 56-23-5 Chlorobenzene ND ug/kg 10.9 2.1 1 02/15/22 21:19 02/17/22 18:40 108-90-7 Chloroethane ND ug/kg 21.8 8.4 1 02/15/22 21:19 02/17/22 18:40 75-00-3 Chloroform ND ug/kg 10.9 6.6 1 02/15/22 21:19 02/17/22 18:40 67-66-3 Chloromethane ND ug/kg 21.8 9.1 1 02/15/22 21:19 02/17/22 18:40 74-87-3 2-Chlorotoluene ND ug/kg 10.9 3.9 1 02/15/22 21:19 02/17/22 18:40 95-49-8 4-Chlorotoluene ND ug/kg 10.9 1.9 1 02/15/22 21:19 02/17/22 18:40 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 10.9 4.2 1 02/15/22 21:19 02/17/22 18:40 96-12-8 Dibromochloromethane ND ug/kg 10.9 6.1 1 02/15/22 21:19 02/17/22 18:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 10.9 4.8 1 02/15/22 21:19 02/17/22 18:40 106-93-4 Dibromomethane ND ug/kg 10.9 2.3 1 02/15/22 21:19 02/17/22 18:40 74-95-3 1,2-Dichlorobenzene ND ug/kg 10.9 3.9 1 02/15/22 21:19 02/17/22 18:40 95-50-1 1,3-Dichlorobenzene ND ug/kg 10.9 3.4 1 02/15/22 21:19 02/17/22 18:40 541-73-1 1,4-Dichlorobenzene ND ug/kg 10.9 2.8 1 02/15/22 21:19 02/17/22 18:40 106-46-7 Dichlorodifluoromethane ND ug/kg 21.8 4.7 1 02/15/22 21:19 02/17/22 18:40 75-71-8 1,1-Dichloroethane ND ug/kg 10.9 4.5 1 02/15/22 21:19 02/17/22 18:40 75-34-3 1,2-Dichloroethane ND ug/kg 10.9 7.2 1 02/15/22 21:19 02/17/22 18:40 107-06-2 1,1-Dichloroethene ND ug/kg 10.9 4.5 1 02/15/22 21:19 02/17/22 18:40 75-35-4 cis-1,2-Dichloroethene ND ug/kg 10.9 3.7 1 02/15/22 21:19 02/17/22 18:40 156-59-2 trans-1,2-Dichloroethene ND ug/kg 10.9 3.8 1 02/15/22 21:19 02/17/22 18:40 156-60-5 1,2-Dichloropropane ND ug/kg 10.9 3.3 1 02/15/22 21:19 02/17/22 18:40 78-87-5 1,3-Dichloropropane ND ug/kg 10.9 3.4 1 02/15/22 21:19 02/17/22 18:40 142-28-9 2,2-Dichloropropane ND ug/kg 10.9 3.5 1 02/15/22 21:19 02/17/22 18:40 594-20-7 1,1-Dichloropropene ND ug/kg 10.9 5.2 1 02/15/22 21:19 02/17/22 18:40 563-58-6 cis-1,3-Dichloropropene ND ug/kg 10.9 3.0 1 02/15/22 21:19 02/17/22 18:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 10.9 3.7 1 02/15/22 21:19 02/17/22 18:40 10061-02-6 Diisopropyl ether ND ug/kg 10.9 2.9 1 02/15/22 21:19 02/17/22 18:40 108-20-3 Ethylbenzene ND ug/kg 10.9 5.1 1 02/15/22 21:19 02/17/22 18:40 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 21.8 17.8 1 02/15/22 21:19 02/17/22 18:40 87-68-3 2-Hexanone ND ug/kg 109 10.5 1 02/15/22 21:19 02/17/22 18:40 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 10.9 3.7 1 02/15/22 21:19 02/17/22 18:40 98-82-8 p-Isopropyltoluene ND ug/kg 10.9 5.4 1 02/15/22 21:19 02/17/22 18:40 99-87-6 Methylene Chloride ND ug/kg 43.5 29.8 1 02/15/22 21:19 02/17/22 18:40 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 109 10.5 1 02/15/22 21:19 02/17/22 18:40 108-10-1 Methyl-tert-butyl ether ND ug/kg 10.9 4.1 1 02/15/22 21:19 02/17/22 18:40 1634-04-4 Naphthalene ND ug/kg 10.9 5.7 1 02/15/22 21:19 02/17/22 18:40 91-20-3 n-Propylbenzene ND ug/kg 10.9 3.9 1 02/15/22 21:19 02/17/22 18:40 103-65-1 Styrene ND ug/kg 10.9 2.9 1 02/15/22 21:19 02/17/22 18:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 10.9 4.2 1 02/15/22 21:19 02/17/22 18:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 10.9 2.9 1 02/15/22 21:19 02/17/22 18:40 79-34-5 Tetrachloroethene ND ug/kg 10.9 3.4 1 02/15/22 21:19 02/17/22 18:40 127-18-4 Toluene ND ug/kg 10.9 3.1 1 02/15/22 21:19 02/17/22 18:40 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 10.9 8.8 1 02/15/22 21:19 02/17/22 18:40 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 10.9 9.1 1 02/15/22 21:19 02/17/22 18:40 120-82-1 1,1,1-Trichloroethane ND ug/kg 10.9 5.7 1 02/15/22 21:19 02/17/22 18:40 71-55-6 1,1,2-Trichloroethane ND ug/kg 10.9 3.6 1 02/15/22 21:19 02/17/22 18:40 79-00-5 Trichloroethene ND ug/kg 10.9 2.8 1 02/15/22 21:19 02/17/22 18:40 79-01-6 Trichlorofluoromethane ND ug/kg 10.9 6.0 1 02/15/22 21:19 02/17/22 18:40 75-69-4 1,2,3-Trichloropropane ND ug/kg 10.9 5.5 1 02/15/22 21:19 02/17/22 18:40 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 10.9 3.0 1 02/15/22 21:19 02/17/22 18:40 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 10.9 3.7 1 02/15/22 21:19 02/17/22 18:40 108-67-8 Vinyl acetate ND ug/kg 109 7.9 1 02/15/22 21:19 02/17/22 18:40 108-05-4 Vinyl chloride ND ug/kg 21.8 5.5 1 02/15/22 21:19 02/17/22 18:40 75-01-4 v2 Xylene (Total) ND ug/kg 21.8 6.2 1 02/15/22 21:19 02/17/22 18:40 1330-20-7 m&p-Xylene ND ug/kg 21.8 7.4 1 02/15/22 21:19 02/17/22 18:40 179601-23-1 o-Xylene ND ug/kg 10.9 4.8 1 02/15/22 21:19 02/17/22 18:40 95-47-6 Surrogates Toluene-d8 (S) 100 % 70-130 1 02/15/22 21:19 02/17/22 18:40 2037-26-5 4-Bromofluorobenzene (S) 99 % 69-134 1 02/15/22 21:19 02/17/22 18:40 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 02/15/22 21:19 02/17/22 18:40 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 28.8 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 4.7 4.7 1 02/16/22 13:41 02/16/22 18:53 Aliphatic(C09-C12)Adjusted ND mg/kg 4.7 4.7 1 02/16/22 13:41 02/16/22 18:53 Aromatic (C09-C10) ND mg/kg 4.7 4.7 1 02/16/22 13:41 02/16/22 18:53 Surrogates 4-Bromofluorobenzene (FID) (S) 99 % 70-130 1 02/16/22 13:41 02/16/22 18:53 460-00-4 4-Bromofluorobenzene (PID) (S) 85 % 70-130 1 02/16/22 13:41 02/16/22 18:53 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 438 154 1 02/16/22 11:33 02/17/22 13:48 83-32-9 Acenaphthylene ND ug/kg 438 154 1 02/16/22 11:33 02/17/22 13:48 208-96-8 Aniline ND ug/kg 438 171 1 02/16/22 11:33 02/17/22 13:48 62-53-3 Anthracene ND ug/kg 438 143 1 02/16/22 11:33 02/17/22 13:48 120-12-7 Benzo(a)anthracene ND ug/kg 438 146 1 02/16/22 11:33 02/17/22 13:48 56-55-3 Benzo(a)pyrene ND ug/kg 438 151 1 02/16/22 11:33 02/17/22 13:48 50-32-8 Benzo(b)fluoranthene ND ug/kg 438 146 1 02/16/22 11:33 02/17/22 13:48 205-99-2 Benzo(g,h,i)perylene ND ug/kg 438 170 1 02/16/22 11:33 02/17/22 13:48 191-24-2 Benzo(k)fluoranthene ND ug/kg 438 154 1 02/16/22 11:33 02/17/22 13:48 207-08-9 Benzoic Acid ND ug/kg 2190 941 1 02/16/22 11:33 02/17/22 13:48 65-85-0 Benzyl alcohol ND ug/kg 876 332 1 02/16/22 11:33 02/17/22 13:48 100-51-6 4-Bromophenylphenyl ether ND ug/kg 438 169 1 02/16/22 11:33 02/17/22 13:48 101-55-3 Butylbenzylphthalate ND ug/kg 438 184 1 02/16/22 11:33 02/17/22 13:48 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 876 308 1 02/16/22 11:33 02/17/22 13:48 59-50-7 4-Chloroaniline ND ug/kg 876 344 1 02/16/22 11:33 02/17/22 13:48 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 438 182 1 02/16/22 11:33 02/17/22 13:48 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 438 165 1 02/16/22 11:33 02/17/22 13:48 111-44-4 2-Chloronaphthalene ND ug/kg 438 174 1 02/16/22 11:33 02/17/22 13:48 91-58-7 2-Chlorophenol ND ug/kg 438 165 1 02/16/22 11:33 02/17/22 13:48 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 438 163 1 02/16/22 11:33 02/17/22 13:48 7005-72-3 Chrysene ND ug/kg 438 159 1 02/16/22 11:33 02/17/22 13:48 218-01-9 Dibenz(a,h)anthracene ND ug/kg 438 169 1 02/16/22 11:33 02/17/22 13:48 53-70-3 Dibenzofuran ND ug/kg 438 158 1 02/16/22 11:33 02/17/22 13:48 132-64-9 1,2-Dichlorobenzene ND ug/kg 438 158 1 02/16/22 11:33 02/17/22 13:48 95-50-1 1,3-Dichlorobenzene ND ug/kg 438 155 1 02/16/22 11:33 02/17/22 13:48 541-73-1 1,4-Dichlorobenzene ND ug/kg 438 167 1 02/16/22 11:33 02/17/22 13:48 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 876 296 1 02/16/22 11:33 02/17/22 13:48 91-94-1 2,4-Dichlorophenol ND ug/kg 438 171 1 02/16/22 11:33 02/17/22 13:48 120-83-2 Diethylphthalate ND ug/kg 438 161 1 02/16/22 11:33 02/17/22 13:48 84-66-2 2,4-Dimethylphenol ND ug/kg 438 182 1 02/16/22 11:33 02/17/22 13:48 105-67-9 Dimethylphthalate ND ug/kg 438 159 1 02/16/22 11:33 02/17/22 13:48 131-11-3 Di-n-butylphthalate ND ug/kg 438 147 1 02/16/22 11:33 02/17/22 13:48 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 876 409 1 02/16/22 11:33 02/17/22 13:48 534-52-1 2,4-Dinitrophenol ND ug/kg 2190 1350 1 02/16/22 11:33 02/17/22 13:48 51-28-5 2,4-Dinitrotoluene ND ug/kg 438 169 1 02/16/22 11:33 02/17/22 13:48 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 438 161 1 02/16/22 11:33 02/17/22 13:48 606-20-2 Di-n-octylphthalate ND ug/kg 438 173 1 02/16/22 11:33 02/17/22 13:48 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 438 170 1 02/16/22 11:33 02/17/22 13:48 117-81-7 Fluoranthene ND ug/kg 438 150 1 02/16/22 11:33 02/17/22 13:48 206-44-0 Fluorene ND ug/kg 438 154 1 02/16/22 11:33 02/17/22 13:48 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 438 190 1 02/16/22 11:33 02/17/22 13:48 87-68-3 Hexachlorobenzene ND ug/kg 438 171 1 02/16/22 11:33 02/17/22 13:48 118-74-1 Hexachlorocyclopentadiene ND ug/kg 438 251 1 02/16/22 11:33 02/17/22 13:48 77-47-4 Hexachloroethane ND ug/kg 438 167 1 02/16/22 11:33 02/17/22 13:48 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 438 173 1 02/16/22 11:33 02/17/22 13:48 193-39-5 Isophorone ND ug/kg 438 195 1 02/16/22 11:33 02/17/22 13:48 78-59-1 1-Methylnaphthalene ND ug/kg 438 154 1 02/16/22 11:33 02/17/22 13:48 90-12-0 2-Methylnaphthalene ND ug/kg 438 175 1 02/16/22 11:33 02/17/22 13:48 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 438 179 1 02/16/22 11:33 02/17/22 13:48 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 438 177 1 02/16/22 11:33 02/17/22 13:48 15831-10-4 Naphthalene ND ug/kg 438 149 1 02/16/22 11:33 02/17/22 13:48 91-20-3 2-Nitroaniline ND ug/kg 2190 358 1 02/16/22 11:33 02/17/22 13:48 88-74-4 3-Nitroaniline ND ug/kg 2190 344 1 02/16/22 11:33 02/17/22 13:48 99-09-2 4-Nitroaniline ND ug/kg 876 333 1 02/16/22 11:33 02/17/22 13:48 100-01-6 Nitrobenzene ND ug/kg 438 203 1 02/16/22 11:33 02/17/22 13:48 98-95-3 2-Nitrophenol ND ug/kg 438 190 1 02/16/22 11:33 02/17/22 13:48 88-75-5 4-Nitrophenol ND ug/kg 2190 847 1 02/16/22 11:33 02/17/22 13:48 100-02-7 N-Nitrosodimethylamine ND ug/kg 438 147 1 02/16/22 11:33 02/17/22 13:48 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 438 165 1 02/16/22 11:33 02/17/22 13:48 621-64-7 N-Nitrosodiphenylamine ND ug/kg 438 155 1 02/16/22 11:33 02/17/22 13:48 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 438 208 1 02/16/22 11:33 02/17/22 13:48 108-60-1 Pentachlorophenol ND ug/kg 876 429 1 02/16/22 11:33 02/17/22 13:48 87-86-5 Phenanthrene ND ug/kg 438 143 1 02/16/22 11:33 02/17/22 13:48 85-01-8 Phenol ND ug/kg 438 195 1 02/16/22 11:33 02/17/22 13:48 108-95-2 Pyrene ND ug/kg 438 178 1 02/16/22 11:33 02/17/22 13:48 129-00-0 Pyridine ND ug/kg 438 138 1 02/16/22 11:33 02/17/22 13:48 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 438 173 1 02/16/22 11:33 02/17/22 13:48 120-82-1 2,4,5-Trichlorophenol ND ug/kg 438 200 1 02/16/22 11:33 02/17/22 13:48 95-95-4 2,4,6-Trichlorophenol ND ug/kg 438 180 1 02/16/22 11:33 02/17/22 13:48 88-06-2 Surrogates Nitrobenzene-d5 (S) 66 % 21-130 1 02/16/22 11:33 02/17/22 13:48 4165-60-0 2-Fluorobiphenyl (S) 53 % 19-130 1 02/16/22 11:33 02/17/22 13:48 321-60-8 Terphenyl-d14 (S) 59 % 15-130 1 02/16/22 11:33 02/17/22 13:48 1718-51-0 Phenol-d6 (S) 59 % 18-130 1 02/16/22 11:33 02/17/22 13:48 13127-88-3 2-Fluorophenol (S) 54 % 18-130 1 02/16/22 11:33 02/17/22 13:48 367-12-4 2,4,6-Tribromophenol (S) 38 % 18-130 1 02/16/22 11:33 02/17/22 13:48 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 199 64.0 1 02/15/22 21:19 02/17/22 18:58 67-64-1 Benzene ND ug/kg 10 4.0 1 02/15/22 21:19 02/17/22 18:58 71-43-2 Bromobenzene ND ug/kg 10 3.2 1 02/15/22 21:19 02/17/22 18:58 108-86-1 Bromochloromethane ND ug/kg 10 2.9 1 02/15/22 21:19 02/17/22 18:58 74-97-5 Bromodichloromethane ND ug/kg 10 3.8 1 02/15/22 21:19 02/17/22 18:58 75-27-4 Bromoform ND ug/kg 10 3.5 1 02/15/22 21:19 02/17/22 18:58 75-25-2 Bromomethane ND ug/kg 19.9 15.7 1 02/15/22 21:19 02/17/22 18:58 74-83-9 2-Butanone (MEK) ND ug/kg 199 47.8 1 02/15/22 21:19 02/17/22 18:58 78-93-3 n-Butylbenzene ND ug/kg 10 4.7 1 02/15/22 21:19 02/17/22 18:58 104-51-8 sec-Butylbenzene ND ug/kg 10 4.4 1 02/15/22 21:19 02/17/22 18:58 135-98-8 tert-Butyl benzene ND ug/kg 10 3.5 1 02/15/22 21:19 02/17/22 18:58 98-06-6 Carbon tetrachloride ND ug/kg 10 3.7 1 02/15/22 21:19 02/17/22 18:58 56-23-5 Chlorobenzene ND ug/kg 10 1.9 1 02/15/22 21:19 02/17/22 18:58 108-90-7 Chloroethane ND ug/kg 19.9 7.7 1 02/15/22 21:19 02/17/22 18:58 75-00-3 Chloroform ND ug/kg 10 6.1 1 02/15/22 21:19 02/17/22 18:58 67-66-3 Chloromethane ND ug/kg 19.9 8.4 1 02/15/22 21:19 02/17/22 18:58 74-87-3 2-Chlorotoluene ND ug/kg 10 3.5 1 02/15/22 21:19 02/17/22 18:58 95-49-8 4-Chlorotoluene ND ug/kg 10 1.8 1 02/15/22 21:19 02/17/22 18:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 10 3.9 1 02/15/22 21:19 02/17/22 18:58 96-12-8 Dibromochloromethane ND ug/kg 10 5.6 1 02/15/22 21:19 02/17/22 18:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 10 4.4 1 02/15/22 21:19 02/17/22 18:58 106-93-4 Dibromomethane ND ug/kg 10 2.1 1 02/15/22 21:19 02/17/22 18:58 74-95-3 1,2-Dichlorobenzene ND ug/kg 10 3.6 1 02/15/22 21:19 02/17/22 18:58 95-50-1 1,3-Dichlorobenzene ND ug/kg 10 3.1 1 02/15/22 21:19 02/17/22 18:58 541-73-1 1,4-Dichlorobenzene ND ug/kg 10 2.6 1 02/15/22 21:19 02/17/22 18:58 106-46-7 Dichlorodifluoromethane ND ug/kg 19.9 4.3 1 02/15/22 21:19 02/17/22 18:58 75-71-8 1,1-Dichloroethane ND ug/kg 10 4.1 1 02/15/22 21:19 02/17/22 18:58 75-34-3 1,2-Dichloroethane ND ug/kg 10 6.6 1 02/15/22 21:19 02/17/22 18:58 107-06-2 1,1-Dichloroethene ND ug/kg 10 4.1 1 02/15/22 21:19 02/17/22 18:58 75-35-4 cis-1,2-Dichloroethene ND ug/kg 10 3.4 1 02/15/22 21:19 02/17/22 18:58 156-59-2 trans-1,2-Dichloroethene ND ug/kg 10 3.5 1 02/15/22 21:19 02/17/22 18:58 156-60-5 1,2-Dichloropropane ND ug/kg 10 3.0 1 02/15/22 21:19 02/17/22 18:58 78-87-5 1,3-Dichloropropane ND ug/kg 10 3.1 1 02/15/22 21:19 02/17/22 18:58 142-28-9 2,2-Dichloropropane ND ug/kg 10 3.2 1 02/15/22 21:19 02/17/22 18:58 594-20-7 1,1-Dichloropropene ND ug/kg 10 4.8 1 02/15/22 21:19 02/17/22 18:58 563-58-6 cis-1,3-Dichloropropene ND ug/kg 10 2.7 1 02/15/22 21:19 02/17/22 18:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 10 3.4 1 02/15/22 21:19 02/17/22 18:58 10061-02-6 Diisopropyl ether ND ug/kg 10 2.7 1 02/15/22 21:19 02/17/22 18:58 108-20-3 Ethylbenzene ND ug/kg 10 4.6 1 02/15/22 21:19 02/17/22 18:58 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 19.9 16.3 1 02/15/22 21:19 02/17/22 18:58 87-68-3 2-Hexanone ND ug/kg 99.6 9.6 1 02/15/22 21:19 02/17/22 18:58 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 10 3.4 1 02/15/22 21:19 02/17/22 18:58 98-82-8 p-Isopropyltoluene ND ug/kg 10 4.9 1 02/15/22 21:19 02/17/22 18:58 99-87-6 Methylene Chloride ND ug/kg 39.9 27.3 1 02/15/22 21:19 02/17/22 18:58 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 99.6 9.6 1 02/15/22 21:19 02/17/22 18:58 108-10-1 Methyl-tert-butyl ether ND ug/kg 10 3.7 1 02/15/22 21:19 02/17/22 18:58 1634-04-4 Naphthalene ND ug/kg 10 5.2 1 02/15/22 21:19 02/17/22 18:58 91-20-3 n-Propylbenzene ND ug/kg 10 3.5 1 02/15/22 21:19 02/17/22 18:58 103-65-1 Styrene ND ug/kg 10 2.6 1 02/15/22 21:19 02/17/22 18:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 10 3.8 1 02/15/22 21:19 02/17/22 18:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 10 2.6 1 02/15/22 21:19 02/17/22 18:58 79-34-5 Tetrachloroethene ND ug/kg 10 3.1 1 02/15/22 21:19 02/17/22 18:58 127-18-4 Toluene ND ug/kg 10 2.8 1 02/15/22 21:19 02/17/22 18:58 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 10 8.0 1 02/15/22 21:19 02/17/22 18:58 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 10 8.4 1 02/15/22 21:19 02/17/22 18:58 120-82-1 1,1,1-Trichloroethane ND ug/kg 10 5.2 1 02/15/22 21:19 02/17/22 18:58 71-55-6 1,1,2-Trichloroethane ND ug/kg 10 3.3 1 02/15/22 21:19 02/17/22 18:58 79-00-5 Trichloroethene ND ug/kg 10 2.6 1 02/15/22 21:19 02/17/22 18:58 79-01-6 Trichlorofluoromethane ND ug/kg 10 5.5 1 02/15/22 21:19 02/17/22 18:58 75-69-4 1,2,3-Trichloropropane ND ug/kg 10 5.0 1 02/15/22 21:19 02/17/22 18:58 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 10 2.7 1 02/15/22 21:19 02/17/22 18:58 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 10 3.3 1 02/15/22 21:19 02/17/22 18:58 108-67-8 Vinyl acetate ND ug/kg 99.6 7.3 1 02/15/22 21:19 02/17/22 18:58 108-05-4 Vinyl chloride ND ug/kg 19.9 5.1 1 02/15/22 21:19 02/17/22 18:58 75-01-4 v2 Xylene (Total) ND ug/kg 19.9 5.7 1 02/15/22 21:19 02/17/22 18:58 1330-20-7 m&p-Xylene ND ug/kg 19.9 6.8 1 02/15/22 21:19 02/17/22 18:58 179601-23-1 o-Xylene ND ug/kg 10 4.4 1 02/15/22 21:19 02/17/22 18:58 95-47-6 Surrogates Toluene-d8 (S) 98 % 70-130 1 02/15/22 21:19 02/17/22 18:58 2037-26-5 4-Bromofluorobenzene (S) 98 % 69-134 1 02/15/22 21:19 02/17/22 18:58 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 02/15/22 21:19 02/17/22 18:58 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 23.6 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-13 Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 8.2 8.2 1 02/16/22 13:41 02/16/22 19:21 Aliphatic(C09-C12)Adjusted ND mg/kg 8.2 8.2 1 02/16/22 13:41 02/16/22 19:21 Aromatic (C09-C10) ND mg/kg 8.2 8.2 1 02/16/22 13:41 02/16/22 19:21 Surrogates 4-Bromofluorobenzene (FID) (S) 102 % 70-130 1 02/16/22 13:41 02/16/22 19:21 460-00-4 4-Bromofluorobenzene (PID) (S) 85 % 70-130 1 02/16/22 13:41 02/16/22 19:21 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 443 156 1 02/16/22 11:33 02/17/22 14:15 83-32-9 Acenaphthylene ND ug/kg 443 156 1 02/16/22 11:33 02/17/22 14:15 208-96-8 Aniline ND ug/kg 443 173 1 02/16/22 11:33 02/17/22 14:15 62-53-3 Anthracene ND ug/kg 443 145 1 02/16/22 11:33 02/17/22 14:15 120-12-7 Benzo(a)anthracene ND ug/kg 443 148 1 02/16/22 11:33 02/17/22 14:15 56-55-3 Benzo(a)pyrene ND ug/kg 443 153 1 02/16/22 11:33 02/17/22 14:15 50-32-8 Benzo(b)fluoranthene ND ug/kg 443 148 1 02/16/22 11:33 02/17/22 14:15 205-99-2 Benzo(g,h,i)perylene ND ug/kg 443 172 1 02/16/22 11:33 02/17/22 14:15 191-24-2 Benzo(k)fluoranthene ND ug/kg 443 156 1 02/16/22 11:33 02/17/22 14:15 207-08-9 Benzoic Acid ND ug/kg 2210 952 1 02/16/22 11:33 02/17/22 14:15 65-85-0 Benzyl alcohol ND ug/kg 886 336 1 02/16/22 11:33 02/17/22 14:15 100-51-6 4-Bromophenylphenyl ether ND ug/kg 443 170 1 02/16/22 11:33 02/17/22 14:15 101-55-3 Butylbenzylphthalate ND ug/kg 443 187 1 02/16/22 11:33 02/17/22 14:15 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 886 311 1 02/16/22 11:33 02/17/22 14:15 59-50-7 4-Chloroaniline ND ug/kg 886 348 1 02/16/22 11:33 02/17/22 14:15 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 443 184 1 02/16/22 11:33 02/17/22 14:15 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 443 166 1 02/16/22 11:33 02/17/22 14:15 111-44-4 2-Chloronaphthalene ND ug/kg 443 176 1 02/16/22 11:33 02/17/22 14:15 91-58-7 2-Chlorophenol ND ug/kg 443 166 1 02/16/22 11:33 02/17/22 14:15 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 443 165 1 02/16/22 11:33 02/17/22 14:15 7005-72-3 Chrysene ND ug/kg 443 161 1 02/16/22 11:33 02/17/22 14:15 218-01-9 Dibenz(a,h)anthracene ND ug/kg 443 170 1 02/16/22 11:33 02/17/22 14:15 53-70-3 Dibenzofuran ND ug/kg 443 160 1 02/16/22 11:33 02/17/22 14:15 132-64-9 1,2-Dichlorobenzene ND ug/kg 443 160 1 02/16/22 11:33 02/17/22 14:15 95-50-1 1,3-Dichlorobenzene ND ug/kg 443 157 1 02/16/22 11:33 02/17/22 14:15 541-73-1 1,4-Dichlorobenzene ND ug/kg 443 169 1 02/16/22 11:33 02/17/22 14:15 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 886 299 1 02/16/22 11:33 02/17/22 14:15 91-94-1 2,4-Dichlorophenol ND ug/kg 443 173 1 02/16/22 11:33 02/17/22 14:15 120-83-2 Diethylphthalate ND ug/kg 443 162 1 02/16/22 11:33 02/17/22 14:15 84-66-2 2,4-Dimethylphenol ND ug/kg 443 184 1 02/16/22 11:33 02/17/22 14:15 105-67-9 Dimethylphthalate ND ug/kg 443 161 1 02/16/22 11:33 02/17/22 14:15 131-11-3 Di-n-butylphthalate ND ug/kg 443 149 1 02/16/22 11:33 02/17/22 14:15 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 886 413 1 02/16/22 11:33 02/17/22 14:15 534-52-1 2,4-Dinitrophenol ND ug/kg 2210 1370 1 02/16/22 11:33 02/17/22 14:15 51-28-5 2,4-Dinitrotoluene ND ug/kg 443 170 1 02/16/22 11:33 02/17/22 14:15 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-13 Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 443 162 1 02/16/22 11:33 02/17/22 14:15 606-20-2 Di-n-octylphthalate ND ug/kg 443 174 1 02/16/22 11:33 02/17/22 14:15 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 443 172 1 02/16/22 11:33 02/17/22 14:15 117-81-7 Fluoranthene ND ug/kg 443 152 1 02/16/22 11:33 02/17/22 14:15 206-44-0 Fluorene ND ug/kg 443 156 1 02/16/22 11:33 02/17/22 14:15 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 443 192 1 02/16/22 11:33 02/17/22 14:15 87-68-3 Hexachlorobenzene ND ug/kg 443 173 1 02/16/22 11:33 02/17/22 14:15 118-74-1 Hexachlorocyclopentadiene ND ug/kg 443 254 1 02/16/22 11:33 02/17/22 14:15 77-47-4 Hexachloroethane ND ug/kg 443 169 1 02/16/22 11:33 02/17/22 14:15 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 443 174 1 02/16/22 11:33 02/17/22 14:15 193-39-5 Isophorone ND ug/kg 443 197 1 02/16/22 11:33 02/17/22 14:15 78-59-1 1-Methylnaphthalene ND ug/kg 443 156 1 02/16/22 11:33 02/17/22 14:15 90-12-0 2-Methylnaphthalene ND ug/kg 443 177 1 02/16/22 11:33 02/17/22 14:15 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 443 181 1 02/16/22 11:33 02/17/22 14:15 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 443 179 1 02/16/22 11:33 02/17/22 14:15 15831-10-4 Naphthalene ND ug/kg 443 150 1 02/16/22 11:33 02/17/22 14:15 91-20-3 2-Nitroaniline ND ug/kg 2210 362 1 02/16/22 11:33 02/17/22 14:15 88-74-4 3-Nitroaniline ND ug/kg 2210 348 1 02/16/22 11:33 02/17/22 14:15 99-09-2 4-Nitroaniline ND ug/kg 886 337 1 02/16/22 11:33 02/17/22 14:15 100-01-6 Nitrobenzene ND ug/kg 443 205 1 02/16/22 11:33 02/17/22 14:15 98-95-3 2-Nitrophenol ND ug/kg 443 192 1 02/16/22 11:33 02/17/22 14:15 88-75-5 4-Nitrophenol ND ug/kg 2210 856 1 02/16/22 11:33 02/17/22 14:15 100-02-7 N-Nitrosodimethylamine ND ug/kg 443 149 1 02/16/22 11:33 02/17/22 14:15 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 443 166 1 02/16/22 11:33 02/17/22 14:15 621-64-7 N-Nitrosodiphenylamine ND ug/kg 443 157 1 02/16/22 11:33 02/17/22 14:15 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 443 211 1 02/16/22 11:33 02/17/22 14:15 108-60-1 Pentachlorophenol ND ug/kg 886 434 1 02/16/22 11:33 02/17/22 14:15 87-86-5 Phenanthrene ND ug/kg 443 145 1 02/16/22 11:33 02/17/22 14:15 85-01-8 Phenol ND ug/kg 443 197 1 02/16/22 11:33 02/17/22 14:15 108-95-2 Pyrene ND ug/kg 443 180 1 02/16/22 11:33 02/17/22 14:15 129-00-0 Pyridine ND ug/kg 443 140 1 02/16/22 11:33 02/17/22 14:15 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 443 174 1 02/16/22 11:33 02/17/22 14:15 120-82-1 2,4,5-Trichlorophenol ND ug/kg 443 203 1 02/16/22 11:33 02/17/22 14:15 95-95-4 2,4,6-Trichlorophenol ND ug/kg 443 183 1 02/16/22 11:33 02/17/22 14:15 88-06-2 Surrogates Nitrobenzene-d5 (S) 67 % 21-130 1 02/16/22 11:33 02/17/22 14:15 4165-60-0 2-Fluorobiphenyl (S) 52 % 19-130 1 02/16/22 11:33 02/17/22 14:15 321-60-8 Terphenyl-d14 (S) 64 % 15-130 1 02/16/22 11:33 02/17/22 14:15 1718-51-0 Phenol-d6 (S) 60 % 18-130 1 02/16/22 11:33 02/17/22 14:15 13127-88-3 2-Fluorophenol (S) 55 % 18-130 1 02/16/22 11:33 02/17/22 14:15 367-12-4 2,4,6-Tribromophenol (S) 51 % 18-130 1 02/16/22 11:33 02/17/22 14:15 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-B Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 276 88.7 1 02/15/22 21:19 02/17/22 19:16 67-64-1 Benzene ND ug/kg 13.8 5.5 1 02/15/22 21:19 02/17/22 19:16 71-43-2 Bromobenzene ND ug/kg 13.8 4.5 1 02/15/22 21:19 02/17/22 19:16 108-86-1 Bromochloromethane ND ug/kg 13.8 4.1 1 02/15/22 21:19 02/17/22 19:16 74-97-5 Bromodichloromethane ND ug/kg 13.8 5.3 1 02/15/22 21:19 02/17/22 19:16 75-27-4 Bromoform ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 19:16 75-25-2 Bromomethane ND ug/kg 27.6 21.8 1 02/15/22 21:19 02/17/22 19:16 74-83-9 2-Butanone (MEK) ND ug/kg 276 66.4 1 02/15/22 21:19 02/17/22 19:16 78-93-3 n-Butylbenzene ND ug/kg 13.8 6.5 1 02/15/22 21:19 02/17/22 19:16 104-51-8 sec-Butylbenzene ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 19:16 135-98-8 tert-Butyl benzene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 19:16 98-06-6 Carbon tetrachloride ND ug/kg 13.8 5.2 1 02/15/22 21:19 02/17/22 19:16 56-23-5 Chlorobenzene ND ug/kg 13.8 2.7 1 02/15/22 21:19 02/17/22 19:16 108-90-7 Chloroethane ND ug/kg 27.6 10.7 1 02/15/22 21:19 02/17/22 19:16 75-00-3 Chloroform ND ug/kg 13.8 8.4 1 02/15/22 21:19 02/17/22 19:16 67-66-3 Chloromethane ND ug/kg 27.6 11.6 1 02/15/22 21:19 02/17/22 19:16 74-87-3 2-Chlorotoluene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 19:16 95-49-8 4-Chlorotoluene ND ug/kg 13.8 2.4 1 02/15/22 21:19 02/17/22 19:16 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 13.8 5.4 1 02/15/22 21:19 02/17/22 19:16 96-12-8 Dibromochloromethane ND ug/kg 13.8 7.8 1 02/15/22 21:19 02/17/22 19:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 19:16 106-93-4 Dibromomethane ND ug/kg 13.8 3.0 1 02/15/22 21:19 02/17/22 19:16 74-95-3 1,2-Dichlorobenzene ND ug/kg 13.8 5.0 1 02/15/22 21:19 02/17/22 19:16 95-50-1 1,3-Dichlorobenzene ND ug/kg 13.8 4.3 1 02/15/22 21:19 02/17/22 19:16 541-73-1 1,4-Dichlorobenzene ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 19:16 106-46-7 Dichlorodifluoromethane ND ug/kg 27.6 6.0 1 02/15/22 21:19 02/17/22 19:16 75-71-8 1,1-Dichloroethane ND ug/kg 13.8 5.7 1 02/15/22 21:19 02/17/22 19:16 75-34-3 1,2-Dichloroethane ND ug/kg 13.8 9.2 1 02/15/22 21:19 02/17/22 19:16 107-06-2 1,1-Dichloroethene ND ug/kg 13.8 5.7 1 02/15/22 21:19 02/17/22 19:16 75-35-4 cis-1,2-Dichloroethene ND ug/kg 13.8 4.7 1 02/15/22 21:19 02/17/22 19:16 156-59-2 trans-1,2-Dichloroethene ND ug/kg 13.8 4.8 1 02/15/22 21:19 02/17/22 19:16 156-60-5 1,2-Dichloropropane ND ug/kg 13.8 4.1 1 02/15/22 21:19 02/17/22 19:16 78-87-5 1,3-Dichloropropane ND ug/kg 13.8 4.3 1 02/15/22 21:19 02/17/22 19:16 142-28-9 2,2-Dichloropropane ND ug/kg 13.8 4.5 1 02/15/22 21:19 02/17/22 19:16 594-20-7 1,1-Dichloropropene ND ug/kg 13.8 6.6 1 02/15/22 21:19 02/17/22 19:16 563-58-6 cis-1,3-Dichloropropene ND ug/kg 13.8 3.8 1 02/15/22 21:19 02/17/22 19:16 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 13.8 4.8 1 02/15/22 21:19 02/17/22 19:16 10061-02-6 Diisopropyl ether ND ug/kg 13.8 3.7 1 02/15/22 21:19 02/17/22 19:16 108-20-3 Ethylbenzene ND ug/kg 13.8 6.4 1 02/15/22 21:19 02/17/22 19:16 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 27.6 22.6 1 02/15/22 21:19 02/17/22 19:16 87-68-3 2-Hexanone ND ug/kg 138 13.3 1 02/15/22 21:19 02/17/22 19:16 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 13.8 4.7 1 02/15/22 21:19 02/17/22 19:16 98-82-8 p-Isopropyltoluene ND ug/kg 13.8 6.8 1 02/15/22 21:19 02/17/22 19:16 99-87-6 Methylene Chloride ND ug/kg 55.3 37.9 1 02/15/22 21:19 02/17/22 19:16 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-13 Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 138 13.3 1 02/15/22 21:19 02/17/22 19:16 108-10-1 Methyl-tert-butyl ether ND ug/kg 13.8 5.2 1 02/15/22 21:19 02/17/22 19:16 1634-04-4 Naphthalene 24.4 ug/kg 13.8 7.3 1 02/15/22 21:19 02/17/22 19:16 91-20-3 n-Propylbenzene ND ug/kg 13.8 4.9 1 02/15/22 21:19 02/17/22 19:16 103-65-1 Styrene ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 19:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 13.8 5.3 1 02/15/22 21:19 02/17/22 19:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 19:16 79-34-5 Tetrachloroethene ND ug/kg 13.8 4.4 1 02/15/22 21:19 02/17/22 19:16 127-18-4 Toluene ND ug/kg 13.8 3.9 1 02/15/22 21:19 02/17/22 19:16 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 13.8 11.2 1 02/15/22 21:19 02/17/22 19:16 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 13.8 11.6 1 02/15/22 21:19 02/17/22 19:16 120-82-1 1,1,1-Trichloroethane ND ug/kg 13.8 7.2 1 02/15/22 21:19 02/17/22 19:16 71-55-6 1,1,2-Trichloroethane ND ug/kg 13.8 4.6 1 02/15/22 21:19 02/17/22 19:16 79-00-5 Trichloroethene ND ug/kg 13.8 3.6 1 02/15/22 21:19 02/17/22 19:16 79-01-6 Trichlorofluoromethane ND ug/kg 13.8 7.6 1 02/15/22 21:19 02/17/22 19:16 75-69-4 1,2,3-Trichloropropane ND ug/kg 13.8 7.0 1 02/15/22 21:19 02/17/22 19:16 96-18-4 1,2,4-Trimethylbenzene 9.01 ug/kg 13.8 3.8 1 02/15/22 21:19 02/17/22 19:16 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 13.8 4.6 1 02/15/22 21:19 02/17/22 19:16 108-67-8 Vinyl acetate ND ug/kg 138 10.1 1 02/15/22 21:19 02/17/22 19:16 108-05-4 Vinyl chloride ND ug/kg 27.6 7.0 1 02/15/22 21:19 02/17/22 19:16 75-01-4 v2 Xylene (Total) ND ug/kg 27.6 7.9 1 02/15/22 21:19 02/17/22 19:16 1330-20-7 m&p-Xylene ND ug/kg 27.6 9.5 1 02/15/22 21:19 02/17/22 19:16 179601-23-1 o-Xylene ND ug/kg 13.8 6.1 1 02/15/22 21:19 02/17/22 19:16 95-47-6 Surrogates Toluene-d8 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 19:16 2037-26-5 4-Bromofluorobenzene (S) 98 % 69-134 1 02/15/22 21:19 02/17/22 19:16 460-00-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 02/15/22 21:19 02/17/22 19:16 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 25.7 % 0.10 0.10 1 02/15/22 17:10 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 4.3 4.3 1 02/16/22 13:41 02/16/22 19:50 Aliphatic(C09-C12)Adjusted ND mg/kg 4.3 4.3 1 02/16/22 13:41 02/16/22 19:50 Aromatic (C09-C10) ND mg/kg 4.3 4.3 1 02/16/22 13:41 02/16/22 19:50 Surrogates 4-Bromofluorobenzene (FID) (S) 101 % 70-130 1 02/16/22 13:41 02/16/22 19:50 460-00-4 4-Bromofluorobenzene (PID) (S) 85 % 70-130 1 02/16/22 13:41 02/16/22 19:50 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 449 158 1 02/16/22 11:33 02/17/22 14:42 83-32-9 Acenaphthylene ND ug/kg 449 158 1 02/16/22 11:33 02/17/22 14:42 208-96-8 Aniline ND ug/kg 449 175 1 02/16/22 11:33 02/17/22 14:42 62-53-3 Anthracene ND ug/kg 449 147 1 02/16/22 11:33 02/17/22 14:42 120-12-7 Benzo(a)anthracene ND ug/kg 449 150 1 02/16/22 11:33 02/17/22 14:42 56-55-3 Benzo(a)pyrene ND ug/kg 449 155 1 02/16/22 11:33 02/17/22 14:42 50-32-8 Benzo(b)fluoranthene ND ug/kg 449 150 1 02/16/22 11:33 02/17/22 14:42 205-99-2 Benzo(g,h,i)perylene ND ug/kg 449 174 1 02/16/22 11:33 02/17/22 14:42 191-24-2 Benzo(k)fluoranthene ND ug/kg 449 158 1 02/16/22 11:33 02/17/22 14:42 207-08-9 Benzoic Acid ND ug/kg 2240 964 1 02/16/22 11:33 02/17/22 14:42 65-85-0 Benzyl alcohol ND ug/kg 898 340 1 02/16/22 11:33 02/17/22 14:42 100-51-6 4-Bromophenylphenyl ether ND ug/kg 449 173 1 02/16/22 11:33 02/17/22 14:42 101-55-3 Butylbenzylphthalate ND ug/kg 449 189 1 02/16/22 11:33 02/17/22 14:42 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 898 315 1 02/16/22 11:33 02/17/22 14:42 59-50-7 4-Chloroaniline ND ug/kg 898 352 1 02/16/22 11:33 02/17/22 14:42 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 449 186 1 02/16/22 11:33 02/17/22 14:42 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 449 169 1 02/16/22 11:33 02/17/22 14:42 111-44-4 2-Chloronaphthalene ND ug/kg 449 178 1 02/16/22 11:33 02/17/22 14:42 91-58-7 2-Chlorophenol ND ug/kg 449 169 1 02/16/22 11:33 02/17/22 14:42 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 449 167 1 02/16/22 11:33 02/17/22 14:42 7005-72-3 Chrysene ND ug/kg 449 163 1 02/16/22 11:33 02/17/22 14:42 218-01-9 Dibenz(a,h)anthracene ND ug/kg 449 173 1 02/16/22 11:33 02/17/22 14:42 53-70-3 Dibenzofuran ND ug/kg 449 162 1 02/16/22 11:33 02/17/22 14:42 132-64-9 1,2-Dichlorobenzene ND ug/kg 449 162 1 02/16/22 11:33 02/17/22 14:42 95-50-1 1,3-Dichlorobenzene ND ug/kg 449 159 1 02/16/22 11:33 02/17/22 14:42 541-73-1 1,4-Dichlorobenzene ND ug/kg 449 171 1 02/16/22 11:33 02/17/22 14:42 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 898 303 1 02/16/22 11:33 02/17/22 14:42 91-94-1 2,4-Dichlorophenol ND ug/kg 449 175 1 02/16/22 11:33 02/17/22 14:42 120-83-2 Diethylphthalate ND ug/kg 449 165 1 02/16/22 11:33 02/17/22 14:42 84-66-2 2,4-Dimethylphenol ND ug/kg 449 186 1 02/16/22 11:33 02/17/22 14:42 105-67-9 Dimethylphthalate ND ug/kg 449 163 1 02/16/22 11:33 02/17/22 14:42 131-11-3 Di-n-butylphthalate ND ug/kg 449 151 1 02/16/22 11:33 02/17/22 14:42 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 898 419 1 02/16/22 11:33 02/17/22 14:42 534-52-1 2,4-Dinitrophenol ND ug/kg 2240 1390 1 02/16/22 11:33 02/17/22 14:42 51-28-5 2,4-Dinitrotoluene ND ug/kg 449 173 1 02/16/22 11:33 02/17/22 14:42 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 449 165 1 02/16/22 11:33 02/17/22 14:42 606-20-2 Di-n-octylphthalate ND ug/kg 449 177 1 02/16/22 11:33 02/17/22 14:42 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 449 174 1 02/16/22 11:33 02/17/22 14:42 117-81-7 Fluoranthene ND ug/kg 449 154 1 02/16/22 11:33 02/17/22 14:42 206-44-0 Fluorene ND ug/kg 449 158 1 02/16/22 11:33 02/17/22 14:42 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 449 194 1 02/16/22 11:33 02/17/22 14:42 87-68-3 Hexachlorobenzene ND ug/kg 449 175 1 02/16/22 11:33 02/17/22 14:42 118-74-1 Hexachlorocyclopentadiene ND ug/kg 449 257 1 02/16/22 11:33 02/17/22 14:42 77-47-4 Hexachloroethane ND ug/kg 449 171 1 02/16/22 11:33 02/17/22 14:42 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 449 177 1 02/16/22 11:33 02/17/22 14:42 193-39-5 Isophorone ND ug/kg 449 200 1 02/16/22 11:33 02/17/22 14:42 78-59-1 1-Methylnaphthalene ND ug/kg 449 158 1 02/16/22 11:33 02/17/22 14:42 90-12-0 2-Methylnaphthalene ND ug/kg 449 180 1 02/16/22 11:33 02/17/22 14:42 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 449 184 1 02/16/22 11:33 02/17/22 14:42 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 449 181 1 02/16/22 11:33 02/17/22 14:42 15831-10-4 Naphthalene ND ug/kg 449 152 1 02/16/22 11:33 02/17/22 14:42 91-20-3 2-Nitroaniline ND ug/kg 2240 367 1 02/16/22 11:33 02/17/22 14:42 88-74-4 3-Nitroaniline ND ug/kg 2240 352 1 02/16/22 11:33 02/17/22 14:42 99-09-2 4-Nitroaniline ND ug/kg 898 341 1 02/16/22 11:33 02/17/22 14:42 100-01-6 Nitrobenzene ND ug/kg 449 208 1 02/16/22 11:33 02/17/22 14:42 98-95-3 2-Nitrophenol ND ug/kg 449 194 1 02/16/22 11:33 02/17/22 14:42 88-75-5 4-Nitrophenol ND ug/kg 2240 868 1 02/16/22 11:33 02/17/22 14:42 100-02-7 N-Nitrosodimethylamine ND ug/kg 449 151 1 02/16/22 11:33 02/17/22 14:42 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 449 169 1 02/16/22 11:33 02/17/22 14:42 621-64-7 N-Nitrosodiphenylamine ND ug/kg 449 159 1 02/16/22 11:33 02/17/22 14:42 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 449 214 1 02/16/22 11:33 02/17/22 14:42 108-60-1 Pentachlorophenol ND ug/kg 898 439 1 02/16/22 11:33 02/17/22 14:42 87-86-5 Phenanthrene ND ug/kg 449 147 1 02/16/22 11:33 02/17/22 14:42 85-01-8 Phenol ND ug/kg 449 200 1 02/16/22 11:33 02/17/22 14:42 108-95-2 Pyrene ND ug/kg 449 182 1 02/16/22 11:33 02/17/22 14:42 129-00-0 Pyridine ND ug/kg 449 141 1 02/16/22 11:33 02/17/22 14:42 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 449 177 1 02/16/22 11:33 02/17/22 14:42 120-82-1 2,4,5-Trichlorophenol ND ug/kg 449 205 1 02/16/22 11:33 02/17/22 14:42 95-95-4 2,4,6-Trichlorophenol ND ug/kg 449 185 1 02/16/22 11:33 02/17/22 14:42 88-06-2 Surrogates Nitrobenzene-d5 (S) 51 % 21-130 1 02/16/22 11:33 02/17/22 14:42 4165-60-0 2-Fluorobiphenyl (S) 41 % 19-130 1 02/16/22 11:33 02/17/22 14:42 321-60-8 Terphenyl-d14 (S) 47 % 15-130 1 02/16/22 11:33 02/17/22 14:42 1718-51-0 Phenol-d6 (S) 48 % 18-130 1 02/16/22 11:33 02/17/22 14:42 13127-88-3 2-Fluorophenol (S) 44 % 18-130 1 02/16/22 11:33 02/17/22 14:42 367-12-4 2,4,6-Tribromophenol (S) 37 % 18-130 1 02/16/22 11:33 02/17/22 14:42 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 189 60.7 1 02/15/22 21:19 02/17/22 19:33 67-64-1 Benzene ND ug/kg 9.5 3.8 1 02/15/22 21:19 02/17/22 19:33 71-43-2 Bromobenzene ND ug/kg 9.5 3.1 1 02/15/22 21:19 02/17/22 19:33 108-86-1 Bromochloromethane ND ug/kg 9.5 2.8 1 02/15/22 21:19 02/17/22 19:33 74-97-5 Bromodichloromethane ND ug/kg 9.5 3.6 1 02/15/22 21:19 02/17/22 19:33 75-27-4 Bromoform ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 19:33 75-25-2 Bromomethane ND ug/kg 18.9 14.9 1 02/15/22 21:19 02/17/22 19:33 74-83-9 2-Butanone (MEK) ND ug/kg 189 45.4 1 02/15/22 21:19 02/17/22 19:33 78-93-3 n-Butylbenzene ND ug/kg 9.5 4.5 1 02/15/22 21:19 02/17/22 19:33 104-51-8 sec-Butylbenzene ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 19:33 135-98-8 tert-Butyl benzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 19:33 98-06-6 Carbon tetrachloride ND ug/kg 9.5 3.5 1 02/15/22 21:19 02/17/22 19:33 56-23-5 Chlorobenzene ND ug/kg 9.5 1.8 1 02/15/22 21:19 02/17/22 19:33 108-90-7 Chloroethane ND ug/kg 18.9 7.3 1 02/15/22 21:19 02/17/22 19:33 75-00-3 Chloroform ND ug/kg 9.5 5.7 1 02/15/22 21:19 02/17/22 19:33 67-66-3 Chloromethane ND ug/kg 18.9 7.9 1 02/15/22 21:19 02/17/22 19:33 74-87-3 2-Chlorotoluene ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 19:33 95-49-8 4-Chlorotoluene ND ug/kg 9.5 1.7 1 02/15/22 21:19 02/17/22 19:33 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 9.5 3.7 1 02/15/22 21:19 02/17/22 19:33 96-12-8 Dibromochloromethane ND ug/kg 9.5 5.3 1 02/15/22 21:19 02/17/22 19:33 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 19:33 106-93-4 Dibromomethane ND ug/kg 9.5 2.0 1 02/15/22 21:19 02/17/22 19:33 74-95-3 1,2-Dichlorobenzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 19:33 95-50-1 1,3-Dichlorobenzene ND ug/kg 9.5 2.9 1 02/15/22 21:19 02/17/22 19:33 541-73-1 1,4-Dichlorobenzene ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 19:33 106-46-7 Dichlorodifluoromethane ND ug/kg 18.9 4.1 1 02/15/22 21:19 02/17/22 19:33 75-71-8 1,1-Dichloroethane ND ug/kg 9.5 3.9 1 02/15/22 21:19 02/17/22 19:33 75-34-3 1,2-Dichloroethane ND ug/kg 9.5 6.3 1 02/15/22 21:19 02/17/22 19:33 107-06-2 1,1-Dichloroethene ND ug/kg 9.5 3.9 1 02/15/22 21:19 02/17/22 19:33 75-35-4 cis-1,2-Dichloroethene ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 19:33 156-59-2 trans-1,2-Dichloroethene ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 19:33 156-60-5 1,2-Dichloropropane ND ug/kg 9.5 2.8 1 02/15/22 21:19 02/17/22 19:33 78-87-5 1,3-Dichloropropane ND ug/kg 9.5 2.9 1 02/15/22 21:19 02/17/22 19:33 142-28-9 2,2-Dichloropropane ND ug/kg 9.5 3.1 1 02/15/22 21:19 02/17/22 19:33 594-20-7 1,1-Dichloropropene ND ug/kg 9.5 4.5 1 02/15/22 21:19 02/17/22 19:33 563-58-6 cis-1,3-Dichloropropene ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 19:33 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 19:33 10061-02-6 Diisopropyl ether ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 19:33 108-20-3 Ethylbenzene ND ug/kg 9.5 4.4 1 02/15/22 21:19 02/17/22 19:33 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 18.9 15.5 1 02/15/22 21:19 02/17/22 19:33 87-68-3 2-Hexanone ND ug/kg 94.5 9.1 1 02/15/22 21:19 02/17/22 19:33 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 19:33 98-82-8 p-Isopropyltoluene ND ug/kg 9.5 4.7 1 02/15/22 21:19 02/17/22 19:33 99-87-6 Methylene Chloride ND ug/kg 37.8 25.9 1 02/15/22 21:19 02/17/22 19:33 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 94.5 9.1 1 02/15/22 21:19 02/17/22 19:33 108-10-1 Methyl-tert-butyl ether ND ug/kg 9.5 3.5 1 02/15/22 21:19 02/17/22 19:33 1634-04-4 Naphthalene 5.51 ug/kg 9.5 5.0 1 02/15/22 21:19 02/17/22 19:33 91-20-3 n-Propylbenzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 19:33 103-65-1 Styrene ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 19:33 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 9.5 3.6 1 02/15/22 21:19 02/17/22 19:33 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 19:33 79-34-5 Tetrachloroethene ND ug/kg 9.5 3.0 1 02/15/22 21:19 02/17/22 19:33 127-18-4 Toluene ND ug/kg 9.5 2.7 1 02/15/22 21:19 02/17/22 19:33 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 9.5 7.6 1 02/15/22 21:19 02/17/22 19:33 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 9.5 7.9 1 02/15/22 21:19 02/17/22 19:33 120-82-1 1,1,1-Trichloroethane ND ug/kg 9.5 4.9 1 02/15/22 21:19 02/17/22 19:33 71-55-6 1,1,2-Trichloroethane ND ug/kg 9.5 3.1 1 02/15/22 21:19 02/17/22 19:33 79-00-5 Trichloroethene ND ug/kg 9.5 2.4 1 02/15/22 21:19 02/17/22 19:33 79-01-6 Trichlorofluoromethane ND ug/kg 9.5 5.2 1 02/15/22 21:19 02/17/22 19:33 75-69-4 1,2,3-Trichloropropane ND ug/kg 9.5 4.8 1 02/15/22 21:19 02/17/22 19:33 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 19:33 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 19:33 108-67-8 Vinyl acetate ND ug/kg 94.5 6.9 1 02/15/22 21:19 02/17/22 19:33 108-05-4 Vinyl chloride ND ug/kg 18.9 4.8 1 02/15/22 21:19 02/17/22 19:33 75-01-4 v2 Xylene (Total) ND ug/kg 18.9 5.4 1 02/15/22 21:19 02/17/22 19:33 1330-20-7 m&p-Xylene ND ug/kg 18.9 6.5 1 02/15/22 21:19 02/17/22 19:33 179601-23-1 o-Xylene ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 19:33 95-47-6 Surrogates Toluene-d8 (S) 99 % 70-130 1 02/15/22 21:19 02/17/22 19:33 2037-26-5 4-Bromofluorobenzene (S) 97 % 69-134 1 02/15/22 21:19 02/17/22 19:33 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 02/15/22 21:19 02/17/22 19:33 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 26.7 % 0.10 0.10 1 02/15/22 17:11 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-13 Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 20:19 Aliphatic(C09-C12) Adjusted ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 20:19 Aromatic (C09-C10) ND mg/kg 5.6 5.6 1 02/16/22 13:41 02/16/22 20:19 Surrogates 4-Bromofluorobenzene (FID) (S) 98 % 70-130 1 02/16/22 13:41 02/16/22 20:19 460-00-4 4-Bromofluorobenzene (PID) (S) 84 % 70-130 1 02/16/22 13:41 02/16/22 20:19 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 445 156 1 02/16/22 11:33 02/17/22 15:08 83-32-9 Acenaphthylene ND ug/kg 445 156 1 02/16/22 11:33 02/17/22 15:08 208-96-8 Aniline ND ug/kg 445 174 1 02/16/22 11:33 02/17/22 15:08 62-53-3 Anthracene ND ug/kg 445 146 1 02/16/22 11:33 02/17/22 15:08 120-12-7 Benzo(a)anthracene ND ug/kg 445 148 1 02/16/22 11:33 02/17/22 15:08 56-55-3 Benzo(a)pyrene ND ug/kg 445 154 1 02/16/22 11:33 02/17/22 15:08 50-32-8 Benzo(b)fluoranthene ND ug/kg 445 148 1 02/16/22 11:33 02/17/22 15:08 205-99-2 Benzo(g,h,i)perylene ND ug/kg 445 172 1 02/16/22 11:33 02/17/22 15:08 191-24-2 Benzo(k)fluoranthene ND ug/kg 445 156 1 02/16/22 11:33 02/17/22 15:08 207-08-9 Benzoic Acid ND ug/kg 2220 955 1 02/16/22 11:33 02/17/22 15:08 65-85-0 Benzyl alcohol ND ug/kg 889 337 1 02/16/22 11:33 02/17/22 15:08 100-51-6 4-Bromophenylphenyl ether ND ug/kg 445 171 1 02/16/22 11:33 02/17/22 15:08 101-55-3 Butylbenzylphthalate ND ug/kg 445 187 1 02/16/22 11:33 02/17/22 15:08 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 889 313 1 02/16/22 11:33 02/17/22 15:08 59-50-7 4-Chloroaniline ND ug/kg 889 349 1 02/16/22 11:33 02/17/22 15:08 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 445 185 1 02/16/22 11:33 02/17/22 15:08 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 445 167 1 02/16/22 11:33 02/17/22 15:08 111-44-4 2-Chloronaphthalene ND ug/kg 445 177 1 02/16/22 11:33 02/17/22 15:08 91-58-7 2-Chlorophenol ND ug/kg 445 167 1 02/16/22 11:33 02/17/22 15:08 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 445 166 1 02/16/22 11:33 02/17/22 15:08 7005-72-3 Chrysene ND ug/kg 445 162 1 02/16/22 11:33 02/17/22 15:08 218-01-9 Dibenz(a,h)anthracene ND ug/kg 445 171 1 02/16/22 11:33 02/17/22 15:08 53-70-3 Dibenzofuran ND ug/kg 445 160 1 02/16/22 11:33 02/17/22 15:08 132-64-9 1,2-Dichlorobenzene ND ug/kg 445 160 1 02/16/22 11:33 02/17/22 15:08 95-50-1 1,3-Dichlorobenzene ND ug/kg 445 158 1 02/16/22 11:33 02/17/22 15:08 541-73-1 1,4-Dichlorobenzene ND ug/kg 445 170 1 02/16/22 11:33 02/17/22 15:08 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 889 300 1 02/16/22 11:33 02/17/22 15:08 91-94-1 2,4-Dichlorophenol ND ug/kg 445 174 1 02/16/22 11:33 02/17/22 15:08 120-83-2 Diethylphthalate ND ug/kg 445 163 1 02/16/22 11:33 02/17/22 15:08 84-66-2 2,4-Dimethylphenol ND ug/kg 445 185 1 02/16/22 11:33 02/17/22 15:08 105-67-9 Dimethylphthalate ND ug/kg 445 162 1 02/16/22 11:33 02/17/22 15:08 131-11-3 Di-n-butylphthalate ND ug/kg 445 150 1 02/16/22 11:33 02/17/22 15:08 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 889 415 1 02/16/22 11:33 02/17/22 15:08 534-52-1 2,4-Dinitrophenol ND ug/kg 2220 1370 1 02/16/22 11:33 02/17/22 15:08 51-28-5 2,4-Dinitrotoluene ND ug/kg 445 171 1 02/16/22 11:33 02/17/22 15:08 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-13 Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 445 163 1 02/16/22 11:33 02/17/22 15:08 606-20-2 Di-n-octylphthalate ND ug/kg 445 175 1 02/16/22 11:33 02/17/22 15:08 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 445 172 1 02/16/22 11:33 02/17/22 15:08 117-81-7 Fluoranthene ND ug/kg 445 152 1 02/16/22 11:33 02/17/22 15:08 206-44-0 Fluorene ND ug/kg 445 156 1 02/16/22 11:33 02/17/22 15:08 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 445 193 1 02/16/22 11:33 02/17/22 15:08 87-68-3 Hexachlorobenzene ND ug/kg 445 174 1 02/16/22 11:33 02/17/22 15:08 118-74-1 Hexachlorocyclopentadiene ND ug/kg 445 255 1 02/16/22 11:33 02/17/22 15:08 77-47-4 Hexachloroethane ND ug/kg 445 170 1 02/16/22 11:33 02/17/22 15:08 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 445 175 1 02/16/22 11:33 02/17/22 15:08 193-39-5 Isophorone ND ug/kg 445 198 1 02/16/22 11:33 02/17/22 15:08 78-59-1 1-Methylnaphthalene ND ug/kg 445 156 1 02/16/22 11:33 02/17/22 15:08 90-12-0 2-Methylnaphthalene ND ug/kg 445 178 1 02/16/22 11:33 02/17/22 15:08 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 445 182 1 02/16/22 11:33 02/17/22 15:08 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 445 179 1 02/16/22 11:33 02/17/22 15:08 15831-10-4 Naphthalene ND ug/kg 445 151 1 02/16/22 11:33 02/17/22 15:08 91-20-3 2-Nitroaniline ND ug/kg 2220 364 1 02/16/22 11:33 02/17/22 15:08 88-74-4 3-Nitroaniline ND ug/kg 2220 349 1 02/16/22 11:33 02/17/22 15:08 99-09-2 4-Nitroaniline ND ug/kg 889 338 1 02/16/22 11:33 02/17/22 15:08 100-01-6 Nitrobenzene ND ug/kg 445 206 1 02/16/22 11:33 02/17/22 15:08 98-95-3 2-Nitrophenol ND ug/kg 445 193 1 02/16/22 11:33 02/17/22 15:08 88-75-5 4-Nitrophenol ND ug/kg 2220 860 1 02/16/22 11:33 02/17/22 15:08 100-02-7 N-Nitrosodimethylamine ND ug/kg 445 150 1 02/16/22 11:33 02/17/22 15:08 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 445 167 1 02/16/22 11:33 02/17/22 15:08 621-64-7 N-Nitrosodiphenylamine ND ug/kg 445 158 1 02/16/22 11:33 02/17/22 15:08 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 445 212 1 02/16/22 11:33 02/17/22 15:08 108-60-1 Pentachlorophenol ND ug/kg 889 435 1 02/16/22 11:33 02/17/22 15:08 87-86-5 Phenanthrene ND ug/kg 445 146 1 02/16/22 11:33 02/17/22 15:08 85-01-8 Phenol ND ug/kg 445 198 1 02/16/22 11:33 02/17/22 15:08 108-95-2 Pyrene ND ug/kg 445 181 1 02/16/22 11:33 02/17/22 15:08 129-00-0 Pyridine ND ug/kg 445 140 1 02/16/22 11:33 02/17/22 15:08 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 445 175 1 02/16/22 11:33 02/17/22 15:08 120-82-1 2,4,5-Trichlorophenol ND ug/kg 445 203 1 02/16/22 11:33 02/17/22 15:08 95-95-4 2,4,6-Trichlorophenol ND ug/kg 445 183 1 02/16/22 11:33 02/17/22 15:08 88-06-2 Surrogates Nitrobenzene-d5 (S) 64 % 21-130 1 02/16/22 11:33 02/17/22 15:08 4165-60-0 2-Fluorobiphenyl (S) 53 % 19-130 1 02/16/22 11:33 02/17/22 15:08 321-60-8 Terphenyl-d14 (S) 64 % 15-130 1 02/16/22 11:33 02/17/22 15:08 1718-51-0 Phenol-d6 (S) 56 % 18-130 1 02/16/22 11:33 02/17/22 15:08 13127-88-3 2-Fluorophenol (S) 47 % 18-130 1 02/16/22 11:33 02/17/22 15:08 367-12-4 2,4,6-Tribromophenol (S) 39 % 18-130 1 02/16/22 11:33 02/17/22 15:08 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-B Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 192 61.6 1 02/15/22 21:19 02/17/22 19:51 67-64-1 Benzene ND ug/kg 9.6 3.8 1 02/15/22 21:19 02/17/22 19:51 71-43-2 Bromobenzene ND ug/kg 9.6 3.1 1 02/15/22 21:19 02/17/22 19:51 108-86-1 Bromochloromethane ND ug/kg 9.6 2.8 1 02/15/22 21:19 02/17/22 19:51 74-97-5 Bromodichloromethane ND ug/kg 9.6 3.7 1 02/15/22 21:19 02/17/22 19:51 75-27-4 Bromoform ND ug/kg 9.6 3.4 1 02/15/22 21:19 02/17/22 19:51 75-25-2 Bromomethane ND ug/kg 19.2 15.2 1 02/15/22 21:19 02/17/22 19:51 74-83-9 2-Butanone (MEK) ND ug/kg 192 46.1 1 02/15/22 21:19 02/17/22 19:51 78-93-3 n-Butylbenzene ND ug/kg 9.6 4.5 1 02/15/22 21:19 02/17/22 19:51 104-51-8 sec-Butylbenzene ND ug/kg 9.6 4.2 1 02/15/22 21:19 02/17/22 19:51 135-98-8 tert-Butyl benzene ND ug/kg 9.6 3.4 1 02/15/22 21:19 02/17/22 19:51 98-06-6 Carbon tetrachloride ND ug/kg 9.6 3.6 1 02/15/22 21:19 02/17/22 19:51 56-23-5 Chlorobenzene ND ug/kg 9.6 1.8 1 02/15/22 21:19 02/17/22 19:51 108-90-7 Chloroethane ND ug/kg 19.2 7.4 1 02/15/22 21:19 02/17/22 19:51 75-00-3 Chloroform ND ug/kg 9.6 5.8 1 02/15/22 21:19 02/17/22 19:51 67-66-3 Chloromethane ND ug/kg 19.2 8.1 1 02/15/22 21:19 02/17/22 19:51 74-87-3 2-Chlorotoluene ND ug/kg 9.6 3.4 1 02/15/22 21:19 02/17/22 19:51 95-49-8 4-Chlorotoluene ND ug/kg 9.6 1.7 1 02/15/22 21:19 02/17/22 19:51 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 9.6 3.7 1 02/15/22 21:19 02/17/22 19:51 96-12-8 Dibromochloromethane ND ug/kg 9.6 5.4 1 02/15/22 21:19 02/17/22 19:51 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 9.6 4.2 1 02/15/22 21:19 02/17/22 19:51 106-93-4 Dibromomethane ND ug/kg 9.6 2.1 1 02/15/22 21:19 02/17/22 19:51 74-95-3 1,2-Dichlorobenzene ND ug/kg 9.6 3.5 1 02/15/22 21:19 02/17/22 19:51 95-50-1 1,3-Dichlorobenzene ND ug/kg 9.6 3.0 1 02/15/22 21:19 02/17/22 19:51 541-73-1 1,4-Dichlorobenzene ND ug/kg 9.6 2.5 1 02/15/22 21:19 02/17/22 19:51 106-46-7 Dichlorodifluoromethane ND ug/kg 19.2 4.2 1 02/15/22 21:19 02/17/22 19:51 75-71-8 1,1-Dichloroethane ND ug/kg 9.6 4.0 1 02/15/22 21:19 02/17/22 19:51 75-34-3 1,2-Dichloroethane ND ug/kg 9.6 6.4 1 02/15/22 21:19 02/17/22 19:51 107-06-2 1,1-Dichloroethene ND ug/kg 9.6 4.0 1 02/15/22 21:19 02/17/22 19:51 75-35-4 cis-1,2-Dichloroethene ND ug/kg 9.6 3.3 1 02/15/22 21:19 02/17/22 19:51 156-59-2 trans-1,2-Dichloroethene ND ug/kg 9.6 3.4 1 02/15/22 21:19 02/17/22 19:51 156-60-5 1,2-Dichloropropane ND ug/kg 9.6 2.9 1 02/15/22 21:19 02/17/22 19:51 78-87-5 1,3-Dichloropropane ND ug/kg 9.6 3.0 1 02/15/22 21:19 02/17/22 19:51 142-28-9 2,2-Dichloropropane ND ug/kg 9.6 3.1 1 02/15/22 21:19 02/17/22 19:51 594-20-7 1,1-Dichloropropene ND ug/kg 9.6 4.6 1 02/15/22 21:19 02/17/22 19:51 563-58-6 cis-1,3-Dichloropropene ND ug/kg 9.6 2.6 1 02/15/22 21:19 02/17/22 19:51 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 9.6 3.3 1 02/15/22 21:19 02/17/22 19:51 10061-02-6 Diisopropyl ether ND ug/kg 9.6 2.6 1 02/15/22 21:19 02/17/22 19:51 108-20-3 Ethylbenzene ND ug/kg 9.6 4.5 1 02/15/22 21:19 02/17/22 19:51 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 19.2 15.7 1 02/15/22 21:19 02/17/22 19:51 87-68-3 2-Hexanone ND ug/kg 95.9 9.2 1 02/15/22 21:19 02/17/22 19:51 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 9.6 3.3 1 02/15/22 21:19 02/17/22 19:51 98-82-8 p-Isopropyltoluene ND ug/kg 9.6 4.7 1 02/15/22 21:19 02/17/22 19:51 99-87-6 Methylene Chloride ND ug/kg 38.4 26.3 1 02/15/22 21:19 02/17/22 19:51 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-13 Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 95.9 9.2 1 02/15/22 21:19 02/17/22 19:51 108-10-1 Methyl-tert-butyl ether ND ug/kg 9.6 3.6 1 02/15/22 21:19 02/17/22 19:51 1634-04-4 Naphthalene ND ug/kg 9.6 5.0 1 02/15/22 21:19 02/17/22 19:51 91-20-3 n-Propylbenzene ND ug/kg 9.6 3.4 1 02/15/22 21:19 02/17/22 19:51 103-65-1 Styrene ND ug/kg 9.6 2.5 1 02/15/22 21:19 02/17/22 19:51 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 9.6 3.7 1 02/15/22 21:19 02/17/22 19:51 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 9.6 2.5 1 02/15/22 21:19 02/17/22 19:51 79-34-5 Tetrachloroethene ND ug/kg 9.6 3.0 1 02/15/22 21:19 02/17/22 19:51 127-18-4 Toluene ND ug/kg 9.6 2.7 1 02/15/22 21:19 02/17/22 19:51 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 9.6 7.8 1 02/15/22 21:19 02/17/22 19:51 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 9.6 8.1 1 02/15/22 21:19 02/17/22 19:51 120-82-1 1,1,1-Trichloroethane ND ug/kg 9.6 5.0 1 02/15/22 21:19 02/17/22 19:51 71-55-6 1,1,2-Trichloroethane ND ug/kg 9.6 3.2 1 02/15/22 21:19 02/17/22 19:51 79-00-5 Trichloroethene ND ug/kg 9.6 2.5 1 02/15/22 21:19 02/17/22 19:51 79-01-6 Trichlorofluoromethane ND ug/kg 9.6 5.3 1 02/15/22 21:19 02/17/22 19:51 75-69-4 1,2,3-Trichloropropane ND ug/kg 9.6 4.9 1 02/15/22 21:19 02/17/22 19:51 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 9.6 2.6 1 02/15/22 21:19 02/17/22 19:51 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 9.6 3.2 1 02/15/22 21:19 02/17/22 19:51 108-67-8 Vinyl acetate ND ug/kg 95.9 7.0 1 02/15/22 21:19 02/17/22 19:51 108-05-4 Vinyl chloride ND ug/kg 19.2 4.9 1 02/15/22 21:19 02/17/22 19:51 75-01-4 v2 Xylene (Total) ND ug/kg 19.2 5.5 1 02/15/22 21:19 02/17/22 19:51 1330-20-7 m&p-Xylene ND ug/kg 19.2 6.6 1 02/15/22 21:19 02/17/22 19:51 179601-23-1 o-Xylene ND ug/kg 9.6 4.2 1 02/15/22 21:19 02/17/22 19:51 95-47-6 Surrogates Toluene-d8 (S) 98 % 70-130 1 02/15/22 21:19 02/17/22 19:51 2037-26-5 4-Bromofluorobenzene (S) 99 % 69-134 1 02/15/22 21:19 02/17/22 19:51 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 02/15/22 21:19 02/17/22 19:51 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 25.3 % 0.10 0.10 1 02/15/22 17:11 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Pace Analytical Services - Charlotte Aliphatic (C05-CO8) ND mg/kg 5.1 5.1 1 02/16/22 13:41 02/16/22 20:48 Aliphatic(C09-C12) Adjusted ND mg/kg 5.1 5.1 1 02/16/22 13:41 02/16/22 20:48 Aromatic (C09-C10) ND mg/kg 5.1 5.1 1 02/16/22 13:41 02/16/22 20:48 Surrogates 4-Bromofluorobenzene (FID) (S) 99 % 70-130 1 02/16/22 13:41 02/16/22 20:48 460-00-4 4-Bromofluorobenzene (PID) (S) 85 % 70-130 1 02/16/22 13:41 02/16/22 20:48 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte Acenaphthene ND ug/kg 448 158 1 02/16/22 11:33 02/17/22 15:35 83-32-9 Acenaphthylene ND ug/kg 448 158 1 02/16/22 11:33 02/17/22 15:35 208-96-8 Aniline ND ug/kg 448 175 1 02/16/22 11:33 02/17/22 15:35 62-53-3 Anthracene ND ug/kg 448 147 1 02/16/22 11:33 02/17/22 15:35 120-12-7 Benzo(a)anthracene ND ug/kg 448 149 1 02/16/22 11:33 02/17/22 15:35 56-55-3 Benzo(a)pyrene ND ug/kg 448 155 1 02/16/22 11:33 02/17/22 15:35 50-32-8 Benzo(b)fluoranthene ND ug/kg 448 149 1 02/16/22 11:33 02/17/22 15:35 205-99-2 Benzo(g,h,i)perylene ND ug/kg 448 174 1 02/16/22 11:33 02/17/22 15:35 191-24-2 Benzo(k)fluoranthene ND ug/kg 448 158 1 02/16/22 11:33 02/17/22 15:35 207-08-9 Benzoic Acid ND ug/kg 2240 963 1 02/16/22 11:33 02/17/22 15:35 65-85-0 Benzyl alcohol ND ug/kg 896 339 1 02/16/22 11:33 02/17/22 15:35 100-51-6 4-Bromophenylphenyl ether ND ug/kg 448 172 1 02/16/22 11:33 02/17/22 15:35 101-55-3 Butylbenzylphthalate ND ug/kg 448 189 1 02/16/22 11:33 02/17/22 15:35 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 896 315 1 02/16/22 11:33 02/17/22 15:35 59-50-7 4-Chloroaniline ND ug/kg 896 352 1 02/16/22 11:33 02/17/22 15:35 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 448 186 1 02/16/22 11:33 02/17/22 15:35 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 448 168 1 02/16/22 11:33 02/17/22 15:35 111-44-4 2-Chloronaphthalene ND ug/kg 448 178 1 02/16/22 11:33 02/17/22 15:35 91-58-7 2-Chlorophenol ND ug/kg 448 168 1 02/16/22 11:33 02/17/22 15:35 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 448 167 1 02/16/22 11:33 02/17/22 15:35 7005-72-3 Chrysene ND ug/kg 448 163 1 02/16/22 11:33 02/17/22 15:35 218-01-9 Dibenz(a,h)anthracene ND ug/kg 448 172 1 02/16/22 11:33 02/17/22 15:35 53-70-3 Dibenzofuran ND ug/kg 448 162 1 02/16/22 11:33 02/17/22 15:35 132-64-9 1,2-Dichlorobenzene ND ug/kg 448 162 1 02/16/22 11:33 02/17/22 15:35 95-50-1 1,3-Dichlorobenzene ND ug/kg 448 159 1 02/16/22 11:33 02/17/22 15:35 541-73-1 1,4-Dichlorobenzene ND ug/kg 448 171 1 02/16/22 11:33 02/17/22 15:35 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 896 303 1 02/16/22 11:33 02/17/22 15:35 91-94-1 2,4-Dichlorophenol ND ug/kg 448 175 1 02/16/22 11:33 02/17/22 15:35 120-83-2 Diethylphthalate ND ug/kg 448 164 1 02/16/22 11:33 02/17/22 15:35 84-66-2 2,4-Dimethylphenol ND ug/kg 448 186 1 02/16/22 11:33 02/17/22 15:35 105-67-9 Dimethylphthalate ND ug/kg 448 163 1 02/16/22 11:33 02/17/22 15:35 131-11-3 Di-n-butylphthalate ND ug/kg 448 151 1 02/16/22 11:33 02/17/22 15:35 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 896 418 1 02/16/22 11:33 02/17/22 15:35 534-52-1 2,4-Dinitrophenol ND ug/kg 2240 1390 1 02/16/22 11:33 02/17/22 15:35 51-28-5 2,4-Dinitrotoluene ND ug/kg 448 172 1 02/16/22 11:33 02/17/22 15:35 121-14-2 REPORT OF LABORATORY ANALYSIS N2 N2 N2 IL This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 2,6-Dinitrotoluene ND ug/kg 448 164 1 02/16/22 11:33 02/17/22 15:35 606-20-2 Di-n-octylphthalate ND ug/kg 448 177 1 02/16/22 11:33 02/17/22 15:35 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 448 174 1 02/16/22 11:33 02/17/22 15:35 117-81-7 Fluoranthene ND ug/kg 448 153 1 02/16/22 11:33 02/17/22 15:35 206-44-0 Fluorene ND ug/kg 448 158 1 02/16/22 11:33 02/17/22 15:35 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 448 194 1 02/16/22 11:33 02/17/22 15:35 87-68-3 Hexachlorobenzene ND ug/kg 448 175 1 02/16/22 11:33 02/17/22 15:35 118-74-1 Hexachlorocyclopentadiene ND ug/kg 448 257 1 02/16/22 11:33 02/17/22 15:35 77-47-4 Hexachloroethane ND ug/kg 448 171 1 02/16/22 11:33 02/17/22 15:35 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 448 177 1 02/16/22 11:33 02/17/22 15:35 193-39-5 Isophorone ND ug/kg 448 200 1 02/16/22 11:33 02/17/22 15:35 78-59-1 1-Methylnaphthalene ND ug/kg 448 158 1 02/16/22 11:33 02/17/22 15:35 90-12-0 2-Methylnaphthalene ND ug/kg 448 179 1 02/16/22 11:33 02/17/22 15:35 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 448 183 1 02/16/22 11:33 02/17/22 15:35 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 448 181 1 02/16/22 11:33 02/17/22 15:35 15831-10-4 Naphthalene ND ug/kg 448 152 1 02/16/22 11:33 02/17/22 15:35 91-20-3 2-Nitroaniline ND ug/kg 2240 367 1 02/16/22 11:33 02/17/22 15:35 88-74-4 3-Nitroaniline ND ug/kg 2240 352 1 02/16/22 11:33 02/17/22 15:35 99-09-2 4-Nitroaniline ND ug/kg 896 341 1 02/16/22 11:33 02/17/22 15:35 100-01-6 Nitrobenzene ND ug/kg 448 208 1 02/16/22 11:33 02/17/22 15:35 98-95-3 2-Nitrophenol ND ug/kg 448 194 1 02/16/22 11:33 02/17/22 15:35 88-75-5 4-Nitrophenol ND ug/kg 2240 866 1 02/16/22 11:33 02/17/22 15:35 100-02-7 N-Nitrosodimethylamine ND ug/kg 448 151 1 02/16/22 11:33 02/17/22 15:35 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 448 168 1 02/16/22 11:33 02/17/22 15:35 621-64-7 N-Nitrosodiphenylamine ND ug/kg 448 159 1 02/16/22 11:33 02/17/22 15:35 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 448 213 1 02/16/22 11:33 02/17/22 15:35 108-60-1 Pentachlorophenol ND ug/kg 896 439 1 02/16/22 11:33 02/17/22 15:35 87-86-5 Phenanthrene ND ug/kg 448 147 1 02/16/22 11:33 02/17/22 15:35 85-01-8 Phenol ND ug/kg 448 200 1 02/16/22 11:33 02/17/22 15:35 108-95-2 Pyrene ND ug/kg 448 182 1 02/16/22 11:33 02/17/22 15:35 129-00-0 Pyridine ND ug/kg 448 141 1 02/16/22 11:33 02/17/22 15:35 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 448 177 1 02/16/22 11:33 02/17/22 15:35 120-82-1 2,4,5-Trichlorophenol ND ug/kg 448 205 1 02/16/22 11:33 02/17/22 15:35 95-95-4 2,4,6-Trichlorophenol ND ug/kg 448 185 1 02/16/22 11:33 02/17/22 15:35 88-06-2 Surrogates Nitrobenzene-d5 (S) 63 % 21-130 1 02/16/22 11:33 02/17/22 15:35 4165-60-0 2-Fluorobiphenyl (S) 51 % 19-130 1 02/16/22 11:33 02/17/22 15:35 321-60-8 Terphenyl-d14 (S) 56 % 15-130 1 02/16/22 11:33 02/17/22 15:35 1718-51-0 Phenol-d6 (S) 61 % 18-130 1 02/16/22 11:33 02/17/22 15:35 13127-88-3 2-Fluorophenol (S) 60 % 18-130 1 02/16/22 11:33 02/17/22 15:35 367-12-4 2,4,6-Tribromophenol (S) 57 % 18-130 1 02/16/22 11:33 02/17/22 15:35 118-79-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte Acetone ND ug/kg 190 61.0 1 02/15/22 21:19 02/17/22 20:09 67-64-1 Benzene ND ug/kg 9.5 3.8 1 02/15/22 21:19 02/17/22 20:09 71-43-2 Bromobenzene ND ug/kg 9.5 3.1 1 02/15/22 21:19 02/17/22 20:09 108-86-1 Bromochloromethane ND ug/kg 9.5 2.8 1 02/15/22 21:19 02/17/22 20:09 74-97-5 Bromodichloromethane ND ug/kg 9.5 3.7 1 02/15/22 21:19 02/17/22 20:09 75-27-4 Bromoform ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 20:09 75-25-2 Bromomethane ND ug/kg 19.0 15.0 1 02/15/22 21:19 02/17/22 20:09 74-83-9 2-Butanone (MEK) ND ug/kg 190 45.6 1 02/15/22 21:19 02/17/22 20:09 78-93-3 n-Butylbenzene ND ug/kg 9.5 4.5 1 02/15/22 21:19 02/17/22 20:09 104-51-8 sec-Butylbenzene ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 20:09 135-98-8 tert-Butyl benzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 20:09 98-06-6 Carbon tetrachloride ND ug/kg 9.5 3.6 1 02/15/22 21:19 02/17/22 20:09 56-23-5 Chlorobenzene ND ug/kg 9.5 1.8 1 02/15/22 21:19 02/17/22 20:09 108-90-7 Chloroethane ND ug/kg 19.0 7.3 1 02/15/22 21:19 02/17/22 20:09 75-00-3 Chloroform ND ug/kg 9.5 5.8 1 02/15/22 21:19 02/17/22 20:09 67-66-3 Chloromethane ND ug/kg 19.0 8.0 1 02/15/22 21:19 02/17/22 20:09 74-87-3 2-Chlorotoluene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 20:09 95-49-8 4-Chlorotoluene ND ug/kg 9.5 1.7 1 02/15/22 21:19 02/17/22 20:09 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 9.5 3.7 1 02/15/22 21:19 02/17/22 20:09 96-12-8 Dibromochloromethane ND ug/kg 9.5 5.3 1 02/15/22 21:19 02/17/22 20:09 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 20:09 106-93-4 Dibromomethane ND ug/kg 9.5 2.0 1 02/15/22 21:19 02/17/22 20:09 74-95-3 1,2-Dichlorobenzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 20:09 95-50-1 1,3-Dichlorobenzene ND ug/kg 9.5 2.9 1 02/15/22 21:19 02/17/22 20:09 541-73-1 1,4-Dichlorobenzene ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 20:09 106-46-7 Dichlorodifluoromethane ND ug/kg 19.0 4.1 1 02/15/22 21:19 02/17/22 20:09 75-71-8 1,1-Dichloroethane ND ug/kg 9.5 3.9 1 02/15/22 21:19 02/17/22 20:09 75-34-3 1,2-Dichloroethane ND ug/kg 9.5 6.3 1 02/15/22 21:19 02/17/22 20:09 107-06-2 1,1-Dichloroethene ND ug/kg 9.5 3.9 1 02/15/22 21:19 02/17/22 20:09 75-35-4 cis-1,2-Dichloroethene ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 20:09 156-59-2 trans-1,2-Dichloroethene ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 20:09 156-60-5 1,2-Dichloropropane ND ug/kg 9.5 2.9 1 02/15/22 21:19 02/17/22 20:09 78-87-5 1,3-Dichloropropane ND ug/kg 9.5 3.0 1 02/15/22 21:19 02/17/22 20:09 142-28-9 2,2-Dichloropropane ND ug/kg 9.5 3.1 1 02/15/22 21:19 02/17/22 20:09 594-20-7 1,1-Dichloropropene ND ug/kg 9.5 4.6 1 02/15/22 21:19 02/17/22 20:09 563-58-6 cis-1,3-Dichloropropene ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 20:09 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 9.5 3.3 1 02/15/22 21:19 02/17/22 20:09 10061-02-6 Diisopropyl ether ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 20:09 108-20-3 Ethylbenzene ND ug/kg 9.5 4.4 1 02/15/22 21:19 02/17/22 20:09 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 19.0 15.5 1 02/15/22 21:19 02/17/22 20:09 87-68-3 2-Hexanone ND ug/kg 95.0 9.2 1 02/15/22 21:19 02/17/22 20:09 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 20:09 98-82-8 p-Isopropyltoluene ND ug/kg 9.5 4.7 1 02/15/22 21:19 02/17/22 20:09 99-87-6 Methylene Chloride ND ug/kg 38.0 26.0 1 02/15/22 21:19 02/17/22 20:09 75-09-2 REPORT OF LABORATORY ANALYSIS IK,L1 v2 v2 v2 This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 104 laceAnalytical" WWW.pacalahs.0 m Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: CCW-006 Pace Project No.: 92588327 Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 4-Methyl-2-pentanone (MIBK) ND ug/kg 95.0 9.2 1 02/15/22 21:19 02/17/22 20:09 108-10-1 Methyl-tert-butyl ether ND ug/kg 9.5 3.6 1 02/15/22 21:19 02/17/22 20:09 1634-04-4 Naphthalene ND ug/kg 9.5 5.0 1 02/15/22 21:19 02/17/22 20:09 91-20-3 n-Propylbenzene ND ug/kg 9.5 3.4 1 02/15/22 21:19 02/17/22 20:09 103-65-1 Styrene ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 20:09 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 9.5 3.6 1 02/15/22 21:19 02/17/22 20:09 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 20:09 79-34-5 Tetrachloroethene ND ug/kg 9.5 3.0 1 02/15/22 21:19 02/17/22 20:09 127-18-4 Toluene ND ug/kg 9.5 2.7 1 02/15/22 21:19 02/17/22 20:09 108-88-3 1,2,3-Trichlorobenzene ND ug/kg 9.5 7.7 1 02/15/22 21:19 02/17/22 20:09 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 9.5 8.0 1 02/15/22 21:19 02/17/22 20:09 120-82-1 1,1,1-Trichloroethane ND ug/kg 9.5 4.9 1 02/15/22 21:19 02/17/22 20:09 71-55-6 1,1,2-Trichloroethane ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 20:09 79-00-5 Trichloroethene ND ug/kg 9.5 2.5 1 02/15/22 21:19 02/17/22 20:09 79-01-6 Trichlorofluoromethane ND ug/kg 9.5 5.2 1 02/15/22 21:19 02/17/22 20:09 75-69-4 1,2,3-Trichloropropane ND ug/kg 9.5 4.8 1 02/15/22 21:19 02/17/22 20:09 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 9.5 2.6 1 02/15/22 21:19 02/17/22 20:09 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 9.5 3.2 1 02/15/22 21:19 02/17/22 20:09 108-67-8 Vinyl acetate ND ug/kg 95.0 6.9 1 02/15/22 21:19 02/17/22 20:09 108-05-4 Vinyl chloride ND ug/kg 19.0 4.8 1 02/15/22 21:19 02/17/22 20:09 75-01-4 v2 Xylene (Total) ND ug/kg 19.0 5.4 1 02/15/22 21:19 02/17/22 20:09 1330-20-7 m&p-Xylene ND ug/kg 19.0 6.5 1 02/15/22 21:19 02/17/22 20:09 179601-23-1 o-Xylene ND ug/kg 9.5 4.2 1 02/15/22 21:19 02/17/22 20:09 95-47-6 Surrogates Toluene-d8 (S) 100 % 70-130 1 02/15/22 21:19 02/17/22 20:09 2037-26-5 4-Bromofluorobenzene (S) 99 % 69-134 1 02/15/22 21:19 02/17/22 20:09 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 02/15/22 21:19 02/17/22 20:09 17060-07-0 Percent Moisture Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture 27.1 % 0.10 0.10 1 02/15/22 17:11 N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678726 Analysis Method: EPA 8015C QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327001 METHOD BLANK: 3551778 Matrix: Solid Associated Lab Samples: 92588327001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Gas Range Organics (C6-C10) mg/kg ND 6.0 1.5 02/16/22 13:18 4-Bromofluorobenzene (S) % 86 66-131 02/16/22 13:18 LABORATORY CONTROL SAMPLE: 3551779 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/kg 49.7 48.8 98 70-130 4-Bromofluorobenzene (S) % 89 66-131 MATRIX SPIKE SAMPLE: 3551781 35696367001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/kg 294 74.9 373 106 70-145 4-Bromofluorobenzene (S) % 161 66-131 S2 SAMPLE DUPLICATE: 3551780 92588181001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Gas Range Organics (C6-C10) mg/kg ND ND 30 4-Bromofluorobenzene (S) % 86 84 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 679111 Analysis Method: EPA 8015C QC Batch Method: EPA 5030B Analysis Description: Gasoline Range Organics Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327002 METHOD BLANK: 3553476 Matrix: Solid Associated Lab Samples: 92588327002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Gas Range Organics (C6-C10) mg/kg ND 6.0 1.5 02/17/22 13:51 4-Bromofluorobenzene (S) % 87 66-131 02/17/22 13:51 LABORATORY CONTROL SAMPLE: 3553477 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/kg 50 48.3 97 70-130 4-Bromofluorobenzene (S) % 92 66-131 MATRIX SPIKE SAMPLE: 3553479 92587641001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Gas Range Organics (C6-C10) mg/kg ND 61.5 61.5 100 70-145 4-Bromofluorobenzene (S) % 89 66-131 SAMPLE DUPLICATE: 3553478 35696367002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Gas Range Organics (C6-C10) mg/kg 8.9 8.4 5 30 4-Bromofluorobenzene (S) % 81 81 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 104 laceAnalytical" WWW.pacalabs.Com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678754 Analysis Method: MADEP VPH QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 METHOD BLANK: 3551916 Matrix: Solid Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Aliphatic (C05-CO8) mg/kg ND 2.5 2.5 02/16/22 15:29 N2 Aromatic (C09-C10) mg/kg ND 2.5 2.5 02/16/22 15:29 N2 4-Bromofluorobenzene (FID) (S) % 97 70-130 02/16/22 15:29 4-Bromofluorobenzene (PID) (S) % 83 70-130 02/16/22 15:29 LABORATORY CONTROL SAMPLE & LCSD: 3551917 3551918 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) mg/kg 14.9 14.4 13.1 97 88 70-130 10 25 N2 Aromatic (C09-C10) mg/kg 5 4.2 4.2 85 84 70-130 1 25 N2 4-Bromofluorobenzene (FID) (S) % 97 98 70-130 4-Bromofluorobenzene (PID) (S) % 84 84 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678538 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 METHOD BLANK: 3551065 Matrix: Solid Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 1.9 02/17/22 12:12 1,1,1-Trichloroethane ug/kg ND 5.0 2.6 02/17/22 12:12 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 1.3 02/17/22 12:12 1,1,2-Trichloroethane ug/kg ND 5.0 1.7 02/17/22 12:12 1,1-Dichloroethane ug/kg ND 5.0 2.1 02/17/22 12:12 1,1-Dichloroethene ug/kg ND 5.0 2.1 02/17/22 12:12 1,1-Dichloropropene ug/kg ND 5.0 2.4 02/17/22 12:12 1,2,3-Trichlorobenzene ug/kg ND 5.0 4.0 02/17/22 12:12 1,2,3-Trichloropropane ug/kg ND 5.0 2.5 02/17/22 12:12 1,2,4-Trichlorobenzene ug/kg ND 5.0 4.2 02/17/22 12:12 1,2,4-Trimethylbenzene ug/kg ND 5.0 1.4 02/17/22 12:12 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 1.9 02/17/22 12:12 1,2-Dibromoethane (EDB) ug/kg ND 5.0 2.2 02/17/22 12:12 1,2-Dichlorobenzene ug/kg ND 5.0 1.8 02/17/22 12:12 1,2-Dichloroethane ug/kg ND 5.0 3.3 02/17/22 12:12 1,2-Dichloropropane ug/kg ND 5.0 1.5 02/17/22 12:12 1,3,5-Trimethylbenzene ug/kg ND 5.0 1.7 02/17/22 12:12 1,3-Dichlorobenzene ug/kg ND 5.0 1.6 02/17/22 12:12 1,3-Dichloropropane ug/kg ND 5.0 1.6 02/17/22 12:12 1,4-Dichlorobenzene ug/kg ND 5.0 1.3 02/17/22 12:12 2,2-Dichloropropane ug/kg ND 5.0 1.6 02/17/22 12:12 2-Butanone (MEK) ug/kg ND 100 24.0 02/17/22 12:12 2-Chlorotoluene ug/kg ND 5.0 1.8 02/17/22 12:12 2-Hexanone ug/kg ND 50.0 4.8 02/17/22 12:12 4-Chlorotoluene ug/kg ND 5.0 0.88 02/17/22 12:12 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 4.8 02/17/22 12:12 Acetone ug/kg ND 100 32.1 02/17/22 12:12 Benzene ug/kg ND 5.0 2.0 02/17/22 12:12 Bromobenzene ug/kg ND 5.0 1.6 02/17/22 12:12 Bromochloromethane ug/kg ND 5.0 1.5 02/17/22 12:12 Bromodichloromethane ug/kg ND 5.0 1.9 02/17/22 12:12 Bromoform ug/kg ND 5.0 1.8 02/17/22 12:12 Bromomethane ug/kg ND 10.0 7.9 02/17/22 12:12 Carbon tetrachloride ug/kg ND 5.0 1.9 02/17/22 12:12 Chlorobenzene ug/kg ND 5.0 0.96 02/17/22 12:12 Chloroethane ug/kg ND 10.0 3.9 02/17/22 12:12 Chloroform ug/kg ND 5.0 3.0 02/17/22 12:12 Chloromethane ug/kg ND 10.0 4.2 02/17/22 12:12 cis-1,2-Dichloroethene ug/kg ND 5.0 1.7 02/17/22 12:12 IK v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 METHOD BLANK: 3551065 Matrix: Solid Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers cis-1,3-Dichloropropene ug/kg ND 5.0 1.4 02/17/22 12:12 Dibromochloromethane ug/kg ND 5.0 2.8 02/17/22 12:12 Dibromomethane ug/kg ND 5.0 1.1 02/17/22 12:12 Dichlorodifluoromethane ug/kg ND 10.0 2.2 02/17/22 12:12 Diisopropyl ether ug/kg ND 5.0 1.4 02/17/22 12:12 Ethylbenzene ug/kg ND 5.0 2.3 02/17/22 12:12 Hexachloro-1,3-butadiene ug/kg ND 10.0 8.2 02/17/22 12:12 Isopropylbenzene (Cumene) ug/kg ND 5.0 1.7 02/17/22 12:12 m&p-Xylene ug/kg ND 10.0 3.4 02/17/22 12:12 Methyl-tert-butyl ether ug/kg ND 5.0 1.9 02/17/22 12:12 Methylene Chloride ug/kg ND 20.0 13.7 02/17/22 12:12 n-Butylbenzene ug/kg ND 5.0 2.4 02/17/22 12:12 n-Propylbenzene ug/kg ND 5.0 1.8 02/17/22 12:12 Naphthalene ug/kg ND 5.0 2.6 02/17/22 12:12 o-Xylene ug/kg ND 5.0 2.2 02/17/22 12:12 p-Isopropyltoluene ug/kg ND 5.0 2.5 02/17/22 12:12 sec-Butylbenzene ug/kg ND 5.0 2.2 02/17/22 12:12 Styrene ug/kg ND 5.0 1.3 02/17/22 12:12 tert-Butyl benzene ug/kg ND 5.0 1.8 02/17/22 12:12 Tetrachloroethene ug/kg ND 5.0 1.6 02/17/22 12:12 Toluene ug/kg ND 5.0 1.4 02/17/22 12:12 trans-1,2-Dichloroethene ug/kg ND 5.0 1.8 02/17/22 12:12 trans- 1,3-Dichloropropene ug/kg ND 5.0 1.7 02/17/22 12:12 Trichloroethene ug/kg ND 5.0 1.3 02/17/22 12:12 Trichlorofluoromethane ug/kg ND 5.0 2.8 02/17/22 12:12 Vinyl acetate ug/kg ND 50.0 3.6 02/17/22 12:12 Vinyl chloride ug/kg ND 10.0 2.5 02/17/22 12:12 Xylene (Total) ug/kg ND 10.0 2.8 02/17/22 12:12 1,2-Dichloroethane-d4 (S) % 109 70-130 02/17/22 12:12 4-Bromofluorobenzene (S) % 102 69-134 02/17/22 12:12 Toluene-d8 (S) % 102 70-130 02/17/22 12:12 v2 v2 LABORATORY CONTROL SAMPLE: 3551066 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 1250 1120 90 70-130 1,1,1-Trichloroethane ug/kg 1250 1090 87 70-130 1,1,2,2-Tetrachloroethane ug/kg 1250 1050 84 70-130 1,1,2-Trichloroethane ug/kg 1250 1090 87 70-130 1,1-Dichloroethane ug/kg 1250 1070 85 70-130 1,1-Dichloroethene ug/kg 1250 1100 88 70-130 1,1-Dichloropropene ug/kg 1250 1080 87 70-130 1,2,3-Trichlorobenzene ug/kg 1250 1140 91 65-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: CCW-006 Pace Project No.: 92588327 LABORATORY CONTROL SAMPLE: 3551066 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,2,3-Trichloropropane ug/kg 1250 1060 85 70-130 1,2,4-Trichlorobenzene ug/kg 1250 1150 92 68-130 1,2,4-Trimethylbenzene ug/kg 1250 1070 86 70-130 1,2-Dibromo-3-chloropropane ug/kg 1250 1100 88 70-130 1,2-Dibromoethane (EDB) ug/kg 1250 1060 85 70-130 1,2-Dichlorobenzene ug/kg 1250 1100 88 70-130 1,2-Dichloroethane ug/kg 1250 1070 86 63-130 1,2-Dichloropropane ug/kg 1250 1080 86 70-130 1,3,5-Trimethylbenzene ug/kg 1250 1120 89 70-130 1,3-Dichlorobenzene ug/kg 1250 1130 90 70-130 1,3-Dichloropropane ug/kg 1250 1060 85 70-130 1,4-Dichlorobenzene ug/kg 1250 1120 89 70-130 2,2-Dichloropropane ug/kg 1250 1120 89 66-130 2-Butanone (MEK) ug/kg 2500 2070 83 70-130 2-Chlorotoluene ug/kg 1250 1090 87 70-130 2-Hexanone ug/kg 2500 2110 84 70-130 4-Chlorotoluene ug/kg 1250 1050 84 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 2500 2190 88 70-130 Acetone ug/kg 2500 2160 86 69-130 Benzene ug/kg 1250 1030 83 70-130 Bromobenzene ug/kg 1250 1120 90 70-130 Bromochloromethane ug/kg 1250 1090 87 70-130 Bromodichloromethane ug/kg 1250 1130 90 69-130 Bromoform ug/kg 1250 1170 94 70-130 Bromomethane ug/kg 1250 1830 146 52-130lK,L1 Carbon tetrachloride ug/kg 1250 1180 94 70-130 Chlorobenzene ug/kg 1250 1100 88 70-130 Chloroethane ug/kg 1250 1230 99 65-130 v3 Chloroform ug/kg 1250 1100 88 70-130 Chloromethane ug/kg 1250 1120 90 55-130 v3 cis-1,2-Dichloroethene ug/kg 1250 1090 87 70-130 cis-1,3-Dichloropropene ug/kg 1250 1080 86 70-130 Dibromochloromethane ug/kg 1250 1060 85 70-130 Dibromomethane ug/kg 1250 1120 89 70-130 Dichlorodifluoromethane ug/kg 1250 1360 109 45-156 v3 Diisopropyl ether ug/kg 1250 1020 82 70-130 Ethylbenzene ug/kg 1250 1050 84 70-130 Hexachloro-1,3-butadiene ug/kg 1250 1300 104 66-130 Isopropylbenzene (Cumene) ug/kg 1250 1170 93 70-130 m&p-Xylene ug/kg 2500 2250 90 70-130 Methyl-tert-butyl ether ug/kg 1250 1020 82 70-130 Methylene Chloride ug/kg 1250 1180 95 65-130 n-Butylbenzene ug/kg 1250 1160 93 67-130 n-Propylbenzene ug/kg 1250 1070 86 70-130 Naphthalene ug/kg 1250 1070 85 70-130 o-Xylene ug/kg 1250 1120 89 70-130 p-Isopropyltoluene ug/kg 1250 1170 94 67-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 LABORATORY CONTROL SAMPLE: Parameter 3551066 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers sec-Butylbenzene ug/kg 1250 1120 90 69-130 Styrene ug/kg 1250 1160 93 70-130 tert-Butyl benzene ug/kg 1250 1100 88 67-130 Tetrachloroethene ug/kg 1250 1080 87 70-130 Toluene ug/kg 1250 1070 86 70-130 trans-1,2-Dichloroethene ug/kg 1250 1090 87 70-130 trans- 1,3-Dichloropropene ug/kg 1250 1130 90 68-130 Trichloroethene ug/kg 1250 1060 84 70-130 Trichlorofluoromethane ug/kg 1250 1060 85 70-130 Vinyl acetate ug/kg 2500 2510 101 70-130 Vinyl chloride ug/kg 1250 1130 90 61-130 v3 Xylene (Total) ug/kg 3750 3360 90 70-130 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 101 69-134 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: Parameter 3551067 Units 92588327003 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 1160 892 77 70-131 1,1,1-Trichloroethane ug/kg ND 1160 907 78 65-133 1,1,2,2-Tetrachloroethane ug/kg ND 1160 816 70 66-130 1,1,2-Trichloroethane ug/kg ND 1160 855 73 66-133 1,1-Dichloroethane ug/kg ND 1160 906 78 65-130 1,1-Dichloroethene ug/kg ND 1160 916 79 10-158 1,1-Dichloropropene ug/kg ND 1160 879 75 68-133 1,2,3-Trichlorobenzene ug/kg ND 1160 905 78 27-138 1,2,3-Trichloropropane ug/kg ND 1160 764 66 67-130 M1 1,2,4-Trichlorobenzene ug/kg ND 1160 867 74 51-134 1,2,4-Trimethylbenzene ug/kg 6.1J 1160 814 69 63-136 1,2-Dibromo-3-chloropropane ug/kg ND 1160 760 65 32-130 1,2-Dibromoethane (EDB) ug/kg ND 1160 881 76 70-130 1,2-Dichlorobenzene ug/kg ND 1160 883 76 69-130 1,2-Dichloroethane ug/kg ND 1160 864 74 59-130 1,2-Dichloropropane ug/kg ND 1160 877 75 70-130 1,3,5-Trimethylbenzene ug/kg ND 1160 861 74 65-137 1,3-Dichlorobenzene ug/kg ND 1160 883 76 70-130 1,3-Dichloropropane ug/kg ND 1160 876 75 70-130 1,4-Dichlorobenzene ug/kg ND 1160 828 71 68-130 2,2-Dichloropropane ug/kg ND 1160 612 53 32-130 2-Butanone (MEK) ug/kg ND 2330 1600 69 10-136 2-Chlorotoluene ug/kg ND 1160 825 71 69-141 2-Hexanone ug/kg ND 2330 1510 65 10-144 4-Chlorotoluene ug/kg ND 1160 770 66 70-132 M1 4-Methyl-2-pentanone (MIBK) ug/kg ND 2330 1620 70 25-143 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 MATRIX SPIKE SAMPLE: 3551067 92588327003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Acetone ug/kg ND 2330 1440 62 10-130 Benzene ug/kg 6.9J 1160 894 76 67-130 Bromobenzene ug/kg ND 1160 898 77 70-130 Bromochloromethane ug/kg ND 1160 877 75 69-134 Bromodichloromethane ug/kg ND 1160 875 75 64-130 Bromoform ug/kg ND 1160 788 68 62-130 Bromomethane ug/kg ND 1160 742 64 20-1761K Carbon tetrachloride ug/kg ND 1160 924 79 65-140 Chlorobenzene ug/kg ND 1160 896 77 70-130 Chloroethane ug/kg ND 1160 449 39 10-130 v3 Chloroform ug/kg ND 1160 920 79 63-130 Chloromethane ug/kg ND 1160 930 80 58-130 v3 cis-1,2-Dichloroethene ug/kg ND 1160 899 77 66-130 cis-1,3-Dichloropropene ug/kg ND 1160 797 68 67-130 Dibromochloromethane ug/kg ND 1160 796 68 67-130 Dibromomethane ug/kg ND 1160 899 77 63-131 Dichlorodifluoromethane ug/kg ND 1160 858 74 44-180 v3 Diisopropyl ether ug/kg ND 1160 823 71 63-130 Ethylbenzene ug/kg 6.OJ 1160 842 72 66-130 Hexachloro-1,3-butadiene ug/kg ND 1160 882 76 64-150 Isopropylbenzene (Cumene) ug/kg ND 1160 915 79 69-135 m&p-Xylene ug/kg 11.3J 2330 1780 76 60-133 Methyl-tert-butyl ether ug/kg ND 1160 834 72 65-130 Methylene Chloride ug/kg ND 1160 961 81 61-130 n-Butylbenzene ug/kg ND 1160 761 65 65-140 n-Propylbenzene ug/kg ND 1160 784 67 67-140 Naphthalene ug/kg 17.7 1160 877 74 15-145 o-Xylene ug/kg 6.2J 1160 891 76 66-133 p-Isopropyltoluene ug/kg ND 1160 838 72 56-147 sec-Butylbenzene ug/kg ND 1160 850 73 65-139 Styrene ug/kg ND 1160 896 77 70-132 tert-Butyl benzene ug/kg ND 1160 878 75 62-135 Tetrachloroethene ug/kg ND 1160 813 70 70-135 Toluene ug/kg 19.7 1160 911 77 67-130 trans-1,2-Dichloroethene ug/kg ND 1160 917 79 69-130 trans- 1,3-Dichloropropene ug/kg ND 1160 819 70 62-130 Trichloroethene ug/kg ND 1160 891 77 70-135 Trichlorofluoromethane ug/kg ND 1160 579 50 10-130 Vinyl acetate ug/kg ND 2330 1780 76 53-130 Vinyl chloride ug/kg ND 1160 843 72 61-148 v3 Xylene (Total) ug/kg 17AJ 3500 2670 76 63-132 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 100 69-134 Toluene-d8 (S) % 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 SAMPLE DUPLICATE: 3551068 Parameter Units 92588327004 Result Dup Result Max RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND ND 30 1,1,1-Trichloroethane ug/kg ND ND 30 1,1,2,2-Tetrachloroethane ug/kg ND ND 30 1,1,2-Trichloroethane ug/kg ND ND 30 1,1-Dichloroethane ug/kg ND ND 30 1,1-Dichloroethene ug/kg ND ND 30 1,1-Dichloropropene ug/kg ND ND 30 1,2,3-Trichlorobenzene ug/kg ND ND 30 1,2,3-Trichloropropane ug/kg ND ND 30 1,2,4-Trichlorobenzene ug/kg ND ND 30 1,2,4-Trimethylbenzene ug/kg 76.6 76.4 0 30 1,2-Dibromo-3-chloropropane ug/kg ND ND 30 1,2-Dibromoethane (EDB) ug/kg ND ND 30 1,2-Dichlorobenzene ug/kg ND ND 30 1,2-Dichloroethane ug/kg ND ND 30 1,2-Dichloropropane ug/kg ND ND 30 1,3,5-Trimethylbenzene ug/kg 32.7 ND 30 1,3-Dichlorobenzene ug/kg ND ND 30 1,3-Dichloropropane ug/kg ND ND 30 1,4-Dichlorobenzene ug/kg ND ND 30 2,2-Dichloropropane ug/kg ND ND 30 2-Butanone (MEK) ug/kg ND ND 30 2-Chlorotoluene ug/kg ND ND 30 2-Hexanone ug/kg ND ND 30 4-Chlorotoluene ug/kg ND ND 30 4-Methyl-2-pentanone (MIBK) ug/kg ND ND 30 Acetone ug/kg ND ND 30 Benzene ug/kg ND ND 30 Bromobenzene ug/kg ND ND 30 Bromochloromethane ug/kg ND ND 30 Bromodichloromethane ug/kg ND ND 30 Bromoform ug/kg ND ND 30 Bromomethane ug/kg ND ND 301K Carbon tetrachloride ug/kg ND ND 30 Chlorobenzene ug/kg ND ND 30 Chloroethane ug/kg ND ND 30 v2 Chloroform ug/kg ND ND 30 Chloromethane ug/kg ND ND 30 v2 cis-1,2-Dichloroethene ug/kg ND ND 30 cis-1,3-Dichloropropene ug/kg ND ND 30 Dibromochloromethane ug/kg ND ND 30 Dibromomethane ug/kg ND ND 30 Dichlorodifluoromethane ug/kg ND ND 30 v2 Diisopropyl ether ug/kg ND ND 30 Ethylbenzene ug/kg 10.8 11.3 5 30 Hexachloro-1,3-butadiene ug/kg ND ND 30 Isopropylbenzene (Cumene) ug/kg 6.5J ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 SAMPLE DUPLICATE: 3551068 Parameter Units 92588327004 Result Dup Result m&p-Xylene ug/kg 34.9 34.6 Methyl-tert-butyl ether ug/kg ND ND Methylene Chloride ug/kg ND ND n-Butylbenzene ug/kg ND ND n-Propylbenzene ug/kg ND ND Naphthalene ug/kg 65.3 70.3 o-Xylene ug/kg 18.7 17.9 p-Isopropyltoluene ug/kg ND ND sec-Butylbenzene ug/kg ND ND Styrene ug/kg ND ND tert-Butyl benzene ug/kg ND ND Tetrachloroethene ug/kg ND ND Toluene ug/kg 8.91 9.9 trans-1,2-Dichloroethene ug/kg ND ND trans- 1,3-Dichloropropene ug/kg ND ND Trichloroethene ug/kg ND ND Trichlorofluoromethane ug/kg ND ND Vinyl acetate ug/kg ND ND Vinyl chloride ug/kg ND ND Xylene (Total) ug/kg 53.6 52.4 1,2-Dichloroethane-d4 (S) % 95 93 4-Bromofluorobenzene (S) % 104 99 Toluene-d8 (S) % 99 99 RPD Max RPD Qualifiers 1 30 30 30 30 30 7 30 5 30 30 30 30 30 30 30 30 30 30 30 30 30 v2 2 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678539 Analysis Method: EPA 8015C QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327001, 92588327002 METHOD BLANK: 3551069 Matrix: Solid Associated Lab Samples: 92588327001, 92588327002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Diesel Range Organics(C10-C28) mg/kg ND 5.0 3.6 02/16/22 13:28 n-Pentacosane (S) % 77 32-130 02/16/22 13:28 LABORATORY CONTROL SAMPLE: 3551070 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Diesel Range Organics(C10-C28) mg/kg 67.1 50.0 74 47-130 n-Pentacosane (S) % 79 32-130 MATRIX SPIKE SAMPLE: 3551071 92588181001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Diesel Range Organics(C10-C28) mg/kg ND 87.4 72.8 77 10-133 n-Pentacosane(S) % 74 32-130 SAMPLE DUPLICATE: 3551072 92588041001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Diesel Range Organics(C10-C28) mg/kg 26600 26500 0 30 n-Pentacosane (S) % 0 0 S4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678638 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 METHOD BLANK: 3551319 Matrix: Solid Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 333 131 02/17/22 08:54 1,2-Dichlorobenzene ug/kg ND 333 120 02/17/22 08:54 1,3-Dichlorobenzene ug/kg ND 333 118 02/17/22 08:54 1,4-Dichlorobenzene ug/kg ND 333 127 02/17/22 08:54 1-Methylnaphthalene ug/kg ND 333 117 02/17/22 08:54 2,2'-Oxybis(1-chloropropane) ug/kg ND 333 159 02/17/22 08:54 2,4,5-Trichlorophenol ug/kg ND 333 153 02/17/22 08:54 2,4,6-Trichlorophenol ug/kg ND 333 137 02/17/22 08:54 2,4-DichIorophenol ug/kg ND 333 130 02/17/22 08:54 2,4-Dimethylphenol ug/kg ND 333 138 02/17/22 08:54 2,4-Dinitrophenol ug/kg ND 1670 1030 02/17/22 08:54 2,4-Dinitrotoluene ug/kg ND 333 128 02/17/22 08:54 2,6-Dinitrotoluene ug/kg ND 333 122 02/17/22 08:54 2-Chloronaphthalene ug/kg ND 333 132 02/17/22 08:54 2-Chlorophenol ug/kg ND 333 125 02/17/22 08:54 2-Methylnaphthalene ug/kg ND 333 133 02/17/22 08:54 2-Methylphenol(o-Cresol) ug/kg ND 333 136 02/17/22 08:54 2-Nitroaniline ug/kg ND 1670 273 02/17/22 08:54 2-Nitrophenol ug/kg ND 333 144 02/17/22 08:54 3&4-Methylphenol (m&p Cresol) ug/kg ND 333 134 02/17/22 08:54 3,3'-Dichlorobenzidine ug/kg ND 667 225 02/17/22 08:54 3-Nitroaniline ug/kg ND 1670 262 02/17/22 08:54 4,6-Dinitro-2-methyl phenol ug/kg ND 667 311 02/17/22 08:54 4-Bromophenylphenyl ether ug/kg ND 333 128 02/17/22 08:54 4-Chloro-3-methyl phenol ug/kg ND 667 234 02/17/22 08:54 4-Chloroaniline ug/kg ND 667 262 02/17/22 08:54 4-Chlorophenylphenyl ether ug/kg ND 333 124 02/17/22 08:54 4-Nitroaniline ug/kg ND 667 254 02/17/22 08:54 4-Nitrophenol ug/kg ND 1670 644 02/17/22 08:54 Acenaphthene ug/kg ND 333 117 02/17/22 08:54 Acenaphthylene ug/kg ND 333 117 02/17/22 08:54 Aniline ug/kg ND 333 130 02/17/22 08:54 Anthracene ug/kg ND 333 109 02/17/22 08:54 Benzo(a)anthracene ug/kg ND 333 111 02/17/22 08:54 Benzo(a)pyrene ug/kg ND 333 115 02/17/22 08:54 Benzo(b)fluoranthene ug/kg ND 333 111 02/17/22 08:54 Benzo(g,h,i)perylene ug/kg ND 333 129 02/17/22 08:54 Benzo(k)fluoranthene ug/kg ND 333 117 02/17/22 08:54 Benzoic Acid ug/kg ND 1670 716 02/17/22 08:54 IL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 METHOD BLANK: 3551319 Matrix: Solid Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009, 92588327010,92588327011,92588327012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzyl alcohol ug/kg ND 667 253 02/17/22 08:54 bis(2-Chloroethoxy)methane ug/kg ND 333 138 02/17/22 08:54 bis(2-Chloroethyl) ether ug/kg ND 333 125 02/17/22 08:54 bis(2-Ethylhexyl)phthalate ug/kg ND 333 129 02/17/22 08:54 Butylbenzylphthalate ug/kg ND 333 140 02/17/22 08:54 Chrysene ug/kg ND 333 121 02/17/22 08:54 Di-n-butylphthalate ug/kg ND 333 112 02/17/22 08:54 Di-n-octylphthalate ug/kg ND 333 131 02/17/22 08:54 Dibenz(a,h)anthracene ug/kg ND 333 128 02/17/22 08:54 Dibenzofuran ug/kg ND 333 120 02/17/22 08:54 Diethylphthalate ug/kg ND 333 122 02/17/22 08:54 Dimethylphthalate ug/kg ND 333 121 02/17/22 08:54 Fluoranthene ug/kg ND 333 114 02/17/22 08:54 Fluorene ug/kg ND 333 117 02/17/22 08:54 Hexachloro-1,3-butadiene ug/kg ND 333 144 02/17/22 08:54 Hexachlorobenzene ug/kg ND 333 130 02/17/22 08:54 Hexachlorocyclopentadiene ug/kg ND 333 191 02/17/22 08:54 Hexachloroethane ug/kg ND 333 127 02/17/22 08:54 Indeno(1,2,3-cd)pyrene ug/kg ND 333 131 02/17/22 08:54 Isophorone ug/kg ND 333 148 02/17/22 08:54 N-Nitroso-di-n-propylamine ug/kg ND 333 125 02/17/22 08:54 N-Nitrosodimethylamine ug/kg ND 333 112 02/17/22 08:54 N-Nitrosodiphenylamine ug/kg ND 333 118 02/17/22 08:54 Naphthalene ug/kg ND 333 113 02/17/22 08:54 Nitrobenzene ug/kg ND 333 155 02/17/22 08:54 Pentachlorophenol ug/kg ND 667 326 02/17/22 08:54 Phenanthrene ug/kg ND 333 109 02/17/22 08:54 Phenol ug/kg ND 333 148 02/17/22 08:54 Pyrene ug/kg ND 333 135 02/17/22 08:54 Pyridine ug/kg ND 333 105 02/17/22 08:54 2,4,6-Tribromophenol (S) % 70 18-130 02/17/22 08:54 2-Fluorobiphenyl (S) % 64 19-130 02/17/22 08:54 2-Fluorophenol(S) % 69 18-130 02/17/22 08:54 Nitrobenzene-d5 (S) % 67 21-130 02/17/22 08:54 Phenol-d6 (S) % 72 18-130 02/17/22 08:54 Terphenyl-d14 (S) % 70 15-130 02/17/22 08:54 v1 v1 v1 LABORATORY CONTROL SAMPLE: 3551320 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1680 1170 69 47-130 1,2-Dichlorobenzene ug/kg 1680 1110 66 49-130 1,3-Dichlorobenzene ug/kg 1680 1070 64 48-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 LABORATORY CONTROL SAMPLE: Parameter 3551320 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/kg 1680 1090 64 49-130 1-Methylnaphthalene ug/kg 1680 1250 74 54-130 2,2'-Oxybis(1-chloropropane) ug/kg 1680 1210 72 38-130 2,4,5-Trichlorophenol ug/kg 1680 1370 81 49-130 2,4,6-Trichlorophenol ug/kg 1680 1380 82 50-130 2,4-Dichlorophenol ug/kg 1680 1320 78 51-130 2,4-Dimethylphenol ug/kg 1680 1310 78 53-130 2,4-Dinitrophenol ug/kg 8420 6990 83 39-130 2,4-Dinitrotoluene ug/kg 1680 1510 90 53-130 2,6-Dinitrotoluene ug/kg 1680 1480 88 55-130 2-Chloronaphthalene ug/kg 1680 1290 77 48-130 2-Chlorophenol ug/kg 1680 1170 69 54-130 2-Methylnaphthalene ug/kg 1680 1280 76 57-130 2-Methylphenol(o-Cresol) ug/kg 1680 1260 75 50-130 2-Nitroaniline ug/kg 3370 2750 82 49-130 2-Nitrophenol ug/kg 1680 1290 77 50-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1680 1350 80 50-130 3,3'-Dichlorobenzidine ug/kg 3370 2500 74 47-130IL 3-Nitroaniline ug/kg 3370 2820 84 45-130 4,6-Dinitro-2-methyl phenol ug/kg 3370 2970 88 50-142 4-Bromophenylphenyl ether ug/kg 1680 1350 80 55-130 4-ChIoro-3-methyl phenol ug/kg 3370 2740 81 52-130 4-Chloroaniline ug/kg 3370 2460 73 49-130 4-Chlorophenylphenyl ether ug/kg 1680 1340 80 53-130 4-Nitroaniline ug/kg 3370 2780 83 51-130 4-Nitrophenol ug/kg 8420 7330 87 40-130 Acenaphthene ug/kg 1680 1390 82 56-130 Acenaphthylene ug/kg 1680 1320 79 58-130 Aniline ug/kg 1680 1120 66 44-130 Anthracene ug/kg 1680 1340 80 60-130 Benzo(a)anthracene ug/kg 1680 1400 83 59-130 Benzo(a)pyrene ug/kg 1680 1380 82 57-130 Benzo(b)fluoranthene ug/kg 1680 1320 78 54-130 Benzo(g,h,i)perylene ug/kg 1680 1310 78 59-130 Benzo(k)fluoranthene ug/kg 1680 1400 83 54-130 Benzoic Acid ug/kg 8420 5010 60 19-130 Benzyl alcohol ug/kg 3370 2500 74 50-130 bis(2-Chloroethoxy)methane ug/kg 1680 1280 76 55-130 bis(2-Chloroethyl) ether ug/kg 1680 1170 70 53-130 bis(2-Ethylhexyl)phthalate ug/kg 1680 1530 91 58-130 Butylbenzylphthalate ug/kg 1680 1560 93 46-138 Chrysene ug/kg 1680 1410 84 57-130 Di-n-butylphthalate ug/kg 1680 1390 83 57-130 Di-n-octylphthalate ug/kg 1680 1540 91 57-130 Dibenz(a,h)anthracene ug/kg 1680 1260 75 60-130 Dibenzofuran ug/kg 1680 1400 83 54-130 Diethylphthalate ug/kg 1680 1390 82 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 LABORATORY CONTROL SAMPLE: Parameter 3551320 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Dimethylphthalate ug/kg 1680 1400 83 57-130 Fluoranthene ug/kg 1680 1350 80 57-130 Fluorene ug/kg 1680 1410 84 56-130 Hexachloro-1,3-butadiene ug/kg 1680 1050 62 41-130 Hexachlorobenzene ug/kg 1680 1380 82 53-130 Hexachlorocyclopentadiene ug/kg 1680 880 52 23-130 Hexachloroethane ug/kg 1680 1100 65 48-130 Indeno(1,2,3-cd)pyrene ug/kg 1680 1270 76 61-130 Isophorone ug/kg 1680 1290 77 49-130 N-Nitroso-di-n-propylamine ug/kg 1680 1290 77 52-130 N-Nitrosodimethylamine ug/kg 1680 1140 68 45-130 v1 N-Nitrosodiphenylamine ug/kg 1680 1330 79 56-130 Naphthalene ug/kg 1680 1170 69 56-130 Nitrobenzene ug/kg 1680 1220 72 50-130 Pentachlorophenol ug/kg 3370 2770 82 33-130 Phenanthrene ug/kg 1680 1410 84 60-130 Phenol ug/kg 1680 1380 82 54-130 v1 Pyrene ug/kg 1680 1420 85 61-130 Pyridine ug/kg 1680 994 59 35-130 v1 2,4,6-Tribromophenol (S) % 88 18-130 2-Fluorobiphenyl (S) % 68 19-130 2-Fluorophenol(S) % 65 18-130 Nitrobenzene-d5(S) % 67 21-130 Phenol-d6 (S) % 70 18-130 Terphenyl-d14 (S) % 71 15-130 MATRIX SPIKE SAMPLE: Parameter 3551321 Units 92587972001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 2120 1260 60 22-130 1,2-Dichlorobenzene ug/kg ND 2120 1240 59 23-130 1,3-Dichlorobenzene ug/kg ND 2120 1230 58 26-130 1,4-Dichlorobenzene ug/kg ND 2120 1210 57 27-130 1-Methylnaphthalene ug/kg ND 2120 1310 62 30-130 2,2'-Oxybis(1-chloropropane) ug/kg ND 2120 1370 65 30-130 2,4,5-Trichlorophenol ug/kg ND 2120 1500 71 26-130 2,4,6-Trichlorophenol ug/kg ND 2120 1520 71 23-130 2,4-Dichlorophenol ug/kg ND 2120 1430 67 29-130 2,4-Dimethylphenol ug/kg ND 2120 1280 60 13-130 2,4-Dinitrophenol ug/kg ND 10600 5610 53 10-131 2,4-Dinitrotoluene ug/kg ND 2120 1580 74 28-130 2,6-Dinitrotoluene ug/kg ND 2120 1520 72 36-130 2-Chloronaphthalene ug/kg ND 2120 1360 64 27-130 2-Chlorophenol ug/kg ND 2120 1340 63 29-130 2-Methylnaphthalene ug/kg ND 2120 1320 62 29-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 MATRIX SPIKE SAMPLE: 3551321 92587972001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Methylphenol(o-Cresol) ug/kg ND 2120 1340 63 20-130 2-Nitroaniline ug/kg ND 4240 2910 69 29-130 2-Nitrophenol ug/kg ND 2120 1450 68 26-130 3&4-Methyl phenol (m&p Cresol) ug/kg ND 2120 1430 68 10-176 3,3'-Dichlorobenzidine ug/kg ND 4240 2530 60 15-130IL 3-Nitroaniline ug/kg ND 4240 3020 71 28-130 4,6-Dinitro-2-methyl phenol ug/kg ND 4240 3180 75 15-132 4-Bromophenylphenyl ether ug/kg ND 2120 1350 64 35-130 4-Chloro-3-methylphenol ug/kg ND 4240 2900 68 30-130 4-Chloroaniline ug/kg ND 4240 2530 60 28-130 4-Chlorophenylphenyl ether ug/kg ND 2120 1360 64 32-130 4-Nitroaniline ug/kg ND 4240 2920 69 30-130 4-Nitrophenol ug/kg ND 10600 7860 74 17-130 Acenaphthene ug/kg ND 2120 1420 67 29-130 Acenaphthylene ug/kg ND 2120 1370 65 31-130 Aniline ug/kg ND 2120 1100 52 10-130 Anthracene ug/kg ND 2120 1350 64 33-130 Benzo(a)anthracene ug/kg ND 2120 1390 65 32-130 Benzo(a)pyrene ug/kg ND 2120 1380 65 32-130 Benzo(b)fluoranthene ug/kg ND 2120 1340 63 33-130 Benzo(g,h,i)perylene ug/kg ND 2120 1340 63 28-130 Benzo(k)fluoranthene ug/kg ND 2120 1380 65 31-130 Benzoic Acid ug/kg ND 10600 ND 8 10-130 M1 Benzyl alcohol ug/kg ND 4240 2700 64 31-130 bis(2-Chloroethoxy)methane ug/kg ND 2120 1370 64 30-130 bis(2-Chloroethyl) ether ug/kg ND 2120 1300 61 68-130 M1 bis(2-Ethylhexyl)phthalate ug/kg ND 2120 1580 75 40-130 Butylbenzylphthalate ug/kg ND 2120 1530 72 40-130 Chrysene ug/kg ND 2120 1410 66 30-130 Di-n-butylphthalate ug/kg ND 2120 1420 67 41-130 Di-n-octylphthalate ug/kg ND 2120 1580 74 42-130 Dibenz(a,h)anthracene ug/kg ND 2120 1250 59 27-130 Dibenzofuran ug/kg ND 2120 1430 67 32-130 Diethylphthalate ug/kg ND 2120 1430 67 40-130 Dimethylphthalate ug/kg ND 2120 1480 70 37-130 Fluoranthene ug/kg ND 2120 1380 65 26-130 Fluorene ug/kg ND 2120 1420 67 31-130 Hexachloro-1,3-butadiene ug/kg ND 2120 1120 53 20-130 Hexachlorobenzene ug/kg ND 2120 1370 64 29-130 Hexachlorocyclopentadiene ug/kg ND 2120 896 42 10-130 Hexachloroethane ug/kg ND 2120 1240 59 21-130 Indeno(1,2,3-cd)pyrene ug/kg ND 2120 1260 59 28-130 Isophorone ug/kg ND 2120 1340 63 32-130 N-Nitroso-di-n-propylamine ug/kg ND 2120 1340 63 31-130 N-Nitrosodimethylamine ug/kg ND 2120 1280 60 20-130 v1 N-Nitrosodiphenylamine ug/kg ND 2120 1370 65 32-130 Naphthalene ug/kg ND 2120 1270 60 30-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 MATRIX SPIKE SAMPLE: Parameter 3551321 Units 92587972001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Nitrobenzene ug/kg ND 2120 1340 63 25-130 Pentachlorophenol ug/kg ND 4240 3060 72 10-130 Phenanthrene ug/kg ND 2120 1430 67 34-130 Phenol ug/kg ND 2120 1490 70 14-130 v1 Pyrene ug/kg ND 2120 1400 66 31-130 Pyridine ug/kg ND 2120 1170 55 10-130 v1 2,4,6-Tribromophenol (S) % 69 18-130 2-Fluorobiphenyl (S) % 48 19-130 2-Fluorophenol (S) % 56 18-130 Nitrobenzene-d5 (S) % 59 21-130 Phenol-d6 (S) % 59 18-130 Terphenyl-d14 (S) % 53 15-130 SAMPLE DUPLICATE: 3551322 Parameter Units 92587972002 Result Dup Result RPD Max RPD Qualifiers 1,2,4-Trichlorobenzene ug/kg ND ND 30 1,2-Dichlorobenzene ug/kg ND ND 30 1,3-Dichlorobenzene ug/kg ND ND 30 1,4-Dichlorobenzene ug/kg ND ND 30 1-Methylnaphthalene ug/kg ND ND 30 2,2'-Oxybis(1-chloropropane) ug/kg ND ND 30 2,4,5-Trichlorophenol ug/kg ND ND 30 2,4,6-Trichlorophenol ug/kg ND ND 30 2,4-Dichlorophenol ug/kg ND ND 30 2,4-Dimethylphenol ug/kg ND ND 30 2,4-Dinitrophenol ug/kg ND ND 30 2,4-Dinitrotoluene ug/kg ND ND 30 2,6-Dinitrotoluene ug/kg ND ND 30 2-Chloronaphthalene ug/kg ND ND 30 2-Chlorophenol ug/kg ND ND 30 2-Methylnaphthalene ug/kg ND ND 30 2-Methylphenol(o-Cresol) ug/kg ND ND 30 2-Nitroaniline ug/kg ND ND 30 2-Nitrophenol ug/kg ND ND 30 3&4-Methyl phenol (m&p Cresol) ug/kg ND ND 30 3,3'-Dichlorobenzidine ug/kg ND ND 30 IL 3-Nitroaniline ug/kg ND ND 30 4,6-Dinitro-2-methyl phenol ug/kg ND ND 30 4-Bromophenylphenyl ether ug/kg ND ND 30 4-Chloro-3-methylphenol ug/kg ND ND 30 4-Chloroaniline ug/kg ND ND 30 4-Chlorophenylphenyl ether ug/kg ND ND 30 4-Nitroaniline ug/kg ND ND 30 4-Nitrophenol ug/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 SAMPLE DUPLICATE: 3551322 Parameter Units 92587972002 Result Dup Result Acenaphthene ug/kg ND ND Acenaphthylene ug/kg ND ND Aniline ug/kg ND ND Anthracene ug/kg ND ND Benzo(a)anthracene ug/kg ND ND Benzo(a)pyrene ug/kg ND ND Benzo(b)fluoranthene ug/kg ND ND Benzo(g,h,i)perylene ug/kg ND ND Benzo(k)fluoranthene ug/kg ND ND Benzoic Acid ug/kg ND ND Benzyl alcohol ug/kg ND ND bis(2-Chloroethoxy)methane ug/kg ND ND bis(2-Chloroethyl) ether ug/kg ND ND bis(2-Ethylhexyl)phthalate ug/kg ND ND Butylbenzylphthalate ug/kg ND ND Chrysene ug/kg ND ND Di-n-butylphthalate ug/kg ND ND Di-n-octylphthalate ug/kg ND ND Dibenz(a,h)anthracene ug/kg ND ND Dibenzofuran ug/kg ND ND Diethylphthalate ug/kg ND ND Dimethylphthalate ug/kg ND ND Fluoranthene ug/kg ND ND Fluorene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Hexachlorobenzene ug/kg ND ND Hexachlorocyclopentadiene ug/kg ND ND Hexachloroethane ug/kg ND ND Indeno(1,2,3-cd)pyrene ug/kg ND ND Isophorone ug/kg ND ND N-Nitroso-di-n-propylamine ug/kg ND ND N-Nitrosodimethylamine ug/kg ND ND N-Nitrosodiphenylamine ug/kg ND ND Naphthalene ug/kg ND ND Nitrobenzene ug/kg ND ND Pentachlorophenol ug/kg ND ND Phenanthrene ug/kg ND ND Phenol ug/kg ND ND Pyrene ug/kg ND ND Pyridine ug/kg ND ND 2,4,6-Tribromophenol (S) % 71 63 2-Fluorobiphenyl (S) % 57 52 2-Fluorophenol(S) % 68 62 Nitrobenzene-d5 (S) % 68 62 Phenol-d6 (S) % 71 65 Terphenyl-d14 (S) % 61 56 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 v1 30 30 30 30 30 30 v1 30 30 v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 104 laceAnalytical" wwmpacalahs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: CCW-006 Pace Project No.: 92588327 QC Batch: 678506 Analysis Method: SW-846 QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92588327001, 92588327002, 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008,92588327009,92588327010,92588327011,92588327012 SAMPLE DUPLICATE: 3550913 92588181001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 23.0 22.5 2 25 N2 SAMPLE DUPLICATE: 3550914 92588098003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 24.4 21.2 14 25 N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 104 laceAnalytical" WWW.pacalabs,com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: CCW-006 Pace Project No.: 92588327 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re -analysis). S4 Surrogate recovery not evaluated against control limits due to sample dilution. S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 104 laceAnalyticaf` WWW.pacalahs'com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: CCW-006 92588327 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92588327001 UST-1 EPA 3546 678539 EPA 8015C 678806 92588327002 UST-3 EPA 3546 678539 EPA 8015C 678806 92588327001 UST-1 EPA 5030B 678726 EPA 8015C 678770 92588327002 UST-3 EPA 5030B 679111 EPA 8015C 679131 92588327003 UST-1-B MADEP VPH 678754 MADEP VPH 678772 92588327004 UST-1-SW-F MADEP VPH 678754 MADEP VPH 678772 92588327005 UST-1-SW-B MADEP VPH 678754 MADEP VPH 678772 92588327006 UST-1-SW-R MADEP VPH 678754 MADEP VPH 678772 92588327007 UST-1-SW-L MADEP VPH 678754 MADEP VPH 678772 92588327008 UST-2-SW-L MADEP VPH 678754 MADEP VPH 678772 92588327009 UST-2-B MADEP VPH 678754 MADEP VPH 678772 92588327010 UST-2-SW-R MADEP VPH 678754 MADEP VPH 678772 92588327011 UST-2-SW-B MADEP VPH 678754 MADEP VPH 678772 92588327012 UST-2-SW-F MADEP VPH 678754 MADEP VPH 678772 92588327003 UST-1-B EPA 3546 678638 EPA 8270E 679059 92588327004 UST-1-SW-F EPA 3546 678638 EPA 8270E 679059 92588327005 UST-1-SW-B EPA 3546 678638 EPA 8270E 679059 92588327006 UST-1-SW-R EPA 3546 678638 EPA 8270E 679059 92588327007 UST-1-SW-L EPA 3546 678638 EPA 8270E 679059 92588327008 UST-2-SW-L EPA 3546 678638 EPA 8270E 679059 92588327009 UST-2-B EPA 3546 678638 EPA 8270E 679059 92588327010 UST-2-SW-R EPA 3546 678638 EPA 8270E 679059 92588327011 UST-2-SW-B EPA 3546 678638 EPA 8270E 679059 92588327012 UST-2-SW-F EPA 3546 678638 EPA 8270E 679059 92588327003 UST-1-B EPA 5035A/5030B 678538 EPA 8260D 678757 92588327004 UST-1-SW-F EPA 5035A/5030B 678538 EPA 8260D 678757 92588327005 UST-1-SW-B EPA 5035A/5030B 678538 EPA 8260D 678757 92588327006 UST-1-SW-R EPA 5035A/5030B 678538 EPA 8260D 678757 92588327007 UST-1-SW-L EPA 5035A/5030B 678538 EPA 8260D 678757 92588327008 UST-2-SW-L EPA 5035A/5030B 678538 EPA 8260D 678757 92588327009 UST-2-B EPA 5035A/5030B 678538 EPA 8260D 678757 92588327010 UST-2-SW-R EPA 5035A/5030B 678538 EPA 8260D 678757 92588327011 UST-2-SW-B EPA 5035A/5030B 678538 EPA 8260D 678757 92588327012 UST-2-SW-F EPA 5035A/5030B 678538 EPA 8260D 678757 92588327001 UST-1 SW-846 678506 92588327002 UST-3 SW-846 678506 92588327003 UST-1-B SW-846 678506 92588327004 UST-1-SW-F SW-846 678506 92588327005 UST-1-SW-B SW-846 678506 92588327006 UST-1-SW-R SW-846 678506 92588327007 UST-1-SW-L SW-846 678506 92588327008 UST-2-SW-L SW-846 678506 92588327009 UST-2-B SW-846 678506 92588327010 UST-2-SW-R SW-846 678506 92588327011 UST-2-SW-B SW-846 678506 92588327012 UST-2-SW-F SW-846 678506 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 104 laceAnalyticaf` WWW.pacalahs'com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CCW-006 Pace Project No.: 92588327 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 104 Document Name: Dor=ument Revised: November 15, 2021 Sample Condition Upon Recef t (SCUR) Page 1 of I ArraWal n Document No.: Issuing Authority: F-CAR-CS-033-ftev.09 Pace Carolinas Quality Office Laboratory receiving samples: Asheville Eden[] Greenwood ❑ Hurttersvllle � Raleigh[] Mechanicsville[] Atlanta[] Iternersville❑ Up nn Client Name: WO : 92/588327 Receipti.. i, � f f Project ri: t� � [ -q i �— 1 `-i 7" "') + ff II I Courier: Fed Ex ❑UPS LJLJ5P5 OClient ❑ Commercial ❑Pace ❑Other: II 1 I j 92588:327 Custody Seel Present? Oyes ❑No Seals Intact? Des ❑N+ Date/Initlak Person Examining Contents: 13 j Packing Material: ❑Bubble Wrap El -Bubble Bags []None ❑ Other Biological Tissue Fryten? Thermometer: ❑Yes []No -N/A EIJA Gun lD: Z� �� bl ❑VM1 et ❑Blue ❑Kane — - Type of Ice: Correction Factor: Cooler Temp: Add/Subtract (°C) Temp should be above Freezing to G°C —Coal erTemp#orrected-('£-}❑Samples out of temp criteria. Samples ors ice, Cooling process . as USDA Regulated Sail ([] N/A, water sample] Old samples originate in a quarantine zone within the United States: CA, NY, or SC (check mapsl7 aid samples Originate from a Foreign source {Interns ' naliy, El Yes 0116, including Hawaii and Puerto Rico)? ❑Yes ON- [nm men tSl DI sere ua n cv: Chain of Custody Present? ❑Yes EIND ONJA 1. Samples Arrived within Hold Time? Yes []Na N/A 2. Short Hold lime Analysis (1472 hr. 7 Yes EI! N/A 3. R us h Turn Aro u n d Time Requested? Yes Env ]N/A 4. Sufficient Volume? OVe-S No N/A S. Correct Containers Used? Ors ❑N❑ []N/A 5 -Pate Containers Used? Dfes EINO ❑NIA Containers Intact? E yes rNo N/A 7. Dissolved analysis: Sa mp Ias Vield Piitered7 Yrs Mo 117A 8. 5ampie LabelsMatchCCC? Dyes ❑No []N/A 9. r Andudesnate/Time/ID/Analysis Matrix: Heads pace in VOA Vials >5.6mmj7 El Yes No OH/A 10. Trip Blank Present? ❑Yes ❑Ne- ❑N/A 11. %p Blank Custody Seals Present? ❑Yes []No Gi'WrA COMMENTS/SAMPLE t]ISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Datefrime: Project Manager SCURF Review: pate: Project Manager 5RF Review: Oate: Field Date Required? [-]Yes ❑No Page 70 of 104 Document Name: 0 Sample Condition Upon Recall alylrca� . Document No-- F-CAR-CS•033•Rev-08 *Check mark top half of box If pH and/or dechiorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Caliform, TOC, Oil and Grease, OR018015 (water) DOC, LLHg **Bottom half of box is to list number of bottles w N Ln 2 L Z ti 2 V W 3 w & N V = r m a LM E ry Y Q 3N a E b A M ii E � � r A = V a i E ? _ y a. d d g 1 I � f 3 f 4 5 i 7 8 I 9 + 10 I i 11 I t2 I Oocument Revised: November 15, 2021 Page 2 of 2 Issuing Authority: Pace Carolinas quality Office Project#E WO# ■ 92'58V327 Phi: KRG Due Date: 02/22/22 CLIEH7: 92—Hart Hick ` i z ? u u ry 4 G 2 rc �a rq '� a —^ 1° n v Y I Q C d VJ iv a C a V N u3 T a E 1 x ❑ f'Y y N r s � r M .4. J. v� g' a a m a y N Z ? } d G C - 5 E a E a .� E E ¢ a Ln J _ a a d o > ¢ C > �' a - `m Ln a E E a it `+�•r a .a `as rev m N .�i L7 tKa711 �y Q iri � E lC=5 E �QY E or E S g m x E E E N rV E E V O ry - Q f• 1.. R"r - a a a o 7 } ,N pH Adjustment Log for Preserved Samples Sample ID Type of P►eservativa w upon raeeip! Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 4 -- - - - --- ---- - - - •-r-..-r -• .n ..,•.•.. _, —­ —, —IL, —, o cur, -- 11— wnu wui uv dent to ine r4ortn Larouna OENNR CerElflCatfon office {I.e. Out of hold, intorrect preservatve, out of temp, incorrect containers. Page 71 of 104 ti Received nn Ice (YIN) uSIO Sealed C baler Ym- S amoles nlacl {YIN) N 8 W QT -4 - UP A W N I I if w � k, f � � j C ;� C •- nn� C 9 lMO siimm mm allmalomumm N no m In MEMEMM ..■.■ - m MMMM Won �iiiiiiiiii k • ITEM # a'v rn n 0 mn - n A rn 4 z n 37 N 2 ry m 3 a 111 � O R � fjl GI pl 7 r = C 3 i Q m c � n W 3 In s `� v a m O �° aQ���y�❑ n � � � � � p n 3 MAT Rip( COIDE [se a valid r des m Ion) u xr 3 a SFMpLE TVpE (G�GRlB C.COMP) 0 _ n q o c a Qj n � mrL m 3 nr 0 Q 01 ID T m a 0 2 va O SAM F L E TEM P A T C OL LEC'IrON ry C TI In 6%OF COHIAI N ERS a1-0 m e A 7 N C C LJnpreserved a � ro �. n o- H c . H2504 z s a n eb -Amfl HNO3 T] cD D C) a a r FiCf f ju NaOH phi � l n n n Na262W M 1-9 Q HE m� Melhanal ,p' Olher c y Anal � a Page 72 of 104 Page 72 of 104 ton -test° A Pace Analyb'cale LaboWxy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 February 22, 2022 Kevin Godwin Pace Analytical Services - NC 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Project Location: NC Client Job Number: Project Number: 92588327 Laboratory Work Order Number: 22B 1040 Enclosed are results of analyses for samples as received by the laboratory on February 17, 2022. If you have any questions concerning this report, please feel free to contact me. Sincerely, Raymond J. McCarthy Project Manager EZURIMMEMINVI 1ffiW=.WrA[11- 91 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 22B 1040-01 22B 1040-02 22B 1040-03 22B 1040-04 22B 1040-05 22B 1040-06 22B 1040-07 22B 1040-08 22B 1040-09 22B 1040-10 Sample Preparation Information QC Data Petroleum Hydrocarbons Analyses - EPH B301417 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 7 9 11 13 15 17 19 21 23 25 26 26 26 28 29 30 srrsiszr.� Table of Contents con -testa A Pace Analyb'cale LaboWxy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Pace Analytical Services - NC 9800 Kincey Avenue, Suite 100 REPORT DATE: 2/22/2022 Huntersville, NC 28078 PURCHASE ORDER NUMBER: ATTN: Kevin Godwin PROJECT NUMBER: 92588327 ANALYTICAL SUMMARY WORK ORDER NUMBER: 22B1040 The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB UST-1-13 22B 1040-01 Soil MADEP EPH rev 2.1 SM 2540G UST-I-SW-F 22B1040-02 Soil MADEP EPH rev 2.1 SM 2540G UST-I-SW-B 22B1040-03 Soil MADEP EPH rev 2.1 SM 2540G UST-I-SW-R 22B1040-04 Soil MADEP EPH rev 2.1 SM 2540G UST-I-SW-L 22B1040-05 Soil MADEP EPH rev 2.1 SM 2540G UST-2-SW-L 22B 1040-06 Soil MADEP EPH rev 2.1 SM 2540G UST-2-13 22B 1040-07 Soil MADEP EPH rev 2.1 SM 2540G UST-2-SW-R 22B1040-08 Soil MADEP EPH rev 2.1 SM 2540G UST-2-SW-B 22B 1040-09 Soil MADEP EPH rev 2.1 SM 2540G UST-2-SW-F 22B1040-10 Soil MADEP EPH rev 2.1 SM 2540G Page 3 of 32 ton -test° A Pace Analyb'cale LaboWxy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method MA EPH, only hydrocarbon ranges were requested and reported. The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative ST.TSL^L{�rs'r ■ • • Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-1-B Sampled: 2/14/2022 15:25 Samule ID: 22131040-01 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 15 15 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:21 TYH C 19-C36 Aliphatics ND 15 15 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:21 TYH Unadjusted Cl 1-C22 Aromatics ND 15 15 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:21 TYH C 11-C22 Aromatics ND 15 15 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:21 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 55.7 40-140 2/18/22 17:21 o-Terphenyl (OTP) 54.8 40-140 2/18/22 17:21 2-Bromonaphthalene 99.6 40-140 2/18/22 17:21 2-Fluorobiphenyl 97.6 40-140 2/18/22 17:21 Page 5 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-1-B Sampled: 2/14/2022 15:25 Sample ID: 22131040-01 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 68.6 % Wt 1 SM 2540G 2/21/22 2/22/22 11:49 AVF Page 6 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-F Sampled: 2/14/2022 15:15 Samule ID: 22B1040-02 Samule Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:40 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:40 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:40 TYH C 11-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:40 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 49.1 40-140 2/18/22 17:40 o-Terphenyl(OTP) 52.6 40-140 2/18/22 17:40 2-Bromonaphthalene 103 40-140 2/18/22 17:40 2-Fluorobiphenyl 101 40-140 2/18/22 17:40 Page 7 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-F Sampled: 2/14/2022 15:15 Sample ID: 22B1040-02 Samule Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 70.9 % Wt 1 SM 2540G 2/21/22 2/22/22 11:49 AVF Page 8 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-B Sampled: 2/14/2022 15:35 Samule ID: 22B1040-03 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:59 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:59 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:59 TYH C 11-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 17:59 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 55.9 40-140 2/18/22 17:59 o-Terphenyl(OTP) 56.3 40-140 2/18/22 17:59 2-Bromonaphthalene 103 40-140 2/18/22 17:59 2-Fluorobiphenyl 100 40-140 2/18/22 17:59 Page 9 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-B Sampled: 2/14/2022 15:35 Sample ID: 22B1040-03 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.1 % Wt 1 SM 2540G 2/21/22 2/22/22 11:49 AVF srrs_rrnzr•� Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-R Sampled: 2/14/2022 15:40 Samule ID: 22B1040-04 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:19 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:19 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:19 TYH C 11-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:19 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 52.0 40-140 2/18/22 18:19 o-Terphenyl(OTP) 49.8 40-140 2/18/22 18:19 2-Bromonaphthalene 101 40-140 2/18/22 18:19 2-Fluorobiphenyl 99.4 40-140 2/18/22 18:19 Page 11 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-R Sampled: 2/14/2022 15:40 Sample ID: 22B1040-04 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 71.0 % Wt 1 SM 2540G 2/21/22 2/22/22 11:49 AVF srrs_irizr•� Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-L Sampled: 2/14/2022 15:50 Samule ID: 22B1040-05 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:38 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:38 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:38 TYH C11-C22Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:38 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 59.1 40-140 2/18/22 18:38 o-Terphenyl(OTP) 59.8 40-140 2/18/22 18:38 2-Bromonaphthalene 91.9 40-140 2/18/22 18:38 2-Fluorobiphenyl 86.5 40-140 2/18/22 18:38 ST.TSSL'�S�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-I-SW-L Sampled: 2/14/2022 15:50 Sample ID: 22B1040-05 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 71.2 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.TSSt:ES�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-L Sampled: 2/14/2022 16:00 Samule ID: 22B1040-06 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:57 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:57 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:57 TYH C 11-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 18:57 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 55.6 40-140 2/18/22 18:57 o-Terphenyl(OTP) 68.4 40-140 2/18/22 18:57 2-Bromonaphthalene 110 40-140 2/18/22 18:57 2-Fluorobiphenyl 107 40-140 2/18/22 18:57 ST.TSSi�S�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-L Sampled: 2/14/2022 16:00 Sample ID: 22BI040-06 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.8 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.TS:i:�S�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-B Sampled: 2/14/2022 16:20 Samule ID: 22131040-07 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics 35 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:16 TYH C 19-C36 Aliphatics 23 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:16 TYH Unadjusted Cl 1-C22 Aromatics 19 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:16 TYH C 11-C22 Aromatics 19 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:16 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 58.3 40-140 2/18/22 19:16 o-Terphenyl(OTP) 64.3 40-140 2/18/22 19:16 2-Bromonaphthalene 103 40-140 2/18/22 19:16 2-Fluorobiphenyl 101 40-140 2/18/22 19:16 Page 17 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-B Sampled: 2/14/2022 16:20 Sample ID: 22131040-07 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.1 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.TS!T•ES�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-R Sampled: 2/14/2022 16:10 Samule ID: 22BI040-08 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics 31 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:36 TYH C 19-C36 Aliphatics 14 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:36 TYH Unadjusted Cl 1-C22 Aromatics 20 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:36 TYH C 11-C22 Aromatics 19 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:36 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 57.3 40-140 2/18/22 19:36 o-Terphenyl(OTP) 60.2 40-140 2/18/22 19:36 2-Bromonaphthalene 102 40-140 2/18/22 19:36 2-Fluorobiphenyl 101 40-140 2/18/22 19:36 Page 19 of 32 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-R Sampled: 2/14/2022 16:10 Sample ID: 22BI040-08 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 77.7 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.TS!TIl.S�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-B Sampled: 2/14/2022 16:30 Samule ID: 22BI040-09 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:55 TYH C 19-C36 Aliphatics ND 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:55 TYH Unadjusted Cl 1-C22 Aromatics ND 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:55 TYH C 11-C22 Aromatics ND 13 13 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 19:55 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 52.9 40-140 2/18/22 19:55 o-Terphenyl(OTP) 63.5 40-140 2/18/22 19:55 2-Bromonaphthalene 101 40-140 2/18/22 19:55 2-Fluorobiphenyl 96.0 40-140 2/18/22 19:55 ST.TS!Y>rS�if�7 • Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-B Sampled: 2/14/2022 16:30 Sample ID: 22BI040-09 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 75.9 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.T- NIM ifN Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-F Sampled: 2/14/2022 16:40 Samule ID: 22131040-10 Sample Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst C9-C 18 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 20:14 TYH C 19-C36 Aliphatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 20:14 TYH Unadjusted Cl 1-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 20:14 TYH C 11-C22 Aromatics ND 14 14 mg/Kg dry 1 MADEP EPH rev 2.1 2/17/22 2/18/22 20:14 TYH Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 45.6 40-140 2/18/22 20:14 o-Terphenyl(OTP) 60.0 40-140 2/18/22 20:14 2-Bromonaphthalene 102 40-140 2/18/22 20:14 2-Fluorobiphenyl 99.6 40-140 2/18/22 20:14 ST.TS!L'�S�if•7 Table of Contents con -testa A Pace Analyb'cO LaboWoiy 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Project Location: NC Sample Description: Work Order: 22B 1040 Date Received: 2/17/2022 Field Sample #: UST-2-SW-F Sampled: 2/14/2022 16:40 Sample ID: 22131040-10 Sample Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.2 % Wt 1 SM 2540G 2/21/22 2/22/22 11:50 AVF ST.TS!T:ES�if•7 Table of Contents con -testa A Pace Analyb'cale LaboWory 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546 Analytical Method: MADEP EPH rev 2.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 22B1040-01 [UST-1-B] B301417 20.0 2.00 02/17/22 22B1040-02 [UST-I-SW-F] B301417 20.0 2.00 02/17/22 22B1040-03 [UST-1-SW-B] B301417 20.0 2.00 02/17/22 22B1040-04 [UST-I-SW-R] B301417 20.0 2.00 02/17/22 22B1040-05 [UST-I-SW-L] B301417 20.0 2.00 02/17/22 22131040-06 [UST-2-SW-L] B301417 20.0 2.00 02/17/22 22131040-07 [UST-2-13] B301417 20.0 2.00 02/17/22 22B1040-08 [UST-2-SW-R] B301417 20.0 2.00 02/17/22 22B1040-09 [UST-2-SW-B] B301417 20.0 2.00 02/17/22 22B1040-10 [UST-2-SW-F] B301417 20.0 2.00 02/17/22 Prep Method: % Solids Analytical Method: SM 2540G Lab Number [Field ID] Batch Date 22B1040-01 [UST-1-B] B301658 02/21/22 22B1040-02 [UST-I-SW-F] B301658 02/21/22 22B1040-03 [UST-I-SW-B] B301658 02/21/22 22131040-04 [UST-I-SW-R] B301658 02/21/22 22B1040-05 [UST-I-SW-L] B301658 02/21/22 22131040-06 [UST-2-SW-L] B301658 02/21/22 22131040-07 [UST-2-13] B301658 02/21/22 22131040-08 [UST-2-SW-R] B301658 02/21/22 22B1040-09 [UST-2-SW-B] B301658 02/21/22 22B1040-10 [UST-2-SW-F] B301658 02/21/22 EST.TS!fm10111N7 N g L7,W49A• ton -test° A Pace Analyb'cale LaboWxy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD lnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B301417 - SW-846 3546 Blank (B301417-BLK1) Prepared: 02/17/22 Analyzed: 02/18/22 C9-C 18 Aliphatics ND 10 mg/Kg wet C 19-C36 Aliphatics ND 10 mg/Kg wet Unadjusted Cl I -C22 Aromatics ND 10 mg/Kg wet C l l-C22 Aromatics ND 10 mg/Kg wet Acenaphthene ND 0.10 mg/Kg wet Acenaphthylene ND 0.10 mg/Kg wet Anthracene ND 0.10 mg/Kg wet Benzo(a)anthracene ND 0.10 mg/Kg wet Benzo(a)pyrene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Benzo(g,h,i)perylene ND 0.10 mg/Kg wet Benzo(k)fluoranthene ND 0.10 mg/Kg wet Chrysene ND 0.10 mg/Kg wet Dibenz(a,h)anthracene ND 0.10 mg/Kg wet Fluoranthene ND 0.10 mg/Kg wet Fluorene ND 0.10 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.10 mg/Kg wet 2-Methylnaphthalene ND 0.10 mg/Kg wet Naphthalene ND 0.10 mg/Kg wet Phenanthrene ND 0.10 mg/Kg wet Pyrene ND 0.10 mg/Kg wet Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet Surrogate: Chlorooctadecane (COD) 2.53 mg/Kg wet 5.00 50.6 40-140 Surrogate: o-Terphenyl (OTP) 2.96 mg/Kg wet 5.00 59.3 40-140 Surrogate:2-Bromonaphthalene 4.74 mg/Kg wet 5.00 94.8 40-140 Surrogate:2-Fluorobiphenyl 4.61 mg/Kg wet 5.00 92.3 40-140 LCS (B301417-BS1) Prepared: 02/17/22 Analyzed: 02/18/22 C9-C18Aliphatics 20.1 10 mg/Kg wet 30.0 66.9 40-140 C 19-06 Aliphatics; 29.4 10 mg/Kg wet 40.0 73.5 40-140 Unadjusted C11-C22 Aromatics 37.4 10 mg/Kg wet 85.0 67.5 40-140 Acenaphthene 2.98 0.10 mg/Kg wet 5.00 59.5 40-140 Acenaphthylene 2.79 0.10 mg/Kg wet 5.00 55.8 40-140 Anthracene 3.12 0.10 mg/Kg wet 5.00 62.4 40-140 Benzo(a)anthracene 3.36 0.10 mg/Kg wet 5.00 67.3 40-140 Benzo(a)pyrene 3.20 0.10 mg/Kg wet 5.00 64.0 40-140 Benzo(b)fluoranthene 3.36 0.10 mg/Kg wet 5.00 71.3 40-140 Benzo(g,h,i)perylene 2.91 0.10 mg/Kg wet 5.00 58.2 40-140 Benzo(k)fluoranthene 2.71 0.10 mg/Kg wet 5.00 54.3 40-140 Chrysene 3.25 0.10 mg/Kg wet 5.00 65.0 40-140 Dibenz(a,h)anthracene 3.17 0.10 mg/Kg wet 5.00 63.3 40-140 Fluoranthene 3.18 0.10 mg/Kg wet 5.00 63.7 40-140 Fluorene 3.03 0.10 mg/Kg wet 5.00 60.5 40-140 Indeno(1,2,3-cd)pyrene 2.97 0.10 mg/Kg wet 5.00 59.4 40-140 2-Methylnaphthalene 2.79 0.10 mg/Kg wet 5.00 55.9 40-140 Naphthalene 2.63 0.10 mg/Kg wet 5.00 52.5 40-140 Phenanthrene 3.16 0.10 mg/Kg wet 5.00 63.2 40-140 Pyrene 3.24 0.10 mg/Kg wet 5.00 64.8 40-140 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 2.96 mg/Kg wet 5.00 59.2 40-140 Rage Page 26 of 32 ton -test° A Pace Analyb'cale LaboWxy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B301417 - SW-846 3546 LCS (B301417-BS1) Prepared: 02/17/22 Analyzed: 02/18/22 Surrogate: o-Terphenyl (OTP) 3.13 mg/Kg wet 5.00 62.5 40-140 Surrogate:2-Bromonaphthalene 4.60 mg/Kg wet 5.00 92.1 40-140 Surrogate:2-Fluorobiphenyl 4.60 mg/Kg wet 5.00 91.9 40-140 LCS Dup (B301417-BSD1) Prepared: 02/17/22 Analyzed: 02/18/22 C9-C18Aliphatics 17.9 10 mg/Kg wet 30.0 59.7 40-140 11.4 25 C19-C36Aliphatics 30.3 10 mg/Kgwet 40.0 75.7 40-140 2.99 25 Unadjusted C11-C22 Aromatics 55.7 10 mg/Kg wet 85.0 65.5 40-140 3.09 25 Acenaphthene 2.74 0.10 mg/Kg wet 5.00 54.7 40-140 8.33 25 Acenaphthylene 2.54 0.10 mg/Kgwet 5.00 50.8 40-140 9.30 25 Anthracene 2.98 0.10 mg/Kg wet 5.00 59.5 40-140 4.64 25 Benzo(a)anthracene 3.35 0.10 mg/Kg wet 5.00 67.1 40-140 0.319 25 Benzo(a)pyrene 3.17 0.10 mg/Kgwet 5.00 63.3 40-140 1.08 25 Benzo(b)fluoranthene 3.67 0.10 mg/Kg wet 5.00 73.4 40-140 2.88 25 Benzo(g,h,i)perylene 2.84 0.10 mg/Kg wet 5.00 56.9 40-140 2.23 25 Benzo(k)fluoranthene 2.69 0.10 mg/Kg wet 5.00 53.8 40-140 0.941 25 Chrysene 3.21 0.10 mg/Kg wet 5.00 64.3 40-140 1.08 25 Dibenz(a,h)anthracene 3.09 0.10 mg/Kg wet 5.00 61.8 40-140 2.38 25 Fluoranthene 3.16 0.10 mg/Kgwet 5.00 63.2 40-140 0.754 25 Fluorene 2.77 0.10 mg/Kg wet 5.00 55.4 40-140 8.90 25 Indeno(1,2,3-cd)pyrene 2.95 0.10 mg/Kg wet 5.00 58.9 40-140 0.825 25 2-Methylnaphthalene 2.45 0.10 mg/Kg wet 5.00 49.1 40-140 12.9 25 Naphthalene 2.29 0.10 mg/Kg wet 5.00 45.7 40-140 13.8 25 Phenanthrene 3.02 0.10 mg/Kg wet 5.00 60.5 40-140 4.31 25 Pyrene 3.23 0.10 mg/Kgwet 5.00 64.6 40-140 0.319 25 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 2.99 mg/Kg wet 5.00 59.8 40-140 Surrogate: o-Terphenyl (OTP) 3.02 mg/Kg wet 5.00 60.4 40-140 Surrogate:2-Bromonaphthalene 4.89 mg/Kg wet 5.00 97.7 40-140 Surrogate:2-Fluorobiphenyl 4.80 mg/Kg wet 5.00 96.1 40-140 ST.T- 01M ifM ton -test° A Pace Analyb'cale LaboWoiy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. j Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. ST.TSi f •7•ES t ti f •7 con -testa A Pace Analyb'caie LaboWoiy Table of Contents 39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEPEPHrev 2.1 in Soil C9-C18 Aliphatics C 19-C36 Aliphatics Unadjusted Cl 1-C22 Aromatics Cl 1-C22 Aromatics MADEP EPH rev 2.1 in Water CT,NC,ME,NH-P CT,NC,ME,NH-P CT,NC,ME,NH-P CT,NC,ME,NH-P C9-C18 Aliphatics CT,NC,ME,NH-P C 19-C36 Aliphatics CT,NC,ME,NH-P Unadjusted Cl 1-C22 Aromatics CT,NC,ME,NH-P Cl 1-C22 Aromatics CT,NC,ME,NH-P Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2024 MA Massachusetts DEP M-MA100 06/30/2022 CT Connecticut Department of Publilc Health PH-0165 12/31/2022 NY New York State Department of Health 10899 NELAP 04/l/2022 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2023 RI Rhode Island Department of Health LA000373 12/30/2022 NC North Carolina Div. of Water Quality 652 12/31/2022 NJ New Jersey DEP MA007 NELAP 06/30/2022 FL Florida Department of Health E871027 NELAP 06/30/2022 VT Vermont Department of Health Lead Laboratory LL720741 07/30/2022 ME State of Maine MA00100 06/9/2023 VA Commonwealth of Virginia 460217 12/14/2022 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2022 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2022 NC-DW North Carolina Department of Health 25703 07/31/2022 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2022 MI Dept. of Env, Great Lakes, and Energy 9100 09/6/2022 srrsr, zrizr•'r, •r, g mmuzel Table of Contents LU RS T CD cz d Y!s t . 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N cy [� N N rat � 4 zk* �'��- � � 7 Y ,�. s:,°�• i� yam,, tv co �. }�:. :�:g.yx � r r r w• a� wa� r r � i'°.• U 5❑i fir r► �� � r• .`3'��: �;�:�i,�-.� �b� T^ fV racq NOW z Y f.?sy m 02 w m12 C Q a~s U�] 4�7 V} 3 wo u y O ;:�� r N M tfa fp A . 4, # iffirfinumq . • • Table of Contents FedEx Tracking 997548491949 ADD NICKNAME ON TIME Delivered Thursday, February 17, 2022 at 9:58 am FROM Huntersville, NC US Travel History TWE ZONE Local Scan Time Thursday, Fabruary 17, 2022 9:58 AM 9.00 AM 8:52 AM 7:5 7 AM 6:30 AM 6 28 AM 3:20 AM 103 AM 12:48 AM DELIVERED Signed for by: R.RIOS GET STATUS UPDATES OBTAIN PROOF OF DELIVERY TO BAST LONGMEAL1{}W MA US MANAGE DELIVERY v EAST LONGMEADOW. MA Delivered WINDSOR LOCKS, CT Can FedEx vehicle for delivery WINDSOR LOCKS, CT At local FedEx facility EAST GRANBY, CT At destination sort facility INDIANAPOLIS, IN In transit INDIANAPOLIS, IN Departed FedEx hula INDIANAPOLIS, IN In transit INDIANAPOLIS, IN Shipment drriving On -Time INDIANAPOLIS, IN Arrived at FedEx hub WWII ST.TSif•Y9%S0f•7 10 . •rMA me] Table of Contents l Have Not Confirmed Sample Container Numbers With Lab Staff Before Retinquishing ARtALYT1 A� LIrBORAT�i tY Over Samples . Login Sample Receipt Checklist - [Rejedion Criteria Listing - Using Acceptance Policy] Any False Statement will be brought to the attention of the Client - State True or False Client q Received By112 Date How were the samples received? Time In Cooler - r- No Cooler On Ice r No Ice Direct from Sampling Ambient Melted Ice Were samples within By Gun # 3 Actual Temp . Temperature? 2-6°C i By Blank # Actual Teme - as Custody Seal Intact? A4 Were Samples Tampered with? Was CQC Relinquished ? -T— Does Chain Agree With Samples? �— Are there brokenneaking/loose caps on any samples? Is CDC in ink/ Legible? j Were samples received within holding time? .l Did COC inciude all Client 1 Analysis T _ Sampler Name pertinent Information? Project »�- ID`s i Collection Dates/Times -F- A re Sample labels filled out and legible? ,_ ""--- Are there Lab to Filters? r �' Are there Rushes? �- Are there Short Holds? --JE-� Is there enough Volume? i Is there Headspace wh x ?. Proper MediatContainer T Were trip blanks received? Do all samples have the proper pH? Who was notified? Who was notified?_ Who was notified? M5/IyA�D?_ �- -f;� On CoC Acid Base Page 32 of 32 Beverly, Trudy From: Nathan O'Leary <noleary@harthickman.com> Sent: Tuesday, March 8, 2022 1:20 PM To: Beverly, Trudy Subject: RE: [External] Heating Oil UST IAA CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. That sounds great, thanks Trudy! Nathan Nathan O'Leary, Project Manager Hart & Hickman, PC 2923 S Tryon Street, Suite 100 •Charlotte, NC 28203 Direct: 704-887-4607 • Mobile: 515-239-7197 www.harthickman.com 10 From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Tuesday, March 8, 2022 1:16 PM To: Nathan O'Leary <noleary@harthickman.com> Subject: RE: [External] Heating Oil UST IAA Hey Nathan, I'll do my best to get to it soon. It may be next week before I can review the report. Trudy Trudy Beverly, L.G. D�EQ Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality n"���t., � UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy. B everly_kncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: h_ptt s:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: https://dea.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): https://deq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hfiles.nc.gov/ncdeg/Waste%2OManatiement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policv.pdf https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Nathan O'Leary [mailto:noleary@harthickman.co Sent: Tuesday, March 8, 2022 12:01 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] Heating Oil UST IAA Importance: High CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Good Morning Trudy, Attached, please find the Initial Abatement Action report prepared in relation to three heating oil USTs removed from the property located at 729 East 361h Street and 3315 North McDowell Street in Charlotte, North Carolina. Analytical results of closure samples indicated the presence of TPH-GRO and TPH-DRO at concentrations above the action levels. Confirmation samples collected following the removal of impacted soil did not indicate the presence of VOCs, SVOCs, VPH, or EPA at concentrations above MSCCs. As such, H&H is requesting an unrestricted use No Further Action (NFA) be issued. Please note, this property is set to be transacted in mid to late March 2022. This UST removal work was completed by the potential purchaser of the property to meet requirements of the lending institute. The lending institute is requesting closure documentation from DEQ prior to closing of the property. If you have any questions or would like additional information, please let me know. Thanks, Nathan Nathan O'Leary, Project Manager Hart & Hickman, PC 2923 S Tryon Street, Suite 100 • Charlotte, NC 28203 Direct: 704-887-4607 • Mobile: 515-239-7197 www.harthickman.com I Im