HomeMy WebLinkAboutMO-29143_48325_CA_IAR_20220308_Initial Abatement Action Reporthart'` hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
March 8, 2021
North Carolina Department
of Environmental Quality
UST Section
610 East Center Avenue
Suite 301
Mooresville, NC 28115
Attn: Ms. Trudy Beverly
Re: Heating Oil UST Removals
Presbyterian Church
729 East 36th Street and
3315 North McDowell Street
Charlotte, North Carolina 28205
H&H Job No. ASC-003
Dear Ms. Beverly:
Hart & Hickman, PC (H&H) is providing the attached Initial Abatement Action (IAA) report in
relation to three heating oil underground storage tanks (USTs) removed from the Presbyterian
Church property located at 729 East 36th Street and 3315 North McDowell Street in Charlotte,
North Carolina. Analytical results of closure samples indicated the presence of impacts to soil
above action levels at two of the UST locations. Analytical results of confirmation samples
collected following the removal of impacted soil did not indicate the presence of analyzed
compounds at concentrations above Maximum Soil Contaminant Concentrations (MSCCs). As
such, H&H is requesting an unrestricted use No Further Action (NFA) in relation to the former
USTs.
Please contact us if you have any questions or require additional information.
Sincerely,
Hart & Hickman, PC
r
Nathan O'Le ry,
Project Manager
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main
Initial Abatement Action Report
Presbyterian Church
729 East 36th Street and
3315 North McDowell Street
Charlotte, North Carolina
DEQ Incident No. TBD
H&H Job No. ASC-003
March 3, 2022
hart � hickman
SMARTER ENVIRONMENTAL SOLUTIONS
C-1269 Engineering
#C-245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main
Initial Abatement Action Report
A. Site Information
1. Site Identification
Date of Report: March 2 2022
Facility ID: NA UST Incident Number: NA
Site Name. Presbyterian Church
Site Street Address: 729 East 36 Street and 3315 North McDowell Street
City, Town: Charlotte Zip Code: 28205 County: Mecklenburg
Description of Geographical Data Point: Former UST location
Location Method: Goo le Earth
Latitude: 35.2463°N Longitude:-80.8010°Vie
2. Information about Contacts Associated with the Leaking UST System
UST Owner/Operator: North Charlotte Presbvterian Church
Address: 1010 Vickery Drive, Charlotte, NC 28215 Tel.: Unknown
Property Owner: North Charlotte Presbyterian Church
Address: 1010 Vickery Drive, Charlotte, NC 28215 Tel.: Unknown
Property Occupant: Vacant
Address: Tel.:
Consultant/Contractor: Hart & Hickman, PC
Address: 2923 South Trvon Street. Suite 100, Charlotte. NC 28203
Tel.: 704 586-0007 Attn: Steve Libbe PG
Analytical Laboratory: Pace Analytical State Cert. No. 12
Address: 9800 Kincey Ave. Ste 100 Huntersville NC 28078
Tel.: 704 875-9092
3. Information About Release
Date Discovered: October 12. 2018
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Heating Oil USTs
Sizes and contents of UST system: One 550- allon heating oil UST and one
1000- allon heating oil UST
4. Certification
I, Stephen Libbgy, PG a Licensed Geologist at Hart & Hickman, PC, do certify that the
information co
Ag din this report is correct and accurate to the best of my knowledge.
SEAL f 3 j31Zv
•m
Hart & 'icensed to practice geology/engineering in North Carolina. The
certification n' wS l' of the company are C-2451C-1269.
1 Hart "ti hickman
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B. Site History and Characterization
1. UST Owner and Operator Information:
UST ID Number
UST-1, UST-2, & UST-3
Facility ID Number
N/A
Name of Owner
Dates of Ownership
North Charlotte Presbyterian Church
—1955-2022
Street Address
1010 Vickery Dr
City
State
Zip
Telephone Number
Charlotte
NC
28215
Unknown
Name of Operator
Dates of Operation
Same as Above
Unknown
Street Address
City
State
Zip
Telephone Number
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2. UST/AST Information:
Was
release
Approximate
Description of
Date
UST ID
Current/Last
Previous
Capacity
Construction
Status of
associated
Tank
Associated Piping and
Tank
Number
Contents
Contents
(gallons)
Details
UST
with the
Dimensions
Pumps
Installed
UST
System?
UST-1
Heating Oil
N/A
1,000
Steel
I x 4'
N/A
Unknown
Removed
Yes
UST-2
Heating Oil
N/A
550
Steel
6' x 3.33'
N/A
Unknown
Removed
Yes
UST-3
I Heating Oil
I N/A
1 550
1 Steel
1 6' x 3.33'
N/A
Unknown
I Removed
No
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SMARTER ENWONMENTAL 50LUTION5
3. Non -UST spills at the site:
No non -UST spills are known to have occurred at the site.
4. Description of release:
During previous Phase I Environmental Site Assessment (ESA) activities
conducted at the site by others in 2018, heating oil tank UST-2 was identified
adjacent to the church building and heating oil tank UST-3 was identified adjacent
to an on -site residential structure. Heating oil tank UST-1 located adjacent to the
church school building was not identified in 2018 and was identified by H&H
during a subsequent Phase I ESA in 2021.
To evaluate the potential for impact from the USTs, two soil borings were
advanced adjacent to UST-2 and UST-3 during the 2018 Phase I ESA. Analytical
results of soil samples collected adjacent to UST-2 indicated gasoline range total
petroleum hydrocarbons (TPH-GRO) and diesel range total petroleum
hydrocarbons (TPH-DRO) concentrations up to 26,000 mg/kg. TPH-GRO and
TPH-DRO were not detected at concentrations above the laboratory reporting
limits in samples collected adjacent to UST-3.
A soil sampling results summary table, sample locations map, and laboratory
analytical data from the 2018 Phase I ESA are presented in Appendix A.
5. Site characteristics:
The site is comprised of two parcels of land totaling approximately 1.65 acres in
area, the westernmost site parcel is developed with an approximately 6,550 square
foot (sq ft) church building, an approximately 2,300 sq ft single-family residence,
and an approximately 4,500 sq ft school building. The easternmost parcel is
currently vacant land but was most recently utilized as a community garden. A
site location map is presented as Figure 1, and a site map is presented as Figure 2.
The subject site is located in the Piedmont Physiographic Province of North
Carolina. According to the Geologic Map of North Carolina dated 1985, the
subject property lies within the Charlotte Belt. In the site area, underlying
bedrock is composed of granitic rock. The land surface of the area is generally
characterized as gently sloping, which may become moderately steep where
intersected by streams.
In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed
saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand
with lesser amounts of rock fragments. Due to the range of parent rock types and
their variable susceptibility to weathering, the saprolite ranges widely in color,
texture, and thickness. Generally, the saprolite is thickest near interstream divides
and thins toward streambeds. In profile, the saprolite normally grades from
clayey soils near the land surface to highly weathered rock above competent
bedrock.
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SIdAR7ER pNY1RONME l At SOLL7I %
The occurrence and movement of groundwater in the Piedmont is typically within
two separate but interconnected water -bearing zones. A shallow water -bearing
zone occurs within the saprolite, and a deeper water -bearing zone occurs within
the underlying bedrock.
The site is located at an approximate elevation of 730 ft above mean sea level.
Topography in the source area generally slopes to the northeast (Figure 1). Based
on topography, H&H anticipates that the groundwater flow direction at the site is
to the northeast toward an unnamed tributary of Little Sugar Creek located
approximately 500 ft from the former UST.
Visual observations during excavation activities and soil sample collection
indicated that the soil surrounding UST system consisted of orange to brown silty
clays (saprolite). Groundwater and bedrock were not encountered in the
excavation.
Municipal water is available to the site and the areas surrounding the site. A
formal water supply well survey was not performed. No obvious water supply
wells were observed during area reconnaissance.
6. Initial abatement actions, assessment activities, and corrective actions
performed to date:
Other than the 2018 soil sampling discussed above, no other known initial
abatement actions, assessments, or corrective action activities have been
conducted at the site.
C. Site Check Report
Not applicable.
D. UST Closure Report following UST-12 format and Site Investigation Report
for Permanent Closure or Change -in -Service of UST (UST-2 Form)
1. Preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to clean and purge the tanks:
Prior to the UST closure activities, a permit authorizing the UST removal was
obtained from the City of Charlotte Fire Department by EVO Environmental and
Industrial Resources (EVO) of Winston-Salem, North Carolina.
Prior to removal, residual fluids were removed from the USTs. The USTs were
then triple -rinsed with a pressure washer and vacuum truck by EVO in accordance
with Mecklenburg County requirements. Approximately 625 gallons of residual
fluids and rinse water were removed from the USTs. Following removal of the
residual fluids and rinse water, the USTs were purged of combustible vapors with
dry -ice and subsequently tested with a combustible gas indicator to evaluate
whether combustible vapors had dissipated.
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SIdAR7ER pNY1RONME l At SOLL7I %
2. Closure procedures:
Initially, soil was removed from the top and sides of the USTs with a backhoe so
that the tanks could be removed from the ground. Soils encountered during the
excavations were evaluated in the field for the presence of odors and staining, and
for the presence of organic vapor with a photoionization detector (PID). The PID
was calibrated prior to its use against an isobutylene standard.
Following removal, the USTs were inspected for holes or other signs of structural
damage. The USTs were single -walled and constructed of steel. The bottom
surface of UST-1 and UST-2 were moderately pitted and contained several small
holes. No surface pitting or holes were observed in the bottom surface of UST-3.
3. Note the amount of residual material pumped from the tank and describes
the storage, sampling and disposal of the residual material and the disposal
of the tank, pumps and piping:
As stated above, EVO removed approximately 625 gallons of residual and rinse
liquids from the USTs. The fluid was disposed by EVO at their facility in
Winston-Salem, North Carolina. The disposal certificate for the residual fluid is
included in Appendix B.
The three USTs were transported off -site for disposal at Foss Recycling in
Winston-Salem, North Carolina. The tank disposal certificate is included in
Appendix C.
4. Initial response actions and initial abatement actions:
Initial response and abatement actions are discussed in the following section.
5. Soil excavation and Site Investigation activities:
After removal of the USTs, one closure soil sample was collected below UST-1
and one closure soil sample was collected below UST-3. Due to previous soil
sampling data from 2018 which confirmed that a release had occurred from UST-
2, a closure sample was not collected below UST-2. The closure samples were
analyzed for TPH-GRO by EPA Method 8015C and TPH-DRO by EPA Method
8015C.
The analytical results of the closure sample collected below UST-1 indicated the
presence of TPH-GRO and TPH-DRO at concentrations of 146 mg/kg and 838
mg/kg, respectively. The detected concentrations are above the DEQ action
levels of 50 mg/kg and 100 mg/kg for TPH-GRO and TPH-DRO, respectively.
TPH-GRO and TPH-DRO were not detected above the DEQ action levels in the
soil sample collected below UST-3.
Approximately 26 tons of impacted soils were excavated from the UST-1 and
UST-2 basins on February 14, 2022. The excavated soil was stockpiled on plastic
adjacent to the USTs and later transported to EVO's facility in Winston-Salem,
North Carolina for proper disposal on February 24, 2022. A copy of the
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SIdAR7ER pNY1RONME l At SOLL7I %
certificate of disposal, non -hazardous waste manifests, and certified weight tickets
for the excavated soil are provided in Appendix B.
The approximate dimensions of the UST-1 basin excavation were approximately
15 ft long by 8 ft wide by 8 ft deep, and the approximate dimensions of the UST-2
basin excavation were approximately 11 ft long by 7 ft wide by 7 ft deep. The
approximate extents of the excavations are depicted on Figure 3.
Following soil over -excavation activities, four confirmation sidewall soil samples
(UST-I-SW-L, UST-I-SW-R, UST-I-SW-F, and UST-I-SW-B) were collected
from the UST-1 basin excavation, and four confirmation sidewall soil samples
(UST-2-SW-L, UST-2-SW-R, UST-2-SW-F, and UST-2-SW-B) were collected
from the UST-2 basin excavation. In addition, confirmation base soil samples
UST-1-13 and UST-2-13 were collected from the UST-1 and UST-2 excavations,
respectively. In accordance with DEQ guidance, the collected post -excavation
soil samples were analyzed for volatile organic compounds (VOCs) by EPA
Method 8260B/5035A, semi-VOCs (SVOCs) by EPA Method 8270, and
extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons
(VPH) using the Massachusetts Department of Environmental Protection
(MADEP) Methods.
Analytical results of the post -excavation samples from the UST basin excavations
indicate the presence of trace concentrations of several VOCs and naphthalene.
In addition, C9-C 18 Aliphatics and C 11-C22 Aromatics were detected at trace
concentrations in confirmation soil samples UST-2-13 and UST-2-SW-R. None of
the compounds were detected at concentrations above DEQ Soil -to -Groundwater,
Residential, or Industrial/Commercial Maximum Soil Contaminant
Concentrations (MSCCs).
Soil samples were analyzed by a North Carolina certified laboratory. A chain -of -
custody record was completed for samples collected and included sample
description, date collected, time collected, matrix, sample container information,
and analyses required. The chain -of -custody was signed by H&H prior to
placement in an iced cooler for shipment to the laboratory. Prior to shipment, the
cooler was closed with a seal indicating the H&H representative's signature and
date such that a potential disturbance of the cooler contents could be detected by
the laboratory.
Soil analytical results are summarized in Table 1 and the sample locations are
depicted on Figure 3. Laboratory analytical sheets are included in Appendix D.
Following soil removal, the excavation was backfilled with clean imported
backfill material. The imported backfill material consisted primarily of brown
silty clays.
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SIdAR7ER pNY1RONME l At SOLL7I %
E. Free Product Investigation and Recovery Report
Not applicable.
F. Groundwater and Surface Water Investigation
Not applicable.
G. Initial Response and Abatement Activities
See Section B.
H. Excavation of Contaminated Soil
See Section D.
I. Conclusions and Recommendations:
In February 2022, two inactive 550-gallon heating oil USTs (UST-2 and UST-3)
and one inactive 1,000-gallon heating oil UST (UST-1) were removed from the site.
No soil impacts were identified below UST-3 based on laboratory analytical results.
Approximately 26 tons of impacted soils were excavated for off -site disposal from
the UST-1 and UST-2 basins. Analytical results of confirmation soil samples
collected from the UST-1 and UST-2 basins do not indicate the presence of VOCs,
SVOCs, VPH, or EPH at concentrations above DEQ MSCCs.
Based on the results of the initial abatement action activities, H&H recommends
that DEQ issue a no further action (NFA) letter for the UST incident.
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Tables
qd
hart hickman
SMARTER ENVIRONMENTAL SOWT1ONS
Table 1
Summary of Heating Oil UST Soil Sample Results
Presbyterian Church
729 E. 36th Street and 3315 North McDowell Street
Charlotte, North Carolina
H&H Job. No. ASC-003
5030/
3550/
Analytical Method
8015C
8015C
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8260B
8270D
N
U
U
to
U
U
U
m
C
m
C
Contaminant of Concern
Q
o
o
N
N
<
<
<
_Q
<
(9
<
N
<
N
co
N
CID
00
co
U
O
N
U
N
N
a)
C
c
m
m
U
6
rn
U
a)
c
>
E
F
U
O
U
U
U
U io
U
m
o
a)
c
>
Date
Sample
Incident
=
_
_
_
_
= Q
=
= o
c
Q
Q
D
Sample ID
Collected
Source Area
Depth (ft)
Phase
0
0-
F--
0-
>
0-
>
0-
w
O
F--
0-
w <
0-
>
0
w <
O
1---
a)
m
1 w
O
E
(0
z
p1---
1---
N
M
T
X
a)
cn
UST-1
02/14/22
UST
5
CL
146
838
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
UST-3
02/14/22
UST
5
CL
5.9 J
<2.1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
UST-1-13
02/14/22
UST
8
IA
NA
NA
<5.6
<5.6
<15
BRL
<15
<5.6
<15
BRL
0.0069 J
0.0060 J
<0.0040
0.0177
0.0197
0.0061 J
<0.0039
0.0174 J
ALL BRL
UST-1-SW-F
02/14/22
UST
7
IA
NA
NA
<4.6
<4.6
<14
BRL
<14
<4.6
<14
BRL
<0.0038
0.0108
0.0065 J
0.0653
0.0089 J
0.0766
0.0327
0.0536
ALL BRL
UST-1-SW-B
02/14/22
UST
7
IA
NA
NA
<5.2
<5.2
<14
BRL
<14
<5.2
<14
BRL
<0.0055
<0.0065
<0.0047
<0.0073
<0.0039
<0.0038
<0.0047
<0.0079
ALL BRL
UST-1-SW-R
02/14/22
UST
7
IA
NA
NA
<6.7
<6.7
<14
BRL
<14
<6.7
<14
BRL
<0.0041
<0.0048
<0.0035
<0.0055
0.0089 J
<0.0028
<0.0035
<0.0059
ALL BRL
UST-1-SW-L
02/14/22
UST
7
IA
NA
NA
<6.2
<6.2
<14
BRL
<14
<6.2
<14
BRL
<0.0043
<0.0051
<0.0037
<0.0057
<0.0031
<0.0030
<0.0037
<0.0062
ALL BRL
UST-2-13
02/14/22
UST
7
IA
NA
NA
<8.2
<8.2
35
35
23
<8.2
19
19
<0.0055
<0.0064
<0.0047
0.0244
<0.0039
0.0090 J
<0.0046
<0.0079
ALL BRL
UST-2-SW-F
02/14/22
UST
6
IA
NA
NA
<5.1
<5.1
<14
BRL
<14
<5.1
<14
BRL
<0.0038
<0.0044
<0.0032
<0.0050
<0.0027
<0.0026
<0.0032
<0.0054
ALL BRL
UST-2-SW-B
02/14/22
UST
6
IA
NA
NA
<5.6
<5.6
<13
BRL
<13
<5.6
<13
BRL
<0.0038
<0.0045
<0.0033
<0.0050
<0.0027
<0.0026
<0.0032
<0.0055
ALL BRL
UST-2-SW-R
02/14/22
UST
6
IA
NA
NA
<4.3
<4.3
31
31
14
<4.3
19
19
<0.0038
<0.0044
<0.0032
0.0055 J
<0.0027
<0.0026
<0.0032
<0.0054
ALL BRL
UST-2-SW-L
02/14/22
UST
6
IA
NA
NA
<4.7
<4.7
<14
BRL
<14
<4.7
<14
BRL
<0.0040
<0.0046
<0.0034
<0.0052
<0.0028
<0.0027
<0.0033
<0.0057
ALL BRL
Action Level (mg/kg)
50
100
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Soil to Ground Water MSCC (mg/kg)
NS
NS
68
NS
NS
540
NS
NS
NS
31
0.0072
8
1.3
0.2
5.4
6.6
6.6
6
Varies
Residential MSCC (mg/kg)
NS
NS
625
NS
NS
1,500
31,200
NS
NS
469
12
60.3
1,560
5.5
1,250
156
156
3,120
Varies
Industrial/Commercial MSCC (mg/kg)
NS
NS
9,340
NS
NS
40,000
467,000
NS
NS
7,000
1 59.4
297
23,300
27
18,600
1 2,330
1 2,330
1 46,700
Varies
Notes:
Apart from VPH and EPH, only those compounds detected are shown.
Concentrations are reported in milligrams per kilogram (mg/kg).
UST = Underground Storage Tank Basin; CL = Closure Sample; IA = Initial Abatement Sample; TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum
Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons; NA = Not Analyzed; NS = Not Specified; MSCC = Maximum Soil Contaminant Concentration; BRL = Below Reporting Limits; J = Estimated value between method detection limit and laboratory reporting limit.
Table 1 (Page 1 of 1)
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Appendix A
2018 Soil Assessment Data
qd
hart hickman
SMARTER ENVIRONMENTAL SOWT1ONS
Table 1: Summary of Soil Sampling Results
Revision 10/2612018 Project: Forest Hill Church Parcels Project No, CH18.0129.GE
Date:
Analytical Method
TPH (mg/kg)
Contaminant of Concern
❑
0
Sample
Location
Sample
depth (ft)
Date
Collected
I.
HA-1
7.5
10/512018
E9.9
{ 7.5
HA-2
8
10/512018
<9.9
<7.5
HA-3
$
10/12/2018
26,000
2,300
HA-4
10
10/1212018
3,500
99
North Carolina Action limits for Total
Petroleum Hydrocarbons (TPH)
100
50
LEGEND:
approximate Location of
SaFnpEes
Uudaground Storage
Tank
lk
s
4
GEOSCIENCE GROUP, INC.
CHARLOTTE, NORTH CAROLINA
SCALE-- 1" 25' ,APPROVED BY: DRAWN BY; Mecklenburg Co.
DATE! October 18, 2018 REVISED: ANP
I FOREST HILL CHURCH PARCELS I
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION DIAGRAM
E NUMBER:
CH18.129-4
Full -Service Analytical F
/'PRISMI Environmental Solutions
nA
Geoscience Group
Tam Hassett
500-K Clanton Rd.
Charlotte, NC 28217
INC. Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
Project: Forest Hill Church Parcels
Lab Submittal Date: 1010512018
Prism Work Order: 8100119
Case Narrative
t Oil 8/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody, Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please calf if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATQR.IES, INC.
Angela D. Overcash
VP Laboratory Services
Reviewed By Angela D. Overcesh
VP Laboratory Services
Data Qualifiers Key Reference:
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a T
This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 20224-0543
Phone: 704)529-U64 -Tull Free Number: I41DW529.5364 - Fax: 700525-0409 page i of $
ZR-I S n A ErivIr nrvice Analytical s
e ' V' Envl�anmentni Solutions
Sample Receipt Summary
10/1812018
Prism Work Order: 8100119
Client Sample ID Lab Sample ID Matrix Daterrime Sampled DatefTime Received
HA-1 6100119-01 Sand 10105/18 0.00 10/05/18 15:05
HA-2 8100119-02 Solid 10/05118 0:00 10/05/18 15:05
Samples were received In good condition at 4.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the wri}ten consent of Prism Laborstorles, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-DS43
Phone: 704f529-6364 - Toll Free Number: 1-0001529.6364 - Fax: 7WS25.0409 Page 2 of 8
Full-
.`P,AR I S M n envir " ice Anatyutio s
[V' E�vEranm�rrtsl Solutions
LI5wwomwsS, C:
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hilt Church Parcels
Sample Matrix: Solid
Laboratory Report
1011812018
Client Sample ID: HA-1
Prism Sample ID: 8100119-01
Prism Work Order: 8100119
Time Collected: 10105118 0a:00
Time Submitted: 1010&18 15:05
Parameter Result Units Report MIL Dilution Method Analysis Analyst Batch
Limit Factor datefrime II]
Diesel Range Organics by GCIFID
diesel Range Organics BRL mglkg dry
9.9 2.6 1
Surrogate
•8015c 10/11/18 16:36 ZRC PSJ0194
Recovery Control Limits
o-Terphenyl
84 % 31-123
Gasoline Range Organics by GCIFID
RLM
Gasoilne Range Organics BRL
molt dry
7.5 1,6
50 18015C 1018N8 19:38 ANCW PeJ0103
Surrogate
Recovery Control Limits
s.a.a-Trifluorotoluone
148 % 50.137 SR
General Chemistry Parameters
%solids 70.3
%by
0,100 0.100
1 'SM2540 G 1W16M8 16:40 TJY P&J0305
Weight
This report should not be reproduced, except in its entirety, without the written consent at Prism Lahoratories. Inc.
449 Springbrook Road - P.O. Box 240543 . Charlotrs, NC 28224-0543
Phone. 7WS29.6364-Toll Free Number:l-600;5x9-6364- Fax: 704152"4" Page 4 of 8
I FvliSer ice Annlylicel 8.
En�lronmenf�l Boiuti�ns
'-: �AKIRwTw�ame
Summary of Detections
1011 B!2018
Prism Work Order: 8100119
PHam ID Client ID Parameter Method Result Lirits
There were no detections reported.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: 7641529-6364 - Toll free Number: 9-8901529-6354 -Fax, 7041525-0409 Page 3 of 8
/ri®r-i!Service Anaiyt tl %; EnYironmantal Sulutlona
l•BDRATORIES 'NV
Geoscienoe Group
Attn: Tom Hassett
500.K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Laboratory Report
10AW018
Client Sample I❑: HA-2
Prism Sample I❑: 8100119-02
Prism Work finder: 8100119
Time Collected: 10105/18 00:00
Time Submitted: 10/05/18 15.06
Parameter Result Units Report VIAL Dilution Method Analysis Analyst Batch
Limit Factor ❑ate/Time I
Diesel Range Organics by GC1FID
Diesel Range Organics 13RL mglkg dry 9.9 2.6 1 'S0i5C 10111/18 17;1a ZRC P8J0194
Surrogate Recovery Control Limits
o-Terphenyl
St) 96 31-129
Gasoline Range Organics by GC/FlD
Gasoline Range Organics 6RL mglkg dry 9.9 2.1 50 *8015C 1018f18 20;O6 ANWJ PSJ0103
Surrogate Recovery Control Limb
a.a,a-Trikurotoluen e
General Chemistry Parameters
134 % 50-137
% Sol Ids 70.6 %by 0.100 0.100 1 '5012540G 10119/18 16;40 TJY Pt1J0305
weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"0 Sprsngbrook Road , P.O. Box 240543 - Chariotte, NC 2822"U3
Phone: 7041529$364 -Toll Free Number. 1-8001529.6364 • Fax; 70415254409 Page 5 of 8
L"P.,pLq
Full -Service Analylleal Environmental Solutions
Geoscience Group Project: Forest Hill Church Parcels
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, INC 28217
Gasoline Range Organics by GC*lD - quality Control
Level II QC Report
10/18118
Prism Work Order: 8100119
Time Submitted: 1015I2018 3:05:00PM
Reporting Spike Source %REG RPD
Ana lyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBJ0103 - 6035
Blank lPBJ0103-BLK1y
Prepared & Analyzed: 10/08118
Gasoline Range Organics
BRL
5.0 mglkg wet
Surrogate' a, a, a -Tiff uornVuene
5.20
rrlglkg
5.000 104
50-137
LCS (PBJ010343S1)
Prepared & Analyzed: 10108118
Gasoline Range Organics
59.7
5.0 mglkg wet
50.00 119
41-138
Surrogafe.' e,a,a-Trffuorofaluene
5.65
mg/kg
5.000 113
50-137
LCS Dup (158J0103-113SOI)
Prepared & Analyzed: 10/08118
Gasoline Range Organics
64.8
6-0 mg/kg wet
50,00 130
41-139 a 20
Surrogate: a,a,a-TriRuorotoiuerre
5.45
mg/kg
5.000 109
50-137
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratodes, Irr.
449 Springbraok Road - P.Q. Box 240543 - Cha►latte, NC 28224-0543
Phone, 704f$29-6364 -Toll Free Number: 1-0401529-5364 - t=ax: 70415254MO9 Page 6 of 8
P LgF I q M I FUIP-SeryiGe Analytical &
Envirenmpnral Solutions
L�eES �Nc
Geoscience Group Project: Forest Hill Church Parcels
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Diesel Range Organics by GCIFiD - Quality Control
Level fl QC Report
10116/18
Prism Work Order: 8100119
Time Submitted: 10f512018 3:05;04PM
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P830194 - 3546
Blank (PU0194-BLK1)
Prepared & Analyzed: 10111/18
❑iesel Range Organics
BRL
7.0
mglkg wet
Svrrogafe: a-Terphenyl
7.p7
mg*g wet
1.332 81
31-123
LCS (138J0194-13S'I) _
Prepared & Analyzed:_ 1_0111118
Diesel Range Drganics
51A
7.0
mglkg wet
66.64 77
46-126
Sun-ople: o-Tsrphenyf
1.18
mglkg wet
1.333 89
31-123
LCS Dup (PaJ0194-BS01)
Prepared & Analyzed. 1011 ill
Diesel Range Organics
54.0
7A
mg/kg wet
66.67 81
46.126 5 20
Surrogate:-7"mphenyl
1.16
rnglkg wet
1.333 87
31-121
Sample Extraction data
Prep Method- 3348
Lab Number Batch Initlal Final DateMme
8100119-01 PRJ0194 30.1 g 1 mL 10J11J18 8:42
6100119-02 PBJ0194 30.07 g 1 mL 10111J18 8:42
Prep Method: 5035
L.ab Number Batch Initial Final Dekslilme
6100119-01 PBJO103 4.77 g 5 mL ioiw18 12:03
8100119-02 P8J0103 3.58 g 5 mL 1p108f18 12:03
Prep Method: Solids, Dry Weight
Lab Humber Batch initial Final Dateirime
9100119-01 P8d0305 30 g 30 g 1(VI 8118 16:40
8100119-02 P8J0305 30 g 30 g 10116118 16:40
This report should not be reproduced, except in its enlirety, wlthout the written consent of Prism Laboratories, Inc.
449 Sprh►gbrook Road - P.U. Box 2405t3 - Charlotte, NC 28224-0543
Phone: 704J528-fs36d -Toll Free Number: 1-SM529.6364 - Fax: 7WS29-0409
Page 7 of 8
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INC CBrti Drinking
iOn Water
ert
■ � :. Full -Service Analytical � INCNC ❑risking Water Cert Iva. 37735 � p12412p1 g
Environmental Solutions SC GertiTrcatlon No. 99012
L a9MATOnIM INC.
Geoscience Group Project: Forest Hill Church Parcels
Tom Hessen
500-K Clanton Rd. Late Submittal Date. 10/12/2018
Charlotte, NC 28217 Prism Work Order: 8100259
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully.
PRISM LABORATORIES, INC.
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference
Reviewed By Robbi A, Jones For Angela D. Overcash
President/Project Manager
DO Surrogates diluted out.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not he reproduced, except in its entirety, without the written eonsent of Prism Laboratories, Inc.
449 5pringbrook Road - P.a. ISox 240543 - Chatlotte. NC 28224.0543
Phone: 704l529.6364 - Toll Free Number: 1-6001529-6364 - Fax: 7041523.0409 Page 1 of $
PRISM I Full Service al Golubo a
Sample Receipt Summary
Enviranm®oral Solutions 1012412018
LA6pgA;nRCa LNG
Prism Work Order; 8100289
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
HA-3 8100259-01 Solid 10/12118 10:08 10/12/18 13:30
HA-4 8100259-02 Solid 10112J18 11:45 10/12/18 13:30
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road . P.O. Box 240543 - Charlotte, INC 26224-6543
Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 -Fax: 7U/625-0409 Page 2 of i3
4 Full -Service AnaEytical&
ISM I Envrranmental Solutlons
LAB�P�TGRILR IMr,
Summary of Detections
1012412018
Prism Work Order: 8100259
Prism ID
Client I❑
Parameter
Method
Result
Units
8100259-01
HA-3
Diesel Range Organics
'8i315G
26000
Mg/kg dry
81002$9-01
HA-3
Gasoline Range Organics
'9Et1SC
2300
mglkg dry
8100259-02
HAA
Diesel Range Organics
'8015C
3500
mglkg dry
8100259-02
HA-4
Gasoline Range Organics
18aisc
99
mglkg dry
This report should not be reproduced, except in its entirety, without the written consent otPrism Laboratories, Inc.
4449 8pringbrook Read - P.O. Box 240543 . Charlotte, NC 28224d1S43
Phone: 7041529.6364 - Toil Free Number: f-soW529-6364 - Fax: 704Ai2S-Wl1 Page 3 of 8
I S n � I Full-Serorce Analytical a
V' I Environmental Solutions
�Rn,aAcs ��
Geoscience Group
Attn: Tom Hassett
50D-K Clanton Rd.
Charlotte, NO 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Laboratory Report
10124/2010
Client Sample ID: HA-3
Prism Sample ID: 8100259-01
Prism Work Order: 8100259
rme Collected: 10/12/18 10-08
Time Submitted: 10112I18 13:30
Parameter Result Units Report MOL Dilution Method Analysls Analyst Balch
Limit Factor Dat"Mme ID
Diesel Range Organics by GCIFID
Diesel Range Organics 26000 rngfhg dry 1900 500 200 18615C 10M7118 9:08 IRC P8J0283
Surrogate R--ery Cdhtrol Limits
o-Terphenyl 0 % 31-123 OQ
Gasoline Range Organlcs by GCIFID
Gasoline Range Organics 2300 m9/kg dry 93 20 Sao "8015C 10119118 9:33 ANGIJ PBJ0333
Surrogate
a, a,a-Triflu orotalV en e
Retavery Contrd Limits
110 % 50-137
General Chemistry Parameters
% Solids 73.9 'Y by 0.100 0.100 1 `SM2S40 G 10122I18 1410 TJY P810417
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism LabDfatones, Inc_
449 Springhroott Road - P.O. Box 240543 • Charlotte, NC 28224-0543
Phone: 7041529-5354 -Tall Free (dumber: 1-8001529-6354- Fay: 70d1525-"09 Page 4 0f 8
Laboratory Report
�FR ISM I E, vir amen analytical 8
! Environmental 801ufign3 10r2412018
'%` .AHWTpMl" iaq
Geoscienee Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Client Sample ID: HA-4
Prism Sample ID: 8100259-02
Prism Work Order: 8100259
Time Cotlected: 10/12/18 11:45
Time Submitted: 1011211813:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatelTme Ill
Diesel Range Organics by GCIFID
Diesel Flange Organics 3500 mglkg dry 490 18$ 50 *$015G 10MVi8 7:50 ZRC PSJ0283
Surrogate Recovery Control Limits
o-Terphenyl
0 % 3f-723 00
Gasoline Range Organics by GC1FID
Gasoline Range Organics 99 myfky dry 7.9 1.7 So "8olsc 10119118 511 ANGM P$J0333
Surrogate Recovery Control Limits
a,a.a-Trifluorotaluene 118 % 5D-137
General Chemistry Parameters
%Solids 71.0 %by 0.100 0.100 1 '3M2540G 1012211814:30 TJY PSJ0417
Weight
This report should not be reproduced, except in ita entirety, without the written consent of Prtsrn Laboratories, Inc.
449 Springbrook Road • P.O. Bum 240543 - Charlotte, NC 28224-0543
Phone: 7041529-0364 • Toil Free plumber: 1$001529-4384 - Fax: 7041525-MO Page 5 of 8
�R I S h ,♦� Full -Service Analytical
I V I � Environmental Sofu[fans
its- h&
Geosoience Group Project: Forest Hill Church Parcels
Attu: Torn Hassett
500-K Clanton Rd.
Charlotte. NC 28217
Gasoline Range Organics by GGlFID -{duality Control
Level li QC Report
10124l18
Prism Work Order: 8100259
Time Submitted: 10/12/2018 1:30:OOPM
Reporting
Spike Source
%REC RPD
Analyse
Result
Urnk
Units
Level Result %REC
Limits RP❑ Limit Notes
Batch MOM - 5035
Blank (P8J0333-BLK1)
Prepared BAnaWed: iOil all 8
Gasoline Range Organics
RRL
5.0
rnglkg wet
Surr*g'?fe: a,a,a-7nfl(forW010ene
5.05
mg*9
5.00U 101
50-137
LCS (P8J0333-051)
Prepared & Analyzed: 10118/18
_
Gasoline Range organics
55.4
5.0
mglkg wet
50.00 111
41-138
Surrogate: a,a,a-Tnfiuorat0iuene
4.90
mglkg
5.000 98
50-137
l_CS Dup IMID333-MI)
Prepared & Analyzed: i0/18/18
Gasoline Range Organics
81A
5.0
Mog wet
50.00 122
41-139 10 20
Surrogate: a,a,a-Trtluarotoluene
&00
mglkg
5.000 100
50-137
This report should not be reproduced. except in Its entirety, without the written consent of prism Laboratories. Inc,.
448 Springhrook Rnad - P.O. Box 24OS43 - Charlotte, INC 28224.0543
Phone: 7041529-6364 - Tall Free Humber: 1.8001529-6364 - fax: 704(525-0409
Page 6of8
+� R I S i Fuu-Service AnafS'xical 8
Enviranmenx>Ri SaEu[fona
ORA70o OL ING
Geoscdence Group Project; Forest Hill Church Parcels
Attn: Tam Hassett
5OD-K Clanton Rd.
Charlotte, NC 28217
Diesel Range organics by GCIFID - Quality Control
Level II QC Report
10124118
Prism Work Order: 8100259
Time Submitted: 10/12/2018 1:30:OOPM
Reporting Spike Source %REC RPO
Anaiyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBJ0283 - 3546
Blank (PSJ0283-BLK1 )
Prepared a& Analyzed: 1 D116118
Dlesel Range Organics
BRL
7.0 mglkg wet
Surrogate: o-Terphenyl
0.929
mg/kg wet
1,333 70
31.12.3
LIDS (P8J0283-1351) _
Prepared & Analyzed: 1011-6118
Diesel Range Organics
59.1
7.0 mglkg wet
66.67 69
46.126
Surrogate: u-Terphenyl
1.24
mgft wet
1.333 93
39-123
LCS oup (P8J0253-BSDI)
Prepared &Anatyze_d: 10116118
Diesel Range Organics
55.8
7.o mglkg wet
66.67 84
46-126 6 20
Surrogate. o-Terphenyl
1.08
mglkg wet
1.333 81
31-123
Sample Extraction Data
Prop Method: 3546
Lab Number Batch Inkial Final Daterrinn
8100259-01 PBJ0283 30.1 g 1 mL 10118118 11:35
8100259-02 PBJ0283 30A2 g 1 mL 10116118 11:35
Prep Method: 5035
Lab Number Batch
Initial
Final
DatalTime
81 OD259-01 POJ0333
3.62 g
5 mL
1 WI8118 10:64
81D0259-02 P8J0333
4.46 g
5 mL
10/18118 11154
Prep Method: Sands, Dry V"ht
Lab Number Batch
inlitlal
Final
Datefllme
8100269.01 P8J0417 30 g 30 9 1W2118 14:30
811DO259-02 P8J0417 30 g 30 g 10122118 14:30
This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2a224.0543
Phone: 704I529-6364 -Toll Free Number. 1.8001529.6364 - Fax: 704/525-04H Page 7 of 8
Phase I Environmental Site Assessment
Forest Hill Church Parcels
Charlotte, North Carolina
Ceoscience Project No. CHI8.0129. GE
Prepared For:
Forest Hill Church
elo Johnston, Allison, & Hord Attorneys
1065 East Morehead Street
Charlotte, Noilh Carolina 28204
December 13, 2018
Prepared By:
GECDSCENCE GROUP
500 Clanton Road, Suite K
Charlotte, North Carolina 28217
Phone (704) 525-2003 Facsimile (704) 525-2051
December 13, 2018
Consulting Engineers
Forest Hill Church
GEQSCIENCE c/o Johnston, Allison, & Hord Attorneys
GROUP 1065 East Morehead Street
Charlotte, North Carolina 28204
Attention, Mr. William Berkeley
Reference. Phase 1 Environmental Site Assessment
Forest Hill Church Parcels
Concord, North Carolina
Geoscience Project No. CHI 8.0129.GE
EXECUTIVE SU1MI1lfARY
Geoscience Group, Inc. (Geoscience) has completed a Phase I Environmental Site
Assessment (ESA) of an approximate 1.854t acre tract located along the northeastern side of
East 36"' Street, immediately north of its intersection with North McDowell Street in Charlotte,
North Carolina. This Phase I ESA has been performed in general accordance with the scope
and limitations of ASTM Standard E 1527.13 and in compliance with Geoscience's proposal
dated August 21, 2018 (Geoscience Proposal No. CH18.197P.EV). Any exceptions to, or
deletions from, the ASTM E 1527-13 standard of practice are described in the
INTRODUCTION section of the report. Based upon our findings, this assessment has revealed
no evidence of recognized environmental conditions in association with the subject property
with the exception of the following:
1) Two (2) underground storage tanks (USTs) used to stnre heating oil were observed on
the subject property: UST-1 adjacent to the single-family dwelling and UST-2 adjacent
to the existing church. In an attempt to determine whether releases have occurred
from these USTs, Geoscience advanced a total of four (4) hand auger borings HA-1
through HA-4) adjacent to the ends of the tanks. Soil samples collected from the
borings were analyzed for total petroleum hydrocarbons in the gasoline and diesel fuel
ranges (TPH-GRG and TPH-DRO).
Neither TPH-GRO nor TPH-DRO were detected in the samples (HA-1 and HA-2)
collected adjacent to UST-1. As such, it does not appear that releases have occurred
from that tank. However, the soil samples collected adjacent to UST-2 (HA-3 and
HA-4) exhibited TPH-GRO and TPH-DRO concentrations exceeding Action Limits
established by NCDEQ (see Table 1 in Appendix 1). Based on the sample results, it is
apparent a heating oil release has occurred from UST-2. Therefore, UST-2 is
considered to be a recognized environmental condition in association with the subject
property.
50G Cra';ion Roan Charsore. North. Carolina Teseohone Fac rue r.'C License
5ui1e K 2821', M4 525.2003 7C•152^ 210F-DS85
Forest Hill Church
Geoscience Project No. CH18.0129.GE
December 13, 2018
Page 2
INTRODUCTION
Purpose: This Phase I ESA was performed to identify the presence or likely presence of any
hazardous substances [as defined by CERCLA 42 USC §9601(14)] or petroleum products on
the property under conditions that indicate an existing release, a past release, or a material
threat of a release of these products into structures on the property or into the ground,
groundwater, or surface water of the property. This includes hazardous substances or
petroleum substances under conditions in compliance with laws. It should be noted that the
ASTM E 1527-13 standard of practice does not include an assessment of all passible
conditions or circumstances that may exist at the subject site. Several anon -scope
considerations that were not a part of these assessment activities included reviews for
asbestos, lead based paint, wetlands, and radon, among other items not addressed by ASTM
Standard E 1527--13.
Based on the information provided, the Phase I ESA was performed as part of a property
transaction. As such, Geoscience understands that the purpose of the assessment was, in
part, to satisfy a requirement to qualify for the innocent landowner defense to CERCLA
liability. In accordance with the ASTM E 1527-13 standard of practice, this Phase I ESA
included a reconnaissance of the subject site and adjoining properties, interviews with persons
knowledgeable about the site, and a review of historical and regulatory databases. The site
reconnaissance and interviews were performed as part of the assessment to obtain
information indicating the likelihood of the presence of recognized environmental
conditions. Historical and regulatory sources were reviewed to help identify recognized
environmental conditions in connection with the property and to develop a history with
respect to site usage.
Practically reviewable, publicly available information pertaining to the property was also
used to prepare the Phase I ESA. This report interprets and summarizes the information
obtained from interviews, document reviews, and site reconnaissance. Per ASTM E
1527-13, it is the responsibility of the User of this document to investigate the existence of
environmental liens in reasonably ascertainable recorded land title records.
Site Reconnaissance: The most recent site visit was performed by Geoscience on October
12, 2018. The reconnaissance consisted of observing the periphery of the property and
viewing the site from accessible adjacent public thoroughfares, where possible. Interior
portions of the property were systematically traversed to provide an overlapping field of view.
Visual reconnaissance of adjoining properties was limited to areas and facilities that were
readily observable from the subject property or from public access areas. Photographs were
taken to document the features observed and environmental conditions of concern. Due to the
general limitations imposed by the method of observation, the potential exists that undisclosed
environmental conditions may be present beneath the areas observed. A photographic log
(Photographs l through 19) of the subject site has been provided in Appendix it of this report.
The approximate locations and directions of the photographs are shown on the Site Layout,
Figure No. CH18.129-3, in Appendix 1.
Forest Hill Church
Geoscience Project No_ CHI8.0129.GE
December 13, 2018
Page 3
Interviews: The persons noted in the following table were contacted to obtain information for
this assessment. Documentation of our contact with the listed parties is included in Appendix
V of this report. Pertinent information reported by the listed parties is discussed in the
appropriate sections of the report.
Name
Title/Function
Affiliation
Date
Contact Information
Mr. William
Client
Forest Hill Church
Various
(704) 622-8584
Berkeley
Representive
Mr. Tim
Charlotte Fire
Hartsell
Battalion Ctcief
Department
14J3118
(704) 336-2461
Information Provided by User: Geoscience requested that Forest Hill Church Attorneys (the
Client and User of this document) communicate any specialized knowledge or experience that
is material to recognized environmental conditions in connection with the property and to
identify key personnel for interview purposes. As part of that request, User and Environmental
Questionnaires were submitted to the Client for completion by appropriate people. Review of
the questionnaires, as completed by Mr. William Berkeley, that revealed an oil tank is located
adjacent to the church. Concerns related to the tank are discussed in the Site Reconnaissance
Findings section later in this report. Copies of the completed User and Environmental
Questionnaires are included in Appendix V.
SITE DESCRIPTION AND PHYSICAL SEWNG
Location And Leval_ Description: As shown on the enclosed. Vicinity Map, Figure No.
CH18.129-1, the subject site, with the physical addresses of 719 and 729 East 36'h Street and
3315 North McDowell Street, is located along the northeastern side of East 36h Street,
immediately north of its intersection with McDowell Street in Charlotte, North Carolina. The
site is comprised of Mecklenburg County Tax Parcel ID Nos. 09110401 and 09110402. The
approximate legal boundaries of the site are shown on the Tax Line Map included in Appendix
I as Figure No. CH 18.129-2.
Site And Vicinity Characteristics: As depicted on the Site Layout, Figure No. CHI8.129-3,
the subject property is comprised of a 1.854+ acre tract. As shown in Photographs 1 through
7 in Appendix II, an existing church, its associated school, a single-family dwelling, and
their associated outbuildings currently occupy the southern portion of the subject site. The
remainder of the property, as shown in Photograph 8 through 11, consists of landscaped
areas and a small garden.
North Alexander Street extends along the northern property boundary. The land across this
roadway fiom the subject site is occupied by The Church of Jesus Christ, its associated
outbuildings, Mercury Apartments and a single-family dwelling. Six (6) single-family
dwellings adjoin the subject site to the east. North McDowell Road extends along the
southern property boundary.
Forest Hill Church
Geoscience Project No. CH18.0129.GE
December 13, 2018
Page 4
The land across North McDowell Road from the subject site is occupied by condominiums
and two (2) single-family dwellings. East 36eh Street extends along the western properly
boundary. The land across this roadway from the subject site is occupied by five (5) single-
family dwellings.
Topography: As part of this assessment, the 2015 County Topographic Map (Figure No.
CH18.129-5), and the 1967 (Photorevised 1988) "Charlotte East, North Carolina" United
States Geological Survey (USGS) 7.5-minute quadrangle map (Figure No. CH 18.129-6) were
reviewed to obtain information relative to the topography of the subject site and surrounding
areas. According to the contour lines of the above listed topographic maps, the subject site is
located between approximately 724 and 730 feet above mean sea level (MSL). The ground
surface across the project site generally slopes downward toward the northwest. The low
elevation of 724 feet MSL is located on the northern property boundary and the high elevation
of 730 feet MSL is located on the and southeastern portion of the site.
Surficial And Bedrock Geoloy: The 1985 Geologic Map of North Carolina was reviewed as
a part of this assessment to provide discretionary and non-standard physical setting source
information relative to the geology in the vicinity of the subject property. A review of this map
indicates that the subject site is located within the Charlotte Belt of the Piedmont
Physiographic Province. This Province is generally characterized by igneous intrusive and
metamorphic bedrock that is Pennian to Ordovician in age. The intrusive rock is typically
overlain with a layer of soil and weathered rock, ranging in thickness from 0 to 150 feet.
Bedrock within the Charlotte Belt consists primarily of the diorite -granite complex, with
granite appearing to be the predominant component of the complex_ According to the
geologic map of North Carolina, the regional bedrock underlying the subject property
generally consists of metamorphosed quartz diorite.
Surface Water And Groundwater Flow: The predominant source of groundwater in the area
is the unconfined aquifer system. Water availability in the aquifer varies with location, rock
type, topographic setting, and geologic structure. Recharge of the aquifer system is through
the infiltration of rainwater.
Surface water and groundwater flow rates and directions were not determined as part of this
assessment. However, based upon review of the USGS topographic map, the infen�ed
direction of groundwater flow beneath the subject property is northwestward. Based upon
visual observations and the site topography, Geoscience expects that surface water at the site
flows towards the northwest.
Soil Conservation Service Map Review: The United States Department of Agriculture Sail
Conservation Service (SCS) conducted a soil survey of Mecklenburg County, North
Carolina in cooperation with the North Carolina Agricultural Experiment Station. The soil
survey information reviewed for this report was issued by the SCS in September 2016 and
describes the soils at the subject site as Cecil -Urban land complex with 2 to 8 percent slopes
(CuB) and Helena -Urban land complex with 2 to 8 percent slopes (HuB).
Forest Hill Church
Geosczence Project No. CHI8.0129,GE
December 13, 2018
Page 5
Utilities: Utilities provided to the subject property include:
• Electricity provided by Duke Energy;
Natural gas provided by Piedmont Natural Gas;
• Sewage disposal provided by Charlotte Water; and
Potable water provided by Charlotte Water.
Environmental Liens: Per ASTM E 1527-13 it is the responsibility of the User of this
document to investigate the existence of environmental liens in reasonably ascertainable
recorded land title records.
PROPERTY USAGE
Current Uses Of The Property: As previously described, the subject site is currently occupied
by a church and a single-family dwelling.
Past Uses Of The Property: To the extent practically possible, past uses of the subject property
were identified through historical records review, reconnaissance observation, interviews,
andlor through client -provided information. Historical information sources researched during
this assessment date back to 1905. A summary of the standard historical sources and data
reviewed by Geoscience to identify past uses of the property are listed in the table below.
Copies of representative: historical source information are provided in the applicable
Appendices.
Historical Data Sources
Years Reviewed
Data Source/PubUsher
Note
1948, 1956, 1965, 1968, 1971, 1976,
1983, 1988, 1993, 1996, 1998, 2002,
Mecklenburg County GIS,
Aerial Photographs
2004, 2045, 2006, 2007, 2008, 2009,
Google Faith and EDR
2010, 2012, 2013, 2014, 2015, 2016,
2017, and 2018
Sanborn Maps
p
1911, 1929, 19M, 1953, 1958, 1962,
EDR
and 1963
1921, 1925, 1931, 1937, 1944, 1949,
City Directories1979,
1953, 1959, 1964, 1969,1974, 1975,
EDR
1984, 1989, 1991,1994, 1999,
2005, 2010, and 2014
Property Tax Listings
2018
Mecklenburg County GIS
County Topographic Map
2015
Mecklenburg; County GIS
U5GS Topflt;raphic Map
1942
USGS, "Charlotte, NC'
30-minute quadrangle
Forest Hill Church
Geoscience Project No. CHI 8.0129.GE
December 13, 2018
Page 6
USGS Topographic Map
1905 and 1907
USGS, "Charlotte, NC"
15-minute quadrangle
1948, 1949, 1967, 1980, 1988, and
USGS, "Charlotte East;
USGS Topographic Map
NC" 7.5-minute
2013
uadra le
USGS Topographic Map
1949, 1972, 1996, mid 2013
USGS, "Derita, NC" 7.5-
minute quadrangle
Forest Hill Church, the church's school, a single-family dwelling, and their associated
outbuildings currently occupy the site. Mecklenburg County tax listings indicate that the
church and its school were constructed in 1929 and 1957, respectively. The single --family
dwelling was reportedly constructed in 1941. These dates are consistent with our review of
aerial photographs and Sanborn reaps. Our review of city directory listings revealed that prior
to operating as Forest Hill Church, the church had been occupied by North Charlotte
Presbyterian Church and Johnston Memorial Presbyterian Church. Further review of aerial
photographs and Sanborn maps reveals a former single-family dwelling occupied the
southeastern portion of the site from at least 1929 until it was demolished in 2008. The 2013
aerial photograph depicts the southeastern portion of the site being used as a garden. The
remainder of the site has been vacant land since at least 1929.
Current And Past Uses Of Adjoining Properties: The current and past uses of adjoining
properties were identified through reconnaissance observation and records review.
North: North Alexander Street extends along the northern property boundary. Our review of
Sanborn maps reveals construction of this roadway occurxed sometime between 1911 and
1929. The land across North Alexander Street from the subject site is occupied by The Church
of Jesus Christ, its associated outbuildings, Mercury Apartments, and a single-family dwelling.
Mecklenburg Cotmty tax listings indicate the church and its outbuildings were constructed in
1979, 1969, and 1980, respectively. Mercury Apartments and the single-family dwelling were
reportedly constructed in 2014 and 1926, respectively. These dates are consistent with our
review of aerial photographs and Sanborn maps. Further review of aerial photographs reveals
that prior to construction of the existing improvernents, the areas northwest and north of the
subject site had been occupied by single-family dwellings since at least 1929.
EaW: Six (6) single-family dwellings adjoin the subject site to the east. Mecklenburg County
tax listings indicate the houses were constructed at various times between 1926 and 2012_
These dates are consistent with our review of aerial photographs and Sanborn maps. Prior to
construction of the newer homes, those eastern adjoining lots had been occupied by previous
houses since at least 1929.
South: North McDowell Street extends along the southern property boundary. Our review of
Sanbom maps reveals this roadway was constructed before 1929. The land across North
McDowell from the subject site is occupied by condominiums and two (2) single-family
dwellings. Mecklenburg County tax listings indicate the condominiums were constructed in
2010 and the single-family dwellings in 2009 and 1926, respectively.
Forest Hill Church
Geoscience Project No. CH18.0129.GE
December 13, 2018
Page 7
These dates are consistent with our review of aerial photographs and Sanborn maps. Further
review of historical sources reveals that prior to construction of the existing buildings, the land
that adjoins the subject site to the south had been occupied by single-family dwellings since at
least 1929.
West-: East 36`h Street extends along the western property boundary. Construction of this
roadway predates the 1911 Sanborn map. Our review of Sanbom maps reveals the road was
named 323,d Street from at least 1929 until at least 1950 when it is renamed 36 h Street. The
land across East 36"' Street fiorn the subject site is occupied by five (5) single-family
dwellings_ Mecklenburg County tax listings indicate the houses were constructed between
1905 and 1940. These dates are consistent with our review of aerial photographs and Sanborn
maps.
REGULATORY RECORDS REV2`EW
Information for the standard Federal, State and Tribal environmental record sources specified
in ASTM Standard E 1527-13 § 8.2.1 was obtained through Environmental Data Resources,
Inc. (EDR). Regulatory database information was reviewed to help identify evidence of
recognized environmental conditions in connection with the property. The number of listed
sites identified within the approximate minimum search distance (AMSD) specified in the
standard environmental records database are summarized in the table on the following pages.
Detailed information for sites identified within the AMSD is provided following the table
along with our professional judgment about the significance, if any, of the listing. Copies of
the EDR research data and a description of the databases are included in Appendix 1V of this
report.
Target
Search
Total
Database
Distance
<'A
'A—'I4
'1-1/a
'A— 1
>1
Plotted
(Miles)
Federal Records
NPL
1
0
a
0
❑
NR
0
Proposed NPL
1
0
0
0
0
NR
0
Delisted NPL
1
0
0
0
0
NR
0
NPL LIENS
TP
NR
NR
NR
NR
NR
0
CERCLIS
'/7.
0
0
1
NR
NR
1
CERC-NFRAP
'/2
0
0
1
NR
NR
1
LIENS 2
TP
NR
NR
NR
NR
NR
0.
CORRACTS
1
0
0
1
1
NR
2
RCRA L G
'1
0
0
NR
NR
NR
0
RCRA S G
'I
0
a
NR
NR
NR
0
RCRA CES G
1
0
0
NR
NR
NR
0
RCRA NonGen
'I
0
1
NR
NR
NR
1
RCRA-TSDF
'%2
0
0
1
NR
NR
l
US ENG
CONTROLS
'%
0
0
0
NR
NR
0
Forest Hill Church
Geoscience Project No. CHI8.0129.GE
December 13, 2018
Page S
Search
Total
Database
Propeerty
Distance
<'/e
/x-'/a
%-Vx
%7- 1
>1
Plotted
(Miles)
Federal Records (Continued)
US INST
CONTROL
%
0
0
0
NR
NR
0
ERNS
TP
NR
NR
NR
NR
NR
0
HMIRS
TP
NR
NR
NR
NR
NR
0
DOT OP S
TP
NR
NR
NR
NR
NR
0
US CDL
TP
NR
NR
NR
NR
NR
0
US
BROWN FIELDS
'1/a
0
0
0
NR
NR
0
DOD
1
0
0
0
0
NR
0
FMS
1
0
0
0
0
NR
0
LUCIS
�6
0
0
0
NR
NR
0
CONSENT
1
0
0
0
0
NR
0
ROD
1
0
0
0
0
NR
0
UIVITRA
'!2
0
0
0
NR
NR
0
ODI
'/a
0
0
0
NR
NR
0
MINES
J
0
0
NR
NR
NR
0
TRI5
TP
NR
NR
NR
NR
NR
0
TSCA
TP
NR
NR
NR
NR
NR
0
FTTS
TP
NR
NR
NR
NR
NR
0
HIST FTTS
TP
NR
NR
NR
NR
NR
0
SSTS
TI'
NR
NR
NR
NR
NR
0
ICIS
TP
NR
NR
NR
NR
NR
0
PADS
TP
NR
NR
NR
NR
NR
0
NITS
TP
NR
NR
NR
NR
NR
0
RADINFO
T?
NR
Nit
NR
NR
NR
0
FMS
TP
NR
NR
NR
NR
NR
0
ECHO
TP
WR
NR
NR
NR
NR
0
RAATS
TP
NR
NR
NR
NR
NR
0
SCRD
DRYCLEANERS
0
0
0
NR
NR
0
State and Local Records
SHW S
1
0
0
4
12
NR
16
NC HSDS
1
0
0
I
4
NR
5
IMD
'h
2
0
16
NR
NR
18
SWFILF
'/.
0
1
0
NR
NR
1
OLI
��
0
0
0
NR
NR
0
HIST LF
'IA
0
1
0
NR
NR
I
LUST
'fx
2
4
I5
NR
NR
21
LAST
%
0
0
I
NR
NR
1
LUST TRUST
'A
0
3
3
NR
NR
6
UST
V.
2
0
NR
NR
NR
2
AST
V4
0
0
NR
NR
NR
0
INST CONTROL
%
0
0
0
NR
NR
0
SWRCY
'I2
0
0
1
NR
NR
I
Forest Hill Church
Geoscience Project No. GHI8.0129.GE
December 13, 2018
Page 9
Search
Total
Database
Propecrty
Distance
<''A
t1/9--'/a
VI—'/z
'/z— 1
>1
(Miles)
Plotted
State and Local Records (Continued)
VCP
Vz
0
1 0
0
NR
NR
0
DRYCLEANERS
V
0
0
NR
KR
NR
0
BRDWNFIELDS
2
2
NR
NR
4
NPDES
TP
NR
NR
NR
NR
NR
0
Tribal Records
INDIAN
RESERV
1
0
0
0
0
NR
0
INDIAN DDI
'/2
0
0
0
NR
NR
0
INDIAN LUST
°/2
0
0
0
NR
NR
0
INDIAN UST
%
0
0
NR
NR
NR
0
INDIAN VCP
1
�/z
0
0
0
1 NR
NR
0
EDR Proprietary Records
Manufactmd Gas
1
0
0
0
0
NR
0
Plant
EDR Historical
''
3
NR
NR
NR
NR
3
Auto Stations
EDR Historical
%
2
NR
NR
NR
NR
2
Cleaners
NOTES. TP = Target Property; NR = Not Requested at this Search distance; Sites may be listed in snore than one database.
Subject Property Database Findings: No listings for the subject property were discovered
during the regulatory records review,
Adjoining Property Database Findings: No listings for adjoining properties were discovered
during the regulatory records review.
Non-Adioiniag Property Database Findings: EDR reported sixty-seven (67) listings for
non -adjoining sites within the AMSD. Based upon their EDR-reported locations and review
of the USGS topographic map, the non -adjoining sites appear to be situated within areas that
are considered to be hydraulically down gradient or cross gradient from the subject
property, with inferred directions of groundwater flowing away from the subject property.
Given their inferred directions of groundwater flow, distances from the subject property,
and/or regulatory status, the incidents associated with the non -adjoining properties are not
expected to adversely impact the subject site. As such, we do not consider these sites to be
recognized environmental conditions in association with the subject property.
orphan Sites: During compilation of the EDR database report, some potential risk properties
may be identified which cannot be accurately mapped due to poor or inadequate address
information. These properties are usually listed in the EDR report as unmappable. According
to EDR, three (3) listings for unznappable (orphan) sites were identified in the database
findings. At the time of our site visit, a vehicular reconnaissance of the area within
Forest Hill Church
Geoscience Project No. CH18.0129.GE
December 13, 2018
Page 10
approximately ''/s mile of the subject property was conducted in an effort to locate orphan sites.
No orphan sites were identified as being in close proximity to the subject property.
Additional Environmental Record Sources: Pursuant to ASTM Standard E 1527-13,
additional environmental record sources were obtained to enhance and/or supplement the
standard environmental record sources. As part of this Phase I ESA, records available an the
North Carolina Department of Environmental Quality (NCDEQ) website were reviewed. In
addition, the Mecklenburg County Emergency Management Department was contacted to
provide supplemental information and determine if any environmental conditions are known to
exist or have formerly existed at the subject site and/or off -site adjoining properties. The
following issues were addressed with respect to the subject site and adjoining properties:
• Groundwater Quality;
• Surface Water Quality;
• Solid Waste;
• Surface Spills;
• Hazardous Waste Storage and Disposal; and
• Underground Storage Tanks (USTs).
Geoscience discovered no records maintained by NCDEQ pertaining to the subject site or
adjoining properties.
The Mecklenburg County Emergency Management Department indicated that they had no
records of hazardous material responses in the vicinity of the subject site.
SITE RECONNAISSANCE FINDINGS
Sub ect Property Reconnaissance Findings: As mentioned previously, a reconnaissance was
performed at the subject site to obtain information indicating the likelihood of recognized
environmental conditions in connection with the property. A summary of uses and conditions
specifically addressed and consistent with ASTM Standard E 1527-13 is provided below:
• Hazardous Substances In Connection With Identified Uses: No hazardous substances
were observed on the subject site.
Storage Tanks: As shown in Photographs 12 and 13 in Appendix II, two (2)
underground storage tanks (USTs) used to store heating oil were observed on the
subject site. UST-1 adjacent to the house; and UST-2 adjacent to the church. In an
effort to determine whether releases have occurred from the tanks, Geosciertce
performed four (4) hand auger borings (HA-1 through HA-4) adjacent to the ends of
the USTs. The approximate locations of the tanks and hand auger borings are
indicatod on the Sample Location Diagram, Figure No. CH18.129 4 in Appendix I.
Each boring was advanced to a depth of ten (10) feet below the ground surface, and the
retrieved cuttings were screened in the field with a photoionization detector (PID).
Forest Hill Church
Geoscience Project No. CH18.0129.GE
December 13, 2018
Page 11
Based on the PID readings, one soil sample was selected from each boring for
laboratory analysis. The selected samples (HA-1 through HA-4) were placed in
laboratory supplied containem, packed on ice, and submitted under appropriate chain -
of -custody to Prism Laboratories to be analyzed for total petroleum hydrocarbons in
the gasoline and diesel fuel ranges (TPH-GRO and TPOH-DRO).
The results of the soil sample analyses are listed in Table 1 in Appendix 1. As shown,
neither TPH-GRO nor TOH-DRO were detected in the samples collected adjacent to
UST-1. Based on these findings in conjunction with our observation of the soils fi-om
borings HA-1 and HA-2, Geoscience concludes that a release from UST-1 is not
likely. As such, we do not consider UST-1 to be a recognized environmental condition
in association with the subject property.
The soil samples collected adjacent to UST-2 (HA-3 and HA-4) exhibited petroleum
concentrations exceeding the Action Limits of 100 mglkg and 50 mg/kg established by
NCDEQ for TPH-GRO and TPH-DRO, respectively. Specifically, TPH-GRO and
TPH-DRO were detected in sample HA-3 at concentrations of 2,300 mg/kg and
26,000 mg/kg, respectively. The concentration in sample HA-4 were 99 mg/kg
TPH-GRO and 3,500 mgfkg TPH-DRO. Based on these sample results, it is apparent
a heating oil release has occurred from UST-2. Therefore, the release from UST-2 is
considered to be a recognized envirorunental condition in association with the subject
property. Copies of the laboratory test reports are included in Appendix V.
• Polychlorinated Biphenyls_ fPCBs : During the reconnaissance, three (3) pole
mounted electrical transformers were observed on the subject site. As observed, the
transformers appeared to be in good condition with no evidence of leak or discharge.
Based on our observations, Geoscience does not consider the on -site transformers to
be recognized environmental conditions in association with the subject property.
• Indications Of Solid 'Waste Disposal: As shown in Photographs 14 through 19 in
Appendix II, solid wastes consisting of empty bulk totes, plastic drums, plastic, and
wood were observed on the southeastern portion of the site. No evidence of improper
hazardous material disposal, staining, leaks, or unusual odors were observed in the
vicinity of the observed wastes. With the exception of de minimis litter, no other
indications of solid waste disposal were observed on the subject property.
Adioinin2 Properties Reconnaissance Findings: A summary of uses and conditions
specifically addressed at adjoining properties that are consistent with ASTM Standard E 1527-
13 § 9.4.2.3 through § 9.4.4.7 and indicate the likelihood of recognized environmental
conditions in connection with the subject Site is provided below:
• Bazardous Substances In Connection With Identified Uses: No hazardous substances
were observed on properties adjoining the subject site.
Forest Hill Church
Geoscience Project No. CHI 8.0129.GE
December 13, 2018
Page 12
■ Storage Tanis: No above ground or underground storage tanks were observed on
properties adjoining the subject site -
Polychlorinated Bi hen is (PCBs): During the reconnaissance, three (3) pole
mounted electrical transformers were observed on adjoining properties. As observed,
the transformers appeared to be in good condition with no evidence of leak or
discharge. Based on our observations, Geoscience does not consider the off -site
transformers to be recognized enviroutnental conditions in association with the
subject property.
• Indications Of Solid Waste Disposal: With the exception of de minimis litter, no
evidence of improper solid waste disposal, staining, leaks, or unusual odors were
observed on adjoining properties during our reconnaissance.
FINDINGS AND CONCLUSIONS
Geoscience Group, Inc. (Geoscience) has completed a Phase I Environmental Site
Assessment (ESA) of an approximate 1.854± acre tract located along the northeastern side of
East 361h Street, immediately north of its intersection with North McDowell Street in Charlotte,
North Carolina_ This Phase l ESA has been performed in general accordance with the scope
and limitations of ASTM Standard E 1527-13 and in compliance with Geoscience's proposal
dated August 21, 2018 (Geoscience Proposal No. CH18.197REV). Any exceptions to, or
deletions from, the ASTM E 1527-13 standard of practice are described in the
INTRODUCIYON section of the report. Based upon our findings, this assessment has revealed
no evidence of recognized environmental conditions in association with the subject property
with the exception of the following:
1) Two (2) underground storage tanks (USTs) used to store heating oil were observed on
the subject property: UST-1 adjacent to the single-family dwelling and UST-2 adjacent
to the existing church. In an attempt to determine whether releases have occurred
from these USTs, Geoscience advanced a total of four (4) band auger borings HA-1
through HA-4) adjacent to the ends of the tanks. Soil samples collected frorn the
borings were analyzed for total petroleum hydrocarbons in the gasoline and diesel fuel
ranges (TPH-GRO and TPH-DRO).
Neither TPH-GRO nor TPH-DRO were detected in the samples (HA-1 and HA-2)
collected adjacent to UST-1. As such, it does not appear that releases have occurred
from that tank. However, the soil samples collected adjacent to UST-2 (HA-3 and
HA-4) exhibited TPH-GRO and TPH-DRO concentrations exceeding Action Limits
established. by NCDEQ (see Table 1 in Appendix 1). Based on the sample results, it is
apparent a heating oil release has occurred from UST-2. Therefore, UST-2 is
considered to be a recognized environmental condition in association with the subject
property.
Forest Hill Church
Consulting Enginms
Geoscience Project No. CHI 8.0129.GE
December 13, 2018
Page 13
Much of the information provided in this summary report is based upon personal interviews
and review of available documents, records, and maps held by the appropriate govenunent
GE9SCIENCE and private agencies. This summary is subject to the limitations of historical
GROUP documentation, availability and accuracy of pertinent records and the personal recollection
of those persons contacted.
RELIANCE
This report is intended for the sole use of Forest Hill Church, and its lending institution for
this project. This report should not be relied upon by any other parties without the express
written consent of Geoscience Group, Inc.
QUALIFICATIONS
This report was prepared by the undersigned environmental professionals whose
qualifications are included in Appendix V11 of this report. We declare that, to the best of
our professional knowledge and belief, we meet the definition of Environmental
Professional as defined in §312.10 of 40 CFR§ 312. We have the specific qualifications
based on education, training, and experience to assess a property of the nature, history, and
setting of the subject property. We have developed and performed the all appropriate
inquiries in conformance with the standards and practices set forth in 40 CFR Part 312.
Geoscience appreciates the opportunity to be of service to you on this project. If you have any
questions regarding this report or require additional information, please contact us.
Respectfully,
GEOSCIENCE GROUP, INC.
Ashley N. Proctor
Assistant Project Manager
Thomas C. Hassett, P.E.
Senior Engineer
Enclosures
EW 201,Y129 — kr= HUU C3meb Parcels ESA_dm
APPENDIX I
Maps and Sketches:
Figure No. CHI 8.129-1 - Vicinity Map
Figure No. CHI 8.129-2 - Tax Line Map
Figure No. CHI 8,129-3 - Site Layout
Figure No. CH 18.129-4 — Sample Location Diagram
Figure No. CHI8.129-4 - 2015 County Topographic Map
Figure No. CHI 8.129-5— 1967 (Photorevised 1988) USGS Topographic Map
Table 1: Summary of Soil Sampling Results
GEOSCIENCE GROUP, INC. J
CHARLOTTE, NORTH CAROLINA I
SCALE: ]";� 210m, APPROVED BY: DRAWN BY ADC
DATE; Octobci 3, 2018 1<w REVISED: ANP
FOREST HILL CHURCH PARCELS I
CHARLOTTE, NORTH CAROLINA
VICINITY MAP
RGURL NUMBER:
CH18.129-1
o ,
3ti �'tsaoart� � %
06830RT14 �
/083087
12��
.(, o
�534411A ,� titi%68
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jos
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ti
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I GEOSCIENCE GROUP, INC:
CHARLOTTE, NORTH CAROLINA
SCALE: V � 123' APPROVED BY: DRAWN BY. Mecklenburg Co.
4i� I
DATE: October 3, 2018 REVISED: ANP
FOREST HILL CHURCH PARCELS
CHARLOTTE, NORTH CAROLINA
TAX LINE MAP
E NUMBER:
CH18.129-2
€t Sj( itial
ehaitorrc
Charlotte
S�
�.
isirlFtifxifl
{{
`�.
�
ti
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ct,srtotte
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Residential
. p
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.
Condominiums
irnis� /
y rio XdLSiflE'nt.ial
r: Itesic]entit .,_�
/fha joy e
-1 a,
LEGEND:
approximate Location of
SaFnpEes
Uudaground Storage
Tank
lk
s
4
GEOSCIENCE GROUP, INC.
CHARLOTTE, NORTH CAROLINA
SCALE-- 1" 25' ,APPROVED BY: DRAWN BY; Mecklenburg Co.
DATE! October 18, 2018 REVISED: ANP
I FOREST HILL CHURCH PARCELS I
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION DIAGRAM
E NUMBER:
CH18.129-4
• 4 •� tt
9
K'
C11
r �
r � '
e
SITE
5�i � • r
• • a,
p •.fix e
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r
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s
GEGSCIENCE GROUP, INC.
CHARLOTTE, NORTH CAROLINA
SCALE: 1" 95' APPRQVFT) BY: BRAWN BY: Mecklenburg Co.
�aN
DATE: October 3, 20IS I �c I REVISED; ANP
FOREST HILL CHURCH PARCELS
CHARLOTTE, NORTH CAROLINA
FIGURE IVLIIVIBER:
2015 COUNTY TOPOGRAPHIC MAP CH1BER: 5
6-
ThQ
GEOSCIENCE GROUP, INC.
CHARLOTTE, NORTH CAROLINA
SCALE: V z 2,000' JAPPROVED BY: , A / DRAWN BY: USGS
TE: October 3, 2018
FOREST HILL CHURCH PARCELS
CHARLOTTE, NORTH CAROLINA
1967 USG5 TOPOGRAPHIC MAP
(PHOTOREVISED 1988)
ANP
E NUMBER-
CH18.129-6
Table 1: Summary of Soil Sampling Results
Revision 10/2612018 Project: Forest Hill Church Parcels Project No, CH18.0129.GE
Date:
Analytical Method
TPH (mg/kg)
Contaminant of Concern
❑
0
Sample
Location
Sample
depth (ft)
Date
Collected
I.
HA-1
7.5
10/512018
E9.9
{ 7.5
HA-2
8
10/512018
<9.9
<7.5
HA-3
$
10/12/2018
26,000
2,300
HA-4
10
10/1212018
3,500
99
North Carolina Action limits for Total
Petroleum Hydrocarbons (TPH)
100
50
APPENDIX II
Site Photographs 1 through 19
1) Forest Hill Church located on the on the southern portion of the subject site.
3) The existing house located on the southern -central portion of the site.
site.
4) Shed located on the northern -central portion of the subject
property.
5) Shed located on the eastern portion of the subject site.
6) Portable restrooms located on the eastern portion of the site.
7) Shed located on the eastern portion of the site.
8) The northern portion of the subject site as seen facing southeast from North Alexander Street.
9) The subject site as seen facing southwest from the eastern property boundary.
10) The southern portion of the subject site as seen facing northwest from North McDowell Street.
11) The western portion of the site as seen facing northeast from East 36`" Street.
12) Vent and fill pipe for an underground storage tank (UST) observed
adjacent to the house on the southern -central portion of the site.
14) Drum observed on the eastern portion of the subject site.
13) Vent and fill pipe for a UST observed adjacent to the
church on the southern portion of the subject property.
15) Bulk totes observed on the eastern portion of the subject site.
I Lin,
'. x,i�,yr' •S �r•�:1+�i}r_ _•�'yy�.,•:'ni�.' l ��*
M
APPENDIX III
Historical Research Documentation:
EDR Aerial Photo Decade Package
Certified Sanborn Map Report
EDR City Directory Abstract
EDR Historical Topo Map Report
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
Inquiry Number: 5441860.8
October 03, 2018
6 Armstrong Road, 4th floor
Shelton, CT 06484
(rEDR� Toll Free: 800.352.0050
www.edrnet.com
EDR Aerial Photo Decade Package 10/03/18 I
Site Name:
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
EDR Inquiry # 5441860.8
Client Name:
Geoscience Group
500 Clanton Road
Charlotte, NC 28217
Contact: Ashley Proctor
2ra
Environmental Data Resources, Inc. (EDR) Aerial Photo Decade Package is a screening tool designed to assist
environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR's
professional researchers provide digitally reproduced historical aerial photographs, and when available, provide one photo
perdecade.
Search Results:
Year
Scale
Details
Source
2016
1 "=500'
Flight Year: 2016
USDA/NAIP
2012
1 "=500'
Flight Year: 2012
USDA/NAIP
2009
1 "=500'
Flight Year: 2009
USDA/NAIP
2006
1 "=500'
Flight Year: 2006
USDA/NAIP
1996
1 "=500'
Flight Date: April 25, 1996
NCDOT
1993
1 "=500'
Acquisition Date: January 28, 1993
USGS/DOQQ
1988
1 "=500'
Flight Date: October 12, 1988
USDA
1983
1 "=500'
Flight Date: March 03, 1983
USGS
1976
1 "=500'
Flight Date: March 01, 1976
USGS
1971
1 "=500'
Flight Date: March 18, 1971
USGS
1968
1 "=500'
Flight Date: February 25, 1968
USDA
1965
1 "=500'
Flight Date: February 22, 1965
USGS
1956
1 "=500'
Flight Date: March 31, 1956
USDA
1948
1 "=500'
Flight Date: May 15, 1948
USGS
When delivered electronically by EDR, the aerial photo images included with this report are for ONE TIME USE
ONLY. Further reproduction of these aerial photo images is prohibited without permission from EDR. For more
information contact your EDR Account Executive.
Disclaimer - Copyright and Trademark Notice
This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot
be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY
EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY
DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE
OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE,
WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING,
WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL
DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any
analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to
provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I
Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property.
Additionally, the information provided in this Report is not to be construed as legal advice.
Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of
Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.
EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are
the property of their respective owners.
5441860 - 8 page 2
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Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
Inquiry Number: 5441860.3
October 02, 2018
6 Armstrong Road, 4th floor
(rEDR� Shelton, CT 06484
Toll Free: 800.352.0050
www.edrnet.com
Certified Sanborn® Map Report 10/02/18
Site Name:
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
EDR Inquiry # 5441860.3
Client Name:
Geoscience Group
500 Clanton Road
Charlotte, NC 28217
Contact: Ashley Proctor
The Sanborn Library has been searched by EDR and maps covering the target property location as provided by Geoscience Group were
identified for the years listed below. The Sanborn Library is the largest, most complete collection of fire insurance maps. The collection
includes maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow, and others. Only Environmental Data Resources Inc. (EDR) is
authorized to grant rights for commercial reproduction of maps by the Sanborn Library LLC, the copyright holder for the collection. Results
can be authenticated by visiting www.edrnet.com/sanborn.
The Sanborn Library is continually enhanced with newly identified map archives. This report accesses all maps in the collection as of the
day this report was generated.
Certified Sanborn Results:
Certification # 9006-4D7E-8BD7
Po #
Project
Maps Provided:
1963
1962
1958
1953
1950
1929
1911
NA
Forest Hill Church Parcels
Limited Permission To Make Copies
Sanborn® Library search results
Certification #: 9006-4D7E-8BD7
The Sanborn Library includes more than 1.2 million
fire insurance maps from Sanborn, Bromley, Perris &
Browne, Hopkins, Barlow and others which track
historical property usage in approximately 12,000
American cities and towns. Collections searched:
f Library of Congress
f University Publications of America
f EDR Private Collection
The Sanborn Library LLC Since 1866T"
Geoscience Group (the client) is permitted to make up to FIVE photocopies of this Sanborn Map transmittal and each fire insurance map accompanying this report
solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made directly to an EDR Account Executive, the
client may be permitted to make a limited number of additional photocopies. This permission is conditioned upon compliance by the client, its customer and their
agents with EDR's copyright policy; a copy of which is available upon request.
Disclaimer - Copyright and Trademark Notice
This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot
be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY
EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY
DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE
OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE,
WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING,
WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL
DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any
analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to
provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I
Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property.
Additionally, the information provided in this Report is not to be construed as leqal advice.
Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of
Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.
EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein
are the property of their respective owners.
5441860 - 3 page 2
Sanborn Sheet Key
This Certified Sanborn Map Report is based upon the following Sanborn
Fire Insurance map sheets.
1963 Source Sheets
Volume 2, Sheet 257 Volume 2, Sheet
1963 1963
1962 Source Sheets
Volume 2, Sheet 257 Volume 2, Sheet
1962 1962
1958 Source Sheets
Volume 2, Sheet 257 Volume 2, Sheet
1958 1958
1953 Source Sheets
Volume 2, Sheet 259 Volume 2, Shee
1953 1953
5441860 - 3 page 3
Sanborn Sheet Key
This Certified Sanborn Map Report is based upon the following Sanborn
Fire Insurance map sheets.
1950 Source Sheets
Volume 2, Sheet 259
1950
1929 Source Sheets
Volume 2, Sheet 259
1929
1911 Source Sheets
Volume 1, Sheet 91
1911
5441860 - 3
page 4
CEDW Certified Sanborn® Map 1963
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Site Name: Forest Hill Church Parcels �]
Address: 729E 36TH ST
City, ZIP: CHARLOTTE, 28205
Client:
Geoscience Group
EDR Inquiry: 5441860.3
Order Dale: 10/02/2018
CertWcation! 9006-4D7E-8BD7
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
1 Volume 2, Sheet 259
e 6 Volume 2, Sheet 257
257
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Site Name: Forest Hill Church Parcels `
Address: 729 E 36TH ST,
City, ST, ZIP: CHARLOTTE, INC 28205 ��. �• 9
Client: Geoscie—Group
EDR Inquiry: 5441860.3
Order Dale: 1018 w
Certification t 9006-4D063D7E-BBD7
8
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
Volume 2, Sheet 259
V01ume 2, Sheet 257
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0 Feet 150 300 600
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5441860 - 3 page 6
EDR°
Certified Sanborn® Map
1958
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Site Name: Forest Hill Church Parcels
Address: 729 E 36TH ST
City, ST, ZIP: CHARLOTTE, INC 28205
Client: Geoscie—Group
EDR Inquiry: 5441860.3
Order Dale: 10/02/2018 �p/
Certification E 9006-4D7E-8BD7 -
956
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
Volume 2, Sheet 259
Volume 2, Sheet 257
257
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5441860 - 3 page 7
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Site Name. Forest HIII Church Parcels r � n
Address: 729 E 36TH ST�Ji� /{�\
City, ST, ZIP: CHARLOTTE, NC 28205
Client: Ge—ie—Group
EDR Inquiry5441860.3
Ord,, Date: 10/02/2018 71 ti
Certification t 90064NE-BBD7
l
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
Volume 2, Sheet 257
'- Volume 2, Sheet 259
257
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1953
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5441860 - 3 page 8
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Site Name: Forest Hill Church Parcels
Address: 729 E 36TH ST
City, ST, ZIP: CHARLOTTE, INC 28205
Client: Geoscience Group
EDR Inquiry: 5441860.3
Order Dale: 10/02/2018
Certification E 9006-4D7E-8BD7
1
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
Volume 2, Sheet 259
p � 0II 4 a
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5441860 - 3 page 9
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Site Name: Forest Hill Church Parcels `
P
Address 729 E 36TH ST \ 1 l • @-
City, ST, ZIP: CHARLOTTE, INC 28205
•Y CA
Client: Geoscience Group '.}'-''0
EDR Inquiry: 5441860.3
Order Dale: 10/02/2018
Certification E 9006-4D7E-8BD7
C—riaht 1929 M SR f �t ,�, Y•
This Certified Sanborn Map combines the following sheets.
Outlined areas indicate map sheets within the collection.
v.. Volume 2, Sheet 259
16
® A e
! 4 A 259
✓' o-
0 Feet 150 300 600
I
-N•
5441860 - 3 page 10
(CEDR'
Certified Sanborn® Map
'k,
2,
A
IV
Site Name: Forest Hill Church Parcels
Add— 729 E 36TH ST
City, ST, ZIP: CHARLOTTE, INC 28205
Client: Geowie— Group
EDIR Inquiry 5441860.3
This Certified Sanborn Map combines the following sheets
Outlined areas indicate map sheets within the collection.
Volume 1, Sheet 91
I i I I
0 Feet 150 300 600
5441860 - 3 page 11
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
Inquiry Number: 5441860.4
October 02, 2018
6 Armstrong Road, 4th floor
(rEDR� Shelton, CT 06484
Toll Free: 800.352.0050
www.edrnet.com
EDR Historical Topo Map Report
10/02/18
Site Name:
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
EDR Inquiry # 5441860.4
Client Name:
Geoscience Group
500 Clanton Road
Charlotte, NC 28217
Contact: Ashley Proctor
CEDW
EDR Topographic Map Library has been searched by EDR and maps covering the target property location as provided by
Geoscience Group were identified for the years listed below. EDR's Historical Topo Map Report is designed to assist
professionals in evaluating potential liability on a target property resulting from past activities. EDRs Historical Topo Map
Report includes a search of a collection of public and private color historical topographic maps, dating back to the late
1800s.
Search Results: Coordinates:
P.O.# NA Latitude: 35.246331 35' 14' 47" North
Project: Forest Hill Church Parcels Longitude:-80.802412 -80° 48' 9" West
UTM Zone: Zone 17 North
UTM X Meters: 517976.04
UTM Y Meters: 3900378.68
Elevation: 729.66' above sea level
Maps Provided:
2013 1907
1996 1905
1988
1980
1967,1972
1949
1948
1942
Disclaimer - Copyright and Trademark Notice
This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot
be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY
EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY
DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE
OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE,
WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING,
WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL
DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any
analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to
provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I
Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property.
Additionally, the information provided in this Report is not to be construed as legal advice.
Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of
Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.
EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein
are the property of their respective owners.
5441860 - 4 page 2
Topo Sheet Key
This EDR Topo Map Report is based upon the following USGS topographic map sheets.
2013 Source Sheets
Charlotte East Derita
2013 2013
7.5-minute, 24000 7.5-minute, 24000
1996 Source Sheets
Derita
1996
7.5-minute, 24000
Aerial Photo Revised 1993
1988 Source Sheets
Charlotte East
1988
7.5-minute, 24000
Aerial Photo Revised 1984
1980 Source Sheets
Charlotte East
1980
7.5-minute, 24000
Aerial Photo Revised 1976
5441860 - 4 page 3
Topo Sheet Key
This EDR Topo Map Report is based upon the following USGS topographic map sheets.
1967, 1972 Source Sheets
Charlotte East
1967
7.5-minute, 24000
Aerial Photo Revised 1965
1949 Source Sheets
Charlotte East
1949
7.5-minute, 24000
Aerial Photo Revised 1948
1948 Source Sheets
Charlotte East
1948
7.5-minute, 24000
Aerial Photo Revised 1948
1942 Source Sheets
CHARLOTTE
1942
30-minute, 125000
Derita
1972
7.5-minute, 24000
Aerial Photo Revised 1971
Derita
1948
7.5-minute, 24000
Aerial Photo Revised 1948
5441860 - 4 page 4
Topo Sheet Key
This EDR Topo Map Report is based upon the following USGS topographic map sheets.
1907 Source Sheets
r
Charlotte
1907
15-minute, 62500
1905 Source Sheets
Charlotte
1905
15-minute, 48000
5441860 - 4 page 5
(eEDW Historical Topo Map 201;
SugarV Of
Creek ii airta
3 x. Wood
.CjrOOERELtARR.` �0
{� a }
110,
R458URY AVE
ASBURYAVE I.,'' o GLVRYST;
_ ---...- _..... -LIB.
29
ills ,— Junction
z Sugar Greek y
} efl Burying Ground qg j
c• 1 Ir` `
CA
o g h
RAL�rGN ST.29
RQ
REDWOOD AVE- OWEN
2aT ` _ ti 4 m LARO. SY p� a ,y pR£
s�
ewood _ 4 ff _ 4� �yF Ea:t no oair c
h•4�F drT _ ,? \. .. h.CH. s ' Sr., `\ ° ''I ' •yEE'r, 9 Ake �.. ❑
5 s -
yA��
iR4j - LAW' WpQ . Lf7GH AVf 54fJp
Ayf-
!• ``�a �y��a � �� ��y��"sj,� ETrERf T'f ��'• � ����{ I �r� i i � � �sTyST ��C, 1�',, -_- _ ��� � !
Y
Rp 5l i��gA4�L .. - ;� - -•: p4�A�
o H
�r BEI.MI]1VT : �- G _ .e.� -_ Ai4bARD o
'rI, � �a �'AViN
ARLQTT w - Ar;_
R �. MECKLENBURG AVE
o� 2 0 a .
�
s� N w4�P � ���y4.;• �p�'. I ,, ti r .�. - �`:��F. .f I--.� — _ _(„ @Fyr��,r� �
s� q Midwood -R -
4. '
� V N
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 2013, 7.5-minute
N, Derita, 2013, 7.5-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N
5441860 - 4 page 6
CEDW Historical Topo Map gc
f
' Y
Druid
�• J� g S i k kCh04
7,
�.1F$
�o
• T7 rr --ty �
ill � ~ �I '4 •/ $'1 ��i
This report includes information from the
following map sheet(s).
NW N NE
N, Derita, 1996, 7.5-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N
5441860 - 4 page 7
CEDW Historical Topo Map ggE
�z.. � H.,•�i n k ti ,.fir,.
- I'► p
r.i., ,AW
lx f�
J i
a.
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 1988, 7.5-minute
t t�
• �• y i � � .Il LyJ'. ., e'�
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 11
N
5441860 - 4 page 8
CEDW Historical Topo Map gg
t• j r
r� � g I � � ..A. � I•I l,ia
If
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 1980, 7.5-minute
Go�
OV�S
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N
5441860 - 4 page 9
CEDW Historical Topo Map 1967. 19
f � L
A A �J ■ 1 P r�O�
� e
ndv Juno ` o . �7J,• �� G _ N
urnlrxaek
is W
•ce t yyt TM
5❑ f� I jGS
urse
• % ;y �' ram. d L _ � +�,���• ��- ' Wit
a�Fo.Trn+ : ✓ :'a) ! land
AM, .os7d harlRf� J,
,,per r ¢vuntry ukr �y
. rH 4
i`. .lr n tiihJ
'u f'EN
d Hi¢h
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 1967, 7.5-minute
N, Derita, 1972, 7.5-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 11
lN•
5441860 - 4 page 10
CEDW Historical Topo Map 194�
Sn •
46� ''s• GFeaLwGGd
Tow
it
OVA �r 1 •
• Q �
f�
r + i`J rF
I t it
1 �I+ • • • • IL--__ �- it
.F, jr
�j •'► • Ala I�r L��i 1
'. • r • C ario#te u
'��Vou Clubpiedm
ram"` d • ° "� "•� ds
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 1949, 7.5-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N
5441860 - 4 page 11
CEDW Historical Topo Map 194E
• b m
ter Grove r • �' �� ti c -
.
,AtandB ��� ii u • `@@h• ° ��o - �.
June
t �': , • 4�=tea Y r• JI
.r • . :y. f ''� Sugar Creek o I
Ch
&� Jh y•• 1° ����,� �� o¢therd States
��� g4 ��S•� 'r `;;'.- _�Fairgrbunds I'
Ire
Jf�• `� +' ��5» +i + ,. , ..`_ � der°'•,,
to
!�•• • � • .IYNF.•�N = `l•�`•'- � c� 1�•`'J�' of -
Ba J.t £�R •"r � l�l � Eastwood
e Tcwerr =
i ] a �s �7��1 �'++ ♦ � � � o'er y*`��•� ' ...
WWI-
� l` ••AN
r
1E{tfl7Jr h
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte East, 1948, 7.5-minute
N, Derita, 1948, 7.5-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N•
5441860 - 4 page 12
s
•
Ojef ■iof: le
t
A
goes
ILI
CEDW Historical Topo Map 190
t•�— �-
f "�
�0A
0 •
f. r�
c 4 Ole « * +
If
rI L _ Uri
r, 4
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte, 1907, 15-minute
E1
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N
5441860 - 4 page 14
CEDR' Historical Topo Map g(
• - I � y� J r
v! •
This report includes information from the
following map sheet(s).
NW N NE
TP, Charlotte, 1905, 15-minute
0 Miles 0.25 0.5 1 1.5
SITE NAME: Forest Hill Church Parcels
ADDRESS: 729 E 36TH ST
CHARLOTTE, NC 28205
CLIENT: Geoscience Group 1
N�
5441860 - 4 page 15
APPENDIX IV
Regulatory Records Documentation:
EDR Radius Map Report
Forest Hill Church Parcels
729 E 36TH ST
CHARLOTTE, NC 28205
Inquiry Number: 5441860.2s
October 02, 2018
6 Armstrong Road, 4th floor
Shelton, CT 06484
,fc Toll Free: 800.352.0050
rEDR' www.edrnet.com
FORM-LBC-CCA
TABLE OF CONTENTS
SECTION
PAGE
Executive Summary
ES1
OverviewMap-----------------------------------------------------------
2
DetailMap--------------------------------------------------------------
3
Map Findings Summary
4
MapFindings------------------------------------------------------------
8
Orphan Summary---------------------------------------------------------
452
Government Records Searched/Data Currency Tracking- - - - - - - - - - - - - -
- - - - - - - - - - - - GR-1
GEOCHECK ADDENDUM
Physical Setting Source Addendum
A-1
Physical Setting Source Summary
A-2
Physical Setting SSURGO Soil Map -------------------------------------------
A-6
Physical Setting Source Map------------------------------------------------
A-13
Physical Setting Source Map Findings
A-15
Physical Setting Source Records Searched
PSGRA
Thank you for your business.
Please contact EDR at 1-800-352-0050
with any questions or comments.
Disclaimer - Copyright and Trademark Notice
This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data
Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from
other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL
DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION,
MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL
ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE,
ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL,
CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY
LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings,
environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor
should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I
Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any
property. Additionally, the information provided in this Report is not to be construed as legal advice.
Copyright 2018 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole
or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.
EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other
trademarks used herein are the property of their respective owners.
TC5441860.2s Page 1
EXECUTIVE SUMMARY
A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR).
The report was designed to assist parties seeking to meet the search requirements of EPA's Standards
and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for
Environmental Site Assessments (E 1527-13), the ASTM Standard Practice for Environmental Site
Assessments for Forestland or Rural Property (E 2247-16), the ASTM Standard Practice for Limited
Environmental Due Diligence: Transaction Screen Process (E 1528-14) or custom requirements developed
for the evaluation of environmental risk associated with a parcel of real estate.
TARGET PROPERTY INFORMATION
ADDRESS
729 E 36TH ST
CHARLOTTE, NC 28205
COORDINATES
Latitude (North):
Longitude (West):
Universal Tranverse Mercator:
UTM X (Meters):
UTM Y (Meters):
Elevation:
35.2463310 - 35' 14' 46.79"
80.8024120 - 80° 48' 8.68"
Zone 17
517976.5
3900180.5
730 ft. above sea level
USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY
Target Property Map:
Version Date:
North Map:
Version Date:
AERIAL PHOTOGRAPHY IN THIS REPORT
5948285 CHARLOTTE EAST, NC
2013
5948299 DERITA, NC
2013
Portions of Photo from: 20140524, 20140603
Source: USDA
TC5441860.2s EXECUTIVE SUMMARY 1
MAPPED SITES SUMMARY
Target Property Address:
729 E 36TH ST
CHARLOTTE, NC 28205
Click on Map ID to see full detail.
MAP
ID SITE NAME ADDRESS
Reg
SAFETY KLEEN CORP
Reg
GENERAL LATEX & CHEM
Reg
ICI - AMERICAS INC
Reg
DETREX CHEMICAL INDU
Reg
HENKEL CORP.
Al
COLUMBUS OIL CO (BRS
516 E 36TH
A2
NORTH CHARLOTTE SERV
516 EAST 36TH STREET
A3
NORTH CHARLOTTE LAUN
3306B N DAVIDSON ST
4
JOHNSTON MILL APARTM
3315 NORTH DAVIDSON
A5
NORTH HIGHLANDER CEN
3220 N DAVIDSON
A6
CHARLOTTE MOTOR CO
500 E 36TH
A7
FIRE STATION 7
3210 N DAVIDSON ST
A8
BILLS SERVICE GROC
3307 N DAVIDSON ST
B9
BIO ECOLOGICAL SERVI
720 HERRIN AVE
B10
BIO ECOLOGICAL SERVI
720 HERRIN AVENUE
C11
VESPOINT PROPERTY
3112 NORTH DAVIDSON
C12
FAT CITY SITE
3123 NORTH DAVIDSON
13
SINCLAIR REFINING CO
409 E. 35TH ST. AND
14
NEW LIFE THEOLOGICAL
3117 WHITING AVENUE
15
NODA TEXTILE
430 E. 36TH STREET
16
STEEL GARDENS
3445 SPENCER STREET
17
PAUL MCBROOM RESIDEN
3000 NORTH DAVIDSON
D18
L & N TIRE SERVICE
300 E 36TH STREET
D19
L & N TIRE SERVICE
300 EAST 36TH STREET
E20
HIGHLAND MILLS PARK
2901 N DAVIDSON STRE
E21
HIGHLAND MILLS
2901 NORTH DAVIDSON
22
INX (FORMER) FACILIT
3200 & 3210 CULLMAN
D23
L & N TIRE CO.
240 E. 36TH ST.
F24
TRANSMISSION SUPPLY
624 ANDERSON STREET
F25
TRANSMISSION SUPPLY
642 ANDERSON STREET
G26
ABERNATHY LUMBER COM
308 EAST CRAIGHEAD R
G27
ABERNATHY LUMBER COM
308 E. CRAIGHEAD ROA
G28
CRAIGHEAD RD.
308 E. CRAIGHEAD RD;
29
VIRGINIA MOORE TRUST
3404 RITCH AVENUE
H30
TREX PROPERTIES SITE
3114 CULLMAN AVENUE
H31
DETREX CHEMICAL INDU
3114 CULLMAN
132
YUASA-EXIDE DISTRIBU
3713 N. DAVIDSON ST.
J33
QUICK SHOPPE # 9
3435 THE PLAZA
J34
QUIK SHOPPE 9
3435 THE PLAZA
DATABASE ACRONYMS
RELATIVE
ELEVATION
NC HSDS
Same
NC HSDS
Same
NC HSDS
Same
NC HSDS
Same
NC HSDS
Same
EDR Hist Auto
Lower
NC LUST, NC UST, NC IMD
Lower
EDR Hist Cleaner
Lower
NC LUST, NC IMD
Lower
EDR Hist Cleaner
Lower
EDR Hist Auto
Lower
NC UST
Higher
EDR Hist Auto
Lower
RCRA NonGen / NLR
Higher
NC SWF/LF, NC HIST LF
Higher
NC LUST, NC LUST TRUST
Lower
NC LUST, NC LUST TRUST
Lower
NC BROWNFIELDS
Lower
NC LUST, NC LUST TRUST
Higher
NC BROWNFIELDS
Higher
NC LUST
Higher
NC LAST
Lower
NC IMD
Lower
NC LUST
Lower
NC LUST, NC BROWNFIELDS, NC IMD
Lower
NC IMD
Lower
NC SHWS
Lower
NC LUST, NC UST, NC IMD
Lower
NC IMD
Higher
NC LUST
Higher
NC LUST
Lower
NC UST, NC IMD
Lower
NC BROWNFIELDS
Lower
NC LUST
Lower
SEMS
Lower
SEMS-ARCHIVE, CORRACTS, RCRA-TSDF, RCRA-LQG, NC ...
Lower
NC SHWS
Higher
NC IMD
Higher
NC LUST, NC LUST TRUST, NC UST
Higher
DIST (ft. & mi.)
DIRECTION
3151, 0.597, SW
3623, 0.686, WSW
4868, 0.922, West
1798, 0.341, WNW
3022, 0.572, NE
554, 0.105, NW
554, 0.105, NW
556, 0.105, NW
590, 0.112, NNW
593, 0.112, WNW
601, 0.114, NW
622, 0.118, WNW
631, 0.120, NW
692, 0.131, ENE
692, 0.131, ENE
869, 0.165, West
928, 0.176, WNW
988, 0.187, WNW
1093, 0.207, South
1134, 0.215, NW
1195, 0.226, East
1577, 0.299, WSW
1594, 0.302, NW
1594, 0.302, NW
1805, 0.342, West
1805, 0.342, West
1807, 0.342, NW
1846, 0.350, NW
1933, 0.366, ENE
1960, 0.371, ENE
2098, 0.397, NNE
2098, 0.397, NNE
2098, 0.397, NNE
2191, 0.415, NNW
2215, 0.420, WNW
2215, 0.420, WNW
2254, 0.427, NE
2264, 0.429, ESE
2264, 0.429, ESE
5441860.2s Page 2
MAPPED SITES SUMMARY
Target Property Address:
729 E 36TH ST
CHARLOTTE, NC 28205
Click on Map ID to see full detail.
MAP
ID SITE NAME
ADDRESS
RELATIVE
DATABASE ACRONYMS ELEVATION
DIST (ft. & mi.)
DIRECTION
35
PHILEMON AVE SITE
E CRAIGHEAD RD & PHI
NC SHWS
Lower
2305, 0.437, NNE
K36
EXPRESS #525(E-Z SER
3400 THE PLAZA
NC LUST TRUST
Higher
2406, 0.456, SE
K37
SAMS MART 26
3400 THE PLAZA
NC LUST, NC UST, NC Financial Assurance
Higher
2406, 0.456, SE
K38
E-Z SERVE #525
3400 THE PLAZA
NC IMD
Higher
2406, 0.456, SE
139
COX, BORDERS, SHAVER
3725 N DAVIDSON STRE
NC LUST, NC IMD
Higher
2426, 0.459, ENE
L40
PET DAIRY
3300 THE PLAZA
NC LUST TRUST, NC IMD
Higher
2437, 0.462, SE
L41
PET DAIRY
3300 THE PLAZA
NC LUST, NC UST
Higher
2437, 0.462, SE
M42
AMOCO #1106-GORDIES
3129 THE PLAZA
NC IMD
Higher
2438, 0.462, SSE
M43
GORDIES AMOCO
3129 THE PLAZA
NC LUST, NC UST
Higher
2438, 0.462, SSE
44
CAROLINA CONSOLIDATO
400 E 33RD STREET
NC SHWS, NC LUST, NC UST, NC IMD
Lower
2519, 0.477, West
M45
C MART 442
3109 THE PLAZA
NC LUST, NC UST
Higher
2519, 0.477, SSE
M46
COASTAL MART #442
3109 THE PLAZA
NC IMD
Higher
2519, 0.477, SSE
47
SOUTHERN RESOURCES,
3826 RALEIGH ST.
NC SWRCY
Lower
2576, 0.488, NNE
48
AMBROSIA HOOTEN CHOC
3746 NORTH DAVIDSON
NC LUST, NC IMD
Higher
2615, 0.495, ENE
49
TARMAC VIRGINIA, INC
3934 RALEIGH STREET
NC LUST, NC IMD
Lower
2628, 0.498, NE
50
CHADBOURN GOTHAM, IN
JORDAN PL & DAVIDSON
NC SHWS
Lower
2953, 0.559, WSW
51
MELATEX INC (FORMER
3818 NORTHMORE ST
NC SHWS
Higher
3009, 0.570, ENE
52
WISE RECYCLING - CHA
600 E. SUGAR CREEK R
NC SHWS, NC SWRCY
Higher
3249, 0.615, NE
53
GENUINE PARTS COMPAN
124 ATANDO AVENUE
NC SHWS, NC VCP
Lower
3330, 0.631, NW
54
KAISER FLUID TECHNOL
530 SUGAR CREEK RD E
NC SHWS, NC BROWNFIELDS, NC IMD, RCRA NonGen /...
Lower
3723, 0.705, NE
N55
GENERAL LATEX & CHEM
2321 N. DAVIDSON ST
NC SHWS
Lower
3738, 0.708, WSW
N56
RH BOULIGNY INC.
2320 NORTH DAVIDSON
NC SHWS, NC LUST, NC LAST, NC IMD
Lower
3762, 0.712, WSW
57
SAFETY KLEEN CORP
20 YADKIN AVE (2320)
SEMS-ARCHIVE, CORRACTS, RCRA-TSDF, RCRA-LQG, US ...
Lower
3795, 0.719, SW
058
GIBBS ELECTROPLATING
2229 N DAVIDSON
NC SHWS, NC IMD
Lower
4144, 0.785, WSW
59
NCDOT DIV 10 FACILIT
1119 E SUGAR CREEK R
NC SHWS, NC LAST, NC IMD
Higher
4197, 0.795, East
060
APPLIED RESEARCH GRO
2221 N. DAVIDSON STR
NC SHWS
Lower
4228, 0.801, WSW
61
DIXON QUICK COUPLING
332 ATANDO AVE
NC SHWS, NC LAST, NC BROWNFIELDS, NC IMD, RCRA...
Lower
4369, 0.827, NW
62
OMNISOURCE SE/ATLANT
410 ATANDO AVE
NC SHWS
Lower
4806, 0.910, NW
5441860.2s Page 3
EXECUTIVE SUMMARY
TARGET PROPERTY SEARCH RESULTS
The target property was not listed in any of the databases searched by EDR.
DATABASES WITH NO MAPPED SITES
No mapped sites were found in EDR's search of available ("reasonably ascertainable ") government
records either on the target property or within the search radius around the target property for the
following databases:
STANDARD ENVIRONMENTAL RECORDS
Federal NPL site list
NPL National Priority List
Proposed NPL---------------- Proposed National Priority List Sites
NPL LIENS Federal Superfund Liens
Federal Delisted NPL site list
Delisted NPL National Priority List Deletions
Federal CERCLIS list
FEDERAL FACILITY---------. Federal Facility Site Information listing
Federal RCRA generators list
RCRA-SQG RCRA - Small Quantity Generators
RCRA-CESQG RCRA - Conditionally Exempt Small Quantity Generator
Federal institutional controls / engineering controls registries
LUCIS------------------------ Land Use Control Information System
US ENG CONTROLS Engineering Controls Sites List
US INST CONTROL Sites with Institutional Controls
Federal ERNS list
ERNS------------------------ Emergency Response Notification System
State and tribal landfill and/or solid waste disposal site lists
NC OLI Old Landfill Inventory
State and tribal leaking storage tank lists
INDIAN LUST Leaking Underground Storage Tanks on Indian Land
State and tribal registered storage tank lists
FEMA UST------------------- Underground Storage Tank Listing
TC5441860.2s EXECUTIVE SUMMARY 4
EXECUTIVE SUMMARY
NC AST______________________ AST Database
INDIAN UST Underground Storage Tanks on Indian Land
State and tribal institutional control / engineering control registries
NC INST CONTROL No Further Action Sites With Land Use Restrictions Monitoring
State and tribal voluntary cleanup sites
INDIAN VCP------------------ Voluntary Cleanup Priority Listing
ADDITIONAL ENVIRONMENTAL RECORDS
Local Brownfield lists
US BROWNFIELDS A Listing of Brownfields Sites
Local Lists of Landfill / Solid Waste Disposal Sites
INDIAN ODI Report on the Status of Open Dumps on Indian Lands
DEBRIS REGION 9----------- Torres Martinez Reservation Illegal Dump Site Locations
ODI Open Dump Inventory
IHS OPEN DUMPS Open Dumps on Indian Land
Local Lists of Hazardous waste / Contaminated Sites
US HIST CDL---------------- Delisted National Clandestine Laboratory Register
US CDL National Clandestine Laboratory Register
Local Land Records
LIENS 2 CERCLA Lien Information
Records of Emergency Release Reports
HMIRS_______________________ Hazardous Materials Information Reporting System
NC SPILLS Spills Incident Listing
NC SPILLS 90 SPILLS 90 data from FirstSearch
NC SPILLS 80________________ SPILLS 80 data from FirstSearch
Other Ascertainable Records
FUDS
Formerly Used Defense Sites
DOD
Department of Defense Sites
SCRD DRYCLEANERS______.
State Coalition for Remediation of Drycleaners Listing
EPA WATCH LIST
EPA WATCH LIST
TSCA
Toxic Substances Control Act
TRIS_________________________
Toxic Chemical Release Inventory System
SSTS
Section 7 Tracking Systems
ROD
Records Of Decision
RMP _________________
Risk Management Plans
RAATS
RCRA Administrative Action Tracking System
PRP
Potentially Responsible Parties
PADS________________________
PCB Activity Database System
TC5441860.2s EXECUTIVE SUMMARY 5
EXECUTIVE SUMMARY
ICIS--------------------------
Integrated Compliance Information System
FTTS
FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide
Act)/TSCA (Toxic Substances Control Act)
MLTS------------------------
Material Licensing Tracking System
COAL ASH DOE
Steam -Electric Plant Operation Data
COAL ASH EPA
Coal Combustion Residues Surface Impoundments List
PCB TRANSFORMER-------_
PCB Transformer Registration Database
RADINFO
Radiation Information Database
HIST FTTS
FIFRA/TSCA Tracking System Administrative Case Listing
DOT OPS--------------------
Incident and Accident Data
CONSENT
Superfund (CERCLA) Consent Decrees
INDIAN RESERV
Indian Reservations
FUSRAP---------------------
Formerly Utilized Sites Remedial Action Program
UMTRA
Uranium Mill Tailings Sites
LEAD SMELTERS
Lead Smelter Sites
US AIRS---------------------
Aerometric Information Retrieval System Facility Subsystem
US MINES
Mines Master Index File
ABANDONED MINES
Abandoned Mines
FINDS-----------------------.
Facility Index System/Facility Registry System
ECHO
Enforcement & Compliance History Information
UXO
Unexploded Ordnance Sites
DOCKET HWC---------------
Hazardous Waste Compliance Docket Listing
FUELS PROGRAM
EPA Fuels Program Registered Listing
NC AIRS
Air Quality Permit Listing
NC COAL ASH---------------
Coal Ash Disposal Sites
NC DRYCLEANERS
Drycleaning Sites
NC NPDES
NPDES Facility Location Listing
NC UIC----------------------.
Underground Injection Wells Listing
NC AOP
Animal Operation Permits Listing
EDR HIGH RISK HISTORICAL RECORDS
EDR Exclusive Records
EDR MGP EDR Proprietary Manufactured Gas Plants
EDR RECOVERED GOVERNMENT ARCHIVES
Exclusive Recovered Govt. Archives
NC RGA HWS---------------- Recovered Government Archive State Hazardous Waste Facilities List
NC RGA LF Recovered Government Archive Solid Waste Facilities List
NC RGA LUST Recovered Government Archive Leaking Underground Storage Tank
SURROUNDING SITES: SEARCH RESULTS
Surrounding sites were identified in the following databases
Elevations have been determined from the USGS Digital Elevation Model and should be evaluated on
a relative (not an absolute) basis. Relative elevation information between sites of close proximity
should be field verified. Sites with an elevation equal to or higher than the target property have been
differentiated below from sites with an elevation lower than the target property.
Page numbers and map identification numbers refer to the EDR Radius Map report where detailed
data on individual sites can be reviewed.
Sites listed in bold italics are in multiple databases.
Unmappable (orphan) sites are not considered in the foregoing analysis.
TC5441860.2s EXECUTIVE SUMMARY 6
EXECUTIVE SUMMARY
STANDARD ENVIRONMENTAL RECORDS
Federal CERCLIS list
SEMS: SEMS (Superfund Enterprise Management System) tracks hazardous waste sites, potentially
hazardous waste sites, and remedial activities performed in support of EPA's Superfund Program across the
United States. The list was formerly know as CERCLIS, renamed to SEMS by the EPA in 2015. The list contains
data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities,
private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response,
Compensation, and Liability Act (CERCLA). This dataset also contains sites which are either proposed to or on
the National Priorities List (NPL) and the sites which are in the screening and assessment phase for possible
inclusion on the NPL.
A review of the SEMS list, as provided by EDR, and dated 07/17/2018 has revealed that there is 1 SEMS
site within approximately 0.5 miles of the target property.
Lower Elevation Address Direction / Distance Map ID Page
TREX PROPERTIES SITE 3114 CULLMAN AVENUE WNW 1/4 - 1/2 (0.420 mi.) H30 52
Federal CERCLIS NFRAP site list
SEMS-ARCHIVE: SEMS-ARCHIVE (Superfund Enterprise Management System Archive) tracks sites that have no
further interest under the Federal Superfund Program based on available information. The list was formerly
known as the CERCLIS-NFRAP, renamed to SEMS ARCHIVE by the EPA in 2015. EPA may perform a minimal level of
assessment work at a site while it is archived if site conditions change and/or new information becomes
available. Archived sites have been removed and archived from the inventory of SEMS sites. Archived status
indicates that, to the best of EPA's knowledge, assessment at a site has been completed and that EPA has
determined no further steps will be taken to list the site on the National Priorities List (NPL), unless
information indicates this decision was not appropriate or other considerations require a recommendation for
listing at a later time. The decision does not necessarily mean that there is no hazard associated with a
given site; it only means that. based upon available information, the location is not judged to be potential
NPL site.
A review of the SEMS-ARCHIVE list, as provided by EDR, and dated 07/17/2018 has revealed that there
is 1 SEMS-ARCHIVE site within approximately 0.5 miles of the target property.
Lower Elevation Address Direction / Distance Map ID Page
DETREX CHEMICAL INDU
Site ID: 0402782
EPA Id: NCD049773245
Federal RCRA CORRACTS facilities list
3114 CULLMAN WNW 114 - 112 (0.420 mi.) H31 53
CORRACTS: CORRACTS is a list of handlers with RCRA Corrective Action Activity. This report shows
which nationally -defined corrective action core events have occurred for every handler that has had corrective
action activity.
A review of the CORRACTS list, as provided by EDR, and dated 03/01/2018 has revealed that there are 2
TC5441860.2s EXECUTIVE SUMMARY 7
EXECUTIVE SUMMARY
CORRACTS sites within approximately 1 mile of the target property.
Lower Elevation
DETREX CHEMICAL INDU
EPA ID:: NCD049773245
SAFETY KLEEN CORP
EPA ID:: NCD079060059
Address
RTifL�fl9��u/ 6�1
20 YADKIN AVE (2320)
Federal RCRA non-CORRACTS TSD facilities list
Direction / Distance Map ID Page
WNW 114 - 112 (0.420 mi.) H31 53
SW 112 - 1 (0.719 mi.) 57 311
RCRA-TSDF: RCRAInfo is EPA's comprehensive information system, providing access to data supporting
the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA)
of 1984. The database includes selective information on sites which generate, transport, store, treat and/or
dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Transporters are
individuals or entities that move hazardous waste from the generator offsite to a facility that can recycle,
treat, store, or dispose of the waste. TSDFs treat, store, or dispose of the waste.
A review of the RCRA-TSDF list, as provided by EDR, and dated 03/01/2018 has revealed that there is 1
RCRA-TSDF site within approximately 0.5 miles of the target property.
Lower Elevation Address Direction / Distance Map ID Page
DETREX CHEMICAL INDU 3114 CULLMAN WNW 114 - 112 (0.420 mi.) H31 53
EPA ID:: NCD049773245
State- and tribal - equivalent NPL
NC HSDS: The Hazardous Substance Disposal Sites list contains locations of uncontrolled and
unregulated hazardous waste sites. The file contains sites on the national priority list as well as the state
priority list. The data source is the North Carolina Center for Geographic Information and Analysis.
A review of the NC HSDS list, as provided by EDR, and dated 08/09/2011 has revealed that there are 5
NC HSDS sites within approximately 1 mile of the target property.
Equal/Higher Elevation Address
SAFETY KLEEN CORP
GENERAL LATEX & CHEM
ICI - AMERICAS INC
DETREX CHEMICAL INDU
HENKEL CORP.
State- and tribal - equivalent CERCLIS
Direction / Distance Map ID Page
SW 1/2 - 1 (0.597 mi.) 0
WSW 1/2 - 1 (0.686 mi.) 0
W 1/2 -1 (0.922 mi.) 0
WNW 1/4 - 1/2 (0.341 mi.) 0
NE 1/2 -1 (0.572 mi.) 0
NC SHWS: The State Hazardous Waste Sites records are the states' equivalent to CERCLIS. These sites
may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state
funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by
potentially responsible parties. The data come from the Department of Environment & Natural Resources'
Inactive Hazardous Sites Program.
A review of the NC SHWS list, as provided by EDR, and dated 05/01/2018 has revealed that there are 16
TC5441860.2s EXECUTIVE SUMMARY 8
EXECUTIVE SUMMARY
NC SHWS sites within approximately 1 mile of the target property
Equal/Higher Elevation Address
YUASA-EXIDE DISTRIBU
3713 N. DAVIDSON ST.
Facility Id: NONCD0001051
MELATEX INC (FORMER
3818 NORTHMORE ST
Facility Id: NONCD0002820
WISE RECYCLING - CHA
600 E. SUGAR CREEK R
Facility Id: NCD990715062
NCDOT DIV 10 FACILIT
1119 E SUGAR CREEK R
Facility Id: NONCD0002179
Lower Elevation
Address
INX (FORMER) FACILIT
Facility Id: NCD081332900
PHILEMON AVE SITE
Facility Id: NONCD0003005
CAROLINA CONSOLIDATO
Facility Id: NONCD0002890
CHADBOURN GOTHAM, IN
Facility Id: NONCD0003012
GENUINE PARTS COMPAN
Facility Id: NONCD0001764
KAISER FLUID TECHNOL
Facility Id: NONCD0001946
GENERAL LATEX & CHEM
Facility Id: NCD081430258
RH BOULIGNY INC.
Facility Id: NONCD0002356
GIBBS ELECTROPLATING
Facility Id: NONCD0001022
APPLIED RESEARCH GRO
Facility Id: NCD047257472
DIXON QUICK COUPLING
Facility Id: NONCD0002293
OMNISOURCE SE/ATLANT
Facility Id: NONCD0001333
3200 & 3210 CULLMAN
E CRAIGHEAD RD & PHI
400 E 33RD STREET
JORDAN PL & DAVIDSON
124 ATANDO AVENUE
530 SUGAR CREEK RD E
2321 N. DAVIDSON ST
2320 NORTH DAVIDSON
2229 N DAVIDSON
2221 N. DAVIDSON STIR
332 ATANDO AVE
410 ATANDO AVE
Direction / Distance
Map ID
Page
NE 1/4 - 1/2 (0.427 mi.)
132
251
ENE 1/2 - 1 (0.570 mi.)
51
287
NE 112 - 1 (0.615 mi.)
52
288
E 112 - 1 (0.795 mi.)
59
441
Direction / Distance
Map ID
Page
NW 1/4 - 1/2 (0.342 mi.)
22
38
NNE 1/4 - 1/2 (0.437 mi.)
35
255
W 114 - 112 (0.477 mi.)
44
274
WSW 1/2 - 1 (0.559 mi.)
50
287
NW 112 - 1 (0.631 mi.)
53
288
NE 112 - 1 (0.705 mi.)
54
288
WSW 1/2 - 1 (0.708 mi.)
N55
305
WSW 112 - 1 (0.712 mi.)
N56
305
WSW 112 - 1 (0.785 mi.)
058
439
WSW 1/2 - 1 (0.801 mi.)
060
444
NW 112 - 1 (0.827 mi.)
61
444
NW 1/2 - 1 (0.910 mi.)
62
451
State and tribal landfill and/or solid waste disposal site lists
NC SWF/LF: The Solid Waste Facilities/Landfill Sites records typically contain an inventory of solid
waste disposal facilities or landfills in a particular state. The data come from the Department of Environment
& Natural Resources' List of Solid Waste Facility Contacts in Alpha Order.
A review of the INC SWF/LF list, as provided by EDR, and dated 04/18/2018 has revealed that there is 1
TC5441860.2s EXECUTIVE SUMMARY 9
EXECUTIVE SUMMARY
NC SWF/LF site within approximately 0.5 miles of the target property.
Equal/Higher Elevation Address Direction / Distance Map ID Page
BIO ECOLOGICAL SERVI 720 HERRIN AVENUE ENE 118 - 114 (0.131 mi.) B10 21
Facility Status: InactiveClosed
Permit Num: 60071-INCIN-1-
State and tribal leaking storage tank lists
NC LUST: The Leaking Underground Storage Tank Incidents Management
Database contains an
inventory
of reported leaking underground storage tank incidents. The data come from the Department of Environment, &
Natural Resources' Incidents by Address.
A review of the NC LUST list, as provided by EDR, and dated 08/03/2018 has revealed that there
are 21
NC LUST sites within approximately 0.5 miles of the target property.
Equal/Higher Elevation Address
Direction / Distance
Map ID Page
NEW LIFE THEOLOGICAL 3117 WHITING AVENUE
S 118 - 114 (0.207 mi.)
14 25
Incident Number: 40079
Current Status: File Located in Archives
STEEL GARDENS 3445 SPENCER STREET
E 1/8 - 1/4 (0.226 mi.)
16 27
Incident Number: 36141
Current Status: File Located in House
TRANSMISSION SUPPLY 642 ANDERSON STREET
ENE 1/4 - 1/2 (0.371 mi.)
F25 43
Incident Phase: Closed Out
Incident Number: 8826
Current Status: File Located in Archives
QUIK SHOPPE 9 3435 THE PLAZA
ESE 114 - 112 (0.429 mi.)
J34 252
Incident Phase: Follow Up
Incident Number: 8641
Current Status: File Located in House
SAMS MART 26 3400 THE PLAZA
SE 114 - 112 (0.456 mi.)
K37 256
Incident Phase: Closed Out
Incident Number: 22149
Current Status: File Located in Archives
COX, BORDERS, SHAVER 3725 N DAVIDSON STRE
ENE 114 - 112 (0.459 mi.)
139 260
Incident Phase: Closed Out
Incident Number: 8633
Current Status: File Located in Archives
PET DAIRY 3300 THE PLAZA
SE 114 - 112 (0.462 mi.)
L41 264
Incident Phase: Follow Up
Incident Number: 5705
Current Status: File Located in House
GORDIES AMOCO 3129 THE PLAZA
SSE 114 - 112 (0.462 mi.)
M43 268
Incident Phase: Closed Out
Incident Number: 3475
Current Status: File Located in Archives
C MART 442 3109 THE PLAZA
SSE 114 - 112 (0.477 mi.)
M45 277
Incident Phase: Response
TC5441860.2s EXECUTIVE SUMMARY 10
EXECUTIVE SUMMARY
Incident Number: 8792
Current Status: File Located in House
AMBROSIA HOOTEN CHOC
Incident Phase: Closed Out
Incident Number: 27127
Current Status: File Located in Archives
Lower Elevation
3746 NORTH DAVIDSON ENE 114 - 112 (0.495 mi.) 48 282
Address Direction / Distance Map ID Page
NORTH CHARLOTTE SERV
516 EAST 36TH STREET
NW 0 - 118 (0.105 mi.)
A2
10
Incident Phase: Closed Out
Incident Number: 21688
Current Status: File Located in Archives
JOHNSTON MILL APARTM
3315 NORTH DAVIDSON
NNW 0 - 118 (0.112 mi.)
4
14
Incident Phase: Closed Out
Incident Number: 27257
Current Status: File Located in Archives
VESPOINT PROPERTY
3112 NORTH DAVIDSON
W 118 - 114 (0.165 mi.)
C11
21
Incident Phase: Closed Out
Incident Number: 40183
Current Status: File Located in Archives
FAT CITY SITE
3123 NORTH DAVIDSON
WNW 118 - 114 (0.176 mi.)
C12
23
Incident Number: 36395
Current Status: File Located in House
L & N TIRE SERVICE
300 EAST 36TH STREET
NW 1/4 - 1/2 (0.302 mi.)
D19
32
Incident Phase: Closed Out
Incident Number: 16670
Current Status: File Located in Archives
HIGHLAND MILLS PARK
2901 N DAVIDSON STRE
W 114 - 112 (0.342 mi.)
E20
34
Incident Phase: Closed Out
Incident Number: 23762
Current Status: File Located in Archives
L & N TIRE CO.
240 E. 36TH ST.
NW 114 - 112 (0.350 mi.)
D23
38
Incident Phase: Closed Out
Incident Number: 14306
Current Status: File Located in Archives
ABERNATHY LUMBER COM
308 EAST CRAIGHEAD R
NNE 1/4 - 1/2 (0.397 mi.)
G26
44
Incident Phase: Closed Out
Incident Number: 27267
Incident Number: 36559
Current Status: File Located in Archives
VIRGINIA MOORE TRUST
3404 RITCH AVENUE
NNW 1/4 - 1/2 (0.415 mi.)
29
50
Incident Phase: Closed Out
Incident Number: 40211
Current Status: File Located in Archives
CAROLINA CONSOLIDATO
400 E 33RD STREET
W 114 - 112 (0.477 mi.)
44
274
Incident Phase: Closed Out
Incident Number: 13260
Current Status: File Located in Archives
TARMAC VIRGINIA, INC
3934 RALEIGH STREET
NE 114 - 112 (0.498 mi.)
49
284
Incident Phase: Follow Up
TC5441860.2s EXECUTIVE SUMMARY 11
EXECUTIVE SUMMARY
Incident Number: 8613
Current Status: File Located in House
NC LAST: A listing of leaking aboveground storage tank site locations.
A review of the NC LAST list, as provided by EDR, and dated 08/03/2018 has revealed that there is 1
NC LAST site within approximately 0.5 miles of the target property.
Lower Elevation Address Direction / Distance Map ID
PAUL MCBROOM RESIDEN 3000 NORTH DAVIDSON
Incident Number: 91013
Current Status: C
WSW 1/4 - 1/2 (0.299 mi.) 17
NC LUST TRUST: This database contains information about claims against the State Trust Funds for
reimbursements for expenses incurred while remediating Leaking USTs.
A review of the INC LUST TRUST list, as provided by EDR, and dated 07/06/2018 has revealed that there
are 6 NC LUST TRUST sites within approximately 0.5 miles of the target property.
Equal/Higher Elevation Address Direction / Distance Map ID
NEW LIFE THEOLOGICAL 3117 WHITING AVENUE S 118 - 114 (0.207 mi.) 14
Site ID: 40079
QUIK SHOPPE 9 3435 THE PLAZA ESE 114 - 112 (0.429 mi.) J34
Facility Id: 0-013942
Site ID: 8641
EXPRESS #525(E-Z SER 3400 THE PLAZA SE 1/4 - 1/2 (0.456 mi.) K36
Facility Id: 0-013873
Site ID: 22149
PET DAIRY 3300 THE PLAZA SE 114 - 112 (0.462 mi.) L40
Facility Id: 0-013774
Site ID: 5705
Lower Elevation
VESPO/NT PROPERTY
Site ID: 40183
FAT CITY SITE
Site ID: 36395
r.lr_ r_ erraa
3112 NORTH DAVIDSON
3123 NORTH DAVIDSON
Direction / Distance Map ID
W 118 - 114 (0.165 mi.) C11
WNW 118 - 114 (0.176 mi.) C12
State and tribal registered storage tank lists
NC UST: The Underground Storage Tank database contains registered USTs. USTs are regulated under
Subtitle I of the Resource Conservation and Recovery Act (RCRA). The data come from the Department of
Environment & Natural Resources' Petroleum Underground Storage Tank Database.
A review of the NC UST list, as provided by EDR, and dated 07/27/2018 has revealed that there are 2
Page
29
Page
25
252
255
263
Page
21
23
TC5441860.2s EXECUTIVE SUMMARY 12
EXECUTIVE SUMMARY
NC UST sites within approximately 0.25 miles of the target property.
Equal/Higher Elevation
Address
Direction / Distance
Map ID
Page
FIRE STATION 7
3210 N DAVIDSON ST
WNW 0 - 1/8 (0.118 mi.)
A7
17
Tank Status: Removed
Tank Status: Current
Facility Id: 00-0-0000017340
Lower Elevation
Address
Direction / Distance
Map ID
Page
NORTH CHARLOTTE SERV
516 EAST 36TH STREET
NW 0 - 118 (0.105 mi.)
A2
10
Tank Status: Removed
Facility Id: 00-0-0000003325
State and tribal Brownfields sites
NC BROWNFIELDS: A brownfield site is an abandoned, idled, or underused property where the threat of
environmental contamination has hindered its redevelopment. All of the sites in the inventory are working
toward a a brownfield agreement for cleanup and liabitliy control.
A review of the INC BROWNFIELDS list, as provided by EDR, and dated 06/01/2018 has revealed that there
are 4 NC BROWNFIELDS sites within approximately 0.5 miles of the target property.
Equal/Higher Elevation Address Direction / Distance Map ID Page
NODA TEXTILE 430 E. 36TH STREET NW 1/8 - 1/4 (0.215 mi.) 15 27
Project ID: 19028-15-60
Lower Elevation
SINCLAIR REFINING CO
Project ID: 20019-16-60
HIGHLAND MILLS PARK
Project ID: 20037-16-60
CRAIGHEAD RD.
Project ID: 18015-14-60
ADDITIONAL ENVIRONMENTAL RECORDS
Address Direction / Distance Map ID Page
409 E. 35TH ST. AND WNW 1/8 - 1/4 (0.187 mi.) 13 25
2901 N DAVIDSON STRE W 1/4 - 1/2 (0.342 mi.) E20 34
308 E. CRAIGHEAD RD; NNE 1/4 - 1/2 (0.397 mi.) G28 50
Local Lists of Landfill / Solid Waste Disposal Sites
NC HIST LF: A listing of solid waste facilities.
A review of the NC HIST LF list, as provided by EDR, and dated 11/06/2006 has revealed that there is
1 NC HIST LF site within approximately 0.5 miles of the target property.
Equal/Higher Elevation Address Direction / Distance Map ID Page
BIO ECOLOGICAL SERVI 720 HERRIN AVENUE ENE 118 - 114 (0.131 mi.) B10 21
TC5441860.2s EXECUTIVE SUMMARY 13
EXECUTIVE SUMMARY
Facility Status: CLOSED
Facility Id: P0667
NC SWRCY: A listing of recycling center locations.
A review of the NC SWRCY list, as provided by EDR, and dated 05/03/2018 has revealed that there is 1
NC SWRCY site within approximately 0.5 miles of the target property.
Lower Elevation Address Direction / Distance Map ID Page
SOUTHERN RESOURCES, 3826 RALEIGH ST. NNE 1/4 - 1/2 (0.488 mi.) 47 281
Records of Emergency Release Reports
NC IMD: Incident Management Database.
A review of the NC IMD list, as provided by EDR, and dated 07/21/2006 has revealed that there are 18
NC IMD sites within approximately 0.5 miles of the target property.
Equal/Higher Elevation
Address
Direction / Distance
Map ID
Page
TRANSMISSION SUPPLY
624 ANDERSON STREET
ENE 1/4 - 1/2 (0.366 mi.)
F24
42
Facility Id: 8826
QUICK SHOPPE # 9
3435 THE PLAZA
ESE 1/4 - 1/2 (0.429 mi.)
J33
251
Facility Id: 8641
E-Z SERVE #525
3400 THE PLAZA
SE 1/4 - 1/2 (0.456 mi.)
K38
259
Facility Id: 22149
COX, BORDERS, SHAVER
3725 N DAVIDSON SIRE
ENE 114 - 112 (0.459 mi.)
139
260
Facility Id: 8633
PET DAIRY
3300 THE PLAZA
SE 114 - 112 (0.462 mi.)
L40
263
Facility Id: 5705
AMOCO #1106-GORDIES
3129 THE PLAZA
SSE 1/4 - 1/2 (0.462 mi.)
M42
267
Facility Id: 3475
COASTAL MART #442
3109 THE PLAZA
SSE 1/4 - 1/2 (0.477 mi.)
M46
280
Facility Id: 8792
AMBROSIA HOOTEN CHOC
3746 NORTH DAVIDSON
ENE 114 - 112 (0.495 mi.)
48
282
Facility Id: 27127
Lower Elevation
Address
Direction / Distance
Map ID
Page
NORTH CHARLOTTE SERV
516 EAST 36TH STREET
NW 0 - 118 (0.105 mi.)
A2
10
Facility Id: 21688
JOHNSTON MILL APARTM
3315 NORTH DAVIDSON
NNW 0 - 118 (0.112 mi.)
4
14
Facility Id: 27257
L & N TIRE SERVICE
300 E 36TH STREET
NW 1/4 - 1/2 (0.302 mi.)
D18
31
Facility Id: 16670
HIGHLAND MILLS PARK
2901 N DAVIDSON STRE
W 114 - 112 (0.342 mi.)
E20
34
Facility Id: 23762
HIGHLAND MILLS
2901 NORTH DAVIDSON
W 1/4 - 1/2 (0.342 mi.)
E21
36
TC5441860.2s EXECUTIVE SUMMARY 14
Facility Id: 85764
L & N TIRE CO.
Facility Id: 14306
ABERNATHY LUMBER COM
Facility Id: 27267
DETREX CHEMICAL INDU
Facility Id: 85654
CAROLINA CONSOLIDATO
Facility Id: 13260
TARMAC VIRGINIA, INC
Facility Id: 8613
Other Ascertainable Records
EXECUTIVE SUMMARY
240 E. 36TH ST.
NW 114 - 112 (0.350 mi.)
D23
38
308 E. CRAIGHEAD ROA
NNE 114 - 112 (0.397 mi.)
G27
48
3114 CULLMAN
WNW 114 - 112 (0.420 mi.)
H31
53
400 E 33RD STREET
W 114 - 112 (0.477 mi.)
44
274
3934 RALEIGH STREET
NE 114 - 112 (0.498 mi.)
49
284
RCRA NonGen / NLR: RCRAInfo is EPA's comprehensive information system, providing access to data supporting
the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA)
of 1984. The database includes selective information on sites which generate, transport, store, treat and/or
dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non -Generators do
not presently generate hazardous waste.
A review of the RCRA NonGen / NLR list, as provided by EDR, and dated 03/01/2018 has revealed that
there is 1 RCRA NonGen / NLR site within approximately 0.25 miles of the target property.
Equal/Higher Elevation
BIO ECOLOGICAL SERVI
EPA ID:: NCD982099889
EDR HIGH RISK HISTORICAL RECORDS
EDR Exclusive Records
Address Direction / Distance Map ID Page
720 HERRIN AVE ENE l/8 - 1/4 (0.131 mi.) B9 19
EDR Hist Auto: EDR has searched selected national collections of business directories and has collected
listings of potential gas station/filling station/service station sites that were available to EDR
researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include
gas station/filling station/service station establishments. The categories reviewed included, but were not
limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station,
service station, etc. This database falls within a category of information EDR classifies as "High Risk
Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past
sites and operations that typically create environmental concerns, but may not show up in current government
records searches.
A review of the EDR Hist Auto list, as provided by EDR, has revealed that there are 3 EDR Hist Auto
sites within approximately 0.125 miles of the target property.
Lower Elevation
COLUMBUS OIL CO (BRS
CHARLOTTE MOTOR CO
BILLS SERVICE GROC
Address Direction / Distance Map ID Page
516 E 36TH NW 0 - 1/8 (0.105 mi.) Al 9
500 E 36TH NW 0 - 1/8 (0.114 mi.) A6 17
3307 N DAVIDSON ST NW 0 - 1/8 (0.120 mi.) A8 19
TC5441860.2s EXECUTIVE SUMMARY 15
EXECUTIVE SUMMARY
EDR Hist Cleaner: EDR has searched selected national collections of business directories and has collected
listings of potential dry cleaner sites that were available to EDR researchers. EDR's review was limited to
those categories of sources that might, in EDR's opinion, include dry cleaning establishments. The categories
reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash
& dry etc. This database falls within a category of information EDR classifies as "High Risk Historical
Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and
operations that typically create environmental concerns, but may not show up in current government records
searches.
A review of the EDR Hist Cleaner list, as provided by EDR, has revealed that there are 2 EDR Hist
Cleaner sites within approximately 0.125 miles of the target property.
Lower Elevation Address Direction / Distance Map ID Page
NORTH CHARLOTTE LAUN 3306E N DAVIDSON ST NW 0 - 1/8 (0.105 mi.) A3 14
NORTH HIGHLANDER CEN 3220 N DAVIDSON WNW 0 - 1/8 (0.112 mi.) A5 17
TC5441860.2s EXECUTIVE SUMMARY 16
EXECUTIVE SUMMARY
Due to poor or inadequate address information, the following sites were not mapped. Count: 3 records.
Site Name
Database(s)
J C TEETER NC SWF/LF
BP STATION #24175(FORMER PLAZA ROA NC LUST TRUST
VIRGINIA MOORE TRUST NC LUST TRUST
TC5441860.2s EXECUTIVE SUMMARY 17
OVERVIEW MAP - 5441860.2S
Target Property
o 1 a
112 t 1Miles
Sites at elevations higher than
or equal to the target property
Indian Reservations BIA
Upgradient Area
♦
Sites at elevations lower than
°
°
Power transmission lines
Hazardous Substance
the target property
100-year flood zone
Disposal Sites
1
Manufactured Gas Plants
500-year flood zone
National Priority List Sites
Dept. Defense Sites
National Wetland Inventory
State Wetlands
This report includes Interactive Map Layers to
display and/or hide map information. The
legend includes only those icons for the
default map view.
SITE NAME: Forest Hill Church Parcels CLIENT: Geoscience Group
ADDRESS: 729 E 36TH ST CONTACT: Ashley Proctor
CHARLOTTE NC 28205 INQUIRY #: 5441860.2s
LAT/LONG: 35.246331 / 80.802412 DATE: October 02, 2018 4:44 pm
Copyright m 2018 EDR, Inc. (c) 2015 TornTom Rel. 2015.
DETAIL MAP - 5441860.2S
i
r
-
4
*_
1610
�13
u>
eel
-=r e
Cl
I
t '
��lllo Ml�SON CHILD OEV[I OPMCtrT. TER
?
_
�.�
16
JOHNSTON YMCA SCHO�U.t n('F I'RQf RAM
MCHEALTHCENTERAI u? AN5f16N YMCA
\
' CM SUCCESS RV G
e
-
N
PRINCE & PRINC H� F- AV CASE 't
MANS
\
\
ad AHLANQ I NIT
{Ip
T
MON&
I
i
N
Target Property
A
Sites at elevations higher than
or equal to the target property
♦
Sites at elevations lower than
the target property
1
Manufactured Gas Plants
r
Sensitive Receptors
National Priority List Sites
Dept. Defense Sites
0 1116
1/8 1/4Miles
Indian Reservations BIA
Hazardous Substance
Power transmission lines
Disposal Sites
100-year flood zone
500-year flood zone
17
National Wetland Inventory
State Wetlands
This report includes Interactive Map Layers to
display and/or hide map information. The
legend includes only those icons for the
default map view.
SITE NAME: Forest Hill Church Parcels CLIENT: Geoscience Group
ADDRESS: 729 E 36TH ST CONTACT: Ashley Proctor
CHARLOTTE NC 28205 INQUIRY #: 5441860.2s
LAT/LONG: 35.246331 / 80.802412 DATE: October 02, 2018 4:47 pm
Copyright m 2018 EDR, Inc. (c) 2015 TomTom Rel. 2015.
APPENDIX V
User Questionnaire
Environmental Questionnaire
Records Of Communication
Laboratory Report
USER QUESTIONNAIRE
Forest Hal! Church Parceh
Charlotte, North Catodfiaa
ntiC end Si�tsture of son ,a of ne
q/ie��6
-Dgte
P'eease provide an anr4wr to each question to the best of your inawledge or artuch pertlncrat
info rma#on and Mant{ry a nwnberfar each atrachmen t.
(I.) Are you aware of any enviro"m=tat el eanug liens against the property that are filed ; or
r`CM4M Lander federal, tribal, state or local law?
No ❑ Yes (Describe or attach information) Attachment No.
(2.) Are you aware of any Activity and Use Limitations (AULs), such as engineering controls (egg.
engineered caps, faundations, liners, treatment methods, etc, in use to prevent contamination from
migrating to swTounding arms), land use restrictiarns ar institutinnAl controls (e.g. administrative
measures restricting grunndwatcr use, construction, or property use) that are in place at time site
and/co- have been filed or rccordc d in a registry- under federal, tribal, state or local law?
XNO ❑ Yes Pescn'l)t or attach information) Attachment No.
(3.) Da yov have any sntcialmz d knorwIedge or experience related to the property or nearby
Pr°1artie3? For cxauxple, are you involved in tht same line of business as the can=t or former
occupants of the property or an adjoining property so that you would have speeiaiized knowledge of
the chemicals and processes used by this type of business?
No ❑ Yes (Describe or attach int'orrnation) Anse Mont No.
USER QUESTIONNAIE (Continued)
Fare Hill Chump Putcels
Charlotte, North Carolina
K) Does the purchase price being paid for this property reasonably reflect the fair market value of
the property?
❑ No Yes (Describe or attach inf'ortnetion) Attachment No.
if you conclude that there is a dif eMncc, Dave you considered whether the lower purchase price is
pause cantarnivation is known or believed to be present at the property?
No ❑ Yes (Describe or attach infaxruation) Attachment No.
(S.) Arc you aware of commonly ImoAm or reasonably ascertainable infonnatlon about the property
that would help the environmental professional to identify conditions indicative of releases or
threatened releases? For exauVlc., a<5 User,
(a.) Do you knaw the past uses of the property?
o ❑ Yes (Describe or attach inforniati m) Attachriwa No.
(b) Do you know of specific chemicals that are present or once were present at the property?
)�No ❑ Yes (Describe or attach infortnation) Attachment No.
(c) Do you snow of spills or other them icat releases that have taken place at the propertyl
XNv ❑ Yes (Describe or attach information) Attat:btr = No,
(d.) Do you know of any environmental cleanups that have takers place at the property?
No ❑ Yes (Describe or attach inforrrtation) Attachment No.
(5.) As the User of the ESA, based on your knowledge and eaperienca related to the property an
there any obvious indicators that point to the presence or likely presence of enatamirtation at floe
property?
io ❑ Yes (Describe or attach information) Attachmmt No.
GBOSCIENCE GAMP, INC.
Eavlrorun wl Questionetaire
(to be completed by current property owner)
Forest Hill Church Parcels, Charlotte, North Carolina
1. la for pruputy Or anp 4OiWW Property used for an industrial use?
YES
If Yea, please explain:
NO
UNKNOWN
2, T'o tbt heat of your knowledge, bm the property or =Y Ad,l ❑mk4 PgPdy been used far an iadtisttial use in the pest?
YES w 0 UNKNOWN
If YrM, vitae explain,
3. lathe property or say adl oiuiag pmperty used as a gasoline station, motor repair fatality, commmial printing fmdity,
dry cleancrs, Photo developing laboratory, hwkyurd or landfill, or as a waste treatment; storage, disposal, processing„or
recycli% facility?
YES
If Yes, please explain:
C!�
UNKNOWN
d. To the best of your knowledge has the property or adjeibing property been used as a gasoline astiop, motor relish
fsc"'sty, ooF*.rn=cU printing facility, dr'y cleaners, pbcto devziopitag laboratory, bmkyard ❑r landfill, or as a waste
treatment, sttxsge, dispos&I, praeming, or reeycring acnity?
YES t No ulvxlca
If Yes, please explain;
S. Ate there currently, or to the best of yvua kmowlWgc have there been previously, MY damaged or discarded
mtowotiva or industrial batteries, or pesticides, paint, or othcr chor6rab its individust 0=iners of g,eatax tl= 3
gallow (19L) in volume or 50 gallons (190L) in the a egate, stared on or used at the property or at the facili t
YES NO UHIICMOWN
IfYes, pleaseexplain:_ __�.._...
b. Are there cunentiy, or to the beg of your knowledge have there berm previously, any iaduat W drums (typically 55'
gallons (208L)) ar sacks of chcnicals located an the property or at the FaaiW
YES QNp j rv—NMMM+—
IfYes, ply
7. Has Ell dirt been bmught onto the property that originew from a cantmai =tad site or that is of an usnIMovM origm7
YES NO l�a�
If Yea, Please explaia:
8. Are there currently, or to the best of yam knowledge have there been previously. my Aug, tom, or laeaW
on the property m connection with waste treatment or waste disposal? r�
YES
If Yea. PWM Win -
Page t of 3
GEOSC1ENCE GROVP, RVC
Fnvimnmrntal Questionnaire
(to be completed by current property owner)
Forut Hill Church Parcels, Charlotle, North Carolma
P. is there cusnmay, or to the lest of yow knowledge have there have been previo nn t#�e prvpdxtyri
YES NO 13PiKNOWN
If Yea, please explain.
10- l8 there currently, or to the best of your knowledge have there been previously, Any registered or unr &tMW maw
t ka (above or ur! otnd) located on the pmpert}ri
If Yes,
11_ Are there sw-rently, or to the best of your knowledge have there bem previously, any vent pipes, fill pipes, or Acoese
ways indicating a fill pipe protruding from the gmuzid an the property or adjacent to any structure located on the
prop-t]7
YES No UNKNOWN
Yes, please
12, Are there cumatly, or to the best of your kmwledge have there been previously, any flooring, drains, ar walls located
vviffin the facility that are stained by substances caw than water or am crnining foul odors?
YES _ — NO _ UNKNOWN
—
Yes, please explain:
13_ If the property is served by a private wail Of non-public water system, have contaminants been identified its the well
or system that exceed guidelines applicable to toe water t s`tem or bass the well been designated as canes by any
gavcreunerit eavitoanjM UVheaith ageXy?
YES C
UNKNOWN
If Yes, please explain:
14. Dm the owner or occupant of the property have any lawwledge of eavitonmenUl liens or governmental notifaeaaim
relating to past or MWTMI violations of eatvironmenW laws with respect to the property or any facility located an thts
YES
If Yes, please explain:
AM t 51.
15. Hoe the owner or occupant ofthe property been iufornsed of she past or current existence of hazardous substage or
petroleum products m environmental violations with respect to tkac property or any facility located on the property?
YES lvo UNKNOWN
if Yes, please explain:_ __.._.
16. Does the owner or occupant of the property have any knowledge of.any environmental aite assessment of the property
or fatality that ittdirated the pmsenee of hazardous substances or pelroletun paaducta nu, ar ContaMination of, the
ptope ny or reeommendsd fttrtber asmeamEnt ofthe pr�
YES NO UNKNOWN
If Yes, please explain:
Page 2 of 3
GBOSCIF.NCE CROVP, nvG
Enviraamentm Qus3ti0f=ire
(to be vomplaed by current property cover)
Forest Hill Church Parcels, Charlotte, North Carolina
17.17oes the owner of occupant of the pxoparty kao w of any Past, threatened, or pending lawsviU or admis,istrati%'V
PzmcOdiugs coixeraing a relegate or threatened r+el WC pf any baxardms stti+stence or pctrokeum praducta imrolvft the
PropWy by any owner or Occupant of the pro y7
YES
NO� UNKNOWN
If yes, Ply rxplain:
is. Does the property dischuge was to wa ter on ar f to the Property Ott= than sittmn vmW into a aenitkry Sewer.
System?
YES NO
If Ycs, please explain — y� M1—�� �lA+fKNOWAI 4
19. To the beat of your knowledge, have any hazanious mbstanae- ar petrole= praducts, uftWentified waste Ro ials,
tires, automotive Or industrial bancries or any other waste materWh been dumped above grade, buried andlar burned or
the property?
YES,
If yea, please explain: UN"OWN
20. is there a ttansformm,, capacitor, or a¢iy hydraulic equipment for which there sae any record indicating flee pntscnw
ofPC'E3s7
YES
If Yes, please cvlain:`---
---(7w-
21. To die best of your knowledge, are there n the subject property?
YES ',` I
+lp UNKNOWN
If Yes, please explain:_ — _
%twine Of Person Completing Questo—a=:
TAIL:
Fn-m:
Address:
Oi f 1 t N
x represent that to the of my knowledge the above stateatettts and {sets are true wed ec►Ftrct to the best of my
actual 1 awTedgc na to 'a] fasts have been suppmmed or m1hstated.
hoe Osu.
Page 3 of 3
CHARLOTTE FIRE
DEPARTMENT
Battalion Chief Tim Hartsell
500 Dalton Ave.
Charlotte, NC 28206
Phone — 704-336-2461
Fax — 704-336-4204
To: Ashley Proctor
Re; 719 East 36" Street, Charlotte
Project:
Date: 03 October 2018
Fax. Sent Via Email
X
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. There are no records of any CFD response to this address involving
Petroleum or other hazardous substances.
A search of our records has not turned up any responses for hazardous materials at or
near the above address.. Please be advised that prior to annexation in the City of Charlotte
there may have been a response by the VFD that provided protection. We do not
maintain any of those records. The Mecklenburg County Fire Marshalls office may be
contacted for additional information. Their number is 704-336-2154
In your FOI request your reference additional information pertaining to fire code violations,
permits, and underground f above ground storage tanks, and remedial actions. Please fax
that request to the Fire Prevention office at 704-336-5190.
Parcel or Address is listed as residing in
unincorporated Mecklenburg County or one of the other municipalities.
VFI3 is presently the fire department that responds to this property. As such if they
handled an emergency themselves without any assistance from Emergency Management
or CFD Hazmat team, we would have no record of those responses. The Mecklenburg
County Fire Marshal's Office may be Contacted for additional information. Their num ber is
7Q4 336-2 154
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. The following records were found for this property I address involving
petroleum or other hazardous substances,
Information related to underground and aboveground storage tanks may be requested from INC
Department of Environment and Natural Resources at 704-663-1699.
Sincerely
Tim Hartsell
Battalion Chief, Charlotte Fire Department
Hazardous Materials Coordinator,
Charlotte Mecklenburg Emergency Management
* The property researched is by address. If the street had a former designation, that is not searched unless the
previous names are proved by the requestor.
CHARLOTTE FIRE
DEPARTMENT
Battalion Chief Tim Hartsell
500 Dalton Ave.
Charlotte, NC 28206
Phone — 704-336-2461
Fax — 704-331fi-4204
To: Ashley Proctor
Re: 729 East 361h Street, Charlotte
Project:
Date: 03 October 2018
Fax: Sent Via Email
x
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. There are no records of any CFD response to this address involving
Petro leum or other hazardous substances.
A search of our records has not turned up any responses for hazardous materials at or
near the above address. Please be advised that prior to annexation in the City of Charlotte
there may have been a response by the VFD that provided protection. We do not
maintain any of those records. The Mecklenburg County Fire Marshalls office may be
contacted for additional information. Their number is 704-336-2154
In your FOI request your reference additional information pertaining to fire code violations,
permits, and underground I above ground storage tanks, and remedial actions. Please fax
that request to the Fire Prevention office at 704-336-5196.
Parcel or Address is listed as residing in
unincorporated Mecklenburg County or one of the other municipalities.
VFD is presently the fire department that responds to this property. As such if they
handled an emergency themselves without any assistance from Emergency Management
or CFD Hazmat team, we would have no record of those responses. The Mecklenburg
County Fire Marshal's Office may be contacted for additional information. Their number is
704-336-2154
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. The following records were found for this property 1 address involving
petroleum or other hazardous substances,
Information related to underground and above ground storage tanks may be requested from NC
Department of Environment and Natural Resources at 704-663-1699.
Sincerely
Tim Hartsell
Battalion Chief, Charlotte Fire Department
Hazardous Materials Coordinator,
Charlotte Mecklenburg Emergency Management
* The property researched is by address. if the street had a former designation, that is not searched unless the
previous names are proved by the requester.
CHARLOTTE FIRE
DEPARTMENT
Battalion Chief Tim Hartsell
13ik 500 Dalton Ave,
Charlotte, NC 28206
Phone — 704-336-2461
Fax — 704-336-4204
To; Ashley Proctor
Re: 3315 North McDowell Street, Charlotte
Project:
Date: 03 October 2018
Fax: Sent Via Email
X
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. There are no records of any CFD response to this address involving
petroleum or other hazardous substances.
A search of our records has not turned up any responses for hazardous materials at or
near the above address. Please be advised that prior to annexation in the City of Charlotte
there may have been a response by the VFD that provided protection. We do not
maintain any of those records. The Mecklenburg County Fire Marshalls office may be
contacted for additional information. Their number is 704-336-2154
In your FCI request your reference additional information pertaining to fire code violations,
permits, and underground 1 above ground storage tanks, and remedial actions. Please fax
that request to the Fire Prevention office at 704-336-5190.
Parcel or Address is listed as residing in
unincorporated Mecklenburg County or one of the other municipalities.
VFD is preseritty the fire department that responds to this property. As such if they
handled an emergency themselves without any assistance from Emergency Management
or CFD Hazmat team, we would have no record of those responses. The Mecklenburg
County Fire Marshal's Office may be contacted for additional information. Their number is
704-336-2154
A search of our records for spills or fires involving petroleum or hazardous materials has
been conducted. The following records were found for this property J address involving
petroleum or other hazardous substances,
Information related to underground and above ground storage tanks may be requested from NC
Department of Environment and Natural Resources at 704-663-1699,
Sincerely
Tim Hartsell
Battalion Chief, Charlotte Fire Department
Hazardous Materials Coordinator,
Charlotte Mecklenburg Emergency Management
* i lie property researched is by address. If the street had a former designation, that is not searched unless the
previous names are proved by the requestor.
Full -Service Analytical F
/'PRISMI Environmental Solutions
nA
Geoscience Group
Tam Hassett
500-K Clanton Rd.
Charlotte, NC 28217
INC. Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
Project: Forest Hill Church Parcels
Lab Submittal Date: 1010512018
Prism Work Order: 8100119
Case Narrative
t Oil 8/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody, Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please calf if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATQR.IES, INC.
Angela D. Overcash
VP Laboratory Services
Reviewed By Angela D. Overcesh
VP Laboratory Services
Data Qualifiers Key Reference:
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a T
This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 20224-0543
Phone: 704)529-U64 -Tull Free Number: I41DW529.5364 - Fax: 700525-0409 page i of $
ZR-I S n A ErivIr nrvice Analytical s
e ' V' Envl�anmentni Solutions
Sample Receipt Summary
10/1812018
Prism Work Order: 8100119
Client Sample ID Lab Sample ID Matrix Daterrime Sampled DatefTime Received
HA-1 6100119-01 Sand 10105/18 0.00 10/05/18 15:05
HA-2 8100119-02 Solid 10/05118 0:00 10/05/18 15:05
Samples were received In good condition at 4.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the wri}ten consent of Prism Laborstorles, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-DS43
Phone: 704f529-6364 - Toll Free Number: 1-0001529.6364 - Fax: 7WS25.0409 Page 2 of 8
Full-
.`P,AR I S M n envir " ice Anatyutio s
[V' E�vEranm�rrtsl Solutions
LI5wwomwsS, C:
Geoscience Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hilt Church Parcels
Sample Matrix: Solid
Laboratory Report
1011812018
Client Sample ID: HA-1
Prism Sample ID: 8100119-01
Prism Work Order: 8100119
Time Collected: 10105118 0a:00
Time Submitted: 1010&18 15:05
Parameter Result Units Report MIL Dilution Method Analysis Analyst Batch
Limit Factor datefrime II]
Diesel Range Organics by GCIFID
diesel Range Organics BRL mglkg dry
9.9 2.6 1
Surrogate
•8015c 10/11/18 16:36 ZRC PSJ0194
Recovery Control Limits
o-Terphenyl
84 % 31-123
Gasoline Range Organics by GCIFID
RLM
Gasoilne Range Organics BRL
molt dry
7.5 1,6
50 18015C 1018N8 19:38 ANCW PeJ0103
Surrogate
Recovery Control Limits
s.a.a-Trifluorotoluone
148 % 50.137 SR
General Chemistry Parameters
%solids 70.3
%by
0,100 0.100
1 'SM2540 G 1W16M8 16:40 TJY P&J0305
Weight
This report should not be reproduced, except in its entirety, without the written consent at Prism Lahoratories. Inc.
449 Springbrook Road - P.O. Box 240543 . Charlotrs, NC 28224-0543
Phone. 7WS29.6364-Toll Free Number:l-600;5x9-6364- Fax: 704152"4" Page 4 of 8
I FvliSer ice Annlylicel 8.
En�lronmenf�l Boiuti�ns
'-: �AKIRwTw�ame
Summary of Detections
1011 B!2018
Prism Work Order: 8100119
PHam ID Client ID Parameter Method Result Lirits
There were no detections reported.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: 7641529-6364 - Toll free Number: 9-8901529-6354 -Fax, 7041525-0409 Page 3 of 8
/ri®r-i!Service Anaiyt tl %; EnYironmantal Sulutlona
l•BDRATORIES 'NV
Geoscienoe Group
Attn: Tom Hassett
500.K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Laboratory Report
10AW018
Client Sample I❑: HA-2
Prism Sample I❑: 8100119-02
Prism Work finder: 8100119
Time Collected: 10105/18 00:00
Time Submitted: 10/05/18 15.06
Parameter Result Units Report VIAL Dilution Method Analysis Analyst Batch
Limit Factor ❑ate/Time I
Diesel Range Organics by GC1FID
Diesel Range Organics 13RL mglkg dry 9.9 2.6 1 'S0i5C 10111/18 17;1a ZRC P8J0194
Surrogate Recovery Control Limits
o-Terphenyl
St) 96 31-129
Gasoline Range Organics by GC/FlD
Gasoline Range Organics 6RL mglkg dry 9.9 2.1 50 *8015C 1018f18 20;O6 ANWJ PSJ0103
Surrogate Recovery Control Limb
a.a,a-Trikurotoluen e
General Chemistry Parameters
134 % 50-137
% Sol Ids 70.6 %by 0.100 0.100 1 '5012540G 10119/18 16;40 TJY Pt1J0305
weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"0 Sprsngbrook Road , P.O. Box 240543 - Chariotte, NC 2822"U3
Phone: 7041529$364 -Toll Free Number. 1-8001529.6364 • Fax; 70415254409 Page 5 of 8
L"P.,pLq
Full -Service Analylleal Environmental Solutions
Geoscience Group Project: Forest Hill Church Parcels
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, INC 28217
Gasoline Range Organics by GC*lD - quality Control
Level II QC Report
10/18118
Prism Work Order: 8100119
Time Submitted: 1015I2018 3:05:00PM
Reporting Spike Source %REG RPD
Ana lyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBJ0103 - 6035
Blank lPBJ0103-BLK1y
Prepared & Analyzed: 10/08118
Gasoline Range Organics
BRL
5.0 mglkg wet
Surrogate' a, a, a -Tiff uornVuene
5.20
rrlglkg
5.000 104
50-137
LCS (PBJ010343S1)
Prepared & Analyzed: 10108118
Gasoline Range Organics
59.7
5.0 mglkg wet
50.00 119
41-138
Surrogafe.' e,a,a-Trffuorofaluene
5.65
mg/kg
5.000 113
50-137
LCS Dup (158J0103-113SOI)
Prepared & Analyzed: 10/08118
Gasoline Range Organics
64.8
6-0 mg/kg wet
50,00 130
41-139 a 20
Surrogate: a,a,a-TriRuorotoiuerre
5.45
mg/kg
5.000 109
50-137
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratodes, Irr.
449 Springbraok Road - P.Q. Box 240543 - Cha►latte, NC 28224-0543
Phone, 704f$29-6364 -Toll Free Number: 1-0401529-5364 - t=ax: 70415254MO9 Page 6 of 8
P LgF I q M I FUIP-SeryiGe Analytical &
Envirenmpnral Solutions
L�eES �Nc
Geoscience Group Project: Forest Hill Church Parcels
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Diesel Range Organics by GCIFiD - Quality Control
Level fl QC Report
10116/18
Prism Work Order: 8100119
Time Submitted: 10f512018 3:05;04PM
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P830194 - 3546
Blank (PU0194-BLK1)
Prepared & Analyzed: 10111/18
❑iesel Range Organics
BRL
7.0
mglkg wet
Svrrogafe: a-Terphenyl
7.p7
mg*g wet
1.332 81
31-123
LCS (138J0194-13S'I) _
Prepared & Analyzed:_ 1_0111118
Diesel Range Drganics
51A
7.0
mglkg wet
66.64 77
46-126
Sun-ople: o-Tsrphenyf
1.18
mglkg wet
1.333 89
31-123
LCS Dup (PaJ0194-BS01)
Prepared & Analyzed. 1011 ill
Diesel Range Organics
54.0
7A
mg/kg wet
66.67 81
46.126 5 20
Surrogate:-7"mphenyl
1.16
rnglkg wet
1.333 87
31-121
Sample Extraction data
Prep Method- 3348
Lab Number Batch Initlal Final DateMme
8100119-01 PRJ0194 30.1 g 1 mL 10J11J18 8:42
6100119-02 PBJ0194 30.07 g 1 mL 10111J18 8:42
Prep Method: 5035
L.ab Number Batch Initial Final Dekslilme
6100119-01 PBJO103 4.77 g 5 mL ioiw18 12:03
8100119-02 P8J0103 3.58 g 5 mL 1p108f18 12:03
Prep Method: Solids, Dry Weight
Lab Humber Batch initial Final Dateirime
9100119-01 P8d0305 30 g 30 g 1(VI 8118 16:40
8100119-02 P8J0305 30 g 30 g 10116118 16:40
This report should not be reproduced, except in its enlirety, wlthout the written consent of Prism Laboratories, Inc.
449 Sprh►gbrook Road - P.U. Box 2405t3 - Charlotte, NC 28224-0543
Phone: 704J528-fs36d -Toll Free Number: 1-SM529.6364 - Fax: 7WS29-0409
Page 7 of 8
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INC CBrti Drinking
iOn Water
ert
■ � :. Full -Service Analytical � INCNC ❑risking Water Cert Iva. 37735 � p12412p1 g
Environmental Solutions SC GertiTrcatlon No. 99012
L a9MATOnIM INC.
Geoscience Group Project: Forest Hill Church Parcels
Tom Hessen
500-K Clanton Rd. Late Submittal Date. 10/12/2018
Charlotte, NC 28217 Prism Work Order: 8100259
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully.
PRISM LABORATORIES, INC.
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference
Reviewed By Robbi A, Jones For Angela D. Overcash
President/Project Manager
DO Surrogates diluted out.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not he reproduced, except in its entirety, without the written eonsent of Prism Laboratories, Inc.
449 5pringbrook Road - P.a. ISox 240543 - Chatlotte. NC 28224.0543
Phone: 704l529.6364 - Toll Free Number: 1-6001529-6364 - Fax: 7041523.0409 Page 1 of $
PRISM I Full Service al Golubo a
Sample Receipt Summary
Enviranm®oral Solutions 1012412018
LA6pgA;nRCa LNG
Prism Work Order; 8100289
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
HA-3 8100259-01 Solid 10/12118 10:08 10/12/18 13:30
HA-4 8100259-02 Solid 10112J18 11:45 10/12/18 13:30
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road . P.O. Box 240543 - Charlotte, INC 26224-6543
Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 -Fax: 7U/625-0409 Page 2 of i3
4 Full -Service AnaEytical&
ISM I Envrranmental Solutlons
LAB�P�TGRILR IMr,
Summary of Detections
1012412018
Prism Work Order: 8100259
Prism ID
Client I❑
Parameter
Method
Result
Units
8100259-01
HA-3
Diesel Range Organics
'8i315G
26000
Mg/kg dry
81002$9-01
HA-3
Gasoline Range Organics
'9Et1SC
2300
mglkg dry
8100259-02
HAA
Diesel Range Organics
'8015C
3500
mglkg dry
8100259-02
HA-4
Gasoline Range Organics
18aisc
99
mglkg dry
This report should not be reproduced, except in its entirety, without the written consent otPrism Laboratories, Inc.
4449 8pringbrook Read - P.O. Box 240543 . Charlotte, NC 28224d1S43
Phone: 7041529.6364 - Toil Free Number: f-soW529-6364 - Fax: 704Ai2S-Wl1 Page 3 of 8
I S n � I Full-Serorce Analytical a
V' I Environmental Solutions
�Rn,aAcs ��
Geoscience Group
Attn: Tom Hassett
50D-K Clanton Rd.
Charlotte, NO 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Laboratory Report
10124/2010
Client Sample ID: HA-3
Prism Sample ID: 8100259-01
Prism Work Order: 8100259
rme Collected: 10/12/18 10-08
Time Submitted: 10112I18 13:30
Parameter Result Units Report MOL Dilution Method Analysls Analyst Balch
Limit Factor Dat"Mme ID
Diesel Range Organics by GCIFID
Diesel Range Organics 26000 rngfhg dry 1900 500 200 18615C 10M7118 9:08 IRC P8J0283
Surrogate R--ery Cdhtrol Limits
o-Terphenyl 0 % 31-123 OQ
Gasoline Range Organlcs by GCIFID
Gasoline Range Organics 2300 m9/kg dry 93 20 Sao "8015C 10119118 9:33 ANGIJ PBJ0333
Surrogate
a, a,a-Triflu orotalV en e
Retavery Contrd Limits
110 % 50-137
General Chemistry Parameters
% Solids 73.9 'Y by 0.100 0.100 1 `SM2S40 G 10122I18 1410 TJY P810417
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism LabDfatones, Inc_
449 Springhroott Road - P.O. Box 240543 • Charlotte, NC 28224-0543
Phone: 7041529-5354 -Tall Free (dumber: 1-8001529-6354- Fay: 70d1525-"09 Page 4 0f 8
Laboratory Report
�FR ISM I E, vir amen analytical 8
! Environmental 801ufign3 10r2412018
'%` .AHWTpMl" iaq
Geoscienee Group
Attn: Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: Forest Hill Church Parcels
Sample Matrix: Solid
Client Sample ID: HA-4
Prism Sample ID: 8100259-02
Prism Work Order: 8100259
Time Cotlected: 10/12/18 11:45
Time Submitted: 1011211813:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatelTme Ill
Diesel Range Organics by GCIFID
Diesel Flange Organics 3500 mglkg dry 490 18$ 50 *$015G 10MVi8 7:50 ZRC PSJ0283
Surrogate Recovery Control Limits
o-Terphenyl
0 % 3f-723 00
Gasoline Range Organics by GC1FID
Gasoline Range Organics 99 myfky dry 7.9 1.7 So "8olsc 10119118 511 ANGM P$J0333
Surrogate Recovery Control Limits
a,a.a-Trifluorotaluene 118 % 5D-137
General Chemistry Parameters
%Solids 71.0 %by 0.100 0.100 1 '3M2540G 1012211814:30 TJY PSJ0417
Weight
This report should not be reproduced, except in ita entirety, without the written consent of Prtsrn Laboratories, Inc.
449 Springbrook Road • P.O. Bum 240543 - Charlotte, NC 28224-0543
Phone: 7041529-0364 • Toil Free plumber: 1$001529-4384 - Fax: 7041525-MO Page 5 of 8
�R I S h ,♦� Full -Service Analytical
I V I � Environmental Sofu[fans
its- h&
Geosoience Group Project: Forest Hill Church Parcels
Attu: Torn Hassett
500-K Clanton Rd.
Charlotte. NC 28217
Gasoline Range Organics by GGlFID -{duality Control
Level li QC Report
10124l18
Prism Work Order: 8100259
Time Submitted: 10/12/2018 1:30:OOPM
Reporting
Spike Source
%REC RPD
Analyse
Result
Urnk
Units
Level Result %REC
Limits RP❑ Limit Notes
Batch MOM - 5035
Blank (P8J0333-BLK1)
Prepared BAnaWed: iOil all 8
Gasoline Range Organics
RRL
5.0
rnglkg wet
Surr*g'?fe: a,a,a-7nfl(forW010ene
5.05
mg*9
5.00U 101
50-137
LCS (P8J0333-051)
Prepared & Analyzed: 10118/18
_
Gasoline Range organics
55.4
5.0
mglkg wet
50.00 111
41-138
Surrogate: a,a,a-Tnfiuorat0iuene
4.90
mglkg
5.000 98
50-137
l_CS Dup IMID333-MI)
Prepared & Analyzed: i0/18/18
Gasoline Range Organics
81A
5.0
Mog wet
50.00 122
41-139 10 20
Surrogate: a,a,a-Trtluarotoluene
&00
mglkg
5.000 100
50-137
This report should not be reproduced. except in Its entirety, without the written consent of prism Laboratories. Inc,.
448 Springhrook Rnad - P.O. Box 24OS43 - Charlotte, INC 28224.0543
Phone: 7041529-6364 - Tall Free Humber: 1.8001529-6364 - fax: 704(525-0409
Page 6of8
+� R I S i Fuu-Service AnafS'xical 8
Enviranmenx>Ri SaEu[fona
ORA70o OL ING
Geoscdence Group Project; Forest Hill Church Parcels
Attn: Tam Hassett
5OD-K Clanton Rd.
Charlotte, NC 28217
Diesel Range organics by GCIFID - Quality Control
Level II QC Report
10124118
Prism Work Order: 8100259
Time Submitted: 10/12/2018 1:30:OOPM
Reporting Spike Source %REC RPO
Anaiyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBJ0283 - 3546
Blank (PSJ0283-BLK1 )
Prepared a& Analyzed: 1 D116118
Dlesel Range Organics
BRL
7.0 mglkg wet
Surrogate: o-Terphenyl
0.929
mg/kg wet
1,333 70
31.12.3
LIDS (P8J0283-1351) _
Prepared & Analyzed: 1011-6118
Diesel Range Organics
59.1
7.0 mglkg wet
66.67 69
46.126
Surrogate: u-Terphenyl
1.24
mgft wet
1.333 93
39-123
LCS oup (P8J0253-BSDI)
Prepared &Anatyze_d: 10116118
Diesel Range Organics
55.8
7.o mglkg wet
66.67 84
46-126 6 20
Surrogate. o-Terphenyl
1.08
mglkg wet
1.333 81
31-123
Sample Extraction Data
Prop Method: 3546
Lab Number Batch Inkial Final Daterrinn
8100259-01 PBJ0283 30.1 g 1 mL 10118118 11:35
8100259-02 PBJ0283 30A2 g 1 mL 10116118 11:35
Prep Method: 5035
Lab Number Batch
Initial
Final
DatalTime
81 OD259-01 POJ0333
3.62 g
5 mL
1 WI8118 10:64
81D0259-02 P8J0333
4.46 g
5 mL
10/18118 11154
Prep Method: Sands, Dry V"ht
Lab Number Batch
inlitlal
Final
Datefllme
8100269.01 P8J0417 30 g 30 9 1W2118 14:30
811DO259-02 P8J0417 30 g 30 g 10122118 14:30
This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2a224.0543
Phone: 704I529-6364 -Toll Free Number. 1.8001529.6364 - Fax: 704/525-04H Page 7 of 8
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APPENDIX VI
Qualifications of Environmental Professionals
Consulting Engineea•s
Ashley N. Proctor
Assistant Project Manager - Charlotte, NC
SPECIAL QUALIFICATIONS & EXPERIENCE RELATED TO THIS ASSIGNMENT
Recent entry into the field of environmental assessments after completing Bachelor of Arts
GEQSCIENCE Degree at Winthrop University. Training in basic principles of ArcGIS. Hands on experience
GROUP and continuing education in environmental investigations.
EDUCATION
Bachelor of Arts in Environmental Studies
Minor in Social Sciences
Winthrop University, 2012 - 2016
SHORT COURSES
Phase I and I1 Environmental Site Assessments for Commercial Real Estate
ASTM - Practice E 1527-13
EXPERIENCE
2017 - Present: Assistant Project Manager
Geoscience Group - Charlotte NC
Perform onsite inspections and investigations, conduct field testing of soils and water, and
prepare Phase I Environmental Site Assessment reports.
Consulting Engineers
Thomas C. Hassett, P.E.
Senior Engineer - Charlotte, NC
SPECIAL QUALIFICATIONS & EXPERIENCE RELATED TO THIS ASSIGNMENT
Over twenty (20) years experience in a wide variety of environmental, geotechnical, and
GEPSCIENCE construction materials engineering projects. Special training and experience in environmental
GROUT' investigations and construction material evaluations.
EDUCATION
BS Studies in Mechanical Engineering
McGill university, 1987 --1991
Webb Institute Of Naval Architecture, 1985 - 1986
EXPERIENCE
2014 - Present: Senior Engineer
Geoscience Group - Charlotte, NC
Manage site investigations, perform onsite
inspections, and prepare reports for
commercial and industrial. clients, Work
includes environmental investigations,
segmental block retaining wail design and
materials testing.
20082014: Project Engineer
Geoscience Group - Charlotte, NC
Performed onsite inspections, managed site
investigations and prepared reports for
commercial and industrial clients. Work
included environmental investigations,
segmental block retaiztii-ig wall design, and
materials testing.
1997-2008: Project Manager
Geoscience Group - Charlotte, NC
Conducted and directed environmental
assessments, remediation projects and
prepared construction materials testing
reports.
Short Courses
Environmental Site Assessment
Practices for Commercial Real Estate
A5TM - Practice E 1527-13
Evaluation Of Indoor Inhalation Pathway
National Environmental Health Association
National Radon Proficiency Program
Residential Radon Measurement
1495-1997: Laboratory Manager
Geoscience Group - Charlotte, NC
Conducted laboratory tests and field
inspections for the selection and utilization
of construction materials.
1993-1995; Engineering Technician
Geoscience Group -Charlotte, NC
Conducted field testing of soils, stone,
concrete, asphalt, fasteners, and steel for a
variety of construction projects.
1989: Laboratory Assistant
Array Carps Of Engineers - Hanover, NH
Evaluated simulated sea ices used for scale
model testing of ship hulls.
PROFESSIONAL ENGINEERING REGISTRATIONS
North Carolina
PROFESSIONAL CERTIFICATIONS
National Environmental Health Association - Residential Radon Measurement Provider
Brownfields Property Application
North Carolina Brownfields Program
www. n cbrownf iel d s. o ra
I. PROSPECTIVE DEVELOPER (PD) INFORMATION {USE TAB KEY TO GET TO NEXT
DATA ENTRY LINE — DO NOT USE THE RETURN KEY}
A. PD information:
Entity name
Forest Hill Church
Principal Officer
Tom Emmrich
Representative
Nick Dusenbury
Mailing Address
7224 Park Road
Charlotte, North Carolina 28210
E-mail address
nick.dusenbury@foresthill.org
Phone No.
704-71 b-8700
Fax No.
NIA
Web site
www.foresthill.org
B. PD contact, person information (i.e., individual who will serve as the NQP's point of
contact if different than above):
Name Amy Rickers
Company Johnston, Allison & Hord, P.A.
Mailing Address 1065 East Morehead Street
Charlotte, North Carolina 28204
E-Mail Address arickers@jahlaw_com
Phone No. 704-998-2253
Fax No. 704-323-4653
C. Information reaardina all parent companies,. subsidiaries or other affiliates of i'D !attach
swarate sheets) if necessary),:
(Use for LLCs)
Member -managed or manager -managed? Answer: NIA
Cl
If manager -managed, provide name of manager and percent of ownership:
Name
Ownership (%)
Mailing Address
E-Mail Address
Phone No,
Fax No.
For all LLCs, list all members of the LLC and provide their percent of ownership:
Name
Ownership
Mailing Address
E-Mail Address
Phone No.
Fax No.
Name
Ownership (%)
Mailing Address
E-Mail Address
Phone No.
Fax No.
Name
Ownership
Mailing Address
E-Mail Address
Phone No.
Fax No.
E
Managers of manager -managed LLCs are required to execute all brownfield documents for
the LLC; as to member -managed LLCs, state name of member who will sign these
documents.
List all parent companies, subsidiaries and other affiliates:
(Use for Partnerships) N/A
Check one: ❑General Partnership ❑Limited Partnership
List all partners and percent of ownership:
Name
Ownership
Mailing Address
E-Mail Address
Phone No.
Fax No.
Is this person a general or limited partner?
Name
Ownership {°/o}
Mailing Address
E-Mail Address
Phone No.
Fax No.
Is this person a general or limited partner?
List all parent companies, subsidiaries and other affiliates:
C
(Use for corporations other than LLCs)
(If information is the same as shown in 1.A., please indicate "same as 1.A."below.)
Name same as I.A. above
Mailing Address
E-Mail Address
Phone No.
Fax No.
List all parent companies, subsidiaries and other affiliates:
Seeds of Hope, Inc.
(Use for individuals)
(if individual is the same as shown in 1.A., please indicate "same as ?.A."above.)
Name NIA
Mailing Address
E-Mail Address
Phone No.
Fax No.
D. Does PD have or can it obtain the financial means to fully implement a brownfields
agreement and assure the safe reuse of the property? (Attach supporting documentation
such as letters of credit, financial statements, etc.)
Answer Yes
Explanation PD is a going concern with the ability and intention to utilize and develop the property to its safe and
full reuse. Independent Auditor Financial Statements for year-end 2016, 2017, and 2018 are
submitted with this application.
E. Does PD have or can it obtain the managerial means to fully implement a brownfields
agreement and assure the safe use of the property?
Answer Yes
Explanation The corporate structure of the organization provides the leadership to oversee the process of implementation of
the Brownfields Agreement. Forest Hill Church will also work with its environmental consultant and counsel
to ensure compliance and implementation of the Brownfields Agreement
7
F. Does PD have or can it obtain the technical means to fully implement a brownfields
agreement and assure the safe use of the property?
Answer Yes
Explanation Forest Hill Church will work with its environmental consultant and its
environmental counsel to ensure the Agreement is fully and properly
imolemented.
G. Does PD commit that it will comply (and has complied, if PD has had a prior project in the
NCBP) with all applicable procedural requirements of the NCBP, including prompt payment of
all statutorily required fees?
Answer yes
(List all NCBP project name(s) and NCBP project 1D numbers where PD or any parent
company, subsidiary and other affiliate of PD has been a party to.)
NIA
H. Does PD currently own the property?
Answer No
If yes, when did PD purchase the property and from whom? (Provide name, address,
telephone number and email address of the contact person for the current
property owner. )
NIA
If no, provide the name, address, telephone number and e-mail address of the contact
person for the current property owner
Johnston Memorial Presbyterian Church ffkla North Carolina Presbyterian Church c/o
Molly Griffin, 1010 Vickery Drive, Charlotte, North Carolina 28215
I. If PD does not currently own the property, does PD have the property under contract to
purchase?
Answer Yes
If yes, provide date of contract. July 31, 2018
If no, when does the PD intend to purchase the property (e.g., after the project is determined
to be eligible for participation in the NCBP, after PD receives a draft BFA, after the
conclusion of the brownfields process)?
NIA
0
J. Describe all activities that have taken place on the property since PD or PUs parents,
subsidiaries and/or other affiliates, and/or lessees or sublessees of PD, took ownership of or
operated at the property (e.g., industrial, manufacturing or commercial activities, etc.).
(Include a list of all regulated substances as defined at NCGS § 130A-310.31(b)(11) that have
been used, stored on, or otherwise present at the property while those activities were
conducted, and explain how they were used.)
Forest Hill Church has been leasing the property since August 1, 2018 and has been operating on
the property as a religious organization holding meetings and worship services.
II. SITE INFORMATION
A. Information reaardinq the proposed brownfields Property:
Proposed project name 3315 McDowell Street
acreage 1.887 acres County Mecklenburg
street address(es) 729 East 36th Street and 3315 North McDowell Street
City Charlotte zip 28205
tax ID(s) or PIN(s) 9110401 and 9110402
Past uses) Church related purposes since at least 1929 with some singly -family use,
current use(s) The property is used for Church related purposes.
causes)/source(s) of contamination:
known Two on -site USTs used to store heating oil. One of which has been determined to have
leaked
suspected None
B. Regulatory Agency Involvement: List the site names and all identifying numbers (ID No.)
previously or currently assigned by any federal, state or local environmental regulatory
agencies for the property. The ID No's may include CERCLIS numbers, RCRA generator
numbers for past and present operations, UST database, Division of Water Quality's incident
management database, and/or Inactive Hazardous Sites Branch inventory numbers. (In
many instances, the PD will need to actively seek out this information by reading
environmental site assessment reports, reviewing government files, contacting government
officials, and through the use of government databases, many of which may be available over
the internet.)
Agency Name/lD No: NIA
Agency Name/l❑ No:
Agency Name/ID No:
Agency Name/10 No:
0
Agency Name/l❑ No:
Agency NamellD No:
C. In what way(s) is the property is abandoned, idled, or underused?
Property is currently used for church purposes but PD intends to expand its use into a thriving
church and related use property-
D. In what way(s) is the actual or possible contamination at the property a hindrance to
develo ment or redevelo ment of the property (attach any supporting documentation such as
letters from lending Institutions)?
As a potential purchaser of the property and a nonprofit corporation, it is important that PD have any environmental issues addressed prior to
possession. Without the protection afforded by the Brownfield program, the PD is unable to risk environmental liabilities associated with
lingering contamination that could risk funding needed for its primary purposes.
E. In what way(s) is the redevelopment of the property difficult or impossible without a
brownfields agreement (attach any su000rtina documentation such as letters form lending
institutions)?
The possibility of environmental liability for this non-profit organization is not acceptable and
the Brownfield Agreement and liability protection will resolve this issue for the PD.
F. What are the planned uses of the redevelo ed brownfields property to which the PD will
commit? Be as specific as specific as possible.
Forest Hill intends to develop and expand the church related use of the property.
G. Current tax value of brownfields property: $1,788,400.00
H. Estimated capital investment in redevelopment project: $ Approximately $4 million.
I. List and describe the public benefits that will result from the property's redevelopment. Be as
specific as possible. (Examples of public benefits for brownhelds projects include job creation,
fax base increases, revitalization of blighted areas, preserved green space, preserved historic
places, improving disadvantaged neighborhood quality -of -fife related retail shopping
opportunities, affordable housing, environmental cleanup activities or set asides that have
community or environmental benefits. In gauging public benefit, NGBP places great value
upon fetters of support from community groups and local government that describe
anticipated improvements in quality of life for neighboring communities that the project will
bring about. The inclusion of such support letters with this apnlicatiorl is recommended and
encouraged.)
This project will update and enhance the area by providing a thriving place of worship into a developing area. The improvements to the property will
further increase the tax value of the property as well.
Special Note: Please describe all environment -friendly technologies and designs PD plans
to utilize in its redevelopment strategy. For example, environment friendly redevelopment
plans could include: Leadership in Energy and Environmental Design (LEED) Certification,
green building materials; green landscaping techniques such as using drought resistant
plants; energy efficient designs, materials, appliances, machinery, etc.; renewable sources of
energy, and/or recycling/reuse of old building materials such as brick or wood.
10
J. Who will own the brownfields property when the Notice of Brownfields Property is filed with
the register of deeds at the conclusion of the brown„fields process? (If information is the
same as I.A. above, please indicate.)
Name likely same as l .A above or if closing has not occurred will be with owner listed in I .H.
Mailing Address
E-Mail Address
Phone No.
Fax No.
Ili. OTHER REQUIRED INFORMATION
A. Brownfields Affidavit: PD must provide its certification, in the form of a signed and
notarized original of the unmodified model brownfields affidavit provided by NCSP, that it
did not cause or contribute to contamination at the property and that it meets all other
statutory eligibility requirements. (Note: The form to use for this affidavit is attached to this
application. An original hard copy of this affidavit must be filled out, signed, notarized and
submitted with this application.)
Is the required affidavit as described above included with this application
Answer Yes
B. Proposed Brownfields Agreement Form: PD must provide the completed form Proposed
Brownfields Agreement. (Note: The form to use for this document is attached to this
application. It must be filled out, initialed, and attached on your submittal.)
Is the reciuired Proposed Brownfields Acireement, as described above included with this
application?
Answer Yes
C. Location May: P❑ must provide a copy of the relevant portion of the 1:24,000 scale
LI.S.G.S. topographic quadrangle may that shows the location of the property, clearly
plotted, and that measures at least an 8 Y2 by 11 inches. (Note: these maps can be
purchased through the above link, or often through retail outdoor recreation stores that can
print out the relevant map. Often environmental reports have location maps that use this
type of map format as the base for its location map.)
Is the required location map included with this application?
Answer Yes
11
D. Survey Plat: P❑ must provide a preliminary survey plat of the brownfields property with the
property boundaries clearly identified, and a metes and bounds legal description that
matches the property description on the plat. At this stage of the brownfields process, one
or more existing survey plats from a previous property conveyance will suffice. (Before the
brownfields project enters the public comment phase of the brownfields process, the PD will
be required to submit a final brownfields survey plat which includes the information fisted in
the brownfields survey plat guidance.)
Is the recluired meliminary survey plat included with this application?
Answer Yes
E. Site Photoaraohs: PD must provide at least one pre -redevelopment photograph of the
property, in either hard copy or electronic format, that shows existing facilities and
structures. Please note that the NCBP prefers to have electronic photos instead of or
in addition to hard copies. Electronic copies of photographs should be emailed to:
Shirlev.Liooinsftedenr.gov with a clear indication as to which Brownfields
Application they apply to.
Are photographs of the orop_erty included with this application?
Answer Yes
Have electronic ca ies of the ohotograiphs been emailed to NCBP?
Answer Yes
F. Environmental Reports/Data: If it makes an affirmative eligibility determination, the NCBP
will request that P❑ provide any and all existing environmental reports and data for the
property on CD only. The brownfields process may be expedited if PD submits such
reports/data with this application.
Are any environmental reports/data being submitted with this application?
Answer yes
If environmental reports/data are being submitted with this application, please provide the
title, date and author of each item being submitted:
Phase I Environmental Site Assessment
Forest Hill Church Parcels
Charlotte, North Carolina
Geoscience Project No. CH M0129.GE
December 13, 2018
Geoscience Group
IV. ADDITIONAL REQUIRED FORMS
The following forms are to be filled out and submitted with the application including the
Responsibility and Compliance Affidavit and the Proposed Brownfields Agreement.
Submittal of the Affidavit requires signature and notarization, and the Proposed
Brownfields Application requires an initial.
12
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
NORTH CAROLINA HROWNFIELDS PROGRAM
IN THE 'MATTER OF: Forest Hill Church
UNDER THE AUTHORITY OF ) AFFIDAVIT
NORTH CAROLINA GENERAL } RE: RESPONSIBILITY
STATUTES ❑ 130A-310.30, et. seq. ) AND COMPLIANCE
Nick Dusenbury , being duly sworn, hereby deposes and says:
1. I am Representative of Forest Hill Church
2. [if signatory is not President, add this paragraph: "I am fully authorized to make the declarations
contained herein and to legally bind Forest )-lill C`hnrch .9
3. Forest Hill Church is applying for a Brownfields Agreement with the North Carolina
Department of Environmental Quality, pursuant to N.C.G.S. 0 130A, Article 9, Part 5 (Brownfields
Act), in relation to the following 09110401 and 091 10402 parcel(s) in Charlotte
_Mecklenburg , County, North Carolina: 729 East 36(h Street _
3315 North McDowell Street
4. I hereby certify, under the pains and penalties of perjury and of the Brownfields Act, that
Forest Hill Church , and any parent, subsidiary or other affiliate meets the eligibility
requirements of N.C.G.S. ❑ 130A-310.31(b)(10), in that it has a bona fide, demonstrable desire to
develop or redevelop, and did not cause or contribute to the contamination at, the parcel(s) cited in the
preceding paragraph.
5. I hereby certify, under the pains and penalties of perjury and of the Brownfields Act, that
Forest Hill Church meets the eligibility requirement ofN.C.G.S.❑130A-
310.32(a)(1) in that it and any parent, subsidiary or other affiliate have substantially complied with:
a. the terms of any brownfields or similar agreement to which it or any parent, subsidiary or
other affiliate has been a party;
b. the requirements applicable to any remediation in which it or any parent, subsidiary or other
affiliate has previously engaged;
c. federal and state laws, regulations and rules for the protection of the environment.
Affiant furtkr saith not.
5ignatafe/Mnted Name
Date,
Sworn to and subscribed before me
this day of-
OFROX SEAL
' NOn Puhlic North Carona
Notary Public,;t;
S _. .A i�f -1 1 ENBURC. COUNTY, NC
t.
My commission expires:_
MY C. nmis$On FxOres July 1. 2023
13
Preliminary Proposed Brown -fields Agreement
I. Property Facts
a. Property Address(es): 729 East 36th Street and 3315 North McDowell Street
b. Property Seller: Johnston Memorial Presbyterian Church flkla North Charlotte Presbyterian Chi
c. Property Buyer: Forest Hill Church
d. Brief Property Usage History: Church related purposes since at least 1929 with some single-family
use.
e. The planned reuse will potentially involve the following use classification(s) (check all that
apply):
❑ School/childcare/senior care
❑R Residential
❑ Commercial, retail (specify)
❑ Other commercial (specify)
❑ Office
❑ Light industrial
❑ Heavy industrial
❑ Recreational
❑ Open space
❑X Other (specify) Religious services and meeting uses
I1. Contaminant Information
a. The contaminant situation at the property is hest described by the following (check all that
apply):
❑ Contaminants are from an on -property source(s)
❑ Contaminants are from an off -property source(s)
❑ Contaminants are from an unknown source(s)
❑ Contaminants have not yet been documented on the property
14
b. Contaminated Media Table. (If known, check appropriate boxes below)
Contaminant
Soil
Groundwater
Private Wells
Vapor Intrusion
Types
and/or Surface
Water
known
Suspected
known
Suspected
known
suspected
known
suspected
o
Chlorinated
r
Solvents
9
(list):
a
n
i
c
5
Petroleum:
Two
ASTs ❑
heating
USTs 0
❑i] UST,
Other ❑
Other (list):
i
Metals
n
(list):
0
r
9
a
n
i
Other (list):
C
5
III. Protective Measures
I am prepared to take steps necessary to make the property suitable for its planned uses while
fully protecting public health and the environment. I propose that NCBP consider a brownfields
agreement that will make the property suitable for the planned use(s) through the following
mechanism(s) (check all that apply):
❑ Contaminant remediation to risk -based levels.
0 Engineered Controls (e.g., low permeability caps, vapor mitigation systems, etc)
❑ Land use restrictions that run with the land that will restrict or prohibit uses that are
unacceptable from a risk assessment/management perspective. (Important Note: In any
15
final brownfields agreement generated by the NCBP, land use restrictions will ultimately
come with the continuing obligation to submit an annual certification that the Land Use
Restrictions are being complied with and remain recorded at the applicable register of
deeds office. )
IV. Fees
In connection with a brownfields agreement, the Act requires that the developer pay fees to
offset the cost to the Department of Environmental Quality and the Department of Justice. In
satisfaction of the Act, the following fees apply to a brownfields agreement that is developed for
this project under the standard program, subject to negotiation of the brownfields agreement:
a. A $2,000 initial fee will be due from the applicant PD when both of the following occur:
1) NCBP receives this application, the affidavit and proposed brownfields agreement, AND
2) NCBP notifies the applicant in writing that the applicant PD and the project are eligible for
participation in the NCBP and continued negotiation of a brownfields agreement.
b. A second fee of $6,000 will be due from the PD prior to execution of the brownfields
agreement. Should the prospective developer choose to negotiate changes to the agreement
that necessitate evaluation by the Department of Justice, additional fees shall apply.
c. Any addendum/modifications to the BFA or NBP after they are in effect will result in an
additional fee of at least $1,000.
d. In the unexpected event that the environmental conditions at the property are unusually
complex, such that NCBP's costs will clearly exceed the above amounts, NCBP and PD will
negotiate additional fees.
e. Additional fees are charged for the Ready for Reuse and Redevelopment Now programs.
Vk—tViowgement
Please check this box and initial in space provided to indicate your
of the standard brownfields fee structure.
❑ Please check this box and initial in space provided to indicate your interest in the
Redevelopment Now program and your acknowledgement of the alternate fee structure as
outlined in the Redevelopment Now Fee Consent Document (under separate cover).
❑ Please check this box and initial in space provided to indicate your interest in the
Ready for Reuse program.
Date of Submittal:
16
Financial Statements
Location Map
� cis � rl� ����, �� , .. ...... j� � •:
1
V
••y •ten• • ., +•• ' �
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• �f ••1 k• \ � 4
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w
GEOSCIENCE GROUP, INC.
j CHARLOTTE, NORTH CAROLINA
J SCALE I'd 95' APPROVED BY: DPAWNI HY Mec;Mcnburg Co -
DATE. October 3, 2018 REVISED: ANP
FOREST HILL CHURCH PARCELS
CHARLOTTE, NORTH CAROLINA
FrUtrttE ���sEx:
2015 COUNTY TOPOGRAPHIC MAP CH1BEFt 9 5
GEOSCIENCE GROUP, INC.
CHARLOTTE, NORTH CAROLINA
SCALE: ] " = 2,000' APPROVED BY. DRAWN BY: 1iSGS
DATE- October 3, 2019 REVISED, ANP
1 FOREST HILL CHURCH PARCELS
CHARLOTTE, NORTH CAROLINA
1967 USGS TOPOGRAPHIC MAP rRLNUMBER
(PHOTOREVISED 1988) CH18.129-6
Survey Plat
pa
$ Ggg iZ S:I 3I
All
i I
::.... ...... _......_.—.....—._.'.._T— _ •-
d
f'
d'
•SS9YOQOri
Site Photographs
APPENDIX X II
Site Photographs i through ] 9
Q
rn
E
m
2
-Zf �7
Environmental/Reports/Data
ROY COOPER
Governor
MIC1 AEL S. REGAN
NORTH CAROLINA
Environmental Quality
Secretary July 5, 2019
MICHAEL SCOTT
Director Sent Via USPS and email
Torn Emmrich
Forest Dill Church
7224 Park Road
Charlotte, NC 28210
Nick.dusenbury@foresthill.org
Subject: Letter of Eligibility
N. Charlotte Presbyterian Church
729 East 36' Street and 3315 North McDowell Street
Charlotte, Mecklenburg County
Brownfields Project Number 23039-19-060
Dear Mr. Emmrich:
The North Carolina Department of Environmental Quality (DEQ) has received and reviewed
your June 13, 2019 Brownfields Property Application (BPA) submitted by Forest Hill Church as a
Prospective Developer seeking a Brownfields Agreement regarding the Brownfields Property. Upon
review of the BPA with respect to the requirements of the Brownfields Property Reuse Act of 1997,
DEQ has determined that this project is eligible for entry into the North Carolina Brownfields
Program (NCBP) and for continued evaluation for a Brownfields Agreement (BFA).
The next step in the BFA process will involve a detailed review of available environmental
and other relevant data to determine what is currently known about contamination at the Brownfields
Property, and what, if any, information gaps may exist that may require additional assessment. We
are in receipt of the following documents submitted with your BPA:
Report
Prepared By
Date
Phase I ESA
Geoscience Group
December 13, 2018
If available, historical Brownfields Property information from the files of DEQ's Division of Waste
Management will also be utilized during the evaluation process. Please forward any additional
information or data you may have or can acquire for our evaluation. This should include reports
from other DEQ agencies or regional offices. We will contact you regarding any additional
assessment that may be necessary to establish that the Brownfields Property is or can be made
suitable for the intended reuse, as required by statute.
Deprb�sd�a MarcelY�l brl�
North Carolina Department of Environmental Quality I Division of Waste Management
217 West Jones Street 1 1646 Mail Service Center I Raleigh, NDrth Caraltna 2709-lb46
N. Charlotte Presbyterian Church
July S, 2019
Page 2
According to the BPA, the intended redevelopment for the Brownfields Property is to
develop and expand the church related use of the property. Because risk management decisions
may vary depending on the nature of the redevelopment, it will be important that DEQ review
the locations of the various elements. Please forward any maps or drawings indicating these
details, even if they are only preliminary or conceptual.
Please note: pending execution of a final BFA, NCBP eligibility is provisional. The
protections a BFA offers the Prospective Developer are not in effect, unless and until, the BFA is
executed. If you occupy the Brownfields Property or operate or conduct activities at the
Brownfields Property that result in a release of regulated substances before a BFA has been
finalized for the Brownfields Property, you may be considered to have caused or contributed to
contamination at the Brownfields Property. Because an entity that could be considered to have
caused or contributed to contamination at the Brownfields Property cannot be a Prospective
Developer under the Act, your eligibility for participation in the NCBP would be placed in
jeopardy. Consult closely with your Project Manager regarding any planned site activities prior
to agreement finalization. You are cautioned to conduct all such operations and activities at the
Brownfields Property with great care not to cause a release of regulated substances at the
Brownfields Property that could jeopardize your eligibility for participation in the NCBP.
If a party other than Forest Hill Church will own the Brownfields Property at the conclusion of
the brownftelds process, the final document (which gets recorded at the register of deeds' office)
must be signed not only by Prospective Developer, but by that owner. Failure by the Prospective
Developer to ensure, by the time the BFA negotiations are complete, the willingness to sign of
any such party, and to provide DEQ the exact name, email address, telephone number, and US
mail address of the party (along with the signatory/signatory's tile in the case of an entity) will
delay, and could prevent, the BFA taking effect.
We are excited about the potential for public benefit offered by the reuse of the N.
Charlotte Presbyterian Church Site and look forward to working with you to advance this
brownfields redevelopment project. If you have questions about this correspondence or require
additional information, please feel free to contact the project manager Carolyn Mirinich by phone
at 704-661-0330, or by e-mail at carol yn.minnich(d�ncdenr.goW.
Sincerely,
Bruce Nicholson
Brownfields Program Manager
ec: Central Files, DEQ
Michael E. Scott, DEQ
Carolyn Minnich, DEQ
Amy Rickers, Johnston., Allison & Hord, P.A.
V
JQALLISON H RD
Amy L. Rickers
Attorney
WRITER'S E-MAIL ADDRESS:
arickers@jahlaw.com
WRITER'S DIRECT DIAL:
704-995-2253
April 16, 2020
Bruce Nicholson
Program Manager — Brownfield Program
North Carolina Department of Environmental Quality
Mail Service Center 1646
Raleigh, NC 27699-1646
Re: Refund of Brownfield Application Fee for BF#23039-19-060
Dear Mr. Nicholson:
I am writing on behalf of my client, Forest Hill Church (the Church). The Church applied
for acceptance and was deemed eligible for the Brownfield Program in 2019. Subsequent to that
notification, the Church submitted its $2,000 application fee.
In further review of the project the Brownfields group advised the Church it was, in fact,
not eligible for the Brownfield Program and that the UST program would be a more applicable
avenue for resolution of environmental concerns at the property. The Church has since been
working to seek resolution in this manner.
Given that the Church is a non-profit entity it is requesting that the application fee it has
paid be refunded as the Brownfield Program has determined the project is no longer eligible for
coverage in its program. Please deliver the refund, made out to Forest Hill Church, to:
Nick Dusenbury
Forest Hill Church
7224 Park Road
Charlotte, NC 28210
1065 East Morehead Street, Charlotte, NC 28204 Trr MERITAS' jahlaw.corn
SAW 31Meli W0L0,m0E
Mr. Nicholson
April 16, 2020
Page 2
Please let me know if you need any additional information in order to process this request.
The Church looks forward to receiving its refund at your earliest convenience.
Regards,
JOHNSTON, ALLISON & HORD, P.A.
Amy Rickers
Cc: Carolyn Minnich, via email: carolyn.minnich@ncdenr.gov
Appendix B
Certificate of Disposal, Non -Hazardous Waste Manifests, and Backfill
Documentation
hart F hickman
SMARTER ENVIRONMENTAL'GLUTIONS
�.�C:)
CORPORATION
1703 Vargrave Street
Winston-Salam, NC 27107
ph 33&725-5844
fax 33B-725-6244
CERTIFICATE OF DISPOSAL
Eva Corporation does hereby certify that 625 gallons of non -hazardous product
received on 2/1412022 from:
Generator: Ascent Real Estate Capital
Originating at: 719 E. 36" Street
Charlotte, NC
EC Waste ID #: 022222
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.ewncorp net TH E NEXT LEVEL.
EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 81800
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Site Address:
City/State: EE Contact:
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.n.?w-: -`ti?= %-_�.;.•'s .e.�=.F4` Ly M.. r wS F F.� Yk�"%'?r:,-. 7;._..�-k":' r<.:-3:83.^.i•h.i
u
.. S� o+:.! .a- s�.C. .. � � v�i .Y w .�.....qF 8. } � F.;rv-e^.� i � _ "^t a.. V s.•i �!eid � Yf�<,�Y� i . ..'u.J �� ns.F.� e x,�i K: ;•,�� .�. >t� �.� .MAY D�S:C l :TIQN��U� � a� ,�.,.�, ::�:�...,:x.r ::��.._� .. ���r�� ^ �.��!__ _ R_P� r'Q AIiTITY�J_1NE1:C Y T ..hv. .u..... ..:.-. a .... .. �.w-a...».-- .�.n..:....�.T•:+...,.:.:...,....x..,..-....k.s...�..-......i-... =: �Y.:..,...� Ffv-x -
Gross Weight (Ibs):
Empty Weight (lbs):
Net Weight (lbs):
Material:
adwct
Contaminant:
Quantity 9�_ Tons Drums Pails Sacs Yards Other: r�.f
r
.......,.�.-.,.�......r�::�.......a:n^_..r..5�o- ..,,, � � ..�a::x..:.r��..ID"� ,.•".•a:t:�n:�>�.sx�ri F•��"`;�tw�� :,.;�- n.;,.
Transporter: Phone:
Truck #: rWIaltiolm Contact: 336- 5--5844
Tony Usher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are In proper condition for transport
In commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility deAnate.
Driver Signature:
EVO CORPORATION
1 703 Vargrave Street
Winston-Salem, NC 27107
Date: allvhz
Evo Project #: (22222
Phone: 336 725-5W
Contact: Tony Disher
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina,
Facifi Signature:,,- Date: p9
white/Facility Canary/Invoice Goldenrod/Generator P
'Evo Corppmiion, �408
AME=.'Xf[3
CORPORATION
1703 VwUrave 5treat
Motori•Salem, SEC 27107
ph 338-725-6844
tax 335-725-6244
CERTIFICATE OF DISPOSAL
Evo Corporation does hereby certify that 25.86 tons of non -hazardous
contaminated material received on 2/24/2022 from:
Generator: Ascent Real Estate Capital
Originating at: 719 E. 36th Street
Charlotte, NC
EC Waste ID #: 022222
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.evocorp,net T HNEXT LEVEL.
EVO CORPORATION
1703 Vargrav'e Street, Winston-Salem, SIC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # {Manifest No.14161
GENERATOR INFORMATION
Generator: Ascent F4%d Estate Ckpital Phone:
Site Address:
City/State: Contact:
CWai otte, lu C act ,der
(MATERIAL DESCRIPTION / QUANTITY I WEIGHT
Gross Weight (lbs): _ .� Sa
Empty Weight (Ibs):
Net Weight (Ibs): 2, � { 700
Quantity V s
(Material:
Contaminant:
6ons Drums Pails Sacs Yards Other:
TR�t�S��RT�R INF®RfMATlOI4i =
Transporter:
a rro_n
Truck #: _ Q►_ _____
,I_
Contact: 336--725-5:844
' ny RGher
As the transparter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature: Date:,
FACILITY INFORMATION �1
BVO CIDrPOD-ration Evo Project * -- .222
1703 Vagr;ve fleet Phone: _
Istoxi Salcm IC 27107 Contact:
the carrier has delivered the materials described above to this facility, and I hereby accept this
Ireatrnent and/or disposal in a manner that has been authorized by the State of North Carolina.
�iture: Date: - -
White/Facility Canary/invoice Pink/Carder
EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Lead # Manifest No, 14162
GENERATOR INFORMATION
Ascent Baal Ek�te Capital 401-935-4802
Generator: Ascent
Site Address: 719 E 3151th St-
City/State: chaAo w, NC Contact: Caci Jam
MATERIAL DESCRIPTION f QUANTITY 1 WEIGHT ___1
Gross Weight (Ibs):�� �]
Empty Weight (Ibs):
Net Weight (lbs):
Quantity
Material:
Contaminant: _a
Elmatm,
`(`ens Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter: BVO OMPOratioa Phone: 6-725-5844-
Truck #: 3 0 — 4 e7' V Contact: Ihrim- 1-%a16.as-
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
deliverer to the facility designate.
Driver Signature.- Jr ®ate;,._.......
FACILITY INFORMATION
FerroQ)rporadon
Eye Project #: 2222
1703 Vugr"e street 336.72 5-5 84-4-
Phone: _
Wmeto -Salem 1U 27107 'o:ay Usher
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
F%70 CoToratimn,1008
Corporation
cal Ticket
. ........ ---- ---
Ti lis is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster,
:and when properly signed and sealed shall be prima facia e►ridence of the accuracy of the weight shown as prescribed by law.
Feb 24 2022�' 649 PUBLIC WEIGHMASTER
Tichet : 6546
Cust. Name: EVO
Truck IB: 30-698
Trailer IDS:
Reweigh Fee 2.00
Quilktrip 1044
2790 Lane St
Kannapal i s, NC 28083
Axle 1 211@0 1b
Axle 2 a 37300 lb
Axle 3 00 lb
Total c 58400 lb
N�A�iIY
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 2022
COREYALVERSON 41656
WEIGHMASTER OR
WEIGHER SIGNATURE zV(54
DIVA LESS SIGNED
DRIVER IN TRUCK U SS CHECKED HERE:
CERTIFICATE OF
WEIGHT & MEASURE
IMPRINT SEAL. HERE
fI F APPLICABL.Ej
FULL WEIGH
T1CXET N
(IF REWEIGH)
CorporationScale Ticket
:This Is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster,
`and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law.
Feb 24 2022 O L Z 7-ZZ.
PUBLIC WEIGHMASTER'S
Ticket 6545 CERTIFICATE OF
CuSt . Name: EU❑ WEIGHT & MEASURE
Track I D : 30-fi98
Trailer ID:
Weigh Fee: 12.50
[�uiktriA 11i344 aR� WP
2790 lane St N
Hannapo 1 i s, N6 28093 PUBLIC WEIGHMASTER
r ENSE EXPIRES JUNE 30, 2022
Axle ! : 19420 lb COREY ALVERSON 41656
HNIR e
Axle
Total
30660 lb
00 lb WEIGHMASTI 4R
ILb)'n ez_
50080 lb
WEIGHER SIGNATURE
INVALID UNLESS SIGNET]
DRIVER IN TRUCK UNLESS CHECKED HERE:
FULLWEIGH
TICKET it
[IF REWEIGH]
R.H. 199I-L ,
McGIRT
•� TRUCKING CO., INC.
13DO1 General Drive + Charlotte. NC 28273
Phone (7 4) 588-8527
CUSTOMER
JOB NAME — 5c�' -/7, ,
CUSTOMER'S
SIGNATURE
NDT RESPONSIBLE FOR OVERWEIGHT TICKETS OR FINES.
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Appendix C
Tank Disposal Certificate
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
_. .,. ph 335-725-5944
fax 336-725-a2"
'SANK DISPOSAL CERTIFICATE
Tank Owner: Ascent Real Estate Capital
Site Address: 719 E. 36th Street
Charlotte, NC
Description of Tanks:
Tank
Size of Tank
Contents
Number
1
1,000 Gallons
12 Fuel Oil
?
550 Gallons
42 Fuel Oil
3
550 Gallons
42 Fuel Oil
Transporter: Eva Corporation
EC Project M 022222
Disposal Certification:
Eva Corporation does hereby certify that the above named storage tanks were
transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem, NC for
proper disposal and recycling.
Signature
Thomas W. Hammett
CEO
Eva Corporation
►mw evocarpmet T E NEXT LEVEL.
Appendix D
Laboratory Analytical Report
qd
hart hickman
SMARTER ENVIRONMENTAL SOWT1ONS
aceAnalytical
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
February 22, 2022
Nathan O'Leary
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
RE: Project: CCW-006
Pace Project No.: 92588327
Dear Nathan O'Leary:
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
kevin.godwin@pacelabs.com
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 104
accAnafyfical
www, pa c ela b5-m m
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: CCW-006
Pace Project No.: 92588327
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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9800 Kincey Ave. Suite 100
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(704)875-9092
SAMPLE SUMMARY
Project: CCW-006
Pace Project No.: 92588327
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92588327001
UST-1
Solid
02/14/2214:30
02/15/2214:54
92588327002
UST-3
Solid
02/14/2214:55
02/15/2214:54
92588327003
UST-1-13
Solid
02/14/2215:25
02/15/2214:54
92588327004
UST-1-SW-F
Solid
02/14/2215:15
02/15/2214:54
92588327005
UST-1-SW-13
Solid
02/14/2215:35
02/15/2214:54
92588327006
UST-1-SW-R
Solid
02/14/2215:40
02/15/2214:54
92588327007
UST-1-SW-L
Solid
02/14/2215:50
02/15/2214:54
92588327008
UST-2-SW-L
Solid
02/14/2216:00
02/15/2214:54
92588327009
UST-2-13
Solid
02/14/2216:20
02/15/2214:54
92588327010
UST-2-SW-R
Solid
02/14/2216:10
02/15/2214:54
92588327011
UST-2-SW-13
Solid
02/14/2216:30
02/15/2214:54
92588327012
UST-2-SW-F
Solid
02/14/2216:40
02/15/2214:54
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CCW-006
92588327
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92588327001
UST-1
EPA 8015C
AP2
2
PASI-C
EPA 8015C
MAD
2
PASI-C
SW-846
KDF
1
PASI-C
92588327002
UST-3
EPA 8015C
AP2
2
PASI-C
EPA 8015C
MAD
2
PASI-C
SW-846
KDF
1
PASI-C
92588327003
UST-1-13
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327004
UST-1-SW-F
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327005
UST-1-SW-13
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327006
UST-1-SW-R
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327007
UST-1-SW-L
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327008
UST-2-SW-L
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327009
UST-2-13
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327010
UST-2-SW-R
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 104
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
CCW-006
Pace Project No.:
92588327
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
SW-846
KDF
1
PASI-C
92588327011
UST-2-SW-13
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92588327012
UST-2-SW-F
MADEP VPH
MAD
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 104
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1
Lab ID: 92588327001 Collected: 02/14/22 14:30 Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
838 mg/kg 15.4 10.9 2 02/15/22 22:51
02/16/22 17:24
C28)
Surrogates
n-Pentacosane (S)
55 % 32-130 2 02/15/22 22:51
02/16/22 17:24 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
146 mg/kg 12.9 3.3 1 02/16/22 12:47
02/16/22 19:24
Surrogates
4-Bromofluorobenzene (S)
138 % 66-131 1 02/16/22 12:47
02/16/22 19:24 460-00-4 S5
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
33.9 % 0.10 0.10 1
02/15/22 17:10 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
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(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-3
Lab ID: 92588327002 Collected: 02/14/22 14:55 Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
5.91 mg/kg 6.3 4.5 1 02/15/22 22:51
02/16/22 16:17
C28)
Surrogates
n-Pentacosane (S)
57 % 32-130 1 02/15/22 22:51
02/16/22 16:17 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
ND mg/kg 8.4 2.1 1 02/17/22 14:29
02/17/22 16:40
Surrogates
4-Bromofluorobenzene (S)
82 % 66-131 1 02/17/22 14:29
02/17/22 16:40 460-00-4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
20.2 % 0.10 0.10 1
02/15/22 17:10 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
Page 7 of 104
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-13 Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 16:29
Aliphatic(C09-C12)Adjusted
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 16:29
Aromatic (C09-C10)
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 16:29
Surrogates
4-Bromofluorobenzene (FID) (S)
89
%
70-130
1
02/16/22 13:41
02/16/22 16:29
460-00-4
4-Bromofluorobenzene (PID) (S)
76
%
70-130
1
02/16/22 13:41
02/16/22 16:29
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
483
170
1
02/16/22 11:33
02/17/22 11:34
83-32-9
Acenaphthylene
ND
ug/kg
483
170
1
02/16/22 11:33
02/17/22 11:34
208-96-8
Aniline
ND
ug/kg
483
189
1
02/16/22 11:33
02/17/22 11:34
62-53-3
Anthracene
ND
ug/kg
483
158
1
02/16/22 11:33
02/17/22 11:34
120-12-7
Benzo(a)anthracene
ND
ug/kg
483
161
1
02/16/22 11:33
02/17/22 11:34
56-55-3
Benzo(a)pyrene
ND
ug/kg
483
167
1
02/16/22 11:33
02/17/22 11:34
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
483
161
1
02/16/22 11:33
02/17/22 11:34
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
483
187
1
02/16/22 11:33
02/17/22 11:34
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
483
170
1
02/16/22 11:33
02/17/22 11:34
207-08-9
Benzoic Acid
ND
ug/kg
2420
1040
1
02/16/22 11:33
02/17/22 11:34
65-85-0
Benzyl alcohol
ND
ug/kg
966
366
1
02/16/22 11:33
02/17/22 11:34
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
483
186
1
02/16/22 11:33
02/17/22 11:34
101-55-3
Butylbenzylphthalate
ND
ug/kg
483
204
1
02/16/22 11:33
02/17/22 11:34
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
966
340
1
02/16/22 11:33
02/17/22 11:34
59-50-7
4-Chloroaniline
ND
ug/kg
966
379
1
02/16/22 11:33
02/17/22 11:34
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
483
201
1
02/16/22 11:33
02/17/22 11:34
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
483
182
1
02/16/22 11:33
02/17/22 11:34
111-44-4
2-Chloronaphthalene
ND
ug/kg
483
192
1
02/16/22 11:33
02/17/22 11:34
91-58-7
2-Chlorophenol
ND
ug/kg
483
182
1
02/16/22 11:33
02/17/22 11:34
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
483
180
1
02/16/22 11:33
02/17/22 11:34
7005-72-3
Chrysene
ND
ug/kg
483
176
1
02/16/22 11:33
02/17/22 11:34
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
483
186
1
02/16/22 11:33
02/17/22 11:34
53-70-3
Dibenzofuran
ND
ug/kg
483
174
1
02/16/22 11:33
02/17/22 11:34
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
483
174
1
02/16/22 11:33
02/17/22 11:34
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
483
171
1
02/16/22 11:33
02/17/22 11:34
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
483
185
1
02/16/22 11:33
02/17/22 11:34
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
966
327
1
02/16/22 11:33
02/17/22 11:34
91-94-1
2,4-Dichlorophenol
ND
ug/kg
483
189
1
02/16/22 11:33
02/17/22 11:34
120-83-2
Diethylphthalate
ND
ug/kg
483
177
1
02/16/22 11:33
02/17/22 11:34
84-66-2
2,4-Dimethylphenol
ND
ug/kg
483
201
1
02/16/22 11:33
02/17/22 11:34
105-67-9
Dimethylphthalate
ND
ug/kg
483
176
1
02/16/22 11:33
02/17/22 11:34
131-11-3
Di-n-butylphthalate
ND
ug/kg
483
163
1
02/16/22 11:33
02/17/22 11:34
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
966
451
1
02/16/22 11:33
02/17/22 11:34
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2420
1490
1
02/16/22 11:33
02/17/22 11:34
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
483
186
1
02/16/22 11:33
02/17/22 11:34
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
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Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-13 Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
483
177
1
02/16/22 11:33
02/17/22 11:34
606-20-2
Di-n-octylphthalate
ND
ug/kg
483
190
1
02/16/22 11:33
02/17/22 11:34
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
483
187
1
02/16/22 11:33
02/17/22 11:34
117-81-7
Fluoranthene
ND
ug/kg
483
165
1
02/16/22 11:33
02/17/22 11:34
206-44-0
Fluorene
ND
ug/kg
483
170
1
02/16/22 11:33
02/17/22 11:34
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
483
209
1
02/16/22 11:33
02/17/22 11:34
87-68-3
Hexachlorobenzene
ND
ug/kg
483
189
1
02/16/22 11:33
02/17/22 11:34
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
483
277
1
02/16/22 11:33
02/17/22 11:34
77-47-4
Hexachloroethane
ND
ug/kg
483
185
1
02/16/22 11:33
02/17/22 11:34
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
483
190
1
02/16/22 11:33
02/17/22 11:34
193-39-5
Isophorone
ND
ug/kg
483
215
1
02/16/22 11:33
02/17/22 11:34
78-59-1
1-Methylnaphthalene
ND
ug/kg
483
170
1
02/16/22 11:33
02/17/22 11:34
90-12-0
2-Methylnaphthalene
ND
ug/kg
483
193
1
02/16/22 11:33
02/17/22 11:34
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
483
198
1
02/16/22 11:33
02/17/22 11:34
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
483
195
1
02/16/22 11:33
02/17/22 11:34
15831-10-4
Naphthalene
ND
ug/kg
483
164
1
02/16/22 11:33
02/17/22 11:34
91-20-3
2-Nitroaniline
ND
ug/kg
2420
395
1
02/16/22 11:33
02/17/22 11:34
88-74-4
3-Nitroaniline
ND
ug/kg
2420
379
1
02/16/22 11:33
02/17/22 11:34
99-09-2
4-Nitroaniline
ND
ug/kg
966
368
1
02/16/22 11:33
02/17/22 11:34
100-01-6
Nitrobenzene
ND
ug/kg
483
224
1
02/16/22 11:33
02/17/22 11:34
98-95-3
2-Nitrophenol
ND
ug/kg
483
209
1
02/16/22 11:33
02/17/22 11:34
88-75-5
4-Nitrophenol
ND
ug/kg
2420
934
1
02/16/22 11:33
02/17/22 11:34
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
483
163
1
02/16/22 11:33
02/17/22 11:34
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
483
182
1
02/16/22 11:33
02/17/22 11:34
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
483
171
1
02/16/22 11:33
02/17/22 11:34
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
483
230
1
02/16/22 11:33
02/17/22 11:34
108-60-1
Pentachlorophenol
ND
ug/kg
966
473
1
02/16/22 11:33
02/17/22 11:34
87-86-5
Phenanthrene
ND
ug/kg
483
158
1
02/16/22 11:33
02/17/22 11:34
85-01-8
Phenol
ND
ug/kg
483
215
1
02/16/22 11:33
02/17/22 11:34
108-95-2
Pyrene
ND
ug/kg
483
196
1
02/16/22 11:33
02/17/22 11:34
129-00-0
Pyridine
ND
ug/kg
483
152
1
02/16/22 11:33
02/17/22 11:34
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
483
190
1
02/16/22 11:33
02/17/22 11:34
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
483
221
1
02/16/22 11:33
02/17/22 11:34
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
483
199
1
02/16/22 11:33
02/17/22 11:34
88-06-2
Surrogates
Nitrobenzene-d5 (S)
64
%
21-130
1
02/16/22 11:33
02/17/22 11:34
4165-60-0
2-Fluorobiphenyl (S)
52
%
19-130
1
02/16/22 11:33
02/17/22 11:34
321-60-8
Terphenyl-d14 (S)
46
%
15-130
1
02/16/22 11:33
02/17/22 11:34
1718-51-0
Phenol-d6 (S)
65
%
18-130
1
02/16/22 11:33
02/17/22 11:34
13127-88-3
2-Fluorophenol (S)
62
%
18-130
1
02/16/22 11:33
02/17/22 11:34
367-12-4
2,4,6-Tribromophenol (S)
63
%
18-130
1
02/16/22 11:33
02/17/22 11:34
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-B Lab ID: 92588327003 Collected: 02/14/22 15:25 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
233
74.7
1
02/15/22 21:19
02/17/22 17:12
67-64-1
Benzene
6.9J
ug/kg
11.6
4.6
1
02/15/22 21:19
02/17/22 17:12
71-43-2
Bromobenzene
ND
ug/kg
11.6
3.8
1
02/15/22 21:19
02/17/22 17:12
108-86-1
Bromochloromethane
ND
ug/kg
11.6
3.4
1
02/15/22 21:19
02/17/22 17:12
74-97-5
Bromodichloromethane
ND
ug/kg
11.6
4.5
1
02/15/22 21:19
02/17/22 17:12
75-27-4
Bromoform
ND
ug/kg
11.6
4.1
1
02/15/22 21:19
02/17/22 17:12
75-25-2
Bromomethane
ND
ug/kg
23.3
18.4
1
02/15/22 21:19
02/17/22 17:12
74-83-9
2-Butanone (MEK)
ND
ug/kg
233
55.9
1
02/15/22 21:19
02/17/22 17:12
78-93-3
n-Butylbenzene
ND
ug/kg
11.6
5.5
1
02/15/22 21:19
02/17/22 17:12
104-51-8
sec-Butylbenzene
ND
ug/kg
11.6
5.1
1
02/15/22 21:19
02/17/22 17:12
135-98-8
tert-Butyl benzene
ND
ug/kg
11.6
4.1
1
02/15/22 21:19
02/17/22 17:12
98-06-6
Carbon tetrachloride
ND
ug/kg
11.6
4.4
1
02/15/22 21:19
02/17/22 17:12
56-23-5
Chlorobenzene
ND
ug/kg
11.6
2.2
1
02/15/22 21:19
02/17/22 17:12
108-90-7
Chloroethane
ND
ug/kg
23.3
9.0
1
02/15/22 21:19
02/17/22 17:12
75-00-3
Chloroform
ND
ug/kg
11.6
7.1
1
02/15/22 21:19
02/17/22 17:12
67-66-3
Chloromethane
ND
ug/kg
23.3
9.8
1
02/15/22 21:19
02/17/22 17:12
74-87-3
2-Chlorotoluene
ND
ug/kg
11.6
4.1
1
02/15/22 21:19
02/17/22 17:12
95-49-8
4-Chlorotoluene
ND
ug/kg
11.6
2.1
1
02/15/22 21:19
02/17/22 17:12
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
11.6
4.5
1
02/15/22 21:19
02/17/22 17:12
96-12-8
Dibromochloromethane
ND
ug/kg
11.6
6.5
1
02/15/22 21:19
02/17/22 17:12
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
11.6
5.1
1
02/15/22 21:19
02/17/22 17:12
106-93-4
Dibromomethane
ND
ug/kg
11.6
2.5
1
02/15/22 21:19
02/17/22 17:12
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
11.6
4.2
1
02/15/22 21:19
02/17/22 17:12
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
11.6
3.6
1
02/15/22 21:19
02/17/22 17:12
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
11.6
3.0
1
02/15/22 21:19
02/17/22 17:12
106-46-7
Dichlorodifluoromethane
ND
ug/kg
23.3
5.1
1
02/15/22 21:19
02/17/22 17:12
75-71-8
1,1-Dichloroethane
ND
ug/kg
11.6
4.8
1
02/15/22 21:19
02/17/22 17:12
75-34-3
1,2-Dichloroethane
ND
ug/kg
11.6
7.7
1
02/15/22 21:19
02/17/22 17:12
107-06-2
1,1-Dichloroethene
ND
ug/kg
11.6
4.8
1
02/15/22 21:19
02/17/22 17:12
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
11.6
4.0
1
02/15/22 21:19
02/17/22 17:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
11.6
4.1
1
02/15/22 21:19
02/17/22 17:12
156-60-5
1,2-Dichloropropane
ND
ug/kg
11.6
3.5
1
02/15/22 21:19
02/17/22 17:12
78-87-5
1,3-Dichloropropane
ND
ug/kg
11.6
3.6
1
02/15/22 21:19
02/17/22 17:12
142-28-9
2,2-Dichloropropane
ND
ug/kg
11.6
3.8
1
02/15/22 21:19
02/17/22 17:12
594-20-7
1,1-Dichloropropene
ND
ug/kg
11.6
5.6
1
02/15/22 21:19
02/17/22 17:12
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
11.6
3.2
1
02/15/22 21:19
02/17/22 17:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
11.6
4.0
1
02/15/22 21:19
02/17/22 17:12
10061-02-6
Diisopropyl ether
ND
ug/kg
11.6
3.1
1
02/15/22 21:19
02/17/22 17:12
108-20-3
Ethylbenzene
6.OJ
ug/kg
11.6
5.4
1
02/15/22 21:19
02/17/22 17:12
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
23.3
19.0
1
02/15/22 21:19
02/17/22 17:12
87-68-3
2-Hexanone
ND
ug/kg
116
11.2
1
02/15/22 21:19
02/17/22 17:12
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
11.6
4.0
1
02/15/22 21:19
02/17/22 17:12
98-82-8
p-Isopropyltoluene
ND
ug/kg
11.6
5.7
1
02/15/22 21:19
02/17/22 17:12
99-87-6
Methylene Chloride
ND
ug/kg
46.6
31.9
1
02/15/22 21:19
02/17/22 17:12
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
M1
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-13
Lab ID:
92588327003
Collected:
02/14/22
15:25
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
116
11.2
1
02/15/22 21:19
02/17/22 17:12
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
11.6
4.4
1
02/15/22 21:19
02/17/22 17:12
1634-04-4
Naphthalene
17.7
ug/kg
11.6
6.1
1
02/15/22 21:19
02/17/22 17:12
91-20-3
n-Propylbenzene
ND
ug/kg
11.6
4.1
1
02/15/22 21:19
02/17/22 17:12
103-65-1
Styrene
ND
ug/kg
11.6
3.1
1
02/15/22 21:19
02/17/22 17:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
11.6
4.5
1
02/15/22 21:19
02/17/22 17:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
11.6
3.1
1
02/15/22 21:19
02/17/22 17:12
79-34-5
Tetrachloroethene
ND
ug/kg
11.6
3.7
1
02/15/22 21:19
02/17/22 17:12
127-18-4
Toluene
19.7
ug/kg
11.6
3.3
1
02/15/22 21:19
02/17/22 17:12
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
11.6
9.4
1
02/15/22 21:19
02/17/22 17:12
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
11.6
9.8
1
02/15/22 21:19
02/17/22 17:12
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
11.6
6.1
1
02/15/22 21:19
02/17/22 17:12
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
11.6
3.9
1
02/15/22 21:19
02/17/22 17:12
79-00-5
Trichloroethene
ND
ug/kg
11.6
3.0
1
02/15/22 21:19
02/17/22 17:12
79-01-6
Trichlorofluoromethane
ND
ug/kg
11.6
6.4
1
02/15/22 21:19
02/17/22 17:12
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
11.6
5.9
1
02/15/22 21:19
02/17/22 17:12
96-18-4 M1
1,2,4-Trimethylbenzene
6.1J
ug/kg
11.6
3.2
1
02/15/22 21:19
02/17/22 17:12
95-63-6
1,3,5-Trimethyl benzene
ND
ug/kg
11.6
3.9
1
02/15/22 21:19
02/17/22 17:12
108-67-8
Vinyl acetate
ND
ug/kg
116
8.5
1
02/15/22 21:19
02/17/22 17:12
108-05-4
Vinyl chloride
ND
ug/kg
23.3
5.9
1
02/15/22 21:19
02/17/22 17:12
75-01-4 v2
Xylene (Total)
17AJ
ug/kg
23.3
6.6
1
02/15/22 21:19
02/17/22 17:12
1330-20-7
m&p-Xylene
11.3J
ug/kg
23.3
8.0
1
02/15/22 21:19
02/17/22 17:12
179601-23-1
o-Xylene
6.2J
ug/kg
11.6
5.1
1
02/15/22 21:19
02/17/22 17:12
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 17:12
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
02/15/22 21:19
02/17/22 17:12
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
02/15/22 21:19
02/17/22 17:12
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
30.8
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
4.6
4.6
1
02/16/22 13:41
02/16/22 16:58
Aliphatic(C09-C12)Adjusted
ND
mg/kg
4.6
4.6
1
02/16/22 13:41
02/16/22 16:58
Aromatic (C09-C10)
ND
mg/kg
4.6
4.6
1
02/16/22 13:41
02/16/22 16:58
Surrogates
4-Bromofluorobenzene (FID) (S)
95
%
70-130
1
02/16/22 13:41
02/16/22 16:58
460-00-4
4-Bromofluorobenzene (PID) (S)
81
%
70-130
1
02/16/22 13:41
02/16/22 16:58
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
453
159
1
02/16/22 11:33
02/17/22 12:01
83-32-9
Acenaphthylene
ND
ug/kg
453
159
1
02/16/22 11:33
02/17/22 12:01
208-96-8
Aniline
ND
ug/kg
453
177
1
02/16/22 11:33
02/17/22 12:01
62-53-3
Anthracene
ND
ug/kg
453
148
1
02/16/22 11:33
02/17/22 12:01
120-12-7
Benzo(a)anthracene
ND
ug/kg
453
151
1
02/16/22 11:33
02/17/22 12:01
56-55-3
Benzo(a)pyrene
ND
ug/kg
453
157
1
02/16/22 11:33
02/17/22 12:01
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
453
151
1
02/16/22 11:33
02/17/22 12:01
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
453
176
1
02/16/22 11:33
02/17/22 12:01
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
453
159
1
02/16/22 11:33
02/17/22 12:01
207-08-9
Benzoic Acid
ND
ug/kg
2270
973
1
02/16/22 11:33
02/17/22 12:01
65-85-0
Benzyl alcohol
ND
ug/kg
906
343
1
02/16/22 11:33
02/17/22 12:01
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
453
174
1
02/16/22 11:33
02/17/22 12:01
101-55-3
Butylbenzylphthalate
ND
ug/kg
453
191
1
02/16/22 11:33
02/17/22 12:01
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
906
319
1
02/16/22 11:33
02/17/22 12:01
59-50-7
4-Chloroaniline
ND
ug/kg
906
356
1
02/16/22 11:33
02/17/22 12:01
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
453
188
1
02/16/22 11:33
02/17/22 12:01
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
453
170
1
02/16/22 11:33
02/17/22 12:01
111-44-4
2-Chloronaphthalene
ND
ug/kg
453
180
1
02/16/22 11:33
02/17/22 12:01
91-58-7
2-Chlorophenol
ND
ug/kg
453
170
1
02/16/22 11:33
02/17/22 12:01
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
453
169
1
02/16/22 11:33
02/17/22 12:01
7005-72-3
Chrysene
ND
ug/kg
453
165
1
02/16/22 11:33
02/17/22 12:01
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
453
174
1
02/16/22 11:33
02/17/22 12:01
53-70-3
Dibenzofuran
ND
ug/kg
453
163
1
02/16/22 11:33
02/17/22 12:01
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
453
163
1
02/16/22 11:33
02/17/22 12:01
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
453
161
1
02/16/22 11:33
02/17/22 12:01
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
453
173
1
02/16/22 11:33
02/17/22 12:01
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
906
306
1
02/16/22 11:33
02/17/22 12:01
91-94-1
2,4-Dichlorophenol
ND
ug/kg
453
177
1
02/16/22 11:33
02/17/22 12:01
120-83-2
Diethylphthalate
ND
ug/kg
453
166
1
02/16/22 11:33
02/17/22 12:01
84-66-2
2,4-Dimethylphenol
ND
ug/kg
453
188
1
02/16/22 11:33
02/17/22 12:01
105-67-9
Dimethylphthalate
ND
ug/kg
453
165
1
02/16/22 11:33
02/17/22 12:01
131-11-3
Di-n-butylphthalate
ND
ug/kg
453
152
1
02/16/22 11:33
02/17/22 12:01
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
906
423
1
02/16/22 11:33
02/17/22 12:01
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2270
1400
1
02/16/22 11:33
02/17/22 12:01
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
453
174
1
02/16/22 11:33
02/17/22 12:01
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
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Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
453
166
1
02/16/22 11:33
02/17/22 12:01
606-20-2
Di-n-octylphthalate
ND
ug/kg
453
178
1
02/16/22 11:33
02/17/22 12:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
453
176
1
02/16/22 11:33
02/17/22 12:01
117-81-7
Fluoranthene
ND
ug/kg
453
155
1
02/16/22 11:33
02/17/22 12:01
206-44-0
Fluorene
ND
ug/kg
453
159
1
02/16/22 11:33
02/17/22 12:01
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
453
196
1
02/16/22 11:33
02/17/22 12:01
87-68-3
Hexachlorobenzene
ND
ug/kg
453
177
1
02/16/22 11:33
02/17/22 12:01
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
453
259
1
02/16/22 11:33
02/17/22 12:01
77-47-4
Hexachloroethane
ND
ug/kg
453
173
1
02/16/22 11:33
02/17/22 12:01
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
453
178
1
02/16/22 11:33
02/17/22 12:01
193-39-5
Isophorone
ND
ug/kg
453
202
1
02/16/22 11:33
02/17/22 12:01
78-59-1
1-Methylnaphthalene
ND
ug/kg
453
159
1
02/16/22 11:33
02/17/22 12:01
90-12-0
2-Methylnaphthalene
ND
ug/kg
453
181
1
02/16/22 11:33
02/17/22 12:01
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
453
185
1
02/16/22 11:33
02/17/22 12:01
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
453
183
1
02/16/22 11:33
02/17/22 12:01
15831-10-4
Naphthalene
ND
ug/kg
453
154
1
02/16/22 11:33
02/17/22 12:01
91-20-3
2-Nitroaniline
ND
ug/kg
2270
371
1
02/16/22 11:33
02/17/22 12:01
88-74-4
3-Nitroaniline
ND
ug/kg
2270
356
1
02/16/22 11:33
02/17/22 12:01
99-09-2
4-Nitroaniline
ND
ug/kg
906
345
1
02/16/22 11:33
02/17/22 12:01
100-01-6
Nitrobenzene
ND
ug/kg
453
210
1
02/16/22 11:33
02/17/22 12:01
98-95-3
2-Nitrophenol
ND
ug/kg
453
196
1
02/16/22 11:33
02/17/22 12:01
88-75-5
4-Nitrophenol
ND
ug/kg
2270
876
1
02/16/22 11:33
02/17/22 12:01
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
453
152
1
02/16/22 11:33
02/17/22 12:01
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
453
170
1
02/16/22 11:33
02/17/22 12:01
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
453
161
1
02/16/22 11:33
02/17/22 12:01
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
453
216
1
02/16/22 11:33
02/17/22 12:01
108-60-1
Pentachlorophenol
ND
ug/kg
906
443
1
02/16/22 11:33
02/17/22 12:01
87-86-5
Phenanthrene
ND
ug/kg
453
148
1
02/16/22 11:33
02/17/22 12:01
85-01-8
Phenol
ND
ug/kg
453
202
1
02/16/22 11:33
02/17/22 12:01
108-95-2
Pyrene
ND
ug/kg
453
184
1
02/16/22 11:33
02/17/22 12:01
129-00-0
Pyridine
ND
ug/kg
453
143
1
02/16/22 11:33
02/17/22 12:01
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
453
178
1
02/16/22 11:33
02/17/22 12:01
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
453
207
1
02/16/22 11:33
02/17/22 12:01
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
453
187
1
02/16/22 11:33
02/17/22 12:01
88-06-2
Surrogates
Nitrobenzene-d5 (S)
64
%
21-130
1
02/16/22 11:33
02/17/22 12:01
4165-60-0
2-Fluorobiphenyl (S)
57
%
19-130
1
02/16/22 11:33
02/17/22 12:01
321-60-8
Terphenyl-d14 (S)
59
%
15-130
1
02/16/22 11:33
02/17/22 12:01
1718-51-0
Phenol-d6 (S)
64
%
18-130
1
02/16/22 11:33
02/17/22 12:01
13127-88-3
2-Fluorophenol (S)
63
%
18-130
1
02/16/22 11:33
02/17/22 12:01
367-12-4
2,4,6-Tribromophenol (S)
65
%
18-130
1
02/16/22 11:33
02/17/22 12:01
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-F Lab ID: 92588327004 Collected: 02/14/22 15:15 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
189
60.6
1
02/15/22 21:19
02/17/22 17:30
67-64-1
Benzene
ND
ug/kg
9.4
3.8
1
02/15/22 21:19
02/17/22 17:30
71-43-2
Bromobenzene
ND
ug/kg
9.4
3.1
1
02/15/22 21:19
02/17/22 17:30
108-86-1
Bromochloromethane
ND
ug/kg
9.4
2.8
1
02/15/22 21:19
02/17/22 17:30
74-97-5
Bromodichloromethane
ND
ug/kg
9.4
3.6
1
02/15/22 21:19
02/17/22 17:30
75-27-4
Bromoform
ND
ug/kg
9.4
3.3
1
02/15/22 21:19
02/17/22 17:30
75-25-2
Bromomethane
ND
ug/kg
18.9
14.9
1
02/15/22 21:19
02/17/22 17:30
74-83-9
2-Butanone (MEK)
ND
ug/kg
189
45.3
1
02/15/22 21:19
02/17/22 17:30
78-93-3
n-Butylbenzene
ND
ug/kg
9.4
4.5
1
02/15/22 21:19
02/17/22 17:30
104-51-8
sec-Butylbenzene
ND
ug/kg
9.4
4.2
1
02/15/22 21:19
02/17/22 17:30
135-98-8
tert-Butyl benzene
ND
ug/kg
9.4
3.4
1
02/15/22 21:19
02/17/22 17:30
98-06-6
Carbon tetrachloride
ND
ug/kg
9.4
3.5
1
02/15/22 21:19
02/17/22 17:30
56-23-5
Chlorobenzene
ND
ug/kg
9.4
1.8
1
02/15/22 21:19
02/17/22 17:30
108-90-7
Chloroethane
ND
ug/kg
18.9
7.3
1
02/15/22 21:19
02/17/22 17:30
75-00-3
Chloroform
ND
ug/kg
9.4
5.7
1
02/15/22 21:19
02/17/22 17:30
67-66-3
Chloromethane
ND
ug/kg
18.9
7.9
1
02/15/22 21:19
02/17/22 17:30
74-87-3
2-Chlorotoluene
ND
ug/kg
9.4
3.3
1
02/15/22 21:19
02/17/22 17:30
95-49-8
4-Chlorotoluene
ND
ug/kg
9.4
1.7
1
02/15/22 21:19
02/17/22 17:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.4
3.7
1
02/15/22 21:19
02/17/22 17:30
96-12-8
Dibromochloromethane
ND
ug/kg
9.4
5.3
1
02/15/22 21:19
02/17/22 17:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.4
4.2
1
02/15/22 21:19
02/17/22 17:30
106-93-4
Dibromomethane
ND
ug/kg
9.4
2.0
1
02/15/22 21:19
02/17/22 17:30
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.4
3.4
1
02/15/22 21:19
02/17/22 17:30
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.4
2.9
1
02/15/22 21:19
02/17/22 17:30
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.4
2.5
1
02/15/22 21:19
02/17/22 17:30
106-46-7
Dichlorodifluoromethane
ND
ug/kg
18.9
4.1
1
02/15/22 21:19
02/17/22 17:30
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.4
3.9
1
02/15/22 21:19
02/17/22 17:30
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.4
6.2
1
02/15/22 21:19
02/17/22 17:30
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.4
3.9
1
02/15/22 21:19
02/17/22 17:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.4
3.2
1
02/15/22 21:19
02/17/22 17:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.4
3.3
1
02/15/22 21:19
02/17/22 17:30
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.4
2.8
1
02/15/22 21:19
02/17/22 17:30
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.4
2.9
1
02/15/22 21:19
02/17/22 17:30
142-28-9
2,2-Dichloropropane
ND
ug/kg
9.4
3.1
1
02/15/22 21:19
02/17/22 17:30
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.4
4.5
1
02/15/22 21:19
02/17/22 17:30
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.4
2.6
1
02/15/22 21:19
02/17/22 17:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.4
3.2
1
02/15/22 21:19
02/17/22 17:30
10061-02-6
Diisopropyl ether
ND
ug/kg
9.4
2.5
1
02/15/22 21:19
02/17/22 17:30
108-20-3
Ethylbenzene
10.8
ug/kg
9.4
4.4
1
02/15/22 21:19
02/17/22 17:30
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
18.9
15.4
1
02/15/22 21:19
02/17/22 17:30
87-68-3
2-Hexanone
ND
ug/kg
94.4
9.1
1
02/15/22 21:19
02/17/22 17:30
591-78-6
Isopropylbenzene (Cumene)
6.5J
ug/kg
9.4
3.2
1
02/15/22 21:19
02/17/22 17:30
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.4
4.6
1
02/15/22 21:19
02/17/22 17:30
99-87-6
Methylene Chloride
ND
ug/kg
37.8
25.9
1
02/15/22 21:19
02/17/22 17:30
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-F
Lab ID:
92588327004
Collected:
02/14/22
15:15
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
94.4
9.1
1
02/15/22 21:19
02/17/22 17:30
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.4
3.5
1
02/15/22 21:19
02/17/22 17:30
1634-04-4
Naphthalene
65.3
ug/kg
9.4
5.0
1
02/15/22 21:19
02/17/22 17:30
91-20-3
n-Propylbenzene
ND
ug/kg
9.4
3.4
1
02/15/22 21:19
02/17/22 17:30
103-65-1
Styrene
ND
ug/kg
9.4
2.5
1
02/15/22 21:19
02/17/22 17:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
9.4
3.6
1
02/15/22 21:19
02/17/22 17:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
9.4
2.5
1
02/15/22 21:19
02/17/22 17:30
79-34-5
Tetrachloroethene
ND
ug/kg
9.4
3.0
1
02/15/22 21:19
02/17/22 17:30
127-18-4
Toluene
8.9J
ug/kg
9.4
2.7
1
02/15/22 21:19
02/17/22 17:30
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
9.4
7.6
1
02/15/22 21:19
02/17/22 17:30
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
9.4
7.9
1
02/15/22 21:19
02/17/22 17:30
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
9.4
4.9
1
02/15/22 21:19
02/17/22 17:30
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
9.4
3.1
1
02/15/22 21:19
02/17/22 17:30
79-00-5
Trichloroethene
ND
ug/kg
9.4
2.4
1
02/15/22 21:19
02/17/22 17:30
79-01-6
Trichlorofluoromethane
ND
ug/kg
9.4
5.2
1
02/15/22 21:19
02/17/22 17:30
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
9.4
4.8
1
02/15/22 21:19
02/17/22 17:30
96-18-4
1,2,4-Trimethylbenzene
76.6
ug/kg
9.4
2.6
1
02/15/22 21:19
02/17/22 17:30
95-63-6
1,3,5-Trimethylbenzene
32.7
ug/kg
9.4
3.2
1
02/15/22 21:19
02/17/22 17:30
108-67-8
Vinyl acetate
ND
ug/kg
94.4
6.9
1
02/15/22 21:19
02/17/22 17:30
108-05-4
Vinyl chloride
ND
ug/kg
18.9
4.8
1
02/15/22 21:19
02/17/22 17:30
75-01-4 v2
Xylene (Total)
53.6
ug/kg
18.9
5.4
1
02/15/22 21:19
02/17/22 17:30
1330-20-7
m&p-Xylene
34.9
ug/kg
18.9
6.5
1
02/15/22 21:19
02/17/22 17:30
179601-23-1
o-Xylene
18.7
ug/kg
9.4
4.2
1
02/15/22 21:19
02/17/22 17:30
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 17:30
2037-26-5
4-Bromofluorobenzene (S)
104
%
69-134
1
02/15/22 21:19
02/17/22 17:30
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/15/22 21:19
02/17/22 17:30
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
26.4
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-13 Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
5.2
5.2
1
02/16/22 13:41
02/16/22 17:27
Aliphatic(C09-C12)Adjusted
ND
mg/kg
5.2
5.2
1
02/16/22 13:41
02/16/22 17:27
Aromatic (C09-C10)
ND
mg/kg
5.2
5.2
1
02/16/22 13:41
02/16/22 17:27
Surrogates
4-Bromofluorobenzene (FID) (S)
95
%
70-130
1
02/16/22 13:41
02/16/22 17:27
460-00-4
4-Bromofluorobenzene (PID) (S)
81
%
70-130
1
02/16/22 13:41
02/16/22 17:27
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
478
168
1
02/16/22 11:33
02/17/22 12:28
83-32-9
Acenaphthylene
ND
ug/kg
478
168
1
02/16/22 11:33
02/17/22 12:28
208-96-8
Aniline
ND
ug/kg
478
187
1
02/16/22 11:33
02/17/22 12:28
62-53-3
Anthracene
ND
ug/kg
478
156
1
02/16/22 11:33
02/17/22 12:28
120-12-7
Benzo(a)anthracene
ND
ug/kg
478
159
1
02/16/22 11:33
02/17/22 12:28
56-55-3
Benzo(a)pyrene
ND
ug/kg
478
165
1
02/16/22 11:33
02/17/22 12:28
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
478
159
1
02/16/22 11:33
02/17/22 12:28
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
478
185
1
02/16/22 11:33
02/17/22 12:28
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
478
168
1
02/16/22 11:33
02/17/22 12:28
207-08-9
Benzoic Acid
ND
ug/kg
2390
1030
1
02/16/22 11:33
02/17/22 12:28
65-85-0
Benzyl alcohol
ND
ug/kg
956
362
1
02/16/22 11:33
02/17/22 12:28
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
478
184
1
02/16/22 11:33
02/17/22 12:28
101-55-3
Butylbenzylphthalate
ND
ug/kg
478
201
1
02/16/22 11:33
02/17/22 12:28
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
956
336
1
02/16/22 11:33
02/17/22 12:28
59-50-7
4-Chloroaniline
ND
ug/kg
956
375
1
02/16/22 11:33
02/17/22 12:28
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
478
198
1
02/16/22 11:33
02/17/22 12:28
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
478
180
1
02/16/22 11:33
02/17/22 12:28
111-44-4
2-Chloronaphthalene
ND
ug/kg
478
190
1
02/16/22 11:33
02/17/22 12:28
91-58-7
2-Chlorophenol
ND
ug/kg
478
180
1
02/16/22 11:33
02/17/22 12:28
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
478
178
1
02/16/22 11:33
02/17/22 12:28
7005-72-3
Chrysene
ND
ug/kg
478
174
1
02/16/22 11:33
02/17/22 12:28
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
478
184
1
02/16/22 11:33
02/17/22 12:28
53-70-3
Dibenzofuran
ND
ug/kg
478
172
1
02/16/22 11:33
02/17/22 12:28
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
478
172
1
02/16/22 11:33
02/17/22 12:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
478
169
1
02/16/22 11:33
02/17/22 12:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
478
183
1
02/16/22 11:33
02/17/22 12:28
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
956
323
1
02/16/22 11:33
02/17/22 12:28
91-94-1
2,4-Dichlorophenol
ND
ug/kg
478
187
1
02/16/22 11:33
02/17/22 12:28
120-83-2
Diethylphthalate
ND
ug/kg
478
175
1
02/16/22 11:33
02/17/22 12:28
84-66-2
2,4-Dimethylphenol
ND
ug/kg
478
198
1
02/16/22 11:33
02/17/22 12:28
105-67-9
Dimethylphthalate
ND
ug/kg
478
174
1
02/16/22 11:33
02/17/22 12:28
131-11-3
Di-n-butylphthalate
ND
ug/kg
478
161
1
02/16/22 11:33
02/17/22 12:28
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
956
446
1
02/16/22 11:33
02/17/22 12:28
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2390
1480
1
02/16/22 11:33
02/17/22 12:28
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
478
184
1
02/16/22 11:33
02/17/22 12:28
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-13 Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
478
175
1
02/16/22 11:33
02/17/22 12:28
606-20-2
Di-n-octylphthalate
ND
ug/kg
478
188
1
02/16/22 11:33
02/17/22 12:28
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
478
185
1
02/16/22 11:33
02/17/22 12:28
117-81-7
Fluoranthene
ND
ug/kg
478
164
1
02/16/22 11:33
02/17/22 12:28
206-44-0
Fluorene
ND
ug/kg
478
168
1
02/16/22 11:33
02/17/22 12:28
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
478
207
1
02/16/22 11:33
02/17/22 12:28
87-68-3
Hexachlorobenzene
ND
ug/kg
478
187
1
02/16/22 11:33
02/17/22 12:28
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
478
274
1
02/16/22 11:33
02/17/22 12:28
77-47-4
Hexachloroethane
ND
ug/kg
478
183
1
02/16/22 11:33
02/17/22 12:28
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
478
188
1
02/16/22 11:33
02/17/22 12:28
193-39-5
Isophorone
ND
ug/kg
478
213
1
02/16/22 11:33
02/17/22 12:28
78-59-1
1-Methylnaphthalene
ND
ug/kg
478
168
1
02/16/22 11:33
02/17/22 12:28
90-12-0
2-Methylnaphthalene
ND
ug/kg
478
191
1
02/16/22 11:33
02/17/22 12:28
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
478
196
1
02/16/22 11:33
02/17/22 12:28
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
478
193
1
02/16/22 11:33
02/17/22 12:28
15831-10-4
Naphthalene
ND
ug/kg
478
162
1
02/16/22 11:33
02/17/22 12:28
91-20-3
2-Nitroaniline
ND
ug/kg
2390
391
1
02/16/22 11:33
02/17/22 12:28
88-74-4
3-Nitroaniline
ND
ug/kg
2390
375
1
02/16/22 11:33
02/17/22 12:28
99-09-2
4-Nitroaniline
ND
ug/kg
956
364
1
02/16/22 11:33
02/17/22 12:28
100-01-6
Nitrobenzene
ND
ug/kg
478
222
1
02/16/22 11:33
02/17/22 12:28
98-95-3
2-Nitrophenol
ND
ug/kg
478
207
1
02/16/22 11:33
02/17/22 12:28
88-75-5
4-Nitrophenol
ND
ug/kg
2390
924
1
02/16/22 11:33
02/17/22 12:28
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
478
161
1
02/16/22 11:33
02/17/22 12:28
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
478
180
1
02/16/22 11:33
02/17/22 12:28
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
478
169
1
02/16/22 11:33
02/17/22 12:28
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
478
227
1
02/16/22 11:33
02/17/22 12:28
108-60-1
Pentachlorophenol
ND
ug/kg
956
468
1
02/16/22 11:33
02/17/22 12:28
87-86-5
Phenanthrene
ND
ug/kg
478
156
1
02/16/22 11:33
02/17/22 12:28
85-01-8
Phenol
ND
ug/kg
478
213
1
02/16/22 11:33
02/17/22 12:28
108-95-2
Pyrene
ND
ug/kg
478
194
1
02/16/22 11:33
02/17/22 12:28
129-00-0
Pyridine
ND
ug/kg
478
151
1
02/16/22 11:33
02/17/22 12:28
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
478
188
1
02/16/22 11:33
02/17/22 12:28
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
478
219
1
02/16/22 11:33
02/17/22 12:28
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
478
197
1
02/16/22 11:33
02/17/22 12:28
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
21-130
1
02/16/22 11:33
02/17/22 12:28
4165-60-0
2-Fluorobiphenyl (S)
55
%
19-130
1
02/16/22 11:33
02/17/22 12:28
321-60-8
Terphenyl-d14 (S)
54
%
15-130
1
02/16/22 11:33
02/17/22 12:28
1718-51-0
Phenol-d6 (S)
63
%
18-130
1
02/16/22 11:33
02/17/22 12:28
13127-88-3
2-Fluorophenol (S)
61
%
18-130
1
02/16/22 11:33
02/17/22 12:28
367-12-4
2,4,6-Tribromophenol (S)
62
%
18-130
1
02/16/22 11:33
02/17/22 12:28
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-B Lab ID: 92588327005 Collected: 02/14/22 15:35 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
277
88.9
1
02/15/22 21:19
02/17/22 18:05
67-64-1
Benzene
ND
ug/kg
13.8
5.5
1
02/15/22 21:19
02/17/22 18:05
71-43-2
Bromobenzene
ND
ug/kg
13.8
4.5
1
02/15/22 21:19
02/17/22 18:05
108-86-1
Bromochloromethane
ND
ug/kg
13.8
4.1
1
02/15/22 21:19
02/17/22 18:05
74-97-5
Bromodichloromethane
ND
ug/kg
13.8
5.3
1
02/15/22 21:19
02/17/22 18:05
75-27-4
Bromoform
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 18:05
75-25-2
Bromomethane
ND
ug/kg
27.7
21.9
1
02/15/22 21:19
02/17/22 18:05
74-83-9
2-Butanone (MEK)
ND
ug/kg
277
66.5
1
02/15/22 21:19
02/17/22 18:05
78-93-3
n-Butylbenzene
ND
ug/kg
13.8
6.5
1
02/15/22 21:19
02/17/22 18:05
104-51-8
sec-Butylbenzene
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 18:05
135-98-8
tert-Butyl benzene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 18:05
98-06-6
Carbon tetrachloride
ND
ug/kg
13.8
5.2
1
02/15/22 21:19
02/17/22 18:05
56-23-5
Chlorobenzene
ND
ug/kg
13.8
2.7
1
02/15/22 21:19
02/17/22 18:05
108-90-7
Chloroethane
ND
ug/kg
27.7
10.7
1
02/15/22 21:19
02/17/22 18:05
75-00-3
Chloroform
ND
ug/kg
13.8
8.4
1
02/15/22 21:19
02/17/22 18:05
67-66-3
Chloromethane
ND
ug/kg
27.7
11.6
1
02/15/22 21:19
02/17/22 18:05
74-87-3
2-Chlorotoluene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 18:05
95-49-8
4-Chlorotoluene
ND
ug/kg
13.8
2.5
1
02/15/22 21:19
02/17/22 18:05
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
13.8
5.4
1
02/15/22 21:19
02/17/22 18:05
96-12-8
Dibromochloromethane
ND
ug/kg
13.8
7.8
1
02/15/22 21:19
02/17/22 18:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 18:05
106-93-4
Dibromomethane
ND
ug/kg
13.8
3.0
1
02/15/22 21:19
02/17/22 18:05
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
13.8
5.0
1
02/15/22 21:19
02/17/22 18:05
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
13.8
4.3
1
02/15/22 21:19
02/17/22 18:05
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 18:05
106-46-7
Dichlorodifluoromethane
ND
ug/kg
27.7
6.0
1
02/15/22 21:19
02/17/22 18:05
75-71-8
1,1-Dichloroethane
ND
ug/kg
13.8
5.7
1
02/15/22 21:19
02/17/22 18:05
75-34-3
1,2-Dichloroethane
ND
ug/kg
13.8
9.2
1
02/15/22 21:19
02/17/22 18:05
107-06-2
1,1-Dichloroethene
ND
ug/kg
13.8
5.7
1
02/15/22 21:19
02/17/22 18:05
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
13.8
4.7
1
02/15/22 21:19
02/17/22 18:05
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
13.8
4.8
1
02/15/22 21:19
02/17/22 18:05
156-60-5
1,2-Dichloropropane
ND
ug/kg
13.8
4.2
1
02/15/22 21:19
02/17/22 18:05
78-87-5
1,3-Dichloropropane
ND
ug/kg
13.8
4.3
1
02/15/22 21:19
02/17/22 18:05
142-28-9
2,2-Dichloropropane
ND
ug/kg
13.8
4.5
1
02/15/22 21:19
02/17/22 18:05
594-20-7
1,1-Dichloropropene
ND
ug/kg
13.8
6.6
1
02/15/22 21:19
02/17/22 18:05
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
13.8
3.8
1
02/15/22 21:19
02/17/22 18:05
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
13.8
4.8
1
02/15/22 21:19
02/17/22 18:05
10061-02-6
Diisopropyl ether
ND
ug/kg
13.8
3.7
1
02/15/22 21:19
02/17/22 18:05
108-20-3
Ethylbenzene
ND
ug/kg
13.8
6.5
1
02/15/22 21:19
02/17/22 18:05
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
27.7
22.7
1
02/15/22 21:19
02/17/22 18:05
87-68-3
2-Hexanone
ND
ug/kg
138
13.3
1
02/15/22 21:19
02/17/22 18:05
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
13.8
4.7
1
02/15/22 21:19
02/17/22 18:05
98-82-8
p-Isopropyltoluene
ND
ug/kg
13.8
6.8
1
02/15/22 21:19
02/17/22 18:05
99-87-6
Methylene Chloride
ND
ug/kg
55.4
37.9
1
02/15/22 21:19
02/17/22 18:05
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-13
Lab ID:
92588327005
Collected:
02/14/22
15:35
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
138
13.3
1
02/15/22 21:19
02/17/22 18:05
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
13.8
5.2
1
02/15/22 21:19
02/17/22 18:05
1634-04-4
Naphthalene
ND
ug/kg
13.8
7.3
1
02/15/22 21:19
02/17/22 18:05
91-20-3
n-Propylbenzene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 18:05
103-65-1
Styrene
ND
ug/kg
13.8
3.7
1
02/15/22 21:19
02/17/22 18:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
13.8
5.3
1
02/15/22 21:19
02/17/22 18:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
13.8
3.7
1
02/15/22 21:19
02/17/22 18:05
79-34-5
Tetrachloroethene
ND
ug/kg
13.8
4.4
1
02/15/22 21:19
02/17/22 18:05
127-18-4
Toluene
ND
ug/kg
13.8
3.9
1
02/15/22 21:19
02/17/22 18:05
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
13.8
11.2
1
02/15/22 21:19
02/17/22 18:05
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
13.8
11.6
1
02/15/22 21:19
02/17/22 18:05
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
13.8
7.2
1
02/15/22 21:19
02/17/22 18:05
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
13.8
4.6
1
02/15/22 21:19
02/17/22 18:05
79-00-5
Trichloroethene
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 18:05
79-01-6
Trichlorofluoromethane
ND
ug/kg
13.8
7.6
1
02/15/22 21:19
02/17/22 18:05
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
13.8
7.0
1
02/15/22 21:19
02/17/22 18:05
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
13.8
3.8
1
02/15/22 21:19
02/17/22 18:05
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
13.8
4.7
1
02/15/22 21:19
02/17/22 18:05
108-67-8
Vinyl acetate
ND
ug/kg
138
10.1
1
02/15/22 21:19
02/17/22 18:05
108-05-4
Vinyl chloride
ND
ug/kg
27.7
7.0
1
02/15/22 21:19
02/17/22 18:05
75-01-4 v2
Xylene (Total)
ND
ug/kg
27.7
7.9
1
02/15/22 21:19
02/17/22 18:05
1330-20-7
m&p-Xylene
ND
ug/kg
27.7
9.5
1
02/15/22 21:19
02/17/22 18:05
179601-23-1
o-Xylene
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 18:05
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
02/15/22 21:19
02/17/22 18:05
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
02/15/22 21:19
02/17/22 18:05
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 18:05
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
30.3
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
Page 19 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
6.7
6.7
1
02/16/22 13:41
02/16/22 17:55
Aliphatic(C09-C12)Adjusted
ND
mg/kg
6.7
6.7
1
02/16/22 13:41
02/16/22 17:55
Aromatic (C09-C10)
ND
mg/kg
6.7
6.7
1
02/16/22 13:41
02/16/22 17:55
Surrogates
4-Bromofluorobenzene (FID) (S)
96
%
70-130
1
02/16/22 13:41
02/16/22 17:55
460-00-4
4-Bromofluorobenzene (PID) (S)
82
%
70-130
1
02/16/22 13:41
02/16/22 17:55
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
484
170
1
02/16/22 11:33
02/17/22 12:55
83-32-9
Acenaphthylene
ND
ug/kg
484
170
1
02/16/22 11:33
02/17/22 12:55
208-96-8
Aniline
ND
ug/kg
484
189
1
02/16/22 11:33
02/17/22 12:55
62-53-3
Anthracene
ND
ug/kg
484
158
1
02/16/22 11:33
02/17/22 12:55
120-12-7
Benzo(a)anthracene
ND
ug/kg
484
161
1
02/16/22 11:33
02/17/22 12:55
56-55-3
Benzo(a)pyrene
ND
ug/kg
484
167
1
02/16/22 11:33
02/17/22 12:55
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
484
161
1
02/16/22 11:33
02/17/22 12:55
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
484
188
1
02/16/22 11:33
02/17/22 12:55
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
484
170
1
02/16/22 11:33
02/17/22 12:55
207-08-9
Benzoic Acid
ND
ug/kg
2420
1040
1
02/16/22 11:33
02/17/22 12:55
65-85-0
Benzyl alcohol
ND
ug/kg
967
366
1
02/16/22 11:33
02/17/22 12:55
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
484
186
1
02/16/22 11:33
02/17/22 12:55
101-55-3
Butylbenzylphthalate
ND
ug/kg
484
204
1
02/16/22 11:33
02/17/22 12:55
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
967
340
1
02/16/22 11:33
02/17/22 12:55
59-50-7
4-Chloroaniline
ND
ug/kg
967
380
1
02/16/22 11:33
02/17/22 12:55
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
484
201
1
02/16/22 11:33
02/17/22 12:55
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
484
182
1
02/16/22 11:33
02/17/22 12:55
111-44-4
2-Chloronaphthalene
ND
ug/kg
484
192
1
02/16/22 11:33
02/17/22 12:55
91-58-7
2-Chlorophenol
ND
ug/kg
484
182
1
02/16/22 11:33
02/17/22 12:55
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
484
180
1
02/16/22 11:33
02/17/22 12:55
7005-72-3
Chrysene
ND
ug/kg
484
176
1
02/16/22 11:33
02/17/22 12:55
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
484
186
1
02/16/22 11:33
02/17/22 12:55
53-70-3
Dibenzofuran
ND
ug/kg
484
174
1
02/16/22 11:33
02/17/22 12:55
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
484
174
1
02/16/22 11:33
02/17/22 12:55
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
484
172
1
02/16/22 11:33
02/17/22 12:55
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
484
185
1
02/16/22 11:33
02/17/22 12:55
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
967
327
1
02/16/22 11:33
02/17/22 12:55
91-94-1
2,4-Dichlorophenol
ND
ug/kg
484
189
1
02/16/22 11:33
02/17/22 12:55
120-83-2
Diethylphthalate
ND
ug/kg
484
177
1
02/16/22 11:33
02/17/22 12:55
84-66-2
2,4-Dimethylphenol
ND
ug/kg
484
201
1
02/16/22 11:33
02/17/22 12:55
105-67-9
Dimethylphthalate
ND
ug/kg
484
176
1
02/16/22 11:33
02/17/22 12:55
131-11-3
Di-n-butylphthalate
ND
ug/kg
484
163
1
02/16/22 11:33
02/17/22 12:55
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
967
451
1
02/16/22 11:33
02/17/22 12:55
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2420
1500
1
02/16/22 11:33
02/17/22 12:55
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
484
186
1
02/16/22 11:33
02/17/22 12:55
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
484
177
1
02/16/22 11:33
02/17/22 12:55
606-20-2
Di-n-octylphthalate
ND
ug/kg
484
191
1
02/16/22 11:33
02/17/22 12:55
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
484
188
1
02/16/22 11:33
02/17/22 12:55
117-81-7
Fluoranthene
ND
ug/kg
484
166
1
02/16/22 11:33
02/17/22 12:55
206-44-0
Fluorene
ND
ug/kg
484
170
1
02/16/22 11:33
02/17/22 12:55
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
484
210
1
02/16/22 11:33
02/17/22 12:55
87-68-3
Hexachlorobenzene
ND
ug/kg
484
189
1
02/16/22 11:33
02/17/22 12:55
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
484
277
1
02/16/22 11:33
02/17/22 12:55
77-47-4
Hexachloroethane
ND
ug/kg
484
185
1
02/16/22 11:33
02/17/22 12:55
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
484
191
1
02/16/22 11:33
02/17/22 12:55
193-39-5
Isophorone
ND
ug/kg
484
215
1
02/16/22 11:33
02/17/22 12:55
78-59-1
1-Methylnaphthalene
ND
ug/kg
484
170
1
02/16/22 11:33
02/17/22 12:55
90-12-0
2-Methylnaphthalene
ND
ug/kg
484
193
1
02/16/22 11:33
02/17/22 12:55
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
484
198
1
02/16/22 11:33
02/17/22 12:55
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
484
195
1
02/16/22 11:33
02/17/22 12:55
15831-10-4
Naphthalene
ND
ug/kg
484
164
1
02/16/22 11:33
02/17/22 12:55
91-20-3
2-Nitroaniline
ND
ug/kg
2420
396
1
02/16/22 11:33
02/17/22 12:55
88-74-4
3-Nitroaniline
ND
ug/kg
2420
380
1
02/16/22 11:33
02/17/22 12:55
99-09-2
4-Nitroaniline
ND
ug/kg
967
368
1
02/16/22 11:33
02/17/22 12:55
100-01-6
Nitrobenzene
ND
ug/kg
484
224
1
02/16/22 11:33
02/17/22 12:55
98-95-3
2-Nitrophenol
ND
ug/kg
484
210
1
02/16/22 11:33
02/17/22 12:55
88-75-5
4-Nitrophenol
ND
ug/kg
2420
935
1
02/16/22 11:33
02/17/22 12:55
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
484
163
1
02/16/22 11:33
02/17/22 12:55
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
484
182
1
02/16/22 11:33
02/17/22 12:55
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
484
172
1
02/16/22 11:33
02/17/22 12:55
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
484
230
1
02/16/22 11:33
02/17/22 12:55
108-60-1
Pentachlorophenol
ND
ug/kg
967
473
1
02/16/22 11:33
02/17/22 12:55
87-86-5
Phenanthrene
ND
ug/kg
484
158
1
02/16/22 11:33
02/17/22 12:55
85-01-8
Phenol
ND
ug/kg
484
215
1
02/16/22 11:33
02/17/22 12:55
108-95-2
Pyrene
ND
ug/kg
484
196
1
02/16/22 11:33
02/17/22 12:55
129-00-0
Pyridine
ND
ug/kg
484
152
1
02/16/22 11:33
02/17/22 12:55
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
484
191
1
02/16/22 11:33
02/17/22 12:55
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
484
221
1
02/16/22 11:33
02/17/22 12:55
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
484
199
1
02/16/22 11:33
02/17/22 12:55
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
21-130
1
02/16/22 11:33
02/17/22 12:55
4165-60-0
2-Fluorobiphenyl (S)
52
%
19-130
1
02/16/22 11:33
02/17/22 12:55
321-60-8
Terphenyl-d14 (S)
52
%
15-130
1
02/16/22 11:33
02/17/22 12:55
1718-51-0
Phenol-d6 (S)
61
%
18-130
1
02/16/22 11:33
02/17/22 12:55
13127-88-3
2-Fluorophenol (S)
59
%
18-130
1
02/16/22 11:33
02/17/22 12:55
367-12-4
2,4,6-Tribromophenol (S)
53
%
18-130
1
02/16/22 11:33
02/17/22 12:55
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-R Lab ID: 92588327006 Collected: 02/14/22 15:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
207
66.6
1
02/15/22 21:19
02/17/22 18:23
67-64-1
Benzene
ND
ug/kg
10.4
4.1
1
02/15/22 21:19
02/17/22 18:23
71-43-2
Bromobenzene
ND
ug/kg
10.4
3.4
1
02/15/22 21:19
02/17/22 18:23
108-86-1
Bromochloromethane
ND
ug/kg
10.4
3.1
1
02/15/22 21:19
02/17/22 18:23
74-97-5
Bromodichloromethane
ND
ug/kg
10.4
4.0
1
02/15/22 21:19
02/17/22 18:23
75-27-4
Bromoform
ND
ug/kg
10.4
3.7
1
02/15/22 21:19
02/17/22 18:23
75-25-2
Bromomethane
ND
ug/kg
20.7
16.4
1
02/15/22 21:19
02/17/22 18:23
74-83-9
2-Butanone (MEK)
ND
ug/kg
207
49.8
1
02/15/22 21:19
02/17/22 18:23
78-93-3
n-Butylbenzene
ND
ug/kg
10.4
4.9
1
02/15/22 21:19
02/17/22 18:23
104-51-8
sec-Butylbenzene
ND
ug/kg
10.4
4.6
1
02/15/22 21:19
02/17/22 18:23
135-98-8
tert-Butyl benzene
ND
ug/kg
10.4
3.7
1
02/15/22 21:19
02/17/22 18:23
98-06-6
Carbon tetrachloride
ND
ug/kg
10.4
3.9
1
02/15/22 21:19
02/17/22 18:23
56-23-5
Chlorobenzene
ND
ug/kg
10.4
2.0
1
02/15/22 21:19
02/17/22 18:23
108-90-7
Chloroethane
ND
ug/kg
20.7
8.0
1
02/15/22 21:19
02/17/22 18:23
75-00-3
Chloroform
ND
ug/kg
10.4
6.3
1
02/15/22 21:19
02/17/22 18:23
67-66-3
Chloromethane
ND
ug/kg
20.7
8.7
1
02/15/22 21:19
02/17/22 18:23
74-87-3
2-Chlorotoluene
ND
ug/kg
10.4
3.7
1
02/15/22 21:19
02/17/22 18:23
95-49-8
4-Chlorotoluene
ND
ug/kg
10.4
1.8
1
02/15/22 21:19
02/17/22 18:23
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
10.4
4.0
1
02/15/22 21:19
02/17/22 18:23
96-12-8
Dibromochloromethane
ND
ug/kg
10.4
5.8
1
02/15/22 21:19
02/17/22 18:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
10.4
4.6
1
02/15/22 21:19
02/17/22 18:23
106-93-4
Dibromomethane
ND
ug/kg
10.4
2.2
1
02/15/22 21:19
02/17/22 18:23
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
10.4
3.7
1
02/15/22 21:19
02/17/22 18:23
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10.4
3.2
1
02/15/22 21:19
02/17/22 18:23
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10.4
2.7
1
02/15/22 21:19
02/17/22 18:23
106-46-7
Dichlorodifluoromethane
ND
ug/kg
20.7
4.5
1
02/15/22 21:19
02/17/22 18:23
75-71-8
1,1-Dichloroethane
ND
ug/kg
10.4
4.3
1
02/15/22 21:19
02/17/22 18:23
75-34-3
1,2-Dichloroethane
ND
ug/kg
10.4
6.9
1
02/15/22 21:19
02/17/22 18:23
107-06-2
1,1-Dichloroethene
ND
ug/kg
10.4
4.3
1
02/15/22 21:19
02/17/22 18:23
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
10.4
3.5
1
02/15/22 21:19
02/17/22 18:23
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
10.4
3.6
1
02/15/22 21:19
02/17/22 18:23
156-60-5
1,2-Dichloropropane
ND
ug/kg
10.4
3.1
1
02/15/22 21:19
02/17/22 18:23
78-87-5
1,3-Dichloropropane
ND
ug/kg
10.4
3.2
1
02/15/22 21:19
02/17/22 18:23
142-28-9
2,2-Dichloropropane
ND
ug/kg
10.4
3.4
1
02/15/22 21:19
02/17/22 18:23
594-20-7
1,1-Dichloropropene
ND
ug/kg
10.4
5.0
1
02/15/22 21:19
02/17/22 18:23
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
10.4
2.8
1
02/15/22 21:19
02/17/22 18:23
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
10.4
3.6
1
02/15/22 21:19
02/17/22 18:23
10061-02-6
Diisopropyl ether
ND
ug/kg
10.4
2.8
1
02/15/22 21:19
02/17/22 18:23
108-20-3
Ethylbenzene
ND
ug/kg
10.4
4.8
1
02/15/22 21:19
02/17/22 18:23
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
20.7
17.0
1
02/15/22 21:19
02/17/22 18:23
87-68-3
2-Hexanone
ND
ug/kg
104
10.0
1
02/15/22 21:19
02/17/22 18:23
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
10.4
3.5
1
02/15/22 21:19
02/17/22 18:23
98-82-8
p-Isopropyltoluene
ND
ug/kg
10.4
5.1
1
02/15/22 21:19
02/17/22 18:23
99-87-6
Methylene Chloride
ND
ug/kg
41.5
28.4
1
02/15/22 21:19
02/17/22 18:23
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-R
Lab ID:
92588327006
Collected:
02/14/22
15:40
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
104
10.0
1
02/15/22 21:19
02/17/22 18:23
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
10.4
3.9
1
02/15/22 21:19
02/17/22 18:23
1634-04-4
Naphthalene
ND
ug/kg
10.4
5.5
1
02/15/22 21:19
02/17/22 18:23
91-20-3
n-Propylbenzene
ND
ug/kg
10.4
3.7
1
02/15/22 21:19
02/17/22 18:23
103-65-1
Styrene
ND
ug/kg
10.4
2.7
1
02/15/22 21:19
02/17/22 18:23
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
10.4
4.0
1
02/15/22 21:19
02/17/22 18:23
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
10.4
2.7
1
02/15/22 21:19
02/17/22 18:23
79-34-5
Tetrachloroethene
ND
ug/kg
10.4
3.3
1
02/15/22 21:19
02/17/22 18:23
127-18-4
Toluene
8.9J
ug/kg
10.4
2.9
1
02/15/22 21:19
02/17/22 18:23
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
10.4
8.4
1
02/15/22 21:19
02/17/22 18:23
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
10.4
8.7
1
02/15/22 21:19
02/17/22 18:23
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
10.4
5.4
1
02/15/22 21:19
02/17/22 18:23
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
10.4
3.4
1
02/15/22 21:19
02/17/22 18:23
79-00-5
Trichloroethene
ND
ug/kg
10.4
2.7
1
02/15/22 21:19
02/17/22 18:23
79-01-6
Trichlorofluoromethane
ND
ug/kg
10.4
5.7
1
02/15/22 21:19
02/17/22 18:23
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
10.4
5.2
1
02/15/22 21:19
02/17/22 18:23
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
10.4
2.8
1
02/15/22 21:19
02/17/22 18:23
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
10.4
3.5
1
02/15/22 21:19
02/17/22 18:23
108-67-8
Vinyl acetate
ND
ug/kg
104
7.6
1
02/15/22 21:19
02/17/22 18:23
108-05-4
Vinyl chloride
ND
ug/kg
20.7
5.3
1
02/15/22 21:19
02/17/22 18:23
75-01-4 v2
Xylene (Total)
ND
ug/kg
20.7
5.9
1
02/15/22 21:19
02/17/22 18:23
1330-20-7
m&p-Xylene
ND
ug/kg
20.7
7.1
1
02/15/22 21:19
02/17/22 18:23
179601-23-1
o-Xylene
ND
ug/kg
10.4
4.6
1
02/15/22 21:19
02/17/22 18:23
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 18:23
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
02/15/22 21:19
02/17/22 18:23
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
02/15/22 21:19
02/17/22 18:23
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
30.9
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
6.2
6.2
1
02/16/22 13:41
02/16/22 18:24
Aliphatic(C09-C12)Adjusted
ND
mg/kg
6.2
6.2
1
02/16/22 13:41
02/16/22 18:24
Aromatic (C09-C10)
ND
mg/kg
6.2
6.2
1
02/16/22 13:41
02/16/22 18:24
Surrogates
4-Bromofluorobenzene (FID) (S)
96
%
70-130
1
02/16/22 13:41
02/16/22 18:24
460-00-4
4-Bromofluorobenzene (PID) (S)
83
%
70-130
1
02/16/22 13:41
02/16/22 18:24
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
465
164
1
02/16/22 11:33
02/17/22 13:21
83-32-9
Acenaphthylene
ND
ug/kg
465
164
1
02/16/22 11:33
02/17/22 13:21
208-96-8
Aniline
ND
ug/kg
465
182
1
02/16/22 11:33
02/17/22 13:21
62-53-3
Anthracene
ND
ug/kg
465
152
1
02/16/22 11:33
02/17/22 13:21
120-12-7
Benzo(a)anthracene
ND
ug/kg
465
155
1
02/16/22 11:33
02/17/22 13:21
56-55-3
Benzo(a)pyrene
ND
ug/kg
465
161
1
02/16/22 11:33
02/17/22 13:21
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
465
155
1
02/16/22 11:33
02/17/22 13:21
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
465
180
1
02/16/22 11:33
02/17/22 13:21
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
465
164
1
02/16/22 11:33
02/17/22 13:21
207-08-9
Benzoic Acid
ND
ug/kg
2330
999
1
02/16/22 11:33
02/17/22 13:21
65-85-0
Benzyl alcohol
ND
ug/kg
930
352
1
02/16/22 11:33
02/17/22 13:21
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
465
179
1
02/16/22 11:33
02/17/22 13:21
101-55-3
Butylbenzylphthalate
ND
ug/kg
465
196
1
02/16/22 11:33
02/17/22 13:21
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
930
327
1
02/16/22 11:33
02/17/22 13:21
59-50-7
4-Chloroaniline
ND
ug/kg
930
365
1
02/16/22 11:33
02/17/22 13:21
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
465
193
1
02/16/22 11:33
02/17/22 13:21
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
465
175
1
02/16/22 11:33
02/17/22 13:21
111-44-4
2-Chloronaphthalene
ND
ug/kg
465
185
1
02/16/22 11:33
02/17/22 13:21
91-58-7
2-Chlorophenol
ND
ug/kg
465
175
1
02/16/22 11:33
02/17/22 13:21
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
465
173
1
02/16/22 11:33
02/17/22 13:21
7005-72-3
Chrysene
ND
ug/kg
465
169
1
02/16/22 11:33
02/17/22 13:21
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
465
179
1
02/16/22 11:33
02/17/22 13:21
53-70-3
Dibenzofuran
ND
ug/kg
465
168
1
02/16/22 11:33
02/17/22 13:21
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
465
168
1
02/16/22 11:33
02/17/22 13:21
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
465
165
1
02/16/22 11:33
02/17/22 13:21
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
465
178
1
02/16/22 11:33
02/17/22 13:21
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
930
314
1
02/16/22 11:33
02/17/22 13:21
91-94-1
2,4-Dichlorophenol
ND
ug/kg
465
182
1
02/16/22 11:33
02/17/22 13:21
120-83-2
Diethylphthalate
ND
ug/kg
465
171
1
02/16/22 11:33
02/17/22 13:21
84-66-2
2,4-Dimethylphenol
ND
ug/kg
465
193
1
02/16/22 11:33
02/17/22 13:21
105-67-9
Dimethylphthalate
ND
ug/kg
465
169
1
02/16/22 11:33
02/17/22 13:21
131-11-3
Di-n-butylphthalate
ND
ug/kg
465
156
1
02/16/22 11:33
02/17/22 13:21
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
930
434
1
02/16/22 11:33
02/17/22 13:21
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2330
1440
1
02/16/22 11:33
02/17/22 13:21
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
465
179
1
02/16/22 11:33
02/17/22 13:21
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
465
171
1
02/16/22 11:33
02/17/22 13:21
606-20-2
Di-n-octylphthalate
ND
ug/kg
465
183
1
02/16/22 11:33
02/17/22 13:21
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
465
180
1
02/16/22 11:33
02/17/22 13:21
117-81-7
Fluoranthene
ND
ug/kg
465
159
1
02/16/22 11:33
02/17/22 13:21
206-44-0
Fluorene
ND
ug/kg
465
164
1
02/16/22 11:33
02/17/22 13:21
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
465
202
1
02/16/22 11:33
02/17/22 13:21
87-68-3
Hexachlorobenzene
ND
ug/kg
465
182
1
02/16/22 11:33
02/17/22 13:21
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
465
266
1
02/16/22 11:33
02/17/22 13:21
77-47-4
Hexachloroethane
ND
ug/kg
465
178
1
02/16/22 11:33
02/17/22 13:21
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
465
183
1
02/16/22 11:33
02/17/22 13:21
193-39-5
Isophorone
ND
ug/kg
465
207
1
02/16/22 11:33
02/17/22 13:21
78-59-1
1-Methylnaphthalene
ND
ug/kg
465
164
1
02/16/22 11:33
02/17/22 13:21
90-12-0
2-Methylnaphthalene
ND
ug/kg
465
186
1
02/16/22 11:33
02/17/22 13:21
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
465
190
1
02/16/22 11:33
02/17/22 13:21
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
465
187
1
02/16/22 11:33
02/17/22 13:21
15831-10-4
Naphthalene
ND
ug/kg
465
158
1
02/16/22 11:33
02/17/22 13:21
91-20-3
2-Nitroaniline
ND
ug/kg
2330
381
1
02/16/22 11:33
02/17/22 13:21
88-74-4
3-Nitroaniline
ND
ug/kg
2330
365
1
02/16/22 11:33
02/17/22 13:21
99-09-2
4-Nitroaniline
ND
ug/kg
930
354
1
02/16/22 11:33
02/17/22 13:21
100-01-6
Nitrobenzene
ND
ug/kg
465
216
1
02/16/22 11:33
02/17/22 13:21
98-95-3
2-Nitrophenol
ND
ug/kg
465
202
1
02/16/22 11:33
02/17/22 13:21
88-75-5
4-Nitrophenol
ND
ug/kg
2330
899
1
02/16/22 11:33
02/17/22 13:21
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
465
156
1
02/16/22 11:33
02/17/22 13:21
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
465
175
1
02/16/22 11:33
02/17/22 13:21
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
465
165
1
02/16/22 11:33
02/17/22 13:21
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
465
221
1
02/16/22 11:33
02/17/22 13:21
108-60-1
Pentachlorophenol
ND
ug/kg
930
455
1
02/16/22 11:33
02/17/22 13:21
87-86-5
Phenanthrene
ND
ug/kg
465
152
1
02/16/22 11:33
02/17/22 13:21
85-01-8
Phenol
ND
ug/kg
465
207
1
02/16/22 11:33
02/17/22 13:21
108-95-2
Pyrene
ND
ug/kg
465
189
1
02/16/22 11:33
02/17/22 13:21
129-00-0
Pyridine
ND
ug/kg
465
147
1
02/16/22 11:33
02/17/22 13:21
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
465
183
1
02/16/22 11:33
02/17/22 13:21
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
465
213
1
02/16/22 11:33
02/17/22 13:21
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
465
192
1
02/16/22 11:33
02/17/22 13:21
88-06-2
Surrogates
Nitrobenzene-d5 (S)
53
%
21-130
1
02/16/22 11:33
02/17/22 13:21
4165-60-0
2-Fluorobiphenyl (S)
50
%
19-130
1
02/16/22 11:33
02/17/22 13:21
321-60-8
Terphenyl-d14 (S)
48
%
15-130
1
02/16/22 11:33
02/17/22 13:21
1718-51-0
Phenol-d6 (S)
54
%
18-130
1
02/16/22 11:33
02/17/22 13:21
13127-88-3
2-Fluorophenol (S)
52
%
18-130
1
02/16/22 11:33
02/17/22 13:21
367-12-4
2,4,6-Tribromophenol (S)
54
%
18-130
1
02/16/22 11:33
02/17/22 13:21
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-L Lab ID: 92588327007 Collected: 02/14/22 15:50 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
218
69.9
1
02/15/22 21:19
02/17/22 18:40
67-64-1
Benzene
ND
ug/kg
10.9
4.3
1
02/15/22 21:19
02/17/22 18:40
71-43-2
Bromobenzene
ND
ug/kg
10.9
3.5
1
02/15/22 21:19
02/17/22 18:40
108-86-1
Bromochloromethane
ND
ug/kg
10.9
3.2
1
02/15/22 21:19
02/17/22 18:40
74-97-5
Bromodichloromethane
ND
ug/kg
10.9
4.2
1
02/15/22 21:19
02/17/22 18:40
75-27-4
Bromoform
ND
ug/kg
10.9
3.8
1
02/15/22 21:19
02/17/22 18:40
75-25-2
Bromomethane
ND
ug/kg
21.8
17.2
1
02/15/22 21:19
02/17/22 18:40
74-83-9
2-Butanone (MEK)
ND
ug/kg
218
52.2
1
02/15/22 21:19
02/17/22 18:40
78-93-3
n-Butylbenzene
ND
ug/kg
10.9
5.1
1
02/15/22 21:19
02/17/22 18:40
104-51-8
sec-Butylbenzene
ND
ug/kg
10.9
4.8
1
02/15/22 21:19
02/17/22 18:40
135-98-8
tert-Butyl benzene
ND
ug/kg
10.9
3.9
1
02/15/22 21:19
02/17/22 18:40
98-06-6
Carbon tetrachloride
ND
ug/kg
10.9
4.1
1
02/15/22 21:19
02/17/22 18:40
56-23-5
Chlorobenzene
ND
ug/kg
10.9
2.1
1
02/15/22 21:19
02/17/22 18:40
108-90-7
Chloroethane
ND
ug/kg
21.8
8.4
1
02/15/22 21:19
02/17/22 18:40
75-00-3
Chloroform
ND
ug/kg
10.9
6.6
1
02/15/22 21:19
02/17/22 18:40
67-66-3
Chloromethane
ND
ug/kg
21.8
9.1
1
02/15/22 21:19
02/17/22 18:40
74-87-3
2-Chlorotoluene
ND
ug/kg
10.9
3.9
1
02/15/22 21:19
02/17/22 18:40
95-49-8
4-Chlorotoluene
ND
ug/kg
10.9
1.9
1
02/15/22 21:19
02/17/22 18:40
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
10.9
4.2
1
02/15/22 21:19
02/17/22 18:40
96-12-8
Dibromochloromethane
ND
ug/kg
10.9
6.1
1
02/15/22 21:19
02/17/22 18:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
10.9
4.8
1
02/15/22 21:19
02/17/22 18:40
106-93-4
Dibromomethane
ND
ug/kg
10.9
2.3
1
02/15/22 21:19
02/17/22 18:40
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
10.9
3.9
1
02/15/22 21:19
02/17/22 18:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10.9
3.4
1
02/15/22 21:19
02/17/22 18:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10.9
2.8
1
02/15/22 21:19
02/17/22 18:40
106-46-7
Dichlorodifluoromethane
ND
ug/kg
21.8
4.7
1
02/15/22 21:19
02/17/22 18:40
75-71-8
1,1-Dichloroethane
ND
ug/kg
10.9
4.5
1
02/15/22 21:19
02/17/22 18:40
75-34-3
1,2-Dichloroethane
ND
ug/kg
10.9
7.2
1
02/15/22 21:19
02/17/22 18:40
107-06-2
1,1-Dichloroethene
ND
ug/kg
10.9
4.5
1
02/15/22 21:19
02/17/22 18:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
10.9
3.7
1
02/15/22 21:19
02/17/22 18:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
10.9
3.8
1
02/15/22 21:19
02/17/22 18:40
156-60-5
1,2-Dichloropropane
ND
ug/kg
10.9
3.3
1
02/15/22 21:19
02/17/22 18:40
78-87-5
1,3-Dichloropropane
ND
ug/kg
10.9
3.4
1
02/15/22 21:19
02/17/22 18:40
142-28-9
2,2-Dichloropropane
ND
ug/kg
10.9
3.5
1
02/15/22 21:19
02/17/22 18:40
594-20-7
1,1-Dichloropropene
ND
ug/kg
10.9
5.2
1
02/15/22 21:19
02/17/22 18:40
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
10.9
3.0
1
02/15/22 21:19
02/17/22 18:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
10.9
3.7
1
02/15/22 21:19
02/17/22 18:40
10061-02-6
Diisopropyl ether
ND
ug/kg
10.9
2.9
1
02/15/22 21:19
02/17/22 18:40
108-20-3
Ethylbenzene
ND
ug/kg
10.9
5.1
1
02/15/22 21:19
02/17/22 18:40
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
21.8
17.8
1
02/15/22 21:19
02/17/22 18:40
87-68-3
2-Hexanone
ND
ug/kg
109
10.5
1
02/15/22 21:19
02/17/22 18:40
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
10.9
3.7
1
02/15/22 21:19
02/17/22 18:40
98-82-8
p-Isopropyltoluene
ND
ug/kg
10.9
5.4
1
02/15/22 21:19
02/17/22 18:40
99-87-6
Methylene Chloride
ND
ug/kg
43.5
29.8
1
02/15/22 21:19
02/17/22 18:40
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-1-SW-L
Lab ID:
92588327007
Collected:
02/14/22
15:50
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
109
10.5
1
02/15/22 21:19
02/17/22 18:40
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
10.9
4.1
1
02/15/22 21:19
02/17/22 18:40
1634-04-4
Naphthalene
ND
ug/kg
10.9
5.7
1
02/15/22 21:19
02/17/22 18:40
91-20-3
n-Propylbenzene
ND
ug/kg
10.9
3.9
1
02/15/22 21:19
02/17/22 18:40
103-65-1
Styrene
ND
ug/kg
10.9
2.9
1
02/15/22 21:19
02/17/22 18:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
10.9
4.2
1
02/15/22 21:19
02/17/22 18:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
10.9
2.9
1
02/15/22 21:19
02/17/22 18:40
79-34-5
Tetrachloroethene
ND
ug/kg
10.9
3.4
1
02/15/22 21:19
02/17/22 18:40
127-18-4
Toluene
ND
ug/kg
10.9
3.1
1
02/15/22 21:19
02/17/22 18:40
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
10.9
8.8
1
02/15/22 21:19
02/17/22 18:40
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
10.9
9.1
1
02/15/22 21:19
02/17/22 18:40
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
10.9
5.7
1
02/15/22 21:19
02/17/22 18:40
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
10.9
3.6
1
02/15/22 21:19
02/17/22 18:40
79-00-5
Trichloroethene
ND
ug/kg
10.9
2.8
1
02/15/22 21:19
02/17/22 18:40
79-01-6
Trichlorofluoromethane
ND
ug/kg
10.9
6.0
1
02/15/22 21:19
02/17/22 18:40
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
10.9
5.5
1
02/15/22 21:19
02/17/22 18:40
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
10.9
3.0
1
02/15/22 21:19
02/17/22 18:40
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
10.9
3.7
1
02/15/22 21:19
02/17/22 18:40
108-67-8
Vinyl acetate
ND
ug/kg
109
7.9
1
02/15/22 21:19
02/17/22 18:40
108-05-4
Vinyl chloride
ND
ug/kg
21.8
5.5
1
02/15/22 21:19
02/17/22 18:40
75-01-4 v2
Xylene (Total)
ND
ug/kg
21.8
6.2
1
02/15/22 21:19
02/17/22 18:40
1330-20-7
m&p-Xylene
ND
ug/kg
21.8
7.4
1
02/15/22 21:19
02/17/22 18:40
179601-23-1
o-Xylene
ND
ug/kg
10.9
4.8
1
02/15/22 21:19
02/17/22 18:40
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
02/15/22 21:19
02/17/22 18:40
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
02/15/22 21:19
02/17/22 18:40
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
02/15/22 21:19
02/17/22 18:40
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
28.8
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
Page 27 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
4.7
4.7
1
02/16/22 13:41
02/16/22 18:53
Aliphatic(C09-C12)Adjusted
ND
mg/kg
4.7
4.7
1
02/16/22 13:41
02/16/22 18:53
Aromatic (C09-C10)
ND
mg/kg
4.7
4.7
1
02/16/22 13:41
02/16/22 18:53
Surrogates
4-Bromofluorobenzene (FID) (S)
99
%
70-130
1
02/16/22 13:41
02/16/22 18:53
460-00-4
4-Bromofluorobenzene (PID) (S)
85
%
70-130
1
02/16/22 13:41
02/16/22 18:53
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
438
154
1
02/16/22 11:33
02/17/22 13:48
83-32-9
Acenaphthylene
ND
ug/kg
438
154
1
02/16/22 11:33
02/17/22 13:48
208-96-8
Aniline
ND
ug/kg
438
171
1
02/16/22 11:33
02/17/22 13:48
62-53-3
Anthracene
ND
ug/kg
438
143
1
02/16/22 11:33
02/17/22 13:48
120-12-7
Benzo(a)anthracene
ND
ug/kg
438
146
1
02/16/22 11:33
02/17/22 13:48
56-55-3
Benzo(a)pyrene
ND
ug/kg
438
151
1
02/16/22 11:33
02/17/22 13:48
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
438
146
1
02/16/22 11:33
02/17/22 13:48
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
438
170
1
02/16/22 11:33
02/17/22 13:48
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
438
154
1
02/16/22 11:33
02/17/22 13:48
207-08-9
Benzoic Acid
ND
ug/kg
2190
941
1
02/16/22 11:33
02/17/22 13:48
65-85-0
Benzyl alcohol
ND
ug/kg
876
332
1
02/16/22 11:33
02/17/22 13:48
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
438
169
1
02/16/22 11:33
02/17/22 13:48
101-55-3
Butylbenzylphthalate
ND
ug/kg
438
184
1
02/16/22 11:33
02/17/22 13:48
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
876
308
1
02/16/22 11:33
02/17/22 13:48
59-50-7
4-Chloroaniline
ND
ug/kg
876
344
1
02/16/22 11:33
02/17/22 13:48
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
438
182
1
02/16/22 11:33
02/17/22 13:48
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
438
165
1
02/16/22 11:33
02/17/22 13:48
111-44-4
2-Chloronaphthalene
ND
ug/kg
438
174
1
02/16/22 11:33
02/17/22 13:48
91-58-7
2-Chlorophenol
ND
ug/kg
438
165
1
02/16/22 11:33
02/17/22 13:48
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
438
163
1
02/16/22 11:33
02/17/22 13:48
7005-72-3
Chrysene
ND
ug/kg
438
159
1
02/16/22 11:33
02/17/22 13:48
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
438
169
1
02/16/22 11:33
02/17/22 13:48
53-70-3
Dibenzofuran
ND
ug/kg
438
158
1
02/16/22 11:33
02/17/22 13:48
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
438
158
1
02/16/22 11:33
02/17/22 13:48
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
438
155
1
02/16/22 11:33
02/17/22 13:48
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
438
167
1
02/16/22 11:33
02/17/22 13:48
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
876
296
1
02/16/22 11:33
02/17/22 13:48
91-94-1
2,4-Dichlorophenol
ND
ug/kg
438
171
1
02/16/22 11:33
02/17/22 13:48
120-83-2
Diethylphthalate
ND
ug/kg
438
161
1
02/16/22 11:33
02/17/22 13:48
84-66-2
2,4-Dimethylphenol
ND
ug/kg
438
182
1
02/16/22 11:33
02/17/22 13:48
105-67-9
Dimethylphthalate
ND
ug/kg
438
159
1
02/16/22 11:33
02/17/22 13:48
131-11-3
Di-n-butylphthalate
ND
ug/kg
438
147
1
02/16/22 11:33
02/17/22 13:48
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
876
409
1
02/16/22 11:33
02/17/22 13:48
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2190
1350
1
02/16/22 11:33
02/17/22 13:48
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
438
169
1
02/16/22 11:33
02/17/22 13:48
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
438
161
1
02/16/22 11:33
02/17/22 13:48
606-20-2
Di-n-octylphthalate
ND
ug/kg
438
173
1
02/16/22 11:33
02/17/22 13:48
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
438
170
1
02/16/22 11:33
02/17/22 13:48
117-81-7
Fluoranthene
ND
ug/kg
438
150
1
02/16/22 11:33
02/17/22 13:48
206-44-0
Fluorene
ND
ug/kg
438
154
1
02/16/22 11:33
02/17/22 13:48
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
438
190
1
02/16/22 11:33
02/17/22 13:48
87-68-3
Hexachlorobenzene
ND
ug/kg
438
171
1
02/16/22 11:33
02/17/22 13:48
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
438
251
1
02/16/22 11:33
02/17/22 13:48
77-47-4
Hexachloroethane
ND
ug/kg
438
167
1
02/16/22 11:33
02/17/22 13:48
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
438
173
1
02/16/22 11:33
02/17/22 13:48
193-39-5
Isophorone
ND
ug/kg
438
195
1
02/16/22 11:33
02/17/22 13:48
78-59-1
1-Methylnaphthalene
ND
ug/kg
438
154
1
02/16/22 11:33
02/17/22 13:48
90-12-0
2-Methylnaphthalene
ND
ug/kg
438
175
1
02/16/22 11:33
02/17/22 13:48
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
438
179
1
02/16/22 11:33
02/17/22 13:48
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
438
177
1
02/16/22 11:33
02/17/22 13:48
15831-10-4
Naphthalene
ND
ug/kg
438
149
1
02/16/22 11:33
02/17/22 13:48
91-20-3
2-Nitroaniline
ND
ug/kg
2190
358
1
02/16/22 11:33
02/17/22 13:48
88-74-4
3-Nitroaniline
ND
ug/kg
2190
344
1
02/16/22 11:33
02/17/22 13:48
99-09-2
4-Nitroaniline
ND
ug/kg
876
333
1
02/16/22 11:33
02/17/22 13:48
100-01-6
Nitrobenzene
ND
ug/kg
438
203
1
02/16/22 11:33
02/17/22 13:48
98-95-3
2-Nitrophenol
ND
ug/kg
438
190
1
02/16/22 11:33
02/17/22 13:48
88-75-5
4-Nitrophenol
ND
ug/kg
2190
847
1
02/16/22 11:33
02/17/22 13:48
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
438
147
1
02/16/22 11:33
02/17/22 13:48
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
438
165
1
02/16/22 11:33
02/17/22 13:48
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
438
155
1
02/16/22 11:33
02/17/22 13:48
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
438
208
1
02/16/22 11:33
02/17/22 13:48
108-60-1
Pentachlorophenol
ND
ug/kg
876
429
1
02/16/22 11:33
02/17/22 13:48
87-86-5
Phenanthrene
ND
ug/kg
438
143
1
02/16/22 11:33
02/17/22 13:48
85-01-8
Phenol
ND
ug/kg
438
195
1
02/16/22 11:33
02/17/22 13:48
108-95-2
Pyrene
ND
ug/kg
438
178
1
02/16/22 11:33
02/17/22 13:48
129-00-0
Pyridine
ND
ug/kg
438
138
1
02/16/22 11:33
02/17/22 13:48
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
438
173
1
02/16/22 11:33
02/17/22 13:48
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
438
200
1
02/16/22 11:33
02/17/22 13:48
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
438
180
1
02/16/22 11:33
02/17/22 13:48
88-06-2
Surrogates
Nitrobenzene-d5 (S)
66
%
21-130
1
02/16/22 11:33
02/17/22 13:48
4165-60-0
2-Fluorobiphenyl (S)
53
%
19-130
1
02/16/22 11:33
02/17/22 13:48
321-60-8
Terphenyl-d14 (S)
59
%
15-130
1
02/16/22 11:33
02/17/22 13:48
1718-51-0
Phenol-d6 (S)
59
%
18-130
1
02/16/22 11:33
02/17/22 13:48
13127-88-3
2-Fluorophenol (S)
54
%
18-130
1
02/16/22 11:33
02/17/22 13:48
367-12-4
2,4,6-Tribromophenol (S)
38
%
18-130
1
02/16/22 11:33
02/17/22 13:48
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-L Lab ID: 92588327008 Collected: 02/14/22 16:00 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
199
64.0
1
02/15/22 21:19
02/17/22 18:58
67-64-1
Benzene
ND
ug/kg
10
4.0
1
02/15/22 21:19
02/17/22 18:58
71-43-2
Bromobenzene
ND
ug/kg
10
3.2
1
02/15/22 21:19
02/17/22 18:58
108-86-1
Bromochloromethane
ND
ug/kg
10
2.9
1
02/15/22 21:19
02/17/22 18:58
74-97-5
Bromodichloromethane
ND
ug/kg
10
3.8
1
02/15/22 21:19
02/17/22 18:58
75-27-4
Bromoform
ND
ug/kg
10
3.5
1
02/15/22 21:19
02/17/22 18:58
75-25-2
Bromomethane
ND
ug/kg
19.9
15.7
1
02/15/22 21:19
02/17/22 18:58
74-83-9
2-Butanone (MEK)
ND
ug/kg
199
47.8
1
02/15/22 21:19
02/17/22 18:58
78-93-3
n-Butylbenzene
ND
ug/kg
10
4.7
1
02/15/22 21:19
02/17/22 18:58
104-51-8
sec-Butylbenzene
ND
ug/kg
10
4.4
1
02/15/22 21:19
02/17/22 18:58
135-98-8
tert-Butyl benzene
ND
ug/kg
10
3.5
1
02/15/22 21:19
02/17/22 18:58
98-06-6
Carbon tetrachloride
ND
ug/kg
10
3.7
1
02/15/22 21:19
02/17/22 18:58
56-23-5
Chlorobenzene
ND
ug/kg
10
1.9
1
02/15/22 21:19
02/17/22 18:58
108-90-7
Chloroethane
ND
ug/kg
19.9
7.7
1
02/15/22 21:19
02/17/22 18:58
75-00-3
Chloroform
ND
ug/kg
10
6.1
1
02/15/22 21:19
02/17/22 18:58
67-66-3
Chloromethane
ND
ug/kg
19.9
8.4
1
02/15/22 21:19
02/17/22 18:58
74-87-3
2-Chlorotoluene
ND
ug/kg
10
3.5
1
02/15/22 21:19
02/17/22 18:58
95-49-8
4-Chlorotoluene
ND
ug/kg
10
1.8
1
02/15/22 21:19
02/17/22 18:58
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
10
3.9
1
02/15/22 21:19
02/17/22 18:58
96-12-8
Dibromochloromethane
ND
ug/kg
10
5.6
1
02/15/22 21:19
02/17/22 18:58
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
10
4.4
1
02/15/22 21:19
02/17/22 18:58
106-93-4
Dibromomethane
ND
ug/kg
10
2.1
1
02/15/22 21:19
02/17/22 18:58
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
10
3.6
1
02/15/22 21:19
02/17/22 18:58
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10
3.1
1
02/15/22 21:19
02/17/22 18:58
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10
2.6
1
02/15/22 21:19
02/17/22 18:58
106-46-7
Dichlorodifluoromethane
ND
ug/kg
19.9
4.3
1
02/15/22 21:19
02/17/22 18:58
75-71-8
1,1-Dichloroethane
ND
ug/kg
10
4.1
1
02/15/22 21:19
02/17/22 18:58
75-34-3
1,2-Dichloroethane
ND
ug/kg
10
6.6
1
02/15/22 21:19
02/17/22 18:58
107-06-2
1,1-Dichloroethene
ND
ug/kg
10
4.1
1
02/15/22 21:19
02/17/22 18:58
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
10
3.4
1
02/15/22 21:19
02/17/22 18:58
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
10
3.5
1
02/15/22 21:19
02/17/22 18:58
156-60-5
1,2-Dichloropropane
ND
ug/kg
10
3.0
1
02/15/22 21:19
02/17/22 18:58
78-87-5
1,3-Dichloropropane
ND
ug/kg
10
3.1
1
02/15/22 21:19
02/17/22 18:58
142-28-9
2,2-Dichloropropane
ND
ug/kg
10
3.2
1
02/15/22 21:19
02/17/22 18:58
594-20-7
1,1-Dichloropropene
ND
ug/kg
10
4.8
1
02/15/22 21:19
02/17/22 18:58
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
10
2.7
1
02/15/22 21:19
02/17/22 18:58
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
10
3.4
1
02/15/22 21:19
02/17/22 18:58
10061-02-6
Diisopropyl ether
ND
ug/kg
10
2.7
1
02/15/22 21:19
02/17/22 18:58
108-20-3
Ethylbenzene
ND
ug/kg
10
4.6
1
02/15/22 21:19
02/17/22 18:58
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
19.9
16.3
1
02/15/22 21:19
02/17/22 18:58
87-68-3
2-Hexanone
ND
ug/kg
99.6
9.6
1
02/15/22 21:19
02/17/22 18:58
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
10
3.4
1
02/15/22 21:19
02/17/22 18:58
98-82-8
p-Isopropyltoluene
ND
ug/kg
10
4.9
1
02/15/22 21:19
02/17/22 18:58
99-87-6
Methylene Chloride
ND
ug/kg
39.9
27.3
1
02/15/22 21:19
02/17/22 18:58
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-L
Lab ID:
92588327008
Collected:
02/14/22
16:00
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
99.6
9.6
1
02/15/22 21:19
02/17/22 18:58
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
10
3.7
1
02/15/22 21:19
02/17/22 18:58
1634-04-4
Naphthalene
ND
ug/kg
10
5.2
1
02/15/22 21:19
02/17/22 18:58
91-20-3
n-Propylbenzene
ND
ug/kg
10
3.5
1
02/15/22 21:19
02/17/22 18:58
103-65-1
Styrene
ND
ug/kg
10
2.6
1
02/15/22 21:19
02/17/22 18:58
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
10
3.8
1
02/15/22 21:19
02/17/22 18:58
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
10
2.6
1
02/15/22 21:19
02/17/22 18:58
79-34-5
Tetrachloroethene
ND
ug/kg
10
3.1
1
02/15/22 21:19
02/17/22 18:58
127-18-4
Toluene
ND
ug/kg
10
2.8
1
02/15/22 21:19
02/17/22 18:58
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
10
8.0
1
02/15/22 21:19
02/17/22 18:58
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
10
8.4
1
02/15/22 21:19
02/17/22 18:58
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
10
5.2
1
02/15/22 21:19
02/17/22 18:58
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
10
3.3
1
02/15/22 21:19
02/17/22 18:58
79-00-5
Trichloroethene
ND
ug/kg
10
2.6
1
02/15/22 21:19
02/17/22 18:58
79-01-6
Trichlorofluoromethane
ND
ug/kg
10
5.5
1
02/15/22 21:19
02/17/22 18:58
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
10
5.0
1
02/15/22 21:19
02/17/22 18:58
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
10
2.7
1
02/15/22 21:19
02/17/22 18:58
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
10
3.3
1
02/15/22 21:19
02/17/22 18:58
108-67-8
Vinyl acetate
ND
ug/kg
99.6
7.3
1
02/15/22 21:19
02/17/22 18:58
108-05-4
Vinyl chloride
ND
ug/kg
19.9
5.1
1
02/15/22 21:19
02/17/22 18:58
75-01-4 v2
Xylene (Total)
ND
ug/kg
19.9
5.7
1
02/15/22 21:19
02/17/22 18:58
1330-20-7
m&p-Xylene
ND
ug/kg
19.9
6.8
1
02/15/22 21:19
02/17/22 18:58
179601-23-1
o-Xylene
ND
ug/kg
10
4.4
1
02/15/22 21:19
02/17/22 18:58
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
02/15/22 21:19
02/17/22 18:58
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
02/15/22 21:19
02/17/22 18:58
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
02/15/22 21:19
02/17/22 18:58
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
23.6
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
Page 31 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-13 Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
8.2
8.2
1
02/16/22 13:41
02/16/22 19:21
Aliphatic(C09-C12)Adjusted
ND
mg/kg
8.2
8.2
1
02/16/22 13:41
02/16/22 19:21
Aromatic (C09-C10)
ND
mg/kg
8.2
8.2
1
02/16/22 13:41
02/16/22 19:21
Surrogates
4-Bromofluorobenzene (FID) (S)
102
%
70-130
1
02/16/22 13:41
02/16/22 19:21
460-00-4
4-Bromofluorobenzene (PID) (S)
85
%
70-130
1
02/16/22 13:41
02/16/22 19:21
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
443
156
1
02/16/22 11:33
02/17/22 14:15
83-32-9
Acenaphthylene
ND
ug/kg
443
156
1
02/16/22 11:33
02/17/22 14:15
208-96-8
Aniline
ND
ug/kg
443
173
1
02/16/22 11:33
02/17/22 14:15
62-53-3
Anthracene
ND
ug/kg
443
145
1
02/16/22 11:33
02/17/22 14:15
120-12-7
Benzo(a)anthracene
ND
ug/kg
443
148
1
02/16/22 11:33
02/17/22 14:15
56-55-3
Benzo(a)pyrene
ND
ug/kg
443
153
1
02/16/22 11:33
02/17/22 14:15
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
443
148
1
02/16/22 11:33
02/17/22 14:15
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
443
172
1
02/16/22 11:33
02/17/22 14:15
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
443
156
1
02/16/22 11:33
02/17/22 14:15
207-08-9
Benzoic Acid
ND
ug/kg
2210
952
1
02/16/22 11:33
02/17/22 14:15
65-85-0
Benzyl alcohol
ND
ug/kg
886
336
1
02/16/22 11:33
02/17/22 14:15
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
443
170
1
02/16/22 11:33
02/17/22 14:15
101-55-3
Butylbenzylphthalate
ND
ug/kg
443
187
1
02/16/22 11:33
02/17/22 14:15
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
886
311
1
02/16/22 11:33
02/17/22 14:15
59-50-7
4-Chloroaniline
ND
ug/kg
886
348
1
02/16/22 11:33
02/17/22 14:15
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
443
184
1
02/16/22 11:33
02/17/22 14:15
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
443
166
1
02/16/22 11:33
02/17/22 14:15
111-44-4
2-Chloronaphthalene
ND
ug/kg
443
176
1
02/16/22 11:33
02/17/22 14:15
91-58-7
2-Chlorophenol
ND
ug/kg
443
166
1
02/16/22 11:33
02/17/22 14:15
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
443
165
1
02/16/22 11:33
02/17/22 14:15
7005-72-3
Chrysene
ND
ug/kg
443
161
1
02/16/22 11:33
02/17/22 14:15
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
443
170
1
02/16/22 11:33
02/17/22 14:15
53-70-3
Dibenzofuran
ND
ug/kg
443
160
1
02/16/22 11:33
02/17/22 14:15
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
443
160
1
02/16/22 11:33
02/17/22 14:15
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
443
157
1
02/16/22 11:33
02/17/22 14:15
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
443
169
1
02/16/22 11:33
02/17/22 14:15
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
886
299
1
02/16/22 11:33
02/17/22 14:15
91-94-1
2,4-Dichlorophenol
ND
ug/kg
443
173
1
02/16/22 11:33
02/17/22 14:15
120-83-2
Diethylphthalate
ND
ug/kg
443
162
1
02/16/22 11:33
02/17/22 14:15
84-66-2
2,4-Dimethylphenol
ND
ug/kg
443
184
1
02/16/22 11:33
02/17/22 14:15
105-67-9
Dimethylphthalate
ND
ug/kg
443
161
1
02/16/22 11:33
02/17/22 14:15
131-11-3
Di-n-butylphthalate
ND
ug/kg
443
149
1
02/16/22 11:33
02/17/22 14:15
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
886
413
1
02/16/22 11:33
02/17/22 14:15
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2210
1370
1
02/16/22 11:33
02/17/22 14:15
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
443
170
1
02/16/22 11:33
02/17/22 14:15
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-13 Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
443
162
1
02/16/22 11:33
02/17/22 14:15
606-20-2
Di-n-octylphthalate
ND
ug/kg
443
174
1
02/16/22 11:33
02/17/22 14:15
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
443
172
1
02/16/22 11:33
02/17/22 14:15
117-81-7
Fluoranthene
ND
ug/kg
443
152
1
02/16/22 11:33
02/17/22 14:15
206-44-0
Fluorene
ND
ug/kg
443
156
1
02/16/22 11:33
02/17/22 14:15
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
443
192
1
02/16/22 11:33
02/17/22 14:15
87-68-3
Hexachlorobenzene
ND
ug/kg
443
173
1
02/16/22 11:33
02/17/22 14:15
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
443
254
1
02/16/22 11:33
02/17/22 14:15
77-47-4
Hexachloroethane
ND
ug/kg
443
169
1
02/16/22 11:33
02/17/22 14:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
443
174
1
02/16/22 11:33
02/17/22 14:15
193-39-5
Isophorone
ND
ug/kg
443
197
1
02/16/22 11:33
02/17/22 14:15
78-59-1
1-Methylnaphthalene
ND
ug/kg
443
156
1
02/16/22 11:33
02/17/22 14:15
90-12-0
2-Methylnaphthalene
ND
ug/kg
443
177
1
02/16/22 11:33
02/17/22 14:15
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
443
181
1
02/16/22 11:33
02/17/22 14:15
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
443
179
1
02/16/22 11:33
02/17/22 14:15
15831-10-4
Naphthalene
ND
ug/kg
443
150
1
02/16/22 11:33
02/17/22 14:15
91-20-3
2-Nitroaniline
ND
ug/kg
2210
362
1
02/16/22 11:33
02/17/22 14:15
88-74-4
3-Nitroaniline
ND
ug/kg
2210
348
1
02/16/22 11:33
02/17/22 14:15
99-09-2
4-Nitroaniline
ND
ug/kg
886
337
1
02/16/22 11:33
02/17/22 14:15
100-01-6
Nitrobenzene
ND
ug/kg
443
205
1
02/16/22 11:33
02/17/22 14:15
98-95-3
2-Nitrophenol
ND
ug/kg
443
192
1
02/16/22 11:33
02/17/22 14:15
88-75-5
4-Nitrophenol
ND
ug/kg
2210
856
1
02/16/22 11:33
02/17/22 14:15
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
443
149
1
02/16/22 11:33
02/17/22 14:15
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
443
166
1
02/16/22 11:33
02/17/22 14:15
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
443
157
1
02/16/22 11:33
02/17/22 14:15
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
443
211
1
02/16/22 11:33
02/17/22 14:15
108-60-1
Pentachlorophenol
ND
ug/kg
886
434
1
02/16/22 11:33
02/17/22 14:15
87-86-5
Phenanthrene
ND
ug/kg
443
145
1
02/16/22 11:33
02/17/22 14:15
85-01-8
Phenol
ND
ug/kg
443
197
1
02/16/22 11:33
02/17/22 14:15
108-95-2
Pyrene
ND
ug/kg
443
180
1
02/16/22 11:33
02/17/22 14:15
129-00-0
Pyridine
ND
ug/kg
443
140
1
02/16/22 11:33
02/17/22 14:15
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
443
174
1
02/16/22 11:33
02/17/22 14:15
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
443
203
1
02/16/22 11:33
02/17/22 14:15
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
443
183
1
02/16/22 11:33
02/17/22 14:15
88-06-2
Surrogates
Nitrobenzene-d5 (S)
67
%
21-130
1
02/16/22 11:33
02/17/22 14:15
4165-60-0
2-Fluorobiphenyl (S)
52
%
19-130
1
02/16/22 11:33
02/17/22 14:15
321-60-8
Terphenyl-d14 (S)
64
%
15-130
1
02/16/22 11:33
02/17/22 14:15
1718-51-0
Phenol-d6 (S)
60
%
18-130
1
02/16/22 11:33
02/17/22 14:15
13127-88-3
2-Fluorophenol (S)
55
%
18-130
1
02/16/22 11:33
02/17/22 14:15
367-12-4
2,4,6-Tribromophenol (S)
51
%
18-130
1
02/16/22 11:33
02/17/22 14:15
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-B Lab ID: 92588327009 Collected: 02/14/22 16:20 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
276
88.7
1
02/15/22 21:19
02/17/22 19:16
67-64-1
Benzene
ND
ug/kg
13.8
5.5
1
02/15/22 21:19
02/17/22 19:16
71-43-2
Bromobenzene
ND
ug/kg
13.8
4.5
1
02/15/22 21:19
02/17/22 19:16
108-86-1
Bromochloromethane
ND
ug/kg
13.8
4.1
1
02/15/22 21:19
02/17/22 19:16
74-97-5
Bromodichloromethane
ND
ug/kg
13.8
5.3
1
02/15/22 21:19
02/17/22 19:16
75-27-4
Bromoform
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 19:16
75-25-2
Bromomethane
ND
ug/kg
27.6
21.8
1
02/15/22 21:19
02/17/22 19:16
74-83-9
2-Butanone (MEK)
ND
ug/kg
276
66.4
1
02/15/22 21:19
02/17/22 19:16
78-93-3
n-Butylbenzene
ND
ug/kg
13.8
6.5
1
02/15/22 21:19
02/17/22 19:16
104-51-8
sec-Butylbenzene
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 19:16
135-98-8
tert-Butyl benzene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 19:16
98-06-6
Carbon tetrachloride
ND
ug/kg
13.8
5.2
1
02/15/22 21:19
02/17/22 19:16
56-23-5
Chlorobenzene
ND
ug/kg
13.8
2.7
1
02/15/22 21:19
02/17/22 19:16
108-90-7
Chloroethane
ND
ug/kg
27.6
10.7
1
02/15/22 21:19
02/17/22 19:16
75-00-3
Chloroform
ND
ug/kg
13.8
8.4
1
02/15/22 21:19
02/17/22 19:16
67-66-3
Chloromethane
ND
ug/kg
27.6
11.6
1
02/15/22 21:19
02/17/22 19:16
74-87-3
2-Chlorotoluene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 19:16
95-49-8
4-Chlorotoluene
ND
ug/kg
13.8
2.4
1
02/15/22 21:19
02/17/22 19:16
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
13.8
5.4
1
02/15/22 21:19
02/17/22 19:16
96-12-8
Dibromochloromethane
ND
ug/kg
13.8
7.8
1
02/15/22 21:19
02/17/22 19:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 19:16
106-93-4
Dibromomethane
ND
ug/kg
13.8
3.0
1
02/15/22 21:19
02/17/22 19:16
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
13.8
5.0
1
02/15/22 21:19
02/17/22 19:16
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
13.8
4.3
1
02/15/22 21:19
02/17/22 19:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 19:16
106-46-7
Dichlorodifluoromethane
ND
ug/kg
27.6
6.0
1
02/15/22 21:19
02/17/22 19:16
75-71-8
1,1-Dichloroethane
ND
ug/kg
13.8
5.7
1
02/15/22 21:19
02/17/22 19:16
75-34-3
1,2-Dichloroethane
ND
ug/kg
13.8
9.2
1
02/15/22 21:19
02/17/22 19:16
107-06-2
1,1-Dichloroethene
ND
ug/kg
13.8
5.7
1
02/15/22 21:19
02/17/22 19:16
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
13.8
4.7
1
02/15/22 21:19
02/17/22 19:16
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
13.8
4.8
1
02/15/22 21:19
02/17/22 19:16
156-60-5
1,2-Dichloropropane
ND
ug/kg
13.8
4.1
1
02/15/22 21:19
02/17/22 19:16
78-87-5
1,3-Dichloropropane
ND
ug/kg
13.8
4.3
1
02/15/22 21:19
02/17/22 19:16
142-28-9
2,2-Dichloropropane
ND
ug/kg
13.8
4.5
1
02/15/22 21:19
02/17/22 19:16
594-20-7
1,1-Dichloropropene
ND
ug/kg
13.8
6.6
1
02/15/22 21:19
02/17/22 19:16
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
13.8
3.8
1
02/15/22 21:19
02/17/22 19:16
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
13.8
4.8
1
02/15/22 21:19
02/17/22 19:16
10061-02-6
Diisopropyl ether
ND
ug/kg
13.8
3.7
1
02/15/22 21:19
02/17/22 19:16
108-20-3
Ethylbenzene
ND
ug/kg
13.8
6.4
1
02/15/22 21:19
02/17/22 19:16
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
27.6
22.6
1
02/15/22 21:19
02/17/22 19:16
87-68-3
2-Hexanone
ND
ug/kg
138
13.3
1
02/15/22 21:19
02/17/22 19:16
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
13.8
4.7
1
02/15/22 21:19
02/17/22 19:16
98-82-8
p-Isopropyltoluene
ND
ug/kg
13.8
6.8
1
02/15/22 21:19
02/17/22 19:16
99-87-6
Methylene Chloride
ND
ug/kg
55.3
37.9
1
02/15/22 21:19
02/17/22 19:16
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-13
Lab ID:
92588327009
Collected:
02/14/22
16:20
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
138
13.3
1
02/15/22 21:19
02/17/22 19:16
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
13.8
5.2
1
02/15/22 21:19
02/17/22 19:16
1634-04-4
Naphthalene
24.4
ug/kg
13.8
7.3
1
02/15/22 21:19
02/17/22 19:16
91-20-3
n-Propylbenzene
ND
ug/kg
13.8
4.9
1
02/15/22 21:19
02/17/22 19:16
103-65-1
Styrene
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 19:16
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
13.8
5.3
1
02/15/22 21:19
02/17/22 19:16
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 19:16
79-34-5
Tetrachloroethene
ND
ug/kg
13.8
4.4
1
02/15/22 21:19
02/17/22 19:16
127-18-4
Toluene
ND
ug/kg
13.8
3.9
1
02/15/22 21:19
02/17/22 19:16
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
13.8
11.2
1
02/15/22 21:19
02/17/22 19:16
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
13.8
11.6
1
02/15/22 21:19
02/17/22 19:16
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
13.8
7.2
1
02/15/22 21:19
02/17/22 19:16
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
13.8
4.6
1
02/15/22 21:19
02/17/22 19:16
79-00-5
Trichloroethene
ND
ug/kg
13.8
3.6
1
02/15/22 21:19
02/17/22 19:16
79-01-6
Trichlorofluoromethane
ND
ug/kg
13.8
7.6
1
02/15/22 21:19
02/17/22 19:16
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
13.8
7.0
1
02/15/22 21:19
02/17/22 19:16
96-18-4
1,2,4-Trimethylbenzene
9.01
ug/kg
13.8
3.8
1
02/15/22 21:19
02/17/22 19:16
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
13.8
4.6
1
02/15/22 21:19
02/17/22 19:16
108-67-8
Vinyl acetate
ND
ug/kg
138
10.1
1
02/15/22 21:19
02/17/22 19:16
108-05-4
Vinyl chloride
ND
ug/kg
27.6
7.0
1
02/15/22 21:19
02/17/22 19:16
75-01-4 v2
Xylene (Total)
ND
ug/kg
27.6
7.9
1
02/15/22 21:19
02/17/22 19:16
1330-20-7
m&p-Xylene
ND
ug/kg
27.6
9.5
1
02/15/22 21:19
02/17/22 19:16
179601-23-1
o-Xylene
ND
ug/kg
13.8
6.1
1
02/15/22 21:19
02/17/22 19:16
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 19:16
2037-26-5
4-Bromofluorobenzene (S)
98
%
69-134
1
02/15/22 21:19
02/17/22 19:16
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
02/15/22 21:19
02/17/22 19:16
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
25.7
%
0.10
0.10
1
02/15/22 17:10
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
4.3
4.3
1
02/16/22 13:41
02/16/22 19:50
Aliphatic(C09-C12)Adjusted
ND
mg/kg
4.3
4.3
1
02/16/22 13:41
02/16/22 19:50
Aromatic (C09-C10)
ND
mg/kg
4.3
4.3
1
02/16/22 13:41
02/16/22 19:50
Surrogates
4-Bromofluorobenzene (FID) (S)
101
%
70-130
1
02/16/22 13:41
02/16/22 19:50
460-00-4
4-Bromofluorobenzene (PID) (S)
85
%
70-130
1
02/16/22 13:41
02/16/22 19:50
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
449
158
1
02/16/22 11:33
02/17/22 14:42
83-32-9
Acenaphthylene
ND
ug/kg
449
158
1
02/16/22 11:33
02/17/22 14:42
208-96-8
Aniline
ND
ug/kg
449
175
1
02/16/22 11:33
02/17/22 14:42
62-53-3
Anthracene
ND
ug/kg
449
147
1
02/16/22 11:33
02/17/22 14:42
120-12-7
Benzo(a)anthracene
ND
ug/kg
449
150
1
02/16/22 11:33
02/17/22 14:42
56-55-3
Benzo(a)pyrene
ND
ug/kg
449
155
1
02/16/22 11:33
02/17/22 14:42
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
449
150
1
02/16/22 11:33
02/17/22 14:42
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
449
174
1
02/16/22 11:33
02/17/22 14:42
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
449
158
1
02/16/22 11:33
02/17/22 14:42
207-08-9
Benzoic Acid
ND
ug/kg
2240
964
1
02/16/22 11:33
02/17/22 14:42
65-85-0
Benzyl alcohol
ND
ug/kg
898
340
1
02/16/22 11:33
02/17/22 14:42
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
449
173
1
02/16/22 11:33
02/17/22 14:42
101-55-3
Butylbenzylphthalate
ND
ug/kg
449
189
1
02/16/22 11:33
02/17/22 14:42
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
898
315
1
02/16/22 11:33
02/17/22 14:42
59-50-7
4-Chloroaniline
ND
ug/kg
898
352
1
02/16/22 11:33
02/17/22 14:42
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
449
186
1
02/16/22 11:33
02/17/22 14:42
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
449
169
1
02/16/22 11:33
02/17/22 14:42
111-44-4
2-Chloronaphthalene
ND
ug/kg
449
178
1
02/16/22 11:33
02/17/22 14:42
91-58-7
2-Chlorophenol
ND
ug/kg
449
169
1
02/16/22 11:33
02/17/22 14:42
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
449
167
1
02/16/22 11:33
02/17/22 14:42
7005-72-3
Chrysene
ND
ug/kg
449
163
1
02/16/22 11:33
02/17/22 14:42
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
449
173
1
02/16/22 11:33
02/17/22 14:42
53-70-3
Dibenzofuran
ND
ug/kg
449
162
1
02/16/22 11:33
02/17/22 14:42
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
449
162
1
02/16/22 11:33
02/17/22 14:42
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
449
159
1
02/16/22 11:33
02/17/22 14:42
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
449
171
1
02/16/22 11:33
02/17/22 14:42
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
898
303
1
02/16/22 11:33
02/17/22 14:42
91-94-1
2,4-Dichlorophenol
ND
ug/kg
449
175
1
02/16/22 11:33
02/17/22 14:42
120-83-2
Diethylphthalate
ND
ug/kg
449
165
1
02/16/22 11:33
02/17/22 14:42
84-66-2
2,4-Dimethylphenol
ND
ug/kg
449
186
1
02/16/22 11:33
02/17/22 14:42
105-67-9
Dimethylphthalate
ND
ug/kg
449
163
1
02/16/22 11:33
02/17/22 14:42
131-11-3
Di-n-butylphthalate
ND
ug/kg
449
151
1
02/16/22 11:33
02/17/22 14:42
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
898
419
1
02/16/22 11:33
02/17/22 14:42
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2240
1390
1
02/16/22 11:33
02/17/22 14:42
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
449
173
1
02/16/22 11:33
02/17/22 14:42
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
449
165
1
02/16/22 11:33
02/17/22 14:42
606-20-2
Di-n-octylphthalate
ND
ug/kg
449
177
1
02/16/22 11:33
02/17/22 14:42
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
449
174
1
02/16/22 11:33
02/17/22 14:42
117-81-7
Fluoranthene
ND
ug/kg
449
154
1
02/16/22 11:33
02/17/22 14:42
206-44-0
Fluorene
ND
ug/kg
449
158
1
02/16/22 11:33
02/17/22 14:42
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
449
194
1
02/16/22 11:33
02/17/22 14:42
87-68-3
Hexachlorobenzene
ND
ug/kg
449
175
1
02/16/22 11:33
02/17/22 14:42
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
449
257
1
02/16/22 11:33
02/17/22 14:42
77-47-4
Hexachloroethane
ND
ug/kg
449
171
1
02/16/22 11:33
02/17/22 14:42
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
449
177
1
02/16/22 11:33
02/17/22 14:42
193-39-5
Isophorone
ND
ug/kg
449
200
1
02/16/22 11:33
02/17/22 14:42
78-59-1
1-Methylnaphthalene
ND
ug/kg
449
158
1
02/16/22 11:33
02/17/22 14:42
90-12-0
2-Methylnaphthalene
ND
ug/kg
449
180
1
02/16/22 11:33
02/17/22 14:42
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
449
184
1
02/16/22 11:33
02/17/22 14:42
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
449
181
1
02/16/22 11:33
02/17/22 14:42
15831-10-4
Naphthalene
ND
ug/kg
449
152
1
02/16/22 11:33
02/17/22 14:42
91-20-3
2-Nitroaniline
ND
ug/kg
2240
367
1
02/16/22 11:33
02/17/22 14:42
88-74-4
3-Nitroaniline
ND
ug/kg
2240
352
1
02/16/22 11:33
02/17/22 14:42
99-09-2
4-Nitroaniline
ND
ug/kg
898
341
1
02/16/22 11:33
02/17/22 14:42
100-01-6
Nitrobenzene
ND
ug/kg
449
208
1
02/16/22 11:33
02/17/22 14:42
98-95-3
2-Nitrophenol
ND
ug/kg
449
194
1
02/16/22 11:33
02/17/22 14:42
88-75-5
4-Nitrophenol
ND
ug/kg
2240
868
1
02/16/22 11:33
02/17/22 14:42
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
449
151
1
02/16/22 11:33
02/17/22 14:42
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
449
169
1
02/16/22 11:33
02/17/22 14:42
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
449
159
1
02/16/22 11:33
02/17/22 14:42
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
449
214
1
02/16/22 11:33
02/17/22 14:42
108-60-1
Pentachlorophenol
ND
ug/kg
898
439
1
02/16/22 11:33
02/17/22 14:42
87-86-5
Phenanthrene
ND
ug/kg
449
147
1
02/16/22 11:33
02/17/22 14:42
85-01-8
Phenol
ND
ug/kg
449
200
1
02/16/22 11:33
02/17/22 14:42
108-95-2
Pyrene
ND
ug/kg
449
182
1
02/16/22 11:33
02/17/22 14:42
129-00-0
Pyridine
ND
ug/kg
449
141
1
02/16/22 11:33
02/17/22 14:42
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
449
177
1
02/16/22 11:33
02/17/22 14:42
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
449
205
1
02/16/22 11:33
02/17/22 14:42
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
449
185
1
02/16/22 11:33
02/17/22 14:42
88-06-2
Surrogates
Nitrobenzene-d5 (S)
51
%
21-130
1
02/16/22 11:33
02/17/22 14:42
4165-60-0
2-Fluorobiphenyl (S)
41
%
19-130
1
02/16/22 11:33
02/17/22 14:42
321-60-8
Terphenyl-d14 (S)
47
%
15-130
1
02/16/22 11:33
02/17/22 14:42
1718-51-0
Phenol-d6 (S)
48
%
18-130
1
02/16/22 11:33
02/17/22 14:42
13127-88-3
2-Fluorophenol (S)
44
%
18-130
1
02/16/22 11:33
02/17/22 14:42
367-12-4
2,4,6-Tribromophenol (S)
37
%
18-130
1
02/16/22 11:33
02/17/22 14:42
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-R Lab ID: 92588327010 Collected: 02/14/22 16:10 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
189
60.7
1
02/15/22 21:19
02/17/22 19:33
67-64-1
Benzene
ND
ug/kg
9.5
3.8
1
02/15/22 21:19
02/17/22 19:33
71-43-2
Bromobenzene
ND
ug/kg
9.5
3.1
1
02/15/22 21:19
02/17/22 19:33
108-86-1
Bromochloromethane
ND
ug/kg
9.5
2.8
1
02/15/22 21:19
02/17/22 19:33
74-97-5
Bromodichloromethane
ND
ug/kg
9.5
3.6
1
02/15/22 21:19
02/17/22 19:33
75-27-4
Bromoform
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 19:33
75-25-2
Bromomethane
ND
ug/kg
18.9
14.9
1
02/15/22 21:19
02/17/22 19:33
74-83-9
2-Butanone (MEK)
ND
ug/kg
189
45.4
1
02/15/22 21:19
02/17/22 19:33
78-93-3
n-Butylbenzene
ND
ug/kg
9.5
4.5
1
02/15/22 21:19
02/17/22 19:33
104-51-8
sec-Butylbenzene
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 19:33
135-98-8
tert-Butyl benzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 19:33
98-06-6
Carbon tetrachloride
ND
ug/kg
9.5
3.5
1
02/15/22 21:19
02/17/22 19:33
56-23-5
Chlorobenzene
ND
ug/kg
9.5
1.8
1
02/15/22 21:19
02/17/22 19:33
108-90-7
Chloroethane
ND
ug/kg
18.9
7.3
1
02/15/22 21:19
02/17/22 19:33
75-00-3
Chloroform
ND
ug/kg
9.5
5.7
1
02/15/22 21:19
02/17/22 19:33
67-66-3
Chloromethane
ND
ug/kg
18.9
7.9
1
02/15/22 21:19
02/17/22 19:33
74-87-3
2-Chlorotoluene
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 19:33
95-49-8
4-Chlorotoluene
ND
ug/kg
9.5
1.7
1
02/15/22 21:19
02/17/22 19:33
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.5
3.7
1
02/15/22 21:19
02/17/22 19:33
96-12-8
Dibromochloromethane
ND
ug/kg
9.5
5.3
1
02/15/22 21:19
02/17/22 19:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 19:33
106-93-4
Dibromomethane
ND
ug/kg
9.5
2.0
1
02/15/22 21:19
02/17/22 19:33
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 19:33
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.5
2.9
1
02/15/22 21:19
02/17/22 19:33
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 19:33
106-46-7
Dichlorodifluoromethane
ND
ug/kg
18.9
4.1
1
02/15/22 21:19
02/17/22 19:33
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.5
3.9
1
02/15/22 21:19
02/17/22 19:33
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.5
6.3
1
02/15/22 21:19
02/17/22 19:33
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.5
3.9
1
02/15/22 21:19
02/17/22 19:33
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 19:33
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 19:33
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.5
2.8
1
02/15/22 21:19
02/17/22 19:33
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.5
2.9
1
02/15/22 21:19
02/17/22 19:33
142-28-9
2,2-Dichloropropane
ND
ug/kg
9.5
3.1
1
02/15/22 21:19
02/17/22 19:33
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.5
4.5
1
02/15/22 21:19
02/17/22 19:33
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 19:33
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 19:33
10061-02-6
Diisopropyl ether
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 19:33
108-20-3
Ethylbenzene
ND
ug/kg
9.5
4.4
1
02/15/22 21:19
02/17/22 19:33
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
18.9
15.5
1
02/15/22 21:19
02/17/22 19:33
87-68-3
2-Hexanone
ND
ug/kg
94.5
9.1
1
02/15/22 21:19
02/17/22 19:33
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 19:33
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.5
4.7
1
02/15/22 21:19
02/17/22 19:33
99-87-6
Methylene Chloride
ND
ug/kg
37.8
25.9
1
02/15/22 21:19
02/17/22 19:33
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
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Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-R
Lab ID:
92588327010
Collected:
02/14/22
16:10
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
94.5
9.1
1
02/15/22 21:19
02/17/22 19:33
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.5
3.5
1
02/15/22 21:19
02/17/22 19:33
1634-04-4
Naphthalene
5.51
ug/kg
9.5
5.0
1
02/15/22 21:19
02/17/22 19:33
91-20-3
n-Propylbenzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 19:33
103-65-1
Styrene
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 19:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
9.5
3.6
1
02/15/22 21:19
02/17/22 19:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 19:33
79-34-5
Tetrachloroethene
ND
ug/kg
9.5
3.0
1
02/15/22 21:19
02/17/22 19:33
127-18-4
Toluene
ND
ug/kg
9.5
2.7
1
02/15/22 21:19
02/17/22 19:33
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
9.5
7.6
1
02/15/22 21:19
02/17/22 19:33
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
9.5
7.9
1
02/15/22 21:19
02/17/22 19:33
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
9.5
4.9
1
02/15/22 21:19
02/17/22 19:33
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
9.5
3.1
1
02/15/22 21:19
02/17/22 19:33
79-00-5
Trichloroethene
ND
ug/kg
9.5
2.4
1
02/15/22 21:19
02/17/22 19:33
79-01-6
Trichlorofluoromethane
ND
ug/kg
9.5
5.2
1
02/15/22 21:19
02/17/22 19:33
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
9.5
4.8
1
02/15/22 21:19
02/17/22 19:33
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 19:33
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 19:33
108-67-8
Vinyl acetate
ND
ug/kg
94.5
6.9
1
02/15/22 21:19
02/17/22 19:33
108-05-4
Vinyl chloride
ND
ug/kg
18.9
4.8
1
02/15/22 21:19
02/17/22 19:33
75-01-4 v2
Xylene (Total)
ND
ug/kg
18.9
5.4
1
02/15/22 21:19
02/17/22 19:33
1330-20-7
m&p-Xylene
ND
ug/kg
18.9
6.5
1
02/15/22 21:19
02/17/22 19:33
179601-23-1
o-Xylene
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 19:33
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/15/22 21:19
02/17/22 19:33
2037-26-5
4-Bromofluorobenzene (S)
97
%
69-134
1
02/15/22 21:19
02/17/22 19:33
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/15/22 21:19
02/17/22 19:33
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
26.7
%
0.10
0.10
1
02/15/22 17:11
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-13 Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 20:19
Aliphatic(C09-C12) Adjusted
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 20:19
Aromatic (C09-C10)
ND
mg/kg
5.6
5.6
1
02/16/22 13:41
02/16/22 20:19
Surrogates
4-Bromofluorobenzene (FID) (S)
98
%
70-130
1
02/16/22 13:41
02/16/22 20:19
460-00-4
4-Bromofluorobenzene (PID) (S)
84
%
70-130
1
02/16/22 13:41
02/16/22 20:19
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
445
156
1
02/16/22 11:33
02/17/22 15:08
83-32-9
Acenaphthylene
ND
ug/kg
445
156
1
02/16/22 11:33
02/17/22 15:08
208-96-8
Aniline
ND
ug/kg
445
174
1
02/16/22 11:33
02/17/22 15:08
62-53-3
Anthracene
ND
ug/kg
445
146
1
02/16/22 11:33
02/17/22 15:08
120-12-7
Benzo(a)anthracene
ND
ug/kg
445
148
1
02/16/22 11:33
02/17/22 15:08
56-55-3
Benzo(a)pyrene
ND
ug/kg
445
154
1
02/16/22 11:33
02/17/22 15:08
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
445
148
1
02/16/22 11:33
02/17/22 15:08
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
445
172
1
02/16/22 11:33
02/17/22 15:08
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
445
156
1
02/16/22 11:33
02/17/22 15:08
207-08-9
Benzoic Acid
ND
ug/kg
2220
955
1
02/16/22 11:33
02/17/22 15:08
65-85-0
Benzyl alcohol
ND
ug/kg
889
337
1
02/16/22 11:33
02/17/22 15:08
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
445
171
1
02/16/22 11:33
02/17/22 15:08
101-55-3
Butylbenzylphthalate
ND
ug/kg
445
187
1
02/16/22 11:33
02/17/22 15:08
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
889
313
1
02/16/22 11:33
02/17/22 15:08
59-50-7
4-Chloroaniline
ND
ug/kg
889
349
1
02/16/22 11:33
02/17/22 15:08
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
445
185
1
02/16/22 11:33
02/17/22 15:08
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
445
167
1
02/16/22 11:33
02/17/22 15:08
111-44-4
2-Chloronaphthalene
ND
ug/kg
445
177
1
02/16/22 11:33
02/17/22 15:08
91-58-7
2-Chlorophenol
ND
ug/kg
445
167
1
02/16/22 11:33
02/17/22 15:08
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
445
166
1
02/16/22 11:33
02/17/22 15:08
7005-72-3
Chrysene
ND
ug/kg
445
162
1
02/16/22 11:33
02/17/22 15:08
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
445
171
1
02/16/22 11:33
02/17/22 15:08
53-70-3
Dibenzofuran
ND
ug/kg
445
160
1
02/16/22 11:33
02/17/22 15:08
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
445
160
1
02/16/22 11:33
02/17/22 15:08
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
445
158
1
02/16/22 11:33
02/17/22 15:08
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
445
170
1
02/16/22 11:33
02/17/22 15:08
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
889
300
1
02/16/22 11:33
02/17/22 15:08
91-94-1
2,4-Dichlorophenol
ND
ug/kg
445
174
1
02/16/22 11:33
02/17/22 15:08
120-83-2
Diethylphthalate
ND
ug/kg
445
163
1
02/16/22 11:33
02/17/22 15:08
84-66-2
2,4-Dimethylphenol
ND
ug/kg
445
185
1
02/16/22 11:33
02/17/22 15:08
105-67-9
Dimethylphthalate
ND
ug/kg
445
162
1
02/16/22 11:33
02/17/22 15:08
131-11-3
Di-n-butylphthalate
ND
ug/kg
445
150
1
02/16/22 11:33
02/17/22 15:08
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
889
415
1
02/16/22 11:33
02/17/22 15:08
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2220
1370
1
02/16/22 11:33
02/17/22 15:08
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
445
171
1
02/16/22 11:33
02/17/22 15:08
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-13 Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
445
163
1
02/16/22 11:33
02/17/22 15:08
606-20-2
Di-n-octylphthalate
ND
ug/kg
445
175
1
02/16/22 11:33
02/17/22 15:08
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
445
172
1
02/16/22 11:33
02/17/22 15:08
117-81-7
Fluoranthene
ND
ug/kg
445
152
1
02/16/22 11:33
02/17/22 15:08
206-44-0
Fluorene
ND
ug/kg
445
156
1
02/16/22 11:33
02/17/22 15:08
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
445
193
1
02/16/22 11:33
02/17/22 15:08
87-68-3
Hexachlorobenzene
ND
ug/kg
445
174
1
02/16/22 11:33
02/17/22 15:08
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
445
255
1
02/16/22 11:33
02/17/22 15:08
77-47-4
Hexachloroethane
ND
ug/kg
445
170
1
02/16/22 11:33
02/17/22 15:08
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
445
175
1
02/16/22 11:33
02/17/22 15:08
193-39-5
Isophorone
ND
ug/kg
445
198
1
02/16/22 11:33
02/17/22 15:08
78-59-1
1-Methylnaphthalene
ND
ug/kg
445
156
1
02/16/22 11:33
02/17/22 15:08
90-12-0
2-Methylnaphthalene
ND
ug/kg
445
178
1
02/16/22 11:33
02/17/22 15:08
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
445
182
1
02/16/22 11:33
02/17/22 15:08
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
445
179
1
02/16/22 11:33
02/17/22 15:08
15831-10-4
Naphthalene
ND
ug/kg
445
151
1
02/16/22 11:33
02/17/22 15:08
91-20-3
2-Nitroaniline
ND
ug/kg
2220
364
1
02/16/22 11:33
02/17/22 15:08
88-74-4
3-Nitroaniline
ND
ug/kg
2220
349
1
02/16/22 11:33
02/17/22 15:08
99-09-2
4-Nitroaniline
ND
ug/kg
889
338
1
02/16/22 11:33
02/17/22 15:08
100-01-6
Nitrobenzene
ND
ug/kg
445
206
1
02/16/22 11:33
02/17/22 15:08
98-95-3
2-Nitrophenol
ND
ug/kg
445
193
1
02/16/22 11:33
02/17/22 15:08
88-75-5
4-Nitrophenol
ND
ug/kg
2220
860
1
02/16/22 11:33
02/17/22 15:08
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
445
150
1
02/16/22 11:33
02/17/22 15:08
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
445
167
1
02/16/22 11:33
02/17/22 15:08
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
445
158
1
02/16/22 11:33
02/17/22 15:08
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
445
212
1
02/16/22 11:33
02/17/22 15:08
108-60-1
Pentachlorophenol
ND
ug/kg
889
435
1
02/16/22 11:33
02/17/22 15:08
87-86-5
Phenanthrene
ND
ug/kg
445
146
1
02/16/22 11:33
02/17/22 15:08
85-01-8
Phenol
ND
ug/kg
445
198
1
02/16/22 11:33
02/17/22 15:08
108-95-2
Pyrene
ND
ug/kg
445
181
1
02/16/22 11:33
02/17/22 15:08
129-00-0
Pyridine
ND
ug/kg
445
140
1
02/16/22 11:33
02/17/22 15:08
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
445
175
1
02/16/22 11:33
02/17/22 15:08
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
445
203
1
02/16/22 11:33
02/17/22 15:08
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
445
183
1
02/16/22 11:33
02/17/22 15:08
88-06-2
Surrogates
Nitrobenzene-d5 (S)
64
%
21-130
1
02/16/22 11:33
02/17/22 15:08
4165-60-0
2-Fluorobiphenyl (S)
53
%
19-130
1
02/16/22 11:33
02/17/22 15:08
321-60-8
Terphenyl-d14 (S)
64
%
15-130
1
02/16/22 11:33
02/17/22 15:08
1718-51-0
Phenol-d6 (S)
56
%
18-130
1
02/16/22 11:33
02/17/22 15:08
13127-88-3
2-Fluorophenol (S)
47
%
18-130
1
02/16/22 11:33
02/17/22 15:08
367-12-4
2,4,6-Tribromophenol (S)
39
%
18-130
1
02/16/22 11:33
02/17/22 15:08
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-B Lab ID: 92588327011 Collected: 02/14/22 16:30 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
192
61.6
1
02/15/22 21:19
02/17/22 19:51
67-64-1
Benzene
ND
ug/kg
9.6
3.8
1
02/15/22 21:19
02/17/22 19:51
71-43-2
Bromobenzene
ND
ug/kg
9.6
3.1
1
02/15/22 21:19
02/17/22 19:51
108-86-1
Bromochloromethane
ND
ug/kg
9.6
2.8
1
02/15/22 21:19
02/17/22 19:51
74-97-5
Bromodichloromethane
ND
ug/kg
9.6
3.7
1
02/15/22 21:19
02/17/22 19:51
75-27-4
Bromoform
ND
ug/kg
9.6
3.4
1
02/15/22 21:19
02/17/22 19:51
75-25-2
Bromomethane
ND
ug/kg
19.2
15.2
1
02/15/22 21:19
02/17/22 19:51
74-83-9
2-Butanone (MEK)
ND
ug/kg
192
46.1
1
02/15/22 21:19
02/17/22 19:51
78-93-3
n-Butylbenzene
ND
ug/kg
9.6
4.5
1
02/15/22 21:19
02/17/22 19:51
104-51-8
sec-Butylbenzene
ND
ug/kg
9.6
4.2
1
02/15/22 21:19
02/17/22 19:51
135-98-8
tert-Butyl benzene
ND
ug/kg
9.6
3.4
1
02/15/22 21:19
02/17/22 19:51
98-06-6
Carbon tetrachloride
ND
ug/kg
9.6
3.6
1
02/15/22 21:19
02/17/22 19:51
56-23-5
Chlorobenzene
ND
ug/kg
9.6
1.8
1
02/15/22 21:19
02/17/22 19:51
108-90-7
Chloroethane
ND
ug/kg
19.2
7.4
1
02/15/22 21:19
02/17/22 19:51
75-00-3
Chloroform
ND
ug/kg
9.6
5.8
1
02/15/22 21:19
02/17/22 19:51
67-66-3
Chloromethane
ND
ug/kg
19.2
8.1
1
02/15/22 21:19
02/17/22 19:51
74-87-3
2-Chlorotoluene
ND
ug/kg
9.6
3.4
1
02/15/22 21:19
02/17/22 19:51
95-49-8
4-Chlorotoluene
ND
ug/kg
9.6
1.7
1
02/15/22 21:19
02/17/22 19:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.6
3.7
1
02/15/22 21:19
02/17/22 19:51
96-12-8
Dibromochloromethane
ND
ug/kg
9.6
5.4
1
02/15/22 21:19
02/17/22 19:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.6
4.2
1
02/15/22 21:19
02/17/22 19:51
106-93-4
Dibromomethane
ND
ug/kg
9.6
2.1
1
02/15/22 21:19
02/17/22 19:51
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.6
3.5
1
02/15/22 21:19
02/17/22 19:51
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.6
3.0
1
02/15/22 21:19
02/17/22 19:51
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.6
2.5
1
02/15/22 21:19
02/17/22 19:51
106-46-7
Dichlorodifluoromethane
ND
ug/kg
19.2
4.2
1
02/15/22 21:19
02/17/22 19:51
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.6
4.0
1
02/15/22 21:19
02/17/22 19:51
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.6
6.4
1
02/15/22 21:19
02/17/22 19:51
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.6
4.0
1
02/15/22 21:19
02/17/22 19:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.6
3.3
1
02/15/22 21:19
02/17/22 19:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.6
3.4
1
02/15/22 21:19
02/17/22 19:51
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.6
2.9
1
02/15/22 21:19
02/17/22 19:51
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.6
3.0
1
02/15/22 21:19
02/17/22 19:51
142-28-9
2,2-Dichloropropane
ND
ug/kg
9.6
3.1
1
02/15/22 21:19
02/17/22 19:51
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.6
4.6
1
02/15/22 21:19
02/17/22 19:51
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.6
2.6
1
02/15/22 21:19
02/17/22 19:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.6
3.3
1
02/15/22 21:19
02/17/22 19:51
10061-02-6
Diisopropyl ether
ND
ug/kg
9.6
2.6
1
02/15/22 21:19
02/17/22 19:51
108-20-3
Ethylbenzene
ND
ug/kg
9.6
4.5
1
02/15/22 21:19
02/17/22 19:51
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
19.2
15.7
1
02/15/22 21:19
02/17/22 19:51
87-68-3
2-Hexanone
ND
ug/kg
95.9
9.2
1
02/15/22 21:19
02/17/22 19:51
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
9.6
3.3
1
02/15/22 21:19
02/17/22 19:51
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.6
4.7
1
02/15/22 21:19
02/17/22 19:51
99-87-6
Methylene Chloride
ND
ug/kg
38.4
26.3
1
02/15/22 21:19
02/17/22 19:51
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-13
Lab ID:
92588327011
Collected:
02/14/22
16:30
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
95.9
9.2
1
02/15/22 21:19
02/17/22 19:51
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.6
3.6
1
02/15/22 21:19
02/17/22 19:51
1634-04-4
Naphthalene
ND
ug/kg
9.6
5.0
1
02/15/22 21:19
02/17/22 19:51
91-20-3
n-Propylbenzene
ND
ug/kg
9.6
3.4
1
02/15/22 21:19
02/17/22 19:51
103-65-1
Styrene
ND
ug/kg
9.6
2.5
1
02/15/22 21:19
02/17/22 19:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
9.6
3.7
1
02/15/22 21:19
02/17/22 19:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
9.6
2.5
1
02/15/22 21:19
02/17/22 19:51
79-34-5
Tetrachloroethene
ND
ug/kg
9.6
3.0
1
02/15/22 21:19
02/17/22 19:51
127-18-4
Toluene
ND
ug/kg
9.6
2.7
1
02/15/22 21:19
02/17/22 19:51
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
9.6
7.8
1
02/15/22 21:19
02/17/22 19:51
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
9.6
8.1
1
02/15/22 21:19
02/17/22 19:51
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
9.6
5.0
1
02/15/22 21:19
02/17/22 19:51
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
9.6
3.2
1
02/15/22 21:19
02/17/22 19:51
79-00-5
Trichloroethene
ND
ug/kg
9.6
2.5
1
02/15/22 21:19
02/17/22 19:51
79-01-6
Trichlorofluoromethane
ND
ug/kg
9.6
5.3
1
02/15/22 21:19
02/17/22 19:51
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
9.6
4.9
1
02/15/22 21:19
02/17/22 19:51
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
9.6
2.6
1
02/15/22 21:19
02/17/22 19:51
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
9.6
3.2
1
02/15/22 21:19
02/17/22 19:51
108-67-8
Vinyl acetate
ND
ug/kg
95.9
7.0
1
02/15/22 21:19
02/17/22 19:51
108-05-4
Vinyl chloride
ND
ug/kg
19.2
4.9
1
02/15/22 21:19
02/17/22 19:51
75-01-4 v2
Xylene (Total)
ND
ug/kg
19.2
5.5
1
02/15/22 21:19
02/17/22 19:51
1330-20-7
m&p-Xylene
ND
ug/kg
19.2
6.6
1
02/15/22 21:19
02/17/22 19:51
179601-23-1
o-Xylene
ND
ug/kg
9.6
4.2
1
02/15/22 21:19
02/17/22 19:51
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
02/15/22 21:19
02/17/22 19:51
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
02/15/22 21:19
02/17/22 19:51
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/15/22 21:19
02/17/22 19:51
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
25.3
%
0.10
0.10
1
02/15/22 17:11
N2
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written
consent of Pace Analytical Services, LLC.
Page 43 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services - Charlotte
Aliphatic (C05-CO8)
ND
mg/kg
5.1
5.1
1
02/16/22 13:41
02/16/22 20:48
Aliphatic(C09-C12) Adjusted
ND
mg/kg
5.1
5.1
1
02/16/22 13:41
02/16/22 20:48
Aromatic (C09-C10)
ND
mg/kg
5.1
5.1
1
02/16/22 13:41
02/16/22 20:48
Surrogates
4-Bromofluorobenzene (FID) (S)
99
%
70-130
1
02/16/22 13:41
02/16/22 20:48
460-00-4
4-Bromofluorobenzene (PID) (S)
85
%
70-130
1
02/16/22 13:41
02/16/22 20:48
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
448
158
1
02/16/22 11:33
02/17/22 15:35
83-32-9
Acenaphthylene
ND
ug/kg
448
158
1
02/16/22 11:33
02/17/22 15:35
208-96-8
Aniline
ND
ug/kg
448
175
1
02/16/22 11:33
02/17/22 15:35
62-53-3
Anthracene
ND
ug/kg
448
147
1
02/16/22 11:33
02/17/22 15:35
120-12-7
Benzo(a)anthracene
ND
ug/kg
448
149
1
02/16/22 11:33
02/17/22 15:35
56-55-3
Benzo(a)pyrene
ND
ug/kg
448
155
1
02/16/22 11:33
02/17/22 15:35
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
448
149
1
02/16/22 11:33
02/17/22 15:35
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
448
174
1
02/16/22 11:33
02/17/22 15:35
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
448
158
1
02/16/22 11:33
02/17/22 15:35
207-08-9
Benzoic Acid
ND
ug/kg
2240
963
1
02/16/22 11:33
02/17/22 15:35
65-85-0
Benzyl alcohol
ND
ug/kg
896
339
1
02/16/22 11:33
02/17/22 15:35
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
448
172
1
02/16/22 11:33
02/17/22 15:35
101-55-3
Butylbenzylphthalate
ND
ug/kg
448
189
1
02/16/22 11:33
02/17/22 15:35
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
896
315
1
02/16/22 11:33
02/17/22 15:35
59-50-7
4-Chloroaniline
ND
ug/kg
896
352
1
02/16/22 11:33
02/17/22 15:35
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
448
186
1
02/16/22 11:33
02/17/22 15:35
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
448
168
1
02/16/22 11:33
02/17/22 15:35
111-44-4
2-Chloronaphthalene
ND
ug/kg
448
178
1
02/16/22 11:33
02/17/22 15:35
91-58-7
2-Chlorophenol
ND
ug/kg
448
168
1
02/16/22 11:33
02/17/22 15:35
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
448
167
1
02/16/22 11:33
02/17/22 15:35
7005-72-3
Chrysene
ND
ug/kg
448
163
1
02/16/22 11:33
02/17/22 15:35
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
448
172
1
02/16/22 11:33
02/17/22 15:35
53-70-3
Dibenzofuran
ND
ug/kg
448
162
1
02/16/22 11:33
02/17/22 15:35
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
448
162
1
02/16/22 11:33
02/17/22 15:35
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
448
159
1
02/16/22 11:33
02/17/22 15:35
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
448
171
1
02/16/22 11:33
02/17/22 15:35
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
896
303
1
02/16/22 11:33
02/17/22 15:35
91-94-1
2,4-Dichlorophenol
ND
ug/kg
448
175
1
02/16/22 11:33
02/17/22 15:35
120-83-2
Diethylphthalate
ND
ug/kg
448
164
1
02/16/22 11:33
02/17/22 15:35
84-66-2
2,4-Dimethylphenol
ND
ug/kg
448
186
1
02/16/22 11:33
02/17/22 15:35
105-67-9
Dimethylphthalate
ND
ug/kg
448
163
1
02/16/22 11:33
02/17/22 15:35
131-11-3
Di-n-butylphthalate
ND
ug/kg
448
151
1
02/16/22 11:33
02/17/22 15:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
896
418
1
02/16/22 11:33
02/17/22 15:35
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2240
1390
1
02/16/22 11:33
02/17/22 15:35
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
448
172
1
02/16/22 11:33
02/17/22 15:35
121-14-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
IL
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,6-Dinitrotoluene
ND
ug/kg
448
164
1
02/16/22 11:33
02/17/22 15:35
606-20-2
Di-n-octylphthalate
ND
ug/kg
448
177
1
02/16/22 11:33
02/17/22 15:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
448
174
1
02/16/22 11:33
02/17/22 15:35
117-81-7
Fluoranthene
ND
ug/kg
448
153
1
02/16/22 11:33
02/17/22 15:35
206-44-0
Fluorene
ND
ug/kg
448
158
1
02/16/22 11:33
02/17/22 15:35
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
448
194
1
02/16/22 11:33
02/17/22 15:35
87-68-3
Hexachlorobenzene
ND
ug/kg
448
175
1
02/16/22 11:33
02/17/22 15:35
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
448
257
1
02/16/22 11:33
02/17/22 15:35
77-47-4
Hexachloroethane
ND
ug/kg
448
171
1
02/16/22 11:33
02/17/22 15:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
448
177
1
02/16/22 11:33
02/17/22 15:35
193-39-5
Isophorone
ND
ug/kg
448
200
1
02/16/22 11:33
02/17/22 15:35
78-59-1
1-Methylnaphthalene
ND
ug/kg
448
158
1
02/16/22 11:33
02/17/22 15:35
90-12-0
2-Methylnaphthalene
ND
ug/kg
448
179
1
02/16/22 11:33
02/17/22 15:35
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
448
183
1
02/16/22 11:33
02/17/22 15:35
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
448
181
1
02/16/22 11:33
02/17/22 15:35
15831-10-4
Naphthalene
ND
ug/kg
448
152
1
02/16/22 11:33
02/17/22 15:35
91-20-3
2-Nitroaniline
ND
ug/kg
2240
367
1
02/16/22 11:33
02/17/22 15:35
88-74-4
3-Nitroaniline
ND
ug/kg
2240
352
1
02/16/22 11:33
02/17/22 15:35
99-09-2
4-Nitroaniline
ND
ug/kg
896
341
1
02/16/22 11:33
02/17/22 15:35
100-01-6
Nitrobenzene
ND
ug/kg
448
208
1
02/16/22 11:33
02/17/22 15:35
98-95-3
2-Nitrophenol
ND
ug/kg
448
194
1
02/16/22 11:33
02/17/22 15:35
88-75-5
4-Nitrophenol
ND
ug/kg
2240
866
1
02/16/22 11:33
02/17/22 15:35
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
448
151
1
02/16/22 11:33
02/17/22 15:35
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
448
168
1
02/16/22 11:33
02/17/22 15:35
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
448
159
1
02/16/22 11:33
02/17/22 15:35
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
448
213
1
02/16/22 11:33
02/17/22 15:35
108-60-1
Pentachlorophenol
ND
ug/kg
896
439
1
02/16/22 11:33
02/17/22 15:35
87-86-5
Phenanthrene
ND
ug/kg
448
147
1
02/16/22 11:33
02/17/22 15:35
85-01-8
Phenol
ND
ug/kg
448
200
1
02/16/22 11:33
02/17/22 15:35
108-95-2
Pyrene
ND
ug/kg
448
182
1
02/16/22 11:33
02/17/22 15:35
129-00-0
Pyridine
ND
ug/kg
448
141
1
02/16/22 11:33
02/17/22 15:35
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
448
177
1
02/16/22 11:33
02/17/22 15:35
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
448
205
1
02/16/22 11:33
02/17/22 15:35
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
448
185
1
02/16/22 11:33
02/17/22 15:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
21-130
1
02/16/22 11:33
02/17/22 15:35
4165-60-0
2-Fluorobiphenyl (S)
51
%
19-130
1
02/16/22 11:33
02/17/22 15:35
321-60-8
Terphenyl-d14 (S)
56
%
15-130
1
02/16/22 11:33
02/17/22 15:35
1718-51-0
Phenol-d6 (S)
61
%
18-130
1
02/16/22 11:33
02/17/22 15:35
13127-88-3
2-Fluorophenol (S)
60
%
18-130
1
02/16/22 11:33
02/17/22 15:35
367-12-4
2,4,6-Tribromophenol (S)
57
%
18-130
1
02/16/22 11:33
02/17/22 15:35
118-79-6
REPORT OF LABORATORY ANALYSIS
v1
v1
v1
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-F Lab ID: 92588327012 Collected: 02/14/22 16:40 Received: 02/15/22 14:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
190
61.0
1
02/15/22 21:19
02/17/22 20:09
67-64-1
Benzene
ND
ug/kg
9.5
3.8
1
02/15/22 21:19
02/17/22 20:09
71-43-2
Bromobenzene
ND
ug/kg
9.5
3.1
1
02/15/22 21:19
02/17/22 20:09
108-86-1
Bromochloromethane
ND
ug/kg
9.5
2.8
1
02/15/22 21:19
02/17/22 20:09
74-97-5
Bromodichloromethane
ND
ug/kg
9.5
3.7
1
02/15/22 21:19
02/17/22 20:09
75-27-4
Bromoform
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 20:09
75-25-2
Bromomethane
ND
ug/kg
19.0
15.0
1
02/15/22 21:19
02/17/22 20:09
74-83-9
2-Butanone (MEK)
ND
ug/kg
190
45.6
1
02/15/22 21:19
02/17/22 20:09
78-93-3
n-Butylbenzene
ND
ug/kg
9.5
4.5
1
02/15/22 21:19
02/17/22 20:09
104-51-8
sec-Butylbenzene
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 20:09
135-98-8
tert-Butyl benzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 20:09
98-06-6
Carbon tetrachloride
ND
ug/kg
9.5
3.6
1
02/15/22 21:19
02/17/22 20:09
56-23-5
Chlorobenzene
ND
ug/kg
9.5
1.8
1
02/15/22 21:19
02/17/22 20:09
108-90-7
Chloroethane
ND
ug/kg
19.0
7.3
1
02/15/22 21:19
02/17/22 20:09
75-00-3
Chloroform
ND
ug/kg
9.5
5.8
1
02/15/22 21:19
02/17/22 20:09
67-66-3
Chloromethane
ND
ug/kg
19.0
8.0
1
02/15/22 21:19
02/17/22 20:09
74-87-3
2-Chlorotoluene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 20:09
95-49-8
4-Chlorotoluene
ND
ug/kg
9.5
1.7
1
02/15/22 21:19
02/17/22 20:09
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.5
3.7
1
02/15/22 21:19
02/17/22 20:09
96-12-8
Dibromochloromethane
ND
ug/kg
9.5
5.3
1
02/15/22 21:19
02/17/22 20:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 20:09
106-93-4
Dibromomethane
ND
ug/kg
9.5
2.0
1
02/15/22 21:19
02/17/22 20:09
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 20:09
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.5
2.9
1
02/15/22 21:19
02/17/22 20:09
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 20:09
106-46-7
Dichlorodifluoromethane
ND
ug/kg
19.0
4.1
1
02/15/22 21:19
02/17/22 20:09
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.5
3.9
1
02/15/22 21:19
02/17/22 20:09
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.5
6.3
1
02/15/22 21:19
02/17/22 20:09
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.5
3.9
1
02/15/22 21:19
02/17/22 20:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 20:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 20:09
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.5
2.9
1
02/15/22 21:19
02/17/22 20:09
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.5
3.0
1
02/15/22 21:19
02/17/22 20:09
142-28-9
2,2-Dichloropropane
ND
ug/kg
9.5
3.1
1
02/15/22 21:19
02/17/22 20:09
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.5
4.6
1
02/15/22 21:19
02/17/22 20:09
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 20:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.5
3.3
1
02/15/22 21:19
02/17/22 20:09
10061-02-6
Diisopropyl ether
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 20:09
108-20-3
Ethylbenzene
ND
ug/kg
9.5
4.4
1
02/15/22 21:19
02/17/22 20:09
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
19.0
15.5
1
02/15/22 21:19
02/17/22 20:09
87-68-3
2-Hexanone
ND
ug/kg
95.0
9.2
1
02/15/22 21:19
02/17/22 20:09
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 20:09
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.5
4.7
1
02/15/22 21:19
02/17/22 20:09
99-87-6
Methylene Chloride
ND
ug/kg
38.0
26.0
1
02/15/22 21:19
02/17/22 20:09
75-09-2
REPORT OF LABORATORY ANALYSIS
IK,L1
v2
v2
v2
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 104
laceAnalytical"
WWW.pacalahs.0 m
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: CCW-006
Pace Project No.: 92588327
Sample: UST-2-SW-F
Lab ID:
92588327012
Collected:
02/14/22
16:40
Received: 02/15/22
14:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
95.0
9.2
1
02/15/22 21:19
02/17/22 20:09
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.5
3.6
1
02/15/22 21:19
02/17/22 20:09
1634-04-4
Naphthalene
ND
ug/kg
9.5
5.0
1
02/15/22 21:19
02/17/22 20:09
91-20-3
n-Propylbenzene
ND
ug/kg
9.5
3.4
1
02/15/22 21:19
02/17/22 20:09
103-65-1
Styrene
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 20:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
9.5
3.6
1
02/15/22 21:19
02/17/22 20:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 20:09
79-34-5
Tetrachloroethene
ND
ug/kg
9.5
3.0
1
02/15/22 21:19
02/17/22 20:09
127-18-4
Toluene
ND
ug/kg
9.5
2.7
1
02/15/22 21:19
02/17/22 20:09
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
9.5
7.7
1
02/15/22 21:19
02/17/22 20:09
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
9.5
8.0
1
02/15/22 21:19
02/17/22 20:09
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
9.5
4.9
1
02/15/22 21:19
02/17/22 20:09
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 20:09
79-00-5
Trichloroethene
ND
ug/kg
9.5
2.5
1
02/15/22 21:19
02/17/22 20:09
79-01-6
Trichlorofluoromethane
ND
ug/kg
9.5
5.2
1
02/15/22 21:19
02/17/22 20:09
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
9.5
4.8
1
02/15/22 21:19
02/17/22 20:09
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
9.5
2.6
1
02/15/22 21:19
02/17/22 20:09
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
9.5
3.2
1
02/15/22 21:19
02/17/22 20:09
108-67-8
Vinyl acetate
ND
ug/kg
95.0
6.9
1
02/15/22 21:19
02/17/22 20:09
108-05-4
Vinyl chloride
ND
ug/kg
19.0
4.8
1
02/15/22 21:19
02/17/22 20:09
75-01-4 v2
Xylene (Total)
ND
ug/kg
19.0
5.4
1
02/15/22 21:19
02/17/22 20:09
1330-20-7
m&p-Xylene
ND
ug/kg
19.0
6.5
1
02/15/22 21:19
02/17/22 20:09
179601-23-1
o-Xylene
ND
ug/kg
9.5
4.2
1
02/15/22 21:19
02/17/22 20:09
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
02/15/22 21:19
02/17/22 20:09
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
02/15/22 21:19
02/17/22 20:09
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/15/22 21:19
02/17/22 20:09
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
27.1
%
0.10
0.10
1
02/15/22 17:11
N2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM
without the written consent of Pace Analytical Services, LLC.
Page 47 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678726
Analysis Method: EPA 8015C
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327001
METHOD BLANK: 3551778
Matrix: Solid
Associated Lab Samples: 92588327001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 1.5
02/16/22 13:18
4-Bromofluorobenzene (S)
%
86 66-131
02/16/22 13:18
LABORATORY CONTROL SAMPLE:
3551779
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.7 48.8 98
70-130
4-Bromofluorobenzene (S)
%
89
66-131
MATRIX SPIKE SAMPLE:
3551781
35696367001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
294 74.9 373
106
70-145
4-Bromofluorobenzene (S)
%
161
66-131 S2
SAMPLE DUPLICATE: 3551780
92588181001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND ND
30
4-Bromofluorobenzene (S)
%
86 84
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 679111
Analysis Method:
EPA 8015C
QC Batch Method: EPA 5030B
Analysis Description:
Gasoline Range Organics
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327002
METHOD BLANK: 3553476
Matrix: Solid
Associated Lab Samples: 92588327002
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
6.0 1.5 02/17/22 13:51
4-Bromofluorobenzene (S)
%
87 66-131
02/17/22 13:51
LABORATORY CONTROL SAMPLE:
3553477
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50 48.3
97 70-130
4-Bromofluorobenzene (S)
%
92 66-131
MATRIX SPIKE SAMPLE:
3553479
92587641001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 61.5
61.5 100
70-145
4-Bromofluorobenzene (S)
%
89
66-131
SAMPLE DUPLICATE: 3553478
35696367002 Dup
Max
Parameter
Units
Result Result
RPD RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
8.9
8.4 5 30
4-Bromofluorobenzene (S)
%
81
81
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 104
laceAnalytical"
WWW.pacalabs.Com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678754 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
METHOD BLANK: 3551916
Matrix:
Solid
Associated Lab Samples: 92588327003, 92588327004,
92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
2.5
2.5 02/16/22 15:29 N2
Aromatic (C09-C10)
mg/kg
ND
2.5
2.5 02/16/22 15:29 N2
4-Bromofluorobenzene (FID) (S)
%
97
70-130
02/16/22 15:29
4-Bromofluorobenzene (PID) (S)
%
83
70-130
02/16/22 15:29
LABORATORY CONTROL SAMPLE & LCSD:
3551917
3551918
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg 14.9
14.4 13.1
97
88
70-130 10 25 N2
Aromatic (C09-C10)
mg/kg 5
4.2 4.2
85
84
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
98
70-130
4-Bromofluorobenzene (PID) (S)
%
84
84
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678538 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
METHOD BLANK: 3551065 Matrix: Solid
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
02/17/22 12:12
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
02/17/22 12:12
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
02/17/22 12:12
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
02/17/22 12:12
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
02/17/22 12:12
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
02/17/22 12:12
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
02/17/22 12:12
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
02/17/22 12:12
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
02/17/22 12:12
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
02/17/22 12:12
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
02/17/22 12:12
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
02/17/22 12:12
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
02/17/22 12:12
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
02/17/22 12:12
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
02/17/22 12:12
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
02/17/22 12:12
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
02/17/22 12:12
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
02/17/22 12:12
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
02/17/22 12:12
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
02/17/22 12:12
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
02/17/22 12:12
2-Butanone (MEK)
ug/kg
ND
100
24.0
02/17/22 12:12
2-Chlorotoluene
ug/kg
ND
5.0
1.8
02/17/22 12:12
2-Hexanone
ug/kg
ND
50.0
4.8
02/17/22 12:12
4-Chlorotoluene
ug/kg
ND
5.0
0.88
02/17/22 12:12
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
02/17/22 12:12
Acetone
ug/kg
ND
100
32.1
02/17/22 12:12
Benzene
ug/kg
ND
5.0
2.0
02/17/22 12:12
Bromobenzene
ug/kg
ND
5.0
1.6
02/17/22 12:12
Bromochloromethane
ug/kg
ND
5.0
1.5
02/17/22 12:12
Bromodichloromethane
ug/kg
ND
5.0
1.9
02/17/22 12:12
Bromoform
ug/kg
ND
5.0
1.8
02/17/22 12:12
Bromomethane
ug/kg
ND
10.0
7.9
02/17/22 12:12
Carbon tetrachloride
ug/kg
ND
5.0
1.9
02/17/22 12:12
Chlorobenzene
ug/kg
ND
5.0
0.96
02/17/22 12:12
Chloroethane
ug/kg
ND
10.0
3.9
02/17/22 12:12
Chloroform
ug/kg
ND
5.0
3.0
02/17/22 12:12
Chloromethane
ug/kg
ND
10.0
4.2
02/17/22 12:12
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
02/17/22 12:12
IK
v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
METHOD BLANK: 3551065 Matrix: Solid
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
02/17/22 12:12
Dibromochloromethane
ug/kg
ND
5.0
2.8
02/17/22 12:12
Dibromomethane
ug/kg
ND
5.0
1.1
02/17/22 12:12
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
02/17/22 12:12
Diisopropyl ether
ug/kg
ND
5.0
1.4
02/17/22 12:12
Ethylbenzene
ug/kg
ND
5.0
2.3
02/17/22 12:12
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
02/17/22 12:12
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
02/17/22 12:12
m&p-Xylene
ug/kg
ND
10.0
3.4
02/17/22 12:12
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
02/17/22 12:12
Methylene Chloride
ug/kg
ND
20.0
13.7
02/17/22 12:12
n-Butylbenzene
ug/kg
ND
5.0
2.4
02/17/22 12:12
n-Propylbenzene
ug/kg
ND
5.0
1.8
02/17/22 12:12
Naphthalene
ug/kg
ND
5.0
2.6
02/17/22 12:12
o-Xylene
ug/kg
ND
5.0
2.2
02/17/22 12:12
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
02/17/22 12:12
sec-Butylbenzene
ug/kg
ND
5.0
2.2
02/17/22 12:12
Styrene
ug/kg
ND
5.0
1.3
02/17/22 12:12
tert-Butyl benzene
ug/kg
ND
5.0
1.8
02/17/22 12:12
Tetrachloroethene
ug/kg
ND
5.0
1.6
02/17/22 12:12
Toluene
ug/kg
ND
5.0
1.4
02/17/22 12:12
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
02/17/22 12:12
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
02/17/22 12:12
Trichloroethene
ug/kg
ND
5.0
1.3
02/17/22 12:12
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
02/17/22 12:12
Vinyl acetate
ug/kg
ND
50.0
3.6
02/17/22 12:12
Vinyl chloride
ug/kg
ND
10.0
2.5
02/17/22 12:12
Xylene (Total)
ug/kg
ND
10.0
2.8
02/17/22 12:12
1,2-Dichloroethane-d4 (S)
%
109
70-130
02/17/22 12:12
4-Bromofluorobenzene (S)
%
102
69-134
02/17/22 12:12
Toluene-d8 (S)
%
102
70-130
02/17/22 12:12
v2
v2
LABORATORY CONTROL SAMPLE:
3551066
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1120
90
70-130
1,1,1-Trichloroethane
ug/kg
1250
1090
87
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1050
84
70-130
1,1,2-Trichloroethane
ug/kg
1250
1090
87
70-130
1,1-Dichloroethane
ug/kg
1250
1070
85
70-130
1,1-Dichloroethene
ug/kg
1250
1100
88
70-130
1,1-Dichloropropene
ug/kg
1250
1080
87
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1140
91
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: CCW-006
Pace Project No.: 92588327
LABORATORY CONTROL SAMPLE: 3551066
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,2,3-Trichloropropane
ug/kg
1250
1060
85
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1150
92
68-130
1,2,4-Trimethylbenzene
ug/kg
1250
1070
86
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1100
88
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1060
85
70-130
1,2-Dichlorobenzene
ug/kg
1250
1100
88
70-130
1,2-Dichloroethane
ug/kg
1250
1070
86
63-130
1,2-Dichloropropane
ug/kg
1250
1080
86
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1120
89
70-130
1,3-Dichlorobenzene
ug/kg
1250
1130
90
70-130
1,3-Dichloropropane
ug/kg
1250
1060
85
70-130
1,4-Dichlorobenzene
ug/kg
1250
1120
89
70-130
2,2-Dichloropropane
ug/kg
1250
1120
89
66-130
2-Butanone (MEK)
ug/kg
2500
2070
83
70-130
2-Chlorotoluene
ug/kg
1250
1090
87
70-130
2-Hexanone
ug/kg
2500
2110
84
70-130
4-Chlorotoluene
ug/kg
1250
1050
84
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2190
88
70-130
Acetone
ug/kg
2500
2160
86
69-130
Benzene
ug/kg
1250
1030
83
70-130
Bromobenzene
ug/kg
1250
1120
90
70-130
Bromochloromethane
ug/kg
1250
1090
87
70-130
Bromodichloromethane
ug/kg
1250
1130
90
69-130
Bromoform
ug/kg
1250
1170
94
70-130
Bromomethane
ug/kg
1250
1830
146
52-130lK,L1
Carbon tetrachloride
ug/kg
1250
1180
94
70-130
Chlorobenzene
ug/kg
1250
1100
88
70-130
Chloroethane
ug/kg
1250
1230
99
65-130 v3
Chloroform
ug/kg
1250
1100
88
70-130
Chloromethane
ug/kg
1250
1120
90
55-130 v3
cis-1,2-Dichloroethene
ug/kg
1250
1090
87
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1080
86
70-130
Dibromochloromethane
ug/kg
1250
1060
85
70-130
Dibromomethane
ug/kg
1250
1120
89
70-130
Dichlorodifluoromethane
ug/kg
1250
1360
109
45-156 v3
Diisopropyl ether
ug/kg
1250
1020
82
70-130
Ethylbenzene
ug/kg
1250
1050
84
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1300
104
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1170
93
70-130
m&p-Xylene
ug/kg
2500
2250
90
70-130
Methyl-tert-butyl ether
ug/kg
1250
1020
82
70-130
Methylene Chloride
ug/kg
1250
1180
95
65-130
n-Butylbenzene
ug/kg
1250
1160
93
67-130
n-Propylbenzene
ug/kg
1250
1070
86
70-130
Naphthalene
ug/kg
1250
1070
85
70-130
o-Xylene
ug/kg
1250
1120
89
70-130
p-Isopropyltoluene
ug/kg
1250
1170
94
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
LABORATORY CONTROL SAMPLE:
Parameter
3551066
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
sec-Butylbenzene
ug/kg
1250
1120
90
69-130
Styrene
ug/kg
1250
1160
93
70-130
tert-Butyl benzene
ug/kg
1250
1100
88
67-130
Tetrachloroethene
ug/kg
1250
1080
87
70-130
Toluene
ug/kg
1250
1070
86
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1090
87
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1130
90
68-130
Trichloroethene
ug/kg
1250
1060
84
70-130
Trichlorofluoromethane
ug/kg
1250
1060
85
70-130
Vinyl acetate
ug/kg
2500
2510
101
70-130
Vinyl chloride
ug/kg
1250
1130
90
61-130 v3
Xylene (Total)
ug/kg
3750
3360
90
70-130
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
3551067
Units
92588327003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
1160
892
77
70-131
1,1,1-Trichloroethane
ug/kg
ND
1160
907
78
65-133
1,1,2,2-Tetrachloroethane
ug/kg
ND
1160
816
70
66-130
1,1,2-Trichloroethane
ug/kg
ND
1160
855
73
66-133
1,1-Dichloroethane
ug/kg
ND
1160
906
78
65-130
1,1-Dichloroethene
ug/kg
ND
1160
916
79
10-158
1,1-Dichloropropene
ug/kg
ND
1160
879
75
68-133
1,2,3-Trichlorobenzene
ug/kg
ND
1160
905
78
27-138
1,2,3-Trichloropropane
ug/kg
ND
1160
764
66
67-130 M1
1,2,4-Trichlorobenzene
ug/kg
ND
1160
867
74
51-134
1,2,4-Trimethylbenzene
ug/kg
6.1J
1160
814
69
63-136
1,2-Dibromo-3-chloropropane
ug/kg
ND
1160
760
65
32-130
1,2-Dibromoethane (EDB)
ug/kg
ND
1160
881
76
70-130
1,2-Dichlorobenzene
ug/kg
ND
1160
883
76
69-130
1,2-Dichloroethane
ug/kg
ND
1160
864
74
59-130
1,2-Dichloropropane
ug/kg
ND
1160
877
75
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
1160
861
74
65-137
1,3-Dichlorobenzene
ug/kg
ND
1160
883
76
70-130
1,3-Dichloropropane
ug/kg
ND
1160
876
75
70-130
1,4-Dichlorobenzene
ug/kg
ND
1160
828
71
68-130
2,2-Dichloropropane
ug/kg
ND
1160
612
53
32-130
2-Butanone (MEK)
ug/kg
ND
2330
1600
69
10-136
2-Chlorotoluene
ug/kg
ND
1160
825
71
69-141
2-Hexanone
ug/kg
ND
2330
1510
65
10-144
4-Chlorotoluene
ug/kg
ND
1160
770
66
70-132 M1
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
2330
1620
70
25-143
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
MATRIX SPIKE SAMPLE:
3551067
92588327003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Acetone
ug/kg
ND
2330
1440
62
10-130
Benzene
ug/kg
6.9J
1160
894
76
67-130
Bromobenzene
ug/kg
ND
1160
898
77
70-130
Bromochloromethane
ug/kg
ND
1160
877
75
69-134
Bromodichloromethane
ug/kg
ND
1160
875
75
64-130
Bromoform
ug/kg
ND
1160
788
68
62-130
Bromomethane
ug/kg
ND
1160
742
64
20-1761K
Carbon tetrachloride
ug/kg
ND
1160
924
79
65-140
Chlorobenzene
ug/kg
ND
1160
896
77
70-130
Chloroethane
ug/kg
ND
1160
449
39
10-130 v3
Chloroform
ug/kg
ND
1160
920
79
63-130
Chloromethane
ug/kg
ND
1160
930
80
58-130 v3
cis-1,2-Dichloroethene
ug/kg
ND
1160
899
77
66-130
cis-1,3-Dichloropropene
ug/kg
ND
1160
797
68
67-130
Dibromochloromethane
ug/kg
ND
1160
796
68
67-130
Dibromomethane
ug/kg
ND
1160
899
77
63-131
Dichlorodifluoromethane
ug/kg
ND
1160
858
74
44-180 v3
Diisopropyl ether
ug/kg
ND
1160
823
71
63-130
Ethylbenzene
ug/kg
6.OJ
1160
842
72
66-130
Hexachloro-1,3-butadiene
ug/kg
ND
1160
882
76
64-150
Isopropylbenzene (Cumene)
ug/kg
ND
1160
915
79
69-135
m&p-Xylene
ug/kg
11.3J
2330
1780
76
60-133
Methyl-tert-butyl ether
ug/kg
ND
1160
834
72
65-130
Methylene Chloride
ug/kg
ND
1160
961
81
61-130
n-Butylbenzene
ug/kg
ND
1160
761
65
65-140
n-Propylbenzene
ug/kg
ND
1160
784
67
67-140
Naphthalene
ug/kg
17.7
1160
877
74
15-145
o-Xylene
ug/kg
6.2J
1160
891
76
66-133
p-Isopropyltoluene
ug/kg
ND
1160
838
72
56-147
sec-Butylbenzene
ug/kg
ND
1160
850
73
65-139
Styrene
ug/kg
ND
1160
896
77
70-132
tert-Butyl benzene
ug/kg
ND
1160
878
75
62-135
Tetrachloroethene
ug/kg
ND
1160
813
70
70-135
Toluene
ug/kg
19.7
1160
911
77
67-130
trans-1,2-Dichloroethene
ug/kg
ND
1160
917
79
69-130
trans- 1,3-Dichloropropene
ug/kg
ND
1160
819
70
62-130
Trichloroethene
ug/kg
ND
1160
891
77
70-135
Trichlorofluoromethane
ug/kg
ND
1160
579
50
10-130
Vinyl acetate
ug/kg
ND
2330
1780
76
53-130
Vinyl chloride
ug/kg
ND
1160
843
72
61-148 v3
Xylene (Total)
ug/kg
17AJ
3500
2670
76
63-132
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
100
69-134
Toluene-d8 (S)
%
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
SAMPLE DUPLICATE: 3551068
Parameter
Units
92588327004
Result
Dup
Result
Max
RPD RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
76.6
76.4
0 30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
32.7
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
301K
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30 v2
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30 v2
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30 v2
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
10.8
11.3
5 30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
6.5J
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
SAMPLE DUPLICATE: 3551068
Parameter
Units
92588327004
Result
Dup
Result
m&p-Xylene
ug/kg
34.9
34.6
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
65.3
70.3
o-Xylene
ug/kg
18.7
17.9
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
8.91
9.9
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
53.6
52.4
1,2-Dichloroethane-d4 (S)
%
95
93
4-Bromofluorobenzene (S)
%
104
99
Toluene-d8 (S)
%
99
99
RPD
Max
RPD Qualifiers
1
30
30
30
30
30
7
30
5
30
30
30
30
30
30
30
30
30
30
30
30
30 v2
2
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678539
Analysis Method: EPA 8015C
QC Batch Method: EPA 3546
Analysis Description: 8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327001, 92588327002
METHOD BLANK: 3551069
Matrix: Solid
Associated Lab Samples: 92588327001, 92588327002
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 5.0 3.6
02/16/22 13:28
n-Pentacosane (S)
%
77 32-130
02/16/22 13:28
LABORATORY CONTROL SAMPLE:
3551070
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
67.1 50.0 74
47-130
n-Pentacosane (S)
%
79
32-130
MATRIX SPIKE SAMPLE:
3551071
92588181001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 87.4 72.8
77
10-133
n-Pentacosane(S)
%
74
32-130
SAMPLE DUPLICATE: 3551072
92588041001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
26600 26500 0
30
n-Pentacosane (S)
%
0 0
S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678638 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
METHOD BLANK: 3551319 Matrix: Solid
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
333
131
02/17/22 08:54
1,2-Dichlorobenzene
ug/kg
ND
333
120
02/17/22 08:54
1,3-Dichlorobenzene
ug/kg
ND
333
118
02/17/22 08:54
1,4-Dichlorobenzene
ug/kg
ND
333
127
02/17/22 08:54
1-Methylnaphthalene
ug/kg
ND
333
117
02/17/22 08:54
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
333
159
02/17/22 08:54
2,4,5-Trichlorophenol
ug/kg
ND
333
153
02/17/22 08:54
2,4,6-Trichlorophenol
ug/kg
ND
333
137
02/17/22 08:54
2,4-DichIorophenol
ug/kg
ND
333
130
02/17/22 08:54
2,4-Dimethylphenol
ug/kg
ND
333
138
02/17/22 08:54
2,4-Dinitrophenol
ug/kg
ND
1670
1030
02/17/22 08:54
2,4-Dinitrotoluene
ug/kg
ND
333
128
02/17/22 08:54
2,6-Dinitrotoluene
ug/kg
ND
333
122
02/17/22 08:54
2-Chloronaphthalene
ug/kg
ND
333
132
02/17/22 08:54
2-Chlorophenol
ug/kg
ND
333
125
02/17/22 08:54
2-Methylnaphthalene
ug/kg
ND
333
133
02/17/22 08:54
2-Methylphenol(o-Cresol)
ug/kg
ND
333
136
02/17/22 08:54
2-Nitroaniline
ug/kg
ND
1670
273
02/17/22 08:54
2-Nitrophenol
ug/kg
ND
333
144
02/17/22 08:54
3&4-Methylphenol (m&p Cresol)
ug/kg
ND
333
134
02/17/22 08:54
3,3'-Dichlorobenzidine
ug/kg
ND
667
225
02/17/22 08:54
3-Nitroaniline
ug/kg
ND
1670
262
02/17/22 08:54
4,6-Dinitro-2-methyl phenol
ug/kg
ND
667
311
02/17/22 08:54
4-Bromophenylphenyl ether
ug/kg
ND
333
128
02/17/22 08:54
4-Chloro-3-methyl phenol
ug/kg
ND
667
234
02/17/22 08:54
4-Chloroaniline
ug/kg
ND
667
262
02/17/22 08:54
4-Chlorophenylphenyl ether
ug/kg
ND
333
124
02/17/22 08:54
4-Nitroaniline
ug/kg
ND
667
254
02/17/22 08:54
4-Nitrophenol
ug/kg
ND
1670
644
02/17/22 08:54
Acenaphthene
ug/kg
ND
333
117
02/17/22 08:54
Acenaphthylene
ug/kg
ND
333
117
02/17/22 08:54
Aniline
ug/kg
ND
333
130
02/17/22 08:54
Anthracene
ug/kg
ND
333
109
02/17/22 08:54
Benzo(a)anthracene
ug/kg
ND
333
111
02/17/22 08:54
Benzo(a)pyrene
ug/kg
ND
333
115
02/17/22 08:54
Benzo(b)fluoranthene
ug/kg
ND
333
111
02/17/22 08:54
Benzo(g,h,i)perylene
ug/kg
ND
333
129
02/17/22 08:54
Benzo(k)fluoranthene
ug/kg
ND
333
117
02/17/22 08:54
Benzoic Acid
ug/kg
ND
1670
716
02/17/22 08:54
IL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
METHOD BLANK: 3551319 Matrix: Solid
Associated Lab Samples: 92588327003, 92588327004, 92588327005, 92588327006, 92588327007, 92588327008, 92588327009,
92588327010,92588327011,92588327012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Benzyl alcohol
ug/kg
ND
667
253
02/17/22 08:54
bis(2-Chloroethoxy)methane
ug/kg
ND
333
138
02/17/22 08:54
bis(2-Chloroethyl) ether
ug/kg
ND
333
125
02/17/22 08:54
bis(2-Ethylhexyl)phthalate
ug/kg
ND
333
129
02/17/22 08:54
Butylbenzylphthalate
ug/kg
ND
333
140
02/17/22 08:54
Chrysene
ug/kg
ND
333
121
02/17/22 08:54
Di-n-butylphthalate
ug/kg
ND
333
112
02/17/22 08:54
Di-n-octylphthalate
ug/kg
ND
333
131
02/17/22 08:54
Dibenz(a,h)anthracene
ug/kg
ND
333
128
02/17/22 08:54
Dibenzofuran
ug/kg
ND
333
120
02/17/22 08:54
Diethylphthalate
ug/kg
ND
333
122
02/17/22 08:54
Dimethylphthalate
ug/kg
ND
333
121
02/17/22 08:54
Fluoranthene
ug/kg
ND
333
114
02/17/22 08:54
Fluorene
ug/kg
ND
333
117
02/17/22 08:54
Hexachloro-1,3-butadiene
ug/kg
ND
333
144
02/17/22 08:54
Hexachlorobenzene
ug/kg
ND
333
130
02/17/22 08:54
Hexachlorocyclopentadiene
ug/kg
ND
333
191
02/17/22 08:54
Hexachloroethane
ug/kg
ND
333
127
02/17/22 08:54
Indeno(1,2,3-cd)pyrene
ug/kg
ND
333
131
02/17/22 08:54
Isophorone
ug/kg
ND
333
148
02/17/22 08:54
N-Nitroso-di-n-propylamine
ug/kg
ND
333
125
02/17/22 08:54
N-Nitrosodimethylamine
ug/kg
ND
333
112
02/17/22 08:54
N-Nitrosodiphenylamine
ug/kg
ND
333
118
02/17/22 08:54
Naphthalene
ug/kg
ND
333
113
02/17/22 08:54
Nitrobenzene
ug/kg
ND
333
155
02/17/22 08:54
Pentachlorophenol
ug/kg
ND
667
326
02/17/22 08:54
Phenanthrene
ug/kg
ND
333
109
02/17/22 08:54
Phenol
ug/kg
ND
333
148
02/17/22 08:54
Pyrene
ug/kg
ND
333
135
02/17/22 08:54
Pyridine
ug/kg
ND
333
105
02/17/22 08:54
2,4,6-Tribromophenol (S)
%
70
18-130
02/17/22 08:54
2-Fluorobiphenyl (S)
%
64
19-130
02/17/22 08:54
2-Fluorophenol(S)
%
69
18-130
02/17/22 08:54
Nitrobenzene-d5 (S)
%
67
21-130
02/17/22 08:54
Phenol-d6 (S)
%
72
18-130
02/17/22 08:54
Terphenyl-d14 (S)
%
70
15-130
02/17/22 08:54
v1
v1
v1
LABORATORY CONTROL SAMPLE:
3551320
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
1170 69 47-130
1,2-Dichlorobenzene
ug/kg
1680
1110 66 49-130
1,3-Dichlorobenzene
ug/kg
1680
1070 64 48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
LABORATORY CONTROL SAMPLE:
Parameter
3551320
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/kg
1680
1090
64
49-130
1-Methylnaphthalene
ug/kg
1680
1250
74
54-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
1210
72
38-130
2,4,5-Trichlorophenol
ug/kg
1680
1370
81
49-130
2,4,6-Trichlorophenol
ug/kg
1680
1380
82
50-130
2,4-Dichlorophenol
ug/kg
1680
1320
78
51-130
2,4-Dimethylphenol
ug/kg
1680
1310
78
53-130
2,4-Dinitrophenol
ug/kg
8420
6990
83
39-130
2,4-Dinitrotoluene
ug/kg
1680
1510
90
53-130
2,6-Dinitrotoluene
ug/kg
1680
1480
88
55-130
2-Chloronaphthalene
ug/kg
1680
1290
77
48-130
2-Chlorophenol
ug/kg
1680
1170
69
54-130
2-Methylnaphthalene
ug/kg
1680
1280
76
57-130
2-Methylphenol(o-Cresol)
ug/kg
1680
1260
75
50-130
2-Nitroaniline
ug/kg
3370
2750
82
49-130
2-Nitrophenol
ug/kg
1680
1290
77
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1350
80
50-130
3,3'-Dichlorobenzidine
ug/kg
3370
2500
74
47-130IL
3-Nitroaniline
ug/kg
3370
2820
84
45-130
4,6-Dinitro-2-methyl phenol
ug/kg
3370
2970
88
50-142
4-Bromophenylphenyl ether
ug/kg
1680
1350
80
55-130
4-ChIoro-3-methyl phenol
ug/kg
3370
2740
81
52-130
4-Chloroaniline
ug/kg
3370
2460
73
49-130
4-Chlorophenylphenyl ether
ug/kg
1680
1340
80
53-130
4-Nitroaniline
ug/kg
3370
2780
83
51-130
4-Nitrophenol
ug/kg
8420
7330
87
40-130
Acenaphthene
ug/kg
1680
1390
82
56-130
Acenaphthylene
ug/kg
1680
1320
79
58-130
Aniline
ug/kg
1680
1120
66
44-130
Anthracene
ug/kg
1680
1340
80
60-130
Benzo(a)anthracene
ug/kg
1680
1400
83
59-130
Benzo(a)pyrene
ug/kg
1680
1380
82
57-130
Benzo(b)fluoranthene
ug/kg
1680
1320
78
54-130
Benzo(g,h,i)perylene
ug/kg
1680
1310
78
59-130
Benzo(k)fluoranthene
ug/kg
1680
1400
83
54-130
Benzoic Acid
ug/kg
8420
5010
60
19-130
Benzyl alcohol
ug/kg
3370
2500
74
50-130
bis(2-Chloroethoxy)methane
ug/kg
1680
1280
76
55-130
bis(2-Chloroethyl) ether
ug/kg
1680
1170
70
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1530
91
58-130
Butylbenzylphthalate
ug/kg
1680
1560
93
46-138
Chrysene
ug/kg
1680
1410
84
57-130
Di-n-butylphthalate
ug/kg
1680
1390
83
57-130
Di-n-octylphthalate
ug/kg
1680
1540
91
57-130
Dibenz(a,h)anthracene
ug/kg
1680
1260
75
60-130
Dibenzofuran
ug/kg
1680
1400
83
54-130
Diethylphthalate
ug/kg
1680
1390
82
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 104
laceAnalytical"
WWW.pacalabs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
LABORATORY CONTROL SAMPLE:
Parameter
3551320
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Dimethylphthalate
ug/kg
1680
1400
83
57-130
Fluoranthene
ug/kg
1680
1350
80
57-130
Fluorene
ug/kg
1680
1410
84
56-130
Hexachloro-1,3-butadiene
ug/kg
1680
1050
62
41-130
Hexachlorobenzene
ug/kg
1680
1380
82
53-130
Hexachlorocyclopentadiene
ug/kg
1680
880
52
23-130
Hexachloroethane
ug/kg
1680
1100
65
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1680
1270
76
61-130
Isophorone
ug/kg
1680
1290
77
49-130
N-Nitroso-di-n-propylamine
ug/kg
1680
1290
77
52-130
N-Nitrosodimethylamine
ug/kg
1680
1140
68
45-130 v1
N-Nitrosodiphenylamine
ug/kg
1680
1330
79
56-130
Naphthalene
ug/kg
1680
1170
69
56-130
Nitrobenzene
ug/kg
1680
1220
72
50-130
Pentachlorophenol
ug/kg
3370
2770
82
33-130
Phenanthrene
ug/kg
1680
1410
84
60-130
Phenol
ug/kg
1680
1380
82
54-130 v1
Pyrene
ug/kg
1680
1420
85
61-130
Pyridine
ug/kg
1680
994
59
35-130 v1
2,4,6-Tribromophenol (S)
%
88
18-130
2-Fluorobiphenyl (S)
%
68
19-130
2-Fluorophenol(S)
%
65
18-130
Nitrobenzene-d5(S)
%
67
21-130
Phenol-d6 (S)
%
70
18-130
Terphenyl-d14 (S)
%
71
15-130
MATRIX SPIKE SAMPLE:
Parameter
3551321
Units
92587972001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
2120
1260
60
22-130
1,2-Dichlorobenzene
ug/kg
ND
2120
1240
59
23-130
1,3-Dichlorobenzene
ug/kg
ND
2120
1230
58
26-130
1,4-Dichlorobenzene
ug/kg
ND
2120
1210
57
27-130
1-Methylnaphthalene
ug/kg
ND
2120
1310
62
30-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2120
1370
65
30-130
2,4,5-Trichlorophenol
ug/kg
ND
2120
1500
71
26-130
2,4,6-Trichlorophenol
ug/kg
ND
2120
1520
71
23-130
2,4-Dichlorophenol
ug/kg
ND
2120
1430
67
29-130
2,4-Dimethylphenol
ug/kg
ND
2120
1280
60
13-130
2,4-Dinitrophenol
ug/kg
ND
10600
5610
53
10-131
2,4-Dinitrotoluene
ug/kg
ND
2120
1580
74
28-130
2,6-Dinitrotoluene
ug/kg
ND
2120
1520
72
36-130
2-Chloronaphthalene
ug/kg
ND
2120
1360
64
27-130
2-Chlorophenol
ug/kg
ND
2120
1340
63
29-130
2-Methylnaphthalene
ug/kg
ND
2120
1320
62
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 104
laceAnalytical"
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Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
MATRIX SPIKE SAMPLE:
3551321
92587972001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Methylphenol(o-Cresol)
ug/kg
ND
2120
1340
63
20-130
2-Nitroaniline
ug/kg
ND
4240
2910
69
29-130
2-Nitrophenol
ug/kg
ND
2120
1450
68
26-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
2120
1430
68
10-176
3,3'-Dichlorobenzidine
ug/kg
ND
4240
2530
60
15-130IL
3-Nitroaniline
ug/kg
ND
4240
3020
71
28-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4240
3180
75
15-132
4-Bromophenylphenyl ether
ug/kg
ND
2120
1350
64
35-130
4-Chloro-3-methylphenol
ug/kg
ND
4240
2900
68
30-130
4-Chloroaniline
ug/kg
ND
4240
2530
60
28-130
4-Chlorophenylphenyl ether
ug/kg
ND
2120
1360
64
32-130
4-Nitroaniline
ug/kg
ND
4240
2920
69
30-130
4-Nitrophenol
ug/kg
ND
10600
7860
74
17-130
Acenaphthene
ug/kg
ND
2120
1420
67
29-130
Acenaphthylene
ug/kg
ND
2120
1370
65
31-130
Aniline
ug/kg
ND
2120
1100
52
10-130
Anthracene
ug/kg
ND
2120
1350
64
33-130
Benzo(a)anthracene
ug/kg
ND
2120
1390
65
32-130
Benzo(a)pyrene
ug/kg
ND
2120
1380
65
32-130
Benzo(b)fluoranthene
ug/kg
ND
2120
1340
63
33-130
Benzo(g,h,i)perylene
ug/kg
ND
2120
1340
63
28-130
Benzo(k)fluoranthene
ug/kg
ND
2120
1380
65
31-130
Benzoic Acid
ug/kg
ND
10600
ND
8
10-130 M1
Benzyl alcohol
ug/kg
ND
4240
2700
64
31-130
bis(2-Chloroethoxy)methane
ug/kg
ND
2120
1370
64
30-130
bis(2-Chloroethyl) ether
ug/kg
ND
2120
1300
61
68-130 M1
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2120
1580
75
40-130
Butylbenzylphthalate
ug/kg
ND
2120
1530
72
40-130
Chrysene
ug/kg
ND
2120
1410
66
30-130
Di-n-butylphthalate
ug/kg
ND
2120
1420
67
41-130
Di-n-octylphthalate
ug/kg
ND
2120
1580
74
42-130
Dibenz(a,h)anthracene
ug/kg
ND
2120
1250
59
27-130
Dibenzofuran
ug/kg
ND
2120
1430
67
32-130
Diethylphthalate
ug/kg
ND
2120
1430
67
40-130
Dimethylphthalate
ug/kg
ND
2120
1480
70
37-130
Fluoranthene
ug/kg
ND
2120
1380
65
26-130
Fluorene
ug/kg
ND
2120
1420
67
31-130
Hexachloro-1,3-butadiene
ug/kg
ND
2120
1120
53
20-130
Hexachlorobenzene
ug/kg
ND
2120
1370
64
29-130
Hexachlorocyclopentadiene
ug/kg
ND
2120
896
42
10-130
Hexachloroethane
ug/kg
ND
2120
1240
59
21-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2120
1260
59
28-130
Isophorone
ug/kg
ND
2120
1340
63
32-130
N-Nitroso-di-n-propylamine
ug/kg
ND
2120
1340
63
31-130
N-Nitrosodimethylamine
ug/kg
ND
2120
1280
60
20-130 v1
N-Nitrosodiphenylamine
ug/kg
ND
2120
1370
65
32-130
Naphthalene
ug/kg
ND
2120
1270
60
30-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 104
laceAnalytical"
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
MATRIX SPIKE SAMPLE:
Parameter
3551321
Units
92587972001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Nitrobenzene
ug/kg
ND
2120
1340
63
25-130
Pentachlorophenol
ug/kg
ND
4240
3060
72
10-130
Phenanthrene
ug/kg
ND
2120
1430
67
34-130
Phenol
ug/kg
ND
2120
1490
70
14-130 v1
Pyrene
ug/kg
ND
2120
1400
66
31-130
Pyridine
ug/kg
ND
2120
1170
55
10-130 v1
2,4,6-Tribromophenol (S)
%
69
18-130
2-Fluorobiphenyl (S)
%
48
19-130
2-Fluorophenol (S)
%
56
18-130
Nitrobenzene-d5 (S)
%
59
21-130
Phenol-d6 (S)
%
59
18-130
Terphenyl-d14 (S)
%
53
15-130
SAMPLE DUPLICATE: 3551322
Parameter
Units
92587972002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
ND
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30 IL
3-Nitroaniline
ug/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-Chloro-3-methylphenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC.
Page 64 of 104
laceAnalytical"
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9800 Kincey Ave. Suite 100
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QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
SAMPLE DUPLICATE: 3551322
Parameter
Units
92587972002
Result
Dup
Result
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
Pyridine
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
71
63
2-Fluorobiphenyl (S)
%
57
52
2-Fluorophenol(S)
%
68
62
Nitrobenzene-d5 (S)
%
68
62
Phenol-d6 (S)
%
71
65
Terphenyl-d14 (S)
%
61
56
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30 v1
30
30
30
30
30
30 v1
30
30 v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 104
laceAnalytical"
wwmpacalahs,com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: CCW-006
Pace Project No.: 92588327
QC Batch: 678506 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588327001, 92588327002, 92588327003, 92588327004, 92588327005, 92588327006, 92588327007,
92588327008,92588327009,92588327010,92588327011,92588327012
SAMPLE DUPLICATE: 3550913
92588181001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 23.0 22.5 2 25 N2
SAMPLE DUPLICATE: 3550914
92588098003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 24.4 21.2 14 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC.
Page 66 of 104
laceAnalytical"
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QUALIFIERS
Project: CCW-006
Pace Project No.: 92588327
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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laceAnalyticaf`
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9800 Kincey Ave. Suite 100
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(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CCW-006
92588327
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92588327001
UST-1
EPA 3546
678539
EPA 8015C
678806
92588327002
UST-3
EPA 3546
678539
EPA 8015C
678806
92588327001
UST-1
EPA 5030B
678726
EPA 8015C
678770
92588327002
UST-3
EPA 5030B
679111
EPA 8015C
679131
92588327003
UST-1-B
MADEP VPH
678754
MADEP VPH
678772
92588327004
UST-1-SW-F
MADEP VPH
678754
MADEP VPH
678772
92588327005
UST-1-SW-B
MADEP VPH
678754
MADEP VPH
678772
92588327006
UST-1-SW-R
MADEP VPH
678754
MADEP VPH
678772
92588327007
UST-1-SW-L
MADEP VPH
678754
MADEP VPH
678772
92588327008
UST-2-SW-L
MADEP VPH
678754
MADEP VPH
678772
92588327009
UST-2-B
MADEP VPH
678754
MADEP VPH
678772
92588327010
UST-2-SW-R
MADEP VPH
678754
MADEP VPH
678772
92588327011
UST-2-SW-B
MADEP VPH
678754
MADEP VPH
678772
92588327012
UST-2-SW-F
MADEP VPH
678754
MADEP VPH
678772
92588327003
UST-1-B
EPA 3546
678638
EPA 8270E
679059
92588327004
UST-1-SW-F
EPA 3546
678638
EPA 8270E
679059
92588327005
UST-1-SW-B
EPA 3546
678638
EPA 8270E
679059
92588327006
UST-1-SW-R
EPA 3546
678638
EPA 8270E
679059
92588327007
UST-1-SW-L
EPA 3546
678638
EPA 8270E
679059
92588327008
UST-2-SW-L
EPA 3546
678638
EPA 8270E
679059
92588327009
UST-2-B
EPA 3546
678638
EPA 8270E
679059
92588327010
UST-2-SW-R
EPA 3546
678638
EPA 8270E
679059
92588327011
UST-2-SW-B
EPA 3546
678638
EPA 8270E
679059
92588327012
UST-2-SW-F
EPA 3546
678638
EPA 8270E
679059
92588327003
UST-1-B
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327004
UST-1-SW-F
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327005
UST-1-SW-B
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327006
UST-1-SW-R
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327007
UST-1-SW-L
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327008
UST-2-SW-L
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327009
UST-2-B
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327010
UST-2-SW-R
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327011
UST-2-SW-B
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327012
UST-2-SW-F
EPA 5035A/5030B
678538
EPA 8260D
678757
92588327001
UST-1
SW-846
678506
92588327002
UST-3
SW-846
678506
92588327003
UST-1-B
SW-846
678506
92588327004
UST-1-SW-F
SW-846
678506
92588327005
UST-1-SW-B
SW-846
678506
92588327006
UST-1-SW-R
SW-846
678506
92588327007
UST-1-SW-L
SW-846
678506
92588327008
UST-2-SW-L
SW-846
678506
92588327009
UST-2-B
SW-846
678506
92588327010
UST-2-SW-R
SW-846
678506
92588327011
UST-2-SW-B
SW-846
678506
92588327012
UST-2-SW-F
SW-846
678506
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 02/22/2022 01:26
PM
without the written consent of Pace Analytical Services, LLC.
Page 68 of 104
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Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CCW-006
Pace Project No.: 92588327
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2022 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 104
Document Name: Dor=ument Revised: November 15, 2021
Sample Condition Upon Recef t (SCUR) Page 1 of I
ArraWal n Document No.: Issuing Authority:
F-CAR-CS-033-ftev.09 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville Eden[] Greenwood ❑ Hurttersvllle � Raleigh[] Mechanicsville[] Atlanta[] Iternersville❑
Up nn Client Name: WO : 92/588327
Receipti.. i, � f f Project ri:
t� � [ -q i �— 1 `-i 7" "') + ff II I
Courier: Fed Ex ❑UPS LJLJ5P5 OClient
❑ Commercial ❑Pace ❑Other: II 1 I j
92588:327
Custody Seel Present? Oyes ❑No Seals Intact? Des ❑N+
Date/Initlak Person Examining Contents: 13 j
Packing Material: ❑Bubble Wrap El -Bubble Bags []None ❑ Other Biological Tissue Fryten?
Thermometer: ❑Yes []No -N/A
EIJA Gun lD: Z� �� bl ❑VM1 et ❑Blue ❑Kane
— - Type of Ice:
Correction Factor:
Cooler Temp: Add/Subtract (°C) Temp should be above Freezing to G°C
—Coal erTemp#orrected-('£-}❑Samples out of temp criteria. Samples ors ice, Cooling process
.
as
USDA Regulated Sail ([] N/A, water sample]
Old samples originate in a quarantine zone within the United States: CA, NY, or SC (check mapsl7 aid samples Originate from a Foreign source {Interns ' naliy,
El Yes 0116, including Hawaii and Puerto Rico)? ❑Yes ON-
[nm men tSl DI sere ua n cv:
Chain of Custody Present?
❑Yes
EIND
ONJA
1.
Samples Arrived within Hold Time?
Yes
[]Na
N/A
2.
Short Hold lime Analysis (1472 hr. 7
Yes
EI!
N/A
3.
R us h Turn Aro u n d Time Requested?
Yes
Env
]N/A
4.
Sufficient Volume?
OVe-S
No
N/A
S.
Correct Containers Used?
Ors
❑N❑
[]N/A
5
-Pate Containers Used?
Dfes
EINO
❑NIA
Containers Intact?
E yes
rNo
N/A
7.
Dissolved analysis: Sa mp Ias Vield Piitered7
Yrs
Mo
117A
8.
5ampie LabelsMatchCCC?
Dyes
❑No
[]N/A
9.
r
Andudesnate/Time/ID/Analysis Matrix:
Heads pace in VOA Vials >5.6mmj7
El Yes
No
OH/A
10.
Trip Blank Present?
❑Yes
❑Ne-
❑N/A
11.
%p Blank Custody Seals Present?
❑Yes
[]No
Gi'WrA
COMMENTS/SAMPLE t]ISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Datefrime:
Project Manager SCURF Review: pate:
Project Manager 5RF Review:
Oate:
Field Date Required? [-]Yes ❑No
Page 70 of 104
Document Name:
0 Sample Condition Upon Recall
alylrca� . Document No--
F-CAR-CS•033•Rev-08
*Check mark top half of box If pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Caliform, TOC, Oil and Grease, OR018015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
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Oocument Revised: November 15, 2021
Page 2 of 2
Issuing Authority:
Pace Carolinas quality Office
Project#E WO# ■ 92'58V327
Phi: KRG Due Date: 02/22/22
CLIEH7: 92—Hart Hick
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pH Adjustment Log for Preserved Samples
Sample ID
Type of P►eservativa
w upon raeeip!
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 4
-- - - - --- ---- - - - •-r-..-r -• .n ..,•.•.. _, — —, —IL, —, o cur, -- 11— wnu wui uv dent to ine r4ortn Larouna OENNR CerElflCatfon office {I.e.
Out of hold, intorrect preservatve, out of temp, incorrect containers.
Page 71 of 104
ti
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Page 72 of 104
Page 72 of 104
ton -test°
A Pace Analyb'cale LaboWxy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
February 22, 2022
Kevin Godwin
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: NC
Client Job Number:
Project Number: 92588327
Laboratory Work Order Number: 22B 1040
Enclosed are results of analyses for samples as received by the laboratory on February 17, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Raymond J. McCarthy
Project Manager
EZURIMMEMINVI
1ffiW=.WrA[11- 91
Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
22B 1040-01
22B 1040-02
22B 1040-03
22B 1040-04
22B 1040-05
22B 1040-06
22B 1040-07
22B 1040-08
22B 1040-09
22B 1040-10
Sample Preparation Information
QC Data
Petroleum Hydrocarbons Analyses - EPH
B301417
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
7
9
11
13
15
17
19
21
23
25
26
26
26
28
29
30
srrsiszr.�
Table of Contents
con -testa
A Pace Analyb'cale LaboWxy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100 REPORT DATE: 2/22/2022
Huntersville, NC 28078 PURCHASE ORDER NUMBER:
ATTN: Kevin Godwin
PROJECT NUMBER: 92588327
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 22B1040
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
UST-1-13
22B 1040-01
Soil
MADEP EPH rev 2.1
SM 2540G
UST-I-SW-F
22B1040-02
Soil
MADEP EPH rev 2.1
SM 2540G
UST-I-SW-B
22B1040-03
Soil
MADEP EPH rev 2.1
SM 2540G
UST-I-SW-R
22B1040-04
Soil
MADEP EPH rev 2.1
SM 2540G
UST-I-SW-L
22B1040-05
Soil
MADEP EPH rev 2.1
SM 2540G
UST-2-SW-L
22B 1040-06
Soil
MADEP EPH rev 2.1
SM 2540G
UST-2-13
22B 1040-07
Soil
MADEP EPH rev 2.1
SM 2540G
UST-2-SW-R
22B1040-08
Soil
MADEP EPH rev 2.1
SM 2540G
UST-2-SW-B
22B 1040-09
Soil
MADEP EPH rev 2.1
SM 2540G
UST-2-SW-F
22B1040-10
Soil
MADEP EPH rev 2.1
SM 2540G
Page 3 of 32
ton -test°
A Pace Analyb'cale LaboWxy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA EPH, only hydrocarbon ranges were requested and reported.
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
ST.TSL^L{�rs'r
■ • •
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-1-B
Sampled: 2/14/2022 15:25
Samule ID: 22131040-01
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
15 15 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:21
TYH
C 19-C36 Aliphatics
ND
15 15 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:21
TYH
Unadjusted Cl 1-C22 Aromatics
ND
15 15 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:21
TYH
C 11-C22 Aromatics
ND
15 15 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:21
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
55.7 40-140
2/18/22 17:21
o-Terphenyl (OTP)
54.8 40-140
2/18/22 17:21
2-Bromonaphthalene
99.6 40-140
2/18/22 17:21
2-Fluorobiphenyl
97.6 40-140
2/18/22 17:21
Page 5 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-1-B Sampled: 2/14/2022 15:25
Sample ID: 22131040-01
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 68.6 % Wt 1
SM 2540G 2/21/22 2/22/22 11:49 AVF
Page 6 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-F
Sampled: 2/14/2022 15:15
Samule ID: 22B1040-02
Samule Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:40
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:40
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:40
TYH
C 11-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:40
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
49.1 40-140
2/18/22 17:40
o-Terphenyl(OTP)
52.6 40-140
2/18/22 17:40
2-Bromonaphthalene
103 40-140
2/18/22 17:40
2-Fluorobiphenyl
101 40-140
2/18/22 17:40
Page 7 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-F Sampled: 2/14/2022 15:15
Sample ID: 22B1040-02
Samule Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 70.9 % Wt 1
SM 2540G 2/21/22 2/22/22 11:49 AVF
Page 8 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-B
Sampled: 2/14/2022 15:35
Samule ID: 22B1040-03
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:59
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:59
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:59
TYH
C 11-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 17:59
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
55.9 40-140
2/18/22 17:59
o-Terphenyl(OTP)
56.3 40-140
2/18/22 17:59
2-Bromonaphthalene
103 40-140
2/18/22 17:59
2-Fluorobiphenyl
100 40-140
2/18/22 17:59
Page 9 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-B Sampled: 2/14/2022 15:35
Sample ID: 22B1040-03
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.1 % Wt 1
SM 2540G 2/21/22 2/22/22 11:49 AVF
srrs_rrnzr•�
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-R
Sampled: 2/14/2022 15:40
Samule ID: 22B1040-04
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:19
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:19
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:19
TYH
C 11-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:19
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
52.0 40-140
2/18/22 18:19
o-Terphenyl(OTP)
49.8 40-140
2/18/22 18:19
2-Bromonaphthalene
101 40-140
2/18/22 18:19
2-Fluorobiphenyl
99.4 40-140
2/18/22 18:19
Page 11 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-R Sampled: 2/14/2022 15:40
Sample ID: 22B1040-04
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 71.0 % Wt 1
SM 2540G 2/21/22 2/22/22 11:49 AVF
srrs_irizr•�
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-L
Sampled: 2/14/2022 15:50
Samule ID: 22B1040-05
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:38
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:38
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:38
TYH
C11-C22Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:38
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
59.1 40-140
2/18/22 18:38
o-Terphenyl(OTP)
59.8 40-140
2/18/22 18:38
2-Bromonaphthalene
91.9 40-140
2/18/22 18:38
2-Fluorobiphenyl
86.5 40-140
2/18/22 18:38
ST.TSSL'�S�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-I-SW-L Sampled: 2/14/2022 15:50
Sample ID: 22B1040-05
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 71.2 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.TSSt:ES�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-L
Sampled: 2/14/2022 16:00
Samule ID: 22B1040-06
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:57
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:57
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:57
TYH
C 11-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 18:57
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
55.6 40-140
2/18/22 18:57
o-Terphenyl(OTP)
68.4 40-140
2/18/22 18:57
2-Bromonaphthalene
110 40-140
2/18/22 18:57
2-Fluorobiphenyl
107 40-140
2/18/22 18:57
ST.TSSi�S�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-L Sampled: 2/14/2022 16:00
Sample ID: 22BI040-06
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.8 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.TS:i:�S�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-B
Sampled: 2/14/2022 16:20
Samule ID: 22131040-07
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
35
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:16
TYH
C 19-C36 Aliphatics
23
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:16
TYH
Unadjusted Cl 1-C22 Aromatics
19
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:16
TYH
C 11-C22 Aromatics
19
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:16
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
58.3 40-140
2/18/22 19:16
o-Terphenyl(OTP)
64.3 40-140
2/18/22 19:16
2-Bromonaphthalene
103 40-140
2/18/22 19:16
2-Fluorobiphenyl
101 40-140
2/18/22 19:16
Page 17 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-B Sampled: 2/14/2022 16:20
Sample ID: 22131040-07
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.1 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.TS!T•ES�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-R
Sampled: 2/14/2022 16:10
Samule ID: 22BI040-08
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
31
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:36
TYH
C 19-C36 Aliphatics
14
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:36
TYH
Unadjusted Cl 1-C22 Aromatics
20
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:36
TYH
C 11-C22 Aromatics
19
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:36
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
57.3 40-140
2/18/22 19:36
o-Terphenyl(OTP)
60.2 40-140
2/18/22 19:36
2-Bromonaphthalene
102 40-140
2/18/22 19:36
2-Fluorobiphenyl
101 40-140
2/18/22 19:36
Page 19 of 32
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-R Sampled: 2/14/2022 16:10
Sample ID: 22BI040-08
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 77.7 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.TS!TIl.S�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-B
Sampled: 2/14/2022 16:30
Samule ID: 22BI040-09
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:55
TYH
C 19-C36 Aliphatics
ND
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:55
TYH
Unadjusted Cl 1-C22 Aromatics
ND
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:55
TYH
C 11-C22 Aromatics
ND
13 13 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 19:55
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
52.9 40-140
2/18/22 19:55
o-Terphenyl(OTP)
63.5 40-140
2/18/22 19:55
2-Bromonaphthalene
101 40-140
2/18/22 19:55
2-Fluorobiphenyl
96.0 40-140
2/18/22 19:55
ST.TS!Y>rS�if�7
•
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-B Sampled: 2/14/2022 16:30
Sample ID: 22BI040-09
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 75.9 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.T- NIM ifN
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC
Sample Description:
Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-F
Sampled: 2/14/2022 16:40
Samule ID: 22131040-10
Sample Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date
Date/Time
Analyte
Results
RL DL Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
C9-C 18 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 20:14
TYH
C 19-C36 Aliphatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 20:14
TYH
Unadjusted Cl 1-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 20:14
TYH
C 11-C22 Aromatics
ND
14 14 mg/Kg dry 1
MADEP EPH rev 2.1
2/17/22
2/18/22 20:14
TYH
Surrogates
% Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)
45.6 40-140
2/18/22 20:14
o-Terphenyl(OTP)
60.0 40-140
2/18/22 20:14
2-Bromonaphthalene
102 40-140
2/18/22 20:14
2-Fluorobiphenyl
99.6 40-140
2/18/22 20:14
ST.TS!L'�S�if•7
Table of Contents
con -testa
A Pace Analyb'cO LaboWoiy
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Project Location: NC Sample Description: Work Order: 22B 1040
Date Received: 2/17/2022
Field Sample #: UST-2-SW-F Sampled: 2/14/2022 16:40
Sample ID: 22131040-10
Sample Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.2 % Wt 1
SM 2540G 2/21/22 2/22/22 11:50 AVF
ST.TS!T:ES�if•7
Table of Contents
con -testa
A Pace Analyb'cale LaboWory
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
Sample Extraction Data
Prep Method: SW-846 3546
Analytical Method: MADEP EPH rev 2.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
22B1040-01 [UST-1-B]
B301417
20.0
2.00
02/17/22
22B1040-02 [UST-I-SW-F]
B301417
20.0
2.00
02/17/22
22B1040-03 [UST-1-SW-B]
B301417
20.0
2.00
02/17/22
22B1040-04 [UST-I-SW-R]
B301417
20.0
2.00
02/17/22
22B1040-05 [UST-I-SW-L]
B301417
20.0
2.00
02/17/22
22131040-06 [UST-2-SW-L]
B301417
20.0
2.00
02/17/22
22131040-07 [UST-2-13]
B301417
20.0
2.00
02/17/22
22B1040-08 [UST-2-SW-R]
B301417
20.0
2.00
02/17/22
22B1040-09 [UST-2-SW-B]
B301417
20.0
2.00
02/17/22
22B1040-10 [UST-2-SW-F]
B301417
20.0
2.00
02/17/22
Prep Method: % Solids
Analytical Method: SM 2540G
Lab Number [Field ID]
Batch
Date
22B1040-01 [UST-1-B]
B301658
02/21/22
22B1040-02 [UST-I-SW-F]
B301658
02/21/22
22B1040-03 [UST-I-SW-B]
B301658
02/21/22
22131040-04 [UST-I-SW-R]
B301658
02/21/22
22B1040-05 [UST-I-SW-L]
B301658
02/21/22
22131040-06 [UST-2-SW-L]
B301658
02/21/22
22131040-07 [UST-2-13]
B301658
02/21/22
22131040-08 [UST-2-SW-R]
B301658
02/21/22
22B1040-09 [UST-2-SW-B]
B301658
02/21/22
22B1040-10 [UST-2-SW-F]
B301658
02/21/22
EST.TS!fm10111N7
N g L7,W49A•
ton -test°
A Pace Analyb'cale LaboWxy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
lnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B301417 - SW-846 3546
Blank (B301417-BLK1) Prepared: 02/17/22 Analyzed: 02/18/22
C9-C 18 Aliphatics
ND
10
mg/Kg wet
C 19-C36 Aliphatics
ND
10
mg/Kg wet
Unadjusted Cl I -C22 Aromatics
ND
10
mg/Kg wet
C l l-C22 Aromatics
ND
10
mg/Kg wet
Acenaphthene
ND
0.10
mg/Kg wet
Acenaphthylene
ND
0.10
mg/Kg wet
Anthracene
ND
0.10
mg/Kg wet
Benzo(a)anthracene
ND
0.10
mg/Kg wet
Benzo(a)pyrene
ND
0.10
mg/Kg wet
Benzo(b)fluoranthene
ND
0.10
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.10
mg/Kg wet
Benzo(k)fluoranthene
ND
0.10
mg/Kg wet
Chrysene
ND
0.10
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.10
mg/Kg wet
Fluoranthene
ND
0.10
mg/Kg wet
Fluorene
ND
0.10
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.10
mg/Kg wet
2-Methylnaphthalene
ND
0.10
mg/Kg wet
Naphthalene
ND
0.10
mg/Kg wet
Phenanthrene
ND
0.10
mg/Kg wet
Pyrene
ND
0.10
mg/Kg wet
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
Surrogate: Chlorooctadecane (COD)
2.53 mg/Kg wet
5.00 50.6 40-140
Surrogate: o-Terphenyl (OTP)
2.96 mg/Kg wet
5.00 59.3 40-140
Surrogate:2-Bromonaphthalene
4.74 mg/Kg wet
5.00 94.8 40-140
Surrogate:2-Fluorobiphenyl
4.61 mg/Kg wet
5.00 92.3 40-140
LCS (B301417-BS1)
Prepared: 02/17/22 Analyzed: 02/18/22
C9-C18Aliphatics
20.1
10
mg/Kg wet
30.0
66.9
40-140
C 19-06 Aliphatics;
29.4
10
mg/Kg wet
40.0
73.5
40-140
Unadjusted C11-C22 Aromatics
37.4
10
mg/Kg wet
85.0
67.5
40-140
Acenaphthene
2.98
0.10
mg/Kg wet
5.00
59.5
40-140
Acenaphthylene
2.79
0.10
mg/Kg wet
5.00
55.8
40-140
Anthracene
3.12
0.10
mg/Kg wet
5.00
62.4
40-140
Benzo(a)anthracene
3.36
0.10
mg/Kg wet
5.00
67.3
40-140
Benzo(a)pyrene
3.20
0.10
mg/Kg wet
5.00
64.0
40-140
Benzo(b)fluoranthene
3.36
0.10
mg/Kg wet
5.00
71.3
40-140
Benzo(g,h,i)perylene
2.91
0.10
mg/Kg wet
5.00
58.2
40-140
Benzo(k)fluoranthene
2.71
0.10
mg/Kg wet
5.00
54.3
40-140
Chrysene
3.25
0.10
mg/Kg wet
5.00
65.0
40-140
Dibenz(a,h)anthracene
3.17
0.10
mg/Kg wet
5.00
63.3
40-140
Fluoranthene
3.18
0.10
mg/Kg wet
5.00
63.7
40-140
Fluorene
3.03
0.10
mg/Kg wet
5.00
60.5
40-140
Indeno(1,2,3-cd)pyrene
2.97
0.10
mg/Kg wet
5.00
59.4
40-140
2-Methylnaphthalene
2.79
0.10
mg/Kg wet
5.00
55.9
40-140
Naphthalene
2.63
0.10
mg/Kg wet
5.00
52.5
40-140
Phenanthrene
3.16
0.10
mg/Kg wet
5.00
63.2
40-140
Pyrene
3.24
0.10
mg/Kg wet
5.00
64.8
40-140
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD) 2.96 mg/Kg wet 5.00 59.2 40-140
Rage
Page 26 of 32
ton -test°
A Pace Analyb'cale LaboWxy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B301417 - SW-846 3546
LCS (B301417-BS1) Prepared: 02/17/22 Analyzed: 02/18/22
Surrogate: o-Terphenyl (OTP) 3.13 mg/Kg wet 5.00 62.5 40-140
Surrogate:2-Bromonaphthalene 4.60 mg/Kg wet 5.00 92.1 40-140
Surrogate:2-Fluorobiphenyl 4.60 mg/Kg wet 5.00 91.9 40-140
LCS Dup (B301417-BSD1) Prepared: 02/17/22 Analyzed: 02/18/22
C9-C18Aliphatics
17.9
10
mg/Kg wet
30.0
59.7
40-140
11.4
25
C19-C36Aliphatics
30.3
10
mg/Kgwet
40.0
75.7
40-140
2.99
25
Unadjusted C11-C22 Aromatics
55.7
10
mg/Kg wet
85.0
65.5
40-140
3.09
25
Acenaphthene
2.74
0.10
mg/Kg wet
5.00
54.7
40-140
8.33
25
Acenaphthylene
2.54
0.10
mg/Kgwet
5.00
50.8
40-140
9.30
25
Anthracene
2.98
0.10
mg/Kg wet
5.00
59.5
40-140
4.64
25
Benzo(a)anthracene
3.35
0.10
mg/Kg wet
5.00
67.1
40-140
0.319
25
Benzo(a)pyrene
3.17
0.10
mg/Kgwet
5.00
63.3
40-140
1.08
25
Benzo(b)fluoranthene
3.67
0.10
mg/Kg wet
5.00
73.4
40-140
2.88
25
Benzo(g,h,i)perylene
2.84
0.10
mg/Kg wet
5.00
56.9
40-140
2.23
25
Benzo(k)fluoranthene
2.69
0.10
mg/Kg wet
5.00
53.8
40-140
0.941
25
Chrysene
3.21
0.10
mg/Kg wet
5.00
64.3
40-140
1.08
25
Dibenz(a,h)anthracene
3.09
0.10
mg/Kg wet
5.00
61.8
40-140
2.38
25
Fluoranthene
3.16
0.10
mg/Kgwet
5.00
63.2
40-140
0.754
25
Fluorene
2.77
0.10
mg/Kg wet
5.00
55.4
40-140
8.90
25
Indeno(1,2,3-cd)pyrene
2.95
0.10
mg/Kg wet
5.00
58.9
40-140
0.825
25
2-Methylnaphthalene
2.45
0.10
mg/Kg wet
5.00
49.1
40-140
12.9
25
Naphthalene
2.29
0.10
mg/Kg wet
5.00
45.7
40-140
13.8
25
Phenanthrene
3.02
0.10
mg/Kg wet
5.00
60.5
40-140
4.31
25
Pyrene
3.23
0.10
mg/Kgwet
5.00
64.6
40-140
0.319
25
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD)
2.99 mg/Kg wet 5.00 59.8 40-140
Surrogate: o-Terphenyl (OTP)
3.02 mg/Kg wet 5.00 60.4 40-140
Surrogate:2-Bromonaphthalene
4.89 mg/Kg wet 5.00 97.7 40-140
Surrogate:2-Fluorobiphenyl
4.80 mg/Kg wet 5.00 96.1 40-140
ST.T- 01M ifM
ton -test°
A Pace Analyb'cale LaboWoiy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
j
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
ST.TSi f •7•ES t ti f •7
con -testa
A Pace Analyb'caie LaboWoiy
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX 413/525-6405 "TEL. 413/525-2332
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
MADEPEPHrev 2.1 in Soil
C9-C18 Aliphatics
C 19-C36 Aliphatics
Unadjusted Cl 1-C22 Aromatics
Cl 1-C22 Aromatics
MADEP EPH rev 2.1 in Water
CT,NC,ME,NH-P
CT,NC,ME,NH-P
CT,NC,ME,NH-P
CT,NC,ME,NH-P
C9-C18 Aliphatics
CT,NC,ME,NH-P
C 19-C36 Aliphatics
CT,NC,ME,NH-P
Unadjusted Cl 1-C22
Aromatics CT,NC,ME,NH-P
Cl 1-C22 Aromatics
CT,NC,ME,NH-P
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2024
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2023
RI
Rhode Island Department of Health
LA000373
12/30/2022
NC
North Carolina Div. of Water Quality
652
12/31/2022
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2022
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2022
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2022
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Table of Contents
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Table of Contents
l Have Not Confirmed Sample Container
Numbers With Lab Staff Before Retinquishing ARtALYT1 A� LIrBORAT�i tY
Over Samples
.
Login Sample Receipt Checklist - [Rejedion Criteria Listing - Using Acceptance Policy] Any False
Statement will be brought to the attention of the Client - State True or False
Client q
Received By112 Date
How were the samples
received?
Time
In Cooler - r- No Cooler On Ice r No Ice
Direct from Sampling
Ambient
Melted Ice
Were samples within By Gun # 3 Actual Temp .
Temperature? 2-6°C i By Blank # Actual Teme -
as Custody Seal Intact? A4 Were Samples Tampered with?
Was CQC Relinquished ? -T— Does Chain Agree With Samples? �—
Are there brokenneaking/loose caps on any samples?
Is CDC in ink/ Legible? j Were samples received within holding time? .l
Did COC inciude all Client 1 Analysis T _ Sampler Name
pertinent Information? Project »�- ID`s i Collection Dates/Times -F-
A
re Sample labels filled out and legible? ,_ ""---
Are there Lab to Filters? r �'
Are there Rushes? �-
Are there Short Holds? --JE-�
Is there enough Volume? i
Is there Headspace wh x ?.
Proper MediatContainer T
Were trip blanks received?
Do all samples have the proper pH?
Who was notified?
Who was notified?_
Who was notified?
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Page 32 of 32
Beverly, Trudy
From: Nathan O'Leary <noleary@harthickman.com>
Sent: Tuesday, March 8, 2022 1:20 PM
To: Beverly, Trudy
Subject: RE: [External] Heating Oil UST IAA
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
That sounds great, thanks Trudy!
Nathan
Nathan O'Leary, Project Manager
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 •Charlotte, NC 28203
Direct: 704-887-4607 • Mobile: 515-239-7197
www.harthickman.com 10
From: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Sent: Tuesday, March 8, 2022 1:16 PM
To: Nathan O'Leary <noleary@harthickman.com>
Subject: RE: [External] Heating Oil UST IAA
Hey Nathan,
I'll do my best to get to it soon. It may be next week before I can review the report.
Trudy
Trudy Beverly, L.G.
D�EQ Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
n"���t., � UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everly_kncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: h_ptt s:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://dea.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc.gov/ncdeg/Waste%2OManatiement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policv.pdf
https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Nathan O'Leary [mailto:noleary@harthickman.co
Sent: Tuesday, March 8, 2022 12:01 PM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: [External] Heating Oil UST IAA
Importance: High
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Good Morning Trudy,
Attached, please find the Initial Abatement Action report prepared in relation to three heating oil USTs removed from
the property located at 729 East 361h Street and 3315 North McDowell Street in Charlotte, North Carolina. Analytical
results of closure samples indicated the presence of TPH-GRO and TPH-DRO at concentrations above the action
levels. Confirmation samples collected following the removal of impacted soil did not indicate the presence of VOCs,
SVOCs, VPH, or EPA at concentrations above MSCCs. As such, H&H is requesting an unrestricted use No Further Action
(NFA) be issued.
Please note, this property is set to be transacted in mid to late March 2022. This UST removal work was completed by
the potential purchaser of the property to meet requirements of the lending institute. The lending institute is
requesting closure documentation from DEQ prior to closing of the property.
If you have any questions or would like additional information, please let me know.
Thanks,
Nathan
Nathan O'Leary, Project Manager
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 • Charlotte, NC 28203
Direct: 704-887-4607 • Mobile: 515-239-7197
www.harthickman.com I Im